**Instructions for using the Emission Test Reporting Template for the Primary Aluminum Test Program**

This Information Collection Request (ICR) spreadsheet is intended to be used to report emissions data from primary aluminum reduction facilities as an alternative to the Electronic Reporting Tool (ERT), as well as in cases where the test methods arenot currently supported by the ERT.**Data for multiple process units should be reported by using separate copies of the appropriate tabs of this spreadsheet.** **Please Do Not delete rows or columns , addition of rows and columns is appropriate**  **as necessary. Emission Data Worksheets**  The emission data worksheets are provided for each test required for this testing program, although all facilities are not required to conduct all of the tests. On each worksheet,please enter process unit operating informationduring sampling and emission test results. The emission test results to be entered depends on the constituent. **Source Operating Information** 1. Please provide the Exhaust Flow Rate (acfm and dscfm) and the Exhaust Temperature (deg F). 2. Please provide the values of all requested parametersfor each of the sample testing periods in the appropriate cells. 3. Please provide any other supporting informationor commentsin the Other Supporting Informationfield.

# Primary Aluminum Testing: Filterable Particulate Matter

**Parent company**

**name:** Noranda Aluminum, Inc. **Facility address:** 391 St. Jude Industrial Park

New Madrid, MO 63869 **Description of source tested:** Past Plant Stack

**Test Method Used (e.g. Method 5)**  **Data Flag**

**(A DL, BDL, DLL)**  **Test Method Comments**

**Moisture (%) CO2 (%)**  **O2 (%) Flow (acfm)**  **Temperature (°F)**

**lb/hr lb/ton of** 

**throughput Ma** **terial Rate (ton/hr)**  1 0.664 0.105 Aluminum 6.30 2 0.930 0.148 Aluminum 6.30 3 0.552 0.088 Aluminum 6.30 **Run Number**  **Calculated Emission Rate Production or Throughput**  **Filterable Particulate Emission Test Results Concentration**  **(ug/dscm)**

**Exhaust Gas Other Supporting Information**  **Test End Date**  **Test End**

**Time**

**Flow (dscfm) Run**  **Number Run**  **Number Test Start** 

**Date Test Start** 

**Time**

## Primary Aluminum Testing: HAP Metals

**Parent company name:** Noranda Aluminum, Inc. **Facility address:**391 St. Jude Industrial Park New Madrid, MO 63869 

### Description of source:

**Pollutant Concentration**  **(ug/dscm) Test Method Used** 

**(e.g. Method 29) Data Flag** 

**(A DL, BDL, DLL)**  **Test Method Comments** 1 Antimony 2 Antimony 3 Antimony 1 Arsenic 2 Arsenic 3 Arsenic 1 Beryllium 2 Beryllium 3 Beryllium 1 Cadmium 2 Cadmium 3 Cadmium 1 Chromium 2 Chromium 3 Chromium 1 Cobalt 2 Cobalt 3 Cobalt 1 Lead 2 Lead 3 Lead 1 Manganese 2 Manganese 3 Manganese 1 Nickel 2 Nickel 3 Nickel 1 Selenium 2 Selenium 3 Selenium 1 Mercury 2 Mercury 3 Mercury **Run Number** **Test Start**

**Date Test Start** 

**Time Test End** 

**Date Test End** 

**Time Filterable Particulate Emission Test Results** 

## Primary Aluminum Testing: HAP Metals

**Parent company name:** Noranda Aluminum, Inc. **Facility address:** 391 St. Jude Industrial Park New Madrid, MO 63869 

### Description of source:

**lb/hr lb/ton of** 

**throughput Material**  **Rate (tons/hour)**  **Moisture**

**(%) CO** **2**

**(%) O** **2**

**(%) Flow** 

**(acfm) Flow** 

**(dscfm) Temp** 

**( °F)**  1 2 3 1 2 3 1 2 3 1 2 3 1 2 3 1 2 3 1 2 3 1 2 3 1 2 3 1 2 3 1 2 3 **Other Supporting Information Calculated Emission Rate**  **Production or Throughput Exhaust Gas**  **Run Number** 

# Primary Aluminum Testing: Hexavalent Chromium

**Parent company**

**name:** Noranda Aluminum, Inc. **Facility address:** 391 St. Jude Industrial Park

New Madrid, MO 63869 

### Description of source tested:

**Test Method Used (SW-846 M0061)**  **Data Flag**

**(A DL, BDL, DLL)**  **Test Method Comments** 1 2 3

**Moisture (%) CO2 (%)**  **O2 (%) Flow (acfm)**  **Temperature (°F)** 1 2 3

**lb/hr lb/ton of**  **throughput Ma** **terial Rate**  **(tons/hour)** 1 2 3 **Run Number**  **Calculated Emission Rate Production or Throughput**  **Run Number**  **Exhaust Gas Other Supporting Information**  **Flow (dscfm) Run**  **Number Test Start** 

**Date Test Start** 

**Time Test End** 

**Date Test End** 

**Time Hexavalent Chromium Emission Test Results** 

**Concentration (ug/dscm)** 

# Primary Aluminum Testing: PM and POM as MCEM **Parent company**

**name:** Noranda Aluminum, Inc. **Facility address:** 391 St. Jude Industrial Park

New Madrid, MO 63869 

### Description of source tested:

**Rate (tons/hour)** 1 2 3

**Moisture (%) CO2 (%)**  **O2 (%) Flow (acfm)**  **Temperature (°F)** 1 2 3

**lb/hr lb/ton of**  **throughput Pollutant**  **Conc (ug/dscm)**  **Test Method Used (e.g. Method 315)**  PM POM as MCEM PM POM as MCEM PM POM as MCEM 1
2
3 **Production or Throughput**

