# • Raymond Professional Group. Inc
.

. Engineer'S - Architects
.. Consultants. Builders

1001 16th Street· Moline, Illinois 61265 Tel: (309)157-9800· Fax: 1309)757-1.812 www.raymondgroup.com January 24,2001 Mr. AI Kriegel Cargill Oilseed Processrng 1110 12th Avenue S.W. P.O. Box 2817 Cedar Rapids, Iowa 52406 

### SUBJECT: PARTICULATE TES'"ING 

### ON EMISSION POINT DUST 

### COLLECTOR Dear Mr. Kriegel 

### #009 - 

### ELEVATOR 

# • In accordance with The Raymond Professional Group, tnc. contract dated December 6, 2000, Raymond is pleased to supply the results of particulate emission tests performed on January 10. 2001. Emission tests were conducted on Emission Point #009, the Elevator Dust Collector, for Particulate Emissions
. We appreciate the opportunity 

### to have been of service to you on this project and hope to assist you on your future engineering and environmental projects. Respectfully,

### ~; ::;SIONAL GROUP, INCORPORATED

# q~O!land Prol" Manager

# &v,~?r($' David 

### M. Bloss Environmental Manager tam cc: File #518319 

# •

Formerly Doyen and Associtl!f!s, Incorporated; Raymond·BeUng, incarpomted; Raymond Management SeTTilCIBS, Inccrpomted; Raymond-NOBB, InC<>1pOmkld; and Raymond-Williams Limited i

# • Raymond Professional Group, Incorporated Report No. 518319


### I. INTRODUCTION In accordance with The Raymond Professional Group, Inc. (Raymond) Contract dated December 6, 2000, emissions tests were conducted on Emission Point 

### #009 , The Elevator Dust Collector for Particulate Emissions. Tests were performed on January 10,2001 by Tim Moriand and Jeff Ogden. The tests were coordinated with Mr. AI Kriegel of Cargill Corporation. Mr. Anthony Daugherty of the Linn County Health Department was on site for the testing. The tests were conducted and data evaluated in accordance with 

### U,S. Environmental Protection Agency (EPA) Methods 1-5, as listed in 40 CFR 60, Appendix A, and the Iowa Air Compliance Manual. 

### DISCLAIMER The results from this stack test reflect the emission conditions at the time the tests 

# • were conducted. Compfiance with conditions listed fn the source permit are determined by the regulatory agency responsible for enforcement of that permit.



# • 1. 

### Raymond Professional Group, lncorgorated Report No. 518319



## , , 

# • ! i


## II. SUMMARY OF RESULTS The following Table presents a summary of the emission testing performed 

### by Raymond at Cargill Corporation located in Cedar Rapids, Iowa. See Appendices for data utilized a nd developed as part of the tests.
.


### Particulate Emission Tests Emission Point #009 Elevator Dust Collector

Cedar Rapids, Iowa

January 

### 10,2001 

# • Test Number Particulate Emissions 

### gr/dscf Ib/hr 

### 1 0.0053 1.40 

### 2 0.0045 1.19 3 0.0038 1.01 Average 0.0045 1.20 Stack Gas Average Velocity: Stack Gas Average Flow Rate: Stack Gas Average Temperature: Stack Gas Average Moisture: gr/dscf :::: grains per dry standard cubic foot ACFM 

## =: Actual Cubic Feet per Minute 64.073 ftlsec 30,294 ACFM 39.2° F 

### 1.1%

; , . 

### 2

# • Raymond Professional Group, Incorporated Report No. 518319



## IILTEST METHODS
Emission Point 

### #009, The Elevator Dust Collector, was tested for particulate emissions. The emissions were tested using EPA Methods 1-5, and the Iowa Compliance Sampling Manual Procedures. EPA METHODS 14 EPA Method 

### 1, "Sample and Ve!ocityTraverses for Stationary Sources", as revised August 14. 1986, is used to determine the quantity and location of velocity traverse points. The method el,ccounts for flow disturbances, both upstream and downstream of the sampling points. EPA Method 2. "Determination of Stack Gas Velocity and Volumetric Flow Rate (type 

### S Pitot Tube}", is used to determine the flue gas velocity and flow rate. An S-type pitot tube is connected to an inclined manometer 

### (O.OO-1.00 inches of water incline 

# • . range and 

### 1.0 to 10,0 

### inches water vertical range) to measure velocity pressures in the flue. Temperatures are measured with a type 

### K thermocouple attached to a calibrated digital temperature indicator. EPA Method 

### 3, "Gas Analysis for 

### CO 2 • 

### O2 , 

### Excess Air, and Dry Molecular 

### O 2 

### Weight", uses an integrated gas sample collected during the test period for determination of gas composition by orsat analyzer. The orsat analyzer is used to determine the percent carbon dioxide and oxygen, which is subtracted from 100% 

### to determine the percent nitrogen. EPA Method 

### 4, "Determination of Moisture Content in Stack Gases", 

### is accomplished 

# by weighing the impingers before and after tests. The weight gain is used to calculate the moistUre content of the flue gas. .

-.

- :!**~** 

### EPA METHOD 5
EPA Method 5 is the "Determination of Particulate Emissions from Stationary Sources", EPA Reference Methods 1 through 4 are used to determine the sampling paints, flue gas velocity, gas composition and moisture content. Based on these preliminary measurements, a sampling nozzle of appropriate diameter is selected to maintain isokinetic sampling
. 

# • 3

# • Raymond Professional Group. Incorporated Report No. 

### 518319

The stack gas 

### is drawn through a calibrated stainless steel nozzle into a heated,**glass~lined** probe and through a heated filter assembly held at 250 ;!; 25 0 F. The gas

, then passes through an ice-cooled impinger train. The moisture in the flue gas is

condensed as it passes through the ice-cooled impingertrain, which is maintained at 

### a temperature of 

### 68°F or less 

### as it leaves the last impinger. The first, third and fourth impingers are modified by replacing the high velocity tip with 

### a one-half inch inside diameter glass tube. The second impinger 

### is of the standard GreenburgSmith design. The gas then flows through a leak!ess vacuum pump, 

## a dry gas meter and 

### a calibrated orifice. The dry gas meter and orifice are calibrated before and after each sampling event. The sampling rate 

### is adjusted during the sampling period to maintain isokinetic conditions. At isoklnetic conditions, the velocity of the stack gas entering the nozzle should be equal 

### to the stack gas velocity at the sampling point. These condrtions are maintained by adjusting the pressure drop across the orifice meter relative to the stack gas velocity pressure. The proper orifice differential is determined by , calculation. 

