# Brightwater, South, Vashon, and West Point Treatment Plants Alki, Carkeek, Elliott West, and MLK/Henderson CSO Storage
and Treatment Facilities



# Receiving Water Characterization Study

King County NPDES Monitoring Program



# Final Report

Prepared for the

King County Department of Natural Resources and Parks
Wastewater Treatment Division

and the

Washington State Department of Ecology

by the

King County Department of Natural Resources and Parks Marine and Sediment Assessment Group

June 2013

# Brightwater, South, Vashon, and West Point Treatment Plants Alki, Carkeek, Elliott West, and MLK/Henderson CSO Storage
and Treatment Facilities



# Receiving Water Characterization Study

King County NPDES Monitoring Program



# Final Report

Prepared by

Scott Mickelson, Senior Water Quality Project Manager
Marine and Sediment Assessment Group King County Department of Natural Resources and Parks 201 South Jackson Street, Suite 600 Seattle, Washington 98104

206

- 296

- 8247 scott.mickelson@kingcounty.gov

June 2013

# Table of Contents

1.0 Introduction 1

1.1 Study Design for Routine Water Quality Monitoring 1
1.1.1 Station KSBP01 3

1.1.2 Station LSNT01 3
1.1.3 Station LTED04 3
1.1.4 Station LTXQ01 4 1.1.5 Data Submission from Routine Monitoring 4 1.2 Study Design for New Water Quality Monitoring 4 1.3 Scope of Report 5 2.0 Sample Collection and Analysis 6 2.1 Sample Collection and Field Measurements 6 2.1.1 Stations KSBP01, LSNT01, and LTED04 6
2.1.2 Station LTXQ01 7 2.2 Laboratory Analysis 7
2.2.1 Trace Metals and Hardness 8 2.2.2 Fecal Coliform Bacteria 8 2.2.3 Conventional Water Quality Parameters 8 2.3 Data Quality Assessment and Data Reporting 9 3.0 Summary of Results 10
3.1 Station KSBP01 10 3.1.1 Fecal Coliform Bacteria 10 3.1.2 Conventional Water Quality Parameters 10
3.1.3 Trace Metals 11

3.2 Station LSNT01 12 3.2.1 Fecal Coliform Bacteria 12 3.2.2 Conventional Water Quality Parameters 12
3.2.3 Trace Metals 12 3.2.4 Alkalinity 13 3.2.5 Cyanide 1 4
3.3 Station LTED04 14 3.3.1 Fecal Coliform Bacteria 14 3.3.2 Conventional Water Quality Parameters 14
3.3.3 Trace Metals 14
3.4 Station LTXQ01 15 3.4.1 Fecal Coliform Bacteria 15 3.4.2 Conventional Water Quality Parameters 16
3.4.3 Trace Metals 16
3.4.4 Hardness 17
4.0 References 18 Appendix A

– Complete Analytical Results Appendix B

– Trace Metals Data Validation Memorandum

i

# 1.0 Introduction

This report presents results of a characterization study of ambient receiving waters in central Puget Sound, Elliott Bay, and the Duwamish River. King County conducted this study to fulfill one requirement of its National Pollutant Discharge Elimination System (NPDES) permits for
the Br ightwater Treatment Plant (WA0032247), South Treatment Plant (WA

- 002958

- 1), Vashon Treatment Plant (WA0022527), and West Point Treatment Plant and Al ki, Carkeek, Elliott West, and MLK/Henderson CSO Storage and Treatment Facilities (WA

- 002918

- 1), issued by the Washington State Department of Ecology (Ecology).

King County’s NPDES permits for the se treatment fa cilities require that “ . . . the Permittee must provide data via ambient monitoring stations or collect receiving water information via field sampling necessary to determine if the effluent has a reasonable potential to cause a violation of the water quality standards. If reasonable potential exis ts, Ecology will use this information to calculate effluent limits. Field sampling will be required where ambient monitoring station
data does not exist.” (Ecology 2009a,b ; 2011a,b )

.

A sampling and analysis plan (SAP) for this study (King County 2010) wa s submitted to Ecology in December 2010 and approved on December 21, 2010 (Ecology 2010)

. The original SAP was submitted to meet the permit requirements for the South and West Point T reatment P lants. Similar monitoring requirements were included in the s ubsequent NPDES permits for both the Brightwater and Vashon T reatment P lants issued in 2011 . The original, approved SAP was determined by Ecology to be applicable to the Vashon Treatment Plant receiving water monitoring requirement (Section S.9) during pe rmit negotiations. The SAP was also determined by Ecology to be applicable to the Brightwater Treatment Plant receiving water monitoring requirement (Section S.11) after a request from King County. Ecology forwarded a letter of approval to King County in September 2012 (Ecology 2012).

The study was designed to provide Ecology with a combination of data from the County’s ongoing water quality monitoring programs for conventional parameters and bacteria, along with a new, focused data gathering effort for trace metals, pH, cyanide, and alkalinity, which were additional analyses required by the NPDES permits.



## 1.1 Study Design for Ongoing Water Quality Monitoring As part of the SAP preparation process, King County worked with Ecology to select monitoring stations that were in the vicinity of treatment facility outfalls but outside the zone of influence of the effluent. The four stations shown in Figure 1 were sele cted to provide data from receiving waters in the vicinity of all four treatment plants as well as the four CSO storage and treatment facilities. Station KSBP01, located in the n orth ern Central Puget Sound Basin, was selected to represent ambient receivin g water in the vicinity of the Brightwater and West Point treatment plants and the Carkeek CSO treatment facility. Station LSNT01, located in the
southern Central Puget Sound Basin, was selected to represent ambient receiving water in the vicinity of the South and Vashon treatment plants and the Alki CSO treatment facility.

1

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### Station LTED04, located in Elliott Bay, was selected to represent ambient receiving water in the vicinity of the Elliot West CSO treatment facility. Station LTXQ01, located in the Duwamish River, was selected to represent ambient receiving water in the vicinity of the MLK/Henderson CSO treatment facility.

1 .1.1 Station KSBP01
Station KSBP01 is located in the northern Central Puget Sound Basin, approximately two miles
from the Brig htwater outfall s , six miles from the West Point outfall

, and two miles from the
Carkeek outfall (see Figure 1). The monitoring history for this station goes back to 1966 and, for certain parameters, it has been monitored continuously since 1988. King Cou nty currently samples this station on a monthly basis for in situ field measurement of temperature, dissolved oxygen, salinity, density, chlorophyll

- a fluorescence, and transmissivity

. These parameters are measured throughout the entire water column. Samples for laboratory analysis of fecal coliform and enterococcus bacteria, nutrients (ammonia, nitrate + nitrite nitrogen, total nitrogen, orthophosphorus, and silica, ), chlorophyll

- a and pheophytin, and total suspended
solids are collected are from spec ific depths . Nutrient and total suspended solids samples are collected from seven depths at this station

– 1, 15, 25, 35, 55, 100, and 200 meters. Chlorophyll

- a and pheophytin samples are collected from four depths

– 1, 15, 25, and 35

meters. Bacteria a nd total nitrogen samples are collected from a single depth

– 1 meter.

Beginning in 2008, this station has been sampled twice a month from March through October as part of the County’s marine phytoplankton monitoring program. Additional nutrient and
chlo rophyll

- a samples are collected from two depths during this second sampling event. The in

situ field measurements listed above are also collected for a portion of the water column.

1 .1.2 Station LSNT01
Station LSNT01 is located in the southern Central P uget Sound Basin, approximately five miles
from the South outfall

, five miles from the Vashon outfall, and three miles from the Alki outfall (see Figure 1). This station has been monitored continuously since 1988. King County currently samples this stati on on a monthly basis for in situ field measurement of temperature, dissolved oxygen, salinity, density, chlorophyll

- a fluorescence and transmissivity

. These parameters are measured throughout the entire water column. Samples for laboratory analysis of fe cal coliform and enterococcus bacteria, nutrients

, chlorophyll

- a and pheophytin, and total suspended solids are collected from specific depths . Nutrient and total suspended solids samples are collected from seven depths at this station

– 1, 15, 25, 35, 55 , 100, and 180 meters. Chlorophyll

- a and pheophytin samples are collected from four depths

– 1, 15, 25, and 35

meters. Bacteria and total nitrogen samples are collected from a single depth

– 1 meter.

1 .1.3 Station LTED04 Station LTED04 is located in Elliott Bay, approximately one mile from the Elliott West outfall (see Figure 1). This station has been monitored continuously since 1997. King County currently samples this station on a monthly basis for in situ field measur ement of temperature, dissolved oxygen, salinity, density, chlorophyll

- a fluorescence, and transmissivity . These parameters are measured throughout the entire water column. Samples for laboratory analysis of fecal

3

### coliform and enterococcus bacteria, nutr ients, chlorophyll

- a and pheophytin, and total suspended solids are collected from specific depths. N utrient and total suspended solids samples are collected from six depths at this station

– 1, 15, 25, 35, 55, and 75 meters. Chlorophyll

- a and pheophytin samples are collected from four depths

– 1, 15, 25, and 3 5
meters. Bacteria and total nitrogen samples are collected from a single depth

– 1 meter.

1 .1.4 Station LTXQ01 Station LTXQ01 is located in the Duwamish River, approximately 600 feet downstream of the MLK/Henderson outfall (see Figure 1 inset ). King County currently samples this station on a monthly basis for field measurement of temperature and dissolved oxygen and laboratory analysis of fecal coliform and enterococcus bacteria, nutrients salin ity, hardness, and total suspended solids. Samples are collected mid

- channel from a pedestrian bridge over the river

. Data have been collected at this station since May 2009.

1.1.5 Data Submission from Routine Monitoring Stations KSBP01, LSNT01, LTED04 , and LTXQ01 are sampled monthly as part of King County’s ongoing ambient monitoring program. The County is submitting to Ecology two years of monthly data from these stations, collected in 2011 and 2012, for total suspended solids, dissolved oxygen, temperature, fecal coliform bacteria, and salinity. Additionally, two years of hardness data are being submitted for Station LTXQ01

. The Vashon T reatment Plant permit also requires the submission of ammonia nitrogen data. Two years of ammonia nitrogen data are being submitted for Station LSNT01.



## 1 .2 Study Design for New Water Quality Monitoring The County’s NPDES permits also require d submittal of data for certain water quality parameters that have not been measured previously on a regular basis or have not been
measured within the last 10 years . These include d trace metals and pH for all sampling locations and weak acid dissociable cyanide and alkalinity for Station LSNT01 (South Treatment Plant receiving water)

.

King County collected a total of 12 samples over four sampling events from Stations KSBP01 and

LTED04 for analysis of total and dissolved metals

. A total of 16 samples (including on e field replicate per sampling event) were collected from Stations LSNT01 and LTXQ01. The four sampling events were timed to occur during a spring tide in December 2010, July 2011, December 2011, and July 2012. This timing met the requirements of all four permits . New sampling at Station LSNT01 also include d weak acid dissociable cyanide as required in the South Treatment Plant permit and alkalinity as required in the South and Vashon T reatment plant permit s

. Sixteen samples were collected and analyz ed for both of these parameters.

During each trace metals sampling event, samples were collected from three depths at Stations KSBP01, LSNT01, and LTED04

– 5 and 50 meters below the surface and a deeper depth, which

was dependent upon the total depth of t he station. Due to the shallow depth at Station LTXQ01 in the Duwamish River, trace metals samples were only collected from a single depth.

4

### Station LTXQ01 s amples were collected from a depth of approximately one meter below the
surface on each of three c onsecutive days during each sampling event.

Given the periodic excursion of the Duwamish River salt wedge into the area in which Station

LTX Q 01 is located, synoptic hardness and salinity data were also collected along with trace metals, to allow compariso n of metals data with appropriate water quality criteria. At the three offshore stations, pH was measured in situ during each monthly sampling event in 2011 in a

continu ous surface to bottom profile. At Station LTXQ01, pH was measured in the field each

t ime samples were collected for analysis of trace metals.



## 1.3 Scope of Report This report presents the methodologies employed to collect samples, gather field measurements, and perform laboratory analysis on the samples. Also presented is an

assessment o f overall data quality. A summary of the resulting water quality data is presented, providing minimum and maximum values detected for each of the water quality constituents reported , along with mean and median values and standard deviations, when appropriate. Complete analytical results for all reported paramete rs are included as Appendix A to this report and a data validation memorandum for all trace metals results is included as Appendix B. Although a large number of conventional parameters ar e routinely collected at the four monitoring stations, this report provides data only for those conventional parameters required in the four NPDES permits

– ammonia nitrogen, dissolved oxygen, pH, salinity, and total suspended solids

.

5

# 2.0 Sample Collecti on and Analysis

This section describes methodologies that were employed during the receiving water characterization study for collection of samples, field measurements, and laboratory analysis. Also included are a description of how data quality was veri fied and validated and how data have been reported.



## 2.1 Sample Collection and Field Measurements Sample collection and in situ field measurements at offshore S tations KSBP01, LSNT01, and LTED04 were accomplished both during routine monthly water column profiling and sampling events as well as the four focused sampling events for trace metals and other required water quality constituents. These sampling events w ere conducted aboard King County’s research
vessel Liberty and are described in Section 2.1.1. Due to the shallow depths and dynamic
nature of the Duwamish River at S tation LTXQ01, samples from this location, along with field measurements, were collected using alternative methods described in Section 2.1.2.

2.1.1 Stations KSBP01, LSNT01, and LTED04

In situ water column profiles were conducted at the three offshore stations both during routine monthly sampling as well as during the four focused sampling e vents. These measurements
were collected in continuous surface to near

- bottom water column profiles using a conductivity/temperature/depth (CTD) datalogger. The SBE 25 SEALOGGER  

### CTD, manufactured by SeaBird Electronics of Bellevue, Washington, is a prof iling system for lake, coastal, estuarine, and deep water work. In addition to measuring conductivity, temperature, and depth, the instrument also measures dissolved oxygen, chlorophyll, light intensity, turbidity, and pH. Direct measurements are also u sed to calculate salinity and density.

The CTD is deployed from the Liberty by hydraulic winch and allowed to equilibrate to surface conditions for approximately five minutes before data recording begins. The CTD is lowered at a specified descent rate fr om the surface to approximately five meters above the sea floor (downcast). Data are recorded both on the down cast and during the instrument's return to the surface (upcast). Data are recorded to a datalogger at a frequency of eight hertz or eight

reco rdings per second. These data are then averaged or “binned” to half

- meter intervals.

Upon retrieval of the instrument, field measurement data are uploaded to a laptop computer from the datalogger prior to the next cast. System software converts paramete r data into
surface

- to

- depth plots which are field

- reviewed for quality control.

Samples for analysis of total suspended solids and fecal coliform bacteria were collected using Niskin sample bottles deployed on the CTD "rosette." Predetermined samplin g depths were programmed into the CTD and the instrument deployed as described in the previous paragraphs. Analytical samples were collected on the upcast of the CTD. Upon retrieval of the CTD, sample aliquots were transferred from the Niskin bottles int o sample containers.

6

### During the four focused sampling events for the collection of trace metals samples, sampling procedures followed the "clean hands/dirty hands" technique outlined in EPA Method 1669 (EPA 1995). Before arriving at the initial sampling site, sampling personnel were designated "clean hands," "dirty hands," and "crane operator." "Clean hands" handle d all operations

invo lving contact with the sample container and transfer of the sample from the sampling device to the sample container. "Dirty hands" was responsible for preparation of the sampling
device and for all other activities that did not involve direct contact with the sample. "Crane operator" was responsible for setup and operation of the clean winch system along with backup "dirty hands" responsibilities.

All sampling equipment was non

- metallic and, prior to each sampling event, a pre

- deployment equipment blank was collected and all sampling equipment was double

- bagged in zippered, plastic bags. Samples wer e collected using Niskin

- X bottles attached to a synthetic hydroline. A specialized, non

- contaminating winch system mounted on the rear deck of the Liberty

c ontrol led the hydroline. The Niskin

- X bottles were attached to the hydroline and lowered to the specified sampling depth. A "messenger" was released down the hydroline to trip the
bottles. The Niskin

- X bottles were then brought up and samples dispensed into sample containers immediately upon coming out of the water and while still attached to the hydroline. Sample containers were then double

- bagged and stored in ice

- filled coolers until delivery to the King County Environmental Laboratory. Other field blanks collected during the trace metals sampling events included atmosphere blanks and trip blanks.

2. 1 .2 Station LTXQ01 Due to logistics at sampling S tation LTXQ01, routine monthly water samples were collected from a bridge over the Duwamish River . Samples were collected from center channel, using a modified, van Dorn

- style sampling device deployed on a sampling line from the bridge. Upon retrieval of the sampling device, sample aliquots were collected for laboratory analysis of bacteria, total s uspended solids, salinity, and hardness. Field measurements for temperature, dissolved oxygen, and pH were performed ex situ . A separate aliquot of sample was placed into a measurement cup, in which the field measurements were performed as soon as possib le after sample collection. Field measurement of temperature, dissolved oxygen, and pH employed a Hydrolab  

### multi

- probe field meter

.

Sample collection for trace metals at Station LTXQ01 was also accomplished following EPA Method 1669. Samples were colle cted at this station by lowering a single

- use Teflon bailer attached to a clean rope from a bridge above the river. Two sampling staff, designated “clean hands” and “dirty hands” accomplished all sampling. An additional aliquot of water was collected usi ng the modified van Doren

- style bottle for laboratory analysis of salinity and hardness as well as field measurement of dissolved oxygen, pH, and temperature.



## 2.2 Laboratory Analysis Laboratory analyses performed during this study included total and diss olved trace metals, hardness, fecal coliform bacteria, alkalinity, cyanide, total suspended solids , and salinity (for

7

### samples collected from station LTXQ01) . All analyses were performed by the King County Environmental Laboratory.

2.2. 1 Trace Metals and Hardness Total and dissolved mercury analysis was performed according to EPA Method 1631E (EPA

2002 ), which is by cold vapor atomic fluorescence spectrometry (CVAF) following a 12

- hour sample digestion.

Other t otal and dissolved metals were analyzed according to EPA Method 1640 (EPA 1 997 )

, which is by inductively coupled plasma mass spectrometry (ICPMS), with on

- line preconcentration

.

Determination of h ardness was performed according to Standard Method ( SM ) 2340B (APHA 1998), which is a calc ulation based upon separately determined total calcium and total magnesium concentrations. Calcium and magnesium were analyzed by ICPMS according to EPA Method 200.8r5.4 (EPA 1994)

.

2.2.2 Fecal Coliform Bacteria Fecal coliform bacteria analysis was pe rformed by membrane filtration according to SM9222D (APHA 1998). Appropriate dilutions, if necessary, were prepared and the sample and its dilutions were filtered through a sterile 0.45 μ m nitrocellulose membrane. The membrane was then applied to an mFC agar plate. After incubation at 44.5 o 

### C for approximately 24 hours, all colonies with a characteristic blue color were counted. The number of colonies per 100 mL of sample was calculated based on the colonies counted and the dilutions used per plate.

2.2

. 3 Conventional Water Quality Parameters Alkalinity analysis was performed according to SM2320B (APHA 1998) , in which the sample is titrated using a standard acid to a pH of 4.5. The volume of titrant needed to reach the pH endpoint is then used to calcu late the total alkalinity of the sample.

Cyanide analysis was performed according to SM4500CN

- I,E (APHA 1998), which is for determination of weak acid dissociable cyanide. The cyanide concentration is determined through a buffered, weak

- acid distillation followed by a colorometric measurement

.

Salinity analysis was performed acc ording to SM 2520B (APHA 1998), in which s alinity is determined by measuring the conductance of an electrical current through the salt water sample kept at constant temperature of 25 ° C and comparing the measurement to the conductivity of a standard sea water or reference potassium chloride solution.

Total suspended solids analysis was performed according to SM2540D (APHA 1998), in which a measured volume of a well

- mixed water sample is filtered through a 934AH glass fiber filter. The residue retained on the glass fiber filter is dried to a constant weight at 103 to 105 ° C. The resulting net weight represents the total suspended solids.

8

## 2.3 Data Quality Assessment and Data Reporting All laboratory analytical data and some field measurements generated during this study were
entered into King County’s Laboratory Information Management System (LIMS). Field data,
such as in situ data mea surements or recorded environmental observations, were routinely re

checked by a second field scientist prior to entry into LIMS. Laboratory analytical data were reviewed, first by the primary analyst and then by a senior peer reviewer, prior to entry of the data into LIMS. Analytical data were reviewed for completeness and quality control ( QC ) sample data were rev iewed for compliance with project and method QC requirements.

The King County laboratory project manager (LPM) for the receiving water chara cterization study provide d the next data review step, at a “per

- sampling

- event” level. The LPM verif ied the completeness of the data set and report ed any QC failures or anomalies. Upon completion of all sampling and analysis, the project manager (study l ead) provide d a final data validation process of all data to ensure t hat they met the project data quality objective s.

Section 3.0 of this report provides a brief summary of data generated during the 24

- month monitoring period of 2011 and 2012 from King County’s ongoing ambient monitoring program. This section also provides a summary of data collected during the four focused sampling events
for trace metals and oth er required parameters. Appendix A includes data for the four sampling stations in Tables A

- 1 through A

- 4. These data include both laboratory

- analyzed parameters as well as those parameters collected via CTD at the discrete depths at which other

water sa mples were collected for laboratory analysis. Appendix B includes the data validation memorandum for trace metals data. Formal data validation of the trace metals was performed following guidance outlined in the USEPA’s National Functional Guidelines for Inorganic Superfund Data Review (EPA 2010).

Collection of CTD data binned at 0.5

- meter depth intervals generates a very large data set for each sampling event and precludes inclusion of these data on LIMS. Some CTD data that have been averaged at discre te depths are maintained on LIMS, however, complete CTD data are maintained in a separate web

- accessible database. These additional CTD data may be found
and downloaded at the County’s website ht tp://green.kingcounty.gov/marine/CTD.aspx

.

All reported data generated during this study and included in this report have been uploaded to Ecology’s Environmental Inform ation Management (EIM) database. Data from this study may
be found on EIM under the Study ID code KC_Rec_Water_Char

.

9

# 3.0 Summary of Results

This section provides a summary of laboratory analytical results and field measurements for bacteria and conventional parameters from King County’s ongoing ambient water quality monitoring program during the 24

- month period of 2011 and 2012

, as well as the four focused sampling events for trace metals and other required parameters. Tables in each sub

- section provide the minimum and maximum detected or measur ed values, as well as means, medians, and standard deviations, when appropriate. Complete results for those parameters submitted
to EIM from each of the four monitoring stations may be found in Tables A

- 1 through A

- 4, included as Appendix A to this docume nt.



## 3.1 Station KSBP01
King County’s long

- term monitoring S tation KSBP01 was chosen to represent ambient receiving

water conditions for the West Point and Brightwater wastewater treatment plants and the
Carkeek CSO treatment facility.

3.1.1 Fecal Coliform Bacteria During the 24

- month sampling period from January 2011 through December 2012, fecal coliform bacteria were detected in 3 out of 24 samples. One sample had a bacteria count of 4 colony forming units per 100 milliliters (CFU/100 ml) and the other two samples had counts of 1 CFU/100 ml each. The calculated fecal coliform bacteria geometric mean for the 24

- month sampling period is 1 CFU/100 ml.

3.1.2 Conventional Water Quality Parameters
Table 3

- 1 presents a summary of data for conventional water quality parameters collected monthly from Station KSBP01 during 2011 and 2012. These data

– a combination of in situ measurement (dissolved oxygen, pH, salinity, and temperature) and laboratory analys i s (total suspended solids)

– were collected fro m seven discrete sampling depths; 1, 15, 25, 35, 55, 100,
and 198 meters below the surface during each of the sampling events . The numbers of data points on which the presented metrics were calculated (n) are noted in the “Parameter”
column. Note that pH was measured only during the 12

- month period during 2011.

Please note that these metrics are for pooled data collected over several depths throughout the water column and are presented for summary purposes only. When more

- thoroughly analyzing these data, sample depth should be taken into consideration to account for spatial (vertical) and temporal vari ations due to freshwater runoff, intrusion of deep oceanic waters into Puget
Sound , and seasonal variations in temperature

. Due to the variable nature, both spatial and temporal, of parameters such as dissolved oxy gen and temperature, the reporting of a mean value and calculated standard deviation are not particularly helpful for data assessment. For these two parameters, only the minimum, maximum, and median values are reported.

10

## Table 3

- 1 Summary of Conventiona l Water Quality Parameters at Monitoring Station KSBP01

Parameter Min Max Mean Median StDev DO (mg/L) n = 254 5.6 12.9

-- 8.0

-- pH (unitless) n = 108 7.5 8.0 7.7 7.7 0.1 Salinity (PSS) n = 262 26.061 30.719 29.175 29.431 0.932 Temperature ( o 

### C) n = 262 7.177 13.951

-- 9.933

-- TSS (mg/L) n = 128 0.6 7.0 2.4 2.1 1.4



### 3.1.3 Trace Metals
Table 3

- 2 presents a summary of trace metals data for the 12 samples collected from Station KSBP01 in July and December of 2011 and 2012. The trace metals samples were collected from three depths during each of the four sampling event s ; 5, 50, and 198 meters below the surface.



## Table 3

- 2

Total and Dissolv ed Trace Metal Concentrations

at Monitoring Station KSBP01 Based on 12 Samples

Metal (μg/L) Min Max Mean Median StDev Arsenic, Total 1.11 1.41 1.29 1.33 0.10 Arsenic, Dissolved 1.15 1.43 1.33 1.37 0.09 Cadmium, Total 0.0636 0.0864 0.0732 0.0715 0.0064 Cadmium, Dissolved 0.0520 0.0734 0.0664 0.0693 0.0068 Chromium, Total 0.096 0.377 0.144 0.110 0.079 Chromium, Dissolved 0.092 0.150 0.114 0.110 0.020 Copper, Total 0.314 1.220 0.437 0.373 0.249 Copper, Dissolved 0.234 0.617 0.322 0.308 0.104 Lead, Total 0.007 0.046 0.020 0.014 0.015 Lead, Dissolved a



### -- -- -- -- -- Mercury, Total b 

### 0.00020 0.00055 0.00030 0.00026 0.00012 Mercury, Dissolved c



### -- -- -- -- -- Nickel, Total 0.400 0.593 0.435 0.423 0.051 Nickel, Dissolved 0.387 0.443 0.408 0.407 0.016 Silver, Total d 

### 0.016 0.030

-- -- -- Silver, Dissolved d 

### 0.019 0.029

-- -- -- Zinc, Total 0.330 0.890 0.513 0.475 0.152 Zinc, Dissolved 0.170 0.694 0.438 0.417 0.187

a Dissolved lead was detected in 1 out of 12 samples at a concentration of 0.010 μg/L. The method detection limit for dissolved lead was 0.005 μg/L.

b Total mercury was detected in 9 out of 12 samples. The minimum value for total mercury represents the lowest detected value. The method detection limit of 0.00020 μg/L was used as the value o f the 3 undetected samples when computing the mean, median, and standard deviation.

c Dissolved mercury was not detected in any of the 12 samples at a method detection limit of 0.00020 μg/L.

d Total and dissolved silver were detected in 6 out of 12 samples. The minimum value s for total and dissolved silver
represent the lowest detected value. The method detection limit for silver was 0.010 μg/L. Due to the low number of detections, meaningful mean and median values cannot be presented.

11

### Please note that, for arsenic and silver data, the detected dissolved concentrations were occasionally greater than the detected total concentrations. When the data were pooled, this resulted in the summary metrics being slightly greater for the dissolved concentrations th an the total concentrations. Both of these metals appear to be present in the marine environment largely in the dissolved fraction. The slight differences between detected total and dissolved concentrations are well within analytical precision.



## 3. 2 Sta tion LSNT01
King County’s long

- term monitoring S tation LSNT01 was chosen to represent ambient receiving water conditions for the South and Vashon wastewater treatment plants and the Alki CSO treatment facility.

3. 2 .1 Fecal Coliform Bacteria During the 24

- month sampling period from January 2011 through December 2012, fecal
coliform bacteria were detected in 2 out of 24 samples , both with a count of 1 CFU/100 ml each. The calculated fecal coliform bacteria geometric mean for the 24

- month sampling period is 1 CFU/100 ml.

3. 2

. 2 Conventional Water Quality Parameters
Table 3

- 3 presents a summary of data for conventional water quality parameters collected monthly from Station LSNT01 during 2011 and 2012. These data were collected from seven discrete sampling depths; 1, 15, 25, 35, 55, 100, and 1 58 meters below the surface during each of the sampling events. The numbers of data points on which the presented metrics were calculated ( n) are noted in the “Parameter” column. Note that pH was measured only during
the 12

- month period during 2011.



## Table 3

- 3 Summary of Conventional Water Quality Parameters at Monitoring Station LSNT01

Parameter Min Max Mean Median StDev

Ammonia a 

### (mg/L) n = 191 0.0051 0.0853 0.0188 0.0051 0.0207 DO (mg/L) n = 200 5.3 12.1

-- 7.5

-- pH (unitless) n = 1 12 7.4 8.0 7.6 7.7 0.1 Salinity (PSS) n = 208 27.705 30.713 29.487 29.537 0.557 Temperature ( o 

### C) n = 208 7.5 12.7

-- 9.8

-- TSS (mg/L) n = 131 0.6 7.5 2.4 2.2 1.4

a Ammonia was detected in 97 out of 191 samples. The minimum value for ammonia represents the lowest detected value. The method detection limit of 0.0050 mg/L was used for the value of the undetected sample when computing the mean, median, and standard dev iation. Note that this large number of non

- detected results

causes a skewed median value and a large standard deviation.



### 3. 2

. 3 Trace Metals
Table 3

- 4 presents a summary of trace metals data for the 1 6 samples collected from Station

LSNT01 in July and December of 2011 and 2012. The trace metals samples were collected from

12

### three depths during each of the four sampling events; 5, 50, and 1 5 8 meters below the surface.
The 158

- meter depth samples were collected in duplicate during each sampli ng event.



## Table 3

- 4

Total and Dissolved Trace Metal Concentrations

A t Monitoring Station LSNT01 Based on 1 6 Samples Metal (μg/L) Min Max Mean Median StDev Antimony, Total 0.157 0.183 0.168 0.166 0.008 Antimony, Dissolved 0.143 0.173 0.159 0.158 0.011 Arsenic, Total 1.22 1.49 1.39 1.41 0.07 Arsenic, Dissolved 1.22 1.46 1.37 1.40 0.08 Cadmium, Total 0.0611 0.0830 0.0736 0.0735 0.0057 Cadmium, Dissolved 0.0618 0.0749 0.0699 0.0708 0.0037 Chromium, Total 0.088 0.160 0.120 0.115 0.022 Chromium, Dissolved 0.088 0.180 0.112 0.100 0.026 Copper, Total 0.260 1.99 0.451 0.352 0.413 Copper, Dissolved 0.231 0.387 0.299 0.287 0.046 Lead, Total a 

### 0.014 0.049 0.026 0.024 0.012 Lead, Dissolved b



### -- -- -- -- -- Mercury, Total c 

### 0.00023 0.00040 0.00027 0.00026 0.00007 Mercury, Dissolved d



### -- -- -- -- -- Nickel, Total 0.402 0.511 0.436 0.427 0.030 Nickel, Dissolved 0.390 0.430 0.411 0.412 0.014 Silver, Total e 

### 0.016 0.030

-- -- -- Silver, Dissolved e 

### 0.011 0.027

-- -- -- Zinc, Total 0.400 0.647 0.482 0.470 0.063 Zinc, Dissolved 0.270 0.707 0.447 0.395 0.137

a Total lead was detected in 15 out of 16 samples. The minimum value for total lead represents the lowest detected value. The method detection limit of 0.0050 μg/L was used for the value of the undetected sample when computing the mean, median, and standard deviation.

b Dissolved lead was detected in 2 out of 16 samples at concentration s of 0.0 063 and 0.0077 μg/L.

c Total mercury was detected in 12 out of 16 samples. The minimum value for total mercury represents the lowest detected value. The method detection limit of 0.00020 μg/L was used for the value of th e 4 undetected samples when computing the mean, median, and standard deviation.

d Dissolved mercury was detected in 1 of 16 samples at a concentration of 0.0002 3 μg/L.

e Total and dissolved silver were detected in 8 out of 16 samples and 9 out of 1 6 samples, respectively . The minimum values for total and dissolved silver represent the lowest detected value s

. The method detection limit
for silver was 0.010 μg/L. Due to the low number of detections, meaningful mean and median values cannot be presented.



### 3.2

. 4 Alkalinity Alkalinity samples were collected from the same three depths at Station LSNT01 during the four trace metals sampling events. Total alkalinity values in the 16 samples ranged from 97 to 103 milligrams of calcium carbonate per liter (mg CaCO 3 

### /L), with mean and median values of 100 and 101 mg CaCO 3 

### /L, respectively, and a standard deviation of 2 mg CaCO 3 

### /L.

13

### 3.2. 5 Cyanide Cyanide (weak acid dissociable) samples were collected from the same three depths at Station LSNT01 during the four trace m etals sampling events. Cyanide was not detected in any of the 16 samples at a method detection limit of 0.005 mg/L.



## 3.3 Station LTED04
King County’s long

- term monitoring S tation LTED04 was chosen to represent ambient receiving
water conditions for the E lliott West CSO treatment facility.

3.3.1 Fecal Coliform Bacteria During the 24

- month sampling period from January 2011 through December 2012, fecal
coliform bacteria were detected in 12 out of 24 samples, with counts ranging from 1 to 29 CFU/100 ml. The calculated fecal coliform bacteria geometric mean for the 24

- month sampling period is 2 CFU/100 ml.

3.3.2 Conventional Water Quality Parameters
Table 3

- 5 presents a summary of data for conventional water quality parameters collected monthly from Station LTED04 during 2011 and 2012. These data were collected from six discrete sampling depths; 1, 15, 25, 35, 55, and 75 meters below the surface during each o f the sampling events. The numbers of data points on which the presented metrics were calculated (n) are noted in the “Parameter” column. Note that pH was measured only during the 12

- month period during 2011.



## Table 3

- 5 Summary of Conventional Water Qual ity Parameters at Monitoring Station LTED04

Parameter Min Max Mean Median StDev DO (mg/L) n = 150 4.9 11.0

-- 7.7

-- pH (unitless) n = 84 7.4 8.0 7.6 7.6 0.1 Salinity (PSS) n = 156 23.982 30.443 29.136 29.282 0.923 Temperature ( o 

### C) n = 156 7.5 13.4

-- 9.9

-- TSS (mg/L) n = 102 0.5 8.1 2.7 2.3 1.8



### 3.3.3 Trace Metals
Table 3

- 6 presents a summary of trace metals data for the 1 2 samples collected from Station

LTED04 in July and December of 2011 and 2012. The trace metals samples were collected from three depths during each of the four sampling events; 5, 50, and 75 meters below the surface.

14

## Table 3

- 6

Total and Dissolved Trace Metal Concentrations

a t Monito ring Station L TED04 Based on 1 2 Samples Metal (μg/L) Min Max Mean Median StDev Arsenic, Total 1.14 1.45 1.31 1.33 0.10 Arsenic, Dissolved 1.12 1.39 1.31 1.35 0.08 Cadmium, Total 0.0552 0.0799 0.0716 0.0735 0.0070 Cadmium, Dissolved 0.0610 0.0763 0.0682 0.0684 0.0047 Chromium, Total 0.077 0.180 0.114 0.105 0.033 Chromium, Dissolved 0.085 0.140 0.108 0.100 0.019 Copper, Total 0.301 0.815 0.485 0.483 0.161 Copper, Dissolved 0.277 0.635 0.374 0.316 0.109 Lead, Total a 

### 0.010 0.084 0.035 0.025 0.025 Lead, Dissolved b



### -- -- -- -- -- Mercury, Total c 

### 0.00020 0.00052 0.00028 0.00024 0.00010 Mercury, Dissolved d



### -- -- -- -- -- Nickel, Total 0.393 0.501 0.425 0.414 0.031 Nickel, Dissolved 0.383 0.436 0.410 0.407 0.018 Silver, Total e 

### 0.016 0.033

-- -- -- Silver, Dissolved e 

### 0.019 0.028

-- -- -- Zinc, Total 0.350 1.01 0.652 0.583 0.216 Zinc, Dissolved 0.300 1.02 0.611 0.577 0.260

a Total lead was detected in 1 1 out of 1 2 samples. The minimum value for total lead represents the lowest detected value. The method detection limit of 0.0050 μg/L was used for the value of the undetected sample when computing the mean, median, and standard deviation.

b Dissolved lead was detected in 1 out of 1 2 samples at a c oncentration of 0.0052 μg/L.

c Total mercury was detected in 1 0 out of 1 2 samples. The minimum value for total mercury represents the lowest detected value. The method detection limit of 0.00020 μg/L was used for the value of the 2 undetected samples
wh en computing the mean, median, and standard deviation.

d Dissolved mercury was not detected in any of the 12 samples at a method detection limit of 0.0002 0 μg/L.

e Total and dissolved silver were detected in 6 out of 12 samples. The minimum values for total and dissolved silver represent the lowest detected value s

. The method detection limit for silver was 0.010 μg/L. Due to the low number of detections, meaningful mean and median values cannot be presented.



## 3. 4 Station LTXQ01
King County’s long

- term monitoring S tation LTXQ01 was chosen to represent ambient receiving water conditions for the Henderson/MLK CSO treatment facility. The county routinely samples this station on a monthly basis,. Discrete wate r samples are collected from a single depth at
this shallow Duwamish River station.

3. 4 .1 Fecal Coliform Bacteria During the 24

- month sampling period from January 2011 through December 2012, fecal
coliform bacteria were detected in all 24 samples

. Bac teria counts in the 24 samples ranged
from 5 CFU/100 ml to greater than 600 CFU/100 ml . The calculated fecal coliform bacteria geometric mean for the 24

- month sampling period is 33 CFU/100 ml. Please note that the sample which returned a bacteria count of “greater than 600 CFU/100 ml” had an unexpectedly

15

### high bacteria count which, analytically, made it impossible to determine a more

- precise bacteria count. In calculating the geometric mean fo r this data set, a bacteria count of 600 CFU/100 ml was used for this sample.

3. 4 .2 Conventional Water Quality Parameters
Table 3

- 7 presents a summary of data for conventional water quality parameters collected monthly from Station LTXQ01 during 2011 and 2012. These data

– a combination of ex situ field measurements (dissolved oxygen, pH, and temperature) and laboratory analyses (total suspended solids and salinity )

– were collected from a single depth (between 0.5 and 1 meter ) during each of the samplin g events. The table provides the minimum and maximum concentrations measured or detected, along with calculated means, medians, and standard deviations. The numbers of data points on which these metrics were calculated (n) are noted in
the “Parameter” co lumn. Field measurement of pH was collected only during the trace metals sampling events and salinity samples were collected both monthly and during the trace metals sampling events.

Please note that these metrics are presented for summary purposes only. The location of this sampling station is in a dynamic portion of the Duwamish River with varying seasonal
freshwater flows and diurnal tidal excursions of the salt wedge

. These factors cause wide variations in parameters such a s salinity and total suspended solids , as well as dissolved oxygen

. The shallow overall depth of the river at this sampling station, coupled with the sampling depth (0.5 to 1 meter), also leads to wide seasonal variations in temperature.



## Table 3

- 7 Summary of Conventional Water Quality Parameters at Monitoring Station LTXQ01

Parameter Min Max Mean Median StDev Dissolved Oxygen (mg/L) n = 24 6.5 12.2

-- 10.1

-- pH (unitless) n = 16 6.9 7.3 7.1 7.1 0.1 Salinity a 

### (PSS) n = 40 2.33 29.65

-- -- -- Temperature ( o 

### C) n = 24 5.1 18.7

-- 9.4

-- Total Suspended Solids (mg/L) n = 22 2.5 116

-- 10.4

--

a Salinity was detectable in 15 out of 40 samples. The minimum value for salinity represents the lowest detected
value. The method detection limit was 2.00 PSS . Due to the low number of detections, meaningful mean and median values cannot be presented.



### 3. 4 .3 Trace Metals
Table 3

- 8 presents a summary of trace metals data for the 1 6 samples collected from Station
LTXQ01 in July and December of 2011 and 2012. The trace metals samples were collected from a single depth during each of the four sampling events ; with samples collected on three consecutive days. Including a field replicate during each sampling event, a total of 16 samples
were collected for trace metals analysis.

16

## Table 3

- 8

Total and Disso lved Trace Metal Concentrations

a t Monitoring Station LTXQ01 Based on 16 Samples Metal (μg/L) Min Max Mean Median StDev Arsenic, Total 0.474 0.857 0.628 0.618 0.121 Arsenic, Dissolved 0.391 0.577 0.456 0.440 0.062 Cadmium, Total a 

### 0.005 0.023 0.011 0.010 0.006 Cadmium, Dissolved b 

### 0.007 0.022 0.009 0.005 0.007 Chromium, Total 0.11 0.22 0.17 0.18 0.03 Chromium, Dissolved c 

### 0.06 0.11 0.07 0.07 0.01 Copper, Total 0.613 1.370 0.904 0.892 0.222 Copper, Dissolved 0.306 0.637 0.440 0.448 0.093 Lead, Total 0.048 0.327 0.136 0.112 0.084 Lead, Dissolved d 

### 0.009 0.029 0.016 0.017 0.008 Mercury, Total 0.00056 0.00199 0.00123 0.00127 0.00042 Mercury, Dissolved 0.00024 0.00088 0.00046 0.00035 0.00020 Nickel, Total 0.242 1.020 0.540 0.421 0.258 Nickel, Dissolved 0.156 1.090 0.418 0.263 0.332 Silver, Total e 

### 0.010 0.052 0.020 0.013 0.015 Silver, Dissolved e 

### 0.017 0.022 0.013 0.010 0.005 Zinc, Total 0.711 2.160 1.284 1.280 0.372 Zinc, Dissolved 0.460 1.270 0.774 0.721 0.254

a Total cadmium was detected in 15 out of 16 samples. The minimum value for total cadmium represents the lowest detected value. The method detection limit of 0.0050 μg/L was used for the value of the undetected sample when computing the mean, median, and standard deviation.

b Dissolved cadmium was detected in 7 out of 16 samples

. The minimum v alue for dissolved cadmium represents the lowest detected value. The method detection limit of 0.0050 μg/L was used for the value of the undetected samples when computing the mean, median, and standard deviation.

c Dissolved chromium was detected in 15 out of 16 samples. The minimum value for dissolved chromium represents the lowest detected value. The method detection limit of 0.050 μg/L was used for the value of the undetected sample when computing the mean, median, and standard deviation.

d Dissolved l ead was detected in 13 out of 16 samples. The minimum value for dissolved lead represents the lowest detected value. The method detection limit of 0.0050 μg/L was used for the value of the undetected samples when computing the mean, median, and standard d eviation.

e Total and dissolved silver were detected in 14 out of 16 samples and 4 out of 16 samples, respectively. The minimum values for total and dissolved silver represent the lowest detected values. The method detection limit of 0.010 μg/L was used f or the value of the undetected samples when computing the mean, median, and standard
deviation for total silver

. Due to the low number of detections, meaningful mean and median values cannot be presented for dissolved silver.



### 3.4. 4 Hardness

Har dness was also measured monthly, as well as the in trace metals samples collected from Station LTXQ01. Hardness values in these 40 samples ranged from 25.6 to 3,000 milligrams of calcium carbonate per liter (mg CaCO 3 

### /L) with mean and median values of 384 and 83 mg

CaCO 3 

### /L. This wide range of values produced a large calculated standard deviation of 635 mg

CaCO 3 

### /L. The wide range of hardness values correspond with associated wide ranges of salinity in the samples (see Appendix A).

17

# 4.0 References

APHA 1998

. Standard Methods for the Examination of Water and Wastewater, 20 th 

### Edition. American Public Health Association. Washington, D.C.

Ecology 2009a. National Pollutant Discharge Elimination System Waste Discharge permit No.

WA

- 002958

- 1 . Washington State Department of Ecology. Olympia, WA.

Ecology 2009b. National Pollutant Discharge Elimination System Waste Discharge permit No.

WA

- 002918

- 1 . Washington State Department of Ecology. Olympia, WA.

Ecology 2010. Interagency communication approving sampling and analysis plan (December 21, 2010) . Washington State Department of Ecology. Bellevue, WA.

Ecology 2011a. National Pollutant Discharge Elimination System Waste Discharge permit No.

WA0032247 . Washington State Department of Ecology. Olympia , WA.

Ecology 2011b. National Pollutant Discharge Elimination System Waste Discharge permit No.

WA0022527 . Washington State Department of Ecology. Olympia, WA.

Ecology 2012. Interagency communication approving sampling and analysis plan (September 5, 2012) . Washington State Department of Ecology. Bellevue, WA.

EPA 1994. Method 200.8

– Determination of Trace Elements in Waters and Wastes by Inductively Coupled Plasma Mass Spectrometry (Revision 5.4) . United States Environmental Protection Agency O ffice of Research and Development. Cincinnati, OH.

EPA 1995. Method 1669: Sampling Ambient Water for Trace Metals at EPA Water Quality
Criteria Levels EPA

- R

- 95

- 034 (April 1995 Draft). United States Environmental Protection Agency Office of Water. W ashington, DC.

EPA 1997. Method 1640: Determination of Trace Elements in Water by Preconcentration and Inductively Coupled Plasma

– Mass Spectrometry. United States Environmental Protection Agency Office of Water. Washington, DC.

EPA 2002. Method 163 1, Revision E: Mercury in Water by Oxidation, Purge and Trap, and Cold Vapor Atomic Fluorescence Spectrometry

. United States Environmental Protection Agency Office of Water. Washington, DC.

EPA 2010. USEPA Contract Laboratory Program National Functional Guidelines for Superfund Inorganic Data Review . OSWER 9240.1

- 51, USEPA

- 540

- R

- 10

- 011. United States Environmental Protection Agency. Washington, D.C.

King County 2010. Receiving Water Characterization Study, King County NPDES Mo nitoring Program, Final Sampling and Analysis Plan and Quality Assurance Project Plan . King County Department of Natural Resources and Parks. Seattle, WA.

18

# Appendix A Complete Analytical ResultsPage 1 of 25 

## Table A-1
Complete Water Quality Monitoring Data for Station KSBP01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 01/18/11 L52381-6 1.2 Fecal Coliform CFU/100ml <MDL 1 02/22/11 L52539-6 0.96 Fecal Coliform CFU/100ml <MDL 1 03/21/11 L52727-6 1.5 Fecal Coliform CFU/100ml <MDL 1 04/18/11 L52883-6 1.9 Fecal Coliform CFU/100ml <MDL 1 05/16/11 L53206-6 1.5 Fecal Coliform CFU/100ml <MDL 1 06/20/11 L53331-6 1.3 Fecal Coliform CFU/100ml <MDL 1 07/18/11 L53542-6 1.2 Fecal Coliform CFU/100ml <MDL 1 08/15/11 L53889-6 1.3 Fecal Coliform CFU/100ml <MDL 1 09/19/11 L54019-6 1.2 Fecal Coliform CFU/100ml <MDL 1 10/17/11 L54269-6 1.1 Fecal Coliform CFU/100ml <MDL 1 11/28/11 L54474-6 1.6 Fecal Coliform CFU/100ml <MDL 1 12/19/11 L54766-6 1 Fecal Coliform CFU/100ml <MDL 1 01/23/12 L54840-6 1.2 Fecal Coliform 4 CFU/100ml 1 02/21/12 L55087-6 1.2 Fecal Coliform CFU/100ml <MDL 1 03/19/12 L55193-6 2.8 Fecal Coliform CFU/100ml <MDL 1 04/16/12 L55370-6 1.3 Fecal Coliform CFU/100ml <MDL 1 05/21/12 L55534-6 1.6 Fecal Coliform CFU/100ml <MDL 1 06/18/12 L55788-6 1.3 Fecal Coliform CFU/100ml <MDL 1 07/16/12 L55944-6 1.3 Fecal Coliform CFU/100ml <MDL 1 08/20/12 L56238-6 1.2 Fecal Coliform CFU/100ml <MDL 1 09/17/12 L56394-6 0.99 Fecal Coliform CFU/100ml <MDL 1 10/16/12 L56533-6 1.3 Fecal Coliform 1 CFU/100ml 1 11/26/12 L56803-6 0.61 Fecal Coliform CFU/100ml <MDL 1 12/18/12 L57085-6 0.45 Fecal Coliform 1 CFU/100ml 1 01/18/11 L52381-6 1.2 Sample Temperature, Field 8.3819 deg C 01/18/11 L52381-7 15 Sample Temperature, Field 8.6863 deg C 01/18/11 L52381-8 24.9 Sample Temperature, Field 8.7252 deg C 01/18/11 L52381-9 34.8 Sample Temperature, Field 8.7664 deg C 01/18/11 L52381-10 54.7 Sample Temperature, Field 8.6292 deg C 01/18/11 L52381-11 99.3 Sample Temperature, Field 8.5310 deg C 01/18/11 L52381-12 198 Sample Temperature, Field 8.1736 deg C 01/18/11 L52381-13 198 Sample Temperature, Field 8.1732 deg C 02/22/11 L52539-6 0.96 Sample Temperature, Field 7.7261 deg C 02/22/11 L52539-7 14.8 Sample Temperature, Field 8.1228 deg C 02/22/11 L52539-8 24.7 Sample Temperature, Field 8.1915 deg C 02/22/11 L52539-9 34.6 Sample Temperature, Field 8.1888 deg C 02/22/11 L52539-10 54.4 Sample Temperature, Field 8.1533 deg C 02/22/11 L52539-11 98.9 Sample Temperature, Field 8.0737 deg C 02/22/11 L52539-12 197 Sample Temperature, Field 7.9810 deg C 02/22/11 L52539-13 198 Sample Temperature, Field 7.9812 deg C 03/21/11 L52727-6 1.5 Sample Temperature, Field 7.8055 deg C 03/21/11 L52732-1 1.5 Sample Temperature, Field 7.8055 deg C 03/21/11 L52732-2 6 Sample Temperature, Field 7.7910 deg C 03/21/11 L52727-7 15.3 Sample Temperature, Field 7.7599 deg C 03/21/11 L52727-8 25.2 Sample Temperature, Field 7.7397 deg C 03/21/11 L52727-9 35.1 Sample Temperature, Field 7.7378 deg C 03/21/11 L52727-10 54.9 Sample Temperature, Field 7.7152 deg C 03/21/11 L52727-11 99.6 Sample Temperature, Field 7.6892 deg C 03/21/11 L52727-12 198 Sample Temperature, Field 7.5913 deg C 03/21/11 L52727-13 198 Sample Temperature, Field 7.5912 deg C 04/04/11 L52882-1 1.2 Sample Temperature, Field 7.9883 deg C 04/04/11 L52882-2 2.5 Sample Temperature, Field 7.9849 deg CPage 2 of 25 

## Table A-1
Complete Water Quality Monitoring Data for Station KSBP01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 04/18/11 L52886-1 1.9 Sample Temperature, Field 8.3546 deg C 04/18/11 L52883-6 1.9 Sample Temperature, Field 8.3546 deg C 04/18/11 L52886-2 6.6 Sample Temperature, Field 8.3478 deg C 04/18/11 L52883-7 16.1 Sample Temperature, Field 8.1237 deg C 04/18/11 L52883-8 25.9 Sample Temperature, Field 7.9959 deg C 04/18/11 L52883-9 35.9 Sample Temperature, Field 7.9861 deg C 04/18/11 L52883-10 54.4 Sample Temperature, Field 7.9684 deg C 04/18/11 L52883-11 99.1 Sample Temperature, Field 7.9566 deg C 04/18/11 L52883-12 198 Sample Temperature, Field 7.9042 deg C 04/18/11 L52883-13 198 Sample Temperature, Field 7.9040 deg C 05/04/11 L53125-1 1.2 Sample Temperature, Field 9.4099 deg C 05/04/11 L53125-2 5.5 Sample Temperature, Field 9.6382 deg C 05/16/11 L53206-6 1.5 Sample Temperature, Field 9.3803 deg C 05/16/11 L53209-1 1.5 Sample Temperature, Field 9.3803 deg C 05/16/11 L53209-2 2.9 Sample Temperature, Field 9.3754 deg C 05/16/11 L53206-7 15.2 Sample Temperature, Field 8.9990 deg C 05/16/11 L53206-8 25 Sample Temperature, Field 8.8475 deg C 05/16/11 L53206-9 35 Sample Temperature, Field 8.7143 deg C 05/16/11 L53206-10 54.7 Sample Temperature, Field 8.5685 deg C 05/16/11 L53206-11 99.4 Sample Temperature, Field 8.4590 deg C 05/16/11 L53206-12 198 Sample Temperature, Field 8.6792 deg C 05/16/11 L53206-13 198 Sample Temperature, Field 8.6812 deg C 06/08/11 L53226-1 1.2 Sample Temperature, Field 10.4910 deg C 06/08/11 L53226-2 2.6 Sample Temperature, Field 10.4563 deg C 06/20/11 L53429-1 1.3 Sample Temperature, Field 11.4120 deg C 06/20/11 L53331-6 1.3 Sample Temperature, Field 11.4120 deg C 06/20/11 L53429-2 2.8 Sample Temperature, Field 11.3785 deg C 06/20/11 L53331-7 15.1 Sample Temperature, Field 10.0880 deg C 06/20/11 L53331-8 24.9 Sample Temperature, Field 9.9345 deg C 06/20/11 L53331-9 34.8 Sample Temperature, Field 9.9328 deg C 06/20/11 L53331-10 54.4 Sample Temperature, Field 9.8563 deg C 06/20/11 L53331-11 99.1 Sample Temperature, Field 9.7591 deg C 06/20/11 L53331-12 198 Sample Temperature, Field 9.4112 deg C 06/20/11 L53331-13 198 Sample Temperature, Field 9.4113 deg C 07/06/11 L53327-1 1.3 Sample Temperature, Field 12.9281 deg C 07/06/11 L53327-2 3.6 Sample Temperature, Field 12.4272 deg C 07/14/11 L53626-1 4.7 Sample Temperature, Field 12.1427 deg C 07/14/11 L53626-2 49.3 Sample Temperature, Field 10.6787 deg C 07/14/11 L53626-3 198 Sample Temperature, Field 10.0463 deg C 07/18/11 L53542-6 1.2 Sample Temperature, Field 11.7902 deg C 07/18/11 L53545-1 1.2 Sample Temperature, Field 11.7102 deg C 07/18/11 L53545-2 3.6 Sample Temperature, Field 11.5744 deg C 07/18/11 L53542-7 15.1 Sample Temperature, Field 10.9568 deg C 07/18/11 L53542-8 24.8 Sample Temperature, Field 10.8520 deg C 07/18/11 L53542-9 34.8 Sample Temperature, Field 10.7684 deg C 07/18/11 L53542-10 54.7 Sample Temperature, Field 10.6033 deg C 07/18/11 L53542-11 99.3 Sample Temperature, Field 10.5382 deg C 07/18/11 L53542-12 198 Sample Temperature, Field 10.1377 deg C 07/18/11 L53542-13 198 Sample Temperature, Field 10.1379 deg C 08/03/11 L53731-1 1.2 Sample Temperature, Field 12.9579 deg C 08/03/11 L53731-2 2.7 Sample Temperature, Field 13.1900 deg C 08/15/11 L53889-6 1.3 Sample Temperature, Field 13.1419 deg CPage 3 of 25 

## Table A-1
Complete Water Quality Monitoring Data for Station KSBP01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 08/15/11 L53892-1 1.3 Sample Temperature, Field 13.1419 deg C 08/15/11 L53892-2 3.8 Sample Temperature, Field 13.0456 deg C 08/15/11 L53889-7 15.1 Sample Temperature, Field 12.4575 deg C 08/15/11 L53889-8 25 Sample Temperature, Field 11.4875 deg C 08/15/11 L53889-9 34.8 Sample Temperature, Field 11.4120 deg C 08/15/11 L53889-10 54.5 Sample Temperature, Field 11.2654 deg C 08/15/11 L53889-11 99.3 Sample Temperature, Field 11.1090 deg C 08/15/11 L53889-12 198 Sample Temperature, Field 10.9231 deg C 08/15/11 L53889-13 198 Sample Temperature, Field 10.9231 deg C 09/07/11 L54044-1 1.2 Sample Temperature, Field 12.8521 deg C 09/07/11 L54044-2 2.6 Sample Temperature, Field 12.8359 deg C 09/19/11 L54019-6 1.2 Sample Temperature, Field 12.3565 deg C 09/19/11 L54022-1 1.2 Sample Temperature, Field 12.3565 deg C 09/19/11 L54022-2 8.1 Sample Temperature, Field 12.3423 deg C 09/19/11 L54019-7 15 Sample Temperature, Field 12.2471 deg C 09/19/11 L54019-8 24.9 Sample Temperature, Field 12.0205 deg C 09/19/11 L54019-9 34.8 Sample Temperature, Field 11.8962 deg C 09/19/11 L54019-10 54.6 Sample Temperature, Field 11.5550 deg C 09/19/11 L54019-11 99.2 Sample Temperature, Field 11.4752 deg C 09/19/11 L54019-12 198 Sample Temperature, Field 11.3392 deg C 09/19/11 L54019-13 198 Sample Temperature, Field 11.3336 deg C 10/06/11 L54268-1 1.2 Sample Temperature, Field 12.0699 deg C 10/06/11 L54268-2 5.6 Sample Temperature, Field 12.0230 deg C 10/17/11 L54270-1 1.1 Sample Temperature, Field 11.4833 deg C 10/17/11 L54269-6 1.1 Sample Temperature, Field 11.4833 deg C 10/17/11 L54270-2 5.6 Sample Temperature, Field 11.6493 deg C 10/17/11 L54269-7 14.9 Sample Temperature, Field 11.6805 deg C 10/17/11 L54269-8 24.8 Sample Temperature, Field 11.5219 deg C 10/17/11 L54269-9 34.7 Sample Temperature, Field 11.5190 deg C 10/17/11 L54269-10 54.5 Sample Temperature, Field 11.4165 deg C 10/17/11 L54269-11 99.1 Sample Temperature, Field 11.1930 deg C 10/17/11 L54269-12 198 Sample Temperature, Field 11.1136 deg C 10/17/11 L54269-13 198 Sample Temperature, Field 11.1133 deg C 11/28/11 L54474-6 1.6 Sample Temperature, Field 10.0238 deg C 11/28/11 L54474-7 14.9 Sample Temperature, Field 10.0912 deg C 11/28/11 L54474-8 24.7 Sample Temperature, Field 10.0978 deg C 11/28/11 L54474-9 34.7 Sample Temperature, Field 10.0026 deg C 11/28/11 L54474-10 54.5 Sample Temperature, Field 9.9469 deg C 11/28/11 L54474-11 99 Sample Temperature, Field 9.7738 deg C 11/28/11 L54474-12 198 Sample Temperature, Field 9.5073 deg C 11/28/11 L54474-13 198 Sample Temperature, Field 9.5050 deg C 12/14/11 L54765-1 4.9 Sample Temperature, Field 8.9912 deg C 12/14/11 L54765-2 49.5 Sample Temperature, Field 9.5055 deg C 12/14/11 L54765-3 198 Sample Temperature, Field 8.9946 deg C 12/19/11 L54766-6 1 Sample Temperature, Field 9.2823 deg C 12/19/11 L54766-7 14.8 Sample Temperature, Field 9.4382 deg C 12/19/11 L54766-8 24.6 Sample Temperature, Field 9.4676 deg C 12/19/11 L54766-9 34.6 Sample Temperature, Field 9.4726 deg C 12/19/11 L54766-10 54.3 Sample Temperature, Field 9.1692 deg C 12/19/11 L54766-11 98.9 Sample Temperature, Field 8.9511 deg C 12/19/11 L54766-12 198 Sample Temperature, Field 8.7678 deg C 12/19/11 L54766-13 198 Sample Temperature, Field 8.7615 deg CPage 4 of 25 

## Table A-1
Complete Water Quality Monitoring Data for Station KSBP01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 01/23/12 L54840-6 1.2 Sample Temperature, Field 7.9581 deg C 01/23/12 L54840-7 15.1 Sample Temperature, Field 8.1207 deg C 01/23/12 L54840-8 25 Sample Temperature, Field 8.1937 deg C 01/23/12 L54840-9 34.9 Sample Temperature, Field 8.1751 deg C 01/23/12 L54840-10 54.4 Sample Temperature, Field 8.1249 deg C 01/23/12 L54840-11 99.1 Sample Temperature, Field 7.9655 deg C 01/23/12 L54840-12 198 Sample Temperature, Field 7.5976 deg C 01/23/12 L54840-13 199 Sample Temperature, Field 7.5961 deg C 02/21/12 L55087-6 1.2 Sample Temperature, Field 7.8167 deg C 02/21/12 L55087-7 15.1 Sample Temperature, Field 7.8138 deg C 02/21/12 L55087-8 25 Sample Temperature, Field 7.8120 deg C 02/21/12 L55087-9 34.9 Sample Temperature, Field 7.8122 deg C 02/21/12 L55087-10 54.7 Sample Temperature, Field 7.7945 deg C 02/21/12 L55087-11 99.4 Sample Temperature, Field 7.7457 deg C 02/21/12 L55087-12 198 Sample Temperature, Field 7.7355 deg C 02/21/12 L55087-13 198 Sample Temperature, Field 7.7354 deg C 03/19/12 L55193-6 2.8 Sample Temperature, Field 7.1768 deg C 03/19/12 L55193-7 16 Sample Temperature, Field 7.5678 deg C 03/19/12 L55193-8 25 Sample Temperature, Field 7.6101 deg C 03/19/12 L55193-9 34.9 Sample Temperature, Field 7.5818 deg C 03/19/12 L55193-10 54.4 Sample Temperature, Field 7.5498 deg C 03/19/12 L55193-11 99.2 Sample Temperature, Field 7.5052 deg C 03/19/12 L55193-12 198 Sample Temperature, Field 7.4920 deg C 03/19/12 L55193-13 198 Sample Temperature, Field 7.4919 deg C 04/03/12 L55355-1 1.2 Sample Temperature, Field 7.8788 deg C 04/03/12 L55355-2 5.3 Sample Temperature, Field 7.8629 deg C 04/16/12 L55373-1 1.3 Sample Temperature, Field 8.9614 deg C 04/16/12 L55370-6 1.3 Sample Temperature, Field 8.9614 deg C 04/16/12 L55373-2 3.8 Sample Temperature, Field 8.7488 deg C 04/16/12 L55370-7 15.1 Sample Temperature, Field 8.3034 deg C 04/16/12 L55370-8 24.8 Sample Temperature, Field 8.0915 deg C 04/16/12 L55370-9 34.7 Sample Temperature, Field 7.8738 deg C 04/16/12 L55370-10 54.6 Sample Temperature, Field 7.8883 deg C 04/16/12 L55370-11 99.2 Sample Temperature, Field 7.9071 deg C 04/16/12 L55370-12 198 Sample Temperature, Field 7.7212 deg C 04/16/12 L55370-13 198 Sample Temperature, Field 7.7207 deg C 05/09/12 L55525-1 1.2 Sample Temperature, Field 10.7967 deg C 05/09/12 L55525-2 3.5 Sample Temperature, Field 10.6665 deg C 05/21/12 L55535-1 1.6 Sample Temperature, Field 10.6800 deg C 05/21/12 L55534-6 1.6 Sample Temperature, Field 10.6800 deg C 05/21/12 L55535-2 3.9 Sample Temperature, Field 10.5036 deg C 05/21/12 L55534-7 15.1 Sample Temperature, Field 9.3810 deg C 05/21/12 L55534-8 25 Sample Temperature, Field 8.9898 deg C 05/21/12 L55534-9 34.8 Sample Temperature, Field 8.9664 deg C 05/21/12 L55534-10 54.6 Sample Temperature, Field 9.0055 deg C 05/21/12 L55534-11 99.3 Sample Temperature, Field 8.8772 deg C 05/21/12 L55534-12 198 Sample Temperature, Field 9.1021 deg C 05/21/12 L55534-13 198 Sample Temperature, Field 9.1020 deg C 06/06/12 L55730-1 1.1 Sample Temperature, Field 10.8088 deg C 06/06/12 L55730-2 3.5 Sample Temperature, Field 10.8635 deg C 06/18/12 L55788-6 1.3 Sample Temperature, Field 11.8418 deg C 06/18/12 L55791-1 1.3 Sample Temperature, Field 11.8418 deg CPage 5 of 25 

## Table A-1
Complete Water Quality Monitoring Data for Station KSBP01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 06/18/12 L55791-2 2.7 Sample Temperature, Field 11.7926 deg C 06/18/12 L55788-7 15.1 Sample Temperature, Field 10.1343 deg C 06/18/12 L55788-8 24.8 Sample Temperature, Field 9.9213 deg C 06/18/12 L55788-9 34.8 Sample Temperature, Field 9.7550 deg C 06/18/12 L55788-10 54.6 Sample Temperature, Field 9.5567 deg C 06/18/12 L55788-11 99.1 Sample Temperature, Field 9.5224 deg C 06/18/12 L55788-12 198 Sample Temperature, Field 9.5186 deg C 06/18/12 L55788-13 198 Sample Temperature, Field 9.5186 deg C 07/03/12 L55889-1 1.3 Sample Temperature, Field 12.5950 deg C 07/03/12 L55889-2 2.6 Sample Temperature, Field 12.2817 deg C 07/16/12 L55944-6 1.3 Sample Temperature, Field 13.6706 deg C 07/16/12 L55946-1 1.3 Sample Temperature, Field 13.6706 deg C 07/16/12 L55946-2 2.8 Sample Temperature, Field 13.6342 deg C 07/16/12 L55944-7 15 Sample Temperature, Field 12.6161 deg C 07/16/12 L55944-8 24.3 Sample Temperature, Field 11.1509 deg C 07/16/12 L55944-9 24.9 Sample Temperature, Field 11.1374 deg C 07/16/12 L55944-10 34.9 Sample Temperature, Field 10.8669 deg C 07/16/12 L55944-11 54.6 Sample Temperature, Field 10.2743 deg C 07/16/12 L55944-12 99.2 Sample Temperature, Field 10.1065 deg C 07/16/12 L55944-13 198 Sample Temperature, Field 10.1366 deg C 07/30/12 L56062-1 4.8 Sample Temperature, Field 12.1289 deg C 07/30/12 L56062-2 49.4 Sample Temperature, Field 10.8233 deg C 07/30/12 L56062-3 198 Sample Temperature, Field 10.4998 deg C 08/08/12 L56173-1 1.1 Sample Temperature, Field 12.6592 deg C 08/08/12 L56173-2 2.6 Sample Temperature, Field 12.5489 deg C 08/20/12 L56174-1 1.2 Sample Temperature, Field 13.9506 deg C 08/20/12 L56238-6 1.2 Sample Temperature, Field 13.9506 deg C 08/20/12 L56174-2 5.6 Sample Temperature, Field 13.6685 deg C 08/20/12 L56238-7 15 Sample Temperature, Field 12.4524 deg C 08/20/12 L56238-8 24.8 Sample Temperature, Field 11.8547 deg C 08/20/12 L56238-9 34.7 Sample Temperature, Field 11.5677 deg C 08/20/12 L56238-10 54.6 Sample Temperature, Field 11.3739 deg C 08/20/12 L56238-11 99.2 Sample Temperature, Field 11.2779 deg C 08/20/12 L56238-12 198 Sample Temperature, Field 10.9819 deg C 08/20/12 L56238-13 198 Sample Temperature, Field 10.9742 deg C 09/05/12 L56391-1 1 Sample Temperature, Field 12.7887 deg C 09/05/12 L56391-2 2.4 Sample Temperature, Field 12.7298 deg C 09/17/12 L56394-6 0.99 Sample Temperature, Field 12.8616 deg C 09/17/12 L56393-1 0.99 Sample Temperature, Field 12.8616 deg C 09/17/12 L56393-2 3.5 Sample Temperature, Field 12.8443 deg C 09/17/12 L56394-7 15 Sample Temperature, Field 12.3114 deg C 09/17/12 L56394-8 24.9 Sample Temperature, Field 11.7810 deg C 09/17/12 L56394-9 34.7 Sample Temperature, Field 11.7357 deg C 09/17/12 L56394-10 54.2 Sample Temperature, Field 11.6110 deg C 09/17/12 L56394-11 99.2 Sample Temperature, Field 11.5534 deg C 09/17/12 L56394-12 198 Sample Temperature, Field 11.1792 deg C 09/17/12 L56394-13 198 Sample Temperature, Field 11.1749 deg C 10/03/12 L56648-1 0.95 Sample Temperature, Field 12.1247 deg C 10/03/12 L56648-2 7.7 Sample Temperature, Field 12.1296 deg C 10/16/12 L56533-6 1.3 Sample Temperature, Field 11.8637 deg C 10/16/12 L56533-7 15.1 Sample Temperature, Field 11.7529 deg C 10/16/12 L56533-8 25.1 Sample Temperature, Field 11.6405 deg CPage 6 of 25 

## Table A-1
Complete Water Quality Monitoring Data for Station KSBP01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 10/16/12 L56533-9 35.1 Sample Temperature, Field 11.5902 deg C 10/16/12 L56533-10 54.9 Sample Temperature, Field 11.3076 deg C 10/16/12 L56533-11 99.3 Sample Temperature, Field 11.2007 deg C 10/16/12 L56533-12 198 Sample Temperature, Field 10.8169 deg C 10/16/12 L56533-13 199 Sample Temperature, Field 10.8171 deg C 10/18/12 L56781-1 1.3 Sample Temperature, Field 11.8068 deg C 10/18/12 L56781-2 5.7 Sample Temperature, Field 11.7435 deg C 11/26/12 L56803-6 0.61 Sample Temperature, Field 9.6539 deg C 11/26/12 L56803-7 14.5 Sample Temperature, Field 10.3681 deg C 11/26/12 L56803-8 24.4 Sample Temperature, Field 10.3505 deg C 11/26/12 L56803-9 34.2 Sample Temperature, Field 10.3079 deg C 11/26/12 L56803-10 54.1 Sample Temperature, Field 10.2558 deg C 11/26/12 L56803-11 98.6 Sample Temperature, Field 10.0811 deg C 11/26/12 L56803-12 198 Sample Temperature, Field 9.8582 deg C 11/26/12 L56803-13 198 Sample Temperature, Field 9.8580 deg C 12/12/12 L56990-1 4.9 Sample Temperature, Field 9.5119 deg C 12/12/12 L56990-2 49.3 Sample Temperature, Field 9.4941 deg C 12/12/12 L56990-3 198 Sample Temperature, Field 9.9325 deg C 12/18/12 L57085-6 0.45 Sample Temperature, Field 9.6037 deg C 12/18/12 L57085-7 14.4 Sample Temperature, Field 9.6383 deg C 12/18/12 L57085-8 24.2 Sample Temperature, Field 9.6416 deg C 12/18/12 L57085-9 34 Sample Temperature, Field 9.6491 deg C 12/18/12 L57085-10 53.8 Sample Temperature, Field 9.6073 deg C 12/18/12 L57085-11 98.6 Sample Temperature, Field 9.6173 deg C 12/18/12 L57085-12 197 Sample Temperature, Field 9.9199 deg C 12/18/12 L57085-13 198 Sample Temperature, Field 9.9249 deg C 01/18/11 L52381-6 1.2 Dissolved Oxygen, Field 8.8 mg/L 0.5 1 01/18/11 L52381-7 15 Dissolved Oxygen, Field 8.4 mg/L 0.5 1 01/18/11 L52381-8 24.9 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 01/18/11 L52381-9 34.8 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 01/18/11 L52381-10 54.7 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 01/18/11 L52381-11 99.3 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 01/18/11 L52381-12 198 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 01/18/11 L52381-13 198 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 02/22/11 L52539-6 0.96 Dissolved Oxygen, Field 9.0 mg/L 0.5 1 02/22/11 L52539-7 14.8 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 02/22/11 L52539-8 24.7 Dissolved Oxygen, Field 8.1 mg/L 0.5 1 02/22/11 L52539-9 34.6 Dissolved Oxygen, Field 8.1 mg/L 0.5 1 02/22/11 L52539-10 54.4 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 02/22/11 L52539-11 98.9 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 02/22/11 L52539-12 197 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 02/22/11 L52539-13 198 Dissolved Oxygen, Field 7.9 mg/L 0.5 1 03/21/11 L52727-6 1.5 Dissolved Oxygen, Field 9.3 mg/L 0.5 1 03/21/11 L52732-1 1.5 Dissolved Oxygen, Field 9.3 mg/L 0.5 1 03/21/11 L52732-2 6 Dissolved Oxygen, Field 8.7 mg/L 0.5 1 03/21/11 L52727-7 15.3 Dissolved Oxygen, Field 9.0 mg/L 0.5 1 03/21/11 L52727-8 25.2 Dissolved Oxygen, Field 8.9 mg/L 0.5 1 03/21/11 L52727-9 35.1 Dissolved Oxygen, Field 8.8 mg/L 0.5 1 03/21/11 L52727-10 54.9 Dissolved Oxygen, Field 8.9 mg/L 0.5 1 03/21/11 L52727-11 99.6 Dissolved Oxygen, Field 8.7 mg/L 0.5 1 03/21/11 L52727-12 198 Dissolved Oxygen, Field 8.4 mg/L 0.5 1 03/21/11 L52727-13 198 Dissolved Oxygen, Field 8.4 mg/L 0.5 1Page 7 of 25 