**Data Flag (A** **DL, BDL, DLL) Particulate Matter and POM as MCEM Emission Test Results**  **Test Method Comments Run**  **Number Run**  **Number Exhaust Gas** 

**Calculated Emission Rate Other Supporting Information**  **Flow (dscfm) Run**  **Number Test Start** 

**Date Test Start** 

**Time Test End** 

**Date Test End** 

**Time Ma** **terial**

### Page 1 of 8 

# Primary Aluminum Testing: Polycyclic Aromatic Hydrocarbons **Parent company**

**name:** Noranda Aluminum, Inc. **Facility address:**  391 St. Jude Industrial Park

New Madrid, MO 63869 **Description of source tested:** Paste Plant Stack

**lb/hr lb/ton**  **Throughput** 1 4/26/2013 12:21 4/26/2013 15:26 7.72E-02 2.29E-03 33.7 2 4/26/2013 15:53 4/26/2013 18:57 8.68E-02 2.58E-03 33.7 1 4/26/2013 12:21 4/26/2013 15:26 1.37E-04 4.06E-06 33.7 2 4/26/2013 15:53 4/26/2013 18:57 1.43E-04 4.24E-06 33.7 1 4/26/2013 12:21 4/26/2013 15:26 2.31E-03 6.86E-05 33.7 2 4/26/2013 15:53 4/26/2013 18:57 2.50E-03 7.41E-05 33.7 1 4/26/2013 12:21 4/26/2013 15:26 8.69E-06 2.58E-07 33.7 2 4/26/2013 15:53 4/26/2013 18:57 1.83E-05 5.44E-07 33.7 1 4/26/2013 12:21 4/26/2013 15:26 4.96E-07 1.47E-08 33.7 2 4/26/2013 15:53 4/26/2013 18:57 3.09E-06 9.16E-08 33.7 1 4/26/2013 12:21 4/26/2013 15:26 1.08E-06 3.20E-08 33.7 2 4/26/2013 15:53 4/26/2013 18:57 4.55E-06 1.35E-07 33.7 1 4/26/2013 12:21 4/26/2013 15:26 2.23E-06 6.63E-08 33.7 2 4/26/2013 15:53 4/26/2013 18:57 9.25E-06 2.74E-07 33.7 1 4/26/2013 12:21 4/26/2013 15:26 7.92E-08 2.35E-09 33.7 2 4/26/2013 15:53 4/26/2013 18:57 9.23E-07 2.74E-08 33.7 Acenaphthene (83-32-9) **Test Start Time**  **Test End**

**Date Test End** 

**Time Calculated Emission Rate**  **Throughput (ton/hr)**  **Compound Run**  **Number Test Start** 

**Date**

Anthracene (120-12-7) Benz[a]anthracene (56-55-3) Benzo[a]pyrene (50-32-8) Benzo(e)pyrene (192-97-2) Benzo[b]fluoranthene (205-99-2) Benzo[g,h,i]perylene (191-24-2) Acenaphthylene (208-96-8)

### Page 2 of 8

**lb/hr lb/ton** 

**Throughput Test Start**  **Time Test End** 

**Date Test End** 

**Time Calculated Emission Rate**  **Throughput (ton/hr)**  **Compound Run**  **Number Test Start** 

**Date** 1 4/26/2013 12:21 4/26/2013 15:26 6.95E-07 2.06E-08 33.7 2 4/26/2013 15:53 4/26/2013 18:57 2.85E-06 8.45E-08 33.7 1 4/26/2013 12:21 4/26/2013 15:26 9.29E-06 2.76E-07 33.7 2 4/26/2013 15:53 4/26/2013 18:57 2.12E-05 6.30E-07 33.7 1 4/26/2013 12:21 4/26/2013 15:26 1.26E-07 3.73E-09 33.7 2 4/26/2013 15:53 4/26/2013 18:57 3.45E-07 1.02E-08 33.7 1 4/26/2013 12:21 4/26/2013 15:26 2.22E-03 6.60E-05 33.7 2 4/26/2013 15:53 4/26/2013 18:57 2.18E-03 6.46E-05 33.7 1 4/26/2013 12:21 4/26/2013 15:26 1.09E-02 3.24E-04 33.7 2 4/26/2013 15:53 4/26/2013 18:57 1.01E-02 2.99E-04 33.7 1 4/26/2013 12:21 4/26/2013 15:26 7.29E-08 2.16E-09 33.7 2 4/26/2013 15:53 4/26/2013 18:57 9.72E-07 2.88E-08 33.7 1 4/26/2013 12:21 4/26/2013 15:26 5.65E-03 1.68E-04 33.7 2 4/26/2013 15:53 4/26/2013 18:57 5.28E-03 1.57E-04 33.7 1 4/26/2013 12:21 4/26/2013 15:26 2.13E-03 6.33E-05 33.7 2 4/26/2013 15:53 4/26/2013 18:57 2.19E-03 6.50E-05 33.7 1 4/26/2013 12:21 4/26/2013 15:26 3.04E-02 9.02E-04 33.7 2 4/26/2013 15:53 4/26/2013 18:57 3.21E-02 9.51E-04 33.7 1 4/26/2013 12:21 4/26/2013 15:26 9.55E-08 2.83E-09 33.7 2 4/26/2013 15:53 4/26/2013 18:57 6.12E-07 1.82E-08 33.7 1 4/26/2013 12:21 4/26/2013 15:26 1.23E-03 3.65E-05 33.7 2 4/26/2013 15:53 4/26/2013 18:57 1.12E-03 3.32E-05 33.7 Benzo[k]fluoranthene (207-08-9) Chrysene (218-01-9)

