Instructions for using the Emission Test Reporting Template for the Primary Aluminum Test Program

This Information Collection Request (ICR) spreadsheet is intended to be used to report emissions data from primary aluminum 

reduction facilities as an alternative to the Electronic Reporting Tool (ERT), as well as in cases where the test methods are not 

currently supported by the ERT. Data for multiple process units should be reported by using separate copies of the 

appropriate tabs of this spreadsheet. Please Do Not delete rows or columns, addition of rows and columns is appropriate 

as necessary. 

Emission Data Worksheets 

The emission data worksheets are provided for each test required for this testing program, although all facilities are not 

required to conduct all of the tests. On each worksheet, please enter process unit operating information during sampling 

and emission test results. The emission test results to be entered depends on the constituent. 

Source Operating Information

1. Please provide the Exhaust Flow Rate (acfm and dscfm) and the Exhaust Temperature (deg F). 

2. Please provide the values of all requested parameters for each of the sample testing periods in the appropriate cells.

3. Please provide any other supporting information or comments in the Other Supporting Information field.
Primary Aluminum Testing: Filterable Particulate Matter

Parent company name: Noranda Aluminum, Inc. Facility address: 391 St. Jude Industrial Park

 New Madrid, MO 63869

Description of source tested: Past Plant Stack

Test Method Used 

(e.g. Method 5)

Data Flag 

(ADL, BDL, DLL) Test Method Comments

Moisture (%) CO2 (%) O2 (%) Flow (acfm) Temperature (°F)

lb/hr lb/ton of 

throughput Material Rate (ton/hr)

1 0.664 0.105 Aluminum 6.30

2 0.930 0.148 Aluminum 6.30

3 0.552 0.088 Aluminum 6.30

Run 

Number

Calculated Emission Rate Production or Throughput

Filterable Particulate Emission Test Results

Concentration 

(ug/dscm)

Exhaust Gas

Other Supporting Information

Test End 

Date

Test End 

Time

Flow (dscfm)

Run 

Number

Run 

Number

Test Start 

Date

Test Start 

Time
Primary Aluminum Testing: HAP Metals

Parent company name: Noranda Aluminum, Inc. Facility address: 391 St. Jude Industrial Park

 New Madrid, MO 63869

Description of source:

Pollutant Concentration 

(ug/dscm)

Test Method Used 

(e.g. Method 29)

Data Flag 

(ADL, BDL, DLL) Test Method Comments

1 Antimony

2 Antimony

3 Antimony

1 Arsenic

2 Arsenic

3 Arsenic

1 Beryllium

2 Beryllium

3 Beryllium

1 Cadmium

2 Cadmium

3 Cadmium

1 Chromium

2 Chromium

3 Chromium

1 Cobalt

2 Cobalt

3 Cobalt

1 Lead

2 Lead

3 Lead

1 Manganese

2 Manganese

3 Manganese

1 Nickel

2 Nickel

3 Nickel

1 Selenium

2 Selenium

3 Selenium

1 Mercury

2 Mercury

3 Mercury

Run 

Number

Test Start 

Date

Test Start 

Time

Test End 

Date

Test End 

Time

Filterable Particulate Emission Test Results
Primary Aluminum Testing: HAP Metals

Parent company name: Noranda Aluminum, Inc. Facility address: 391 St. Jude Industrial Park

 New Madrid, MO 63869

Description of source:

lb/hr lb/ton of 

throughput Material Rate (tons/hour)

Moisture 

(%)

CO2 

(%)

O2 

(%)

Flow 

(acfm)

Flow 

(dscfm)

Temp 

(°F)

1

2

3

1

2

3

1

2

3

1

2

3

1

2

3

1

2

3

1

2

3

1

2

3

1

2

3

1

2

3

1

2

3

Other Supporting Information

Calculated Emission Rate Production or Throughput Exhaust Gas

Run 

Number
Primary Aluminum Testing: Hexavalent Chromium

Parent company name: Noranda Aluminum, Inc. Facility address: 391 St. Jude Industrial Park

 New Madrid, MO 63869

Description of source tested:

Test Method Used 

(SW-846 M0061)

Data Flag 

(ADL, BDL, DLL) Test Method Comments

1

2

3

Moisture (%) CO2 (%) O2 (%) Flow (acfm) Temperature (°F)

1

2

3

lb/hr lb/ton of 

throughput Material Rate (tons/hour)

1

2

3

Run 

Number

Calculated Emission Rate Production or Throughput

Run 

Number

Exhaust Gas

Other Supporting Information

Flow (dscfm)

Run 

Number

Test Start 

Date

Test Start 

Time

Test End 

Date

Test End 

Time

Hexavalent Chromium Emission Test Results

Concentration 

(ug/dscm)
Primary Aluminum Testing: PM and POM as MCEM

Parent company name: Noranda Aluminum, Inc. Facility address: 391 St. Jude Industrial Park

 New Madrid, MO 63869

Description of source tested:

Rate (tons/hour)

1

2

3

Moisture (%) CO2 (%) O2 (%) Flow (acfm) Temperature (°F)

1

2

3

lb/hr lb/ton of 

throughput Pollutant Conc (ug/dscm)

Test Method Used 

(e.g. Method 315)