## Table A-1
Complete Water Quality Monitoring Data for Station KSBP01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 04/04/11 L52882-1 1.2 Dissolved Oxygen, Field 9.2 mg/L 0.5 1 04/04/11 L52882-2 2.5 Dissolved Oxygen, Field 9.2 mg/L 0.5 1 04/18/11 L52886-1 1.9 Dissolved Oxygen, Field 9.8 mg/L 0.5 1 04/18/11 L52883-6 1.9 Dissolved Oxygen, Field 9.8 mg/L 0.5 1 04/18/11 L52886-2 6.6 Dissolved Oxygen, Field 9.4 mg/L 0.5 1 04/18/11 L52883-7 16.1 Dissolved Oxygen, Field 9.0 mg/L 0.5 1 04/18/11 L52883-8 25.9 Dissolved Oxygen, Field 8.8 mg/L 0.5 1 04/18/11 L52883-9 35.9 Dissolved Oxygen, Field 8.7 mg/L 0.5 1 04/18/11 L52883-10 54.4 Dissolved Oxygen, Field 8.5 mg/L 0.5 1 04/18/11 L52883-11 99.1 Dissolved Oxygen, Field 8.5 mg/L 0.5 1 04/18/11 L52883-12 198 Dissolved Oxygen, Field 8.2 mg/L 0.5 1 04/18/11 L52883-13 198 Dissolved Oxygen, Field 8.2 mg/L 0.5 1 05/04/11 L53125-1 1.2 Dissolved Oxygen, Field 12.8 mg/L 0.5 1 05/04/11 L53125-2 5.5 Dissolved Oxygen, Field 12.4 mg/L 0.5 1 05/16/11 L53206-6 1.5 Dissolved Oxygen, Field 11.4 mg/L 0.5 1 05/16/11 L53209-1 1.5 Dissolved Oxygen, Field 11.4 mg/L 0.5 1 05/16/11 L53209-2 2.9 Dissolved Oxygen, Field 11.3 mg/L 0.5 1 05/16/11 L53206-7 15.2 Dissolved Oxygen, Field 10.2 mg/L 0.5 1 05/16/11 L53206-8 25 Dissolved Oxygen, Field 9.8 mg/L 0.5 1 05/16/11 L53206-9 35 Dissolved Oxygen, Field 9.2 mg/L 0.5 1 05/16/11 L53206-10 54.7 Dissolved Oxygen, Field 8.8 mg/L 0.5 1 05/16/11 L53206-11 99.4 Dissolved Oxygen, Field 8.2 mg/L 0.5 1 05/16/11 L53206-12 198 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 05/16/11 L53206-13 198 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 06/08/11 L53226-1 1.2 Dissolved Oxygen, Field 11.5 mg/L 0.5 1 06/08/11 L53226-2 2.6 Dissolved Oxygen, Field 11.0 mg/L 0.5 1 06/20/11 L53429-1 1.3 Dissolved Oxygen, Field 9.2 mg/L 0.5 1 06/20/11 L53331-6 1.3 Dissolved Oxygen, Field 9.2 mg/L 0.5 1 06/20/11 L53429-2 2.8 Dissolved Oxygen, Field 9.2 mg/L 0.5 1 06/20/11 L53331-7 15.1 Dissolved Oxygen, Field 8.5 mg/L 0.5 1 06/20/11 L53331-8 24.9 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 06/20/11 L53331-9 34.8 Dissolved Oxygen, Field 8.2 mg/L 0.5 1 06/20/11 L53331-10 54.4 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 06/20/11 L53331-11 99.1 Dissolved Oxygen, Field 7.5 mg/L 0.5 1 06/20/11 L53331-12 198 Dissolved Oxygen, Field 7.4 mg/L 0.5 1 06/20/11 L53331-13 198 Dissolved Oxygen, Field 7.4 mg/L 0.5 1 07/06/11 L53327-1 1.3 Dissolved Oxygen, Field 12.8 mg/L 0.5 1 07/06/11 L53327-2 3.6 Dissolved Oxygen, Field 12.0 mg/L 0.5 1 07/14/11 L53626-1 4.7 Dissolved Oxygen, Field 9.8 mg/L 0.5 1 07/14/11 L53626-2 49.3 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 07/14/11 L53626-3 198 Dissolved Oxygen, Field 6.5 mg/L 0.5 1 07/18/11 L53542-6 1.2 Dissolved Oxygen, Field 8.4 mg/L 0.5 1 07/18/11 L53545-1 1.2 Dissolved Oxygen, Field 8.5 mg/L 0.5 1 07/18/11 L53545-2 3.6 Dissolved Oxygen, Field 8.4 mg/L 0.5 1 07/18/11 L53542-7 15.1 Dissolved Oxygen, Field 7.9 mg/L 0.5 1 07/18/11 L53542-8 24.8 Dissolved Oxygen, Field 7.7 mg/L 0.5 1 07/18/11 L53542-9 34.8 Dissolved Oxygen, Field 7.7 mg/L 0.5 1 07/18/11 L53542-10 54.7 Dissolved Oxygen, Field 7.3 mg/L 0.5 1 07/18/11 L53542-11 99.3 Dissolved Oxygen, Field 7.0 mg/L 0.5 1 07/18/11 L53542-12 198 Dissolved Oxygen, Field 6.5 mg/L 0.5 1 07/18/11 L53542-13 198 Dissolved Oxygen, Field 6.5 mg/L 0.5 1 08/03/11 L53731-1 1.2 Dissolved Oxygen, Field 10.4 mg/L 0.5 1Page 8 of 25 

## Table A-1
Complete Water Quality Monitoring Data for Station KSBP01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 08/03/11 L53731-2 2.7 Dissolved Oxygen, Field 10.0 mg/L 0.5 1 08/15/11 L53889-6 1.3 Dissolved Oxygen, Field 8.6 mg/L 0.5 1 08/15/11 L53892-1 1.3 Dissolved Oxygen, Field 8.6 mg/L 0.5 1 08/15/11 L53892-2 3.8 Dissolved Oxygen, Field 8.5 mg/L 0.5 1 08/15/11 L53889-7 15.1 Dissolved Oxygen, Field 7.4 mg/L 0.5 1 08/15/11 L53889-8 25 Dissolved Oxygen, Field 6.4 mg/L 0.5 1 08/15/11 L53889-9 34.8 Dissolved Oxygen, Field 6.4 mg/L 0.5 1 08/15/11 L53889-10 54.5 Dissolved Oxygen, Field 6.3 mg/L 0.5 1 08/15/11 L53889-11 99.3 Dissolved Oxygen, Field 6.2 mg/L 0.5 1 08/15/11 L53889-12 198 Dissolved Oxygen, Field 6.0 mg/L 0.5 1 08/15/11 L53889-13 198 Dissolved Oxygen, Field 6.0 mg/L 0.5 1 09/07/11 L54044-1 1.2 Dissolved Oxygen, Field 7.3 mg/L 0.5 1 09/07/11 L54044-2 2.6 Dissolved Oxygen, Field 7.3 mg/L 0.5 1 09/19/11 L54019-6 1.2 Dissolved Oxygen, Field 7.2 mg/L 0.5 1 09/19/11 L54022-1 1.2 Dissolved Oxygen, Field 7.2 mg/L 0.5 1 09/19/11 L54022-2 8.1 Dissolved Oxygen, Field 7.1 mg/L 0.5 1 09/19/11 L54019-7 15 Dissolved Oxygen, Field 6.7 mg/L 0.5 1 09/19/11 L54019-8 24.9 Dissolved Oxygen, Field 6.5 mg/L 0.5 1 09/19/11 L54019-9 34.8 Dissolved Oxygen, Field 6.4 mg/L 0.5 1 09/19/11 L54019-10 54.6 Dissolved Oxygen, Field 6.1 mg/L 0.5 1 09/19/11 L54019-11 99.2 Dissolved Oxygen, Field 6.2 mg/L 0.5 1 09/19/11 L54019-12 198 Dissolved Oxygen, Field 6.2 mg/L 0.5 1 09/19/11 L54019-13 198 Dissolved Oxygen, Field 6.2 mg/L 0.5 1 10/06/11 L54268-1 1.2 Dissolved Oxygen, Field 6.1 mg/L 0.5 1 10/06/11 L54268-2 5.6 Dissolved Oxygen, Field 6.0 mg/L 0.5 1 10/17/11 L54270-1 1.1 Dissolved Oxygen, Field 7.8 mg/L 0.5 1 10/17/11 L54269-6 1.1 Dissolved Oxygen, Field 7.8 mg/L 0.5 1 10/17/11 L54270-2 5.6 Dissolved Oxygen, Field 7.5 mg/L 0.5 1 10/17/11 L54269-7 14.9 Dissolved Oxygen, Field 6.7 mg/L 0.5 1 10/17/11 L54269-8 24.8 Dissolved Oxygen, Field 6.1 mg/L 0.5 1 10/17/11 L54269-9 34.7 Dissolved Oxygen, Field 6.1 mg/L 0.5 1 10/17/11 L54269-10 54.5 Dissolved Oxygen, Field 6.0 mg/L 0.5 1 10/17/11 L54269-11 99.1 Dissolved Oxygen, Field 6.0 mg/L 0.5 1 10/17/11 L54269-12 198 Dissolved Oxygen, Field 5.9 mg/L 0.5 1 10/17/11 L54269-13 198 Dissolved Oxygen, Field 5.9 mg/L 0.5 1 11/28/11 L54474-6 1.6 Dissolved Oxygen, Field 7.3 mg/L 0.5 1 11/28/11 L54474-7 14.9 Dissolved Oxygen, Field 7.2 mg/L 0.5 1 11/28/11 L54474-8 24.7 Dissolved Oxygen, Field 6.9 mg/L 0.5 1 11/28/11 L54474-9 34.7 Dissolved Oxygen, Field 6.9 mg/L 0.5 1 11/28/11 L54474-10 54.5 Dissolved Oxygen, Field 7.0 mg/L 0.5 1 11/28/11 L54474-11 99 Dissolved Oxygen, Field 7.1 mg/L 0.5 1 11/28/11 L54474-12 198 Dissolved Oxygen, Field 7.2 mg/L 0.5 1 11/28/11 L54474-13 198 Dissolved Oxygen, Field 7.2 mg/L 0.5 1 12/14/11 L54765-1 4.9 Dissolved Oxygen, Field 7.6 mg/L 0.5 1 12/14/11 L54765-2 49.5 Dissolved Oxygen, Field 6.8 mg/L 0.5 1 12/14/11 L54765-3 198 Dissolved Oxygen, Field 7.1 mg/L 0.5 1 12/19/11 L54766-6 1 Dissolved Oxygen, Field 7.2 mg/L 0.5 1 12/19/11 L54766-7 14.8 Dissolved Oxygen, Field 7.0 mg/L 0.5 1 12/19/11 L54766-8 24.6 Dissolved Oxygen, Field 6.8 mg/L 0.5 1 12/19/11 L54766-9 34.6 Dissolved Oxygen, Field 6.8 mg/L 0.5 1 12/19/11 L54766-10 54.3 Dissolved Oxygen, Field 6.9 mg/L 0.5 1 12/19/11 L54766-11 98.9 Dissolved Oxygen, Field 7.0 mg/L 0.5 1Page 9 of 25 

## Table A-1
Complete Water Quality Monitoring Data for Station KSBP01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 12/19/11 L54766-12 198 Dissolved Oxygen, Field 6.9 mg/L 0.5 1 12/19/11 L54766-13 198 Dissolved Oxygen, Field 6.9 mg/L 0.5 1 01/23/12 L54840-6 1.2 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 01/23/12 L54840-7 15.1 Dissolved Oxygen, Field 7.8 mg/L 0.5 1 01/23/12 L54840-8 25 Dissolved Oxygen, Field 7.6 mg/L 0.5 1 01/23/12 L54840-9 34.9 Dissolved Oxygen, Field 7.6 mg/L 0.5 1 01/23/12 L54840-10 54.4 Dissolved Oxygen, Field 7.6 mg/L 0.5 1 01/23/12 L54840-11 99.1 Dissolved Oxygen, Field 7.6 mg/L 0.5 1 01/23/12 L54840-12 198 Dissolved Oxygen, Field 7.7 mg/L 0.5 1 01/23/12 L54840-13 199 Dissolved Oxygen, Field 7.7 mg/L 0.5 1 02/21/12 L55087-6 1.2 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 02/21/12 L55087-7 15.1 Dissolved Oxygen, Field 7.9 mg/L 0.5 1 02/21/12 L55087-8 25 Dissolved Oxygen, Field 7.9 mg/L 0.5 1 02/21/12 L55087-9 34.9 Dissolved Oxygen, Field 7.8 mg/L 0.5 1 02/21/12 L55087-10 54.7 Dissolved Oxygen, Field 7.8 mg/L 0.5 1 02/21/12 L55087-11 99.4 Dissolved Oxygen, Field 7.6 mg/L 0.5 1 02/21/12 L55087-12 198 Dissolved Oxygen, Field 7.8 mg/L 0.5 1 02/21/12 L55087-13 198 Dissolved Oxygen, Field 7.8 mg/L 0.5 1 03/19/12 L55193-6 2.8 Dissolved Oxygen, Field 9.4 mg/L 0.5 1 03/19/12 L55193-7 16 Dissolved Oxygen, Field 8.7 mg/L 0.5 1 03/19/12 L55193-8 25 Dissolved Oxygen, Field 8.5 mg/L 0.5 1 03/19/12 L55193-9 34.9 Dissolved Oxygen, Field 8.6 mg/L 0.5 1 03/19/12 L55193-10 54.4 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 03/19/12 L55193-11 99.2 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 03/19/12 L55193-12 198 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 03/19/12 L55193-13 198 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 04/03/12 L55355-1 1.2 Dissolved Oxygen, Field 9.4 mg/L 0.5 1 04/03/12 L55355-2 5.3 Dissolved Oxygen, Field 9.3 mg/L 0.5 1 04/16/12 L55373-1 1.3 Dissolved Oxygen, Field 12.5 mg/L 0.5 1 04/16/12 L55370-6 1.3 Dissolved Oxygen, Field 12.5 mg/L 0.5 1 04/16/12 L55373-2 3.8 Dissolved Oxygen, Field 12.2 mg/L 0.5 1 04/16/12 L55370-7 15.1 Dissolved Oxygen, Field 10.1 mg/L 0.5 1 04/16/12 L55370-8 24.8 Dissolved Oxygen, Field 9.2 mg/L 0.5 1 04/16/12 L55370-9 34.7 Dissolved Oxygen, Field 8.6 mg/L 0.5 1 04/16/12 L55370-10 54.6 Dissolved Oxygen, Field 8.5 mg/L 0.5 1 04/16/12 L55370-11 99.2 Dissolved Oxygen, Field 8.5 mg/L 0.5 1 04/16/12 L55370-12 198 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 04/16/12 L55370-13 198 Dissolved Oxygen, Field 8.1 mg/L 0.5 1 05/09/12 L55525-1 1.2 Dissolved Oxygen, Field 12.9 mg/L 0.5 1 05/09/12 L55525-2 3.5 Dissolved Oxygen, Field 12.7 mg/L 0.5 1 05/21/12 L55535-1 1.6 Dissolved Oxygen, Field 11.6 mg/L 0.5 1 05/21/12 L55534-6 1.6 Dissolved Oxygen, Field 11.6 mg/L 0.5 1 05/21/12 L55535-2 3.9 Dissolved Oxygen, Field 11.4 mg/L 0.5 1 05/21/12 L55534-7 15.1 Dissolved Oxygen, Field 9.3 mg/L 0.5 1 05/21/12 L55534-8 25 Dissolved Oxygen, Field 8.8 mg/L 0.5 1 05/21/12 L55534-9 34.8 Dissolved Oxygen, Field 8.7 mg/L 0.5 1 05/21/12 L55534-10 54.6 Dissolved Oxygen, Field 8.5 mg/L 0.5 1 05/21/12 L55534-11 99.3 Dissolved Oxygen, Field 8.1 mg/L 0.5 1 05/21/12 L55534-12 198 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 05/21/12 L55534-13 198 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 06/06/12 L55730-1 1.1 Dissolved Oxygen, Field 10.5 mg/L 0.5 1 06/06/12 L55730-2 3.5 Dissolved Oxygen, Field 10.5 mg/L 0.5 1Page 10 of 25 

## Table A-1
Complete Water Quality Monitoring Data for Station KSBP01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 06/18/12 L55788-6 1.3 Dissolved Oxygen, Field 9.8 mg/L 0.5 1 06/18/12 L55791-1 1.3 Dissolved Oxygen, Field 9.8 mg/L 0.5 1 06/18/12 L55791-2 2.7 Dissolved Oxygen, Field 9.8 mg/L 0.5 1 06/18/12 L55788-7 15.1 Dissolved Oxygen, Field 8.2 mg/L 0.5 1 06/18/12 L55788-8 24.8 Dissolved Oxygen, Field 7.9 mg/L 0.5 1 06/18/12 L55788-9 34.8 Dissolved Oxygen, Field 7.7 mg/L 0.5 1 06/18/12 L55788-10 54.6 Dissolved Oxygen, Field 7.3 mg/L 0.5 1 06/18/12 L55788-11 99.1 Dissolved Oxygen, Field 7.0 mg/L 0.5 1 06/18/12 L55788-12 198 Dissolved Oxygen, Field 6.7 mg/L 0.5 1 06/18/12 L55788-13 198 Dissolved Oxygen, Field 6.7 mg/L 0.5 1 07/03/12 L55889-1 1.3 Dissolved Oxygen, Field 7.1 mg/L 0.5 1 07/03/12 L55889-2 2.6 Dissolved Oxygen, Field 9.7 mg/L 0.5 1 07/16/12 L55944-6 1.3 Dissolved Oxygen, Field 9.9 mg/L 0.5 1 07/16/12 L55946-1 1.3 Dissolved Oxygen, Field 9.9 mg/L 0.5 1 07/16/12 L55946-2 2.8 Dissolved Oxygen, Field 9.9 mg/L 0.5 1 07/16/12 L55944-7 15 Dissolved Oxygen, Field 8.7 mg/L 0.5 1 07/16/12 L55944-8 24.3 Dissolved Oxygen, Field 7.8 mg/L 0.5 1 07/16/12 L55944-9 24.9 Dissolved Oxygen, Field 7.8 mg/L 0.5 1 07/16/12 L55944-10 34.9 Dissolved Oxygen, Field 7.4 mg/L 0.5 1 07/16/12 L55944-11 54.6 Dissolved Oxygen, Field 6.5 mg/L 0.5 1 07/16/12 L55944-12 99.2 Dissolved Oxygen, Field 6.3 mg/L 0.5 1 07/16/12 L55944-13 198 Dissolved Oxygen, Field 6.3 mg/L 0.5 1 07/30/12 L56062-1 4.8 Dissolved Oxygen, Field 7.7 mg/L 0.5 1 07/30/12 L56062-2 49.4 Dissolved Oxygen, Field 6.3 mg/L 0.5 1 07/30/12 L56062-3 198 Dissolved Oxygen, Field 5.8 mg/L 0.5 1 08/08/12 L56173-1 1.1 Dissolved Oxygen, Field 9.3 mg/L 0.5 1 08/08/12 L56173-2 2.6 Dissolved Oxygen, Field 8.8 mg/L 0.5 1 08/20/12 L56174-1 1.2 Dissolved Oxygen, Field 10.0 mg/L 0.5 1 08/20/12 L56238-6 1.2 Dissolved Oxygen, Field 10.0 mg/L 0.5 1 08/20/12 L56174-2 5.6 Dissolved Oxygen, Field 9.6 mg/L 0.5 1 08/20/12 L56238-7 15 Dissolved Oxygen, Field 7.4 mg/L 0.5 1 08/20/12 L56238-8 24.8 Dissolved Oxygen, Field 6.6 mg/L 0.5 1 08/20/12 L56238-9 34.7 Dissolved Oxygen, Field 6.4 mg/L 0.5 1 08/20/12 L56238-10 54.6 Dissolved Oxygen, Field 6.3 mg/L 0.5 1 08/20/12 L56238-11 99.2 Dissolved Oxygen, Field 6.3 mg/L 0.5 1 08/20/12 L56238-12 198 Dissolved Oxygen, Field 5.8 mg/L 0.5 1 08/20/12 L56238-13 198 Dissolved Oxygen, Field 5.8 mg/L 0.5 1 09/05/12 L56391-1 1 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 09/05/12 L56391-2 2.4 Dissolved Oxygen, Field 7.5 mg/L 0.5 1 09/17/12 L56394-6 0.99 Dissolved Oxygen, Field 9.3 mg/L 0.5 1 09/17/12 L56393-1 0.99 Dissolved Oxygen, Field 9.3 mg/L 0.5 1 09/17/12 L56393-2 3.5 Dissolved Oxygen, Field 9.2 mg/L 0.5 1 09/17/12 L56394-7 15 Dissolved Oxygen, Field 6.7 mg/L 0.5 1 09/17/12 L56394-8 24.9 Dissolved Oxygen, Field 6.0 mg/L 0.5 1 09/17/12 L56394-9 34.7 Dissolved Oxygen, Field 6.1 mg/L 0.5 1 09/17/12 L56394-10 54.2 Dissolved Oxygen, Field 6.1 mg/L 0.5 1 09/17/12 L56394-11 99.2 Dissolved Oxygen, Field 5.8 mg/L 0.5 1 09/17/12 L56394-12 198 Dissolved Oxygen, Field 5.6 mg/L 0.5 1 09/17/12 L56394-13 198 Dissolved Oxygen, Field 5.6 mg/L 0.5 1 10/03/12 L56648-1 0.95 Dissolved Oxygen, Field 12.2 mg/L 0.5 1 10/03/12 L56648-2 7.7 Dissolved Oxygen, Field 12.2 mg/L 0.5 1 10/16/12 L56533-6 1.3 Dissolved Oxygen, Field 6.4 mg/L 0.5 1Page 11 of 25 

## Table A-1
Complete Water Quality Monitoring Data for Station KSBP01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 10/16/12 L56533-7 15.1 Dissolved Oxygen, Field 6.3 mg/L 0.5 1 10/16/12 L56533-8 25.1 Dissolved Oxygen, Field 6.1 mg/L 0.5 1 10/16/12 L56533-9 35.1 Dissolved Oxygen, Field 6.0 mg/L 0.5 1 10/16/12 L56533-10 54.9 Dissolved Oxygen, Field 5.8 mg/L 0.5 1 10/16/12 L56533-11 99.3 Dissolved Oxygen, Field 5.7 mg/L 0.5 1 10/16/12 L56533-12 198 Dissolved Oxygen, Field 5.8 mg/L 0.5 1 10/16/12 L56533-13 199 Dissolved Oxygen, Field 5.8 mg/L 0.5 1 10/18/12 L56781-1 1.3 Dissolved Oxygen, Field 6.4 mg/L 0.5 1 10/18/12 L56781-2 5.7 Dissolved Oxygen, Field 6.2 mg/L 0.5 1 11/26/12 L56803-6 0.61 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 11/26/12 L56803-7 14.5 Dissolved Oxygen, Field 7.0 mg/L 0.5 1 11/26/12 L56803-8 24.4 Dissolved Oxygen, Field 6.8 mg/L 0.5 1 11/26/12 L56803-9 34.2 Dissolved Oxygen, Field 6.7 mg/L 0.5 1 11/26/12 L56803-10 54.1 Dissolved Oxygen, Field 6.6 mg/L 0.5 1 11/26/12 L56803-11 98.6 Dissolved Oxygen, Field 6.3 mg/L 0.5 1 11/26/12 L56803-12 198 Dissolved Oxygen, Field 6.2 mg/L 0.5 1 11/26/12 L56803-13 198 Dissolved Oxygen, Field 6.2 mg/L 0.5 1 12/12/12 L56990-1 4.9 Dissolved Oxygen, Field 8.1 mg/L 0.5 1 12/12/12 L56990-2 49.3 Dissolved Oxygen, Field 7.5 mg/L 0.5 1 12/12/12 L56990-3 198 Dissolved Oxygen, Field 6.0 mg/L 0.5 1 12/18/12 L57085-6 0.45 Dissolved Oxygen, Field 7.5 mg/L JL 0.5 1 12/18/12 L57085-7 14.4 Dissolved Oxygen, Field 7.3 mg/L JL 0.5 1 12/18/12 L57085-8 24.2 Dissolved Oxygen, Field 7.2 mg/L JL 0.5 1 12/18/12 L57085-9 34 Dissolved Oxygen, Field 7.1 mg/L JL 0.5 1 12/18/12 L57085-10 53.8 Dissolved Oxygen, Field 7.1 mg/L JL 0.5 1 12/18/12 L57085-11 98.6 Dissolved Oxygen, Field 6.9 mg/L JL 0.5 1 12/18/12 L57085-12 197 Dissolved Oxygen, Field 6.0 mg/L JL 0.5 1 12/18/12 L57085-13 198 Dissolved Oxygen, Field 6.0 mg/L JL 0.5 1 08/15/11 L53889-6 1.3 Total Suspended Solids 2.9 mg/L <RDL 0.5 10 08/15/11 L53889-7 15.1 Total Suspended Solids 1.7 mg/L <RDL 0.5 10 08/15/11 L53889-8 25 Total Suspended Solids 1.5 mg/L <RDL 0.5 10 08/15/11 L53889-9 34.8 Total Suspended Solids 1.5 mg/L <RDL 0.5 10 08/15/11 L53889-10 54.5 Total Suspended Solids 2.2 mg/L <RDL 0.5 10 08/15/11 L53889-11 99.3 Total Suspended Solids 1.6 mg/L <RDL 0.5 10 08/15/11 L53889-12 198 Total Suspended Solids 2.1 mg/L <RDL 0.5 10 08/15/11 L53889-13 198 Total Suspended Solids 2.7 mg/L <RDL 0.5 10 09/19/11 L54019-6 1.2 Total Suspended Solids 1.6 mg/L <RDL 0.5 10 09/19/11 L54019-7 15 Total Suspended Solids 1.3 mg/L <RDL 0.5 10 09/19/11 L54019-8 24.9 Total Suspended Solids 0.9 mg/L <RDL 0.5 10 09/19/11 L54019-9 34.8 Total Suspended Solids 1.2 mg/L <RDL 0.5 10 09/19/11 L54019-10 54.6 Total Suspended Solids 1.5 mg/L <RDL 0.5 10 09/19/11 L54019-11 99.2 Total Suspended Solids 0.9 mg/L <RDL 0.5 10 09/19/11 L54019-12 198 Total Suspended Solids 1.6 mg/L <RDL 0.5 10 09/19/11 L54019-13 198 Total Suspended Solids 2.0 mg/L <RDL 0.5 10 10/17/11 L54269-6 1.1 Total Suspended Solids 1.4 mg/L <RDL 0.5 10 10/17/11 L54269-7 14.9 Total Suspended Solids 1.2 mg/L <RDL 0.5 10 10/17/11 L54269-8 24.8 Total Suspended Solids 0.5 mg/L <RDL 0.5 10 10/17/11 L54269-9 34.7 Total Suspended Solids 0.6 mg/L <RDL 0.5 10 10/17/11 L54269-10 54.5 Total Suspended Solids 0.9 mg/L <RDL 0.5 10 10/17/11 L54269-11 99.1 Total Suspended Solids 0.9 mg/L <RDL 0.5 10 10/17/11 L54269-13 198 Total Suspended Solids 2.0 mg/L <RDL 0.5 10 10/17/11 L54269-12 198 Total Suspended Solids 1.6 mg/L <RDL 1 20Page 12 of 25 

## Table A-1
Complete Water Quality Monitoring Data for Station KSBP01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 11/28/11 L54474-6 1.6 Total Suspended Solids 1.1 mg/L <RDL 0.5 10 11/28/11 L54474-7 14.9 Total Suspended Solids 1.1 mg/L <RDL 0.5 10 11/28/11 L54474-8 24.7 Total Suspended Solids 0.7 mg/L <RDL 0.5 10 11/28/11 L54474-9 34.7 Total Suspended Solids 1.2 mg/L <RDL 0.5 10 11/28/11 L54474-10 54.5 Total Suspended Solids 1.0 mg/L <RDL 0.5 10 11/28/11 L54474-11 99 Total Suspended Solids 1.0 mg/L <MDL 1 20 11/28/11 L54474-12 198 Total Suspended Solids 1.5 mg/L <RDL 0.5 10 11/28/11 L54474-13 198 Total Suspended Solids 1.7 mg/L <RDL 0.5 10 12/19/11 L54766-6 1 Total Suspended Solids 1.2 mg/L <RDL 0.5 10 12/19/11 L54766-7 14.8 Total Suspended Solids 1.1 mg/L <RDL 0.5 10 12/19/11 L54766-8 24.6 Total Suspended Solids 0.7 mg/L <RDL 0.5 10 12/19/11 L54766-9 34.6 Total Suspended Solids 1.2 mg/L <RDL 0.5 10 12/19/11 L54766-10 54.3 Total Suspended Solids 1.4 mg/L <RDL 0.5 10 12/19/11 L54766-11 98.9 Total Suspended Solids 1.0 mg/L <RDL 0.5 10 12/19/11 L54766-12 198 Total Suspended Solids 1.4 mg/L <RDL 0.5 10 12/19/11 L54766-13 198 Total Suspended Solids 1.6 mg/L <RDL 0.5 10 01/23/12 L54840-6 1.2 Total Suspended Solids 0.6 mg/L <RDL 0.5 10 01/23/12 L54840-7 15.1 Total Suspended Solids mg/L <MDL 0.5 10 01/23/12 L54840-8 25 Total Suspended Solids mg/L <MDL 0.5 10 01/23/12 L54840-9 34.9 Total Suspended Solids 0.5 mg/L <RDL 0.5 10 01/23/12 L54840-10 54.4 Total Suspended Solids 0.7 mg/L <RDL 0.5 10 01/23/12 L54840-11 99.1 Total Suspended Solids 1.3 mg/L <RDL 0.5 10 01/23/12 L54840-12 198 Total Suspended Solids 2.3 mg/L <RDL 0.5 10 01/23/12 L54840-13 199 Total Suspended Solids 2.3 mg/L <RDL 0.5 10 02/21/12 L55087-6 1.2 Total Suspended Solids 2.0 mg/L <RDL 0.5 10 02/21/12 L55087-7 15.1 Total Suspended Solids 0.7 mg/L <RDL 0.5 10 02/21/12 L55087-8 25 Total Suspended Solids 1.4 mg/L <RDL 0.5 10 02/21/12 L55087-9 34.9 Total Suspended Solids 1.0 mg/L <RDL 0.5 10 02/21/12 L55087-10 54.7 Total Suspended Solids 1.3 mg/L <RDL 0.5 10 02/21/12 L55087-11 99.4 Total Suspended Solids 2.5 mg/L <RDL 0.5 10 02/21/12 L55087-12 198 Total Suspended Solids 2.1 mg/L <RDL 0.5 10 02/21/12 L55087-13 198 Total Suspended Solids 1.9 mg/L <RDL 0.5 10 03/19/12 L55193-6 2.8 Total Suspended Solids 2.7 mg/L <RDL 0.5 10 03/19/12 L55193-7 16 Total Suspended Solids 1.3 mg/L <RDL 0.5 10 03/19/12 L55193-8 25 Total Suspended Solids 2.0 mg/L <RDL 0.5 10 03/19/12 L55193-9 34.9 Total Suspended Solids 2.1 mg/L <RDL 0.5 10 03/19/12 L55193-10 54.4 Total Suspended Solids 2.3 mg/L <RDL 0.5 10 03/19/12 L55193-11 99.2 Total Suspended Solids 2.1 mg/L <RDL 0.5 10 03/19/12 L55193-12 198 Total Suspended Solids 3.4 mg/L <RDL 0.5 10 03/19/12 L55193-13 198 Total Suspended Solids 2.1 mg/L <RDL 0.5 10 04/16/12 L55370-6 1.3 Total Suspended Solids 3.9 mg/L <RDL 0.5 11 04/16/12 L55370-7 15.1 Total Suspended Solids 2.7 mg/L <RDL 0.5 10 04/16/12 L55370-8 24.8 Total Suspended Solids 4.7 mg/L <RDL 0.5 10 04/16/12 L55370-9 34.7 Total Suspended Solids 4.0 mg/L <RDL 1 20 04/16/12 L55370-10 54.6 Total Suspended Solids 3.1 mg/L <RDL 0.5 10 04/16/12 L55370-11 99.2 Total Suspended Solids 2.0 mg/L <RDL 0.5 10 04/16/12 L55370-12 198 Total Suspended Solids 2.9 mg/L <RDL 0.5 10 04/16/12 L55370-13 198 Total Suspended Solids 4.7 mg/L <RDL 0.5 10 05/21/12 L55534-6 1.6 Total Suspended Solids 4.8 mg/L <RDL 1 20 05/21/12 L55534-7 15.1 Total Suspended Solids 3.5 mg/L <RDL 0.5 10 05/21/12 L55534-8 25 Total Suspended Solids 1.7 mg/L <RDL 0.5 10 05/21/12 L55534-9 34.8 Total Suspended Solids 2.7 mg/L <RDL 0.5 10Page 13 of 25 

## Table A-1
Complete Water Quality Monitoring Data for Station KSBP01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 05/21/12 L55534-10 54.6 Total Suspended Solids 2.9 mg/L <RDL 0.5 10 05/21/12 L55534-11 99.3 Total Suspended Solids 1.7 mg/L <RDL 0.5 10 05/21/12 L55534-12 198 Total Suspended Solids 4.3 mg/L <RDL 0.5 10 05/21/12 L55534-13 198 Total Suspended Solids 3.9 mg/L <RDL 0.5 10 06/18/12 L55788-6 1.3 Total Suspended Solids 3.7 mg/L <RDL 0.5 10 06/18/12 L55788-7 15.1 Total Suspended Solids 3.0 mg/L <RDL 0.5 10 06/18/12 L55788-8 24.8 Total Suspended Solids 2.2 mg/L <RDL 0.5 10 06/18/12 L55788-9 34.8 Total Suspended Solids 3.2 mg/L <RDL 0.5 10 06/18/12 L55788-10 54.6 Total Suspended Solids 2.3 mg/L <RDL 0.5 10 06/18/12 L55788-11 99.1 Total Suspended Solids 1.6 mg/L <RDL 0.5 10 06/18/12 L55788-12 198 Total Suspended Solids 7.0 mg/L <RDL 0.5 10 06/18/12 L55788-13 198 Total Suspended Solids 6.1 mg/L <RDL 0.5 10 07/16/12 L55944-6 1.3 Total Suspended Solids 5.6 mg/L <RDL 0.5 11 07/16/12 L55944-7 15 Total Suspended Solids 1.5 mg/L <RDL 0.5 10 07/16/12 L55944-8 24.3 Total Suspended Solids 2.4 mg/L <RDL 0.5 10 07/16/12 L55944-9 24.9 Total Suspended Solids 4.0 mg/L <RDL 0.5 10 07/16/12 L55944-10 34.9 Total Suspended Solids 2.5 mg/L <RDL 0.5 10 07/16/12 L55944-11 54.6 Total Suspended Solids 3.2 mg/L <RDL 0.5 10 07/16/12 L55944-12 99.2 Total Suspended Solids 2.2 mg/L <RDL 0.5 10 07/16/12 L55944-13 198 Total Suspended Solids 4.0 mg/L <RDL 0.5 10 08/20/12 L56238-6 1.2 Total Suspended Solids 6.7 mg/L <RDL 0.5 10 08/20/12 L56238-7 15 Total Suspended Solids 5.2 mg/L <RDL 0.5 10 08/20/12 L56238-8 24.8 Total Suspended Solids 2.2 mg/L <RDL 0.5 10 08/20/12 L56238-9 34.7 Total Suspended Solids 2.6 mg/L <RDL 0.5 10 08/20/12 L56238-10 54.6 Total Suspended Solids 3.9 mg/L <RDL 0.5 10 08/20/12 L56238-11 99.2 Total Suspended Solids 2.2 mg/L <RDL 0.5 10 08/20/12 L56238-12 198 Total Suspended Solids 3.3 mg/L <RDL 0.5 10 08/20/12 L56238-13 198 Total Suspended Solids 4.2 mg/L <RDL 0.5 10 09/17/12 L56394-6 0.99 Total Suspended Solids 4.9 mg/L <RDL 0.5 10 09/17/12 L56394-7 15 Total Suspended Solids 3.0 mg/L <RDL 0.5 10 09/17/12 L56394-8 24.9 Total Suspended Solids 5.2 mg/L <RDL 0.5 10 09/17/12 L56394-9 34.7 Total Suspended Solids 3.6 mg/L <RDL 0.5 10 09/17/12 L56394-10 54.2 Total Suspended Solids 5.0 mg/L <RDL 1 20 09/17/12 L56394-11 99.2 Total Suspended Solids 3.9 mg/L <RDL 0.5 10 09/17/12 L56394-12 198 Total Suspended Solids 3.7 mg/L <RDL 0.5 10 09/17/12 L56394-13 198 Total Suspended Solids 3.5 mg/L <RDL 0.5 10 10/16/12 L56533-6 1.3 Total Suspended Solids 2.2 mg/L <RDL 0.5 10 10/16/12 L56533-7 15.1 Total Suspended Solids 5.5 mg/L <RDL 0.5 10 10/16/12 L56533-8 25.1 Total Suspended Solids 2.2 mg/L <RDL 0.5 10 10/16/12 L56533-9 35.1 Total Suspended Solids 2.4 mg/L <RDL 0.5 10 10/16/12 L56533-10 54.9 Total Suspended Solids 2.8 mg/L <RDL 0.5 10 10/16/12 L56533-11 99.3 Total Suspended Solids 1.9 mg/L <RDL 0.5 10 10/16/12 L56533-12 198 Total Suspended Solids 4.7 mg/L <RDL 0.5 10 10/16/12 L56533-13 199 Total Suspended Solids 3.5 mg/L <RDL 0.5 10 11/26/12 L56803-6 0.61 Total Suspended Solids 1.7 mg/L <RDL 0.5 10 11/26/12 L56803-7 14.5 Total Suspended Solids 2.2 mg/L <RDL 0.5 10 11/26/12 L56803-8 24.4 Total Suspended Solids 1.4 mg/L <RDL 1 20 11/26/12 L56803-9 34.2 Total Suspended Solids 3.0 mg/L <RDL 0.5 10 11/26/12 L56803-10 54.1 Total Suspended Solids 1.2 mg/L <RDL 0.5 10 11/26/12 L56803-11 98.6 Total Suspended Solids 1.8 mg/L <RDL 0.5 10 11/26/12 L56803-12 198 Total Suspended Solids 2.3 mg/L <RDL 0.5 10 11/26/12 L56803-13 198 Total Suspended Solids 2.9 mg/L <RDL 0.5 10Page 14 of 25 

## Table A-1
Complete Water Quality Monitoring Data for Station KSBP01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 01/18/11 L52381-6 1.2 pH, Field 7.7 pH 01/18/11 L52381-7 15 pH, Field 7.7 pH 01/18/11 L52381-8 24.9 pH, Field 7.7 pH 01/18/11 L52381-9 34.8 pH, Field 7.7 pH 01/18/11 L52381-10 54.7 pH, Field 7.7 pH 01/18/11 L52381-11 99.3 pH, Field 7.7 pH 01/18/11 L52381-12 198 pH, Field 7.7 pH 01/18/11 L52381-13 198 pH, Field 7.7 pH 02/22/11 L52539-6 0.96 pH, Field 7.6 pH 02/22/11 L52539-7 14.8 pH, Field 7.7 pH 02/22/11 L52539-8 24.7 pH, Field 7.7 pH 02/22/11 L52539-9 34.6 pH, Field 7.7 pH 02/22/11 L52539-10 54.4 pH, Field 7.7 pH 02/22/11 L52539-11 98.9 pH, Field 7.7 pH 02/22/11 L52539-12 197 pH, Field 7.7 pH 02/22/11 L52539-13 198 pH, Field 7.7 pH 03/21/11 L52727-6 1.5 pH, Field 7.8 pH 03/21/11 L52727-7 15.3 pH, Field 7.8 pH 03/21/11 L52727-8 25.2 pH, Field 7.8 pH 03/21/11 L52727-9 35.1 pH, Field 7.8 pH 03/21/11 L52727-10 54.9 pH, Field 7.8 pH 03/21/11 L52727-11 99.6 pH, Field 7.7 pH 03/21/11 L52727-12 198 pH, Field 7.7 pH 03/21/11 L52727-13 198 pH, Field 7.7 pH 04/18/11 L52883-6 1.9 pH, Field 7.8 pH 04/18/11 L52883-7 16.1 pH, Field 7.8 pH 04/18/11 L52883-8 25.9 pH, Field 7.8 pH 04/18/11 L52883-9 35.9 pH, Field 7.8 pH 04/18/11 L52883-10 54.4 pH, Field 7.8 pH 04/18/11 L52883-11 99.1 pH, Field 7.8 pH 04/18/11 L52883-12 198 pH, Field 7.8 pH 04/18/11 L52883-13 198 pH, Field 7.8 pH 05/16/11 L53206-6 1.5 pH, Field 8.0 pH 05/16/11 L53206-7 15.2 pH, Field 7.9 pH 05/16/11 L53206-8 25 pH, Field 7.8 pH 05/16/11 L53206-9 35 pH, Field 7.8 pH 05/16/11 L53206-10 54.7 pH, Field 7.7 pH 05/16/11 L53206-11 99.4 pH, Field 7.7 pH 05/16/11 L53206-12 198 pH, Field 7.7 pH 05/16/11 L53206-13 198 pH, Field 7.7 pH 06/20/11 L53331-6 1.3 pH, Field 7.9 pH 06/20/11 L53331-7 15.1 pH, Field 7.8 pH 06/20/11 L53331-8 24.9 pH, Field 7.8 pH 06/20/11 L53331-9 34.8 pH, Field 7.8 pH 06/20/11 L53331-10 54.4 pH, Field 7.8 pH 06/20/11 L53331-11 99.1 pH, Field 7.7 pH 06/20/11 L53331-12 198 pH, Field 7.7 pH 06/20/11 L53331-13 198 pH, Field 7.7 pH 07/14/11 L53626-1 4.7 pH, Field 8.0 pH 07/14/11 L53626-2 49.3 pH, Field 7.8 pH 07/14/11 L53626-3 198 pH, Field 7.6 pH 07/18/11 L53542-6 1.2 pH, Field 7.9 pHPage 15 of 25 

## Table A-1
Complete Water Quality Monitoring Data for Station KSBP01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 07/18/11 L53542-7 15.1 pH, Field 7.8 pH 07/18/11 L53542-8 24.8 pH, Field 7.8 pH 07/18/11 L53542-9 34.8 pH, Field 7.8 pH 07/18/11 L53542-10 54.7 pH, Field 7.8 pH 07/18/11 L53542-11 99.3 pH, Field 7.7 pH 07/18/11 L53542-12 198 pH, Field 7.7 pH 07/18/11 L53542-13 198 pH, Field 7.7 pH 08/15/11 L53889-6 1.3 pH, Field 7.8 pH 08/15/11 L53889-7 15.1 pH, Field 7.8 pH 08/15/11 L53889-8 25 pH, Field 7.7 pH 08/15/11 L53889-9 34.8 pH, Field 7.7 pH 08/15/11 L53889-10 54.5 pH, Field 7.6 pH 08/15/11 L53889-11 99.3 pH, Field 7.6 pH 08/15/11 L53889-12 198 pH, Field 7.6 pH 08/15/11 L53889-13 198 pH, Field 7.6 pH 09/19/11 L54019-6 1.2 pH, Field 7.7 pH 09/19/11 L54019-7 15 pH, Field 7.6 pH 09/19/11 L54019-8 24.9 pH, Field 7.6 pH 09/19/11 L54019-9 34.8 pH, Field 7.6 pH 09/19/11 L54019-10 54.6 pH, Field 7.6 pH 09/19/11 L54019-11 99.2 pH, Field 7.6 pH 09/19/11 L54019-12 198 pH, Field 7.6 pH 09/19/11 L54019-13 198 pH, Field 7.6 pH 10/17/11 L54269-6 1.1 pH, Field 7.7 pH 10/17/11 L54269-7 14.9 pH, Field 7.6 pH 10/17/11 L54269-8 24.8 pH, Field 7.6 pH 10/17/11 L54269-9 34.7 pH, Field 7.6 pH 10/17/11 L54269-10 54.5 pH, Field 7.5 pH 10/17/11 L54269-11 99.1 pH, Field 7.5 pH 10/17/11 L54269-12 198 pH, Field 7.5 pH 10/17/11 L54269-13 198 pH, Field 7.5 pH 11/28/11 L54474-6 1.6 pH, Field 7.5 pH 11/28/11 L54474-7 14.9 pH, Field 7.5 pH 11/28/11 L54474-8 24.7 pH, Field 7.5 pH 11/28/11 L54474-9 34.7 pH, Field 7.5 pH 11/28/11 L54474-10 54.5 pH, Field 7.5 pH 11/28/11 L54474-11 99 pH, Field 7.5 pH 11/28/11 L54474-12 198 pH, Field 7.5 pH 11/28/11 L54474-13 198 pH, Field 7.5 pH 12/14/11 L54765-1 4.9 pH, Field 7.5 pH 12/14/11 L54765-2 49.5 pH, Field 7.5 pH 12/14/11 L54765-3 198 pH, Field 7.5 pH 12/19/11 L54766-6 1 pH, Field 7.5 pH 12/19/11 L54766-7 14.8 pH, Field 7.5 pH 12/19/11 L54766-8 24.6 pH, Field 7.5 pH 12/19/11 L54766-9 34.6 pH, Field 7.5 pH 12/19/11 L54766-10 54.3 pH, Field 7.5 pH 12/19/11 L54766-11 98.9 pH, Field 7.5 pH 12/19/11 L54766-12 198 pH, Field 7.5 pH 12/19/11 L54766-13 198 pH, Field 7.5 pH 07/30/12 L56062-1 4.8 pH, Field 7.8 pH 07/30/12 L56062-2 49.4 pH, Field 7.6 pHPage 16 of 25 

## Table A-1
Complete Water Quality Monitoring Data for Station KSBP01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 07/30/12 L56062-3 198 pH, Field 7.6 pH 12/12/12 L56990-1 4.9 pH, Field 7.6 pH 12/12/12 L56990-2 49.3 pH, Field 7.6 pH 12/12/12 L56990-3 198 pH, Field 7.5 pH 01/18/11 L52381-6 1.2 Salinity, Field 26.712 PSS 01/18/11 L52381-7 15 Salinity, Field 28.468 PSS 01/18/11 L52381-8 24.9 Salinity, Field 28.911 PSS 01/18/11 L52381-9 34.8 Salinity, Field 29.240 PSS 01/18/11 L52381-10 54.7 Salinity, Field 29.424 PSS 01/18/11 L52381-11 99.3 Salinity, Field 29.505 PSS 01/18/11 L52381-12 198 Salinity, Field 29.747 PSS 01/18/11 L52381-13 198 Salinity, Field 29.747 PSS 02/22/11 L52539-6 0.96 Salinity, Field 28.040 PSS 02/22/11 L52539-7 14.8 Salinity, Field 28.776 PSS 02/22/11 L52539-8 24.7 Salinity, Field 29.013 PSS 02/22/11 L52539-9 34.6 Salinity, Field 29.053 PSS 02/22/11 L52539-10 54.4 Salinity, Field 29.120 PSS 02/22/11 L52539-11 98.9 Salinity, Field 29.280 PSS 02/22/11 L52539-12 197 Salinity, Field 29.452 PSS 02/22/11 L52539-13 198 Salinity, Field 29.452 PSS 03/21/11 L52727-6 1.5 Salinity, Field 27.950 PSS 03/21/11 L52732-1 1.5 Salinity, Field 27.950 PSS 03/21/11 L52732-2 6 Salinity, Field 28.849 PSS 03/21/11 L52727-7 15.3 Salinity, Field 28.719 PSS 03/21/11 L52727-8 25.2 Salinity, Field 28.931 PSS 03/21/11 L52727-9 35.1 Salinity, Field 28.970 PSS 03/21/11 L52727-10 54.9 Salinity, Field 29.025 PSS 03/21/11 L52727-11 99.6 Salinity, Field 29.184 PSS 03/21/11 L52727-12 198 Salinity, Field 29.570 PSS 03/21/11 L52727-13 198 Salinity, Field 29.571 PSS 04/04/11 L52882-1 1.2 Salinity, Field 27.692 PSS 04/04/11 L52882-2 2.5 Salinity, Field 27.834 PSS 04/18/11 L52886-1 1.9 Salinity, Field 26.157 PSS 04/18/11 L52883-6 1.9 Salinity, Field 26.157 PSS 04/18/11 L52886-2 6.6 Salinity, Field 27.182 PSS 04/18/11 L52883-7 16.1 Salinity, Field 28.309 PSS 04/18/11 L52883-8 25.9 Salinity, Field 28.614 PSS 04/18/11 L52883-9 35.9 Salinity, Field 28.663 PSS 04/18/11 L52883-10 54.4 Salinity, Field 28.785 PSS 04/18/11 L52883-11 99.1 Salinity, Field 28.905 PSS 04/18/11 L52883-12 198 Salinity, Field 29.217 PSS 04/18/11 L52883-13 198 Salinity, Field 29.218 PSS 05/04/11 L53125-1 1.2 Salinity, Field 27.229 PSS 05/04/11 L53125-2 5.5 Salinity, Field 27.504 PSS 05/16/11 L53206-6 1.5 Salinity, Field 27.886 PSS 05/16/11 L53209-1 1.5 Salinity, Field 27.886 PSS 05/16/11 L53209-2 2.9 Salinity, Field 27.893 PSS 05/16/11 L53206-7 15.2 Salinity, Field 28.382 PSS 05/16/11 L53206-8 25 Salinity, Field 28.531 PSS 05/16/11 L53206-9 35 Salinity, Field 28.678 PSS 05/16/11 L53206-10 54.7 Salinity, Field 28.809 PSS 05/16/11 L53206-11 99.4 Salinity, Field 29.224 PSSPage 17 of 25 

## Table A-1
Complete Water Quality Monitoring Data for Station KSBP01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 05/16/11 L53206-12 198 Salinity, Field 29.571 PSS 05/16/11 L53206-13 198 Salinity, Field 29.576 PSS 06/08/11 L53226-1 1.2 Salinity, Field 28.171 PSS 06/08/11 L53226-2 2.6 Salinity, Field 28.222 PSS 06/20/11 L53429-1 1.3 Salinity, Field 27.964 PSS 06/20/11 L53331-6 1.3 Salinity, Field 27.964 PSS 06/20/11 L53429-2 2.8 Salinity, Field 28.014 PSS 06/20/11 L53331-7 15.1 Salinity, Field 28.866 PSS 06/20/11 L53331-8 24.9 Salinity, Field 28.982 PSS 06/20/11 L53331-9 34.8 Salinity, Field 29.036 PSS 06/20/11 L53331-10 54.4 Salinity, Field 29.175 PSS 06/20/11 L53331-11 99.1 Salinity, Field 29.522 PSS 06/20/11 L53331-12 198 Salinity, Field 29.635 PSS 06/20/11 L53331-13 198 Salinity, Field 29.634 PSS 07/06/11 L53327-1 1.3 Salinity, Field 26.597 PSS 07/06/11 L53327-2 3.6 Salinity, Field 27.697 PSS 07/14/11 L53626-1 4.7 Salinity, Field 28.552 PSS 07/14/11 L53626-2 49.3 Salinity, Field 29.132 PSS 07/14/11 L53626-3 198 Salinity, Field 29.773 PSS 07/18/11 L53542-6 1.2 Salinity, Field 28.752 PSS 07/18/11 L53545-1 1.2 Salinity, Field 28.817 PSS 07/18/11 L53545-2 3.6 Salinity, Field 28.860 PSS 07/18/11 L53542-7 15.1 Salinity, Field 29.113 PSS 07/18/11 L53542-8 24.8 Salinity, Field 29.194 PSS 07/18/11 L53542-9 34.8 Salinity, Field 29.222 PSS 07/18/11 L53542-10 54.7 Salinity, Field 29.357 PSS 07/18/11 L53542-11 99.3 Salinity, Field 29.653 PSS 07/18/11 L53542-12 198 Salinity, Field 29.708 PSS 07/18/11 L53542-13 198 Salinity, Field 29.709 PSS 08/03/11 L53731-1 1.2 Salinity, Field 28.573 PSS 08/03/11 L53731-2 2.7 Salinity, Field 28.440 PSS 08/15/11 L53889-6 1.3 Salinity, Field 29.012 PSS 08/15/11 L53892-1 1.3 Salinity, Field 29.012 PSS 08/15/11 L53892-2 3.8 Salinity, Field 29.047 PSS 08/15/11 L53889-7 15.1 Salinity, Field 29.154 PSS 08/15/11 L53889-8 25 Salinity, Field 29.422 PSS 08/15/11 L53889-9 34.8 Salinity, Field 29.468 PSS 08/15/11 L53889-10 54.5 Salinity, Field 29.572 PSS 08/15/11 L53889-11 99.3 Salinity, Field 29.729 PSS 08/15/11 L53889-12 198 Salinity, Field 29.887 PSS 08/15/11 L53889-13 198 Salinity, Field 29.887 PSS 09/07/11 L54044-1 1.2 Salinity, Field 29.483 PSS 09/07/11 L54044-2 2.6 Salinity, Field 29.490 PSS 09/19/11 L54019-6 1.2 Salinity, Field 29.722 PSS 09/19/11 L54022-1 1.2 Salinity, Field 29.722 PSS 09/19/11 L54022-2 8.1 Salinity, Field 29.733 PSS 09/19/11 L54019-7 15 Salinity, Field 29.767 PSS 09/19/11 L54019-8 24.9 Salinity, Field 29.834 PSS 09/19/11 L54019-9 34.8 Salinity, Field 29.934 PSS 09/19/11 L54019-10 54.6 Salinity, Field 30.155 PSS 09/19/11 L54019-11 99.2 Salinity, Field 30.255 PSS 09/19/11 L54019-12 198 Salinity, Field 30.356 PSSPage 18 of 25 

## Table A-1
Complete Water Quality Monitoring Data for Station KSBP01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 09/19/11 L54019-13 198 Salinity, Field 30.360 PSS 10/06/11 L54268-1 1.2 Salinity, Field 29.880 PSS 10/06/11 L54268-2 5.6 Salinity, Field 29.968 PSS 10/17/11 L54270-1 1.1 Salinity, Field 28.681 PSS 10/17/11 L54269-6 1.1 Salinity, Field 28.681 PSS 10/17/11 L54270-2 5.6 Salinity, Field 29.028 PSS 10/17/11 L54269-7 14.9 Salinity, Field 29.773 PSS 10/17/11 L54269-8 24.8 Salinity, Field 30.169 PSS 10/17/11 L54269-9 34.7 Salinity, Field 30.170 PSS 10/17/11 L54269-10 54.5 Salinity, Field 30.217 PSS 10/17/11 L54269-11 99.1 Salinity, Field 30.336 PSS 10/17/11 L54269-12 198 Salinity, Field 30.367 PSS 10/17/11 L54269-13 198 Salinity, Field 30.367 PSS 11/28/11 L54474-6 1.6 Salinity, Field 29.828 PSS 11/28/11 L54474-7 14.9 Salinity, Field 29.902 PSS 11/28/11 L54474-8 24.7 Salinity, Field 30.092 PSS 11/28/11 L54474-9 34.7 Salinity, Field 30.114 PSS 11/28/11 L54474-10 54.5 Salinity, Field 30.114 PSS 11/28/11 L54474-11 99 Salinity, Field 30.171 PSS 11/28/11 L54474-12 198 Salinity, Field 30.211 PSS 11/28/11 L54474-13 198 Salinity, Field 30.213 PSS 12/14/11 L54765-1 4.9 Salinity, Field 29.384 PSS 12/14/11 L54765-2 49.5 Salinity, Field 29.879 PSS 12/14/11 L54765-3 198 Salinity, Field 29.966 PSS 12/19/11 L54766-6 1 Salinity, Field 29.538 PSS 12/19/11 L54766-7 14.8 Salinity, Field 29.746 PSS 12/19/11 L54766-8 24.6 Salinity, Field 29.855 PSS 12/19/11 L54766-9 34.6 Salinity, Field 29.878 PSS 12/19/11 L54766-10 54.3 Salinity, Field 29.919 PSS 12/19/11 L54766-11 98.9 Salinity, Field 29.937 PSS 12/19/11 L54766-12 198 Salinity, Field 30.049 PSS 12/19/11 L54766-13 198 Salinity, Field 30.056 PSS 01/23/12 L54840-6 1.2 Salinity, Field 29.320 PSS 01/23/12 L54840-7 15.1 Salinity, Field 29.586 PSS 01/23/12 L54840-8 25 Salinity, Field 29.775 PSS 01/23/12 L54840-9 34.9 Salinity, Field 29.777 PSS 01/23/12 L54840-10 54.4 Salinity, Field 29.829 PSS 01/23/12 L54840-11 99.1 Salinity, Field 29.888 PSS 01/23/12 L54840-12 198 Salinity, Field 29.900 PSS 01/23/12 L54840-13 199 Salinity, Field 29.901 PSS 02/21/12 L55087-6 1.2 Salinity, Field 29.263 PSS 02/21/12 L55087-7 15.1 Salinity, Field 29.390 PSS 02/21/12 L55087-8 25 Salinity, Field 29.419 PSS 02/21/12 L55087-9 34.9 Salinity, Field 29.442 PSS 02/21/12 L55087-10 54.7 Salinity, Field 29.522 PSS 02/21/12 L55087-11 99.4 Salinity, Field 29.701 PSS 02/21/12 L55087-12 198 Salinity, Field 29.752 PSS 02/21/12 L55087-13 198 Salinity, Field 29.752 PSS 03/19/12 L55193-6 2.8 Salinity, Field 26.061 PSS 03/19/12 L55193-7 16 Salinity, Field 29.118 PSS 03/19/12 L55193-8 25 Salinity, Field 29.276 PSS 03/19/12 L55193-9 34.9 Salinity, Field 29.350 PSSPage 19 of 25 

## Table A-1
Complete Water Quality Monitoring Data for Station KSBP01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 03/19/12 L55193-10 54.4 Salinity, Field 29.578 PSS 03/19/12 L55193-11 99.2 Salinity, Field 29.697 PSS 03/19/12 L55193-12 198 Salinity, Field 29.940 PSS 03/19/12 L55193-13 198 Salinity, Field 29.940 PSS 04/03/12 L55355-1 1.2 Salinity, Field 28.770 PSS 04/03/12 L55355-2 5.3 Salinity, Field 28.806 PSS 04/16/12 L55373-1 1.3 Salinity, Field 28.185 PSS 04/16/12 L55370-6 1.3 Salinity, Field 28.185 PSS 04/16/12 L55373-2 3.8 Salinity, Field 28.470 PSS 04/16/12 L55370-7 15.1 Salinity, Field 28.823 PSS 04/16/12 L55370-8 24.8 Salinity, Field 28.926 PSS 04/16/12 L55370-9 34.7 Salinity, Field 29.154 PSS 04/16/12 L55370-10 54.6 Salinity, Field 29.210 PSS 04/16/12 L55370-11 99.2 Salinity, Field 29.263 PSS 04/16/12 L55370-12 198 Salinity, Field 29.506 PSS 04/16/12 L55370-13 198 Salinity, Field 29.506 PSS 05/09/12 L55525-1 1.2 Salinity, Field 26.762 PSS 05/09/12 L55525-2 3.5 Salinity, Field 26.902 PSS 05/21/12 L55535-1 1.6 Salinity, Field 27.602 PSS 05/21/12 L55534-6 1.6 Salinity, Field 27.602 PSS 05/21/12 L55535-2 3.9 Salinity, Field 27.817 PSS 05/21/12 L55534-7 15.1 Salinity, Field 28.568 PSS 05/21/12 L55534-8 25 Salinity, Field 28.754 PSS 05/21/12 L55534-9 34.8 Salinity, Field 28.812 PSS 05/21/12 L55534-10 54.6 Salinity, Field 28.896 PSS 05/21/12 L55534-11 99.3 Salinity, Field 29.161 PSS 05/21/12 L55534-12 198 Salinity, Field 29.539 PSS 05/21/12 L55534-13 198 Salinity, Field 29.539 PSS 06/06/12 L55730-1 1.1 Salinity, Field 26.811 PSS 06/06/12 L55730-2 3.5 Salinity, Field 27.160 PSS 06/18/12 L55788-6 1.3 Salinity, Field 26.778 PSS 06/18/12 L55791-1 1.3 Salinity, Field 26.778 PSS 06/18/12 L55791-2 2.7 Salinity, Field 27.301 PSS 06/18/12 L55788-7 15.1 Salinity, Field 28.763 PSS 06/18/12 L55788-8 24.8 Salinity, Field 28.880 PSS 06/18/12 L55788-9 34.8 Salinity, Field 29.006 PSS 06/18/12 L55788-10 54.6 Salinity, Field 29.305 PSS 06/18/12 L55788-11 99.1 Salinity, Field 29.475 PSS 06/18/12 L55788-12 198 Salinity, Field 29.944 PSS 06/18/12 L55788-13 198 Salinity, Field 29.945 PSS 07/03/12 L55889-1 1.3 Salinity, Field 26.277 PSS 07/03/12 L55889-2 2.6 Salinity, Field 26.669 PSS 07/16/12 L55944-6 1.3 Salinity, Field 27.861 PSS 07/16/12 L55946-1 1.3 Salinity, Field 27.861 PSS 07/16/12 L55946-2 2.8 Salinity, Field 27.861 PSS 07/16/12 L55944-7 15 Salinity, Field 28.348 PSS 07/16/12 L55944-8 24.3 Salinity, Field 28.947 PSS 07/16/12 L55944-9 24.9 Salinity, Field 28.954 PSS 07/16/12 L55944-10 34.9 Salinity, Field 29.052 PSS 07/16/12 L55944-11 54.6 Salinity, Field 29.464 PSS 07/16/12 L55944-12 99.2 Salinity, Field 29.692 PSS 07/16/12 L55944-13 198 Salinity, Field 30.000 PSSPage 20 of 25 

## Table A-1
Complete Water Quality Monitoring Data for Station KSBP01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 07/30/12 L56062-1 4.8 Salinity, Field 28.804 PSS 07/30/12 L56062-2 49.4 Salinity, Field 29.353 PSS 07/30/12 L56062-3 198 Salinity, Field 29.965 PSS 08/08/12 L56173-1 1.1 Salinity, Field 28.982 PSS 08/08/12 L56173-2 2.6 Salinity, Field 29.013 PSS 08/20/12 L56174-1 1.2 Salinity, Field 28.873 PSS 08/20/12 L56238-6 1.2 Salinity, Field 28.873 PSS 08/20/12 L56174-2 5.6 Salinity, Field 28.896 PSS 08/20/12 L56238-7 15 Salinity, Field 29.209 PSS 08/20/12 L56238-8 24.8 Salinity, Field 29.348 PSS 08/20/12 L56238-9 34.7 Salinity, Field 29.559 PSS 08/20/12 L56238-10 54.6 Salinity, Field 29.664 PSS 08/20/12 L56238-11 99.2 Salinity, Field 29.836 PSS 08/20/12 L56238-12 198 Salinity, Field 29.970 PSS 08/20/12 L56238-13 198 Salinity, Field 29.979 PSS 09/05/12 L56391-1 1 Salinity, Field 29.482 PSS 09/05/12 L56391-2 2.4 Salinity, Field 29.471 PSS 09/17/12 L56394-6 0.99 Salinity, Field 29.521 PSS 09/17/12 L56393-1 0.99 Salinity, Field 29.521 PSS 09/17/12 L56393-2 3.5 Salinity, Field 29.522 PSS 09/17/12 L56394-7 15 Salinity, Field 29.722 PSS 09/17/12 L56394-8 24.9 Salinity, Field 29.923 PSS 09/17/12 L56394-9 34.7 Salinity, Field 29.983 PSS 09/17/12 L56394-10 54.2 Salinity, Field 30.069 PSS 09/17/12 L56394-11 99.2 Salinity, Field 30.096 PSS 09/17/12 L56394-12 198 Salinity, Field 30.428 PSS 09/17/12 L56394-13 198 Salinity, Field 30.431 PSS 10/03/12 L56648-1 0.95 Salinity, Field 29.951 PSS 10/03/12 L56648-2 7.7 Salinity, Field 29.951 PSS 10/16/12 L56533-6 1.3 Salinity, Field 30.091 PSS 10/16/12 L56533-7 15.1 Salinity, Field 30.128 PSS 10/16/12 L56533-8 25.1 Salinity, Field 30.210 PSS 10/16/12 L56533-9 35.1 Salinity, Field 30.233 PSS 10/16/12 L56533-10 54.9 Salinity, Field 30.400 PSS 10/16/12 L56533-11 99.3 Salinity, Field 30.469 PSS 10/16/12 L56533-12 198 Salinity, Field 30.719 PSS 10/16/12 L56533-13 199 Salinity, Field 30.719 PSS 10/18/12 L56781-1 1.3 Salinity, Field 30.163 PSS 10/18/12 L56781-2 5.7 Salinity, Field 30.166 PSS 11/26/12 L56803-6 0.61 Salinity, Field 26.647 PSS 11/26/12 L56803-7 14.5 Salinity, Field 29.331 PSS 11/26/12 L56803-8 24.4 Salinity, Field 29.724 PSS 11/26/12 L56803-9 34.2 Salinity, Field 29.866 PSS 11/26/12 L56803-10 54.1 Salinity, Field 29.933 PSS 11/26/12 L56803-11 98.6 Salinity, Field 30.177 PSS 11/26/12 L56803-12 198 Salinity, Field 30.246 PSS 11/26/12 L56803-13 198 Salinity, Field 30.246 PSS 12/12/12 L56990-1 4.9 Salinity, Field 28.567 PSS 12/12/12 L56990-2 49.3 Salinity, Field 29.441 PSS 12/12/12 L56990-3 198 Salinity, Field 29.943 PSS 12/18/12 L57085-6 0.45 Salinity, Field 29.420 PSS 12/18/12 L57085-7 14.4 Salinity, Field 29.437 PSSPage 21 of 25 

## Table A-1
Complete Water Quality Monitoring Data for Station KSBP01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 12/18/12 L57085-8 24.2 Salinity, Field 29.438 PSS 12/18/12 L57085-9 34 Salinity, Field 29.448 PSS 12/18/12 L57085-10 53.8 Salinity, Field 29.503 PSS 12/18/12 L57085-11 98.6 Salinity, Field 29.507 PSS 12/18/12 L57085-12 197 Salinity, Field 29.867 PSS 12/18/12 L57085-13 198 Salinity, Field 29.871 PSS 07/14/11 L53626-1 4.7 Arsenic, Dissolved, ICP-MS 1.15 ug/L 0.01 0.05 07/14/11 L53626-2 49.3 Arsenic, Dissolved, ICP-MS 1.26 ug/L 0.01 0.05 07/14/11 L53626-3 198 Arsenic, Dissolved, ICP-MS 1.32 ug/L 0.01 0.05 12/14/11 L54765-1 4.9 Arsenic, Dissolved, ICP-MS 1.36 ug/L 0.01 0.05 12/14/11 L54765-2 49.5 Arsenic, Dissolved, ICP-MS 1.37 ug/L 0.01 0.05 12/14/11 L54765-3 198 Arsenic, Dissolved, ICP-MS 1.39 ug/L 0.01 0.05 07/30/12 L56062-1 4.8 Arsenic, Dissolved, ICP-MS 1.15 ug/L 0.01 0.05 07/30/12 L56062-2 49.4 Arsenic, Dissolved, ICP-MS 1.35 ug/L 0.01 0.05 07/30/12 L56062-3 198 Arsenic, Dissolved, ICP-MS 1.39 ug/L 0.01 0.05 12/12/12 L56990-1 4.9 Arsenic, Dissolved, ICP-MS 1.37 ug/L 0.01 0.05 12/12/12 L56990-2 49.3 Arsenic, Dissolved, ICP-MS 1.38 ug/L 0.01 0.05 12/12/12 L56990-3 198 Arsenic, Dissolved, ICP-MS 1.43 ug/L 0.01 0.05 07/14/11 L53626-1 4.7 Arsenic, Total, ICP-MS 1.11 ug/L 0.01 0.05 07/14/11 L53626-2 49.3 Arsenic, Total, ICP-MS 1.13 ug/L 0.01 0.05 07/14/11 L53626-3 198 Arsenic, Total, ICP-MS 1.33 ug/L 0.01 0.05 12/14/11 L54765-1 4.9 Arsenic, Total, ICP-MS 1.34 ug/L 0.01 0.05 12/14/11 L54765-2 49.5 Arsenic, Total, ICP-MS 1.31 ug/L 0.01 0.05 12/14/11 L54765-3 198 Arsenic, Total, ICP-MS 1.32 ug/L 0.01 0.05 07/30/12 L56062-1 4.8 Arsenic, Total, ICP-MS 1.14 ug/L 0.01 0.05 07/30/12 L56062-2 49.4 Arsenic, Total, ICP-MS 1.31 ug/L 0.01 0.05 07/30/12 L56062-3 198 Arsenic, Total, ICP-MS 1.36 ug/L 0.01 0.05 12/12/12 L56990-1 4.9 Arsenic, Total, ICP-MS 1.34 ug/L 0.01 0.05 12/12/12 L56990-2 49.3 Arsenic, Total, ICP-MS 1.36 ug/L 0.01 0.05 12/12/12 L56990-3 198 Arsenic, Total, ICP-MS 1.41 ug/L 0.01 0.05 07/14/11 L53626-1 4.7 Cadmium, Dissolved, ICP-MS 0.0566 ug/L 0.005 0.025 07/14/11 L53626-2 49.3 Cadmium, Dissolved, ICP-MS 0.0605 ug/L 0.005 0.025 07/14/11 L53626-3 198 Cadmium, Dissolved, ICP-MS 0.0660 ug/L 0.005 0.025 12/14/11 L54765-1 4.9 Cadmium, Dissolved, ICP-MS 0.0692 ug/L 0.005 0.025 12/14/11 L54765-2 49.5 Cadmium, Dissolved, ICP-MS 0.0732 ug/L 0.005 0.025 12/14/11 L54765-3 198 Cadmium, Dissolved, ICP-MS 0.0704 ug/L 0.005 0.025 07/30/12 L56062-1 4.8 Cadmium, Dissolved, ICP-MS 0.0520 ug/L 0.005 0.025 07/30/12 L56062-2 49.4 Cadmium, Dissolved, ICP-MS 0.0651 ug/L 0.005 0.025 07/30/12 L56062-3 198 Cadmium, Dissolved, ICP-MS 0.0704 ug/L 0.005 0.025 12/12/12 L56990-1 4.9 Cadmium, Dissolved, ICP-MS 0.0693 ug/L 0.005 0.025 12/12/12 L56990-2 49.3 Cadmium, Dissolved, ICP-MS 0.0709 ug/L 0.005 0.025 12/12/12 L56990-3 198 Cadmium, Dissolved, ICP-MS 0.0734 ug/L 0.005 0.025 07/14/11 L53626-1 4.7 Cadmium, Total, ICP-MS 0.0636 ug/L 0.005 0.025 07/14/11 L53626-2 49.3 Cadmium, Total, ICP-MS 0.0668 ug/L 0.005 0.025 07/14/11 L53626-3 198 Cadmium, Total, ICP-MS 0.0721 ug/L 0.005 0.025 12/14/11 L54765-1 4.9 Cadmium, Total, ICP-MS 0.0693 ug/L 0.005 0.025 12/14/11 L54765-2 49.5 Cadmium, Total, ICP-MS 0.0709 ug/L 0.005 0.025 12/14/11 L54765-3 198 Cadmium, Total, ICP-MS 0.0700 ug/L 0.005 0.025 07/30/12 L56062-1 4.8 Cadmium, Total, ICP-MS 0.0698 ug/L 0.005 0.025 07/30/12 L56062-2 49.4 Cadmium, Total, ICP-MS 0.0812 ug/L 0.005 0.025 07/30/12 L56062-3 198 Cadmium, Total, ICP-MS 0.0864 ug/L 0.005 0.025 12/12/12 L56990-1 4.9 Cadmium, Total, ICP-MS 0.074 ug/L 0.005 0.025Page 22 of 25 