# • Priorto each test run, the test trains are leak checked 

### at fifteen inches 

### of vacuum. At the conclusion of each test. the system is leak checked at the highest vacuum drawn during the sampling period. Allowable leakage rate under EPA Reference Methods 

### is 0.02 cubic feet per minute.
. After each test, the particulate samples are carefully recovered. The filter is removed from the holder with tweezers, placed in a petri-dish and sealed 

### with tape. The nozzle, probe assembly and front half of the filter holder are rinsed with acetone. A probe brush is used to remove particles which adhere to the walls of the nozzle, probe and filter assemblies. The washing is collected in sample containers and transported to the laboratory for analysis. The acetone washing of the front half ofthe particulate sampling train (nozzle, probe assembly and front half of the filter holder) 

### is quantitatively transferred to a desiccated tared 250-milliliter beaker. The volume of acetone 

### is recorded and evaporated to dryness. The beaker with sample 

### is desiccated and weighed to a constant weight, to the nearest O.1-milligram. 

## For purposes of definition. the term "constant weight" means 

## a deviation of no more than ±O.5 milligrams between consecutive weighings,' conducted at intervals of not less than six hours apart. 

# • 4

# • Raymond Professional Group, Incorporated Report No. 518319



# • , 

### A blank sample is obtained from each lot of acetone used during the test program. The blanks are processed and analyzed in the same manner as a particulate sample. Filters from the particulate test runs are removed from their sample containers and placed in a desiccator for a 24 hour period prior to weighing to a constant weight. The impinger contents are recovered 

### by pouring the original 

### 01 water and any moisture collected in the first three impingers into a graduated cylinder. The total volume is measured and recorded. The water is then transferred to a glass or plastic bottle. The liquid portion of the impinger train is then rinsed, at Jeast twice, with DI water and the contents are added to the irnpinger catch. A blank sample of rinse DI water Is set aside in a separate container for use as a blank sample. In the lab, the impinger contents are analyzed for organic and inorganic condensable matter as follows: the impinger contents are transferred to a separatory funnel and· first extracted with three 25 milliliter portions of ethyl ether and three 25 milliliter portions of chloroform. The two extractions are combined in a tared 250 mL beaker and evaporated to dryness. The remaining water fraction is placed in its own 250 mL tared beaker and also evaporated to dryness. Following evaporation, both sets of beakers are placed in a desiccator for a 24 hour period then weighed to the nearest 

### 0.1 mg. The water fraction represents the inorganic condensable material and the ethyl ether/chloroform fraction represents the organic condensable material



# • 5IMPINGER TRAIN OPTIONAL, MAY BE REPLACED -;. .BY AN EQUIVALENT CONDENSER 

# o .**~T~::::NSOR** . .
THERMOMETER
. 

# .' 'j." HEATH] AREA

. THERMOMETER 

# : 0 CHECK VALVE

VACUUM.



### LINE'
. \

. TEMPERATURE SENSOR PITOT TUBE



### . I REVERSE·TYPE

PI TOT TUBE 

### t,
. 

# 11 'STACK 

### U-WAll fl.L 

### J' •FIL TEA HOLDER

. --;- ­ - - - - - - - -1 1 .....---1'--. I I



# I PITOT MANOMETER

MAIN VALVE
DRY GAS METER AIR·TlG HT PUMP Partlcula.le.s.amPllni. traln. 

# -J:-::

. , _f.**~_** -- -- -­ . ,

# .•..

_

# .~ 

# ••••••

.....

### SAMPLE POINT' SCHEMATIC

PI

# 'InrG(~\'l} o')SE'PC 

## f

# p(cr:(sSJ~ 

# P}&;I7INo. Stdck

### Oidme~eq Upstredm 

### DIsturbance 

# 5.3'2. D.II.p. }.; } 

## V.O I ltJ • 

### Stack 

### Diameters

## Oownstred~ 01

## stu~bance 

# -1':**<~2** Source 

# .e ItUCt/u! 

# du,:r (!o}J#Clor

# ~. of Sdmple Ports 

# ? ­ St.dck Oi dmeter 

## ""3 

# 8 II No • 

### of

## S~mp 1 

# e Po i 

### n

## ts_---I<?~'/_· 

# __

; 

### . SAMPLE POINTS i 

### <AT EACH PORT 

### FROM .§ tOENAL!. POINT**"::ES~ANCE** NO. . ( i tlches') 

## J. 

# ,,0 ?->t:J" 1. 

### i)'YB '3 

## , • ., .> 'i 

# t ';(**').~** 

## (q I' 

# e. ) j. 

### Y'7 7 

# " ?1.).Y'7 

# t t**~ ?~.g>**  

# 0 0;

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### 3>S'1 )/

### '3~Y7"" 

### )t 

### 37.'1'" 

# -;to.}"

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# 1 •

,

)i 

# • ,



# •

• PARTICULATE RESULTS Company CARGILL OILSEED PROCESSING City CEDAR RAPIDS, IOWA Source ELEVATOR DUST COLLECTOR Test Team TIM MORLAND 

