# CLEAN SITES

Environmental Services , Inc

.



### December 9,2009
Mr. Ron Davis Remedial Project Manager U.S. E nvironmenta l Protection Agency Region III 1650 Arch Street Philadelphia, PA 191 03 Subject: 

### November 2009 Monitoring Report Coker's Lan df ills Cheswold, Delaware
Dear Mr. Davis: Clean Sites Environmental Services , Inc. (Clean Sites) hereby submits this monitoring repoli as requested by EPA in their T hird Five-Year Review Report for the Site

. The Five-Year Review Report also requests that monitoring events be conducted every five years coinciding with EPA ' s Five- Year Reviews.
T his report includes a summary of the field and laboratory test results from the monitoring event conducted on November 14 and November 

### IS , 2009. It 

### was prepared in accordance with the Consent Decree and Part 4 .C of the March 1993 Remedial Design submittal with the exception that the analytical parameters were expanded as requested by EPA and discussed below. 

### Gr oundwater Sampling Prior to groundwater sampling , each of the wells to be sampled was inspected and the depth to water level was recorded. The water l e vels were used to calculate the well purge volumes and to create groundwater contour maps as detailed below

. The wells were purged using either a submersible pump and disposable poly-flow tubing or disposable bailers. Groundwater samples were either collected using a submersible pump (decontaminated between wells) or disposable bailers. All Groundwater , surface water , and sediment samples were sent to Test America in Pittsburgh, Pennsylvania for analysis. As requested by EPA, groundwater samples for Coker's 1 and 2 were analyzed for volatile organic compounds (VOCs) by Method 8260 , semivolatile organic compounds (SVOCs) by Method 8270C, Target Analyte List (TAL) metals by Method 8020B, and total organic carbon (TOC) by Method 5310B. In addition, groundwater samples for Coker's 2 were also analyzed for total phenolics b y Method 9066. Field measurements of p H , sp ecific conductance , an d temp erature we re re corde d for e a ch w e l l. A t rip blank accompanied the sample coolers and a rinse blank was collected from the submersible pump to verify it was being thoroughly decontaminated between well s

C LEAN S IT ES ENV I RONMENTAL SERVICES

. INC

. ... 4616 1 WES T LAKE DRIVE

. SUITE 230·6

... PO T OMAC FAL L S , VIRG I N I A 2 0 165 TE L: (703) 5 1 9·2 1 40

... F AX: ( 7 03 ) 519·2 14 1

### Water and Sediment Sampling

water samples were collected from to Coker's 1 in accordance with the by was collected prior to sediment were stream 

### a sampler. collected likely depositional areas using decontaminated samples were collected from sediment bed

and YOCs,

niPIPn: 

### as Field measurements of pH, oxygen were recorded for the water**"'~"U"j;,** 

### Results locations 

### s J 

### and 2 are on Estimated groundwater each landfill are figures. These contours have using ofthe water data is provided on Table 

### 1. analytical water and in Appendix are



### or total phenolics detected in 1. 

### It 1.3 samples. was mg/I in the monitoring to 10

no Maximum sampling events 

### Site
There were no at Coker's 1. A new lock

### Should you have any questions regarding this report or need additional information, please call me at (703) 519-2142. ly yours,

Scott R. Miller, P. E

. Proj ect Coordinator

cc: Sandra Guastaferr o, Reichhold, I nc . Stephen Johnson, DNRE C Lisa D. Krogman, P

. E ., Kraft Foods Global , Inc

. Jeffrey Srulovitz, Esq. , Kraft Foods Global, Inc.NOVEMBER 2009TOP OF CASINGDEPTH TOGROUNDWATERMONITORING WELLELEVATION (FT, MSL)WATER (FT)(1)ELEVATIONL1-S141.734.0337.70L1-S342.4111.2231.19L1-S428.882.1126.77MW-1S45.521.2744.25MW-3S45.191.6743.52L2-S150.332.4347.90Notes:(1) Depth to water readings were measured on November 14, 2009.Coker's 1Coker's 2TABLE 1GROUNDWATER ELEVATIONSCOKER'S LANDFILLS SITECHESWOLD, DELAWARENOVEMBER 2009PARAMETER(1)L1-S1L1-S3L1-S4MW-1SMW-3SL2-S1Aluminum4865971451,7302,8802,110ArsenicND1.9NDNDNDNDBarium18.765.433.647.013495.4BerylliumNDNDNDND2.2NDCalcium3,93031,60045,10010,5008,7704,150Cobalt1.32.8ND3.54.12.9Chromium35.13.03.96.56.47.1CopperNDNDND2.52.1NDIron92210,2003,4201,5202,2805,950Potassium6332,3601,9109951,2401,040Magnesium2,35018,5003,5003,1405,9002,420Manganese11.9277194162163104Sodium5,8304,6407,0503,7604,7204,990Nickel5.11.73.12.63.94.2LeadNDNDND1.42.01.3VanadiumND2.29.92.96.06.3Zinc7.710.35.19.615.311.0Phenolics (mg/l)NANANANDNDNDTotal Organic Carbon (mg/l)1.34.67.310.26.32.3Temperature (oC)14.714.714.913.714.214.7pH5.435.855.545.274.715.19Specific Conductance (μmhos/cm)84.8343.0302.6112.0157.5103.3Notes:(1) Only the detected parameters are shown on the table.ND indicates parameter was not detected.NA indicates parameter was not analyzed.Bold numbers indicate an MCL exceedance.Coker's 1Coker's 2TABLE 2SUMMARY OF GROUNDWATER SAMPLING RESULTSCOKER'S LANDFILLS SITECHESWOLD, DELAWARENOVEMBER 2009PARAMETER(1)SW-1SW-2SW-3SED-1SED-2SED-3Aluminum4464484151,4701,0802,080ArsenicNDNDND0.170.430.28Barium65.861.560.014.512.523.0BerylliumNDNDND0.75ND0.19Calcium16,50016,00016,300885386631Cobalt1.10.980.913.50.931.6Chromium4.13.73.92.42.23.3CopperNDNDND0.600.470.78Iron1,0009941,04010,9002,4302,780Potassium3,7003,4803,44072.982.5114Magnesium5,1205,1205,140293121252Manganese10289.992.294.532.057.5Sodium6,1705,8505,70029.325.929.9Nickel2.22.12.11.20.751.3LeadNDNDND2.12.13.1Vanadium2.51.92.54.62.72.5Zinc15.411.412.216.810.216.0Total Organic Carbon (mg/l or mg/kg)19.619.019.4ND8172,810Temperature (oC)14.514.113.6NANANApH7.117.117.04NANANADissolved Oxygen (mg/l)665NANANASpecific Conductance (μmhos/cm)175.4178.9177.7NANANANotes:(1) Only the detected parameters are shown on the table.ND indicates parameter was not detected.NA indicates parameter was not analyzed.Bold numbers indicate an MCL exceedance.Surface Water (μg/l)Sediments (μg/kg)TABLE 3SUMMARY OF WILLIS BRANCH SAMPLING RESULTSCOKER'S LANDFILLS SITECHESWOLD, DELAWARE

# Appendix A Analytical Results

### C9K180557 1 of 161

### C9K180557 2 of 161

### C9K180557 3 of 161

### C9K180557 4 of 161

### C9K180557 5 of 161

### C9K180557 6 of 161

## METHODS SUMMARY
C9K180557

ANALYTICAL PREPARATION PARAMETER __________________________________________________ METHOD _______________ METHOD

_______________ ICP-MS (6020) SW846 6020 SW846 3010 ICP-MS (6020) SW846 6020 SW846 3050B Mercury in Liquid Waste (Manual Cold-Vapor) SW846 7470A SW846 7470A Mercury in Solid Waste (Manual Cold-Vapor) SW846 7471A SW846 7471A Phenolics SW846 9066 SW846 9066 Semivolatile Organic Compounds by GC/MS SW846 8270C SW846 3520C Semivolatile Organic Compounds by GC/MS SW846 8270C SW846 3541 Total Organic Carbon, TOC 5310B SM20 5310B SM20 5310B Total Residue as Percent Solids SM20 2540G TOC Lloyd Kahn Lloyd Kahn EPA Lloyd Kahn EPA Lloyd Kahn Volatile Organics by GC/MS SW846 8260B SW846 5030B
References:
EPA "EASTERN ENVIRONMENTAL RADIATION FACILITY RADIOCHEMISTRY

PROCEDURES MANUAL" US EPA EPA 520/5-84-006 AUGUST 1984
SM20 "STANDARD METHODS FOR THE EXAMINATION OF WATER AND

WASTEWATER", 20TH EDITION." SW846 "Test Methods for Evaluating Solid Waste, Physical/Chemical

Methods", Third Edition, November 1986 and its updates.



### C9K180557 7 of 161

## SAMPLE SUMMARY
C9K180557

SAMPLED SAMP WO #_____ SAMPLE# _______ CLIENT SAMPLE ID

________________________________________________________________ DATE ________ TIME

_____ LPPF5 001 MW-1S 11/14/09 10:35 LPPGN 002 MW-3S 11/14/09 10:45 LPPGP 003 L2-S1 11/14/09 11:40 LPPGR 004 RINSE BLANK-1 11/14/09 11:15 LPPGV 005 TRIP BLANK-COKER 2 11/14/09 LPPG1 006 L1-S1 11/14/09 15:20 LPPG6 007 L1-S3 11/14/09 16:10 LPPG8 008 L1-S4 11/14/09 15:40 LPPHA 009 SW-1 11/15/09 11:25 LPPHF 010 SW-2 11/15/09 10:30 LPPHG 011 SW-3 11/15/09 09:45 LPPHK 012 SED-1 11/15/09 11:35 LPPHM 013 SED-2 11/15/09 10:40 LPPHN 014 SED-3 11/15/09 09:55 LPPHV 015 TRIP BLANK-COKER 1 11/15/09 NOTE(S):

_____________________________________________________________________________________________ - The analytical results of the samples listed above are presented on the following pages. - All calculations are performed before rounding to avoid round-off errors in calculated results. - Results noted as "ND" were not detected at or above the stated limit. - This report must not be reproduced, except in full, without the written approval of the laboratory. - Results for the following parameters are never reported on a dry weight basis: color, corrosivity, density, flashpoint, ignitability, layers, odor, paint filter test, pH, porosity pressure, reactivity, redox potential, specific gravity, spot tests, solids, solubility, temperature, viscosity, and weight.



### C9K180557 8 of 161Clean Sites Environmental Services Inc Client Sample ID: MW-1S GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-001 Work Order #...: Work Order #...: LPPF51AD Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9328229 Prep Date......: Prep Date......: 11/24/09 Analysis Date..: Analysis Date..: 11/24/09 Prep Batch #...: Prep Batch #...: 9328345 Analysis Time..: Analysis Time..: 13:46 Dilution Factor: Dilution Factor: 1 Method.........: Method.........: SW846 8260B
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acetone ND 20 ug/L Benzene ND 5.0 ug/L Bromodichloromethane ND 5.0 ug/L Bromoform ND 5.0 ug/L Bromomethane ND 5.0 ug/L 2-Butanone ND 5.0 ug/L Carbon disulfide ND 5.0 ug/L Carbon tetrachloride ND 5.0 ug/L Chlorobenzene ND 5.0 ug/L Chloroethane ND 5.0 ug/L Chloroform ND 5.0 ug/L Chloromethane ND 5.0 ug/L Cyclohexane ND 5.0 ug/L Dibromochloromethane ND 5.0 ug/L 1,2-Dibromo-3-chloro- ND 5.0 ug/L propane 1,2-Dibromoethane ND 5.0 ug/L 1,3-Dichlorobenzene ND 5.0 ug/L 1,4-Dichlorobenzene ND 5.0 ug/L 1,2-Dichlorobenzene ND 5.0 ug/L Dichlorodifluoromethane ND 5.0 ug/L 1,1-Dichloroethane ND 5.0 ug/L 1,2-Dichloroethane ND 5.0 ug/L 1,1-Dichloroethene ND 5.0 ug/L cis-1,2-Dichloroethene ND 5.0 ug/L trans-1,2-Dichloroethene ND 5.0 ug/L 1,2-Dichloropropane ND 5.0 ug/L cis-1,3-Dichloropropene ND 5.0 ug/L trans-1,3-Dichloropropene ND 5.0 ug/L Ethylbenzene ND 5.0 ug/L 2-Hexanone ND 5.0 ug/L Isopropylbenzene ND 5.0 ug/L Methyl acetate ND 5.0 ug/L Methylene chloride ND 5.0 ug/L Methylcyclohexane ND 5.0 ug/L 4-Methyl-2-pentanone ND 5.0 ug/L Methyl tert-butyl ether ND 5.0 ug/L Styrene ND 5.0 ug/L (Continued on next page)



### C9K180557 9 of 161Clean Sites Environmental Services Inc Client Sample ID: MW-1S GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-001 Work Order #...: Work Order #...: LPPF51AD Matrix.........: Matrix.........: WATER
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 1,1,2,2-Tetrachloroethane ND 5.0 ug/L 1,2,4-Trichloro- ND 5.0 ug/L benzene Tetrachloroethene ND 5.0 ug/L 1,1,1-Trichloroethane ND 5.0 ug/L 1,1,2-Trichloroethane ND 5.0 ug/L Trichloroethene ND 5.0 ug/L Trichlorofluoromethane ND 5.0 ug/L 1,1,2-Trichloro- ND 5.0 ug/L 1,2,2-trifluoroethane Toluene ND 5.0 ug/L Vinyl chloride ND 5.0 ug/L Xylenes (total) ND 15 ug/L
PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 1,2-Dichloroethane-d4 100 (62 - 123) Toluene-d8 95 (80 - 120) 4-Bromofluorobenzene 86 (75 - 120) Dibromofluoromethane 108 (80 - 120)



### C9K180557 10 of 161Clean Sites Environmental Services Inc Client Sample ID: MW-3S GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-002 Work Order #...: Work Order #...: LPPGN1AL Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9329152 Prep Date......: Prep Date......: 11/25/09 Analysis Date..: Analysis Date..: 11/25/09 Prep Batch #...: Prep Batch #...: 9329174 Analysis Time..: Analysis Time..: 09:51 Dilution Factor: Dilution Factor: 1 Method.........: Method.........: SW846 8260B
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acetone ND 20 ug/L Benzene ND 5.0 ug/L Bromodichloromethane ND 5.0 ug/L Bromoform ND 5.0 ug/L Bromomethane ND 5.0 ug/L 2-Butanone ND 5.0 ug/L Carbon disulfide ND 5.0 ug/L Carbon tetrachloride ND 5.0 ug/L Chlorobenzene ND 5.0 ug/L Chloroethane ND 5.0 ug/L Chloroform ND 5.0 ug/L Chloromethane ND 5.0 ug/L Cyclohexane ND 5.0 ug/L Dibromochloromethane ND 5.0 ug/L 1,2-Dibromo-3-chloro- ND 5.0 ug/L propane 1,2-Dibromoethane ND 5.0 ug/L 1,3-Dichlorobenzene ND 5.0 ug/L 1,4-Dichlorobenzene ND 5.0 ug/L 1,2-Dichlorobenzene ND 5.0 ug/L Dichlorodifluoromethane ND 5.0 ug/L 1,1-Dichloroethane ND 5.0 ug/L 1,2-Dichloroethane ND 5.0 ug/L 1,1-Dichloroethene ND 5.0 ug/L cis-1,2-Dichloroethene ND 5.0 ug/L trans-1,2-Dichloroethene ND 5.0 ug/L 1,2-Dichloropropane ND 5.0 ug/L cis-1,3-Dichloropropene ND 5.0 ug/L trans-1,3-Dichloropropene ND 5.0 ug/L Ethylbenzene ND 5.0 ug/L 2-Hexanone ND 5.0 ug/L Isopropylbenzene ND 5.0 ug/L Methyl acetate ND 5.0 ug/L Methylene chloride ND 5.0 ug/L Methylcyclohexane ND 5.0 ug/L 4-Methyl-2-pentanone ND 5.0 ug/L Methyl tert-butyl ether ND 5.0 ug/L Styrene ND 5.0 ug/L (Continued on next page)



### C9K180557 11 of 161Clean Sites Environmental Services Inc Client Sample ID: MW-3S GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-002 Work Order #...: Work Order #...: LPPGN1AL Matrix.........: Matrix.........: WATER
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 1,1,2,2-Tetrachloroethane ND 5.0 ug/L 1,2,4-Trichloro- ND 5.0 ug/L benzene Tetrachloroethene ND 5.0 ug/L 1,1,1-Trichloroethane ND 5.0 ug/L 1,1,2-Trichloroethane ND 5.0 ug/L Trichloroethene ND 5.0 ug/L Trichlorofluoromethane ND 5.0 ug/L 1,1,2-Trichloro- ND 5.0 ug/L 1,2,2-trifluoroethane Toluene ND 5.0 ug/L Vinyl chloride ND 5.0 ug/L Xylenes (total) ND 15 ug/L
PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 1,2-Dichloroethane-d4 94 (62 - 123) Toluene-d8 101 (80 - 120) 4-Bromofluorobenzene 90 (75 - 120) Dibromofluoromethane 104 (80 - 120)



### C9K180557 12 of 161Clean Sites Environmental Services Inc Client Sample ID: L2-S1 GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-003 Work Order #...: Work Order #...: LPPGP1AL Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9328229 Prep Date......: Prep Date......: 11/24/09 Analysis Date..: Analysis Date..: 11/24/09 Prep Batch #...: Prep Batch #...: 9328345 Analysis Time..: Analysis Time..: 19:38 Dilution Factor: Dilution Factor: 1 Method.........: Method.........: SW846 8260B
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acetone ND 20 ug/L Benzene ND 5.0 ug/L Bromodichloromethane ND 5.0 ug/L Bromoform ND 5.0 ug/L Bromomethane ND 5.0 ug/L 2-Butanone ND 5.0 ug/L Carbon disulfide ND 5.0 ug/L Carbon tetrachloride ND 5.0 ug/L Chlorobenzene ND 5.0 ug/L Chloroethane ND 5.0 ug/L Chloroform ND 5.0 ug/L Chloromethane ND 5.0 ug/L Cyclohexane ND 5.0 ug/L Dibromochloromethane ND 5.0 ug/L 1,2-Dibromo-3-chloro- ND 5.0 ug/L propane 1,2-Dibromoethane ND 5.0 ug/L 1,3-Dichlorobenzene ND 5.0 ug/L 1,4-Dichlorobenzene ND 5.0 ug/L 1,2-Dichlorobenzene ND 5.0 ug/L Dichlorodifluoromethane ND 5.0 ug/L 1,1-Dichloroethane ND 5.0 ug/L 1,2-Dichloroethane ND 5.0 ug/L 1,1-Dichloroethene ND 5.0 ug/L cis-1,2-Dichloroethene ND 5.0 ug/L trans-1,2-Dichloroethene ND 5.0 ug/L 1,2-Dichloropropane ND 5.0 ug/L cis-1,3-Dichloropropene ND 5.0 ug/L trans-1,3-Dichloropropene ND 5.0 ug/L Ethylbenzene ND 5.0 ug/L 2-Hexanone ND 5.0 ug/L Isopropylbenzene ND 5.0 ug/L Methyl acetate ND 5.0 ug/L Methylene chloride ND 5.0 ug/L Methylcyclohexane ND 5.0 ug/L 4-Methyl-2-pentanone ND 5.0 ug/L Methyl tert-butyl ether ND 5.0 ug/L Styrene ND 5.0 ug/L (Continued on next page)



### C9K180557 13 of 161Clean Sites Environmental Services Inc Client Sample ID: L2-S1 GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-003 Work Order #...: Work Order #...: LPPGP1AL Matrix.........: Matrix.........: WATER
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 1,1,2,2-Tetrachloroethane ND 5.0 ug/L 1,2,4-Trichloro- ND 5.0 ug/L benzene Tetrachloroethene ND 5.0 ug/L 1,1,1-Trichloroethane ND 5.0 ug/L 1,1,2-Trichloroethane ND 5.0 ug/L Trichloroethene ND 5.0 ug/L Trichlorofluoromethane ND 5.0 ug/L 1,1,2-Trichloro- ND 5.0 ug/L 1,2,2-trifluoroethane Toluene ND 5.0 ug/L Vinyl chloride ND 5.0 ug/L Xylenes (total) ND 15 ug/L
PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 1,2-Dichloroethane-d4 85 (62 - 123) Toluene-d8 108 (80 - 120) 4-Bromofluorobenzene 85 (75 - 120) Dibromofluoromethane 96 (80 - 120)



### C9K180557 14 of 161Clean Sites Environmental Services Inc Client Sample ID: RINSE BLANK-1

GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-004 Work Order #...: Work Order #...: LPPGR1AA Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9329152 Prep Date......: Prep Date......: 11/25/09 Analysis Date..: Analysis Date..: 11/25/09 Prep Batch #...: Prep Batch #...: 9329174 Analysis Time..: Analysis Time..: 13:35 Dilution Factor: Dilution Factor: 1 Method.........: Method.........: SW846 8260B
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acetone ND 20 ug/L Benzene ND 5.0 ug/L Bromodichloromethane ND 5.0 ug/L Bromoform ND 5.0 ug/L Bromomethane ND 5.0 ug/L 2-Butanone ND 5.0 ug/L Carbon disulfide ND 5.0 ug/L Carbon tetrachloride ND 5.0 ug/L Chlorobenzene ND 5.0 ug/L Chloroethane ND 5.0 ug/L Chloroform ND 5.0 ug/L Chloromethane ND 5.0 ug/L Cyclohexane ND 5.0 ug/L Dibromochloromethane ND 5.0 ug/L 1,2-Dibromo-3-chloro- ND 5.0 ug/L propane 1,2-Dibromoethane ND 5.0 ug/L 1,3-Dichlorobenzene ND 5.0 ug/L 1,4-Dichlorobenzene ND 5.0 ug/L 1,2-Dichlorobenzene ND 5.0 ug/L Dichlorodifluoromethane ND 5.0 ug/L 1,1-Dichloroethane ND 5.0 ug/L 1,2-Dichloroethane ND 5.0 ug/L 1,1-Dichloroethene ND 5.0 ug/L cis-1,2-Dichloroethene ND 5.0 ug/L trans-1,2-Dichloroethene ND 5.0 ug/L 1,2-Dichloropropane ND 5.0 ug/L cis-1,3-Dichloropropene ND 5.0 ug/L trans-1,3-Dichloropropene ND 5.0 ug/L Ethylbenzene ND 5.0 ug/L 2-Hexanone ND 5.0 ug/L Isopropylbenzene ND 5.0 ug/L Methyl acetate ND 5.0 ug/L Methylene chloride ND 5.0 ug/L Methylcyclohexane ND 5.0 ug/L 4-Methyl-2-pentanone ND 5.0 ug/L Methyl tert-butyl ether ND 5.0 ug/L Styrene ND 5.0 ug/L (Continued on next page)



### C9K180557 15 of 161Clean Sites Environmental Services Inc Client Sample ID: RINSE BLANK-1

GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-004 Work Order #...: Work Order #...: LPPGR1AA Matrix.........: Matrix.........: WATER
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 1,1,2,2-Tetrachloroethane ND 5.0 ug/L 1,2,4-Trichloro- ND 5.0 ug/L benzene Tetrachloroethene ND 5.0 ug/L 1,1,1-Trichloroethane ND 5.0 ug/L 1,1,2-Trichloroethane ND 5.0 ug/L Trichloroethene ND 5.0 ug/L Trichlorofluoromethane ND 5.0 ug/L 1,1,2-Trichloro- ND 5.0 ug/L 1,2,2-trifluoroethane Toluene ND 5.0 ug/L Vinyl chloride ND 5.0 ug/L Xylenes (total) ND 15 ug/L
PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 1,2-Dichloroethane-d4 90 (62 - 123) Toluene-d8 105 (80 - 120) 4-Bromofluorobenzene 88 (75 - 120) Dibromofluoromethane 97 (80 - 120)



### C9K180557 16 of 161Clean Sites Environmental Services Inc Client Sample ID: TRIP BLANK-COKER 2

GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-005 Work Order #...: Work Order #...: LPPGV1AA Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9329152 Prep Date......: Prep Date......: 11/25/09 Analysis Date..: Analysis Date..: 11/25/09 Prep Batch #...: Prep Batch #...: 9329174 Analysis Time..: Analysis Time..: 14:00 Dilution Factor: Dilution Factor: 1 Method.........: Method.........: SW846 8260B
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acetone ND 20 ug/L Benzene ND 5.0 ug/L Bromodichloromethane ND 5.0 ug/L Bromoform ND 5.0 ug/L Bromomethane ND 5.0 ug/L 2-Butanone ND 5.0 ug/L Carbon disulfide ND 5.0 ug/L Carbon tetrachloride ND 5.0 ug/L Chlorobenzene ND 5.0 ug/L Chloroethane ND 5.0 ug/L Chloroform ND 5.0 ug/L Chloromethane ND 5.0 ug/L Cyclohexane ND 5.0 ug/L Dibromochloromethane ND 5.0 ug/L 1,2-Dibromo-3-chloro- ND 5.0 ug/L propane 1,2-Dibromoethane ND 5.0 ug/L 1,3-Dichlorobenzene ND 5.0 ug/L 1,4-Dichlorobenzene ND 5.0 ug/L 1,2-Dichlorobenzene ND 5.0 ug/L Dichlorodifluoromethane ND 5.0 ug/L 1,1-Dichloroethane ND 5.0 ug/L 1,2-Dichloroethane ND 5.0 ug/L 1,1-Dichloroethene ND 5.0 ug/L cis-1,2-Dichloroethene ND 5.0 ug/L trans-1,2-Dichloroethene ND 5.0 ug/L 1,2-Dichloropropane ND 5.0 ug/L cis-1,3-Dichloropropene ND 5.0 ug/L trans-1,3-Dichloropropene ND 5.0 ug/L Ethylbenzene ND 5.0 ug/L 2-Hexanone ND 5.0 ug/L Isopropylbenzene ND 5.0 ug/L Methyl acetate ND 5.0 ug/L Methylene chloride ND 5.0 ug/L Methylcyclohexane ND 5.0 ug/L 4-Methyl-2-pentanone ND 5.0 ug/L Methyl tert-butyl ether ND 5.0 ug/L Styrene ND 5.0 ug/L (Continued on next page)



### C9K180557 17 of 161Clean Sites Environmental Services Inc Client Sample ID: TRIP BLANK-COKER 2

GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-005 Work Order #...: Work Order #...: LPPGV1AA Matrix.........: Matrix.........: WATER
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 1,1,2,2-Tetrachloroethane ND 5.0 ug/L 1,2,4-Trichloro- ND 5.0 ug/L benzene Tetrachloroethene ND 5.0 ug/L 1,1,1-Trichloroethane ND 5.0 ug/L 1,1,2-Trichloroethane ND 5.0 ug/L Trichloroethene ND 5.0 ug/L Trichlorofluoromethane ND 5.0 ug/L 1,1,2-Trichloro- ND 5.0 ug/L 1,2,2-trifluoroethane Toluene ND 5.0 ug/L Vinyl chloride ND 5.0 ug/L Xylenes (total) ND 15 ug/L
PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 1,2-Dichloroethane-d4 88 (62 - 123) Toluene-d8 106 (80 - 120) 4-Bromofluorobenzene 88 (75 - 120) Dibromofluoromethane 96 (80 - 120)



### C9K180557 18 of 161Clean Sites Environmental Services Inc Client Sample ID: L1-S1 GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-006 Work Order #...: Work Order #...: LPPG11AC Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9328229 Prep Date......: Prep Date......: 11/24/09 Analysis Date..: Analysis Date..: 11/24/09 Prep Batch #...: Prep Batch #...: 9328345 Analysis Time..: Analysis Time..: 20:04 Dilution Factor: Dilution Factor: 1 Method.........: Method.........: SW846 8260B
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acetone ND 20 ug/L Benzene ND 5.0 ug/L Bromodichloromethane ND 5.0 ug/L Bromoform ND 5.0 ug/L Bromomethane ND 5.0 ug/L 2-Butanone ND 5.0 ug/L Carbon disulfide ND 5.0 ug/L Carbon tetrachloride ND 5.0 ug/L Chlorobenzene ND 5.0 ug/L Chloroethane ND 5.0 ug/L Chloroform ND 5.0 ug/L Chloromethane ND 5.0 ug/L Cyclohexane ND 5.0 ug/L Dibromochloromethane ND 5.0 ug/L 1,2-Dibromo-3-chloro- ND 5.0 ug/L propane 1,2-Dibromoethane ND 5.0 ug/L 1,3-Dichlorobenzene ND 5.0 ug/L 1,4-Dichlorobenzene ND 5.0 ug/L 1,2-Dichlorobenzene ND 5.0 ug/L Dichlorodifluoromethane ND 5.0 ug/L 1,1-Dichloroethane ND 5.0 ug/L 1,2-Dichloroethane ND 5.0 ug/L 1,1-Dichloroethene ND 5.0 ug/L cis-1,2-Dichloroethene ND 5.0 ug/L trans-1,2-Dichloroethene ND 5.0 ug/L 1,2-Dichloropropane ND 5.0 ug/L cis-1,3-Dichloropropene ND 5.0 ug/L trans-1,3-Dichloropropene ND 5.0 ug/L Ethylbenzene ND 5.0 ug/L 2-Hexanone ND 5.0 ug/L Isopropylbenzene ND 5.0 ug/L Methyl acetate ND 5.0 ug/L Methylene chloride ND 5.0 ug/L Methylcyclohexane ND 5.0 ug/L 4-Methyl-2-pentanone ND 5.0 ug/L Methyl tert-butyl ether ND 5.0 ug/L Styrene ND 5.0 ug/L (Continued on next page)



### C9K180557 19 of 161Clean Sites Environmental Services Inc Client Sample ID: L1-S1 GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-006 Work Order #...: Work Order #...: LPPG11AC Matrix.........: Matrix.........: WATER
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 1,1,2,2-Tetrachloroethane ND 5.0 ug/L 1,2,4-Trichloro- ND 5.0 ug/L benzene Tetrachloroethene ND 5.0 ug/L 1,1,1-Trichloroethane ND 5.0 ug/L 1,1,2-Trichloroethane ND 5.0 ug/L Trichloroethene ND 5.0 ug/L Trichlorofluoromethane ND 5.0 ug/L 1,1,2-Trichloro- ND 5.0 ug/L 1,2,2-trifluoroethane Toluene ND 5.0 ug/L Vinyl chloride ND 5.0 ug/L Xylenes (total) ND 15 ug/L
PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 1,2-Dichloroethane-d4 89 (62 - 123) Toluene-d8 106 (80 - 120) 4-Bromofluorobenzene 87 (75 - 120) Dibromofluoromethane 99 (80 - 120)