## Table A-1
Complete Water Quality Monitoring Data for Station KSBP01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 12/12/12 L56990-2 49.3 Cadmium, Total, ICP-MS 0.0745 ug/L 0.005 0.025 12/12/12 L56990-3 198 Cadmium, Total, ICP-MS 0.0792 ug/L 0.005 0.025 07/14/11 L53626-1 4.7 Chromium, Dissolved, ICP-MS 0.099 ug/L <RDL 0.05 0.25 07/14/11 L53626-2 49.3 Chromium, Dissolved, ICP-MS 0.11 ug/L <RDL 0.05 0.25 07/14/11 L53626-3 198 Chromium, Dissolved, ICP-MS 0.11 ug/L <RDL 0.05 0.25 12/14/11 L54765-1 4.9 Chromium, Dissolved, ICP-MS 0.093 ug/L <RDL 0.05 0.25 12/14/11 L54765-2 49.5 Chromium, Dissolved, ICP-MS 0.11 ug/L <RDL 0.05 0.25 12/14/11 L54765-3 198 Chromium, Dissolved, ICP-MS 0.11 ug/L <RDL 0.05 0.25 07/30/12 L56062-1 4.8 Chromium, Dissolved, ICP-MS 0.15 ug/L <RDL 0.05 0.25 07/30/12 L56062-2 49.4 Chromium, Dissolved, ICP-MS 0.13 ug/L <RDL 0.05 0.25 07/30/12 L56062-3 198 Chromium, Dissolved, ICP-MS 0.15 ug/L <RDL 0.05 0.25 12/12/12 L56990-1 4.9 Chromium, Dissolved, ICP-MS 0.10 ug/L <RDL 0.05 0.25 12/12/12 L56990-2 49.3 Chromium, Dissolved, ICP-MS 0.11 ug/L <RDL 0.05 0.25 12/12/12 L56990-3 198 Chromium, Dissolved, ICP-MS 0.092 ug/L <RDL 0.05 0.25 07/14/11 L53626-1 4.7 Chromium, Total, ICP-MS 0.088 ug/L <RDL 0.05 0.25 07/14/11 L53626-2 49.3 Chromium, Total, ICP-MS 0.10 ug/L <RDL 0.05 0.25 07/14/11 L53626-3 198 Chromium, Total, ICP-MS 0.16 ug/L <RDL 0.05 0.25 12/14/11 L54765-1 4.9 Chromium, Total, ICP-MS 0.10 ug/L <RDL 0.05 0.25 12/14/11 L54765-2 49.5 Chromium, Total, ICP-MS 0.11 ug/L <RDL 0.05 0.25 12/14/11 L54765-3 198 Chromium, Total, ICP-MS 0.12 ug/L <RDL 0.05 0.25 07/30/12 L56062-1 4.8 Chromium, Total, ICP-MS 0.11 ug/L <RDL 0.05 0.25 07/30/12 L56062-2 49.4 Chromium, Total, ICP-MS 0.11 ug/L <RDL 0.05 0.25 07/30/12 L56062-3 198 Chromium, Total, ICP-MS 0.19 ug/L <RDL 0.05 0.25 12/12/12 L56990-1 4.9 Chromium, Total, ICP-MS 0.11 ug/L <RDL 0.05 0.25 12/12/12 L56990-2 49.3 Chromium, Total, ICP-MS 0.096 ug/L <RDL 0.05 0.25 12/12/12 L56990-3 198 Chromium, Total, ICP-MS 0.15 ug/L <RDL 0.05 0.25 07/14/11 L53626-1 4.7 Copper, Dissolved, ICP-MS 0.348 ug/L 0.025 0.125 07/14/11 L53626-2 49.3 Copper, Dissolved, ICP-MS 0.332 ug/L 0.025 0.125 07/14/11 L53626-3 198 Copper, Dissolved, ICP-MS 0.236 ug/L 0.025 0.125 12/14/11 L54765-1 4.9 Copper, Dissolved, ICP-MS 0.617 ug/L 0.025 0.125 12/14/11 L54765-2 49.5 Copper, Dissolved, ICP-MS 0.332 ug/L 0.025 0.125 12/14/11 L54765-3 198 Copper, Dissolved, ICP-MS 0.279 ug/L 0.025 0.125 07/30/12 L56062-1 4.8 Copper, Dissolved, ICP-MS 0.365 ug/L 0.025 0.125 07/30/12 L56062-2 49.4 Copper, Dissolved, ICP-MS 0.283 ug/L 0.025 0.125 07/30/12 L56062-3 198 Copper, Dissolved, ICP-MS 0.234 ug/L 0.025 0.125 12/12/12 L56990-1 4.9 Copper, Dissolved, ICP-MS 0.346 ug/L 0.025 0.125 12/12/12 L56990-2 49.3 Copper, Dissolved, ICP-MS 0.258 ug/L 0.025 0.125 12/12/12 L56990-3 198 Copper, Dissolved, ICP-MS 0.238 ug/L 0.025 0.125 07/14/11 L53626-1 4.7 Copper, Total, ICP-MS 0.377 ug/L 0.025 0.125 07/14/11 L53626-2 49.3 Copper, Total, ICP-MS 0.366 ug/L 0.025 0.125 07/14/11 L53626-3 198 Copper, Total, ICP-MS 0.412 ug/L 0.025 0.125 12/14/11 L54765-1 4.9 Copper, Total, ICP-MS 1.22 ug/L 0.025 0.125 12/14/11 L54765-2 49.5 Copper, Total, ICP-MS 0.367 ug/L 0.025 0.125 12/14/11 L54765-3 198 Copper, Total, ICP-MS 0.322 ug/L 0.025 0.125 07/30/12 L56062-1 4.8 Copper, Total, ICP-MS 0.390 ug/L 0.025 0.125 07/30/12 L56062-2 49.4 Copper, Total, ICP-MS 0.314 ug/L 0.025 0.125 07/30/12 L56062-3 198 Copper, Total, ICP-MS 0.395 ug/L 0.025 0.125 12/12/12 L56990-1 4.9 Copper, Total, ICP-MS 0.392 ug/L 0.025 0.125 12/12/12 L56990-2 49.3 Copper, Total, ICP-MS 0.315 ug/L 0.025 0.125 12/12/12 L56990-3 198 Copper, Total, ICP-MS 0.369 ug/L 0.025 0.125 07/14/11 L53626-1 4.7 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 07/14/11 L53626-2 49.3 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025Page 23 of 25 

## Table A-1
Complete Water Quality Monitoring Data for Station KSBP01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 07/14/11 L53626-3 198 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 12/14/11 L54765-1 4.9 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 12/14/11 L54765-2 49.5 Lead, Dissolved, ICP-MS 0.010 ug/L <RDL 0.005 0.025 12/14/11 L54765-3 198 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 07/30/12 L56062-1 4.8 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 07/30/12 L56062-2 49.4 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 07/30/12 L56062-3 198 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 12/12/12 L56990-1 4.9 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 12/12/12 L56990-2 49.3 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 12/12/12 L56990-3 198 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 07/14/11 L53626-1 4.7 Lead, Total, ICP-MS 0.0091 ug/L <RDL 0.005 0.025 07/14/11 L53626-2 49.3 Lead, Total, ICP-MS 0.0068 ug/L <RDL 0.005 0.025 07/14/11 L53626-3 198 Lead, Total, ICP-MS 0.0444 ug/L 0.005 0.025 12/14/11 L54765-1 4.9 Lead, Total, ICP-MS 0.019 ug/L <RDL 0.005 0.025 12/14/11 L54765-2 49.5 Lead, Total, ICP-MS 0.011 ug/L <RDL 0.005 0.025 12/14/11 L54765-3 198 Lead, Total, ICP-MS 0.013 ug/L <RDL 0.005 0.025 07/30/12 L56062-1 4.8 Lead, Total, ICP-MS 0.0098 ug/L <RDL 0.005 0.025 07/30/12 L56062-2 49.4 Lead, Total, ICP-MS 0.0098 ug/L <RDL 0.005 0.025 07/30/12 L56062-3 198 Lead, Total, ICP-MS 0.0408 ug/L 0.005 0.025 12/12/12 L56990-1 4.9 Lead, Total, ICP-MS 0.017 ug/L <RDL 0.005 0.025 12/12/12 L56990-2 49.3 Lead, Total, ICP-MS 0.014 ug/L <RDL 0.005 0.025 12/12/12 L56990-3 198 Lead, Total, ICP-MS 0.0460 ug/L 0.005 0.025 07/14/11 L53626-1 4.7 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 07/14/11 L53626-2 49.3 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 07/14/11 L53626-3 198 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 12/14/11 L54765-1 4.9 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 12/14/11 L54765-2 49.5 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 12/14/11 L54765-3 198 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 07/30/12 L56062-1 4.8 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 07/30/12 L56062-2 49.4 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 07/30/12 L56062-3 198 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 12/12/12 L56990-1 4.9 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 12/12/12 L56990-2 49.3 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 12/12/12 L56990-3 198 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 07/14/11 L53626-1 4.7 Mercury, Total, CVAF 0.00039 ug/L <RDL 0.0002 0.0005 07/14/11 L53626-2 49.3 Mercury, Total, CVAF 0.00025 ug/L <RDL 0.0002 0.0005 07/14/11 L53626-3 198 Mercury, Total, CVAF 0.00049 ug/L <RDL 0.0002 0.0005 12/14/11 L54765-1 4.9 Mercury, Total, CVAF ug/L <MDL 0.0002 0.0005 12/14/11 L54765-2 49.5 Mercury, Total, CVAF ug/L <MDL 0.0002 0.0005 12/14/11 L54765-3 198 Mercury, Total, CVAF 0.00020 ug/L <RDL 0.0002 0.0005 07/30/12 L56062-1 4.8 Mercury, Total, CVAF 0.00021 ug/L <RDL 0.0002 0.0005 07/30/12 L56062-2 49.4 Mercury, Total, CVAF ug/L <MDL 0.0002 0.0005 07/30/12 L56062-3 198 Mercury, Total, CVAF 0.00033 ug/L <RDL 0.0002 0.0005 12/12/12 L56990-1 4.9 Mercury, Total, CVAF 0.00034 ug/L <RDL 0.0002 0.0005 12/12/12 L56990-2 49.3 Mercury, Total, CVAF 0.00026 ug/L <RDL 0.0002 0.0005 12/12/12 L56990-3 198 Mercury, Total, CVAF 0.00055 ug/L 0.0002 0.0005 07/14/11 L53626-1 4.7 Nickel, Dissolved, ICP-MS 0.405 ug/L 0.025 0.125 07/14/11 L53626-2 49.3 Nickel, Dissolved, ICP-MS 0.398 ug/L 0.025 0.125 07/14/11 L53626-3 198 Nickel, Dissolved, ICP-MS 0.395 ug/L 0.025 0.125 12/14/11 L54765-1 4.9 Nickel, Dissolved, ICP-MS 0.415 ug/L 0.025 0.125 12/14/11 L54765-2 49.5 Nickel, Dissolved, ICP-MS 0.419 ug/L 0.025 0.125 12/14/11 L54765-3 198 Nickel, Dissolved, ICP-MS 0.408 ug/L 0.025 0.125Page 24 of 25 

## Table A-1
Complete Water Quality Monitoring Data for Station KSBP01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 07/30/12 L56062-1 4.8 Nickel, Dissolved, ICP-MS 0.387 ug/L 0.025 0.125 07/30/12 L56062-2 49.4 Nickel, Dissolved, ICP-MS 0.399 ug/L 0.025 0.125 07/30/12 L56062-3 198 Nickel, Dissolved, ICP-MS 0.391 ug/L 0.025 0.125 12/12/12 L56990-1 4.9 Nickel, Dissolved, ICP-MS 0.443 ug/L 0.025 0.125 12/12/12 L56990-2 49.3 Nickel, Dissolved, ICP-MS 0.414 ug/L 0.025 0.125 12/12/12 L56990-3 198 Nickel, Dissolved, ICP-MS 0.425 ug/L 0.025 0.125 07/14/11 L53626-1 4.7 Nickel, Total, ICP-MS 0.421 ug/L 0.025 0.125 07/14/11 L53626-2 49.3 Nickel, Total, ICP-MS 0.420 ug/L 0.025 0.125 07/14/11 L53626-3 198 Nickel, Total, ICP-MS 0.593 ug/L 0.025 0.125 12/14/11 L54765-1 4.9 Nickel, Total, ICP-MS 0.424 ug/L 0.025 0.125 12/14/11 L54765-2 49.5 Nickel, Total, ICP-MS 0.425 ug/L 0.025 0.125 12/14/11 L54765-3 198 Nickel, Total, ICP-MS 0.437 ug/L 0.025 0.125 07/30/12 L56062-1 4.8 Nickel, Total, ICP-MS 0.412 ug/L 0.025 0.125 07/30/12 L56062-2 49.4 Nickel, Total, ICP-MS 0.417 ug/L 0.025 0.125 07/30/12 L56062-3 198 Nickel, Total, ICP-MS 0.428 ug/L 0.025 0.125 12/12/12 L56990-1 4.9 Nickel, Total, ICP-MS 0.434 ug/L 0.025 0.125 12/12/12 L56990-2 49.3 Nickel, Total, ICP-MS 0.414 ug/L 0.025 0.125 12/12/12 L56990-3 198 Nickel, Total, ICP-MS 0.400 ug/L 0.025 0.125 07/14/11 L53626-1 4.7 Silver, Dissolved, ICP-MS 0.019 ug/L <RDL 0.01 0.05 07/14/11 L53626-2 49.3 Silver, Dissolved, ICP-MS 0.019 ug/L <RDL 0.01 0.05 07/14/11 L53626-3 198 Silver, Dissolved, ICP-MS 0.019 ug/L <RDL 0.01 0.05 12/14/11 L54765-1 4.9 Silver, Dissolved, ICP-MS 0.027 ug/L <RDL 0.01 0.05 12/14/11 L54765-2 49.5 Silver, Dissolved, ICP-MS 0.027 ug/L <RDL 0.01 0.05 12/14/11 L54765-3 198 Silver, Dissolved, ICP-MS 0.029 ug/L <RDL 0.01 0.05 07/30/12 L56062-1 4.8 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 07/30/12 L56062-2 49.4 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 07/30/12 L56062-3 198 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 12/12/12 L56990-1 4.9 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 12/12/12 L56990-2 49.3 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 12/12/12 L56990-3 198 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 07/14/11 L53626-1 4.7 Silver, Total, ICP-MS 0.016 ug/L <RDL 0.01 0.05 07/14/11 L53626-2 49.3 Silver, Total, ICP-MS 0.017 ug/L <RDL 0.01 0.05 07/14/11 L53626-3 198 Silver, Total, ICP-MS 0.017 ug/L <RDL 0.01 0.05 12/14/11 L54765-1 4.9 Silver, Total, ICP-MS 0.028 ug/L <RDL 0.01 0.05 12/14/11 L54765-2 49.5 Silver, Total, ICP-MS 0.030 ug/L <RDL 0.01 0.05 12/14/11 L54765-3 198 Silver, Total, ICP-MS 0.026 ug/L <RDL 0.01 0.05 07/30/12 L56062-1 4.8 Silver, Total, ICP-MS ug/L <MDL 0.01 0.05 07/30/12 L56062-2 49.4 Silver, Total, ICP-MS ug/L <MDL 0.01 0.05 07/30/12 L56062-3 198 Silver, Total, ICP-MS ug/L <MDL 0.01 0.05 12/12/12 L56990-1 4.9 Silver, Total, ICP-MS ug/L <MDL 0.01 0.05 12/12/12 L56990-2 49.3 Silver, Total, ICP-MS ug/L <MDL 0.01 0.05 12/12/12 L56990-3 198 Silver, Total, ICP-MS ug/L <MDL 0.01 0.05 07/14/11 L53626-1 4.7 Zinc, Dissolved, ICP-MS 0.635 ug/L 0.1 0.5 07/14/11 L53626-2 49.3 Zinc, Dissolved, ICP-MS 0.628 ug/L 0.1 0.5 07/14/11 L53626-3 198 Zinc, Dissolved, ICP-MS 0.644 ug/L 0.1 0.5 12/14/11 L54765-1 4.9 Zinc, Dissolved, ICP-MS 0.536 ug/L 0.1 0.5 12/14/11 L54765-2 49.5 Zinc, Dissolved, ICP-MS 0.694 ug/L 0.1 0.5 12/14/11 L54765-3 198 Zinc, Dissolved, ICP-MS 0.32 ug/L <RDL 0.1 0.5 07/30/12 L56062-1 4.8 Zinc, Dissolved, ICP-MS 0.17 ug/L <RDL 0.1 0.5 07/30/12 L56062-2 49.4 Zinc, Dissolved, ICP-MS 0.26 ug/L <RDL 0.1 0.5 07/30/12 L56062-3 198 Zinc, Dissolved, ICP-MS 0.23 ug/L <RDL 0.1 0.5 12/12/12 L56990-1 4.9 Zinc, Dissolved, ICP-MS 0.503 ug/L 0.1 0.5Page 25 of 25 

## Table A-1
Complete Water Quality Monitoring Data for Station KSBP01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 12/12/12 L56990-2 49.3 Zinc, Dissolved, ICP-MS 0.33 ug/L <RDL 0.1 0.5 12/12/12 L56990-3 198 Zinc, Dissolved, ICP-MS 0.31 ug/L <RDL 0.1 0.5 07/14/11 L53626-1 4.7 Zinc, Total, ICP-MS 0.89 ug/L <RDL 0.5 2.5 07/14/11 L53626-2 49.3 Zinc, Total, ICP-MS 0.519 ug/L 0.1 0.5 07/14/11 L53626-3 198 Zinc, Total, ICP-MS 0.700 ug/L 0.1 0.5 12/14/11 L54765-1 4.9 Zinc, Total, ICP-MS 0.539 ug/L 0.1 0.5 12/14/11 L54765-2 49.5 Zinc, Total, ICP-MS 0.41 ug/L <RDL 0.1 0.5 12/14/11 L54765-3 198 Zinc, Total, ICP-MS 0.37 ug/L <RDL 0.1 0.5 07/30/12 L56062-1 4.8 Zinc, Total, ICP-MS 0.46 ug/L <RDL 0.1 0.5 07/30/12 L56062-2 49.4 Zinc, Total, ICP-MS 0.45 ug/L <RDL 0.1 0.5 07/30/12 L56062-3 198 Zinc, Total, ICP-MS 0.553 ug/L 0.1 0.5 12/12/12 L56990-1 4.9 Zinc, Total, ICP-MS 0.49 ug/L <RDL 0.1 0.5 12/12/12 L56990-2 49.3 Zinc, Total, ICP-MS 0.33 ug/L <RDL 0.1 0.5 12/12/12 L56990-3 198 Zinc, Total, ICP-MS 0.45 ug/L <RDL 0.1 0.5

Notes Depth (m) - Depth below the water's surface (in meters) from which the sample was collected.
MDL - Method detection limit; the limit of reliable detection

. RDL - Reporting detection limit; the limit of reliable quantitation (PQL). <MDL - Analyte was not detected <RDL - Analyte was detected at a concentration less than the RDL. CFU/100 ml - Colony forming units per 100 milliliters. deg C - Degrees Celcius. mg/L - Milligrams per liter. PSS - Practical Salinity Scale. ug/L - Micrograms per liter. JL - Analytical result is an estimate with a probable high bias.Page 1 of 24 

## Table A-2
Complete Water Quality Monitoring Data for Station LSNT01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 01/19/11 L52444-14 1.3 Fecal Coliform CFU/100ml <MDL 1 02/23/11 L52544-14 1.3 Fecal Coliform 1 CFU/100ml 1 03/22/11 L52735-14 1.4 Fecal Coliform 1 CFU/100ml 1 04/19/11 L52887-14 1.3 Fecal Coliform CFU/100ml <MDL 1 05/17/11 L53210-14 1.4 Fecal Coliform CFU/100ml <MDL 1 06/21/11 L53334-14 1.3 Fecal Coliform CFU/100ml <MDL 1 07/19/11 L53547-14 1.2 Fecal Coliform CFU/100ml <MDL 1 08/16/11 L53893-14 1.3 Fecal Coliform CFU/100ml <MDL 1 09/20/11 L54027-14 1.3 Fecal Coliform CFU/100ml <MDL 1 10/18/11 L54273-14 1.3 Fecal Coliform CFU/100ml <MDL 1 11/29/11 L54479-14 1.2 Fecal Coliform CFU/100ml <MDL 1 12/20/11 L54810-14 1.2 Fecal Coliform CFU/100ml <MDL 1 01/26/12 L54843-14 1.2 Fecal Coliform CFU/100ml <MDL 1 02/23/12 L55090-14 1.2 Fecal Coliform CFU/100ml <MDL 1 03/22/12 L55196-14 1.3 Fecal Coliform CFU/100ml <MDL 1 04/17/12 L55374-14 1.5 Fecal Coliform CFU/100ml <MDL 1 05/22/12 L55538-14 1.4 Fecal Coliform CFU/100ml <MDL 1 06/19/12 L55792-14 1.3 Fecal Coliform CFU/100ml <MDL 1 07/17/12 L55945-14 1.2 Fecal Coliform CFU/100ml <MDL 1 08/21/12 L56172-14 1.3 Fecal Coliform CFU/100ml <MDL 1 09/18/12 L56392-14 1.2 Fecal Coliform CFU/100ml <MDL 1 10/18/12 L56639-14 1.2 Fecal Coliform CFU/100ml <MDL 1 11/27/12 L56806-14 0.78 Fecal Coliform CFU/100ml <MDL 1 12/27/12 L57088-14 1 Fecal Coliform CFU/100ml <MDL 1 01/19/11 L52444-14 1.3 Sample Temperature, Field 8.5392 deg C 01/19/11 L52444-15 15.2 Sample Temperature, Field 8.6886 deg C 01/19/11 L52444-16 25.1 Sample Temperature, Field 8.7080 deg C 01/19/11 L52444-17 34.9 Sample Temperature, Field 8.7279 deg C 01/19/11 L52444-18 54.8 Sample Temperature, Field 8.7369 deg C 01/19/11 L52444-19 99.4 Sample Temperature, Field 8.5919 deg C 01/19/11 L52444-20 198 Sample Temperature, Field 8.3591 deg C 01/19/11 L52444-21 198 Sample Temperature, Field 8.3583 deg C 02/23/11 L52544-14 1.3 Sample Temperature, Field 8.0417 deg C 02/23/11 L52544-15 15 Sample Temperature, Field 8.0688 deg C 02/23/11 L52544-16 24.9 Sample Temperature, Field 8.1242 deg C 02/23/11 L52544-17 34.7 Sample Temperature, Field 8.1269 deg C 02/23/11 L52544-18 54.8 Sample Temperature, Field 8.1271 deg C 02/23/11 L52544-19 99.3 Sample Temperature, Field 8.1238 deg C 02/23/11 L52544-20 178 Sample Temperature, Field 8.0664 deg C 02/23/11 L52544-21 178 Sample Temperature, Field 8.0664 deg C 03/22/11 L52735-14 1.4 Sample Temperature, Field 7.7744 deg C 03/22/11 L52735-15 15.3 Sample Temperature, Field 7.7127 deg C 03/22/11 L52735-16 25.2 Sample Temperature, Field 7.7201 deg C 03/22/11 L52735-17 35.1 Sample Temperature, Field 7.7171 deg C 03/22/11 L52735-18 54.9 Sample Temperature, Field 7.6966 deg C 03/22/11 L52735-19 99.6 Sample Temperature, Field 7.6340 deg C 03/22/11 L52735-20 178 Sample Temperature, Field 7.5650 deg C 03/22/11 L52735-21 179 Sample Temperature, Field 7.5648 deg C 04/19/11 L52887-14 1.3 Sample Temperature, Field 8.3505 deg C 04/19/11 L52887-15 15.1 Sample Temperature, Field 8.1180 deg C 04/19/11 L52887-16 24.9 Sample Temperature, Field 8.0840 deg C 04/19/11 L52887-17 35 Sample Temperature, Field 8.0659 deg C 04/19/11 L52887-18 54.8 Sample Temperature, Field 8.0485 deg CPage 2 of 24 

## Table A-2
Complete Water Quality Monitoring Data for Station LSNT01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 04/19/11 L52887-19 99.2 Sample Temperature, Field 7.8867 deg C 04/19/11 L52887-20 178 Sample Temperature, Field 7.7931 deg C 04/19/11 L52887-21 179 Sample Temperature, Field 7.7932 deg C 05/17/11 L53210-14 1.4 Sample Temperature, Field 9.3560 deg C 05/17/11 L53210-15 15.2 Sample Temperature, Field 8.9641 deg C 05/17/11 L53210-16 25.1 Sample Temperature, Field 8.7714 deg C 05/17/11 L53210-17 35 Sample Temperature, Field 8.6841 deg C 05/17/11 L53210-18 54.8 Sample Temperature, Field 8.6575 deg C 05/17/11 L53210-19 99.4 Sample Temperature, Field 8.5045 deg C 05/17/11 L53210-20 178 Sample Temperature, Field 8.5917 deg C 05/17/11 L53210-21 179 Sample Temperature, Field 8.5917 deg C 06/21/11 L53334-14 1.3 Sample Temperature, Field 10.7048 deg C 06/21/11 L53334-15 15.2 Sample Temperature, Field 10.4069 deg C 06/21/11 L53334-16 25.1 Sample Temperature, Field 10.2013 deg C 06/21/11 L53334-17 35 Sample Temperature, Field 10.1603 deg C 06/21/11 L53334-18 54.7 Sample Temperature, Field 9.8579 deg C 06/21/11 L53334-19 99.5 Sample Temperature, Field 9.4725 deg C 06/21/11 L53334-20 179 Sample Temperature, Field 9.1510 deg C 06/21/11 L53334-21 179 Sample Temperature, Field 9.1499 deg C 07/14/11 L53626-7 5.2 Sample Temperature, Field 11.7513 deg C 07/14/11 L53626-8 49.8 Sample Temperature, Field 11.1343 deg C 07/14/11 L53626-9 158 Sample Temperature, Field 9.8710 deg C 07/14/11 L53626-10 159 Sample Temperature, Field 9.8695 deg C 07/19/11 L53547-14 1.2 Sample Temperature, Field 11.4126 deg C 07/19/11 L53547-15 15.1 Sample Temperature, Field 11.2649 deg C 07/19/11 L53547-16 24.9 Sample Temperature, Field 11.1705 deg C 07/19/11 L53547-17 34.9 Sample Temperature, Field 11.0739 deg C 07/19/11 L53547-18 54.6 Sample Temperature, Field 10.6928 deg C 07/19/11 L53547-19 99.3 Sample Temperature, Field 10.1979 deg C 07/19/11 L53547-20 178 Sample Temperature, Field 9.9005 deg C 07/19/11 L53547-21 179 Sample Temperature, Field 9.8999 deg C 08/16/11 L53893-14 1.3 Sample Temperature, Field 12.2887 deg C 08/16/11 L53893-15 15.1 Sample Temperature, Field 12.1325 deg C 08/16/11 L53893-16 25 Sample Temperature, Field 11.9403 deg C 08/16/11 L53893-17 35 Sample Temperature, Field 11.8729 deg C 08/16/11 L53893-18 54.8 Sample Temperature, Field 11.6138 deg C 08/16/11 L53893-19 99.3 Sample Temperature, Field 10.8318 deg C 08/16/11 L53893-20 179 Sample Temperature, Field 10.6192 deg C 08/16/11 L53893-21 179 Sample Temperature, Field 10.6198 deg C 09/20/11 L54027-14 1.3 Sample Temperature, Field 12.2917 deg C 09/20/11 L54027-15 15.1 Sample Temperature, Field 12.1066 deg C 09/20/11 L54027-16 25.1 Sample Temperature, Field 11.9677 deg C 09/20/11 L54027-17 35 Sample Temperature, Field 11.6288 deg C 09/20/11 L54027-18 54.7 Sample Temperature, Field 11.4934 deg C 09/20/11 L54027-19 99.2 Sample Temperature, Field 11.3529 deg C 09/20/11 L54027-20 178 Sample Temperature, Field 11.3496 deg C 09/20/11 L54027-21 179 Sample Temperature, Field 11.3496 deg C 10/18/11 L54273-14 1.3 Sample Temperature, Field 11.7209 deg C 10/18/11 L54273-15 14.6 Sample Temperature, Field 11.7581 deg C 10/18/11 L54273-16 25 Sample Temperature, Field 11.7017 deg C 10/18/11 L54273-17 34.6 Sample Temperature, Field 11.6559 deg C 10/18/11 L54273-18 54.6 Sample Temperature, Field 11.4702 deg C 10/18/11 L54273-19 99.4 Sample Temperature, Field 11.2110 deg CPage 3 of 24 

## Table A-2
Complete Water Quality Monitoring Data for Station LSNT01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 10/18/11 L54273-20 178 Sample Temperature, Field 11.2127 deg C 10/18/11 L54273-21 178 Sample Temperature, Field 11.2123 deg C 11/29/11 L54479-14 1.2 Sample Temperature, Field 10.1208 deg C 11/29/11 L54479-15 15 Sample Temperature, Field 10.1248 deg C 11/29/11 L54479-16 24.8 Sample Temperature, Field 10.1407 deg C 11/29/11 L54479-17 34.7 Sample Temperature, Field 10.0552 deg C 11/29/11 L54479-18 54.7 Sample Temperature, Field 9.9856 deg C 11/29/11 L54479-19 99.1 Sample Temperature, Field 9.8847 deg C 11/29/11 L54479-20 178 Sample Temperature, Field 9.7977 deg C 11/29/11 L54479-21 178 Sample Temperature, Field 9.7970 deg C 12/14/11 L54765-7 5 Sample Temperature, Field 9.3079 deg C 12/14/11 L54765-8 49.5 Sample Temperature, Field 9.6241 deg C 12/14/11 L54765-9 158 Sample Temperature, Field 9.7567 deg C 12/14/11 L54765-10 159 Sample Temperature, Field 9.7565 deg C 12/20/11 L54810-14 1.2 Sample Temperature, Field 9.4762 deg C 12/20/11 L54810-15 15.1 Sample Temperature, Field 9.4905 deg C 12/20/11 L54810-16 24.9 Sample Temperature, Field 9.4952 deg C 12/20/11 L54810-17 34.9 Sample Temperature, Field 9.4681 deg C 12/20/11 L54810-18 54.6 Sample Temperature, Field 9.4356 deg C 12/20/11 L54810-19 99.2 Sample Temperature, Field 9.0262 deg C 12/20/11 L54810-20 178 Sample Temperature, Field 8.7757 deg C 12/20/11 L54810-21 179 Sample Temperature, Field 8.7778 deg C 01/26/12 L54843-14 1.2 Sample Temperature, Field 8.1873 deg C 01/26/12 L54843-15 15.1 Sample Temperature, Field 8.2050 deg C 01/26/12 L54843-16 24.9 Sample Temperature, Field 8.2104 deg C 01/26/12 L54843-17 34.9 Sample Temperature, Field 8.1836 deg C 01/26/12 L54843-18 54.6 Sample Temperature, Field 8.0287 deg C 01/26/12 L54843-19 99.2 Sample Temperature, Field 7.9857 deg C 01/26/12 L54843-20 178 Sample Temperature, Field 7.8575 deg C 01/26/12 L54843-21 179 Sample Temperature, Field 7.8537 deg C 02/23/12 L55090-14 1.2 Sample Temperature, Field 7.8176 deg C 02/23/12 L55090-15 15.1 Sample Temperature, Field 7.8175 deg C 02/23/12 L55090-16 24.9 Sample Temperature, Field 7.8178 deg C 02/23/12 L55090-17 34.7 Sample Temperature, Field 7.8354 deg C 02/23/12 L55090-18 54.4 Sample Temperature, Field 7.8186 deg C 02/23/12 L55090-19 99 Sample Temperature, Field 7.7475 deg C 02/23/12 L55090-20 178 Sample Temperature, Field 7.7085 deg C 02/23/12 L55090-21 179 Sample Temperature, Field 7.7084 deg C 03/22/12 L55196-14 1.3 Sample Temperature, Field 7.6020 deg C 03/22/12 L55196-15 15.1 Sample Temperature, Field 7.5829 deg C 03/22/12 L55196-16 25.1 Sample Temperature, Field 7.5803 deg C 03/22/12 L55196-17 35 Sample Temperature, Field 7.5798 deg C 03/22/12 L55196-18 54.6 Sample Temperature, Field 7.5870 deg C 03/22/12 L55196-19 99.3 Sample Temperature, Field 7.5598 deg C 03/22/12 L55196-20 178 Sample Temperature, Field 7.5061 deg C 03/22/12 L55196-21 179 Sample Temperature, Field 7.5061 deg C 04/17/12 L55374-14 1.5 Sample Temperature, Field 8.3201 deg C 04/17/12 L55374-15 15.4 Sample Temperature, Field 8.1942 deg C 04/17/12 L55374-16 25.2 Sample Temperature, Field 8.1138 deg C 04/17/12 L55374-17 35.1 Sample Temperature, Field 8.0742 deg C 04/17/12 L55374-18 54.8 Sample Temperature, Field 8.0131 deg C 04/17/12 L55374-19 99.6 Sample Temperature, Field 7.8364 deg C 04/17/12 L55374-20 179 Sample Temperature, Field 7.6362 deg CPage 4 of 24 

## Table A-2
Complete Water Quality Monitoring Data for Station LSNT01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 04/17/12 L55374-21 179 Sample Temperature, Field 7.6362 deg C 05/22/12 L55538-14 1.4 Sample Temperature, Field 10.0226 deg C 05/22/12 L55538-15 15.3 Sample Temperature, Field 9.6803 deg C 05/22/12 L55538-16 25.1 Sample Temperature, Field 9.5112 deg C 05/22/12 L55538-17 35 Sample Temperature, Field 9.4181 deg C 05/22/12 L55538-18 54.8 Sample Temperature, Field 9.2346 deg C 05/22/12 L55538-19 99.5 Sample Temperature, Field 8.6976 deg C 05/22/12 L55538-20 179 Sample Temperature, Field 8.6840 deg C 05/22/12 L55538-21 179 Sample Temperature, Field 8.6829 deg C 06/19/12 L55792-14 1.3 Sample Temperature, Field 11.3218 deg C 06/19/12 L55792-15 15.2 Sample Temperature, Field 10.8193 deg C 06/19/12 L55792-16 25.1 Sample Temperature, Field 10.5682 deg C 06/19/12 L55792-17 34.9 Sample Temperature, Field 10.2442 deg C 06/19/12 L55792-18 54.4 Sample Temperature, Field 9.9914 deg C 06/19/12 L55792-19 99.3 Sample Temperature, Field 9.4047 deg C 06/19/12 L55792-20 178 Sample Temperature, Field 9.5245 deg C 06/19/12 L55792-21 179 Sample Temperature, Field 9.5240 deg C 07/17/12 L55945-14 1.2 Sample Temperature, Field 12.2884 deg C 07/17/12 L55945-15 15 Sample Temperature, Field 11.6177 deg C 07/17/12 L55945-16 24.9 Sample Temperature, Field 11.2100 deg C 07/17/12 L55945-17 35 Sample Temperature, Field 11.0948 deg C 07/17/12 L55945-18 54.7 Sample Temperature, Field 10.9013 deg C 07/17/12 L55945-19 99.3 Sample Temperature, Field 10.0400 deg C 07/17/12 L55945-20 179 Sample Temperature, Field 9.9664 deg C 07/17/12 L55945-21 179 Sample Temperature, Field 9.9671 deg C 07/30/12 L56062-7 5 Sample Temperature, Field 12.3847 deg C 07/30/12 L56062-8 49.4 Sample Temperature, Field 10.7781 deg C 07/30/12 L56062-10 158 Sample Temperature, Field 10.1743 deg C 07/30/12 L56062-9 158 Sample Temperature, Field 10.1746 deg C 08/21/12 L56172-14 1.3 Sample Temperature, Field 12.7322 deg C 08/21/12 L56172-15 15.1 Sample Temperature, Field 12.1793 deg C 08/21/12 L56172-16 24.9 Sample Temperature, Field 12.1515 deg C 08/21/12 L56172-17 34.8 Sample Temperature, Field 12.0914 deg C 08/21/12 L56172-18 54.7 Sample Temperature, Field 11.6541 deg C 08/21/12 L56172-19 99.2 Sample Temperature, Field 10.9226 deg C 08/21/12 L56172-20 178 Sample Temperature, Field 10.8053 deg C 08/21/12 L56172-21 179 Sample Temperature, Field 10.8055 deg C 09/18/12 L56392-14 1.2 Sample Temperature, Field 12.4956 deg C 09/18/12 L56392-15 15.1 Sample Temperature, Field 12.3694 deg C 09/18/12 L56392-16 24.6 Sample Temperature, Field 12.2807 deg C 09/18/12 L56392-17 34.9 Sample Temperature, Field 12.2619 deg C 09/18/12 L56392-18 54.6 Sample Temperature, Field 12.1306 deg C 09/18/12 L56392-19 99.4 Sample Temperature, Field 11.3808 deg C 09/18/12 L56392-20 178 Sample Temperature, Field 11.1348 deg C 09/18/12 L56392-21 179 Sample Temperature, Field 11.1348 deg C 10/18/12 L56639-14 1.2 Sample Temperature, Field 11.7300 deg C 10/18/12 L56639-15 15.3 Sample Temperature, Field 11.7071 deg C 10/18/12 L56639-16 25.1 Sample Temperature, Field 11.6567 deg C 10/18/12 L56639-17 35.1 Sample Temperature, Field 11.5945 deg C 10/18/12 L56639-18 54.8 Sample Temperature, Field 11.5344 deg C 10/18/12 L56639-19 99.5 Sample Temperature, Field 11.1151 deg C 10/18/12 L56639-20 178 Sample Temperature, Field 10.8507 deg C 10/18/12 L56639-21 179 Sample Temperature, Field 10.8509 deg CPage 5 of 24 

## Table A-2
Complete Water Quality Monitoring Data for Station LSNT01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 11/27/12 L56806-14 0.78 Sample Temperature, Field 9.8110 deg C 11/27/12 L56806-15 14.5 Sample Temperature, Field 10.4972 deg C 11/27/12 L56806-16 24.8 Sample Temperature, Field 10.5123 deg C 11/27/12 L56806-17 34.5 Sample Temperature, Field 10.5364 deg C 11/27/12 L56806-18 54 Sample Temperature, Field 10.5732 deg C 11/27/12 L56806-19 98.7 Sample Temperature, Field 10.5165 deg C 11/27/12 L56806-20 177 Sample Temperature, Field 10.4855 deg C 11/27/12 L56806-21 178 Sample Temperature, Field 10.4861 deg C 12/12/12 L56990-7 4.9 Sample Temperature, Field 10.1431 deg C 12/12/12 L56990-8 49.5 Sample Temperature, Field 10.1566 deg C 12/12/12 L56990-10 158 Sample Temperature, Field 10.2281 deg C 12/12/12 L56990-9 158 Sample Temperature, Field 10.2270 deg C 12/27/12 L57088-14 1 Sample Temperature, Field 9.4536 deg C 12/27/12 L57088-15 14.9 Sample Temperature, Field 9.6122 deg C 12/27/12 L57088-16 24.7 Sample Temperature, Field 9.6301 deg C 12/27/12 L57088-17 34.4 Sample Temperature, Field 9.6455 deg C 12/27/12 L57088-18 54.3 Sample Temperature, Field 9.6491 deg C 12/27/12 L57088-19 98.9 Sample Temperature, Field 9.6819 deg C 12/27/12 L57088-20 178 Sample Temperature, Field 9.2970 deg C 12/27/12 L57088-21 178 Sample Temperature, Field 9.2952 deg C 07/14/11 L53626-7 5.2 Total Alkalinity 97.4 mg CaCO3/L 1 5 07/14/11 L53626-8 49.8 Total Alkalinity 101 mg CaCO3/L 1 5 07/14/11 L53626-9 158 Total Alkalinity 102 mg CaCO3/L 1 5 07/14/11 L53626-10 159 Total Alkalinity 103 mg CaCO3/L 1 5 12/14/11 L54765-7 5 Total Alkalinity 97.1 mg CaCO3/L 1 5 12/14/11 L54765-8 49.5 Total Alkalinity 98.3 mg CaCO3/L 1 5 12/14/11 L54765-9 158 Total Alkalinity 97.5 mg CaCO3/L 1 5 12/14/11 L54765-10 159 Total Alkalinity 103 mg CaCO3/L 1 5 07/30/12 L56062-7 5 Total Alkalinity 97.7 mg CaCO3/L 1 5 07/30/12 L56062-8 49.4 Total Alkalinity 101 mg CaCO3/L 1 5 07/30/12 L56062-10 158 Total Alkalinity 100 mg CaCO3/L 1 5 07/30/12 L56062-9 158 Total Alkalinity 100 mg CaCO3/L 1 5 12/12/12 L56990-7 4.9 Total Alkalinity 101 mg CaCO3/L 1 5 12/12/12 L56990-8 49.5 Total Alkalinity 101 mg CaCO3/L 1 5 12/12/12 L56990-10 158 Total Alkalinity 103 mg CaCO3/L 1 5 12/12/12 L56990-9 158 Total Alkalinity 102 mg CaCO3/L 1 5 07/14/11 L53626-7 5.2 Cyanide, Weak & Dissociable mg/L <MDL 0.005 0.01 07/14/11 L53626-8 49.8 Cyanide, Weak & Dissociable mg/L <MDL 0.005 0.01 07/14/11 L53626-9 158 Cyanide, Weak & Dissociable mg/L <MDL 0.005 0.01 07/14/11 L53626-10 159 Cyanide, Weak & Dissociable mg/L <MDL 0.005 0.01 12/14/11 L54765-7 5 Cyanide, Weak & Dissociable mg/L <MDL 0.005 0.01 12/14/11 L54765-8 49.5 Cyanide, Weak & Dissociable mg/L <MDL 0.005 0.01 12/14/11 L54765-9 158 Cyanide, Weak & Dissociable mg/L <MDL 0.005 0.01 12/14/11 L54765-10 159 Cyanide, Weak & Dissociable mg/L <MDL 0.005 0.01 07/30/12 L56062-7 5 Cyanide, Weak & Dissociable mg/L <MDL 0.005 0.01 07/30/12 L56062-8 49.4 Cyanide, Weak & Dissociable mg/L <MDL 0.005 0.01 07/30/12 L56062-10 158 Cyanide, Weak & Dissociable mg/L <MDL 0.005 0.01 07/30/12 L56062-9 158 Cyanide, Weak & Dissociable mg/L <MDL 0.005 0.01 12/12/12 L56990-7 4.9 Cyanide, Weak & Dissociable mg/L <MDL 0.005 0.01 12/12/12 L56990-8 49.5 Cyanide, Weak & Dissociable mg/L <MDL 0.005 0.01 12/12/12 L56990-10 158 Cyanide, Weak & Dissociable mg/L <MDL 0.005 0.01 12/12/12 L56990-9 158 Cyanide, Weak & Dissociable mg/L <MDL 0.005 0.01 01/19/11 L52444-14 1.3 Dissolved Oxygen, Field 8.3 mg/L 0.5 1Page 6 of 24 

## Table A-2
Complete Water Quality Monitoring Data for Station LSNT01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 01/19/11 L52444-15 15.2 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 01/19/11 L52444-16 25.1 Dissolved Oxygen, Field 7.9 mg/L 0.5 1 01/19/11 L52444-17 34.9 Dissolved Oxygen, Field 7.8 mg/L 0.5 1 01/19/11 L52444-18 54.8 Dissolved Oxygen, Field 7.7 mg/L 0.5 1 01/19/11 L52444-19 99.4 Dissolved Oxygen, Field 7.7 mg/L 0.5 1 01/19/11 L52444-20 198 Dissolved Oxygen, Field 7.8 mg/L 0.5 1 01/19/11 L52444-21 198 Dissolved Oxygen, Field 7.7 mg/L 0.5 1 02/23/11 L52544-14 1.3 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 02/23/11 L52544-15 15 Dissolved Oxygen, Field 8.2 mg/L 0.5 1 02/23/11 L52544-16 24.9 Dissolved Oxygen, Field 8.1 mg/L 0.5 1 02/23/11 L52544-17 34.7 Dissolved Oxygen, Field 8.1 mg/L 0.5 1 02/23/11 L52544-18 54.8 Dissolved Oxygen, Field 8.1 mg/L 0.5 1 02/23/11 L52544-19 99.3 Dissolved Oxygen, Field 7.7 mg/L 0.5 1 02/23/11 L52544-20 178 Dissolved Oxygen, Field 7.6 mg/L 0.5 1 02/23/11 L52544-21 178 Dissolved Oxygen, Field 7.6 mg/L 0.5 1 03/22/11 L52735-14 1.4 Dissolved Oxygen, Field 8.8 mg/L 0.5 1 03/22/11 L52735-15 15.3 Dissolved Oxygen, Field 8.5 mg/L 0.5 1 03/22/11 L52735-16 25.2 Dissolved Oxygen, Field 8.5 mg/L 0.5 1 03/22/11 L52735-17 35.1 Dissolved Oxygen, Field 8.5 mg/L 0.5 1 03/22/11 L52735-18 54.9 Dissolved Oxygen, Field 8.4 mg/L 0.5 1 03/22/11 L52735-19 99.6 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 03/22/11 L52735-20 178 Dissolved Oxygen, Field 8.1 mg/L 0.5 1 03/22/11 L52735-21 179 Dissolved Oxygen, Field 8.1 mg/L 0.5 1 04/19/11 L52887-14 1.3 Dissolved Oxygen, Field 9.2 mg/L 0.5 1 04/19/11 L52887-15 15.1 Dissolved Oxygen, Field 8.8 mg/L 0.5 1 04/19/11 L52887-16 24.9 Dissolved Oxygen, Field 8.8 mg/L 0.5 1 04/19/11 L52887-17 35 Dissolved Oxygen, Field 8.8 mg/L 0.5 1 04/19/11 L52887-18 54.8 Dissolved Oxygen, Field 8.7 mg/L 0.5 1 04/19/11 L52887-19 99.2 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 04/19/11 L52887-20 178 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 04/19/11 L52887-21 179 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 05/17/11 L53210-14 1.4 Dissolved Oxygen, Field 12.1 mg/L 0.5 1 05/17/11 L53210-15 15.2 Dissolved Oxygen, Field 10.1 mg/L 0.5 1 05/17/11 L53210-16 25.1 Dissolved Oxygen, Field 9.4 mg/L 0.5 1 05/17/11 L53210-17 35 Dissolved Oxygen, Field 9.2 mg/L 0.5 1 05/17/11 L53210-18 54.8 Dissolved Oxygen, Field 9.1 mg/L 0.5 1 05/17/11 L53210-19 99.4 Dissolved Oxygen, Field 8.4 mg/L 0.5 1 05/17/11 L53210-20 178 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 05/17/11 L53210-21 179 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 06/21/11 L53334-14 1.3 Dissolved Oxygen, Field 9.2 mg/L 0.5 1 06/21/11 L53334-15 15.2 Dissolved Oxygen, Field 8.8 mg/L 0.5 1 06/21/11 L53334-16 25.1 Dissolved Oxygen, Field 8.7 mg/L 0.5 1 06/21/11 L53334-17 35 Dissolved Oxygen, Field 8.6 mg/L 0.5 1 06/21/11 L53334-18 54.7 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 06/21/11 L53334-19 99.5 Dissolved Oxygen, Field 7.8 mg/L 0.5 1 06/21/11 L53334-20 179 Dissolved Oxygen, Field 7.5 mg/L 0.5 1 06/21/11 L53334-21 179 Dissolved Oxygen, Field 7.5 mg/L 0.5 1 07/14/11 L53626-7 5.2 Dissolved Oxygen, Field 9.8 mg/L 0.5 1 07/14/11 L53626-8 49.8 Dissolved Oxygen, Field 8.7 mg/L 0.5 1 07/14/11 L53626-9 158 Dissolved Oxygen, Field 6.5 mg/L 0.5 1 07/14/11 L53626-10 159 Dissolved Oxygen, Field 6.5 mg/L 0.5 1 07/19/11 L53547-14 1.2 Dissolved Oxygen, Field 8.2 mg/L 0.5 1 07/19/11 L53547-15 15.1 Dissolved Oxygen, Field 8.1 mg/L 0.5 1Page 7 of 24 

## Table A-2
Complete Water Quality Monitoring Data for Station LSNT01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 07/19/11 L53547-16 24.9 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 07/19/11 L53547-17 34.9 Dissolved Oxygen, Field 7.9 mg/L 0.5 1 07/19/11 L53547-18 54.6 Dissolved Oxygen, Field 7.4 mg/L 0.5 1 07/19/11 L53547-19 99.3 Dissolved Oxygen, Field 6.6 mg/L 0.5 1 07/19/11 L53547-20 178 Dissolved Oxygen, Field 6.2 mg/L 0.5 1 07/19/11 L53547-21 179 Dissolved Oxygen, Field 6.2 mg/L 0.5 1 08/16/11 L53893-14 1.3 Dissolved Oxygen, Field 7.4 mg/L 0.5 1 08/16/11 L53893-15 15.1 Dissolved Oxygen, Field 7.2 mg/L 0.5 1 08/16/11 L53893-16 25 Dissolved Oxygen, Field 6.9 mg/L 0.5 1 08/16/11 L53893-17 35 Dissolved Oxygen, Field 6.8 mg/L 0.5 1 08/16/11 L53893-18 54.8 Dissolved Oxygen, Field 6.5 mg/L 0.5 1 08/16/11 L53893-19 99.3 Dissolved Oxygen, Field 5.7 mg/L 0.5 1 08/16/11 L53893-20 179 Dissolved Oxygen, Field 5.4 mg/L 0.5 1 08/16/11 L53893-21 179 Dissolved Oxygen, Field 5.4 mg/L 0.5 1 09/20/11 L54027-14 1.3 Dissolved Oxygen, Field 6.8 mg/L 0.5 1 09/20/11 L54027-15 15.1 Dissolved Oxygen, Field 6.5 mg/L 0.5 1 09/20/11 L54027-16 25.1 Dissolved Oxygen, Field 6.2 mg/L 0.5 1 09/20/11 L54027-17 35 Dissolved Oxygen, Field 5.9 mg/L 0.5 1 09/20/11 L54027-18 54.7 Dissolved Oxygen, Field 5.8 mg/L 0.5 1 09/20/11 L54027-19 99.2 Dissolved Oxygen, Field 5.7 mg/L 0.5 1 09/20/11 L54027-20 178 Dissolved Oxygen, Field 5.9 mg/L 0.5 1 09/20/11 L54027-21 179 Dissolved Oxygen, Field 5.9 mg/L 0.5 1 10/18/11 L54273-14 1.3 Dissolved Oxygen, Field 7.2 mg/L 0.5 1 10/18/11 L54273-15 14.6 Dissolved Oxygen, Field 6.4 mg/L 0.5 1 10/18/11 L54273-16 25 Dissolved Oxygen, Field 6.3 mg/L 0.5 1 10/18/11 L54273-17 34.6 Dissolved Oxygen, Field 6.1 mg/L 0.5 1 10/18/11 L54273-18 54.6 Dissolved Oxygen, Field 5.8 mg/L 0.5 1 10/18/11 L54273-19 99.4 Dissolved Oxygen, Field 5.6 mg/L 0.5 1 10/18/11 L54273-20 178 Dissolved Oxygen, Field 5.5 mg/L 0.5 1 10/18/11 L54273-21 178 Dissolved Oxygen, Field 5.5 mg/L 0.5 1 11/29/11 L54479-14 1.2 Dissolved Oxygen, Field 6.9 mg/L 0.5 1 11/29/11 L54479-15 15 Dissolved Oxygen, Field 6.8 mg/L 0.5 1 11/29/11 L54479-16 24.8 Dissolved Oxygen, Field 6.8 mg/L 0.5 1 11/29/11 L54479-17 34.7 Dissolved Oxygen, Field 6.7 mg/L 0.5 1 11/29/11 L54479-18 54.7 Dissolved Oxygen, Field 6.7 mg/L 0.5 1 11/29/11 L54479-19 99.1 Dissolved Oxygen, Field 6.7 mg/L 0.5 1 11/29/11 L54479-20 178 Dissolved Oxygen, Field 6.7 mg/L 0.5 1 11/29/11 L54479-21 178 Dissolved Oxygen, Field 6.7 mg/L 0.5 1 12/14/11 L54765-7 5 Dissolved Oxygen, Field 7.3 mg/L 0.5 1 12/14/11 L54765-8 49.5 Dissolved Oxygen, Field 6.8 mg/L 0.5 1 12/14/11 L54765-9 158 Dissolved Oxygen, Field 6.5 mg/L 0.5 1 12/14/11 L54765-10 159 Dissolved Oxygen, Field 6.5 mg/L 0.5 1 12/20/11 L54810-14 1.2 Dissolved Oxygen, Field 6.9 mg/L 0.5 1 12/20/11 L54810-15 15.1 Dissolved Oxygen, Field 6.8 mg/L 0.5 1 12/20/11 L54810-16 24.9 Dissolved Oxygen, Field 6.8 mg/L 0.5 1 12/20/11 L54810-17 34.9 Dissolved Oxygen, Field 6.8 mg/L 0.5 1 12/20/11 L54810-18 54.6 Dissolved Oxygen, Field 6.8 mg/L 0.5 1 12/20/11 L54810-19 99.2 Dissolved Oxygen, Field 6.8 mg/L 0.5 1 12/20/11 L54810-20 178 Dissolved Oxygen, Field 6.8 mg/L 0.5 1 12/20/11 L54810-21 179 Dissolved Oxygen, Field 6.8 mg/L 0.5 1 01/26/12 L54843-14 1.2 Dissolved Oxygen, Field 7.6 mg/L 0.5 1 01/26/12 L54843-15 15.1 Dissolved Oxygen, Field 7.6 mg/L 0.5 1 01/26/12 L54843-16 24.9 Dissolved Oxygen, Field 7.5 mg/L 0.5 1Page 8 of 24 

## Table A-2
Complete Water Quality Monitoring Data for Station LSNT01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 01/26/12 L54843-17 34.9 Dissolved Oxygen, Field 7.4 mg/L 0.5 1 01/26/12 L54843-18 54.6 Dissolved Oxygen, Field 7.5 mg/L 0.5 1 01/26/12 L54843-19 99.2 Dissolved Oxygen, Field 7.5 mg/L 0.5 1 01/26/12 L54843-20 178 Dissolved Oxygen, Field 7.5 mg/L 0.5 1 01/26/12 L54843-21 179 Dissolved Oxygen, Field 7.6 mg/L 0.5 1 02/23/12 L55090-14 1.2 Dissolved Oxygen, Field 8.2 mg/L 0.5 1 02/23/12 L55090-15 15.1 Dissolved Oxygen, Field 8.2 mg/L 0.5 1 02/23/12 L55090-16 24.9 Dissolved Oxygen, Field 8.2 mg/L 0.5 1 02/23/12 L55090-17 34.7 Dissolved Oxygen, Field 8.1 mg/L 0.5 1 02/23/12 L55090-18 54.4 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 02/23/12 L55090-19 99 Dissolved Oxygen, Field 7.8 mg/L 0.5 1 02/23/12 L55090-20 178 Dissolved Oxygen, Field 7.8 mg/L 0.5 1 02/23/12 L55090-21 179 Dissolved Oxygen, Field 7.8 mg/L 0.5 1 03/22/12 L55196-14 1.3 Dissolved Oxygen, Field 8.5 mg/L 0.5 1 03/22/12 L55196-15 15.1 Dissolved Oxygen, Field 8.5 mg/L 0.5 1 03/22/12 L55196-16 25.1 Dissolved Oxygen, Field 8.5 mg/L 0.5 1 03/22/12 L55196-17 35 Dissolved Oxygen, Field 8.5 mg/L 0.5 1 03/22/12 L55196-18 54.6 Dissolved Oxygen, Field 8.5 mg/L 0.5 1 03/22/12 L55196-19 99.3 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 03/22/12 L55196-20 178 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 03/22/12 L55196-21 179 Dissolved Oxygen, Field 8.2 mg/L 0.5 1 04/17/12 L55374-14 1.5 Dissolved Oxygen, Field 9.6 mg/L 0.5 1 04/17/12 L55374-15 15.4 Dissolved Oxygen, Field 9.3 mg/L 0.5 1 04/17/12 L55374-16 25.2 Dissolved Oxygen, Field 9.1 mg/L 0.5 1 04/17/12 L55374-17 35.1 Dissolved Oxygen, Field 8.9 mg/L 0.5 1 04/17/12 L55374-18 54.8 Dissolved Oxygen, Field 8.7 mg/L 0.5 1 04/17/12 L55374-19 99.6 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 04/17/12 L55374-20 179 Dissolved Oxygen, Field 7.9 mg/L 0.5 1 04/17/12 L55374-21 179 Dissolved Oxygen, Field 7.8 mg/L 0.5 1 05/22/12 L55538-14 1.4 Dissolved Oxygen, Field 10.6 mg/L 0.5 1 05/22/12 L55538-15 15.3 Dissolved Oxygen, Field 9.8 mg/L 0.5 1 05/22/12 L55538-16 25.1 Dissolved Oxygen, Field 9.6 mg/L 0.5 1 05/22/12 L55538-17 35 Dissolved Oxygen, Field 9.4 mg/L 0.5 1 05/22/12 L55538-18 54.8 Dissolved Oxygen, Field 9.0 mg/L 0.5 1 05/22/12 L55538-19 99.5 Dissolved Oxygen, Field 7.9 mg/L 0.5 1 05/22/12 L55538-20 179 Dissolved Oxygen, Field 7.7 mg/L 0.5 1 05/22/12 L55538-21 179 Dissolved Oxygen, Field 7.7 mg/L 0.5 1 06/19/12 L55792-14 1.3 Dissolved Oxygen, Field 8.8 mg/L 0.5 1 06/19/12 L55792-15 15.2 Dissolved Oxygen, Field 8.6 mg/L 0.5 1 06/19/12 L55792-16 25.1 Dissolved Oxygen, Field 8.5 mg/L 0.5 1 06/19/12 L55792-17 34.9 Dissolved Oxygen, Field 8.1 mg/L 0.5 1 06/19/12 L55792-18 54.4 Dissolved Oxygen, Field 7.7 mg/L 0.5 1 06/19/12 L55792-19 99.3 Dissolved Oxygen, Field 6.9 mg/L 0.5 1 06/19/12 L55792-20 178 Dissolved Oxygen, Field 6.7 mg/L 0.5 1 06/19/12 L55792-21 179 Dissolved Oxygen, Field 6.7 mg/L 0.5 1 07/17/12 L55945-14 1.2 Dissolved Oxygen, Field 8.6 mg/L 0.5 1 07/17/12 L55945-15 15 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 07/17/12 L55945-16 24.9 Dissolved Oxygen, Field 7.6 mg/L 0.5 1 07/17/12 L55945-17 35 Dissolved Oxygen, Field 7.5 mg/L 0.5 1 07/17/12 L55945-18 54.7 Dissolved Oxygen, Field 7.2 mg/L 0.5 1 07/17/12 L55945-19 99.3 Dissolved Oxygen, Field 6.2 mg/L 0.5 1 07/17/12 L55945-20 179 Dissolved Oxygen, Field 6.0 mg/L 0.5 1 07/17/12 L55945-21 179 Dissolved Oxygen, Field 6.0 mg/L 0.5 1Page 9 of 24 

## Table A-2
Complete Water Quality Monitoring Data for Station LSNT01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 07/30/12 L56062-7 5 Dissolved Oxygen, Field 7.7 mg/L 0.5 1 07/30/12 L56062-8 49.4 Dissolved Oxygen, Field 6.3 mg/L 0.5 1 07/30/12 L56062-10 158 Dissolved Oxygen, Field 5.7 mg/L 0.5 1 07/30/12 L56062-9 158 Dissolved Oxygen, Field 5.7 mg/L 0.5 1 08/21/12 L56172-14 1.3 Dissolved Oxygen, Field 7.7 mg/L 0.5 1 08/21/12 L56172-15 15.1 Dissolved Oxygen, Field 7.1 mg/L 0.5 1 08/21/12 L56172-16 24.9 Dissolved Oxygen, Field 7.0 mg/L 0.5 1 08/21/12 L56172-17 34.8 Dissolved Oxygen, Field 7.0 mg/L 0.5 1 08/21/12 L56172-18 54.7 Dissolved Oxygen, Field 6.4 mg/L 0.5 1 08/21/12 L56172-19 99.2 Dissolved Oxygen, Field 5.7 mg/L 0.5 1 08/21/12 L56172-20 178 Dissolved Oxygen, Field 5.6 mg/L 0.5 1 08/21/12 L56172-21 179 Dissolved Oxygen, Field 5.6 mg/L 0.5 1 09/18/12 L56392-14 1.2 Dissolved Oxygen, Field 6.8 mg/L 0.5 1 09/18/12 L56392-15 15.1 Dissolved Oxygen, Field 6.7 mg/L 0.5 1 09/18/12 L56392-16 24.6 Dissolved Oxygen, Field 6.6 mg/L 0.5 1 09/18/12 L56392-17 34.9 Dissolved Oxygen, Field 6.6 mg/L 0.5 1 09/18/12 L56392-18 54.6 Dissolved Oxygen, Field 6.4 mg/L 0.5 1 09/18/12 L56392-19 99.4 Dissolved Oxygen, Field 5.7 mg/L 0.5 1 09/18/12 L56392-20 178 Dissolved Oxygen, Field 5.5 mg/L 0.5 1 09/18/12 L56392-21 179 Dissolved Oxygen, Field 5.6 mg/L 0.5 1 10/18/12 L56639-14 1.2 Dissolved Oxygen, Field 6.1 mg/L 0.5 1 10/18/12 L56639-15 15.3 Dissolved Oxygen, Field 6.1 mg/L 0.5 1 10/18/12 L56639-16 25.1 Dissolved Oxygen, Field 6.0 mg/L 0.5 1 10/18/12 L56639-17 35.1 Dissolved Oxygen, Field 5.9 mg/L 0.5 1 10/18/12 L56639-18 54.8 Dissolved Oxygen, Field 5.9 mg/L 0.5 1 10/18/12 L56639-19 99.5 Dissolved Oxygen, Field 5.6 mg/L 0.5 1 10/18/12 L56639-20 178 Dissolved Oxygen, Field 5.4 mg/L 0.5 1 10/18/12 L56639-21 179 Dissolved Oxygen, Field 5.4 mg/L 0.5 1 11/27/12 L56806-14 0.78 Dissolved Oxygen, Field 7.8 mg/L 0.5 1 11/27/12 L56806-15 14.5 Dissolved Oxygen, Field 6.6 mg/L 0.5 1 11/27/12 L56806-16 24.8 Dissolved Oxygen, Field 6.5 mg/L 0.5 1 11/27/12 L56806-17 34.5 Dissolved Oxygen, Field 6.4 mg/L 0.5 1 11/27/12 L56806-18 54 Dissolved Oxygen, Field 6.3 mg/L 0.5 1 11/27/12 L56806-19 98.7 Dissolved Oxygen, Field 5.9 mg/L 0.5 1 11/27/12 L56806-20 177 Dissolved Oxygen, Field 5.3 mg/L 0.5 1 11/27/12 L56806-21 178 Dissolved Oxygen, Field 5.3 mg/L 0.5 1 12/12/12 L56990-7 4.9 Dissolved Oxygen, Field 7.0 mg/L 0.5 1 12/12/12 L56990-8 49.5 Dissolved Oxygen, Field 6.7 mg/L 0.5 1 12/12/12 L56990-10 158 Dissolved Oxygen, Field 5.6 mg/L 0.5 1 12/12/12 L56990-9 158 Dissolved Oxygen, Field 5.6 mg/L 0.5 1 08/16/11 L53893-14 1.3 Total Suspended Solids 1.4 mg/L 0.5 1 08/16/11 L53893-15 15.1 Total Suspended Solids 1.6 mg/L 0.5 1 08/16/11 L53893-16 25 Total Suspended Solids 1.0 mg/L 0.5 1 08/16/11 L53893-17 35 Total Suspended Solids 1.3 mg/L 0.5 1 08/16/11 L53893-18 54.8 Total Suspended Solids 1.1 mg/L 0.5 1 08/16/11 L53893-19 99.3 Total Suspended Solids 1.7 mg/L 0.5 1 08/16/11 L53893-20 179 Total Suspended Solids 2.0 mg/L 0.5 1 08/16/11 L53893-21 179 Total Suspended Solids 2.9 mg/L 0.5 1 09/20/11 L54027-14 1.3 Total Suspended Solids 1.1 mg/L <RDL 0.5 10 09/20/11 L54027-15 15.1 Total Suspended Solids 1.1 mg/L <RDL 0.5 10 09/20/11 L54027-16 25.1 Total Suspended Solids 1.3 mg/L <RDL 0.5 10 09/20/11 L54027-17 35 Total Suspended Solids 1.4 mg/L <RDL 0.5 10 09/20/11 L54027-18 54.7 Total Suspended Solids 1.0 mg/L <RDL 0.5 10Page 10 of 24 

## Table A-2
Complete Water Quality Monitoring Data for Station LSNT01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 09/20/11 L54027-19 99.2 Total Suspended Solids 1.8 mg/L <RDL 0.5 10 09/20/11 L54027-20 178 Total Suspended Solids 1.5 mg/L <RDL 0.5 10 09/20/11 L54027-21 179 Total Suspended Solids 1.6 mg/L <RDL 0.5 10 10/18/11 L54273-14 1.3 Total Suspended Solids 0.9 mg/L <RDL 0.5 10 10/18/11 L54273-15 14.6 Total Suspended Solids 0.8 mg/L <RDL 0.5 10 10/18/11 L54273-16 25 Total Suspended Solids 1.1 mg/L <RDL 0.5 10 10/18/11 L54273-17 34.6 Total Suspended Solids 0.8 mg/L <RDL 0.5 10 10/18/11 L54273-18 54.6 Total Suspended Solids mg/L <MDL 0.5 10 10/18/11 L54273-19 99.4 Total Suspended Solids 0.6 mg/L <RDL 0.5 10 10/18/11 L54273-20 178 Total Suspended Solids 1.0 mg/L <RDL 0.5 10 10/18/11 L54273-21 178 Total Suspended Solids 1.2 mg/L <RDL 0.5 10 11/29/11 L54479-14 1.2 Total Suspended Solids 0.9 mg/L <RDL 0.5 10 11/29/11 L54479-15 15 Total Suspended Solids 0.6 mg/L <RDL 0.5 10 11/29/11 L54479-16 24.8 Total Suspended Solids 1.4 mg/L <RDL 0.5 10 11/29/11 L54479-17 34.7 Total Suspended Solids 1.4 mg/L <RDL 0.5 10 11/29/11 L54479-18 54.7 Total Suspended Solids 1.3 mg/L <RDL 0.5 10 11/29/11 L54479-19 99.1 Total Suspended Solids 2.3 mg/L <RDL 0.5 10 11/29/11 L54479-20 178 Total Suspended Solids 1.6 mg/L <RDL 1 20 11/29/11 L54479-21 178 Total Suspended Solids 1.7 mg/L <RDL 0.5 10 12/20/11 L54810-14 1.2 Total Suspended Solids 0.7 mg/L <RDL 0.5 10 12/20/11 L54810-15 15.1 Total Suspended Solids 0.9 mg/L <RDL 0.5 10 12/20/11 L54810-16 24.9 Total Suspended Solids 1.1 mg/L <RDL 0.5 10 12/20/11 L54810-17 34.9 Total Suspended Solids 1.6 mg/L <RDL 1 20 12/20/11 L54810-18 54.6 Total Suspended Solids 0.9 mg/L <RDL 0.5 10 12/20/11 L54810-19 99.2 Total Suspended Solids 1.4 mg/L <RDL 0.5 10 12/20/11 L54810-20 178 Total Suspended Solids 2.1 mg/L <RDL 0.5 10 12/20/11 L54810-21 179 Total Suspended Solids 2.2 mg/L <RDL 0.5 10 01/26/12 L54843-14 1.2 Total Suspended Solids 1.5 mg/L <RDL 0.5 10 01/26/12 L54843-15 15.1 Total Suspended Solids 1.2 mg/L <RDL 0.5 10 01/26/12 L54843-16 24.9 Total Suspended Solids 1.6 mg/L <RDL 0.5 10 01/26/12 L54843-17 34.9 Total Suspended Solids 2.1 mg/L <RDL 0.5 10 01/26/12 L54843-18 54.6 Total Suspended Solids 1.9 mg/L <RDL 0.5 10 01/26/12 L54843-19 99.2 Total Suspended Solids 1.0 mg/L <RDL 0.5 10 01/26/12 L54843-21 179 Total Suspended Solids 1.5 mg/L <RDL 0.5 10 02/23/12 L55090-14 1.2 Total Suspended Solids mg/L <MDL 1 20 02/23/12 L55090-15 15.1 Total Suspended Solids 1.6 mg/L <RDL 0.5 10 02/23/12 L55090-16 24.9 Total Suspended Solids 0.8 mg/L <RDL 0.5 10 02/23/12 L55090-17 34.7 Total Suspended Solids 2.6 mg/L <RDL 0.5 10 02/23/12 L55090-18 54.4 Total Suspended Solids 2.2 mg/L <RDL 0.5 10 02/23/12 L55090-19 99 Total Suspended Solids 2.3 mg/L <RDL 0.5 10 02/23/12 L55090-20 178 Total Suspended Solids 2.4 mg/L <RDL 0.5 10 02/23/12 L55090-21 179 Total Suspended Solids 2.8 mg/L <RDL 0.5 10 03/22/12 L55196-14 1.3 Total Suspended Solids 2.1 mg/L <RDL 0.5 10 03/22/12 L55196-15 15.1 Total Suspended Solids 1.8 mg/L <RDL 0.5 10 03/22/12 L55196-16 25.1 Total Suspended Solids 2.5 mg/L <RDL 0.5 10 03/22/12 L55196-17 35 Total Suspended Solids 1.4 mg/L <RDL 0.5 10 03/22/12 L55196-18 54.6 Total Suspended Solids 1.6 mg/L <RDL 0.5 10 03/22/12 L55196-19 99.3 Total Suspended Solids 2.2 mg/L <RDL 0.5 10 03/22/12 L55196-20 178 Total Suspended Solids 4.2 mg/L <RDL 0.5 10 03/22/12 L55196-21 179 Total Suspended Solids 2.4 mg/L <RDL 0.5 10 04/17/12 L55374-14 1.5 Total Suspended Solids 5.3 mg/L <RDL 0.5 10 04/17/12 L55374-15 15.4 Total Suspended Solids 4.3 mg/L <RDL 0.5 10 04/17/12 L55374-16 25.2 Total Suspended Solids 4.6 mg/L <RDL 1 20Page 11 of 24 