### & JEFF OGDEN Test Date WEDNESDAY 1-10-01 Parameter 1 2 3 

### averageunits**=-==~~=========;;~================================;===~===~~===~~~** 

### P bar )0.08 30.02 30.06 30.05 in Hg 

### SqRt(delta P) 1.147 

### 1.162 1.164 1.158 

### in water 

### T stack 500.2 499.7 497.6 499.2 

### deg R 

### Cp 0.84 0.84 0.84: 0.84 

### no units l? 

### static -11.00 -11. 00 -11.00 

### -11.00 in water A· 

### stack 7.88 7.88 7.88 7.88 

### aq ft C02 0.0 0.0 0.0 

### 0.0 percent 02 20.8 20.8 20.8 20.8 

### percent CO 0.0 0.0 

### 0.0 0.0 percent 

### N2 79.2 79.2 79.2 79.2 

### percent 

### M dry 28.832 28.832 28.832 28.832 

### Ib/lb*mole M 

### stack 28.698 28.713 28.113 28.708 

### Ib/lb*mole B ws 0.012 0.011 0.011 0.011 

### mole fract V 

### imp 5 2 3 

### 3 

### ml V 89 7.21 9.06 8.17 8.15 

### gm 

### V meter 4S .112 46.153 46.644 45.970 

### cubic ft y 1.0083 1. 0083 1.00B3 1.00B3 

### no units Delta H 1. 678 1.720 1. 725 

### 1.708 in 

### water T 

### meter 526.4 527.8 531.6 528.6 deg R L 

### post 0.016 0.002 0.003 

### 0.007 cfm Theda 60.0 60.0 

### 60.0 60.0 min Particulate wt. 0.0163 0.0140 0.0119 0.0141 gm 

### Blank -0.0004 -0.0004 -0.0004 -0.0004 

### gm D 

### nozzle 0.188 0.188 0.188 0.188 inches 

### Results 1 

### :2 3 

### averageunits**==========================~~=====~======~====~==========~~=~======** 

### P 

### stack 29.271 29.211 29.251 29.245 

### in P 

### meter 30.203 30.146 30.187 30.179 in Hg V water 0.579 0.524 

### 0.529 0.544 

### cubic ft 

### V meter (std cond) 46.221 47.073 47.297 46.864 

### cubic ft V stack 63.530 64.378 64.309 64.073 

### ft/sec Q 

### stack 30751 31172 31313 31079 

### dscfm Isokinetic rate 102.404 102.884 102.908 102.732 

### percent C 

### part 0.0053 0.0045 

### 0.0038 0.0045 gr/dscf C' 

### part 1.3991 1.1911 

### 1.0069 1.1990 

### Ib/hr

# •

• SAMPLE CALCULATION

- TEST NO.**-()~**

J' 

### , 

### PInt 

# C C. Purpose 

### Co Supliag T.ocaHOI**-z.-:.!r:'L.:..!.L:-:!........,~.!!:.-L.l.....----';.,...:...--f:-;.~-~~"'-'::::.:..,;,.:.::....,J!;.......::-** Piut calditiou**..p...~!.:....!..=::...-** _________**~--:;r** _____ D&te**~~** _ fest Procedm**~~(£l......t.J....IC..,,~u..:..._.L-_--** __ 

## _**'1~/"-.~** 

## ___ nate {. ) 7·01


### Necessary Data:



### B1n Vm ..6.H 

## 1,6. P 

### Tm Ts Ps 

### Pb A s 

## Au y 

### C

p 

### Collection Interval, 

# ----'=b'---u__ mi,n Water Colleeted, ) 

# 2. Z I gm 

### Particulates Collected 1 

### Meter Volullle, 

## 'Lj" S.)J 

## 7.. Avera.ge Meter 

### Pressure, ). ( 

### 7 

# S in H 2 0 A";'erage 

# r- Velocity 

### Pressure, ). ) 

### L}7 j in H 20 Average Meter Temperature, 

# Ct. ,/ of 

### + 460 

## =**S~{.** 1/ oR Average Stack Temperature,

### ~t1. 

## L of 

### + 460 ;:;: 

## §vo. L oR Stack Absolute Pressure,

## ?0~ '/'71 in Hg Barometric Pressure, in Hg 

# 3£. () '6 Stack Area, 

# 7.**8~** ft2 Probe 

### Nozzle 'Area, ).

## CZ))(J~-¥ ft2 Dry Gas Meter Calibration Factor, 

# ).00 6..J Pitot Tube Coefficient, 

# D·8'/ stack Gas Composition: % CO 2

## _-..:::D~ __ % 02 

# :;20' If X,CO r %N2 

# Q9 .'?

# ., SAMPLE CALCULATION

- TEST NO.

- 

### c:J/L< lobBo. 

# C; J '6)} 

# '7

Moisture Content of Stack Gas, Bws 

# • 'i



# , 1. 

### Hater Collected in Impingers, 

## sCF VWlstd:: 

### 0.0414 ft 3 

### /gm 

### (L7. 7 ( gm) V td:: 

### g. 

## 5: 7C,SCF 

### w,s , 2. 

### Moisture Content of 

### Stack Gas, BW8 

### Vw,std Bws :: Vw,std + 

### Vm,std B:: 

### fJ.!3r:7 SCF

ws

### "~CF 

### +1-)J4u DSCF :;;**O.o)~** 

### Bws 

## c. Molecular Weight of 

### Stack Gas,**Ib/lb~mole** 

### 1. Dry Molecular Weight, Md M'd ::: 

# I>xBx Md ::**O.44(~%** 

### CO 2 ) 

### +**O.32~%** 

### 0Z} +**O.28(~%** 

### CO) 

### +**O.28~$~%** 

### N 2 ) Md ::: 

# dB. S}Llb/lb-mole 

# • 2. 

### Wet Molecular Weight, Ms Ms ::: M d (l-B ws ) 

### + 18(B ws ) M 

# Q!6.S>1. (l..oQ}'t ) 

### +**l8(O.~J1** )

s Ms 

### =d8.b'7g'lb/lb-mole B.

### SAMPLE CALCULATION

- TEST NO.

-**~~**



# - UdC7(

# ~0)?1/5 J'd/l, S/(s3/7 Job 10. Plnl 

### U. Average stack. Gas 

### Velocity, Vs Vg = 

# KpCpj Ts 

# J b,P 

### PsMs Vg 

### = 85.45 fps :I:

## D.8~1 

# * / 

# Se>6.1. oR ;. 

# * J.) 't2J in H 2 0

### V~in 

### Hg***;I~b/lb-mole** V s 

# = 

# b

>. ):>i> IpS

;

. ; 

