CLEAN SITES 


Environmental Services, Inc. 

December 9,2009 

Mr. Ron Davis 


Remedial Project Manager 


U.S. Environmental Protection Agency 


Region III 


1650 Arch Street 


Philadelphia, PA 191 03 


Subject: 	 November 2009 Monitoring Report 


Coker's Landfills 


Cheswold, Delaware 


Dear Mr. Davis: 

Clean Sites Environmental Services, Inc. (Clean Sites) hereby submits this monitoring repoli as 

requested by EPA in their Third Five-Year Review Report for the Site. The Five-Year Review 

Report also requests that monitoring events be conducted every five years coinciding with EPA's 

Five-Year Reviews. 

This report includes a summary of the field and laboratory test results from the monitoring event 

conducted on November 14 and November IS , 2009. It was prepared in accordance with the 

Consent Decree and Part 4.C ofthe March 1993 Remedial Design submittal with the exception that 

the analytical parameters were expanded as requested by EPA and discussed below. 

Groundwater Sampling 

Prior to groundwater sampling, each ofthe wells to be sampled was inspected and the depth to water 

level was recorded. The water levels were used to calculate the well purge volumes and to create 

groundwater contour maps as detailed below. The wells were purged using either a submersible 

pump and disposable poly-flow tubing or disposable bailers. 

Groundwater samples were either collected using a submersible pump (decontaminated between 

wells) or disposable bailers. All Groundwater, surface water, and sediment samples were sent to 

Test America in Pittsburgh, Pennsylvania for analysis. As requested by EPA, groundwater samples 

for Coker's 1 and 2 were analyzed for volatile organic compounds (VOCs) by Method 8260, semivolatile organic compounds (SVOCs) by Method 8270C, Target Analyte List (TAL) metals by 

Method 8020B, and total organic carbon (TOC) by Method 5310B. In addition, groundwater 

samples for Coker's 2 were also analyzed for total phenolics by Method 9066. Field measurements 

of pH, specific conductance, and temperature were recorded for each well. A trip blank 

accompanied the sample coolers and a rinse blank was collected from the submersible pump to 

verify it was being thoroughly decontaminated between wells 

C LEAN SIT ES ENV I RONMENTAL SERVICES . INC . ... 4616 1 WES T LAKE DRIVE . SUITE 230·6 ... PO T OMAC FAL L S, VIRG I N I A 2 0 165 

TE L: (703) 5 19·2 140 ... FAX: ( 7 03 ) 519·2 14 1 
Water and Sediment Sampling 

water samples were collected from to Coker's 1 in accordance with 

the by 

was collected 

prior to sediment were stream 

a sampler. collected likely depositional areas using 

decontaminated samples were collected from sediment bed 

and YOCs, 


niPIPn: as Field measurements of pH, 


oxygen were recorded for the water 


"'~"U"j;, Results 

locations s J and 2 are on Estimated groundwater 

each landfill are figures. These contours have using 

ofthe water data is provided on Table 1. 

analytical 

water and 

in Appendix are 

or total phenolics detected in 

1. It 1.3 

samples. was 

mg/I in the monitoring 

to 10 

no Maximum 

sampling events 

Site 

There were no 

at Coker's 1. A new lock 
Should you have any questions regarding this report or need additional information, please call me at 

(703) 519-2142. 

ly yours, 

Scott R. Miller, P.E. 

Proj ect Coordinator 

cc: 	 Sandra Guastaferro, Reichhold, Inc. 

Stephen Johnson, DNREC 

Lisa D. Krogman, P.E., Kraft Foods Global, Inc. 

Jeffrey Srulovitz, Esq., Kraft Foods Global, Inc. 
NOVEMBER 2009

TOP OF CASING DEPTH TO GROUNDW

MONITORING WELL ELEVATION (FT, MSL) WATER (FT)(1) ELEVATI

L1-S1 41.73 4.03 37.70

L1-S3 42.41 11.22 31.19L1-S4 28.88 2.11 26.77

MW-1S 45.52 1.27 44.25

MW-3S 45.19 1.67 43.52

L2-S1 50.33 2.43 47.90

Notes:(1) Depth to water readings were measured on November 14, 2009.

Coker's 1Coker's 2

TABLE 1

GROUNDWATER ELEVATIONS

COKER'S LANDFILLS SITE

CHESWOLD, DELAWARE
NOVEMBER 2009

PARAMETER(1) L1-S1 L1-S3 L1-S4 MW-1S MW-3S L2

Aluminum 486 597 145 1,730 2,880 2,

Arsenic ND 1.9 ND ND ND N

Barium 18.7 65.4 33.6 47.0 134 9

Beryllium ND ND ND ND 2.2 NCalcium 3,930 31,600 45,100 10,500 8,770 4,Cobalt 1.3 2.8 ND 3.5 4.1 2

Chromium 35.1 3.0 3.9 6.5 6.4 7

Copper ND ND ND 2.5 2.1 N

Iron 922 10,200 3,420 1,520 2,280 5,

Potassium 633 2,360 1,910 995 1,240 1,

Magnesium 2,350 18,500 3,500 3,140 5,900 2,

Manganese 11.9 277 194 162 163 1

Sodium 5,830 4,640 7,050 3,760 4,720 4,

Nickel 5.1 1.7 3.1 2.6 3.9 4

Lead ND ND ND 1.4 2.0 

Vanadium ND 2.2 9.9 2.9 6.0 6

Zinc 7.7 10.3 5.1 9.6 15.3 1

Phenolics (mg/l) NA NA NA ND ND N

Total Organic Carbon (mg/l) 1.3 4.6 7.3 10.2 6.3 2

Temperature (oC) 14.7 14.7 14.9 13.7 14.2 1

pH 5.43 5.85 5.54 5.27 4.71 5

Specific Conductance (μmhos/cm) 84.8 343.0 302.6 112.0 157.5 10

Notes:(1) Only the detected parameters are shown on the table.ND indicates parameter was not detected.NA indicates parameter was not analyzed.Bold numbers indicate an MCL exceedance.

Coker's 1 Coker's 2

TABLE 2

SUMMARY OF GROUNDWATER SAMPLING RESULTS

COKER'S LANDFILLS SITE

CHESWOLD, DELAWARE
NOVEMBER 2009

PARAMETER(1) SW-1 SW-2 SW-3 SED-1 SED-2 

Aluminum 446 448 415 1,470 1,080 

Arsenic ND ND ND 0.17 0.43 

Barium 65.8 61.5 60.0 14.5 12.5 

Beryllium ND ND ND 0.75 ND 

Calcium 16,500 16,000 16,300 885 386 

Cobalt 1.1 0.98 0.91 3.5 0.93 

Chromium 4.1 3.7 3.9 2.4 2.2 Copper ND ND ND 0.60 0.47 

Iron 1,000 994 1,040 10,900 2,430 Potassium 3,700 3,480 3,440 72.9 82.5 Magnesium 5,120 5,120 5,140 293 121 

Manganese 102 89.9 92.2 94.5 32.0 

Sodium 6,170 5,850 5,700 29.3 25.9 

Nickel 2.2 2.1 2.1 1.2 0.75 Lead ND ND ND 2.1 2.1 

Vanadium 2.5 1.9 2.5 4.6 2.7 Zinc 15.4 11.4 12.2 16.8 10.2 

Total Organic Carbon (mg/l or mg/kg) 19.6 19.0 19.4 ND 817 

Temperature (oC) 14.5 14.1 13.6 NA NA 

pH 7.11 7.11 7.04 NA NA 

Dissolved Oxygen (mg/l) 6 6 5 NA NA 

Specific Conductance (μmhos/cm) 175.4 178.9 177.7 NA NA 

Notes:(1) Only the detected parameters are shown on the table.ND indicates parameter was not detected.NA indicates parameter was not analyzed.Bold numbers indicate an MCL exceedance.

Surface Water (μg/l) Sediments (μg/kg)

TABLE 3

SUMMARY OF WILLIS BRANCH SAMPLING RESULTS

COKER'S LANDFILLS SITE

CHESWOLD, DELAWARE


Appendix A 

 Analytical Results
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METHODS SUMMARY

C9K180557

ANALYTICAL PREPARATION

PARAMETER __________________________________________________ METHOD _______________ METHOD _______________

ICP-MS (6020) SW846 6020 SW846 3010

ICP-MS (6020) SW846 6020 SW846 3050B

Mercury in Liquid Waste (Manual Cold-Vapor) SW846 7470A SW846 7470A

Mercury in Solid Waste (Manual Cold-Vapor) SW846 7471A SW846 7471A

Phenolics SW846 9066 SW846 9066

Semivolatile Organic Compounds by GC/MS SW846 8270C SW846 3520C

Semivolatile Organic Compounds by GC/MS SW846 8270C SW846 3541

Total Organic Carbon, TOC 5310B SM20 5310B SM20 5310B

Total Residue as Percent Solids SM20 2540G

TOC Lloyd Kahn Lloyd Kahn EPA Lloyd Kahn EPA Lloyd Kahn

Volatile Organics by GC/MS SW846 8260B SW846 5030B

References:

EPA "EASTERN ENVIRONMENTAL RADIATION FACILITY RADIOCHEMISTRY

PROCEDURES MANUAL" US EPA EPA 520/5-84-006 AUGUST 1984

SM20 "STANDARD METHODS FOR THE EXAMINATION OF WATER AND

WASTEWATER", 20TH EDITION."

SW846 "Test Methods for Evaluating Solid Waste, Physical/Chemical

Methods", Third Edition, November 1986 and its updates.

C9K180557 7 of 161
SAMPLE SUMMARY

C9K180557

SAMPLED SAMP

WO #_____ SAMPLE# _______ CLIENT SAMPLE ID ________________________________________________________________ DATE ________ TIME _____

LPPF5 001 MW-1S 11/14/09 10:35

LPPGN 002 MW-3S 11/14/09 10:45

LPPGP 003 L2-S1 11/14/09 11:40

LPPGR 004 RINSE BLANK-1 11/14/09 11:15

LPPGV 005 TRIP BLANK-COKER 2 11/14/09

LPPG1 006 L1-S1 11/14/09 15:20

LPPG6 007 L1-S3 11/14/09 16:10

LPPG8 008 L1-S4 11/14/09 15:40

LPPHA 009 SW-1 11/15/09 11:25

LPPHF 010 SW-2 11/15/09 10:30

LPPHG 011 SW-3 11/15/09 09:45

LPPHK 012 SED-1 11/15/09 11:35

LPPHM 013 SED-2 11/15/09 10:40

LPPHN 014 SED-3 11/15/09 09:55

LPPHV 015 TRIP BLANK-COKER 1 11/15/09

NOTE(S): _____________________________________________________________________________________________

- The analytical results of the samples listed above are presented on the following pages.

- All calculations are performed before rounding to avoid round-off errors in calculated results.

- Results noted as "ND" were not detected at or above the stated limit.

- This report must not be reproduced, except in full, without the written approval of the laboratory.

- Results for the following parameters are never reported on a dry weight basis: color, corrosivity, density, flashpoint, ignitability, layers, odor,

paint filter test, pH, porosity pressure, reactivity, redox potential, specific gravity, spot tests, solids, solubility, temperature, viscosity, and weight.

C9K180557 8 of 161
Clean Sites Environmental Services Inc

Client Sample ID: MW-1S

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-001 Work Order #...: Work Order #...: LPPF51AD Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9328229

Prep Date......: Prep Date......: 11/24/09 Analysis Date..: Analysis Date..: 11/24/09

Prep Batch #...: Prep Batch #...: 9328345 Analysis Time..: Analysis Time..: 13:46

Dilution Factor: Dilution Factor: 1

Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acetone ND 20 ug/L

Benzene ND 5.0 ug/L

Bromodichloromethane ND 5.0 ug/L

Bromoform ND 5.0 ug/L

Bromomethane ND 5.0 ug/L

2-Butanone ND 5.0 ug/L

Carbon disulfide ND 5.0 ug/L

Carbon tetrachloride ND 5.0 ug/L

Chlorobenzene ND 5.0 ug/L

Chloroethane ND 5.0 ug/L

Chloroform ND 5.0 ug/L

Chloromethane ND 5.0 ug/L

Cyclohexane ND 5.0 ug/L

Dibromochloromethane ND 5.0 ug/L

1,2-Dibromo-3-chloro- ND 5.0 ug/L

propane

1,2-Dibromoethane ND 5.0 ug/L

1,3-Dichlorobenzene ND 5.0 ug/L

1,4-Dichlorobenzene ND 5.0 ug/L

1,2-Dichlorobenzene ND 5.0 ug/L

Dichlorodifluoromethane ND 5.0 ug/L

1,1-Dichloroethane ND 5.0 ug/L

1,2-Dichloroethane ND 5.0 ug/L

1,1-Dichloroethene ND 5.0 ug/L

cis-1,2-Dichloroethene ND 5.0 ug/L

trans-1,2-Dichloroethene ND 5.0 ug/L

1,2-Dichloropropane ND 5.0 ug/L

cis-1,3-Dichloropropene ND 5.0 ug/L

trans-1,3-Dichloropropene ND 5.0 ug/L

Ethylbenzene ND 5.0 ug/L

2-Hexanone ND 5.0 ug/L

Isopropylbenzene ND 5.0 ug/L

Methyl acetate ND 5.0 ug/L

Methylene chloride ND 5.0 ug/L

Methylcyclohexane ND 5.0 ug/L

4-Methyl-2-pentanone ND 5.0 ug/L

Methyl tert-butyl ether ND 5.0 ug/L

Styrene ND 5.0 ug/L

(Continued on next page)

C9K180557 9 of 161
Clean Sites Environmental Services Inc

Client Sample ID: MW-1S

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-001 Work Order #...: Work Order #...: LPPF51AD Matrix.........: Matrix.........: WATER

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

1,1,2,2-Tetrachloroethane ND 5.0 ug/L

1,2,4-Trichloro- ND 5.0 ug/L

benzene

Tetrachloroethene ND 5.0 ug/L

1,1,1-Trichloroethane ND 5.0 ug/L

1,1,2-Trichloroethane ND 5.0 ug/L

Trichloroethene ND 5.0 ug/L

Trichlorofluoromethane ND 5.0 ug/L

1,1,2-Trichloro- ND 5.0 ug/L

1,2,2-trifluoroethane

Toluene ND 5.0 ug/L

Vinyl chloride ND 5.0 ug/L

Xylenes (total) ND 15 ug/L

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 100 (62 - 123)

Toluene-d8 95 (80 - 120)

4-Bromofluorobenzene 86 (75 - 120)

Dibromofluoromethane 108 (80 - 120)

C9K180557 10 of 161
Clean Sites Environmental Services Inc

Client Sample ID: MW-3S

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-002 Work Order #...: Work Order #...: LPPGN1AL Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9329152

Prep Date......: Prep Date......: 11/25/09 Analysis Date..: Analysis Date..: 11/25/09

Prep Batch #...: Prep Batch #...: 9329174 Analysis Time..: Analysis Time..: 09:51

Dilution Factor: Dilution Factor: 1

Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acetone ND 20 ug/L

Benzene ND 5.0 ug/L

Bromodichloromethane ND 5.0 ug/L

Bromoform ND 5.0 ug/L

Bromomethane ND 5.0 ug/L

2-Butanone ND 5.0 ug/L

Carbon disulfide ND 5.0 ug/L

Carbon tetrachloride ND 5.0 ug/L

Chlorobenzene ND 5.0 ug/L

Chloroethane ND 5.0 ug/L

Chloroform ND 5.0 ug/L

Chloromethane ND 5.0 ug/L

Cyclohexane ND 5.0 ug/L

Dibromochloromethane ND 5.0 ug/L

1,2-Dibromo-3-chloro- ND 5.0 ug/L

propane

1,2-Dibromoethane ND 5.0 ug/L

1,3-Dichlorobenzene ND 5.0 ug/L

1,4-Dichlorobenzene ND 5.0 ug/L

1,2-Dichlorobenzene ND 5.0 ug/L

Dichlorodifluoromethane ND 5.0 ug/L

1,1-Dichloroethane ND 5.0 ug/L

1,2-Dichloroethane ND 5.0 ug/L

1,1-Dichloroethene ND 5.0 ug/L

cis-1,2-Dichloroethene ND 5.0 ug/L

trans-1,2-Dichloroethene ND 5.0 ug/L

1,2-Dichloropropane ND 5.0 ug/L

cis-1,3-Dichloropropene ND 5.0 ug/L

trans-1,3-Dichloropropene ND 5.0 ug/L

Ethylbenzene ND 5.0 ug/L

2-Hexanone ND 5.0 ug/L

Isopropylbenzene ND 5.0 ug/L

Methyl acetate ND 5.0 ug/L

Methylene chloride ND 5.0 ug/L

Methylcyclohexane ND 5.0 ug/L

4-Methyl-2-pentanone ND 5.0 ug/L

Methyl tert-butyl ether ND 5.0 ug/L

Styrene ND 5.0 ug/L

(Continued on next page)

C9K180557 11 of 161
Clean Sites Environmental Services Inc

Client Sample ID: MW-3S

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-002 Work Order #...: Work Order #...: LPPGN1AL Matrix.........: Matrix.........: WATER

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

1,1,2,2-Tetrachloroethane ND 5.0 ug/L

1,2,4-Trichloro- ND 5.0 ug/L

benzene

Tetrachloroethene ND 5.0 ug/L

1,1,1-Trichloroethane ND 5.0 ug/L

1,1,2-Trichloroethane ND 5.0 ug/L

Trichloroethene ND 5.0 ug/L

Trichlorofluoromethane ND 5.0 ug/L

1,1,2-Trichloro- ND 5.0 ug/L

1,2,2-trifluoroethane

Toluene ND 5.0 ug/L

Vinyl chloride ND 5.0 ug/L

Xylenes (total) ND 15 ug/L

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 94 (62 - 123)

Toluene-d8 101 (80 - 120)

4-Bromofluorobenzene 90 (75 - 120)

Dibromofluoromethane 104 (80 - 120)

C9K180557 12 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L2-S1

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-003 Work Order #...: Work Order #...: LPPGP1AL Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9328229

Prep Date......: Prep Date......: 11/24/09 Analysis Date..: Analysis Date..: 11/24/09

Prep Batch #...: Prep Batch #...: 9328345 Analysis Time..: Analysis Time..: 19:38

Dilution Factor: Dilution Factor: 1

Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acetone ND 20 ug/L

Benzene ND 5.0 ug/L

Bromodichloromethane ND 5.0 ug/L

Bromoform ND 5.0 ug/L

Bromomethane ND 5.0 ug/L

2-Butanone ND 5.0 ug/L

Carbon disulfide ND 5.0 ug/L

Carbon tetrachloride ND 5.0 ug/L

Chlorobenzene ND 5.0 ug/L

Chloroethane ND 5.0 ug/L

Chloroform ND 5.0 ug/L

Chloromethane ND 5.0 ug/L

Cyclohexane ND 5.0 ug/L

Dibromochloromethane ND 5.0 ug/L

1,2-Dibromo-3-chloro- ND 5.0 ug/L

propane

1,2-Dibromoethane ND 5.0 ug/L

1,3-Dichlorobenzene ND 5.0 ug/L

1,4-Dichlorobenzene ND 5.0 ug/L

1,2-Dichlorobenzene ND 5.0 ug/L

Dichlorodifluoromethane ND 5.0 ug/L

1,1-Dichloroethane ND 5.0 ug/L

1,2-Dichloroethane ND 5.0 ug/L

1,1-Dichloroethene ND 5.0 ug/L

cis-1,2-Dichloroethene ND 5.0 ug/L

trans-1,2-Dichloroethene ND 5.0 ug/L

1,2-Dichloropropane ND 5.0 ug/L

cis-1,3-Dichloropropene ND 5.0 ug/L

trans-1,3-Dichloropropene ND 5.0 ug/L

Ethylbenzene ND 5.0 ug/L

2-Hexanone ND 5.0 ug/L

Isopropylbenzene ND 5.0 ug/L

Methyl acetate ND 5.0 ug/L

Methylene chloride ND 5.0 ug/L

Methylcyclohexane ND 5.0 ug/L

4-Methyl-2-pentanone ND 5.0 ug/L

Methyl tert-butyl ether ND 5.0 ug/L

Styrene ND 5.0 ug/L

(Continued on next page)

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Clean Sites Environmental Services Inc

Client Sample ID: L2-S1

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-003 Work Order #...: Work Order #...: LPPGP1AL Matrix.........: Matrix.........: WATER

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

1,1,2,2-Tetrachloroethane ND 5.0 ug/L

1,2,4-Trichloro- ND 5.0 ug/L

benzene

Tetrachloroethene ND 5.0 ug/L

1,1,1-Trichloroethane ND 5.0 ug/L

1,1,2-Trichloroethane ND 5.0 ug/L

Trichloroethene ND 5.0 ug/L

Trichlorofluoromethane ND 5.0 ug/L

1,1,2-Trichloro- ND 5.0 ug/L

1,2,2-trifluoroethane

Toluene ND 5.0 ug/L

Vinyl chloride ND 5.0 ug/L

Xylenes (total) ND 15 ug/L

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 85 (62 - 123)

Toluene-d8 108 (80 - 120)