### C9K180557 20 of 161Clean Sites Environmental Services Inc Client Sample ID: L1-S3 GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-007 Work Order #...: Work Order #...: LPPG61AJ Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9328229 Prep Date......: Prep Date......: 11/24/09 Analysis Date..: Analysis Date..: 11/24/09 Prep Batch #...: Prep Batch #...: 9328345 Analysis Time..: Analysis Time..: 20:30 Dilution Factor: Dilution Factor: 1 Method.........: Method.........: SW846 8260B
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acetone ND 20 ug/L Benzene ND 5.0 ug/L Bromodichloromethane ND 5.0 ug/L Bromoform ND 5.0 ug/L Bromomethane ND 5.0 ug/L 2-Butanone ND 5.0 ug/L Carbon disulfide ND 5.0 ug/L Carbon tetrachloride ND 5.0 ug/L Chlorobenzene ND 5.0 ug/L Chloroethane ND 5.0 ug/L Chloroform ND 5.0 ug/L Chloromethane ND 5.0 ug/L Cyclohexane ND 5.0 ug/L Dibromochloromethane ND 5.0 ug/L 1,2-Dibromo-3-chloro- ND 5.0 ug/L propane 1,2-Dibromoethane ND 5.0 ug/L 1,3-Dichlorobenzene ND 5.0 ug/L 1,4-Dichlorobenzene ND 5.0 ug/L 1,2-Dichlorobenzene ND 5.0 ug/L Dichlorodifluoromethane ND 5.0 ug/L 1,1-Dichloroethane ND 5.0 ug/L 1,2-Dichloroethane ND 5.0 ug/L 1,1-Dichloroethene ND 5.0 ug/L cis-1,2-Dichloroethene ND 5.0 ug/L trans-1,2-Dichloroethene ND 5.0 ug/L 1,2-Dichloropropane ND 5.0 ug/L cis-1,3-Dichloropropene ND 5.0 ug/L trans-1,3-Dichloropropene ND 5.0 ug/L Ethylbenzene ND 5.0 ug/L 2-Hexanone ND 5.0 ug/L Isopropylbenzene ND 5.0 ug/L Methyl acetate ND 5.0 ug/L Methylene chloride ND 5.0 ug/L Methylcyclohexane ND 5.0 ug/L 4-Methyl-2-pentanone ND 5.0 ug/L Methyl tert-butyl ether ND 5.0 ug/L Styrene ND 5.0 ug/L (Continued on next page)



### C9K180557 21 of 161Clean Sites Environmental Services Inc Client Sample ID: L1-S3 GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-007 Work Order #...: Work Order #...: LPPG61AJ Matrix.........: Matrix.........: WATER
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 1,1,2,2-Tetrachloroethane ND 5.0 ug/L 1,2,4-Trichloro- ND 5.0 ug/L benzene Tetrachloroethene ND 5.0 ug/L 1,1,1-Trichloroethane ND 5.0 ug/L 1,1,2-Trichloroethane ND 5.0 ug/L Trichloroethene ND 5.0 ug/L Trichlorofluoromethane ND 5.0 ug/L 1,1,2-Trichloro- ND 5.0 ug/L 1,2,2-trifluoroethane Toluene ND 5.0 ug/L Vinyl chloride ND 5.0 ug/L Xylenes (total) ND 15 ug/L
PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 1,2-Dichloroethane-d4 94 (62 - 123) Toluene-d8 103 (80 - 120) 4-Bromofluorobenzene 88 (75 - 120) Dibromofluoromethane 100 (80 - 120)



### C9K180557 22 of 161Clean Sites Environmental Services Inc Client Sample ID: L1-S4 GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-008 Work Order #...: Work Order #...: LPPG81AQ Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9328229 Prep Date......: Prep Date......: 11/24/09 Analysis Date..: Analysis Date..: 11/24/09 Prep Batch #...: Prep Batch #...: 9328345 Analysis Time..: Analysis Time..: 20:56 Dilution Factor: Dilution Factor: 1 Method.........: Method.........: SW846 8260B
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acetone ND 20 ug/L Benzene ND 5.0 ug/L Bromodichloromethane ND 5.0 ug/L Bromoform ND 5.0 ug/L Bromomethane ND 5.0 ug/L 2-Butanone ND 5.0 ug/L Carbon disulfide ND 5.0 ug/L Carbon tetrachloride ND 5.0 ug/L Chlorobenzene ND 5.0 ug/L Chloroethane ND 5.0 ug/L Chloroform ND 5.0 ug/L Chloromethane ND 5.0 ug/L Cyclohexane ND 5.0 ug/L Dibromochloromethane ND 5.0 ug/L 1,2-Dibromo-3-chloro- ND 5.0 ug/L propane 1,2-Dibromoethane ND 5.0 ug/L 1,3-Dichlorobenzene ND 5.0 ug/L 1,4-Dichlorobenzene ND 5.0 ug/L 1,2-Dichlorobenzene ND 5.0 ug/L Dichlorodifluoromethane ND 5.0 ug/L 1,1-Dichloroethane ND 5.0 ug/L 1,2-Dichloroethane ND 5.0 ug/L 1,1-Dichloroethene ND 5.0 ug/L cis-1,2-Dichloroethene ND 5.0 ug/L trans-1,2-Dichloroethene ND 5.0 ug/L 1,2-Dichloropropane ND 5.0 ug/L cis-1,3-Dichloropropene ND 5.0 ug/L trans-1,3-Dichloropropene ND 5.0 ug/L Ethylbenzene ND 5.0 ug/L 2-Hexanone ND 5.0 ug/L Isopropylbenzene ND 5.0 ug/L Methyl acetate ND 5.0 ug/L Methylene chloride ND 5.0 ug/L Methylcyclohexane ND 5.0 ug/L 4-Methyl-2-pentanone ND 5.0 ug/L Methyl tert-butyl ether ND 5.0 ug/L Styrene ND 5.0 ug/L (Continued on next page)



### C9K180557 23 of 161Clean Sites Environmental Services Inc Client Sample ID: L1-S4 GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-008 Work Order #...: Work Order #...: LPPG81AQ Matrix.........: Matrix.........: WATER
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 1,1,2,2-Tetrachloroethane ND 5.0 ug/L 1,2,4-Trichloro- ND 5.0 ug/L benzene Tetrachloroethene ND 5.0 ug/L 1,1,1-Trichloroethane ND 5.0 ug/L 1,1,2-Trichloroethane ND 5.0 ug/L Trichloroethene ND 5.0 ug/L Trichlorofluoromethane ND 5.0 ug/L 1,1,2-Trichloro- ND 5.0 ug/L 1,2,2-trifluoroethane Toluene ND 5.0 ug/L Vinyl chloride ND 5.0 ug/L Xylenes (total) ND 15 ug/L
PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 1,2-Dichloroethane-d4 90 (62 - 123) Toluene-d8 107 (80 - 120) 4-Bromofluorobenzene 88 (75 - 120) Dibromofluoromethane 98 (80 - 120)



### C9K180557 24 of 161Clean Sites Environmental Services Inc Client Sample ID: SW-1 GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-009 Work Order #...: Work Order #...: LPPHA1AX Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9328229 Prep Date......: Prep Date......: 11/24/09 Analysis Date..: Analysis Date..: 11/24/09 Prep Batch #...: Prep Batch #...: 9328345 Analysis Time..: Analysis Time..: 21:22 Dilution Factor: Dilution Factor: 1 Method.........: Method.........: SW846 8260B
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acetone ND 20 ug/L Benzene ND 5.0 ug/L Bromodichloromethane ND 5.0 ug/L Bromoform ND 5.0 ug/L Bromomethane ND 5.0 ug/L 2-Butanone ND 5.0 ug/L Carbon disulfide ND 5.0 ug/L Carbon tetrachloride ND 5.0 ug/L Chlorobenzene ND 5.0 ug/L Chloroethane ND 5.0 ug/L Chloroform ND 5.0 ug/L Chloromethane ND 5.0 ug/L Cyclohexane ND 5.0 ug/L Dibromochloromethane ND 5.0 ug/L 1,2-Dibromo-3-chloro- ND 5.0 ug/L propane 1,2-Dibromoethane ND 5.0 ug/L 1,3-Dichlorobenzene ND 5.0 ug/L 1,4-Dichlorobenzene ND 5.0 ug/L 1,2-Dichlorobenzene ND 5.0 ug/L Dichlorodifluoromethane ND 5.0 ug/L 1,1-Dichloroethane ND 5.0 ug/L 1,2-Dichloroethane ND 5.0 ug/L 1,1-Dichloroethene ND 5.0 ug/L cis-1,2-Dichloroethene ND 5.0 ug/L trans-1,2-Dichloroethene ND 5.0 ug/L 1,2-Dichloropropane ND 5.0 ug/L cis-1,3-Dichloropropene ND 5.0 ug/L trans-1,3-Dichloropropene ND 5.0 ug/L Ethylbenzene ND 5.0 ug/L 2-Hexanone ND 5.0 ug/L Isopropylbenzene ND 5.0 ug/L Methyl acetate ND 5.0 ug/L Methylene chloride ND 5.0 ug/L Methylcyclohexane ND 5.0 ug/L 4-Methyl-2-pentanone ND 5.0 ug/L Methyl tert-butyl ether ND 5.0 ug/L Styrene ND 5.0 ug/L (Continued on next page)



### C9K180557 25 of 161Clean Sites Environmental Services Inc Client Sample ID: SW-1 GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-009 Work Order #...: Work Order #...: LPPHA1AX Matrix.........: Matrix.........: WATER
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 1,1,2,2-Tetrachloroethane ND 5.0 ug/L 1,2,4-Trichloro- ND 5.0 ug/L benzene Tetrachloroethene ND 5.0 ug/L 1,1,1-Trichloroethane ND 5.0 ug/L 1,1,2-Trichloroethane ND 5.0 ug/L Trichloroethene ND 5.0 ug/L Trichlorofluoromethane ND 5.0 ug/L 1,1,2-Trichloro- ND 5.0 ug/L 1,2,2-trifluoroethane Toluene ND 5.0 ug/L Vinyl chloride ND 5.0 ug/L Xylenes (total) ND 15 ug/L
PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 1,2-Dichloroethane-d4 87 (62 - 123) Toluene-d8 108 (80 - 120) 4-Bromofluorobenzene 87 (75 - 120) Dibromofluoromethane 97 (80 - 120)



### C9K180557 26 of 161Clean Sites Environmental Services Inc Client Sample ID: SW-2 GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-010 Work Order #...: Work Order #...: LPPHF1A5 Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9328229 Prep Date......: Prep Date......: 11/24/09 Analysis Date..: Analysis Date..: 11/24/09 Prep Batch #...: Prep Batch #...: 9328345 Analysis Time..: Analysis Time..: 21:47 Dilution Factor: Dilution Factor: 1 Method.........: Method.........: SW846 8260B
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acetone ND 20 ug/L Benzene ND 5.0 ug/L Bromodichloromethane ND 5.0 ug/L Bromoform ND 5.0 ug/L Bromomethane ND 5.0 ug/L 2-Butanone ND 5.0 ug/L Carbon disulfide ND 5.0 ug/L Carbon tetrachloride ND 5.0 ug/L Chlorobenzene ND 5.0 ug/L Chloroethane ND 5.0 ug/L Chloroform ND 5.0 ug/L Chloromethane ND 5.0 ug/L Cyclohexane ND 5.0 ug/L Dibromochloromethane ND 5.0 ug/L 1,2-Dibromo-3-chloro- ND 5.0 ug/L propane 1,2-Dibromoethane ND 5.0 ug/L 1,3-Dichlorobenzene ND 5.0 ug/L 1,4-Dichlorobenzene ND 5.0 ug/L 1,2-Dichlorobenzene ND 5.0 ug/L Dichlorodifluoromethane ND 5.0 ug/L 1,1-Dichloroethane ND 5.0 ug/L 1,2-Dichloroethane ND 5.0 ug/L 1,1-Dichloroethene ND 5.0 ug/L cis-1,2-Dichloroethene ND 5.0 ug/L trans-1,2-Dichloroethene ND 5.0 ug/L 1,2-Dichloropropane ND 5.0 ug/L cis-1,3-Dichloropropene ND 5.0 ug/L trans-1,3-Dichloropropene ND 5.0 ug/L Ethylbenzene ND 5.0 ug/L 2-Hexanone ND 5.0 ug/L Isopropylbenzene ND 5.0 ug/L Methyl acetate ND 5.0 ug/L Methylene chloride ND 5.0 ug/L Methylcyclohexane ND 5.0 ug/L 4-Methyl-2-pentanone ND 5.0 ug/L Methyl tert-butyl ether ND 5.0 ug/L Styrene ND 5.0 ug/L (Continued on next page)



### C9K180557 27 of 161Clean Sites Environmental Services Inc Client Sample ID: SW-2 GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-010 Work Order #...: Work Order #...: LPPHF1A5 Matrix.........: Matrix.........: WATER
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 1,1,2,2-Tetrachloroethane ND 5.0 ug/L 1,2,4-Trichloro- ND 5.0 ug/L benzene Tetrachloroethene ND 5.0 ug/L 1,1,1-Trichloroethane ND 5.0 ug/L 1,1,2-Trichloroethane ND 5.0 ug/L Trichloroethene ND 5.0 ug/L Trichlorofluoromethane ND 5.0 ug/L 1,1,2-Trichloro- ND 5.0 ug/L 1,2,2-trifluoroethane Toluene ND 5.0 ug/L Vinyl chloride ND 5.0 ug/L Xylenes (total) ND 15 ug/L
PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 1,2-Dichloroethane-d4 89 (62 - 123) Toluene-d8 107 (80 - 120) 4-Bromofluorobenzene 87 (75 - 120) Dibromofluoromethane 97 (80 - 120)



### C9K180557 28 of 161Clean Sites Environmental Services Inc Client Sample ID: SW-3 GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-011 Work Order #...: Work Order #...: LPPHG1A5 Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9328229 Prep Date......: Prep Date......: 11/24/09 Analysis Date..: Analysis Date..: 11/24/09 Prep Batch #...: Prep Batch #...: 9328345 Analysis Time..: Analysis Time..: 22:13 Dilution Factor: Dilution Factor: 1 Method.........: Method.........: SW846 8260B
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acetone ND 20 ug/L Benzene ND 5.0 ug/L Bromodichloromethane ND 5.0 ug/L Bromoform ND 5.0 ug/L Bromomethane ND 5.0 ug/L 2-Butanone ND 5.0 ug/L Carbon disulfide ND 5.0 ug/L Carbon tetrachloride ND 5.0 ug/L Chlorobenzene ND 5.0 ug/L Chloroethane ND 5.0 ug/L Chloroform ND 5.0 ug/L Chloromethane ND 5.0 ug/L Cyclohexane ND 5.0 ug/L Dibromochloromethane ND 5.0 ug/L 1,2-Dibromo-3-chloro- ND 5.0 ug/L propane 1,2-Dibromoethane ND 5.0 ug/L 1,3-Dichlorobenzene ND 5.0 ug/L 1,4-Dichlorobenzene ND 5.0 ug/L 1,2-Dichlorobenzene ND 5.0 ug/L Dichlorodifluoromethane ND 5.0 ug/L 1,1-Dichloroethane ND 5.0 ug/L 1,2-Dichloroethane ND 5.0 ug/L 1,1-Dichloroethene ND 5.0 ug/L cis-1,2-Dichloroethene ND 5.0 ug/L trans-1,2-Dichloroethene ND 5.0 ug/L 1,2-Dichloropropane ND 5.0 ug/L cis-1,3-Dichloropropene ND 5.0 ug/L trans-1,3-Dichloropropene ND 5.0 ug/L Ethylbenzene ND 5.0 ug/L 2-Hexanone ND 5.0 ug/L Isopropylbenzene ND 5.0 ug/L Methyl acetate ND 5.0 ug/L Methylene chloride ND 5.0 ug/L Methylcyclohexane ND 5.0 ug/L 4-Methyl-2-pentanone ND 5.0 ug/L Methyl tert-butyl ether ND 5.0 ug/L Styrene ND 5.0 ug/L (Continued on next page)



### C9K180557 29 of 161Clean Sites Environmental Services Inc Client Sample ID: SW-3 GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-011 Work Order #...: Work Order #...: LPPHG1A5 Matrix.........: Matrix.........: WATER
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 1,1,2,2-Tetrachloroethane ND 5.0 ug/L 1,2,4-Trichloro- ND 5.0 ug/L benzene Tetrachloroethene ND 5.0 ug/L 1,1,1-Trichloroethane ND 5.0 ug/L 1,1,2-Trichloroethane ND 5.0 ug/L Trichloroethene ND 5.0 ug/L Trichlorofluoromethane ND 5.0 ug/L 1,1,2-Trichloro- ND 5.0 ug/L 1,2,2-trifluoroethane Toluene ND 5.0 ug/L Vinyl chloride ND 5.0 ug/L Xylenes (total) ND 15 ug/L
PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 1,2-Dichloroethane-d4 88 (62 - 123) Toluene-d8 108 (80 - 120) 4-Bromofluorobenzene 87 (75 - 120) Dibromofluoromethane 99 (80 - 120)



### C9K180557 30 of 161Clean Sites Environmental Services Inc Client Sample ID: SED-1 GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-012 Work Order #...: Work Order #...: LPPHK1AD Matrix.........: Matrix.........: SOLID Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9329143 Prep Date......: Prep Date......: 11/25/09 Analysis Date..: Analysis Date..: 11/25/09 Prep Batch #...: Prep Batch #...: 9329221 Analysis Time..: Analysis Time..: 12:36 Dilution Factor: Dilution Factor: 1 % Moisture.....: % Moisture.....: 20 Method.........: Method.........: SW846 8260B
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acetone ND 25 ug/kg Benzene ND 6.2 ug/kg Bromodichloromethane ND 6.2 ug/kg Bromoform ND 6.2 ug/kg Bromomethane ND 6.2 ug/kg 2-Butanone ND 6.2 ug/kg Carbon disulfide ND 6.2 ug/kg Carbon tetrachloride ND 6.2 ug/kg Chlorobenzene ND 6.2 ug/kg Chloroethane ND 6.2 ug/kg Chloroform ND 6.2 ug/kg Chloromethane ND 6.2 ug/kg Cyclohexane ND 6.2 ug/kg Dibromochloromethane ND 6.2 ug/kg 1,2-Dibromo-3-chloro- ND 6.2 ug/kg propane 1,2-Dibromoethane ND 6.2 ug/kg 1,3-Dichlorobenzene ND 6.2 ug/kg 1,4-Dichlorobenzene ND 6.2 ug/kg 1,2-Dichlorobenzene ND 6.2 ug/kg Dichlorodifluoromethane ND 6.2 ug/kg 1,1-Dichloroethane ND 6.2 ug/kg 1,2-Dichloroethane ND 6.2 ug/kg 1,1-Dichloroethene ND 6.2 ug/kg cis-1,2-Dichloroethene ND 6.2 ug/kg trans-1,2-Dichloroethene ND 6.2 ug/kg 1,2-Dichloropropane ND 6.2 ug/kg cis-1,3-Dichloropropene ND 6.2 ug/kg trans-1,3-Dichloropropene ND 6.2 ug/kg Ethylbenzene ND 6.2 ug/kg 2-Hexanone ND 6.2 ug/kg Isopropylbenzene ND 6.2 ug/kg Methyl acetate ND 6.2 ug/kg Methylene chloride ND 6.2 ug/kg Methylcyclohexane ND 6.2 ug/kg 4-Methyl-2-pentanone ND 6.2 ug/kg Methyl tert-butyl ether ND 6.2 ug/kg Styrene ND 6.2 ug/kg (Continued on next page)



### C9K180557 31 of 161Clean Sites Environmental Services Inc Client Sample ID: SED-1 GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-012 Work Order #...: Work Order #...: LPPHK1AD Matrix.........: Matrix.........: SOLID
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 1,1,2,2-Tetrachloroethane ND 6.2 ug/kg 1,2,4-Trichloro- ND 6.2 ug/kg benzene Tetrachloroethene ND 6.2 ug/kg 1,1,1-Trichloroethane ND 6.2 ug/kg 1,1,2-Trichloroethane ND 6.2 ug/kg Trichloroethene ND 6.2 ug/kg Trichlorofluoromethane ND 6.2 ug/kg 1,1,2-Trichloro- ND 6.2 ug/kg 1,2,2-trifluoroethane Toluene ND 6.2 ug/kg Vinyl chloride ND 6.2 ug/kg Xylenes (total) ND 19 ug/kg
PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 1,2-Dichloroethane-d4 102 (52 - 124) Toluene-d8 89 (72 - 127) 4-Bromofluorobenzene 96 (63 - 120) Dibromofluoromethane 115 (68 - 121) NOTE(S):

_______________________________________________________________________________________ Results and reporting limits have been adjusted for dry weight.



### C9K180557 32 of 161Clean Sites Environmental Services Inc Client Sample ID: SED-2 GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-013 Work Order #...: Work Order #...: LPPHM1AL Matrix.........: Matrix.........: SOLID Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9329143 Prep Date......: Prep Date......: 11/25/09 Analysis Date..: Analysis Date..: 11/25/09 Prep Batch #...: Prep Batch #...: 9329221 Analysis Time..: Analysis Time..: 13:00 Dilution Factor: Dilution Factor: 1 % Moisture.....: % Moisture.....: 20 Method.........: Method.........: SW846 8260B
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acetone ND 25 ug/kg Benzene ND 6.2 ug/kg Bromodichloromethane ND 6.2 ug/kg Bromoform ND 6.2 ug/kg Bromomethane ND 6.2 ug/kg 2-Butanone ND 6.2 ug/kg Carbon disulfide ND 6.2 ug/kg Carbon tetrachloride ND 6.2 ug/kg Chlorobenzene ND 6.2 ug/kg Chloroethane ND 6.2 ug/kg Chloroform ND 6.2 ug/kg Chloromethane ND 6.2 ug/kg Cyclohexane ND 6.2 ug/kg Dibromochloromethane ND 6.2 ug/kg 1,2-Dibromo-3-chloro- ND 6.2 ug/kg propane 1,2-Dibromoethane ND 6.2 ug/kg 1,3-Dichlorobenzene ND 6.2 ug/kg 1,4-Dichlorobenzene ND 6.2 ug/kg 1,2-Dichlorobenzene ND 6.2 ug/kg Dichlorodifluoromethane ND 6.2 ug/kg 1,1-Dichloroethane ND 6.2 ug/kg 1,2-Dichloroethane ND 6.2 ug/kg 1,1-Dichloroethene ND 6.2 ug/kg cis-1,2-Dichloroethene ND 6.2 ug/kg trans-1,2-Dichloroethene ND 6.2 ug/kg 1,2-Dichloropropane ND 6.2 ug/kg cis-1,3-Dichloropropene ND 6.2 ug/kg trans-1,3-Dichloropropene ND 6.2 ug/kg Ethylbenzene ND 6.2 ug/kg 2-Hexanone ND 6.2 ug/kg Isopropylbenzene ND 6.2 ug/kg Methyl acetate ND 6.2 ug/kg Methylene chloride ND 6.2 ug/kg Methylcyclohexane ND 6.2 ug/kg 4-Methyl-2-pentanone ND 6.2 ug/kg Methyl tert-butyl ether ND 6.2 ug/kg Styrene ND 6.2 ug/kg (Continued on next page)



### C9K180557 33 of 161Clean Sites Environmental Services Inc Client Sample ID: SED-2 GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-013 Work Order #...: Work Order #...: LPPHM1AL Matrix.........: Matrix.........: SOLID
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 1,1,2,2-Tetrachloroethane ND 6.2 ug/kg 1,2,4-Trichloro- ND 6.2 ug/kg benzene Tetrachloroethene ND 6.2 ug/kg 1,1,1-Trichloroethane ND 6.2 ug/kg 1,1,2-Trichloroethane ND 6.2 ug/kg Trichloroethene ND 6.2 ug/kg Trichlorofluoromethane ND 6.2 ug/kg 1,1,2-Trichloro- ND 6.2 ug/kg 1,2,2-trifluoroethane Toluene ND 6.2 ug/kg Vinyl chloride ND 6.2 ug/kg Xylenes (total) ND 19 ug/kg
PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 1,2-Dichloroethane-d4 101 (52 - 124) Toluene-d8 87 (72 - 127) 4-Bromofluorobenzene 97 (63 - 120) Dibromofluoromethane 111 (68 - 121) NOTE(S):

_______________________________________________________________________________________ Results and reporting limits have been adjusted for dry weight.



### C9K180557 34 of 161Clean Sites Environmental Services Inc Client Sample ID: SED-3 GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-014 Work Order #...: Work Order #...: LPPHN1AU Matrix.........: Matrix.........: SOLID Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9329143 Prep Date......: Prep Date......: 11/25/09 Analysis Date..: Analysis Date..: 11/25/09 Prep Batch #...: Prep Batch #...: 9329221 Analysis Time..: Analysis Time..: 13:25 Dilution Factor: Dilution Factor: 1 % Moisture.....: % Moisture.....: 23 Method.........: Method.........: SW846 8260B
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acetone ND 26 ug/kg Benzene ND 6.5 ug/kg Bromodichloromethane ND 6.5 ug/kg Bromoform ND 6.5 ug/kg Bromomethane ND 6.5 ug/kg 2-Butanone ND 6.5 ug/kg Carbon disulfide ND 6.5 ug/kg Carbon tetrachloride ND 6.5 ug/kg Chlorobenzene ND 6.5 ug/kg Chloroethane ND 6.5 ug/kg Chloroform ND 6.5 ug/kg Chloromethane ND 6.5 ug/kg Cyclohexane ND 6.5 ug/kg Dibromochloromethane ND 6.5 ug/kg 1,2-Dibromo-3-chloro- ND 6.5 ug/kg propane 1,2-Dibromoethane ND 6.5 ug/kg 1,3-Dichlorobenzene ND 6.5 ug/kg 1,4-Dichlorobenzene ND 6.5 ug/kg 1,2-Dichlorobenzene ND 6.5 ug/kg Dichlorodifluoromethane ND 6.5 ug/kg 1,1-Dichloroethane ND 6.5 ug/kg 1,2-Dichloroethane ND 6.5 ug/kg 1,1-Dichloroethene ND 6.5 ug/kg cis-1,2-Dichloroethene ND 6.5 ug/kg trans-1,2-Dichloroethene ND 6.5 ug/kg 1,2-Dichloropropane ND 6.5 ug/kg cis-1,3-Dichloropropene ND 6.5 ug/kg trans-1,3-Dichloropropene ND 6.5 ug/kg Ethylbenzene ND 6.5 ug/kg 2-Hexanone ND 6.5 ug/kg Isopropylbenzene ND 6.5 ug/kg Methyl acetate ND 6.5 ug/kg Methylene chloride ND 6.5 ug/kg Methylcyclohexane ND 6.5 ug/kg 4-Methyl-2-pentanone ND 6.5 ug/kg Methyl tert-butyl ether ND 6.5 ug/kg Styrene ND 6.5 ug/kg (Continued on next page)



### C9K180557 35 of 161Clean Sites Environmental Services Inc Client Sample ID: SED-3 GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-014 Work Order #...: Work Order #...: LPPHN1AU Matrix.........: Matrix.........: SOLID
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 1,1,2,2-Tetrachloroethane ND 6.5 ug/kg 1,2,4-Trichloro- ND 6.5 ug/kg benzene Tetrachloroethene ND 6.5 ug/kg 1,1,1-Trichloroethane ND 6.5 ug/kg 1,1,2-Trichloroethane ND 6.5 ug/kg Trichloroethene ND 6.5 ug/kg Trichlorofluoromethane ND 6.5 ug/kg 1,1,2-Trichloro- ND 6.5 ug/kg 1,2,2-trifluoroethane Toluene ND 6.5 ug/kg Vinyl chloride ND 6.5 ug/kg Xylenes (total) ND 19 ug/kg
PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 1,2-Dichloroethane-d4 101 (52 - 124) Toluene-d8 89 (72 - 127) 4-Bromofluorobenzene 97 (63 - 120) Dibromofluoromethane 112 (68 - 121) NOTE(S):

_______________________________________________________________________________________ Results and reporting limits have been adjusted for dry weight.



