### Instructions for filling in the Emission Test Template

This Information Collection Request (ICR) spreadsheet is intended to collect information about emission data from fossil fuel burning power plants and which test methods were used to do so for cases where the test methods are not currently supported by the Electronic Reporting Tool (ERT). This spreadsheet should only be used if the method is not in the ERT or if you do not have access to a lab which performs methods that are in the ERT. You must complete at least 3 separate runs or sampling events for each of the requested constituents. This spreadsheet is intended to be used for one boiler of one facility. Data for multiple boilers should be handled by using separate copies of this spreadsheet. yellow are required. All cells that are shaded in green are populated using drop

- down lists. You do not need to populate cells shaded in gray, as they are automatically populated from the Boiler Information worksheet. resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_EmisTestMethods.xls (example: 8100_Unit_2_EmisTestMethods.xls).

Please refer to the following steps when using these spreadsheets.

Boiler Information Worksheet

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the control device configuration.

Emission Data Worksheets

The emission data worksheets are provided for each constituent or constituent family required for this analysis. On each spreadsheet, you must enter boiler operating information during sampling, fuel input information, and emission test results. There are generally 1 to 3 emission test results records to be entered depending on the constituent or constituent family. For example, CO only requires 1 record with 3 sample events, while Mercury requires that you enter both Hg Hg +2

### , or if the Ontario

- Hydro Method was used, you would need to enter Hg0

### , HgP, and Hg Volatile Organic HAP and Speciated Semi

-Volatile Organic HAP worksheets allow you to use a drop Constituent field to define as many records as needed to record each HAP that you have results for. General instructions follow for these worksheets:

Boiler Operation Information

1. Please provide the values of all requested parameters for each of test run/sample. 2. Please provide any other supporting information or comments in the Other Supporting Information field.

Fuel Information

1. Please enter what types of fuel are being used in your boiler using the drop

- downs in the Fuel Type Selection field. You may enter up to 4 fuel types. If you are not burning one or more of the fuel types entered in one or more samples, then enter an input rate of zero. 2. Please enter the unit of measure using the drop down provided. 3. Please enter the test method used to determine the fuel input rate. 4. Please provide any other information that you feel may be important in the Other Supporting Information field.

Emission Data

### 1. Some constituents ask for the emission rate results of each run in two different units of measure, while others do not. If emission rate results are requested in two different units of measure (ex. lb/MMBtu (Pounds per million BTU) and ppmvd @ 7% O 2 

### (parts per million by volume dry basis at 7 percent oxygen)), you are required to provide both. 2. Please provide the test method used. This may or may not match the example given in the Test Method Used field. Please ensure that the name includes the owning organization of the test method (ex. U.S. EPA Method 0010). 3. Please provide any other information that you feel may be important in the Other Supporting Information field. 4. If data sheets and QA/QC documentation tables are provided for the test method you are entering data for please also enter these data.

### This Information Collection Request (ICR) spreadsheet is intended to collect information about emission data from fossil fuel burning power plants and which test methods were used to do so for cases where the test methods are not currently supported by the Electronic Reporting Tool (ERT). This spreadsheet should only be used if the method is not in the ERT or if you do not have access to a lab which performs methods that are in the ERT. You must complete at least 3 separate This spreadsheet is intended to be used for one boiler of one facility. Data for multiple boilers should be handled by using separate copies of this spreadsheet. Fields shaded in down lists. You do not need to populate cells shaded in gray, as they are automatically populated from the Boiler Information worksheet. Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_EmisTestMethods.xls

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

The emission data worksheets are provided for each constituent or constituent family required for this analysis. On each spreadsheet, you must enter boiler operating information during sampling, fuel input information, and emission test results. There are generally 1 to 3 emission test results records to be entered depending on the constituent or constituent family. For example, CO only requires 1 record with 3 sample events, while Mercury requires that you enter both Hg0 

### and , HgP, and Hg+2 

### . However, both the Speciated Volatile Organic HAP worksheets allow you to use a drop

- down provided in the Constituent field to define as many records as needed to record each HAP that you have results for. General instructions

2. Please provide any other supporting information or comments in the Other Supporting Information field.

downs in the Fuel Type Selection field. You may enter up to 4 fuel types. If you are not burning one or more of the fuel types entered in one or more samples,