4-Bromofluorobenzene 85 (75 - 120)

Dibromofluoromethane 96 (80 - 120)

C9K180557 14 of 161
Clean Sites Environmental Services Inc

Client Sample ID: RINSE BLANK-1

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-004 Work Order #...: Work Order #...: LPPGR1AA Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9329152

Prep Date......: Prep Date......: 11/25/09 Analysis Date..: Analysis Date..: 11/25/09

Prep Batch #...: Prep Batch #...: 9329174 Analysis Time..: Analysis Time..: 13:35

Dilution Factor: Dilution Factor: 1

Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acetone ND 20 ug/L

Benzene ND 5.0 ug/L

Bromodichloromethane ND 5.0 ug/L

Bromoform ND 5.0 ug/L

Bromomethane ND 5.0 ug/L

2-Butanone ND 5.0 ug/L

Carbon disulfide ND 5.0 ug/L

Carbon tetrachloride ND 5.0 ug/L

Chlorobenzene ND 5.0 ug/L

Chloroethane ND 5.0 ug/L

Chloroform ND 5.0 ug/L

Chloromethane ND 5.0 ug/L

Cyclohexane ND 5.0 ug/L

Dibromochloromethane ND 5.0 ug/L

1,2-Dibromo-3-chloro- ND 5.0 ug/L

propane

1,2-Dibromoethane ND 5.0 ug/L

1,3-Dichlorobenzene ND 5.0 ug/L

1,4-Dichlorobenzene ND 5.0 ug/L

1,2-Dichlorobenzene ND 5.0 ug/L

Dichlorodifluoromethane ND 5.0 ug/L

1,1-Dichloroethane ND 5.0 ug/L

1,2-Dichloroethane ND 5.0 ug/L

1,1-Dichloroethene ND 5.0 ug/L

cis-1,2-Dichloroethene ND 5.0 ug/L

trans-1,2-Dichloroethene ND 5.0 ug/L

1,2-Dichloropropane ND 5.0 ug/L

cis-1,3-Dichloropropene ND 5.0 ug/L

trans-1,3-Dichloropropene ND 5.0 ug/L

Ethylbenzene ND 5.0 ug/L

2-Hexanone ND 5.0 ug/L

Isopropylbenzene ND 5.0 ug/L

Methyl acetate ND 5.0 ug/L

Methylene chloride ND 5.0 ug/L

Methylcyclohexane ND 5.0 ug/L

4-Methyl-2-pentanone ND 5.0 ug/L

Methyl tert-butyl ether ND 5.0 ug/L

Styrene ND 5.0 ug/L

(Continued on next page)

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Clean Sites Environmental Services Inc

Client Sample ID: RINSE BLANK-1

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-004 Work Order #...: Work Order #...: LPPGR1AA Matrix.........: Matrix.........: WATER

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

1,1,2,2-Tetrachloroethane ND 5.0 ug/L

1,2,4-Trichloro- ND 5.0 ug/L

benzene

Tetrachloroethene ND 5.0 ug/L

1,1,1-Trichloroethane ND 5.0 ug/L

1,1,2-Trichloroethane ND 5.0 ug/L

Trichloroethene ND 5.0 ug/L

Trichlorofluoromethane ND 5.0 ug/L

1,1,2-Trichloro- ND 5.0 ug/L

1,2,2-trifluoroethane

Toluene ND 5.0 ug/L

Vinyl chloride ND 5.0 ug/L

Xylenes (total) ND 15 ug/L

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 90 (62 - 123)

Toluene-d8 105 (80 - 120)

4-Bromofluorobenzene 88 (75 - 120)

Dibromofluoromethane 97 (80 - 120)

C9K180557 16 of 161
Clean Sites Environmental Services Inc

Client Sample ID: TRIP BLANK-COKER 2

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-005 Work Order #...: Work Order #...: LPPGV1AA Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9329152

Prep Date......: Prep Date......: 11/25/09 Analysis Date..: Analysis Date..: 11/25/09

Prep Batch #...: Prep Batch #...: 9329174 Analysis Time..: Analysis Time..: 14:00

Dilution Factor: Dilution Factor: 1

Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acetone ND 20 ug/L

Benzene ND 5.0 ug/L

Bromodichloromethane ND 5.0 ug/L

Bromoform ND 5.0 ug/L

Bromomethane ND 5.0 ug/L

2-Butanone ND 5.0 ug/L

Carbon disulfide ND 5.0 ug/L

Carbon tetrachloride ND 5.0 ug/L

Chlorobenzene ND 5.0 ug/L

Chloroethane ND 5.0 ug/L

Chloroform ND 5.0 ug/L

Chloromethane ND 5.0 ug/L

Cyclohexane ND 5.0 ug/L

Dibromochloromethane ND 5.0 ug/L

1,2-Dibromo-3-chloro- ND 5.0 ug/L

propane

1,2-Dibromoethane ND 5.0 ug/L

1,3-Dichlorobenzene ND 5.0 ug/L

1,4-Dichlorobenzene ND 5.0 ug/L

1,2-Dichlorobenzene ND 5.0 ug/L

Dichlorodifluoromethane ND 5.0 ug/L

1,1-Dichloroethane ND 5.0 ug/L

1,2-Dichloroethane ND 5.0 ug/L

1,1-Dichloroethene ND 5.0 ug/L

cis-1,2-Dichloroethene ND 5.0 ug/L

trans-1,2-Dichloroethene ND 5.0 ug/L

1,2-Dichloropropane ND 5.0 ug/L

cis-1,3-Dichloropropene ND 5.0 ug/L

trans-1,3-Dichloropropene ND 5.0 ug/L

Ethylbenzene ND 5.0 ug/L

2-Hexanone ND 5.0 ug/L

Isopropylbenzene ND 5.0 ug/L

Methyl acetate ND 5.0 ug/L

Methylene chloride ND 5.0 ug/L

Methylcyclohexane ND 5.0 ug/L

4-Methyl-2-pentanone ND 5.0 ug/L

Methyl tert-butyl ether ND 5.0 ug/L

Styrene ND 5.0 ug/L

(Continued on next page)

C9K180557 17 of 161
Clean Sites Environmental Services Inc

Client Sample ID: TRIP BLANK-COKER 2

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-005 Work Order #...: Work Order #...: LPPGV1AA Matrix.........: Matrix.........: WATER

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

1,1,2,2-Tetrachloroethane ND 5.0 ug/L

1,2,4-Trichloro- ND 5.0 ug/L

benzene

Tetrachloroethene ND 5.0 ug/L

1,1,1-Trichloroethane ND 5.0 ug/L

1,1,2-Trichloroethane ND 5.0 ug/L

Trichloroethene ND 5.0 ug/L

Trichlorofluoromethane ND 5.0 ug/L

1,1,2-Trichloro- ND 5.0 ug/L

1,2,2-trifluoroethane

Toluene ND 5.0 ug/L

Vinyl chloride ND 5.0 ug/L

Xylenes (total) ND 15 ug/L

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 88 (62 - 123)

Toluene-d8 106 (80 - 120)

4-Bromofluorobenzene 88 (75 - 120)

Dibromofluoromethane 96 (80 - 120)

C9K180557 18 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L1-S1

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-006 Work Order #...: Work Order #...: LPPG11AC Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9328229

Prep Date......: Prep Date......: 11/24/09 Analysis Date..: Analysis Date..: 11/24/09

Prep Batch #...: Prep Batch #...: 9328345 Analysis Time..: Analysis Time..: 20:04

Dilution Factor: Dilution Factor: 1

Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acetone ND 20 ug/L

Benzene ND 5.0 ug/L

Bromodichloromethane ND 5.0 ug/L

Bromoform ND 5.0 ug/L

Bromomethane ND 5.0 ug/L

2-Butanone ND 5.0 ug/L

Carbon disulfide ND 5.0 ug/L

Carbon tetrachloride ND 5.0 ug/L

Chlorobenzene ND 5.0 ug/L

Chloroethane ND 5.0 ug/L

Chloroform ND 5.0 ug/L

Chloromethane ND 5.0 ug/L

Cyclohexane ND 5.0 ug/L

Dibromochloromethane ND 5.0 ug/L

1,2-Dibromo-3-chloro- ND 5.0 ug/L

propane

1,2-Dibromoethane ND 5.0 ug/L

1,3-Dichlorobenzene ND 5.0 ug/L

1,4-Dichlorobenzene ND 5.0 ug/L

1,2-Dichlorobenzene ND 5.0 ug/L

Dichlorodifluoromethane ND 5.0 ug/L

1,1-Dichloroethane ND 5.0 ug/L

1,2-Dichloroethane ND 5.0 ug/L

1,1-Dichloroethene ND 5.0 ug/L

cis-1,2-Dichloroethene ND 5.0 ug/L

trans-1,2-Dichloroethene ND 5.0 ug/L

1,2-Dichloropropane ND 5.0 ug/L

cis-1,3-Dichloropropene ND 5.0 ug/L

trans-1,3-Dichloropropene ND 5.0 ug/L

Ethylbenzene ND 5.0 ug/L

2-Hexanone ND 5.0 ug/L

Isopropylbenzene ND 5.0 ug/L

Methyl acetate ND 5.0 ug/L

Methylene chloride ND 5.0 ug/L

Methylcyclohexane ND 5.0 ug/L

4-Methyl-2-pentanone ND 5.0 ug/L

Methyl tert-butyl ether ND 5.0 ug/L

Styrene ND 5.0 ug/L

(Continued on next page)

C9K180557 19 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L1-S1

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-006 Work Order #...: Work Order #...: LPPG11AC Matrix.........: Matrix.........: WATER

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

1,1,2,2-Tetrachloroethane ND 5.0 ug/L

1,2,4-Trichloro- ND 5.0 ug/L

benzene

Tetrachloroethene ND 5.0 ug/L

1,1,1-Trichloroethane ND 5.0 ug/L

1,1,2-Trichloroethane ND 5.0 ug/L

Trichloroethene ND 5.0 ug/L

Trichlorofluoromethane ND 5.0 ug/L

1,1,2-Trichloro- ND 5.0 ug/L

1,2,2-trifluoroethane

Toluene ND 5.0 ug/L

Vinyl chloride ND 5.0 ug/L

Xylenes (total) ND 15 ug/L

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 89 (62 - 123)

Toluene-d8 106 (80 - 120)

4-Bromofluorobenzene 87 (75 - 120)

Dibromofluoromethane 99 (80 - 120)

C9K180557 20 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L1-S3

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-007 Work Order #...: Work Order #...: LPPG61AJ Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9328229

Prep Date......: Prep Date......: 11/24/09 Analysis Date..: Analysis Date..: 11/24/09

Prep Batch #...: Prep Batch #...: 9328345 Analysis Time..: Analysis Time..: 20:30

Dilution Factor: Dilution Factor: 1

Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acetone ND 20 ug/L

Benzene ND 5.0 ug/L

Bromodichloromethane ND 5.0 ug/L

Bromoform ND 5.0 ug/L

Bromomethane ND 5.0 ug/L

2-Butanone ND 5.0 ug/L

Carbon disulfide ND 5.0 ug/L

Carbon tetrachloride ND 5.0 ug/L

Chlorobenzene ND 5.0 ug/L

Chloroethane ND 5.0 ug/L

Chloroform ND 5.0 ug/L

Chloromethane ND 5.0 ug/L

Cyclohexane ND 5.0 ug/L

Dibromochloromethane ND 5.0 ug/L

1,2-Dibromo-3-chloro- ND 5.0 ug/L

propane

1,2-Dibromoethane ND 5.0 ug/L

1,3-Dichlorobenzene ND 5.0 ug/L

1,4-Dichlorobenzene ND 5.0 ug/L

1,2-Dichlorobenzene ND 5.0 ug/L

Dichlorodifluoromethane ND 5.0 ug/L

1,1-Dichloroethane ND 5.0 ug/L

1,2-Dichloroethane ND 5.0 ug/L

1,1-Dichloroethene ND 5.0 ug/L

cis-1,2-Dichloroethene ND 5.0 ug/L

trans-1,2-Dichloroethene ND 5.0 ug/L

1,2-Dichloropropane ND 5.0 ug/L

cis-1,3-Dichloropropene ND 5.0 ug/L

trans-1,3-Dichloropropene ND 5.0 ug/L

Ethylbenzene ND 5.0 ug/L

2-Hexanone ND 5.0 ug/L

Isopropylbenzene ND 5.0 ug/L

Methyl acetate ND 5.0 ug/L

Methylene chloride ND 5.0 ug/L

Methylcyclohexane ND 5.0 ug/L

4-Methyl-2-pentanone ND 5.0 ug/L

Methyl tert-butyl ether ND 5.0 ug/L

Styrene ND 5.0 ug/L

(Continued on next page)

C9K180557 21 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L1-S3

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-007 Work Order #...: Work Order #...: LPPG61AJ Matrix.........: Matrix.........: WATER

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

1,1,2,2-Tetrachloroethane ND 5.0 ug/L

1,2,4-Trichloro- ND 5.0 ug/L

benzene

Tetrachloroethene ND 5.0 ug/L

1,1,1-Trichloroethane ND 5.0 ug/L

1,1,2-Trichloroethane ND 5.0 ug/L

Trichloroethene ND 5.0 ug/L

Trichlorofluoromethane ND 5.0 ug/L

1,1,2-Trichloro- ND 5.0 ug/L

1,2,2-trifluoroethane

Toluene ND 5.0 ug/L

Vinyl chloride ND 5.0 ug/L

Xylenes (total) ND 15 ug/L

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 94 (62 - 123)

Toluene-d8 103 (80 - 120)

4-Bromofluorobenzene 88 (75 - 120)

Dibromofluoromethane 100 (80 - 120)

C9K180557 22 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L1-S4

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-008 Work Order #...: Work Order #...: LPPG81AQ Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9328229

Prep Date......: Prep Date......: 11/24/09 Analysis Date..: Analysis Date..: 11/24/09

Prep Batch #...: Prep Batch #...: 9328345 Analysis Time..: Analysis Time..: 20:56

Dilution Factor: Dilution Factor: 1

Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acetone ND 20 ug/L

Benzene ND 5.0 ug/L

Bromodichloromethane ND 5.0 ug/L

Bromoform ND 5.0 ug/L

Bromomethane ND 5.0 ug/L

2-Butanone ND 5.0 ug/L

Carbon disulfide ND 5.0 ug/L

Carbon tetrachloride ND 5.0 ug/L

Chlorobenzene ND 5.0 ug/L

Chloroethane ND 5.0 ug/L

Chloroform ND 5.0 ug/L

Chloromethane ND 5.0 ug/L

Cyclohexane ND 5.0 ug/L

Dibromochloromethane ND 5.0 ug/L

1,2-Dibromo-3-chloro- ND 5.0 ug/L

propane

1,2-Dibromoethane ND 5.0 ug/L

1,3-Dichlorobenzene ND 5.0 ug/L

1,4-Dichlorobenzene ND 5.0 ug/L

1,2-Dichlorobenzene ND 5.0 ug/L

Dichlorodifluoromethane ND 5.0 ug/L

1,1-Dichloroethane ND 5.0 ug/L

1,2-Dichloroethane ND 5.0 ug/L

1,1-Dichloroethene ND 5.0 ug/L

cis-1,2-Dichloroethene ND 5.0 ug/L

trans-1,2-Dichloroethene ND 5.0 ug/L

1,2-Dichloropropane ND 5.0 ug/L

cis-1,3-Dichloropropene ND 5.0 ug/L

trans-1,3-Dichloropropene ND 5.0 ug/L

Ethylbenzene ND 5.0 ug/L

2-Hexanone ND 5.0 ug/L

Isopropylbenzene ND 5.0 ug/L

Methyl acetate ND 5.0 ug/L

Methylene chloride ND 5.0 ug/L

Methylcyclohexane ND 5.0 ug/L

4-Methyl-2-pentanone ND 5.0 ug/L

Methyl tert-butyl ether ND 5.0 ug/L

Styrene ND 5.0 ug/L

(Continued on next page)

C9K180557 23 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L1-S4

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-008 Work Order #...: Work Order #...: LPPG81AQ Matrix.........: Matrix.........: WATER

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

1,1,2,2-Tetrachloroethane ND 5.0 ug/L

1,2,4-Trichloro- ND 5.0 ug/L

benzene

Tetrachloroethene ND 5.0 ug/L

1,1,1-Trichloroethane ND 5.0 ug/L

1,1,2-Trichloroethane ND 5.0 ug/L

Trichloroethene ND 5.0 ug/L

Trichlorofluoromethane ND 5.0 ug/L

1,1,2-Trichloro- ND 5.0 ug/L

1,2,2-trifluoroethane

Toluene ND 5.0 ug/L

Vinyl chloride ND 5.0 ug/L

Xylenes (total) ND 15 ug/L

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 90 (62 - 123)

Toluene-d8 107 (80 - 120)

4-Bromofluorobenzene 88 (75 - 120)

Dibromofluoromethane 98 (80 - 120)

C9K180557 24 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SW-1

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-009 Work Order #...: Work Order #...: LPPHA1AX Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9328229

Prep Date......: Prep Date......: 11/24/09 Analysis Date..: Analysis Date..: 11/24/09

Prep Batch #...: Prep Batch #...: 9328345 Analysis Time..: Analysis Time..: 21:22

Dilution Factor: Dilution Factor: 1

Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acetone ND 20 ug/L

Benzene ND 5.0 ug/L

Bromodichloromethane ND 5.0 ug/L

Bromoform ND 5.0 ug/L

Bromomethane ND 5.0 ug/L

2-Butanone ND 5.0 ug/L

Carbon disulfide ND 5.0 ug/L

Carbon tetrachloride ND 5.0 ug/L

Chlorobenzene ND 5.0 ug/L

Chloroethane ND 5.0 ug/L

Chloroform ND 5.0 ug/L

Chloromethane ND 5.0 ug/L

Cyclohexane ND 5.0 ug/L

Dibromochloromethane ND 5.0 ug/L

1,2-Dibromo-3-chloro- ND 5.0 ug/L

propane

1,2-Dibromoethane ND 5.0 ug/L

1,3-Dichlorobenzene ND 5.0 ug/L

1,4-Dichlorobenzene ND 5.0 ug/L

1,2-Dichlorobenzene ND 5.0 ug/L

Dichlorodifluoromethane ND 5.0 ug/L

1,1-Dichloroethane ND 5.0 ug/L

1,2-Dichloroethane ND 5.0 ug/L

1,1-Dichloroethene ND 5.0 ug/L

cis-1,2-Dichloroethene ND 5.0 ug/L

trans-1,2-Dichloroethene ND 5.0 ug/L

1,2-Dichloropropane ND 5.0 ug/L

cis-1,3-Dichloropropene ND 5.0 ug/L

trans-1,3-Dichloropropene ND 5.0 ug/L

Ethylbenzene ND 5.0 ug/L

2-Hexanone ND 5.0 ug/L

Isopropylbenzene ND 5.0 ug/L

Methyl acetate ND 5.0 ug/L

Methylene chloride ND 5.0 ug/L

Methylcyclohexane ND 5.0 ug/L

4-Methyl-2-pentanone ND 5.0 ug/L

Methyl tert-butyl ether ND 5.0 ug/L

Styrene ND 5.0 ug/L

(Continued on next page)

C9K180557 25 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SW-1

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-009 Work Order #...: Work Order #...: LPPHA1AX Matrix.........: Matrix.........: WATER

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

1,1,2,2-Tetrachloroethane ND 5.0 ug/L

1,2,4-Trichloro- ND 5.0 ug/L

benzene

Tetrachloroethene ND 5.0 ug/L

1,1,1-Trichloroethane ND 5.0 ug/L

1,1,2-Trichloroethane ND 5.0 ug/L

Trichloroethene ND 5.0 ug/L

Trichlorofluoromethane ND 5.0 ug/L

1,1,2-Trichloro- ND 5.0 ug/L

1,2,2-trifluoroethane

Toluene ND 5.0 ug/L

Vinyl chloride ND 5.0 ug/L

Xylenes (total) ND 15 ug/L

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 87 (62 - 123)

Toluene-d8 108 (80 - 120)

4-Bromofluorobenzene 87 (75 - 120)

Dibromofluoromethane 97 (80 - 120)

C9K180557 26 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SW-2

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-010 Work Order #...: Work Order #...: LPPHF1A5 Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9328229

Prep Date......: Prep Date......: 11/24/09 Analysis Date..: Analysis Date..: 11/24/09

Prep Batch #...: Prep Batch #...: 9328345 Analysis Time..: Analysis Time..: 21:47