Naphthalene (91-20-3) 2-Methylnaphthalene (91-57-6) Phenanthrene (85-01-8) Perylene (198-55-0) Dibenz[a,h]anthracene (53-70-3) Fluoranthene (206-44-0) Fluorene (86-73-7) Indeno (1,2,3-cd) pyrene (193-39-5)

Pyrene (129-00-0)

### Page 3 of 8



# Primary Aluminum Testing: Polycyclic Aromatic Hydrocarbons
391 St. Jude Industrial Park**Parent company name:**  Noranda Aluminum, Inc. **Facility address:**  New Madrid, MO 63869 **Description of source tested:** Paste Plant Stack

**Me asured**  **Value (n g)**  **Wet or Dry**

**Basis Test Method** 

**(e.g.,CA RB 429)**  **Data Flag**

**(A DL, BDL, DLL)** **Front Half**

**Ma****ss* (ng)** **Back Half**

**Ma ss**  (ng)****Condensate**

**Ma ss** * (ng)** Aluminum 1 6.14E+06 Dry CARB 429 ADL Aluminum 2 6.85E+06 Dry CARB 429 ADL Aluminum 1 1.09E+04 Dry CARB 429 ADL Aluminum 2 1.13E+04 Dry CARB 429 ADL Aluminum 1 1.84E+05 Dry CARB 429 ADL Aluminum 2 1.97E+05 Dry CARB 429 ADL Aluminum 1 6.92E+02 Dry CARB 429 ADL Aluminum 2 1.45E+03 Dry CARB 429 ADL Aluminum 1 3.95E+01 Dry CARB 429 ADL Aluminum 2 2.44E+02 Dry CARB 429 ADL Aluminum 1 8.57E+01 Dry CARB 429 ADL Aluminum 2 3.59E+02 Dry CARB 429 ADL Aluminum 1 1.78E+02 Dry CARB 429 ADL Aluminum 2 7.30E+02 Dry CARB 429 ADL Aluminum 1 6.30E+00 Dry CARB 429 ADL Aluminum 2 7.28E+01 Dry CARB 429 ADL

**Compound Run** 

**Number Throughput**  **Ma terial** 

Benzo(e) pyrene

Acenaphthene Acenaphthylene
Anthracene Benz[a] anthracene Benzo[a] pyrene

Benzo[b] fluoranthene Benzo[g,h,i]peryle ne **Polycyclic A romatic Hydrocarbons Emission Test Results** 

### Page 4 of 8

**Me asured**  **Value (n g)**  **Wet or Dry**

**Basis Test Method** 

**(e.g.,CA RB 429)**  **Data Flag**

**(A DL, BDL, DLL)** **Front Half**

**Ma****ss* (ng)** **Back Half**

**Ma ss**  (ng)****Condensate**

**Ma ss** * (ng)** **Compound Run** 

**Number Throughput**  **Ma terial**  **Polycyclic A romatic Hydrocarbons Emission Test Results** 

Aluminum 1 5.53E+01 Dry CARB 429 ADL Aluminum 2 2.25E+02 Dry CARB 429 ADL Aluminum 1 7.39E+02 Dry CARB 429 ADL Aluminum 2 1.68E+03 Dry CARB 429 ADL Aluminum 1 1.00E+01 Dry CARB 429 ADL Aluminum 2 2.72E+01 Dry CARB 429 ADL Aluminum 1 1.77E+05 Dry CARB 429 ADL Aluminum 2 1.72E+05 Dry CARB 429 ADL Aluminum 1 8.69E+05 Dry CARB 429 ADL Aluminum 2 7.95E+05 Dry CARB 429 ADL Aluminum 1 5.80E+00 Dry CARB 429 ADL Aluminum 2 7.67E+01 Dry CARB 429 ADL Aluminum 1 4.49E+05 Dry CARB 429 ADL Aluminum 2 4.16E+05 Dry CARB 429 ADL Aluminum 1 1.70E+05 Dry CARB 429 ADL Aluminum 2 1.73E+05 Dry CARB 429 ADL Aluminum 1 2.42E+06 Dry CARB 429 ADL Aluminum 2 2.53E+06 Dry CARB 429 ADL Aluminum 1 7.60E+00 Dry CARB 429 ADL Aluminum 2 4.83E+01 Dry CARB 429 ADL Aluminum 1 9.79E+04 Dry CARB 429 ADL Aluminum 2 8.83E+04 Dry CARB 429 ADL

* Contains particulate filter, front half of filter holder and probe solvent rinses *** Contains condensate, impinger contents and glassware solvent rinses ** Contains XAD-2 resin tube, back half of filter holder and coil condenser solvent rinses Benzo[k] fluoranthene Chrysene

Phenan threne Perylene Dibenz[a,h] anthracene Fluoranthene
Fluorene Indeno (1,2,3-cd) pyrene