### C9K180557 36 of 161Clean Sites Environmental Services Inc Client Sample ID: TRIP BLANK-COKER 1

GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-015 Work Order #...: Work Order #...: LPPHV1AA Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9329152 Prep Date......: Prep Date......: 11/25/09 Analysis Date..: Analysis Date..: 11/25/09 Prep Batch #...: Prep Batch #...: 9329174 Analysis Time..: Analysis Time..: 14:26 Dilution Factor: Dilution Factor: 1 Method.........: Method.........: SW846 8260B
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acetone ND 20 ug/L Benzene ND 5.0 ug/L Bromodichloromethane ND 5.0 ug/L Bromoform ND 5.0 ug/L Bromomethane ND 5.0 ug/L 2-Butanone ND 5.0 ug/L Carbon disulfide ND 5.0 ug/L Carbon tetrachloride ND 5.0 ug/L Chlorobenzene ND 5.0 ug/L Chloroethane ND 5.0 ug/L Chloroform ND 5.0 ug/L Chloromethane ND 5.0 ug/L Cyclohexane ND 5.0 ug/L Dibromochloromethane ND 5.0 ug/L 1,2-Dibromo-3-chloro- ND 5.0 ug/L propane 1,2-Dibromoethane ND 5.0 ug/L 1,3-Dichlorobenzene ND 5.0 ug/L 1,4-Dichlorobenzene ND 5.0 ug/L 1,2-Dichlorobenzene ND 5.0 ug/L Dichlorodifluoromethane ND 5.0 ug/L 1,1-Dichloroethane ND 5.0 ug/L 1,2-Dichloroethane ND 5.0 ug/L 1,1-Dichloroethene ND 5.0 ug/L cis-1,2-Dichloroethene ND 5.0 ug/L trans-1,2-Dichloroethene ND 5.0 ug/L 1,2-Dichloropropane ND 5.0 ug/L cis-1,3-Dichloropropene ND 5.0 ug/L trans-1,3-Dichloropropene ND 5.0 ug/L Ethylbenzene ND 5.0 ug/L 2-Hexanone ND 5.0 ug/L Isopropylbenzene ND 5.0 ug/L Methyl acetate ND 5.0 ug/L Methylene chloride ND 5.0 ug/L Methylcyclohexane ND 5.0 ug/L 4-Methyl-2-pentanone ND 5.0 ug/L Methyl tert-butyl ether ND 5.0 ug/L Styrene ND 5.0 ug/L (Continued on next page)



### C9K180557 37 of 161Clean Sites Environmental Services Inc Client Sample ID: TRIP BLANK-COKER 1

GC/MS Volatiles Lot-Sample #...: Lot-Sample #...: C9K180557-015 Work Order #...: Work Order #...: LPPHV1AA Matrix.........: Matrix.........: WATER
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 1,1,2,2-Tetrachloroethane ND 5.0 ug/L 1,2,4-Trichloro- ND 5.0 ug/L benzene Tetrachloroethene ND 5.0 ug/L 1,1,1-Trichloroethane ND 5.0 ug/L 1,1,2-Trichloroethane ND 5.0 ug/L Trichloroethene ND 5.0 ug/L Trichlorofluoromethane ND 5.0 ug/L 1,1,2-Trichloro- ND 5.0 ug/L 1,2,2-trifluoroethane Toluene ND 5.0 ug/L Vinyl chloride ND 5.0 ug/L Xylenes (total) ND 15 ug/L
PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 1,2-Dichloroethane-d4 94 (62 - 123) Toluene-d8 103 (80 - 120) 4-Bromofluorobenzene 90 (75 - 120) Dibromofluoromethane 102 (80 - 120)



### C9K180557 38 of 161METHOD BLANK REPORT GC/MS Volatiles Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LP2741AA Matrix.........: Matrix.........: WATER MB Lot-Sample #: MB Lot-Sample #: C9K240000-345 Prep Date......: Prep Date......: 11/24/09 Analysis Time..: Analysis Time..: 13:14 Analysis Date..: Analysis Date..: 11/24/09 Prep Batch #...: Prep Batch #...: 9328345 Dilution Factor: Dilution Factor: 1
REPORTING PARAMETER _________________________ RESULT _______________ LIMIT

_________ UNITS

__________ METHOD

_________________ Acetone ND 20 ug/L SW846 8260B Benzene ND 5.0 ug/L SW846 8260B Bromodichloromethane ND 5.0 ug/L SW846 8260B Bromoform ND 5.0 ug/L SW846 8260B Bromomethane ND 5.0 ug/L SW846 8260B 2-Butanone ND 5.0 ug/L SW846 8260B Carbon disulfide ND 5.0 ug/L SW846 8260B Carbon tetrachloride ND 5.0 ug/L SW846 8260B Chlorobenzene ND 5.0 ug/L SW846 8260B Chloroethane ND 5.0 ug/L SW846 8260B Chloroform ND 5.0 ug/L SW846 8260B Chloromethane ND 5.0 ug/L SW846 8260B Cyclohexane ND 5.0 ug/L SW846 8260B Dibromochloromethane ND 5.0 ug/L SW846 8260B 1,2-Dibromo-3-chloro- ND 5.0 ug/L SW846 8260B propane 1,2-Dibromoethane ND 5.0 ug/L SW846 8260B 1,3-Dichlorobenzene ND 5.0 ug/L SW846 8260B 1,4-Dichlorobenzene ND 5.0 ug/L SW846 8260B 1,2-Dichlorobenzene ND 5.0 ug/L SW846 8260B Dichlorodifluoromethane ND 5.0 ug/L SW846 8260B 1,1-Dichloroethane ND 5.0 ug/L SW846 8260B 1,2-Dichloroethane ND 5.0 ug/L SW846 8260B 1,1-Dichloroethene ND 5.0 ug/L SW846 8260B cis-1,2-Dichloroethene ND 5.0 ug/L SW846 8260B trans-1,2-Dichloroethene ND 5.0 ug/L SW846 8260B 1,2-Dichloropropane ND 5.0 ug/L SW846 8260B cis-1,3-Dichloropropene ND 5.0 ug/L SW846 8260B trans-1,3-Dichloropropene ND 5.0 ug/L SW846 8260B Ethylbenzene ND 5.0 ug/L SW846 8260B 2-Hexanone ND 5.0 ug/L SW846 8260B Isopropylbenzene ND 5.0 ug/L SW846 8260B Methyl acetate ND 5.0 ug/L SW846 8260B Methylene chloride ND 5.0 ug/L SW846 8260B Methylcyclohexane ND 5.0 ug/L SW846 8260B 4-Methyl-2-pentanone ND 5.0 ug/L SW846 8260B Methyl tert-butyl ether ND 5.0 ug/L SW846 8260B Styrene ND 5.0 ug/L SW846 8260B 1,1,2,2-Tetrachloroethane ND 5.0 ug/L SW846 8260B 1,2,4-Trichloro- ND 5.0 ug/L SW846 8260B benzene (Continued on next page)



### C9K180557 39 of 161METHOD BLANK REPORT GC/MS Volatiles Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LP2741AA Matrix.........: Matrix.........: WATER
REPORTING PARAMETER _________________________ RESULT _______________ LIMIT

_________ UNITS

__________ METHOD

_________________ Tetrachloroethene ND 5.0 ug/L SW846 8260B 1,1,1-Trichloroethane ND 5.0 ug/L SW846 8260B 1,1,2-Trichloroethane ND 5.0 ug/L SW846 8260B Trichloroethene ND 5.0 ug/L SW846 8260B Trichlorofluoromethane ND 5.0 ug/L SW846 8260B 1,1,2-Trichloro- ND 5.0 ug/L SW846 8260B 1,2,2-trifluoroethane Toluene ND 5.0 ug/L SW846 8260B Vinyl chloride ND 5.0 ug/L SW846 8260B Xylenes (total) ND 15 ug/L SW846 8260B
PERCENT RECOVERY SURROGATE _________________________ RECOVERY ________ LIMITS

__________ 1,2-Dichloroethane-d4 102 (62 - 123) Toluene-d8 99 (80 - 120) 4-Bromofluorobenzene 89 (75 - 120) Dibromofluoromethane 110 (80 - 120) NOTE(S):

___________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results.



### C9K180557 40 of 161METHOD BLANK REPORT GC/MS Volatiles Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LP42D1AA Matrix.........: Matrix.........: WATER MB Lot-Sample #: MB Lot-Sample #: C9K250000-174 Prep Date......: Prep Date......: 11/25/09 Analysis Time..: Analysis Time..: 08:36 Analysis Date..: Analysis Date..: 11/25/09 Prep Batch #...: Prep Batch #...: 9329174 Dilution Factor: Dilution Factor: 1
REPORTING PARAMETER _________________________ RESULT _______________ LIMIT

_________ UNITS

__________ METHOD

_________________ Acetone ND 20 ug/L SW846 8260B Benzene ND 5.0 ug/L SW846 8260B Bromodichloromethane ND 5.0 ug/L SW846 8260B Bromoform ND 5.0 ug/L SW846 8260B Bromomethane ND 5.0 ug/L SW846 8260B 2-Butanone ND 5.0 ug/L SW846 8260B Carbon disulfide ND 5.0 ug/L SW846 8260B Carbon tetrachloride ND 5.0 ug/L SW846 8260B Chlorobenzene ND 5.0 ug/L SW846 8260B Chloroethane ND 5.0 ug/L SW846 8260B Chloroform ND 5.0 ug/L SW846 8260B Chloromethane ND 5.0 ug/L SW846 8260B Cyclohexane ND 5.0 ug/L SW846 8260B Dibromochloromethane ND 5.0 ug/L SW846 8260B 1,2-Dibromo-3-chloro- ND 5.0 ug/L SW846 8260B propane 1,2-Dibromoethane ND 5.0 ug/L SW846 8260B 1,3-Dichlorobenzene ND 5.0 ug/L SW846 8260B 1,4-Dichlorobenzene ND 5.0 ug/L SW846 8260B 1,2-Dichlorobenzene ND 5.0 ug/L SW846 8260B Dichlorodifluoromethane ND 5.0 ug/L SW846 8260B 1,1-Dichloroethane ND 5.0 ug/L SW846 8260B 1,2-Dichloroethane ND 5.0 ug/L SW846 8260B 1,1-Dichloroethene ND 5.0 ug/L SW846 8260B cis-1,2-Dichloroethene ND 5.0 ug/L SW846 8260B trans-1,2-Dichloroethene ND 5.0 ug/L SW846 8260B 1,2-Dichloropropane ND 5.0 ug/L SW846 8260B cis-1,3-Dichloropropene ND 5.0 ug/L SW846 8260B trans-1,3-Dichloropropene ND 5.0 ug/L SW846 8260B Ethylbenzene ND 5.0 ug/L SW846 8260B 2-Hexanone ND 5.0 ug/L SW846 8260B Isopropylbenzene ND 5.0 ug/L SW846 8260B Methyl acetate ND 5.0 ug/L SW846 8260B Methylene chloride ND 5.0 ug/L SW846 8260B Methylcyclohexane ND 5.0 ug/L SW846 8260B 4-Methyl-2-pentanone ND 5.0 ug/L SW846 8260B Methyl tert-butyl ether ND 5.0 ug/L SW846 8260B Styrene ND 5.0 ug/L SW846 8260B 1,1,2,2-Tetrachloroethane ND 5.0 ug/L SW846 8260B 1,2,4-Trichloro- ND 5.0 ug/L SW846 8260B benzene (Continued on next page)



### C9K180557 41 of 161METHOD BLANK REPORT GC/MS Volatiles Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LP42D1AA Matrix.........: Matrix.........: WATER
REPORTING PARAMETER _________________________ RESULT _______________ LIMIT

_________ UNITS

__________ METHOD

_________________ Tetrachloroethene ND 5.0 ug/L SW846 8260B 1,1,1-Trichloroethane ND 5.0 ug/L SW846 8260B 1,1,2-Trichloroethane ND 5.0 ug/L SW846 8260B Trichloroethene ND 5.0 ug/L SW846 8260B Trichlorofluoromethane ND 5.0 ug/L SW846 8260B 1,1,2-Trichloro- ND ug/L SW846 8260B 1,2,2-trifluoroethane Toluene ND 5.0 ug/L SW846 8260B Vinyl chloride ND 5.0 ug/L SW846 8260B Xylenes (total) ND 15 ug/L SW846 8260B
PERCENT RECOVERY SURROGATE _________________________ RECOVERY ________ LIMITS

__________ 1,2-Dichloroethane-d4 95 (62 - 123) Toluene-d8 103 (80 - 120) 4-Bromofluorobenzene 89 (75 - 120) Dibromofluoromethane 101 (80 - 120) NOTE(S):

___________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results.



### C9K180557 42 of 161METHOD BLANK REPORT GC/MS Volatiles Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LP4721AA Matrix.........: Matrix.........: SOLID MB Lot-Sample #: MB Lot-Sample #: C9K250000-221 Prep Date......: Prep Date......: 11/25/09 Analysis Time..: Analysis Time..: 10:39 Analysis Date..: Analysis Date..: 11/25/09 Prep Batch #...: Prep Batch #...: 9329221 Dilution Factor: Dilution Factor: 1
REPORTING PARAMETER _________________________ RESULT _______________ LIMIT

_________ UNITS

__________ METHOD

_________________ Acetone ND 20 ug/kg SW846 8260B Benzene ND 5.0 ug/kg SW846 8260B Bromodichloromethane ND 5.0 ug/kg SW846 8260B Bromoform ND 5.0 ug/kg SW846 8260B Bromomethane ND 5.0 ug/kg SW846 8260B 2-Butanone ND 5.0 ug/kg SW846 8260B Carbon disulfide ND 5.0 ug/kg SW846 8260B Carbon tetrachloride ND 5.0 ug/kg SW846 8260B Chlorobenzene ND 5.0 ug/kg SW846 8260B Chloroethane ND 5.0 ug/kg SW846 8260B Chloroform ND 5.0 ug/kg SW846 8260B Chloromethane ND 5.0 ug/kg SW846 8260B Cyclohexane ND 5.0 ug/kg SW846 8260B Dibromochloromethane ND 5.0 ug/kg SW846 8260B 1,2-Dibromo-3-chloro- ND 5.0 ug/kg SW846 8260B propane 1,2-Dibromoethane ND 5.0 ug/kg SW846 8260B 1,3-Dichlorobenzene ND 5.0 ug/kg SW846 8260B 1,4-Dichlorobenzene ND 5.0 ug/kg SW846 8260B 1,2-Dichlorobenzene ND 5.0 ug/kg SW846 8260B Dichlorodifluoromethane ND 5.0 ug/kg SW846 8260B 1,1-Dichloroethane ND 5.0 ug/kg SW846 8260B 1,2-Dichloroethane ND 5.0 ug/kg SW846 8260B 1,1-Dichloroethene ND 5.0 ug/kg SW846 8260B cis-1,2-Dichloroethene ND 5.0 ug/kg SW846 8260B trans-1,2-Dichloroethene ND 5.0 ug/kg SW846 8260B 1,2-Dichloropropane ND 5.0 ug/kg SW846 8260B cis-1,3-Dichloropropene ND 5.0 ug/kg SW846 8260B trans-1,3-Dichloropropene ND 5.0 ug/kg SW846 8260B Ethylbenzene ND 5.0 ug/kg SW846 8260B 2-Hexanone ND 5.0 ug/kg SW846 8260B Isopropylbenzene ND 5.0 ug/kg SW846 8260B Methyl acetate ND 5.0 ug/kg SW846 8260B Methylene chloride ND 5.0 ug/kg SW846 8260B Methylcyclohexane ND 5.0 ug/kg SW846 8260B 4-Methyl-2-pentanone ND 5.0 ug/kg SW846 8260B Methyl tert-butyl ether ND 5.0 ug/kg SW846 8260B Styrene ND 5.0 ug/kg SW846 8260B 1,1,2,2-Tetrachloroethane ND 5.0 ug/kg SW846 8260B 1,2,4-Trichloro- ND 5.0 ug/kg SW846 8260B benzene (Continued on next page)



### C9K180557 43 of 161METHOD BLANK REPORT GC/MS Volatiles Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LP4721AA Matrix.........: Matrix.........: SOLID
REPORTING PARAMETER _________________________ RESULT _______________ LIMIT

_________ UNITS

__________ METHOD

_________________ Tetrachloroethene ND 5.0 ug/kg SW846 8260B 1,1,1-Trichloroethane ND 5.0 ug/kg SW846 8260B 1,1,2-Trichloroethane ND 5.0 ug/kg SW846 8260B Trichloroethene ND 5.0 ug/kg SW846 8260B Trichlorofluoromethane ND 5.0 ug/kg SW846 8260B 1,1,2-Trichloro- ND 5.0 ug/kg SW846 8260B 1,2,2-trifluoroethane Toluene ND 5.0 ug/kg SW846 8260B Vinyl chloride ND 5.0 ug/kg SW846 8260B Xylenes (total) ND 15 ug/kg SW846 8260B
PERCENT RECOVERY SURROGATE _________________________ RECOVERY ________ LIMITS

__________ 1,2-Dichloroethane-d4 105 (52 - 124) Toluene-d8 96 (72 - 127) 4-Bromofluorobenzene 90 (63 - 120) Dibromofluoromethane 104 (68 - 121) NOTE(S):

___________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results.



### C9K180557 44 of 161LABORATORY CONTROL SAMPLE EVALUATION REPORT GC/MS Volatiles Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LP2741AC Matrix.........: Matrix.........: WATER LCS Lot-Sample#: LCS Lot-Sample#: C9K240000-345 Prep Date......: Prep Date......: 11/24/09 Analysis Date..: Analysis Date..: 11/24/09 Prep Batch #...: Prep Batch #...: 9328345 Analysis Time..: Analysis Time..: 14:11 Dilution Factor: Dilution Factor: 1
PERCENT RECOVERY PARAMETER ________________________ RECOVERY ________ LIMITS

__________ METHOD

_________________ Benzene Benzene 114 (80 - 120)

(80 - 120) SW846 8260B

SW846 8260B Chlorobenzene Chlorobenzene 99 (83 - 120)

(83 - 120) SW846 8260B

SW846 8260B 1,1-Dichloroethene 1,1-Dichloroethene 113 (69 - 127)

(69 - 127) SW846 8260B

SW846 8260B Trichloroethene Trichloroethene 115 (80 - 120)

(80 - 120) SW846 8260B

SW846 8260B Toluene Toluene 97 (80 - 124)

(80 - 124) SW846 8260B

SW846 8260B
PERCENT RECOVERY SURROGATE _________________________ RECOVERY ________ LIMITS

__________ 1,2-Dichloroethane-d4 97 (62 - 123) Toluene-d8 94 (80 - 120) 4-Bromofluorobenzene 91 (75 - 120) Dibromofluoromethane 106 (80 - 120) NOTE(S):

_____________________________________________________________________________________ _____________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results. Bold print denotes control parameters



### C9K180557 45 of 161LABORATORY CONTROL SAMPLE EVALUATION REPORT GC/MS Volatiles Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LP42D1AC Matrix.........: Matrix.........: WATER LCS Lot-Sample#: LCS Lot-Sample#: C9K250000-174 Prep Date......: Prep Date......: 11/25/09 Analysis Date..: Analysis Date..: 11/25/09 Prep Batch #...: Prep Batch #...: 9329174 Analysis Time..: Analysis Time..: 10:15 Dilution Factor: Dilution Factor: 1
PERCENT RECOVERY PARAMETER ________________________ RECOVERY ________ LIMITS

__________ METHOD

_________________ Benzene Benzene 106 (80 - 120)

(80 - 120) SW846 8260B

SW846 8260B Chlorobenzene Chlorobenzene 106 (83 - 120)

(83 - 120) SW846 8260B

SW846 8260B 1,1-Dichloroethene 1,1-Dichloroethene 104 (69 - 127)

(69 - 127) SW846 8260B

SW846 8260B Trichloroethene Trichloroethene 106 (80 - 120)

(80 - 120) SW846 8260B

SW846 8260B Toluene Toluene 102 (80 - 124)

(80 - 124) SW846 8260B

SW846 8260B
PERCENT RECOVERY SURROGATE _________________________ RECOVERY ________ LIMITS

__________ 1,2-Dichloroethane-d4 91 (62 - 123) Toluene-d8 100 (80 - 120) 4-Bromofluorobenzene 91 (75 - 120) Dibromofluoromethane 99 (80 - 120) NOTE(S):

_____________________________________________________________________________________ _____________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results. Bold print denotes control parameters



### C9K180557 46 of 161LABORATORY CONTROL SAMPLE EVALUATION REPORT GC/MS Volatiles Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LP4721AC Matrix.........: Matrix.........: SOLID LCS Lot-Sample#: LCS Lot-Sample#: C9K250000-221 Prep Date......: Prep Date......: 11/25/09 Analysis Date..: Analysis Date..: 11/25/09 Prep Batch #...: Prep Batch #...: 9329221 Analysis Time..: Analysis Time..: 11:02 Dilution Factor: Dilution Factor: 1
PERCENT RECOVERY PARAMETER ________________________ RECOVERY ________ LIMITS

__________ METHOD

_________________ Benzene Benzene 98 (77 - 120)

(77 - 120) SW846 8260B

SW846 8260B Chlorobenzene Chlorobenzene 103 (79 - 120)

(79 - 120) SW846 8260B

SW846 8260B 1,1-Dichloroethene 1,1-Dichloroethene 75 (59 - 129)

(59 - 129) SW846 8260B

SW846 8260B Trichloroethene Trichloroethene 99 (76 - 119)

(76 - 119) SW846 8260B

SW846 8260B Toluene Toluene 104 (78 - 124)

(78 - 124) SW846 8260B

SW846 8260B
PERCENT RECOVERY SURROGATE _________________________ RECOVERY ________ LIMITS

__________ 1,2-Dichloroethane-d4 98 (52 - 124) Toluene-d8 99 (72 - 127) 4-Bromofluorobenzene 94 (63 - 120) Dibromofluoromethane 99 (68 - 121) NOTE(S):

_____________________________________________________________________________________ _____________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results. Bold print denotes control parameters



### C9K180557 47 of 161MATRIX SPIKE SAMPLE EVALUATION REPORT GC/MS Volatiles Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPPF51A9-MS Matrix.........: Matrix.........: WATER MS Lot-Sample #: MS Lot-Sample #: C9K180557-001 LPPF51CA-MSD Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9328229 Prep Date......: Prep Date......: 11/24/09 Analysis Date..: Analysis Date..: 11/24/09 Prep Batch #...: Prep Batch #...: 9328345 Analysis Time..: Analysis Time..: 14:43 Dilution Factor: Dilution Factor: 1
PERCENT RECOVERY RPD PARAMETER _________________________ RECOVERY _________ LIMITS

__________ RPD

____ LIMITS _________ METHOD

_________________ Benzene Benzene 112 (80 - 120)

(80 - 120) SW846 8260B SW846 8260B 115 (80 - 120)

(80 - 120) 2.4

(0-20) SW846 8260B

SW846 8260B Chlorobenzene Chlorobenzene 97 (83 - 120)

(83 - 120) SW846 8260B SW846 8260B 100 (83 - 120)

(83 - 120) 3.2

(0-20) SW846 8260B

SW846 8260B 1,1-Dichloroethene 1,1-Dichloroethene 110 (69 - 127)

(69 - 127) SW846 8260B SW846 8260B 114 (69 - 127)

(69 - 127) 3.4

(0-20) SW846 8260B

SW846 8260B Trichloroethene Trichloroethene 112 (80 - 120)

(80 - 120) SW846 8260B SW846 8260B 116 (80 - 120)

(80 - 120) 3.5

(0-20) SW846 8260B

SW846 8260B Toluene Toluene 96 (80 - 124)

(80 - 124) SW846 8260B SW846 8260B 99 (80 - 124)

(80 - 124) 3.1

(0-20) SW846 8260B

SW846 8260B
PERCENT RECOVERY SURROGATE _________________________ RECOVERY ________ LIMITS

__________ 1,2-Dichloroethane-d4 95 (62 - 123) 95 (62 - 123) Toluene-d8 96 (80 - 120) 95 (80 - 120) 4-Bromofluorobenzene 90 (75 - 120) 90 (75 - 120) Dibromofluoromethane 104 (80 - 120) 104 (80 - 120) NOTE(S):

___________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results. Bold print denotes control parameters



### C9K180557 48 of 161MATRIX SPIKE SAMPLE EVALUATION REPORT GC/MS Volatiles Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPPGN1A7-MS Matrix.........: Matrix.........: WATER MS Lot-Sample #: MS Lot-Sample #: C9K180557-002 LPPGN1A8-MSD Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9329152 Prep Date......: Prep Date......: 11/25/09 Analysis Date..: Analysis Date..: 11/25/09 Prep Batch #...: Prep Batch #...: 9329174 Analysis Time..: Analysis Time..: 10:47 Dilution Factor: Dilution Factor: 1
PERCENT RECOVERY RPD PARAMETER _________________________ RECOVERY _________ LIMITS

__________ RPD

____ LIMITS _________ METHOD

_________________ Benzene Benzene 109 (80 - 120)

(80 - 120) SW846 8260B SW846 8260B 108 (80 - 120)

(80 - 120) 0.83

(0-20) SW846 8260B

SW846 8260B Chlorobenzene Chlorobenzene 109 (83 - 120)

(83 - 120) SW846 8260B SW846 8260B 107 (83 - 120)

(83 - 120) 1.7

(0-20) SW846 8260B

SW846 8260B 1,1-Dichloroethene 1,1-Dichloroethene 108 (69 - 127)

(69 - 127) SW846 8260B SW846 8260B 109 (69 - 127)

(69 - 127) 1.1

(0-20) SW846 8260B

SW846 8260B Trichloroethene Trichloroethene 110 (80 - 120)

(80 - 120) SW846 8260B SW846 8260B 109 (80 - 120)

(80 - 120) 0.75

(0-20) SW846 8260B

SW846 8260B Toluene Toluene 108 (80 - 124)

(80 - 124) SW846 8260B SW846 8260B 107 (80 - 124)

(80 - 124) 0.37

(0-20) SW846 8260B

SW846 8260B
PERCENT RECOVERY SURROGATE _________________________ RECOVERY ________ LIMITS

__________ 1,2-Dichloroethane-d4 90 (62 - 123) 90 (62 - 123) Toluene-d8 102 (80 - 120) 101 (80 - 120) 4-Bromofluorobenzene 91 (75 - 120) 91 (75 - 120) Dibromofluoromethane 98 (80 - 120) 98 (80 - 120) NOTE(S):

___________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results. Bold print denotes control parameters



### C9K180557 49 of 161MATRIX SPIKE SAMPLE EVALUATION REPORT GC/MS Volatiles Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPP3L1AE-MS Matrix.........: Matrix.........: SOLID MS Lot-Sample #: MS Lot-Sample #: C9K180619-007 LPP3L1AF-MSD Date Sampled...: Date Sampled...: 11/16/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9329143 Prep Date......: Prep Date......: 11/25/09 Analysis Date..: Analysis Date..: 11/25/09 Prep Batch #...: Prep Batch #...: 9329221 Analysis Time..: Analysis Time..: 11:25 Dilution Factor: Dilution Factor: 1 % Moisture.....: % Moisture.....: 31
PERCENT RECOVERY RPD PARAMETER _________________________ RECOVERY _________ LIMITS

__________ RPD

____ LIMITS _________ METHOD

_________________ Benzene Benzene 97 (77 - 120)

(77 - 120) SW846 8260B SW846 8260B 96 (77 - 120)

(77 - 120) 1.0

(0-20) SW846 8260B

SW846 8260B Chlorobenzene Chlorobenzene 101 (79 - 120)

(79 - 120) SW846 8260B SW846 8260B 94 (79 - 120)

(79 - 120) 7.0

(0-20) SW846 8260B

SW846 8260B 1,1-Dichloroethene 1,1-Dichloroethene 75 (59 - 129)

(59 - 129) SW846 8260B SW846 8260B 84 (59 - 129)

(59 - 129) 11

(0-25) SW846 8260B

SW846 8260B Trichloroethene Trichloroethene 99 (76 - 119)

(76 - 119) SW846 8260B SW846 8260B 96 (76 - 119)

(76 - 119) 2.7

(0-21) SW846 8260B

SW846 8260B Toluene Toluene 98 (78 - 124)

(78 - 124) SW846 8260B SW846 8260B 90 (78 - 124)

(78 - 124) 8.6

(0-21) SW846 8260B

SW846 8260B
PERCENT RECOVERY SURROGATE _________________________ RECOVERY ________ LIMITS

__________ 1,2-Dichloroethane-d4 100 (52 - 124) 97 (52 - 124) Toluene-d8 99 (72 - 127) 91 (72 - 127) 4-Bromofluorobenzene 97 (63 - 120) 94 (63 - 120) Dibromofluoromethane 105 (68 - 121) 105 (68 - 121) NOTE(S):

___________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results. Bold print denotes control parameters Results and reporting limits have been adjusted for dry weight.