4. Please provide any other information that you feel may be important in the Other Supporting Information field.

### 1. Some constituents ask for the emission rate results of each run in two different units of measure, while others do not. If emission rate results are requested in two different units of measure (ex. lb/MMBtu (Pounds per million BTU) and

(parts per million by volume dry basis at 7 percent oxygen)), you are required to provide both. 2. Please provide the test method used. This may or may not match the example given in the Test Method Used field. Please ensure that the name includes the owning organization of the test method (ex. U.S. EPA Method 0010). 3. Please provide any other information that you feel may be important in the Other Supporting Information field. 4. If data sheets and QA/QC documentation tables are provided for the test method you are entering data for please alsoEIA

Facility Code Facility Name Boiler ID

2451 San Juan Unit 4Control Device Configuraton

Listed (by

boiler) in the Configuration Order Section of the Facility Unit Configurations Section of the Electronic ICRListed (by boiler) in the Configuration Order Section of the Facility Unit Configurations Section of the Electronic ICREIA

Facility Code Facility Name Boiler ID 2451 San Juan Unit 4

1 5/19/2010 8:35 1 5/19/2010 8:35 2 5/19/2010 12:10 2 5/19/2010 12:10 3 5/20/2010 7:31 3 5/20/2010 7:31 Run Number Test Start Date Test Start TimePlease note QA/QC documentation starting in Column "AI"

Measured Value (μg/dscm) Basis (Wet or Dry)

5/19/2010 11:35 0.075 Dry 5/19/2010 11:35 0.081 Dry 5/19/2010 15:10 0.028 Dry 5/19/2010 15:10 0.030 Dry 5/20/2010 10:31 0.020 Dry 5/20/2010 10:31 0.021 Dry Total Vapor Phase Mercury Emission Test Results

Test End Time Test End DatePlease note QA/QC documentation starting in Column "AI"

Test Method Used Data Flag (ADL, BDL, DDL) Test Method

Comments (lb/mmBtu)

U.S. EPA Method 30B 0.0000000631 2471 U.S. EPA Method 30B 0.0000000684 2471 U.S. EPA Method 30B 0.0000000234 2471 U.S. EPA Method 30B 0.0000000249 2471 U.S. EPA Method 30B 0.0000000164 2513 U.S. EPA Method 30B 0.0000000171 2513 Total Vapor Phase Mercury Emission Test Results Steam Output (1000 lb/hr)Fuel Input Rate
4599 12.3 13.5 5.7 1042797 116 458174 4599 12.3 13.5 5.7 1042797 116 458174 4666 12.2 13.5 5.7 1042797 117 457117 4666 12.2 13.5 5.7 1042797 117 457117 4637 12.1 13.5 5.5 1131652 115 453425 4637 12.1 13.5 5.5 1131652 115 453425 Flue Gas Moisture (%) Flue Gas Temperature (F) Total Heat Input (mmBtu/hr) Flue Gas CO 2(%) Flue Gas

O 2(%) Flue Gas

Flow Rate (dscfm)QA /QC Documentation

Fuel Type Units of

Measure Measurement

Method Trap ID Section 1 Mass (ng)
subbituminous lb/hour F-Factor 67764 28.9 subbituminous lb/hour F-Factor 66109 29.6 subbituminous lb/hour F-Factor 677533 22.9 subbituminous lb/hour F-Factor 66147 23.4 subbituminous lb/hour F-Factor 67763 21.4 subbituminous lb/hour F-Factor 66112 37.4

Fuel #1 Other Supporting InformationQA /QC Documentation

Section 2 Mass (ng) Total

Mass (ng) Initial

Spike (ng) Total NonSpike (ng) Sample

Volume (dscm) Volume

Difference (%) Volume Diff. Limit Breaktrough

(%)
1.3 30.2 20 10.2 0.1444 4.5 2.6 32.2 20 12.2 0.1467 8.8 0.5 23.4 20 3.4 0.1434 2.2 1.1 24.5 20 4.5 0.1458 4.7 0.9 22.3 20 2.3 0.1452 4.2 1.5 38.9 20 18.9 0.1475 4.0 ≤20% of field recovery test Trap #1Breaktrough