## Table A-2
Complete Water Quality Monitoring Data for Station LSNT01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 04/17/12 L55374-17 35.1 Total Suspended Solids 2.1 mg/L <RDL 0.5 10 04/17/12 L55374-18 54.8 Total Suspended Solids 1.9 mg/L <RDL 0.5 10 04/17/12 L55374-19 99.6 Total Suspended Solids 2.5 mg/L <RDL 0.5 10 04/17/12 L55374-20 179 Total Suspended Solids 3.2 mg/L <RDL 0.5 10 04/17/12 L55374-21 179 Total Suspended Solids 2.1 mg/L <RDL 0.5 10 05/22/12 L55538-14 1.4 Total Suspended Solids 6.0 mg/L <RDL 1 20 05/22/12 L55538-15 15.3 Total Suspended Solids 3.2 mg/L <RDL 0.5 10 05/22/12 L55538-16 25.1 Total Suspended Solids 2.0 mg/L <RDL 0.5 10 05/22/12 L55538-17 35 Total Suspended Solids 3.2 mg/L <RDL 0.5 11 05/22/12 L55538-18 54.8 Total Suspended Solids 2.8 mg/L <RDL 0.5 10 05/22/12 L55538-19 99.5 Total Suspended Solids 2.2 mg/L <RDL 0.5 10 05/22/12 L55538-20 179 Total Suspended Solids 3.3 mg/L <RDL 0.5 10 05/22/12 L55538-21 179 Total Suspended Solids 3.1 mg/L <RDL 0.5 10 06/19/12 L55792-14 1.3 Total Suspended Solids 2.7 mg/L <RDL 0.5 10 06/19/12 L55792-15 15.2 Total Suspended Solids 2.6 mg/L <RDL 0.5 10 06/19/12 L55792-16 25.1 Total Suspended Solids 4.0 mg/L <RDL 0.5 10 06/19/12 L55792-17 34.9 Total Suspended Solids 1.9 mg/L <RDL 0.5 10 06/19/12 L55792-18 54.4 Total Suspended Solids 3.0 mg/L <RDL 0.5 10 06/19/12 L55792-19 99.3 Total Suspended Solids 1.9 mg/L <RDL 0.5 10 06/19/12 L55792-20 178 Total Suspended Solids 3.6 mg/L <RDL 0.5 10 06/19/12 L55792-21 179 Total Suspended Solids 4.4 mg/L <RDL 1 20 07/17/12 L55945-14 1.2 Total Suspended Solids 2.4 mg/L <RDL 0.5 10 07/17/12 L55945-15 15 Total Suspended Solids 1.6 mg/L <RDL 0.5 10 07/17/12 L55945-16 24.9 Total Suspended Solids 2.3 mg/L <RDL 0.5 10 07/17/12 L55945-17 35 Total Suspended Solids 2.8 mg/L <RDL 0.5 10 07/17/12 L55945-19 99.3 Total Suspended Solids 2.3 mg/L <RDL 0.5 10 07/17/12 L55945-20 179 Total Suspended Solids 3.2 mg/L <RDL 0.5 10 07/17/12 L55945-21 179 Total Suspended Solids 3.8 mg/L <RDL 0.5 10 08/21/12 L56172-14 1.3 Total Suspended Solids 3.4 mg/L <RDL 0.5 10 08/21/12 L56172-15 15.1 Total Suspended Solids 2.9 mg/L <RDL 0.5 10 08/21/12 L56172-16 24.9 Total Suspended Solids 3.5 mg/L <RDL 0.5 11 08/21/12 L56172-17 34.8 Total Suspended Solids 2.4 mg/L <RDL 0.5 10 08/21/12 L56172-18 54.7 Total Suspended Solids 2.8 mg/L <RDL 0.5 10 08/21/12 L56172-19 99.2 Total Suspended Solids 2.9 mg/L <RDL 0.5 10 08/21/12 L56172-20 178 Total Suspended Solids 4.2 mg/L <RDL 0.5 10 08/21/12 L56172-21 179 Total Suspended Solids 5.1 mg/L <RDL 0.5 10 09/18/12 L56392-14 1.2 Total Suspended Solids 4.9 mg/L <RDL 0.5 10 09/18/12 L56392-15 15.1 Total Suspended Solids 3.3 mg/L <RDL 0.5 10 09/18/12 L56392-16 24.6 Total Suspended Solids 4.8 mg/L <RDL 0.5 10 09/18/12 L56392-17 34.9 Total Suspended Solids 4.5 mg/L <RDL 0.5 10 09/18/12 L56392-18 54.6 Total Suspended Solids 3.7 mg/L <RDL 0.5 10 09/18/12 L56392-19 99.4 Total Suspended Solids 3.9 mg/L <RDL 0.5 10 09/18/12 L56392-20 178 Total Suspended Solids 3.5 mg/L <RDL 0.5 10 09/18/12 L56392-21 179 Total Suspended Solids 3.9 mg/L <RDL 0.5 10 10/18/12 L56639-14 1.2 Total Suspended Solids 1.4 mg/L <RDL 0.5 10 10/18/12 L56639-15 15.3 Total Suspended Solids 2.6 mg/L <RDL 0.5 10 10/18/12 L56639-16 25.1 Total Suspended Solids 3.2 mg/L <RDL 0.5 10 10/18/12 L56639-17 35.1 Total Suspended Solids 2.1 mg/L <RDL 0.5 10 10/18/12 L56639-18 54.8 Total Suspended Solids 3.5 mg/L <RDL 0.5 10 10/18/12 L56639-19 99.5 Total Suspended Solids 3.1 mg/L <RDL 0.5 10 10/18/12 L56639-20 178 Total Suspended Solids 4.0 mg/L <RDL 0.5 10 10/18/12 L56639-21 179 Total Suspended Solids 4.7 mg/L <RDL 0.5 10 11/27/12 L56806-14 0.78 Total Suspended Solids 1.2 mg/L <RDL 0.5 10Page 12 of 24 

## Table A-2
Complete Water Quality Monitoring Data for Station LSNT01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 11/27/12 L56806-15 14.5 Total Suspended Solids 0.9 mg/L <RDL 0.5 10 11/27/12 L56806-16 24.8 Total Suspended Solids 4.2 mg/L <RDL 0.5 10 11/27/12 L56806-17 34.5 Total Suspended Solids mg/L <MDL 0.5 10 11/27/12 L56806-18 54 Total Suspended Solids 1.6 mg/L <RDL 1 20 11/27/12 L56806-19 98.7 Total Suspended Solids 4.7 mg/L <RDL 0.5 10 11/27/12 L56806-20 177 Total Suspended Solids 3.9 mg/L <RDL 0.5 10 11/27/12 L56806-21 178 Total Suspended Solids 7.5 mg/L <RDL 0.5 10 12/27/12 L57088-14 1 Total Suspended Solids 0.8 mg/L <RDL 0.5 10 12/27/12 L57088-15 14.9 Total Suspended Solids 4.7 mg/L <RDL 0.5 10 12/27/12 L57088-16 24.7 Total Suspended Solids 0.8 mg/L <RDL 0.5 10 12/27/12 L57088-17 34.4 Total Suspended Solids 5.1 mg/L <RDL 0.5 10 12/27/12 L57088-18 54.3 Total Suspended Solids 2.9 mg/L <RDL 0.5 10 12/27/12 L57088-19 98.9 Total Suspended Solids 1.7 mg/L <RDL 0.5 10 12/27/12 L57088-20 178 Total Suspended Solids 6.2 mg/L <RDL 0.5 10 12/27/12 L57088-21 178 Total Suspended Solids 3.8 mg/L <RDL 0.5 10 01/19/11 L52444-14 1.3 pH, Field 7.7 pH 01/19/11 L52444-15 15.2 pH, Field 7.7 pH 01/19/11 L52444-16 25.1 pH, Field 7.7 pH 01/19/11 L52444-17 34.9 pH, Field 7.7 pH 01/19/11 L52444-18 54.8 pH, Field 7.7 pH 01/19/11 L52444-19 99.4 pH, Field 7.7 pH 01/19/11 L52444-20 198 pH, Field 7.7 pH 01/19/11 L52444-21 198 pH, Field 7.7 pH 02/23/11 L52544-14 1.3 pH, Field 7.7 pH 02/23/11 L52544-15 15 pH, Field 7.7 pH 02/23/11 L52544-16 24.9 pH, Field 7.7 pH 02/23/11 L52544-17 34.7 pH, Field 7.7 pH 02/23/11 L52544-18 54.8 pH, Field 7.7 pH 02/23/11 L52544-19 99.3 pH, Field 7.7 pH 02/23/11 L52544-20 178 pH, Field 7.7 pH 02/23/11 L52544-21 178 pH, Field 7.7 pH 03/22/11 L52735-14 1.4 pH, Field 7.7 pH 03/22/11 L52735-15 15.3 pH, Field 7.7 pH 03/22/11 L52735-16 25.2 pH, Field 7.7 pH 03/22/11 L52735-17 35.1 pH, Field 7.7 pH 03/22/11 L52735-18 54.9 pH, Field 7.7 pH 03/22/11 L52735-19 99.6 pH, Field 7.7 pH 03/22/11 L52735-20 178 pH, Field 7.7 pH 03/22/11 L52735-21 179 pH, Field 7.7 pH 04/19/11 L52887-14 1.3 pH, Field 7.9 pH 04/19/11 L52887-15 15.1 pH, Field 7.8 pH 04/19/11 L52887-16 24.9 pH, Field 7.8 pH 04/19/11 L52887-17 35 pH, Field 7.8 pH 04/19/11 L52887-18 54.8 pH, Field 7.8 pH 04/19/11 L52887-19 99.2 pH, Field 7.8 pH 04/19/11 L52887-20 178 pH, Field 7.8 pH 04/19/11 L52887-21 179 pH, Field 7.8 pH 05/17/11 L53210-14 1.4 pH, Field 8.0 pH 05/17/11 L53210-15 15.2 pH, Field 7.8 pH 05/17/11 L53210-16 25.1 pH, Field 7.8 pH 05/17/11 L53210-17 35 pH, Field 7.7 pH 05/17/11 L53210-18 54.8 pH, Field 7.7 pH 05/17/11 L53210-19 99.4 pH, Field 7.7 pHPage 13 of 24 

## Table A-2
Complete Water Quality Monitoring Data for Station LSNT01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 05/17/11 L53210-20 178 pH, Field 7.7 pH 05/17/11 L53210-21 179 pH, Field 7.7 pH 06/21/11 L53334-14 1.3 pH, Field 7.8 pH 06/21/11 L53334-15 15.2 pH, Field 7.8 pH 06/21/11 L53334-16 25.1 pH, Field 7.8 pH 06/21/11 L53334-17 35 pH, Field 7.8 pH 06/21/11 L53334-18 54.7 pH, Field 7.8 pH 06/21/11 L53334-19 99.5 pH, Field 7.7 pH 06/21/11 L53334-20 179 pH, Field 7.7 pH 06/21/11 L53334-21 179 pH, Field 7.7 pH 07/14/11 L53626-7 5.2 pH, Field 8.0 pH 07/14/11 L53626-8 49.8 pH, Field 7.9 pH 07/14/11 L53626-9 158 pH, Field 7.6 pH 07/14/11 L53626-10 159 pH, Field 7.6 pH 07/19/11 L53547-14 1.2 pH, Field 7.8 pH 07/19/11 L53547-15 15.1 pH, Field 7.8 pH 07/19/11 L53547-16 24.9 pH, Field 7.8 pH 07/19/11 L53547-17 34.9 pH, Field 7.8 pH 07/19/11 L53547-18 54.6 pH, Field 7.8 pH 07/19/11 L53547-19 99.3 pH, Field 7.7 pH 07/19/11 L53547-20 178 pH, Field 7.6 pH 07/19/11 L53547-21 179 pH, Field 7.6 pH 08/16/11 L53893-14 1.3 pH, Field 7.8 pH 08/16/11 L53893-15 15.1 pH, Field 7.7 pH 08/16/11 L53893-16 25 pH, Field 7.7 pH 08/16/11 L53893-17 35 pH, Field 7.7 pH 08/16/11 L53893-18 54.8 pH, Field 7.7 pH 08/16/11 L53893-19 99.3 pH, Field 7.6 pH 08/16/11 L53893-20 179 pH, Field 7.6 pH 08/16/11 L53893-21 179 pH, Field 7.6 pH 09/20/11 L54027-14 1.3 pH, Field 7.7 pH 09/20/11 L54027-15 15.1 pH, Field 7.6 pH 09/20/11 L54027-16 25.1 pH, Field 7.6 pH 09/20/11 L54027-17 35 pH, Field 7.6 pH 09/20/11 L54027-18 54.7 pH, Field 7.6 pH 09/20/11 L54027-19 99.2 pH, Field 7.6 pH 09/20/11 L54027-20 178 pH, Field 7.6 pH 09/20/11 L54027-21 179 pH, Field 7.6 pH 10/18/11 L54273-14 1.3 pH, Field 7.7 pH 10/18/11 L54273-15 14.6 pH, Field 7.6 pH 10/18/11 L54273-16 25 pH, Field 7.6 pH 10/18/11 L54273-17 34.6 pH, Field 7.6 pH 10/18/11 L54273-18 54.6 pH, Field 7.6 pH 10/18/11 L54273-19 99.4 pH, Field 7.5 pH 10/18/11 L54273-20 178 pH, Field 7.5 pH 10/18/11 L54273-21 178 pH, Field 7.5 pH 11/29/11 L54479-14 1.2 pH, Field 7.4 pH 11/29/11 L54479-15 15 pH, Field 7.4 pH 11/29/11 L54479-16 24.8 pH, Field 7.4 pH 11/29/11 L54479-17 34.7 pH, Field 7.4 pH 11/29/11 L54479-18 54.7 pH, Field 7.4 pH 11/29/11 L54479-19 99.1 pH, Field 7.4 pH 11/29/11 L54479-20 178 pH, Field 7.4 pHPage 14 of 24 

## Table A-2
Complete Water Quality Monitoring Data for Station LSNT01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 11/29/11 L54479-21 178 pH, Field 7.4 pH 12/14/11 L54765-7 5 pH, Field 7.5 pH 12/14/11 L54765-8 49.5 pH, Field 7.4 pH 12/14/11 L54765-9 158 pH, Field 7.4 pH 12/14/11 L54765-10 159 pH, Field 7.4 pH 12/20/11 L54810-14 1.2 pH, Field 7.5 pH 12/20/11 L54810-15 15.1 pH, Field 7.5 pH 12/20/11 L54810-16 24.9 pH, Field 7.5 pH 12/20/11 L54810-17 34.9 pH, Field 7.5 pH 12/20/11 L54810-18 54.6 pH, Field 7.5 pH 12/20/11 L54810-19 99.2 pH, Field 7.5 pH 12/20/11 L54810-20 178 pH, Field 7.4 pH 12/20/11 L54810-21 179 pH, Field 7.4 pH 07/30/12 L56062-7 5 pH, Field 7.8 pH 07/30/12 L56062-8 49.4 pH, Field 7.6 pH 07/30/12 L56062-9 158 pH, Field 7.5 pH 07/30/12 L56062-10 158 pH, Field 7.5 pH 12/12/12 L56990-7 4.9 pH, Field 7.5 pH 12/12/12 L56990-8 49.5 pH, Field 7.5 pH 12/12/12 L56990-10 158 pH, Field 7.5 pH 12/12/12 L56990-9 158 pH, Field 7.5 pH 01/19/11 L52444-14 1.3 Salinity, Field 28.256 PSS 01/19/11 L52444-15 15.2 Salinity, Field 29.181 PSS 01/19/11 L52444-16 25.1 Salinity, Field 29.259 PSS 01/19/11 L52444-17 34.9 Salinity, Field 29.323 PSS 01/19/11 L52444-18 54.8 Salinity, Field 29.396 PSS 01/19/11 L52444-19 99.4 Salinity, Field 29.638 PSS 01/19/11 L52444-20 198 Salinity, Field 29.730 PSS 01/19/11 L52444-21 198 Salinity, Field 29.730 PSS 02/23/11 L52544-14 1.3 Salinity, Field 28.868 PSS 02/23/11 L52544-15 15 Salinity, Field 28.882 PSS 02/23/11 L52544-16 24.9 Salinity, Field 28.923 PSS 02/23/11 L52544-17 34.7 Salinity, Field 28.929 PSS 02/23/11 L52544-18 54.8 Salinity, Field 29.012 PSS 02/23/11 L52544-19 99.3 Salinity, Field 29.417 PSS 02/23/11 L52544-20 178 Salinity, Field 29.543 PSS 02/23/11 L52544-21 178 Salinity, Field 29.544 PSS 03/22/11 L52735-14 1.4 Salinity, Field 28.716 PSS 03/22/11 L52735-15 15.3 Salinity, Field 28.871 PSS 03/22/11 L52735-16 25.2 Salinity, Field 28.906 PSS 03/22/11 L52735-17 35.1 Salinity, Field 28.934 PSS 03/22/11 L52735-18 54.9 Salinity, Field 29.038 PSS 03/22/11 L52735-19 99.6 Salinity, Field 29.278 PSS 03/22/11 L52735-20 178 Salinity, Field 29.528 PSS 03/22/11 L52735-21 179 Salinity, Field 29.528 PSS 04/19/11 L52887-14 1.3 Salinity, Field 27.866 PSS 04/19/11 L52887-15 15.1 Salinity, Field 28.431 PSS 04/19/11 L52887-16 24.9 Salinity, Field 28.502 PSS 04/19/11 L52887-17 35 Salinity, Field 28.544 PSS 04/19/11 L52887-18 54.8 Salinity, Field 28.593 PSS 04/19/11 L52887-19 99.2 Salinity, Field 28.965 PSS 04/19/11 L52887-20 178 Salinity, Field 29.229 PSS 04/19/11 L52887-21 179 Salinity, Field 29.229 PSSPage 15 of 24 

## Table A-2
Complete Water Quality Monitoring Data for Station LSNT01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 05/17/11 L53210-14 1.4 Salinity, Field 28.158 PSS 05/17/11 L53210-15 15.2 Salinity, Field 28.528 PSS 05/17/11 L53210-16 25.1 Salinity, Field 28.648 PSS 05/17/11 L53210-17 35 Salinity, Field 28.713 PSS 05/17/11 L53210-18 54.8 Salinity, Field 28.859 PSS 05/17/11 L53210-19 99.4 Salinity, Field 29.254 PSS 05/17/11 L53210-20 178 Salinity, Field 29.505 PSS 05/17/11 L53210-21 179 Salinity, Field 29.505 PSS 06/21/11 L53334-14 1.3 Salinity, Field 28.746 PSS 06/21/11 L53334-15 15.2 Salinity, Field 28.785 PSS 06/21/11 L53334-16 25.1 Salinity, Field 28.827 PSS 06/21/11 L53334-17 35 Salinity, Field 28.849 PSS 06/21/11 L53334-18 54.7 Salinity, Field 29.079 PSS 06/21/11 L53334-19 99.5 Salinity, Field 29.437 PSS 06/21/11 L53334-20 179 Salinity, Field 29.618 PSS 06/21/11 L53334-21 179 Salinity, Field 29.618 PSS 07/14/11 L53626-7 5.2 Salinity, Field 28.821 PSS 07/14/11 L53626-8 49.8 Salinity, Field 28.994 PSS 07/14/11 L53626-9 158 Salinity, Field 29.750 PSS 07/14/11 L53626-10 159 Salinity, Field 29.751 PSS 07/19/11 L53547-14 1.2 Salinity, Field 29.026 PSS 07/19/11 L53547-15 15.1 Salinity, Field 29.043 PSS 07/19/11 L53547-16 24.9 Salinity, Field 29.055 PSS 07/19/11 L53547-17 34.9 Salinity, Field 29.074 PSS 07/19/11 L53547-18 54.6 Salinity, Field 29.260 PSS 07/19/11 L53547-19 99.3 Salinity, Field 29.612 PSS 07/19/11 L53547-20 178 Salinity, Field 29.734 PSS 07/19/11 L53547-21 179 Salinity, Field 29.735 PSS 08/16/11 L53893-14 1.3 Salinity, Field 29.283 PSS 08/16/11 L53893-15 15.1 Salinity, Field 29.305 PSS 08/16/11 L53893-16 25 Salinity, Field 29.323 PSS 08/16/11 L53893-17 35 Salinity, Field 29.334 PSS 08/16/11 L53893-18 54.8 Salinity, Field 29.415 PSS 08/16/11 L53893-19 99.3 Salinity, Field 29.780 PSS 08/16/11 L53893-20 179 Salinity, Field 29.896 PSS 08/16/11 L53893-21 179 Salinity, Field 29.897 PSS 09/20/11 L54027-14 1.3 Salinity, Field 29.750 PSS 09/20/11 L54027-15 15.1 Salinity, Field 29.779 PSS 09/20/11 L54027-16 25.1 Salinity, Field 29.828 PSS 09/20/11 L54027-17 35 Salinity, Field 30.012 PSS 09/20/11 L54027-18 54.7 Salinity, Field 30.104 PSS 09/20/11 L54027-19 99.2 Salinity, Field 30.218 PSS 09/20/11 L54027-20 178 Salinity, Field 30.344 PSS 09/20/11 L54027-21 179 Salinity, Field 30.343 PSS 10/18/11 L54273-14 1.3 Salinity, Field 29.785 PSS 10/18/11 L54273-15 14.6 Salinity, Field 29.969 PSS 10/18/11 L54273-16 25 Salinity, Field 30.015 PSS 10/18/11 L54273-17 34.6 Salinity, Field 30.074 PSS 10/18/11 L54273-18 54.6 Salinity, Field 30.222 PSS 10/18/11 L54273-19 99.4 Salinity, Field 30.376 PSS 10/18/11 L54273-20 178 Salinity, Field 30.385 PSS 10/18/11 L54273-21 178 Salinity, Field 30.385 PSS 11/29/11 L54479-14 1.2 Salinity, Field 29.954 PSSPage 16 of 24 

## Table A-2
Complete Water Quality Monitoring Data for Station LSNT01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 11/29/11 L54479-15 15 Salinity, Field 29.958 PSS 11/29/11 L54479-16 24.8 Salinity, Field 29.973 PSS 11/29/11 L54479-17 34.7 Salinity, Field 30.089 PSS 11/29/11 L54479-18 54.7 Salinity, Field 30.155 PSS 11/29/11 L54479-19 99.1 Salinity, Field 30.232 PSS 11/29/11 L54479-20 178 Salinity, Field 30.259 PSS 11/29/11 L54479-21 178 Salinity, Field 30.259 PSS 12/14/11 L54765-7 5 Salinity, Field 29.638 PSS 12/14/11 L54765-8 49.5 Salinity, Field 29.864 PSS 12/14/11 L54765-9 158 Salinity, Field 30.146 PSS 12/14/11 L54765-10 159 Salinity, Field 30.146 PSS 12/20/11 L54810-14 1.2 Salinity, Field 29.778 PSS 12/20/11 L54810-15 15.1 Salinity, Field 29.784 PSS 12/20/11 L54810-16 24.9 Salinity, Field 29.784 PSS 12/20/11 L54810-17 34.9 Salinity, Field 29.780 PSS 12/20/11 L54810-18 54.6 Salinity, Field 29.855 PSS 12/20/11 L54810-19 99.2 Salinity, Field 29.960 PSS 12/20/11 L54810-20 178 Salinity, Field 30.019 PSS 12/20/11 L54810-21 179 Salinity, Field 30.019 PSS 01/26/12 L54843-14 1.2 Salinity, Field 29.605 PSS 01/26/12 L54843-15 15.1 Salinity, Field 29.630 PSS 01/26/12 L54843-16 24.9 Salinity, Field 29.697 PSS 01/26/12 L54843-17 34.9 Salinity, Field 29.799 PSS 01/26/12 L54843-18 54.6 Salinity, Field 29.863 PSS 01/26/12 L54843-19 99.2 Salinity, Field 29.891 PSS 01/26/12 L54843-20 178 Salinity, Field 29.905 PSS 01/26/12 L54843-21 179 Salinity, Field 29.905 PSS 02/23/12 L55090-14 1.2 Salinity, Field 29.382 PSS 02/23/12 L55090-15 15.1 Salinity, Field 29.383 PSS 02/23/12 L55090-16 24.9 Salinity, Field 29.387 PSS 02/23/12 L55090-17 34.7 Salinity, Field 29.418 PSS 02/23/12 L55090-18 54.4 Salinity, Field 29.512 PSS 02/23/12 L55090-19 99 Salinity, Field 29.682 PSS 02/23/12 L55090-20 178 Salinity, Field 29.771 PSS 02/23/12 L55090-21 179 Salinity, Field 29.772 PSS 03/22/12 L55196-14 1.3 Salinity, Field 29.239 PSS 03/22/12 L55196-15 15.1 Salinity, Field 29.242 PSS 03/22/12 L55196-16 25.1 Salinity, Field 29.242 PSS 03/22/12 L55196-17 35 Salinity, Field 29.242 PSS 03/22/12 L55196-18 54.6 Salinity, Field 29.242 PSS 03/22/12 L55196-19 99.3 Salinity, Field 29.545 PSS 03/22/12 L55196-20 178 Salinity, Field 29.781 PSS 03/22/12 L55196-21 179 Salinity, Field 29.781 PSS 04/17/12 L55374-14 1.5 Salinity, Field 28.868 PSS 04/17/12 L55374-15 15.4 Salinity, Field 28.916 PSS 04/17/12 L55374-16 25.2 Salinity, Field 28.958 PSS 04/17/12 L55374-17 35.1 Salinity, Field 28.980 PSS 04/17/12 L55374-18 54.8 Salinity, Field 29.037 PSS 04/17/12 L55374-19 99.6 Salinity, Field 29.237 PSS 04/17/12 L55374-20 179 Salinity, Field 29.511 PSS 04/17/12 L55374-21 179 Salinity, Field 29.511 PSS 05/22/12 L55538-14 1.4 Salinity, Field 28.313 PSS 05/22/12 L55538-15 15.3 Salinity, Field 28.431 PSSPage 17 of 24 

## Table A-2
Complete Water Quality Monitoring Data for Station LSNT01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 05/22/12 L55538-16 25.1 Salinity, Field 28.495 PSS 05/22/12 L55538-17 35 Salinity, Field 28.544 PSS 05/22/12 L55538-18 54.8 Salinity, Field 28.652 PSS 05/22/12 L55538-19 99.5 Salinity, Field 29.291 PSS 05/22/12 L55538-20 179 Salinity, Field 29.408 PSS 05/22/12 L55538-21 179 Salinity, Field 29.408 PSS 06/19/12 L55792-14 1.3 Salinity, Field 28.293 PSS 06/19/12 L55792-15 15.2 Salinity, Field 28.558 PSS 06/19/12 L55792-16 25.1 Salinity, Field 28.696 PSS 06/19/12 L55792-17 34.9 Salinity, Field 28.861 PSS 06/19/12 L55792-18 54.4 Salinity, Field 28.990 PSS 06/19/12 L55792-19 99.3 Salinity, Field 29.531 PSS 06/19/12 L55792-20 178 Salinity, Field 29.816 PSS 06/19/12 L55792-21 179 Salinity, Field 29.816 PSS 07/17/12 L55945-14 1.2 Salinity, Field 28.733 PSS 07/17/12 L55945-15 15 Salinity, Field 28.902 PSS 07/17/12 L55945-16 24.9 Salinity, Field 29.031 PSS 07/17/12 L55945-17 35 Salinity, Field 29.080 PSS 07/17/12 L55945-18 54.7 Salinity, Field 29.158 PSS 07/17/12 L55945-19 99.3 Salinity, Field 29.559 PSS 07/17/12 L55945-20 179 Salinity, Field 29.818 PSS 07/17/12 L55945-21 179 Salinity, Field 29.818 PSS 07/30/12 L56062-7 5 Salinity, Field 28.853 PSS 07/30/12 L56062-8 49.4 Salinity, Field 29.454 PSS 07/30/12 L56062-10 158 Salinity, Field 29.791 PSS 07/30/12 L56062-9 158 Salinity, Field 29.791 PSS 08/21/12 L56172-14 1.3 Salinity, Field 29.255 PSS 08/21/12 L56172-15 15.1 Salinity, Field 29.332 PSS 08/21/12 L56172-16 24.9 Salinity, Field 29.341 PSS 08/21/12 L56172-17 34.8 Salinity, Field 29.355 PSS 08/21/12 L56172-18 54.7 Salinity, Field 29.489 PSS 08/21/12 L56172-19 99.2 Salinity, Field 29.852 PSS 08/21/12 L56172-20 178 Salinity, Field 30.040 PSS 08/21/12 L56172-21 179 Salinity, Field 30.040 PSS 09/18/12 L56392-14 1.2 Salinity, Field 29.718 PSS 09/18/12 L56392-15 15.1 Salinity, Field 29.737 PSS 09/18/12 L56392-16 24.6 Salinity, Field 29.762 PSS 09/18/12 L56392-17 34.9 Salinity, Field 29.770 PSS 09/18/12 L56392-18 54.6 Salinity, Field 29.820 PSS 09/18/12 L56392-19 99.4 Salinity, Field 30.219 PSS 09/18/12 L56392-20 178 Salinity, Field 30.445 PSS 09/18/12 L56392-21 179 Salinity, Field 30.445 PSS 10/18/12 L56639-14 1.2 Salinity, Field 30.152 PSS 10/18/12 L56639-15 15.3 Salinity, Field 30.162 PSS 10/18/12 L56639-16 25.1 Salinity, Field 30.192 PSS 10/18/12 L56639-17 35.1 Salinity, Field 30.230 PSS 10/18/12 L56639-18 54.8 Salinity, Field 30.269 PSS 10/18/12 L56639-19 99.5 Salinity, Field 30.523 PSS 10/18/12 L56639-20 178 Salinity, Field 30.713 PSS 10/18/12 L56639-21 179 Salinity, Field 30.713 PSS 11/27/12 L56806-14 0.78 Salinity, Field 27.705 PSS 11/27/12 L56806-15 14.5 Salinity, Field 29.593 PSS 11/27/12 L56806-16 24.8 Salinity, Field 29.683 PSSPage 18 of 24 

## Table A-2
Complete Water Quality Monitoring Data for Station LSNT01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 11/27/12 L56806-17 34.5 Salinity, Field 29.767 PSS 11/27/12 L56806-18 54 Salinity, Field 29.877 PSS 11/27/12 L56806-19 98.7 Salinity, Field 30.205 PSS 11/27/12 L56806-20 177 Salinity, Field 30.333 PSS 11/27/12 L56806-21 178 Salinity, Field 30.334 PSS 12/12/12 L56990-7 4.9 Salinity, Field 29.519 PSS 12/12/12 L56990-8 49.5 Salinity, Field 29.577 PSS 12/12/12 L56990-10 158 Salinity, Field 30.070 PSS 12/12/12 L56990-9 158 Salinity, Field 30.068 PSS 12/27/12 L57088-14 1 Salinity, Field 29.218 PSS 12/27/12 L57088-15 14.9 Salinity, Field 29.295 PSS 12/27/12 L57088-16 24.7 Salinity, Field 29.313 PSS 12/27/12 L57088-17 34.4 Salinity, Field 29.329 PSS 12/27/12 L57088-18 54.3 Salinity, Field 29.354 PSS 12/27/12 L57088-19 98.9 Salinity, Field 29.658 PSS 12/27/12 L57088-20 178 Salinity, Field 29.754 PSS 12/27/12 L57088-21 178 Salinity, Field 29.754 PSS 07/14/11 L53626-7 5.2 Antimony, Dissolved, ICP-MS 0.155 ug/L 0.005 0.025 07/14/11 L53626-8 49.8 Antimony, Dissolved, ICP-MS 0.152 ug/L 0.005 0.025 07/14/11 L53626-9 158 Antimony, Dissolved, ICP-MS 0.155 ug/L 0.005 0.025 07/14/11 L53626-10 159 Antimony, Dissolved, ICP-MS 0.154 ug/L 0.005 0.025 12/14/11 L54765-7 5 Antimony, Dissolved, ICP-MS 0.171 ug/L 0.005 0.025 12/14/11 L54765-8 49.5 Antimony, Dissolved, ICP-MS 0.168 ug/L 0.005 0.025 12/14/11 L54765-9 158 Antimony, Dissolved, ICP-MS 0.173 ug/L 0.005 0.025 12/14/11 L54765-10 159 Antimony, Dissolved, ICP-MS 0.171 ug/L 0.005 0.025 07/30/12 L56062-7 5 Antimony, Dissolved, ICP-MS 0.143 ug/L 0.005 0.025 07/30/12 L56062-8 49.4 Antimony, Dissolved, ICP-MS 0.148 ug/L 0.005 0.025 07/30/12 L56062-10 158 Antimony, Dissolved, ICP-MS 0.144 ug/L 0.005 0.025 07/30/12 L56062-9 158 Antimony, Dissolved, ICP-MS 0.146 ug/L 0.005 0.025 12/12/12 L56990-7 4.9 Antimony, Dissolved, ICP-MS 0.160 ug/L 0.005 0.025 12/12/12 L56990-8 49.5 Antimony, Dissolved, ICP-MS 0.160 ug/L 0.005 0.025 12/12/12 L56990-10 158 Antimony, Dissolved, ICP-MS 0.173 ug/L 0.005 0.025 12/12/12 L56990-9 158 Antimony, Dissolved, ICP-MS 0.165 ug/L 0.005 0.025 07/14/11 L53626-7 5.2 Antimony, Total, ICP-MS 0.160 ug/L 0.005 0.025 07/14/11 L53626-8 49.8 Antimony, Total, ICP-MS 0.158 ug/L 0.005 0.025 07/14/11 L53626-9 158 Antimony, Total, ICP-MS 0.164 ug/L 0.005 0.025 07/14/11 L53626-10 159 Antimony, Total, ICP-MS 0.161 ug/L 0.005 0.025 12/14/11 L54765-7 5 Antimony, Total, ICP-MS 0.157 ug/L 0.005 0.025 12/14/11 L54765-8 49.5 Antimony, Total, ICP-MS 0.163 ug/L 0.005 0.025 12/14/11 L54765-9 158 Antimony, Total, ICP-MS 0.162 ug/L 0.005 0.025 12/14/11 L54765-10 159 Antimony, Total, ICP-MS 0.167 ug/L 0.005 0.025 07/30/12 L56062-7 5 Antimony, Total, ICP-MS 0.171 ug/L 0.005 0.025 07/30/12 L56062-8 49.4 Antimony, Total, ICP-MS 0.172 ug/L 0.005 0.025 07/30/12 L56062-10 158 Antimony, Total, ICP-MS 0.164 ug/L 0.005 0.025 07/30/12 L56062-9 158 Antimony, Total, ICP-MS 0.171 ug/L 0.005 0.025 12/12/12 L56990-7 4.9 Antimony, Total, ICP-MS 0.172 ug/L 0.005 0.025 12/12/12 L56990-8 49.5 Antimony, Total, ICP-MS 0.182 ug/L 0.005 0.025 12/12/12 L56990-10 158 Antimony, Total, ICP-MS 0.183 ug/L 0.005 0.025 12/12/12 L56990-9 158 Antimony, Total, ICP-MS 0.174 ug/L 0.005 0.025 07/14/11 L53626-7 5.2 Arsenic, Dissolved, ICP-MS 1.22 ug/L 0.01 0.05 07/14/11 L53626-8 49.8 Arsenic, Dissolved, ICP-MS 1.22 ug/L 0.01 0.05 07/14/11 L53626-9 158 Arsenic, Dissolved, ICP-MS 1.28 ug/L 0.01 0.05 07/14/11 L53626-10 159 Arsenic, Dissolved, ICP-MS 1.26 ug/L 0.01 0.05Page 19 of 24 

## Table A-2
Complete Water Quality Monitoring Data for Station LSNT01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 12/14/11 L54765-7 5 Arsenic, Dissolved, ICP-MS 1.40 ug/L 0.01 0.05 12/14/11 L54765-8 49.5 Arsenic, Dissolved, ICP-MS 1.40 ug/L 0.01 0.05 12/14/11 L54765-9 158 Arsenic, Dissolved, ICP-MS 1.43 ug/L 0.01 0.05 12/14/11 L54765-10 159 Arsenic, Dissolved, ICP-MS 1.46 ug/L 0.01 0.05 07/30/12 L56062-7 5 Arsenic, Dissolved, ICP-MS 1.28 ug/L 0.01 0.05 07/30/12 L56062-8 49.4 Arsenic, Dissolved, ICP-MS 1.37 ug/L 0.01 0.05 07/30/12 L56062-10 158 Arsenic, Dissolved, ICP-MS 1.43 ug/L 0.01 0.05 07/30/12 L56062-9 158 Arsenic, Dissolved, ICP-MS 1.42 ug/L 0.01 0.05 12/12/12 L56990-7 4.9 Arsenic, Dissolved, ICP-MS 1.39 ug/L 0.01 0.05 12/12/12 L56990-8 49.5 Arsenic, Dissolved, ICP-MS 1.40 ug/L 0.01 0.05 12/12/12 L56990-10 158 Arsenic, Dissolved, ICP-MS 1.45 ug/L 0.01 0.05 12/12/12 L56990-9 158 Arsenic, Dissolved, ICP-MS 1.45 ug/L 0.01 0.05 07/14/11 L53626-7 5.2 Arsenic, Total, ICP-MS 1.22 ug/L 0.01 0.05 07/14/11 L53626-8 49.8 Arsenic, Total, ICP-MS 1.32 ug/L 0.01 0.05 07/14/11 L53626-9 158 Arsenic, Total, ICP-MS 1.39 ug/L 0.01 0.05 07/14/11 L53626-10 159 Arsenic, Total, ICP-MS 1.35 ug/L 0.01 0.05 12/14/11 L54765-7 5 Arsenic, Total, ICP-MS 1.37 ug/L 0.01 0.05 12/14/11 L54765-8 49.5 Arsenic, Total, ICP-MS 1.42 ug/L 0.01 0.05 12/14/11 L54765-9 158 Arsenic, Total, ICP-MS 1.41 ug/L 0.01 0.05 12/14/11 L54765-10 159 Arsenic, Total, ICP-MS 1.45 ug/L 0.01 0.05 07/30/12 L56062-7 5 Arsenic, Total, ICP-MS 1.30 ug/L 0.01 0.05 07/30/12 L56062-8 49.4 Arsenic, Total, ICP-MS 1.37 ug/L 0.01 0.05 07/30/12 L56062-10 158 Arsenic, Total, ICP-MS 1.44 ug/L 0.01 0.05 07/30/12 L56062-9 158 Arsenic, Total, ICP-MS 1.44 ug/L 0.01 0.05 12/12/12 L56990-7 4.9 Arsenic, Total, ICP-MS 1.43 ug/L 0.01 0.05 12/12/12 L56990-8 49.5 Arsenic, Total, ICP-MS 1.41 ug/L 0.01 0.05 12/12/12 L56990-10 158 Arsenic, Total, ICP-MS 1.45 ug/L 0.01 0.05 12/12/12 L56990-9 158 Arsenic, Total, ICP-MS 1.49 ug/L 0.01 0.05 07/14/11 L53626-7 5.2 Cadmium, Dissolved, ICP-MS 0.0658 ug/L 0.005 0.025 07/14/11 L53626-8 49.8 Cadmium, Dissolved, ICP-MS 0.0636 ug/L 0.005 0.025 07/14/11 L53626-9 158 Cadmium, Dissolved, ICP-MS 0.0679 ug/L 0.005 0.025 07/14/11 L53626-10 159 Cadmium, Dissolved, ICP-MS 0.0700 ug/L 0.005 0.025 12/14/11 L54765-7 5 Cadmium, Dissolved, ICP-MS 0.0730 ug/L 0.005 0.025 12/14/11 L54765-8 49.5 Cadmium, Dissolved, ICP-MS 0.0709 ug/L 0.005 0.025 12/14/11 L54765-9 158 Cadmium, Dissolved, ICP-MS 0.0736 ug/L 0.005 0.025 12/14/11 L54765-10 159 Cadmium, Dissolved, ICP-MS 0.0749 ug/L 0.005 0.025 07/30/12 L56062-7 5 Cadmium, Dissolved, ICP-MS 0.0618 ug/L 0.005 0.025 07/30/12 L56062-8 49.4 Cadmium, Dissolved, ICP-MS 0.0676 ug/L 0.005 0.025 07/30/12 L56062-10 158 Cadmium, Dissolved, ICP-MS 0.0706 ug/L 0.005 0.025 07/30/12 L56062-9 158 Cadmium, Dissolved, ICP-MS 0.0724 ug/L 0.005 0.025 12/12/12 L56990-7 4.9 Cadmium, Dissolved, ICP-MS 0.0703 ug/L 0.005 0.025 12/12/12 L56990-8 49.5 Cadmium, Dissolved, ICP-MS 0.0732 ug/L 0.005 0.025 12/12/12 L56990-10 158 Cadmium, Dissolved, ICP-MS 0.0715 ug/L 0.005 0.025 12/12/12 L56990-9 158 Cadmium, Dissolved, ICP-MS 0.0717 ug/L 0.005 0.025 07/14/11 L53626-7 5.2 Cadmium, Total, ICP-MS 0.0611 ug/L 0.005 0.025 07/14/11 L53626-8 49.8 Cadmium, Total, ICP-MS 0.0653 ug/L 0.005 0.025 07/14/11 L53626-9 158 Cadmium, Total, ICP-MS 0.0703 ug/L 0.005 0.025 07/14/11 L53626-10 159 Cadmium, Total, ICP-MS 0.0721 ug/L 0.005 0.025 12/14/11 L54765-7 5 Cadmium, Total, ICP-MS 0.0708 ug/L 0.005 0.025 12/14/11 L54765-8 49.5 Cadmium, Total, ICP-MS 0.0710 ug/L 0.005 0.025 12/14/11 L54765-9 158 Cadmium, Total, ICP-MS 0.0728 ug/L 0.005 0.025 12/14/11 L54765-10 159 Cadmium, Total, ICP-MS 0.0742 ug/L 0.005 0.025 07/30/12 L56062-7 5 Cadmium, Total, ICP-MS 0.0712 ug/L 0.005 0.025Page 20 of 24 

## Table A-2
Complete Water Quality Monitoring Data for Station LSNT01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 07/30/12 L56062-8 49.4 Cadmium, Total, ICP-MS 0.0744 ug/L 0.005 0.025 07/30/12 L56062-10 158 Cadmium, Total, ICP-MS 0.0755 ug/L 0.005 0.025 07/30/12 L56062-9 158 Cadmium, Total, ICP-MS 0.0764 ug/L 0.005 0.025 12/12/12 L56990-7 4.9 Cadmium, Total, ICP-MS 0.0804 ug/L 0.005 0.025 12/12/12 L56990-8 49.5 Cadmium, Total, ICP-MS 0.0778 ug/L 0.005 0.025 12/12/12 L56990-10 158 Cadmium, Total, ICP-MS 0.0830 ug/L 0.005 0.025 12/12/12 L56990-9 158 Cadmium, Total, ICP-MS 0.0818 ug/L 0.005 0.025 07/14/11 L53626-7 5.2 Chromium, Dissolved, ICP-MS 0.095 ug/L <RDL 0.05 0.25 07/14/11 L53626-8 49.8 Chromium, Dissolved, ICP-MS 0.11 ug/L <RDL 0.05 0.25 07/14/11 L53626-9 158 Chromium, Dissolved, ICP-MS 0.11 ug/L <RDL 0.05 0.25 07/14/11 L53626-10 159 Chromium, Dissolved, ICP-MS 0.11 ug/L <RDL 0.05 0.25 12/14/11 L54765-7 5 Chromium, Dissolved, ICP-MS 0.091 ug/L <RDL 0.05 0.25 12/14/11 L54765-8 49.5 Chromium, Dissolved, ICP-MS 0.088 ug/L <RDL 0.05 0.25 12/14/11 L54765-9 158 Chromium, Dissolved, ICP-MS 0.093 ug/L <RDL 0.05 0.25 12/14/11 L54765-10 159 Chromium, Dissolved, ICP-MS 0.10 ug/L <RDL 0.05 0.25 07/30/12 L56062-7 5 Chromium, Dissolved, ICP-MS 0.18 ug/L <RDL 0.05 0.25 07/30/12 L56062-8 49.4 Chromium, Dissolved, ICP-MS 0.15 ug/L <RDL 0.05 0.25 07/30/12 L56062-10 158 Chromium, Dissolved, ICP-MS 0.15 ug/L <RDL 0.05 0.25 07/30/12 L56062-9 158 Chromium, Dissolved, ICP-MS 0.13 ug/L <RDL 0.05 0.25 12/12/12 L56990-7 4.9 Chromium, Dissolved, ICP-MS 0.10 ug/L <RDL 0.05 0.25 12/12/12 L56990-8 49.5 Chromium, Dissolved, ICP-MS 0.10 ug/L <RDL 0.05 0.25 12/12/12 L56990-10 158 Chromium, Dissolved, ICP-MS 0.10 ug/L <RDL 0.05 0.25 12/12/12 L56990-9 158 Chromium, Dissolved, ICP-MS 0.091 ug/L <RDL 0.05 0.25 07/14/11 L53626-7 5.2 Chromium, Total, ICP-MS 0.094 ug/L <RDL 0.05 0.25 07/14/11 L53626-8 49.8 Chromium, Total, ICP-MS 0.094 ug/L <RDL 0.05 0.25 07/14/11 L53626-9 158 Chromium, Total, ICP-MS 0.11 ug/L <RDL 0.05 0.25 07/14/11 L53626-10 159 Chromium, Total, ICP-MS 0.11 ug/L <RDL 0.05 0.25 12/14/11 L54765-7 5 Chromium, Total, ICP-MS 0.12 ug/L <RDL 0.05 0.25 12/14/11 L54765-8 49.5 Chromium, Total, ICP-MS 0.11 ug/L <RDL 0.05 0.25 12/14/11 L54765-9 158 Chromium, Total, ICP-MS 0.13 ug/L <RDL 0.05 0.25 12/14/11 L54765-10 159 Chromium, Total, ICP-MS 0.14 ug/L <RDL 0.05 0.25 07/30/12 L56062-7 5 Chromium, Total, ICP-MS 0.16 ug/L <RDL 0.05 0.25 07/30/12 L56062-8 49.4 Chromium, Total, ICP-MS 0.13 ug/L <RDL 0.05 0.25 07/30/12 L56062-10 158 Chromium, Total, ICP-MS 0.14 ug/L <RDL 0.05 0.25 07/30/12 L56062-9 158 Chromium, Total, ICP-MS 0.15 ug/L <RDL 0.05 0.25 12/12/12 L56990-7 4.9 Chromium, Total, ICP-MS 0.088 ug/L <RDL 0.05 0.25 12/12/12 L56990-8 49.5 Chromium, Total, ICP-MS 0.10 ug/L <RDL 0.05 0.25 12/12/12 L56990-10 158 Chromium, Total, ICP-MS 0.11 ug/L <RDL 0.05 0.25 12/12/12 L56990-9 158 Chromium, Total, ICP-MS 0.14 ug/L <RDL 0.05 0.25 07/14/11 L53626-7 5.2 Copper, Dissolved, ICP-MS 0.362 ug/L 0.025 0.125 07/14/11 L53626-8 49.8 Copper, Dissolved, ICP-MS 0.271 ug/L 0.025 0.125 07/14/11 L53626-9 158 Copper, Dissolved, ICP-MS 0.231 ug/L 0.025 0.125 07/14/11 L53626-10 159 Copper, Dissolved, ICP-MS 0.235 ug/L 0.025 0.125 12/14/11 L54765-7 5 Copper, Dissolved, ICP-MS 0.342 ug/L 0.025 0.125 12/14/11 L54765-8 49.5 Copper, Dissolved, ICP-MS 0.324 ug/L 0.025 0.125 12/14/11 L54765-9 158 Copper, Dissolved, ICP-MS 0.293 ug/L 0.025 0.125 12/14/11 L54765-10 159 Copper, Dissolved, ICP-MS 0.283 ug/L 0.025 0.125 07/30/12 L56062-7 5 Copper, Dissolved, ICP-MS 0.387 ug/L 0.025 0.125 07/30/12 L56062-8 49.4 Copper, Dissolved, ICP-MS 0.337 ug/L 0.025 0.125 07/30/12 L56062-10 158 Copper, Dissolved, ICP-MS 0.291 ug/L 0.025 0.125 07/30/12 L56062-9 158 Copper, Dissolved, ICP-MS 0.272 ug/L 0.025 0.125 12/12/12 L56990-7 4.9 Copper, Dissolved, ICP-MS 0.347 ug/L 0.025 0.125 12/12/12 L56990-8 49.5 Copper, Dissolved, ICP-MS 0.281 ug/L 0.025 0.125Page 21 of 24 

## Table A-2
Complete Water Quality Monitoring Data for Station LSNT01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 12/12/12 L56990-10 158 Copper, Dissolved, ICP-MS 0.262 ug/L 0.025 0.125 12/12/12 L56990-9 158 Copper, Dissolved, ICP-MS 0.266 ug/L 0.025 0.125 07/14/11 L53626-7 5.2 Copper, Total, ICP-MS 0.298 ug/L 0.025 0.125 07/14/11 L53626-8 49.8 Copper, Total, ICP-MS 0.293 ug/L 0.025 0.125 07/14/11 L53626-9 158 Copper, Total, ICP-MS 0.260 ug/L 0.025 0.125 07/14/11 L53626-10 159 Copper, Total, ICP-MS 0.262 ug/L 0.025 0.125 12/14/11 L54765-7 5 Copper, Total, ICP-MS 0.407 ug/L 0.025 0.125 12/14/11 L54765-8 49.5 Copper, Total, ICP-MS 0.385 ug/L 0.025 0.125 12/14/11 L54765-9 158 Copper, Total, ICP-MS 0.380 ug/L 0.025 0.125 12/14/11 L54765-10 159 Copper, Total, ICP-MS 0.416 ug/L 0.025 0.125 07/30/12 L56062-7 5 Copper, Total, ICP-MS 0.441 ug/L 0.025 0.125 07/30/12 L56062-8 49.4 Copper, Total, ICP-MS 0.349 ug/L 0.025 0.125 07/30/12 L56062-10 158 Copper, Total, ICP-MS 0.343 ug/L 0.025 0.125 07/30/12 L56062-9 158 Copper, Total, ICP-MS 0.340 ug/L 0.025 0.125 12/12/12 L56990-7 4.9 Copper, Total, ICP-MS 1.99 ug/L 0.025 0.125 12/12/12 L56990-8 49.5 Copper, Total, ICP-MS 0.340 ug/L 0.025 0.125 12/12/12 L56990-10 158 Copper, Total, ICP-MS 0.356 ug/L 0.025 0.125 12/12/12 L56990-9 158 Copper, Total, ICP-MS 0.354 ug/L 0.025 0.125 07/14/11 L53626-7 5.2 Lead, Dissolved, ICP-MS 0.0077 ug/L <RDL 0.005 0.025 07/14/11 L53626-8 49.8 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 07/14/11 L53626-9 158 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 07/14/11 L53626-10 159 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 12/14/11 L54765-7 5 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 12/14/11 L54765-8 49.5 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 12/14/11 L54765-9 158 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 12/14/11 L54765-10 159 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 07/30/12 L56062-7 5 Lead, Dissolved, ICP-MS 0.0063 ug/L <RDL 0.005 0.025 07/30/12 L56062-8 49.4 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 07/30/12 L56062-10 158 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 07/30/12 L56062-9 158 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 12/12/12 L56990-7 4.9 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 12/12/12 L56990-8 49.5 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 12/12/12 L56990-10 158 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 12/12/12 L56990-9 158 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 07/14/11 L53626-7 5.2 Lead, Total, ICP-MS ug/L <MDL 0.005 0.025 07/14/11 L53626-8 49.8 Lead, Total, ICP-MS 0.016 ug/L <RDL 0.005 0.025 07/14/11 L53626-9 158 Lead, Total, ICP-MS 0.022 ug/L <RDL 0.005 0.025 07/14/11 L53626-10 159 Lead, Total, ICP-MS 0.023 ug/L <RDL 0.005 0.025 12/14/11 L54765-7 5 Lead, Total, ICP-MS 0.019 ug/L <RDL 0.005 0.025 12/14/11 L54765-8 49.5 Lead, Total, ICP-MS 0.018 ug/L <RDL 0.005 0.025 12/14/11 L54765-9 158 Lead, Total, ICP-MS 0.025 ug/L <RDL 0.005 0.025 12/14/11 L54765-10 159 Lead, Total, ICP-MS 0.035 ug/L 0.005 0.025 07/30/12 L56062-7 5 Lead, Total, ICP-MS 0.014 ug/L <RDL 0.005 0.025 07/30/12 L56062-8 49.4 Lead, Total, ICP-MS 0.014 ug/L <RDL 0.005 0.025 07/30/12 L56062-10 158 Lead, Total, ICP-MS 0.0307 ug/L 0.005 0.025 07/30/12 L56062-9 158 Lead, Total, ICP-MS 0.0302 ug/L 0.005 0.025 12/12/12 L56990-7 4.9 Lead, Total, ICP-MS 0.0413 ug/L 0.005 0.025 12/12/12 L56990-8 49.5 Lead, Total, ICP-MS 0.0335 ug/L 0.005 0.025 12/12/12 L56990-10 158 Lead, Total, ICP-MS 0.0492 ug/L 0.005 0.025 12/12/12 L56990-9 158 Lead, Total, ICP-MS 0.0479 ug/L 0.005 0.025 07/14/11 L53626-7 5.2 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 07/14/11 L53626-8 49.8 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 07/14/11 L53626-9 158 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005Page 22 of 24 

## Table A-2
Complete Water Quality Monitoring Data for Station LSNT01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 07/14/11 L53626-10 159 Mercury, Dissolved, CVAF 0.00023 ug/L <RDL 0.0002 0.0005 12/14/11 L54765-7 5 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 12/14/11 L54765-8 49.5 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 12/14/11 L54765-9 158 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 12/14/11 L54765-10 159 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 07/30/12 L56062-7 5 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 07/30/12 L56062-8 49.4 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 07/30/12 L56062-10 158 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 07/30/12 L56062-9 158 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 12/12/12 L56990-7 4.9 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 12/12/12 L56990-8 49.5 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 12/12/12 L56990-10 158 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 12/12/12 L56990-9 158 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 07/14/11 L53626-7 5.2 Mercury, Total, CVAF 0.00023 ug/L <RDL 0.0002 0.0005 07/14/11 L53626-8 49.8 Mercury, Total, CVAF 0.00024 ug/L <RDL 0.0002 0.0005 07/14/11 L53626-9 158 Mercury, Total, CVAF 0.00027 ug/L <RDL 0.0002 0.0005 07/14/11 L53626-10 159 Mercury, Total, CVAF 0.00024 ug/L <RDL 0.0002 0.0005 12/14/11 L54765-7 5 Mercury, Total, CVAF 0.00023 ug/L <RDL 0.0002 0.0005 12/14/11 L54765-8 49.5 Mercury, Total, CVAF 0.00029 ug/L <RDL 0.0002 0.0005 12/14/11 L54765-9 158 Mercury, Total, CVAF 0.00040 ug/L <RDL 0.0002 0.0005 12/14/11 L54765-10 159 Mercury, Total, CVAF 0.00030 ug/L <RDL 0.0002 0.0005 07/30/12 L56062-7 5 Mercury, Total, CVAF ug/L <MDL 0.0002 0.0005 07/30/12 L56062-8 49.4 Mercury, Total, CVAF ug/L <MDL 0.0002 0.0005 07/30/12 L56062-10 158 Mercury, Total, CVAF ug/L <MDL 0.0002 0.0005 07/30/12 L56062-9 158 Mercury, Total, CVAF ug/L <MDL 0.0002 0.0005 12/12/12 L56990-7 4.9 Mercury, Total, CVAF 0.00030 ug/L <RDL 0.0002 0.0005 12/12/12 L56990-8 49.5 Mercury, Total, CVAF 0.00032 ug/L <RDL 0.0002 0.0005 12/12/12 L56990-10 158 Mercury, Total, CVAF 0.00036 ug/L <RDL 0.0002 0.0005 12/12/12 L56990-9 158 Mercury, Total, CVAF 0.00039 ug/L <RDL 0.0002 0.0005 07/14/11 L53626-7 5.2 Nickel, Dissolved, ICP-MS 0.417 ug/L 0.025 0.125 07/14/11 L53626-8 49.8 Nickel, Dissolved, ICP-MS 0.426 ug/L 0.025 0.125 07/14/11 L53626-9 158 Nickel, Dissolved, ICP-MS 0.421 ug/L 0.025 0.125 07/14/11 L53626-10 159 Nickel, Dissolved, ICP-MS 0.418 ug/L 0.025 0.125 12/14/11 L54765-7 5 Nickel, Dissolved, ICP-MS 0.403 ug/L 0.025 0.125 12/14/11 L54765-8 49.5 Nickel, Dissolved, ICP-MS 0.390 ug/L 0.025 0.125 12/14/11 L54765-9 158 Nickel, Dissolved, ICP-MS 0.395 ug/L 0.025 0.125 12/14/11 L54765-10 159 Nickel, Dissolved, ICP-MS 0.395 ug/L 0.025 0.125 07/30/12 L56062-7 5 Nickel, Dissolved, ICP-MS 0.406 ug/L 0.025 0.125 07/30/12 L56062-8 49.4 Nickel, Dissolved, ICP-MS 0.406 ug/L 0.025 0.125 07/30/12 L56062-10 158 Nickel, Dissolved, ICP-MS 0.398 ug/L 0.025 0.125 07/30/12 L56062-9 158 Nickel, Dissolved, ICP-MS 0.396 ug/L 0.025 0.125 12/12/12 L56990-7 4.9 Nickel, Dissolved, ICP-MS 0.429 ug/L 0.025 0.125 12/12/12 L56990-8 49.5 Nickel, Dissolved, ICP-MS 0.424 ug/L 0.025 0.125 12/12/12 L56990-10 158 Nickel, Dissolved, ICP-MS 0.430 ug/L 0.025 0.125 12/12/12 L56990-9 158 Nickel, Dissolved, ICP-MS 0.424 ug/L 0.025 0.125 07/14/11 L53626-7 5.2 Nickel, Total, ICP-MS 0.422 ug/L 0.025 0.125 07/14/11 L53626-8 49.8 Nickel, Total, ICP-MS 0.420 ug/L 0.025 0.125 07/14/11 L53626-9 158 Nickel, Total, ICP-MS 0.402 ug/L 0.025 0.125 07/14/11 L53626-10 159 Nickel, Total, ICP-MS 0.426 ug/L 0.025 0.125 12/14/11 L54765-7 5 Nickel, Total, ICP-MS 0.446 ug/L 0.025 0.125 12/14/11 L54765-8 49.5 Nickel, Total, ICP-MS 0.434 ug/L 0.025 0.125 12/14/11 L54765-9 158 Nickel, Total, ICP-MS 0.464 ug/L 0.025 0.125 12/14/11 L54765-10 159 Nickel, Total, ICP-MS 0.488 ug/L 0.025 0.125Page 23 of 24 

## Table A-2
Complete Water Quality Monitoring Data for Station LSNT01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 07/30/12 L56062-7 5 Nickel, Total, ICP-MS 0.511 ug/L 0.025 0.125 07/30/12 L56062-8 49.4 Nickel, Total, ICP-MS 0.428 ug/L 0.025 0.125 07/30/12 L56062-10 158 Nickel, Total, ICP-MS 0.444 ug/L 0.025 0.125 07/30/12 L56062-9 158 Nickel, Total, ICP-MS 0.449 ug/L 0.025 0.125 12/12/12 L56990-7 4.9 Nickel, Total, ICP-MS 0.419 ug/L 0.025 0.125 12/12/12 L56990-8 49.5 Nickel, Total, ICP-MS 0.403 ug/L 0.025 0.125 12/12/12 L56990-10 158 Nickel, Total, ICP-MS 0.420 ug/L 0.025 0.125 12/12/12 L56990-9 158 Nickel, Total, ICP-MS 0.404 ug/L 0.025 0.125 07/14/11 L53626-7 5.2 Silver, Dissolved, ICP-MS 0.015 ug/L <RDL 0.01 0.05 07/14/11 L53626-8 49.8 Silver, Dissolved, ICP-MS 0.016 ug/L <RDL 0.01 0.05 07/14/11 L53626-9 158 Silver, Dissolved, ICP-MS 0.017 ug/L <RDL 0.01 0.05 07/14/11 L53626-10 159 Silver, Dissolved, ICP-MS 0.020 ug/L <RDL 0.01 0.05 12/14/11 L54765-7 5 Silver, Dissolved, ICP-MS 0.025 ug/L <RDL 0.01 0.05 12/14/11 L54765-8 49.5 Silver, Dissolved, ICP-MS 0.027 ug/L <RDL 0.01 0.05 12/14/11 L54765-9 158 Silver, Dissolved, ICP-MS 0.025 ug/L <RDL 0.01 0.05 12/14/11 L54765-10 159 Silver, Dissolved, ICP-MS 0.026 ug/L <RDL 0.01 0.05 07/30/12 L56062-7 5 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 07/30/12 L56062-8 49.4 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 07/30/12 L56062-10 158 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 07/30/12 L56062-9 158 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 12/12/12 L56990-7 4.9 Silver, Dissolved, ICP-MS 0.011 ug/L <RDL 0.01 0.05 12/12/12 L56990-8 49.5 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 12/12/12 L56990-10 158 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 12/12/12 L56990-9 158 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 07/14/11 L53626-7 5.2 Silver, Total, ICP-MS 0.018 ug/L <RDL 0.01 0.05 07/14/11 L53626-8 49.8 Silver, Total, ICP-MS 0.016 ug/L <RDL 0.01 0.05 07/14/11 L53626-9 158 Silver, Total, ICP-MS 0.019 ug/L <RDL 0.01 0.05 07/14/11 L53626-10 159 Silver, Total, ICP-MS 0.019 ug/L <RDL 0.01 0.05 12/14/11 L54765-7 5 Silver, Total, ICP-MS 0.029 ug/L <RDL 0.01 0.05 12/14/11 L54765-8 49.5 Silver, Total, ICP-MS 0.030 ug/L <RDL 0.01 0.05 12/14/11 L54765-9 158 Silver, Total, ICP-MS 0.029 ug/L <RDL 0.01 0.05 12/14/11 L54765-10 159 Silver, Total, ICP-MS 0.028 ug/L <RDL 0.01 0.05 07/30/12 L56062-7 5 Silver, Total, ICP-MS ug/L <MDL 0.01 0.05 07/30/12 L56062-8 49.4 Silver, Total, ICP-MS ug/L <MDL 0.01 0.05 07/30/12 L56062-10 158 Silver, Total, ICP-MS ug/L <MDL 0.01 0.05 07/30/12 L56062-9 158 Silver, Total, ICP-MS ug/L <MDL 0.01 0.05 12/12/12 L56990-7 4.9 Silver, Total, ICP-MS ug/L <MDL 0.01 0.05 12/12/12 L56990-8 49.5 Silver, Total, ICP-MS ug/L <MDL 0.01 0.05 12/12/12 L56990-10 158 Silver, Total, ICP-MS ug/L <MDL 0.01 0.05 12/12/12 L56990-9 158 Silver, Total, ICP-MS ug/L <MDL 0.01 0.05 07/14/11 L53626-7 5.2 Zinc, Dissolved, ICP-MS 0.556 ug/L 0.1 0.5 07/14/11 L53626-8 49.8 Zinc, Dissolved, ICP-MS 0.707 ug/L 0.1 0.5 07/14/11 L53626-9 158 Zinc, Dissolved, ICP-MS 0.593 ug/L 0.1 0.5 07/14/11 L53626-10 159 Zinc, Dissolved, ICP-MS 0.581 ug/L 0.1 0.5 12/14/11 L54765-7 5 Zinc, Dissolved, ICP-MS 0.617 ug/L 0.1 0.5 12/14/11 L54765-8 49.5 Zinc, Dissolved, ICP-MS 0.39 ug/L <RDL 0.1 0.5 12/14/11 L54765-9 158 Zinc, Dissolved, ICP-MS 0.36 ug/L <RDL 0.1 0.5 12/14/11 L54765-10 159 Zinc, Dissolved, ICP-MS 0.46 ug/L <RDL 0.1 0.5 07/30/12 L56062-7 5 Zinc, Dissolved, ICP-MS 0.571 ug/L 0.1 0.5 07/30/12 L56062-8 49.4 Zinc, Dissolved, ICP-MS 0.29 ug/L <RDL 0.1 0.5 07/30/12 L56062-10 158 Zinc, Dissolved, ICP-MS 0.31 ug/L <RDL 0.1 0.5 07/30/12 L56062-9 158 Zinc, Dissolved, ICP-MS 0.27 ug/L <RDL 0.1 0.5 12/12/12 L56990-7 4.9 Zinc, Dissolved, ICP-MS 0.40 ug/L <RDL 0.1 0.5Page 24 of 24 

## Table A-2
Complete Water Quality Monitoring Data for Station LSNT01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 12/12/12 L56990-8 49.5 Zinc, Dissolved, ICP-MS 0.37 ug/L <RDL 0.1 0.5 12/12/12 L56990-10 158 Zinc, Dissolved, ICP-MS 0.33 ug/L <RDL 0.1 0.5 12/12/12 L56990-9 158 Zinc, Dissolved, ICP-MS 0.35 ug/L <RDL 0.1 0.5 07/14/11 L53626-7 5.2 Zinc, Total, ICP-MS 0.647 ug/L 0.1 0.5 07/14/11 L53626-8 49.8 Zinc, Total, ICP-MS 0.519 ug/L 0.1 0.5 07/14/11 L53626-9 158 Zinc, Total, ICP-MS 0.531 ug/L 0.1 0.5 07/14/11 L53626-10 159 Zinc, Total, ICP-MS 0.544 ug/L 0.1 0.5 12/14/11 L54765-7 5 Zinc, Total, ICP-MS 0.48 ug/L <RDL 0.1 0.5 12/14/11 L54765-8 49.5 Zinc, Total, ICP-MS 0.44 ug/L <RDL 0.1 0.5 12/14/11 L54765-9 158 Zinc, Total, ICP-MS 0.44 ug/L <RDL 0.1 0.5 12/14/11 L54765-10 159 Zinc, Total, ICP-MS 0.512 ug/L 0.1 0.5 07/30/12 L56062-7 5 Zinc, Total, ICP-MS 0.519 ug/L 0.1 0.5 07/30/12 L56062-8 49.4 Zinc, Total, ICP-MS 0.42 ug/L <RDL 0.1 0.5 07/30/12 L56062-10 158 Zinc, Total, ICP-MS 0.42 ug/L <RDL 0.1 0.5 07/30/12 L56062-9 158 Zinc, Total, ICP-MS 0.43 ug/L <RDL 0.1 0.5 12/12/12 L56990-7 4.9 Zinc, Total, ICP-MS 0.49 ug/L <RDL 0.1 0.5 12/12/12 L56990-8 49.5 Zinc, Total, ICP-MS 0.40 ug/L <RDL 0.1 0.5 12/12/12 L56990-10 158 Zinc, Total, ICP-MS 0.46 ug/L <RDL 0.1 0.5 12/12/12 L56990-9 158 Zinc, Total, ICP-MS 0.46 ug/L <RDL 0.1 0.5

Notes Depth (m) - Depth below the water's surface (in meters) from which the sample was collected.
MDL - Method detection limit; the limit of reliable detection

. RDL - Reporting detection limit; the limit of reliable quantitation (PQL). <MDL - Analyte was not detected <RDL - Analyte was detected at a concentration less than the RDL. CFU/100 ml - Colony forming units per 100 milliliters. deg C - Degrees Celcius. mg/L - Milligrams per liter. mg CaCO3/L - Milligrams of calcium carbonate per liter. PSS - Practical Salinity Scale. ug/L - Micrograms per liter.Page 1 of 16 