PM

POM as MCEM

PM

POM as MCEM

PM

POM as MCEM

1

2

3

Production or Throughput

Data Flag 

(ADL, BDL, DLL)

Particulate Matter and POM as MCEM Emission Test Results

Test Method Comments

Run 

Number

Run 

Number

Exhaust Gas

Calculated Emission Rate

Other Supporting Information

Flow (dscfm)

Run 

Number

Test Start 

Date

Test Start 

Time

Test End 

Date

Test End 

Time Material
Page 1 of 8

Primary Aluminum Testing: Polycyclic Aromatic Hydrocarbons

Parent company name: Noranda Aluminum, Inc. Facility address: 391 St. Jude Industrial Park

 New Madrid, MO 63869

Description of source tested: Paste Plant Stack

lb/hr lb/ton 

Throughput

1 4/26/2013 12:21 4/26/2013 15:26 7.72E-02 2.29E-03 33.7

2 4/26/2013 15:53 4/26/2013 18:57 8.68E-02 2.58E-03 33.7

1 4/26/2013 12:21 4/26/2013 15:26 1.37E-04 4.06E-06 33.7

2 4/26/2013 15:53 4/26/2013 18:57 1.43E-04 4.24E-06 33.7

1 4/26/2013 12:21 4/26/2013 15:26 2.31E-03 6.86E-05 33.7

2 4/26/2013 15:53 4/26/2013 18:57 2.50E-03 7.41E-05 33.7

1 4/26/2013 12:21 4/26/2013 15:26 8.69E-06 2.58E-07 33.7

2 4/26/2013 15:53 4/26/2013 18:57 1.83E-05 5.44E-07 33.7

1 4/26/2013 12:21 4/26/2013 15:26 4.96E-07 1.47E-08 33.7

2 4/26/2013 15:53 4/26/2013 18:57 3.09E-06 9.16E-08 33.7

1 4/26/2013 12:21 4/26/2013 15:26 1.08E-06 3.20E-08 33.7

2 4/26/2013 15:53 4/26/2013 18:57 4.55E-06 1.35E-07 33.7

1 4/26/2013 12:21 4/26/2013 15:26 2.23E-06 6.63E-08 33.7

2 4/26/2013 15:53 4/26/2013 18:57 9.25E-06 2.74E-07 33.7

1 4/26/2013 12:21 4/26/2013 15:26 7.92E-08 2.35E-09 33.7

2 4/26/2013 15:53 4/26/2013 18:57 9.23E-07 2.74E-08 33.7

Acenaphthene (83-32-9)

Test Start 

Time

Test End 

Date

Test End 

Time

Calculated Emission Rate

Throughput 

(ton/hr) Compound Run Number

Test Start 

Date

Anthracene (120-12-7)

Benz[a]anthracene (56-55-3)

Benzo[a]pyrene (50-32-8)

Benzo(e)pyrene (192-97-2)

Benzo[b]fluoranthene (205-99-2)

Benzo[g,h,i]perylene (191-24-2)

Acenaphthylene (208-96-8)
Page 2 of 8

lb/hr lb/ton 

Throughput

Test Start 

Time

Test End 

Date

Test End 

Time

Calculated Emission Rate

Throughput 

(ton/hr) Compound Run Number

Test Start 

Date

1 4/26/2013 12:21 4/26/2013 15:26 6.95E-07 2.06E-08 33.7

2 4/26/2013 15:53 4/26/2013 18:57 2.85E-06 8.45E-08 33.7

1 4/26/2013 12:21 4/26/2013 15:26 9.29E-06 2.76E-07 33.7

2 4/26/2013 15:53 4/26/2013 18:57 2.12E-05 6.30E-07 33.7

1 4/26/2013 12:21 4/26/2013 15:26 1.26E-07 3.73E-09 33.7

2 4/26/2013 15:53 4/26/2013 18:57 3.45E-07 1.02E-08 33.7

1 4/26/2013 12:21 4/26/2013 15:26 2.22E-03 6.60E-05 33.7

2 4/26/2013 15:53 4/26/2013 18:57 2.18E-03 6.46E-05 33.7

1 4/26/2013 12:21 4/26/2013 15:26 1.09E-02 3.24E-04 33.7

2 4/26/2013 15:53 4/26/2013 18:57 1.01E-02 2.99E-04 33.7

1 4/26/2013 12:21 4/26/2013 15:26 7.29E-08 2.16E-09 33.7

2 4/26/2013 15:53 4/26/2013 18:57 9.72E-07 2.88E-08 33.7

1 4/26/2013 12:21 4/26/2013 15:26 5.65E-03 1.68E-04 33.7

2 4/26/2013 15:53 4/26/2013 18:57 5.28E-03 1.57E-04 33.7

1 4/26/2013 12:21 4/26/2013 15:26 2.13E-03 6.33E-05 33.7

2 4/26/2013 15:53 4/26/2013 18:57 2.19E-03 6.50E-05 33.7

1 4/26/2013 12:21 4/26/2013 15:26 3.04E-02 9.02E-04 33.7

2 4/26/2013 15:53 4/26/2013 18:57 3.21E-02 9.51E-04 33.7

1 4/26/2013 12:21 4/26/2013 15:26 9.55E-08 2.83E-09 33.7

2 4/26/2013 15:53 4/26/2013 18:57 6.12E-07 1.82E-08 33.7

1 4/26/2013 12:21 4/26/2013 15:26 1.23E-03 3.65E-05 33.7

2 4/26/2013 15:53 4/26/2013 18:57 1.12E-03 3.32E-05 33.7

Benzo[k]fluoranthene (207-08-9)