Pyrene Naphthalene 2-Methyl naphthalene

### Page 5 of 8 

# Primary Aluminum Testing: Polycyclic Aromatic Hydrocarbons
391 St. Jude Industrial Park **Parent company name:**  Noranda Aluminum, Inc. **Facility address:**  New Madrid, MO 63869 **Description of source tested:** Paste Plant Stack

**Total (ng) Test Method** 

**Comments Moisture**  **(%) CO** **2 (%)**  **O 2** **(%) Flow**  **(acfm) Flow** 

**(dscfm) Temperature** 

**( °F)**  6.14E+06 1 1.5 0.0 20.9 13,678 12,850 93.2 6.85E+06 2 1.4 0.1 20.8 13,308 12,501 93.3 1.09E+04 1 1.5 0.0 20.9 13,678 12,850 93.2 1.13E+04 2 1.4 0.1 20.8 13,308 12,501 93.3 1.84E+05 1 1.5 0.0 20.9 13,678 12,850 93.2 1.97E+05 2 1.4 0.1 20.8 13,308 12,501 93.3 6.92E+02 1 1.5 0.0 20.9 13,678 12,850 93.2 1.45E+03 2 1.4 0.1 20.8 13,308 12,501 93.3 3.95E+01 1 1.5 0.0 20.9 13,678 12,850 93.2 2.44E+02 2 1.4 0.1 20.8 13,308 12,501 93.3 8.57E+01 1 1.5 0.0 20.9 13,678 12,850 93.2 3.59E+02 2 1.4 0.1 20.8 13,308 12,501 93.3 1.78E+02 1 1.5 0.0 20.9 13,678 12,850 93.2 7.30E+02 2 1.4 0.1 20.8 13,308 12,501 93.3 6.30E+00 1 1.5 0.0 20.9 13,678 12,850 93.2 7.28E+01 2 1.4 0.1 20.8 13,308 12,501 93.3 Benzo(e)pyrene **Exhaust Gas Compound**  **Run**

**Number** Acenaphthene Acenaphthylene
Anthracene

Benzo[b] fluoranthene Benzo[g,h,i] perylene Benz[a] anthracene Benzo[a]pyrene

### Page 6 of 8

**Total (ng) Test Method** 

**Comments Moisture**  **(%) CO** **2 (%)**  **O 2** **(%) Flow**  **(acfm) Flow** 

**(dscfm) Temperature** 

**( °F)**  **Exhaust Gas Compound**  **Run**

**Number** 5.53E+01 1 1.5 0.0 20.9 13,678 12,850 93.2 2.25E+02 2 1.4 0.1 20.8 13,308 12,501 93.3 7.39E+02 1 1.5 0.0 20.9 13,678 12,850 93.2 1.68E+03 2 1.4 0.1 20.8 13,308 12,501 93.3 1.00E+01 1 1.5 0.0 20.9 13,678 12,850 93.2 2.72E+01 2 1.4 0.1 20.8 13,308 12,501 93.3 1.77E+05 1 1.5 0.0 20.9 13,678 12,850 93.2 1.72E+05 2 1.4 0.1 20.8 13,308 12,501 93.3 8.69E+05 1 1.5 0.0 20.9 13,678 12,850 93.2 7.95E+05 2 1.4 0.1 20.8 13,308 12,501 93.3 5.80E+00 1 1.5 0.0 20.9 13,678 12,850 93.2 7.67E+01 2 1.4 0.1 20.8 13,308 12,501 93.3 4.49E+05 1 1.5 0.0 20.9 13,678 12,850 93.2 4.16E+05 2 1.4 0.1 20.8 13,308 12,501 93.3 1.70E+05 1 1.5 0.0 20.9 13,678 12,850 93.2 1.73E+05 2 1.4 0.1 20.8 13,308 12,501 93.3 2.42E+06 1 1.5 0.0 20.9 13,678 12,850 93.2 2.53E+06 2 1.4 0.1 20.8 13,308 12,501 93.3 7.60E+00 1 1.5 0.0 20.9 13,678 12,850 93.2 4.83E+01 2 1.4 0.1 20.8 13,308 12,501 93.3 9.79E+04 1 1.5 0.0 20.9 13,678 12,850 93.2 8.83E+04 2 1.4 0.1 20.8 13,308 12,501 93.3 *** Contains condensate, impinger contents and glassware solvent rinses Benzo[k] fluoranthene Chrysene Dibenz[a,h] anthracene Fluoranthene

Pyrene Fluorene Indeno (1,2,3-cd) pyrene Naphthalene 2-Methyl naphthalene Phenanthrene Perylene