Dilution Factor: Dilution Factor: 1

Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acetone ND 20 ug/L

Benzene ND 5.0 ug/L

Bromodichloromethane ND 5.0 ug/L

Bromoform ND 5.0 ug/L

Bromomethane ND 5.0 ug/L

2-Butanone ND 5.0 ug/L

Carbon disulfide ND 5.0 ug/L

Carbon tetrachloride ND 5.0 ug/L

Chlorobenzene ND 5.0 ug/L

Chloroethane ND 5.0 ug/L

Chloroform ND 5.0 ug/L

Chloromethane ND 5.0 ug/L

Cyclohexane ND 5.0 ug/L

Dibromochloromethane ND 5.0 ug/L

1,2-Dibromo-3-chloro- ND 5.0 ug/L

propane

1,2-Dibromoethane ND 5.0 ug/L

1,3-Dichlorobenzene ND 5.0 ug/L

1,4-Dichlorobenzene ND 5.0 ug/L

1,2-Dichlorobenzene ND 5.0 ug/L

Dichlorodifluoromethane ND 5.0 ug/L

1,1-Dichloroethane ND 5.0 ug/L

1,2-Dichloroethane ND 5.0 ug/L

1,1-Dichloroethene ND 5.0 ug/L

cis-1,2-Dichloroethene ND 5.0 ug/L

trans-1,2-Dichloroethene ND 5.0 ug/L

1,2-Dichloropropane ND 5.0 ug/L

cis-1,3-Dichloropropene ND 5.0 ug/L

trans-1,3-Dichloropropene ND 5.0 ug/L

Ethylbenzene ND 5.0 ug/L

2-Hexanone ND 5.0 ug/L

Isopropylbenzene ND 5.0 ug/L

Methyl acetate ND 5.0 ug/L

Methylene chloride ND 5.0 ug/L

Methylcyclohexane ND 5.0 ug/L

4-Methyl-2-pentanone ND 5.0 ug/L

Methyl tert-butyl ether ND 5.0 ug/L

Styrene ND 5.0 ug/L

(Continued on next page)

C9K180557 27 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SW-2

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-010 Work Order #...: Work Order #...: LPPHF1A5 Matrix.........: Matrix.........: WATER

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

1,1,2,2-Tetrachloroethane ND 5.0 ug/L

1,2,4-Trichloro- ND 5.0 ug/L

benzene

Tetrachloroethene ND 5.0 ug/L

1,1,1-Trichloroethane ND 5.0 ug/L

1,1,2-Trichloroethane ND 5.0 ug/L

Trichloroethene ND 5.0 ug/L

Trichlorofluoromethane ND 5.0 ug/L

1,1,2-Trichloro- ND 5.0 ug/L

1,2,2-trifluoroethane

Toluene ND 5.0 ug/L

Vinyl chloride ND 5.0 ug/L

Xylenes (total) ND 15 ug/L

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 89 (62 - 123)

Toluene-d8 107 (80 - 120)

4-Bromofluorobenzene 87 (75 - 120)

Dibromofluoromethane 97 (80 - 120)

C9K180557 28 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SW-3

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-011 Work Order #...: Work Order #...: LPPHG1A5 Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9328229

Prep Date......: Prep Date......: 11/24/09 Analysis Date..: Analysis Date..: 11/24/09

Prep Batch #...: Prep Batch #...: 9328345 Analysis Time..: Analysis Time..: 22:13

Dilution Factor: Dilution Factor: 1

Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acetone ND 20 ug/L

Benzene ND 5.0 ug/L

Bromodichloromethane ND 5.0 ug/L

Bromoform ND 5.0 ug/L

Bromomethane ND 5.0 ug/L

2-Butanone ND 5.0 ug/L

Carbon disulfide ND 5.0 ug/L

Carbon tetrachloride ND 5.0 ug/L

Chlorobenzene ND 5.0 ug/L

Chloroethane ND 5.0 ug/L

Chloroform ND 5.0 ug/L

Chloromethane ND 5.0 ug/L

Cyclohexane ND 5.0 ug/L

Dibromochloromethane ND 5.0 ug/L

1,2-Dibromo-3-chloro- ND 5.0 ug/L

propane

1,2-Dibromoethane ND 5.0 ug/L

1,3-Dichlorobenzene ND 5.0 ug/L

1,4-Dichlorobenzene ND 5.0 ug/L

1,2-Dichlorobenzene ND 5.0 ug/L

Dichlorodifluoromethane ND 5.0 ug/L

1,1-Dichloroethane ND 5.0 ug/L

1,2-Dichloroethane ND 5.0 ug/L

1,1-Dichloroethene ND 5.0 ug/L

cis-1,2-Dichloroethene ND 5.0 ug/L

trans-1,2-Dichloroethene ND 5.0 ug/L

1,2-Dichloropropane ND 5.0 ug/L

cis-1,3-Dichloropropene ND 5.0 ug/L

trans-1,3-Dichloropropene ND 5.0 ug/L

Ethylbenzene ND 5.0 ug/L

2-Hexanone ND 5.0 ug/L

Isopropylbenzene ND 5.0 ug/L

Methyl acetate ND 5.0 ug/L

Methylene chloride ND 5.0 ug/L

Methylcyclohexane ND 5.0 ug/L

4-Methyl-2-pentanone ND 5.0 ug/L

Methyl tert-butyl ether ND 5.0 ug/L

Styrene ND 5.0 ug/L

(Continued on next page)

C9K180557 29 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SW-3

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-011 Work Order #...: Work Order #...: LPPHG1A5 Matrix.........: Matrix.........: WATER

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

1,1,2,2-Tetrachloroethane ND 5.0 ug/L

1,2,4-Trichloro- ND 5.0 ug/L

benzene

Tetrachloroethene ND 5.0 ug/L

1,1,1-Trichloroethane ND 5.0 ug/L

1,1,2-Trichloroethane ND 5.0 ug/L

Trichloroethene ND 5.0 ug/L

Trichlorofluoromethane ND 5.0 ug/L

1,1,2-Trichloro- ND 5.0 ug/L

1,2,2-trifluoroethane

Toluene ND 5.0 ug/L

Vinyl chloride ND 5.0 ug/L

Xylenes (total) ND 15 ug/L

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 88 (62 - 123)

Toluene-d8 108 (80 - 120)

4-Bromofluorobenzene 87 (75 - 120)

Dibromofluoromethane 99 (80 - 120)

C9K180557 30 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SED-1

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-012 Work Order #...: Work Order #...: LPPHK1AD Matrix.........: Matrix.........: SOLID

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9329143

Prep Date......: Prep Date......: 11/25/09 Analysis Date..: Analysis Date..: 11/25/09

Prep Batch #...: Prep Batch #...: 9329221 Analysis Time..: Analysis Time..: 12:36

Dilution Factor: Dilution Factor: 1

% Moisture.....: % Moisture.....: 20 Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acetone ND 25 ug/kg

Benzene ND 6.2 ug/kg

Bromodichloromethane ND 6.2 ug/kg

Bromoform ND 6.2 ug/kg

Bromomethane ND 6.2 ug/kg

2-Butanone ND 6.2 ug/kg

Carbon disulfide ND 6.2 ug/kg

Carbon tetrachloride ND 6.2 ug/kg

Chlorobenzene ND 6.2 ug/kg

Chloroethane ND 6.2 ug/kg

Chloroform ND 6.2 ug/kg

Chloromethane ND 6.2 ug/kg

Cyclohexane ND 6.2 ug/kg

Dibromochloromethane ND 6.2 ug/kg

1,2-Dibromo-3-chloro- ND 6.2 ug/kg

propane

1,2-Dibromoethane ND 6.2 ug/kg

1,3-Dichlorobenzene ND 6.2 ug/kg

1,4-Dichlorobenzene ND 6.2 ug/kg

1,2-Dichlorobenzene ND 6.2 ug/kg

Dichlorodifluoromethane ND 6.2 ug/kg

1,1-Dichloroethane ND 6.2 ug/kg

1,2-Dichloroethane ND 6.2 ug/kg

1,1-Dichloroethene ND 6.2 ug/kg

cis-1,2-Dichloroethene ND 6.2 ug/kg

trans-1,2-Dichloroethene ND 6.2 ug/kg

1,2-Dichloropropane ND 6.2 ug/kg

cis-1,3-Dichloropropene ND 6.2 ug/kg

trans-1,3-Dichloropropene ND 6.2 ug/kg

Ethylbenzene ND 6.2 ug/kg

2-Hexanone ND 6.2 ug/kg

Isopropylbenzene ND 6.2 ug/kg

Methyl acetate ND 6.2 ug/kg

Methylene chloride ND 6.2 ug/kg

Methylcyclohexane ND 6.2 ug/kg

4-Methyl-2-pentanone ND 6.2 ug/kg

Methyl tert-butyl ether ND 6.2 ug/kg

Styrene ND 6.2 ug/kg

(Continued on next page)

C9K180557 31 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SED-1

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-012 Work Order #...: Work Order #...: LPPHK1AD Matrix.........: Matrix.........: SOLID

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

1,1,2,2-Tetrachloroethane ND 6.2 ug/kg

1,2,4-Trichloro- ND 6.2 ug/kg

benzene

Tetrachloroethene ND 6.2 ug/kg

1,1,1-Trichloroethane ND 6.2 ug/kg

1,1,2-Trichloroethane ND 6.2 ug/kg

Trichloroethene ND 6.2 ug/kg

Trichlorofluoromethane ND 6.2 ug/kg

1,1,2-Trichloro- ND 6.2 ug/kg

1,2,2-trifluoroethane

Toluene ND 6.2 ug/kg

Vinyl chloride ND 6.2 ug/kg

Xylenes (total) ND 19 ug/kg

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 102 (52 - 124)

Toluene-d8 89 (72 - 127)

4-Bromofluorobenzene 96 (63 - 120)

Dibromofluoromethane 115 (68 - 121)

NOTE(S): _______________________________________________________________________________________

Results and reporting limits have been adjusted for dry weight.

C9K180557 32 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SED-2

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-013 Work Order #...: Work Order #...: LPPHM1AL Matrix.........: Matrix.........: SOLID

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9329143

Prep Date......: Prep Date......: 11/25/09 Analysis Date..: Analysis Date..: 11/25/09

Prep Batch #...: Prep Batch #...: 9329221 Analysis Time..: Analysis Time..: 13:00

Dilution Factor: Dilution Factor: 1

% Moisture.....: % Moisture.....: 20 Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acetone ND 25 ug/kg

Benzene ND 6.2 ug/kg

Bromodichloromethane ND 6.2 ug/kg

Bromoform ND 6.2 ug/kg

Bromomethane ND 6.2 ug/kg

2-Butanone ND 6.2 ug/kg

Carbon disulfide ND 6.2 ug/kg

Carbon tetrachloride ND 6.2 ug/kg

Chlorobenzene ND 6.2 ug/kg

Chloroethane ND 6.2 ug/kg

Chloroform ND 6.2 ug/kg

Chloromethane ND 6.2 ug/kg

Cyclohexane ND 6.2 ug/kg

Dibromochloromethane ND 6.2 ug/kg

1,2-Dibromo-3-chloro- ND 6.2 ug/kg

propane

1,2-Dibromoethane ND 6.2 ug/kg

1,3-Dichlorobenzene ND 6.2 ug/kg

1,4-Dichlorobenzene ND 6.2 ug/kg

1,2-Dichlorobenzene ND 6.2 ug/kg

Dichlorodifluoromethane ND 6.2 ug/kg

1,1-Dichloroethane ND 6.2 ug/kg

1,2-Dichloroethane ND 6.2 ug/kg

1,1-Dichloroethene ND 6.2 ug/kg

cis-1,2-Dichloroethene ND 6.2 ug/kg

trans-1,2-Dichloroethene ND 6.2 ug/kg

1,2-Dichloropropane ND 6.2 ug/kg

cis-1,3-Dichloropropene ND 6.2 ug/kg

trans-1,3-Dichloropropene ND 6.2 ug/kg

Ethylbenzene ND 6.2 ug/kg

2-Hexanone ND 6.2 ug/kg

Isopropylbenzene ND 6.2 ug/kg

Methyl acetate ND 6.2 ug/kg

Methylene chloride ND 6.2 ug/kg

Methylcyclohexane ND 6.2 ug/kg

4-Methyl-2-pentanone ND 6.2 ug/kg

Methyl tert-butyl ether ND 6.2 ug/kg

Styrene ND 6.2 ug/kg

(Continued on next page)

C9K180557 33 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SED-2

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-013 Work Order #...: Work Order #...: LPPHM1AL Matrix.........: Matrix.........: SOLID

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

1,1,2,2-Tetrachloroethane ND 6.2 ug/kg

1,2,4-Trichloro- ND 6.2 ug/kg

benzene

Tetrachloroethene ND 6.2 ug/kg

1,1,1-Trichloroethane ND 6.2 ug/kg

1,1,2-Trichloroethane ND 6.2 ug/kg

Trichloroethene ND 6.2 ug/kg

Trichlorofluoromethane ND 6.2 ug/kg

1,1,2-Trichloro- ND 6.2 ug/kg

1,2,2-trifluoroethane

Toluene ND 6.2 ug/kg

Vinyl chloride ND 6.2 ug/kg

Xylenes (total) ND 19 ug/kg

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 101 (52 - 124)

Toluene-d8 87 (72 - 127)

4-Bromofluorobenzene 97 (63 - 120)

Dibromofluoromethane 111 (68 - 121)

NOTE(S): _______________________________________________________________________________________

Results and reporting limits have been adjusted for dry weight.

C9K180557 34 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SED-3

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-014 Work Order #...: Work Order #...: LPPHN1AU Matrix.........: Matrix.........: SOLID

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9329143

Prep Date......: Prep Date......: 11/25/09 Analysis Date..: Analysis Date..: 11/25/09

Prep Batch #...: Prep Batch #...: 9329221 Analysis Time..: Analysis Time..: 13:25

Dilution Factor: Dilution Factor: 1

% Moisture.....: % Moisture.....: 23 Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acetone ND 26 ug/kg

Benzene ND 6.5 ug/kg

Bromodichloromethane ND 6.5 ug/kg

Bromoform ND 6.5 ug/kg

Bromomethane ND 6.5 ug/kg

2-Butanone ND 6.5 ug/kg

Carbon disulfide ND 6.5 ug/kg

Carbon tetrachloride ND 6.5 ug/kg

Chlorobenzene ND 6.5 ug/kg

Chloroethane ND 6.5 ug/kg

Chloroform ND 6.5 ug/kg

Chloromethane ND 6.5 ug/kg

Cyclohexane ND 6.5 ug/kg

Dibromochloromethane ND 6.5 ug/kg

1,2-Dibromo-3-chloro- ND 6.5 ug/kg

propane

1,2-Dibromoethane ND 6.5 ug/kg

1,3-Dichlorobenzene ND 6.5 ug/kg

1,4-Dichlorobenzene ND 6.5 ug/kg

1,2-Dichlorobenzene ND 6.5 ug/kg

Dichlorodifluoromethane ND 6.5 ug/kg

1,1-Dichloroethane ND 6.5 ug/kg

1,2-Dichloroethane ND 6.5 ug/kg

1,1-Dichloroethene ND 6.5 ug/kg

cis-1,2-Dichloroethene ND 6.5 ug/kg

trans-1,2-Dichloroethene ND 6.5 ug/kg

1,2-Dichloropropane ND 6.5 ug/kg

cis-1,3-Dichloropropene ND 6.5 ug/kg

trans-1,3-Dichloropropene ND 6.5 ug/kg

Ethylbenzene ND 6.5 ug/kg

2-Hexanone ND 6.5 ug/kg

Isopropylbenzene ND 6.5 ug/kg

Methyl acetate ND 6.5 ug/kg

Methylene chloride ND 6.5 ug/kg

Methylcyclohexane ND 6.5 ug/kg

4-Methyl-2-pentanone ND 6.5 ug/kg

Methyl tert-butyl ether ND 6.5 ug/kg

Styrene ND 6.5 ug/kg

(Continued on next page)

C9K180557 35 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SED-3

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-014 Work Order #...: Work Order #...: LPPHN1AU Matrix.........: Matrix.........: SOLID

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

1,1,2,2-Tetrachloroethane ND 6.5 ug/kg

1,2,4-Trichloro- ND 6.5 ug/kg

benzene

Tetrachloroethene ND 6.5 ug/kg

1,1,1-Trichloroethane ND 6.5 ug/kg

1,1,2-Trichloroethane ND 6.5 ug/kg

Trichloroethene ND 6.5 ug/kg

Trichlorofluoromethane ND 6.5 ug/kg

1,1,2-Trichloro- ND 6.5 ug/kg

1,2,2-trifluoroethane

Toluene ND 6.5 ug/kg

Vinyl chloride ND 6.5 ug/kg

Xylenes (total) ND 19 ug/kg

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 101 (52 - 124)

Toluene-d8 89 (72 - 127)

4-Bromofluorobenzene 97 (63 - 120)

Dibromofluoromethane 112 (68 - 121)

NOTE(S): _______________________________________________________________________________________

Results and reporting limits have been adjusted for dry weight.

C9K180557 36 of 161
Clean Sites Environmental Services Inc

Client Sample ID: TRIP BLANK-COKER 1

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-015 Work Order #...: Work Order #...: LPPHV1AA Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9329152

Prep Date......: Prep Date......: 11/25/09 Analysis Date..: Analysis Date..: 11/25/09

Prep Batch #...: Prep Batch #...: 9329174 Analysis Time..: Analysis Time..: 14:26

Dilution Factor: Dilution Factor: 1

Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acetone ND 20 ug/L

Benzene ND 5.0 ug/L

Bromodichloromethane ND 5.0 ug/L

Bromoform ND 5.0 ug/L

Bromomethane ND 5.0 ug/L

2-Butanone ND 5.0 ug/L

Carbon disulfide ND 5.0 ug/L

Carbon tetrachloride ND 5.0 ug/L

Chlorobenzene ND 5.0 ug/L

Chloroethane ND 5.0 ug/L

Chloroform ND 5.0 ug/L

Chloromethane ND 5.0 ug/L

Cyclohexane ND 5.0 ug/L

Dibromochloromethane ND 5.0 ug/L

1,2-Dibromo-3-chloro- ND 5.0 ug/L

propane

1,2-Dibromoethane ND 5.0 ug/L

1,3-Dichlorobenzene ND 5.0 ug/L

1,4-Dichlorobenzene ND 5.0 ug/L

1,2-Dichlorobenzene ND 5.0 ug/L

Dichlorodifluoromethane ND 5.0 ug/L

1,1-Dichloroethane ND 5.0 ug/L

1,2-Dichloroethane ND 5.0 ug/L

1,1-Dichloroethene ND 5.0 ug/L

cis-1,2-Dichloroethene ND 5.0 ug/L

trans-1,2-Dichloroethene ND 5.0 ug/L

1,2-Dichloropropane ND 5.0 ug/L

cis-1,3-Dichloropropene ND 5.0 ug/L

trans-1,3-Dichloropropene ND 5.0 ug/L

Ethylbenzene ND 5.0 ug/L

2-Hexanone ND 5.0 ug/L

Isopropylbenzene ND 5.0 ug/L

Methyl acetate ND 5.0 ug/L

Methylene chloride ND 5.0 ug/L

Methylcyclohexane ND 5.0 ug/L

4-Methyl-2-pentanone ND 5.0 ug/L

Methyl tert-butyl ether ND 5.0 ug/L

Styrene ND 5.0 ug/L

(Continued on next page)

C9K180557 37 of 161
Clean Sites Environmental Services Inc

Client Sample ID: TRIP BLANK-COKER 1

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-015 Work Order #...: Work Order #...: LPPHV1AA Matrix.........: Matrix.........: WATER

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

1,1,2,2-Tetrachloroethane ND 5.0 ug/L

1,2,4-Trichloro- ND 5.0 ug/L

benzene

Tetrachloroethene ND 5.0 ug/L

1,1,1-Trichloroethane ND 5.0 ug/L

1,1,2-Trichloroethane ND 5.0 ug/L

Trichloroethene ND 5.0 ug/L

Trichlorofluoromethane ND 5.0 ug/L

1,1,2-Trichloro- ND 5.0 ug/L

1,2,2-trifluoroethane

Toluene ND 5.0 ug/L

Vinyl chloride ND 5.0 ug/L

Xylenes (total) ND 15 ug/L

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 94 (62 - 123)

Toluene-d8 103 (80 - 120)

4-Bromofluorobenzene 90 (75 - 120)

Dibromofluoromethane 102 (80 - 120)

C9K180557 38 of 161
METHOD BLANK REPORT

GC/MS Volatiles

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LP2741AA Matrix.........: Matrix.........: WATER

MB Lot-Sample #: MB Lot-Sample #: C9K240000-345

Prep Date......: Prep Date......: 11/24/09 Analysis Time..: Analysis Time..: 13:14

Analysis Date..: Analysis Date..: 11/24/09 Prep Batch #...: Prep Batch #...: 9328345