### E. Average Stack Gas 

### Volumetric Flow Rate, Q s Q 

### ; (3600 

### sec/hr) VSAg(l-Bws)f!stdl

## rp~l

s 

# LpstdJ [TJ
. Q 

### ; (3600

## secihr){b3.~ofPs)(7.~**ft2)(1~'OIL)[** S30 0 

### R 

# J

s 29.92 in fig 

# • Q 

# =**h~'Jb)Cl(** 'DSCFH s . 

# 30) 7?15**D~C** 

# FIh F. Pollutant Mass Rate, PMR PMR;**~** 

# _ .......... - * Vm,std PMR 

### ;0.015'0;. gm 

# Yl11 J 

### DSCF Q g 

### 454 gm/lb

*bgYI)D{JUSCFH 

### 454gm/lb PMR ::: 

## ).3'7a 1-) 

### Ib/hr G. Pollutant Concentration, C std 

# =**~** 

# * 15.43 grains/gm C

std 

### Vm,std C ""O.oJS"c, gm :I: 15.43 grains/gm

std 

### l/6.t1 I 

### DSCF

### ::::O.ov~J grains/DSCF C



### stdSAMPLE CALCULATION - TEST NO. 

# -VV'-t 

# • Cc, 

# I;:; ; I / 0 .1 

# SUe ( 

# fr"'?'55 1 " 

# 7 

# J)e;", I

# I.b~. 5 / 

# '6 J J<; l1"t 

### H. Isokinetic Variation, %1 %1 

# = lOOTgVm;stdPstd (60 

### sec/Min)eVpsAnPsTstd(l-Bws) XI 

### =

### nOO){5ao·t.~){Y6.77'DSCFi(29.92 

### !n Hg) (60 sec/min) 

## (b D 

### min) Q.5Y-'fps)

### (l."1lXlc~9 

### ft2)**(~1.n** Hg)

### (~3QoR)**(1...P,~~** %I 

## ::)01.2 Y..:%
I • Comments 

### a.nd Remarks; 

# •

•

# •• S2mpling 211d 

## Velocity Iraversa Point Determination' '. 

## EPA Method 1

II**mer~ :r:~n**  .a**~(\d** t**Ci~r.;lit4fl** .r:: it**~;:';! Iji~**  .. Ij 12**~** 

# '-t. U.$. a or 9**~t1!.;~**
NC. OF paRiS US2::J 

# -----r.,.----­

_ __ L " PCF\i INSIDE**OIA~I=TE::;** 2 

### if l " 

# --yrr

I I NO. OF PORTS AVAll. • .l,SI.E

S;·::.JI'IAL£NT OIAl.IEi'!.=\: (1 S 't OE ,,-;"''"..: T W'II:";":':

*
....**~... O~~~7M'"**  't'11Cfn

) ,**I~** LS.7**~().~ J=.~**  

### , 

# I 6.;**~.'** 

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# - : :**~.,~** t,LJ Hl.,i 1**~ !~::** **:,.~** !'1.-\.**t,.~** s.;" l •. $ t**~** • , 

### , ;:i • .': ';" 'I**~** ..**~=.~** il
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### ..... '" :7.3 :::.: .1 :.! • A • 17. !**r~.:l** to.3 0IS;':'N<:a 

# I OISiANC::;' 

### I**t=-~CM** INSiG5 F;;\CJ..A**~Lri"~iOEI** ·rYAl,.!.. C:= rOn ':"=

Ctl' nat**~t:1~~** ;lo;n[=I c!e: I't U)**!~iiCX 'W'1U~** **~.O** in
.. lOf**~C3-e:X** <li<L ,.,,1 in. o.,s itt. lot $(::"':X (:\:3.K 11 Co <1--\**1('1~** ;.'l ;n

Figure 6-1.

i'

### PART1CULATE 

### FIELD DATA Page One Page 

### OF,',,_--.,..r;_ 

# C0D2j,'O 

# O,I9.PrJ

# ?rtJCPSS)~'

... 

## O'jJ.r-L nt Run No.

• ; urea Filter No. 

# 1151 Co)) 

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# O. IRS
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. Day/Date Test Started Ended 

# 00; tD

# \1JeJOt~Jt,,'1 

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### 2 V

. 

## t/ 

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# .• ......-----------:----= ----1



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## J1 cQ). J 

## '? "Hq After 

### (/.v I 

# t @ 

# I 

# s Pitot Tube Leak Test Before Before '. , 

## V After 

# V K Factor 

### PARTICULATE FIELD DATA

<. 

### :;; 

### ., ..". "..--+ Q Gas Sample Temp. at: ...... =.**~** <II "' 0­**"'~** 

## ., cr .,..!2. dry gas meter

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# a; ') t No:t::':;le Diameter - in. 

# O. 

# J 

# 38 Ambient Temp. 

### Min./ point
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# •

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## 00'1 b Ended,) 

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# J (c) J 

### 0 "Ho 

### After 

# 0 I 

### (J/) 

## z.. @. / 

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## '2 ")

GaS Sam pill Temp. 3t" dry ga!> meter .". -I = . 

## .,­ 

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### _____ __ _ PARTICUu\TE FJELD DATA Page One



### : nt 

# Cc,m! 

# i 1 

# 0, }CUc{ 

# 2(**"U>5}~j** •

# rc~ 

# 11>51 CoLJec/vL Nozzle Diameter - in. Ambient Temp.

# RC.£IJ5~ ;Ed Test Crew

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### +'-'UI..4--"----,.-------­ 

## j [lay 

### I Date '" • 

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. , Pb in Hg :; 

### tl , 

## 0 SCHEMArrC OF**ST~C"OSS** SECTION) 

### .1 Pitot Cp 

## 0 . ce., 

## t,.}
-, Meter

## ~ H@--

.. -i=-) -.

## '~8-S-t-/------- . Y ractor } 

### .00 

### <6) 

# O.:JQ};Ur

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# ---r---ll
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_____

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## _G..,...;7..,...;'1-5->

_______



## .**t-;.-~-;-'-~~-·~:-~--~-·.~--------Im-p-i"-m-e~-.-.Q-IU-m-5-m-I)~-·~-·----.--.---------~I--·-,·-.---··-·_-_-~~~** 

# • I .j 

# o**H~ijal.i-.~** 

## .. " ;: 

### ....... -:-. 

## ....._­ . I"

### S~.lf~Ge~W~i~=-

### r

# I


# •

### PARTICULA TE' 

### FIELD DATA Page Two 

### ' Pan' Run No. 

# 0(:, II 

## C7. 

# is-f' J 

# p[ vCRS

# ~In , ,- Page



### • ree 

# lli2i CoDe(:jV1 

# =_ Filter 

# I:f­ r1 

## ----D
, Test Craw 

## +;t-'I**~** ij Ambient Temp. 

# 3 () , : Day I Date 

# \.tv t 

# J.
. 0 , Test Started 

## .lIJr-::1..,:;---]Ir-'--f;-n**d-e-d--"l!=~;j-7**

! Meter leak Rate CFM: 8efore 

# a**~(J;)t** " kHq

## Af~ ,O/)::J @ 

# b "Hg**~--~~~~~~**

Pitot Tube Leak Test Before 

### K Factor' 

## j _2. "/ After



# ----­

Gas Sample Temp. 