### C9K180557 50 of 161Clean Sites Environmental Services Inc Client Sample ID: MW-1S GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-001 Work Order #...: Work Order #...: LPPF51AE Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: Prep Date......: Prep Date......: 11/20/09 Analysis Date..: Analysis Date..: 11/24/09 Prep Batch #...: Prep Batch #...: 9324281 Analysis Time..: Analysis Time..: 00:34 Dilution Factor: Dilution Factor: 0.94 Method.........: Method.........: SW846 8270C
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acenaphthene ND 1.9 ug/L Acenaphthylene ND 1.9 ug/L Acetophenone ND 9.4 ug/L Anthracene ND 1.9 ug/L Atrazine ND 9.4 ug/L Benzo(a)anthracene ND 1.9 ug/L Benzo(a)pyrene ND 1.9 ug/L Benzo(b)fluoranthene ND 1.9 ug/L Benzo(ghi)perylene ND 1.9 ug/L Benzo(k)fluoranthene ND 1.9 ug/L Benzaldehyde ND 9.4 ug/L 1,1'-Biphenyl ND 9.4 ug/L bis(2-Chloroethoxy) ND 9.4 ug/L methane bis(2-Chloroethyl)- ND 1.9 ug/L ether bis(2-Ethylhexyl) ND 9.4 ug/L phthalate 4-Bromophenyl phenyl ND 9.4 ug/L ether Butyl benzyl phthalate ND 9.4 ug/L Caprolactam ND 47 ug/L Carbazole ND 1.9 ug/L 4-Chloroaniline ND 9.4 ug/L 4-Chloro-3-methylphenol ND 9.4 ug/L 2-Chloronaphthalene ND 1.9 ug/L 2-Chlorophenol ND 9.4 ug/L 4-Chlorophenyl phenyl ND 9.4 ug/L ether Chrysene ND 1.9 ug/L Dibenz(a,h)anthracene ND 1.9 ug/L Dibenzofuran ND 9.4 ug/L 3,3'-Dichlorobenzidine ND 9.4 ug/L 2,4-Dichlorophenol ND 1.9 ug/L Diethyl phthalate ND 9.4 ug/L 2,4-Dimethylphenol ND 9.4 ug/L Dimethyl phthalate ND 9.4 ug/L Di-n-butyl phthalate ND 9.4 ug/L (Continued on next page)



### C9K180557 51 of 161Clean Sites Environmental Services Inc Client Sample ID: MW-1S GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-001 Work Order #...: Work Order #...: LPPF51AE Matrix.........: Matrix.........: WATER
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 4,6-Dinitro- ND 47 ug/L 2-methylphenol 2,4-Dinitrophenol ND 47 ug/L 2,4-Dinitrotoluene ND 9.4 ug/L 2,6-Dinitrotoluene ND 9.4 ug/L Di-n-octyl phthalate ND 9.4 ug/L Fluoranthene ND 1.9 ug/L Fluorene ND 1.9 ug/L Hexachlorobenzene ND 1.9 ug/L Hexachlorobutadiene ND 1.9 ug/L Hexachlorocyclopenta- ND 9.4 ug/L diene Hexachloroethane ND 9.4 ug/L Indeno(1,2,3-cd)pyrene ND 1.9 ug/L Isophorone ND 9.4 ug/L 2-Methylnaphthalene ND 1.9 ug/L 2-Methylphenol ND 9.4 ug/L 4-Methylphenol ND 9.4 ug/L Naphthalene ND 1.9 ug/L 2-Nitroaniline ND 47 ug/L 3-Nitroaniline ND 47 ug/L 4-Nitroaniline ND 47 ug/L Nitrobenzene ND 1.9 ug/L 2-Nitrophenol ND 9.4 ug/L 4-Nitrophenol ND 47 ug/L N-Nitrosodi-n-propyl- ND 1.9 ug/L amine N-Nitrosodiphenylamine ND 1.9 ug/L 2,2'-oxybis ND 1.9 ug/L (1-Chloropropane) Pentachlorophenol ND 9.4 ug/L Phenanthrene ND 1.9 ug/L Phenol ND 1.9 ug/L Pyrene ND 1.9 ug/L 2,4,5-Trichloro- ND 9.4 ug/L phenol 2,4,6-Trichloro- ND 9.4 ug/L phenol (Continued on next page)



### C9K180557 52 of 161Clean Sites Environmental Services Inc Client Sample ID: MW-1S GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-001 Work Order #...: Work Order #...: LPPF51AE Matrix.........: Matrix.........: WATER

PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 2,4,6-Tribromophenol 54 (33 - 122) 2-Fluorobiphenyl 50 (35 - 108) 2-Fluorophenol 58 (26 - 100) Nitrobenzene-d5 58 (37 - 104) Phenol-d5 58 (30 - 102) Terphenyl-d14 39 (25 - 130)



### C9K180557 53 of 161Clean Sites Environmental Services Inc Client Sample ID: MW-3S GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-002 Work Order #...: Work Order #...: LPPGN1AM Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: Prep Date......: Prep Date......: 11/20/09 Analysis Date..: Analysis Date..: 11/24/09 Prep Batch #...: Prep Batch #...: 9324281 Analysis Time..: Analysis Time..: 00:56 Dilution Factor: Dilution Factor: 0.94 Method.........: Method.........: SW846 8270C
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acenaphthene ND 1.9 ug/L Acenaphthylene ND 1.9 ug/L Acetophenone ND 9.4 ug/L Anthracene ND 1.9 ug/L Atrazine ND 9.4 ug/L Benzo(a)anthracene ND 1.9 ug/L Benzo(a)pyrene ND 1.9 ug/L Benzo(b)fluoranthene ND 1.9 ug/L Benzo(ghi)perylene ND 1.9 ug/L Benzo(k)fluoranthene ND 1.9 ug/L Benzaldehyde ND 9.4 ug/L 1,1'-Biphenyl ND 9.4 ug/L bis(2-Chloroethoxy) ND 9.4 ug/L methane bis(2-Chloroethyl)- ND 1.9 ug/L ether bis(2-Ethylhexyl) ND 9.4 ug/L phthalate 4-Bromophenyl phenyl ND 9.4 ug/L ether Butyl benzyl phthalate ND 9.4 ug/L Caprolactam ND 47 ug/L Carbazole ND 1.9 ug/L 4-Chloroaniline ND 9.4 ug/L 4-Chloro-3-methylphenol ND 9.4 ug/L 2-Chloronaphthalene ND 1.9 ug/L 2-Chlorophenol ND 9.4 ug/L 4-Chlorophenyl phenyl ND 9.4 ug/L ether Chrysene ND 1.9 ug/L Dibenz(a,h)anthracene ND 1.9 ug/L Dibenzofuran ND 9.4 ug/L 3,3'-Dichlorobenzidine ND 9.4 ug/L 2,4-Dichlorophenol ND 1.9 ug/L Diethyl phthalate ND 9.4 ug/L 2,4-Dimethylphenol ND 9.4 ug/L Dimethyl phthalate ND 9.4 ug/L Di-n-butyl phthalate ND 9.4 ug/L (Continued on next page)



### C9K180557 54 of 161Clean Sites Environmental Services Inc Client Sample ID: MW-3S GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-002 Work Order #...: Work Order #...: LPPGN1AM Matrix.........: Matrix.........: WATER
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 4,6-Dinitro- ND 47 ug/L 2-methylphenol 2,4-Dinitrophenol ND 47 ug/L 2,4-Dinitrotoluene ND 9.4 ug/L 2,6-Dinitrotoluene ND 9.4 ug/L Di-n-octyl phthalate ND 9.4 ug/L Fluoranthene ND 1.9 ug/L Fluorene ND 1.9 ug/L Hexachlorobenzene ND 1.9 ug/L Hexachlorobutadiene ND 1.9 ug/L Hexachlorocyclopenta- ND 9.4 ug/L diene Hexachloroethane ND 9.4 ug/L Indeno(1,2,3-cd)pyrene ND 1.9 ug/L Isophorone ND 9.4 ug/L 2-Methylnaphthalene ND 1.9 ug/L 2-Methylphenol ND 9.4 ug/L 4-Methylphenol ND 9.4 ug/L Naphthalene ND 1.9 ug/L 2-Nitroaniline ND 47 ug/L 3-Nitroaniline ND 47 ug/L 4-Nitroaniline ND 47 ug/L Nitrobenzene ND 1.9 ug/L 2-Nitrophenol ND 9.4 ug/L 4-Nitrophenol ND 47 ug/L N-Nitrosodi-n-propyl- ND 1.9 ug/L amine N-Nitrosodiphenylamine ND 1.9 ug/L 2,2'-oxybis ND 1.9 ug/L (1-Chloropropane) Pentachlorophenol ND 9.4 ug/L Phenanthrene ND 1.9 ug/L Phenol ND 1.9 ug/L Pyrene ND 1.9 ug/L 2,4,5-Trichloro- ND 9.4 ug/L phenol 2,4,6-Trichloro- ND 9.4 ug/L phenol (Continued on next page)



### C9K180557 55 of 161Clean Sites Environmental Services Inc Client Sample ID: MW-3S GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-002 Work Order #...: Work Order #...: LPPGN1AM Matrix.........: Matrix.........: WATER

PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 2,4,6-Tribromophenol 61 (33 - 122) 2-Fluorobiphenyl 57 (35 - 108) 2-Fluorophenol 63 (26 - 100) Nitrobenzene-d5 70 (37 - 104) Phenol-d5 63 (30 - 102) Terphenyl-d14 51 (25 - 130)



### C9K180557 56 of 161Clean Sites Environmental Services Inc Client Sample ID: L2-S1 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-003 Work Order #...: Work Order #...: LPPGP1AM Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: Prep Date......: Prep Date......: 11/20/09 Analysis Date..: Analysis Date..: 11/25/09 Prep Batch #...: Prep Batch #...: 9324281 Analysis Time..: Analysis Time..: 13:31 Dilution Factor: Dilution Factor: 0.94 Method.........: Method.........: SW846 8270C
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acenaphthene ND 1.9 ug/L Acenaphthylene ND 1.9 ug/L Acetophenone ND 9.4 ug/L Anthracene ND 1.9 ug/L Atrazine ND 9.4 ug/L Benzo(a)anthracene ND 1.9 ug/L Benzo(a)pyrene ND 1.9 ug/L Benzo(b)fluoranthene ND 1.9 ug/L Benzo(ghi)perylene ND 1.9 ug/L Benzo(k)fluoranthene ND 1.9 ug/L Benzaldehyde ND 9.4 ug/L 1,1'-Biphenyl ND 9.4 ug/L bis(2-Chloroethoxy) ND 9.4 ug/L methane bis(2-Chloroethyl)- ND 1.9 ug/L ether bis(2-Ethylhexyl) ND 9.4 ug/L phthalate 4-Bromophenyl phenyl ND 9.4 ug/L ether Butyl benzyl phthalate ND 9.4 ug/L Caprolactam ND 47 ug/L Carbazole ND 1.9 ug/L 4-Chloroaniline ND 9.4 ug/L 4-Chloro-3-methylphenol ND 9.4 ug/L 2-Chloronaphthalene ND 1.9 ug/L 2-Chlorophenol ND 9.4 ug/L 4-Chlorophenyl phenyl ND 9.4 ug/L ether Chrysene ND 1.9 ug/L Dibenz(a,h)anthracene ND 1.9 ug/L Dibenzofuran ND 9.4 ug/L 3,3'-Dichlorobenzidine ND 9.4 ug/L 2,4-Dichlorophenol ND 1.9 ug/L Diethyl phthalate ND 9.4 ug/L 2,4-Dimethylphenol ND 9.4 ug/L Dimethyl phthalate ND 9.4 ug/L Di-n-butyl phthalate ND 9.4 ug/L (Continued on next page)



### C9K180557 57 of 161Clean Sites Environmental Services Inc Client Sample ID: L2-S1 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-003 Work Order #...: Work Order #...: LPPGP1AM Matrix.........: Matrix.........: WATER
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 4,6-Dinitro- ND 47 ug/L 2-methylphenol 2,4-Dinitrophenol ND 47 ug/L 2,4-Dinitrotoluene ND 9.4 ug/L 2,6-Dinitrotoluene ND 9.4 ug/L Di-n-octyl phthalate ND 9.4 ug/L Fluoranthene ND 1.9 ug/L Fluorene ND 1.9 ug/L Hexachlorobenzene ND 1.9 ug/L Hexachlorobutadiene ND 1.9 ug/L Hexachlorocyclopenta- ND 9.4 ug/L diene Hexachloroethane ND 9.4 ug/L Indeno(1,2,3-cd)pyrene ND 1.9 ug/L Isophorone ND 9.4 ug/L 2-Methylnaphthalene ND 1.9 ug/L 2-Methylphenol ND 9.4 ug/L 4-Methylphenol ND 9.4 ug/L Naphthalene ND 1.9 ug/L 2-Nitroaniline ND 47 ug/L 3-Nitroaniline ND 47 ug/L 4-Nitroaniline ND 47 ug/L Nitrobenzene ND 1.9 ug/L 2-Nitrophenol ND 9.4 ug/L 4-Nitrophenol ND 47 ug/L N-Nitrosodi-n-propyl- ND 1.9 ug/L amine N-Nitrosodiphenylamine ND 1.9 ug/L 2,2'-oxybis ND 1.9 ug/L (1-Chloropropane) Pentachlorophenol ND 9.4 ug/L Phenanthrene ND 1.9 ug/L Phenol ND 1.9 ug/L Pyrene ND 1.9 ug/L 2,4,5-Trichloro- ND 9.4 ug/L phenol 2,4,6-Trichloro- ND 9.4 ug/L phenol (Continued on next page)



### C9K180557 58 of 161Clean Sites Environmental Services Inc Client Sample ID: L2-S1 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-003 Work Order #...: Work Order #...: LPPGP1AM Matrix.........: Matrix.........: WATER

PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 2,4,6-Tribromophenol 70 (33 - 122) 2-Fluorobiphenyl 50 (35 - 108) 2-Fluorophenol 44 (26 - 100) Nitrobenzene-d5 48 (37 - 104) Phenol-d5 48 (30 - 102) Terphenyl-d14 69 (25 - 130)



### C9K180557 59 of 161Clean Sites Environmental Services Inc Client Sample ID: L1-S1 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-006 Work Order #...: Work Order #...: LPPG11AD Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: Prep Date......: Prep Date......: 11/20/09 Analysis Date..: Analysis Date..: 11/25/09 Prep Batch #...: Prep Batch #...: 9324281 Analysis Time..: Analysis Time..: 13:53 Dilution Factor: Dilution Factor: 0.94 Method.........: Method.........: SW846 8270C
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acenaphthene ND 1.9 ug/L Acenaphthylene ND 1.9 ug/L Acetophenone ND 9.4 ug/L Anthracene ND 1.9 ug/L Atrazine ND 9.4 ug/L Benzo(a)anthracene ND 1.9 ug/L Benzo(a)pyrene ND 1.9 ug/L Benzo(b)fluoranthene ND 1.9 ug/L Benzo(ghi)perylene ND 1.9 ug/L Benzo(k)fluoranthene ND 1.9 ug/L Benzaldehyde ND 9.4 ug/L 1,1'-Biphenyl ND 9.4 ug/L bis(2-Chloroethoxy) ND 9.4 ug/L methane bis(2-Chloroethyl)- ND 1.9 ug/L ether bis(2-Ethylhexyl) ND 9.4 ug/L phthalate 4-Bromophenyl phenyl ND 9.4 ug/L ether Butyl benzyl phthalate ND 9.4 ug/L Caprolactam ND 47 ug/L Carbazole ND 1.9 ug/L 4-Chloroaniline ND 9.4 ug/L 4-Chloro-3-methylphenol ND 9.4 ug/L 2-Chloronaphthalene ND 1.9 ug/L 2-Chlorophenol ND 9.4 ug/L 4-Chlorophenyl phenyl ND 9.4 ug/L ether Chrysene ND 1.9 ug/L Dibenz(a,h)anthracene ND 1.9 ug/L Dibenzofuran ND 9.4 ug/L 3,3'-Dichlorobenzidine ND 9.4 ug/L 2,4-Dichlorophenol ND 1.9 ug/L Diethyl phthalate ND 9.4 ug/L 2,4-Dimethylphenol ND 9.4 ug/L Dimethyl phthalate ND 9.4 ug/L Di-n-butyl phthalate ND 9.4 ug/L (Continued on next page)



### C9K180557 60 of 161Clean Sites Environmental Services Inc Client Sample ID: L1-S1 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-006 Work Order #...: Work Order #...: LPPG11AD Matrix.........: Matrix.........: WATER
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 4,6-Dinitro- ND 47 ug/L 2-methylphenol 2,4-Dinitrophenol ND 47 ug/L 2,4-Dinitrotoluene ND 9.4 ug/L 2,6-Dinitrotoluene ND 9.4 ug/L Di-n-octyl phthalate ND 9.4 ug/L Fluoranthene ND 1.9 ug/L Fluorene ND 1.9 ug/L Hexachlorobenzene ND 1.9 ug/L Hexachlorobutadiene ND 1.9 ug/L Hexachlorocyclopenta- ND 9.4 ug/L diene Hexachloroethane ND 9.4 ug/L Indeno(1,2,3-cd)pyrene ND 1.9 ug/L Isophorone ND 9.4 ug/L 2-Methylnaphthalene ND 1.9 ug/L 2-Methylphenol ND 9.4 ug/L 4-Methylphenol ND 9.4 ug/L Naphthalene ND 1.9 ug/L 2-Nitroaniline ND 47 ug/L 3-Nitroaniline ND 47 ug/L 4-Nitroaniline ND 47 ug/L Nitrobenzene ND 1.9 ug/L 2-Nitrophenol ND 9.4 ug/L 4-Nitrophenol ND 47 ug/L N-Nitrosodi-n-propyl- ND 1.9 ug/L amine N-Nitrosodiphenylamine ND 1.9 ug/L 2,2'-oxybis ND 1.9 ug/L (1-Chloropropane) Pentachlorophenol ND 9.4 ug/L Phenanthrene ND 1.9 ug/L Phenol ND 1.9 ug/L Pyrene ND 1.9 ug/L 2,4,5-Trichloro- ND 9.4 ug/L phenol 2,4,6-Trichloro- ND 9.4 ug/L phenol (Continued on next page)



### C9K180557 61 of 161Clean Sites Environmental Services Inc Client Sample ID: L1-S1 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-006 Work Order #...: Work Order #...: LPPG11AD Matrix.........: Matrix.........: WATER

PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 2,4,6-Tribromophenol 66 (33 - 122) 2-Fluorobiphenyl 55 (35 - 108) 2-Fluorophenol 58 (26 - 100) Nitrobenzene-d5 58 (37 - 104) Phenol-d5 59 (30 - 102) Terphenyl-d14 55 (25 - 130)



### C9K180557 62 of 161Clean Sites Environmental Services Inc Client Sample ID: L1-S3 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-007 Work Order #...: Work Order #...: LPPG61AK Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: Prep Date......: Prep Date......: 11/20/09 Analysis Date..: Analysis Date..: 11/25/09 Prep Batch #...: Prep Batch #...: 9324281 Analysis Time..: Analysis Time..: 14:16 Dilution Factor: Dilution Factor: 0.94 Method.........: Method.........: SW846 8270C
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acenaphthene ND 1.9 ug/L Acenaphthylene ND 1.9 ug/L Acetophenone ND 9.4 ug/L Anthracene ND 1.9 ug/L Atrazine ND 9.4 ug/L Benzo(a)anthracene ND 1.9 ug/L Benzo(a)pyrene ND 1.9 ug/L Benzo(b)fluoranthene ND 1.9 ug/L Benzo(ghi)perylene ND 1.9 ug/L Benzo(k)fluoranthene ND 1.9 ug/L Benzaldehyde ND 9.4 ug/L 1,1'-Biphenyl ND 9.4 ug/L bis(2-Chloroethoxy) ND 9.4 ug/L methane bis(2-Chloroethyl)- ND 1.9 ug/L ether bis(2-Ethylhexyl) ND 9.4 ug/L phthalate 4-Bromophenyl phenyl ND 9.4 ug/L ether Butyl benzyl phthalate ND 9.4 ug/L Caprolactam ND 47 ug/L Carbazole ND 1.9 ug/L 4-Chloroaniline ND 9.4 ug/L 4-Chloro-3-methylphenol ND 9.4 ug/L 2-Chloronaphthalene ND 1.9 ug/L 2-Chlorophenol ND 9.4 ug/L 4-Chlorophenyl phenyl ND 9.4 ug/L ether Chrysene ND 1.9 ug/L Dibenz(a,h)anthracene ND 1.9 ug/L Dibenzofuran ND 9.4 ug/L 3,3'-Dichlorobenzidine ND 9.4 ug/L 2,4-Dichlorophenol ND 1.9 ug/L Diethyl phthalate ND 9.4 ug/L 2,4-Dimethylphenol ND 9.4 ug/L Dimethyl phthalate ND 9.4 ug/L Di-n-butyl phthalate ND 9.4 ug/L (Continued on next page)



### C9K180557 63 of 161Clean Sites Environmental Services Inc Client Sample ID: L1-S3 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-007 Work Order #...: Work Order #...: LPPG61AK Matrix.........: Matrix.........: WATER
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 4,6-Dinitro- ND 47 ug/L 2-methylphenol 2,4-Dinitrophenol ND 47 ug/L 2,4-Dinitrotoluene ND 9.4 ug/L 2,6-Dinitrotoluene ND 9.4 ug/L Di-n-octyl phthalate ND 9.4 ug/L Fluoranthene ND 1.9 ug/L Fluorene ND 1.9 ug/L Hexachlorobenzene ND 1.9 ug/L Hexachlorobutadiene ND 1.9 ug/L Hexachlorocyclopenta- ND 9.4 ug/L diene Hexachloroethane ND 9.4 ug/L Indeno(1,2,3-cd)pyrene ND 1.9 ug/L Isophorone ND 9.4 ug/L 2-Methylnaphthalene ND 1.9 ug/L 2-Methylphenol ND 9.4 ug/L 4-Methylphenol ND 9.4 ug/L Naphthalene ND 1.9 ug/L 2-Nitroaniline ND 47 ug/L 3-Nitroaniline ND 47 ug/L 4-Nitroaniline ND 47 ug/L Nitrobenzene ND 1.9 ug/L 2-Nitrophenol ND 9.4 ug/L 4-Nitrophenol ND 47 ug/L N-Nitrosodi-n-propyl- ND 1.9 ug/L amine N-Nitrosodiphenylamine ND 1.9 ug/L 2,2'-oxybis ND 1.9 ug/L (1-Chloropropane) Pentachlorophenol ND 9.4 ug/L Phenanthrene ND 1.9 ug/L Phenol ND 1.9 ug/L Pyrene ND 1.9 ug/L 2,4,5-Trichloro- ND 9.4 ug/L phenol 2,4,6-Trichloro- ND 9.4 ug/L phenol (Continued on next page)



### C9K180557 64 of 161Clean Sites Environmental Services Inc Client Sample ID: L1-S3 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-007 Work Order #...: Work Order #...: LPPG61AK Matrix.........: Matrix.........: WATER

PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 2,4,6-Tribromophenol 58 (33 - 122) 2-Fluorobiphenyl 51 (35 - 108) 2-Fluorophenol 51 (26 - 100) Nitrobenzene-d5 50 (37 - 104) Phenol-d5 52 (30 - 102) Terphenyl-d14 38 (25 - 130)



### C9K180557 65 of 161Clean Sites Environmental Services Inc Client Sample ID: L1-S4 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-008 Work Order #...: Work Order #...: LPPG81AR Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: Prep Date......: Prep Date......: 11/20/09 Analysis Date..: Analysis Date..: 11/25/09 Prep Batch #...: Prep Batch #...: 9324281 Analysis Time..: Analysis Time..: 14:38 Dilution Factor: Dilution Factor: 0.94 Method.........: Method.........: SW846 8270C
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acenaphthene ND 1.9 ug/L Acenaphthylene ND 1.9 ug/L Acetophenone ND 9.4 ug/L Anthracene ND 1.9 ug/L Atrazine ND 9.4 ug/L Benzo(a)anthracene ND 1.9 ug/L Benzo(a)pyrene ND 1.9 ug/L Benzo(b)fluoranthene ND 1.9 ug/L Benzo(ghi)perylene ND 1.9 ug/L Benzo(k)fluoranthene ND 1.9 ug/L Benzaldehyde ND 9.4 ug/L 1,1'-Biphenyl ND 9.4 ug/L bis(2-Chloroethoxy) ND 9.4 ug/L methane bis(2-Chloroethyl)- ND 1.9 ug/L ether bis(2-Ethylhexyl) ND 9.4 ug/L phthalate 4-Bromophenyl phenyl ND 9.4 ug/L ether Butyl benzyl phthalate ND 9.4 ug/L Caprolactam ND 47 ug/L Carbazole ND 1.9 ug/L 4-Chloroaniline ND 9.4 ug/L 4-Chloro-3-methylphenol ND 9.4 ug/L 2-Chloronaphthalene ND 1.9 ug/L 2-Chlorophenol ND 9.4 ug/L 4-Chlorophenyl phenyl ND 9.4 ug/L ether Chrysene ND 1.9 ug/L Dibenz(a,h)anthracene ND 1.9 ug/L Dibenzofuran ND 9.4 ug/L 3,3'-Dichlorobenzidine ND 9.4 ug/L 2,4-Dichlorophenol ND 1.9 ug/L Diethyl phthalate ND 9.4 ug/L 2,4-Dimethylphenol ND 9.4 ug/L Dimethyl phthalate ND 9.4 ug/L Di-n-butyl phthalate ND 9.4 ug/L (Continued on next page)



### C9K180557 66 of 161Clean Sites Environmental Services Inc Client Sample ID: L1-S4 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-008 Work Order #...: Work Order #...: LPPG81AR Matrix.........: Matrix.........: WATER
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 4,6-Dinitro- ND 47 ug/L 2-methylphenol 2,4-Dinitrophenol ND 47 ug/L 2,4-Dinitrotoluene ND 9.4 ug/L 2,6-Dinitrotoluene ND 9.4 ug/L Di-n-octyl phthalate ND 9.4 ug/L Fluoranthene ND 1.9 ug/L Fluorene ND 1.9 ug/L Hexachlorobenzene ND 1.9 ug/L Hexachlorobutadiene ND 1.9 ug/L Hexachlorocyclopenta- ND 9.4 ug/L diene Hexachloroethane ND 9.4 ug/L Indeno(1,2,3-cd)pyrene ND 1.9 ug/L Isophorone ND 9.4 ug/L 2-Methylnaphthalene ND 1.9 ug/L 2-Methylphenol ND 9.4 ug/L 4-Methylphenol ND 9.4 ug/L Naphthalene ND 1.9 ug/L 2-Nitroaniline ND 47 ug/L 3-Nitroaniline ND 47 ug/L 4-Nitroaniline ND 47 ug/L Nitrobenzene ND 1.9 ug/L 2-Nitrophenol ND 9.4 ug/L 4-Nitrophenol ND 47 ug/L N-Nitrosodi-n-propyl- ND 1.9 ug/L amine N-Nitrosodiphenylamine ND 1.9 ug/L 2,2'-oxybis ND 1.9 ug/L (1-Chloropropane) Pentachlorophenol ND 9.4 ug/L Phenanthrene ND 1.9 ug/L Phenol ND 1.9 ug/L Pyrene ND 1.9 ug/L 2,4,5-Trichloro- ND 9.4 ug/L phenol 2,4,6-Trichloro- ND 9.4 ug/L phenol (Continued on next page)



### C9K180557 67 of 161Clean Sites Environmental Services Inc Client Sample ID: L1-S4 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-008 Work Order #...: Work Order #...: LPPG81AR Matrix.........: Matrix.........: WATER

PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 2,4,6-Tribromophenol 64 (33 - 122) 2-Fluorobiphenyl 52 (35 - 108) 2-Fluorophenol 54 (26 - 100) Nitrobenzene-d5 57 (37 - 104) Phenol-d5 57 (30 - 102) Terphenyl-d14 49 (25 - 130)



### C9K180557 68 of 161Clean Sites Environmental Services Inc Client Sample ID: SW-1 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-009 Work Order #...: Work Order #...: LPPHA1A0 Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: Prep Date......: Prep Date......: 11/20/09 Analysis Date..: Analysis Date..: 11/25/09 Prep Batch #...: Prep Batch #...: 9324281 Analysis Time..: Analysis Time..: 15:01 Dilution Factor: Dilution Factor: 0.94 Method.........: Method.........: SW846 8270C
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acenaphthene ND 1.9 ug/L Acenaphthylene ND 1.9 ug/L Acetophenone ND 9.4 ug/L Anthracene ND 1.9 ug/L Atrazine ND 9.4 ug/L Benzo(a)anthracene ND 1.9 ug/L Benzo(a)pyrene ND 1.9 ug/L Benzo(b)fluoranthene ND 1.9 ug/L Benzo(ghi)perylene ND 1.9 ug/L Benzo(k)fluoranthene ND 1.9 ug/L Benzaldehyde ND 9.4 ug/L 1,1'-Biphenyl ND 9.4 ug/L bis(2-Chloroethoxy) ND 9.4 ug/L methane bis(2-Chloroethyl)- ND 1.9 ug/L ether bis(2-Ethylhexyl) ND 9.4 ug/L phthalate 4-Bromophenyl phenyl ND 9.4 ug/L ether Butyl benzyl phthalate ND 9.4 ug/L Caprolactam ND 47 ug/L Carbazole ND 1.9 ug/L 4-Chloroaniline ND 9.4 ug/L 4-Chloro-3-methylphenol ND 9.4 ug/L 2-Chloronaphthalene ND 1.9 ug/L 2-Chlorophenol ND 9.4 ug/L 4-Chlorophenyl phenyl ND 9.4 ug/L ether Chrysene ND 1.9 ug/L Dibenz(a,h)anthracene ND 1.9 ug/L Dibenzofuran ND 9.4 ug/L 3,3'-Dichlorobenzidine ND 9.4 ug/L 2,4-Dichlorophenol ND 1.9 ug/L Diethyl phthalate ND 9.4 ug/L 2,4-Dimethylphenol ND 9.4 ug/L Dimethyl phthalate ND 9.4 ug/L Di-n-butyl phthalate ND 9.4 ug/L (Continued on next page)



### C9K180557 69 of 161Clean Sites Environmental Services Inc Client Sample ID: SW-1 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-009 Work Order #...: Work Order #...: LPPHA1A0 Matrix.........: Matrix.........: WATER
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 4,6-Dinitro- ND 47 ug/L 2-methylphenol 2,4-Dinitrophenol ND 47 ug/L 2,4-Dinitrotoluene ND 9.4 ug/L 2,6-Dinitrotoluene ND 9.4 ug/L Di-n-octyl phthalate ND 9.4 ug/L Fluoranthene ND 1.9 ug/L Fluorene ND 1.9 ug/L Hexachlorobenzene ND 1.9 ug/L Hexachlorobutadiene ND 1.9 ug/L Hexachlorocyclopenta- ND 9.4 ug/L diene Hexachloroethane ND 9.4 ug/L Indeno(1,2,3-cd)pyrene ND 1.9 ug/L Isophorone ND 9.4 ug/L 2-Methylnaphthalene ND 1.9 ug/L 2-Methylphenol ND 9.4 ug/L 4-Methylphenol ND 9.4 ug/L Naphthalene ND 1.9 ug/L 2-Nitroaniline ND 47 ug/L 3-Nitroaniline ND 47 ug/L 4-Nitroaniline ND 47 ug/L Nitrobenzene ND 1.9 ug/L 2-Nitrophenol ND 9.4 ug/L 4-Nitrophenol ND 47 ug/L N-Nitrosodi-n-propyl- ND 1.9 ug/L amine N-Nitrosodiphenylamine ND 1.9 ug/L 2,2'-oxybis ND 1.9 ug/L (1-Chloropropane) Pentachlorophenol ND 9.4 ug/L Phenanthrene ND 1.9 ug/L Phenol ND 1.9 ug/L Pyrene ND 1.9 ug/L 2,4,5-Trichloro- ND 9.4 ug/L phenol 2,4,6-Trichloro- ND 9.4 ug/L phenol (Continued on next page)



### C9K180557 70 of 161Clean Sites Environmental Services Inc Client Sample ID: SW-1 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-009 Work Order #...: Work Order #...: LPPHA1A0 Matrix.........: Matrix.........: WATER

PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 2,4,6-Tribromophenol 68 (33 - 122) 2-Fluorobiphenyl 57 (35 - 108) 2-Fluorophenol 62 (26 - 100) Nitrobenzene-d5 59 (37 - 104) Phenol-d5 64 (30 - 102) Terphenyl-d14 29 (25 - 130)



### C9K180557 71 of 161Clean Sites Environmental Services Inc Client Sample ID: SW-2 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-010 Work Order #...: Work Order #...: LPPHF1AA Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: Prep Date......: Prep Date......: 11/20/09 Analysis Date..: Analysis Date..: 11/25/09 Prep Batch #...: Prep Batch #...: 9324281 Analysis Time..: Analysis Time..: 15:24 Dilution Factor: Dilution Factor: 0.94 Method.........: Method.........: SW846 8270C
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acenaphthene ND 1.9 ug/L Acenaphthylene ND 1.9 ug/L Acetophenone ND 9.4 ug/L Anthracene ND 1.9 ug/L Atrazine ND 9.4 ug/L Benzo(a)anthracene ND 1.9 ug/L Benzo(a)pyrene ND 1.9 ug/L Benzo(b)fluoranthene ND 1.9 ug/L Benzo(ghi)perylene ND 1.9 ug/L Benzo(k)fluoranthene ND 1.9 ug/L Benzaldehyde ND 9.4 ug/L 1,1'-Biphenyl ND 9.4 ug/L bis(2-Chloroethoxy) ND 9.4 ug/L methane bis(2-Chloroethyl)- ND 1.9 ug/L ether bis(2-Ethylhexyl) ND 9.4 ug/L phthalate 4-Bromophenyl phenyl ND 9.4 ug/L ether Butyl benzyl phthalate ND 9.4 ug/L Caprolactam ND 47 ug/L Carbazole ND 1.9 ug/L 4-Chloroaniline ND 9.4 ug/L 4-Chloro-3-methylphenol ND 9.4 ug/L 2-Chloronaphthalene ND 1.9 ug/L 2-Chlorophenol ND 9.4 ug/L 4-Chlorophenyl phenyl ND 9.4 ug/L ether Chrysene ND 1.9 ug/L Dibenz(a,h)anthracene ND 1.9 ug/L Dibenzofuran ND 9.4 ug/L 3,3'-Dichlorobenzidine ND 9.4 ug/L 2,4-Dichlorophenol ND 1.9 ug/L Diethyl phthalate ND 9.4 ug/L 2,4-Dimethylphenol ND 9.4 ug/L Dimethyl phthalate ND 9.4 ug/L Di-n-butyl phthalate ND 9.4 ug/L (Continued on next page)