## Table A-3
Complete Water Quality Monitoring Data for Station LTED04 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 01/18/11 L52381-28 1.2 Fecal Coliform 1 CFU/100ml 1 02/22/11 L52539-28 0.89 Fecal Coliform 1 CFU/100ml 1 03/21/11 L52727-28 1.4 Fecal Coliform 3 CFU/100ml 1 04/19/11 L52883-28 1.2 Fecal Coliform CFU/100ml <MDL 1 05/16/11 L53206-28 1.2 Fecal Coliform 12 CFU/100ml 1 06/20/11 L53331-28 1.1 Fecal Coliform CFU/100ml <MDL 1 07/18/11 L53542-28 1.2 Fecal Coliform CFU/100ml <MDL 1 08/15/11 L53889-28 1.2 Fecal Coliform CFU/100ml <MDL 1 09/19/11 L54019-28 1 Fecal Coliform CFU/100ml <MDL 1 10/17/11 L54269-28 0.97 Fecal Coliform CFU/100ml <MDL 1 11/28/11 L54474-28 0.92 Fecal Coliform 10 CFU/100ml 1 12/19/11 L54766-28 0.83 Fecal Coliform CFU/100ml <MDL 1 01/23/12 L54840-28 1.1 Fecal Coliform 14 CFU/100ml 1 02/21/12 L55087-28 1.2 Fecal Coliform 4 CFU/100ml 1 03/19/12 L55193-28 1.1 Fecal Coliform CFU/100ml <MDL 1 04/16/12 L55370-28 1.1 Fecal Coliform 1 CFU/100ml 1 05/21/12 L55534-28 1.2 Fecal Coliform 6 CFU/100ml 1 06/18/12 L55788-28 1.1 Fecal Coliform CFU/100ml <MDL 1 07/16/12 L55944-28 1.1 Fecal Coliform CFU/100ml <MDL 1 08/20/12 L56238-28 1.1 Fecal Coliform CFU/100ml <MDL 1 09/17/12 L56394-28 1 Fecal Coliform CFU/100ml <MDL 1 10/17/12 L56533-28 1 Fecal Coliform 4 CFU/100ml 11/26/12 L56803-28 0.67 Fecal Coliform 5 CFU/100ml 12/18/12 L57085-28 0.58 Fecal Coliform 29 CFU/100ml 01/18/11 L52381-28 1.2 Sample Temperature, Field 8.5867 deg C 01/18/11 L52381-29 15 Sample Temperature, Field 8.7290 deg C 01/18/11 L52381-30 24.9 Sample Temperature, Field 8.7102 deg C 01/18/11 L52381-31 34.5 Sample Temperature, Field 8.6807 deg C 01/18/11 L52381-32 54.4 Sample Temperature, Field 8.8023 deg C 01/18/11 L52381-33 74.1 Sample Temperature, Field 8.8984 deg C 02/22/11 L52539-28 0.89 Sample Temperature, Field 7.8332 deg C 02/22/11 L52539-29 14.8 Sample Temperature, Field 8.1351 deg C 02/22/11 L52539-30 24.6 Sample Temperature, Field 8.1545 deg C 02/22/11 L52539-31 34.4 Sample Temperature, Field 8.2027 deg C 02/22/11 L52539-32 54.1 Sample Temperature, Field 8.3058 deg C 02/22/11 L52539-33 73.9 Sample Temperature, Field 8.1709 deg C 03/21/11 L52727-28 1.4 Sample Temperature, Field 7.8429 deg C 03/21/11 L52727-29 15.2 Sample Temperature, Field 7.7859 deg C 03/21/11 L52727-30 25.1 Sample Temperature, Field 7.7601 deg C 03/21/11 L52727-31 34.9 Sample Temperature, Field 7.7442 deg C 03/21/11 L52727-32 54.9 Sample Temperature, Field 7.7423 deg C 03/21/11 L52727-33 74.6 Sample Temperature, Field 7.7361 deg C 04/19/11 L52883-28 1.2 Sample Temperature, Field 8.4543 deg C 04/19/11 L52883-29 15.2 Sample Temperature, Field 8.0717 deg C 04/19/11 L52883-30 25.1 Sample Temperature, Field 8.0024 deg C 04/19/11 L52883-31 34.9 Sample Temperature, Field 7.9822 deg C 04/19/11 L52883-32 54.8 Sample Temperature, Field 7.9142 deg C 04/19/11 L52883-33 74.6 Sample Temperature, Field 7.8151 deg C 05/16/11 L53206-28 1.2 Sample Temperature, Field 9.2211 deg C 05/16/11 L53206-29 15 Sample Temperature, Field 9.2175 deg C 05/16/11 L53206-30 24.9 Sample Temperature, Field 8.6544 deg C 05/16/11 L53206-31 34.9 Sample Temperature, Field 8.5945 deg CPage 2 of 16 Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 05/16/11 L53206-32 54.5 Sample Temperature, Field 8.4465 deg C 05/16/11 L53206-33 74.5 Sample Temperature, Field 8.3085 deg C 06/20/11 L53331-28 1.1 Sample Temperature, Field 10.4997 deg C 06/20/11 L53331-29 15 Sample Temperature, Field 10.1089 deg C 06/20/11 L53331-30 24.8 Sample Temperature, Field 9.9469 deg C 06/20/11 L53331-31 34.8 Sample Temperature, Field 9.8942 deg C 06/20/11 L53331-32 54.6 Sample Temperature, Field 9.3849 deg C 06/20/11 L53331-33 74.3 Sample Temperature, Field 9.2592 deg C 07/14/11 L53626-4 4.9 Sample Temperature, Field 11.9016 deg C 07/14/11 L53626-5 49.8 Sample Temperature, Field 10.6829 deg C 07/14/11 L53626-6 74.2 Sample Temperature, Field 10.3586 deg C 07/18/11 L53542-28 1.2 Sample Temperature, Field 11.7113 deg C 07/18/11 L53542-29 15 Sample Temperature, Field 11.0441 deg C 07/18/11 L53542-30 24.9 Sample Temperature, Field 10.9230 deg C 07/18/11 L53542-31 34.8 Sample Temperature, Field 10.7007 deg C 07/18/11 L53542-32 54.5 Sample Temperature, Field 10.2617 deg C 07/18/11 L53542-33 74.5 Sample Temperature, Field 10.0083 deg C 08/15/11 L53889-28 1.2 Sample Temperature, Field 12.9275 deg C 08/15/11 L53889-29 15.1 Sample Temperature, Field 11.9529 deg C 08/15/11 L53889-30 25 Sample Temperature, Field 11.7442 deg C 08/15/11 L53889-31 34.9 Sample Temperature, Field 11.4599 deg C 08/15/11 L53889-32 54.4 Sample Temperature, Field 10.8348 deg C 08/15/11 L53889-33 74.5 Sample Temperature, Field 10.6828 deg C 09/19/11 L54019-28 1 Sample Temperature, Field 12.5660 deg C 09/19/11 L54019-29 15 Sample Temperature, Field 12.1723 deg C 09/19/11 L54019-30 24.9 Sample Temperature, Field 12.1250 deg C 09/19/11 L54019-31 34.8 Sample Temperature, Field 11.9424 deg C 09/19/11 L54019-32 54.5 Sample Temperature, Field 11.3121 deg C 09/19/11 L54019-33 74.3 Sample Temperature, Field 11.2045 deg C 10/17/11 L54269-28 0.97 Sample Temperature, Field 11.8141 deg C 10/17/11 L54269-29 14.9 Sample Temperature, Field 11.7882 deg C 10/17/11 L54269-30 24.8 Sample Temperature, Field 11.7042 deg C 10/17/11 L54269-31 34.7 Sample Temperature, Field 11.6820 deg C 10/17/11 L54269-32 54.5 Sample Temperature, Field 11.6484 deg C 10/17/11 L54269-33 74.2 Sample Temperature, Field 11.2550 deg C 11/28/11 L54474-28 0.92 Sample Temperature, Field 10.1293 deg C 11/28/11 L54474-29 14.8 Sample Temperature, Field 10.1928 deg C 11/28/11 L54474-30 24.8 Sample Temperature, Field 10.2371 deg C 11/28/11 L54474-31 34.5 Sample Temperature, Field 10.2678 deg C 11/28/11 L54474-32 54.4 Sample Temperature, Field 10.2330 deg C 11/28/11 L54474-33 74.2 Sample Temperature, Field 9.9237 deg C 12/14/11 L54765-4 4.8 Sample Temperature, Field 9.5916 deg C 12/14/11 L54765-5 49.1 Sample Temperature, Field 9.7463 deg C 12/14/11 L54765-6 73.9 Sample Temperature, Field 9.8063 deg C 12/19/11 L54766-28 0.83 Sample Temperature, Field 9.4059 deg C 12/19/11 L54766-29 14.7 Sample Temperature, Field 9.4861 deg C 12/19/11 L54766-30 24.3 Sample Temperature, Field 9.4792 deg C 12/19/11 L54766-31 34.5 Sample Temperature, Field 9.4968 deg C 12/19/11 L54766-32 54.3 Sample Temperature, Field 9.5736 deg C 12/19/11 L54766-33 74 Sample Temperature, Field 9.6123 deg C 01/23/12 L54840-28 1.1 Sample Temperature, Field 8.0020 deg C 01/23/12 L54840-29 15 Sample Temperature, Field 8.1946 deg C 01/23/12 L54840-30 24.9 Sample Temperature, Field 8.2059 deg C 01/23/12 L54840-31 34.8 Sample Temperature, Field 8.2976 deg C 01/23/12 L54840-32 54.5 Sample Temperature, Field 8.3578 deg C 01/23/12 L54840-33 74.2 Sample Temperature, Field 8.5061 deg C 02/21/12 L55087-28 1.2 Sample Temperature, Field 7.7857 deg CPage 3 of 16 Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 02/21/12 L55087-29 15.1 Sample Temperature, Field 7.9034 deg C 02/21/12 L55087-30 25 Sample Temperature, Field 7.9004 deg C 02/21/12 L55087-31 34.7 Sample Temperature, Field 7.9067 deg C 02/21/12 L55087-32 54.6 Sample Temperature, Field 7.8740 deg C 02/21/12 L55087-33 74.3 Sample Temperature, Field 7.8303 deg C 03/19/12 L55193-28 1.1 Sample Temperature, Field 7.5551 deg C 03/19/12 L55193-29 15.1 Sample Temperature, Field 7.6229 deg C 03/19/12 L55193-30 25 Sample Temperature, Field 7.6242 deg C 03/19/12 L55193-31 34.7 Sample Temperature, Field 7.6169 deg C 03/19/12 L55193-32 54.3 Sample Temperature, Field 7.6324 deg C 03/19/12 L55193-33 74.2 Sample Temperature, Field 7.6238 deg C 04/16/12 L55370-28 1.1 Sample Temperature, Field 8.7083 deg C 04/16/12 L55370-29 14.8 Sample Temperature, Field 8.0739 deg C 04/16/12 L55370-30 24.7 Sample Temperature, Field 7.9662 deg C 04/16/12 L55370-31 34.8 Sample Temperature, Field 7.9174 deg C 04/16/12 L55370-32 54.5 Sample Temperature, Field 7.8889 deg C 04/16/12 L55370-33 74.4 Sample Temperature, Field 7.7842 deg C 05/21/12 L55534-28 1.2 Sample Temperature, Field 9.8807 deg C 05/21/12 L55534-29 15 Sample Temperature, Field 9.3749 deg C 05/21/12 L55534-30 24.8 Sample Temperature, Field 9.2503 deg C 05/21/12 L55534-31 34.7 Sample Temperature, Field 8.8786 deg C 05/21/12 L55534-32 54.3 Sample Temperature, Field 8.5957 deg C 05/21/12 L55534-33 74.3 Sample Temperature, Field 8.4946 deg C 06/18/12 L55788-28 1.1 Sample Temperature, Field 11.3134 deg C 06/18/12 L55788-29 15 Sample Temperature, Field 10.8666 deg C 06/18/12 L55788-30 25 Sample Temperature, Field 10.3363 deg C 06/18/12 L55788-31 34.8 Sample Temperature, Field 10.1456 deg C 06/18/12 L55788-32 54.6 Sample Temperature, Field 9.4945 deg C 06/18/12 L55788-33 74.4 Sample Temperature, Field 9.3269 deg C 07/16/12 L55944-28 1.1 Sample Temperature, Field 13.1777 deg C 07/16/12 L55944-29 14.9 Sample Temperature, Field 11.5479 deg C 07/16/12 L55944-30 24.8 Sample Temperature, Field 11.3186 deg C 07/16/12 L55944-31 34.8 Sample Temperature, Field 10.9251 deg C 07/16/12 L55944-32 54.7 Sample Temperature, Field 10.2938 deg C 07/16/12 L55944-33 74.4 Sample Temperature, Field 9.9375 deg C 07/30/12 L56062-4 5 Sample Temperature, Field 12.8533 deg C 07/30/12 L56062-5 49.3 Sample Temperature, Field 11.1677 deg C 07/30/12 L56062-6 74.1 Sample Temperature, Field 10.5675 deg C 08/20/12 L56238-28 1.1 Sample Temperature, Field 13.3530 deg C 08/20/12 L56238-29 14.9 Sample Temperature, Field 12.1511 deg C 08/20/12 L56238-30 24.9 Sample Temperature, Field 12.0941 deg C 08/20/12 L56238-31 34.8 Sample Temperature, Field 11.8729 deg C 08/20/12 L56238-32 54.6 Sample Temperature, Field 10.9932 deg C 08/20/12 L56238-33 73.1 Sample Temperature, Field 10.8896 deg C 09/17/12 L56394-28 1 Sample Temperature, Field 13.4036 deg C 09/17/12 L56394-29 14.6 Sample Temperature, Field 12.3247 deg C 09/17/12 L56394-30 24.9 Sample Temperature, Field 12.1145 deg C 09/17/12 L56394-31 34.8 Sample Temperature, Field 12.0321 deg C 09/17/12 L56394-32 54.3 Sample Temperature, Field 11.5711 deg C 09/17/12 L56394-33 74.3 Sample Temperature, Field 11.3472 deg C 10/17/12 L56533-28 1 Sample Temperature, Field 12.0625 deg C 10/17/12 L56533-29 14.7 Sample Temperature, Field 11.8270 deg C 10/17/12 L56533-30 24.5 Sample Temperature, Field 11.7851 deg C 10/17/12 L56533-31 34.9 Sample Temperature, Field 11.7029 deg C 10/17/12 L56533-32 54.5 Sample Temperature, Field 11.5297 deg C 10/17/12 L56533-33 74.5 Sample Temperature, Field 11.2218 deg C 11/26/12 L56803-28 0.67 Sample Temperature, Field 10.4396 deg CPage 4 of 16 Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 11/26/12 L56803-29 14.3 Sample Temperature, Field 10.7089 deg C 11/26/12 L56803-30 24.3 Sample Temperature, Field 10.7256 deg C 11/26/12 L56803-31 34.2 Sample Temperature, Field 10.7869 deg C 11/26/12 L56803-32 54.2 Sample Temperature, Field 10.8262 deg C 11/26/12 L56803-33 73.9 Sample Temperature, Field 10.7409 deg C 12/12/12 L56990-4 4.8 Sample Temperature, Field 9.8333 deg C 12/12/12 L56990-5 49.4 Sample Temperature, Field 10.2720 deg C 12/12/12 L56990-6 74.1 Sample Temperature, Field 10.3654 deg C 12/18/12 L57085-28 0.58 Sample Temperature, Field 9.5942 deg C 12/18/12 L57085-29 14.2 Sample Temperature, Field 9.9351 deg C 12/18/12 L57085-30 24.1 Sample Temperature, Field 9.9457 deg C 12/18/12 L57085-31 34.2 Sample Temperature, Field 9.9579 deg C 12/18/12 L57085-32 53.8 Sample Temperature, Field 10.0196 deg C 12/18/12 L57085-33 73.7 Sample Temperature, Field 10.0442 deg C 01/18/11 L52381-28 1.2 Dissolved Oxygen, Field 8.5 mg/L 0.5 1 01/18/11 L52381-29 15 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 01/18/11 L52381-30 24.9 Dissolved Oxygen, Field 8.2 mg/L 0.5 1 01/18/11 L52381-31 34.5 Dissolved Oxygen, Field 7.9 mg/L 0.5 1 01/18/11 L52381-32 54.4 Dissolved Oxygen, Field 7.5 mg/L 0.5 1 01/18/11 L52381-33 74.1 Dissolved Oxygen, Field 7.2 mg/L 0.5 1 02/22/11 L52539-28 0.89 Dissolved Oxygen, Field 8.7 mg/L 0.5 1 02/22/11 L52539-29 14.8 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 02/22/11 L52539-30 24.6 Dissolved Oxygen, Field 8.2 mg/L 0.5 1 02/22/11 L52539-31 34.4 Dissolved Oxygen, Field 8.1 mg/L 0.5 1 02/22/11 L52539-32 54.1 Dissolved Oxygen, Field 7.8 mg/L 0.5 1 02/22/11 L52539-33 73.9 Dissolved Oxygen, Field 7.6 mg/L 0.5 1 03/21/11 L52727-28 1.4 Dissolved Oxygen, Field 9.2 mg/L 0.5 1 03/21/11 L52727-29 15.2 Dissolved Oxygen, Field 8.6 mg/L 0.5 1 03/21/11 L52727-30 25.1 Dissolved Oxygen, Field 8.5 mg/L 0.5 1 03/21/11 L52727-31 34.9 Dissolved Oxygen, Field 8.5 mg/L 0.5 1 03/21/11 L52727-32 54.9 Dissolved Oxygen, Field 8.4 mg/L 0.5 1 03/21/11 L52727-33 74.6 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 04/19/11 L52883-28 1.2 Dissolved Oxygen, Field 9.3 mg/L 0.5 1 04/19/11 L52883-29 15.2 Dissolved Oxygen, Field 8.8 mg/L 0.5 1 04/19/11 L52883-30 25.1 Dissolved Oxygen, Field 8.6 mg/L 0.5 1 04/19/11 L52883-31 34.9 Dissolved Oxygen, Field 8.6 mg/L 0.5 1 04/19/11 L52883-32 54.8 Dissolved Oxygen, Field 8.4 mg/L 0.5 1 04/19/11 L52883-33 74.6 Dissolved Oxygen, Field 8.1 mg/L 0.5 1 05/16/11 L53206-28 1.2 Dissolved Oxygen, Field 10.5 mg/L 0.5 1 05/16/11 L53206-29 15 Dissolved Oxygen, Field 11.0 mg/L 0.5 1 05/16/11 L53206-30 24.9 Dissolved Oxygen, Field 9.4 mg/L 0.5 1 05/16/11 L53206-31 34.9 Dissolved Oxygen, Field 9.1 mg/L 0.5 1 05/16/11 L53206-32 54.5 Dissolved Oxygen, Field 8.6 mg/L 0.5 1 05/16/11 L53206-33 74.5 Dissolved Oxygen, Field 7.8 mg/L 0.5 1 06/20/11 L53331-28 1.1 Dissolved Oxygen, Field 9.0 mg/L 0.5 1 06/20/11 L53331-29 15 Dissolved Oxygen, Field 8.8 mg/L 0.5 1 06/20/11 L53331-30 24.8 Dissolved Oxygen, Field 8.8 mg/L 0.5 1 06/20/11 L53331-31 34.8 Dissolved Oxygen, Field 8.6 mg/L 0.5 1 06/20/11 L53331-32 54.6 Dissolved Oxygen, Field 7.8 mg/L 0.5 1 06/20/11 L53331-33 74.3 Dissolved Oxygen, Field 5.6 mg/L 0.5 1 07/14/11 L53626-4 4.9 Dissolved Oxygen, Field 10.4 mg/L 0.5 1 07/14/11 L53626-5 49.8 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 07/14/11 L53626-6 74.2 Dissolved Oxygen, Field 7.5 mg/L 0.5 1 07/18/11 L53542-28 1.2 Dissolved Oxygen, Field 8.6 mg/L 0.5 1 07/18/11 L53542-29 15 Dissolved Oxygen, Field 8.2 mg/L 0.5 1 07/18/11 L53542-30 24.9 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 07/18/11 L53542-31 34.8 Dissolved Oxygen, Field 7.8 mg/L 0.5 1Page 5 of 16 Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 07/18/11 L53542-32 54.5 Dissolved Oxygen, Field 6.9 mg/L 0.5 1 07/18/11 L53542-33 74.5 Dissolved Oxygen, Field 6.4 mg/L 0.5 1 08/15/11 L53889-28 1.2 Dissolved Oxygen, Field 7.7 mg/L 0.5 1 08/15/11 L53889-29 15.1 Dissolved Oxygen, Field 6.9 mg/L 0.5 1 08/15/11 L53889-30 25 Dissolved Oxygen, Field 6.8 mg/L 0.5 1 08/15/11 L53889-31 34.9 Dissolved Oxygen, Field 6.3 mg/L 0.5 1 08/15/11 L53889-32 54.4 Dissolved Oxygen, Field 5.6 mg/L 0.5 1 08/15/11 L53889-33 74.5 Dissolved Oxygen, Field 5.4 mg/L 0.5 1 09/19/11 L54019-28 1 Dissolved Oxygen, Field 7.0 mg/L 0.5 1 09/19/11 L54019-29 15 Dissolved Oxygen, Field 6.4 mg/L 0.5 1 09/19/11 L54019-30 24.9 Dissolved Oxygen, Field 6.3 mg/L 0.5 1 09/19/11 L54019-31 34.8 Dissolved Oxygen, Field 6.1 mg/L 0.5 1 09/19/11 L54019-32 54.5 Dissolved Oxygen, Field 5.1 mg/L 0.5 1 09/19/11 L54019-33 74.3 Dissolved Oxygen, Field 4.9 mg/L 0.5 1 10/17/11 L54269-28 0.97 Dissolved Oxygen, Field 6.6 mg/L 0.5 1 10/17/11 L54269-29 14.9 Dissolved Oxygen, Field 6.1 mg/L 0.5 1 10/17/11 L54269-30 24.8 Dissolved Oxygen, Field 6.1 mg/L 0.5 1 10/17/11 L54269-31 34.7 Dissolved Oxygen, Field 6.0 mg/L 0.5 1 10/17/11 L54269-32 54.5 Dissolved Oxygen, Field 5.9 mg/L 0.5 1 10/17/11 L54269-33 74.2 Dissolved Oxygen, Field 5.4 mg/L 0.5 1 11/28/11 L54474-28 0.92 Dissolved Oxygen, Field 7.3 mg/L 0.5 1 11/28/11 L54474-29 14.8 Dissolved Oxygen, Field 7.1 mg/L 0.5 1 11/28/11 L54474-30 24.8 Dissolved Oxygen, Field 7.0 mg/L 0.5 1 11/28/11 L54474-31 34.5 Dissolved Oxygen, Field 6.9 mg/L 0.5 1 11/28/11 L54474-32 54.4 Dissolved Oxygen, Field 6.7 mg/L 0.5 1 11/28/11 L54474-33 74.2 Dissolved Oxygen, Field 6.6 mg/L 0.5 1 12/14/11 L54765-4 4.8 Dissolved Oxygen, Field 7.0 mg/L 0.5 1 12/14/11 L54765-5 49.1 Dissolved Oxygen, Field 6.8 mg/L 0.5 1 12/14/11 L54765-6 73.9 Dissolved Oxygen, Field 6.5 mg/L 0.5 1 12/19/11 L54766-28 0.83 Dissolved Oxygen, Field 7.1 mg/L 0.5 1 12/19/11 L54766-29 14.7 Dissolved Oxygen, Field 6.9 mg/L 0.5 1 12/19/11 L54766-30 24.3 Dissolved Oxygen, Field 7.0 mg/L 0.5 1 12/19/11 L54766-31 34.5 Dissolved Oxygen, Field 6.9 mg/L 0.5 1 12/19/11 L54766-32 54.3 Dissolved Oxygen, Field 6.7 mg/L 0.5 1 12/19/11 L54766-33 74 Dissolved Oxygen, Field 6.6 mg/L 0.5 1 01/23/12 L54840-28 1.1 Dissolved Oxygen, Field 7.9 mg/L 0.5 1 01/23/12 L54840-29 15 Dissolved Oxygen, Field 7.7 mg/L 0.5 1 01/23/12 L54840-30 24.9 Dissolved Oxygen, Field 7.7 mg/L 0.5 1 01/23/12 L54840-31 34.8 Dissolved Oxygen, Field 7.6 mg/L 0.5 1 01/23/12 L54840-32 54.5 Dissolved Oxygen, Field 7.4 mg/L 0.5 1 01/23/12 L54840-33 74.2 Dissolved Oxygen, Field 7.1 mg/L 0.5 1 02/21/12 L55087-28 1.2 Dissolved Oxygen, Field 8.6 mg/L 0.5 1 02/21/12 L55087-29 15.1 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 02/21/12 L55087-30 25 Dissolved Oxygen, Field 7.9 mg/L 0.5 1 02/21/12 L55087-31 34.7 Dissolved Oxygen, Field 7.8 mg/L 0.5 1 02/21/12 L55087-32 54.6 Dissolved Oxygen, Field 7.6 mg/L 0.5 1 02/21/12 L55087-33 74.3 Dissolved Oxygen, Field 7.5 mg/L 0.5 1 03/19/12 L55193-28 1.1 Dissolved Oxygen, Field 8.8 mg/L 0.5 1 03/19/12 L55193-29 15.1 Dissolved Oxygen, Field 8.5 mg/L 0.5 1 03/19/12 L55193-30 25 Dissolved Oxygen, Field 8.4 mg/L 0.5 1 03/19/12 L55193-31 34.7 Dissolved Oxygen, Field 8.4 mg/L 0.5 1 03/19/12 L55193-32 54.3 Dissolved Oxygen, Field 8.2 mg/L 0.5 1 03/19/12 L55193-33 74.2 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 04/16/12 L55370-28 1.1 Dissolved Oxygen, Field 10.9 mg/L 0.5 1 04/16/12 L55370-29 14.8 Dissolved Oxygen, Field 9.4 mg/L 0.5 1 04/16/12 L55370-30 24.7 Dissolved Oxygen, Field 8.9 mg/L 0.5 1 04/16/12 L55370-31 34.8 Dissolved Oxygen, Field 8.8 mg/L 0.5 1Page 6 of 16 Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 04/16/12 L55370-32 54.5 Dissolved Oxygen, Field 8.6 mg/L 0.5 1 04/16/12 L55370-33 74.4 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 05/21/12 L55534-28 1.2 Dissolved Oxygen, Field 10.2 mg/L 0.5 1 05/21/12 L55534-29 15 Dissolved Oxygen, Field 9.5 mg/L 0.5 1 05/21/12 L55534-30 24.8 Dissolved Oxygen, Field 9.3 mg/L 0.5 1 05/21/12 L55534-31 34.7 Dissolved Oxygen, Field 8.7 mg/L 0.5 1 05/21/12 L55534-32 54.3 Dissolved Oxygen, Field 8.0 mg/L 0.5 1 05/21/12 L55534-33 74.3 Dissolved Oxygen, Field 7.8 mg/L 0.5 1 06/18/12 L55788-28 1.1 Dissolved Oxygen, Field 9.2 mg/L 0.5 1 06/18/12 L55788-29 15 Dissolved Oxygen, Field 8.8 mg/L 0.5 1 06/18/12 L55788-30 25 Dissolved Oxygen, Field 8.4 mg/L 0.5 1 06/18/12 L55788-31 34.8 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 06/18/12 L55788-32 54.6 Dissolved Oxygen, Field 7.6 mg/L 0.5 1 06/18/12 L55788-33 74.4 Dissolved Oxygen, Field 7.0 mg/L 0.5 1 07/16/12 L55944-28 1.1 Dissolved Oxygen, Field 10.0 mg/L 0.5 1 07/16/12 L55944-29 14.9 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 07/16/12 L55944-30 24.8 Dissolved Oxygen, Field 8.1 mg/L 0.5 1 07/16/12 L55944-31 34.8 Dissolved Oxygen, Field 7.6 mg/L 0.5 1 07/16/12 L55944-32 54.7 Dissolved Oxygen, Field 6.6 mg/L 0.5 1 07/16/12 L55944-33 74.4 Dissolved Oxygen, Field 5.7 mg/L 0.5 1 07/30/12 L56062-4 5 Dissolved Oxygen, Field 8.3 mg/L 0.5 1 07/30/12 L56062-5 49.3 Dissolved Oxygen, Field 6.8 mg/L 0.5 1 07/30/12 L56062-6 74.1 Dissolved Oxygen, Field 6.0 mg/L 0.5 1 08/20/12 L56238-28 1.1 Dissolved Oxygen, Field 8.8 mg/L 0.5 1 08/20/12 L56238-29 14.9 Dissolved Oxygen, Field 7.0 mg/L 0.5 1 08/20/12 L56238-30 24.9 Dissolved Oxygen, Field 6.9 mg/L 0.5 1 08/20/12 L56238-31 34.8 Dissolved Oxygen, Field 6.6 mg/L 0.5 1 08/20/12 L56238-32 54.6 Dissolved Oxygen, Field 5.3 mg/L 0.5 1 08/20/12 L56238-33 73.1 Dissolved Oxygen, Field 5.2 mg/L 0.5 1 09/17/12 L56394-28 1 Dissolved Oxygen, Field 9.6 mg/L 0.5 1 09/17/12 L56394-29 14.6 Dissolved Oxygen, Field 6.6 mg/L 0.5 1 09/17/12 L56394-30 24.9 Dissolved Oxygen, Field 6.2 mg/L 0.5 1 09/17/12 L56394-31 34.8 Dissolved Oxygen, Field 6.0 mg/L 0.5 1 09/17/12 L56394-32 54.3 Dissolved Oxygen, Field 5.3 mg/L 0.5 1 09/17/12 L56394-33 74.3 Dissolved Oxygen, Field 5.3 mg/L 0.5 1 10/17/12 L56533-28 1 Dissolved Oxygen, Field 6.4 mg/L 0.5 1 10/17/12 L56533-29 14.7 Dissolved Oxygen, Field 5.9 mg/L 0.5 1 10/17/12 L56533-30 24.5 Dissolved Oxygen, Field 5.7 mg/L 0.5 1 10/17/12 L56533-31 34.9 Dissolved Oxygen, Field 5.6 mg/L 0.5 1 10/17/12 L56533-32 54.5 Dissolved Oxygen, Field 5.4 mg/L 0.5 1 10/17/12 L56533-33 74.5 Dissolved Oxygen, Field 5.3 mg/L 0.5 1 11/26/12 L56803-28 0.67 Dissolved Oxygen, Field 7.2 mg/L 0.5 1 11/26/12 L56803-29 14.3 Dissolved Oxygen, Field 6.6 mg/L 0.5 1 11/26/12 L56803-30 24.3 Dissolved Oxygen, Field 6.4 mg/L 0.5 1 11/26/12 L56803-31 34.2 Dissolved Oxygen, Field 6.4 mg/L 0.5 1 11/26/12 L56803-32 54.2 Dissolved Oxygen, Field 6.0 mg/L 0.5 1 11/26/12 L56803-33 73.9 Dissolved Oxygen, Field 5.8 mg/L 0.5 1 12/12/12 L56990-4 4.8 Dissolved Oxygen, Field 7.8 mg/L 0.5 1 12/12/12 L56990-5 49.4 Dissolved Oxygen, Field 6.9 mg/L 0.5 1 12/12/12 L56990-6 74.1 Dissolved Oxygen, Field 5.8 mg/L 0.5 1 08/15/11 L53889-28 1.2 Total Suspended Solids 1.4 mg/L <RDL 0.5 10 08/15/11 L53889-29 15.1 Total Suspended Solids 1.4 mg/L <RDL 0.5 10 08/15/11 L53889-30 25 Total Suspended Solids 1.2 mg/L <RDL 0.5 10 08/15/11 L53889-31 34.9 Total Suspended Solids 3.2 mg/L <RDL 0.5 10 08/15/11 L53889-32 54.4 Total Suspended Solids 1.8 mg/L <RDL 0.5 10 08/15/11 L53889-33 74.5 Total Suspended Solids 3.3 mg/L <RDL 0.5 10 09/19/11 L54019-28 1 Total Suspended Solids 1.5 mg/L <RDL 0.5 10Page 7 of 16 Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 09/19/11 L54019-29 15 Total Suspended Solids 0.6 mg/L <RDL 0.5 10 09/19/11 L54019-30 24.9 Total Suspended Solids 0.9 mg/L <RDL 0.5 10 09/19/11 L54019-31 34.8 Total Suspended Solids 1.1 mg/L <RDL 0.5 10 09/19/11 L54019-32 54.5 Total Suspended Solids 2.0 mg/L <RDL 0.5 10 09/19/11 L54019-33 74.3 Total Suspended Solids 2.5 mg/L <RDL 0.5 10 10/17/11 L54269-28 0.97 Total Suspended Solids 1.0 mg/L <RDL 0.5 10 10/17/11 L54269-29 14.9 Total Suspended Solids mg/L <MDL 1 20 10/17/11 L54269-30 24.8 Total Suspended Solids 1.9 mg/L <RDL 0.5 10 10/17/11 L54269-31 34.7 Total Suspended Solids 0.5 mg/L <RDL 0.5 10 10/17/11 L54269-32 54.5 Total Suspended Solids mg/L <MDL 0.5 10 10/17/11 L54269-33 74.2 Total Suspended Solids 2.2 mg/L <RDL 0.5 10 11/28/11 L54474-28 0.92 Total Suspended Solids 1.2 mg/L <RDL 0.5 10 11/28/11 L54474-29 14.8 Total Suspended Solids 0.8 mg/L <RDL 0.5 10 11/28/11 L54474-30 24.8 Total Suspended Solids 1.0 mg/L <RDL 0.5 10 11/28/11 L54474-31 34.5 Total Suspended Solids 0.9 mg/L <RDL 0.5 10 11/28/11 L54474-32 54.4 Total Suspended Solids 1.8 mg/L <RDL 0.5 10 11/28/11 L54474-33 74.2 Total Suspended Solids 1.9 mg/L <RDL 0.5 10 12/19/11 L54766-28 0.83 Total Suspended Solids 1.0 mg/L <RDL 0.5 10 12/19/11 L54766-29 14.7 Total Suspended Solids 0.8 mg/L <RDL 0.5 10 12/19/11 L54766-30 24.3 Total Suspended Solids 1.0 mg/L <RDL 0.5 10 12/19/11 L54766-31 34.5 Total Suspended Solids 1.3 mg/L <RDL 0.5 10 12/19/11 L54766-32 54.3 Total Suspended Solids 1.6 mg/L <RDL 0.5 10 12/19/11 L54766-33 74 Total Suspended Solids 1.7 mg/L <RDL 0.5 10 01/23/12 L54840-28 1.1 Total Suspended Solids 2.4 mg/L <RDL 0.5 10 01/23/12 L54840-29 15 Total Suspended Solids 1.3 mg/L <RDL 0.5 10 01/23/12 L54840-30 24.9 Total Suspended Solids 0.8 mg/L <RDL 0.5 10 01/23/12 L54840-31 34.8 Total Suspended Solids 4.8 mg/L <RDL 0.5 10 01/23/12 L54840-32 54.5 Total Suspended Solids 2.1 mg/L <RDL 0.5 10 01/23/12 L54840-33 74.2 Total Suspended Solids 3.3 mg/L <RDL 0.5 10 02/21/12 L55087-28 1.2 Total Suspended Solids 0.9 mg/L <RDL 0.5 10 02/21/12 L55087-29 15.1 Total Suspended Solids 2.0 mg/L <RDL 0.5 10 02/21/12 L55087-30 25 Total Suspended Solids 1.3 mg/L <RDL 0.5 10 02/21/12 L55087-31 34.7 Total Suspended Solids 1.5 mg/L <RDL 0.5 10 02/21/12 L55087-32 54.6 Total Suspended Solids 2.9 mg/L <RDL 0.5 10 02/21/12 L55087-33 74.3 Total Suspended Solids 3.4 mg/L <RDL 1 20 03/19/12 L55193-28 1.1 Total Suspended Solids 2.9 mg/L <RDL 0.5 10 03/19/12 L55193-29 15.1 Total Suspended Solids 2.2 mg/L <RDL 0.5 11 03/19/12 L55193-30 25 Total Suspended Solids 1.3 mg/L <RDL 0.5 10 03/19/12 L55193-31 34.7 Total Suspended Solids 2.6 mg/L <RDL 0.5 10 03/19/12 L55193-32 54.3 Total Suspended Solids 2.8 mg/L <RDL 0.5 10 03/19/12 L55193-33 74.2 Total Suspended Solids 1.5 mg/L <RDL 0.5 10 04/16/12 L55370-28 1.1 Total Suspended Solids 3.4 mg/L <RDL 0.5 10 04/16/12 L55370-29 14.8 Total Suspended Solids 4.6 mg/L <RDL 1 20 04/16/12 L55370-30 24.7 Total Suspended Solids 2.4 mg/L <RDL 0.5 10 04/16/12 L55370-31 34.8 Total Suspended Solids 3.3 mg/L <RDL 0.5 10 04/16/12 L55370-32 54.5 Total Suspended Solids 3.9 mg/L <RDL 0.5 10 04/16/12 L55370-33 74.4 Total Suspended Solids 2.8 mg/L <RDL 0.5 10 05/21/12 L55534-28 1.2 Total Suspended Solids 3.6 mg/L <RDL 1 20 05/21/12 L55534-29 15 Total Suspended Solids 3.4 mg/L <RDL 0.5 10 05/21/12 L55534-30 24.8 Total Suspended Solids 1.0 mg/L <RDL 0.5 10 05/21/12 L55534-31 34.7 Total Suspended Solids 2.2 mg/L <RDL 0.5 10 05/21/12 L55534-32 54.3 Total Suspended Solids 3.3 mg/L <RDL 0.5 10 05/21/12 L55534-33 74.3 Total Suspended Solids 3.8 mg/L <RDL 0.5 10 06/18/12 L55788-28 1.1 Total Suspended Solids 2.7 mg/L <RDL 0.5 10 06/18/12 L55788-29 15 Total Suspended Solids 3.1 mg/L <RDL 0.5 10 06/18/12 L55788-30 25 Total Suspended Solids 2.0 mg/L <RDL 0.5 10 06/18/12 L55788-31 34.8 Total Suspended Solids 1.9 mg/L <RDL 0.5 10Page 8 of 16 Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 06/18/12 L55788-32 54.6 Total Suspended Solids 2.9 mg/L <RDL 0.5 10 06/18/12 L55788-33 74.4 Total Suspended Solids 3.2 mg/L <RDL 0.5 10 07/16/12 L55944-28 1.1 Total Suspended Solids 4.5 mg/L <RDL 0.5 10 07/16/12 L55944-29 14.9 Total Suspended Solids 2.5 mg/L <RDL 0.5 10 07/16/12 L55944-30 24.8 Total Suspended Solids 1.9 mg/L <RDL 0.5 10 07/16/12 L55944-31 34.8 Total Suspended Solids 2.3 mg/L <RDL 0.5 10 07/16/12 L55944-32 54.7 Total Suspended Solids 2.1 mg/L <RDL 0.5 10 07/16/12 L55944-33 74.4 Total Suspended Solids 4.7 mg/L <RDL 0.5 10 08/20/12 L56238-28 1.1 Total Suspended Solids 6.9 mg/L <RDL 0.5 10 08/20/12 L56238-29 14.9 Total Suspended Solids 7.9 mg/L <RDL 0.5 10 08/20/12 L56238-30 24.9 Total Suspended Solids 8.1 mg/L <RDL 0.5 10 08/20/12 L56238-31 34.8 Total Suspended Solids 7.9 mg/L <RDL 0.5 10 08/20/12 L56238-32 54.6 Total Suspended Solids 6.0 mg/L <RDL 0.5 10 08/20/12 L56238-33 73.1 Total Suspended Solids 7.1 mg/L <RDL 0.5 10 09/17/12 L56394-28 1 Total Suspended Solids 5.1 mg/L <RDL 0.5 10 09/17/12 L56394-29 14.6 Total Suspended Solids 4.0 mg/L <RDL 1 20 09/17/12 L56394-30 24.9 Total Suspended Solids 2.2 mg/L <RDL 0.5 10 09/17/12 L56394-31 34.8 Total Suspended Solids 2.5 mg/L <RDL 0.5 10 09/17/12 L56394-32 54.3 Total Suspended Solids 3.3 mg/L <RDL 0.5 10 09/17/12 L56394-33 74.3 Total Suspended Solids 5.5 mg/L <RDL 0.5 10 10/17/12 L56533-28 1 Total Suspended Solids 2.7 mg/L <RDL 0.5 10 10/17/12 L56533-29 14.7 Total Suspended Solids 2.3 mg/L <RDL 0.5 10 10/17/12 L56533-30 24.5 Total Suspended Solids 2.6 mg/L <RDL 0.5 10 10/17/12 L56533-31 34.9 Total Suspended Solids 2.1 mg/L <RDL 0.5 10 10/17/12 L56533-32 54.5 Total Suspended Solids 2.4 mg/L <RDL 0.5 10 10/17/12 L56533-33 74.5 Total Suspended Solids 5.6 mg/L <RDL 0.5 10 11/26/12 L56803-28 0.67 Total Suspended Solids 8.0 mg/L <RDL 1 20 11/26/12 L56803-29 14.3 Total Suspended Solids 3.1 mg/L <RDL 0.5 10 11/26/12 L56803-30 24.3 Total Suspended Solids 1.0 mg/L <RDL 0.5 10 11/26/12 L56803-31 34.2 Total Suspended Solids 4.9 mg/L <RDL 0.5 10 11/26/12 L56803-32 54.2 Total Suspended Solids 2.6 mg/L <RDL 0.5 10 11/26/12 L56803-33 73.9 Total Suspended Solids 4.8 mg/L <RDL 0.5 10 01/18/11 L52381-28 1.2 pH, Field 7.7 pH 01/18/11 L52381-29 15 pH, Field 7.7 pH 01/18/11 L52381-30 24.9 pH, Field 7.7 pH 01/18/11 L52381-31 34.5 pH, Field 7.6 pH 01/18/11 L52381-32 54.4 pH, Field 7.6 pH 01/18/11 L52381-33 74.1 pH, Field 7.6 pH 02/22/11 L52539-28 0.89 pH, Field 7.7 pH 02/22/11 L52539-29 14.8 pH, Field 7.6 pH 02/22/11 L52539-30 24.6 pH, Field 7.6 pH 02/22/11 L52539-31 34.4 pH, Field 7.6 pH 02/22/11 L52539-32 54.1 pH, Field 7.6 pH 02/22/11 L52539-33 73.9 pH, Field 7.6 pH 03/21/11 L52727-28 1.4 pH, Field 7.7 pH 03/21/11 L52727-29 15.2 pH, Field 7.7 pH 03/21/11 L52727-30 25.1 pH, Field 7.7 pH 03/21/11 L52727-31 34.9 pH, Field 7.7 pH 03/21/11 L52727-32 54.9 pH, Field 7.7 pH 03/21/11 L52727-33 74.6 pH, Field 7.7 pH 04/19/11 L52883-28 1.2 pH, Field 7.9 pH 04/19/11 L52883-29 15.2 pH, Field 7.8 pH 04/19/11 L52883-30 25.1 pH, Field 7.8 pH 04/19/11 L52883-31 34.9 pH, Field 7.8 pH 04/19/11 L52883-32 54.8 pH, Field 7.8 pH 04/19/11 L52883-33 74.6 pH, Field 7.8 pH 05/16/11 L53206-28 1.2 pH, Field 7.9 pHPage 9 of 16 Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 05/16/11 L53206-29 15 pH, Field 7.9 pH 05/16/11 L53206-30 24.9 pH, Field 7.7 pH 05/16/11 L53206-31 34.9 pH, Field 7.7 pH 05/16/11 L53206-32 54.5 pH, Field 7.7 pH 05/16/11 L53206-33 74.5 pH, Field 7.6 pH 06/20/11 L53331-28 1.1 pH, Field 7.8 pH 06/20/11 L53331-29 15 pH, Field 7.8 pH 06/20/11 L53331-30 24.8 pH, Field 7.8 pH 06/20/11 L53331-31 34.8 pH, Field 7.8 pH 06/20/11 L53331-32 54.6 pH, Field 7.7 pH 06/20/11 L53331-33 74.3 pH, Field 7.7 pH 07/14/11 L53626-4 4.9 pH, Field 8.0 pH 07/14/11 L53626-5 49.8 pH, Field 7.8 pH 07/14/11 L53626-6 74.2 pH, Field 7.8 pH 07/18/11 L53542-28 1.2 pH, Field 7.9 pH 07/18/11 L53542-29 15 pH, Field 7.8 pH 07/18/11 L53542-30 24.9 pH, Field 7.8 pH 07/18/11 L53542-31 34.8 pH, Field 7.8 pH 07/18/11 L53542-32 54.5 pH, Field 7.7 pH 07/18/11 L53542-33 74.5 pH, Field 7.6 pH 08/15/11 L53889-28 1.2 pH, Field 7.8 pH 08/15/11 L53889-29 15.1 pH, Field 7.7 pH 08/15/11 L53889-30 25 pH, Field 7.7 pH 08/15/11 L53889-31 34.9 pH, Field 7.6 pH 08/15/11 L53889-32 54.4 pH, Field 7.6 pH 08/15/11 L53889-33 74.5 pH, Field 7.6 pH 09/19/11 L54019-28 1 pH, Field 7.6 pH 09/19/11 L54019-29 15 pH, Field 7.6 pH 09/19/11 L54019-30 24.9 pH, Field 7.6 pH 09/19/11 L54019-31 34.8 pH, Field 7.6 pH 09/19/11 L54019-32 54.5 pH, Field 7.5 pH 09/19/11 L54019-33 74.3 pH, Field 7.5 pH 10/17/11 L54269-28 0.97 pH, Field 7.6 pH 10/17/11 L54269-29 14.9 pH, Field 7.6 pH 10/17/11 L54269-30 24.8 pH, Field 7.6 pH 10/17/11 L54269-31 34.7 pH, Field 7.6 pH 10/17/11 L54269-32 54.5 pH, Field 7.6 pH 10/17/11 L54269-33 74.2 pH, Field 7.5 pH 11/28/11 L54474-28 0.92 pH, Field 7.5 pH 11/28/11 L54474-29 14.8 pH, Field 7.5 pH 11/28/11 L54474-30 24.8 pH, Field 7.4 pH 11/28/11 L54474-31 34.5 pH, Field 7.4 pH 11/28/11 L54474-32 54.4 pH, Field 7.4 pH 11/28/11 L54474-33 74.2 pH, Field 7.4 pH 12/14/11 L54765-4 4.8 pH, Field 7.4 pH 12/14/11 L54765-5 49.1 pH, Field 7.4 pH 12/14/11 L54765-6 73.9 pH, Field 7.4 pH 12/19/11 L54766-28 0.83 pH, Field 7.5 pH 12/19/11 L54766-29 14.7 pH, Field 7.5 pH 12/19/11 L54766-30 24.3 pH, Field 7.5 pH 12/19/11 L54766-31 34.5 pH, Field 7.4 pH 12/19/11 L54766-32 54.3 pH, Field 7.4 pH 12/19/11 L54766-33 74 pH, Field 7.4 pH 07/30/12 L56062-4 5 pH, Field 7.8 pH 07/30/12 L56062-5 49.3 pH, Field 7.7 pH 07/30/12 L56062-6 74.1 pH, Field 7.6 pH 12/12/12 L56990-4 4.8 pH, Field 7.6 pHPage 10 of 16 Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 12/12/12 L56990-5 49.4 pH, Field 7.5 pH 12/12/12 L56990-6 74.1 pH, Field 7.5 pH 01/18/11 L52381-28 1.2 Salinity, Field 27.272 PSS 01/18/11 L52381-29 15 Salinity, Field 28.966 PSS 01/18/11 L52381-30 24.9 Salinity, Field 29.057 PSS 01/18/11 L52381-31 34.5 Salinity, Field 29.247 PSS 01/18/11 L52381-32 54.4 Salinity, Field 29.496 PSS 01/18/11 L52381-33 74.1 Salinity, Field 29.760 PSS 02/22/11 L52539-28 0.89 Salinity, Field 26.528 PSS 02/22/11 L52539-29 14.8 Salinity, Field 28.723 PSS 02/22/11 L52539-30 24.6 Salinity, Field 28.860 PSS 02/22/11 L52539-31 34.4 Salinity, Field 28.929 PSS 02/22/11 L52539-32 54.1 Salinity, Field 29.056 PSS 02/22/11 L52539-33 73.9 Salinity, Field 29.435 PSS 03/21/11 L52727-28 1.4 Salinity, Field 23.982 PSS 03/21/11 L52727-29 15.2 Salinity, Field 28.937 PSS 03/21/11 L52727-30 25.1 Salinity, Field 29.006 PSS 03/21/11 L52727-31 34.9 Salinity, Field 29.020 PSS 03/21/11 L52727-32 54.9 Salinity, Field 29.086 PSS 03/21/11 L52727-33 74.6 Salinity, Field 29.144 PSS 04/19/11 L52883-28 1.2 Salinity, Field 26.637 PSS 04/19/11 L52883-29 15.2 Salinity, Field 28.424 PSS 04/19/11 L52883-30 25.1 Salinity, Field 28.556 PSS 04/19/11 L52883-31 34.9 Salinity, Field 28.632 PSS 04/19/11 L52883-32 54.8 Salinity, Field 28.732 PSS 04/19/11 L52883-33 74.6 Salinity, Field 29.056 PSS 05/16/11 L53206-28 1.2 Salinity, Field 24.611 PSS 05/16/11 L53206-29 15 Salinity, Field 28.312 PSS 05/16/11 L53206-30 24.9 Salinity, Field 28.498 PSS 05/16/11 L53206-31 34.9 Salinity, Field 28.600 PSS 05/16/11 L53206-32 54.5 Salinity, Field 28.785 PSS 05/16/11 L53206-33 74.5 Salinity, Field 29.147 PSS 06/20/11 L53331-28 1.1 Salinity, Field 28.406 PSS 06/20/11 L53331-29 15 Salinity, Field 28.799 PSS 06/20/11 L53331-30 24.8 Salinity, Field 28.824 PSS 06/20/11 L53331-31 34.8 Salinity, Field 28.878 PSS 06/20/11 L53331-32 54.6 Salinity, Field 29.228 PSS 06/20/11 L53331-33 74.3 Salinity, Field 29.382 PSS 07/14/11 L53626-4 4.9 Salinity, Field 28.328 PSS 07/14/11 L53626-5 49.8 Salinity, Field 28.941 PSS 07/14/11 L53626-6 74.2 Salinity, Field 29.183 PSS 07/18/11 L53542-28 1.2 Salinity, Field 28.313 PSS 07/18/11 L53542-29 15 Salinity, Field 29.023 PSS 07/18/11 L53542-30 24.9 Salinity, Field 29.051 PSS 07/18/11 L53542-31 34.8 Salinity, Field 29.109 PSS 07/18/11 L53542-32 54.5 Salinity, Field 29.375 PSS 07/18/11 L53542-33 74.5 Salinity, Field 29.610 PSS 08/15/11 L53889-28 1.2 Salinity, Field 28.429 PSS 08/15/11 L53889-29 15.1 Salinity, Field 29.273 PSS 08/15/11 L53889-30 25 Salinity, Field 29.279 PSS 08/15/11 L53889-31 34.9 Salinity, Field 29.340 PSS 08/15/11 L53889-32 54.4 Salinity, Field 29.631 PSS 08/15/11 L53889-33 74.5 Salinity, Field 29.740 PSS 09/19/11 L54019-28 1 Salinity, Field 29.398 PSS 09/19/11 L54019-29 15 Salinity, Field 29.735 PSS 09/19/11 L54019-30 24.9 Salinity, Field 29.779 PSS 09/19/11 L54019-31 34.8 Salinity, Field 29.831 PSSPage 11 of 16 Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 09/19/11 L54019-32 54.5 Salinity, Field 30.059 PSS 09/19/11 L54019-33 74.3 Salinity, Field 30.138 PSS 10/17/11 L54269-28 0.97 Salinity, Field 28.701 PSS 10/17/11 L54269-29 14.9 Salinity, Field 30.029 PSS 10/17/11 L54269-30 24.8 Salinity, Field 30.096 PSS 10/17/11 L54269-31 34.7 Salinity, Field 30.114 PSS 10/17/11 L54269-32 54.5 Salinity, Field 30.143 PSS 10/17/11 L54269-33 74.2 Salinity, Field 30.365 PSS 11/28/11 L54474-28 0.92 Salinity, Field 29.679 PSS 11/28/11 L54474-29 14.8 Salinity, Field 29.953 PSS 11/28/11 L54474-30 24.8 Salinity, Field 29.994 PSS 11/28/11 L54474-31 34.5 Salinity, Field 30.020 PSS 11/28/11 L54474-32 54.4 Salinity, Field 30.082 PSS 11/28/11 L54474-33 74.2 Salinity, Field 30.257 PSS 12/14/11 L54765-4 4.8 Salinity, Field 29.594 PSS 12/14/11 L54765-5 49.1 Salinity, Field 29.804 PSS 12/14/11 L54765-6 73.9 Salinity, Field 30.046 PSS 12/19/11 L54766-28 0.83 Salinity, Field 29.372 PSS 12/19/11 L54766-29 14.7 Salinity, Field 29.742 PSS 12/19/11 L54766-30 24.3 Salinity, Field 29.767 PSS 12/19/11 L54766-31 34.5 Salinity, Field 29.799 PSS 12/19/11 L54766-32 54.3 Salinity, Field 29.849 PSS 12/19/11 L54766-33 74 Salinity, Field 29.937 PSS 01/23/12 L54840-28 1.1 Salinity, Field 28.917 PSS 01/23/12 L54840-29 15 Salinity, Field 29.574 PSS 01/23/12 L54840-30 24.9 Salinity, Field 29.588 PSS 01/23/12 L54840-31 34.8 Salinity, Field 29.637 PSS 01/23/12 L54840-32 54.5 Salinity, Field 29.692 PSS 01/23/12 L54840-33 74.2 Salinity, Field 29.939 PSS 02/21/12 L55087-28 1.2 Salinity, Field 26.640 PSS 02/21/12 L55087-29 15.1 Salinity, Field 29.311 PSS 02/21/12 L55087-30 25 Salinity, Field 29.353 PSS 02/21/12 L55087-31 34.7 Salinity, Field 29.385 PSS 02/21/12 L55087-32 54.6 Salinity, Field 29.620 PSS 02/21/12 L55087-33 74.3 Salinity, Field 29.742 PSS 03/19/12 L55193-28 1.1 Salinity, Field 27.601 PSS 03/19/12 L55193-29 15.1 Salinity, Field 29.233 PSS 03/19/12 L55193-30 25 Salinity, Field 29.285 PSS 03/19/12 L55193-31 34.7 Salinity, Field 29.309 PSS 03/19/12 L55193-32 54.3 Salinity, Field 29.392 PSS 03/19/12 L55193-33 74.2 Salinity, Field 29.517 PSS 04/16/12 L55370-28 1.1 Salinity, Field 27.318 PSS 04/16/12 L55370-29 14.8 Salinity, Field 28.886 PSS 04/16/12 L55370-30 24.7 Salinity, Field 28.931 PSS 04/16/12 L55370-31 34.8 Salinity, Field 28.978 PSS 04/16/12 L55370-32 54.5 Salinity, Field 29.039 PSS 04/16/12 L55370-33 74.4 Salinity, Field 29.126 PSS 05/21/12 L55534-28 1.2 Salinity, Field 27.113 PSS 05/21/12 L55534-29 15 Salinity, Field 28.436 PSS 05/21/12 L55534-30 24.8 Salinity, Field 28.508 PSS 05/21/12 L55534-31 34.7 Salinity, Field 28.644 PSS 05/21/12 L55534-32 54.3 Salinity, Field 28.968 PSS 05/21/12 L55534-33 74.3 Salinity, Field 29.188 PSS 06/18/12 L55788-28 1.1 Salinity, Field 27.564 PSS 06/18/12 L55788-29 15 Salinity, Field 28.222 PSS 06/18/12 L55788-30 25 Salinity, Field 28.573 PSS 06/18/12 L55788-31 34.8 Salinity, Field 28.699 PSSPage 12 of 16 Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 06/18/12 L55788-32 54.6 Salinity, Field 29.072 PSS 06/18/12 L55788-33 74.4 Salinity, Field 29.426 PSS 07/16/12 L55944-28 1.1 Salinity, Field 27.508 PSS 07/16/12 L55944-29 14.9 Salinity, Field 28.711 PSS 07/16/12 L55944-30 24.8 Salinity, Field 28.831 PSS 07/16/12 L55944-31 34.8 Salinity, Field 28.966 PSS 07/16/12 L55944-32 54.7 Salinity, Field 29.246 PSS 07/16/12 L55944-33 74.4 Salinity, Field 29.537 PSS 07/30/12 L56062-4 5 Salinity, Field 28.454 PSS 07/30/12 L56062-5 49.3 Salinity, Field 29.155 PSS 07/30/12 L56062-6 74.1 Salinity, Field 29.426 PSS 08/20/12 L56238-28 1.1 Salinity, Field 28.460 PSS 08/20/12 L56238-29 14.9 Salinity, Field 29.194 PSS 08/20/12 L56238-30 24.9 Salinity, Field 29.244 PSS 08/20/12 L56238-31 34.8 Salinity, Field 29.297 PSS 08/20/12 L56238-32 54.6 Salinity, Field 29.592 PSS 08/20/12 L56238-33 73.1 Salinity, Field 29.686 PSS 09/17/12 L56394-28 1 Salinity, Field 28.468 PSS 09/17/12 L56394-29 14.6 Salinity, Field 29.690 PSS 09/17/12 L56394-30 24.9 Salinity, Field 29.697 PSS 09/17/12 L56394-31 34.8 Salinity, Field 29.736 PSS 09/17/12 L56394-32 54.3 Salinity, Field 29.918 PSS 09/17/12 L56394-33 74.3 Salinity, Field 30.143 PSS 10/17/12 L56533-28 1 Salinity, Field 29.376 PSS 10/17/12 L56533-29 14.7 Salinity, Field 30.099 PSS 10/17/12 L56533-30 24.5 Salinity, Field 30.123 PSS 10/17/12 L56533-31 34.9 Salinity, Field 30.164 PSS 10/17/12 L56533-32 54.5 Salinity, Field 30.256 PSS 10/17/12 L56533-33 74.5 Salinity, Field 30.443 PSS 11/26/12 L56803-28 0.67 Salinity, Field 28.579 PSS 11/26/12 L56803-29 14.3 Salinity, Field 29.914 PSS 11/26/12 L56803-30 24.3 Salinity, Field 29.946 PSS 11/26/12 L56803-31 34.2 Salinity, Field 29.985 PSS 11/26/12 L56803-32 54.2 Salinity, Field 30.056 PSS 11/26/12 L56803-33 73.9 Salinity, Field 30.159 PSS 12/12/12 L56990-4 4.8 Salinity, Field 28.747 PSS 12/12/12 L56990-5 49.4 Salinity, Field 29.581 PSS 12/12/12 L56990-6 74.1 Salinity, Field 29.800 PSS 12/18/12 L57085-28 0.58 Salinity, Field 28.367 PSS 12/18/12 L57085-29 14.2 Salinity, Field 29.436 PSS 12/18/12 L57085-30 24.1 Salinity, Field 29.448 PSS 12/18/12 L57085-31 34.2 Salinity, Field 29.462 PSS 12/18/12 L57085-32 53.8 Salinity, Field 29.500 PSS 12/18/12 L57085-33 73.7 Salinity, Field 29.544 PSS 07/14/11 L53626-4 4.9 Arsenic, Dissolved, ICP-MS 1.12 ug/L 0.01 0.05 07/14/11 L53626-5 49.8 Arsenic, Dissolved, ICP-MS 1.23 ug/L 0.01 0.05 07/14/11 L53626-6 74.2 Arsenic, Dissolved, ICP-MS 1.26 ug/L 0.01 0.05 12/14/11 L54765-4 4.8 Arsenic, Dissolved, ICP-MS 1.37 ug/L 0.01 0.05 12/14/11 L54765-5 49.1 Arsenic, Dissolved, ICP-MS 1.35 ug/L 0.01 0.05 12/14/11 L54765-6 73.9 Arsenic, Dissolved, ICP-MS 1.36 ug/L 0.01 0.05 07/30/12 L56062-4 5 Arsenic, Dissolved, ICP-MS 1.22 ug/L 0.01 0.05 07/30/12 L56062-5 49.3 Arsenic, Dissolved, ICP-MS 1.33 ug/L 0.01 0.05 07/30/12 L56062-6 74.1 Arsenic, Dissolved, ICP-MS 1.37 ug/L 0.01 0.05 12/12/12 L56990-4 4.8 Arsenic, Dissolved, ICP-MS 1.34 ug/L 0.01 0.05 12/12/12 L56990-5 49.4 Arsenic, Dissolved, ICP-MS 1.39 ug/L 0.01 0.05 12/12/12 L56990-6 74.1 Arsenic, Dissolved, ICP-MS 1.39 ug/L 0.01 0.05 07/14/11 L53626-4 4.9 Arsenic, Total, ICP-MS 1.14 ug/L 0.01 0.05Page 13 of 16 Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 07/14/11 L53626-5 49.8 Arsenic, Total, ICP-MS 1.19 ug/L 0.01 0.05 07/14/11 L53626-6 74.2 Arsenic, Total, ICP-MS 1.22 ug/L 0.01 0.05 12/14/11 L54765-4 4.8 Arsenic, Total, ICP-MS 1.33 ug/L 0.01 0.05 12/14/11 L54765-5 49.1 Arsenic, Total, ICP-MS 1.34 ug/L 0.01 0.05 12/14/11 L54765-6 73.9 Arsenic, Total, ICP-MS 1.41 ug/L 0.01 0.05 07/30/12 L56062-4 5 Arsenic, Total, ICP-MS 1.20 ug/L 0.01 0.05 07/30/12 L56062-5 49.3 Arsenic, Total, ICP-MS 1.32 ug/L 0.01 0.05 07/30/12 L56062-6 74.1 Arsenic, Total, ICP-MS 1.38 ug/L 0.01 0.05 12/12/12 L56990-4 4.8 Arsenic, Total, ICP-MS 1.31 ug/L 0.01 0.05 12/12/12 L56990-5 49.4 Arsenic, Total, ICP-MS 1.37 ug/L 0.01 0.05 12/12/12 L56990-6 74.1 Arsenic, Total, ICP-MS 1.45 ug/L 0.01 0.05 07/14/11 L53626-4 4.9 Cadmium, Dissolved, ICP-MS 0.0624 ug/L 0.005 0.025 07/14/11 L53626-5 49.8 Cadmium, Dissolved, ICP-MS 0.0627 ug/L 0.005 0.025 07/14/11 L53626-6 74.2 Cadmium, Dissolved, ICP-MS 0.0679 ug/L 0.005 0.025 12/14/11 L54765-4 4.8 Cadmium, Dissolved, ICP-MS 0.0714 ug/L 0.005 0.025 12/14/11 L54765-5 49.1 Cadmium, Dissolved, ICP-MS 0.0722 ug/L 0.005 0.025 12/14/11 L54765-6 73.9 Cadmium, Dissolved, ICP-MS 0.0763 ug/L 0.005 0.025 07/30/12 L56062-4 5 Cadmium, Dissolved, ICP-MS 0.0610 ug/L 0.005 0.025 07/30/12 L56062-5 49.3 Cadmium, Dissolved, ICP-MS 0.0647 ug/L 0.005 0.025 07/30/12 L56062-6 74.1 Cadmium, Dissolved, ICP-MS 0.0689 ug/L 0.005 0.025 12/12/12 L56990-4 4.8 Cadmium, Dissolved, ICP-MS 0.0673 ug/L 0.005 0.025 12/12/12 L56990-5 49.4 Cadmium, Dissolved, ICP-MS 0.0716 ug/L 0.005 0.025 12/12/12 L56990-6 74.1 Cadmium, Dissolved, ICP-MS 0.0718 ug/L 0.005 0.025 07/14/11 L53626-4 4.9 Cadmium, Total, ICP-MS 0.0552 ug/L 0.005 0.025 07/14/11 L53626-5 49.8 Cadmium, Total, ICP-MS 0.0649 ug/L 0.005 0.025 07/14/11 L53626-6 74.2 Cadmium, Total, ICP-MS 0.0662 ug/L 0.005 0.025 12/14/11 L54765-4 4.8 Cadmium, Total, ICP-MS 0.0703 ug/L 0.005 0.025 12/14/11 L54765-5 49.1 Cadmium, Total, ICP-MS 0.0703 ug/L 0.005 0.025 12/14/11 L54765-6 73.9 Cadmium, Total, ICP-MS 0.0727 ug/L 0.005 0.025 07/30/12 L56062-4 5 Cadmium, Total, ICP-MS 0.0745 ug/L 0.005 0.025 07/30/12 L56062-5 49.3 Cadmium, Total, ICP-MS 0.0745 ug/L 0.005 0.025 07/30/12 L56062-6 74.1 Cadmium, Total, ICP-MS 0.0771 ug/L 0.005 0.025 12/12/12 L56990-4 4.8 Cadmium, Total, ICP-MS 0.0743 ug/L 0.005 0.025 12/12/12 L56990-5 49.4 Cadmium, Total, ICP-MS 0.0795 ug/L 0.005 0.025 12/12/12 L56990-6 74.1 Cadmium, Total, ICP-MS 0.0799 ug/L 0.005 0.025 07/14/11 L53626-4 4.9 Chromium, Dissolved, ICP-MS 0.099 ug/L <RDL 0.05 0.25 07/14/11 L53626-5 49.8 Chromium, Dissolved, ICP-MS 0.10 ug/L <RDL 0.05 0.25 07/14/11 L53626-6 74.2 Chromium, Dissolved, ICP-MS 0.11 ug/L <RDL 0.05 0.25 12/14/11 L54765-4 4.8 Chromium, Dissolved, ICP-MS 0.12 ug/L <RDL 0.05 0.25 12/14/11 L54765-5 49.1 Chromium, Dissolved, ICP-MS 0.10 ug/L <RDL 0.05 0.25 12/14/11 L54765-6 73.9 Chromium, Dissolved, ICP-MS 0.085 ug/L <RDL 0.05 0.25 07/30/12 L56062-4 5 Chromium, Dissolved, ICP-MS 0.14 ug/L <RDL 0.05 0.25 07/30/12 L56062-5 49.3 Chromium, Dissolved, ICP-MS 0.13 ug/L <RDL 0.05 0.25 07/30/12 L56062-6 74.1 Chromium, Dissolved, ICP-MS 0.14 ug/L <RDL 0.05 0.25 12/12/12 L56990-4 4.8 Chromium, Dissolved, ICP-MS 0.097 ug/L <RDL 0.05 0.25 12/12/12 L56990-5 49.4 Chromium, Dissolved, ICP-MS 0.087 ug/L <RDL 0.05 0.25 12/12/12 L56990-6 74.1 Chromium, Dissolved, ICP-MS 0.099 ug/L <RDL 0.05 0.25 07/14/11 L53626-4 4.9 Chromium, Total, ICP-MS 0.088 ug/L <RDL 0.05 0.25 07/14/11 L53626-5 49.8 Chromium, Total, ICP-MS 0.091 ug/L <RDL 0.05 0.25 07/14/11 L53626-6 74.2 Chromium, Total, ICP-MS 0.18 ug/L <RDL 0.05 0.25 12/14/11 L54765-4 4.8 Chromium, Total, ICP-MS 0.11 ug/L <RDL 0.05 0.25 12/14/11 L54765-5 49.1 Chromium, Total, ICP-MS 0.12 ug/L <RDL 0.05 0.25 12/14/11 L54765-6 73.9 Chromium, Total, ICP-MS 0.17 ug/L <RDL 0.05 0.25 07/30/12 L56062-4 5 Chromium, Total, ICP-MS 0.11 ug/L <RDL 0.05 0.25 07/30/12 L56062-5 49.3 Chromium, Total, ICP-MS 0.10 ug/L <RDL 0.05 0.25 07/30/12 L56062-6 74.1 Chromium, Total, ICP-MS 0.14 ug/L <RDL 0.05 0.25 12/12/12 L56990-4 4.8 Chromium, Total, ICP-MS 0.097 ug/L <RDL 0.05 0.25Page 14 of 16 Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 12/12/12 L56990-5 49.4 Chromium, Total, ICP-MS 0.077 ug/L <RDL 0.05 0.25 12/12/12 L56990-6 74.1 Chromium, Total, ICP-MS 0.088 ug/L <RDL 0.05 0.25 07/14/11 L53626-4 4.9 Copper, Dissolved, ICP-MS 0.635 ug/L 0.025 0.125 07/14/11 L53626-5 49.8 Copper, Dissolved, ICP-MS 0.303 ug/L 0.025 0.125 07/14/11 L53626-6 74.2 Copper, Dissolved, ICP-MS 0.315 ug/L 0.025 0.125 12/14/11 L54765-4 4.8 Copper, Dissolved, ICP-MS 0.489 ug/L 0.025 0.125 12/14/11 L54765-5 49.1 Copper, Dissolved, ICP-MS 0.316 ug/L 0.025 0.125 12/14/11 L54765-6 73.9 Copper, Dissolved, ICP-MS 0.303 ug/L 0.025 0.125 07/30/12 L56062-4 5 Copper, Dissolved, ICP-MS 0.471 ug/L 0.025 0.125 07/30/12 L56062-5 49.3 Copper, Dissolved, ICP-MS 0.313 ug/L 0.025 0.125 07/30/12 L56062-6 74.1 Copper, Dissolved, ICP-MS 0.340 ug/L 0.025 0.125 12/12/12 L56990-4 4.8 Copper, Dissolved, ICP-MS 0.423 ug/L 0.025 0.125 12/12/12 L56990-5 49.4 Copper, Dissolved, ICP-MS 0.298 ug/L 0.025 0.125 12/12/12 L56990-6 74.1 Copper, Dissolved, ICP-MS 0.277 ug/L 0.025 0.125 07/14/11 L53626-4 4.9 Copper, Total, ICP-MS 0.516 ug/L 0.025 0.125 07/14/11 L53626-5 49.8 Copper, Total, ICP-MS 0.707 ug/L 0.025 0.125 07/14/11 L53626-6 74.2 Copper, Total, ICP-MS 0.301 ug/L 0.025 0.125 12/14/11 L54765-4 4.8 Copper, Total, ICP-MS 0.815 ug/L 0.025 0.125 12/14/11 L54765-5 49.1 Copper, Total, ICP-MS 0.473 ug/L 0.025 0.125 12/14/11 L54765-6 73.9 Copper, Total, ICP-MS 0.492 ug/L 0.025 0.125 07/30/12 L56062-4 5 Copper, Total, ICP-MS 0.602 ug/L 0.025 0.125 07/30/12 L56062-5 49.3 Copper, Total, ICP-MS 0.335 ug/L 0.025 0.125 07/30/12 L56062-6 74.1 Copper, Total, ICP-MS 0.395 ug/L 0.025 0.125 12/12/12 L56990-4 4.8 Copper, Total, ICP-MS 0.507 ug/L 0.025 0.125 12/12/12 L56990-5 49.4 Copper, Total, ICP-MS 0.303 ug/L 0.025 0.125 12/12/12 L56990-6 74.1 Copper, Total, ICP-MS 0.371 ug/L 0.025 0.125 07/14/11 L53626-4 4.9 Lead, Dissolved, ICP-MS 0.0276 ug/L 0.005 0.025 07/14/11 L53626-5 49.8 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 07/14/11 L53626-6 74.2 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 12/14/11 L54765-4 4.8 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 12/14/11 L54765-5 49.1 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 12/14/11 L54765-6 73.9 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 07/30/12 L56062-4 5 Lead, Dissolved, ICP-MS 0.0052 ug/L <RDL 0.005 0.025 07/30/12 L56062-5 49.3 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 07/30/12 L56062-6 74.1 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 12/12/12 L56990-4 4.8 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 12/12/12 L56990-5 49.4 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 12/12/12 L56990-6 74.1 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 07/14/11 L53626-4 4.9 Lead, Total, ICP-MS ug/L <MDL 0.005 0.025 07/14/11 L53626-5 49.8 Lead, Total, ICP-MS 0.0449 ug/L 0.005 0.025 07/14/11 L53626-6 74.2 Lead, Total, ICP-MS 0.020 ug/L <RDL 0.005 0.025 12/14/11 L54765-4 4.8 Lead, Total, ICP-MS 0.0267 ug/L 0.005 0.025 12/14/11 L54765-5 49.1 Lead, Total, ICP-MS 0.023 ug/L <RDL 0.005 0.025 12/14/11 L54765-6 73.9 Lead, Total, ICP-MS 0.0842 ug/L 0.005 0.025 07/30/12 L56062-4 5 Lead, Total, ICP-MS 0.023 ug/L <RDL 0.005 0.025 07/30/12 L56062-5 49.3 Lead, Total, ICP-MS 0.010 ug/L <RDL 0.005 0.025 07/30/12 L56062-6 74.1 Lead, Total, ICP-MS 0.0643 ug/L 0.005 0.025 12/12/12 L56990-4 4.8 Lead, Total, ICP-MS 0.0329 ug/L 0.005 0.025 12/12/12 L56990-5 49.4 Lead, Total, ICP-MS 0.016 ug/L <RDL 0.005 0.025 12/12/12 L56990-6 74.1 Lead, Total, ICP-MS 0.0658 ug/L 0.005 0.025 07/14/11 L53626-4 4.9 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 07/14/11 L53626-5 49.8 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 07/14/11 L53626-6 74.2 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 12/14/11 L54765-4 4.8 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 12/14/11 L54765-5 49.1 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 12/14/11 L54765-6 73.9 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 07/30/12 L56062-4 5 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005Page 15 of 16 Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 07/30/12 L56062-5 49.3 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 07/30/12 L56062-6 74.1 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 12/12/12 L56990-4 4.8 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 12/12/12 L56990-5 49.4 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 12/12/12 L56990-6 74.1 Mercury, Dissolved, CVAF ug/L <MDL 0.0002 0.0005 07/14/11 L53626-4 4.9 Mercury, Total, CVAF 0.00026 ug/L <RDL 0.0002 0.0005 07/14/11 L53626-5 49.8 Mercury, Total, CVAF 0.00021 ug/L <RDL 0.0002 0.0005 07/14/11 L53626-6 74.2 Mercury, Total, CVAF 0.00039 ug/L <RDL 0.0002 0.0005 12/14/11 L54765-4 4.8 Mercury, Total, CVAF 0.00021 ug/L <RDL 0.0002 0.0005 12/14/11 L54765-5 49.1 Mercury, Total, CVAF 0.00021 ug/L <RDL 0.0002 0.0005 12/14/11 L54765-6 73.9 Mercury, Total, CVAF 0.00035 ug/L <RDL 0.0002 0.0005 07/30/12 L56062-4 5 Mercury, Total, CVAF ug/L <MDL 0.0002 0.0005 07/30/12 L56062-5 49.3 Mercury, Total, CVAF ug/L <MDL 0.0002 0.0005 07/30/12 L56062-6 74.1 Mercury, Total, CVAF 0.00020 ug/L <RDL 0.0002 0.0005 12/12/12 L56990-4 4.8 Mercury, Total, CVAF 0.00036 ug/L <RDL 0.0002 0.0005 12/12/12 L56990-5 49.4 Mercury, Total, CVAF 0.00028 ug/L <RDL 0.0002 0.0005 12/12/12 L56990-6 74.1 Mercury, Total, CVAF 0.000517 ug/L 0.0002 0.0005 07/14/11 L53626-4 4.9 Nickel, Dissolved, ICP-MS 0.383 ug/L 0.025 0.125 07/14/11 L53626-5 49.8 Nickel, Dissolved, ICP-MS 0.407 ug/L 0.025 0.125 07/14/11 L53626-6 74.2 Nickel, Dissolved, ICP-MS 0.427 ug/L 0.025 0.125 12/14/11 L54765-4 4.8 Nickel, Dissolved, ICP-MS 0.431 ug/L 0.025 0.125 12/14/11 L54765-5 49.1 Nickel, Dissolved, ICP-MS 0.395 ug/L 0.025 0.125 12/14/11 L54765-6 73.9 Nickel, Dissolved, ICP-MS 0.396 ug/L 0.025 0.125 07/30/12 L56062-4 5 Nickel, Dissolved, ICP-MS 0.392 ug/L 0.025 0.125 07/30/12 L56062-5 49.3 Nickel, Dissolved, ICP-MS 0.401 ug/L 0.025 0.125 07/30/12 L56062-6 74.1 Nickel, Dissolved, ICP-MS 0.406 ug/L 0.025 0.125 12/12/12 L56990-4 4.8 Nickel, Dissolved, ICP-MS 0.432 ug/L 0.025 0.125 12/12/12 L56990-5 49.4 Nickel, Dissolved, ICP-MS 0.436 ug/L 0.025 0.125 12/12/12 L56990-6 74.1 Nickel, Dissolved, ICP-MS 0.415 ug/L 0.025 0.125 07/14/11 L53626-4 4.9 Nickel, Total, ICP-MS 0.393 ug/L 0.025 0.125 07/14/11 L53626-5 49.8 Nickel, Total, ICP-MS 0.426 ug/L 0.025 0.125 07/14/11 L53626-6 74.2 Nickel, Total, ICP-MS 0.467 ug/L 0.025 0.125 12/14/11 L54765-4 4.8 Nickel, Total, ICP-MS 0.439 ug/L 0.025 0.125 12/14/11 L54765-5 49.1 Nickel, Total, ICP-MS 0.412 ug/L 0.025 0.125 12/14/11 L54765-6 73.9 Nickel, Total, ICP-MS 0.501 ug/L 0.025 0.125 07/30/12 L56062-4 5 Nickel, Total, ICP-MS 0.409 ug/L 0.025 0.125 07/30/12 L56062-5 49.3 Nickel, Total, ICP-MS 0.416 ug/L 0.025 0.125 07/30/12 L56062-6 74.1 Nickel, Total, ICP-MS 0.415 ug/L 0.025 0.125 12/12/12 L56990-4 4.8 Nickel, Total, ICP-MS 0.410 ug/L 0.025 0.125 12/12/12 L56990-5 49.4 Nickel, Total, ICP-MS 0.408 ug/L 0.025 0.125 12/12/12 L56990-6 74.1 Nickel, Total, ICP-MS 0.405 ug/L 0.025 0.125 07/14/11 L53626-4 4.9 Silver, Dissolved, ICP-MS 0.019 ug/L <RDL 0.01 0.05 07/14/11 L53626-5 49.8 Silver, Dissolved, ICP-MS 0.020 ug/L <RDL 0.01 0.05 07/14/11 L53626-6 74.2 Silver, Dissolved, ICP-MS 0.019 ug/L <RDL 0.01 0.05 12/14/11 L54765-4 4.8 Silver, Dissolved, ICP-MS 0.028 ug/L <RDL 0.01 0.05 12/14/11 L54765-5 49.1 Silver, Dissolved, ICP-MS 0.028 ug/L <RDL 0.01 0.05 12/14/11 L54765-6 73.9 Silver, Dissolved, ICP-MS 0.028 ug/L <RDL 0.01 0.05 07/30/12 L56062-4 5 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 07/30/12 L56062-5 49.3 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 07/30/12 L56062-6 74.1 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 12/12/12 L56990-4 4.8 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 12/12/12 L56990-5 49.4 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 12/12/12 L56990-6 74.1 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 07/14/11 L53626-4 4.9 Silver, Total, ICP-MS 0.016 ug/L <RDL 0.01 0.05 07/14/11 L53626-5 49.8 Silver, Total, ICP-MS 0.017 ug/L <RDL 0.01 0.05 07/14/11 L53626-6 74.2 Silver, Total, ICP-MS 0.017 ug/L <RDL 0.01 0.05 12/14/11 L54765-4 4.8 Silver, Total, ICP-MS 0.031 ug/L <RDL 0.01 0.05Page 16 of 16 Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 12/14/11 L54765-5 49.1 Silver, Total, ICP-MS 0.033 ug/L <RDL 0.01 0.05 12/14/11 L54765-6 73.9 Silver, Total, ICP-MS 0.032 ug/L <RDL 0.01 0.05 07/30/12 L56062-4 5 Silver, Total, ICP-MS ug/L <MDL 0.01 0.05 07/30/12 L56062-5 49.3 Silver, Total, ICP-MS ug/L <MDL 0.01 0.05 07/30/12 L56062-6 74.1 Silver, Total, ICP-MS ug/L <MDL 0.01 0.05 12/12/12 L56990-4 4.8 Silver, Total, ICP-MS ug/L <MDL 0.01 0.05 12/12/12 L56990-5 49.4 Silver, Total, ICP-MS ug/L <MDL 0.01 0.05 12/12/12 L56990-6 74.1 Silver, Total, ICP-MS ug/L <MDL 0.01 0.05 07/14/11 L53626-4 4.9 Zinc, Dissolved, ICP-MS 1.01 ug/L 0.1 0.5 07/14/11 L53626-5 49.8 Zinc, Dissolved, ICP-MS 0.644 ug/L 0.1 0.5 07/14/11 L53626-6 74.2 Zinc, Dissolved, ICP-MS 0.817 ug/L 0.1 0.5 12/14/11 L54765-4 4.8 Zinc, Dissolved, ICP-MS 1.02 ug/L 0.1 0.5 12/14/11 L54765-5 49.1 Zinc, Dissolved, ICP-MS 0.543 ug/L 0.1 0.5 12/14/11 L54765-6 73.9 Zinc, Dissolved, ICP-MS 0.36 ug/L <RDL 0.1 0.5 07/30/12 L56062-4 5 Zinc, Dissolved, ICP-MS 0.610 ug/L 0.1 0.5 07/30/12 L56062-5 49.3 Zinc, Dissolved, ICP-MS 0.30 ug/L <RDL 0.1 0.5 07/30/12 L56062-6 74.1 Zinc, Dissolved, ICP-MS 0.39 ug/L <RDL 0.1 0.5 12/12/12 L56990-4 4.8 Zinc, Dissolved, ICP-MS 0.858 ug/L 0.1 0.5 12/12/12 L56990-5 49.4 Zinc, Dissolved, ICP-MS 0.40 ug/L <RDL 0.1 0.5 12/12/12 L56990-6 74.1 Zinc, Dissolved, ICP-MS 0.38 ug/L <RDL 0.1 0.5 07/14/11 L53626-4 4.9 Zinc, Total, ICP-MS 1.01 ug/L 0.1 0.5 07/14/11 L53626-5 49.8 Zinc, Total, ICP-MS 0.734 ug/L 0.1 0.5 07/14/11 L53626-6 74.2 Zinc, Total, ICP-MS 0.520 ug/L 0.1 0.5 12/14/11 L54765-4 4.8 Zinc, Total, ICP-MS 0.905 ug/L 0.1 0.5 12/14/11 L54765-5 49.1 Zinc, Total, ICP-MS 0.43 ug/L <RDL 0.1 0.5 12/14/11 L54765-6 73.9 Zinc, Total, ICP-MS 0.608 ug/L 0.1 0.5 07/30/12 L56062-4 5 Zinc, Total, ICP-MS 0.880 ug/L 0.1 0.5 07/30/12 L56062-5 49.3 Zinc, Total, ICP-MS 0.558 ug/L 0.1 0.5 07/30/12 L56062-6 74.1 Zinc, Total, ICP-MS 0.528 ug/L 0.1 0.5 12/12/12 L56990-4 4.8 Zinc, Total, ICP-MS 0.847 ug/L 0.1 0.5 12/12/12 L56990-5 49.4 Zinc, Total, ICP-MS 0.35 ug/L <RDL 0.1 0.5 12/12/12 L56990-6 74.1 Zinc, Total, ICP-MS 0.45 ug/L <RDL 0.1 0.5