### Page 7 of 8



### 391 St. Jude Industrial Park New Madrid, MO 63869

**Other Supporting Information**

### Page 8 of 8

**Other Supporting Information**

### Page 1 of 8 

# Primary Aluminum Testing: Dioxins and Furans **Parent company**

**name:** Noranda Aluminum, Inc. **Facility address:**  391 St. Jude Industrial Park

New Madrid, MO 63869 **Description of source tested:** Paste Plant Stack

**lb/hr lb/ton**  **Throughput** 1 4/26/2013 12:21 4/26/2013 15:26 6.66E-13 1.98E-14 33.7 Aluminum 2 4/26/2013 15:53 4/26/2013 18:57 2.66E-13 7.90E-15 33.7 Aluminum 1 4/26/2013 12:21 4/26/2013 15:26 1.76E-13 5.22E-15 33.7 Aluminum 2 4/26/2013 15:53 4/26/2013 18:57 2.03E-13 6.02E-15 33.7 Aluminum 1 4/26/2013 12:21 4/26/2013 15:26 2.26E-13 6.71E-15 33.7 Aluminum 2 4/26/2013 15:53 4/26/2013 18:57 2.79E-13 8.27E-15 33.7 Aluminum 1 4/26/2013 12:21 4/26/2013 15:26 2.26E-12 6.71E-14 33.7 Aluminum 2 4/26/2013 15:53 4/26/2013 18:57 2.15E-12 6.39E-14 33.7 Aluminum 1 4/26/2013 12:21 4/26/2013 15:26 2.14E-12 6.34E-14 33.7 Aluminum 2 4/26/2013 15:53 4/26/2013 18:57 2.15E-12 6.39E-14 33.7 Aluminum 1 4/26/2013 12:21 4/26/2013 15:26 2.38E-12 7.05E-14 33.7 Aluminum 2 4/26/2013 15:53 4/26/2013 18:57 2.15E-12 6.39E-14 33.7 Aluminum 1 4/26/2013 12:21 4/26/2013 15:26 1.42E-12 4.21E-14 33.7 Aluminum 2 4/26/2013 15:53 4/26/2013 18:57 2.03E-12 6.02E-14 33.7 Aluminum 1 4/26/2013 12:21 4/26/2013 15:26 2.39E-12 7.09E-14 33.7 Aluminum 2 4/26/2013 15:53 4/26/2013 18:57 2.28E-12 6.77E-14 33.7 Aluminum **Test Start Time**  **Test End**

**Date Test End** 

**Time**
1,2,3,4,6,7,8- HpCDD **Throughput (ton/hr)**  **Compound Run** 

**Number Test Start** 

**Date**

1,2,3,4,6,7,8- HpCDF 1,2,3,4,7,8,9- HpCDF 1,2,3,4,7,8- HxCDD 1,2,3,4,7,8- HxCDF 1,2,3,6,7,8- HxCDD 1,2,3,6,7,8- HxCDF 1,2,3,7,8,9- HxCDD **Calculated Emission Rate Throughput**  **Ma terial** 

### Page 2 of 8

**lb/hr lb/ton** 

**Throughput Test Start**  **Time Test End** 

**Date Test End** 

**Time Throughput**  **(ton/hr) Compound**  **Run**

**Number Test Start** 

**Date Calculated Emission Rate**  **Throughput Ma** **terial**

1 4/26/2013 12:21 4/26/2013 15:26 1.51E-12 4.48E-14 33.7 Aluminum 2 4/26/2013 15:53 4/26/2013 18:57 2.66E-12 7.90E-14 33.7 Aluminum 1 4/26/2013 12:21 4/26/2013 15:26 4.06E-11 1.20E-12 33.7 Aluminum 2 4/26/2013 15:53 4/26/2013 18:57 N/A #VALUE! 33.7 Aluminum 1 4/26/2013 12:21 4/26/2013 15:26 8.30E-13 2.46E-14 33.7 Aluminum 2 4/26/2013 15:53 4/26/2013 18:57 8.71E-13 2.58E-14 33.7 Aluminum 1 4/26/2013 12:21 4/26/2013 15:26 1.71E-12 5.07E-14 33.7 Aluminum 2 4/26/2013 15:53 4/26/2013 18:57 3.04E-12 9.02E-14 33.7 Aluminum 1 4/26/2013 12:21 4/26/2013 15:26 4.52E-12 1.34E-13 33.7 Aluminum 2 4/26/2013 15:53 4/26/2013 18:57 4.56E-12 1.35E-13 33.7 Aluminum 1 4/26/2013 12:21 4/26/2013 15:26 3.14E-11 9.32E-13 33.7 Aluminum 2 4/26/2013 15:53 4/26/2013 18:57 3.67E-11 1.09E-12 33.7 Aluminum 1 4/26/2013 12:21 4/26/2013 15:26 1.63E-12 4.85E-14 33.7 Aluminum 2 4/26/2013 15:53 4/26/2013 18:57 2.41E-12 7.14E-14 33.7 Aluminum 1 4/26/2013 12:21 4/26/2013 15:26 4.90E-14 1.45E-15 33.7 Aluminum 2 4/26/2013 15:53 4/26/2013 18:57 2.01E-14 5.98E-16 33.7 Aluminum 1 4/26/2013 12:21 4/26/2013 15:26 1.02E-14 3.02E-16 33.7 Aluminum 2 4/26/2013 15:53 4/26/2013 18:57 1.52E-14 4.51E-16 33.7 Aluminum 1,2,3,7,8,9- HxCDF

1,2,3,7,8- PeCDF 2,3,4,6,7,8- HxCDF 1,2,3,7,8- PeCDD

2,3,4,7,8- PeCDF

OCDF OCDD 2,3,7,8- TCDD 2,3,7,8-TCDF

### Page 3 of 8 

# Primary Aluminum Testing: Dioxins and Furans
391 St. Jude Industrial Park **Parent company name:**  Noranda Aluminum, Inc. **Facility address:** 391 St. Jude Industrial Park New Madrid, MO 63869 New Madrid, MO 63869 **Description of source tested:** Paste Plant Stack