Chrysene (218-01-9)

Naphthalene (91-20-3)

2-Methylnaphthalene (91-57-6)

Phenanthrene (85-01-8)

Perylene (198-55-0)

Dibenz[a,h]anthracene (53-70-3)

Fluoranthene (206-44-0)

Fluorene (86-73-7)

Indeno (1,2,3-cd) pyrene (193-39-5)

Pyrene (129-00-0)
Page 3 of 8

Primary Aluminum Testing: Polycyclic Aromatic Hydrocarbons

de Industrial Park Parent company name: Noranda Aluminum, Inc. Facility address:

d, MO 63869

Description of source tested: Paste Plant Stack

Measured 

Value (ng)

Wet or Dry 

Basis

Test Method 

(e.g.,CARB 429)

Data Flag 

(ADL, BDL, DLL)

Front Half 

Mass* (ng)

Back Half 

Mass** (ng)

Condensate 

Mass*** (ng)

Aluminum 1 6.14E+06 Dry CARB 429 ADL

Aluminum 2 6.85E+06 Dry CARB 429 ADL

Aluminum 1 1.09E+04 Dry CARB 429 ADL

Aluminum 2 1.13E+04 Dry CARB 429 ADL

Aluminum 1 1.84E+05 Dry CARB 429 ADL

Aluminum 2 1.97E+05 Dry CARB 429 ADL

Aluminum 1 6.92E+02 Dry CARB 429 ADL

Aluminum 2 1.45E+03 Dry CARB 429 ADL

Aluminum 1 3.95E+01 Dry CARB 429 ADL

Aluminum 2 2.44E+02 Dry CARB 429 ADL

Aluminum 1 8.57E+01 Dry CARB 429 ADL

Aluminum 2 3.59E+02 Dry CARB 429 ADL

Aluminum 1 1.78E+02 Dry CARB 429 ADL

Aluminum 2 7.30E+02 Dry CARB 429 ADL

Aluminum 1 6.30E+00 Dry CARB 429 ADL

Aluminum 2 7.28E+01 Dry CARB 429 ADL

Compound Run 

Number

Throughput 

Material

Benzo(e) pyrene

Acenaphthene

Acenaphthylene

Anthracene

Benz[a] 

anthracene

Benzo[a] pyrene

Benzo[b] 

fluoranthene

Benzo[g,h,i]peryle

ne

Polycyclic Aromatic Hydrocarbons Emission Test Results
Page 4 of 8

Measured 

Value (ng)

Wet or Dry 

Basis

Test Method 

(e.g.,CARB 429)

Data Flag 

(ADL, BDL, DLL)

Front Half 

Mass* (ng)

Back Half 

Mass** (ng)

Condensate 

Mass*** (ng)

Compound Run 

Number

Throughput 

Material

Polycyclic Aromatic Hydrocarbons Emission Test Results

Aluminum 1 5.53E+01 Dry CARB 429 ADL

Aluminum 2 2.25E+02 Dry CARB 429 ADL

Aluminum 1 7.39E+02 Dry CARB 429 ADL

Aluminum 2 1.68E+03 Dry CARB 429 ADL

Aluminum 1 1.00E+01 Dry CARB 429 ADL

Aluminum 2 2.72E+01 Dry CARB 429 ADL

Aluminum 1 1.77E+05 Dry CARB 429 ADL

Aluminum 2 1.72E+05 Dry CARB 429 ADL

Aluminum 1 8.69E+05 Dry CARB 429 ADL

Aluminum 2 7.95E+05 Dry CARB 429 ADL

Aluminum 1 5.80E+00 Dry CARB 429 ADL

Aluminum 2 7.67E+01 Dry CARB 429 ADL

Aluminum 1 4.49E+05 Dry CARB 429 ADL

Aluminum 2 4.16E+05 Dry CARB 429 ADL

Aluminum 1 1.70E+05 Dry CARB 429 ADL

Aluminum 2 1.73E+05 Dry CARB 429 ADL

Aluminum 1 2.42E+06 Dry CARB 429 ADL

Aluminum 2 2.53E+06 Dry CARB 429 ADL

Aluminum 1 7.60E+00 Dry CARB 429 ADL

Aluminum 2 4.83E+01 Dry CARB 429 ADL

Aluminum 1 9.79E+04 Dry CARB 429 ADL

Aluminum 2 8.83E+04 Dry CARB 429 ADL

* Contains particulate filter, front half of filter holder and probe solvent rinses *** Contains condensate, impinger contents and glassware solven

** Contains XAD-2 resin tube, back half of filter holder and coil condenser solvent rinses

Benzo[k] 

fluoranthene

Chrysene

Phenan threne

Perylene

Dibenz[a,h] 

anthracene

Fluoranthene

Fluorene

Indeno (1,2,3-cd) 

pyrene

Pyrene

Naphthalene

2-Methyl 

naphthalene
Page 5 of 8

Primary Aluminum Testing: Polycyclic Aromatic Hydrocarbons

 391 St. Jude Industrial Park Parent company name: Noranda Aluminum, Inc. Facility address:

 New Madrid, MO 63869

Description of source tested: Paste Plant Stack

Total (ng) Test Method 

Comments

Moisture 

(%) CO2

 (%) O2 (%) Flow 

(acfm)