### C9K180557 72 of 161Clean Sites Environmental Services Inc Client Sample ID: SW-2 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-010 Work Order #...: Work Order #...: LPPHF1AA Matrix.........: Matrix.........: WATER
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 4,6-Dinitro- ND 47 ug/L 2-methylphenol 2,4-Dinitrophenol ND 47 ug/L 2,4-Dinitrotoluene ND 9.4 ug/L 2,6-Dinitrotoluene ND 9.4 ug/L Di-n-octyl phthalate ND 9.4 ug/L Fluoranthene ND 1.9 ug/L Fluorene ND 1.9 ug/L Hexachlorobenzene ND 1.9 ug/L Hexachlorobutadiene ND 1.9 ug/L Hexachlorocyclopenta- ND 9.4 ug/L diene Hexachloroethane ND 9.4 ug/L Indeno(1,2,3-cd)pyrene ND 1.9 ug/L Isophorone ND 9.4 ug/L 2-Methylnaphthalene ND 1.9 ug/L 2-Methylphenol ND 9.4 ug/L 4-Methylphenol ND 9.4 ug/L Naphthalene ND 1.9 ug/L 2-Nitroaniline ND 47 ug/L 3-Nitroaniline ND 47 ug/L 4-Nitroaniline ND 47 ug/L Nitrobenzene ND 1.9 ug/L 2-Nitrophenol ND 9.4 ug/L 4-Nitrophenol ND 47 ug/L N-Nitrosodi-n-propyl- ND 1.9 ug/L amine N-Nitrosodiphenylamine ND 1.9 ug/L 2,2'-oxybis ND 1.9 ug/L (1-Chloropropane) Pentachlorophenol ND 9.4 ug/L Phenanthrene ND 1.9 ug/L Phenol ND 1.9 ug/L Pyrene ND 1.9 ug/L 2,4,5-Trichloro- ND 9.4 ug/L phenol 2,4,6-Trichloro- ND 9.4 ug/L phenol (Continued on next page)



### C9K180557 73 of 161Clean Sites Environmental Services Inc Client Sample ID: SW-2 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-010 Work Order #...: Work Order #...: LPPHF1AA Matrix.........: Matrix.........: WATER

PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 2,4,6-Tribromophenol 50 (33 - 122) 2-Fluorobiphenyl 43 (35 - 108) 2-Fluorophenol 43 (26 - 100) Nitrobenzene-d5 47 (37 - 104) Phenol-d5 41 (30 - 102) Terphenyl-d14 32 (25 - 130)



### C9K180557 74 of 161Clean Sites Environmental Services Inc Client Sample ID: SW-3 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-011 Work Order #...: Work Order #...: LPPHG1AA Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: Prep Date......: Prep Date......: 11/20/09 Analysis Date..: Analysis Date..: 11/25/09 Prep Batch #...: Prep Batch #...: 9324281 Analysis Time..: Analysis Time..: 15:46 Dilution Factor: Dilution Factor: 0.94 Method.........: Method.........: SW846 8270C
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acenaphthene ND 1.9 ug/L Acenaphthylene ND 1.9 ug/L Acetophenone ND 9.4 ug/L Anthracene ND 1.9 ug/L Atrazine ND 9.4 ug/L Benzo(a)anthracene ND 1.9 ug/L Benzo(a)pyrene ND 1.9 ug/L Benzo(b)fluoranthene ND 1.9 ug/L Benzo(ghi)perylene ND 1.9 ug/L Benzo(k)fluoranthene ND 1.9 ug/L Benzaldehyde ND 9.4 ug/L 1,1'-Biphenyl ND 9.4 ug/L bis(2-Chloroethoxy) ND 9.4 ug/L methane bis(2-Chloroethyl)- ND 1.9 ug/L ether bis(2-Ethylhexyl) ND 9.4 ug/L phthalate 4-Bromophenyl phenyl ND 9.4 ug/L ether Butyl benzyl phthalate ND 9.4 ug/L Caprolactam ND 47 ug/L Carbazole ND 1.9 ug/L 4-Chloroaniline ND 9.4 ug/L 4-Chloro-3-methylphenol ND 9.4 ug/L 2-Chloronaphthalene ND 1.9 ug/L 2-Chlorophenol ND 9.4 ug/L 4-Chlorophenyl phenyl ND 9.4 ug/L ether Chrysene ND 1.9 ug/L Dibenz(a,h)anthracene ND 1.9 ug/L Dibenzofuran ND 9.4 ug/L 3,3'-Dichlorobenzidine ND 9.4 ug/L 2,4-Dichlorophenol ND 1.9 ug/L Diethyl phthalate ND 9.4 ug/L 2,4-Dimethylphenol ND 9.4 ug/L Dimethyl phthalate ND 9.4 ug/L Di-n-butyl phthalate ND 9.4 ug/L (Continued on next page)



### C9K180557 75 of 161Clean Sites Environmental Services Inc Client Sample ID: SW-3 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-011 Work Order #...: Work Order #...: LPPHG1AA Matrix.........: Matrix.........: WATER
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 4,6-Dinitro- ND 47 ug/L 2-methylphenol 2,4-Dinitrophenol ND 47 ug/L 2,4-Dinitrotoluene ND 9.4 ug/L 2,6-Dinitrotoluene ND 9.4 ug/L Di-n-octyl phthalate ND 9.4 ug/L Fluoranthene ND 1.9 ug/L Fluorene ND 1.9 ug/L Hexachlorobenzene ND 1.9 ug/L Hexachlorobutadiene ND 1.9 ug/L Hexachlorocyclopenta- ND 9.4 ug/L diene Hexachloroethane ND 9.4 ug/L Indeno(1,2,3-cd)pyrene ND 1.9 ug/L Isophorone ND 9.4 ug/L 2-Methylnaphthalene ND 1.9 ug/L 2-Methylphenol ND 9.4 ug/L 4-Methylphenol ND 9.4 ug/L Naphthalene ND 1.9 ug/L 2-Nitroaniline ND 47 ug/L 3-Nitroaniline ND 47 ug/L 4-Nitroaniline ND 47 ug/L Nitrobenzene ND 1.9 ug/L 2-Nitrophenol ND 9.4 ug/L 4-Nitrophenol ND 47 ug/L N-Nitrosodi-n-propyl- ND 1.9 ug/L amine N-Nitrosodiphenylamine ND 1.9 ug/L 2,2'-oxybis ND 1.9 ug/L (1-Chloropropane) Pentachlorophenol ND 9.4 ug/L Phenanthrene ND 1.9 ug/L Phenol ND 1.9 ug/L Pyrene ND 1.9 ug/L 2,4,5-Trichloro- ND 9.4 ug/L phenol 2,4,6-Trichloro- ND 9.4 ug/L phenol (Continued on next page)



### C9K180557 76 of 161Clean Sites Environmental Services Inc Client Sample ID: SW-3 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-011 Work Order #...: Work Order #...: LPPHG1AA Matrix.........: Matrix.........: WATER

PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 2,4,6-Tribromophenol 51 (33 - 122) 2-Fluorobiphenyl 42 (35 - 108) 2-Fluorophenol 42 (26 - 100) Nitrobenzene-d5 45 (37 - 104) Phenol-d5 42 (30 - 102) Terphenyl-d14 32 (25 - 130)



### C9K180557 77 of 161Clean Sites Environmental Services Inc Client Sample ID: SED-1 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-012 Work Order #...: Work Order #...: LPPHK1AE Matrix.........: Matrix.........: SOLID Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9323002 Prep Date......: Prep Date......: 11/19/09 Analysis Date..: Analysis Date..: 11/20/09 Prep Batch #...: Prep Batch #...: 9323010 Analysis Time..: Analysis Time..: 00:18 Dilution Factor: Dilution Factor: 1 % Moisture.....: % Moisture.....: 20 Method.........: Method.........: SW846 8270C
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acenaphthene ND 83 ug/kg Acenaphthylene ND 83 ug/kg Acetophenone ND 410 ug/kg Anthracene ND 83 ug/kg Atrazine ND 410 ug/kg Benzo(a)anthracene ND 83 ug/kg Benzo(a)pyrene ND 83 ug/kg Benzo(b)fluoranthene ND 83 ug/kg Benzo(ghi)perylene ND 83 ug/kg Benzo(k)fluoranthene ND 83 ug/kg Benzaldehyde ND 410 ug/kg 1,1'-Biphenyl ND 410 ug/kg bis(2-Chloroethoxy) ND 410 ug/kg methane bis(2-Chloroethyl)- ND 83 ug/kg ether bis(2-Ethylhexyl) ND 410 ug/kg phthalate 4-Bromophenyl phenyl ND 410 ug/kg ether Butyl benzyl phthalate ND 410 ug/kg Caprolactam ND 2100 ug/kg Carbazole ND 83 ug/kg 4-Chloroaniline ND 410 ug/kg 4-Chloro-3-methylphenol ND 410 ug/kg 2-Chloronaphthalene ND 83 ug/kg 2-Chlorophenol ND 410 ug/kg 4-Chlorophenyl phenyl ND 410 ug/kg ether Chrysene ND 83 ug/kg Dibenz(a,h)anthracene ND 83 ug/kg Dibenzofuran ND 410 ug/kg 3,3'-Dichlorobenzidine ND 410 ug/kg 2,4-Dichlorophenol ND 83 ug/kg Diethyl phthalate ND 410 ug/kg 2,4-Dimethylphenol ND 410 ug/kg Dimethyl phthalate ND 410 ug/kg Di-n-butyl phthalate ND 410 ug/kg (Continued on next page)



### C9K180557 78 of 161Clean Sites Environmental Services Inc Client Sample ID: SED-1 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-012 Work Order #...: Work Order #...: LPPHK1AE Matrix.........: Matrix.........: SOLID
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 4,6-Dinitro- ND 2100 ug/kg 2-methylphenol 2,4-Dinitrophenol ND 2100 ug/kg 2,4-Dinitrotoluene ND 410 ug/kg 2,6-Dinitrotoluene ND 410 ug/kg Di-n-octyl phthalate ND 410 ug/kg Fluoranthene ND 83 ug/kg Fluorene ND 83 ug/kg Hexachlorobenzene ND 83 ug/kg Hexachlorobutadiene ND 83 ug/kg Hexachlorocyclopenta- ND 410 ug/kg diene Hexachloroethane ND 410 ug/kg Indeno(1,2,3-cd)pyrene ND 83 ug/kg Isophorone ND 410 ug/kg 2-Methylnaphthalene ND 83 ug/kg 2-Methylphenol ND 410 ug/kg 4-Methylphenol ND 410 ug/kg Naphthalene ND 83 ug/kg 2-Nitroaniline ND 2100 ug/kg 3-Nitroaniline ND 2100 ug/kg 4-Nitroaniline ND 2100 ug/kg Nitrobenzene ND 83 ug/kg 2-Nitrophenol ND 410 ug/kg 4-Nitrophenol ND 2100 ug/kg N-Nitrosodi-n-propyl- ND 83 ug/kg amine N-Nitrosodiphenylamine ND 83 ug/kg 2,2'-oxybis ND 83 ug/kg (1-Chloropropane) Pentachlorophenol ND 410 ug/kg Phenanthrene ND 83 ug/kg Phenol ND 83 ug/kg Pyrene ND 83 ug/kg 2,4,5-Trichloro- ND 410 ug/kg phenol 2,4,6-Trichloro- ND 410 ug/kg phenol (Continued on next page)



### C9K180557 79 of 161Clean Sites Environmental Services Inc Client Sample ID: SED-1 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-012 Work Order #...: Work Order #...: LPPHK1AE Matrix.........: Matrix.........: SOLID

PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 2,4,6-Tribromophenol 48 (35 - 124) 2-Fluorobiphenyl 53 (35 - 105) 2-Fluorophenol 65 (39 - 103) Nitrobenzene-d5 62 (25 - 104) Phenol-d5 60 (25 - 105) Terphenyl-d14 54 (25 - 127) NOTE(S):

_______________________________________________________________________________________ Results and reporting limits have been adjusted for dry weight.



### C9K180557 80 of 161Clean Sites Environmental Services Inc Client Sample ID: SED-2 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-013 Work Order #...: Work Order #...: LPPHM1AM Matrix.........: Matrix.........: SOLID Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9323002 Prep Date......: Prep Date......: 11/19/09 Analysis Date..: Analysis Date..: 11/20/09 Prep Batch #...: Prep Batch #...: 9323010 Analysis Time..: Analysis Time..: 01:21 Dilution Factor: Dilution Factor: 1 % Moisture.....: % Moisture.....: 20 Method.........: Method.........: SW846 8270C
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acenaphthene ND 83 ug/kg Acenaphthylene ND 83 ug/kg Acetophenone ND 410 ug/kg Anthracene ND 83 ug/kg Atrazine ND 410 ug/kg Benzo(a)anthracene ND 83 ug/kg Benzo(a)pyrene ND 83 ug/kg Benzo(b)fluoranthene ND 83 ug/kg Benzo(ghi)perylene ND 83 ug/kg Benzo(k)fluoranthene ND 83 ug/kg Benzaldehyde ND 410 ug/kg 1,1'-Biphenyl ND 410 ug/kg bis(2-Chloroethoxy) ND 410 ug/kg methane bis(2-Chloroethyl)- ND 83 ug/kg ether bis(2-Ethylhexyl) ND 410 ug/kg phthalate 4-Bromophenyl phenyl ND 410 ug/kg ether Butyl benzyl phthalate ND 410 ug/kg Caprolactam ND 2100 ug/kg Carbazole ND 83 ug/kg 4-Chloroaniline ND 410 ug/kg 4-Chloro-3-methylphenol ND 410 ug/kg 2-Chloronaphthalene ND 83 ug/kg 2-Chlorophenol ND 410 ug/kg 4-Chlorophenyl phenyl ND 410 ug/kg ether Chrysene ND 83 ug/kg Dibenz(a,h)anthracene ND 83 ug/kg Dibenzofuran ND 410 ug/kg 3,3'-Dichlorobenzidine ND 410 ug/kg 2,4-Dichlorophenol ND 83 ug/kg Diethyl phthalate ND 410 ug/kg 2,4-Dimethylphenol ND 410 ug/kg Dimethyl phthalate ND 410 ug/kg Di-n-butyl phthalate ND 410 ug/kg (Continued on next page)



### C9K180557 81 of 161Clean Sites Environmental Services Inc Client Sample ID: SED-2 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-013 Work Order #...: Work Order #...: LPPHM1AM Matrix.........: Matrix.........: SOLID
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 4,6-Dinitro- ND 2100 ug/kg 2-methylphenol 2,4-Dinitrophenol ND 2100 ug/kg 2,4-Dinitrotoluene ND 410 ug/kg 2,6-Dinitrotoluene ND 410 ug/kg Di-n-octyl phthalate ND 410 ug/kg Fluoranthene ND 83 ug/kg Fluorene ND 83 ug/kg Hexachlorobenzene ND 83 ug/kg Hexachlorobutadiene ND 83 ug/kg Hexachlorocyclopenta- ND 410 ug/kg diene Hexachloroethane ND 410 ug/kg Indeno(1,2,3-cd)pyrene ND 83 ug/kg Isophorone ND 410 ug/kg 2-Methylnaphthalene ND 83 ug/kg 2-Methylphenol ND 410 ug/kg 4-Methylphenol ND 410 ug/kg Naphthalene ND 83 ug/kg 2-Nitroaniline ND 2100 ug/kg 3-Nitroaniline ND 2100 ug/kg 4-Nitroaniline ND 2100 ug/kg Nitrobenzene ND 83 ug/kg 2-Nitrophenol ND 410 ug/kg 4-Nitrophenol ND 2100 ug/kg N-Nitrosodi-n-propyl- ND 83 ug/kg amine N-Nitrosodiphenylamine ND 83 ug/kg 2,2'-oxybis ND 83 ug/kg (1-Chloropropane) Pentachlorophenol ND 410 ug/kg Phenanthrene ND 83 ug/kg Phenol ND 83 ug/kg Pyrene ND 83 ug/kg 2,4,5-Trichloro- ND 410 ug/kg phenol 2,4,6-Trichloro- ND 410 ug/kg phenol (Continued on next page)



### C9K180557 82 of 161Clean Sites Environmental Services Inc Client Sample ID: SED-2 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-013 Work Order #...: Work Order #...: LPPHM1AM Matrix.........: Matrix.........: SOLID

PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 2,4,6-Tribromophenol 59 (35 - 124) 2-Fluorobiphenyl 62 (35 - 105) 2-Fluorophenol 72 (39 - 103) Nitrobenzene-d5 65 (25 - 104) Phenol-d5 66 (25 - 105) Terphenyl-d14 64 (25 - 127) NOTE(S):

_______________________________________________________________________________________ Results and reporting limits have been adjusted for dry weight.



### C9K180557 83 of 161Clean Sites Environmental Services Inc Client Sample ID: SED-3 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-014 Work Order #...: Work Order #...: LPPHN1AV Matrix.........: Matrix.........: SOLID Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9323002 Prep Date......: Prep Date......: 11/19/09 Analysis Date..: Analysis Date..: 11/20/09 Prep Batch #...: Prep Batch #...: 9323010 Analysis Time..: Analysis Time..: 01:41 Dilution Factor: Dilution Factor: 1 % Moisture.....: % Moisture.....: 23 Method.........: Method.........: SW846 8270C
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ Acenaphthene ND 87 ug/kg Acenaphthylene ND 87 ug/kg Acetophenone ND 430 ug/kg Anthracene ND 87 ug/kg Atrazine ND 430 ug/kg Benzo(a)anthracene ND 87 ug/kg Benzo(a)pyrene ND 87 ug/kg Benzo(b)fluoranthene ND 87 ug/kg Benzo(ghi)perylene ND 87 ug/kg Benzo(k)fluoranthene ND 87 ug/kg Benzaldehyde ND 430 ug/kg 1,1'-Biphenyl ND 430 ug/kg bis(2-Chloroethoxy) ND 430 ug/kg methane bis(2-Chloroethyl)- ND 87 ug/kg ether bis(2-Ethylhexyl) ND 430 ug/kg phthalate 4-Bromophenyl phenyl ND 430 ug/kg ether Butyl benzyl phthalate ND 430 ug/kg Caprolactam ND 2200 ug/kg Carbazole ND 87 ug/kg 4-Chloroaniline ND 430 ug/kg 4-Chloro-3-methylphenol ND 430 ug/kg 2-Chloronaphthalene ND 87 ug/kg 2-Chlorophenol ND 430 ug/kg 4-Chlorophenyl phenyl ND 430 ug/kg ether Chrysene ND 87 ug/kg Dibenz(a,h)anthracene ND 87 ug/kg Dibenzofuran ND 430 ug/kg 3,3'-Dichlorobenzidine ND 430 ug/kg 2,4-Dichlorophenol ND 87 ug/kg Diethyl phthalate ND 430 ug/kg 2,4-Dimethylphenol ND 430 ug/kg Dimethyl phthalate ND 430 ug/kg Di-n-butyl phthalate ND 430 ug/kg (Continued on next page)



### C9K180557 84 of 161Clean Sites Environmental Services Inc Client Sample ID: SED-3 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-014 Work Order #...: Work Order #...: LPPHN1AV Matrix.........: Matrix.........: SOLID
REPORTING PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS

_________ 4,6-Dinitro- ND 2200 ug/kg 2-methylphenol 2,4-Dinitrophenol ND 2200 ug/kg 2,4-Dinitrotoluene ND 430 ug/kg 2,6-Dinitrotoluene ND 430 ug/kg Di-n-octyl phthalate ND 430 ug/kg Fluoranthene ND 87 ug/kg Fluorene ND 87 ug/kg Hexachlorobenzene ND 87 ug/kg Hexachlorobutadiene ND 87 ug/kg Hexachlorocyclopenta- ND 430 ug/kg diene Hexachloroethane ND 430 ug/kg Indeno(1,2,3-cd)pyrene ND 87 ug/kg Isophorone ND 430 ug/kg 2-Methylnaphthalene ND 87 ug/kg 2-Methylphenol ND 430 ug/kg 4-Methylphenol ND 430 ug/kg Naphthalene ND 87 ug/kg 2-Nitroaniline ND 2200 ug/kg 3-Nitroaniline ND 2200 ug/kg 4-Nitroaniline ND 2200 ug/kg Nitrobenzene ND 87 ug/kg 2-Nitrophenol ND 430 ug/kg 4-Nitrophenol ND 2200 ug/kg N-Nitrosodi-n-propyl- ND 87 ug/kg amine N-Nitrosodiphenylamine ND 87 ug/kg 2,2'-oxybis ND 87 ug/kg (1-Chloropropane) Pentachlorophenol ND 430 ug/kg Phenanthrene ND 87 ug/kg Phenol ND 87 ug/kg Pyrene ND 87 ug/kg 2,4,5-Trichloro- ND 430 ug/kg phenol 2,4,6-Trichloro- ND 430 ug/kg phenol (Continued on next page)



### C9K180557 85 of 161Clean Sites Environmental Services Inc Client Sample ID: SED-3 GC/MS Semivolatiles Lot-Sample #...: Lot-Sample #...: C9K180557-014 Work Order #...: Work Order #...: LPPHN1AV Matrix.........: Matrix.........: SOLID

PERCENT RECOVERY SURROGATE ______________________________ RECOVERY _______________ LIMITS

__________ 2,4,6-Tribromophenol 62 (35 - 124) 2-Fluorobiphenyl 64 (35 - 105) 2-Fluorophenol 71 (39 - 103) Nitrobenzene-d5 67 (25 - 104) Phenol-d5 68 (25 - 105) Terphenyl-d14 64 (25 - 127) NOTE(S):

_______________________________________________________________________________________ Results and reporting limits have been adjusted for dry weight.



### C9K180557 86 of 161METHOD BLANK REPORT GC/MS Semivolatiles Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPP7G1AA Matrix.........: Matrix.........: SOLID MB Lot-Sample #: MB Lot-Sample #: C9K190000-010 Prep Date......: Prep Date......: 11/19/09 Analysis Time..: Analysis Time..: 23:18 Analysis Date..: Analysis Date..: 11/19/09 Prep Batch #...: Prep Batch #...: 9323010 Dilution Factor: Dilution Factor: 1
REPORTING PARAMETER _________________________ RESULT _______________ LIMIT

_________ UNITS

__________ METHOD

_________________ Acenaphthene ND 67 ug/kg SW846 8270C Acenaphthylene ND 67 ug/kg SW846 8270C Acetophenone ND 330 ug/kg SW846 8270C Anthracene ND 67 ug/kg SW846 8270C Atrazine ND 330 ug/kg SW846 8270C Benzo(a)anthracene ND 67 ug/kg SW846 8270C Benzo(a)pyrene ND 67 ug/kg SW846 8270C Benzo(b)fluoranthene ND 67 ug/kg SW846 8270C Benzo(ghi)perylene ND 67 ug/kg SW846 8270C Benzo(k)fluoranthene ND 67 ug/kg SW846 8270C Benzaldehyde ND 330 ug/kg SW846 8270C 1,1'-Biphenyl ND 330 ug/kg SW846 8270C bis(2-Chloroethoxy) ND 330 ug/kg SW846 8270C methane bis(2-Chloroethyl)- ND 67 ug/kg SW846 8270C ether bis(2-Ethylhexyl) ND 330 ug/kg SW846 8270C phthalate 4-Bromophenyl phenyl ND 330 ug/kg SW846 8270C ether Butyl benzyl phthalate ND 330 ug/kg SW846 8270C Caprolactam ND 1700 ug/kg SW846 8270C Carbazole ND 67 ug/kg SW846 8270C 4-Chloroaniline ND 330 ug/kg SW846 8270C 4-Chloro-3-methylphenol ND 330 ug/kg SW846 8270C 2-Chloronaphthalene ND 67 ug/kg SW846 8270C 2-Chlorophenol ND 330 ug/kg SW846 8270C 4-Chlorophenyl phenyl ND 330 ug/kg SW846 8270C ether Chrysene ND 67 ug/kg SW846 8270C Dibenz(a,h)anthracene ND 67 ug/kg SW846 8270C Dibenzofuran ND 330 ug/kg SW846 8270C 3,3'-Dichlorobenzidine ND 330 ug/kg SW846 8270C 2,4-Dichlorophenol ND 67 ug/kg SW846 8270C Diethyl phthalate ND 330 ug/kg SW846 8270C 2,4-Dimethylphenol ND 330 ug/kg SW846 8270C Dimethyl phthalate ND 330 ug/kg SW846 8270C Di-n-butyl phthalate ND 330 ug/kg SW846 8270C 4,6-Dinitro- ND 1700 ug/kg SW846 8270C 2-methylphenol 2,4-Dinitrophenol ND 1700 ug/kg SW846 8270C (Continued on next page)



### C9K180557 87 of 161METHOD BLANK REPORT GC/MS Semivolatiles Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPP7G1AA Matrix.........: Matrix.........: SOLID
REPORTING PARAMETER _________________________ RESULT _______________ LIMIT

_________ UNITS

__________ METHOD

_________________ 2,4-Dinitrotoluene ND 330 ug/kg SW846 8270C 2,6-Dinitrotoluene ND 330 ug/kg SW846 8270C Di-n-octyl phthalate ND 330 ug/kg SW846 8270C Fluoranthene ND 67 ug/kg SW846 8270C Fluorene ND 67 ug/kg SW846 8270C Hexachlorobenzene ND 67 ug/kg SW846 8270C Hexachlorobutadiene ND 67 ug/kg SW846 8270C Hexachlorocyclopenta- ND 330 ug/kg SW846 8270C diene Hexachloroethane ND 330 ug/kg SW846 8270C Indeno(1,2,3-cd)pyrene ND 67 ug/kg SW846 8270C Isophorone ND 330 ug/kg SW846 8270C 2-Methylnaphthalene ND 67 ug/kg SW846 8270C 2-Methylphenol ND 330 ug/kg SW846 8270C 4-Methylphenol ND 330 ug/kg SW846 8270C Naphthalene ND 67 ug/kg SW846 8270C 2-Nitroaniline ND 1700 ug/kg SW846 8270C 3-Nitroaniline ND 1700 ug/kg SW846 8270C 4-Nitroaniline ND 1700 ug/kg SW846 8270C Nitrobenzene ND 67 ug/kg SW846 8270C 2-Nitrophenol ND 330 ug/kg SW846 8270C 4-Nitrophenol ND 1700 ug/kg SW846 8270C N-Nitrosodi-n-propyl- ND 67 ug/kg SW846 8270C amine N-Nitrosodiphenylamine ND 67 ug/kg SW846 8270C 2,2'-oxybis ND 67 ug/kg SW846 8270C (1-Chloropropane) Pentachlorophenol ND 330 ug/kg SW846 8270C Phenanthrene ND 67 ug/kg SW846 8270C Phenol ND 67 ug/kg SW846 8270C Pyrene ND 67 ug/kg SW846 8270C 2,4,5-Trichloro- ND 330 ug/kg SW846 8270C phenol 2,4,6-Trichloro- ND 330 ug/kg SW846 8270C phenol
PERCENT RECOVERY SURROGATE _________________________ RECOVERY ________ LIMITS

__________ 2,4,6-Tribromophenol 75 (35 - 124) 2-Fluorobiphenyl 73 (35 - 105) 2-Fluorophenol 93 (39 - 103) Nitrobenzene-d5 79 (25 - 104) Phenol-d5 86 (25 - 105) Terphenyl-d14 78 (25 - 127) (Continued on next page)



### C9K180557 88 of 161METHOD BLANK REPORT GC/MS Semivolatiles Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPP7G1AA Matrix.........: Matrix.........: SOLID

NOTE(S):

___________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results.



### C9K180557 89 of 161METHOD BLANK REPORT GC/MS Semivolatiles Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPVAM1AA Matrix.........: Matrix.........: WATER MB Lot-Sample #: MB Lot-Sample #: C9K200000-281 Prep Date......: Prep Date......: 11/20/09 Analysis Time..: Analysis Time..: 12:25 Analysis Date..: Analysis Date..: 11/25/09 Prep Batch #...: Prep Batch #...: 9324281 Dilution Factor: Dilution Factor: 1
REPORTING PARAMETER _________________________ RESULT _______________ LIMIT