**Me asured**  **Value (n g)**  **Wet or Dry**

**Basis Test Method** 

**(e.g.,CA RB 429)**  **Data Flag**

**(A DL, BDL, DLL)** **Front Half**

**Ma****ss* (ng)** **Back Half**

**Ma ss**  (ng)****Impinger Soln**

**Ma ss** * (ng)** 1 5.30E-03 Dry CARB 428 BDL 2 2.10E-03 Dry CARB 428 BDL 1 1.40E-03 Dry CARB 428 BDL 2 1.60E-03 Dry CARB 428 BDL 1 1.80E-03 Dry CARB 428 BDL 2 2.20E-03 Dry CARB 428 BDL 1 1.80E-03 Dry CARB 428 BDL 2 1.70E-03 Dry CARB 428 BDL 1 1.70E-03 Dry CARB 428 BDL 2 1.70E-03 Dry CARB 428 BDL 1 1.89E-03 Dry CARB 428 ADL 2 1.70E-03 Dry CARB 428 BDL 1 1.13E-03 Dry CARB 428 ADL 2 1.60E-03 Dry CARB 428 BDL 1 1.90E-03 Dry CARB 428 BDL 2 1.80E-03 Dry CARB 428 BDL **Run Number**  **Dioxins and Furans Emission Test Results**

1,2,3,4,6,7,8- HpCDD **Test Method Comments Compound** 

1,2,3,4,6,7,8- HpCDF 1,2,3,4,7,8,9- HpCDF 1,2,3,4,7,8- HxCDD 1,2,3,4,7,8- HxCDF 1,2,3,6,7,8- HxCDD 1,2,3,6,7,8- HxCDF 1,2,3,7,8,9- HxCDD **Separate A nalysis** 

### Page 4 of 8

**Me asured**  **Value (n g)**  **Wet or Dry**

**Basis Test Method** 

**(e.g.,CA RB 429)**  **Data Flag**

**(A DL, BDL, DLL)** **Front Half**

**Ma****ss* (ng)** **Back Half**

**Ma ss**  (ng)****Impinger Soln**

**Ma ss** * (ng)** **Run Number**  **Dioxins and Furans Emission Test Results Test Method Comments**  **Compound Separate A** **nalysis**

1 1.20E-03 Dry CARB 428 BDL 2 2.10E-03 Dry CARB 428 BDL 1 3.20E-03 Dry CARB 428 BDL 2 N/A Dry CARB 428 BDL 1 2.20E-03 Dry CARB 428 BDL 2 2.29E-03 Dry CARB 428 ADL 1 1.36E-03 Dry CARB 428 ADL 2 2.40E-03 Dry CARB 428 BDL 1 1.20E-03 Dry CARB 428 BDL 2 1.20E-03 Dry CARB 428 BDL 1 2.50E-03 Dry CARB 428 BDL 2 2.90E-03 Dry CARB 428 BDL 1 1.30E-03 Dry CARB 428 BDL 2 1.90E-03 Dry CARB 428 BDL 1 1.30E-02 Dry CARB 428 BDL 2 5.30E-03 Dry CARB 428 BDL 1 2.70E-03 Dry CARB 428 BDL 2 4.00E-03 Dry CARB 428 BDL * Front Half Composite contains particulate filter, front half of the filter holder, and probe solvent rinses ** Back Half Composite contains XAD-2 resin tube, back half of the filter holder, and coil condenser solvent rinses 1,2,3,7,8,9- HxCDF

1,2,3,7,8- PeCDF 2,3,4,6,7,8- HxCDF 2,3,4,7,8- PeCDF

OCDF 2,3,7,8- TCDD 2,3,7,8-TCDF
OCDD 1,2,3,7,8- PeCDD

### Page 5 of 8 

# Primary Aluminum Testing: Dioxins and Furans
391 St. Jude Industrial Park **Parent company name:**  Noranda Aluminum, Inc. **Facility address:**  New Madrid, MO 63869 **Description of source tested:** Paste Plant Stack

**Composite A nalysis**  **Total (ng) Total (ng)**  **Moisture (%)**  **CO 2** **(%) O** **2 (%)**  **Flow (acfm)**  **Flow**

**(dscfm) Temperature** 

**( °F)**  5.30E-03 5.30E-03 1 1.5 0.0 20.9 13,678 12,850 93.2 2.10E-03 2.10E-03 2 1.4 0.1 20.8 13,308 12,501 93.3 1.40E-03 1.40E-03 1 1.5 0.0 20.9 13,678 12,850 93.2 1.60E-03 1.60E-03 2 1.4 0.1 20.8 13,308 12,501 93.3 1.80E-03 1.80E-03 1 1.5 0.0 20.9 13,678 12,850 93.2 2.20E-03 2.20E-03 2 1.4 0.1 20.8 13,308 12,501 93.3 1.80E-03 1.80E-03 1 1.5 0.0 20.9 13,678 12,850 93.2 1.70E-03 1.70E-03 2 1.4 0.1 20.8 13,308 12,501 93.3 1.70E-03 1.70E-03 1 1.5 0.0 20.9 13,678 12,850 93.2 1.70E-03 1.70E-03 2 1.4 0.1 20.8 13,308 12,501 93.3 1.89E-03 1.89E-03 1 1.5 0.0 20.9 13,678 12,850 93.2 1.70E-03 1.70E-03 2 1.4 0.1 20.8 13,308 12,501 93.3 1.13E-03 1.13E-03 1 1.5 0.0 20.9 13,678 12,850 93.2 1.60E-03 1.60E-03 2 1.4 0.1 20.8 13,308 12,501 93.3 1.90E-03 1.90E-03 1 1.5 0.0 20.9 13,678 12,850 93.2 1.80E-03 1.80E-03 2 1.4 0.1 20.8 13,308 12,501 93.3 **Exhaust Gas Run**  **Number**
1,2,3,4,6,7,8- HpCDD **Compound**