Flow 

(dscfm)

Temperature 

(°F)

6.14E+06 1 1.5 0.0 20.9 13,678 12,850 93.2

6.85E+06 2 1.4 0.1 20.8 13,308 12,501 93.3

1.09E+04 1 1.5 0.0 20.9 13,678 12,850 93.2

1.13E+04 2 1.4 0.1 20.8 13,308 12,501 93.3

1.84E+05 1 1.5 0.0 20.9 13,678 12,850 93.2

1.97E+05 2 1.4 0.1 20.8 13,308 12,501 93.3

6.92E+02 1 1.5 0.0 20.9 13,678 12,850 93.2

1.45E+03 2 1.4 0.1 20.8 13,308 12,501 93.3

3.95E+01 1 1.5 0.0 20.9 13,678 12,850 93.2

2.44E+02 2 1.4 0.1 20.8 13,308 12,501 93.3

8.57E+01 1 1.5 0.0 20.9 13,678 12,850 93.2

3.59E+02 2 1.4 0.1 20.8 13,308 12,501 93.3

1.78E+02 1 1.5 0.0 20.9 13,678 12,850 93.2

7.30E+02 2 1.4 0.1 20.8 13,308 12,501 93.3

6.30E+00 1 1.5 0.0 20.9 13,678 12,850 93.2

7.28E+01 2 1.4 0.1 20.8 13,308 12,501 93.3

Benzo(e)pyrene

Exhaust Gas

Compound Run 

Number

Acenaphthene

Acenaphthylene

Anthracene

Benzo[b] 

fluoranthene

Benzo[g,h,i] 

perylene

Benz[a] 

anthracene

Benzo[a]pyrene
Page 6 of 8

Total (ng) Test Method 

Comments

Moisture 

(%) CO2

 (%) O2 (%) Flow 

(acfm)

Flow 

(dscfm)

Temperature 

(°F)

Exhaust Gas

Compound Run 

Number

5.53E+01 1 1.5 0.0 20.9 13,678 12,850 93.2

2.25E+02 2 1.4 0.1 20.8 13,308 12,501 93.3

7.39E+02 1 1.5 0.0 20.9 13,678 12,850 93.2

1.68E+03 2 1.4 0.1 20.8 13,308 12,501 93.3

1.00E+01 1 1.5 0.0 20.9 13,678 12,850 93.2

2.72E+01 2 1.4 0.1 20.8 13,308 12,501 93.3

1.77E+05 1 1.5 0.0 20.9 13,678 12,850 93.2

1.72E+05 2 1.4 0.1 20.8 13,308 12,501 93.3

8.69E+05 1 1.5 0.0 20.9 13,678 12,850 93.2

7.95E+05 2 1.4 0.1 20.8 13,308 12,501 93.3

5.80E+00 1 1.5 0.0 20.9 13,678 12,850 93.2

7.67E+01 2 1.4 0.1 20.8 13,308 12,501 93.3

4.49E+05 1 1.5 0.0 20.9 13,678 12,850 93.2

4.16E+05 2 1.4 0.1 20.8 13,308 12,501 93.3

1.70E+05 1 1.5 0.0 20.9 13,678 12,850 93.2

1.73E+05 2 1.4 0.1 20.8 13,308 12,501 93.3

2.42E+06 1 1.5 0.0 20.9 13,678 12,850 93.2

2.53E+06 2 1.4 0.1 20.8 13,308 12,501 93.3

7.60E+00 1 1.5 0.0 20.9 13,678 12,850 93.2

4.83E+01 2 1.4 0.1 20.8 13,308 12,501 93.3

9.79E+04 1 1.5 0.0 20.9 13,678 12,850 93.2

8.83E+04 2 1.4 0.1 20.8 13,308 12,501 93.3

s and glassware solvent rinses

Benzo[k] 

fluoranthene

Chrysene

Dibenz[a,h] 

anthracene

Fluoranthene

Pyrene

Fluorene

Indeno (1,2,3-cd) 

pyrene

Naphthalene

2-Methyl 

naphthalene

Phenanthrene

Perylene
Page 7 of 8

 391 St. Jude Industrial Park

 New Madrid, MO 63869

Other Supporting Information
Page 8 of 8

Other Supporting Information
Page 1 of 8 

Primary Aluminum Testing: Dioxins and Furans

Parent company name: Noranda Aluminum, Inc. Facility address: 391 St. Jude Industrial Park