Dilution Factor: Dilution Factor: 1

REPORTING

PARAMETER _________________________ RESULT _______________ LIMIT _________ UNITS __________ METHOD _________________

Acetone ND 20 ug/L SW846 8260B

Benzene ND 5.0 ug/L SW846 8260B

Bromodichloromethane ND 5.0 ug/L SW846 8260B

Bromoform ND 5.0 ug/L SW846 8260B

Bromomethane ND 5.0 ug/L SW846 8260B

2-Butanone ND 5.0 ug/L SW846 8260B

Carbon disulfide ND 5.0 ug/L SW846 8260B

Carbon tetrachloride ND 5.0 ug/L SW846 8260B

Chlorobenzene ND 5.0 ug/L SW846 8260B

Chloroethane ND 5.0 ug/L SW846 8260B

Chloroform ND 5.0 ug/L SW846 8260B

Chloromethane ND 5.0 ug/L SW846 8260B

Cyclohexane ND 5.0 ug/L SW846 8260B

Dibromochloromethane ND 5.0 ug/L SW846 8260B

1,2-Dibromo-3-chloro- ND 5.0 ug/L SW846 8260B

propane

1,2-Dibromoethane ND 5.0 ug/L SW846 8260B

1,3-Dichlorobenzene ND 5.0 ug/L SW846 8260B

1,4-Dichlorobenzene ND 5.0 ug/L SW846 8260B

1,2-Dichlorobenzene ND 5.0 ug/L SW846 8260B

Dichlorodifluoromethane ND 5.0 ug/L SW846 8260B

1,1-Dichloroethane ND 5.0 ug/L SW846 8260B

1,2-Dichloroethane ND 5.0 ug/L SW846 8260B

1,1-Dichloroethene ND 5.0 ug/L SW846 8260B

cis-1,2-Dichloroethene ND 5.0 ug/L SW846 8260B

trans-1,2-Dichloroethene ND 5.0 ug/L SW846 8260B

1,2-Dichloropropane ND 5.0 ug/L SW846 8260B

cis-1,3-Dichloropropene ND 5.0 ug/L SW846 8260B

trans-1,3-Dichloropropene ND 5.0 ug/L SW846 8260B

Ethylbenzene ND 5.0 ug/L SW846 8260B

2-Hexanone ND 5.0 ug/L SW846 8260B

Isopropylbenzene ND 5.0 ug/L SW846 8260B

Methyl acetate ND 5.0 ug/L SW846 8260B

Methylene chloride ND 5.0 ug/L SW846 8260B

Methylcyclohexane ND 5.0 ug/L SW846 8260B

4-Methyl-2-pentanone ND 5.0 ug/L SW846 8260B

Methyl tert-butyl ether ND 5.0 ug/L SW846 8260B

Styrene ND 5.0 ug/L SW846 8260B

1,1,2,2-Tetrachloroethane ND 5.0 ug/L SW846 8260B

1,2,4-Trichloro- ND 5.0 ug/L SW846 8260B

benzene

(Continued on next page)

C9K180557 39 of 161
METHOD BLANK REPORT

GC/MS Volatiles

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LP2741AA Matrix.........: Matrix.........: WATER

REPORTING

PARAMETER _________________________ RESULT _______________ LIMIT _________ UNITS __________ METHOD _________________

Tetrachloroethene ND 5.0 ug/L SW846 8260B

1,1,1-Trichloroethane ND 5.0 ug/L SW846 8260B

1,1,2-Trichloroethane ND 5.0 ug/L SW846 8260B

Trichloroethene ND 5.0 ug/L SW846 8260B

Trichlorofluoromethane ND 5.0 ug/L SW846 8260B

1,1,2-Trichloro- ND 5.0 ug/L SW846 8260B

1,2,2-trifluoroethane

Toluene ND 5.0 ug/L SW846 8260B

Vinyl chloride ND 5.0 ug/L SW846 8260B

Xylenes (total) ND 15 ug/L SW846 8260B

PERCENT RECOVERY

SURROGATE _________________________ RECOVERY ________ LIMITS __________

1,2-Dichloroethane-d4 102 (62 - 123)

Toluene-d8 99 (80 - 120)

4-Bromofluorobenzene 89 (75 - 120)

Dibromofluoromethane 110 (80 - 120)

NOTE(S): ___________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

C9K180557 40 of 161
METHOD BLANK REPORT

GC/MS Volatiles

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LP42D1AA Matrix.........: Matrix.........: WATER

MB Lot-Sample #: MB Lot-Sample #: C9K250000-174

Prep Date......: Prep Date......: 11/25/09 Analysis Time..: Analysis Time..: 08:36

Analysis Date..: Analysis Date..: 11/25/09 Prep Batch #...: Prep Batch #...: 9329174

Dilution Factor: Dilution Factor: 1

REPORTING

PARAMETER _________________________ RESULT _______________ LIMIT _________ UNITS __________ METHOD _________________

Acetone ND 20 ug/L SW846 8260B

Benzene ND 5.0 ug/L SW846 8260B

Bromodichloromethane ND 5.0 ug/L SW846 8260B

Bromoform ND 5.0 ug/L SW846 8260B

Bromomethane ND 5.0 ug/L SW846 8260B

2-Butanone ND 5.0 ug/L SW846 8260B

Carbon disulfide ND 5.0 ug/L SW846 8260B

Carbon tetrachloride ND 5.0 ug/L SW846 8260B

Chlorobenzene ND 5.0 ug/L SW846 8260B

Chloroethane ND 5.0 ug/L SW846 8260B

Chloroform ND 5.0 ug/L SW846 8260B

Chloromethane ND 5.0 ug/L SW846 8260B

Cyclohexane ND 5.0 ug/L SW846 8260B

Dibromochloromethane ND 5.0 ug/L SW846 8260B

1,2-Dibromo-3-chloro- ND 5.0 ug/L SW846 8260B

propane

1,2-Dibromoethane ND 5.0 ug/L SW846 8260B

1,3-Dichlorobenzene ND 5.0 ug/L SW846 8260B

1,4-Dichlorobenzene ND 5.0 ug/L SW846 8260B

1,2-Dichlorobenzene ND 5.0 ug/L SW846 8260B

Dichlorodifluoromethane ND 5.0 ug/L SW846 8260B

1,1-Dichloroethane ND 5.0 ug/L SW846 8260B

1,2-Dichloroethane ND 5.0 ug/L SW846 8260B

1,1-Dichloroethene ND 5.0 ug/L SW846 8260B

cis-1,2-Dichloroethene ND 5.0 ug/L SW846 8260B

trans-1,2-Dichloroethene ND 5.0 ug/L SW846 8260B

1,2-Dichloropropane ND 5.0 ug/L SW846 8260B

cis-1,3-Dichloropropene ND 5.0 ug/L SW846 8260B

trans-1,3-Dichloropropene ND 5.0 ug/L SW846 8260B

Ethylbenzene ND 5.0 ug/L SW846 8260B

2-Hexanone ND 5.0 ug/L SW846 8260B

Isopropylbenzene ND 5.0 ug/L SW846 8260B

Methyl acetate ND 5.0 ug/L SW846 8260B

Methylene chloride ND 5.0 ug/L SW846 8260B

Methylcyclohexane ND 5.0 ug/L SW846 8260B

4-Methyl-2-pentanone ND 5.0 ug/L SW846 8260B

Methyl tert-butyl ether ND 5.0 ug/L SW846 8260B

Styrene ND 5.0 ug/L SW846 8260B

1,1,2,2-Tetrachloroethane ND 5.0 ug/L SW846 8260B

1,2,4-Trichloro- ND 5.0 ug/L SW846 8260B

benzene

(Continued on next page)

C9K180557 41 of 161
METHOD BLANK REPORT

GC/MS Volatiles

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LP42D1AA Matrix.........: Matrix.........: WATER

REPORTING

PARAMETER _________________________ RESULT _______________ LIMIT _________ UNITS __________ METHOD _________________

Tetrachloroethene ND 5.0 ug/L SW846 8260B

1,1,1-Trichloroethane ND 5.0 ug/L SW846 8260B

1,1,2-Trichloroethane ND 5.0 ug/L SW846 8260B

Trichloroethene ND 5.0 ug/L SW846 8260B

Trichlorofluoromethane ND 5.0 ug/L SW846 8260B

1,1,2-Trichloro- ND ug/L SW846 8260B

1,2,2-trifluoroethane

Toluene ND 5.0 ug/L SW846 8260B

Vinyl chloride ND 5.0 ug/L SW846 8260B

Xylenes (total) ND 15 ug/L SW846 8260B

PERCENT RECOVERY

SURROGATE _________________________ RECOVERY ________ LIMITS __________

1,2-Dichloroethane-d4 95 (62 - 123)

Toluene-d8 103 (80 - 120)

4-Bromofluorobenzene 89 (75 - 120)

Dibromofluoromethane 101 (80 - 120)

NOTE(S): ___________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

C9K180557 42 of 161
METHOD BLANK REPORT

GC/MS Volatiles

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LP4721AA Matrix.........: Matrix.........: SOLID

MB Lot-Sample #: MB Lot-Sample #: C9K250000-221

Prep Date......: Prep Date......: 11/25/09 Analysis Time..: Analysis Time..: 10:39

Analysis Date..: Analysis Date..: 11/25/09 Prep Batch #...: Prep Batch #...: 9329221

Dilution Factor: Dilution Factor: 1

REPORTING

PARAMETER _________________________ RESULT _______________ LIMIT _________ UNITS __________ METHOD _________________

Acetone ND 20 ug/kg SW846 8260B

Benzene ND 5.0 ug/kg SW846 8260B

Bromodichloromethane ND 5.0 ug/kg SW846 8260B

Bromoform ND 5.0 ug/kg SW846 8260B

Bromomethane ND 5.0 ug/kg SW846 8260B

2-Butanone ND 5.0 ug/kg SW846 8260B

Carbon disulfide ND 5.0 ug/kg SW846 8260B

Carbon tetrachloride ND 5.0 ug/kg SW846 8260B

Chlorobenzene ND 5.0 ug/kg SW846 8260B

Chloroethane ND 5.0 ug/kg SW846 8260B

Chloroform ND 5.0 ug/kg SW846 8260B

Chloromethane ND 5.0 ug/kg SW846 8260B

Cyclohexane ND 5.0 ug/kg SW846 8260B

Dibromochloromethane ND 5.0 ug/kg SW846 8260B

1,2-Dibromo-3-chloro- ND 5.0 ug/kg SW846 8260B

propane

1,2-Dibromoethane ND 5.0 ug/kg SW846 8260B

1,3-Dichlorobenzene ND 5.0 ug/kg SW846 8260B

1,4-Dichlorobenzene ND 5.0 ug/kg SW846 8260B

1,2-Dichlorobenzene ND 5.0 ug/kg SW846 8260B

Dichlorodifluoromethane ND 5.0 ug/kg SW846 8260B

1,1-Dichloroethane ND 5.0 ug/kg SW846 8260B

1,2-Dichloroethane ND 5.0 ug/kg SW846 8260B

1,1-Dichloroethene ND 5.0 ug/kg SW846 8260B

cis-1,2-Dichloroethene ND 5.0 ug/kg SW846 8260B

trans-1,2-Dichloroethene ND 5.0 ug/kg SW846 8260B

1,2-Dichloropropane ND 5.0 ug/kg SW846 8260B

cis-1,3-Dichloropropene ND 5.0 ug/kg SW846 8260B

trans-1,3-Dichloropropene ND 5.0 ug/kg SW846 8260B

Ethylbenzene ND 5.0 ug/kg SW846 8260B

2-Hexanone ND 5.0 ug/kg SW846 8260B

Isopropylbenzene ND 5.0 ug/kg SW846 8260B

Methyl acetate ND 5.0 ug/kg SW846 8260B

Methylene chloride ND 5.0 ug/kg SW846 8260B

Methylcyclohexane ND 5.0 ug/kg SW846 8260B

4-Methyl-2-pentanone ND 5.0 ug/kg SW846 8260B

Methyl tert-butyl ether ND 5.0 ug/kg SW846 8260B

Styrene ND 5.0 ug/kg SW846 8260B

1,1,2,2-Tetrachloroethane ND 5.0 ug/kg SW846 8260B

1,2,4-Trichloro- ND 5.0 ug/kg SW846 8260B

benzene

(Continued on next page)

C9K180557 43 of 161
METHOD BLANK REPORT

GC/MS Volatiles

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LP4721AA Matrix.........: Matrix.........: SOLID

REPORTING

PARAMETER _________________________ RESULT _______________ LIMIT _________ UNITS __________ METHOD _________________

Tetrachloroethene ND 5.0 ug/kg SW846 8260B

1,1,1-Trichloroethane ND 5.0 ug/kg SW846 8260B

1,1,2-Trichloroethane ND 5.0 ug/kg SW846 8260B

Trichloroethene ND 5.0 ug/kg SW846 8260B

Trichlorofluoromethane ND 5.0 ug/kg SW846 8260B

1,1,2-Trichloro- ND 5.0 ug/kg SW846 8260B

1,2,2-trifluoroethane

Toluene ND 5.0 ug/kg SW846 8260B

Vinyl chloride ND 5.0 ug/kg SW846 8260B

Xylenes (total) ND 15 ug/kg SW846 8260B

PERCENT RECOVERY

SURROGATE _________________________ RECOVERY ________ LIMITS __________

1,2-Dichloroethane-d4 105 (52 - 124)

Toluene-d8 96 (72 - 127)

4-Bromofluorobenzene 90 (63 - 120)

Dibromofluoromethane 104 (68 - 121)

NOTE(S): ___________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

C9K180557 44 of 161
LABORATORY CONTROL SAMPLE EVALUATION REPORT

GC/MS Volatiles

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LP2741AC Matrix.........: Matrix.........: WATER

LCS Lot-Sample#: LCS Lot-Sample#: C9K240000-345

Prep Date......: Prep Date......: 11/24/09 Analysis Date..: Analysis Date..: 11/24/09

Prep Batch #...: Prep Batch #...: 9328345 Analysis Time..: Analysis Time..: 14:11

Dilution Factor: Dilution Factor: 1

PERCENT RECOVERY

PARAMETER ________________________ RECOVERY ________ LIMITS __________ METHOD _________________

Benzene Benzene 114 (80 - 120) (80 - 120) SW846 8260B SW846 8260B

Chlorobenzene Chlorobenzene 99 (83 - 120) (83 - 120) SW846 8260B SW846 8260B

1,1-Dichloroethene 1,1-Dichloroethene 113 (69 - 127) (69 - 127) SW846 8260B SW846 8260B

Trichloroethene Trichloroethene 115 (80 - 120) (80 - 120) SW846 8260B SW846 8260B

Toluene Toluene 97 (80 - 124) (80 - 124) SW846 8260B SW846 8260B

PERCENT RECOVERY

SURROGATE _________________________ RECOVERY ________ LIMITS __________

1,2-Dichloroethane-d4 97 (62 - 123)

Toluene-d8 94 (80 - 120)

4-Bromofluorobenzene 91 (75 - 120)

Dibromofluoromethane 106 (80 - 120)

NOTE(S): _____________________________________________________________________________________ _____________________________________________________________________________________ 

Calculations are performed before rounding to avoid round-off errors in calculated results.

Bold print denotes control parameters

C9K180557 45 of 161
LABORATORY CONTROL SAMPLE EVALUATION REPORT

GC/MS Volatiles

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LP42D1AC Matrix.........: Matrix.........: WATER

LCS Lot-Sample#: LCS Lot-Sample#: C9K250000-174

Prep Date......: Prep Date......: 11/25/09 Analysis Date..: Analysis Date..: 11/25/09

Prep Batch #...: Prep Batch #...: 9329174 Analysis Time..: Analysis Time..: 10:15

Dilution Factor: Dilution Factor: 1

PERCENT RECOVERY

PARAMETER ________________________ RECOVERY ________ LIMITS __________ METHOD _________________

Benzene Benzene 106 (80 - 120) (80 - 120) SW846 8260B SW846 8260B

Chlorobenzene Chlorobenzene 106 (83 - 120) (83 - 120) SW846 8260B SW846 8260B

1,1-Dichloroethene 1,1-Dichloroethene 104 (69 - 127) (69 - 127) SW846 8260B SW846 8260B

Trichloroethene Trichloroethene 106 (80 - 120) (80 - 120) SW846 8260B SW846 8260B

Toluene Toluene 102 (80 - 124) (80 - 124) SW846 8260B SW846 8260B

PERCENT RECOVERY

SURROGATE _________________________ RECOVERY ________ LIMITS __________

1,2-Dichloroethane-d4 91 (62 - 123)

Toluene-d8 100 (80 - 120)

4-Bromofluorobenzene 91 (75 - 120)

Dibromofluoromethane 99 (80 - 120)

NOTE(S): _____________________________________________________________________________________ _____________________________________________________________________________________ 

Calculations are performed before rounding to avoid round-off errors in calculated results.

Bold print denotes control parameters

C9K180557 46 of 161
LABORATORY CONTROL SAMPLE EVALUATION REPORT

GC/MS Volatiles

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LP4721AC Matrix.........: Matrix.........: SOLID

LCS Lot-Sample#: LCS Lot-Sample#: C9K250000-221

Prep Date......: Prep Date......: 11/25/09 Analysis Date..: Analysis Date..: 11/25/09

Prep Batch #...: Prep Batch #...: 9329221 Analysis Time..: Analysis Time..: 11:02

Dilution Factor: Dilution Factor: 1

PERCENT RECOVERY

PARAMETER ________________________ RECOVERY ________ LIMITS __________ METHOD _________________

Benzene Benzene 98 (77 - 120) (77 - 120) SW846 8260B SW846 8260B

Chlorobenzene Chlorobenzene 103 (79 - 120) (79 - 120) SW846 8260B SW846 8260B

1,1-Dichloroethene 1,1-Dichloroethene 75 (59 - 129) (59 - 129) SW846 8260B SW846 8260B

Trichloroethene Trichloroethene 99 (76 - 119) (76 - 119) SW846 8260B SW846 8260B

Toluene Toluene 104 (78 - 124) (78 - 124) SW846 8260B SW846 8260B

PERCENT RECOVERY

SURROGATE _________________________ RECOVERY ________ LIMITS __________

1,2-Dichloroethane-d4 98 (52 - 124)

Toluene-d8 99 (72 - 127)

4-Bromofluorobenzene 94 (63 - 120)

Dibromofluoromethane 99 (68 - 121)

NOTE(S): _____________________________________________________________________________________ _____________________________________________________________________________________ 

Calculations are performed before rounding to avoid round-off errors in calculated results.

Bold print denotes control parameters

C9K180557 47 of 161
MATRIX SPIKE SAMPLE EVALUATION REPORT

GC/MS Volatiles

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPPF51A9-MS Matrix.........: Matrix.........: WATER

MS Lot-Sample #: MS Lot-Sample #: C9K180557-001 LPPF51CA-MSD

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9328229

Prep Date......: Prep Date......: 11/24/09 Analysis Date..: Analysis Date..: 11/24/09

Prep Batch #...: Prep Batch #...: 9328345 Analysis Time..: Analysis Time..: 14:43

Dilution Factor: Dilution Factor: 1

PERCENT RECOVERY RPD

PARAMETER _________________________ RECOVERY _________ LIMITS __________ RPD ____ LIMITS _________ METHOD _________________

Benzene Benzene 112 (80 - 120) (80 - 120) SW846 8260B SW846 8260B

115 (80 - 120) (80 - 120) 2.4 (0-20) SW846 8260B SW846 8260B

Chlorobenzene Chlorobenzene 97 (83 - 120) (83 - 120) SW846 8260B SW846 8260B

100 (83 - 120) (83 - 120) 3.2 (0-20) SW846 8260B SW846 8260B

1,1-Dichloroethene 1,1-Dichloroethene 110 (69 - 127) (69 - 127) SW846 8260B SW846 8260B

114 (69 - 127) (69 - 127) 3.4 (0-20) SW846 8260B SW846 8260B

Trichloroethene Trichloroethene 112 (80 - 120) (80 - 120) SW846 8260B SW846 8260B

116 (80 - 120) (80 - 120) 3.5 (0-20) SW846 8260B SW846 8260B

Toluene Toluene 96 (80 - 124) (80 - 124) SW846 8260B SW846 8260B

99 (80 - 124) (80 - 124) 3.1 (0-20) SW846 8260B SW846 8260B

PERCENT RECOVERY

SURROGATE _________________________ RECOVERY ________ LIMITS __________

1,2-Dichloroethane-d4 95 (62 - 123)

95 (62 - 123)

Toluene-d8 96 (80 - 120)

95 (80 - 120)

4-Bromofluorobenzene 90 (75 - 120)

90 (75 - 120)

Dibromofluoromethane 104 (80 - 120)

104 (80 - 120)

NOTE(S): ___________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

Bold print denotes control parameters

C9K180557 48 of 161
MATRIX SPIKE SAMPLE EVALUATION REPORT

GC/MS Volatiles

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPPGN1A7-MS Matrix.........: Matrix.........: WATER

MS Lot-Sample #: MS Lot-Sample #: C9K180557-002 LPPGN1A8-MSD

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9329152

Prep Date......: Prep Date......: 11/25/09 Analysis Date..: Analysis Date..: 11/25/09

Prep Batch #...: Prep Batch #...: 9329174 Analysis Time..: Analysis Time..: 10:47

Dilution Factor: Dilution Factor: 1

PERCENT RECOVERY RPD

PARAMETER _________________________ RECOVERY _________ LIMITS __________ RPD ____ LIMITS _________ METHOD _________________

Benzene Benzene 109 (80 - 120) (80 - 120) SW846 8260B SW846 8260B

108 (80 - 120) (80 - 120) 0.83 (0-20) SW846 8260B SW846 8260B

Chlorobenzene Chlorobenzene 109 (83 - 120) (83 - 120) SW846 8260B SW846 8260B

107 (83 - 120) (83 - 120) 1.7 (0-20) SW846 8260B SW846 8260B

1,1-Dichloroethene 1,1-Dichloroethene 108 (69 - 127) (69 - 127) SW846 8260B SW846 8260B