1,2,3,4,6,7,8- HpCDF 1,2,3,4,7,8,9- HpCDF 1,2,3,4,7,8- HxCDD 1,2,3,4,7,8- HxCDF 1,2,3,6,7,8- HxCDD 1,2,3,6,7,8- HxCDF 1,2,3,7,8,9- HxCDD

### Page 6 of 8

**Composite A nalysis**  **Total (ng) Total (ng)**  **Moisture (%)**  **CO 2** **(%) O** **2 (%)**  **Flow (acfm)**  **Flow**

**(dscfm) Temperature** 

**( °F)**  **Exhaust Gas Run**  **Number Compound** 

1.20E-03 1.20E-03 1 1.5 0.0 20.9 13,678 12,850 93.2 2.10E-03 2.10E-03 2 1.4 0.1 20.8 13,308 12,501 93.3 3.20E-03 3.20E-03 1 1.5 0.0 20.9 13,678 12,850 93.2 N/A N/A 2 1.4 0.1 20.8 13,308 12,501 93.3 2.20E-03 2.20E-03 1 1.5 0.0 20.9 13,678 12,850 93.2 2.29E-03 2.29E-03 2 1.4 0.1 20.8 13,308 12,501 93.3 1.36E-03 1.36E-03 1 1.5 0.0 20.9 13,678 12,850 93.2 2.40E-03 2.40E-03 2 1.4 0.1 20.8 13,308 12,501 93.3 1.20E-03 1.20E-03 1 1.5 0.0 20.9 13,678 12,850 93.2 1.20E-03 1.20E-03 2 1.4 0.1 20.8 13,308 12,501 93.3 2.50E-03 2.50E-03 1 1.5 0.0 20.9 13,678 12,850 93.2 2.90E-03 2.90E-03 2 1.4 0.1 20.8 13,308 12,501 93.3 1.30E-03 1.30E-03 1 1.5 0.0 20.9 13,678 12,850 93.2 1.90E-03 1.90E-03 2 1.4 0.1 20.8 13,308 12,501 93.3 1.30E-02 1.30E-02 1 1.5 0.0 20.9 13,678 12,850 93.2 5.30E-03 5.30E-03 2 1.4 0.1 20.8 13,308 12,501 93.3 2.70E-03 2.70E-03 1 1.5 0.0 20.9 13,678 12,850 93.2 4.00E-03 4.00E-03 2 1.4 0.1 20.8 13,308 12,501 93.3 1,2,3,7,8,9- HxCDF 1,2,3,7,8-PeCDD 1,2,3,7,8-PeCDF 2,3,4,6,7,8- HxCDF

OCDF OCDD 2,3,7,8-TCDD 2,3,7,8-TCDF 2,3,4,7,8-PeCDF

### Page 7 of 8



### 391 St. Jude Industrial Park New Madrid, MO 63869

**Other Supporting Information**

### Page 8 of 8

**Other Supporting Information**Page 1 of 4 

## Primary Aluminum Testing: Polychlorinate Biphenyls (PCB) **Parent company**

**name:** Noranda Aluminum, Inc. **Facility address:** 391 St. Jude Industrial Park

New Madrid, MO 63869 **Description of source tested:** Paste Plant Stack

**lb/hr lb/ton**  **Throughput** 1 4/26/2013 12:21 4/26/2013 15:26 3.02E-08 8.95E-10 33.7 Green Anode 2 4/26/2013 15:53 4/26/2013 18:57 2.91E-08 8.65E-10 33.7 Green Anode 1 4/26/2013 12:21 4/26/2013 15:26 3.52E-08 1.04E-09 33.7 Green Anode 2 4/26/2013 15:53 4/26/2013 18:57 2.15E-08 6.39E-10 33.7 Green Anode 1 4/26/2013 12:21 4/26/2013 15:26 2.25E-08 6.68E-10 33.7 Green Anode 2 4/26/2013 15:53 4/26/2013 18:57 1.76E-08 5.23E-10 33.7 Green Anode 1 4/26/2013 12:21 4/26/2013 15:26 1.62E-08 4.81E-10 33.7 Green Anode 2 4/26/2013 15:53 4/26/2013 18:57 1.38E-08 4.10E-10 33.7 Green Anode 1 4/26/2013 12:21 4/26/2013 15:26 2.39E-09 7.09E-11 33.7 Green Anode 2 4/26/2013 15:53 4/26/2013 18:57 6.84E-09 2.03E-10 33.7 Green Anode 1 4/26/2013 12:21 4/26/2013 15:26 1.51E-09 4.48E-11 33.7 Green Anode 2 4/26/2013 15:53 4/26/2013 18:57 1.25E-09 3.72E-11 33.7 Green Anode **Calculated Emission Rate**  **Throughput**

**(ton/hr) Compound**  **Run**

**Number Test Start** 

**Date Test Start** 

**Time Test End** 

**Date Test End** 

**Time Test Method Comments** 

Monochlorinated biphenyls **Throughput Material** 

Dichlorinated biphenyls Trichlorinated biphenyls Tetrachlorinated biphenyls Pentachlorinated biphenyls Hexachlorinated biphenylsPage 2 of 4