Notes Depth (m) - Depth below the water's surface (in meters) from which the sample was collected.
MDL - Method detection limit; the limit of reliable detection

. RDL - Reporting detection limit; the limit of reliable quantitation (PQL). <MDL - Analyte was not detected <RDL - Analyte was detected at a concentration less than the RDL. CFU/100 ml - Colony forming units per 100 milliliters. deg C - Degrees Celcius. mg/L - Milligrams per liter. PSS - Practical Salinity Scale. ug/L - Micrograms per liter.Page 1 of 10 

## Table A-4
Complete Water Quality Monitoring Data for Station LTXQ01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 01/19/11 L52466-8 1 Fecal Coliform 17 CFU/100ml 02/22/11 L52573-8 1 Fecal Coliform 7 CFU/100ml 03/23/11 L52815-8 1 Fecal Coliform 5 CFU/100ml 04/20/11 L53021-8 1 Fecal Coliform 5 CFU/100ml 05/18/11 L53246-8 1 Fecal Coliform 600 CFU/100ml JG 06/21/11 L53436-8 1 Fecal Coliform 10 CFU/100ml 07/19/11 L53682-12 1 Fecal Coliform 32 CFU/100ml 08/17/11 L53914-12 1 Fecal Coliform 60 CFU/100ml 09/21/11 L54144-8 1 Fecal Coliform 52 CFU/100ml 10/18/11 L54463-8 1 Fecal Coliform 24 CFU/100ml 11/29/11 L54552-8 1 Fecal Coliform 21 CFU/100ml 12/20/11 L54823-8 1 Fecal Coliform 16 CFU/100ml 01/25/12 L54921-8 1 Fecal Coliform 71 CFU/100ml 02/22/12 L55105-8 1 Fecal Coliform 70 CFU/100ml 03/21/12 L55258-8 1 Fecal Coliform 12 CFU/100ml 04/18/12 L55459-8 1 Fecal Coliform 17 CFU/100ml 05/23/12 L55738-8 1 Fecal Coliform 71 CFU/100ml 06/20/12 L55903-8 1 Fecal Coliform 48 CFU/100ml 07/18/12 L56065-8 1 Fecal Coliform 74 CFU/100ml 08/22/12 L56245-8 1 Fecal Coliform 61 CFU/100ml 09/19/12 L56377-8 1 Fecal Coliform 98 CFU/100ml 10/17/12 L56718-8 1 Fecal Coliform 110 CFU/100ml 11/28/12 L56867-8 1 Fecal Coliform 23 CFU/100ml 12/19/12 L57120-8 1 Fecal Coliform 41 CFU/100ml 01/19/11 L52466-8 1 Sample Temperature, Field 6.0 deg C 02/22/11 L52573-8 1 Sample Temperature, Field 5.9 deg C 03/23/11 L52815-8 1 Sample Temperature, Field 8.9 deg C 04/20/11 L53021-8 1 Sample Temperature, Field 8.9 deg C 05/18/11 L53246-8 1 Sample Temperature, Field 9.5 deg C 06/21/11 L53436-8 1 Sample Temperature, Field 13.3 deg C 07/19/11 L53682-12 1 Sample Temperature, Field 14.9 deg C 08/17/11 L53914-12 1 Sample Temperature, Field 18.7 deg C 09/21/11 L54144-8 1 Sample Temperature, Field 15.1 deg C 10/18/11 L54463-8 1 Sample Temperature, Field 11.4 deg C 11/29/11 L54552-8 1 Sample Temperature, Field 6.2 deg C 12/20/11 L54823-8 1 Sample Temperature, Field 6.4 deg C 01/25/12 L54921-8 1 Sample Temperature, Field 5.1 deg C 02/22/12 L55105-8 1 Sample Temperature, Field 9.1 deg C 03/21/12 L55258-8 1 Sample Temperature, Field 6.3 deg C 04/18/12 L55459-8 1 Sample Temperature, Field 9.2 deg C 05/23/12 L55738-8 1 Sample Temperature, Field 11.0 deg C 06/20/12 L55903-8 1 Sample Temperature, Field 12.7 deg C 07/18/12 L56065-8 1 Sample Temperature, Field 15.9 deg C 08/22/12 L56245-8 1 Sample Temperature, Field 16.8 deg C 09/19/12 L56377-8 1 Sample Temperature, Field 15.2 deg C 10/17/12 L56718-8 1 Sample Temperature, Field 12.9 deg C 11/28/12 L56867-8 1 Sample Temperature, Field 5.7 deg C 12/19/12 L57120-8 1 Sample Temperature, Field 5.3 deg C 01/19/11 L52466-8 1 Hardness, Calc 30.5 mg CaCO3/L 0.25 1.24 02/22/11 L52573-8 1 Hardness, Calc 55.3 mg CaCO3/L 0.25 1.24 03/23/11 L52815-8 1 Hardness, Calc 58.0 mg CaCO3/L 0.25 1.24 04/20/11 L53021-8 1 Hardness, Calc 68.2 mg CaCO3/L 0.25 1.24Page 2 of 10 

## Table A-4
Complete Water Quality Monitoring Data for Station LTXQ01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 05/18/11 L53246-8 1 Hardness, Calc 25.9 mg CaCO3/L 0.25 1.24 06/21/11 L53436-8 1 Hardness, Calc 47.1 mg CaCO3/L 0.25 1.24 07/11/11 L53619-1 0.5 Hardness, Calc 80.1 mg CaCO3/L 0.331 0.331 07/12/11 L53619-13 0.5 Hardness, Calc 82.3 mg CaCO3/L 0.331 0.331 07/12/11 L53619-2 0.5 Hardness, Calc 78.5 mg CaCO3/L 0.331 0.331 07/13/11 L53619-3 0.5 Hardness, Calc 68.9 mg CaCO3/L 0.331 0.331 07/19/11 L53682-12 1 Hardness, Calc 205 mg CaCO3/L 0.25 1.24 08/17/11 L53914-12 1 Hardness, Calc 168 mg CaCO3/L 0.74 3.71 09/21/11 L54144-8 1 Hardness, Calc 3,000 mg CaCO3/L 0.25 1.24 10/18/11 L54463-8 1 Hardness, Calc 782 mg CaCO3/L 0.25 1.24 11/29/11 L54552-8 1 Hardness, Calc 231 mg CaCO3/L 0.25 1.24 12/12/11 L54760-1 1 Hardness, Calc 653 mg CaCO3/L 1.65 1.65 12/13/11 L54760-11 1 Hardness, Calc 719 mg CaCO3/L 1.65 1.65 12/13/11 L54760-2 1 Hardness, Calc 706 mg CaCO3/L 1.65 1.65 12/14/11 L54760-3 1 Hardness, Calc 786 mg CaCO3/L 1.65 1.65 12/20/11 L54823-8 1 Hardness, Calc 1,730 mg CaCO3/L 0.25 1.24 01/25/12 L54921-8 1 Hardness, Calc 117 mg CaCO3/L 0.25 1.24 02/22/12 L55105-8 1 Hardness, Calc 26.1 mg CaCO3/L 0.25 1.24 03/21/12 L55258-8 1 Hardness, Calc 41.4 mg CaCO3/L 0.25 1.24 04/18/12 L55459-8 1 Hardness, Calc 33.4 mg CaCO3/L 0.25 1.24 05/23/12 L55738-8 1 Hardness, Calc 40.1 mg CaCO3/L 0.25 1.24 06/20/12 L55903-8 1 Hardness, Calc 41.1 mg CaCO3/L 0.25 1.24 07/18/12 L56065-8 1 Hardness, Calc 83.4 mg CaCO3/L 0.25 1.24 07/31/12 L56061-1 0.5 Hardness, Calc 76.5 mg CaCO3/L 0.331 0.331 08/01/12 L56061-2 0.5 Hardness, Calc 60.9 mg CaCO3/L 0.331 0.331 08/02/12 L56061-11 0.5 Hardness, Calc 149 mg CaCO3/L 0.331 0.331 08/02/12 L56061-3 0.5 Hardness, Calc 202 mg CaCO3/L 0.331 0.331 08/22/12 L56245-8 1 Hardness, Calc 1,850 mg CaCO3/L 0.25 1.24 09/19/12 L56377-8 1 Hardness, Calc 1,630 mg CaCO3/L 0.25 1.24 10/17/12 L56718-8 1 Hardness, Calc 592 mg CaCO3/L 0.25 1.24 11/28/12 L56867-8 1 Hardness, Calc 90.9 mg CaCO3/L 0.25 1.24 12/10/12 L56989-1 0.5 Hardness, Calc 25.6 mg CaCO3/L 0.331 0.331 12/11/12 L56989-11 0.5 Hardness, Calc 40.1 mg CaCO3/L 0.331 0.331 12/11/12 L56989-2 0.5 Hardness, Calc 41.5 mg CaCO3/L 0.331 0.331 12/13/12 L56989-3 0.5 Hardness, Calc 161 mg CaCO3/L 0.331 0.331 12/19/12 L57120-8 1 Hardness, Calc 491 mg CaCO3/L 0.25 1.24 01/19/11 L52466-8 1 Dissolved Oxygen, Field 11.8 mg/L 0.5 1 02/22/11 L52573-8 1 Dissolved Oxygen, Field 11.8 mg/L 0.5 1 03/23/11 L52815-8 1 Dissolved Oxygen, Field 8.5 mg/L 0.5 1 04/20/11 L53021-8 1 Dissolved Oxygen, Field 9.6 mg/L 0.5 1 05/18/11 L53246-8 1 Dissolved Oxygen, Field 10.8 mg/L 0.5 1 06/21/11 L53436-8 1 Dissolved Oxygen, Field 10.3 mg/L 0.5 1 07/19/11 L53682-12 1 Dissolved Oxygen, Field 9.3 mg/L 0.5 1 08/17/11 L53914-12 1 Dissolved Oxygen, Field 7.4 mg/L 0.5 1 09/21/11 L54144-8 1 Dissolved Oxygen, Field 6.5 mg/L 0.5 1 10/18/11 L54463-8 1 Dissolved Oxygen, Field 7.7 mg/L 0.5 1 11/29/11 L54552-8 1 Dissolved Oxygen, Field 11.9 mg/L 0.5 1 12/20/11 L54823-8 1 Dissolved Oxygen, Field 10.1 mg/L 0.5 1 01/25/12 L54921-8 1 Dissolved Oxygen, Field 11.4 mg/L 0.5 1 02/22/12 L55105-8 1 Dissolved Oxygen, Field 10.0 mg/L 0.5 1 03/21/12 L55258-8 1 Dissolved Oxygen, Field 12.2 mg/L 0.5 1 04/18/12 L55459-8 1 Dissolved Oxygen, Field 10.9 mg/L 0.5 1Page 3 of 10 

## Table A-4
Complete Water Quality Monitoring Data for Station LTXQ01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 05/23/12 L55738-8 1 Dissolved Oxygen, Field 10.7 mg/L 0.5 1 06/20/12 L55903-8 1 Dissolved Oxygen, Field 9.7 mg/L 0.5 1 07/18/12 L56065-8 1 Dissolved Oxygen, Field 7.9 mg/L 0.5 1 08/22/12 L56245-8 1 Dissolved Oxygen, Field 7.7 mg/L 0.5 1 09/19/12 L56377-8 1 Dissolved Oxygen, Field 7.1 mg/L 0.5 1 10/17/12 L56718-8 1 Dissolved Oxygen, Field 8.8 mg/L 0.5 1 11/28/12 L56867-8 1 Dissolved Oxygen, Field 11.1 mg/L 0.5 1 12/19/12 L57120-8 1 Dissolved Oxygen, Field 11.2 mg/L 0.5 1 01/19/11 L52466-8 1 Total Suspended Solids 15.8 mg/L 0.5 10 02/22/11 L52573-8 1 Total Suspended Solids 4.2 mg/L <RDL 0.5 10 03/23/11 L52815-8 1 Total Suspended Solids 13.1 mg/L 0.5 10 04/20/11 L53021-8 1 Total Suspended Solids 20.3 mg/L 0.5 11 05/18/11 L53246-8 1 Total Suspended Solids 47.3 mg/L 0.8 17 06/21/11 L53436-8 1 Total Suspended Solids 9.8 mg/L <RDL 0.5 10 07/19/11 L53682-12 1 Total Suspended Solids 16.0 mg/L <RDL 1 20 09/21/11 L54144-8 1 Total Suspended Solids 5.2 mg/L <RDL 0.5 10 10/18/11 L54463-8 1 Total Suspended Solids 2.5 mg/L <RDL 0.5 10 11/29/11 L54552-8 1 Total Suspended Solids 11.5 mg/L 0.6 11 12/20/11 L54823-8 1 Total Suspended Solids 3.3 mg/L 0.5 1 01/25/12 L54921-8 1 Total Suspended Solids 12.0 mg/L 0.5 10 02/22/12 L55105-8 1 Total Suspended Solids 116.0 mg/L 1 20 03/21/12 L55258-8 1 Total Suspended Solids 13.5 mg/L 0.5 10 04/18/12 L55459-8 1 Total Suspended Solids 5.9 mg/L <RDL 0.5 10 05/23/12 L55738-8 1 Total Suspended Solids 12.6 mg/L 0.5 10 06/20/12 L55903-8 1 Total Suspended Solids 11.0 mg/L <RDL 1 20 07/18/12 L56065-8 1 Total Suspended Solids 5.9 mg/L <RDL 0.5 11 08/22/12 L56245-8 1 Total Suspended Solids 4.7 mg/L <RDL 0.5 10 09/19/12 L56377-8 1 Total Suspended Solids 6.7 mg/L <RDL 0.5 10 10/17/12 L56718-8 1 Total Suspended Solids 8.6 mg/L <RDL 1 20 12/19/12 L57120-8 1 Total Suspended Solids 6.6 mg/L <RDL 1 20 07/11/11 L53619-1 0.5 pH, Field 7.16 pH 07/12/11 L53619-13 0.5 pH, Field 7.16 pH 07/12/11 L53619-2 0.5 pH, Field 7.14 pH 07/13/11 L53619-3 0.5 pH, Field 7.15 pH 12/12/11 L54760-1 1 pH, Field 6.96 pH 12/13/11 L54760-11 1 pH, Field 7.15 pH 12/13/11 L54760-2 1 pH, Field 6.90 pH 12/14/11 L54760-3 1 pH, Field 6.85 pH 07/31/12 L56061-1 0.5 pH, Field 7.16 pH 08/01/12 L56061-2 0.5 pH, Field 7.15 pH 08/02/12 L56061-11 0.5 pH, Field 7.05 pH 08/02/12 L56061-3 0.5 pH, Field 7.07 pH 12/10/12 L56989-1 0.5 pH, Field 7.10 pH 12/11/12 L56989-11 0.5 pH, Field 7.27 pH 12/11/12 L56989-2 0.5 pH, Field 7.27 pH 12/13/12 L56989-3 0.5 pH, Field 7.09 pH 01/19/11 L52466-8 1 Salinity PSS <MDL 2 3 02/22/11 L52573-8 1 Salinity PSS <MDL 2 3 03/23/11 L52815-8 1 Salinity PSS <MDL 2 3 04/20/11 L53021-8 1 Salinity PSS <MDL 2 3 05/18/11 L53246-8 1 Salinity PSS <MDL 2 3 06/21/11 L53436-8 1 Salinity PSS <MDL 2 3Page 4 of 10 

## Table A-4
Complete Water Quality Monitoring Data for Station LTXQ01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 07/11/11 L53619-1 0.5 Salinity PSS <MDL 2 3 07/12/11 L53619-13 0.5 Salinity PSS <MDL 2 3 07/12/11 L53619-2 0.5 Salinity PSS <MDL 2 3 07/13/11 L53619-3 0.5 Salinity PSS <MDL 2 3 07/19/11 L53682-12 1 Salinity 28.809 PSS 2 3 08/17/11 L53914-12 1 Salinity 29.649 PSS 2 3 09/21/11 L54144-8 1 Salinity 11.828 PSS 2 3 10/18/11 L54463-8 1 Salinity 3.907 PSS 2 3 11/29/11 L54552-8 1 Salinity PSS <MDL 2 3 12/12/11 L54760-1 1 Salinity 3.985 PSS 2 3 12/13/11 L54760-11 1 Salinity 4.105 PSS 2 3 12/13/11 L54760-2 1 Salinity 4.369 PSS 2 3 12/14/11 L54760-3 1 Salinity 4.476 PSS 2 3 12/20/11 L54823-8 1 Salinity 9.102 PSS 2 3 01/25/12 L54921-8 1 Salinity PSS <MDL 2 3 02/22/12 L55105-8 1 Salinity PSS <MDL 2 3 03/21/12 L55258-8 1 Salinity PSS <MDL 2 3 04/18/12 L55459-8 1 Salinity 29.645 PSS 2 3 05/23/12 L55738-8 1 Salinity PSS <MDL 2 3 06/20/12 L55903-8 1 Salinity 25.520 PSS 2 3 07/18/12 L56065-8 1 Salinity PSS <MDL 2 3 07/31/12 L56061-1 0.5 Salinity PSS <MDL 2 3 08/01/12 L56061-2 0.5 Salinity PSS <MDL 2 3 08/02/12 L56061-11 0.5 Salinity PSS <MDL 2 3 08/02/12 L56061-3 0.5 Salinity PSS <MDL 2 3 08/22/12 L56245-8 1 Salinity 9.761 PSS 2 3 09/19/12 L56377-8 1 Salinity 9.132 PSS 2 3 10/17/12 L56718-8 1 Salinity 3.180 PSS 2 3 11/28/12 L56867-8 1 Salinity PSS <MDL 2 3 12/10/12 L56989-1 0.5 Salinity PSS <MDL 2 3 12/11/12 L56989-11 0.5 Salinity PSS <MDL 2 3 12/11/12 L56989-2 0.5 Salinity PSS <MDL 2 3 12/13/12 L56989-3 0.5 Salinity PSS <MDL 2 3 12/19/12 L57120-8 1 Salinity 2.330 PSS <RDL 2 3 07/11/11 L53619-1 0.5 Arsenic, Dissolved, ICP-MS 0.402 ug/L 0.01 0.05 07/12/11 L53619-13 0.5 Arsenic, Dissolved, ICP-MS 0.399 ug/L 0.01 0.05 07/12/11 L53619-2 0.5 Arsenic, Dissolved, ICP-MS 0.407 ug/L 0.01 0.05 07/13/11 L53619-3 0.5 Arsenic, Dissolved, ICP-MS 0.391 ug/L 0.01 0.05 12/12/11 L54760-1 1 Arsenic, Dissolved, ICP-MS 0.413 ug/L 0.01 0.05 12/13/11 L54760-11 1 Arsenic, Dissolved, ICP-MS 0.478 ug/L 0.01 0.05 12/13/11 L54760-2 1 Arsenic, Dissolved, ICP-MS 0.459 ug/L 0.01 0.05 12/14/11 L54760-3 1 Arsenic, Dissolved, ICP-MS 0.445 ug/L 0.01 0.05 07/31/12 L56061-1 0.5 Arsenic, Dissolved, ICP-MS 0.512 ug/L 0.01 0.05 08/01/12 L56061-2 0.5 Arsenic, Dissolved, ICP-MS 0.550 ug/L 0.01 0.05 08/02/12 L56061-11 0.5 Arsenic, Dissolved, ICP-MS 0.577 ug/L 0.01 0.05 08/02/12 L56061-3 0.5 Arsenic, Dissolved, ICP-MS 0.559 ug/L 0.01 0.05 12/10/12 L56989-1 0.5 Arsenic, Dissolved, ICP-MS 0.401 ug/L 0.01 0.05 12/11/12 L56989-11 0.5 Arsenic, Dissolved, ICP-MS 0.419 ug/L 0.01 0.05 12/11/12 L56989-2 0.5 Arsenic, Dissolved, ICP-MS 0.434 ug/L 0.01 0.05 12/13/12 L56989-3 0.5 Arsenic, Dissolved, ICP-MS 0.453 ug/L 0.01 0.05 07/11/11 L53619-1 0.5 Arsenic, Total, ICP-MS 0.506 ug/L 0.01 0.05 07/12/11 L53619-13 0.5 Arsenic, Total, ICP-MS 0.537 ug/L 0.01 0.05Page 5 of 10 

## Table A-4
Complete Water Quality Monitoring Data for Station LTXQ01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 07/12/11 L53619-2 0.5 Arsenic, Total, ICP-MS 0.555 ug/L 0.01 0.05 07/13/11 L53619-3 0.5 Arsenic, Total, ICP-MS 0.485 ug/L 0.01 0.05 12/12/11 L54760-1 1 Arsenic, Total, ICP-MS 0.656 ug/L 0.01 0.05 12/13/11 L54760-11 1 Arsenic, Total, ICP-MS 0.640 ug/L 0.01 0.05 12/13/11 L54760-2 1 Arsenic, Total, ICP-MS 0.656 ug/L 0.01 0.05 12/14/11 L54760-3 1 Arsenic, Total, ICP-MS 0.659 ug/L 0.01 0.05 07/31/12 L56061-1 0.5 Arsenic, Total, ICP-MS 0.830 ug/L 0.01 0.05 08/01/12 L56061-2 0.5 Arsenic, Total, ICP-MS 0.757 ug/L 0.01 0.05 08/02/12 L56061-11 0.5 Arsenic, Total, ICP-MS 0.762 ug/L 0.01 0.05 08/02/12 L56061-3 0.5 Arsenic, Total, ICP-MS 0.857 ug/L 0.01 0.05 12/10/12 L56989-1 0.5 Arsenic, Total, ICP-MS 0.474 ug/L 0.01 0.05 12/11/12 L56989-11 0.5 Arsenic, Total, ICP-MS 0.545 ug/L 0.01 0.05 12/11/12 L56989-2 0.5 Arsenic, Total, ICP-MS 0.538 ug/L 0.01 0.05 12/13/12 L56989-3 0.5 Arsenic, Total, ICP-MS 0.596 ug/L 0.01 0.05 07/11/11 L53619-1 0.5 Cadmium, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 07/12/11 L53619-13 0.5 Cadmium, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 07/12/11 L53619-2 0.5 Cadmium, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 07/13/11 L53619-3 0.5 Cadmium, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 12/12/11 L54760-1 1 Cadmium, Dissolved, ICP-MS 0.020 ug/L <RDL 0.005 0.025 12/13/11 L54760-11 1 Cadmium, Dissolved, ICP-MS 0.019 ug/L <RDL 0.005 0.025 12/13/11 L54760-2 1 Cadmium, Dissolved, ICP-MS 0.019 ug/L <RDL 0.005 0.025 12/14/11 L54760-3 1 Cadmium, Dissolved, ICP-MS 0.022 ug/L <RDL 0.005 0.025 07/31/12 L56061-1 0.5 Cadmium, Dissolved, ICP-MS 0.0065 ug/L <RDL 0.005 0.025 08/01/12 L56061-2 0.5 Cadmium, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 08/02/12 L56061-11 0.5 Cadmium, Dissolved, ICP-MS 0.0074 ug/L <RDL 0.005 0.025 08/02/12 L56061-3 0.5 Cadmium, Dissolved, ICP-MS 0.0076 ug/L <RDL 0.005 0.025 12/10/12 L56989-1 0.5 Cadmium, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 12/11/12 L56989-11 0.5 Cadmium, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 12/11/12 L56989-2 0.5 Cadmium, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 12/13/12 L56989-3 0.5 Cadmium, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 07/11/11 L53619-1 0.5 Cadmium, Total, ICP-MS 0.0053 ug/L <RDL 0.005 0.025 07/12/11 L53619-13 0.5 Cadmium, Total, ICP-MS 0.0067 ug/L <RDL 0.005 0.025 07/12/11 L53619-2 0.5 Cadmium, Total, ICP-MS 0.0070 ug/L <RDL 0.005 0.025 07/13/11 L53619-3 0.5 Cadmium, Total, ICP-MS 0.0052 ug/L <RDL 0.005 0.025 12/12/11 L54760-1 1 Cadmium, Total, ICP-MS 0.019 ug/L <RDL 0.005 0.025 12/13/11 L54760-11 1 Cadmium, Total, ICP-MS 0.016 ug/L <RDL 0.005 0.025 12/13/11 L54760-2 1 Cadmium, Total, ICP-MS 0.016 ug/L <RDL 0.005 0.025 12/14/11 L54760-3 1 Cadmium, Total, ICP-MS 0.023 ug/L <RDL 0.005 0.025 07/31/12 L56061-1 0.5 Cadmium, Total, ICP-MS 0.012 ug/L <RDL 0.005 0.025 08/01/12 L56061-2 0.5 Cadmium, Total, ICP-MS 0.011 ug/L <RDL 0.005 0.025 08/02/12 L56061-11 0.5 Cadmium, Total, ICP-MS 0.014 ug/L <RDL 0.005 0.025 08/02/12 L56061-3 0.5 Cadmium, Total, ICP-MS 0.016 ug/L <RDL 0.005 0.025 12/10/12 L56989-1 0.5 Cadmium, Total, ICP-MS ug/L <MDL 0.005 0.025 12/11/12 L56989-11 0.5 Cadmium, Total, ICP-MS 0.0052 ug/L <RDL 0.005 0.025 12/11/12 L56989-2 0.5 Cadmium, Total, ICP-MS 0.0053 ug/L <RDL 0.005 0.025 12/13/12 L56989-3 0.5 Cadmium, Total, ICP-MS 0.0095 ug/L <RDL 0.005 0.025 07/11/11 L53619-1 0.5 Chromium, Dissolved, ICP-MS 0.061 ug/L <RDL 0.05 0.25 07/12/11 L53619-13 0.5 Chromium, Dissolved, ICP-MS 0.059 ug/L <RDL 0.05 0.25 07/12/11 L53619-2 0.5 Chromium, Dissolved, ICP-MS 0.057 ug/L <RDL 0.05 0.25 07/13/11 L53619-3 0.5 Chromium, Dissolved, ICP-MS 0.063 ug/L <RDL 0.05 0.25 12/12/11 L54760-1 1 Chromium, Dissolved, ICP-MS 0.082 ug/L <RDL 0.05 0.25 12/13/11 L54760-11 1 Chromium, Dissolved, ICP-MS 0.075 ug/L <RDL 0.05 0.25Page 6 of 10 

## Table A-4
Complete Water Quality Monitoring Data for Station LTXQ01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 12/13/11 L54760-2 1 Chromium, Dissolved, ICP-MS 0.086 ug/L <RDL 0.05 0.25 12/14/11 L54760-3 1 Chromium, Dissolved, ICP-MS 0.082 ug/L <RDL 0.05 0.25 07/31/12 L56061-1 0.5 Chromium, Dissolved, ICP-MS 0.071 ug/L <RDL 0.05 0.25 08/01/12 L56061-2 0.5 Chromium, Dissolved, ICP-MS 0.070 ug/L <RDL 0.05 0.25 08/02/12 L56061-11 0.5 Chromium, Dissolved, ICP-MS ug/L <MDL 0.05 0.25 08/02/12 L56061-3 0.5 Chromium, Dissolved, ICP-MS 0.064 ug/L <RDL 0.05 0.25 12/10/12 L56989-1 0.5 Chromium, Dissolved, ICP-MS 0.072 ug/L <RDL 0.05 0.25 12/11/12 L56989-11 0.5 Chromium, Dissolved, ICP-MS 0.080 ug/L <RDL 0.05 0.25 12/11/12 L56989-2 0.5 Chromium, Dissolved, ICP-MS 0.082 ug/L <RDL 0.05 0.25 12/13/12 L56989-3 0.5 Chromium, Dissolved, ICP-MS 0.11 ug/L <RDL 0.05 0.25 07/11/11 L53619-1 0.5 Chromium, Total, ICP-MS 0.12 ug/L <RDL 0.05 0.25 07/12/11 L53619-13 0.5 Chromium, Total, ICP-MS 0.16 ug/L <RDL 0.05 0.25 07/12/11 L53619-2 0.5 Chromium, Total, ICP-MS 0.18 ug/L <RDL 0.05 0.25 07/13/11 L53619-3 0.5 Chromium, Total, ICP-MS 0.11 ug/L <RDL 0.05 0.25 12/12/11 L54760-1 1 Chromium, Total, ICP-MS 0.19 ug/L <RDL 0.05 0.25 12/13/11 L54760-11 1 Chromium, Total, ICP-MS 0.16 ug/L <RDL 0.05 0.25 12/13/11 L54760-2 1 Chromium, Total, ICP-MS 0.18 ug/L <RDL 0.05 0.25 12/14/11 L54760-3 1 Chromium, Total, ICP-MS 0.18 ug/L <RDL 0.05 0.25 07/31/12 L56061-1 0.5 Chromium, Total, ICP-MS 0.22 ug/L <RDL 0.05 0.25 08/01/12 L56061-2 0.5 Chromium, Total, ICP-MS 0.16 ug/L <RDL 0.05 0.25 08/02/12 L56061-11 0.5 Chromium, Total, ICP-MS 0.19 ug/L <RDL 0.05 0.25 08/02/12 L56061-3 0.5 Chromium, Total, ICP-MS 0.22 ug/L <RDL 0.05 0.25 12/10/12 L56989-1 0.5 Chromium, Total, ICP-MS 0.14 ug/L <RDL 0.05 0.25 12/11/12 L56989-11 0.5 Chromium, Total, ICP-MS 0.13 ug/L <RDL 0.05 0.25 12/11/12 L56989-2 0.5 Chromium, Total, ICP-MS 0.17 ug/L <RDL 0.05 0.25 12/13/12 L56989-3 0.5 Chromium, Total, ICP-MS 0.21 ug/L <RDL 0.05 0.25 07/11/11 L53619-1 0.5 Copper, Dissolved, ICP-MS 0.366 ug/L 0.025 0.125 07/12/11 L53619-13 0.5 Copper, Dissolved, ICP-MS 0.352 ug/L 0.025 0.125 07/12/11 L53619-2 0.5 Copper, Dissolved, ICP-MS 0.306 ug/L 0.025 0.125 07/13/11 L53619-3 0.5 Copper, Dissolved, ICP-MS 0.328 ug/L 0.025 0.125 12/12/11 L54760-1 1 Copper, Dissolved, ICP-MS 0.468 ug/L 0.025 0.125 12/13/11 L54760-11 1 Copper, Dissolved, ICP-MS 0.360 ug/L 0.025 0.125 12/13/11 L54760-2 1 Copper, Dissolved, ICP-MS 0.377 ug/L 0.025 0.125 12/14/11 L54760-3 1 Copper, Dissolved, ICP-MS 0.387 ug/L 0.025 0.125 07/31/12 L56061-1 0.5 Copper, Dissolved, ICP-MS 0.456 ug/L 0.025 0.125 08/01/12 L56061-2 0.5 Copper, Dissolved, ICP-MS 0.440 ug/L 0.025 0.125 08/02/12 L56061-11 0.5 Copper, Dissolved, ICP-MS 0.486 ug/L 0.025 0.125 08/02/12 L56061-3 0.5 Copper, Dissolved, ICP-MS 0.467 ug/L 0.025 0.125 12/10/12 L56989-1 0.5 Copper, Dissolved, ICP-MS 0.507 ug/L 0.025 0.125 12/11/12 L56989-11 0.5 Copper, Dissolved, ICP-MS 0.550 ug/L 0.025 0.125 12/11/12 L56989-2 0.5 Copper, Dissolved, ICP-MS 0.551 ug/L 0.025 0.125 12/13/12 L56989-3 0.5 Copper, Dissolved, ICP-MS 0.637 ug/L 0.025 0.125 07/11/11 L53619-1 0.5 Copper, Total, ICP-MS 0.613 ug/L 0.025 0.125 07/12/11 L53619-13 0.5 Copper, Total, ICP-MS 0.972 ug/L 0.025 0.125 07/12/11 L53619-2 0.5 Copper, Total, ICP-MS 1.07 ug/L 0.025 0.125 07/13/11 L53619-3 0.5 Copper, Total, ICP-MS 0.656 ug/L 0.025 0.125 12/12/11 L54760-1 1 Copper, Total, ICP-MS 0.710 ug/L 0.025 0.125 12/13/11 L54760-11 1 Copper, Total, ICP-MS 0.692 ug/L 0.025 0.125 12/13/11 L54760-2 1 Copper, Total, ICP-MS 0.894 ug/L 0.025 0.125 12/14/11 L54760-3 1 Copper, Total, ICP-MS 0.636 ug/L 0.025 0.125 07/31/12 L56061-1 0.5 Copper, Total, ICP-MS 1.18 ug/L 0.025 0.125 08/01/12 L56061-2 0.5 Copper, Total, ICP-MS 0.889 ug/L 0.025 0.125Page 7 of 10 

## Table A-4
Complete Water Quality Monitoring Data for Station LTXQ01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 08/02/12 L56061-11 0.5 Copper, Total, ICP-MS 0.848 ug/L 0.025 0.125 08/02/12 L56061-3 0.5 Copper, Total, ICP-MS 1.21 ug/L 0.025 0.125 12/10/12 L56989-1 0.5 Copper, Total, ICP-MS 0.817 ug/L 0.025 0.125 12/11/12 L56989-11 0.5 Copper, Total, ICP-MS 0.979 ug/L 0.025 0.125 12/11/12 L56989-2 0.5 Copper, Total, ICP-MS 0.934 ug/L 0.025 0.125 12/13/12 L56989-3 0.5 Copper, Total, ICP-MS 1.37 ug/L 0.025 0.125 07/11/11 L53619-1 0.5 Lead, Dissolved, ICP-MS 0.013 ug/L <RDL 0.005 0.025 07/12/11 L53619-13 0.5 Lead, Dissolved, ICP-MS 0.015 ug/L <RDL 0.005 0.025 07/12/11 L53619-2 0.5 Lead, Dissolved, ICP-MS 0.013 ug/L <RDL 0.005 0.025 07/13/11 L53619-3 0.5 Lead, Dissolved, ICP-MS 0.023 ug/L <RDL 0.005 0.025 12/12/11 L54760-1 1 Lead, Dissolved, ICP-MS 0.0089 ug/L <RDL 0.005 0.025 12/13/11 L54760-11 1 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 12/13/11 L54760-2 1 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 12/14/11 L54760-3 1 Lead, Dissolved, ICP-MS ug/L <MDL 0.005 0.025 07/31/12 L56061-1 0.5 Lead, Dissolved, ICP-MS 0.017 ug/L <RDL 0.005 0.025 08/01/12 L56061-2 0.5 Lead, Dissolved, ICP-MS 0.017 ug/L <RDL 0.005 0.025 08/02/12 L56061-11 0.5 Lead, Dissolved, ICP-MS 0.019 ug/L <RDL 0.005 0.025 08/02/12 L56061-3 0.5 Lead, Dissolved, ICP-MS 0.021 ug/L <RDL 0.005 0.025 12/10/12 L56989-1 0.5 Lead, Dissolved, ICP-MS 0.022 ug/L <RDL 0.005 0.025 12/11/12 L56989-11 0.5 Lead, Dissolved, ICP-MS 0.025 ug/L <RDL 0.005 0.025 12/11/12 L56989-2 0.5 Lead, Dissolved, ICP-MS 0.025 ug/L <RDL 0.005 0.025 12/13/12 L56989-3 0.5 Lead, Dissolved, ICP-MS 0.029 ug/L 0.005 0.025 07/11/11 L53619-1 0.5 Lead, Total, ICP-MS 0.0681 ug/L 0.005 0.025 07/12/11 L53619-13 0.5 Lead, Total, ICP-MS 0.190 ug/L 0.005 0.025 07/12/11 L53619-2 0.5 Lead, Total, ICP-MS 0.172 ug/L 0.005 0.025 07/13/11 L53619-3 0.5 Lead, Total, ICP-MS 0.0920 ug/L 0.005 0.025 12/12/11 L54760-1 1 Lead, Total, ICP-MS 0.0481 ug/L 0.005 0.025 12/13/11 L54760-11 1 Lead, Total, ICP-MS 0.0573 ug/L 0.005 0.025 12/13/11 L54760-2 1 Lead, Total, ICP-MS 0.0572 ug/L 0.005 0.025 12/14/11 L54760-3 1 Lead, Total, ICP-MS 0.0566 ug/L 0.005 0.025 07/31/12 L56061-1 0.5 Lead, Total, ICP-MS 0.327 ug/L 0.005 0.025 08/01/12 L56061-2 0.5 Lead, Total, ICP-MS 0.159 ug/L 0.005 0.025 08/02/12 L56061-11 0.5 Lead, Total, ICP-MS 0.168 ug/L 0.005 0.025 08/02/12 L56061-3 0.5 Lead, Total, ICP-MS 0.297 ug/L 0.005 0.025 12/10/12 L56989-1 0.5 Lead, Total, ICP-MS 0.0859 ug/L 0.005 0.025 12/11/12 L56989-11 0.5 Lead, Total, ICP-MS 0.115 ug/L 0.005 0.025 12/11/12 L56989-2 0.5 Lead, Total, ICP-MS 0.109 ug/L 0.005 0.025 12/13/12 L56989-3 0.5 Lead, Total, ICP-MS 0.178 ug/L 0.005 0.025 07/11/11 L53619-1 0.5 Mercury, Dissolved, CVAF 0.00043 ug/L <RDL 0.0002 0.0005 07/12/11 L53619-13 0.5 Mercury, Dissolved, CVAF 0.00047 ug/L <RDL 0.0002 0.0005 07/12/11 L53619-2 0.5 Mercury, Dissolved, CVAF 0.00035 ug/L <RDL 0.0002 0.0005 07/13/11 L53619-3 0.5 Mercury, Dissolved, CVAF 0.00047 ug/L <RDL 0.0002 0.0005 12/12/11 L54760-1 1 Mercury, Dissolved, CVAF 0.00033 ug/L <RDL 0.0002 0.0005 12/13/11 L54760-11 1 Mercury, Dissolved, CVAF 0.00029 ug/L <RDL 0.0002 0.0005 12/13/11 L54760-2 1 Mercury, Dissolved, CVAF 0.00033 ug/L <RDL 0.0002 0.0005 12/14/11 L54760-3 1 Mercury, Dissolved, CVAF 0.00024 ug/L <RDL 0.0002 0.0005 07/31/12 L56061-1 0.5 Mercury, Dissolved, CVAF 0.00030 ug/L <RDL 0.0002 0.0005 08/01/12 L56061-2 0.5 Mercury, Dissolved, CVAF 0.00035 ug/L <RDL 0.0002 0.0005 08/02/12 L56061-11 0.5 Mercury, Dissolved, CVAF 0.00034 ug/L <RDL 0.0002 0.0005 08/02/12 L56061-3 0.5 Mercury, Dissolved, CVAF 0.00032 ug/L <RDL 0.0002 0.0005 12/10/12 L56989-1 0.5 Mercury, Dissolved, CVAF 0.000884 ug/L 0.0002 0.0005 12/11/12 L56989-11 0.5 Mercury, Dissolved, CVAF 0.000746 ug/L 0.0002 0.0005Page 8 of 10 

## Table A-4
Complete Water Quality Monitoring Data for Station LTXQ01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 12/11/12 L56989-2 0.5 Mercury, Dissolved, CVAF 0.000683 ug/L 0.0002 0.0005 12/13/12 L56989-3 0.5 Mercury, Dissolved, CVAF 0.000772 ug/L 0.0002 0.0005 07/11/11 L53619-1 0.5 Mercury, Total, CVAF 0.000870 ug/L 0.0002 0.0005 07/12/11 L53619-13 0.5 Mercury, Total, CVAF 0.00199 ug/L 0.0002 0.0005 07/12/11 L53619-2 0.5 Mercury, Total, CVAF 0.00146 ug/L 0.0002 0.0005 07/13/11 L53619-3 0.5 Mercury, Total, CVAF 0.00117 ug/L 0.0002 0.0005 12/12/11 L54760-1 1 Mercury, Total, CVAF 0.00114 ug/L 0.0002 0.0005 12/13/11 L54760-11 1 Mercury, Total, CVAF 0.000608 ug/L 0.0002 0.0005 12/13/11 L54760-2 1 Mercury, Total, CVAF 0.000560 ug/L 0.0002 0.0005 12/14/11 L54760-3 1 Mercury, Total, CVAF 0.000656 ug/L 0.0002 0.0005 07/31/12 L56061-1 0.5 Mercury, Total, CVAF 0.00158 ug/L 0.0002 0.0005 08/01/12 L56061-2 0.5 Mercury, Total, CVAF 0.00128 ug/L 0.0002 0.0005 08/02/12 L56061-11 0.5 Mercury, Total, CVAF 0.00113 ug/L 0.0002 0.0005 08/02/12 L56061-3 0.5 Mercury, Total, CVAF 0.00132 ug/L 0.0002 0.0005 12/10/12 L56989-1 0.5 Mercury, Total, CVAF 0.00125 ug/L 0.0002 0.0005 12/11/12 L56989-11 0.5 Mercury, Total, CVAF 0.00141 ug/L 0.0002 0.0005 12/11/12 L56989-2 0.5 Mercury, Total, CVAF 0.00133 ug/L 0.0002 0.0005 12/13/12 L56989-3 0.5 Mercury, Total, CVAF 0.00192 ug/L 0.0002 0.0005 07/11/11 L53619-1 0.5 Nickel, Dissolved, ICP-MS 0.265 ug/L 0.025 0.125 07/12/11 L53619-13 0.5 Nickel, Dissolved, ICP-MS 0.230 ug/L 0.025 0.125 07/12/11 L53619-2 0.5 Nickel, Dissolved, ICP-MS 0.216 ug/L 0.025 0.125 07/13/11 L53619-3 0.5 Nickel, Dissolved, ICP-MS 0.224 ug/L 0.025 0.125 12/12/11 L54760-1 1 Nickel, Dissolved, ICP-MS 0.830 ug/L 0.025 0.125 12/13/11 L54760-11 1 Nickel, Dissolved, ICP-MS 0.951 ug/L 0.025 0.125 12/13/11 L54760-2 1 Nickel, Dissolved, ICP-MS 0.981 ug/L 0.025 0.125 12/14/11 L54760-3 1 Nickel, Dissolved, ICP-MS 1.09 ug/L 0.025 0.125 07/31/12 L56061-1 0.5 Nickel, Dissolved, ICP-MS 0.327 ug/L 0.025 0.125 08/01/12 L56061-2 0.5 Nickel, Dissolved, ICP-MS 0.260 ug/L 0.025 0.125 08/02/12 L56061-11 0.5 Nickel, Dissolved, ICP-MS 0.274 ug/L 0.025 0.125 08/02/12 L56061-3 0.5 Nickel, Dissolved, ICP-MS 0.319 ug/L 0.025 0.125 12/10/12 L56989-1 0.5 Nickel, Dissolved, ICP-MS 0.156 ug/L 0.025 0.125 12/11/12 L56989-11 0.5 Nickel, Dissolved, ICP-MS 0.169 ug/L 0.025 0.125 12/11/12 L56989-2 0.5 Nickel, Dissolved, ICP-MS 0.180 ug/L 0.025 0.125 12/13/12 L56989-3 0.5 Nickel, Dissolved, ICP-MS 0.212 ug/L 0.025 0.125 07/11/11 L53619-1 0.5 Nickel, Total, ICP-MS 0.312 ug/L 0.025 0.125 07/12/11 L53619-13 0.5 Nickel, Total, ICP-MS 0.411 ug/L 0.025 0.125 07/12/11 L53619-2 0.5 Nickel, Total, ICP-MS 0.431 ug/L 0.025 0.125 07/13/11 L53619-3 0.5 Nickel, Total, ICP-MS 0.271 ug/L 0.025 0.125 12/12/11 L54760-1 1 Nickel, Total, ICP-MS 0.917 ug/L 0.025 0.125 12/13/11 L54760-11 1 Nickel, Total, ICP-MS 1.02 ug/L 0.025 0.125 12/13/11 L54760-2 1 Nickel, Total, ICP-MS 0.951 ug/L 0.025 0.125 12/14/11 L54760-3 1 Nickel, Total, ICP-MS 0.748 ug/L 0.025 0.125 07/31/12 L56061-1 0.5 Nickel, Total, ICP-MS 0.61 ug/L <RDL 0.13 0.625 08/01/12 L56061-2 0.5 Nickel, Total, ICP-MS 0.645 ug/L 0.13 0.625 08/02/12 L56061-11 0.5 Nickel, Total, ICP-MS 0.41 ug/L <RDL 0.13 0.625 08/02/12 L56061-3 0.5 Nickel, Total, ICP-MS 0.656 ug/L 0.13 0.625 12/10/12 L56989-1 0.5 Nickel, Total, ICP-MS 0.242 ug/L 0.025 0.125 12/11/12 L56989-11 0.5 Nickel, Total, ICP-MS 0.315 ug/L 0.025 0.125 12/11/12 L56989-2 0.5 Nickel, Total, ICP-MS 0.316 ug/L 0.025 0.125 12/13/12 L56989-3 0.5 Nickel, Total, ICP-MS 0.388 ug/L 0.025 0.125 07/11/11 L53619-1 0.5 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 07/12/11 L53619-13 0.5 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05Page 9 of 10 

## Table A-4
Complete Water Quality Monitoring Data for Station LTXQ01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 07/12/11 L53619-2 0.5 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 07/13/11 L53619-3 0.5 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 12/12/11 L54760-1 1 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 12/13/11 L54760-11 1 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 12/13/11 L54760-2 1 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 12/14/11 L54760-3 1 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 07/31/12 L56061-1 0.5 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 08/01/12 L56061-2 0.5 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 08/02/12 L56061-11 0.5 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 08/02/12 L56061-3 0.5 Silver, Dissolved, ICP-MS ug/L <MDL 0.01 0.05 12/10/12 L56989-1 0.5 Silver, Dissolved, ICP-MS 0.022 ug/L <RDL 0.01 0.05 12/11/12 L56989-11 0.5 Silver, Dissolved, ICP-MS 0.017 ug/L <RDL 0.01 0.05 12/11/12 L56989-2 0.5 Silver, Dissolved, ICP-MS 0.022 ug/L <RDL 0.01 0.05 12/13/12 L56989-3 0.5 Silver, Dissolved, ICP-MS 0.021 ug/L <RDL 0.01 0.05 07/11/11 L53619-1 0.5 Silver, Total, ICP-MS 0.010 ug/L <RDL 0.01 0.05 07/12/11 L53619-13 0.5 Silver, Total, ICP-MS 0.014 ug/L <RDL 0.01 0.05 07/12/11 L53619-2 0.5 Silver, Total, ICP-MS 0.014 ug/L <RDL 0.01 0.05 07/13/11 L53619-3 0.5 Silver, Total, ICP-MS ug/L <MDL 0.01 0.05 12/12/11 L54760-1 1 Silver, Total, ICP-MS 0.012 ug/L <RDL 0.01 0.05 12/13/11 L54760-11 1 Silver, Total, ICP-MS 0.012 ug/L <RDL 0.01 0.05 12/13/11 L54760-2 1 Silver, Total, ICP-MS 0.012 ug/L <RDL 0.01 0.05 12/14/11 L54760-3 1 Silver, Total, ICP-MS 0.011 ug/L <RDL 0.01 0.05 07/31/12 L56061-1 0.5 Silver, Total, ICP-MS 0.016 ug/L <RDL 0.01 0.05 08/01/12 L56061-2 0.5 Silver, Total, ICP-MS ug/L <MDL 0.01 0.05 08/02/12 L56061-11 0.5 Silver, Total, ICP-MS 0.011 ug/L <RDL 0.01 0.05 08/02/12 L56061-3 0.5 Silver, Total, ICP-MS 0.015 ug/L <RDL 0.01 0.05 12/10/12 L56989-1 0.5 Silver, Total, ICP-MS 0.033 ug/L <RDL 0.01 0.05 12/11/12 L56989-11 0.5 Silver, Total, ICP-MS 0.0506 ug/L 0.01 0.05 12/11/12 L56989-2 0.5 Silver, Total, ICP-MS 0.038 ug/L <RDL 0.01 0.05 12/13/12 L56989-3 0.5 Silver, Total, ICP-MS 0.0524 ug/L 0.01 0.05 07/11/11 L53619-1 0.5 Zinc, Dissolved, ICP-MS 0.554 ug/L 0.1 0.5 07/12/11 L53619-13 0.5 Zinc, Dissolved, ICP-MS 0.611 ug/L 0.1 0.5 07/12/11 L53619-2 0.5 Zinc, Dissolved, ICP-MS 0.47 ug/L <RDL 0.1 0.5 07/13/11 L53619-3 0.5 Zinc, Dissolved, ICP-MS 0.546 ug/L 0.1 0.5 12/12/11 L54760-1 1 Zinc, Dissolved, ICP-MS 1.27 ug/L 0.1 0.5 12/13/11 L54760-11 1 Zinc, Dissolved, ICP-MS 0.938 ug/L 0.1 0.5 12/13/11 L54760-2 1 Zinc, Dissolved, ICP-MS 0.988 ug/L 0.1 0.5 12/14/11 L54760-3 1 Zinc, Dissolved, ICP-MS 1.15 ug/L 0.1 0.5 07/31/12 L56061-1 0.5 Zinc, Dissolved, ICP-MS 1.12 ug/L 0.1 0.5 08/01/12 L56061-2 0.5 Zinc, Dissolved, ICP-MS 0.813 ug/L 0.1 0.5 08/02/12 L56061-11 0.5 Zinc, Dissolved, ICP-MS 0.46 ug/L <RDL 0.1 0.5 08/02/12 L56061-3 0.5 Zinc, Dissolved, ICP-MS 0.575 ug/L 0.1 0.5 12/10/12 L56989-1 0.5 Zinc, Dissolved, ICP-MS 0.628 ug/L 0.1 0.5 12/11/12 L56989-11 0.5 Zinc, Dissolved, ICP-MS 0.684 ug/L 0.1 0.5 12/11/12 L56989-2 0.5 Zinc, Dissolved, ICP-MS 0.757 ug/L 0.1 0.5 12/13/12 L56989-3 0.5 Zinc, Dissolved, ICP-MS 0.814 ug/L 0.1 0.5 07/11/11 L53619-1 0.5 Zinc, Total, ICP-MS 0.867 ug/L 0.1 0.5 07/12/11 L53619-13 0.5 Zinc, Total, ICP-MS 1.33 ug/L 0.1 0.5 07/12/11 L53619-2 0.5 Zinc, Total, ICP-MS 1.28 ug/L 0.1 0.5 07/13/11 L53619-3 0.5 Zinc, Total, ICP-MS 0.938 ug/L 0.1 0.5 12/12/11 L54760-1 1 Zinc, Total, ICP-MS 1.20 ug/L 0.1 0.5 12/13/11 L54760-11 1 Zinc, Total, ICP-MS 1.13 ug/L 0.1 0.5Page 10 of 10 

## Table A-4
Complete Water Quality Monitoring Data for Station LTXQ01 NPDES Receiving Water Characterization Study

Date Sample Depth (m) Parameter Value Units Qualifier MDL RDL 12/13/11 L54760-2 1 Zinc, Total, ICP-MS 1.28 ug/L 0.1 0.5 12/14/11 L54760-3 1 Zinc, Total, ICP-MS 1.32 ug/L 0.1 0.5 07/31/12 L56061-1 0.5 Zinc, Total, ICP-MS 2.16 ug/L 0.1 0.5 08/01/12 L56061-2 0.5 Zinc, Total, ICP-MS 1.28 ug/L 0.1 0.5 08/02/12 L56061-11 0.5 Zinc, Total, ICP-MS 1.28 ug/L 0.1 0.5 08/02/12 L56061-3 0.5 Zinc, Total, ICP-MS 1.87 ug/L 0.1 0.5 12/10/12 L56989-1 0.5 Zinc, Total, ICP-MS 0.711 ug/L 0.1 0.5 12/11/12 L56989-11 0.5 Zinc, Total, ICP-MS 1.08 ug/L 0.1 0.5 12/11/12 L56989-2 0.5 Zinc, Total, ICP-MS 1.07 ug/L 0.1 0.5 12/13/12 L56989-3 0.5 Zinc, Total, ICP-MS 1.75 ug/L 0.1 0.5

Notes Depth (m) - Depth below the water's surface (in meters) from which the sample was collected.
MDL - Method detection limit; the limit of reliable detection

. RDL - Reporting detection limit; the limit of reliable quantitation (PQL). <MDL - Analyte was not detected <RDL - Analyte was detected at a concentration less than the RDL. CFU/100 ml - Colony forming units per 100 milliliters. deg C - Degrees Celcius. mg/L - Milligrams per liter. mg CaCO3/L - Milligrams of calcium carbonate per liter. PSS - Practical Salinity Scale. ug/L - Micrograms per liter. JG - Analytical result is an estimate with a probable low bias.

# Technical Memorandum

Date: April 19, 2013

To: Project File

From: Scott Mickelson, King County Marine and Sediment Assessment Group

Subject: Data Validation Report

NPDES Receiving Water Trace Metals Characterization Study

This technical memorandum summarizes the data validation review performed on Puget Sound, Elliott Bay, and Duwamish River water samples collected between July 2011 and December

2012

. These 44 samples were analyzed for total and dissolved arsenic, cadmium, chromium, copper, lead, mercury, nickel, silver, and zinc. A subset of 16 samples, collected from one of the Puget Sound sampling locations were also analyzed for total and dissolved antimony

. A second
sub set of 16 samples, collected from the Duwamish River sampling location were also analyzed
for hardness. This work was performed as one task in King County’s NPDES Receiving Water Characterization Study for its four wastewater treatment plants and four CSO storage and
treatment facilities.



## 1.0 I NTRODUCTION



### This data validation review has been based, in part, on guidance found in USEPA Contract Laboratory Program National Functional Guidelines for Inorganic Superfund Data Re view (EPA 2010), as well as the project sampling and analysis plan (King County 2010 ). Materials reviewed included Batch Reports and Analytical Quality Control (QC) Reports downloaded from the King County Laboratory Information System (LIMS) database, alo ng with data anomaly forms, all of
which are included in this memorandum as Attachment A . The QC parameters reviewed during this data validation include; holding time s , method blanks, spike blanks, matrix spikes, matrix spike duplicates, and laboratory duplicates , which are described below. The numbers and types of QC samples analyzed with each analytical sample batch (work group) are discussed in each of the following sections.

1.1 Holding Time The analytical holding time is a method

- specific timefr ame, during which sample preparation and analysis should occur to provide valid data. All samples should be analyzed within this prescribed holding time.

1

### 1.2 Method Blank A method blank is an aliquot of clean reference matrix that is generally processed through the entire analytical procedure. Analysis of the method blank is used to evaluate the levels of contamination that might be associated with the processing and analysis of samples. All
method blank results should be less than the method detection limit (MDL). Method blanks were included with all analyses.

1.3 Spike Blank A spike blank is an aliquot of the clean reference matrix used for the method blank, to which a known concentration of target analyte(s) has been added. The spiked aliquot is p rocessed through the entire analytical procedure. Analysis of the spike blank is used as an indicator of method accuracy. Spike blanks were used as part of the QC regimen for all analyses . Spike
blanks are not addressed in the National Functional Guidel ines , however, King County has
method

- defined or empirically

- derived control limits for spike blank analytes, which are shown on the attached QC reports. Spike blank results should be within these control limits.

1. 4 Matrix Spike A matrix spike is a sample aliquot fortified with a known concentration of a target analyte(s). The spiked sample is processed through the entire analytical procedure. Analysis of the matrix spike is used as an indicator of sample matrix effect on the reco very of target analyte(s). Matrix spike analysis was used as part of the QC regimen for all analyses. Matrix spike recoveries for
total and dissolved metals should be within 75 to 125% (EPA 2010).

1. 5 Matrix Spike Duplicate A matrix spike duplicate i s a second sample aliquot fortified with a known concentration of a target analyte(s). The spiked sample is processed through the entire analytical procedure. Matrix spike duplicates were analyzed as part of the QC regimen for mercury and ICP

- MS
metals

. Analysis of the matrix spike duplicate is used as an additional indicator of sample matrix effect on the recovery of target analyte(s) as well as an indicator of method precision. QC results are reported as a relative percent difference (RPD) between the sample and laboratory duplicate results. The RPD between matrix and matrix spike duplicate results should be less than 20% (EPA 2010)

.

1. 6 Laboratory Duplicate A laboratory duplicate is a second aliquot of a sample, processed concurrently and in an identical manner with the original sample. Analysis of the laboratory duplicate is used as an indicator of method precision

. The laboratory duplicate can also be used to provide
informatio n regarding the homogeneity of the sample matrix. QC results are reported as a relative percent difference ( RPD ) between the sample a nd laboratory duplicate results

. Laboratory duplicates were used as part of the QC regimen for hardness analysis. The RP D between laboratory duplicate results should be less than 20% for all hardness analysis (EPA 2010).

2

## 2.0 H ARDNESS 

## C ALCULATION



### Sixteen samples were submitted for analysis of hardness, based on the calculation method of calcium and magnesium

. Calcium and magnesium were analyzed by inductively coupled plasma mass spectrometry (ICP

- MS) according to EPA Method 200.8 (EPA 1994). Associated QC samples analyzed with each work group included method blanks, spike blanks, matrix spikes,
and laborator y duplicates.

2. 1 Holding Times All 16 samples were analyzed within the method

- specified 6

- month holding time.

2.2 Method Blanks All calcium and magnesium method blank results were less than the MDL, indicating that laboratory contamination was not an issue during sample digestion and analysis.

2. 3 Spike Blank s All calcium and magnesium spike blank results were within the empirically

- derived laboratory QC limits of 85 to 115%, ranging from 9 1 to 10 5 %, indicating acceptable overall method

accurac y.

2. 4 Matrix Spik es Calcium and magnesium recoveries in the matrix spike associated with work group WG119704 were outside the 75 to 125% laboratory QC limits recommended in National Functional
Guidelines . Background calcium and magnesium concentrations in the sample on which the matrix spike analysis was performed, however, were both greater than four times the concentrations in the spiking solution. As a result, associated sample data will not be quali fied based on matrix spike recoveries (EPA 2010). All other calcium and magnesium matrix spike recoveries were within the 75 to 125% laboratory QC limits, ranging from 75 to 1 03 %, indicating acceptable matrix

- specific method accuracy.

2.5 Laboratory Duplicates The RPDs between calcium and magnesium laboratory duplicate results were all less than the 20% QC limit recommended in National Functional Guidelines , ranging from 1 to 5%.



## 3.0 Total and Dissolved Mercury

A total of 44 samples were submitted for analysis of total and dissolved mercury by cold vapor atomic fluorescence (CVAF) according to EPA Method 1631E (EPA 2002) . Associated QC samples analyzed with each work group included three method blank s , a spike blank, a matrix spike, and matrix spike duplicate

.

3.1 Holding Time
All 44 total and dissolved mercury samples were analyzed within the method

- specified 28

- day holding time.

3

### 3 .2 Method Blanks
All total and dissolved mercury method blank results were less than the MDL, indicating that laboratory contamination was not an issue during sample digestion and analysis.

3 .3 Spike Blanks
All total and dissolved mercury spike blank results were within the empirically

- derived laboratory QC limits of 77 to 123 %, ranging from 89 to 102 %, indicati ng acceptable overall method accuracy.

3 .4 Matrix Spikes and Matrix Spike Duplicates
All total and dissolved mercury matrix spike recoveries were within the 75 to 125% laboratory QC limits recommended in National Functional Guidelines , ranging from 79 to 104 %, indicating acceptable matrix

- specific method accuracy. The RPDs between matrix spike and matrix spike duplicate results were all less than the 20% laboratory QC limit, ranging from 0 to 8%, indicating acceptable method precision.



## 4 .0 T OTAL AND 

## D ISSOLVED 

## M ETALS BY 

## ICP

- MS

A total of 44 samples were submitted for analysis of total and dissolved arsenic, cadmium, chromium, copper, lead, nickel, silver, and zinc by ICP

- MS according to EPA Method 1640 (EPA

199 7 ). A subset of 16 samples, collected f rom one of the Puget Sound sampling locations were also analyzed for total and dissolved antimony. Associated QC samples analyzed with each work group included method blanks, spike blanks, matrix spikes, and laboratory duplicates

.

4

. 1 Holding Time
All 44 samples were analyzed within the method

- specified 6

- month holding time.

4

. 2 Method Blanks Copper was detected in both method blanks associated with work group WG116287 at concentrations of 0.029 and 0.037 μg/L. Copper was also detected in the method blank associated with work group WG119016 at a concentration of 0.026 μg/L. Total copper

conce ntrations in the samples associated with these work groups were all greater than 10 times the concentrations detected in the method blanks, therefore, sample data will not be qualified
based on these method blank results. All other total and dissolved met als method blank results
were less than the MDL.

4

. 3 Spike Blank s All total and dissolved spike blank results were within the empirically

- derived laboratory QC
limits of 75 to 12 5%, ranging from 75 to 111 %, indicating acceptable overall method accuracy.

4.4 Matrix Spikes/Matrix Spike Duplicates The antimony recovery of 130% in the matrix spike duplicate associated with work group WG116281 exceeded the upper laboratory QC limit of 125%. Antimony, however, was not an analyte of interest in any of the sam ples associated with this work group. All other total and dissolved metals matrix spike recoveries were within the 75 to 125% laboratory QC limits

4

### recommended in National Functional Guidelines , ranging from 7 6 to 1 25 %, indicating acceptable matrix

- specifi c method accuracy. The RPDs between matrix spike and matrix spike duplicate results were all less than the 20% laboratory QC limit, ranging from 0 to 15 %, indicating acceptable method precision.



## 5 .0 D ATA 

## U SABILITY



### As a general data reporting format, total and dissolved metals sample results that are reported
as “<MDL” should be assi gned a “U” flag in all cases and considered undetected. Total and
dissolved metals sample results that are reported as “<RDL” should be assigned a “J” flag in all

cases an d considered estimated with an unknown bias. All other total and dissolved metals sample results, as well as calculated hardness samples results, in this dataset may be used as reported, without qualification

.