109 (69 - 127) (69 - 127) 1.1 (0-20) SW846 8260B SW846 8260B

Trichloroethene Trichloroethene 110 (80 - 120) (80 - 120) SW846 8260B SW846 8260B

109 (80 - 120) (80 - 120) 0.75 (0-20) SW846 8260B SW846 8260B

Toluene Toluene 108 (80 - 124) (80 - 124) SW846 8260B SW846 8260B

107 (80 - 124) (80 - 124) 0.37 (0-20) SW846 8260B SW846 8260B

PERCENT RECOVERY

SURROGATE _________________________ RECOVERY ________ LIMITS __________

1,2-Dichloroethane-d4 90 (62 - 123)

90 (62 - 123)

Toluene-d8 102 (80 - 120)

101 (80 - 120)

4-Bromofluorobenzene 91 (75 - 120)

91 (75 - 120)

Dibromofluoromethane 98 (80 - 120)

98 (80 - 120)

NOTE(S): ___________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

Bold print denotes control parameters

C9K180557 49 of 161
MATRIX SPIKE SAMPLE EVALUATION REPORT

GC/MS Volatiles

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPP3L1AE-MS Matrix.........: Matrix.........: SOLID

MS Lot-Sample #: MS Lot-Sample #: C9K180619-007 LPP3L1AF-MSD

Date Sampled...: Date Sampled...: 11/16/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9329143

Prep Date......: Prep Date......: 11/25/09 Analysis Date..: Analysis Date..: 11/25/09

Prep Batch #...: Prep Batch #...: 9329221 Analysis Time..: Analysis Time..: 11:25

Dilution Factor: Dilution Factor: 1 % Moisture.....: % Moisture.....: 31

PERCENT RECOVERY RPD

PARAMETER _________________________ RECOVERY _________ LIMITS __________ RPD ____ LIMITS _________ METHOD _________________

Benzene Benzene 97 (77 - 120) (77 - 120) SW846 8260B SW846 8260B

96 (77 - 120) (77 - 120) 1.0 (0-20) SW846 8260B SW846 8260B

Chlorobenzene Chlorobenzene 101 (79 - 120) (79 - 120) SW846 8260B SW846 8260B

94 (79 - 120) (79 - 120) 7.0 (0-20) SW846 8260B SW846 8260B

1,1-Dichloroethene 1,1-Dichloroethene 75 (59 - 129) (59 - 129) SW846 8260B SW846 8260B

84 (59 - 129) (59 - 129) 11 (0-25) SW846 8260B SW846 8260B

Trichloroethene Trichloroethene 99 (76 - 119) (76 - 119) SW846 8260B SW846 8260B

96 (76 - 119) (76 - 119) 2.7 (0-21) SW846 8260B SW846 8260B

Toluene Toluene 98 (78 - 124) (78 - 124) SW846 8260B SW846 8260B

90 (78 - 124) (78 - 124) 8.6 (0-21) SW846 8260B SW846 8260B

PERCENT RECOVERY

SURROGATE _________________________ RECOVERY ________ LIMITS __________

1,2-Dichloroethane-d4 100 (52 - 124)

97 (52 - 124)

Toluene-d8 99 (72 - 127)

91 (72 - 127)

4-Bromofluorobenzene 97 (63 - 120)

94 (63 - 120)

Dibromofluoromethane 105 (68 - 121)

105 (68 - 121)

NOTE(S): ___________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

Bold print denotes control parameters

Results and reporting limits have been adjusted for dry weight.

C9K180557 50 of 161
Clean Sites Environmental Services Inc

Client Sample ID: MW-1S

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-001 Work Order #...: Work Order #...: LPPF51AE Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......:

Prep Date......: Prep Date......: 11/20/09 Analysis Date..: Analysis Date..: 11/24/09

Prep Batch #...: Prep Batch #...: 9324281 Analysis Time..: Analysis Time..: 00:34

Dilution Factor: Dilution Factor: 0.94

Method.........: Method.........: SW846 8270C

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acenaphthene ND 1.9 ug/L

Acenaphthylene ND 1.9 ug/L

Acetophenone ND 9.4 ug/L

Anthracene ND 1.9 ug/L

Atrazine ND 9.4 ug/L

Benzo(a)anthracene ND 1.9 ug/L

Benzo(a)pyrene ND 1.9 ug/L

Benzo(b)fluoranthene ND 1.9 ug/L

Benzo(ghi)perylene ND 1.9 ug/L

Benzo(k)fluoranthene ND 1.9 ug/L

Benzaldehyde ND 9.4 ug/L

1,1'-Biphenyl ND 9.4 ug/L

bis(2-Chloroethoxy) ND 9.4 ug/L

methane

bis(2-Chloroethyl)- ND 1.9 ug/L

ether

bis(2-Ethylhexyl) ND 9.4 ug/L

phthalate

4-Bromophenyl phenyl ND 9.4 ug/L

ether

Butyl benzyl phthalate ND 9.4 ug/L

Caprolactam ND 47 ug/L

Carbazole ND 1.9 ug/L

4-Chloroaniline ND 9.4 ug/L

4-Chloro-3-methylphenol ND 9.4 ug/L

2-Chloronaphthalene ND 1.9 ug/L

2-Chlorophenol ND 9.4 ug/L

4-Chlorophenyl phenyl ND 9.4 ug/L

ether

Chrysene ND 1.9 ug/L

Dibenz(a,h)anthracene ND 1.9 ug/L

Dibenzofuran ND 9.4 ug/L

3,3'-Dichlorobenzidine ND 9.4 ug/L

2,4-Dichlorophenol ND 1.9 ug/L

Diethyl phthalate ND 9.4 ug/L

2,4-Dimethylphenol ND 9.4 ug/L

Dimethyl phthalate ND 9.4 ug/L

Di-n-butyl phthalate ND 9.4 ug/L

(Continued on next page)

C9K180557 51 of 161
Clean Sites Environmental Services Inc

Client Sample ID: MW-1S

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-001 Work Order #...: Work Order #...: LPPF51AE Matrix.........: Matrix.........: WATER

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

4,6-Dinitro- ND 47 ug/L

2-methylphenol

2,4-Dinitrophenol ND 47 ug/L

2,4-Dinitrotoluene ND 9.4 ug/L

2,6-Dinitrotoluene ND 9.4 ug/L

Di-n-octyl phthalate ND 9.4 ug/L

Fluoranthene ND 1.9 ug/L

Fluorene ND 1.9 ug/L

Hexachlorobenzene ND 1.9 ug/L

Hexachlorobutadiene ND 1.9 ug/L

Hexachlorocyclopenta- ND 9.4 ug/L

diene

Hexachloroethane ND 9.4 ug/L

Indeno(1,2,3-cd)pyrene ND 1.9 ug/L

Isophorone ND 9.4 ug/L

2-Methylnaphthalene ND 1.9 ug/L

2-Methylphenol ND 9.4 ug/L

4-Methylphenol ND 9.4 ug/L

Naphthalene ND 1.9 ug/L

2-Nitroaniline ND 47 ug/L

3-Nitroaniline ND 47 ug/L

4-Nitroaniline ND 47 ug/L

Nitrobenzene ND 1.9 ug/L

2-Nitrophenol ND 9.4 ug/L

4-Nitrophenol ND 47 ug/L

N-Nitrosodi-n-propyl- ND 1.9 ug/L

amine

N-Nitrosodiphenylamine ND 1.9 ug/L

2,2'-oxybis ND 1.9 ug/L

(1-Chloropropane)

Pentachlorophenol ND 9.4 ug/L

Phenanthrene ND 1.9 ug/L

Phenol ND 1.9 ug/L

Pyrene ND 1.9 ug/L

2,4,5-Trichloro- ND 9.4 ug/L

phenol

2,4,6-Trichloro- ND 9.4 ug/L

phenol

(Continued on next page)

C9K180557 52 of 161
Clean Sites Environmental Services Inc

Client Sample ID: MW-1S

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-001 Work Order #...: Work Order #...: LPPF51AE Matrix.........: Matrix.........: WATER

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

2,4,6-Tribromophenol 54 (33 - 122)

2-Fluorobiphenyl 50 (35 - 108)

2-Fluorophenol 58 (26 - 100)

Nitrobenzene-d5 58 (37 - 104)

Phenol-d5 58 (30 - 102)

Terphenyl-d14 39 (25 - 130)

C9K180557 53 of 161
Clean Sites Environmental Services Inc

Client Sample ID: MW-3S

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-002 Work Order #...: Work Order #...: LPPGN1AM Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......:

Prep Date......: Prep Date......: 11/20/09 Analysis Date..: Analysis Date..: 11/24/09

Prep Batch #...: Prep Batch #...: 9324281 Analysis Time..: Analysis Time..: 00:56

Dilution Factor: Dilution Factor: 0.94

Method.........: Method.........: SW846 8270C

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acenaphthene ND 1.9 ug/L

Acenaphthylene ND 1.9 ug/L

Acetophenone ND 9.4 ug/L

Anthracene ND 1.9 ug/L

Atrazine ND 9.4 ug/L

Benzo(a)anthracene ND 1.9 ug/L

Benzo(a)pyrene ND 1.9 ug/L

Benzo(b)fluoranthene ND 1.9 ug/L

Benzo(ghi)perylene ND 1.9 ug/L

Benzo(k)fluoranthene ND 1.9 ug/L

Benzaldehyde ND 9.4 ug/L

1,1'-Biphenyl ND 9.4 ug/L

bis(2-Chloroethoxy) ND 9.4 ug/L

methane

bis(2-Chloroethyl)- ND 1.9 ug/L

ether

bis(2-Ethylhexyl) ND 9.4 ug/L

phthalate

4-Bromophenyl phenyl ND 9.4 ug/L

ether

Butyl benzyl phthalate ND 9.4 ug/L

Caprolactam ND 47 ug/L

Carbazole ND 1.9 ug/L

4-Chloroaniline ND 9.4 ug/L

4-Chloro-3-methylphenol ND 9.4 ug/L

2-Chloronaphthalene ND 1.9 ug/L

2-Chlorophenol ND 9.4 ug/L

4-Chlorophenyl phenyl ND 9.4 ug/L

ether

Chrysene ND 1.9 ug/L

Dibenz(a,h)anthracene ND 1.9 ug/L

Dibenzofuran ND 9.4 ug/L

3,3'-Dichlorobenzidine ND 9.4 ug/L

2,4-Dichlorophenol ND 1.9 ug/L

Diethyl phthalate ND 9.4 ug/L

2,4-Dimethylphenol ND 9.4 ug/L

Dimethyl phthalate ND 9.4 ug/L

Di-n-butyl phthalate ND 9.4 ug/L

(Continued on next page)

C9K180557 54 of 161
Clean Sites Environmental Services Inc

Client Sample ID: MW-3S

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-002 Work Order #...: Work Order #...: LPPGN1AM Matrix.........: Matrix.........: WATER

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

4,6-Dinitro- ND 47 ug/L

2-methylphenol

2,4-Dinitrophenol ND 47 ug/L

2,4-Dinitrotoluene ND 9.4 ug/L

2,6-Dinitrotoluene ND 9.4 ug/L

Di-n-octyl phthalate ND 9.4 ug/L

Fluoranthene ND 1.9 ug/L

Fluorene ND 1.9 ug/L

Hexachlorobenzene ND 1.9 ug/L

Hexachlorobutadiene ND 1.9 ug/L

Hexachlorocyclopenta- ND 9.4 ug/L

diene

Hexachloroethane ND 9.4 ug/L

Indeno(1,2,3-cd)pyrene ND 1.9 ug/L

Isophorone ND 9.4 ug/L

2-Methylnaphthalene ND 1.9 ug/L

2-Methylphenol ND 9.4 ug/L

4-Methylphenol ND 9.4 ug/L

Naphthalene ND 1.9 ug/L

2-Nitroaniline ND 47 ug/L

3-Nitroaniline ND 47 ug/L

4-Nitroaniline ND 47 ug/L

Nitrobenzene ND 1.9 ug/L

2-Nitrophenol ND 9.4 ug/L

4-Nitrophenol ND 47 ug/L

N-Nitrosodi-n-propyl- ND 1.9 ug/L

amine

N-Nitrosodiphenylamine ND 1.9 ug/L

2,2'-oxybis ND 1.9 ug/L

(1-Chloropropane)

Pentachlorophenol ND 9.4 ug/L

Phenanthrene ND 1.9 ug/L

Phenol ND 1.9 ug/L

Pyrene ND 1.9 ug/L

2,4,5-Trichloro- ND 9.4 ug/L

phenol

2,4,6-Trichloro- ND 9.4 ug/L

phenol

(Continued on next page)

C9K180557 55 of 161
Clean Sites Environmental Services Inc

Client Sample ID: MW-3S

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-002 Work Order #...: Work Order #...: LPPGN1AM Matrix.........: Matrix.........: WATER

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

2,4,6-Tribromophenol 61 (33 - 122)

2-Fluorobiphenyl 57 (35 - 108)

2-Fluorophenol 63 (26 - 100)

Nitrobenzene-d5 70 (37 - 104)

Phenol-d5 63 (30 - 102)

Terphenyl-d14 51 (25 - 130)

C9K180557 56 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L2-S1

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-003 Work Order #...: Work Order #...: LPPGP1AM Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......:

Prep Date......: Prep Date......: 11/20/09 Analysis Date..: Analysis Date..: 11/25/09

Prep Batch #...: Prep Batch #...: 9324281 Analysis Time..: Analysis Time..: 13:31

Dilution Factor: Dilution Factor: 0.94

Method.........: Method.........: SW846 8270C

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acenaphthene ND 1.9 ug/L

Acenaphthylene ND 1.9 ug/L

Acetophenone ND 9.4 ug/L

Anthracene ND 1.9 ug/L

Atrazine ND 9.4 ug/L

Benzo(a)anthracene ND 1.9 ug/L

Benzo(a)pyrene ND 1.9 ug/L

Benzo(b)fluoranthene ND 1.9 ug/L

Benzo(ghi)perylene ND 1.9 ug/L

Benzo(k)fluoranthene ND 1.9 ug/L

Benzaldehyde ND 9.4 ug/L

1,1'-Biphenyl ND 9.4 ug/L

bis(2-Chloroethoxy) ND 9.4 ug/L

methane

bis(2-Chloroethyl)- ND 1.9 ug/L

ether

bis(2-Ethylhexyl) ND 9.4 ug/L

phthalate

4-Bromophenyl phenyl ND 9.4 ug/L

ether

Butyl benzyl phthalate ND 9.4 ug/L

Caprolactam ND 47 ug/L

Carbazole ND 1.9 ug/L

4-Chloroaniline ND 9.4 ug/L

4-Chloro-3-methylphenol ND 9.4 ug/L

2-Chloronaphthalene ND 1.9 ug/L

2-Chlorophenol ND 9.4 ug/L

4-Chlorophenyl phenyl ND 9.4 ug/L

ether

Chrysene ND 1.9 ug/L

Dibenz(a,h)anthracene ND 1.9 ug/L

Dibenzofuran ND 9.4 ug/L

3,3'-Dichlorobenzidine ND 9.4 ug/L

2,4-Dichlorophenol ND 1.9 ug/L

Diethyl phthalate ND 9.4 ug/L

2,4-Dimethylphenol ND 9.4 ug/L

Dimethyl phthalate ND 9.4 ug/L

Di-n-butyl phthalate ND 9.4 ug/L

(Continued on next page)

C9K180557 57 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L2-S1

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-003 Work Order #...: Work Order #...: LPPGP1AM Matrix.........: Matrix.........: WATER

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

4,6-Dinitro- ND 47 ug/L

2-methylphenol

2,4-Dinitrophenol ND 47 ug/L

2,4-Dinitrotoluene ND 9.4 ug/L

2,6-Dinitrotoluene ND 9.4 ug/L

Di-n-octyl phthalate ND 9.4 ug/L

Fluoranthene ND 1.9 ug/L

Fluorene ND 1.9 ug/L

Hexachlorobenzene ND 1.9 ug/L

Hexachlorobutadiene ND 1.9 ug/L

Hexachlorocyclopenta- ND 9.4 ug/L

diene

Hexachloroethane ND 9.4 ug/L

Indeno(1,2,3-cd)pyrene ND 1.9 ug/L

Isophorone ND 9.4 ug/L

2-Methylnaphthalene ND 1.9 ug/L

2-Methylphenol ND 9.4 ug/L

4-Methylphenol ND 9.4 ug/L

Naphthalene ND 1.9 ug/L

2-Nitroaniline ND 47 ug/L

3-Nitroaniline ND 47 ug/L

4-Nitroaniline ND 47 ug/L

Nitrobenzene ND 1.9 ug/L

2-Nitrophenol ND 9.4 ug/L

4-Nitrophenol ND 47 ug/L

N-Nitrosodi-n-propyl- ND 1.9 ug/L

amine

N-Nitrosodiphenylamine ND 1.9 ug/L

2,2'-oxybis ND 1.9 ug/L

(1-Chloropropane)

Pentachlorophenol ND 9.4 ug/L

Phenanthrene ND 1.9 ug/L

Phenol ND 1.9 ug/L

Pyrene ND 1.9 ug/L

2,4,5-Trichloro- ND 9.4 ug/L

phenol

2,4,6-Trichloro- ND 9.4 ug/L

phenol

(Continued on next page)

C9K180557 58 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L2-S1

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-003 Work Order #...: Work Order #...: LPPGP1AM Matrix.........: Matrix.........: WATER

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

2,4,6-Tribromophenol 70 (33 - 122)

2-Fluorobiphenyl 50 (35 - 108)

2-Fluorophenol 44 (26 - 100)

Nitrobenzene-d5 48 (37 - 104)

Phenol-d5 48 (30 - 102)

Terphenyl-d14 69 (25 - 130)

C9K180557 59 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L1-S1

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-006 Work Order #...: Work Order #...: LPPG11AD Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......:

Prep Date......: Prep Date......: 11/20/09 Analysis Date..: Analysis Date..: 11/25/09

Prep Batch #...: Prep Batch #...: 9324281 Analysis Time..: Analysis Time..: 13:53

Dilution Factor: Dilution Factor: 0.94

Method.........: Method.........: SW846 8270C

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acenaphthene ND 1.9 ug/L

Acenaphthylene ND 1.9 ug/L

Acetophenone ND 9.4 ug/L

Anthracene ND 1.9 ug/L

Atrazine ND 9.4 ug/L

Benzo(a)anthracene ND 1.9 ug/L

Benzo(a)pyrene ND 1.9 ug/L

Benzo(b)fluoranthene ND 1.9 ug/L

Benzo(ghi)perylene ND 1.9 ug/L

Benzo(k)fluoranthene ND 1.9 ug/L

Benzaldehyde ND 9.4 ug/L

1,1'-Biphenyl ND 9.4 ug/L

bis(2-Chloroethoxy) ND 9.4 ug/L

methane

bis(2-Chloroethyl)- ND 1.9 ug/L

ether

bis(2-Ethylhexyl) ND 9.4 ug/L

phthalate

4-Bromophenyl phenyl ND 9.4 ug/L

ether

Butyl benzyl phthalate ND 9.4 ug/L

Caprolactam ND 47 ug/L

Carbazole ND 1.9 ug/L

4-Chloroaniline ND 9.4 ug/L

4-Chloro-3-methylphenol ND 9.4 ug/L

2-Chloronaphthalene ND 1.9 ug/L

2-Chlorophenol ND 9.4 ug/L

4-Chlorophenyl phenyl ND 9.4 ug/L

ether

Chrysene ND 1.9 ug/L

Dibenz(a,h)anthracene ND 1.9 ug/L

Dibenzofuran ND 9.4 ug/L

3,3'-Dichlorobenzidine ND 9.4 ug/L

2,4-Dichlorophenol ND 1.9 ug/L

Diethyl phthalate ND 9.4 ug/L

2,4-Dimethylphenol ND 9.4 ug/L

Dimethyl phthalate ND 9.4 ug/L

Di-n-butyl phthalate ND 9.4 ug/L

(Continued on next page)

C9K180557 60 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L1-S1

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-006 Work Order #...: Work Order #...: LPPG11AD Matrix.........: Matrix.........: WATER

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

4,6-Dinitro- ND 47 ug/L

2-methylphenol

2,4-Dinitrophenol ND 47 ug/L

2,4-Dinitrotoluene ND 9.4 ug/L

2,6-Dinitrotoluene ND 9.4 ug/L

Di-n-octyl phthalate ND 9.4 ug/L

Fluoranthene ND 1.9 ug/L

Fluorene ND 1.9 ug/L

Hexachlorobenzene ND 1.9 ug/L

Hexachlorobutadiene ND 1.9 ug/L

Hexachlorocyclopenta- ND 9.4 ug/L

diene

Hexachloroethane ND 9.4 ug/L

Indeno(1,2,3-cd)pyrene ND 1.9 ug/L

Isophorone ND 9.4 ug/L

2-Methylnaphthalene ND 1.9 ug/L

2-Methylphenol ND 9.4 ug/L

4-Methylphenol ND 9.4 ug/L

Naphthalene ND 1.9 ug/L

2-Nitroaniline ND 47 ug/L

3-Nitroaniline ND 47 ug/L

4-Nitroaniline ND 47 ug/L

Nitrobenzene ND 1.9 ug/L

2-Nitrophenol ND 9.4 ug/L

4-Nitrophenol ND 47 ug/L

N-Nitrosodi-n-propyl- ND 1.9 ug/L

amine

N-Nitrosodiphenylamine ND 1.9 ug/L

2,2'-oxybis ND 1.9 ug/L

(1-Chloropropane)