_________ UNITS

__________ METHOD

_________________ Acenaphthene ND 2.0 ug/L SW846 8270C Acenaphthylene ND 2.0 ug/L SW846 8270C Acetophenone ND 10 ug/L SW846 8270C Anthracene ND 2.0 ug/L SW846 8270C Atrazine ND 10 ug/L SW846 8270C Benzo(a)anthracene ND 2.0 ug/L SW846 8270C Benzo(a)pyrene ND 2.0 ug/L SW846 8270C Benzo(b)fluoranthene ND 2.0 ug/L SW846 8270C Benzo(ghi)perylene ND 2.0 ug/L SW846 8270C Benzo(k)fluoranthene ND 2.0 ug/L SW846 8270C Benzaldehyde ND 10 ug/L SW846 8270C 1,1'-Biphenyl ND 10 ug/L SW846 8270C bis(2-Chloroethoxy) ND 10 ug/L SW846 8270C methane bis(2-Chloroethyl)- ND 2.0 ug/L SW846 8270C ether bis(2-Ethylhexyl) ND 10 ug/L SW846 8270C phthalate 4-Bromophenyl phenyl ND 10 ug/L SW846 8270C ether Butyl benzyl phthalate ND 10 ug/L SW846 8270C Caprolactam ND 50 ug/L SW846 8270C Carbazole ND 2.0 ug/L SW846 8270C 4-Chloroaniline ND 10 ug/L SW846 8270C 4-Chloro-3-methylphenol ND 10 ug/L SW846 8270C 2-Chloronaphthalene ND 2.0 ug/L SW846 8270C 2-Chlorophenol ND 10 ug/L SW846 8270C 4-Chlorophenyl phenyl ND 10 ug/L SW846 8270C ether Chrysene ND 2.0 ug/L SW846 8270C Dibenz(a,h)anthracene ND 2.0 ug/L SW846 8270C Dibenzofuran ND 10 ug/L SW846 8270C 3,3'-Dichlorobenzidine ND 10 ug/L SW846 8270C 2,4-Dichlorophenol ND 2.0 ug/L SW846 8270C Diethyl phthalate ND 10 ug/L SW846 8270C 2,4-Dimethylphenol ND 10 ug/L SW846 8270C Dimethyl phthalate ND 10 ug/L SW846 8270C Di-n-butyl phthalate ND 10 ug/L SW846 8270C 4,6-Dinitro- ND 50 ug/L SW846 8270C 2-methylphenol 2,4-Dinitrophenol ND 50 ug/L SW846 8270C (Continued on next page)



### C9K180557 90 of 161METHOD BLANK REPORT GC/MS Semivolatiles Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPVAM1AA Matrix.........: Matrix.........: WATER
REPORTING PARAMETER _________________________ RESULT _______________ LIMIT

_________ UNITS

__________ METHOD

_________________ 2,4-Dinitrotoluene ND 10 ug/L SW846 8270C 2,6-Dinitrotoluene ND 10 ug/L SW846 8270C Di-n-octyl phthalate ND 10 ug/L SW846 8270C Fluoranthene ND 2.0 ug/L SW846 8270C Fluorene ND 2.0 ug/L SW846 8270C Hexachlorobenzene ND 2.0 ug/L SW846 8270C Hexachlorobutadiene ND 2.0 ug/L SW846 8270C Hexachlorocyclopenta- ND 10 ug/L SW846 8270C diene Hexachloroethane ND 10 ug/L SW846 8270C Indeno(1,2,3-cd)pyrene ND 2.0 ug/L SW846 8270C Isophorone ND 10 ug/L SW846 8270C 2-Methylnaphthalene ND 2.0 ug/L SW846 8270C 2-Methylphenol ND 10 ug/L SW846 8270C 4-Methylphenol ND 10 ug/L SW846 8270C Naphthalene ND 2.0 ug/L SW846 8270C 2-Nitroaniline ND 50 ug/L SW846 8270C 3-Nitroaniline ND 50 ug/L SW846 8270C 4-Nitroaniline ND 50 ug/L SW846 8270C Nitrobenzene ND 2.0 ug/L SW846 8270C 2-Nitrophenol ND 10 ug/L SW846 8270C 4-Nitrophenol ND 50 ug/L SW846 8270C N-Nitrosodi-n-propyl- ND 2.0 ug/L SW846 8270C amine N-Nitrosodiphenylamine ND 2.0 ug/L SW846 8270C 2,2'-oxybis ND 2.0 ug/L SW846 8270C (1-Chloropropane) Pentachlorophenol ND 10 ug/L SW846 8270C Phenanthrene ND 2.0 ug/L SW846 8270C Phenol ND 2.0 ug/L SW846 8270C Pyrene ND 2.0 ug/L SW846 8270C 2,4,5-Trichloro- ND 10 ug/L SW846 8270C phenol 2,4,6-Trichloro- ND 10 ug/L SW846 8270C phenol
PERCENT RECOVERY SURROGATE _________________________ RECOVERY ________ LIMITS

__________ 2,4,6-Tribromophenol 70 (33 - 122) 2-Fluorobiphenyl 57 (35 - 108) 2-Fluorophenol 69 (26 - 100) Nitrobenzene-d5 61 (37 - 104) Phenol-d5 73 (30 - 102) Terphenyl-d14 75 (25 - 130) (Continued on next page)



### C9K180557 91 of 161METHOD BLANK REPORT GC/MS Semivolatiles Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPVAM1AA Matrix.........: Matrix.........: WATER

NOTE(S):

___________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results.



### C9K180557 92 of 161LABORATORY CONTROL SAMPLE EVALUATION REPORT GC/MS Semivolatiles Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPP7G1AC Matrix.........: Matrix.........: SOLID LCS Lot-Sample#: LCS Lot-Sample#: C9K190000-010 Prep Date......: Prep Date......: 11/19/09 Analysis Date..: Analysis Date..: 11/19/09 Prep Batch #...: Prep Batch #...: 9323010 Analysis Time..: Analysis Time..: 23:38 Dilution Factor: Dilution Factor: 1
PERCENT RECOVERY PARAMETER ________________________ RECOVERY ________ LIMITS

__________ METHOD

_________________ Acenaphthene Acenaphthene 76 (47 - 104)

(47 - 104) SW846 8270C

SW846 8270C 1,2,4-Trichloro- 1,2,4-Trichloro- 67 (43 - 100)

(43 - 100) SW846 8270C

SW846 8270C benzene 1,4-Dichlorobenzene 1,4-Dichlorobenzene 74 (35 - 99)

(35 - 99) SW846 8270C

SW846 8270C 4-Bromophenyl phenyl 4-Bromophenyl phenyl 72 (47 - 110)

(47 - 110) SW846 8270C

SW846 8270C ether Butyl benzyl phthalate Butyl benzyl phthalate 75 (41 - 118)

(41 - 118) SW846 8270C

SW846 8270C 4-Chloro-3-methylphenol 4-Chloro-3-methylphenol 82 (47 - 109)

(47 - 109) SW846 8270C

SW846 8270C 2-Chlorophenol 2-Chlorophenol 77 (40 - 101)

(40 - 101) SW846 8270C

SW846 8270C 2,4-Dinitrotoluene 2,4-Dinitrotoluene 92 (45 - 124)

(45 - 124) SW846 8270C

SW846 8270C Hexachloroethane Hexachloroethane 74 (37 - 97)

(37 - 97) SW846 8270C

SW846 8270C 4-Methylphenol 4-Methylphenol 81 (42 - 105)

(42 - 105) SW846 8270C

SW846 8270C Naphthalene Naphthalene 73 (43 - 100)

(43 - 100) SW846 8270C

SW846 8270C 4-Nitrophenol 4-Nitrophenol 89 (36 - 127)

(36 - 127) SW846 8270C

SW846 8270C N-Nitrosodi-n-propyl- N-Nitrosodi-n-propyl- 78 (42 - 107)

(42 - 107) SW846 8270C

SW846 8270C amine Pentachlorophenol Pentachlorophenol 75 (17 - 122)

(17 - 122) SW846 8270C

SW846 8270C Phenol 73 (41 - 102)

(41 - 102) SW846 8270C

SW846 8270C Pyrene 70 (41 - 115)

(41 - 115) SW846 8270C

SW846 8270C
PERCENT RECOVERY SURROGATE _________________________ RECOVERY ________ LIMITS

__________ 2,4,6-Tribromophenol 77 (35 - 124) 2-Fluorobiphenyl 77 (35 - 105) 2-Fluorophenol 89 (39 - 103) Nitrobenzene-d5 82 (25 - 104) Phenol-d5 88 (25 - 105) Terphenyl-d14 75 (25 - 127) NOTE(S):

_____________________________________________________________________________________ _____________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results. Bold print denotes control parameters



### C9K180557 93 of 161LABORATORY CONTROL SAMPLE EVALUATION REPORT GC/MS Semivolatiles Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPVAM1AC-LCS Matrix.........: Matrix.........: WATER LCS Lot-Sample#: LCS Lot-Sample#: C9K200000-281 LPVAM1AD-LCSD Prep Date......: Prep Date......: 11/20/09 Analysis Date..: Analysis Date..: 11/25/09 Prep Batch #...: Prep Batch #...: 9324281 Analysis Time..: Analysis Time..: 12:47 Dilution Factor: Dilution Factor: 1
PERCENT RECOVERY RPD PARAMETER ________________________ RECOVERY ________ LIMITS

__________ RPD

_____ LIMITS ______ METHOD

_________________ Acenaphthene Acenaphthene 62 (39 - 106)

(39 - 106) SW846 8270C SW846 8270C 63 (39 - 106)

(39 - 106) 1.7

(0-32) SW846 8270C

SW846 8270C 1,2,4-Trichloro- 1,2,4-Trichloro- 72 (36 - 97)

(36 - 97) SW846 8270C SW846 8270C benzene 73 (36 - 97)

(36 - 97) 2.3

(0-32) SW846 8270C

SW846 8270C 1,4-Dichlorobenzene 1,4-Dichlorobenzene 75 (32 - 94)

(32 - 94) SW846 8270C SW846 8270C 74 (32 - 94)

(32 - 94) 1.3

(0-33) SW846 8270C

SW846 8270C 4-Bromophenyl phenyl 4-Bromophenyl phenyl 73 (38 - 108)

(38 - 108) SW846 8270C SW846 8270C ether 74 (38 - 108)

(38 - 108) 1.7

(0-40) SW846 8270C

SW846 8270C Butyl benzyl phthalate Butyl benzyl phthalate 76 (34 - 110)

(34 - 110) SW846 8270C SW846 8270C 72 (34 - 110)

(34 - 110) 5.5

(0-35) SW846 8270C

SW846 8270C 4-Chloro-3-methylphenol 4-Chloro-3-methylphenol 71 (40 - 107)

(40 - 107) SW846 8270C SW846 8270C 71 (40 - 107)

(40 - 107) 0.36

(0-32) SW846 8270C

SW846 8270C 2-Chlorophenol 2-Chlorophenol 76 (34 - 100)

(34 - 100) SW846 8270C SW846 8270C 75 (34 - 100)

(34 - 100) 1.7

(0-31) SW846 8270C

SW846 8270C 2,4-Dinitrotoluene 2,4-Dinitrotoluene 71 (41 - 117)

(41 - 117) SW846 8270C SW846 8270C 73 (41 - 117)

(41 - 117) 2.1

(0-32) SW846 8270C

SW846 8270C Hexachloroethane Hexachloroethane 71 (27 - 94)

(27 - 94) SW846 8270C SW846 8270C 70 (27 - 94)

(27 - 94) 1.4

(0-43) SW846 8270C

SW846 8270C 4-Methylphenol 4-Methylphenol 75 (34 - 104)

(34 - 104) SW846 8270C SW846 8270C 75 (34 - 104)

(34 - 104) 0.50

(0-34) SW846 8270C

SW846 8270C Naphthalene Naphthalene 72 (35 - 98)

(35 - 98) SW846 8270C SW846 8270C 73 (35 - 98)

(35 - 98) 1.1

(0-39) SW846 8270C

SW846 8270C 4-Nitrophenol 4-Nitrophenol 65 (29 - 120)

(29 - 120) SW846 8270C SW846 8270C 66 (29 - 120)

(29 - 120) 2.0

(0-39) SW846 8270C

SW846 8270C N-Nitrosodi-n-propyl- N-Nitrosodi-n-propyl- 71 (37 - 106)

(37 - 106) SW846 8270C SW846 8270C amine 68 (37 - 106)

(37 - 106) 4.2

(0-36) SW846 8270C

SW846 8270C Pentachlorophenol Pentachlorophenol 65 (10 - 118)

(10 - 118) SW846 8270C SW846 8270C 68 (10 - 118)

(10 - 118) 4.6

(0-49) SW846 8270C

SW846 8270C Phenol 70 (35 - 98)

(35 - 98) SW846 8270C SW846 8270C 69 (35 - 98)

(35 - 98) 1.8

(0-35) SW846 8270C

SW846 8270C Pyrene 80 (36 - 115)

(36 - 115) SW846 8270C SW846 8270C 75 (36 - 115)

(36 - 115) 6.2

(0-38) SW846 8270C

SW846 8270C (Continued on next page)



### C9K180557 94 of 161LABORATORY CONTROL SAMPLE EVALUATION REPORT GC/MS Semivolatiles Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPVAM1AC-LCS Matrix.........: Matrix.........: WATER LCS Lot-Sample#: LCS Lot-Sample#: C9K200000-281 LPVAM1AD-LCSD
PERCENT RECOVERY SURROGATE _________________________ RECOVERY ________ LIMITS

__________ 2,4,6-Tribromophenol 81 (33 - 122) 81 (33 - 122) 2-Fluorobiphenyl 69 (35 - 108) 71 (35 - 108) 2-Fluorophenol 83 (26 - 100) 81 (26 - 100) Nitrobenzene-d5 75 (37 - 104) 72 (37 - 104) Phenol-d5 84 (30 - 102) 82 (30 - 102) Terphenyl-d14 88 (25 - 130) 83 (25 - 130) NOTE(S):

________________________________________________________________________________________ ________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results. Bold print denotes control parameters



### C9K180557 95 of 161MATRIX SPIKE SAMPLE EVALUATION REPORT GC/MS Semivolatiles Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPPHK1A7-MS Matrix.........: Matrix.........: SOLID MS Lot-Sample #: MS Lot-Sample #: C9K180557-012 LPPHK1A8-MSD Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9323002 Prep Date......: Prep Date......: 11/19/09 Analysis Date..: Analysis Date..: 11/20/09 Prep Batch #...: Prep Batch #...: 9323010 Analysis Time..: Analysis Time..: 00:41 Dilution Factor: Dilution Factor: 1 % Moisture.....: % Moisture.....: 20
PERCENT RECOVERY RPD PARAMETER _________________________ RECOVERY _________ LIMITS

__________ RPD

____ LIMITS _________ METHOD

_________________ Acenaphthene Acenaphthene 69 (47 - 104)

(47 - 104) SW846 8270C SW846 8270C 61 (47 - 104)

(47 - 104) 11

(0-40) SW846 8270C

SW846 8270C 1,2,4-Trichloro- 1,2,4-Trichloro- 62 (43 - 100)

(43 - 100) SW846 8270C SW846 8270C benzene 56 (43 - 100)

(43 - 100) 9.7

(0-36) SW846 8270C

SW846 8270C 1,4-Dichlorobenzene 1,4-Dichlorobenzene 62 (35 - 99)

(35 - 99) SW846 8270C SW846 8270C 54 (35 - 99)

(35 - 99) 13

(0-49) SW846 8270C

SW846 8270C 4-Bromophenyl phenyl 4-Bromophenyl phenyl 63 (47 - 110)

(47 - 110) SW846 8270C SW846 8270C ether 56 (47 - 110)

(47 - 110) 11

(0-46) SW846 8270C

SW846 8270C Butyl benzyl phthalate Butyl benzyl phthalate 68 (41 - 118)

(41 - 118) SW846 8270C SW846 8270C 63 (41 - 118)

(41 - 118) 7.4

(0-41) SW846 8270C

SW846 8270C 4-Chloro-3-methylphenol 4-Chloro-3-methylphenol 68 (47 - 109)

(47 - 109) SW846 8270C SW846 8270C 66 (47 - 109)

(47 - 109) 3.2

(0-36) SW846 8270C

SW846 8270C 2-Chlorophenol 2-Chlorophenol 65 (40 - 101)

(40 - 101) SW846 8270C SW846 8270C 57 (40 - 101)

(40 - 101) 13

(0-42) SW846 8270C

SW846 8270C 2,4-Dinitrotoluene 2,4-Dinitrotoluene 80 (45 - 124)

(45 - 124) SW846 8270C SW846 8270C 74 (45 - 124)

(45 - 124) 7.8

(0-41) SW846 8270C

SW846 8270C Hexachloroethane Hexachloroethane 61 (37 - 97)

(37 - 97) SW846 8270C SW846 8270C 53 (37 - 97)

(37 - 97) 14

(0-48) SW846 8270C

SW846 8270C 4-Methylphenol 4-Methylphenol 69 (42 - 105)

(42 - 105) SW846 8270C SW846 8270C 59 (42 - 105)

(42 - 105) 16

(0-43) SW846 8270C

SW846 8270C Naphthalene Naphthalene 65 (43 - 100)

(43 - 100) SW846 8270C SW846 8270C 61 (43 - 100)

(43 - 100) 6.8

(0-32) SW846 8270C

SW846 8270C 4-Nitrophenol 4-Nitrophenol 69 (36 - 127)

(36 - 127) SW846 8270C SW846 8270C 61 (36 - 127)

(36 - 127) 13

(0-43) SW846 8270C

SW846 8270C N-Nitrosodi-n-propyl- N-Nitrosodi-n-propyl- 70 (42 - 107)

(42 - 107) SW846 8270C SW846 8270C amine 59 (42 - 107)

(42 - 107) 17

(0-43) SW846 8270C

SW846 8270C Pentachlorophenol Pentachlorophenol 57 (17 - 122)

(17 - 122) SW846 8270C SW846 8270C 51 (17 - 122)

(17 - 122) 11

(0-52) SW846 8270C

SW846 8270C Phenol 60 (41 - 102)

(41 - 102) SW846 8270C SW846 8270C 55 (41 - 102)

(41 - 102) 8.6

(0-39) SW846 8270C

SW846 8270C Pyrene 64 (41 - 115)

(41 - 115) SW846 8270C SW846 8270C 59 (41 - 115)

(41 - 115) 6.8

(0-43) SW846 8270C

SW846 8270C (Continued on next page)



### C9K180557 96 of 161MATRIX SPIKE SAMPLE EVALUATION REPORT GC/MS Semivolatiles Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPPHK1A7-MS Matrix.........: Matrix.........: SOLID MS Lot-Sample #: MS Lot-Sample #: C9K180557-012 LPPHK1A8-MSD
PERCENT RECOVERY SURROGATE _________________________ RECOVERY ________ LIMITS

__________ 2,4,6-Tribromophenol 67 (35 - 124) 59 (35 - 124) 2-Fluorobiphenyl 68 (35 - 105) 60 (35 - 105) 2-Fluorophenol 74 (39 - 103) 65 (39 - 103) Nitrobenzene-d5 74 (25 - 104) 65 (25 - 104) Phenol-d5 72 (25 - 105) 63 (25 - 105) Terphenyl-d14 64 (25 - 127) 58 (25 - 127) NOTE(S):

___________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results. Bold print denotes control parameters Results and reporting limits have been adjusted for dry weight.



### C9K180557 97 of 161Clean Sites Environmental Services Inc Client Sample ID: MW-1S
TOTAL Metals Lot-Sample #...: Lot-Sample #...: C9K180557-001 Matrix.......: Matrix.......: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09
REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Prep Batch #...: Prep Batch #...: 9328355 Mercury ND 0.20 ug/L SW846 7470A 11/24/09 LPPF51A6 Dilution Factor: 1 Analysis Time..: 15:02 MS Run #.......: 9328186
Prep Batch #...: Prep Batch #...: 9331296 Silver ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPF51AF Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144 Aluminum Aluminum 1730

30.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51AG

LPPF51AG Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144 Arsenic ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPF51AH Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144 Barium 47.0

10.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51AJ

LPPF51AJ Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144 Beryllium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPF51AK Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144 Calcium Calcium 10500

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51AL

LPPF51AL Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144 Cadmium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPF51AM Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144 Cobalt 3.5

0.50

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51AN

LPPF51AN Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144 Chromium Chromium 6.5

2.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51AP

LPPF51AP Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144 Copper 2.5

2.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51AQ

LPPF51AQ Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144
Iron 1520

50.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51AR

LPPF51AR Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144 (Continued on next page)



### C9K180557 98 of 161Clean Sites Environmental Services Inc Client Sample ID: MW-1S
TOTAL Metals Lot-Sample #...: Lot-Sample #...: C9K180557-001 Matrix.........: Matrix.........: WATER

REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Potassium Potassium 995

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51AT

LPPF51AT Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144 Magnesium Magnesium 3140

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51AU

LPPF51AU Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144 Manganese Manganese 162

0.50

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51AV

LPPF51AV Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144 Sodium 3760

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51AW

LPPF51AW Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144 Nickel 2.6

1.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51AX

LPPF51AX Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144 Lead 1.4

1.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51A0

LPPF51A0 Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144 Selenium ND 5.0 ug/L SW846 6020 11/27-11/29/09 LPPF51A1 Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144 Thallium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPF51A2 Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144 Antimony ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPF51A3 Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144 Vanadium Vanadium 2.9

1.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51A4

LPPF51A4 Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144 Zinc 9.6

5.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51A5

LPPF51A5 Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144



### C9K180557 99 of 161Clean Sites Environmental Services Inc Client Sample ID: MW-3S
TOTAL Metals Lot-Sample #...: Lot-Sample #...: C9K180557-002 Matrix.......: Matrix.......: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09
REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Prep Batch #...: Prep Batch #...: 9328355 Mercury ND 0.20 ug/L SW846 7470A 11/24/09 LPPGN1AH Dilution Factor: 1 Analysis Time..: 15:07 MS Run #.......: 9328186
Prep Batch #...: Prep Batch #...: 9331296 Silver ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPGN1AN Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144 Aluminum Aluminum 2880

30.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1AP

LPPGN1AP Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144 Arsenic ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPGN1AQ Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144 Barium 134

10.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1AR

LPPGN1AR Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144 Beryllium Beryllium 2.2

1.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1AT

LPPGN1AT Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144 Calcium Calcium 8770

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1AU

LPPGN1AU Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144 Cadmium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPGN1AV Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144 Cobalt 4.1

0.50

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1AW

LPPGN1AW Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144 Chromium Chromium 6.4

2.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1AX

LPPGN1AX Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144 Copper 2.1

2.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1A0

LPPGN1A0 Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144
Iron 2280

50.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1A1

LPPGN1A1 Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144 (Continued on next page)



### C9K180557 100 of 161Clean Sites Environmental Services Inc Client Sample ID: MW-3S
TOTAL Metals Lot-Sample #...: Lot-Sample #...: C9K180557-002 Matrix.........: Matrix.........: WATER

REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Potassium Potassium 1240

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1A2

LPPGN1A2 Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144 Magnesium Magnesium 5900

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1A3

LPPGN1A3 Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144 Manganese Manganese 163

0.50

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1A4

LPPGN1A4 Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144 Sodium 4720

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1A5

LPPGN1A5 Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144 Nickel 3.9

1.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1A6

LPPGN1A6 Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144 Lead 2.0

1.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1AA

LPPGN1AA Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144 Selenium ND 5.0 ug/L SW846 6020 11/27-11/29/09 LPPGN1AC Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144 Thallium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPGN1AD Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144 Antimony ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPGN1AE Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144 Vanadium Vanadium 6.0

1.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1AF

LPPGN1AF Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144 Zinc 15.3

5.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1AG

LPPGN1AG Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144



### C9K180557 101 of 161Clean Sites Environmental Services Inc Client Sample ID: L2-S1
TOTAL Metals Lot-Sample #...: Lot-Sample #...: C9K180557-003 Matrix.......: Matrix.......: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09
REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Prep Batch #...: Prep Batch #...: 9328355 Mercury ND 0.20 ug/L SW846 7470A 11/24/09 LPPGP1AH Dilution Factor: 1 Analysis Time..: 15:10 MS Run #.......: 9328186
Prep Batch #...: Prep Batch #...: 9331296 Silver ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPGP1AN Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144 Aluminum Aluminum 2110

30.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1AP

LPPGP1AP Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144 Arsenic ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPGP1AQ Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144 Barium 95.4

10.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1AR

LPPGP1AR Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144 Beryllium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPGP1AT Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144 Calcium Calcium 4150

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1AU

LPPGP1AU Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144 Cadmium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPGP1AV Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144 Cobalt 2.9

0.50

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1AW

LPPGP1AW Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144 Chromium Chromium 7.1

2.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1AX

LPPGP1AX Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144 Copper ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPGP1A0 Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144
Iron 5950

50.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1A1

LPPGP1A1 Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144 (Continued on next page)



### C9K180557 102 of 161Clean Sites Environmental Services Inc Client Sample ID: L2-S1
TOTAL Metals Lot-Sample #...: Lot-Sample #...: C9K180557-003 Matrix.........: Matrix.........: WATER

REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Potassium Potassium 1040

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1A2

LPPGP1A2 Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144 Magnesium Magnesium 2420

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1A3

LPPGP1A3 Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144 Manganese Manganese 104

0.50

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1A4

LPPGP1A4 Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144 Sodium 4990

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1A5

LPPGP1A5 Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144 Nickel 4.2

1.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1A6

LPPGP1A6 Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144 Lead 1.3

1.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1AA

LPPGP1AA Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144 Selenium ND 5.0 ug/L SW846 6020 11/27-11/29/09 LPPGP1AC Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144 Thallium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPGP1AD Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144 Antimony ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPGP1AE Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144 Vanadium Vanadium 6.3

1.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1AF

LPPGP1AF Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144 Zinc 11.0

5.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1AG

LPPGP1AG Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144



### C9K180557 103 of 161Clean Sites Environmental Services Inc Client Sample ID: L1-S1
TOTAL Metals Lot-Sample #...: Lot-Sample #...: C9K180557-006 Matrix.......: Matrix.......: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09
REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Prep Batch #...: Prep Batch #...: 9328355 Mercury ND 0.20 ug/L SW846 7470A 11/24/09 LPPG11A5 Dilution Factor: 1 Analysis Time..: 15:12 MS Run #.......: 9328186
Prep Batch #...: Prep Batch #...: 9331296 Silver ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG11AE Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144 Aluminum Aluminum 486

30.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG11AF

LPPG11AF Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144 Arsenic ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG11AG Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144 Barium 18.7

10.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG11AH

LPPG11AH Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144 Beryllium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG11AJ Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144 Calcium Calcium 3930

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG11AK

LPPG11AK Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144 Cadmium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG11AL Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144 Cobalt 1.3

0.50

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG11AM

LPPG11AM Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144 Chromium Chromium 35.1

2.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG11AN

LPPG11AN Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144 Copper ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPG11AP Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144
Iron 922

50.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG11AQ

LPPG11AQ Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144 (Continued on next page)



### C9K180557 104 of 161Clean Sites Environmental Services Inc Client Sample ID: L1-S1
TOTAL Metals Lot-Sample #...: Lot-Sample #...: C9K180557-006 Matrix.........: Matrix.........: WATER

REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Potassium Potassium 633

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG11AR

LPPG11AR Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144 Magnesium Magnesium 2350

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG11AT

LPPG11AT Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144 Manganese Manganese 11.9

0.50

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG11AU

LPPG11AU Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144 Sodium 5830

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG11AV

LPPG11AV Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144 Nickel 5.1

1.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG11AW

LPPG11AW Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144 Lead ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG11AX Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144 Selenium ND 5.0 ug/L SW846 6020 11/27-11/29/09 LPPG11A0 Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144 Thallium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG11A1 Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144 Antimony ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPG11A2 Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144 Vanadium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG11A3 Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144 Zinc 7.7

5.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG11A4

LPPG11A4 Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144



### C9K180557 105 of 161Clean Sites Environmental Services Inc Client Sample ID: L1-S3
TOTAL Metals Lot-Sample #...: Lot-Sample #...: C9K180557-007 Matrix.......: Matrix.......: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09
REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Prep Batch #...: Prep Batch #...: 9328355 Mercury ND 0.20 ug/L SW846 7470A 11/24/09 LPPG61AG Dilution Factor: 1 Analysis Time..: 15:13 MS Run #.......: 9328186
Prep Batch #...: Prep Batch #...: 9331296 Silver ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG61AL Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144 Aluminum Aluminum 597

30.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61AM

LPPG61AM Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144 Arsenic Arsenic 1.9

1.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61AN

LPPG61AN Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144 Barium 65.4

10.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61AP

LPPG61AP Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144 Beryllium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG61AQ Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144 Calcium Calcium 31600

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61AR

LPPG61AR Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144 Cadmium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG61AT Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144 Cobalt 2.8

0.50

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61AU

LPPG61AU Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144 Chromium Chromium 3.0

2.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61AV

LPPG61AV Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144 Copper ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPG61AW Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144
Iron 10200

50.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61AX

LPPG61AX Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144 (Continued on next page)



### C9K180557 106 of 161Clean Sites Environmental Services Inc Client Sample ID: L1-S3
TOTAL Metals Lot-Sample #...: Lot-Sample #...: C9K180557-007 Matrix.........: Matrix.........: WATER

REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Potassium Potassium 2360

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61A0

LPPG61A0 Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144 Magnesium Magnesium 18500

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61A1

LPPG61A1 Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144 Manganese Manganese 277

0.50

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61A2

LPPG61A2 Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144 Sodium 4640

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61A3

LPPG61A3 Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144 Nickel 1.7

1.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61A4

LPPG61A4 Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144 Lead ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG61A5 Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144 Selenium ND 5.0 ug/L SW846 6020 11/27-11/29/09 LPPG61AA Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144 Thallium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG61AC Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144 Antimony ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPG61AD Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144 Vanadium Vanadium 2.2

1.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61AE

LPPG61AE Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144 Zinc 10.3

5.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61AF

LPPG61AF Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144



### C9K180557 107 of 161Clean Sites Environmental Services Inc Client Sample ID: L1-S4
TOTAL Metals Lot-Sample #...: Lot-Sample #...: C9K180557-008 Matrix.......: Matrix.......: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09
REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Prep Batch #...: Prep Batch #...: 9328355 Mercury ND 0.20 ug/L SW846 7470A 11/24/09 LPPG81AN Dilution Factor: 1 Analysis Time..: 15:16 MS Run #.......: 9328186
Prep Batch #...: Prep Batch #...: 9331296 Silver ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG81AT Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144 Aluminum Aluminum 145

30.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG81AU

LPPG81AU Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144 Arsenic ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG81AV Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144 Barium 33.6

10.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG81AW

LPPG81AW Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144 Beryllium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG81AX Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144 Calcium Calcium 45100

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG81A0

LPPG81A0 Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144 Cadmium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG81A1 Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144 Cobalt ND 0.50 ug/L SW846 6020 11/27-11/29/09 LPPG81A2 Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144 Chromium Chromium 3.9

2.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG81A3

LPPG81A3 Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144 Copper ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPG81A4 Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144
Iron 3420

50.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG81A5

LPPG81A5 Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144 (Continued on next page)



### C9K180557 108 of 161Clean Sites Environmental Services Inc Client Sample ID: L1-S4
TOTAL Metals Lot-Sample #...: Lot-Sample #...: C9K180557-008 Matrix.........: Matrix.........: WATER

REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Potassium Potassium 1910

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG81AA

LPPG81AA Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144 Magnesium Magnesium 3500

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG81AC

LPPG81AC Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144 Manganese Manganese 194