5

## 6 .0 R EFERENCES



### EPA 1994. Determination of Trace Elements in Waters and Wastes by Inductively Coupled
Plasma

– Mass Spectrometry

. Method 200.8, Revision 5.4 . United States Environmental Protection Agency, Office of Research and Development. Cincinnati, Ohio.

EPA 1997. Method 16 40: Determination of Trace Elements in Water by Preconcentration and Inductively Coupled Plasma

– Mass Spect ro metry . United States Environmental Protection Agency Office of Water. Washington, DC.

EPA 2002. Method 1631, Revision E: Mercury in Water by Oxidation, Purge and Trap, and Cold Vapor Atomic Fluorescence

. EPA

- 821

- R

- 02

- 019. United States Environmental Protection Agency, Office of Water. Washington, D.C. August 2002.

EPA 2010. USEPA Contract Laboratory Program National Functional Guidelines for Superfund Inorganic Data Review. OSWER 9240.1

- 51, USEPA

- 540

- R

- 10

- 011. United States Environmental Protection Agency. Washington, D.C. January 2010.

King County 2010

. Receiving Water Characterization Study, King County NPDES Monitoring Program, Fi nal Sampling and Analysis Plan and Quality Assurance Project Plan . King County Department of Natural Resources and Parks. Seattle, Washington.

• • •

Should you have questions regarding any of the information contained in this data validation memorandum, please don’t hesitate to contact the undersigned

.
Sincerely,

Scott Mickelson Senior Water Quality Project Manager King County Marine and Sediment As sessment Group

206

- 296

- 8247 scott.mickelson@kingcounty.gov

6

# A TTACHMENT 

# A

L IMS B ATCH AND 

## QC R EPORTSPage 1 of 19 

### WG117399

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L53619-1 421162-300 NPDES RW Charact. Study MTHARD-ICPMS FRESH WTR 07/11/11 09/15/11 09/16/11

L53619-1 421162-300 NPDES RW Charact. Study MTICPMS FRESH WTR 07/11/11 09/15/11 09/15/11

L53619-2 421162-300 NPDES RW Charact. Study MTHARD-ICPMS FRESH WTR 07/12/11 09/15/11 09/16/11

L53619-2 421162-300 NPDES RW Charact. Study MTICPMS FRESH WTR 07/12/11 09/15/11 09/15/11

L53619-3 421162-300 NPDES RW Charact. Study MTHARD-ICPMS FRESH WTR 07/13/11 09/15/11 09/16/11

L53619-3 421162-300 NPDES RW Charact. Study MTICPMS FRESH WTR 07/13/11 09/15/11 09/15/11

L53619-13 421162-300 NPDES RW Charact. Study MTHARD-ICPMS FRESH WTR 07/12/11 09/15/11 09/16/11 FREP@L53619-2

L53619-13 421162-300 NPDES RW Charact. Study MTICPMS FRESH WTR 07/12/11 09/15/11 09/15/11 FREP@L53619-2

WG117399-1 MB MTHARD-ICPMS BLANK WTR 09/15/11 09/16/11 METHOD BLANK

WG117399-1 MB MTICPMS BLANK WTR 09/15/11 09/15/11 METHOD BLANK

WG117399-2 SB MTHARD-ICPMS BLANK WTR 09/15/11 09/16/11 WG117399-1 MS-20

WG117399-2 SB MTICPMS BLANK WTR 09/15/11 09/15/11 WG117399-1 MS-20

WG117399-3 LD MTHARD-ICPMS FRESH WTR 09/15/11 09/16/11 L53619-13 RPD-LIQ

WG117399-3 LD MTICPMS FRESH WTR 09/15/11 09/15/11 L53619-13 RPD-LIQ

WG117399-4 MS MTHARD-ICPMS FRESH WTR 09/15/11 09/16/11 L53619-13 MS-20

WG117399-4 MS MTICPMS FRESH WTR 09/15/11 09/15/11 L53619-13 MS-20



### WG119704

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L54760-1 421162-300 NPDES RW Charact. Study MTHARD-ICPMS FRESH WTR 12/12/11 02/09/12 02/10/12

L54760-1 421162-300 NPDES RW Charact. Study MTICPMS FRESH WTR 12/12/11 02/09/12 02/10/12

L54760-2 421162-300 NPDES RW Charact. Study MTHARD-ICPMS FRESH WTR 12/13/11 02/09/12 02/10/12

L54760-2 421162-300 NPDES RW Charact. Study MTICPMS FRESH WTR 12/13/11 02/09/12 02/10/12

L54760-3 421162-300 NPDES RW Charact. Study MTHARD-ICPMS FRESH WTR 12/14/11 02/09/12 02/10/12

L54760-3 421162-300 NPDES RW Charact. Study MTICPMS FRESH WTR 12/14/11 02/09/12 02/10/12

L54760-11 421162-300 NPDES RW Charact. Study MTHARD-ICPMS FRESH WTR 12/13/11 02/09/12 02/10/12 FREP@L54760-2

L54760-11 421162-300 NPDES RW Charact. Study MTICPMS FRESH WTR 12/13/11 02/09/12 02/10/12 FREP@L54760-2

WG119704-1 MB MTHARD-ICPMS BLANK WTR 02/09/12 02/10/12 METHOD BLANK

WG119704-1 MB MTICPMS BLANK WTR 02/09/12 02/10/12 METHOD BLANK

WG119704-2 SB MTHARD-ICPMS BLANK WTR 02/09/12 02/10/12 WG119704-1 MS-20

WG119704-2 SB MTICPMS BLANK WTR 02/09/12 02/10/12 WG119704-1 MS-20

WG119704-3 LD MTHARD-ICPMS FRESH WTR 02/09/12 02/10/12 L54760-11 RPD-LIQ

WG119704-3 LD MTICPMS FRESH WTR 02/09/12 02/10/12 L54760-11 RPD-LIQ

WG119704-4 MS MTHARD-ICPMS FRESH WTR 02/09/12 02/10/12 L54760-11 MS-20

WG119704-4 MS MTICPMS FRESH WTR 02/09/12 02/10/12 L54760-11 MS-20 

### LIMSView Batch Report for NPDES Receiving Water Characterization Study - Data Validation for MetalsPage 2 of 19 

### LIMSView Batch Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

WG123247

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L56061-1 421162-300 NPDES RW Charact. Study MTHARD-ICPMS FRESH WTR 07/31/12 09/25/12 09/28/12

L56061-1 421162-300 NPDES RW Charact. Study MTICPMS FRESH WTR 07/31/12 09/25/12 09/25/12

L56061-2 421162-300 NPDES RW Charact. Study MTHARD-ICPMS FRESH WTR 08/01/12 09/25/12 09/28/12

L56061-2 421162-300 NPDES RW Charact. Study MTICPMS FRESH WTR 08/01/12 09/25/12 09/25/12

L56061-3 421162-300 NPDES RW Charact. Study MTHARD-ICPMS FRESH WTR 08/02/12 09/25/12 09/28/12

L56061-3 421162-300 NPDES RW Charact. Study MTICPMS FRESH WTR 08/02/12 09/25/12 09/25/12

L56061-11 421162-300 NPDES RW Charact. Study MTHARD-ICPMS FRESH WTR 08/02/12 09/25/12 09/28/12 FREP@L56061-3

L56061-11 421162-300 NPDES RW Charact. Study MTICPMS FRESH WTR 08/02/12 09/25/12 09/25/12 FREP@L56061-3

L56320-2 421422-CHSW-M SWD Cedar Hills SW Mth MTHARD-ICPMS FRESH WTR 09/19/12 09/25/12 09/28/12

L56320-2 421422-CHSW-M SWD Cedar Hills SW Mth MTICPMS FRESH WTR 09/19/12 09/25/12 09/25/12

L56460-8 421196-130 Roads Groundwater MTICPMS GRND WTR 09/19/12 09/25/12 09/25/12

L56460-9 421196-130 Roads Groundwater MTICPMS GRND WTR 09/19/12 09/25/12 09/25/12

L56460-10 421196-130 Roads Groundwater MTICPMS GRND WTR 09/19/12 09/25/12 09/25/12

L56460-11 421196-130 Roads Groundwater MTICPMS GRND WTR 09/19/12 09/25/12 09/25/12

L56460-12 421196-130 Roads Groundwater MTICPMS GRND WTR 09/20/12 09/25/12 09/25/12

L56460-13 421196-130 Roads Groundwater MTICPMS GRND WTR 09/20/12 09/25/12 09/25/12

L56460-14 421196-130 Roads Groundwater MTICPMS GRND WTR 09/20/12 09/25/12 09/25/12

L56460-15 421196-130 Roads Groundwater MTICPMS GRND WTR 09/20/12 09/25/12 09/25/12

L56494-1 421422-CFSW SWD Cedar Falls SW Qtr MTHARD-ICPMS FRESH WTR 09/19/12 09/25/12 09/28/12

L56494-1 421422-CFSW SWD Cedar Falls SW Qtr MTICPMS FRESH WTR 09/19/12 09/25/12 09/25/12

WG123247-1 MB MTHARD-ICPMS BLANK WTR 09/25/12 09/28/12 METHOD BLANK

WG123247-1 MB MTICPMS BLANK WTR 09/25/12 09/25/12 METHOD BLANK

WG123247-2 SB MTHARD-ICPMS BLANK WTR 09/25/12 09/28/12 WG123247-1 MS-20

WG123247-2 SB MTICPMS BLANK WTR 09/25/12 09/25/12 WG123247-1 MS-20

WG123247-3 LD MTHARD-ICPMS FRESH WTR 09/25/12 09/28/12 L56320-2 RPD-LIQ

WG123247-3 LD MTICPMS FRESH WTR 09/25/12 09/25/12 L56320-2 RPD-LIQ

WG123247-4 MS MTHARD-ICPMS FRESH WTR 09/25/12 09/28/12 L56320-2 MS-20

WG123247-4 MS MTICPMS FRESH WTR 09/25/12 09/25/12 L56320-2 MS-20



### WG125075

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L56989-1 421162-300 NPDES RW Charact. Study MTHARD-ICPMS FRESH WTR 12/10/12 01/23/13 01/24/13

L56989-1 421162-300 NPDES RW Charact. Study MTICPMS FRESH WTR 12/10/12 01/23/13 01/24/13

L56989-2 421162-300 NPDES RW Charact. Study MTHARD-ICPMS FRESH WTR 12/11/12 01/23/13 01/24/13

L56989-2 421162-300 NPDES RW Charact. Study MTICPMS FRESH WTR 12/11/12 01/23/13 01/24/13

L56989-3 421162-300 NPDES RW Charact. Study MTHARD-ICPMS FRESH WTR 12/13/12 01/23/13 01/24/13

L56989-3 421162-300 NPDES RW Charact. Study MTICPMS FRESH WTR 12/13/12 01/23/13 01/24/13Page 3 of 19 

### LIMSView Batch Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

L56989-11 421162-300 NPDES RW Charact. Study MTHARD-ICPMS FRESH WTR 12/11/12 01/23/13 01/24/13 FREP@L56989-2

L56989-11 421162-300 NPDES RW Charact. Study MTICPMS FRESH WTR 12/11/12 01/23/13 01/24/13 FREP@L56989-2

WG125075-1 MB MTHARD-ICPMS BLANK WTR 01/23/13 01/24/13 METHOD BLANK

WG125075-1 MB MTICPMS BLANK WTR 01/23/13 01/24/13 METHOD BLANK

WG125075-2 SB MTHARD-ICPMS BLANK WTR 01/23/13 01/24/13 WG125075-1 MS-20 SPIKE BLANK

WG125075-2 SB MTICPMS BLANK WTR 01/23/13 01/24/13 WG125075-1 MS-20 SPIKE BLANK

WG125075-3 LD MTHARD-ICPMS FRESH WTR 01/23/13 01/24/13 L56989-1 RPD-LIQ LAB DUPLICATE

WG125075-3 LD MTICPMS FRESH WTR 01/23/13 01/24/13 L56989-1 RPD-LIQ LAB DUPLICATE

WG125075-4 MS MTHARD-ICPMS FRESH WTR 01/23/13 01/24/13 L56989-1 MS-20 MATRIX SPIKE

WG125075-4 MS MTICPMS FRESH WTR 01/23/13 01/24/13 L56989-1 MS-20 MATRIX SPIKE



### WG116464

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L53592-1 421936 Carnation TP NPDES Mon. MTHG-CVAF EFFLUENT 07/12/11 07/25/11 07/26/11

L53592-7 421936 Carnation TP NPDES Mon. MTHG-CVAF BLANK WTR 07/13/11 07/25/11 07/26/11

L53593-1 421936 Carnation TP NPDES Mon. MTHG-CVAF BLANK WTR 07/07/11 07/25/11 07/26/11 FLDBLK @ L53592-1

L53593-2 421936 Carnation TP NPDES Mon. MTHG-CVAF BLANK WTR 07/07/11 07/25/11 07/26/11

L53619-1 421162-300 NPDES RW Charact. Study MTHG-CVAF FRESH WTR 07/11/11 07/25/11 07/26/11

L53619-2 421162-300 NPDES RW Charact. Study MTHG-CVAF FRESH WTR 07/12/11 07/25/11 07/26/11

L53619-3 421162-300 NPDES RW Charact. Study MTHG-CVAF FRESH WTR 07/13/11 07/25/11 07/26/11

L53619-4 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 07/11/11 07/25/11 07/26/11 ATMOBLANK Day 1

L53619-5 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 07/12/11 07/25/11 07/26/11 ATMOBLANK Day 2

L53619-6 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 07/13/11 07/25/11 07/26/11 ATMOBLANK Day 3

L53619-7 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 07/11/11 07/25/11 07/26/11 CRBOYBLANK Day 1

L53619-8 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 07/11/11 07/25/11 07/26/11 TRIPBLANK Day 1

L53619-9 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 07/11/11 07/25/11 07/26/11 BAILERBLANK Day 1

L53619-13 421162-300 NPDES RW Charact. Study MTHG-CVAF FRESH WTR 07/12/11 07/25/11 07/26/11 FREP@L53619-2

L53626-1 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 07/14/11 07/25/11 07/26/11

L53626-2 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 07/14/11 07/25/11 07/26/11

L53626-3 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 07/14/11 07/25/11 07/26/11

L53626-4 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 07/14/11 07/25/11 07/26/11

L53626-5 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 07/14/11 07/25/11 07/26/11

L53626-6 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 07/14/11 07/25/11 07/26/11

WG116464-1 MB MTHG-CVAF BLANK WTR 07/25/11 07/26/11 METHOD BLANK#1

WG116464-2 MB MTHG-CVAF BLANK WTR 07/25/11 07/26/11 METHOD BLANK#2

WG116464-3 MB MTHG-CVAF BLANK WTR 07/25/11 07/26/11 METHOD BLANK#3

WG116464-4 SB MTHG-CVAF BLANK WTR 07/25/11 07/26/11 WG116464-1 AF-SB

WG116464-5 MS MTHG-CVAF EFFLUENT 07/25/11 07/26/11 L53592-1 AF-MS

WG116464-6 MSD MTHG-CVAF EFFLUENT 07/25/11 07/26/11 WG116464-5 L53592-1 AF-MSD

WG116464-7 MS MTHG-CVAF FRESH WTR 07/25/11 07/26/11 L53619-13 AF-MS

WG116464-8 MSD MTHG-CVAF FRESH WTR 07/25/11 07/26/11 WG116464-7 L53619-13 AF-MSDPage 4 of 19 

### LIMSView Batch Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

WG116695

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L53626-7 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 07/14/11 08/09/11 08/10/11

L53626-8 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 07/14/11 08/09/11 08/10/11

L53626-9 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 07/14/11 08/09/11 08/10/11 FREP@L53626-10

L53626-10 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 07/14/11 08/09/11 08/10/11

L53626-11 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 07/14/11 08/09/11 08/10/11 Equipment Blank- not field Blank

L53626-12 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 07/14/11 08/09/11 08/10/11 ATM BLANK @KSBP01

L53626-13 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 07/14/11 08/09/11 08/10/11 ATM BLANK @LTED04

L53626-14 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 07/14/11 08/09/11 08/10/11 ATM BLANK @LSNT01

L53626-15 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 07/14/11 08/09/11 08/10/11 Time of first sample recorded

L53626-17 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 07/14/11 08/09/11 08/10/11 Carboy Blank @ Lab

WG116695-1 MB MTHG-CVAF BLANK WTR 08/09/11 08/10/11 METHOD BLANK

WG116695-2 MB MTHG-CVAF BLANK WTR 08/09/11 08/10/11 METHOD BLANK

WG116695-3 MB MTHG-CVAF BLANK WTR 08/09/11 08/10/11 METHOD BLANK

WG116695-4 SB MTHG-CVAF BLANK WTR 08/09/11 08/10/11 WG116695-1 AF-SB

WG116695-5 MS MTHG-CVAF SALT WTR 08/09/11 08/10/11 L53626-7 AF-MS

WG116695-6 MSD MTHG-CVAF SALT WTR 08/09/11 08/10/11 WG116695-5 L53626-7 AF-MSD



### WG119056

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L54760-1 421162-300 NPDES RW Charact. Study MTHG-CVAF FRESH WTR 12/12/11 12/19/11 12/20/11

L54760-2 421162-300 NPDES RW Charact. Study MTHG-CVAF FRESH WTR 12/13/11 12/19/11 12/20/11

L54760-5 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 12/13/11 12/19/11 12/20/11 ATMOBLK- Day 2

L54760-6 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 12/14/11 12/19/11 12/20/11 ATMOBLK- Day 3

L54760-7 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 12/12/11 12/19/11 12/20/11 CRBOYBLK

L54760-8 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 12/12/11 12/19/11 12/20/11 TRPBLK

L54760-9 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 12/12/11 12/19/11 12/20/11 BAILERBLK

L54760-11 421162-300 NPDES RW Charact. Study MTHG-CVAF FRESH WTR 12/13/11 12/19/11 12/20/11 FREP@L54760-2

L54765-1 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 12/14/11 12/19/11 12/20/11

L54765-2 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 12/14/11 12/19/11 12/20/11

L54765-3 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 12/14/11 12/19/11 12/20/11

L54765-4 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 12/14/11 12/19/11 12/20/11

L54765-5 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 12/14/11 12/19/11 12/20/11

L54765-6 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 12/14/11 12/19/11 12/20/11

L54782-2 423258-500-1 Brightwater Reclaimed WQ MTHG-CVAF OTHR WTR 12/12/11 12/19/11 12/20/11

L54783-2 423258-500-1 Brightwater Reclaimed WQ MTHG-CVAF OTHR WTR 12/13/11 12/19/11 12/20/11

L54784-2 423258-500-1 Brightwater Reclaimed WQ MTHG-CVAF OTHR WTR 12/14/11 12/19/11 12/20/11

WG119056-1 MB MTHG-CVAF BLANK WTR 12/19/11 12/20/11 METHOD BLANK#1Page 5 of 19 

### LIMSView Batch Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

WG119056-2 MB MTHG-CVAF BLANK WTR 12/19/11 12/20/11 METHOD BLANK#2

WG119056-3 MB MTHG-CVAF BLANK WTR 12/19/11 12/20/11 METHOD BLANK#3

WG119056-4 SB MTHG-CVAF BLANK WTR 12/19/11 12/20/11 WG119056-1 AF-SB

WG119056-5 MS MTHG-CVAF OTHR WTR 12/19/11 12/20/11 L54782-2 AF-MS

WG119056-6 MSD MTHG-CVAF OTHR WTR 12/19/11 12/20/11 WG119056-5 L54782-2 AF-MSD

WG119056-7 MS MTHG-CVAF FRESH WTR 12/19/11 12/20/11 L54760-11 AF-MS

WG119056-8 MSD MTHG-CVAF FRESH WTR 12/19/11 12/20/11 WG119056-7 L54760-11 AF-MSD



### WG119177

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L54760-3 421162-300 NPDES RW Charact. Study MTHG-CVAF FRESH WTR 12/14/11 12/27/11 12/28/11

L54760-4 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 12/12/11 12/27/11 12/28/11 ATMOBLK- Day 1

L54765-7 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 12/14/11 12/27/11 12/28/11

L54765-8 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 12/14/11 12/27/11 12/28/11

L54765-9 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 12/14/11 12/27/11 12/28/11 FREP@L54765-10

L54765-10 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 12/14/11 12/27/11 12/28/11

L54765-11 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 12/14/11 12/27/11 12/28/11 Field Blank @ LTDE04

L54765-12 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 12/14/11 12/27/11 12/28/11 ATM BLANK @KSBP01

L54765-13 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 12/14/11 12/27/11 12/28/11 ATM BLANK @LTED04

L54765-14 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 12/14/11 12/27/11 12/28/11 ATM BLANK @LSNT01

L54765-15 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 12/14/11 12/27/11 12/28/11 Time of first sample recorded

L54765-17 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 12/14/11 12/27/11 12/28/11 Carboy Blank @ LTED04

WG119177-1 MB MTHG-CVAF BLANK WTR 12/27/11 12/28/11 METHOD BLANK#1

WG119177-2 MB MTHG-CVAF BLANK WTR 12/27/11 12/28/11 METHOD BLANK#2

WG119177-3 MB MTHG-CVAF BLANK WTR 12/27/11 12/28/11 METHOD BLANK#3

WG119177-4 SB MTHG-CVAF BLANK WTR 12/27/11 12/28/11 WG119177-1 AF-SB

WG119177-5 MS MTHG-CVAF FRESH WTR 12/27/11 12/28/11 L54760-3 AF-MS

WG119177-6 MSD MTHG-CVAF FRESH WTR 12/27/11 12/28/11 WG119177-5 L54760-3 AF-MSD

WG119177-7 MS MTHG-CVAF SALT WTR 12/27/11 12/28/11 L54765-7 AF-MS

WG119177-8 MSD MTHG-CVAF SALT WTR 12/27/11 12/28/11 WG119177-7 L54765-7 AF-MSD



### WG122560

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L56061-1 421162-300 NPDES RW Charact. Study MTHG-CVAF FRESH WTR 07/31/12 08/15/12 08/16/12

L56061-2 421162-300 NPDES RW Charact. Study MTHG-CVAF FRESH WTR 08/01/12 08/15/12 08/16/12

L56061-3 421162-300 NPDES RW Charact. Study MTHG-CVAF FRESH WTR 08/02/12 08/15/12 08/16/12

L56061-4 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 07/31/12 08/15/12 08/16/12 ATMOBLK Day 1

L56061-5 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 08/01/12 08/15/12 08/16/12 ATMOBLK Day 2

L56061-6 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 08/02/12 08/15/12 08/16/12 ATMOBLK Day 3Page 6 of 19 

### LIMSView Batch Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

L56061-7 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 07/31/12 08/15/12 08/16/12 CRBYBLK Day 1

L56061-8 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 07/31/12 08/15/12 08/16/12 TRPBLK Day 1

L56061-9 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 07/31/12 08/15/12 08/16/12 BAILERBLK Day 1

L56061-11 421162-300 NPDES RW Charact. Study MTHG-CVAF FRESH WTR 08/02/12 08/21/12 08/22/12 FREP@L56061-3

WG122560-1 MB MTHG-CVAF BLANK WTR 08/15/12 08/16/12 METHOD BLANK#1

WG122560-2 MB MTHG-CVAF BLANK WTR 08/15/12 08/16/12 METHOD BLANK#2

WG122560-3 MB MTHG-CVAF BLANK WTR 08/15/12 08/16/12 METHOD BLANK#3

WG122560-4 SB MTHG-CVAF BLANK WTR 08/15/12 08/16/12 WG122560-1 AF-SB

WG122560-5 MS MTHG-CVAF FRESH WTR 08/15/12 08/16/12 L56061-1 AF-MS

WG122560-6 MSD MTHG-CVAF FRESH WTR 08/15/12 08/16/12 WG122560-5 L56061-1 AF-MSD



### WG122713

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L56062-1 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 07/30/12 08/22/12 08/23/12

L56062-2 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 07/30/12 08/22/12 08/23/12

L56062-3 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 07/30/12 08/22/12 08/23/12

L56062-4 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 07/30/12 08/22/12 08/23/12

L56062-5 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 07/30/12 08/22/12 08/23/12

L56062-6 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 07/30/12 08/22/12 08/23/12

L56062-7 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 07/30/12 08/22/12 08/23/12

L56062-8 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 07/30/12 08/22/12 08/23/12

L56062-9 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 07/30/12 08/22/12 08/23/12 FREP@L56062-10

L56062-10 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 07/30/12 08/22/12 08/23/12

WG122713-1 MB MTHG-CVAF BLANK WTR 08/22/12 08/23/12 METHOD BLANK

WG122713-2 MB MTHG-CVAF BLANK WTR 08/22/12 08/23/12 METHOD BLANK

WG122713-3 MB MTHG-CVAF BLANK WTR 08/22/12 08/23/12 METHOD BLANK

WG122713-4 SB MTHG-CVAF BLANK WTR 08/22/12 08/23/12 WG122713-1 AF-SB

WG122713-5 MS MTHG-CVAF SALT WTR 08/22/12 08/23/12 L56062-2 AF-MS

WG122713-6 MSD MTHG-CVAF SALT WTR 08/22/12 08/23/12 WG122713-5 L56062-2 AF-MSD



### WG122844

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L56062-11 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 07/30/12 08/29/12 08/30/12 Field Blank @ LTDE04

L56062-12 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 07/30/12 08/29/12 08/30/12 ATM BLANK @KSBP01

L56062-13 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 07/30/12 08/29/12 08/30/12 ATM BLANK @LTED04

L56062-14 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 07/30/12 08/29/12 08/30/12 ATM BLANK @LSNT01

L56062-15 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 07/30/12 08/29/12 08/30/12 Time of first sample recorded

L56062-17 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 07/30/12 08/29/12 08/30/12 Carboy Blank @ LTED04

L56298-1 421186B RTP INPLNT 3 DAY INT MTHG-CVAF BLANK WTR 08/20/12 08/29/12 08/30/12 FLDBLK (for L56299, 56300, 56301)Page 7 of 19 

### LIMSView Batch Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

L56298-2 421186B RTP INPLNT 3 DAY INT MTHG-CVAF BLANK WTR 08/20/12 08/29/12 08/30/12

L56299-7 421186B RTP INPLNT 3 DAY INT MTHG-CVAF EFFLUENT 08/20/12 08/29/12 08/30/12

L56299-10 421186B RTP INPLNT 3 DAY INT MTHG-CVAF BLANK WTR 08/20/12 08/29/12 08/30/12

L56300-7 421186B RTP INPLNT 3 DAY INT MTHG-CVAF EFFLUENT 08/21/12 08/29/12 08/30/12

L56300-10 421186B RTP INPLNT 3 DAY INT MTHG-CVAF BLANK WTR 08/21/12 08/29/12 08/30/12

L56301-7 421186B RTP INPLNT 3 DAY INT MTHG-CVAF EFFLUENT 08/22/12 08/29/12 08/30/12

L56301-10 421186B RTP INPLNT 3 DAY INT MTHG-CVAF BLANK WTR 08/22/12 08/29/12 08/30/12

WG122844-1 MB MTHG-CVAF BLANK WTR 08/29/12 08/30/12 METHOD BLANK

WG122844-2 MB MTHG-CVAF BLANK WTR 08/29/12 08/30/12 METHOD BLANK

WG122844-3 MB MTHG-CVAF BLANK WTR 08/29/12 08/30/12 METHOD BLANK

WG122844-4 SB MTHG-CVAF BLANK WTR 08/29/12 08/30/12 WG122844-1 AF-SB

WG122844-5 MS MTHG-CVAF EFFLUENT 08/29/12 08/30/12 L56299-7 AF-MS

WG122844-6 MSD MTHG-CVAF EFFLUENT 08/29/12 08/30/12 WG122844-5 L56299-7 AF-MSD

WG122844-7 MS MTHG-CVAF EFFLUENT 08/29/12 08/30/12 L56301-7 AF-MS

WG122844-8 MSD MTHG-CVAF EFFLUENT 08/29/12 08/30/12 WG122844-7 L56301-7 AF-MSD



### WG125309

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L56990-1 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 12/12/12 02/06/13 02/07/13

L56990-2 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 12/12/12 02/06/13 02/07/13

L56990-3 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 12/12/12 02/06/13 02/07/13

L56990-4 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 12/12/12 02/06/13 02/07/13

L56990-5 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 12/12/12 02/06/13 02/07/13

L56990-6 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 12/12/12 02/06/13 02/07/13

L56990-7 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 12/12/12 02/06/13 02/07/13

L56990-8 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 12/12/12 02/06/13 02/07/13

L56990-9 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 12/12/12 02/06/13 02/07/13 FREP@L56990-10

L56990-10 421162-300 NPDES RW Charact. Study MTHG-CVAF SALT WTR 12/12/12 02/06/13 02/07/13

L56990-11 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 12/12/12 02/06/13 02/07/13 Field Blank @ KSBP01

L56990-12 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 12/12/12 02/06/13 02/07/13 ATM BLANK @KSBP01

L56990-13 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 12/12/12 02/06/13 02/07/13 ATM BLANK @LTED04

L56990-14 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 12/12/12 02/06/13 02/07/13 ATM BLANK @LSNT01

L56990-15 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 12/12/12 02/06/13 02/07/13 Time of first sample recorded

L56990-17 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 12/12/12 02/06/13 02/07/13 Carboy Blank @ KSBP01

L57200-5 421185 WP INPLANT 3 Day INT MTHG-CVAF BLANK WTR 01/10/13 02/06/13 02/07/13

L57201-5 421185 WP INPLANT 3 Day INT MTHG-CVAF BLANK WTR 01/10/13 02/06/13 02/07/13

L57227-7 421185 WP INPLANT 3 Day INT MTHG-CVAF BLANK WTR 01/10/13 02/06/13 02/07/13

WG125309-1 MB MTHG-CVAF BLANK WTR 02/06/13 02/07/13 METHOD BLANK

WG125309-2 MB MTHG-CVAF BLANK WTR 02/06/13 02/07/13 METHOD BLANK

WG125309-3 MB MTHG-CVAF BLANK WTR 02/06/13 02/07/13 METHOD BLANKPage 8 of 19 

### LIMSView Batch Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

WG125309-4 SB MTHG-CVAF BLANK WTR 02/06/13 02/07/13 WG125309-1 AF-SB

WG125309-5 MS MTHG-CVAF SALT WTR 02/06/13 02/07/13 L56990-1 AF-MS

WG125309-6 MSD MTHG-CVAF SALT WTR 02/06/13 02/07/13 WG125309-5 L56990-1 AF-MSD

WG125309-7 MS MTHG-CVAF SALT WTR 02/06/13 02/07/13 L56990-10 AF-MS

WG125309-8 MSD MTHG-CVAF SALT WTR 02/06/13 02/07/13 WG125309-7 L56990-10 AF-MSD



### WG125324

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L56989-1 421162-300 NPDES RW Charact. Study MTHG-CVAF FRESH WTR 12/10/12 02/07/13 02/08/13

L56989-2 421162-300 NPDES RW Charact. Study MTHG-CVAF FRESH WTR 12/11/12 02/07/13 02/08/13

L56989-3 421162-300 NPDES RW Charact. Study MTHG-CVAF FRESH WTR 12/13/12 02/07/13 02/08/13

L56989-4 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 12/10/12 02/07/13 02/08/13 ATMOBLK Day 1

L56989-5 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 12/11/12 02/07/13 02/08/13 ATMOBLK Day 2

L56989-6 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 12/13/12 02/07/13 02/08/13 ATMOBLK Day 3

L56989-7 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 12/10/12 02/07/13 02/08/13 CRBOYBLK

L56989-8 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 12/10/12 02/07/13 02/08/13 TRPBLK

L56989-9 421162-300 NPDES RW Charact. Study MTHG-CVAF BLANK WTR 12/10/12 02/07/13 02/08/13 BAILERBLK

L56989-11 421162-300 NPDES RW Charact. Study MTHG-CVAF FRESH WTR 12/11/12 02/07/13 02/08/13 FREP@L56989-2

WG125324-1 MB MTHG-CVAF BLANK WTR 02/07/13 02/08/13 METHOD BLANK

WG125324-2 MB MTHG-CVAF BLANK WTR 02/07/13 02/08/13 METHOD BLANK

WG125324-3 MB MTHG-CVAF BLANK WTR 02/07/13 02/08/13 METHOD BLANK

WG125324-4 SB MTHG-CVAF BLANK WTR 02/07/13 02/08/13 WG125324-1 AF-SB

WG125324-5 MS MTHG-CVAF FRESH WTR 02/07/13 02/08/13 L56989-1 AF-MS

WG125324-6 MSD MTHG-CVAF FRESH WTR 02/07/13 02/08/13 WG125324-5 L56989-1 AF-MSD



### WG116496

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L53619-1 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS FRESH WTR 07/11/11 07/28/11 07/29/11

L53619-2 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS FRESH WTR 07/12/11 07/28/11 07/29/11

L53619-3 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS FRESH WTR 07/13/11 07/28/11 07/29/11

L53619-12 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS FILTER WTR 07/11/11 07/28/11 07/29/11 FFB- Metals

L53619-13 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS FRESH WTR 07/12/11 07/28/11 07/29/11 FREP@L53619-2

L53626-1 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 07/14/11 07/28/11 07/29/11

L53626-2 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 07/14/11 07/28/11 07/29/11

L53626-3 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 07/14/11 07/28/11 07/29/11

L53626-4 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 07/14/11 07/28/11 07/29/11

L53626-5 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 07/14/11 07/28/11 07/29/11

L53626-6 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 07/14/11 07/28/11 07/29/11

L53626-7 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 07/14/11 07/28/11 07/29/11Page 9 of 19 

### LIMSView Batch Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

L53626-8 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 07/14/11 07/28/11 07/29/11

L53626-9 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 07/14/11 07/28/11 07/29/11 FREP@L53626-10

L53626-10 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 07/14/11 07/28/11 07/29/11

L53626-16 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS FILTER WTR 07/14/11 07/28/11 07/29/11 FFB @ KSBP01

WG116496-1 MB MTHG-CVAF-DISS BLANK WTR 07/28/11 07/29/11 METHOD BLANK#1

WG116496-2 MB MTHG-CVAF-DISS BLANK WTR 07/28/11 07/29/11 METHOD BLANK#2

WG116496-3 MB MTHG-CVAF-DISS BLANK WTR 07/28/11 07/29/11 METHOD BLANK#3

WG116496-4 SB MTHG-CVAF-DISS BLANK WTR 07/28/11 07/29/11 WG116496-1 AF-SB

WG116496-5 MS MTHG-CVAF-DISS FRESH WTR 07/28/11 07/29/11 L53619-1 AF-MS

WG116496-6 MSD MTHG-CVAF-DISS FRESH WTR 07/28/11 07/29/11 WG116496-5 L53619-1 AF-MSD

WG116496-7 MS MTHG-CVAF-DISS SALT WTR 07/28/11 07/29/11 L53626-10 AF-MS

WG116496-8 MSD MTHG-CVAF-DISS SALT WTR 07/28/11 07/29/11 WG116496-7 L53626-10 AF-MSD



### WG119081

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L54760-1 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS FRESH WTR 12/12/11 12/20/11 12/21/11

L54760-2 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS FRESH WTR 12/13/11 12/20/11 12/21/11

L54760-3 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS FRESH WTR 12/14/11 12/20/11 12/21/11

L54760-10 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS FILTER WTR 12/12/11 12/20/11 12/21/11 FFB- metals

L54760-11 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS FRESH WTR 12/13/11 12/20/11 12/21/11 FREP@L54760-2

L54765-1 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 12/14/11 12/20/11 12/21/11

L54765-2 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 12/14/11 12/20/11 12/21/11

L54765-3 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 12/14/11 12/20/11 12/21/11

L54765-4 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 12/14/11 12/20/11 12/21/11

L54765-5 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 12/14/11 12/20/11 12/21/11

L54765-6 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 12/14/11 12/20/11 12/21/11

L54765-7 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 12/14/11 12/20/11 12/21/11

L54765-8 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 12/14/11 12/20/11 12/21/11

L54765-9 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 12/14/11 12/20/11 12/21/11 FREP@L54765-10

L54765-10 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 12/14/11 12/20/11 12/21/11

L54765-16 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS FILTER WTR 12/14/11 12/20/11 12/21/11 FFB @ LTED04

WG119081-1 MB MTHG-CVAF-DISS BLANK WTR 12/20/11 12/21/11 METHOD BLANK

WG119081-2 MB MTHG-CVAF-DISS BLANK WTR 12/20/11 12/21/11 METHOD BLANK

WG119081-3 MB MTHG-CVAF-DISS BLANK WTR 12/20/11 12/21/11 METHOD BLANK

WG119081-4 SB MTHG-CVAF-DISS BLANK WTR 12/20/11 12/21/11 WG119081-1 AF-SB

WG119081-5 MS MTHG-CVAF-DISS FRESH WTR 12/20/11 12/21/11 L54760-1 AF-MS

WG119081-6 MSD MTHG-CVAF-DISS FRESH WTR 12/20/11 12/21/11 WG119081-5 L54760-1 AF-MSD

WG119081-7 MS MTHG-CVAF-DISS SALT WTR 12/20/11 12/21/11 L54765-10 AF-MS

WG119081-8 MSD MTHG-CVAF-DISS SALT WTR 12/20/11 12/21/11 WG119081-7 L54765-10 AF-MSDPage 10 of 19 

### LIMSView Batch Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

WG122629

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L56061-1 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS FRESH WTR 07/31/12 08/21/12 08/22/12

L56061-2 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS FRESH WTR 08/01/12 08/21/12 08/22/12

L56061-10 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS FILTER WTR 07/31/12 08/21/12 08/22/12 FFB- metals

L56061-11 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS FRESH WTR 08/02/12 08/15/12 08/16/12 FREP@L56061-3

L56062-1 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 07/30/12 08/21/12 08/22/12

L56062-2 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 07/30/12 08/21/12 08/22/12

L56062-3 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 07/30/12 08/21/12 08/22/12

L56062-5 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 07/30/12 08/21/12 08/22/12

L56062-6 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 07/30/12 08/21/12 08/22/12

L56062-16 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS FILTER WTR 07/30/12 08/21/12 08/22/12 FFB @ LTED04

WG122629-1 MB MTHG-CVAF-DISS BLANK WTR 08/21/12 08/22/12 METHOD BLANK#1

WG122629-2 MB MTHG-CVAF-DISS BLANK WTR 08/21/12 08/22/12 METHOD BLANK#2

WG122629-3 MB MTHG-CVAF-DISS BLANK WTR 08/21/12 08/22/12 METHOD BLANK#3

WG122629-4 SB MTHG-CVAF-DISS BLANK WTR 08/21/12 08/22/12 WG122629-1 AF-SB

WG122629-5 MS MTHG-CVAF-DISS FRESH WTR 08/21/12 08/22/12 L56061-1 AF-MS

WG122629-6 MSD MTHG-CVAF-DISS FRESH WTR 08/21/12 08/22/12 WG122629-5 L56061-1 AF-MSD



### WG122712

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L56061-3 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS FRESH WTR 08/02/12 08/22/12 08/23/12

L56062-4 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 07/30/12 08/22/12 08/23/12

L56062-7 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 07/30/12 08/22/12 08/23/12

L56062-8 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 07/30/12 08/22/12 08/23/12

L56062-9 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 07/30/12 08/22/12 08/23/12 FREP@L56062-10

L56062-10 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 07/30/12 08/22/12 08/23/12

WG122712-1 MB MTHG-CVAF-DISS BLANK WTR 08/22/12 08/23/12 METHOD BLANK

WG122712-2 MB MTHG-CVAF-DISS BLANK WTR 08/22/12 08/23/12 METHOD BLANK

WG122712-3 MB MTHG-CVAF-DISS BLANK WTR 08/22/12 08/23/12 METHOD BLANK

WG122712-4 SB MTHG-CVAF-DISS BLANK WTR 08/22/12 08/23/12 WG122712-1 AF-SB

WG122712-5 MS MTHG-CVAF-DISS SALT WTR 08/22/12 08/23/12 L56062-10 AF-MS

WG122712-6 MSD MTHG-CVAF-DISS SALT WTR 08/22/12 08/23/12 WG122712-5 L56062-10 AF-MSD



### WG124900

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L56989-1 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS FRESH WTR 12/10/12 01/07/13 01/08/13

L56989-2 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS FRESH WTR 12/11/12 01/07/13 01/08/13Page 11 of 19 

### LIMSView Batch Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

L56989-3 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS FRESH WTR 12/13/12 01/07/13 01/08/13

L56989-10 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS FILTER WTR 12/10/12 01/07/13 01/08/13 FFB

L56989-11 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS FRESH WTR 12/11/12 01/07/13 01/08/13 FREP@L56989-2

L56990-1 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 12/12/12 01/07/13 01/08/13

L56990-2 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 12/12/12 01/07/13 01/08/13

L56990-3 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 12/12/12 01/07/13 01/08/13

L56990-4 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 12/12/12 01/07/13 01/08/13

L56990-5 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 12/12/12 01/07/13 01/08/13

L56990-6 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 12/12/12 01/07/13 01/08/13

L56990-7 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 12/12/12 01/07/13 01/08/13

L56990-8 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 12/12/12 01/07/13 01/08/13

L56990-9 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 12/12/12 01/07/13 01/08/13 FREP@L56990-10

L56990-10 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS SALT WTR 12/12/12 01/07/13 01/08/13

L56990-16 421162-300 NPDES RW Charact. Study MTHG-CVAF-DISS FILTER WTR 12/12/12 01/07/13 01/08/13 FFB @ KSBP01

WG124900-1 MB MTHG-CVAF-DISS BLANK WTR 01/07/13 01/08/13 METHOD BLANK

WG124900-2 MB MTHG-CVAF-DISS BLANK WTR 01/07/13 01/08/13 METHOD BLANK

WG124900-3 MB MTHG-CVAF-DISS BLANK WTR 01/07/13 01/08/13 METHOD BLANK

WG124900-4 SB MTHG-CVAF-DISS BLANK WTR 01/07/13 01/08/13 WG124900-1 AF-SB

WG124900-5 MS MTHG-CVAF-DISS FRESH WTR 01/07/13 01/08/13 L56989-1 AF-MS

WG124900-6 MSD MTHG-CVAF-DISS FRESH WTR 01/07/13 01/08/13 WG124900-5 L56989-1 AF-MSD

WG124900-7 MS MTHG-CVAF-DISS SALT WTR 01/07/13 01/08/13 L56990-10 AF-MS

WG124900-8 MSD MTHG-CVAF-DISS SALT WTR 01/07/13 01/08/13 WG124900-7 L56990-10 AF-MSD



### WG116281

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L53619-1 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA FRESH WTR 07/11/11 07/15/11 07/20/11

L53619-2 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA FRESH WTR 07/12/11 07/15/11 07/20/11

L53619-3 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA FRESH WTR 07/13/11 07/15/11 07/20/11

L53619-12 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA FILTER WTR 07/11/11 07/15/11 07/20/11 FFB- Metals

L53619-13 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA FRESH WTR 07/12/11 07/15/11 07/20/11 FREP@L53619-2

L53626-16 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA FILTER WTR 07/14/11 07/15/11 07/20/11 FFB @ KSBP01

WG116281-1 MB MTICPMS-DISS-SEA BLANK WTR 07/15/11 07/20/11 METHOD BLANK

WG116281-2 SB MTICPMS-DISS-SEA BLANK WTR 07/15/11 07/20/11 WG116281-1 MS-SEA SPIKE BLANK

WG116281-3 MS MTICPMS-DISS-SEA FRESH WTR 07/15/11 07/20/11 L53619-2 MS-SEA MATRIX SPIKE

WG116281-4 MSD MTICPMS-DISS-SEA FRESH WTR 07/15/11 07/20/11 WG116281-3 L53619-2 MS-SEA MSD



### WG117861

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L53626-1 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 07/14/11 07/15/11 08/22/11Page 12 of 19 

### LIMSView Batch Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

L53626-2 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 07/14/11 07/15/11 08/22/11

L53626-3 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 07/14/11 07/15/11 08/22/11

L53626-4 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 07/14/11 07/15/11 08/22/11

L53626-5 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 07/14/11 07/15/11 08/22/11

L53626-6 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 07/14/11 07/15/11 08/22/11

L53626-7 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 07/14/11 07/15/11 08/22/11

L53626-8 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 07/14/11 07/15/11 08/22/11

L53626-9 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 07/14/11 07/15/11 08/22/11 FREP@L53626-10

L53626-10 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 07/14/11 07/15/11 08/22/11

WG117861-1 MB MTICPMS-DISS-SEA BLANK WTR 07/15/11 08/22/11 METHOD BLANK

WG117861-2 SB MTICPMS-DISS-SEA BLANK WTR 07/15/11 08/22/11 WG117861-1 MS-SEA SPIKE BLANK

WG117861-3 MS MTICPMS-DISS-SEA SALT WTR 07/15/11 08/22/11 L53626-1 MS-SEA MATRIX SPIKE

WG117861-4 MSD MTICPMS-DISS-SEA SALT WTR 07/15/11 08/22/11 WG117861-3 L53626-1 MS-SEA MSD



### WG119280

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L54760-1 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA FRESH WTR 12/12/11 01/06/12 01/06/12

L54760-2 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA FRESH WTR 12/13/11 01/06/12 01/06/12

L54760-3 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA FRESH WTR 12/14/11 01/06/12 01/06/12

L54760-10 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA FILTER WTR 12/12/11 01/06/12 01/06/12 FFB- metals

L54760-11 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA FRESH WTR 12/13/11 01/06/12 01/06/12 FREP@L54760-2

L54765-16 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA FILTER WTR 12/14/11 01/06/12 01/06/12 FFB @ LTED04

WG119280-1 MB MTICPMS-DISS-SEA BLANK WTR 01/06/12 01/06/12 METHOD BLANK

WG119280-2 SB MTICPMS-DISS-SEA BLANK WTR 01/06/12 01/06/12 WG119280-1 MS-SEA SPIKE BLANK

WG119280-3 MS MTICPMS-DISS-SEA FRESH WTR 01/06/12 01/06/12 L54760-2 MS-SEA MATRIX SPIKE

WG119280-4 MSD MTICPMS-DISS-SEA FRESH WTR 01/06/12 01/06/12 WG119280-3 L54760-2 MS-SEA MSD



### WG119326

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L54765-1 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 12/14/11 01/10/12 01/26/12

L54765-2 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 12/14/11 01/10/12 01/26/12

L54765-3 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 12/14/11 01/10/12 01/26/12

L54765-4 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 12/14/11 01/10/12 01/26/12

L54765-5 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 12/14/11 01/10/12 01/26/12

L54765-6 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 12/14/11 01/10/12 01/26/12

L54765-7 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 12/14/11 01/10/12 01/26/12

L54765-8 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 12/14/11 01/10/12 01/26/12

L54765-9 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 12/14/11 01/10/12 01/26/12 FREP@L54765-10

L54765-10 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 12/14/11 01/10/12 01/26/12Page 13 of 19 

### LIMSView Batch Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

WG119326-1 MB MTICPMS-DISS-SEA BLANK WTR 01/10/12 01/26/12 METHOD BLANK

WG119326-2 SB MTICPMS-DISS-SEA BLANK WTR 01/10/12 01/26/12 WG119326-1 MS-SEA SPIKE BLANK

WG119326-3 MS MTICPMS-DISS-SEA SALT WTR 01/10/12 01/26/12 L54765-10 MS-SEA MATRIX SPIKE

WG119326-4 MSD MTICPMS-DISS-SEA SALT WTR 01/10/12 01/26/12 WG119326-3 L54765-10 MS-SEA MSD



### WG122900

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L56061-1 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA FRESH WTR 07/31/12 09/05/12 09/05/12

L56061-2 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA FRESH WTR 08/01/12 09/05/12 09/05/12

L56061-3 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA FRESH WTR 08/02/12 09/05/12 09/05/12

L56061-10 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA FILTER WTR 07/31/12 09/05/12 09/05/12 FFB- metals

L56061-11 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA FRESH WTR 08/02/12 09/05/12 09/05/12 FREP@L56061-3

L56062-16 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA FILTER WTR 07/30/12 09/05/12 09/05/12 FFB @ LTED04

WG122900-1 MB MTICPMS-DISS-SEA BLANK WTR 09/05/12 09/05/12 METHOD BLANK

WG122900-2 SB MTICPMS-DISS-SEA BLANK WTR 09/05/12 09/05/12 WG122900-1 MS-SEA

WG122900-3 MS MTICPMS-DISS-SEA FRESH WTR 09/05/12 09/05/12 L56061-2 MS-SEA

WG122900-4 MSD MTICPMS-DISS-SEA FRESH WTR 09/05/12 09/05/12 WG122900-3 L56061-2 MS-SEA



### WG123691

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L56062-1 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 07/30/12 10/18/12 10/18/12

L56062-2 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 07/30/12 10/18/12 10/18/12

L56062-3 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 07/30/12 10/18/12 10/18/12

L56062-4 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 07/30/12 10/18/12 10/18/12

L56062-5 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 07/30/12 10/18/12 10/18/12

L56062-6 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 07/30/12 10/18/12 10/18/12

L56062-7 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 07/30/12 10/18/12 10/18/12

L56062-8 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 07/30/12 10/18/12 10/18/12

L56062-9 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 07/30/12 10/18/12 10/18/12 FREP@L56062-10

L56062-10 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 07/30/12 10/18/12 10/18/12

WG123691-1 MB MTICPMS-DISS-SEA SALT WTR 10/18/12 10/18/12 METHOD BLANK

WG123691-2 SB MTICPMS-DISS-SEA SALT WTR 10/18/12 10/18/12 WG123691-1 MS-SEA

WG123691-3 MS MTICPMS-DISS-SEA SALT WTR 10/18/12 10/18/12 L56062-7 MS-SEA

WG123691-4 MSD MTICPMS-DISS-SEA SALT WTR 10/18/12 10/18/12 WG123691-3 L56062-7 MS-SEA



### WG124746

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L56989-1 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA FRESH WTR 12/10/12 12/20/12 12/21/12Page 14 of 19 

### LIMSView Batch Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

L56989-2 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA FRESH WTR 12/11/12 12/20/12 12/21/12

L56989-3 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA FRESH WTR 12/13/12 12/20/12 12/21/12

L56989-10 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA FILTER WTR 12/10/12 12/20/12 12/21/12 FFB

L56989-11 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA FRESH WTR 12/11/12 12/20/12 12/21/12 FREP@L56989-2

L56990-16 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA FILTER WTR 12/12/12 12/20/12 12/21/12 FFB @ KSBP01

WG124746-1 MB MTICPMS-DISS-SEA BLANK WTR 12/20/12 12/21/12 METHOD BLANK

WG124746-2 SB MTICPMS-DISS-SEA BLANK WTR 12/20/12 12/21/12 WG124746-1 MS-SEA SPIKE BLANK

WG124746-3 MS MTICPMS-DISS-SEA FRESH WTR 12/20/12 12/21/12 L56989-1 MS-SEA MATRIX SPIKE

WG124746-4 MSD MTICPMS-DISS-SEA FRESH WTR 12/20/12 12/21/12 WG124746-3 L56989-1 MS-SEA MSD



### WG124855

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L56990-1 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 12/12/12 01/03/13 01/03/13

L56990-2 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 12/12/12 01/03/13 01/03/13

L56990-3 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 12/12/12 01/03/13 01/03/13

L56990-4 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 12/12/12 01/03/13 01/03/13

L56990-5 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 12/12/12 01/03/13 01/03/13

L56990-6 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 12/12/12 01/03/13 01/03/13

L56990-7 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 12/12/12 01/03/13 01/03/13

L56990-8 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 12/12/12 01/03/13 01/03/13

L56990-9 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 12/12/12 01/03/13 01/03/13 FREP@L56990-10

L56990-10 421162-300 NPDES RW Charact. Study MTICPMS-DISS-SEA SALT WTR 12/12/12 01/03/13 01/03/13

WG124855-1 MB MTICPMS-DISS-SEA BLANK WTR 01/03/13 01/03/13 METHOD BLANK

WG124855-2 SB MTICPMS-DISS-SEA BLANK WTR 01/03/13 01/03/13 WG124855-1 MS-SEA SPIKE BLANK

WG124855-3 MS MTICPMS-DISS-SEA SALT WTR 01/03/13 01/03/13 L56990-9 MS-SEA MATRIX SPIKE

WG124855-4 MSD MTICPMS-DISS-SEA SALT WTR 01/03/13 01/03/13 WG124855-3 L56990-9 MS-SEA MSD

WG116287

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L53619-1 421162-300 NPDES RW Charact. Study MTICPMS-SEA FRESH WTR 07/11/11 07/15/11 08/04/11

L53619-2 421162-300 NPDES RW Charact. Study MTICPMS-SEA FRESH WTR 07/12/11 07/15/11 08/04/11

L53619-3 421162-300 NPDES RW Charact. Study MTICPMS-SEA FRESH WTR 07/13/11 07/15/11 08/04/11

L53619-4 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 07/11/11 07/15/11 08/04/11 ATMOBLANK Day 1

L53619-5 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 07/12/11 07/15/11 08/04/11 ATMOBLANK Day 2

L53619-6 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 07/13/11 07/15/11 08/04/11 ATMOBLANK Day 3

L53619-7 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 07/11/11 07/15/11 08/04/11 CRBOYBLANK Day 1

L53619-8 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 07/11/11 07/15/11 08/04/11 TRIPBLANK Day 1

L53619-9 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 07/11/11 07/15/11 08/04/11 BAILERBLANK Day 1

L53619-13 421162-300 NPDES RW Charact. Study MTICPMS-SEA FRESH WTR 07/12/11 07/15/11 08/04/11 FREP@L53619-2Page 15 of 19 

### LIMSView Batch Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

L53626-11 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 07/14/11 07/15/11 08/04/11 Equipment Blank- not field Blank

L53626-12 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 07/14/11 07/15/11 08/04/11 ATM BLANK @KSBP01

L53626-13 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 07/14/11 07/15/11 08/04/11 ATM BLANK @LTED04

L53626-14 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 07/14/11 07/15/11 08/04/11 ATM BLANK @LSNT01

L53626-15 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 07/14/11 07/15/11 08/04/11 Time of first sample recorded

L53626-17 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 07/14/11 07/15/11 08/04/11 Carboy Blank @ Lab

WG116287-1 SB MTICPMS-SEA BLANK WTR 07/15/11 08/04/11 WG116287-3 MS-SEA SPIKE BLANK

WG116287-2 SB MTICPMS-SEA BLANK WTR 07/15/11 08/04/11 WG116287-4 MS-SEA SPIKE BLANK

WG116287-3 MB MTICPMS-SEA BLANK WTR 07/15/11 08/04/11 METHOD BLANK

WG116287-4 MB MTICPMS-SEA BLANK WTR 07/15/11 08/04/11 METHOD BLANK

WG116287-5 MS MTICPMS-SEA FRESH WTR 07/15/11 08/04/11 L53619-1 MS-SEA MATRIX SPIKE

WG116287-6 MSD MTICPMS-SEA FRESH WTR 07/15/11 08/04/11 WG116287-5 L53619-1 MS-SEA MSD

WG116287-7 MS MTICPMS-SEA FRESH WTR 07/15/11 08/04/11 L53619-3 MS-SEA MATRIX SPIKE

WG116287-8 MSD MTICPMS-SEA FRESH WTR 07/15/11 08/04/11 WG116287-7 L53619-3 MS-SEA MSD



### WG116666

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L53626-1 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 07/14/11 07/15/11 08/22/11

L53626-2 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 07/14/11 07/15/11 08/22/11

L53626-3 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 07/14/11 07/15/11 08/22/11

L53626-4 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 07/14/11 07/15/11 08/23/11

L53626-5 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 07/14/11 07/15/11 08/23/11

L53626-6 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 07/14/11 07/15/11 08/23/11

L53626-7 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 07/14/11 07/15/11 08/23/11

L53626-8 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 07/14/11 07/15/11 08/23/11

L53626-9 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 07/14/11 07/15/11 08/23/11 FREP@L53626-10

L53626-10 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 07/14/11 07/15/11 08/23/11

WG116666-2 SB MTICPMS-SEA BLANK WTR 07/15/11 08/22/11 WG116666-4 MS-SEA

WG116666-4 MB MTICPMS-SEA BLANK WTR 07/15/11 08/22/11 METHOD BLANK

WG116666-7 MS MTICPMS-SEA SALT WTR 07/15/11 08/22/11 L53626-1 MS-SEA MATRIX SPIKE

WG116666-8 MSD MTICPMS-SEA SALT WTR 07/15/11 08/22/11 WG116666-7 L53626-1 MS-SEA MSD



### WG118832

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L54739-1 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/02/11 12/06/11 12/06/11

L54739-2 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/02/11 12/06/11 12/06/11

L54739-3 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/02/11 12/06/11 12/06/11

L54739-4 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/02/11 12/06/11 12/06/11

L54739-5 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/02/11 12/06/11 12/06/11Page 16 of 19 

### LIMSView Batch Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

L54739-6 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/02/11 12/06/11 12/06/11

L54739-7 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/02/11 12/06/11 12/06/11

L54739-8 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/02/11 12/06/11 12/06/11

L54739-9 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/02/11 12/06/11 12/06/11

L54739-10 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/02/11 12/06/11 12/06/11

WG118832-1 MB MTICPMS-SEA BLANK WTR 12/06/11 12/06/11 METHOD BLANK



### WG119016

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L54760-1 421162-300 NPDES RW Charact. Study MTICPMS-SEA FRESH WTR 12/12/11 12/19/11 12/22/11

L54760-2 421162-300 NPDES RW Charact. Study MTICPMS-SEA FRESH WTR 12/13/11 12/19/11 12/22/11

L54760-4 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/12/11 12/19/11 12/22/11 ATMOBLK- Day 1

L54760-5 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/13/11 12/19/11 12/22/11 ATMOBLK- Day 2

L54760-7 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/12/11 12/19/11 12/22/11 CRBOYBLK

L54760-8 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/12/11 12/19/11 12/22/11 TRPBLK

L54760-9 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/12/11 12/19/11 12/22/11 BAILERBLK

L54760-11 421162-300 NPDES RW Charact. Study MTICPMS-SEA FRESH WTR 12/13/11 12/19/11 12/22/11 FREP@L54760-2

WG119016-1 MB MTICPMS-SEA BLANK WTR 12/19/11 12/22/11 METHOD BLANK

WG119016-2 SB MTICPMS-SEA BLANK WTR 12/19/11 12/22/11 WG119016-1 MS-SEA SPIKE BLANK

WG119016-3 MS MTICPMS-SEA FRESH WTR 12/19/11 12/22/11 L54760-2 MS-SEA MATRIX SPIKE

WG119016-4 MSD MTICPMS-SEA FRESH WTR 12/19/11 12/22/11 WG119016-3 L54760-2 MS-SEA



### WG119157

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L54760-3 421162-300 NPDES RW Charact. Study MTICPMS-SEA FRESH WTR 12/14/11 01/03/12 01/03/12

L54760-6 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/14/11 01/03/12 01/03/12 ATMOBLK- Day 3

L54765-11 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/14/11 01/03/12 01/03/12 Field Blank @ LTDE04

L54765-12 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/14/11 01/03/12 01/03/12 ATM BLANK @KSBP01

L54765-13 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/14/11 01/03/12 01/03/12 ATM BLANK @LTED04

L54765-14 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/14/11 01/03/12 01/03/12 ATM BLANK @LSNT01

L54765-15 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/14/11 01/03/12 01/03/12 Time of first sample recorded

L54765-17 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/14/11 01/03/12 01/03/12 Carboy Blank @ LTED04

WG119157-1 MB MTICPMS-SEA BLANK WTR 01/03/12 01/03/12 METHOD BLANK

WG119157-2 SB MTICPMS-SEA BLANK WTR 01/03/12 01/03/12 WG119157-1 MS-SEA SPIKE BLANK

WG119157-3 MS MTICPMS-SEA FRESH WTR 01/03/12 01/03/12 L54760-3 MS-SEA MATRIX SPIKE

WG119157-4 MSD MTICPMS-SEA FRESH WTR 01/03/12 01/03/12 WG119157-3 L54760-3 MS-SEA MSDPage 17 of 19 

### LIMSView Batch Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

WG119325

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L54765-1 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 12/14/11 01/10/12 01/26/12

L54765-2 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 12/14/11 01/10/12 01/26/12

L54765-3 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 12/14/11 01/10/12 01/26/12

L54765-4 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 12/14/11 01/10/12 01/26/12

L54765-5 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 12/14/11 01/10/12 01/26/12

L54765-6 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 12/14/11 01/10/12 01/26/12

L54765-7 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 12/14/11 01/10/12 01/26/12

L54765-8 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 12/14/11 01/10/12 01/26/12

L54765-9 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 12/14/11 01/10/12 01/26/12 FREP@L54765-10

L54765-10 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 12/14/11 01/10/12 01/26/12

WG119325-1 MB MTICPMS-SEA BLANK WTR 01/10/12 01/26/12 METHOD BLANK

WG119325-2 SB MTICPMS-SEA BLANK WTR 01/10/12 01/26/12 WG119325-1 MS-SEA SPIKE BLANK

WG119325-3 MS MTICPMS-SEA SALT WTR 01/10/12 01/26/12 L54765-8 MS-SEA MATRIX SPIKE

WG119325-4 MSD MTICPMS-SEA SALT WTR 01/10/12 01/26/12 WG119325-3 L54765-8 MS-SEA MSD



### WG122436

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L56061-1 421162-300 NPDES RW Charact. Study MTICPMS-SEA FRESH WTR 07/31/12 08/08/12 08/09/12

L56061-2 421162-300 NPDES RW Charact. Study MTICPMS-SEA FRESH WTR 08/01/12 08/08/12 08/09/12

L56061-3 421162-300 NPDES RW Charact. Study MTICPMS-SEA FRESH WTR 08/02/12 08/08/12 08/09/12

L56061-11 421162-300 NPDES RW Charact. Study MTICPMS-SEA FRESH WTR 08/02/12 08/08/12 08/09/12 FREP@L56061-3

WG122436-1 MB MTICPMS-SEA BLANK WTR 08/08/12 08/09/12 METHOD BLANK

WG122436-2 SB MTICPMS-SEA BLANK WTR 08/08/12 08/09/12 WG122436-1 MS-SEA SPIKE BLANK

WG122436-3 MS MTICPMS-SEA FRESH WTR 08/08/12 08/09/12 L56061-2 MS-SEA MATRIX SPIKE

WG122436-4 MSD MTICPMS-SEA FRESH WTR 08/08/12 08/09/12 WG122436-3 L56061-2 MS-SEA MSD



### WG122819

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L56061-4 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 07/31/12 08/29/12 08/29/12 ATMOBLK Day 1

L56061-5 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 08/01/12 08/29/12 08/29/12 ATMOBLK Day 2

L56061-6 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 08/02/12 08/29/12 08/29/12 ATMOBLK Day 3

L56061-7 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 07/31/12 08/29/12 08/29/12 CRBYBLK Day 1

L56061-8 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 07/31/12 08/29/12 08/29/12 TRPBLK Day 1

L56061-9 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 07/31/12 08/29/12 08/29/12 BAILERBLK Day 1

L56062-11 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 07/30/12 08/29/12 08/29/12 Field Blank @ LTDE04

L56062-12 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 07/30/12 08/29/12 08/29/12 ATM BLANK @KSBP01Page 18 of 19 

### LIMSView Batch Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

L56062-13 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 07/30/12 08/29/12 08/29/12 ATM BLANK @LTED04

L56062-14 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 07/30/12 08/29/12 08/29/12 ATM BLANK @LSNT01

L56062-15 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 07/30/12 08/29/12 08/29/12 Time of first sample recorded

L56062-17 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 07/30/12 08/29/12 08/29/12 Carboy Blank @ LTED04

WG122819-1 MB MTICPMS-SEA BLANK WTR 08/29/12 08/29/12 METHOD BLANK

WG122819-2 MB MTICPMS-SEA BLANK WTR 08/29/12 08/29/12 METHOD BLANK



### WG122999

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L56062-1 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 07/30/12 09/11/12 09/19/12

L56062-2 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 07/30/12 09/11/12 09/19/12

L56062-3 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 07/30/12 09/11/12 09/19/12

L56062-4 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 07/30/12 09/11/12 09/19/12

L56062-5 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 07/30/12 09/11/12 09/19/12

L56062-6 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 07/30/12 09/11/12 09/19/12

L56062-7 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 07/30/12 09/11/12 09/19/12

L56062-8 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 07/30/12 09/11/12 09/19/12

L56062-9 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 07/30/12 09/11/12 09/19/12 FREP@L56062-10

L56062-10 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 07/30/12 09/11/12 09/19/12

WG122999-1 MB MTICPMS-SEA BLANK WTR 09/11/12 09/19/12 METHOD BLANK

WG122999-2 SB MTICPMS-SEA BLANK WTR 09/11/12 09/19/12 WG122999-1 MS-SEA SPIKE BLANK

WG122999-3 MS MTICPMS-SEA SALT WTR 09/11/12 09/19/12 L56062-7 MS-SEA MATRIX SPIKE

WG122999-4 MSD MTICPMS-SEA SALT WTR 09/11/12 09/19/12 WG122999-3 L56062-7 MS-SEA MSD



### WG124799

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L56989-1 421162-300 NPDES RW Charact. Study MTICPMS-SEA FRESH WTR 12/10/12 12/26/12 12/26/12

L56989-2 421162-300 NPDES RW Charact. Study MTICPMS-SEA FRESH WTR 12/11/12 12/26/12 12/26/12

L56989-3 421162-300 NPDES RW Charact. Study MTICPMS-SEA FRESH WTR 12/13/12 12/26/12 12/26/12

L56989-11 421162-300 NPDES RW Charact. Study MTICPMS-SEA FRESH WTR 12/11/12 12/26/12 12/26/12 FREP@L56989-2

WG124799-1 MB MTICPMS-SEA BLANK WTR 12/26/12 12/26/12 METHOD BLANK

WG124799-2 SB MTICPMS-SEA BLANK WTR 12/26/12 12/26/12 WG124799-1 MS-SEA SPIKE BLANK

WG124799-3 MS MTICPMS-SEA FRESH WTR 12/26/12 12/26/12 L56989-1 MS-SEA MATRIX SPIKE

WG124799-4 MSD MTICPMS-SEA FRESH WTR 12/26/12 12/26/12 WG124799-3 L56989-1 MS-SEA MSD



### WG124800

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L56989-4 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/10/12 12/26/12 12/27/12 ATMOBLK Day 1Page 19 of 19 

### LIMSView Batch Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

L56989-5 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/11/12 12/26/12 12/27/12 ATMOBLK Day 2

L56989-6 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/13/12 12/26/12 12/27/12 ATMOBLK Day 3

L56989-7 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/10/12 12/26/12 12/27/12 CRBOYBLK

L56989-8 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/10/12 12/26/12 12/27/12 TRPBLK

L56989-9 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/10/12 12/26/12 12/27/12 BAILERBLK

L56990-11 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/12/12 12/26/12 12/27/12 Field Blank @ KSBP01

L56990-12 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/12/12 12/26/12 12/27/12 ATM BLANK @KSBP01

L56990-13 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/12/12 12/26/12 12/27/12 ATM BLANK @LTED04

L56990-14 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/12/12 12/26/12 12/27/12 ATM BLANK @LSNT01

L56990-15 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/12/12 12/26/12 12/27/12 Time of first sample recorded

L56990-17 421162-300 NPDES RW Charact. Study MTICPMS-SEA BLANK WTR 12/12/12 12/26/12 12/27/12 Carboy Blank @ KSBP01

WG124800-1 MB MTICPMS-SEA BLANK WTR 12/26/12 12/27/12 METHOD BLANK

WG124800-2 MB MTICPMS-SEA BLANK WTR 12/26/12 12/27/12 METHOD BLANK



### WG125559

Sample Project Project Description List Type Matrix Collect Prep Analysis Comments

L56990-1 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 12/12/12 02/25/13 02/25/13

L56990-2 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 12/12/12 02/25/13 02/25/13

L56990-3 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 12/12/12 02/25/13 02/25/13

L56990-4 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 12/12/12 02/25/13 02/25/13

L56990-5 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 12/12/12 02/25/13 02/25/13

L56990-6 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 12/12/12 02/25/13 02/25/13

L56990-7 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 12/12/12 02/25/13 02/25/13

L56990-8 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 12/12/12 02/25/13 02/25/13

L56990-9 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 12/12/12 02/25/13 02/25/13 FREP@L56990-10

L56990-10 421162-300 NPDES RW Charact. Study MTICPMS-SEA SALT WTR 12/12/12 02/25/13 02/25/13

WG125559-1 MB MTICPMS-SEA BLANK WTR 02/25/13 02/25/13 METHOD BLANK

WG125559-2 SB MTICPMS-SEA BLANK WTR 02/25/13 02/25/13 WG125559-1 MS-SEA SPIKE BLANK

WG125559-3 MS MTICPMS-SEA SALT WTR 02/25/13 02/25/13 L56990-9 MS-SEA MATRIX SPIKE

WG125559-4 MSD MTICPMS-SEA SALT WTR 02/25/13 02/25/13 WG125559-3 L56990-9 MS-SEA MSDPage 1 of 37 

### WG117399

MB:WG117399-1 Matrix: BLANK WTR Listtype:MTHARD-ICPMS Method:EPA 200.8/SW846 6020A*SM2340B Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Hardness, Calc 0.331 0.331 g CaCO3 <MDL

MB:WG117399-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Magnesium, Total, ICP-MS 50 50 ug/L <MDL Calcium, Total, ICP-MS 50 50 ug/L <MDL

SB:WG117399-2 MB:WG117399-1 Matrix: BLANK WTR Listtype:MTHARD-ICPMS Method:EPA 200.8/SW846 6020A*SM2340B Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Hardness, Calc 0.331 0.331 g CaCO3 <MDL 33.1 33.5 101 85--115

SB:WG117399-2 MB:WG117399-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Magnesium, Total, ICP-MS 50 50 ug/L <MDL 5000 5240 105 85--115 Calcium, Total, ICP-MS 50 50 ug/L <MDL 5000 4770 95 85--115

LD:WG117399-3 L53619-13 Matrix: FRESH WTR Listtype:MTHARD-ICPMS Method:EPA 200.8/SW846 6020A*SM2340B Project:421162-300 Pkey:STD (Lab Duplicate)

Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimit Hardness, Calc 0.331 0.331 g CaCO3 82.3 81.6 1 0--20

LD:WG117399-3 L53619-13 Matrix: FRESH WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:421162-300 Pkey:STD (Lab Duplicate)

Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimit Magnesium, Total, ICP-MS 50 50 ug/L 13500 13400 1 0--20 Calcium, Total, ICP-MS 50 50 ug/L 10700 10500 2 0--20

MS:WG117399-4 L53619-13 Matrix: FRESH WTR Listtype:MTHARD-ICPMS Method:EPA 200.8/SW846 6020A*SM2340B Project:421162-300 Pkey:STD (Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit Hardness, Calc 0.331 0.331 g CaCO3 82.3 33.1 115 98 75--125 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for MetalsPage 2 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

MS:WG117399-4 L53619-13 Matrix: FRESH WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:421162-300 Pkey:STD (Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit Magnesium, Total, ICP-MS 50 50 ug/L 13500 5000 18700 103 75--125 Calcium, Total, ICP-MS 50 50 ug/L 10700 5000 15100 88 75--125



### WG119704

MB:WG119704-1 Matrix: BLANK WTR Listtype:MTHARD-ICPMS Method:EPA 200.8/SW846 6020A*SM2340B Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Hardness, Calc 0.331 0.331 g CaCO3 <MDL