### :Jr' dry gas mete!'"

### B(lIUG LABORATORltS lABORATORV IlArA 

# L ? Sheet: 0 f ..;> Anal Y7.e-d -by-:

### -~l~)-h-.-h---::**()-r7r9-n----:(~--=** Date: 

# 1 - J 7.. - 0 

## J Tare Weight final lJeigbt Weight Gain 'i Iter No. (m9,) (1\19) (1119 ) 

# <!IT

- 

# ;...,---­

'ro6e 

### &front Half Wash:&**ImQinq~r** 'Nater ! Back 

# . r:::;-S r I 

# -;"0**Extractio~v** 1 \later

### SOl!l~,~



# .0) 

# E9 (organic)V
.**(inDrganic~** (inal Wt.:: 

# Of7 L/1Sl 'is I1Ig. iindWt.=

### Jo~(;3).JI mg_ linalwt.=

### )~) 

## 0't.7 mg. J Tz Wt.= 

## :17,1-/226 Ing. hre Itt.::: /0 0 , o?",?"7 mg. rare 'ilt. 

## = 

# 1 'dfObt. C:> CJlg. .it • . , Gain ::: ;; 

# G2. 1. mg. !It. Gain =


## __ .. ___J;....._/
_ mg. 'ilt. Gain :: 

## D'2 mg.

### ~c !one Blank: (100 mIL) '.ia 

## ce r Blank: (tOO mIl) Slank Correction**Calc~lations:·** - , samo a salllp e

### i"in~l Wt.::

### C~ 

### l/;)2.**~~.** mg. tina! 'J\:.::: 

# r;**~** 

## 3.7'). 

## v mg. Acetone :: Uml x 

### O. 

# Y 1119/100ml:::

## O.~ mg. 

# ro.,,. G ) 

# lL ')7. IL mg. Tare 'ilt.:::; 

# G3 '3 ") s\.::> mg. 'liater 

## = 

# 'i (J 0 ml x 

### 0 mg/100ml:: 

### 0 mg. ;.t. 'Gain 

## = CJ· 

# "L mg.**I~t.** Gain :: 

### O. i) m9. Corrections for Blanks: (). 

# 'i mg{­**~ ~l**  Particulate: M:!isture: 'i 1 ter .... __ • . • • . • • •• • •• • • • • • • .. • • • . •.

__ 

## L
.... I.:..

•

# ...,7'---- mg. Si lica Gel Fr

### !t~f!alf Wash
....................... ___ C1..;..;.... 

## "l.::.-_:......... mg. ';/eight**Aft~r.** g. 

# 307, 

# z ! Ex 'action (organic) •• , ............... __ ....... ____ mg. ''''eight Be fore, g. 

### 3c;o·c,)U ',4ablr Solubles (inorganic)
............ __

### .,-0....,·,...7..:.-
__ mg. Weight Collechd, g. 

# 7.1 I tin :rrected Particulate fotal •••••••• - 

### _--.-JJ.{,....,,;:,,_. 

## ::!;3-.-
__ ITtg. Volume Collected, mI. 

# /YL:!t Correction for Blanks
................. 

### _--==(£7-'_"...:.,/",,)_·
__ 1119· Impinger

### ~E iParticulate Total 

# 1 5· <=) mg. Volume After, m!. i • • • • • • • • • • • • • • • ••**--"--"~--** Volume Before, mI. Volume Collected, ml. Total Volume 1'oisture .4f Int-Kalf includes sampling train components up to and lllcludillg tile filter. I Back-Half is from tbe filter, up to and including the third impinger • 

# • ml

.........

# _---­

### 8£lIHG LABORATORIES LABORATORY DA TA She!!t: of 

# -2. '3**---------I~~----A·~ -7~--~-------**  Analyzed by: 

### -J.} h-, C(t.? 

# r 'inc ( Oat;:

### -)-_f-I-r)-=(~"**-o.:....;J~~~--** Tare Weight tinal lila i qht**'~eight** Gain (mq) (1119) (o1IQ) 

# G ;;}6. 

# iJ G5).1.

Total HI ter Gain:' 

# ==== =L::J.::,**;:~====** (rug) ImoinQer water ! Extractions' (organic)(f:; l.") Final

# Wt.~~**S¢~ ~**  Tare Wt.::

### '7~;) 5'00, 

### D 

### wt. Gain :; (J. 

# '1l' Sack 

# 51>'" I

. :**:l~e** a1 (100 0111) Blank**CiJrr~etion (;:lc~lations!**  Ie ank: 1 - . sarno .8 Acetone ;; 

### 9 c.) ml x (,). 

# Y mq/100ml:;: 

### 6:.31' mg. 'I/atel" 

## }/d Q IIIl;c (;) mg/100mi '" <:::> mq.

### ~inal 'oit. 

## = (;} (/,;;--2)S 

# :3.," G .). '/ '}? 

# ? it. n::: 

### 0,"') Corrections for Slanks: 

### O. '/ mq/ io il**Puticul~te:** ,l.\Ji sture: 

## :' "'-':**~.:..:..:;.;;...;::".,::,.** 

## VI. V ,"l
... t.ar .......... "" ..................... .., ....................... __......",.1..-.:::°;.,.....
__ iug. Sili.,C:l Gel ;rnn;t-H;alf '!lash •••••••••••••••••••••••