Pentachlorophenol ND 9.4 ug/L

Phenanthrene ND 1.9 ug/L

Phenol ND 1.9 ug/L

Pyrene ND 1.9 ug/L

2,4,5-Trichloro- ND 9.4 ug/L

phenol

2,4,6-Trichloro- ND 9.4 ug/L

phenol

(Continued on next page)

C9K180557 61 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L1-S1

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-006 Work Order #...: Work Order #...: LPPG11AD Matrix.........: Matrix.........: WATER

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

2,4,6-Tribromophenol 66 (33 - 122)

2-Fluorobiphenyl 55 (35 - 108)

2-Fluorophenol 58 (26 - 100)

Nitrobenzene-d5 58 (37 - 104)

Phenol-d5 59 (30 - 102)

Terphenyl-d14 55 (25 - 130)

C9K180557 62 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L1-S3

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-007 Work Order #...: Work Order #...: LPPG61AK Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......:

Prep Date......: Prep Date......: 11/20/09 Analysis Date..: Analysis Date..: 11/25/09

Prep Batch #...: Prep Batch #...: 9324281 Analysis Time..: Analysis Time..: 14:16

Dilution Factor: Dilution Factor: 0.94

Method.........: Method.........: SW846 8270C

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acenaphthene ND 1.9 ug/L

Acenaphthylene ND 1.9 ug/L

Acetophenone ND 9.4 ug/L

Anthracene ND 1.9 ug/L

Atrazine ND 9.4 ug/L

Benzo(a)anthracene ND 1.9 ug/L

Benzo(a)pyrene ND 1.9 ug/L

Benzo(b)fluoranthene ND 1.9 ug/L

Benzo(ghi)perylene ND 1.9 ug/L

Benzo(k)fluoranthene ND 1.9 ug/L

Benzaldehyde ND 9.4 ug/L

1,1'-Biphenyl ND 9.4 ug/L

bis(2-Chloroethoxy) ND 9.4 ug/L

methane

bis(2-Chloroethyl)- ND 1.9 ug/L

ether

bis(2-Ethylhexyl) ND 9.4 ug/L

phthalate

4-Bromophenyl phenyl ND 9.4 ug/L

ether

Butyl benzyl phthalate ND 9.4 ug/L

Caprolactam ND 47 ug/L

Carbazole ND 1.9 ug/L

4-Chloroaniline ND 9.4 ug/L

4-Chloro-3-methylphenol ND 9.4 ug/L

2-Chloronaphthalene ND 1.9 ug/L

2-Chlorophenol ND 9.4 ug/L

4-Chlorophenyl phenyl ND 9.4 ug/L

ether

Chrysene ND 1.9 ug/L

Dibenz(a,h)anthracene ND 1.9 ug/L

Dibenzofuran ND 9.4 ug/L

3,3'-Dichlorobenzidine ND 9.4 ug/L

2,4-Dichlorophenol ND 1.9 ug/L

Diethyl phthalate ND 9.4 ug/L

2,4-Dimethylphenol ND 9.4 ug/L

Dimethyl phthalate ND 9.4 ug/L

Di-n-butyl phthalate ND 9.4 ug/L

(Continued on next page)

C9K180557 63 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L1-S3

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-007 Work Order #...: Work Order #...: LPPG61AK Matrix.........: Matrix.........: WATER

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

4,6-Dinitro- ND 47 ug/L

2-methylphenol

2,4-Dinitrophenol ND 47 ug/L

2,4-Dinitrotoluene ND 9.4 ug/L

2,6-Dinitrotoluene ND 9.4 ug/L

Di-n-octyl phthalate ND 9.4 ug/L

Fluoranthene ND 1.9 ug/L

Fluorene ND 1.9 ug/L

Hexachlorobenzene ND 1.9 ug/L

Hexachlorobutadiene ND 1.9 ug/L

Hexachlorocyclopenta- ND 9.4 ug/L

diene

Hexachloroethane ND 9.4 ug/L

Indeno(1,2,3-cd)pyrene ND 1.9 ug/L

Isophorone ND 9.4 ug/L

2-Methylnaphthalene ND 1.9 ug/L

2-Methylphenol ND 9.4 ug/L

4-Methylphenol ND 9.4 ug/L

Naphthalene ND 1.9 ug/L

2-Nitroaniline ND 47 ug/L

3-Nitroaniline ND 47 ug/L

4-Nitroaniline ND 47 ug/L

Nitrobenzene ND 1.9 ug/L

2-Nitrophenol ND 9.4 ug/L

4-Nitrophenol ND 47 ug/L

N-Nitrosodi-n-propyl- ND 1.9 ug/L

amine

N-Nitrosodiphenylamine ND 1.9 ug/L

2,2'-oxybis ND 1.9 ug/L

(1-Chloropropane)

Pentachlorophenol ND 9.4 ug/L

Phenanthrene ND 1.9 ug/L

Phenol ND 1.9 ug/L

Pyrene ND 1.9 ug/L

2,4,5-Trichloro- ND 9.4 ug/L

phenol

2,4,6-Trichloro- ND 9.4 ug/L

phenol

(Continued on next page)

C9K180557 64 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L1-S3

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-007 Work Order #...: Work Order #...: LPPG61AK Matrix.........: Matrix.........: WATER

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

2,4,6-Tribromophenol 58 (33 - 122)

2-Fluorobiphenyl 51 (35 - 108)

2-Fluorophenol 51 (26 - 100)

Nitrobenzene-d5 50 (37 - 104)

Phenol-d5 52 (30 - 102)

Terphenyl-d14 38 (25 - 130)

C9K180557 65 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L1-S4

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-008 Work Order #...: Work Order #...: LPPG81AR Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......:

Prep Date......: Prep Date......: 11/20/09 Analysis Date..: Analysis Date..: 11/25/09

Prep Batch #...: Prep Batch #...: 9324281 Analysis Time..: Analysis Time..: 14:38

Dilution Factor: Dilution Factor: 0.94

Method.........: Method.........: SW846 8270C

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acenaphthene ND 1.9 ug/L

Acenaphthylene ND 1.9 ug/L

Acetophenone ND 9.4 ug/L

Anthracene ND 1.9 ug/L

Atrazine ND 9.4 ug/L

Benzo(a)anthracene ND 1.9 ug/L

Benzo(a)pyrene ND 1.9 ug/L

Benzo(b)fluoranthene ND 1.9 ug/L

Benzo(ghi)perylene ND 1.9 ug/L

Benzo(k)fluoranthene ND 1.9 ug/L

Benzaldehyde ND 9.4 ug/L

1,1'-Biphenyl ND 9.4 ug/L

bis(2-Chloroethoxy) ND 9.4 ug/L

methane

bis(2-Chloroethyl)- ND 1.9 ug/L

ether

bis(2-Ethylhexyl) ND 9.4 ug/L

phthalate

4-Bromophenyl phenyl ND 9.4 ug/L

ether

Butyl benzyl phthalate ND 9.4 ug/L

Caprolactam ND 47 ug/L

Carbazole ND 1.9 ug/L

4-Chloroaniline ND 9.4 ug/L

4-Chloro-3-methylphenol ND 9.4 ug/L

2-Chloronaphthalene ND 1.9 ug/L

2-Chlorophenol ND 9.4 ug/L

4-Chlorophenyl phenyl ND 9.4 ug/L

ether

Chrysene ND 1.9 ug/L

Dibenz(a,h)anthracene ND 1.9 ug/L

Dibenzofuran ND 9.4 ug/L

3,3'-Dichlorobenzidine ND 9.4 ug/L

2,4-Dichlorophenol ND 1.9 ug/L

Diethyl phthalate ND 9.4 ug/L

2,4-Dimethylphenol ND 9.4 ug/L

Dimethyl phthalate ND 9.4 ug/L

Di-n-butyl phthalate ND 9.4 ug/L

(Continued on next page)

C9K180557 66 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L1-S4

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-008 Work Order #...: Work Order #...: LPPG81AR Matrix.........: Matrix.........: WATER

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

4,6-Dinitro- ND 47 ug/L

2-methylphenol

2,4-Dinitrophenol ND 47 ug/L

2,4-Dinitrotoluene ND 9.4 ug/L

2,6-Dinitrotoluene ND 9.4 ug/L

Di-n-octyl phthalate ND 9.4 ug/L

Fluoranthene ND 1.9 ug/L

Fluorene ND 1.9 ug/L

Hexachlorobenzene ND 1.9 ug/L

Hexachlorobutadiene ND 1.9 ug/L

Hexachlorocyclopenta- ND 9.4 ug/L

diene

Hexachloroethane ND 9.4 ug/L

Indeno(1,2,3-cd)pyrene ND 1.9 ug/L

Isophorone ND 9.4 ug/L

2-Methylnaphthalene ND 1.9 ug/L

2-Methylphenol ND 9.4 ug/L

4-Methylphenol ND 9.4 ug/L

Naphthalene ND 1.9 ug/L

2-Nitroaniline ND 47 ug/L

3-Nitroaniline ND 47 ug/L

4-Nitroaniline ND 47 ug/L

Nitrobenzene ND 1.9 ug/L

2-Nitrophenol ND 9.4 ug/L

4-Nitrophenol ND 47 ug/L

N-Nitrosodi-n-propyl- ND 1.9 ug/L

amine

N-Nitrosodiphenylamine ND 1.9 ug/L

2,2'-oxybis ND 1.9 ug/L

(1-Chloropropane)

Pentachlorophenol ND 9.4 ug/L

Phenanthrene ND 1.9 ug/L

Phenol ND 1.9 ug/L

Pyrene ND 1.9 ug/L

2,4,5-Trichloro- ND 9.4 ug/L

phenol

2,4,6-Trichloro- ND 9.4 ug/L

phenol

(Continued on next page)

C9K180557 67 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L1-S4

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-008 Work Order #...: Work Order #...: LPPG81AR Matrix.........: Matrix.........: WATER

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

2,4,6-Tribromophenol 64 (33 - 122)

2-Fluorobiphenyl 52 (35 - 108)

2-Fluorophenol 54 (26 - 100)

Nitrobenzene-d5 57 (37 - 104)

Phenol-d5 57 (30 - 102)

Terphenyl-d14 49 (25 - 130)

C9K180557 68 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SW-1

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-009 Work Order #...: Work Order #...: LPPHA1A0 Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......:

Prep Date......: Prep Date......: 11/20/09 Analysis Date..: Analysis Date..: 11/25/09

Prep Batch #...: Prep Batch #...: 9324281 Analysis Time..: Analysis Time..: 15:01

Dilution Factor: Dilution Factor: 0.94

Method.........: Method.........: SW846 8270C

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acenaphthene ND 1.9 ug/L

Acenaphthylene ND 1.9 ug/L

Acetophenone ND 9.4 ug/L

Anthracene ND 1.9 ug/L

Atrazine ND 9.4 ug/L

Benzo(a)anthracene ND 1.9 ug/L

Benzo(a)pyrene ND 1.9 ug/L

Benzo(b)fluoranthene ND 1.9 ug/L

Benzo(ghi)perylene ND 1.9 ug/L

Benzo(k)fluoranthene ND 1.9 ug/L

Benzaldehyde ND 9.4 ug/L

1,1'-Biphenyl ND 9.4 ug/L

bis(2-Chloroethoxy) ND 9.4 ug/L

methane

bis(2-Chloroethyl)- ND 1.9 ug/L

ether

bis(2-Ethylhexyl) ND 9.4 ug/L

phthalate

4-Bromophenyl phenyl ND 9.4 ug/L

ether

Butyl benzyl phthalate ND 9.4 ug/L

Caprolactam ND 47 ug/L

Carbazole ND 1.9 ug/L

4-Chloroaniline ND 9.4 ug/L

4-Chloro-3-methylphenol ND 9.4 ug/L

2-Chloronaphthalene ND 1.9 ug/L

2-Chlorophenol ND 9.4 ug/L

4-Chlorophenyl phenyl ND 9.4 ug/L

ether

Chrysene ND 1.9 ug/L

Dibenz(a,h)anthracene ND 1.9 ug/L

Dibenzofuran ND 9.4 ug/L

3,3'-Dichlorobenzidine ND 9.4 ug/L

2,4-Dichlorophenol ND 1.9 ug/L

Diethyl phthalate ND 9.4 ug/L

2,4-Dimethylphenol ND 9.4 ug/L

Dimethyl phthalate ND 9.4 ug/L

Di-n-butyl phthalate ND 9.4 ug/L

(Continued on next page)

C9K180557 69 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SW-1

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-009 Work Order #...: Work Order #...: LPPHA1A0 Matrix.........: Matrix.........: WATER

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

4,6-Dinitro- ND 47 ug/L

2-methylphenol

2,4-Dinitrophenol ND 47 ug/L

2,4-Dinitrotoluene ND 9.4 ug/L

2,6-Dinitrotoluene ND 9.4 ug/L

Di-n-octyl phthalate ND 9.4 ug/L

Fluoranthene ND 1.9 ug/L

Fluorene ND 1.9 ug/L

Hexachlorobenzene ND 1.9 ug/L

Hexachlorobutadiene ND 1.9 ug/L

Hexachlorocyclopenta- ND 9.4 ug/L

diene

Hexachloroethane ND 9.4 ug/L

Indeno(1,2,3-cd)pyrene ND 1.9 ug/L

Isophorone ND 9.4 ug/L

2-Methylnaphthalene ND 1.9 ug/L

2-Methylphenol ND 9.4 ug/L

4-Methylphenol ND 9.4 ug/L

Naphthalene ND 1.9 ug/L

2-Nitroaniline ND 47 ug/L

3-Nitroaniline ND 47 ug/L

4-Nitroaniline ND 47 ug/L

Nitrobenzene ND 1.9 ug/L

2-Nitrophenol ND 9.4 ug/L

4-Nitrophenol ND 47 ug/L

N-Nitrosodi-n-propyl- ND 1.9 ug/L

amine

N-Nitrosodiphenylamine ND 1.9 ug/L

2,2'-oxybis ND 1.9 ug/L

(1-Chloropropane)

Pentachlorophenol ND 9.4 ug/L

Phenanthrene ND 1.9 ug/L

Phenol ND 1.9 ug/L

Pyrene ND 1.9 ug/L

2,4,5-Trichloro- ND 9.4 ug/L

phenol

2,4,6-Trichloro- ND 9.4 ug/L

phenol

(Continued on next page)

C9K180557 70 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SW-1

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-009 Work Order #...: Work Order #...: LPPHA1A0 Matrix.........: Matrix.........: WATER

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

2,4,6-Tribromophenol 68 (33 - 122)

2-Fluorobiphenyl 57 (35 - 108)

2-Fluorophenol 62 (26 - 100)

Nitrobenzene-d5 59 (37 - 104)

Phenol-d5 64 (30 - 102)

Terphenyl-d14 29 (25 - 130)

C9K180557 71 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SW-2

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-010 Work Order #...: Work Order #...: LPPHF1AA Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......:

Prep Date......: Prep Date......: 11/20/09 Analysis Date..: Analysis Date..: 11/25/09

Prep Batch #...: Prep Batch #...: 9324281 Analysis Time..: Analysis Time..: 15:24

Dilution Factor: Dilution Factor: 0.94

Method.........: Method.........: SW846 8270C

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acenaphthene ND 1.9 ug/L

Acenaphthylene ND 1.9 ug/L

Acetophenone ND 9.4 ug/L

Anthracene ND 1.9 ug/L

Atrazine ND 9.4 ug/L

Benzo(a)anthracene ND 1.9 ug/L

Benzo(a)pyrene ND 1.9 ug/L

Benzo(b)fluoranthene ND 1.9 ug/L

Benzo(ghi)perylene ND 1.9 ug/L

Benzo(k)fluoranthene ND 1.9 ug/L

Benzaldehyde ND 9.4 ug/L

1,1'-Biphenyl ND 9.4 ug/L

bis(2-Chloroethoxy) ND 9.4 ug/L

methane

bis(2-Chloroethyl)- ND 1.9 ug/L

ether

bis(2-Ethylhexyl) ND 9.4 ug/L

phthalate

4-Bromophenyl phenyl ND 9.4 ug/L

ether

Butyl benzyl phthalate ND 9.4 ug/L

Caprolactam ND 47 ug/L

Carbazole ND 1.9 ug/L

4-Chloroaniline ND 9.4 ug/L

4-Chloro-3-methylphenol ND 9.4 ug/L

2-Chloronaphthalene ND 1.9 ug/L

2-Chlorophenol ND 9.4 ug/L

4-Chlorophenyl phenyl ND 9.4 ug/L

ether

Chrysene ND 1.9 ug/L

Dibenz(a,h)anthracene ND 1.9 ug/L

Dibenzofuran ND 9.4 ug/L

3,3'-Dichlorobenzidine ND 9.4 ug/L

2,4-Dichlorophenol ND 1.9 ug/L

Diethyl phthalate ND 9.4 ug/L

2,4-Dimethylphenol ND 9.4 ug/L

Dimethyl phthalate ND 9.4 ug/L

Di-n-butyl phthalate ND 9.4 ug/L

(Continued on next page)

C9K180557 72 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SW-2

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-010 Work Order #...: Work Order #...: LPPHF1AA Matrix.........: Matrix.........: WATER

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

4,6-Dinitro- ND 47 ug/L

2-methylphenol

2,4-Dinitrophenol ND 47 ug/L

2,4-Dinitrotoluene ND 9.4 ug/L

2,6-Dinitrotoluene ND 9.4 ug/L

Di-n-octyl phthalate ND 9.4 ug/L

Fluoranthene ND 1.9 ug/L

Fluorene ND 1.9 ug/L

Hexachlorobenzene ND 1.9 ug/L

Hexachlorobutadiene ND 1.9 ug/L

Hexachlorocyclopenta- ND 9.4 ug/L

diene

Hexachloroethane ND 9.4 ug/L

Indeno(1,2,3-cd)pyrene ND 1.9 ug/L

Isophorone ND 9.4 ug/L

2-Methylnaphthalene ND 1.9 ug/L

2-Methylphenol ND 9.4 ug/L

4-Methylphenol ND 9.4 ug/L

Naphthalene ND 1.9 ug/L

2-Nitroaniline ND 47 ug/L

3-Nitroaniline ND 47 ug/L

4-Nitroaniline ND 47 ug/L

Nitrobenzene ND 1.9 ug/L

2-Nitrophenol ND 9.4 ug/L

4-Nitrophenol ND 47 ug/L

N-Nitrosodi-n-propyl- ND 1.9 ug/L

amine

N-Nitrosodiphenylamine ND 1.9 ug/L

2,2'-oxybis ND 1.9 ug/L

(1-Chloropropane)

Pentachlorophenol ND 9.4 ug/L

Phenanthrene ND 1.9 ug/L

Phenol ND 1.9 ug/L

Pyrene ND 1.9 ug/L

2,4,5-Trichloro- ND 9.4 ug/L

phenol

2,4,6-Trichloro- ND 9.4 ug/L

phenol

(Continued on next page)

C9K180557 73 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SW-2

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-010 Work Order #...: Work Order #...: LPPHF1AA Matrix.........: Matrix.........: WATER

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

2,4,6-Tribromophenol 50 (33 - 122)

2-Fluorobiphenyl 43 (35 - 108)

2-Fluorophenol 43 (26 - 100)

Nitrobenzene-d5 47 (37 - 104)

Phenol-d5 41 (30 - 102)

Terphenyl-d14 32 (25 - 130)

C9K180557 74 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SW-3

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-011 Work Order #...: Work Order #...: LPPHG1AA Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......:

Prep Date......: Prep Date......: 11/20/09 Analysis Date..: Analysis Date..: 11/25/09

Prep Batch #...: Prep Batch #...: 9324281 Analysis Time..: Analysis Time..: 15:46