 New Madrid, MO 63869

Description of source tested: Paste Plant Stack

lb/hr lb/ton 

Throughput

1 4/26/2013 12:21 4/26/2013 15:26 6.66E-13 1.98E-14 33.7 Aluminum

2 4/26/2013 15:53 4/26/2013 18:57 2.66E-13 7.90E-15 33.7 Aluminum

1 4/26/2013 12:21 4/26/2013 15:26 1.76E-13 5.22E-15 33.7 Aluminum

2 4/26/2013 15:53 4/26/2013 18:57 2.03E-13 6.02E-15 33.7 Aluminum

1 4/26/2013 12:21 4/26/2013 15:26 2.26E-13 6.71E-15 33.7 Aluminum

2 4/26/2013 15:53 4/26/2013 18:57 2.79E-13 8.27E-15 33.7 Aluminum

1 4/26/2013 12:21 4/26/2013 15:26 2.26E-12 6.71E-14 33.7 Aluminum

2 4/26/2013 15:53 4/26/2013 18:57 2.15E-12 6.39E-14 33.7 Aluminum

1 4/26/2013 12:21 4/26/2013 15:26 2.14E-12 6.34E-14 33.7 Aluminum

2 4/26/2013 15:53 4/26/2013 18:57 2.15E-12 6.39E-14 33.7 Aluminum

1 4/26/2013 12:21 4/26/2013 15:26 2.38E-12 7.05E-14 33.7 Aluminum

2 4/26/2013 15:53 4/26/2013 18:57 2.15E-12 6.39E-14 33.7 Aluminum

1 4/26/2013 12:21 4/26/2013 15:26 1.42E-12 4.21E-14 33.7 Aluminum

2 4/26/2013 15:53 4/26/2013 18:57 2.03E-12 6.02E-14 33.7 Aluminum

1 4/26/2013 12:21 4/26/2013 15:26 2.39E-12 7.09E-14 33.7 Aluminum

2 4/26/2013 15:53 4/26/2013 18:57 2.28E-12 6.77E-14 33.7 Aluminum

Test Start 

Time

Test End 

Date

Test End 

Time

1,2,3,4,6,7,8-

HpCDD

Throughput 

(ton/hr) Compound Run Number

Test Start 

Date

1,2,3,4,6,7,8-

HpCDF

1,2,3,4,7,8,9-

HpCDF

1,2,3,4,7,8-

HxCDD

1,2,3,4,7,8-

HxCDF

1,2,3,6,7,8-

HxCDD

1,2,3,6,7,8-

HxCDF

1,2,3,7,8,9-

HxCDD

Calculated Emission Rate

Throughput 

Material
Page 2 of 8 

lb/hr lb/ton 

Throughput

Test Start 

Time

Test End 

Date

Test End 

Time

Throughput 

(ton/hr) Compound Run Number

Test Start 

Date

Calculated Emission Rate

Throughput 

Material

1 4/26/2013 12:21 4/26/2013 15:26 1.51E-12 4.48E-14 33.7 Aluminum

2 4/26/2013 15:53 4/26/2013 18:57 2.66E-12 7.90E-14 33.7 Aluminum

1 4/26/2013 12:21 4/26/2013 15:26 4.06E-11 1.20E-12 33.7 Aluminum

2 4/26/2013 15:53 4/26/2013 18:57 N/A #VALUE! 33.7 Aluminum

1 4/26/2013 12:21 4/26/2013 15:26 8.30E-13 2.46E-14 33.7 Aluminum

2 4/26/2013 15:53 4/26/2013 18:57 8.71E-13 2.58E-14 33.7 Aluminum

1 4/26/2013 12:21 4/26/2013 15:26 1.71E-12 5.07E-14 33.7 Aluminum

2 4/26/2013 15:53 4/26/2013 18:57 3.04E-12 9.02E-14 33.7 Aluminum

1 4/26/2013 12:21 4/26/2013 15:26 4.52E-12 1.34E-13 33.7 Aluminum

2 4/26/2013 15:53 4/26/2013 18:57 4.56E-12 1.35E-13 33.7 Aluminum

1 4/26/2013 12:21 4/26/2013 15:26 3.14E-11 9.32E-13 33.7 Aluminum

2 4/26/2013 15:53 4/26/2013 18:57 3.67E-11 1.09E-12 33.7 Aluminum

1 4/26/2013 12:21 4/26/2013 15:26 1.63E-12 4.85E-14 33.7 Aluminum

2 4/26/2013 15:53 4/26/2013 18:57 2.41E-12 7.14E-14 33.7 Aluminum

1 4/26/2013 12:21 4/26/2013 15:26 4.90E-14 1.45E-15 33.7 Aluminum

2 4/26/2013 15:53 4/26/2013 18:57 2.01E-14 5.98E-16 33.7 Aluminum

1 4/26/2013 12:21 4/26/2013 15:26 1.02E-14 3.02E-16 33.7 Aluminum

2 4/26/2013 15:53 4/26/2013 18:57 1.52E-14 4.51E-16 33.7 Aluminum

1,2,3,7,8,9-

HxCDF

1,2,3,7,8-

PeCDF

2,3,4,6,7,8-

HxCDF

1,2,3,7,8-

PeCDD

2,3,4,7,8-

PeCDF

OCDF

OCDD

2,3,7,8-

TCDD

2,3,7,8-TCDF
Page 3 of 8 

Primary Aluminum Testing: Dioxins and Furans

ial Park Parent company name: Noranda Aluminum, Inc. Facility address: 391 St. Jude Indu

869 New Madrid, MO 6

Description of source tested: Paste Plant Stack

Measured 

Value (ng)

Wet or Dry 

Basis

Test Method 

(e.g.,CARB 429)

Data Flag 

(ADL, BDL, DLL)

Front Half 

Mass* (ng)

Back Half 

Mass** (ng)

Impinger Soln 

Mass*** (ng)