Limit Concentration

(μg/dscm) Trap ID Section 1 Mass Section 2

Mass Total

Mass Initial

Spike Total NonSpike
0.070619513 60829 10.6 0.9 11.5 0 11.5 0.083139115 60856 9.6 1.9 11.5 0 11.5 0.023705439 60904 4.1 0.5 4.6 0 4.6 0.030866315 60908 3.6 0.5 4.1 0 4.1 0.015841202 60925 2.9 0.5 3.4 0 3.4 0.128159922 60916 8.6 1.4 10 0 10.0 ≤10% of Section 1 Hg

mass for Hg conc. >1
μg/dscm: or ≤ 20% of SectionSample

Volume Volume

Difference (%) Volume Diff. Limit Breaktrough (%) Breaktrough Limit Concentration

(μg/dscm)
0.1446 8.490566038 0.079511042 0.1460 19.79166667 0.078788169 0.1436 12.19512195 0.032041459 0.1450 13.88888889 0.028279958 0.1454 17.24137931 0.023391813 0.1466 16.27906977 0.068212824 ≤10% of Section 1 Hg mass for Hg conc. >1
μg/dscm: or ≤ 20% of Section 1 for Hg conc. ≤1 ≤20% of field recovery test Trap #2Abs. diff. RD (%) Limit C rec R (%) by Run Ravg(%) Limit

0.008892 5.922531 18.2645 91.3 0.004351 2.686975 19.9203 99.6 0.008336 14.95333 18.8236 94.1 0.002586 4.372815 19.7659 98.8 0.007551 19.24555 18.4293 92.5 0.059947 30.5272 28.7153 143.6

≥ 10 % RD mass for Hg conc. >1 μg/dscm: or
≤20% RD or ≤ 0.2 μg/dscm abs.diff. for Hg conc. ≤1 Average Recovery

, between 85 and 115% Measured Spike Recovery ( R )

103.3166667 Paired Trap Agreement (RD)EIA

Facility Code Facility Name Boiler ID

2451 San Juan Unit 4

1 5/19/2010 8:59 5/19/2010 2 5/20/2010 7:34 5/20/2010 3 5/21/2010 7:35 5/21/2010 Run Number Test Start Date Test Start Time Test End DateMeasured Value (ppm) Basis (Wet or Dry)
14:34 0.023 Dry 13:58 0.023 Dry 12:48 0.022 Dry Test End TimeTest Method Used Data Flag (ADL, BDL, DDL) Test Method

Comments U.S. EPA Conditional Test Method 033 (CTM-033) 0.0000213 U.S. EPA Conditional Test Method 033 (CTM-033) 0.0000211 U.S. EPA Conditional Test Method 033 (CTM-033) 0.0000206 Analysis was non detect for HCN and detectition lim it was substituted Hydrogen Cyanide Emission Test Results Calculated Emission Rate (lb/mmBtu)Fuel Input Rate 2471 4655 14.3 13.5 5.7 1034442 114 459725 2513 4681 13.8 13.5 5.5 1041378 114 454410 2542 4763 14.3 13.7 5.4 1033627 114 459150 Flue Gas Temperature (F) Flue Gas Moisture (%) Flue Gas CO 2(%) Flue Gas

O 2(%) Flue Gas

Flow Rate (dscfm) Steam Output (1000 lb/hr) Total Heat

Input (mmBtu/hr)Fuel Type Units of Measure Measurement

Method subbituminous lb/hour F-Factor subbituminous lb/hour F-Factor subbituminous lb/hour F-Factor Other Supporting Information

Fuel #1EIA

Facility Code Facility Name Boiler ID 2451 San Juan Unit 4

1 5/19/2010 8:59 2 5/20/2010 7:34 3 5/21/2010 7:35 Run Number Test Start Date Test Start TimeTotal Dissolved Solids (mg solids/liter) Total Suspended Solids (mg solids/liter)
5/19/2010 14:34 45680 168944 5/20/2010 13:58 Not Available Not Available 5/21/2010 12:48 Not Available Not Available

Test End Time Test End DateTest Method Used Data Flag (ADL, BDL, DDL) Constisuent Emission Test ResultsTest Method Comments

2471 4599 1042797 116

Not Available Not Available Not Available Not Available Not Available Not Available Not Available Not Available Not Available Not Available Steam Output (1000 lb/hr) Total Heat Input

(mmBtu/hr) Flue Gas Temperature (F) Flue Gas Flow Rate (dscfm)Fuel Input Rate Fuel Type Units of Measure Measurement

Method
458174 subbituminous

lb/hour F-Factor Not Available Not Available Other Supporting Information Fuel #1