Dilution Factor: Dilution Factor: 0.94

Method.........: Method.........: SW846 8270C

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acenaphthene ND 1.9 ug/L

Acenaphthylene ND 1.9 ug/L

Acetophenone ND 9.4 ug/L

Anthracene ND 1.9 ug/L

Atrazine ND 9.4 ug/L

Benzo(a)anthracene ND 1.9 ug/L

Benzo(a)pyrene ND 1.9 ug/L

Benzo(b)fluoranthene ND 1.9 ug/L

Benzo(ghi)perylene ND 1.9 ug/L

Benzo(k)fluoranthene ND 1.9 ug/L

Benzaldehyde ND 9.4 ug/L

1,1'-Biphenyl ND 9.4 ug/L

bis(2-Chloroethoxy) ND 9.4 ug/L

methane

bis(2-Chloroethyl)- ND 1.9 ug/L

ether

bis(2-Ethylhexyl) ND 9.4 ug/L

phthalate

4-Bromophenyl phenyl ND 9.4 ug/L

ether

Butyl benzyl phthalate ND 9.4 ug/L

Caprolactam ND 47 ug/L

Carbazole ND 1.9 ug/L

4-Chloroaniline ND 9.4 ug/L

4-Chloro-3-methylphenol ND 9.4 ug/L

2-Chloronaphthalene ND 1.9 ug/L

2-Chlorophenol ND 9.4 ug/L

4-Chlorophenyl phenyl ND 9.4 ug/L

ether

Chrysene ND 1.9 ug/L

Dibenz(a,h)anthracene ND 1.9 ug/L

Dibenzofuran ND 9.4 ug/L

3,3'-Dichlorobenzidine ND 9.4 ug/L

2,4-Dichlorophenol ND 1.9 ug/L

Diethyl phthalate ND 9.4 ug/L

2,4-Dimethylphenol ND 9.4 ug/L

Dimethyl phthalate ND 9.4 ug/L

Di-n-butyl phthalate ND 9.4 ug/L

(Continued on next page)

C9K180557 75 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SW-3

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-011 Work Order #...: Work Order #...: LPPHG1AA Matrix.........: Matrix.........: WATER

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

4,6-Dinitro- ND 47 ug/L

2-methylphenol

2,4-Dinitrophenol ND 47 ug/L

2,4-Dinitrotoluene ND 9.4 ug/L

2,6-Dinitrotoluene ND 9.4 ug/L

Di-n-octyl phthalate ND 9.4 ug/L

Fluoranthene ND 1.9 ug/L

Fluorene ND 1.9 ug/L

Hexachlorobenzene ND 1.9 ug/L

Hexachlorobutadiene ND 1.9 ug/L

Hexachlorocyclopenta- ND 9.4 ug/L

diene

Hexachloroethane ND 9.4 ug/L

Indeno(1,2,3-cd)pyrene ND 1.9 ug/L

Isophorone ND 9.4 ug/L

2-Methylnaphthalene ND 1.9 ug/L

2-Methylphenol ND 9.4 ug/L

4-Methylphenol ND 9.4 ug/L

Naphthalene ND 1.9 ug/L

2-Nitroaniline ND 47 ug/L

3-Nitroaniline ND 47 ug/L

4-Nitroaniline ND 47 ug/L

Nitrobenzene ND 1.9 ug/L

2-Nitrophenol ND 9.4 ug/L

4-Nitrophenol ND 47 ug/L

N-Nitrosodi-n-propyl- ND 1.9 ug/L

amine

N-Nitrosodiphenylamine ND 1.9 ug/L

2,2'-oxybis ND 1.9 ug/L

(1-Chloropropane)

Pentachlorophenol ND 9.4 ug/L

Phenanthrene ND 1.9 ug/L

Phenol ND 1.9 ug/L

Pyrene ND 1.9 ug/L

2,4,5-Trichloro- ND 9.4 ug/L

phenol

2,4,6-Trichloro- ND 9.4 ug/L

phenol

(Continued on next page)

C9K180557 76 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SW-3

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-011 Work Order #...: Work Order #...: LPPHG1AA Matrix.........: Matrix.........: WATER

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

2,4,6-Tribromophenol 51 (33 - 122)

2-Fluorobiphenyl 42 (35 - 108)

2-Fluorophenol 42 (26 - 100)

Nitrobenzene-d5 45 (37 - 104)

Phenol-d5 42 (30 - 102)

Terphenyl-d14 32 (25 - 130)

C9K180557 77 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SED-1

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-012 Work Order #...: Work Order #...: LPPHK1AE Matrix.........: Matrix.........: SOLID

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9323002

Prep Date......: Prep Date......: 11/19/09 Analysis Date..: Analysis Date..: 11/20/09

Prep Batch #...: Prep Batch #...: 9323010 Analysis Time..: Analysis Time..: 00:18

Dilution Factor: Dilution Factor: 1

% Moisture.....: % Moisture.....: 20 Method.........: Method.........: SW846 8270C

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acenaphthene ND 83 ug/kg

Acenaphthylene ND 83 ug/kg

Acetophenone ND 410 ug/kg

Anthracene ND 83 ug/kg

Atrazine ND 410 ug/kg

Benzo(a)anthracene ND 83 ug/kg

Benzo(a)pyrene ND 83 ug/kg

Benzo(b)fluoranthene ND 83 ug/kg

Benzo(ghi)perylene ND 83 ug/kg

Benzo(k)fluoranthene ND 83 ug/kg

Benzaldehyde ND 410 ug/kg

1,1'-Biphenyl ND 410 ug/kg

bis(2-Chloroethoxy) ND 410 ug/kg

methane

bis(2-Chloroethyl)- ND 83 ug/kg

ether

bis(2-Ethylhexyl) ND 410 ug/kg

phthalate

4-Bromophenyl phenyl ND 410 ug/kg

ether

Butyl benzyl phthalate ND 410 ug/kg

Caprolactam ND 2100 ug/kg

Carbazole ND 83 ug/kg

4-Chloroaniline ND 410 ug/kg

4-Chloro-3-methylphenol ND 410 ug/kg

2-Chloronaphthalene ND 83 ug/kg

2-Chlorophenol ND 410 ug/kg

4-Chlorophenyl phenyl ND 410 ug/kg

ether

Chrysene ND 83 ug/kg

Dibenz(a,h)anthracene ND 83 ug/kg

Dibenzofuran ND 410 ug/kg

3,3'-Dichlorobenzidine ND 410 ug/kg

2,4-Dichlorophenol ND 83 ug/kg

Diethyl phthalate ND 410 ug/kg

2,4-Dimethylphenol ND 410 ug/kg

Dimethyl phthalate ND 410 ug/kg

Di-n-butyl phthalate ND 410 ug/kg

(Continued on next page)

C9K180557 78 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SED-1

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-012 Work Order #...: Work Order #...: LPPHK1AE Matrix.........: Matrix.........: SOLID

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

4,6-Dinitro- ND 2100 ug/kg

2-methylphenol

2,4-Dinitrophenol ND 2100 ug/kg

2,4-Dinitrotoluene ND 410 ug/kg

2,6-Dinitrotoluene ND 410 ug/kg

Di-n-octyl phthalate ND 410 ug/kg

Fluoranthene ND 83 ug/kg

Fluorene ND 83 ug/kg

Hexachlorobenzene ND 83 ug/kg

Hexachlorobutadiene ND 83 ug/kg

Hexachlorocyclopenta- ND 410 ug/kg

diene

Hexachloroethane ND 410 ug/kg

Indeno(1,2,3-cd)pyrene ND 83 ug/kg

Isophorone ND 410 ug/kg

2-Methylnaphthalene ND 83 ug/kg

2-Methylphenol ND 410 ug/kg

4-Methylphenol ND 410 ug/kg

Naphthalene ND 83 ug/kg

2-Nitroaniline ND 2100 ug/kg

3-Nitroaniline ND 2100 ug/kg

4-Nitroaniline ND 2100 ug/kg

Nitrobenzene ND 83 ug/kg

2-Nitrophenol ND 410 ug/kg

4-Nitrophenol ND 2100 ug/kg

N-Nitrosodi-n-propyl- ND 83 ug/kg

amine

N-Nitrosodiphenylamine ND 83 ug/kg

2,2'-oxybis ND 83 ug/kg

(1-Chloropropane)

Pentachlorophenol ND 410 ug/kg

Phenanthrene ND 83 ug/kg

Phenol ND 83 ug/kg

Pyrene ND 83 ug/kg

2,4,5-Trichloro- ND 410 ug/kg

phenol

2,4,6-Trichloro- ND 410 ug/kg

phenol

(Continued on next page)

C9K180557 79 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SED-1

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-012 Work Order #...: Work Order #...: LPPHK1AE Matrix.........: Matrix.........: SOLID

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

2,4,6-Tribromophenol 48 (35 - 124)

2-Fluorobiphenyl 53 (35 - 105)

2-Fluorophenol 65 (39 - 103)

Nitrobenzene-d5 62 (25 - 104)

Phenol-d5 60 (25 - 105)

Terphenyl-d14 54 (25 - 127)

NOTE(S): _______________________________________________________________________________________

Results and reporting limits have been adjusted for dry weight.

C9K180557 80 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SED-2

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-013 Work Order #...: Work Order #...: LPPHM1AM Matrix.........: Matrix.........: SOLID

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9323002

Prep Date......: Prep Date......: 11/19/09 Analysis Date..: Analysis Date..: 11/20/09

Prep Batch #...: Prep Batch #...: 9323010 Analysis Time..: Analysis Time..: 01:21

Dilution Factor: Dilution Factor: 1

% Moisture.....: % Moisture.....: 20 Method.........: Method.........: SW846 8270C

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acenaphthene ND 83 ug/kg

Acenaphthylene ND 83 ug/kg

Acetophenone ND 410 ug/kg

Anthracene ND 83 ug/kg

Atrazine ND 410 ug/kg

Benzo(a)anthracene ND 83 ug/kg

Benzo(a)pyrene ND 83 ug/kg

Benzo(b)fluoranthene ND 83 ug/kg

Benzo(ghi)perylene ND 83 ug/kg

Benzo(k)fluoranthene ND 83 ug/kg

Benzaldehyde ND 410 ug/kg

1,1'-Biphenyl ND 410 ug/kg

bis(2-Chloroethoxy) ND 410 ug/kg

methane

bis(2-Chloroethyl)- ND 83 ug/kg

ether

bis(2-Ethylhexyl) ND 410 ug/kg

phthalate

4-Bromophenyl phenyl ND 410 ug/kg

ether

Butyl benzyl phthalate ND 410 ug/kg

Caprolactam ND 2100 ug/kg

Carbazole ND 83 ug/kg

4-Chloroaniline ND 410 ug/kg

4-Chloro-3-methylphenol ND 410 ug/kg

2-Chloronaphthalene ND 83 ug/kg

2-Chlorophenol ND 410 ug/kg

4-Chlorophenyl phenyl ND 410 ug/kg

ether

Chrysene ND 83 ug/kg

Dibenz(a,h)anthracene ND 83 ug/kg

Dibenzofuran ND 410 ug/kg

3,3'-Dichlorobenzidine ND 410 ug/kg

2,4-Dichlorophenol ND 83 ug/kg

Diethyl phthalate ND 410 ug/kg

2,4-Dimethylphenol ND 410 ug/kg

Dimethyl phthalate ND 410 ug/kg

Di-n-butyl phthalate ND 410 ug/kg

(Continued on next page)

C9K180557 81 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SED-2

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-013 Work Order #...: Work Order #...: LPPHM1AM Matrix.........: Matrix.........: SOLID

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

4,6-Dinitro- ND 2100 ug/kg

2-methylphenol

2,4-Dinitrophenol ND 2100 ug/kg

2,4-Dinitrotoluene ND 410 ug/kg

2,6-Dinitrotoluene ND 410 ug/kg

Di-n-octyl phthalate ND 410 ug/kg

Fluoranthene ND 83 ug/kg

Fluorene ND 83 ug/kg

Hexachlorobenzene ND 83 ug/kg

Hexachlorobutadiene ND 83 ug/kg

Hexachlorocyclopenta- ND 410 ug/kg

diene

Hexachloroethane ND 410 ug/kg

Indeno(1,2,3-cd)pyrene ND 83 ug/kg

Isophorone ND 410 ug/kg

2-Methylnaphthalene ND 83 ug/kg

2-Methylphenol ND 410 ug/kg

4-Methylphenol ND 410 ug/kg

Naphthalene ND 83 ug/kg

2-Nitroaniline ND 2100 ug/kg

3-Nitroaniline ND 2100 ug/kg

4-Nitroaniline ND 2100 ug/kg

Nitrobenzene ND 83 ug/kg

2-Nitrophenol ND 410 ug/kg

4-Nitrophenol ND 2100 ug/kg

N-Nitrosodi-n-propyl- ND 83 ug/kg

amine

N-Nitrosodiphenylamine ND 83 ug/kg

2,2'-oxybis ND 83 ug/kg

(1-Chloropropane)

Pentachlorophenol ND 410 ug/kg

Phenanthrene ND 83 ug/kg

Phenol ND 83 ug/kg

Pyrene ND 83 ug/kg

2,4,5-Trichloro- ND 410 ug/kg

phenol

2,4,6-Trichloro- ND 410 ug/kg

phenol

(Continued on next page)

C9K180557 82 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SED-2

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-013 Work Order #...: Work Order #...: LPPHM1AM Matrix.........: Matrix.........: SOLID

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

2,4,6-Tribromophenol 59 (35 - 124)

2-Fluorobiphenyl 62 (35 - 105)

2-Fluorophenol 72 (39 - 103)

Nitrobenzene-d5 65 (25 - 104)

Phenol-d5 66 (25 - 105)

Terphenyl-d14 64 (25 - 127)

NOTE(S): _______________________________________________________________________________________

Results and reporting limits have been adjusted for dry weight.

C9K180557 83 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SED-3

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-014 Work Order #...: Work Order #...: LPPHN1AV Matrix.........: Matrix.........: SOLID

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9323002

Prep Date......: Prep Date......: 11/19/09 Analysis Date..: Analysis Date..: 11/20/09

Prep Batch #...: Prep Batch #...: 9323010 Analysis Time..: Analysis Time..: 01:41

Dilution Factor: Dilution Factor: 1

% Moisture.....: % Moisture.....: 23 Method.........: Method.........: SW846 8270C

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

Acenaphthene ND 87 ug/kg

Acenaphthylene ND 87 ug/kg

Acetophenone ND 430 ug/kg

Anthracene ND 87 ug/kg

Atrazine ND 430 ug/kg

Benzo(a)anthracene ND 87 ug/kg

Benzo(a)pyrene ND 87 ug/kg

Benzo(b)fluoranthene ND 87 ug/kg

Benzo(ghi)perylene ND 87 ug/kg

Benzo(k)fluoranthene ND 87 ug/kg

Benzaldehyde ND 430 ug/kg

1,1'-Biphenyl ND 430 ug/kg

bis(2-Chloroethoxy) ND 430 ug/kg

methane

bis(2-Chloroethyl)- ND 87 ug/kg

ether

bis(2-Ethylhexyl) ND 430 ug/kg

phthalate

4-Bromophenyl phenyl ND 430 ug/kg

ether

Butyl benzyl phthalate ND 430 ug/kg

Caprolactam ND 2200 ug/kg

Carbazole ND 87 ug/kg

4-Chloroaniline ND 430 ug/kg

4-Chloro-3-methylphenol ND 430 ug/kg

2-Chloronaphthalene ND 87 ug/kg

2-Chlorophenol ND 430 ug/kg

4-Chlorophenyl phenyl ND 430 ug/kg

ether

Chrysene ND 87 ug/kg

Dibenz(a,h)anthracene ND 87 ug/kg

Dibenzofuran ND 430 ug/kg

3,3'-Dichlorobenzidine ND 430 ug/kg

2,4-Dichlorophenol ND 87 ug/kg

Diethyl phthalate ND 430 ug/kg

2,4-Dimethylphenol ND 430 ug/kg

Dimethyl phthalate ND 430 ug/kg

Di-n-butyl phthalate ND 430 ug/kg

(Continued on next page)

C9K180557 84 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SED-3

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-014 Work Order #...: Work Order #...: LPPHN1AV Matrix.........: Matrix.........: SOLID

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS _________

4,6-Dinitro- ND 2200 ug/kg

2-methylphenol

2,4-Dinitrophenol ND 2200 ug/kg

2,4-Dinitrotoluene ND 430 ug/kg

2,6-Dinitrotoluene ND 430 ug/kg

Di-n-octyl phthalate ND 430 ug/kg

Fluoranthene ND 87 ug/kg

Fluorene ND 87 ug/kg

Hexachlorobenzene ND 87 ug/kg

Hexachlorobutadiene ND 87 ug/kg

Hexachlorocyclopenta- ND 430 ug/kg

diene

Hexachloroethane ND 430 ug/kg

Indeno(1,2,3-cd)pyrene ND 87 ug/kg

Isophorone ND 430 ug/kg

2-Methylnaphthalene ND 87 ug/kg

2-Methylphenol ND 430 ug/kg

4-Methylphenol ND 430 ug/kg

Naphthalene ND 87 ug/kg

2-Nitroaniline ND 2200 ug/kg

3-Nitroaniline ND 2200 ug/kg

4-Nitroaniline ND 2200 ug/kg

Nitrobenzene ND 87 ug/kg

2-Nitrophenol ND 430 ug/kg

4-Nitrophenol ND 2200 ug/kg

N-Nitrosodi-n-propyl- ND 87 ug/kg

amine

N-Nitrosodiphenylamine ND 87 ug/kg

2,2'-oxybis ND 87 ug/kg

(1-Chloropropane)

Pentachlorophenol ND 430 ug/kg

Phenanthrene ND 87 ug/kg

Phenol ND 87 ug/kg

Pyrene ND 87 ug/kg

2,4,5-Trichloro- ND 430 ug/kg

phenol

2,4,6-Trichloro- ND 430 ug/kg

phenol

(Continued on next page)

C9K180557 85 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SED-3

GC/MS Semivolatiles

Lot-Sample #...: Lot-Sample #...: C9K180557-014 Work Order #...: Work Order #...: LPPHN1AV Matrix.........: Matrix.........: SOLID

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

2,4,6-Tribromophenol 62 (35 - 124)

2-Fluorobiphenyl 64 (35 - 105)

2-Fluorophenol 71 (39 - 103)

Nitrobenzene-d5 67 (25 - 104)

Phenol-d5 68 (25 - 105)

Terphenyl-d14 64 (25 - 127)

NOTE(S): _______________________________________________________________________________________

Results and reporting limits have been adjusted for dry weight.

C9K180557 86 of 161
METHOD BLANK REPORT

GC/MS Semivolatiles

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPP7G1AA Matrix.........: Matrix.........: SOLID

MB Lot-Sample #: MB Lot-Sample #: C9K190000-010

Prep Date......: Prep Date......: 11/19/09 Analysis Time..: Analysis Time..: 23:18

Analysis Date..: Analysis Date..: 11/19/09 Prep Batch #...: Prep Batch #...: 9323010

Dilution Factor: Dilution Factor: 1

REPORTING

PARAMETER _________________________ RESULT _______________ LIMIT _________ UNITS __________ METHOD _________________

Acenaphthene ND 67 ug/kg SW846 8270C

Acenaphthylene ND 67 ug/kg SW846 8270C

Acetophenone ND 330 ug/kg SW846 8270C

Anthracene ND 67 ug/kg SW846 8270C

Atrazine ND 330 ug/kg SW846 8270C

Benzo(a)anthracene ND 67 ug/kg SW846 8270C

Benzo(a)pyrene ND 67 ug/kg SW846 8270C

Benzo(b)fluoranthene ND 67 ug/kg SW846 8270C

Benzo(ghi)perylene ND 67 ug/kg SW846 8270C

Benzo(k)fluoranthene ND 67 ug/kg SW846 8270C

Benzaldehyde ND 330 ug/kg SW846 8270C

1,1'-Biphenyl ND 330 ug/kg SW846 8270C

bis(2-Chloroethoxy) ND 330 ug/kg SW846 8270C

methane

bis(2-Chloroethyl)- ND 67 ug/kg SW846 8270C

ether

bis(2-Ethylhexyl) ND 330 ug/kg SW846 8270C

phthalate

4-Bromophenyl phenyl ND 330 ug/kg SW846 8270C

ether

Butyl benzyl phthalate ND 330 ug/kg SW846 8270C

Caprolactam ND 1700 ug/kg SW846 8270C

Carbazole ND 67 ug/kg SW846 8270C

4-Chloroaniline ND 330 ug/kg SW846 8270C

4-Chloro-3-methylphenol ND 330 ug/kg SW846 8270C

2-Chloronaphthalene ND 67 ug/kg SW846 8270C

2-Chlorophenol ND 330 ug/kg SW846 8270C

4-Chlorophenyl phenyl ND 330 ug/kg SW846 8270C

ether

Chrysene ND 67 ug/kg SW846 8270C

Dibenz(a,h)anthracene ND 67 ug/kg SW846 8270C

Dibenzofuran ND 330 ug/kg SW846 8270C

3,3'-Dichlorobenzidine ND 330 ug/kg SW846 8270C

2,4-Dichlorophenol ND 67 ug/kg SW846 8270C

Diethyl phthalate ND 330 ug/kg SW846 8270C

2,4-Dimethylphenol ND 330 ug/kg SW846 8270C

Dimethyl phthalate ND 330 ug/kg SW846 8270C

Di-n-butyl phthalate ND 330 ug/kg SW846 8270C

4,6-Dinitro- ND 1700 ug/kg SW846 8270C

2-methylphenol

2,4-Dinitrophenol ND 1700 ug/kg SW846 8270C

(Continued on next page)

C9K180557 87 of 161
METHOD BLANK REPORT

GC/MS Semivolatiles

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPP7G1AA Matrix.........: Matrix.........: SOLID