1 5.30E-03 Dry CARB 428 BDL

2 2.10E-03 Dry CARB 428 BDL

1 1.40E-03 Dry CARB 428 BDL

2 1.60E-03 Dry CARB 428 BDL

1 1.80E-03 Dry CARB 428 BDL

2 2.20E-03 Dry CARB 428 BDL

1 1.80E-03 Dry CARB 428 BDL

2 1.70E-03 Dry CARB 428 BDL

1 1.70E-03 Dry CARB 428 BDL

2 1.70E-03 Dry CARB 428 BDL

1 1.89E-03 Dry CARB 428 ADL

2 1.70E-03 Dry CARB 428 BDL

1 1.13E-03 Dry CARB 428 ADL

2 1.60E-03 Dry CARB 428 BDL

1 1.90E-03 Dry CARB 428 BDL

2 1.80E-03 Dry CARB 428 BDL

Run 

Number

Dioxins and Furans Emission Test Results

1,2,3,4,6,7,8-

HpCDD

Test Method Comments Compound

1,2,3,4,6,7,8-

HpCDF

1,2,3,4,7,8,9-

HpCDF

1,2,3,4,7,8-

HxCDD

1,2,3,4,7,8-

HxCDF

1,2,3,6,7,8-

HxCDD

1,2,3,6,7,8-

HxCDF

1,2,3,7,8,9-

HxCDD

Separate Analysis
Page 4 of 8 

Measured 

Value (ng)

Wet or Dry 

Basis

Test Method 

(e.g.,CARB 429)

Data Flag 

(ADL, BDL, DLL)

Front Half 

Mass* (ng)

Back Half 

Mass** (ng)

Impinger Soln 

Mass*** (ng)

Run 

Number

Dioxins and Furans Emission Test Results

Test Method Comments Compound Separate Analysis

1 1.20E-03 Dry CARB 428 BDL

2 2.10E-03 Dry CARB 428 BDL

1 3.20E-03 Dry CARB 428 BDL

2 N/A Dry CARB 428 BDL

1 2.20E-03 Dry CARB 428 BDL

2 2.29E-03 Dry CARB 428 ADL

1 1.36E-03 Dry CARB 428 ADL

2 2.40E-03 Dry CARB 428 BDL

1 1.20E-03 Dry CARB 428 BDL

2 1.20E-03 Dry CARB 428 BDL

1 2.50E-03 Dry CARB 428 BDL

2 2.90E-03 Dry CARB 428 BDL

1 1.30E-03 Dry CARB 428 BDL

2 1.90E-03 Dry CARB 428 BDL

1 1.30E-02 Dry CARB 428 BDL

2 5.30E-03 Dry CARB 428 BDL

1 2.70E-03 Dry CARB 428 BDL

2 4.00E-03 Dry CARB 428 BDL

* Front Half Composite contains particulate filter, front half of the filter holder, and probe solvent rinses

** Back Half Composite contains XAD-2 resin tube, back half of the filter holder, and coil condenser solvent rinses

1,2,3,7,8,9-

HxCDF

1,2,3,7,8-

PeCDF

2,3,4,6,7,8-

HxCDF

2,3,4,7,8-

PeCDF

OCDF

2,3,7,8-

TCDD

2,3,7,8-TCDF

OCDD

1,2,3,7,8-

PeCDD
Page 5 of 8 

Primary Aluminum Testing: Dioxins and Furans

de Industrial Park Parent company name: Noranda Aluminum, Inc. Facility address:

rid, MO 63869

Description of source tested: Paste Plant Stack

Composite Analysis

Total (ng) Total (ng) Moisture 

(%) CO2

 (%) O2 (%) Flow 

(acfm)

Flow 

(dscfm)

Temperature 

(°F)

5.30E-03 5.30E-03 1 1.5 0.0 20.9 13,678 12,850 93.2

2.10E-03 2.10E-03 2 1.4 0.1 20.8 13,308 12,501 93.3

1.40E-03 1.40E-03 1 1.5 0.0 20.9 13,678 12,850 93.2

1.60E-03 1.60E-03 2 1.4 0.1 20.8 13,308 12,501 93.3

1.80E-03 1.80E-03 1 1.5 0.0 20.9 13,678 12,850 93.2

2.20E-03 2.20E-03 2 1.4 0.1 20.8 13,308 12,501 93.3

1.80E-03 1.80E-03 1 1.5 0.0 20.9 13,678 12,850 93.2

1.70E-03 1.70E-03 2 1.4 0.1 20.8 13,308 12,501 93.3

1.70E-03 1.70E-03 1 1.5 0.0 20.9 13,678 12,850 93.2

1.70E-03 1.70E-03 2 1.4 0.1 20.8 13,308 12,501 93.3

1.89E-03 1.89E-03 1 1.5 0.0 20.9 13,678 12,850 93.2

1.70E-03 1.70E-03 2 1.4 0.1 20.8 13,308 12,501 93.3

1.13E-03 1.13E-03 1 1.5 0.0 20.9 13,678 12,850 93.2

1.60E-03 1.60E-03 2 1.4 0.1 20.8 13,308 12,501 93.3

1.90E-03 1.90E-03 1 1.5 0.0 20.9 13,678 12,850 93.2

1.80E-03 1.80E-03 2 1.4 0.1 20.8 13,308 12,501 93.3

Exhaust Gas

Run 

Number

1,2,3,4,6,7,8-

HpCDD

Compound

1,2,3,4,6,7,8-

HpCDF

1,2,3,4,7,8,9-

HpCDF

1,2,3,4,7,8-

HxCDD

1,2,3,4,7,8-

HxCDF

1,2,3,6,7,8-

HxCDD

1,2,3,6,7,8-

HxCDF

1,2,3,7,8,9-

HxCDD
Page 6 of 8 

Composite Analysis

Total (ng) Total (ng) Moisture 

(%) CO2

 (%) O2 (%) Flow 

(acfm)