0.50

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG81AD

LPPG81AD Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144 Sodium 7050

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG81AE

LPPG81AE Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144 Nickel 3.1

1.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG81AF

LPPG81AF Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144 Lead ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG81AG Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144 Selenium ND 5.0 ug/L SW846 6020 11/27-11/29/09 LPPG81AH Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144 Thallium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG81AJ Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144 Antimony ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPG81AK Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144 Vanadium Vanadium 9.9

1.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG81AL

LPPG81AL Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144 Zinc 5.1

5.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG81AM

LPPG81AM Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144



### C9K180557 109 of 161Clean Sites Environmental Services Inc Client Sample ID: SW-1
TOTAL Metals Lot-Sample #...: Lot-Sample #...: C9K180557-009 Matrix.......: Matrix.......: WATER Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09
REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Prep Batch #...: Prep Batch #...: 9328355 Mercury ND 0.20 ug/L SW846 7470A 11/24/09 LPPHA1AV Dilution Factor: 1 Analysis Time..: 15:22 MS Run #.......: 9328186
Prep Batch #...: Prep Batch #...: 9331296 Silver ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHA1A1 Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144 Aluminum Aluminum 446

30.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1A2

LPPHA1A2 Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144 Arsenic ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHA1A3 Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144 Barium 65.8

10.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1A4

LPPHA1A4 Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144 Beryllium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHA1A5 Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144 Calcium Calcium 16500

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1AA

LPPHA1AA Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144 Cadmium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHA1AC Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144 Cobalt 1.1

0.50

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1AD

LPPHA1AD Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144 Chromium Chromium 4.1

2.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1AE

LPPHA1AE Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144 Copper ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPHA1AF Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144
Iron 1000

50.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1AG

LPPHA1AG Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144 (Continued on next page)



### C9K180557 110 of 161Clean Sites Environmental Services Inc Client Sample ID: SW-1
TOTAL Metals Lot-Sample #...: Lot-Sample #...: C9K180557-009 Matrix.........: Matrix.........: WATER

REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Potassium Potassium 3700

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1AH

LPPHA1AH Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144 Magnesium Magnesium 5120

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1AJ

LPPHA1AJ Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144 Manganese Manganese 102

0.50

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1AK

LPPHA1AK Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144 Sodium 6170

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1AL

LPPHA1AL Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144 Nickel 2.2

1.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1AM

LPPHA1AM Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144 Lead ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHA1AN Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144 Selenium ND 5.0 ug/L SW846 6020 11/27-11/29/09 LPPHA1AP Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144 Thallium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHA1AQ Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144 Antimony ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPHA1AR Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144 Vanadium Vanadium 2.5

1.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1AT

LPPHA1AT Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144 Zinc 15.4

5.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1AU

LPPHA1AU Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144



### C9K180557 111 of 161Clean Sites Environmental Services Inc Client Sample ID: SW-2
TOTAL Metals Lot-Sample #...: Lot-Sample #...: C9K180557-010 Matrix.......: Matrix.......: WATER Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09
REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Prep Batch #...: Prep Batch #...: 9328355 Mercury ND 0.20 ug/L SW846 7470A 11/24/09 LPPHF1A3 Dilution Factor: 1 Analysis Time..: 15:24 MS Run #.......: 9328186
Prep Batch #...: Prep Batch #...: 9331296 Silver ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHF1AC Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144 Aluminum Aluminum 448

30.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1AD

LPPHF1AD Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144 Arsenic ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHF1AE Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144 Barium 61.5

10.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1AF

LPPHF1AF Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144 Beryllium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHF1AG Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144 Calcium Calcium 16000

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1AH

LPPHF1AH Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144 Cadmium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHF1AJ Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144 Cobalt 0.98

0.50

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1AK

LPPHF1AK Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144 Chromium Chromium 3.7

2.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1AL

LPPHF1AL Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144 Copper ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPHF1AM Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144
Iron 994

50.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1AN

LPPHF1AN Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144 (Continued on next page)



### C9K180557 112 of 161Clean Sites Environmental Services Inc Client Sample ID: SW-2
TOTAL Metals Lot-Sample #...: Lot-Sample #...: C9K180557-010 Matrix.........: Matrix.........: WATER

REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Potassium Potassium 3480

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1AP

LPPHF1AP Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144 Magnesium Magnesium 5120

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1AQ

LPPHF1AQ Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144 Manganese Manganese 89.9

0.50

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1AR

LPPHF1AR Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144 Sodium 5850

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1AT

LPPHF1AT Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144 Nickel 2.1

1.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1AU

LPPHF1AU Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144 Lead ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHF1AV Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144 Selenium ND 5.0 ug/L SW846 6020 11/27-11/29/09 LPPHF1AW Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144 Thallium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHF1AX Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144 Antimony ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPHF1A0 Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144 Vanadium Vanadium 1.9

1.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1A1

LPPHF1A1 Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144 Zinc 11.4

5.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1A2

LPPHF1A2 Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144



### C9K180557 113 of 161Clean Sites Environmental Services Inc Client Sample ID: SW-3
TOTAL Metals Lot-Sample #...: Lot-Sample #...: C9K180557-011 Matrix.......: Matrix.......: WATER Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09
REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Prep Batch #...: Prep Batch #...: 9328355 Mercury ND 0.20 ug/L SW846 7470A 11/24/09 LPPHG1A3 Dilution Factor: 1 Analysis Time..: 15:25 MS Run #.......: 9328186
Prep Batch #...: Prep Batch #...: 9331296 Silver ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHG1AC Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144 Aluminum Aluminum 415

30.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1AD

LPPHG1AD Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144 Arsenic ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHG1AE Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144 Barium 60.0

10.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1AF

LPPHG1AF Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144 Beryllium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHG1AG Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144 Calcium Calcium 16300

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1AH

LPPHG1AH Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144 Cadmium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHG1AJ Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144 Cobalt 0.91

0.50

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1AK

LPPHG1AK Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144 Chromium Chromium 3.9

2.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1AL

LPPHG1AL Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144 Copper ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPHG1AM Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144
Iron 1040

50.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1AN

LPPHG1AN Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144 (Continued on next page)



### C9K180557 114 of 161Clean Sites Environmental Services Inc Client Sample ID: SW-3
TOTAL Metals Lot-Sample #...: Lot-Sample #...: C9K180557-011 Matrix.........: Matrix.........: WATER

REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Potassium Potassium 3440

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1AP

LPPHG1AP Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144 Magnesium Magnesium 5140

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1AQ

LPPHG1AQ Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144 Manganese Manganese 92.2

0.50

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1AR

LPPHG1AR Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144 Sodium 5700

100

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1AT

LPPHG1AT Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144 Nickel 2.1

1.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1AU

LPPHG1AU Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144 Lead ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHG1AV Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144 Selenium ND 5.0 ug/L SW846 6020 11/27-11/29/09 LPPHG1AW Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144 Thallium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHG1AX Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144 Antimony ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPHG1A0 Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144 Vanadium Vanadium 2.5

1.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1A1

LPPHG1A1 Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144 Zinc 12.2

5.0

ug/L

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1A2

LPPHG1A2 Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144



### C9K180557 115 of 161Clean Sites Environmental Services Inc Client Sample ID: SED-1
TOTAL Metals Lot-Sample #...: Lot-Sample #...: C9K180557-012 Matrix.......: Matrix.......: SOLID Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 % Moisture.....: % Moisture.....: 20
REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Prep Batch #...: Prep Batch #...: 9327175 Mercury ND 0.041 mg/kg SW846 7471A 11/23/09 LPPHK1A6 Dilution Factor: 1 Analysis Time..: 17:57 MS Run #.......: 9327086
Prep Batch #...: Prep Batch #...: 9331299 Silver ND 0.12 mg/kg SW846 6020 11/27-11/29/09 LPPHK1AF Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147 Aluminum Aluminum 1470

3.7

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AG

LPPHK1AG Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147 Arsenic Arsenic 0.17

0.12

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AH

LPPHK1AH Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147 Barium 14.5

1.2

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AJ

LPPHK1AJ Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147 Beryllium Beryllium 0.75

0.12

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AK

LPPHK1AK Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147 Calcium Calcium 885

12.4

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AL

LPPHK1AL Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147 Cadmium ND 0.12 mg/kg SW846 6020 11/27-11/29/09 LPPHK1AM Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147 Cobalt 3.5

0.062

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AN

LPPHK1AN Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147 Chromium Chromium 2.4

0.25

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AP

LPPHK1AP Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147 Copper 0.60

0.25

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AQ

LPPHK1AQ Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147
Iron 10900

6.2

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AR

LPPHK1AR Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147 (Continued on next page)



### C9K180557 116 of 161Clean Sites Environmental Services Inc Client Sample ID: SED-1
TOTAL Metals Lot-Sample #...: Lot-Sample #...: C9K180557-012 Matrix.........: Matrix.........: SOLID

REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Potassium Potassium 72.9

12.4

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AT

LPPHK1AT Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147 Magnesium Magnesium 293

12.4

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AU

LPPHK1AU Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147 Manganese Manganese 94.5

0.062

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AV

LPPHK1AV Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147 Sodium 29.3

12.4

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AW

LPPHK1AW Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147 Nickel 1.2

0.12

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AX

LPPHK1AX Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147 Lead 2.1

0.12

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1A0

LPPHK1A0 Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147 Selenium ND 0.62 mg/kg SW846 6020 11/27-11/29/09 LPPHK1A1 Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147 Thallium ND 0.12 mg/kg SW846 6020 11/27-11/29/09 LPPHK1A2 Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147 Antimony ND 0.25 mg/kg SW846 6020 11/27-11/29/09 LPPHK1A3 Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147 Vanadium Vanadium 4.6

0.12

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1A4

LPPHK1A4 Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147 Zinc 16.8

0.62

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1A5

LPPHK1A5 Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147 NOTE(S):

___________________________________________________________________________________________ Results and reporting limits have been adjusted for dry weight.



### C9K180557 117 of 161Clean Sites Environmental Services Inc Client Sample ID: SED-2
TOTAL Metals Lot-Sample #...: Lot-Sample #...: C9K180557-013 Matrix.......: Matrix.......: SOLID Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 % Moisture.....: % Moisture.....: 20
REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Prep Batch #...: Prep Batch #...: 9327175 Mercury ND 0.041 mg/kg SW846 7471A 11/23/09 LPPHM1AH Dilution Factor: 1 Analysis Time..: 18:03 MS Run #.......: 9327086
Prep Batch #...: Prep Batch #...: 9331299 Silver ND 0.12 mg/kg SW846 6020 11/27-11/29/09 LPPHM1AN Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147 Aluminum Aluminum 1080

3.7

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1AP

LPPHM1AP Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147 Arsenic Arsenic 0.43

0.12

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1AQ

LPPHM1AQ Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147 Barium 12.5

1.2

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1AR

LPPHM1AR Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147 Beryllium ND 0.12 mg/kg SW846 6020 11/27-11/29/09 LPPHM1AT Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147 Calcium Calcium 386

12.5

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1AU

LPPHM1AU Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147 Cadmium ND 0.12 mg/kg SW846 6020 11/27-11/29/09 LPPHM1AV Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147 Cobalt 0.93

0.062

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1AW

LPPHM1AW Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147 Chromium Chromium 2.2

0.25

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1AX

LPPHM1AX Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147 Copper 0.47

0.25

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1A0

LPPHM1A0 Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147
Iron 2430

6.2

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1A1

LPPHM1A1 Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147 (Continued on next page)



### C9K180557 118 of 161Clean Sites Environmental Services Inc Client Sample ID: SED-2
TOTAL Metals Lot-Sample #...: Lot-Sample #...: C9K180557-013 Matrix.........: Matrix.........: SOLID

REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Potassium Potassium 82.5

12.5

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1A2

LPPHM1A2 Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147 Magnesium Magnesium 121

12.5

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1A3

LPPHM1A3 Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147 Manganese Manganese 32.0

0.062

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1A4

LPPHM1A4 Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147 Sodium 25.9

12.5

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1A5

LPPHM1A5 Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147 Nickel 0.75

0.12

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1A6

LPPHM1A6 Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147 Lead 2.1

0.12

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1AA

LPPHM1AA Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147 Selenium ND 0.62 mg/kg SW846 6020 11/27-11/29/09 LPPHM1AC Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147 Thallium ND 0.12 mg/kg SW846 6020 11/27-11/29/09 LPPHM1AD Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147 Antimony ND 0.25 mg/kg SW846 6020 11/27-11/29/09 LPPHM1AE Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147 Vanadium Vanadium 2.7

0.12

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1AF

LPPHM1AF Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147 Zinc 10.2

0.62

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1AG

LPPHM1AG Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147 NOTE(S):

___________________________________________________________________________________________ Results and reporting limits have been adjusted for dry weight.



### C9K180557 119 of 161Clean Sites Environmental Services Inc Client Sample ID: SED-3
TOTAL Metals Lot-Sample #...: Lot-Sample #...: C9K180557-014 Matrix.......: Matrix.......: SOLID Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 % Moisture.....: % Moisture.....: 23
REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Prep Batch #...: Prep Batch #...: 9327175 Mercury ND 0.043 mg/kg SW846 7471A 11/23/09 LPPHN1AQ Dilution Factor: 1 Analysis Time..: 18:09 MS Run #.......: 9327086
Prep Batch #...: Prep Batch #...: 9331299 Silver ND 0.13 mg/kg SW846 6020 11/27-11/29/09 LPPHN1AW Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147 Aluminum Aluminum 2080

3.9

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1AX

LPPHN1AX Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147 Arsenic Arsenic 0.28

0.13

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1A0

LPPHN1A0 Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147 Barium 23.0

1.3

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1A1

LPPHN1A1 Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147 Beryllium Beryllium 0.19

0.13

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1A2

LPPHN1A2 Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147 Calcium Calcium 631

12.9

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1A3

LPPHN1A3 Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147 Cadmium ND 0.13 mg/kg SW846 6020 11/27-11/29/09 LPPHN1A4 Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147 Cobalt 1.6

0.065

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1A5

LPPHN1A5 Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147 Chromium Chromium 3.3

0.26

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1A6

LPPHN1A6 Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147 Copper 0.78

0.26

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1AA

LPPHN1AA Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147
Iron 2780

6.5

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1AC

LPPHN1AC Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147 (Continued on next page)



### C9K180557 120 of 161Clean Sites Environmental Services Inc Client Sample ID: SED-3
TOTAL Metals Lot-Sample #...: Lot-Sample #...: C9K180557-014 Matrix.........: Matrix.........: SOLID

REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Potassium Potassium 114

12.9

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1AD

LPPHN1AD Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147 Magnesium Magnesium 252

12.9

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1AE

LPPHN1AE Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147 Manganese Manganese 57.5

0.065

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1AF

LPPHN1AF Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147 Sodium 29.9

12.9

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1AG

LPPHN1AG Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147 Nickel 1.3

0.13

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1AH

LPPHN1AH Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147 Lead 3.1

0.13

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1AJ

LPPHN1AJ Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147 Selenium ND 0.65 mg/kg SW846 6020 11/27-11/29/09 LPPHN1AK Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147 Thallium ND 0.13 mg/kg SW846 6020 11/27-11/29/09 LPPHN1AL Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147 Antimony ND 0.26 mg/kg SW846 6020 11/27-11/29/09 LPPHN1AM Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147 Vanadium Vanadium 2.5

0.13

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1AN

LPPHN1AN Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147 Zinc 16.0

0.65

mg/kg

SW846 6020

SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1AP

LPPHN1AP Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147 NOTE(S):

___________________________________________________________________________________________ Results and reporting limits have been adjusted for dry weight.



### C9K180557 121 of 161METHOD BLANK REPORT TOTAL Metals Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: SOLID
REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ MB Lot-Sample #: MB Lot-Sample #: C9K230000-175 Prep Batch #...: Prep Batch #...: 9327175 Mercury ND 0.033 mg/kg SW846 7471A 11/23/09 LP05J1AA Dilution Factor: 1 Analysis Time..: 17:40

MB Lot-Sample #: MB Lot-Sample #: C9K270000-299 Prep Batch #...: Prep Batch #...: 9331299 Silver ND 0.10 mg/kg SW846 6020 11/27-11/29/09 LP72P1AA Dilution Factor: 1 Analysis Time..: 01:42 Aluminum ND 3.0 mg/kg SW846 6020 11/27-11/29/09 LP72P1AC Dilution Factor: 1 Analysis Time..: 01:42 Arsenic ND 0.10 mg/kg SW846 6020 11/27-11/29/09 LP72P1AD Dilution Factor: 1 Analysis Time..: 01:42 Barium ND 1.0 mg/kg SW846 6020 11/27-11/29/09 LP72P1AE Dilution Factor: 1 Analysis Time..: 01:42 Beryllium ND 0.10 mg/kg SW846 6020 11/27-11/29/09 LP72P1AF Dilution Factor: 1 Analysis Time..: 01:42 Calcium ND 10.0 mg/kg SW846 6020 11/27-11/29/09 LP72P1AG Dilution Factor: 1 Analysis Time..: 01:42 Cadmium ND 0.10 mg/kg SW846 6020 11/27-11/29/09 LP72P1AH Dilution Factor: 1 Analysis Time..: 01:42 Cobalt ND 0.050 mg/kg SW846 6020 11/27-11/29/09 LP72P1AJ Dilution Factor: 1 Analysis Time..: 01:42 Chromium ND 0.20 mg/kg SW846 6020 11/27-11/29/09 LP72P1AK Dilution Factor: 1 Analysis Time..: 01:42 (Continued on next page)



### C9K180557 122 of 161METHOD BLANK REPORT TOTAL Metals Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: SOLID
REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Copper ND 0.20 mg/kg SW846 6020 11/27-11/29/09 LP72P1AL Dilution Factor: 1 Analysis Time..: 01:42 Iron ND 5.0 mg/kg SW846 6020 11/27-11/29/09 LP72P1AM Dilution Factor: 1 Analysis Time..: 01:42 Potassium ND 10.0 mg/kg SW846 6020 11/27-11/29/09 LP72P1AN Dilution Factor: 1 Analysis Time..: 01:42 Magnesium ND 10.0 mg/kg SW846 6020 11/27-11/29/09 LP72P1AP Dilution Factor: 1 Analysis Time..: 01:42 Manganese ND 0.050 mg/kg SW846 6020 11/27-11/29/09 LP72P1AQ Dilution Factor: 1 Analysis Time..: 01:42 Sodium ND 10.0 mg/kg SW846 6020 11/27-11/29/09 LP72P1AR Dilution Factor: 1 Analysis Time..: 01:42 Nickel ND 0.10 mg/kg SW846 6020 11/27-11/29/09 LP72P1AT Dilution Factor: 1 Analysis Time..: 01:42 Lead ND 0.10 mg/kg SW846 6020 11/27-11/29/09 LP72P1AU Dilution Factor: 1 Analysis Time..: 01:42 Selenium ND 0.50 mg/kg SW846 6020 11/27-11/29/09 LP72P1AV Dilution Factor: 1 Analysis Time..: 01:42 Thallium ND 0.10 mg/kg SW846 6020 11/27-11/29/09 LP72P1AW Dilution Factor: 1 Analysis Time..: 01:42 Antimony ND 0.20 mg/kg SW846 6020 11/27-11/29/09 LP72P1AX Dilution Factor: 1 Analysis Time..: 01:42 Vanadium ND 0.10 mg/kg SW846 6020 11/27-11/29/09 LP72P1A0 Dilution Factor: 1 Analysis Time..: 01:42 (Continued on next page)



### C9K180557 123 of 161METHOD BLANK REPORT TOTAL Metals Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: SOLID
REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Zinc ND 0.50 mg/kg SW846 6020 11/27-11/29/09 LP72P1A1 Dilution Factor: 1 Analysis Time..: 01:42 NOTE(S):

____________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results.



### C9K180557 124 of 161METHOD BLANK REPORT TOTAL Metals Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: WATER
REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ MB Lot-Sample #: MB Lot-Sample #: C9K240000-355 Prep Batch #...: Prep Batch #...: 9328355 Mercury ND 0.20 ug/L SW846 7470A 11/24/09 LP2861AA Dilution Factor: 1 Analysis Time..: 14:58

MB Lot-Sample #: MB Lot-Sample #: C9K270000-296 Prep Batch #...: Prep Batch #...: 9331296 Silver ND 1.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AA Dilution Factor: 1 Analysis Time..: 00:25 Aluminum ND 30.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AC Dilution Factor: 1 Analysis Time..: 00:25 Arsenic ND 1.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AD Dilution Factor: 1 Analysis Time..: 00:25 Barium ND 10.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AE Dilution Factor: 1 Analysis Time..: 00:25 Beryllium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AF Dilution Factor: 1 Analysis Time..: 00:25 Calcium ND 100 ug/L SW846 6020 11/27-11/29/09 LP72G1AG Dilution Factor: 1 Analysis Time..: 00:25 Cadmium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AH Dilution Factor: 1 Analysis Time..: 00:25 Cobalt ND 0.50 ug/L SW846 6020 11/27-11/29/09 LP72G1AJ Dilution Factor: 1 Analysis Time..: 00:25 Chromium ND 2.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AK Dilution Factor: 1 Analysis Time..: 00:25 (Continued on next page)



### C9K180557 125 of 161METHOD BLANK REPORT TOTAL Metals Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: WATER
REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Copper ND 2.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AL Dilution Factor: 1 Analysis Time..: 00:25 Iron ND 50.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AM Dilution Factor: 1 Analysis Time..: 00:25 Potassium ND 100 ug/L SW846 6020 11/27-11/29/09 LP72G1AN Dilution Factor: 1 Analysis Time..: 00:25 Magnesium ND 100 ug/L SW846 6020 11/27-11/29/09 LP72G1AP Dilution Factor: 1 Analysis Time..: 00:25 Manganese ND 0.50 ug/L SW846 6020 11/27-11/29/09 LP72G1AQ Dilution Factor: 1 Analysis Time..: 00:25 Sodium ND 100 ug/L SW846 6020 11/27-11/29/09 LP72G1AR Dilution Factor: 1 Analysis Time..: 00:25 Nickel ND 1.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AT Dilution Factor: 1 Analysis Time..: 00:25 Lead ND 1.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AU Dilution Factor: 1 Analysis Time..: 00:25 Selenium ND 5.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AV Dilution Factor: 1 Analysis Time..: 00:25 Thallium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AW Dilution Factor: 1 Analysis Time..: 00:25 Antimony ND 2.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AX Dilution Factor: 1 Analysis Time..: 00:25 Vanadium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LP72G1A0 Dilution Factor: 1 Analysis Time..: 00:25 (Continued on next page)



### C9K180557 126 of 161METHOD BLANK REPORT TOTAL Metals Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: WATER
REPORTING PREPARATION- WORK PARAMETER _______________ RESULT

_____________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

________ Zinc ND 5.0 ug/L SW846 6020 11/27-11/29/09 LP72G1A1 Dilution Factor: 1 Analysis Time..: 00:25 NOTE(S):

____________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results.



### C9K180557 127 of 161LABORATORY CONTROL SAMPLE EVALUATION REPORT TOTAL Metals Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: SOLID
PERCENT RECOVERY PREPARATIONPARAMETER ___________ RECOVERY ________ LIMITS

__________ METHOD

_________________ ANALYSIS DATE ______________ WORK ORDER #

____________ LCS Lot-Sample#: LCS Lot-Sample#: C9K230000-175 Prep Batch #...: Prep Batch #...: 9327175 Mercury 99 (80 - 120) SW846 7471A 11/23/09 LP05J1AC Dilution Factor: 1 Analysis Time..: 17:46 LCS Lot-Sample#: LCS Lot-Sample#: C9K270000-299 Prep Batch #...: Prep Batch #...: 9331299 Silver 98 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1A2 Dilution Factor: 1 Analysis Time..: 01:46 Aluminum 107 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1A3 Dilution Factor: 1 Analysis Time..: 01:46 Arsenic 87 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1A4 Dilution Factor: 1 Analysis Time..: 01:46 Barium 93 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1A5 Dilution Factor: 1 Analysis Time..: 01:46 Beryllium 83 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1A6 Dilution Factor: 1 Analysis Time..: 01:46 Calcium 99 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1A7 Dilution Factor: 1 Analysis Time..: 01:46 Cadmium 95 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1A8 Dilution Factor: 1 Analysis Time..: 01:46 Cobalt 86 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1A9 Dilution Factor: 1 Analysis Time..: 01:46 Chromium 96 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CA Dilution Factor: 1 Analysis Time..: 01:46 Copper 87 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CC Dilution Factor: 1 Analysis Time..: 01:46 Iron 97 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CD Dilution Factor: 1 Analysis Time..: 01:46 Potassium 87 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CE Dilution Factor: 1 Analysis Time..: 01:46 (Continued on next page)



### C9K180557 128 of 161LABORATORY CONTROL SAMPLE EVALUATION REPORT TOTAL Metals Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: SOLID
PERCENT RECOVERY PREPARATIONPARAMETER ___________ RECOVERY ________ LIMITS

__________ METHOD

_________________ ANALYSIS DATE ______________ WORK ORDER #

____________ Magnesium 108 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CF Dilution Factor: 1 Analysis Time..: 01:46 Manganese 93 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CG Dilution Factor: 1 Analysis Time..: 01:46 Sodium 83 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CH Dilution Factor: 1 Analysis Time..: 01:46 Nickel 84 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CJ Dilution Factor: 1 Analysis Time..: 01:46 Lead 107 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CK Dilution Factor: 1 Analysis Time..: 01:46 Selenium 98 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CL Dilution Factor: 1 Analysis Time..: 01:46 Thallium 104 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CM Dilution Factor: 1 Analysis Time..: 01:46 Antimony 95 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CN Dilution Factor: 1 Analysis Time..: 01:46 Vanadium 96 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CP Dilution Factor: 1 Analysis Time..: 01:46 Zinc 87 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CQ Dilution Factor: 1 Analysis Time..: 01:46 NOTE(S):

____________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results.



### C9K180557 129 of 161LABORATORY CONTROL SAMPLE EVALUATION REPORT TOTAL Metals Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: WATER
PERCENT RECOVERY PREPARATIONPARAMETER ___________ RECOVERY ________ LIMITS

__________ METHOD

_________________ ANALYSIS DATE ______________ WORK ORDER #

____________ LCS Lot-Sample#: LCS Lot-Sample#: C9K240000-355 Prep Batch #...: Prep Batch #...: 9328355 Mercury 108 (80 - 120) SW846 7470A 11/24/09 LP2861AC Dilution Factor: 1 Analysis Time..: 15:00 LCS Lot-Sample#: LCS Lot-Sample#: C9K270000-296 Prep Batch #...: Prep Batch #...: 9331296 Silver 97 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1A2 Dilution Factor: 1 Analysis Time..: 00:30 Aluminum 106 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1A3 Dilution Factor: 1 Analysis Time..: 00:30 Arsenic 91 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1A4 Dilution Factor: 1 Analysis Time..: 00:30 Barium 93 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1A5 Dilution Factor: 1 Analysis Time..: 00:30 Beryllium 86 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1A6 Dilution Factor: 1 Analysis Time..: 00:30 Calcium 99 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1A7 Dilution Factor: 1 Analysis Time..: 00:30 Cadmium 94 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1A8 Dilution Factor: 1 Analysis Time..: 00:30 Cobalt 86 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1A9 Dilution Factor: 1 Analysis Time..: 00:30 Chromium 95 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CA Dilution Factor: 1 Analysis Time..: 00:30 Copper 87 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CC Dilution Factor: 1 Analysis Time..: 00:30 Iron 97 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CD Dilution Factor: 1 Analysis Time..: 00:30 Potassium 88 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CE Dilution Factor: 1 Analysis Time..: 00:30 (Continued on next page)



### C9K180557 130 of 161LABORATORY CONTROL SAMPLE EVALUATION REPORT TOTAL Metals Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: WATER
PERCENT RECOVERY PREPARATIONPARAMETER ___________ RECOVERY ________ LIMITS

__________ METHOD

_________________ ANALYSIS DATE ______________ WORK ORDER #

____________ Magnesium 106 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CF Dilution Factor: 1 Analysis Time..: 00:30 Manganese 93 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CG Dilution Factor: 1 Analysis Time..: 00:30 Sodium 83 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CH Dilution Factor: 1 Analysis Time..: 00:30 Nickel 84 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CJ Dilution Factor: 1 Analysis Time..: 00:30 Lead 105 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CK Dilution Factor: 1 Analysis Time..: 00:30 Selenium 101 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CL Dilution Factor: 1 Analysis Time..: 00:30 Thallium 102 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CM Dilution Factor: 1 Analysis Time..: 00:30 Antimony 95 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CN Dilution Factor: 1 Analysis Time..: 00:30 Vanadium 96 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CP Dilution Factor: 1 Analysis Time..: 00:30 Zinc 88 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CQ Dilution Factor: 1 Analysis Time..: 00:30 NOTE(S):

____________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results.



### C9K180557 131 of 161MATRIX SPIKE SAMPLE EVALUATION REPORT TOTAL Metals Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09
PERCENT RECOVERY RPD PREPARATION- WORK PARAMETER ___________ RECOVERY

________ LIMITS

__________ RPD

____ LIMITS ______ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

_______ MS Lot-Sample #: MS Lot-Sample #: C9K180557-001 Prep Batch #...: Prep Batch #...: 9328355 Mercury 106 (75 - 125) SW846 7470A 11/24/09 LPPF51A7

107 (75 - 125) 0.93 (0-20) SW846 7470A 11/24/09 LPPF51A8 Dilution Factor: 1 Analysis Time..: 15:04 MS Run #.......: 9328186
MS Lot-Sample #: MS Lot-Sample #: C9K180557-001 Prep Batch #...: Prep Batch #...: 9331296 Silver 100 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51CC

99 (75 - 125) 1.2 (0-20) SW846 6020 11/27-11/29/09 LPPF51CD Dilution Factor: 1 Analysis Time..: 00:42 MS Run #.......: 9331144 Aluminum 135 N (75 - 125) SW846 6020 11/27-11/29/09 LPPF51CE

137 N (75 - 125) 0.87 (0-20) SW846 6020 11/27-11/29/09 LPPF51CF Dilution Factor: 1 Analysis Time..: 00:42 MS Run #.......: 9331144 Arsenic 89 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51CG

88 (75 - 125) 0.81 (0-20) SW846 6020 11/27-11/29/09 LPPF51CH Dilution Factor: 1 Analysis Time..: 00:42 MS Run #.......: 9331144 Barium 96 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51CJ

95 (75 - 125) 0.92 (0-20) SW846 6020 11/27-11/29/09 LPPF51CK Dilution Factor: 1 Analysis Time..: 00:42 MS Run #.......: 9331144 Beryllium 84 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51CL

81 (75 - 125) 3.6 (0-20) SW846 6020 11/27-11/29/09 LPPF51CM Dilution Factor: 1 Analysis Time..: 00:42 MS Run #.......: 9331144 Calcium 98 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51CN