___ 1i..>.<.......

__ 

# "l_'-. _l1Ig. weight Af;!r, g. :x

### .~.cti()n (organic)
....... ...... ..... 

# o. '6: mg. 'i/eight Before, g. -lat",r Solubles (inorganic:)
............ __ 

### .O,,:--_'_£)
__ lIIq. Weight**Col!.ect~d!** g. 

## 0.0", 

## } L.J. 0 :.111 trected Particl1late Total
.........**_......,...,~_-.-** __ II1!1. Volume Coll:ectad, mI • Carrection fol" Blanks 

# . . . .. ""
........**_~~: _b,,:-'~~**  

# },--- mg • Imoinqer '1e1Particdate Total ••••••••••••••••• 

### _.....L.)....:3:..-.--..;:.'
____ IDg. VQIume Aft!r, 1111. Ilohme Be fore, mI. Volume Collected, ml. 

# ? di) Total Volume MJisture Collected 

# l f, () b ml

or**~t-HlIli** includes sampling train components liP to and including the filtar.**8o~~-Half** is from the filter, up to and including the third impinger_

t 

# •fare 'lieight fillal '"eight ';/eiQht Gain 7il tar No. (ma) (mq) • (mq)



# _ V33

Total fIlter G ain: 

# =====&='='=== (mg) Imoioaer Water 

### &**aac~** ,**~: Yash~**  £:x:tnctiaru: 

# S"Vl I (organic)

## m~) final Ioit. ;; -,.r...';""':;.J-"';-"';""':---IL.. mq. final

# '~t.**~J"** 

# 20. , 1119. tinal 'ilL '"

# _":-;{...~~~::.:....,-....:m9. r;, \ , Wt. :; Tare 

### ''''to '" 

# L?Zl{;J9.t mg. Tare 'tit.;:

____ .;...-__ mg. lit. Gain :; ) • V IIIg • '>It. Sa! n ::. 'i/atH Stqnk: (100 mil) Blank Cor.actioq CJlctllations: pmp e rLnal 'lit.:; 

### Co**~32** 

## SiD mg. Acetone :; ) I;-'''''>::Il x 0. 

# Y !1lg/10Qml :: O. ',,/ mg. Tm ''';t.::. 

# G;**')?~.;>** mg. 'liatar ;; 

## Ve.4:..> ;111 x () mg/100ml:: 0 1119. lilt. Gain :: 

### O·r) mg. Corrections for 8lanks: 

## O· 

# 'I ;ng/ ,"tlishr'! :

..... i :i.
..**~:er** ... "" ............................................... __
+---=-

___**...!.O!..~** ___ mq. Silica ridl Fr"?t-Hal f 'i/ash
............. , ..........**_~~:......:=----.:...._** mg .. 'Me i gil t**.~ftar,** g.

# 3v~'L 

# 2 '3c,V.<: /u .:;**~ac;tioll** (organic)
.................. __ mg. Weight SerJra, g. ,**'1Iat~r** Solubles (inQrganic)
............ _---,,;...,:-...1...-

___ 

### mg. ',o/eight Coil'!ctad 1 g.

## ~')7 ; Ur. /rrected Particulat; fotal
......... _-s....q..,,---L.....-+-- I1Ig. Volume Collected, ml.

## ~ i:QrreGtioo for Blanks

.. o9' ........ -- ...................... -......-,,..-'-r-':::"""......-- mg • Im oinoar mg • :if .;**?articulat~** rocal

.. ...... .. .... " "
.. ,. ............ ---:-=--'--- Volume Mter, 

### mL 

# 2 u >uv 'j lJolume**8efor~** , ml. 

# 'd O;.J. <:..D )..tl V Vo lume Co Uected, atl**~** Tatal Volume Mii sture 1111 -I ;nt-Half includes sampling train cOlllponents up to and including the fil hr.**L~~k-fia1f** is from the filter, up to**~nd** including the third impinger •



# •

### METER CONSOLE CALIBRATION


## •

# NamtS)}hJl10Ik,n~l D:m' 

# Lj_;;-.U 0

## C(m~)k Illl, Or\" vi.LS

## m~:t~'r tlO, 

# 7 Dr\'

## \J':.l~ 111l'{l'r rOl'rt'niol1 I':u:mr 

### , ,.., (q.,. "> ;/5S"" ' ;'., -­ WI'\ (\':'it tnt'l\"r Illl,]

## 7'£l5~/o8 

## .**C()I'I·p~·tinn** f"Jrtor 

# yw -::-0 

## .C7CJ ;;; 

# f5
. B:11'tlllWtril'

## [In':-~un'. I'hJOJ.:2 

## G ill. I I,\{

## fH'I'\'i!lll~**~'~dibl'aliIlH** ;lI\d tlaLl' 

## C·) t· 

## '7<::t



## .;

. 

# •**T\tmll~·r.HU** rt' Orifin·**(;a~** \ !llu m", (;a" \'(}\umt' w{'\ I')ry**J(J~** ml;'tl;'r manomcu.'1' w\:t**I~":II** II r: 

## "';I,,**~('Hin)(. m~'u.:r**  Jnl'H'r :'>11-11:1' inl,-, OUlh:\ AY<:1"J.gC Tim
... ..lit, \' 

### ,.... VII, 

### I,... 'di' ItllI' ld· II 'in, H:!() 

## r,:! (,:1 OF OF**.~** 

## or min '/**Calcu!ation~**

..lH .lH 13.0 

## .,. r ,".Pb"d _""'

## ~ 

# \' d(Pb +

## ~~:) 

# (I,.. +

## ~60) 

# ,}**~** .lHq;; O,0317.lH 

# [(I

....**~** -160)1;1 

# T Pb(ld -+- 460) 'Y w \/ I.... 

# 0.-:;**O.O~G8** I,OV)6 

### I,,?)D 1 ' () C).Ojj5 ), (7" 

## 53 J.C"7Sl/ 

# d. D 

## 3.0 '-1. .) 

## S',O O,j/}7L 0, 

### ;)")0(. 

# o. -:nlJJ**O·~7b'** 

## 1. 00 

### 0; 

### ).0 

## l3J

.(;}01 , Q 0 

## 7"/ 

## . '9<57**.,~** 

### d) 70St..j 

### ' 7130 

# • " '" Ratio nf .)'·I'Ur:H'y u( WI't**!t'~1** nWl\'r I" ,II'\' 1\.,.1 m('\<'r, '1'ul"I':1I1<:\' 

## = ± 0.01
. .lll@ ;: Orilin'**jln'~ur\'** dirr"n'm;:!1 that**~in'":o** U.7:", ,'fm uf <lir :.11 

## sa Of**~nd** !!9.92 indw:I of m!:'rI'IIfY, in, 1I:!1l. '!**11'·f.ll \~·\'**  .: ::: (1.1;i iltdlt'3,**Urifi~,·** ':'II@ ,1.1I1Il1'! Ldllu'lh',,\,U I.;"'!) :!..O!I indw
.... "" mudifit'Jtion m:ly bl' nt'c!:'ssary for somt'**.,.II11i'lill~ ~iIU.ltit,,~,.**  figure -4-:'3. Form for mo:ccr <;ocuolc c:::dibT:Jdon
i i!-- CALtBRATtOH DATA:



# . 

# p(t:
. -jP 

# 5}
.**PAA!~~pro€DI** • ·Mdbod... • &Ad. Ii (){**Ap~lx** /'0. 

## or**~** O"'R par( 00 .'" .met1ded**~~** {olkrw..: 

# fne/i?r I

t:By .• d<i1ns
.. a.;'"**&ct1Q~** 1:.:1..1 10 M'\lho.:! 4." {Ql!crw..:
. 

# • C**c,./I.brC;;I/~ )..I~'(.~do<sol~""'"** **~w<d** l:.. S(..,;£ ·C
.. ...;..··· .



### .... ; ,".. 

# .. ..,. 

# ) . Ja '- UJ I

# ~**·i.'&ft:~<:"""** ).(,,(/1«1.



## ..... 

# •

:**l,>~cf** Avg. F Tm- Outlet;.; 

### Avg. :i.vg. 'F
0.0319 Tm )**~**



### Pbar F



### 10

­ 

## V:n 

# • r

i

# '00)7

# ~ 

# R'7/ 

# • METEk 

### CONSOLE CAUBRATI0N

### /~, 

## / prCXI'55/1?..:J 

# )-)(0)"**01;J.m~'** 

## L.-C1cfj l 

## ll O·**~/' nal~'** 



# • T<:mp<:r,Uun' OriCk.: (;;a**\utum~- G~:.**  -:.)Ium,· 

### 'I'. l't 11**r.~- ).(~~**  tn..-t ... !' rn:lnomt'll:r w .... t**l~':il c!r~-** **~J~ ~~,tlin~.**  mltl<:r m ...**t~'l' :H~'It:I'** **~nll.'l** Outh·(**Av~r;j~":** Time

..HI. \' W' "'d' t w ' 'dl' tell)' It.!. II in. H
... l) 

### r,:.I f\;\ 

### "'r . "'f of 

## or min i .lH@ 

# - \ '/ :l;,

.0 8J's:¢**~~** 

## .... 

# ..... )

## ~~~~~**~,,7)** 

# lIe 7'6 

# 'co "7.3**16'·~b o~** 

### ).~"VI5 ).0**~1C~(** 

### e;: <$I"\**v.~~** 

# ....))**.~** 

# 77 Sit? 7L 

### IKe;**i~.S'1.7 PM~**  

# Ltt6 

### ? 

## 1.0 1

### ~'~.t:'>(5 'f.''') 

## ft;**$./:1~** 

## 11 

# 'in 76 

## ?>}. 

## C; 15. s'1:?**~."'$!** 

### ]'(,51<:>

...

A
...**<:r:l~1.' ~l''}~)**  

### j.,,'r$/ Calcul:lIiom

r 

# I .lH@ .lH 

# "w P b!ld +4(0) --.,. 0.0:1 I i..\H [(I w -jo -1(0)8 

# r

..HI l:l,o \'d(Pb;' ..l.H 

# )(tw +-160 '/,.,. Pb(ld + -toOl v 

# w'l"­ 1:l,S ..1. 

## \.0 

# I 0
.. (;> 

## 7, (" Ct**,ar;'7o~** 

## /. G'7¥J5' \.0­ U -t:J7!>(" 

## o .o,t:) /'2 

## ),({o 

## e.. 

## 1.0**V,(:;17).~** 0'**.0~<j.;,K** 

# 1-c cj i)

.., Radel 

### "r ..I,',ur:R}' (If wl't It'":>! mC'tt-!' til tlry tnt mI"'HT. '!'o!\'r:l1Il'l' "'" ± 0.02, ..lll@ = Orilkl' pn'"ur,· dirr,'n'tHial (h;l( gin-:. 

## o:m l'fm UI "ir at 68"F:md 29,92 illdws of m("r·
• <'\11';, ill,**lJ~n.** '\.,h-r.III"(­ .; ::: n. E',**it;dw~.** Orifi{,' ..11 f@ ,1:",/1,1 f.tli IWlh',-\'U**I,;l~l** . :!.I)!I il1d1,·,. ur !l'Io<lific;-;nilJn**m;:t~'** U(" nt'cC'ssary (O( sam,' 1> • .1111 plio.l:**~itu..l** t iOll." Figure 4<1. torm for meter console (;?iibr.Hlon

# •

! ;-; 

# •**-.l-l_~** }!.....::...6_
...

# o_)~_~**Tt:mp~'I";;lur\:' ()ri{it'~'** **(;~~** HILum\:' Ga!> ."Iuln,' 

## \\',-, ll..:y**)(:l~** m ... lcr tn:lI1Umt'lt'r wt't 11.'31**dl'~' ~J~** 

WII i 1'1)(.**m~'It:r** rn ..·tt:r .'oh·lt'r Inl
... ! Oudl:l**A~** ...**r::~t'** Timt'

.lli. 

# '"w· Yd' t .... Idi· 'du o Id­ /I in. H:?,1i f!:l ft:! <IF 

### "F 

## . .y .f' min i ..\H@ 

# J."**'~~** 

# B..,J "".S'.}?

... 

# V 77 

# 07. ·7 

# '6 $1:;­ .Clyj**O~!I** 

## J.

# '?~" II/I). I);**~.D .~)** 

### 14~,?J;'A~''''') 

## 77 .?i. I 

## !**~o** '()7**",·/~** 611'14-.**1·7?~L** 

## ?.f)

. 