Flow 

(dscfm)

Temperature 

(°F)

Exhaust Gas

Run 

Number Compound

1.20E-03 1.20E-03 1 1.5 0.0 20.9 13,678 12,850 93.2

2.10E-03 2.10E-03 2 1.4 0.1 20.8 13,308 12,501 93.3

3.20E-03 3.20E-03 1 1.5 0.0 20.9 13,678 12,850 93.2

N/A N/A 2 1.4 0.1 20.8 13,308 12,501 93.3

2.20E-03 2.20E-03 1 1.5 0.0 20.9 13,678 12,850 93.2

2.29E-03 2.29E-03 2 1.4 0.1 20.8 13,308 12,501 93.3

1.36E-03 1.36E-03 1 1.5 0.0 20.9 13,678 12,850 93.2

2.40E-03 2.40E-03 2 1.4 0.1 20.8 13,308 12,501 93.3

1.20E-03 1.20E-03 1 1.5 0.0 20.9 13,678 12,850 93.2

1.20E-03 1.20E-03 2 1.4 0.1 20.8 13,308 12,501 93.3

2.50E-03 2.50E-03 1 1.5 0.0 20.9 13,678 12,850 93.2

2.90E-03 2.90E-03 2 1.4 0.1 20.8 13,308 12,501 93.3

1.30E-03 1.30E-03 1 1.5 0.0 20.9 13,678 12,850 93.2

1.90E-03 1.90E-03 2 1.4 0.1 20.8 13,308 12,501 93.3

1.30E-02 1.30E-02 1 1.5 0.0 20.9 13,678 12,850 93.2

5.30E-03 5.30E-03 2 1.4 0.1 20.8 13,308 12,501 93.3

2.70E-03 2.70E-03 1 1.5 0.0 20.9 13,678 12,850 93.2

4.00E-03 4.00E-03 2 1.4 0.1 20.8 13,308 12,501 93.3

1,2,3,7,8,9-

HxCDF

1,2,3,7,8-PeCDD

1,2,3,7,8-PeCDF

2,3,4,6,7,8-

HxCDF

OCDF

OCDD

2,3,7,8-TCDD

2,3,7,8-TCDF

2,3,4,7,8-PeCDF
Page 7 of 8 

 391 St. Jude Industrial Park

 New Madrid, MO 63869

Other Supporting Information
Page 8 of 8 

Other Supporting Information
Page 1 of 4 

Primary Aluminum Testing: Polychlorinate Biphenyls (PCB)

Parent company name: Noranda Aluminum, Inc. Facility address: 391 St. Jude Industrial Park