**lb/hr lb/ton** 

**Throughput Calculated Emission**  **Rate Throughput** 

**(ton/hr) Compound**  **Run**

**Number Test Start** 

**Date Test Start** 

**Time Test End** 

**Date Test End** 

**Time Test Method Comments**  **Throughput Material** 

1 4/26/2013 12:21 4/26/2013 15:26 2.89E-10 8.58E-12 33.7 Green Anode 2 4/26/2013 15:53 4/26/2013 18:57 1.10E-09 3.27E-11 33.7 Green Anode 1 4/26/2013 12:21 4/26/2013 15:26 2.89E-10 8.58E-12 33.7 Green Anode 2 4/26/2013 15:53 4/26/2013 18:57 9.63E-10 2.86E-11 33.7 Green Anode 1 4/26/2013 12:21 4/26/2013 15:26 1.51E-10 4.48E-12 33.7 Green Anode 2 4/26/2013 15:53 4/26/2013 18:57 6.84E-10 2.03E-11 33.7 Green Anode 1 4/26/2013 12:21 4/26/2013 15:26 1.38E-10 4.10E-12 33.7 Green Anode 2 4/26/2013 15:53 4/26/2013 18:57 4.94E-10 1.47E-11 33.7 Green Anode Heptachlorinated biphenyls Octachlorinated biphenyls

Decachlorinated biphenyls Nonachlorinated biphenylsPage 3 of 4

**Composite Analy**  **sis Compound**  **Total (ng) Total (ng)**  **Moisture (%** **) CO** **2 (%** **) O** **2 (%** **) Flow**  **(acfm) Flow** 

**(dscfm) Temperature** 

**( °F)**  2 2 1 1.5 0.0 20.9 13,678 12,850 93.2 2 2 2 1.4 0.1 20.8 13,308 12,501 93.3 3 3 1 1.5 0.0 20.9 13,678 12,850 93.2 2 2 2 1.4 0.1 20.8 13,308 12,501 93.3 2 2 1 1.5 0.0 20.9 13,678 12,850 93.2 1 1 2 1.4 0.1 20.8 13,308 12,501 93.3 1 1 1 1.5 0.0 20.9 13,678 12,850 93.2 1 1 2 1.4 0.1 20.8 13,308 12,501 93.3 0 0 1 1.5 0.0 20.9 13,678 12,850 93.2 1 1 2 1.4 0.1 20.8 13,308 12,501 93.3 0 0 1 1.5 0.0 20.9 13,678 12,850 93.2 0.1 0.1 2 1.4 0.1 20.8 13,308 12,501 93.3 Pentachlorinated biphenyls Hexachlorinated biphenyls Monochlorinated biphenyls Dichlorinated biphenyls **Other Supporting Information**

**Separate Analy**

**sis**

Monochlorinated biphenyls **Poly chlorinated Bipheny** **ls Emission Test Results Compound**  **Run Number**  **Exhaust Gas**

Dichlorinated biphenyls Trichlorinated biphenyls Trichlorinated biphenyls Tetrachlorinated biphenyls Pentachlorinated biphenyls Tetrachlorinated biphenyls

Hexachlorinated biphenylsPage 4 of 4 **Composite Analy**  **sis Compound**  **Total (ng) Total (ng)**  **Moisture (%** **) CO** **2 (%** **) O** **2 (%** **) Flow**  **(acfm) Flow** 

**(dscfm) Temperature** 

**( °F)**  **Other Supporting Information Separate Analy** 

**sis Poly** **chlorinated Bipheny ls Emission Test Results**  **Compound Run**  **Number Exhaust Gas** 

0.0 0.0 1 1.5 0.0 20.9 13,678 12,850 93.2 0.1 0.1 2 1.4 0.1 20.8 13,308 12,501 93.3 0.0 0.0 1 1.5 0.0 20.9 13,678 12,850 93.2 0.1 0.1 2 1.4 0.1 20.8 13,308 12,501 93.3 0.0 0.0 1 1.5 0.0 20.9 13,678 12,850 93.2 0.1 0.1 2 1.4 0.1 20.8 13,308 12,501 93.3 0.0 0.0 1 1.5 0.0 20.9 13,678 12,850 93.2 0.0 0.0 2 1.4 0.1 20.8 13,308 12,501 93.3 Nonachlorinated biphenyls Heptachlorinated biphenyls Octachlorinated biphenyls Heptachlorinated biphenyls Octachlorinated biphenyls

Decachlorinated biphenyls Nonachlorinated biphenyls Decachlorinated biphenyls

# Primary Aluminum Testing: Exhaust flow rates, temperatures, and O2/CO2 contents **Parent company**

**name:** Noranda Aluminum, Inc. **Facility address:** 391 St. Jude Industrial Park

New Madrid, MO 63869 **Description of source tested:**Paste Plant Stack

**Moisture (%)**  **CO 2** **(%) O** **2 (%)**  **Flow (acfm)**  **Flow**

**(dscfm)** 1 4/26/13 12:21 4/26/13 15:26 Methods 1-4 CARB 428/429 1.5 0.0 20.9 13,678 12,850 2 4/26/13 15:53 4/26/13 18:57 Methods 1-4 CARB 428/429 1.4 0.1 20.8 13,308 12,501 **Test Start Date**  **Run Number**  **Exhaust Gas Simultaneous**  **with which pollutant test?**  **Test Method (e.g. Method 5)**  **Test End Time**  **Test End Date**  **Test Start Time** 

### 391 St. Jude Industrial Park

**Temp ( °F)**  93.2 93.3