MB:WG119704-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Magnesium, Total, ICP-MS 50 50 ug/L <MDL Calcium, Total, ICP-MS 50 50 ug/L <MDL

SB:WG119704-2 MB:WG119704-1 Matrix: BLANK WTR Listtype:MTHARD-ICPMS Method:EPA 200.8/SW846 6020A*SM2340B Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Hardness, Calc 0.331 0.331 g CaCO3 <MDL 33.1 32.7 99 85--115

SB:WG119704-2 MB:WG119704-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Magnesium, Total, ICP-MS 50 50 ug/L <MDL 5000 5180 104 85--115 Calcium, Total, ICP-MS 50 50 ug/L <MDL 5000 4560 91 85--115

LD:WG119704-3 L54760-11 Matrix: FRESH WTR Listtype:MTHARD-ICPMS Method:EPA 200.8/SW846 6020A*SM2340B Project:421162-300 Pkey:STD (Lab Duplicate)

Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimit Hardness, Calc 1.65 1.65 g CaCO3 719 704 2 0--20

LD:WG119704-3 L54760-11 Matrix: FRESH WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:421162-300 Pkey:STD (Lab Duplicate)

Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimit Magnesium, Total, ICP-MS 250 250 ug/L 142000 138000 2 0--20 Calcium, Total, ICP-MS 250 250 ug/L 54600 53800 2 0--20Page 3 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

MS:WG119704-4 L54760-11 Matrix: FRESH WTR Listtype:MTHARD-ICPMS Method:EPA 200.8/SW846 6020A*SM2340B Project:421162-300 Pkey:STD (Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit Hardness, Calc 1.65 1.65 g CaCO3 719 33.1 723 4xRule 75--125

MS:WG119704-4 L54760-11 Matrix: FRESH WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:421162-300 Pkey:STD (Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit Magnesium, Total, ICP-MS 250 250 ug/L 142000 5000 141000 4xRule 75--125 Calcium, Total, ICP-MS 250 250 ug/L 54600 5000 57700 4xRule 75--125



### WG123247

MB:WG123247-1 Matrix: BLANK WTR Listtype:MTHARD-ICPMS Method:EPA 200.8/SW846 6020A*SM2340B Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Hardness, Calc 0.331 0.331 g CaCO3 <MDL

MB:WG123247-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Beryllium, Total, ICP-MS 0.1 0.5 ug/L <MDL Sodium, Total, ICP-MS 100 100 ug/L <MDL Magnesium, Total, ICP-MS 50 50 ug/L <MDL Aluminum, Total, ICP-MS 2 10 ug/L 2.3 B Potassium, Total, ICP-MS 100 500 ug/L <MDL Calcium, Total, ICP-MS 50 50 ug/L <MDL Vanadium, Total, ICP-MS 0.075 0.375 ug/L <MDL Chromium, Total, ICP-MS 0.2 1 ug/L <MDL Iron, Total, ICP-MS 10 50 ug/L <MDL Manganese, Total, ICP-MS 0.1 0.5 ug/L <MDL Cobalt, Total, ICP-MS 0.05 0.25 ug/L <MDL Nickel, Total, ICP-MS 0.1 0.5 ug/L <MDL Copper, Total, ICP-MS 0.4 2 ug/L <MDL Zinc, Total, ICP-MS 0.5 2.5 ug/L <MDL Arsenic, Total, ICP-MS 0.1 0.5 ug/L <MDL Selenium, Total, ICP-MS 0.5 1 ug/L <MDL Silver, Total, ICP-MS 0.04 0.2 ug/L <MDL Cadmium, Total, ICP-MS 0.05 0.25 ug/L <MDL Tin, Total, ICP-MS 0.3 1.5 ug/L <MDL Antimony, Total, ICP-MS 0.3 1 ug/L <MDLPage 4 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

Barium, Total, ICP-MS 0.05 0.25 ug/L <MDL Thallium, Total, ICP-MS 0.04 0.2 ug/L <MDL Lead, Total, ICP-MS 0.1 0.5 ug/L <MDL

SB:WG123247-2 MB:WG123247-1 Matrix: BLANK WTR Listtype:MTHARD-ICPMS Method:EPA 200.8/SW846 6020A*SM2340B Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Hardness, Calc 0.331 0.331 g CaCO3 <MDL 33.1 30.9 94 85--115

SB:WG123247-2 MB:WG123247-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Beryllium, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 18.9 95 85--115 Sodium, Total, ICP-MS 100 100 ug/L <MDL 5000 5000 100 85--115 Magnesium, Total, ICP-MS 50 50 ug/L <MDL 5000 4570 91 85--115 Aluminum, Total, ICP-MS 2 10 ug/L 2.3 20 23.1 104 85--115 Potassium, Total, ICP-MS 100 500 ug/L <MDL 5000 5030 101 85--115 Calcium, Total, ICP-MS 50 50 ug/L <MDL 5000 4860 97 85--115 Vanadium, Total, ICP-MS 0.075 0.375 ug/L <MDL 20 19.9 100 85--115 Chromium, Total, ICP-MS 0.2 1 ug/L <MDL 20 20.3 101 85--115 Iron, Total, ICP-MS 10 50 ug/L <MDL 5000 4900 98 85--115 Manganese, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 21.6 108 85--115 Cobalt, Total, ICP-MS 0.05 0.25 ug/L <MDL 20 19.9 99 85--115 Nickel, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 19.1 96 85--115 Copper, Total, ICP-MS 0.4 2 ug/L <MDL 20 20 100 85--115 Zinc, Total, ICP-MS 0.5 2.5 ug/L <MDL 20 20.4 102 85--115 Arsenic, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 19.3 96 85--115 Selenium, Total, ICP-MS 0.5 1 ug/L <MDL 20 20.3 102 85--115 Silver, Total, ICP-MS 0.04 0.2 ug/L <MDL 20 19 95 85--115 Cadmium, Total, ICP-MS 0.05 0.25 ug/L <MDL 20 19.2 96 85--115 Tin, Total, ICP-MS 0.3 1.5 ug/L <MDL 20 19.7 99 85--115 Antimony, Total, ICP-MS 0.3 1 ug/L <MDL 20 19.8 99 85--115 Barium, Total, ICP-MS 0.05 0.25 ug/L <MDL 20 18.8 94 85--115 Thallium, Total, ICP-MS 0.04 0.2 ug/L <MDL 20 20.2 101 85--115 Lead, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 20.3 101 85--115

LD:WG123247-3 L56320-2 Matrix: FRESH WTR Listtype:MTHARD-ICPMS Method:EPA 200.8/SW846 6020A*SM2340B Project:421422-CHSW-M Pkey:STD (Lab Duplicate)

Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimit Hardness, Calc 0.331 0.331 g CaCO3 63.1 60 5 0--20Page 5 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

LD:WG123247-3 L56320-2 Matrix: FRESH WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:421422-CHSW-M Pkey:STD (Lab Duplicate)

Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimit Beryllium, Total, ICP-MS 0.1 0.5 ug/L <MDL <MDL 0--20 Sodium, Total, ICP-MS 100 100 ug/L 6640 6180 7 0--20 Magnesium, Total, ICP-MS 50 50 ug/L 5550 5310 4 0--20 Aluminum, Total, ICP-MS 2 10 ug/L 110 104 5 0--20 Potassium, Total, ICP-MS 100 500 ug/L 1070 994 7 0--20 Calcium, Total, ICP-MS 50 50 ug/L 16100 15300 5 0--20 Vanadium, Total, ICP-MS 0.075 0.375 ug/L 1.54 1.37 11 0--20 Chromium, Total, ICP-MS 0.2 1 ug/L 0.29 0.27 0--20 Iron, Total, ICP-MS 10 50 ug/L 136 125 8 0--20 Manganese, Total, ICP-MS 0.1 0.5 ug/L 21.7 20.3 7 0--20 Cobalt, Total, ICP-MS 0.05 0.25 ug/L 0.081 0.082 0--20 Nickel, Total, ICP-MS 0.1 0.5 ug/L 0.29 0.29 0--20 Copper, Total, ICP-MS 0.4 2 ug/L 0.62 0.57 0--20 Zinc, Total, ICP-MS 0.5 2.5 ug/L 3.95 3.71 6 0--20 Arsenic, Total, ICP-MS 0.1 0.5 ug/L 0.46 0.43 0--20 Selenium, Total, ICP-MS 0.5 1 ug/L <MDL <MDL 0--20 Silver, Total, ICP-MS 0.04 0.2 ug/L <MDL <MDL 0--20 Cadmium, Total, ICP-MS 0.05 0.25 ug/L <MDL <MDL 0--20 Tin, Total, ICP-MS 0.3 1.5 ug/L <MDL <MDL 0--20 Antimony, Total, ICP-MS 0.3 1 ug/L <MDL <MDL 0--20 Barium, Total, ICP-MS 0.05 0.25 ug/L 6.84 6.33 8 0--20 Thallium, Total, ICP-MS 0.04 0.2 ug/L <MDL <MDL 0--20 Lead, Total, ICP-MS 0.1 0.5 ug/L 0.14 0.14 0--20

MS:WG123247-4 L56320-2 Matrix: FRESH WTR Listtype:MTHARD-ICPMS Method:EPA 200.8/SW846 6020A*SM2340B Project:421422-CHSW-M Pkey:STD (Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit Hardness, Calc 0.331 0.331 g CaCO3 63.1 33.1 89.6 80 75--125

MS:WG123247-4 L56320-2 Matrix: FRESH WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:421422-CHSW-M Pkey:STD (Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit Beryllium, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 18.7 93 75--125 Sodium, Total, ICP-MS 100 100 ug/L 6640 5000 10800 83 75--125 Magnesium, Total, ICP-MS 50 50 ug/L 5550 5000 9720 83 75--125 Aluminum, Total, ICP-MS 2 10 ug/L 110 20 126 4xRule 75--125 Potassium, Total, ICP-MS 100 500 ug/L 1070 5000 5890 97 75--125 Calcium, Total, ICP-MS 50 50 ug/L 16100 5000 19800 75 75--125Page 6 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

Vanadium, Total, ICP-MS 0.075 0.375 ug/L 1.54 20 21 97 75--125 Chromium, Total, ICP-MS 0.2 1 ug/L 0.29 20 20.2 99 75--125 Iron, Total, ICP-MS 10 50 ug/L 136 5000 5020 98 75--125 Manganese, Total, ICP-MS 0.1 0.5 ug/L 21.7 20 39.9 91 75--125 Cobalt, Total, ICP-MS 0.05 0.25 ug/L 0.081 20 18.7 93 75--125 Nickel, Total, ICP-MS 0.1 0.5 ug/L 0.29 20 19.6 97 75--125 Copper, Total, ICP-MS 0.4 2 ug/L 0.62 20 20.4 99 75--125 Zinc, Total, ICP-MS 0.5 2.5 ug/L 3.95 20 24 100 75--125 Arsenic, Total, ICP-MS 0.1 0.5 ug/L 0.46 20 19.3 94 75--125 Selenium, Total, ICP-MS 0.5 1 ug/L <MDL 20 19.4 97 75--125 Silver, Total, ICP-MS 0.04 0.2 ug/L <MDL 20 19.1 95 75--125 Cadmium, Total, ICP-MS 0.05 0.25 ug/L <MDL 20 19 95 75--125 Tin, Total, ICP-MS 0.3 1.5 ug/L <MDL 20 18.9 94 75--125 Antimony, Total, ICP-MS 0.3 1 ug/L <MDL 20 19.6 98 75--125 Barium, Total, ICP-MS 0.05 0.25 ug/L 6.84 20 25.2 92 75--125 Thallium, Total, ICP-MS 0.04 0.2 ug/L <MDL 20 20.1 100 75--125 Lead, Total, ICP-MS 0.1 0.5 ug/L 0.14 20 20.4 101 75--125



### WG125075

MB:WG125075-1 Matrix: BLANK WTR Listtype:MTHARD-ICPMS Method:EPA 200.8/SW846 6020A*SM2340B Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Hardness, Calc 0.331 0.331 g CaCO3 <MDL

MB:WG125075-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Magnesium, Total, ICP-MS 50 50 ug/L <MDL Calcium, Total, ICP-MS 50 50 ug/L <MDL

SB:WG125075-2 MB:WG125075-1 Matrix: BLANK WTR Listtype:MTHARD-ICPMS Method:EPA 200.8/SW846 6020A*SM2340B Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Hardness, Calc 0.331 0.331 g CaCO3 <MDL 33.1 32.7 99 85--115

SB:WG125075-2 MB:WG125075-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Magnesium, Total, ICP-MS 50 50 ug/L <MDL 5000 5000 100 85--115 Calcium, Total, ICP-MS 50 50 ug/L <MDL 5000 4840 97 85--115Page 7 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

LD:WG125075-3 L56989-1 Matrix: FRESH WTR Listtype:MTHARD-ICPMS Method:EPA 200.8/SW846 6020A*SM2340B Project:421162-300 Pkey:STD (Lab Duplicate)

Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimit Hardness, Calc 0.331 0.331 g CaCO3 25.6 25.2 1 0--20

LD:WG125075-3 L56989-1 Matrix: FRESH WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:421162-300 Pkey:STD (Lab Duplicate)

Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimit Magnesium, Total, ICP-MS 50 50 ug/L 2430 2370 3 0--20 Calcium, Total, ICP-MS 50 50 ug/L 6230 6190 1 0--20

MS:WG125075-4 L56989-1 Matrix: FRESH WTR Listtype:MTHARD-ICPMS Method:EPA 200.8/SW846 6020A*SM2340B Project:421162-300 Pkey:STD (Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit Hardness, Calc 0.331 0.331 g CaCO3 25.6 33.1 57.4 96 75--125

MS:WG125075-4 L56989-1 Matrix: FRESH WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:421162-300 Pkey:STD (Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit Magnesium, Total, ICP-MS 50 50 ug/L 2430 5000 7330 98 75--125 Calcium, Total, ICP-MS 50 50 ug/L 6230 5000 10900 93 75--125



### WG116464

MB:WG116464-1 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL

MB:WG116464-2 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL

MB:WG116464-3 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDLPage 8 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

SB:WG116464-4 MB:WG116464-1 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL 0.005 0.00486 97 77--123

MSD:WG116464-6 MS:WG116464-5 L53592-1 Matrix: EFFLUENT Listtype:MTHG-CVAF Method:EPA 1631E Project:421936 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Mercury, Total, CVAF 2E-04 5E-04 ug/L 0.00048 0.005 0.00558 102 71--125 0.005 0.00564 103 1 0--24

MSD:WG116464-8 MS:WG116464-7 L53619-13 Matrix: FRESH WTR Listtype:MTHG-CVAF Method:EPA 1631E Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Mercury, Total, CVAF 2E-04 5E-04 ug/L 0.00199 0.005 0.00677 96 71--125 0.005 0.00692 99 2 0--24



### WG116695

MB:WG116695-1 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL

MB:WG116695-2 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL

MB:WG116695-3 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL

SB:WG116695-4 MB:WG116695-1 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL 0.005 0.00465 93 77--123

MSD:WG116695-6 MS:WG116695-5 L53626-7 Matrix: SALT WTR Listtype:MTHG-CVAF Method:EPA 1631E Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Mercury, Total, CVAF 2E-04 5E-04 ug/L 0.00023 0.005 0.0042 79 71--125 0.005 0.00416 79 1 0--24Page 9 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

WG119056

MB:WG119056-1 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL

MB:WG119056-2 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL

MB:WG119056-3 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL

SB:WG119056-4 MB:WG119056-1 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL 0.005 0.00448 90 77--123

MSD:WG119056-6 MS:WG119056-5 L54782-2 Matrix: OTHR WTR Listtype:MTHG-CVAF Method:EPA 1631E Project:423258-500-1 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Mercury, Total, CVAF 2E-04 5E-04 ug/L 0.000588 0.005 0.00501 88 71--125 0.005 0.00502 89 0 0--24

MSD:WG119056-8 MS:WG119056-7 L54760-11 Matrix: FRESH WTR Listtype:MTHG-CVAF Method:EPA 1631E Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Mercury, Total, CVAF 2E-04 5E-04 ug/L 0.000608 0.005 0.00548 98 71--125 0.005 0.00525 93 4 0--24



### WG119177

MB:WG119177-1 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDLPage 10 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

MB:WG119177-2 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL

MB:WG119177-3 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL

SB:WG119177-4 MB:WG119177-1 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL 0.005 0.00467 93 77--123

MSD:WG119177-6 MS:WG119177-5 L54760-3 Matrix: FRESH WTR Listtype:MTHG-CVAF Method:EPA 1631E Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Mercury, Total, CVAF 2E-04 5E-04 ug/L 0.000656 0.005 0.00522 91 71--125 0.005 0.00554 98 6 0--24

MSD:WG119177-8 MS:WG119177-7 L54765-7 Matrix: SALT WTR Listtype:MTHG-CVAF Method:EPA 1631E Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Mercury, Total, CVAF 2E-04 5E-04 ug/L 0.00023 0.005 0.00479 91 71--125 0.005 0.00488 93 2 0--24



### WG122560

MB:WG122560-1 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL

MB:WG122560-2 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL

MB:WG122560-3 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDLPage 11 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

SB:WG122560-4 MB:WG122560-1 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL 0.005 0.00464 93 77--123

MSD:WG122560-6 MS:WG122560-5 L56061-1 Matrix: FRESH WTR Listtype:MTHG-CVAF Method:EPA 1631E Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Mercury, Total, CVAF 2E-04 5E-04 ug/L 0.00158 0.005 0.00653 99 71--125 0.005 0.00681 105 4 0--24



### WG122713

MB:WG122713-1 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL

MB:WG122713-2 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL

MB:WG122713-3 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL

SB:WG122713-4 MB:WG122713-1 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL 0.005 0.00499 100 77--123

MSD:WG122713-6 MS:WG122713-5 L56062-2 Matrix: SALT WTR Listtype:MTHG-CVAF Method:EPA 1631E Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL 0.005 0.00416 83 71--125 0.005 0.00425 85 2 0--24Page 12 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

WG122844

MB:WG122844-1 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL

MB:WG122844-2 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL

MB:WG122844-3 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL

SB:WG122844-4 MB:WG122844-1 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL 0.005 0.00472 94 77--123

MSD:WG122844-6 MS:WG122844-5 L56299-7 Matrix: EFFLUENT Listtype:MTHG-CVAF Method:EPA 1631E Project:421186B Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Mercury, Total, CVAF 2E-04 5E-04 ug/L 0.00274 0.005 0.00705 86 71--125 0.005 0.00698 85 1 0--24

MSD:WG122844-8 MS:WG122844-7 L56301-7 Matrix: EFFLUENT Listtype:MTHG-CVAF Method:EPA 1631E Project:421186B Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Mercury, Total, CVAF 2E-04 5E-04 ug/L 0.00293 0.005 0.00707 83 71--125 0.005 0.00671 76 5 0--24



### WG125309

MB:WG125309-1 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDLPage 13 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

MB:WG125309-2 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL

MB:WG125309-3 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL

SB:WG125309-4 MB:WG125309-1 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL 0.005 0.00508 102 77--123

MSD:WG125309-6 MS:WG125309-5 L56990-1 Matrix: SALT WTR Listtype:MTHG-CVAF Method:EPA 1631E Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Mercury, Total, CVAF 2E-04 5E-04 ug/L 0.00034 0.005 0.00544 102 71--125 0.005 0.00545 102 0 0--24

MSD:WG125309-8 MS:WG125309-7 L56990-10 Matrix: SALT WTR Listtype:MTHG-CVAF Method:EPA 1631E Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Mercury, Total, CVAF 2E-04 5E-04 ug/L 0.00036 0.005 0.00556 104 71--125 0.005 0.00554 104 0 0--24



### WG125324

MB:WG125324-1 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL

MB:WG125324-2 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL

MB:WG125324-3 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDLPage 14 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

SB:WG125324-4 MB:WG125324-1 Matrix: BLANK WTR Listtype:MTHG-CVAF Method:EPA 1631E Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Mercury, Total, CVAF 2E-04 5E-04 ug/L <MDL 0.005 0.00502 100 77--123

MSD:WG125324-6 MS:WG125324-5 L56989-1 Matrix: FRESH WTR Listtype:MTHG-CVAF Method:EPA 1631E Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Mercury, Total, CVAF 2E-04 5E-04 ug/L 0.00125 0.005 0.00597 94 71--125 0.005 0.00625 100 5 0--24



### WG116496

MB:WG116496-1 Matrix: BLANK WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L <MDL

MB:WG116496-2 Matrix: BLANK WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L <MDL

MB:WG116496-3 Matrix: BLANK WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L <MDL

SB:WG116496-4 MB:WG116496-1 Matrix: BLANK WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L <MDL 0.005 0.00475 95 77--123

MSD:WG116496-6 MS:WG116496-5 L53619-1 Matrix: FRESH WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L 0.00043 0.005 0.00531 98 71--125 0.005 0.00528 97 1 0--24

MSD:WG116496-8 MS:WG116496-7 L53626-10 Matrix: SALT WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L 0.00023 0.005 0.00502 96 71--125 0.005 0.00503 96 0 0--24Page 15 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

WG119081

MB:WG119081-1 Matrix: BLANK WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L <MDL

MB:WG119081-2 Matrix: BLANK WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L <MDL

MB:WG119081-3 Matrix: BLANK WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L <MDL

SB:WG119081-4 MB:WG119081-1 Matrix: BLANK WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L <MDL 0.005 0.00443 89 77--123

MSD:WG119081-6 MS:WG119081-5 L54760-1 Matrix: FRESH WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L 0.00033 0.005 0.00517 97 71--125 0.005 0.00486 90 6 0--24

MSD:WG119081-8 MS:WG119081-7 L54765-10 Matrix: SALT WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L <MDL 0.005 0.00441 88 71--125 0.005 0.00474 95 7 0--24



### WG122629

MB:WG122629-1 Matrix: BLANK WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L <MDLPage 16 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

MB:WG122629-2 Matrix: BLANK WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L <MDL

MB:WG122629-3 Matrix: BLANK WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L <MDL

SB:WG122629-4 MB:WG122629-1 Matrix: BLANK WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L <MDL 0.005 0.005 100 77--123

MSD:WG122629-6 MS:WG122629-5 L56061-1 Matrix: FRESH WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L 0.0003 0.005 0.00492 92 71--125 0.005 0.00533 101 8 0--24



### WG122712

MB:WG122712-1 Matrix: BLANK WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L <MDL

MB:WG122712-2 Matrix: BLANK WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L <MDL

MB:WG122712-3 Matrix: BLANK WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L <MDL

SB:WG122712-4 MB:WG122712-1 Matrix: BLANK WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L <MDL 0.005 0.00511 102 77--123Page 17 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

MSD:WG122712-6 MS:WG122712-5 L56062-10 Matrix: SALT WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L <MDL 0.005 0.00403 81 71--125 0.005 0.00414 83 3 0--24



### WG124900

MB:WG124900-1 Matrix: BLANK WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L <MDL

MB:WG124900-2 Matrix: BLANK WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L <MDL

MB:WG124900-3 Matrix: BLANK WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L <MDL

SB:WG124900-4 MB:WG124900-1 Matrix: BLANK WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L <MDL 0.005 0.00511 102 77--123

MSD:WG124900-6 MS:WG124900-5 L56989-1 Matrix: FRESH WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L 0.000884 0.005 0.00577 98 71--125 0.005 0.00579 98 0 0--24

MSD:WG124900-8 MS:WG124900-7 L56990-10 Matrix: SALT WTR Listtype:MTHG-CVAF-DISS Method:EPA 1631E Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Mercury, Dissolved, CVAF 2E-04 5E-04 ug/L <MDL 0.005 0.00437 87 71--125 0.005 0.00429 86 2 0--24Page 18 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

WG116281

MB:WG116281-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS-SEA Method:EPA 1640 Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Chromium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL Nickel, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL Copper, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL Zinc, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL Arsenic, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL Silver, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL Cadmium, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL Antimony, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL Lead, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL

SB:WG116281-2 MB:WG116281-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS-SEA Method:EPA 1640 Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Chromium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 0.25 0.25 99 75--125 Nickel, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL 1.25 1.09 87 75--125 Copper, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL 1.25 1.08 86 75--125 Zinc, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 1.25 0.94 75 75--125 Arsenic, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL 1.25 1.24 100 75--125 Silver, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL 0.25 0.218 87 75--125 Cadmium, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.25 0.224 90 75--125 Antimony, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.25 0.245 98 75--125 Lead, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.25 0.238 95 75--125

MSD:WG116281-4 MS:WG116281-3 L53619-2 Matrix: FRESH WTR Listtype:MTICPMS-DISS-SEA Method:EPA 1640 Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Chromium, Dissolved, ICP-MS 0.05 0.25 ug/L 0.057 0.25 0.311 102 70--130 0.25 0.321 106 3 0--20 Nickel, Dissolved, ICP-MS 0.025 0.125 ug/L 0.216 1.25 1.49 102 70--130 1.25 1.73 121 15 0--20 Copper, Dissolved, ICP-MS 0.025 0.125 ug/L 0.306 1.25 1.5 96 70--130 1.25 1.42 89 6 0--20 Zinc, Dissolved, ICP-MS 0.1 0.5 ug/L 0.47 1.25 1.42 76 70--130 1.25 1.62 92 13 0--20 Arsenic, Dissolved, ICP-MS 0.01 0.05 ug/L 0.407 1.25 1.55 92 70--130 1.25 1.64 98 5 0--20 Silver, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL 0.25 0.237 95 70--130 0.25 0.249 100 5 0--20 Cadmium, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.25 0.214 86 70--130 0.25 0.237 95 10 0--20 Antimony, Dissolved, ICP-MS 0.005 0.025 ug/L 0.0342 0.25 0.346 125 70--130 0.25 0.359 130 3 0--20 Lead, Dissolved, ICP-MS 0.005 0.025 ug/L 0.013 0.25 0.229 86 70--130 0.25 0.259 99 12 0--20Page 19 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

WG117861

MB:WG117861-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS-SEA Method:EPA 1640 Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Chromium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL Nickel, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL Copper, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL Zinc, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL Arsenic, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL Silver, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL Cadmium, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL Antimony, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL Lead, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL

SB:WG117861-2 MB:WG117861-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS-SEA Method:EPA 1640 Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Chromium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 0.25 0.24 98 75--125 Nickel, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL 1.25 1.14 91 75--125 Copper, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL 1.25 1.09 87 75--125 Zinc, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 1.25 0.951 76 75--125 Arsenic, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL 1.25 1.22 98 75--125 Silver, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL 0.25 0.25 100 75--125 Cadmium, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.25 0.243 97 75--125 Antimony, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.25 0.236 94 75--125 Lead, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.25 0.247 99 75--125

MSD:WG117861-4 MS:WG117861-3 L53626-1 Matrix: SALT WTR Listtype:MTICPMS-DISS-SEA Method:EPA 1640 Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Chromium, Dissolved, ICP-MS 0.05 0.25 ug/L 0.099 0.25 0.35 100 70--130 0.25 0.351 101 0 0--20 Nickel, Dissolved, ICP-MS 0.025 0.125 ug/L 0.405 1.25 1.62 97 70--130 1.25 1.61 97 0 0--20 Copper, Dissolved, ICP-MS 0.025 0.125 ug/L 0.348 1.25 1.47 89 70--130 1.25 1.44 87 2 0--20 Zinc, Dissolved, ICP-MS 0.1 0.5 ug/L 0.635 1.25 1.62 79 70--130 1.25 1.62 79 0 0--20 Arsenic, Dissolved, ICP-MS 0.01 0.05 ug/L 1.15 1.25 2.35 96 70--130 1.25 2.34 95 1 0--20 Silver, Dissolved, ICP-MS 0.01 0.05 ug/L 0.019 0.25 0.285 106 70--130 0.25 0.286 107 0 0--20 Cadmium, Dissolved, ICP-MS 0.005 0.025 ug/L 0.0566 0.25 0.291 94 70--130 0.25 0.289 93 1 0--20 Antimony, Dissolved, ICP-MS 0.005 0.025 ug/L 0.157 0.25 0.383 90 70--130 0.25 0.377 88 2 0--20 Lead, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.25 0.256 103 70--130 0.25 0.255 102 1 0--20Page 20 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

WG119280

MB:WG119280-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS-SEA Method:EPA 1640 Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Chromium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL Nickel, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL Copper, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL Zinc, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL Arsenic, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL Silver, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL Cadmium, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL Antimony, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL Lead, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL

SB:WG119280-2 MB:WG119280-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS-SEA Method:EPA 1640 Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Chromium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 0.5 0.492 98 75--125 Nickel, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL 1.5 1.37 92 75--125 Copper, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL 1.5 1.35 90 75--125 Zinc, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 1.5 1.4 93 75--125 Arsenic, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL 1.5 1.4 93 75--125 Silver, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL 0.5 0.49 98 75--125 Cadmium, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.468 94 75--125 Antimony, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.501 100 75--125 Lead, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.473 95 75--125

MSD:WG119280-4 MS:WG119280-3 L54760-2 Matrix: FRESH WTR Listtype:MTICPMS-DISS-SEA Method:EPA 1640 Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Chromium, Dissolved, ICP-MS 0.05 0.25 ug/L 0.086 0.5 0.617 106 70--130 0.5 0.621 107 1 0--20 Nickel, Dissolved, ICP-MS 0.025 0.125 ug/L 0.981 1.5 2.63 110 70--130 1.5 2.66 112 1 0--20 Copper, Dissolved, ICP-MS 0.025 0.125 ug/L 0.377 1.5 1.8 95 70--130 1.5 1.84 98 2 0--20 Zinc, Dissolved, ICP-MS 0.1 0.5 ug/L 0.988 1.5 2.38 92 70--130 1.5 2.41 95 1 0--20 Arsenic, Dissolved, ICP-MS 0.01 0.05 ug/L 0.459 1.5 2.11 110 70--130 1.5 2.1 110 1 0--20 Silver, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL 0.5 0.502 100 70--130 0.5 0.509 102 1 0--20 Cadmium, Dissolved, ICP-MS 0.005 0.025 ug/L 0.019 0.5 0.449 86 70--130 0.5 0.462 89 3 0--20 Antimony, Dissolved, ICP-MS 0.005 0.025 ug/L 0.0584 0.5 0.548 98 70--130 0.5 0.526 94 4 0--20 Lead, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.385 77 70--130 0.5 0.381 76 1 0--20Page 21 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

WG119326

MB:WG119326-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS-SEA Method:EPA 1640 Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Chromium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL Nickel, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL Copper, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL Zinc, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL Arsenic, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL Silver, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL Cadmium, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL Antimony, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL Lead, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL

SB:WG119326-2 MB:WG119326-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS-SEA Method:EPA 1640 Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Chromium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 0.5 0.489 98 75--125 Nickel, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL 1.5 1.48 99 75--125 Copper, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL 1.5 1.41 94 75--125 Zinc, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 1.5 1.42 95 75--125 Arsenic, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL 1.5 1.43 95 75--125 Silver, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL 0.5 0.477 95 75--125 Cadmium, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.45 90 75--125 Antimony, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.444 89 75--125 Lead, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.445 89 75--125

MSD:WG119326-4 MS:WG119326-3 L54765-10 Matrix: SALT WTR Listtype:MTICPMS-DISS-SEA Method:EPA 1640 Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Chromium, Dissolved, ICP-MS 0.05 0.25 ug/L 0.1 0.5 0.639 108 70--130 0.5 0.605 101 5 0--20 Nickel, Dissolved, ICP-MS 0.025 0.125 ug/L 0.395 1.5 1.98 106 70--130 1.5 1.89 100 5 0--20 Copper, Dissolved, ICP-MS 0.025 0.125 ug/L 0.283 1.5 1.83 103 70--130 1.5 1.74 97 5 0--20 Zinc, Dissolved, ICP-MS 0.1 0.5 ug/L 0.46 1.5 2.02 104 70--130 1.5 1.84 91 10 0--20 Arsenic, Dissolved, ICP-MS 0.01 0.05 ug/L 1.46 1.5 3.08 108 70--130 1.5 2.99 102 3 0--20 Silver, Dissolved, ICP-MS 0.01 0.05 ug/L 0.026 0.5 0.57 109 70--130 0.5 0.526 100 8 0--20 Cadmium, Dissolved, ICP-MS 0.005 0.025 ug/L 0.0749 0.5 0.563 98 70--130 0.5 0.529 91 6 0--20 Antimony, Dissolved, ICP-MS 0.005 0.025 ug/L 0.171 0.5 0.681 102 70--130 0.5 0.633 92 7 0--20 Lead, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.48 96 70--130 0.5 0.445 89 8 0--20Page 22 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

WG122900

MB:WG122900-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS-SEA Method:EPA 1640 Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Chromium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL Silver, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL Arsenic, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL Antimony, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL Nickel, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL Copper, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL Zinc, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL Cadmium, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL Lead, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL

SB:WG122900-2 MB:WG122900-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS-SEA Method:EPA 1640 Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Chromium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 0.5 0.482 96 75--125 Silver, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL 0.5 0.498 100 75--125 Arsenic, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL 1.5 1.6 107 75--125 Nickel, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL 1.5 1.5 100 75--125 Copper, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL 1.5 1.39 93 75--125 Zinc, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 1.5 1.39 93 75--125 Cadmium, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.508 102 75--125 Lead, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.517 103 75--125

MSD:WG122900-4 MS:WG122900-3 L56061-2 Matrix: FRESH WTR Listtype:MTICPMS-DISS-SEA Method:EPA 1640 Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Chromium, Dissolved, ICP-MS 0.05 0.25 ug/L 0.07 0.5 0.564 99 70--130 0.5 0.557 97 1 0--20 Silver, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL 0.5 0.491 98 70--130 0.5 0.488 98 1 0--20 Arsenic, Dissolved, ICP-MS 0.01 0.05 ug/L 0.55 1.5 2.18 109 70--130 1.5 2.09 103 4 0--20 Nickel, Dissolved, ICP-MS 0.025 0.125 ug/L 0.26 1.5 1.77 101 70--130 1.5 1.76 100 1 0--20 Copper, Dissolved, ICP-MS 0.025 0.125 ug/L 0.44 1.5 2.18 116 70--130 1.5 2.16 115 1 0--20 Zinc, Dissolved, ICP-MS 0.1 0.5 ug/L 0.813 1.5 2.44 109 70--130 1.5 2.35 102 4 0--20 Cadmium, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.52 104 70--130 0.5 0.527 105 1 0--20 Lead, Dissolved, ICP-MS 0.005 0.025 ug/L 0.017 0.5 0.519 100 70--130 0.5 0.52 101 0 0--20Page 23 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

WG123691

MB:WG123691-1 Matrix: SALT WTR Listtype:MTICPMS-DISS-SEA Method:EPA 1640 Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Chromium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL Silver, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL Arsenic, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL Antimony, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL Nickel, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL Copper, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL Zinc, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL Cadmium, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL Lead, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL

SB:WG123691-2 MB:WG123691-1 Matrix: SALT WTR Listtype:MTICPMS-DISS-SEA Method:EPA 1640 Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Chromium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 0.5 0.469 94 75--125 Silver, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL 0.5 0.477 95 75--125 Arsenic, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL 1.5 1.55 103 75--125 Antimony, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.477 95 75--125 Nickel, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL 1.5 1.56 104 75--125 Copper, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL 1.5 1.42 95 75--125 Zinc, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 1.5 1.54 102 75--125 Cadmium, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.48 96 75--125 Lead, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.455 91 75--125

MSD:WG123691-4 MS:WG123691-3 L56062-7 Matrix: SALT WTR Listtype:MTICPMS-DISS-SEA Method:EPA 1640 Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Chromium, Dissolved, ICP-MS 0.05 0.25 ug/L 0.18 0.5 0.623 89 70--130 0.5 0.621 88 0 0--20 Silver, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL 0.5 0.482 96 70--130 0.5 0.479 96 1 0--20 Arsenic, Dissolved, ICP-MS 0.01 0.05 ug/L 1.28 1.5 2.85 105 70--130 1.5 2.87 106 1 0--20 Antimony, Dissolved, ICP-MS 0.005 0.025 ug/L 0.143 0.5 0.588 89 70--130 0.5 0.582 88 1 0--20 Nickel, Dissolved, ICP-MS 0.025 0.125 ug/L 0.406 1.5 1.95 103 70--130 1.5 1.95 103 0 0--20 Copper, Dissolved, ICP-MS 0.025 0.125 ug/L 0.387 1.5 1.91 102 70--130 1.5 1.89 100 1 0--20 Zinc, Dissolved, ICP-MS 0.1 0.5 ug/L 0.571 1.5 1.96 93 70--130 1.5 1.96 93 0 0--20 Cadmium, Dissolved, ICP-MS 0.005 0.025 ug/L 0.0618 0.5 0.567 101 70--130 0.5 0.558 99 2 0--20 Lead, Dissolved, ICP-MS 0.005 0.025 ug/L 0.0063 0.5 0.492 97 70--130 0.5 0.485 96 2 0--20Page 24 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

WG124746

MB:WG124746-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS-SEA Method:EPA 1640 Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Chromium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL Silver, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL Arsenic, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL Antimony, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL Nickel, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL Copper, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL Zinc, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL Cadmium, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL Lead, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL

SB:WG124746-2 MB:WG124746-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS-SEA Method:EPA 1640 Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Chromium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 0.5 0.463 93 75--125 Silver, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL 0.5 0.485 97 75--125 Arsenic, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL 1.5 1.56 104 75--125 Nickel, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL 1.5 1.52 101 75--125 Copper, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL 1.5 1.43 95 75--125 Zinc, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 1.5 1.36 91 75--125 Cadmium, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.518 104 75--125 Lead, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.522 104 75--125

MSD:WG124746-4 MS:WG124746-3 L56989-1 Matrix: FRESH WTR Listtype:MTICPMS-DISS-SEA Method:EPA 1640 Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Chromium, Dissolved, ICP-MS 0.05 0.25 ug/L 0.072 0.5 0.598 105 70--130 0.5 0.546 95 9 0--20 Silver, Dissolved, ICP-MS 0.01 0.05 ug/L 0.022 0.5 0.501 96 70--130 0.5 0.494 94 2 0--20 Arsenic, Dissolved, ICP-MS 0.01 0.05 ug/L 0.401 1.5 1.95 104 70--130 1.5 1.91 100 2 0--20 Nickel, Dissolved, ICP-MS 0.025 0.125 ug/L 0.156 1.5 1.5 90 70--130 1.5 1.52 91 1 0--20 Copper, Dissolved, ICP-MS 0.025 0.125 ug/L 0.507 1.5 1.98 98 70--130 1.5 1.96 97 1 0--20 Zinc, Dissolved, ICP-MS 0.1 0.5 ug/L 0.628 1.5 1.99 91 70--130 1.5 2.03 93 2 0--20 Cadmium, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.523 105 70--130 0.5 0.525 105 0 0--20 Lead, Dissolved, ICP-MS 0.005 0.025 ug/L 0.022 0.5 0.544 104 70--130 0.5 0.546 105 0 0--20Page 25 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

WG124855

MB:WG124855-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS-SEA Method:EPA 1640 Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Chromium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL Silver, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL Arsenic, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL Antimony, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL Nickel, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL Copper, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL Zinc, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL Cadmium, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL Lead, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL

SB:WG124855-2 MB:WG124855-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS-SEA Method:EPA 1640 Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Chromium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 0.5 0.538 108 75--125 Silver, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL 0.5 0.513 103 75--125 Arsenic, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL 1.5 1.57 104 75--125 Antimony, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.517 103 75--125 Nickel, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL 1.5 1.67 111 75--125 Copper, Dissolved, ICP-MS 0.025 0.125 ug/L <MDL 1.5 1.5 100 75--125 Zinc, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 1.5 1.52 101 75--125 Cadmium, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.498 100 75--125 Lead, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.494 99 75--125

MSD:WG124855-4 MS:WG124855-3 L56990-9 Matrix: SALT WTR Listtype:MTICPMS-DISS-SEA Method:EPA 1640 Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Chromium, Dissolved, ICP-MS 0.05 0.25 ug/L 0.091 0.5 0.612 104 70--130 0.5 0.615 105 0 0--20 Silver, Dissolved, ICP-MS 0.01 0.05 ug/L <MDL 0.5 0.569 114 70--130 0.5 0.542 108 5 0--20 Arsenic, Dissolved, ICP-MS 0.01 0.05 ug/L 1.45 1.5 2.9 97 70--130 1.5 2.96 101 2 0--20 Antimony, Dissolved, ICP-MS 0.005 0.025 ug/L 0.165 0.5 0.637 95 70--130 0.5 0.641 95 1 0--20 Nickel, Dissolved, ICP-MS 0.025 0.125 ug/L 0.424 1.5 2.08 110 70--130 1.5 2.07 110 0 0--20 Copper, Dissolved, ICP-MS 0.025 0.125 ug/L 0.266 1.5 1.74 98 70--130 1.5 1.78 101 3 0--20 Zinc, Dissolved, ICP-MS 0.1 0.5 ug/L 0.35 1.5 1.89 103 70--130 1.5 1.82 98 4 0--20 Cadmium, Dissolved, ICP-MS 0.005 0.025 ug/L 0.0717 0.5 0.565 99 70--130 0.5 0.57 100 1 0--20 Lead, Dissolved, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.493 99 70--130 0.5 0.494 99 0 0--20Page 26 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

WG116287

SB:WG116287-1 MB:WG116287-3 Matrix: BLANK WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Chromium, Total, ICP-MS 0.05 0.25 ug/L <MDL 0.25 0.24 97 75--125 Nickel, Total, ICP-MS 0.025 0.125 ug/L <MDL 1.25 1.22 97 75--125 Copper, Total, ICP-MS 0.025 0.125 ug/L 0.037 1.25 1.08 83 75--125 Zinc, Total, ICP-MS 0.1 0.5 ug/L <MDL 1.25 0.98 78 75--125 Arsenic, Total, ICP-MS 0.01 0.05 ug/L <MDL 1.25 1.2 96 75--125 Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL 0.25 0.232 93 75--125 Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.25 0.241 96 75--125 Antimony, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.25 0.267 107 75--125 Lead, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.25 0.248 99 75--125

SB:WG116287-2 MB:WG116287-4 Matrix: BLANK WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Chromium, Total, ICP-MS 0.05 0.25 ug/L <MDL 0.25 0.24 97 75--125 Nickel, Total, ICP-MS 0.025 0.125 ug/L <MDL 1.25 1.22 97 75--125 Copper, Total, ICP-MS 0.025 0.125 ug/L 0.029 1.25 1.08 84 75--125 Zinc, Total, ICP-MS 0.1 0.5 ug/L <MDL 1.25 0.984 79 75--125 Arsenic, Total, ICP-MS 0.01 0.05 ug/L <MDL 1.25 1.2 96 75--125 Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL 0.25 0.235 94 75--125 Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.25 0.239 96 75--125 Antimony, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.25 0.267 107 75--125 Lead, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.25 0.246 99 75--125

MB:WG116287-3 Matrix: BLANK WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Chromium, Total, ICP-MS 0.05 0.25 ug/L <MDL Nickel, Total, ICP-MS 0.025 0.125 ug/L <MDL Copper, Total, ICP-MS 0.025 0.125 ug/L 0.037 B Zinc, Total, ICP-MS 0.1 0.5 ug/L <MDL Arsenic, Total, ICP-MS 0.01 0.05 ug/L <MDL Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL Antimony, Total, ICP-MS 0.005 0.025 ug/L <MDL Lead, Total, ICP-MS 0.005 0.025 ug/L <MDLPage 27 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

MB:WG116287-4 Matrix: BLANK WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Chromium, Total, ICP-MS 0.05 0.25 ug/L <MDL Nickel, Total, ICP-MS 0.025 0.125 ug/L <MDL Copper, Total, ICP-MS 0.025 0.125 ug/L 0.029 B Zinc, Total, ICP-MS 0.1 0.5 ug/L <MDL Arsenic, Total, ICP-MS 0.01 0.05 ug/L <MDL Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL Antimony, Total, ICP-MS 0.005 0.025 ug/L <MDL Lead, Total, ICP-MS 0.005 0.025 ug/L <MDL

MSD:WG116287-6 MS:WG116287-5 L53619-1 Matrix: FRESH WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Chromium, Total, ICP-MS 0.05 0.25 ug/L 0.12 0.25 0.354 95 70--130 0.25 0.336 88 5 0--20 Nickel, Total, ICP-MS 0.025 0.125 ug/L 0.312 1.25 1.73 113 70--130 1.25 1.7 111 2 0--20 Copper, Total, ICP-MS 0.025 0.125 ug/L 0.613 1.25 1.97 108 70--130 1.25 1.95 107 1 0--20 Zinc, Total, ICP-MS 0.1 0.5 ug/L 0.867 1.25 2.01 91 70--130 1.25 1.98 89 1 0--20 Arsenic, Total, ICP-MS 0.01 0.05 ug/L 0.506 1.25 1.65 92 70--130 1.25 1.62 89 2 0--20 Silver, Total, ICP-MS 0.01 0.05 ug/L 0.01 0.25 0.24 92 70--130 0.25 0.244 94 2 0--20 Cadmium, Total, ICP-MS 0.005 0.025 ug/L 0.0053 0.25 0.243 95 70--130 0.25 0.242 95 0 0--20 Antimony, Total, ICP-MS 0.005 0.025 ug/L 0.0367 0.25 0.262 90 70--130 0.25 0.258 89 1 0--20 Lead, Total, ICP-MS 0.005 0.025 ug/L 0.0681 0.25 0.304 94 70--130 0.25 0.302 94 0 0--20

MSD:WG116287-8 MS:WG116287-7 L53619-3 Matrix: FRESH WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Chromium, Total, ICP-MS 0.05 0.25 ug/L 0.11 0.25 0.344 93 70--130 0.25 0.393 113 13 0--20 Nickel, Total, ICP-MS 0.025 0.125 ug/L 0.271 1.25 1.7 114 70--130 1.25 1.73 117 2 0--20 Copper, Total, ICP-MS 0.025 0.125 ug/L 0.656 1.25 2.09 115 70--130 1.25 2 108 4 0--20 Zinc, Total, ICP-MS 0.1 0.5 ug/L 0.938 1.25 2.11 94 70--130 1.25 2.03 87 4 0--20 Arsenic, Total, ICP-MS 0.01 0.05 ug/L 0.485 1.25 1.61 90 70--130 1.25 1.54 84 4 0--20 Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL 0.25 0.245 98 70--130 0.25 0.242 97 1 0--20 Cadmium, Total, ICP-MS 0.005 0.025 ug/L 0.0052 0.25 0.248 97 70--130 0.25 0.25 98 0 0--20 Antimony, Total, ICP-MS 0.005 0.025 ug/L 0.0362 0.25 0.26 90 70--130 0.25 0.27 93 4 0--20 Lead, Total, ICP-MS 0.005 0.025 ug/L 0.092 0.25 0.338 98 70--130 0.25 0.334 97 1 0--20Page 28 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

WG116666

SB:WG116666-2 MB:WG116666-4 Matrix: BLANK WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Chromium, Total, ICP-MS 0.05 0.25 ug/L <MDL 0.25 0.25 98 75--125 Nickel, Total, ICP-MS 0.025 0.125 ug/L <MDL 1.25 1.16 92 75--125 Copper, Total, ICP-MS 0.025 0.125 ug/L <MDL 1.25 1.13 90 75--125 Zinc, Total, ICP-MS 0.1 0.5 ug/L <MDL 1.25 0.999 80 75--125 Arsenic, Total, ICP-MS 0.01 0.05 ug/L <MDL 1.25 1.18 94 75--125 Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL 0.25 0.26 104 75--125 Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.25 0.247 99 75--125 Antimony, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.25 0.238 95 75--125 Lead, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.25 0.252 101 75--125

MB:WG116666-4 Matrix: BLANK WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Chromium, Total, ICP-MS 0.05 0.25 ug/L <MDL Nickel, Total, ICP-MS 0.025 0.125 ug/L <MDL Copper, Total, ICP-MS 0.025 0.125 ug/L <MDL Zinc, Total, ICP-MS 0.1 0.5 ug/L <MDL Arsenic, Total, ICP-MS 0.01 0.05 ug/L <MDL Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL Antimony, Total, ICP-MS 0.005 0.025 ug/L <MDL Lead, Total, ICP-MS 0.005 0.025 ug/L <MDL

MSD:WG116666-8 MS:WG116666-7 L53626-1 Matrix: SALT WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Chromium, Total, ICP-MS 0.05 0.25 ug/L 0.088 0.25 0.333 98 70--130 0.25 0.332 98 0 0--20 Nickel, Total, ICP-MS 0.025 0.125 ug/L 0.421 1.25 1.63 97 70--130 1.25 1.6 95 2 0--20 Copper, Total, ICP-MS 0.025 0.125 ug/L 0.377 1.25 1.5 90 70--130 1.25 1.47 87 2 0--20 Zinc, Total, ICP-MS 0.5 2.5 ug/L 0.89 1.25 2.3 110 70--130 1.25 2.1 95 9 0--20 Arsenic, Total, ICP-MS 0.01 0.05 ug/L 1.11 1.25 2.23 90 70--130 1.25 2.18 85 2 0--20 Silver, Total, ICP-MS 0.01 0.05 ug/L 0.016 0.25 0.28 106 70--130 0.25 0.282 107 1 0--20 Cadmium, Total, ICP-MS 0.005 0.025 ug/L 0.0636 0.25 0.308 98 70--130 0.25 0.304 96 1 0--20 Antimony, Total, ICP-MS 0.005 0.025 ug/L 0.154 0.25 0.372 87 70--130 0.25 0.368 86 1 0--20 Lead, Total, ICP-MS 0.005 0.025 ug/L 0.0091 0.25 0.268 103 70--130 0.25 0.259 100 3 0--20Page 29 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

WG118832

MB:WG118832-1 Matrix: BLANK WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Chromium, Total, ICP-MS 0.05 0.25 ug/L <MDL Nickel, Total, ICP-MS 0.025 0.125 ug/L <MDL Copper, Total, ICP-MS 0.025 0.125 ug/L <MDL Zinc, Total, ICP-MS 0.1 0.5 ug/L <MDL Arsenic, Total, ICP-MS 0.01 0.05 ug/L <MDL Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL Antimony, Total, ICP-MS 0.005 0.025 ug/L <MDL Lead, Total, ICP-MS 0.005 0.025 ug/L <MDL



### WG119016

MB:WG119016-1 Matrix: BLANK WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Chromium, Total, ICP-MS 0.05 0.25 ug/L <MDL Nickel, Total, ICP-MS 0.025 0.125 ug/L <MDL Copper, Total, ICP-MS 0.025 0.125 ug/L 0.026 B Zinc, Total, ICP-MS 0.1 0.5 ug/L <MDL Arsenic, Total, ICP-MS 0.01 0.05 ug/L <MDL Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL Lead, Total, ICP-MS 0.005 0.025 ug/L <MDL

SB:WG119016-2 MB:WG119016-1 Matrix: BLANK WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Chromium, Total, ICP-MS 0.05 0.25 ug/L <MDL 0.5 0.489 98 75--125 Nickel, Total, ICP-MS 0.025 0.125 ug/L <MDL 1.5 1.49 99 75--125 Copper, Total, ICP-MS 0.025 0.125 ug/L 0.026 1.5 1.48 97 75--125 Zinc, Total, ICP-MS 0.1 0.5 ug/L <MDL 1.5 1.38 92 75--125 Arsenic, Total, ICP-MS 0.01 0.05 ug/L <MDL 1.5 1.46 97 75--125 Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL 0.5 0.497 99 75--125 Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.535 107 75--125 Lead, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.476 95 75--125Page 30 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

MSD:WG119016-4 MS:WG119016-3 L54760-2 Matrix: FRESH WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Chromium, Total, ICP-MS 0.05 0.25 ug/L 0.18 0.5 0.678 101 70--130 0.5 0.696 104 3 0--20 Nickel, Total, ICP-MS 0.025 0.125 ug/L 0.951 1.5 2.7 117 70--130 1.5 2.72 118 1 0--20 Copper, Total, ICP-MS 0.025 0.125 ug/L 0.894 1.5 2.43 102 70--130 1.5 2.4 100 1 0--20 Zinc, Total, ICP-MS 0.1 0.5 ug/L 1.28 1.5 2.67 93 70--130 1.5 2.65 91 1 0--20 Arsenic, Total, ICP-MS 0.01 0.05 ug/L 0.656 1.5 2.19 102 70--130 1.5 2.19 102 0 0--20 Silver, Total, ICP-MS 0.01 0.05 ug/L 0.012 0.5 0.475 93 70--130 0.5 0.471 92 1 0--20 Cadmium, Total, ICP-MS 0.005 0.025 ug/L 0.016 0.5 0.51 99 70--130 0.5 0.493 95 3 0--20 Lead, Total, ICP-MS 0.005 0.025 ug/L 0.0572 0.5 0.467 82 70--130 0.5 0.454 79 3 0--20



### WG119157

MB:WG119157-1 Matrix: BLANK WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Chromium, Total, ICP-MS 0.05 0.25 ug/L <MDL Nickel, Total, ICP-MS 0.025 0.125 ug/L <MDL Copper, Total, ICP-MS 0.025 0.125 ug/L <MDL Zinc, Total, ICP-MS 0.1 0.5 ug/L <MDL Arsenic, Total, ICP-MS 0.01 0.05 ug/L <MDL Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL Antimony, Total, ICP-MS 0.005 0.025 ug/L <MDL Lead, Total, ICP-MS 0.005 0.025 ug/L <MDL

SB:WG119157-2 MB:WG119157-1 Matrix: BLANK WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Chromium, Total, ICP-MS 0.05 0.25 ug/L <MDL 0.5 0.473 95 75--125 Nickel, Total, ICP-MS 0.025 0.125 ug/L <MDL 1.5 1.38 92 75--125 Copper, Total, ICP-MS 0.025 0.125 ug/L <MDL 1.5 1.3 87 75--125 Zinc, Total, ICP-MS 0.1 0.5 ug/L <MDL 1.5 1.38 92 75--125 Arsenic, Total, ICP-MS 0.01 0.05 ug/L <MDL 1.5 1.44 96 75--125 Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL 0.5 0.484 97 75--125 Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.477 95 75--125 Antimony, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.49 98 75--125 Lead, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.477 95 75--125Page 31 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

MSD:WG119157-4 MS:WG119157-3 L54760-3 Matrix: FRESH WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Chromium, Total, ICP-MS 0.05 0.25 ug/L 0.18 0.5 0.734 111 70--130 0.5 0.719 108 2 0--20 Nickel, Total, ICP-MS 0.025 0.125 ug/L 0.748 1.5 2.52 118 70--130 1.5 2.54 120 1 0--20 Copper, Total, ICP-MS 0.025 0.125 ug/L 0.636 1.5 2.16 102 70--130 1.5 2.13 100 1 0--20 Zinc, Total, ICP-MS 0.1 0.5 ug/L 1.32 1.5 2.82 100 70--130 1.5 2.86 102 1 0--20 Arsenic, Total, ICP-MS 0.01 0.05 ug/L 0.659 1.5 2.26 107 70--130 1.5 2.4 116 6 0--20 Silver, Total, ICP-MS 0.01 0.05 ug/L 0.011 0.5 0.517 101 70--130 0.5 0.528 103 2 0--20 Cadmium, Total, ICP-MS 0.005 0.025 ug/L 0.023 0.5 0.509 97 70--130 0.5 0.502 96 1 0--20 Antimony, Total, ICP-MS 0.005 0.025 ug/L 0.062 0.5 0.537 95 70--130 0.5 0.568 101 6 0--20 Lead, Total, ICP-MS 0.005 0.025 ug/L 0.0566 0.5 0.475 84 70--130 0.5 0.469 83 1 0--20



### WG119325

MB:WG119325-1 Matrix: BLANK WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Chromium, Total, ICP-MS 0.05 0.25 ug/L <MDL Nickel, Total, ICP-MS 0.025 0.125 ug/L <MDL Copper, Total, ICP-MS 0.025 0.125 ug/L <MDL Zinc, Total, ICP-MS 0.1 0.5 ug/L <MDL Arsenic, Total, ICP-MS 0.01 0.05 ug/L <MDL Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL Antimony, Total, ICP-MS 0.005 0.025 ug/L <MDL Lead, Total, ICP-MS 0.005 0.025 ug/L <MDL

SB:WG119325-2 MB:WG119325-1 Matrix: BLANK WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Chromium, Total, ICP-MS 0.05 0.25 ug/L <MDL 0.5 0.493 99 75--125 Nickel, Total, ICP-MS 0.025 0.125 ug/L <MDL 1.5 1.35 90 75--125 Copper, Total, ICP-MS 0.025 0.125 ug/L <MDL 1.5 1.4 93 75--125 Zinc, Total, ICP-MS 0.1 0.5 ug/L <MDL 1.5 1.47 98 75--125 Arsenic, Total, ICP-MS 0.01 0.05 ug/L <MDL 1.5 1.33 89 75--125 Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL 0.5 0.5 100 75--125 Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.468 94 75--125 Antimony, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.534 107 75--125 Lead, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.456 91 75--125Page 32 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

MSD:WG119325-4 MS:WG119325-3 L54765-8 Matrix: SALT WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Chromium, Total, ICP-MS 0.05 0.25 ug/L 0.11 0.5 0.611 100 70--130 0.5 0.633 104 4 0--20 Nickel, Total, ICP-MS 0.025 0.125 ug/L 0.434 1.5 2 105 70--130 1.5 1.91 98 5 0--20 Copper, Total, ICP-MS 0.025 0.125 ug/L 0.385 1.5 1.88 100 70--130 1.5 1.91 102 1 0--20 Zinc, Total, ICP-MS 0.1 0.5 ug/L 0.44 1.5 1.89 97 70--130 1.5 1.94 100 2 0--20 Arsenic, Total, ICP-MS 0.01 0.05 ug/L 1.42 1.5 2.89 98 70--130 1.5 2.98 104 3 0--20 Silver, Total, ICP-MS 0.01 0.05 ug/L 0.03 0.5 0.525 99 70--130 0.5 0.56 106 6 0--20 Cadmium, Total, ICP-MS 0.005 0.025 ug/L 0.071 0.5 0.547 95 70--130 0.5 0.554 97 1 0--20 Antimony, Total, ICP-MS 0.005 0.025 ug/L 0.163 0.5 0.593 86 70--130 0.5 0.619 91 4 0--20 Lead, Total, ICP-MS 0.005 0.025 ug/L 0.018 0.5 0.478 92 70--130 0.5 0.483 93 1 0--20



### WG122436

MB:WG122436-1 Matrix: BLANK WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Chromium, Total, ICP-MS 0.05 0.25 ug/L <MDL Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL Arsenic, Total, ICP-MS 0.01 0.05 ug/L <MDL Nickel, Total, ICP-MS 0.025 0.125 ug/L <MDL Copper, Total, ICP-MS 0.025 0.125 ug/L <MDL Zinc, Total, ICP-MS 0.1 0.5 ug/L <MDL Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL Lead, Total, ICP-MS 0.005 0.025 ug/L <MDL

SB:WG122436-2 MB:WG122436-1 Matrix: BLANK WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Chromium, Total, ICP-MS 0.05 0.25 ug/L <MDL 0.5 0.51 102 75--125 Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL 0.5 0.494 99 75--125 Arsenic, Total, ICP-MS 0.01 0.05 ug/L <MDL 1.5 1.5 100 75--125 Nickel, Total, ICP-MS 0.025 0.125 ug/L <MDL 1.5 1.4 93 75--125 Copper, Total, ICP-MS 0.025 0.125 ug/L <MDL 1.5 1.39 93 75--125 Zinc, Total, ICP-MS 0.1 0.5 ug/L <MDL 1.5 1.37 91 75--125 Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.506 101 75--125 Lead, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.5 100 75--125Page 33 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

MSD:WG122436-4 MS:WG122436-3 L56061-2 Matrix: FRESH WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Chromium, Total, ICP-MS 0.05 0.25 ug/L 0.16 0.5 0.657 99 70--130 0.5 0.675 102 3 0--20 Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL 0.5 0.496 99 70--130 0.5 0.506 101 2 0--20 Arsenic, Total, ICP-MS 0.01 0.05 ug/L 0.757 1.5 2.18 95 70--130 1.5 2.24 99 3 0--20 Nickel, Total, ICP-MS 0.13 0.625 ug/L 0.645 1.5 1.85 80 70--130 1.5 1.94 86 5 0--20 Copper, Total, ICP-MS 0.025 0.125 ug/L 0.889 1.5 2.67 119 70--130 1.5 2.69 120 1 0--20 Zinc, Total, ICP-MS 0.1 0.5 ug/L 1.28 1.5 2.84 104 70--130 1.5 2.87 106 1 0--20 Cadmium, Total, ICP-MS 0.005 0.025 ug/L 0.011 0.5 0.521 102 70--130 0.5 0.542 106 4 0--20 Lead, Total, ICP-MS 0.005 0.025 ug/L 0.159 0.5 0.685 105 70--130 0.5 0.67 102 2 0--20



### WG122819

MB:WG122819-1 Matrix: BLANK WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Chromium, Total, ICP-MS 0.05 0.25 ug/L <MDL Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL Arsenic, Total, ICP-MS 0.01 0.05 ug/L <MDL Antimony, Total, ICP-MS 0.005 0.025 ug/L <MDL Nickel, Total, ICP-MS 0.025 0.125 ug/L <MDL Copper, Total, ICP-MS 0.025 0.125 ug/L <MDL Zinc, Total, ICP-MS 0.1 0.5 ug/L <MDL Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL Lead, Total, ICP-MS 0.005 0.025 ug/L <MDL

MB:WG122819-2 Matrix: BLANK WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Chromium, Total, ICP-MS 0.05 0.25 ug/L <MDL Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL Arsenic, Total, ICP-MS 0.01 0.05 ug/L <MDL Antimony, Total, ICP-MS 0.005 0.025 ug/L <MDL Nickel, Total, ICP-MS 0.025 0.125 ug/L <MDL Copper, Total, ICP-MS 0.025 0.125 ug/L <MDL Zinc, Total, ICP-MS 0.1 0.5 ug/L <MDL Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL Lead, Total, ICP-MS 0.005 0.025 ug/L <MDLPage 34 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

WG122999

MB:WG122999-1 Matrix: BLANK WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Chromium, Total, ICP-MS 0.05 0.25 ug/L <MDL Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL Arsenic, Total, ICP-MS 0.01 0.05 ug/L <MDL Antimony, Total, ICP-MS 0.005 0.025 ug/L <MDL Nickel, Total, ICP-MS 0.025 0.125 ug/L <MDL Copper, Total, ICP-MS 0.025 0.125 ug/L <MDL Zinc, Total, ICP-MS 0.1 0.5 ug/L <MDL Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL Lead, Total, ICP-MS 0.005 0.025 ug/L <MDL

SB:WG122999-2 MB:WG122999-1 Matrix: BLANK WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Chromium, Total, ICP-MS 0.05 0.25 ug/L <MDL 0.5 0.488 98 75--125 Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL 0.5 0.505 101 75--125 Arsenic, Total, ICP-MS 0.01 0.05 ug/L <MDL 1.5 1.62 108 75--125 Antimony, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.514 103 75--125 Nickel, Total, ICP-MS 0.025 0.125 ug/L <MDL 1.5 1.54 103 75--125 Copper, Total, ICP-MS 0.025 0.125 ug/L <MDL 1.5 1.48 99 75--125 Zinc, Total, ICP-MS 0.1 0.5 ug/L <MDL 1.5 1.55 103 75--125 Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.526 105 75--125 Lead, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.515 103 75--125

MSD:WG122999-4 MS:WG122999-3 L56062-7 Matrix: SALT WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Chromium, Total, ICP-MS 0.05 0.25 ug/L 0.16 0.5 0.628 94 70--130 0.5 0.584 86 7 0--20 Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL 0.5 0.518 104 70--130 0.5 0.503 101 3 0--20 Arsenic, Total, ICP-MS 0.01 0.05 ug/L 1.3 1.5 2.85 103 70--130 1.5 2.84 102 0 0--20 Antimony, Total, ICP-MS 0.005 0.025 ug/L 0.171 0.5 0.616 89 70--130 0.5 0.632 92 3 0--20 Nickel, Total, ICP-MS 0.025 0.125 ug/L 0.511 1.5 1.94 95 70--130 1.5 1.91 93 2 0--20 Copper, Total, ICP-MS 0.025 0.125 ug/L 0.441 1.5 1.85 94 70--130 1.5 1.8 91 3 0--20 Zinc, Total, ICP-MS 0.1 0.5 ug/L 0.519 1.5 1.9 92 70--130 1.5 1.9 92 0 0--20 Cadmium, Total, ICP-MS 0.005 0.025 ug/L 0.0712 0.5 0.554 96 70--130 0.5 0.554 97 0 0--20 Lead, Total, ICP-MS 0.005 0.025 ug/L 0.014 0.5 0.515 100 70--130 0.5 0.507 99 1 0--20Page 35 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

WG124799

MB:WG124799-1 Matrix: BLANK WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Chromium, Total, ICP-MS 0.05 0.25 ug/L <MDL Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL Arsenic, Total, ICP-MS 0.01 0.05 ug/L <MDL Nickel, Total, ICP-MS 0.025 0.125 ug/L <MDL Copper, Total, ICP-MS 0.025 0.125 ug/L <MDL Zinc, Total, ICP-MS 0.1 0.5 ug/L <MDL Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL Lead, Total, ICP-MS 0.005 0.025 ug/L <MDL

SB:WG124799-2 MB:WG124799-1 Matrix: BLANK WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Chromium, Total, ICP-MS 0.05 0.25 ug/L <MDL 0.5 0.49 98 75--125 Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL 0.5 0.469 94 75--125 Arsenic, Total, ICP-MS 0.01 0.05 ug/L <MDL 1.5 1.51 101 75--125 Nickel, Total, ICP-MS 0.025 0.125 ug/L <MDL 1.5 1.47 98 75--125 Copper, Total, ICP-MS 0.025 0.125 ug/L <MDL 1.5 1.41 94 75--125 Zinc, Total, ICP-MS 0.1 0.5 ug/L <MDL 1.5 1.36 90 75--125 Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.509 102 75--125 Lead, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.512 102 75--125

MSD:WG124799-4 MS:WG124799-3 L56989-1 Matrix: FRESH WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Chromium, Total, ICP-MS 0.05 0.25 ug/L 0.14 0.5 0.607 94 70--130 0.5 0.607 94 0 0--20 Silver, Total, ICP-MS 0.01 0.05 ug/L 0.033 0.5 0.526 99 70--130 0.5 0.505 94 4 0--20 Arsenic, Total, ICP-MS 0.01 0.05 ug/L 0.474 1.5 2.03 104 70--130 1.5 1.97 100 3 0--20 Nickel, Total, ICP-MS 0.025 0.125 ug/L 0.242 1.5 1.83 106 70--130 1.5 1.8 104 2 0--20 Copper, Total, ICP-MS 0.025 0.125 ug/L 0.817 1.5 2.33 101 70--130 1.5 2.28 97 2 0--20 Zinc, Total, ICP-MS 0.1 0.5 ug/L 0.711 1.5 2.14 95 70--130 1.5 2.09 92 2 0--20 Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.526 105 70--130 0.5 0.525 105 0 0--20 Lead, Total, ICP-MS 0.005 0.025 ug/L 0.0859 0.5 0.593 101 70--130 0.5 0.594 102 0 0--20Page 36 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

WG124800

MB:WG124800-1 Matrix: BLANK WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Chromium, Total, ICP-MS 0.05 0.25 ug/L <MDL Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL Arsenic, Total, ICP-MS 0.01 0.05 ug/L <MDL Antimony, Total, ICP-MS 0.005 0.025 ug/L <MDL Nickel, Total, ICP-MS 0.025 0.125 ug/L <MDL Copper, Total, ICP-MS 0.025 0.125 ug/L <MDL Zinc, Total, ICP-MS 0.1 0.5 ug/L <MDL Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL Lead, Total, ICP-MS 0.005 0.025 ug/L <MDL

MB:WG124800-2 Matrix: BLANK WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Chromium, Total, ICP-MS 0.05 0.25 ug/L <MDL Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL Arsenic, Total, ICP-MS 0.01 0.05 ug/L <MDL Antimony, Total, ICP-MS 0.005 0.025 ug/L <MDL Nickel, Total, ICP-MS 0.025 0.125 ug/L <MDL Copper, Total, ICP-MS 0.025 0.125 ug/L <MDL Zinc, Total, ICP-MS 0.1 0.5 ug/L <MDL Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL Lead, Total, ICP-MS 0.005 0.025 ug/L <MDL



### WG125559

MB:WG125559-1 Matrix: BLANK WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project: Pkey:STD (Method Blank)

Parameter MDL RDL Units MB Value Qual Chromium, Total, ICP-MS 0.05 0.25 ug/L <MDL Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL Arsenic, Total, ICP-MS 0.01 0.05 ug/L <MDL Antimony, Total, ICP-MS 0.005 0.025 ug/L <MDL Nickel, Total, ICP-MS 0.025 0.125 ug/L <MDL Copper, Total, ICP-MS 0.025 0.125 ug/L <MDL Zinc, Total, ICP-MS 0.1 0.5 ug/L <MDL Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL Lead, Total, ICP-MS 0.005 0.025 ug/L <MDLPage 37 of 37 

### LIMSView QC Report for NPDES Receiving Water Characterization Study - Data Validation for Metals

SB:WG125559-2 MB:WG125559-1 Matrix: BLANK WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project: Pkey:STD (Spike Blank, Method Blank)

Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit Chromium, Total, ICP-MS 0.05 0.25 ug/L <MDL 0.5 0.493 99 75--125 Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL 0.5 0.497 99 75--125 Arsenic, Total, ICP-MS 0.01 0.05 ug/L <MDL 1.5 1.53 102 75--125 Antimony, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.504 101 75--125 Nickel, Total, ICP-MS 0.025 0.125 ug/L <MDL 1.5 1.56 104 75--125 Copper, Total, ICP-MS 0.025 0.125 ug/L <MDL 1.5 1.47 98 75--125 Zinc, Total, ICP-MS 0.1 0.5 ug/L <MDL 1.5 1.31 87 75--125 Cadmium, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.504 101 75--125 Lead, Total, ICP-MS 0.005 0.025 ug/L <MDL 0.5 0.493 99 75--125

MSD:WG125559-4 MS:WG125559-3 L56990-9 Matrix: SALT WTR Listtype:MTICPMS-SEA Method:EPA 1640 Project:421162-300 Pkey:STD (Matrix Spike Duplicate, Matrix Spike)

Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimit Chromium, Total, ICP-MS 0.05 0.25 ug/L 0.14 0.5 0.574 87 70--130 0.5 0.573 87 0 0--20 Silver, Total, ICP-MS 0.01 0.05 ug/L <MDL 0.5 0.499 100 70--130 0.5 0.491 98 2 0--20 Arsenic, Total, ICP-MS 0.01 0.05 ug/L 1.49 1.5 2.95 97 70--130 1.5 2.95 98 0 0--20 Antimony, Total, ICP-MS 0.005 0.025 ug/L 0.174 0.5 0.678 101 70--130 0.5 0.691 103 2 0--20 Nickel, Total, ICP-MS 0.025 0.125 ug/L 0.404 1.5 1.69 86 70--130 1.5 1.73 88 2 0--20 Copper, Total, ICP-MS 0.025 0.125 ug/L 0.354 1.5 1.73 92 70--130 1.5 1.75 93 1 0--20 Zinc, Total, ICP-MS 0.1 0.5 ug/L 0.46 1.5 1.74 85 70--130 1.5 1.75 86 1 0--20 Cadmium, Total, ICP-MS 0.005 0.025 ug/L 0.0818 0.5 0.608 105 70--130 0.5 0.606 105 0 0--20 Lead, Total, ICP-MS 0.005 0.025 ug/L 0.0479 0.5 0.547 100 70--130 0.5 0.546 100 0 0--20