 New Madrid, MO 63869

Description of source tested: Paste Plant Stack

lb/hr lb/ton 

Throughput

1 4/26/2013 12:21 4/26/2013 15:26 3.02E-08 8.95E-10 33.7 Green Anode

2 4/26/2013 15:53 4/26/2013 18:57 2.91E-08 8.65E-10 33.7 Green Anode

1 4/26/2013 12:21 4/26/2013 15:26 3.52E-08 1.04E-09 33.7 Green Anode

2 4/26/2013 15:53 4/26/2013 18:57 2.15E-08 6.39E-10 33.7 Green Anode

1 4/26/2013 12:21 4/26/2013 15:26 2.25E-08 6.68E-10 33.7 Green Anode

2 4/26/2013 15:53 4/26/2013 18:57 1.76E-08 5.23E-10 33.7 Green Anode

1 4/26/2013 12:21 4/26/2013 15:26 1.62E-08 4.81E-10 33.7 Green Anode

2 4/26/2013 15:53 4/26/2013 18:57 1.38E-08 4.10E-10 33.7 Green Anode

1 4/26/2013 12:21 4/26/2013 15:26 2.39E-09 7.09E-11 33.7 Green Anode

2 4/26/2013 15:53 4/26/2013 18:57 6.84E-09 2.03E-10 33.7 Green Anode

1 4/26/2013 12:21 4/26/2013 15:26 1.51E-09 4.48E-11 33.7 Green Anode

2 4/26/2013 15:53 4/26/2013 18:57 1.25E-09 3.72E-11 33.7 Green Anode

Calculated Emission 

Rate Throughput 

(ton/hr) Compound Run Number

Test Start 

Date

Test Start 

Time

Test End 

Date

Test End 

Time Test Method Comments

Monochlorinated 

biphenyls

Throughput 

Material

Dichlorinated 

biphenyls

Trichlorinated 

biphenyls

Tetrachlorinated 

biphenyls

Pentachlorinated 

biphenyls

Hexachlorinated 

biphenyls
Page 2 of 4 

lb/hr lb/ton 

Throughput

Calculated Emission 

Rate Throughput 

(ton/hr) Compound Run Number

Test Start 

Date

Test Start 

Time

Test End 

Date

Test End 

Time Test Method Comments Throughput Material

1 4/26/2013 12:21 4/26/2013 15:26 2.89E-10 8.58E-12 33.7 Green Anode 2 4/26/2013 15:53 4/26/2013 18:57 1.10E-09 3.27E-11 33.7 Green Anode 1 4/26/2013 12:21 4/26/2013 15:26 2.89E-10 8.58E-12 33.7 Green Anode 2 4/26/2013 15:53 4/26/2013 18:57 9.63E-10 2.86E-11 33.7 Green Anode 1 4/26/2013 12:21 4/26/2013 15:26 1.51E-10 4.48E-12 33.7 Green Anode 2 4/26/2013 15:53 4/26/2013 18:57 6.84E-10 2.03E-11 33.7 Green Anode 1 4/26/2013 12:21 4/26/2013 15:26 1.38E-10 4.10E-12 33.7 Green Anode 2 4/26/2013 15:53 4/26/2013 18:57 4.94E-10 1.47E-11 33.7 Green Anode

Heptachlorinated 

biphenyls

Octachlorinated 

biphenyls

Decachlorinated 

biphenyls

Nonachlorinated 

biphenyls
Page 3 of 4 

Composite 

Analysis

Compound Total (ng) Total (ng) Moisture 

(%)

CO2 (%) O2 (%)

Flow 

(acfm)

Flow 

(dscfm)

Temperature 

(°F)

2 2 1 1.5 0.0 20.9 13,678 12,850 93.2

2 2 2 1.4 0.1 20.8 13,308 12,501 93.3

3 3 1 1.5 0.0 20.9 13,678 12,850 93.2

2 2 2 1.4 0.1 20.8 13,308 12,501 93.3

2 2 1 1.5 0.0 20.9 13,678 12,850 93.2

1 1 2 1.4 0.1 20.8 13,308 12,501 93.3

1 1 1 1.5 0.0 20.9 13,678 12,850 93.2

1 1 2 1.4 0.1 20.8 13,308 12,501 93.3

0 0 1 1.5 0.0 20.9 13,678 12,850 93.2

1 1 2 1.4 0.1 20.8 13,308 12,501 93.3

0 0 1 1.5 0.0 20.9 13,678 12,850 93.2

0.1 0.1 2 1.4 0.1 20.8 13,308 12,501 93.3

Pentachlorinated 

biphenyls

Hexachlorinated 

biphenyls

Monochlorinated 

biphenyls

Dichlorinated 

biphenyls

Other Supporting Information Separate Analysis

Monochlorinated 

biphenyls

Polychlorinated Biphenyls Emission Test Results

Compound Run 

Number

Exhaust Gas

Dichlorinated 

biphenyls

Trichlorinated 

biphenyls

Trichlorinated 

biphenyls

Tetrachlorinated 

biphenyls

Pentachlorinated 

biphenyls

Tetrachlorinated 

biphenyls

Hexachlorinated 

biphenyls
Page 4 of 4 

Composite 

Analysis

Compound Total (ng) Total (ng) Moisture 

(%)

CO2 (%) O2 (%)

Flow 

(acfm)

Flow 

(dscfm)

Temperature 

(°F)

Other Supporting Information Separate Analysis

Polychlorinated Biphenyls Emission Test Results

Compound Run 

Number

Exhaust Gas

0.0 0.0 1 1.5 0.0 20.9 13,678 12,850 93.2

0.1 0.1 2 1.4 0.1 20.8 13,308 12,501 93.3

0.0 0.0 1 1.5 0.0 20.9 13,678 12,850 93.2

0.1 0.1 2 1.4 0.1 20.8 13,308 12,501 93.3

0.0 0.0 1 1.5 0.0 20.9 13,678 12,850 93.2

0.1 0.1 2 1.4 0.1 20.8 13,308 12,501 93.3

0.0 0.0 1 1.5 0.0 20.9 13,678 12,850 93.2

0.0 0.0 2 1.4 0.1 20.8 13,308 12,501 93.3

Nonachlorinated 

biphenyls

Heptachlorinated 

biphenyls

Octachlorinated 

biphenyls

Heptachlorinated 

biphenyls

Octachlorinated 

biphenyls

Decachlorinated 

biphenyls

Nonachlorinated 

biphenyls

Decachlorinated 

biphenyls
Primary Aluminum Testing: Exhaust flow rates, temperatures, and O2/CO2 contents

Parent company name: Noranda Aluminum, Inc. Facility address: 391 St. Jude Industrial Park

 New Madrid, MO 63869

Description of source tested: Paste Plant Stack

Moisture 

(%) CO2

 (%) O2 (%) Flow 

(acfm)

Flow 

(dscfm)

1 4/26/13 12:21 4/26/13 15:26 Methods 1-4 CARB 428/429 1.5 0.0 20.9 13,678 12,850

2 4/26/13 15:53 4/26/13 18:57 Methods 1-4 CARB 428/429 1.4 0.1 20.8 13,308 12,501

Test Start 

Date

Run 

Number

Simultaneous Exhaust Gas

with which 

pollutant test?

Test Method 

(e.g. Method 5)

Test End 

Time

Test End 

Date

Test Start 

Time
ark

Temp (°F)

93.2

93.3