# 7:f;**~r..>I»** 

# ilfJ;:Sj 

### f? ,.,.,) 

# 7; '77 '-67. (f7

. .; 

## '(,., 7 b ,'*:;1 

## t 711}S 1 

## I I 

# I I I '\\'1:1":1)1;"­ 

### p.<7'3J l / 

### J. ?cOo Calculation:;

-r 

# I j,H@ 

# I ---...

- O.Oj",H 

# [('w 

# .46"q'l ...iIi Vw?b(ld +-460) .lH Vd(Pb +­ ..iH 

# )(t w +-. Hi 

# 1 'jf;.'r- Pbltd +-1(0) V w 

# 0 1:3.5
• i 

# d. w (/.) 'J7J 0.0,0, 

## tJ? 

# 1.6?e" ?f) P.jl)7J 

### 0' .J>;t:7J**~-** 

# J, ?";} 

### fs'O 

# ?-t/ CP.} Lj7/ 0' 

### 0C?3J 

### } .?J 

## Y 

# s

-I**Ra~i"** 

## or ..1l'nJ.r:u--:, Dr Wt-t a-:.t Int't('r tcJ dry It.."**m~·U'r.** Toll-r:lI1C,' "" :!:. 0.02
. .l1l@
.. Orilit't' prt.."utt'**dirr"r~'!llial** th:1l**~i\'l""** 0.75 "fm ur ail" al 68"Fand 2:9.92. inclw:I or m{'r· I'\lry_ in, II:!(J. 'lolt'r;lIln- -= 

## = 0.1;i irldw-s.

­ Ul'i(in' ..ill@' _,I.lnuld r.tI! ]u'I\':n-1\ I.:,!) - :!.ll!l indln. or tmlllific:.tdun m:lr Ix- n<."('"ssuy ror scm ... >..It1lplilll-\ ,iIUJtillll.', Fig'uI'O: 4·.3. Form for mO:I<:r- como1.: c::dibntion

# ------------------------- 

# • Compliance Emission Test Operating Data
Owner: 

# C C; ; 

### 1) 

# C cJ( 

## t?=>

# r~;~~ oate:_1

# _-_l_o~ 

# .. _()_,_**saurce:f>'eV~** dVJ1 COJ&Cjp. Permit #: 

# L C**~)** 

# D 

# 1t 00 C)

Types and sduI'ces ( If any) of Fuels normally Burned Type of Fuel Burned During this test.

______________________ If Fuel Is used Approximate Quantities of each listed above burned AnnuaJly

________ Recyding Capability**Yes~_** No 

# X Recycling in Progress Yes
__ No 

# '"?f 

# eero!3§S cata Dyring Runs Maximum Continuous Process Rate (Manufacturer's Rating)

_____ ---l---!.-!---,..:-

____ Historical

# AVerag~ ProceSs

# Rate,~ ____ 

### ..I.-::d+_()_(.)_0

_ ..JL.::::.::.:.!....:...:::.....:::_4_:,.L---­ Historical Maximum Process Rate.

____**-+.,l.(.,~~~-_4..c:::.:::::.~L--J-** _____

Procass Rate

­ (gallhr, lblhr, tonslhr, etc ... ) rI'OCSS!!I Rate Wet Percent Moisture (%) ProcesS Rate Dry How PrrlCSSS Rate was Determined
PersOI1 Responsible for

### Data,~.4c..t::...J/_...I..l<~r~r....J.'**e....;ff--E..r?~I-** 

### ________ --

___

# S~w~**()f!~** 

# _ l1UeJPosWon

# -ii:tJ:c.i;j.,~ 

# • "'" Please 

### farJicats in the same 1J.CJ.;ts as \tour hisforicallnfQ/TWltl!;a

# ------------------------------------- AIR POLLUTION CONTROL EQUIPMENT OPERATING DATA· 

# • Actual Production**R-u-n-N-o-.p-y.-~~b-h-I~-~;-;** 

# 1 rC;vffJt(

# .....:.....-;;~"'-'r'-"-~~~=-rr~--..+- Locatiop 

# Cfo(c.r 

# }2 C?/ir/J..;:;r·//**+--~~~'---I"'-=Z..a,~~...:...:::.l!!..:~~** 

### Rated Production

____ ___

__**~~~~** 

### __**~~~~** 

### ___________ Mechanical Collector: Tube Dia. 

### in. No. of Tubes _. Design p

__

### in. 

### H 

### 2 0 @ 

### Gas Temp 

### _oF Observed 

### AP

___in 

### H 2 

### 0. Design 

### dm/tube @ 

### Observed 

### AP @ 

### of. Fan Rated 

### HP. Operating 

### Volts
. Operating 

### Amps**-~** 

### Electrostatic Precipitator: 

### Primary Primary
. Secondary Secondary Spark Field Voltage 

### Current Voltage 

### Current 

### Rate No. (volts) 

### (amps) (KV) 

### (rna) (per 

### min.)


# e. Scrubber: 

### Type**_~** 

### _______ -,._ .e.p (across scrubber)

_______ in. 

### H 2 

### 0. Fan Rated H.P. Operating 

### Volts Operating Amps

____ Liquid 

### Circulation Rate gal/min. 

### % Make-up

__**~.** 

### Blowdown

__............ gpm. Scrubbing 

### Water Change Interval

____________________ 

### Settling Tank Cleaning Interval

_____________________ 

### Baghouse: 

### Pressure- Positive



# ----- . Neg,ltive 

# X.
. No. Compartments 

# 16":5'"
. Type 

### Cleaning**I~**

### ~ 

### Clean Cycle min. If If • 

### 0 

### Avg. Baghouse**~p** 

### ..( 

## t:r in HP.AP Range 3..

- 

## 7 In. H";!
. 

### Fan: Rated H.P. 

### IlJd Operating 

### Volts 

## !-ur() Operating Amps

__**~_** 

### Cyclone: 

### Type
_____ .o.p

_____in. 

## Hp. Diameter

__________ Fan: 

### Rated H.P.

____ . Operating Volts

____ 

### Operating Amps

____ 

### Person Responsible for Data:

________________ 

# • Signature:

______ ....... _·-'
.. '";:--

__________ ___

'. 

### TitTeIPosition: 'Averages of operating dow taken <.luring utlu;)1 lcst run unless requestcd otherwise. 

### A-6