97 (75 - 125) 0.59 (0-20) SW846 6020 11/27-11/29/09 LPPF51CP Dilution Factor: 1 Analysis Time..: 00:42 MS Run #.......: 9331144 (Continued on next page)



### C9K180557 132 of 161MATRIX SPIKE SAMPLE EVALUATION REPORT TOTAL Metals Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09
PERCENT RECOVERY RPD PREPARATION- WORK PARAMETER ___________ RECOVERY

________ LIMITS

__________ RPD

____ LIMITS ______ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

_______ Cadmium 97 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51CQ

97 (75 - 125) 0.12 (0-20) SW846 6020 11/27-11/29/09 LPPF51CR Dilution Factor: 1 Analysis Time..: 00:42 MS Run #.......: 9331144 Cobalt 84 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51CT

84 (75 - 125) 0.82 (0-20) SW846 6020 11/27-11/29/09 LPPF51CU Dilution Factor: 1 Analysis Time..: 00:42 MS Run #.......: 9331144 Chromium 92 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51CV

91 (75 - 125) 0.58 (0-20) SW846 6020 11/27-11/29/09 LPPF51CW Dilution Factor: 1 Analysis Time..: 00:42 MS Run #.......: 9331144 Copper 85 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51CX

84 (75 - 125) 1.1 (0-20) SW846 6020 11/27-11/29/09 LPPF51C0 Dilution Factor: 1 Analysis Time..: 00:42 MS Run #.......: 9331144 Iron 93 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51C1

92 (75 - 125) 0.61 (0-20) SW846 6020 11/27-11/29/09 LPPF51C2 Dilution Factor: 1 Analysis Time..: 00:42 MS Run #.......: 9331144 Potassium 86 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51C3

86 (75 - 125) 0.56 (0-20) SW846 6020 11/27-11/29/09 LPPF51C4 Dilution Factor: 1 Analysis Time..: 00:42 MS Run #.......: 9331144 Magnesium 105 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51C5

105 (75 - 125) 0.23 (0-20) SW846 6020 11/27-11/29/09 LPPF51C6 Dilution Factor: 1 Analysis Time..: 00:42 MS Run #.......: 9331144 (Continued on next page)



### C9K180557 133 of 161MATRIX SPIKE SAMPLE EVALUATION REPORT TOTAL Metals Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09
PERCENT RECOVERY RPD PREPARATION- WORK PARAMETER ___________ RECOVERY

________ LIMITS

__________ RPD

____ LIMITS ______ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

_______ Manganese 90 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51C7

90 (75 - 125) 0.45 (0-20) SW846 6020 11/27-11/29/09 LPPF51C8 Dilution Factor: 1 Analysis Time..: 00:42 MS Run #.......: 9331144 Sodium 81 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51C9

81 (75 - 125) 0.51 (0-20) SW846 6020 11/27-11/29/09 LPPF51DA Dilution Factor: 1 Analysis Time..: 00:42 MS Run #.......: 9331144 Nickel 82 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51DC

97 (75 - 125) 17 (0-20) SW846 6020 11/27-11/29/09 LPPF51DD Dilution Factor: 1 Analysis Time..: 00:42 MS Run #.......: 9331144 Lead 109 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51DE

109 (75 - 125) 0.64 (0-20) SW846 6020 11/27-11/29/09 LPPF51DF Dilution Factor: 1 Analysis Time..: 00:42 MS Run #.......: 9331144 Selenium 93 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51DG

94 (75 - 125) 1.1 (0-20) SW846 6020 11/27-11/29/09 LPPF51DH Dilution Factor: 1 Analysis Time..: 00:42 MS Run #.......: 9331144 Thallium 106 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51DJ

105 (75 - 125) 0.11 (0-20) SW846 6020 11/27-11/29/09 LPPF51DK Dilution Factor: 1 Analysis Time..: 00:42 MS Run #.......: 9331144 Antimony 99 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51DL

99 (75 - 125) 0.30 (0-20) SW846 6020 11/27-11/29/09 LPPF51DM Dilution Factor: 1 Analysis Time..: 00:42 MS Run #.......: 9331144 (Continued on next page)



### C9K180557 134 of 161MATRIX SPIKE SAMPLE EVALUATION REPORT TOTAL Metals Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09
PERCENT RECOVERY RPD PREPARATION- WORK PARAMETER ___________ RECOVERY

________ LIMITS

__________ RPD

____ LIMITS ______ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

_______ Vanadium 95 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51DN

94 (75 - 125) 0.33 (0-20) SW846 6020 11/27-11/29/09 LPPF51DP Dilution Factor: 1 Analysis Time..: 00:42 MS Run #.......: 9331144 Zinc 84 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51DQ

84 (75 - 125) 0.23 (0-20) SW846 6020 11/27-11/29/09 LPPF51DR Dilution Factor: 1 Analysis Time..: 00:42 MS Run #.......: 9331144 NOTE(S):

____________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results. N Spiked analyte recovery is outside stated control limits.



### C9K180557 135 of 161MATRIX SPIKE SAMPLE EVALUATION REPORT TOTAL Metals Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: SOLID Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09
PERCENT RECOVERY RPD PREPARATION- WORK PARAMETER ___________ RECOVERY

________ LIMITS

__________ RPD

____ LIMITS ______ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

_______ MS Lot-Sample #: MS Lot-Sample #: C9K180557-012 Prep Batch #...: Prep Batch #...: 9327175 % Moisture.....: % Moisture.....: 20 Mercury 107 (75 - 125) SW846 7471A 11/23/09 LPPHK1CD

106 (75 - 125) 0.93 (0-20) SW846 7471A 11/23/09 LPPHK1CE Dilution Factor: 1 Analysis Time..: 17:59 MS Run #.......: 9327086
MS Lot-Sample #: MS Lot-Sample #: C9K180557-012 Prep Batch #...: Prep Batch #...: 9331299 % Moisture.....: % Moisture.....: 20 Silver 95 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1CF

96 (75 - 125) 1.3 (0-20) SW846 6020 11/27-11/29/09 LPPHK1CG Dilution Factor: 1 Analysis Time..: 02:13 MS Run #.......: 9331147 Aluminum NC (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1CH

NC (75 - 125) (0-20) SW846 6020 11/27-11/29/09 LPPHK1CJ Dilution Factor: 1 Analysis Time..: 02:13 MS Run #.......: 9331147 Arsenic 83 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1CK

86 (75 - 125) 4.1 (0-20) SW846 6020 11/27-11/29/09 LPPHK1CL Dilution Factor: 1 Analysis Time..: 02:13 MS Run #.......: 9331147 Barium 90 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1CM

92 (75 - 125) 2.0 (0-20) SW846 6020 11/27-11/29/09 LPPHK1CN Dilution Factor: 1 Analysis Time..: 02:13 MS Run #.......: 9331147 Beryllium 71 N (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1CP

76 (75 - 125) 5.7 (0-20) SW846 6020 11/27-11/29/09 LPPHK1CQ Dilution Factor: 1 Analysis Time..: 02:13 MS Run #.......: 9331147 (Continued on next page)



### C9K180557 136 of 161MATRIX SPIKE SAMPLE EVALUATION REPORT TOTAL Metals Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: SOLID Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09
PERCENT RECOVERY RPD PREPARATION- WORK PARAMETER ___________ RECOVERY

________ LIMITS

__________ RPD

____ LIMITS ______ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

_______ Calcium 85 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1CR

91 (75 - 125) 6.4 (0-20) SW846 6020 11/27-11/29/09 LPPHK1CT Dilution Factor: 1 Analysis Time..: 02:13 MS Run #.......: 9331147 Cadmium 93 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1CU

95 (75 - 125) 2.2 (0-20) SW846 6020 11/27-11/29/09 LPPHK1CV Dilution Factor: 1 Analysis Time..: 02:13 MS Run #.......: 9331147 Cobalt 78 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1CW

79 (75 - 125) 1.6 (0-20) SW846 6020 11/27-11/29/09 LPPHK1CX Dilution Factor: 1 Analysis Time..: 02:13 MS Run #.......: 9331147 Chromium 89 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1C0

116 * (75 - 125) 24 (0-20) SW846 6020 11/27-11/29/09 LPPHK1C1 Dilution Factor: 1 Analysis Time..: 02:13 MS Run #.......: 9331147 Copper 81 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1C2

83 (75 - 125) 1.8 (0-20) SW846 6020 11/27-11/29/09 LPPHK1C3 Dilution Factor: 1 Analysis Time..: 02:13 MS Run #.......: 9331147 Iron NC (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1C4

NC (75 - 125) (0-20) SW846 6020 11/27-11/29/09 LPPHK1C5 Dilution Factor: 1 Analysis Time..: 02:13 MS Run #.......: 9331147 Potassium 83 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1C6

85 (75 - 125) 2.0 (0-20) SW846 6020 11/27-11/29/09 LPPHK1C7 Dilution Factor: 1 Analysis Time..: 02:13 MS Run #.......: 9331147 (Continued on next page)



### C9K180557 137 of 161MATRIX SPIKE SAMPLE EVALUATION REPORT TOTAL Metals Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: SOLID Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09
PERCENT RECOVERY RPD PREPARATION- WORK PARAMETER ___________ RECOVERY

________ LIMITS

__________ RPD

____ LIMITS ______ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

_______ Magnesium 102 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1C8

110 (75 - 125) 7.2 (0-20) SW846 6020 11/27-11/29/09 LPPHK1C9 Dilution Factor: 1 Analysis Time..: 02:13 MS Run #.......: 9331147 Manganese 18 N (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1DA

54 N (75 - 125) 19 (0-20) SW846 6020 11/27-11/29/09 LPPHK1DC Dilution Factor: 1 Analysis Time..: 02:13 MS Run #.......: 9331147 Sodium 79 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1DD

79 (75 - 125) 0.83 (0-20) SW846 6020 11/27-11/29/09 LPPHK1DE Dilution Factor: 1 Analysis Time..: 02:13 MS Run #.......: 9331147 Nickel 79 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1DF

82 (75 - 125) 3.9 (0-20) SW846 6020 11/27-11/29/09 LPPHK1DG Dilution Factor: 1 Analysis Time..: 02:13 MS Run #.......: 9331147 Lead 100 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1DH

113 (75 - 125) 6.6 (0-20) SW846 6020 11/27-11/29/09 LPPHK1DJ Dilution Factor: 1 Analysis Time..: 02:13 MS Run #.......: 9331147 Selenium 77 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1DK

92 (75 - 125) 16 (0-20) SW846 6020 11/27-11/29/09 LPPHK1DL Dilution Factor: 1 Analysis Time..: 02:13 MS Run #.......: 9331147 Thallium 101 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1DM

103 (75 - 125) 1.9 (0-20) SW846 6020 11/27-11/29/09 LPPHK1DN Dilution Factor: 1 Analysis Time..: 02:13 MS Run #.......: 9331147 (Continued on next page)



### C9K180557 138 of 161MATRIX SPIKE SAMPLE EVALUATION REPORT TOTAL Metals Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: SOLID Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09
PERCENT RECOVERY RPD PREPARATION- WORK PARAMETER ___________ RECOVERY

________ LIMITS

__________ RPD

____ LIMITS ______ METHOD

_________________ ANALYSIS DATE ______________ ORDER #

_______ Antimony 88 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1DP

88 (75 - 125) 0.40 (0-20) SW846 6020 11/27-11/29/09 LPPHK1DQ Dilution Factor: 1 Analysis Time..: 02:13 MS Run #.......: 9331147 Vanadium 88 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1DR

91 (75 - 125) 3.3 (0-20) SW846 6020 11/27-11/29/09 LPPHK1DT Dilution Factor: 1 Analysis Time..: 02:13 MS Run #.......: 9331147 Zinc 73 N (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1DU

96 (75 - 125) 20 (0-20) SW846 6020 11/27-11/29/09 LPPHK1DV Dilution Factor: 1 Analysis Time..: 02:13 MS Run #.......: 9331147 NOTE(S):

____________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results. Results and reporting limits have been adjusted for dry weight. NC The recovery and/or RPD were not calculated. * Relative percent difference (RPD) is outside stated control limits. N Spiked analyte recovery is outside stated control limits.



### C9K180557 139 of 161Clean Sites Environmental Services Inc Client Sample ID: MW-1S General Chemistry Lot-Sample #...: Lot-Sample #...: C9K180557-001 Work Order #...: Work Order #...: LPPF5 Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09
PREPARATION- PREP PARAMETER ____________________ RESULT __________ RL

_______ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ BATCH #

_______ Total Recoverable ND 0.010 mg/L SW846 9066 11/19-11/20/09 9323286 Phenolics Dilution Factor: 1 Analysis Time..: 08:36 MS Run #.......: 9323208 Total Organic Carbon Total Organic Carbon 10.2 1.0

mg/L

SM20 5310B

SM20 5310B 11/20/09 11/20/09 9324028

9324028 (TOC) Dilution Factor: 1 Analysis Time..: 14:06 MS Run #.......:



### C9K180557 140 of 161Clean Sites Environmental Services Inc Client Sample ID: MW-3S General Chemistry Lot-Sample #...: Lot-Sample #...: C9K180557-002 Work Order #...: Work Order #...: LPPGN Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09
PREPARATION- PREP PARAMETER ____________________ RESULT __________ RL

_______ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ BATCH #

_______ Total Recoverable ND 0.010 mg/L SW846 9066 11/19-11/20/09 9323286 Phenolics Dilution Factor: 1 Analysis Time..: 08:11 MS Run #.......: 9323208 Total Organic Carbon Total Organic Carbon 6.3 1.0

mg/L

SM20 5310B

SM20 5310B 11/20/09 11/20/09 9324028

9324028 (TOC) Dilution Factor: 1 Analysis Time..: 14:14 MS Run #.......:



### C9K180557 141 of 161Clean Sites Environmental Services Inc Client Sample ID: L2-S1 General Chemistry Lot-Sample #...: Lot-Sample #...: C9K180557-003 Work Order #...: Work Order #...: LPPGP Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09
PREPARATION- PREP PARAMETER ____________________ RESULT __________ RL

_______ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ BATCH #

_______ Total Recoverable ND 0.010 mg/L SW846 9066 11/19-11/20/09 9323286 Phenolics Dilution Factor: 1 Analysis Time..: 08:11 MS Run #.......: 9323208 Total Organic Carbon Total Organic Carbon 2.3 1.0

mg/L

SM20 5310B

SM20 5310B 11/20/09 11/20/09 9324028

9324028 (TOC) Dilution Factor: 1 Analysis Time..: 14:44 MS Run #.......:



### C9K180557 142 of 161Clean Sites Environmental Services Inc Client Sample ID: L1-S1 General Chemistry Lot-Sample #...: Lot-Sample #...: C9K180557-006 Work Order #...: Work Order #...: LPPG1 Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09
PREPARATION- PREP PARAMETER ____________________ RESULT __________ RL

_______ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ BATCH #

_______ Total Organic Carbon Total Organic Carbon 1.3 1.0

mg/L

SM20 5310B

SM20 5310B 11/20/09 11/20/09 9324028

9324028 (TOC) Dilution Factor: 1 Analysis Time..: 14:52 MS Run #.......:



### C9K180557 143 of 161Clean Sites Environmental Services Inc Client Sample ID: L1-S3 General Chemistry Lot-Sample #...: Lot-Sample #...: C9K180557-007 Work Order #...: Work Order #...: LPPG6 Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09
PREPARATION- PREP PARAMETER ____________________ RESULT __________ RL

_______ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ BATCH #

_______ Total Organic Carbon Total Organic Carbon 4.6 1.0

mg/L

SM20 5310B

SM20 5310B 11/20/09 11/20/09 9324028

9324028 (TOC) Dilution Factor: 1 Analysis Time..: 15:01 MS Run #.......:



### C9K180557 144 of 161Clean Sites Environmental Services Inc Client Sample ID: L1-S4 General Chemistry Lot-Sample #...: Lot-Sample #...: C9K180557-008 Work Order #...: Work Order #...: LPPG8 Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09
PREPARATION- PREP PARAMETER ____________________ RESULT __________ RL

_______ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ BATCH #

_______ Total Organic Carbon Total Organic Carbon 7.3 1.0

mg/L

SM20 5310B

SM20 5310B 11/20/09 11/20/09 9324028

9324028 (TOC) Dilution Factor: 1 Analysis Time..: 15:10 MS Run #.......:



### C9K180557 145 of 161Clean Sites Environmental Services Inc Client Sample ID: SW-1 General Chemistry Lot-Sample #...: Lot-Sample #...: C9K180557-009 Work Order #...: Work Order #...: LPPHA Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09
PREPARATION- PREP PARAMETER ____________________ RESULT __________ RL

_______ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ BATCH #

_______ Total Organic Carbon Total Organic Carbon 19.6 1.0

mg/L

SM20 5310B

SM20 5310B 11/20/09 11/20/09 9324028

9324028 (TOC) Dilution Factor: 1 Analysis Time..: 15:19 MS Run #.......:



### C9K180557 146 of 161Clean Sites Environmental Services Inc Client Sample ID: SW-2 General Chemistry Lot-Sample #...: Lot-Sample #...: C9K180557-010 Work Order #...: Work Order #...: LPPHF Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09
PREPARATION- PREP PARAMETER ____________________ RESULT __________ RL

_______ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ BATCH #

_______ Total Organic Carbon Total Organic Carbon 19.0 1.0

mg/L

SM20 5310B

SM20 5310B 11/20/09 11/20/09 9324028

9324028 (TOC) Dilution Factor: 1 Analysis Time..: 15:27 MS Run #.......:



### C9K180557 147 of 161Clean Sites Environmental Services Inc Client Sample ID: SW-3 General Chemistry Lot-Sample #...: Lot-Sample #...: C9K180557-011 Work Order #...: Work Order #...: LPPHG Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09
PREPARATION- PREP PARAMETER ____________________ RESULT __________ RL

_______ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ BATCH #

_______ Total Organic Carbon Total Organic Carbon 19.4 1.0

mg/L

SM20 5310B

SM20 5310B 11/20/09 11/20/09 9324028

9324028 (TOC) Dilution Factor: 1 Analysis Time..: 15:36 MS Run #.......:



### C9K180557 148 of 161Clean Sites Environmental Services Inc Client Sample ID: SED-1 General Chemistry Lot-Sample #...: Lot-Sample #...: C9K180557-012 Work Order #...: Work Order #...: LPPHK Matrix.........: Matrix.........: SOLID Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 % Moisture.....: % Moisture.....: 20
PREPARATION- PREP PARAMETER ____________________ RESULT __________ RL

_______ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ BATCH #

_______ Percent Solids Percent Solids 80.4 1.0

%

SM20 2540G

SM20 2540G 11/24-11/25/09 11/24-11/25/09 9328026

9328026 Dilution Factor: 1 Analysis Time..: 09:35 MS Run #.......: 9328015 Total Organic Carbon ND 622 mg/kg EPA Lloyd Kahn 11/25-11/27/09 9329104 (TOC) Dilution Factor: 1 Analysis Time..: 00:00 MS Run #.......: 9329086 NOTE(S):

___________________________________________________________________________________________ RL Reporting Limit Results and reporting limits have been adjusted for dry weight.



### C9K180557 149 of 161Clean Sites Environmental Services Inc Client Sample ID: SED-2 General Chemistry Lot-Sample #...: Lot-Sample #...: C9K180557-013 Work Order #...: Work Order #...: LPPHM Matrix.........: Matrix.........: SOLID Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 % Moisture.....: % Moisture.....: 20
PREPARATION- PREP PARAMETER ____________________ RESULT __________ RL

_______ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ BATCH #

_______ Percent Solids Percent Solids 80.3 1.0

%

SM20 2540G

SM20 2540G 11/24-11/25/09 11/24-11/25/09 9328026

9328026 Dilution Factor: 1 Analysis Time..: 09:35 MS Run #.......: 9328015 Total Organic Carbon Total Organic Carbon 817 623

mg/kg

EPA Lloyd Kahn

EPA Lloyd Kahn 11/27/09 11/27/09 9331165

9331165 (TOC) Dilution Factor: 1 Analysis Time..: 15:46 MS Run #.......: 9331072 NOTE(S):

___________________________________________________________________________________________ RL Reporting Limit Results and reporting limits have been adjusted for dry weight.



### C9K180557 150 of 161Clean Sites Environmental Services Inc Client Sample ID: SED-3 General Chemistry Lot-Sample #...: Lot-Sample #...: C9K180557-014 Work Order #...: Work Order #...: LPPHN Matrix.........: Matrix.........: SOLID Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 % Moisture.....: % Moisture.....: 23
PREPARATION- PREP PARAMETER ____________________ RESULT __________ RL

_______ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ BATCH #

_______ Percent Solids Percent Solids 77.3 1.0

%

SM20 2540G

SM20 2540G 11/24-11/25/09 11/24-11/25/09 9328026

9328026 Dilution Factor: 1 Analysis Time..: 09:35 MS Run #.......: 9328015 Total Organic Carbon Total Organic Carbon 2810 647

mg/kg

EPA Lloyd Kahn

EPA Lloyd Kahn 11/27/09 11/27/09 9331165

9331165 (TOC) Dilution Factor: 1 Analysis Time..: 00:00 MS Run #.......: 9331072 NOTE(S):

___________________________________________________________________________________________ RL Reporting Limit Results and reporting limits have been adjusted for dry weight.



### C9K180557 151 of 161METHOD BLANK REPORT General Chemistry Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: WATER
REPORTING PREPARATION- PREP PARAMETER __________________ RESULT __________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ BATCH #

_______ Total Organic Carbon Work Order #: LPTQ81AA MB Lot-Sample #: C9K200000-028 (TOC) ND 1.0 mg/L SM20 5310B 11/20/09 9324028 Dilution Factor: 1 Analysis Time..: 13:33 Total Recoverable Work Order #: LPRH61AA MB Lot-Sample #: C9K190000-286 Phenolics ND 0.010 mg/L SW846 9066 11/19-11/20/09 9323286 Dilution Factor: 1 Analysis Time..: 08:05 NOTE(S):

____________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results.



### C9K180557 152 of 161METHOD BLANK REPORT General Chemistry Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: SOLID
REPORTING PREPARATION- PREP PARAMETER __________________ RESULT __________ LIMIT

_________ UNITS

__________ METHOD

_________________ ANALYSIS DATE ______________ BATCH #

_______ Total Organic Carbon Work Order #: LP4W51AA MB Lot-Sample #: C9K250000-104 (TOC) ND 500 mg/kg EPA Lloyd Kahn 11/25/09 9329104 Dilution Factor: 1 Analysis Time..: 15:48 Total Organic Carbon Work Order #: LP7ME1AA MB Lot-Sample #: C9K270000-165 (TOC) ND 500 mg/kg EPA Lloyd Kahn 11/27/09 9331165 Dilution Factor: 1 Analysis Time..: 15:02 NOTE(S):

____________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results.



### C9K180557 153 of 161LABORATORY CONTROL SAMPLE EVALUATION REPORT General Chemistry Lot-Sample #...: Lot-Sample #...: C9K180557 Matrix.........: Matrix.........: WATER
PERCENT RECOVERY RPD PREPARATION- PREP PARAMETER ___________ RECOVERY

________ LIMITS

__________ RPD

____ LIMITS ______ METHOD

_________________ ANALYSIS DATE ______________ BATCH #

_______ Total Organic Carbon WO#:LPTQ81AC-LCS/LPTQ81AD-LCSD LCS Lot-Sample#: C9K200000-028 (TOC) 99 (80 - 120) SM20 5310B 11/20/09 9324028

100 (80 - 120) 0.63 (0-10) SM20 5310B 11/20/09 9324028 Dilution Factor: 1 Analysis Time..: 13:05

NOTE(S):

____________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results.



### C9K180557 154 of 161LABORATORY CONTROL SAMPLE EVALUATION REPORT General Chemistry Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: WATER
PERCENT RECOVERY PREPARATION- PREP PARAMETER ___________ RECOVERY

________ LIMITS

__________ METHOD

_________________ ANALYSIS DATE ______________ BATCH #

_______ Total Recoverable Work Order #: LPRH61AC LCS Lot-Sample#: C9K190000-286 Phenolics 93 (75 - 125) SW846 9066 11/19-11/20/09 9323286 Dilution Factor: 1 Analysis Time..: 08:05 NOTE(S):

____________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results.



### C9K180557 155 of 161LABORATORY CONTROL SAMPLE EVALUATION REPORT General Chemistry Lot-Sample #...: Lot-Sample #...: C9K180557 Matrix.........: Matrix.........: SOLID
PERCENT RECOVERY RPD PREPARATION- PREP PARAMETER ___________ RECOVERY

________ LIMITS

__________ RPD

____ LIMITS ______ METHOD

_________________ ANALYSIS DATE ______________ BATCH #

_______ Total Organic Carbon WO#:LP4W51AC-LCS/LP4W51AD-LCSD LCS Lot-Sample#: C9K250000-104 (TOC) 96 (75 - 125) EPA Lloyd Kahn 11/25/09 9329104

87 (75 - 125) 9.1 (0-20) EPA Lloyd Kahn 11/25/09 9329104 Dilution Factor: 1.79 Analysis Time..: 16:03 Total Organic Carbon WO#:LP7ME1AC-LCS/LP7ME1AD-LCSD LCS Lot-Sample#: C9K270000-165 (TOC) 97 (75 - 125) EPA Lloyd Kahn 11/27/09 9331165

96 (75 - 125) 1.3 (0-20) EPA Lloyd Kahn 11/27/09 9331165 Dilution Factor: 1.8 Analysis Time..: 15:17

NOTE(S):

____________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results.



### C9K180557 156 of 161MATRIX SPIKE SAMPLE EVALUATION REPORT General Chemistry Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: WATER Date Sampled...: Date Sampled...: 11/17/09 Date Received..: Date Received..: 11/18/09
PERCENT RECOVERY RPD PREPARATION- PREP PARAMETER ___________ RECOVERY

________ LIMITS

__________ RPD

____ LIMITS ______ METHOD

_________________ ANALYSIS DATE ______________ BATCH #

_______ Total Recoverable WO#: LPNN11AF-MS/LPNN11AG-MSD MS Lot-Sample #: C9K180471-002 Phenolics 81 (75 - 125) SW846 9066 11/19-11/20/09 9323284

87 (75 - 125) 7.1 (0-20) SW846 9066 11/19-11/20/09 9323284 Dilution Factor: 1 Analysis Time..: 08:05 MS Run #.......: 9323208 NOTE(S):

____________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results.



### C9K180557 157 of 161MATRIX SPIKE SAMPLE EVALUATION REPORT General Chemistry Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: SOLID Date Sampled...: Date Sampled...: 11/23/09 Date Received..: Date Received..: 11/25/09
PERCENT RECOVERY RPD PREPARATION- PREP PARAMETER ___________ RECOVERY

________ LIMITS

__________ RPD

____ LIMITS ______ METHOD

_________________ ANALYSIS DATE ______________ BATCH #

_______ % Moisture.....: % Moisture.....: 100 Total Organic Carbon WO#: LPTNR1DF-MS/LPTNR1DG-MSD MS Lot-Sample #: C9K190670-015 (TOC) 96 (75 - 125) EPA Lloyd Kahn 11/25/09 9329104

104 (75 - 125) 8.3 (0-20) EPA Lloyd Kahn 11/25/09 9329104 Dilution Factor: 1.74 Analysis Time..: 20:52 MS Run #.......: 9329086 % Moisture.....: % Moisture.....: 100 Total Organic Carbon WO#: LP59K1AH-MS/LP59K1AJ-MSD MS Lot-Sample #: C9K250536-001 (TOC) 96 (75 - 125) EPA Lloyd Kahn 11/27/09 9331165

94 (75 - 125) 4.9 (0-20) EPA Lloyd Kahn 11/27/09 9331165 Dilution Factor: 1.74 Analysis Time..: 19:23 MS Run #.......: 9331072 NOTE(S):

____________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results. Results and reporting limits have been adjusted for dry weight.



### C9K180557 158 of 161SAMPLE DUPLICATE EVALUATION REPORT General Chemistry Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPHK9-SMP Matrix.......: Matrix.......: SOLID LPHK9-DUP Date Sampled...: Date Sampled...: 11/12/09 Date Received..: Date Received..: 11/14/09 % Moisture.....: % Moisture.....: 9.8 DUPLICATE RPD PREPARATION- PREP PARAM_____ RESULT ___________ RESULT

___________ UNITS

________ RPD

_____ LIMIT _______ METHOD

_________________ ANALYSIS DATE ______________ BATCH #

_______ Percent Solids SD Lot-Sample #: C9K140458-001 90.2 87.7 % 2.8 (0-20) SM20 2540G 11/24-11/25/09 9328026 Dilution Factor: 1 Analysis Time..: 09:35 MS Run Number..: 9328015



### C9K180557 159 of 161SAMPLE DUPLICATE EVALUATION REPORT General Chemistry Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPTNR-SMP Matrix.......: Matrix.......: SOLID LPTNR-DUP Date Sampled...: Date Sampled...: 11/18/09 Date Received..: Date Received..: 11/19/09 % Moisture.....: % Moisture.....: 53 DUPLICATE RPD PREPARATION- PREP PARAM_____ RESULT ___________ RESULT

___________ UNITS

________ RPD

_____ LIMIT _______ METHOD

_________________ ANALYSIS DATE ______________ BATCH #

_______ Total Organic Carbon SD Lot-Sample #: C9K190670-015 (TOC) 8980 8210 mg/kg 8.9 (0-20) EPA Lloyd Kahn 11/25/09 9329104 Dilution Factor: 1.8 Analysis Time..: 20:09 MS Run Number..: 9329086

NOTE(S):

___________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results. Results and reporting limits have been adjusted for dry weight.



### C9K180557 160 of 161SAMPLE DUPLICATE EVALUATION REPORT General Chemistry Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LP59K-SMP Matrix.......: Matrix.......: SOLID LP59K-DUP Date Sampled...: Date Sampled...: 11/23/09 Date Received..: Date Received..: 11/25/09
DUPLICATE RPD PREPARATION- PREP PARAM_____ RESULT ___________ RESULT

___________ UNITS

________ RPD

_____ LIMIT _______ METHOD

_________________ ANALYSIS DATE ______________ BATCH #

_______ Total Organic Carbon SD Lot-Sample #: C9K250536-001 (TOC) 12600 11700 mg/kg 8.0 (0-20) EPA Lloyd Kahn 11/27/09 9331165 Dilution Factor: 1.77 Analysis Time..: 18:25 MS Run Number..: 9331072

NOTE(S):

___________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results. Results and reporting limits have been adjusted for dry weight.



### C9K180557 161 of 161