REPORTING

PARAMETER _________________________ RESULT _______________ LIMIT _________ UNITS __________ METHOD _________________

2,4-Dinitrotoluene ND 330 ug/kg SW846 8270C

2,6-Dinitrotoluene ND 330 ug/kg SW846 8270C

Di-n-octyl phthalate ND 330 ug/kg SW846 8270C

Fluoranthene ND 67 ug/kg SW846 8270C

Fluorene ND 67 ug/kg SW846 8270C

Hexachlorobenzene ND 67 ug/kg SW846 8270C

Hexachlorobutadiene ND 67 ug/kg SW846 8270C

Hexachlorocyclopenta- ND 330 ug/kg SW846 8270C

diene

Hexachloroethane ND 330 ug/kg SW846 8270C

Indeno(1,2,3-cd)pyrene ND 67 ug/kg SW846 8270C

Isophorone ND 330 ug/kg SW846 8270C

2-Methylnaphthalene ND 67 ug/kg SW846 8270C

2-Methylphenol ND 330 ug/kg SW846 8270C

4-Methylphenol ND 330 ug/kg SW846 8270C

Naphthalene ND 67 ug/kg SW846 8270C

2-Nitroaniline ND 1700 ug/kg SW846 8270C

3-Nitroaniline ND 1700 ug/kg SW846 8270C

4-Nitroaniline ND 1700 ug/kg SW846 8270C

Nitrobenzene ND 67 ug/kg SW846 8270C

2-Nitrophenol ND 330 ug/kg SW846 8270C

4-Nitrophenol ND 1700 ug/kg SW846 8270C

N-Nitrosodi-n-propyl- ND 67 ug/kg SW846 8270C

amine

N-Nitrosodiphenylamine ND 67 ug/kg SW846 8270C

2,2'-oxybis ND 67 ug/kg SW846 8270C

(1-Chloropropane)

Pentachlorophenol ND 330 ug/kg SW846 8270C

Phenanthrene ND 67 ug/kg SW846 8270C

Phenol ND 67 ug/kg SW846 8270C

Pyrene ND 67 ug/kg SW846 8270C

2,4,5-Trichloro- ND 330 ug/kg SW846 8270C

phenol

2,4,6-Trichloro- ND 330 ug/kg SW846 8270C

phenol

PERCENT RECOVERY

SURROGATE _________________________ RECOVERY ________ LIMITS __________

2,4,6-Tribromophenol 75 (35 - 124)

2-Fluorobiphenyl 73 (35 - 105)

2-Fluorophenol 93 (39 - 103)

Nitrobenzene-d5 79 (25 - 104)

Phenol-d5 86 (25 - 105)

Terphenyl-d14 78 (25 - 127)

(Continued on next page)

C9K180557 88 of 161
METHOD BLANK REPORT

GC/MS Semivolatiles

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPP7G1AA Matrix.........: Matrix.........: SOLID

NOTE(S): ___________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

C9K180557 89 of 161
METHOD BLANK REPORT

GC/MS Semivolatiles

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPVAM1AA Matrix.........: Matrix.........: WATER

MB Lot-Sample #: MB Lot-Sample #: C9K200000-281

Prep Date......: Prep Date......: 11/20/09 Analysis Time..: Analysis Time..: 12:25

Analysis Date..: Analysis Date..: 11/25/09 Prep Batch #...: Prep Batch #...: 9324281

Dilution Factor: Dilution Factor: 1

REPORTING

PARAMETER _________________________ RESULT _______________ LIMIT _________ UNITS __________ METHOD _________________

Acenaphthene ND 2.0 ug/L SW846 8270C

Acenaphthylene ND 2.0 ug/L SW846 8270C

Acetophenone ND 10 ug/L SW846 8270C

Anthracene ND 2.0 ug/L SW846 8270C

Atrazine ND 10 ug/L SW846 8270C

Benzo(a)anthracene ND 2.0 ug/L SW846 8270C

Benzo(a)pyrene ND 2.0 ug/L SW846 8270C

Benzo(b)fluoranthene ND 2.0 ug/L SW846 8270C

Benzo(ghi)perylene ND 2.0 ug/L SW846 8270C

Benzo(k)fluoranthene ND 2.0 ug/L SW846 8270C

Benzaldehyde ND 10 ug/L SW846 8270C

1,1'-Biphenyl ND 10 ug/L SW846 8270C

bis(2-Chloroethoxy) ND 10 ug/L SW846 8270C

methane

bis(2-Chloroethyl)- ND 2.0 ug/L SW846 8270C

ether

bis(2-Ethylhexyl) ND 10 ug/L SW846 8270C

phthalate

4-Bromophenyl phenyl ND 10 ug/L SW846 8270C

ether

Butyl benzyl phthalate ND 10 ug/L SW846 8270C

Caprolactam ND 50 ug/L SW846 8270C

Carbazole ND 2.0 ug/L SW846 8270C

4-Chloroaniline ND 10 ug/L SW846 8270C

4-Chloro-3-methylphenol ND 10 ug/L SW846 8270C

2-Chloronaphthalene ND 2.0 ug/L SW846 8270C

2-Chlorophenol ND 10 ug/L SW846 8270C

4-Chlorophenyl phenyl ND 10 ug/L SW846 8270C

ether

Chrysene ND 2.0 ug/L SW846 8270C

Dibenz(a,h)anthracene ND 2.0 ug/L SW846 8270C

Dibenzofuran ND 10 ug/L SW846 8270C

3,3'-Dichlorobenzidine ND 10 ug/L SW846 8270C

2,4-Dichlorophenol ND 2.0 ug/L SW846 8270C

Diethyl phthalate ND 10 ug/L SW846 8270C

2,4-Dimethylphenol ND 10 ug/L SW846 8270C

Dimethyl phthalate ND 10 ug/L SW846 8270C

Di-n-butyl phthalate ND 10 ug/L SW846 8270C

4,6-Dinitro- ND 50 ug/L SW846 8270C

2-methylphenol

2,4-Dinitrophenol ND 50 ug/L SW846 8270C

(Continued on next page)

C9K180557 90 of 161
METHOD BLANK REPORT

GC/MS Semivolatiles

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPVAM1AA Matrix.........: Matrix.........: WATER

REPORTING

PARAMETER _________________________ RESULT _______________ LIMIT _________ UNITS __________ METHOD _________________

2,4-Dinitrotoluene ND 10 ug/L SW846 8270C

2,6-Dinitrotoluene ND 10 ug/L SW846 8270C

Di-n-octyl phthalate ND 10 ug/L SW846 8270C

Fluoranthene ND 2.0 ug/L SW846 8270C

Fluorene ND 2.0 ug/L SW846 8270C

Hexachlorobenzene ND 2.0 ug/L SW846 8270C

Hexachlorobutadiene ND 2.0 ug/L SW846 8270C

Hexachlorocyclopenta- ND 10 ug/L SW846 8270C

diene

Hexachloroethane ND 10 ug/L SW846 8270C

Indeno(1,2,3-cd)pyrene ND 2.0 ug/L SW846 8270C

Isophorone ND 10 ug/L SW846 8270C

2-Methylnaphthalene ND 2.0 ug/L SW846 8270C

2-Methylphenol ND 10 ug/L SW846 8270C

4-Methylphenol ND 10 ug/L SW846 8270C

Naphthalene ND 2.0 ug/L SW846 8270C

2-Nitroaniline ND 50 ug/L SW846 8270C

3-Nitroaniline ND 50 ug/L SW846 8270C

4-Nitroaniline ND 50 ug/L SW846 8270C

Nitrobenzene ND 2.0 ug/L SW846 8270C

2-Nitrophenol ND 10 ug/L SW846 8270C

4-Nitrophenol ND 50 ug/L SW846 8270C

N-Nitrosodi-n-propyl- ND 2.0 ug/L SW846 8270C

amine

N-Nitrosodiphenylamine ND 2.0 ug/L SW846 8270C

2,2'-oxybis ND 2.0 ug/L SW846 8270C

(1-Chloropropane)

Pentachlorophenol ND 10 ug/L SW846 8270C

Phenanthrene ND 2.0 ug/L SW846 8270C

Phenol ND 2.0 ug/L SW846 8270C

Pyrene ND 2.0 ug/L SW846 8270C

2,4,5-Trichloro- ND 10 ug/L SW846 8270C

phenol

2,4,6-Trichloro- ND 10 ug/L SW846 8270C

phenol

PERCENT RECOVERY

SURROGATE _________________________ RECOVERY ________ LIMITS __________

2,4,6-Tribromophenol 70 (33 - 122)

2-Fluorobiphenyl 57 (35 - 108)

2-Fluorophenol 69 (26 - 100)

Nitrobenzene-d5 61 (37 - 104)

Phenol-d5 73 (30 - 102)

Terphenyl-d14 75 (25 - 130)

(Continued on next page)

C9K180557 91 of 161
METHOD BLANK REPORT

GC/MS Semivolatiles

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPVAM1AA Matrix.........: Matrix.........: WATER

NOTE(S): ___________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

C9K180557 92 of 161
LABORATORY CONTROL SAMPLE EVALUATION REPORT

GC/MS Semivolatiles

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPP7G1AC Matrix.........: Matrix.........: SOLID

LCS Lot-Sample#: LCS Lot-Sample#: C9K190000-010

Prep Date......: Prep Date......: 11/19/09 Analysis Date..: Analysis Date..: 11/19/09

Prep Batch #...: Prep Batch #...: 9323010 Analysis Time..: Analysis Time..: 23:38

Dilution Factor: Dilution Factor: 1

PERCENT RECOVERY

PARAMETER ________________________ RECOVERY ________ LIMITS __________ METHOD _________________

Acenaphthene Acenaphthene 76 (47 - 104) (47 - 104) SW846 8270C SW846 8270C

1,2,4-Trichloro- 1,2,4-Trichloro- 67 (43 - 100) (43 - 100) SW846 8270C SW846 8270C

benzene

1,4-Dichlorobenzene 1,4-Dichlorobenzene 74 (35 - 99) (35 - 99) SW846 8270C SW846 8270C

4-Bromophenyl phenyl 4-Bromophenyl phenyl 72 (47 - 110) (47 - 110) SW846 8270C SW846 8270C

ether

Butyl benzyl phthalate Butyl benzyl phthalate 75 (41 - 118) (41 - 118) SW846 8270C SW846 8270C

4-Chloro-3-methylphenol 4-Chloro-3-methylphenol 82 (47 - 109) (47 - 109) SW846 8270C SW846 8270C

2-Chlorophenol 2-Chlorophenol 77 (40 - 101) (40 - 101) SW846 8270C SW846 8270C

2,4-Dinitrotoluene 2,4-Dinitrotoluene 92 (45 - 124) (45 - 124) SW846 8270C SW846 8270C

Hexachloroethane Hexachloroethane 74 (37 - 97) (37 - 97) SW846 8270C SW846 8270C

4-Methylphenol 4-Methylphenol 81 (42 - 105) (42 - 105) SW846 8270C SW846 8270C

Naphthalene Naphthalene 73 (43 - 100) (43 - 100) SW846 8270C SW846 8270C

4-Nitrophenol 4-Nitrophenol 89 (36 - 127) (36 - 127) SW846 8270C SW846 8270C

N-Nitrosodi-n-propyl- N-Nitrosodi-n-propyl- 78 (42 - 107) (42 - 107) SW846 8270C SW846 8270C

amine

Pentachlorophenol Pentachlorophenol 75 (17 - 122) (17 - 122) SW846 8270C SW846 8270C

Phenol 73 (41 - 102) (41 - 102) SW846 8270C SW846 8270C

Pyrene 70 (41 - 115) (41 - 115) SW846 8270C SW846 8270C

PERCENT RECOVERY

SURROGATE _________________________ RECOVERY ________ LIMITS __________

2,4,6-Tribromophenol 77 (35 - 124)

2-Fluorobiphenyl 77 (35 - 105)

2-Fluorophenol 89 (39 - 103)

Nitrobenzene-d5 82 (25 - 104)

Phenol-d5 88 (25 - 105)

Terphenyl-d14 75 (25 - 127)

NOTE(S): _____________________________________________________________________________________ _____________________________________________________________________________________ 

Calculations are performed before rounding to avoid round-off errors in calculated results.

Bold print denotes control parameters

C9K180557 93 of 161
LABORATORY CONTROL SAMPLE EVALUATION REPORT

GC/MS Semivolatiles

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPVAM1AC-LCS Matrix.........: Matrix.........: WATER

LCS Lot-Sample#: LCS Lot-Sample#: C9K200000-281 LPVAM1AD-LCSD

Prep Date......: Prep Date......: 11/20/09 Analysis Date..: Analysis Date..: 11/25/09

Prep Batch #...: Prep Batch #...: 9324281 Analysis Time..: Analysis Time..: 12:47

Dilution Factor: Dilution Factor: 1

PERCENT RECOVERY RPD

PARAMETER ________________________ RECOVERY ________ LIMITS __________ RPD _____ LIMITS ______ METHOD _________________

Acenaphthene Acenaphthene 62 (39 - 106) (39 - 106) SW846 8270C SW846 8270C

63 (39 - 106) (39 - 106) 1.7 (0-32) SW846 8270C SW846 8270C

1,2,4-Trichloro- 1,2,4-Trichloro- 72 (36 - 97) (36 - 97) SW846 8270C SW846 8270C

benzene

73 (36 - 97) (36 - 97) 2.3 (0-32) SW846 8270C SW846 8270C

1,4-Dichlorobenzene 1,4-Dichlorobenzene 75 (32 - 94) (32 - 94) SW846 8270C SW846 8270C

74 (32 - 94) (32 - 94) 1.3 (0-33) SW846 8270C SW846 8270C

4-Bromophenyl phenyl 4-Bromophenyl phenyl 73 (38 - 108) (38 - 108) SW846 8270C SW846 8270C

ether

74 (38 - 108) (38 - 108) 1.7 (0-40) SW846 8270C SW846 8270C

Butyl benzyl phthalate Butyl benzyl phthalate 76 (34 - 110) (34 - 110) SW846 8270C SW846 8270C

72 (34 - 110) (34 - 110) 5.5 (0-35) SW846 8270C SW846 8270C

4-Chloro-3-methylphenol 4-Chloro-3-methylphenol 71 (40 - 107) (40 - 107) SW846 8270C SW846 8270C

71 (40 - 107) (40 - 107) 0.36 (0-32) SW846 8270C SW846 8270C

2-Chlorophenol 2-Chlorophenol 76 (34 - 100) (34 - 100) SW846 8270C SW846 8270C

75 (34 - 100) (34 - 100) 1.7 (0-31) SW846 8270C SW846 8270C

2,4-Dinitrotoluene 2,4-Dinitrotoluene 71 (41 - 117) (41 - 117) SW846 8270C SW846 8270C

73 (41 - 117) (41 - 117) 2.1 (0-32) SW846 8270C SW846 8270C

Hexachloroethane Hexachloroethane 71 (27 - 94) (27 - 94) SW846 8270C SW846 8270C

70 (27 - 94) (27 - 94) 1.4 (0-43) SW846 8270C SW846 8270C

4-Methylphenol 4-Methylphenol 75 (34 - 104) (34 - 104) SW846 8270C SW846 8270C

75 (34 - 104) (34 - 104) 0.50 (0-34) SW846 8270C SW846 8270C

Naphthalene Naphthalene 72 (35 - 98) (35 - 98) SW846 8270C SW846 8270C

73 (35 - 98) (35 - 98) 1.1 (0-39) SW846 8270C SW846 8270C

4-Nitrophenol 4-Nitrophenol 65 (29 - 120) (29 - 120) SW846 8270C SW846 8270C

66 (29 - 120) (29 - 120) 2.0 (0-39) SW846 8270C SW846 8270C

N-Nitrosodi-n-propyl- N-Nitrosodi-n-propyl- 71 (37 - 106) (37 - 106) SW846 8270C SW846 8270C

amine

68 (37 - 106) (37 - 106) 4.2 (0-36) SW846 8270C SW846 8270C

Pentachlorophenol Pentachlorophenol 65 (10 - 118) (10 - 118) SW846 8270C SW846 8270C

68 (10 - 118) (10 - 118) 4.6 (0-49) SW846 8270C SW846 8270C

Phenol 70 (35 - 98) (35 - 98) SW846 8270C SW846 8270C

69 (35 - 98) (35 - 98) 1.8 (0-35) SW846 8270C SW846 8270C

Pyrene 80 (36 - 115) (36 - 115) SW846 8270C SW846 8270C

75 (36 - 115) (36 - 115) 6.2 (0-38) SW846 8270C SW846 8270C

(Continued on next page)

C9K180557 94 of 161
LABORATORY CONTROL SAMPLE EVALUATION REPORT

GC/MS Semivolatiles

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPVAM1AC-LCS Matrix.........: Matrix.........: WATER

LCS Lot-Sample#: LCS Lot-Sample#: C9K200000-281 LPVAM1AD-LCSD

PERCENT RECOVERY

SURROGATE _________________________ RECOVERY ________ LIMITS __________

2,4,6-Tribromophenol 81 (33 - 122)

81 (33 - 122)

2-Fluorobiphenyl 69 (35 - 108)

71 (35 - 108)

2-Fluorophenol 83 (26 - 100)

81 (26 - 100)

Nitrobenzene-d5 75 (37 - 104)

72 (37 - 104)

Phenol-d5 84 (30 - 102)

82 (30 - 102)

Terphenyl-d14 88 (25 - 130)

83 (25 - 130)

NOTE(S): ________________________________________________________________________________________ ________________________________________________________________________________________ 

Calculations are performed before rounding to avoid round-off errors in calculated results.

Bold print denotes control parameters

C9K180557 95 of 161
MATRIX SPIKE SAMPLE EVALUATION REPORT

GC/MS Semivolatiles

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPPHK1A7-MS Matrix.........: Matrix.........: SOLID

MS Lot-Sample #: MS Lot-Sample #: C9K180557-012 LPPHK1A8-MSD

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09 MS Run #.......: MS Run #.......: 9323002

Prep Date......: Prep Date......: 11/19/09 Analysis Date..: Analysis Date..: 11/20/09

Prep Batch #...: Prep Batch #...: 9323010 Analysis Time..: Analysis Time..: 00:41

Dilution Factor: Dilution Factor: 1 % Moisture.....: % Moisture.....: 20

PERCENT RECOVERY RPD

PARAMETER _________________________ RECOVERY _________ LIMITS __________ RPD ____ LIMITS _________ METHOD _________________

Acenaphthene Acenaphthene 69 (47 - 104) (47 - 104) SW846 8270C SW846 8270C

61 (47 - 104) (47 - 104) 11 (0-40) SW846 8270C SW846 8270C

1,2,4-Trichloro- 1,2,4-Trichloro- 62 (43 - 100) (43 - 100) SW846 8270C SW846 8270C

benzene

56 (43 - 100) (43 - 100) 9.7 (0-36) SW846 8270C SW846 8270C

1,4-Dichlorobenzene 1,4-Dichlorobenzene 62 (35 - 99) (35 - 99) SW846 8270C SW846 8270C

54 (35 - 99) (35 - 99) 13 (0-49) SW846 8270C SW846 8270C

4-Bromophenyl phenyl 4-Bromophenyl phenyl 63 (47 - 110) (47 - 110) SW846 8270C SW846 8270C

ether

56 (47 - 110) (47 - 110) 11 (0-46) SW846 8270C SW846 8270C

Butyl benzyl phthalate Butyl benzyl phthalate 68 (41 - 118) (41 - 118) SW846 8270C SW846 8270C

63 (41 - 118) (41 - 118) 7.4 (0-41) SW846 8270C SW846 8270C

4-Chloro-3-methylphenol 4-Chloro-3-methylphenol 68 (47 - 109) (47 - 109) SW846 8270C SW846 8270C

66 (47 - 109) (47 - 109) 3.2 (0-36) SW846 8270C SW846 8270C

2-Chlorophenol 2-Chlorophenol 65 (40 - 101) (40 - 101) SW846 8270C SW846 8270C

57 (40 - 101) (40 - 101) 13 (0-42) SW846 8270C SW846 8270C

2,4-Dinitrotoluene 2,4-Dinitrotoluene 80 (45 - 124) (45 - 124) SW846 8270C SW846 8270C

74 (45 - 124) (45 - 124) 7.8 (0-41) SW846 8270C SW846 8270C

Hexachloroethane Hexachloroethane 61 (37 - 97) (37 - 97) SW846 8270C SW846 8270C

53 (37 - 97) (37 - 97) 14 (0-48) SW846 8270C SW846 8270C

4-Methylphenol 4-Methylphenol 69 (42 - 105) (42 - 105) SW846 8270C SW846 8270C

59 (42 - 105) (42 - 105) 16 (0-43) SW846 8270C SW846 8270C

Naphthalene Naphthalene 65 (43 - 100) (43 - 100) SW846 8270C SW846 8270C

61 (43 - 100) (43 - 100) 6.8 (0-32) SW846 8270C SW846 8270C

4-Nitrophenol 4-Nitrophenol 69 (36 - 127) (36 - 127) SW846 8270C SW846 8270C

61 (36 - 127) (36 - 127) 13 (0-43) SW846 8270C SW846 8270C

N-Nitrosodi-n-propyl- N-Nitrosodi-n-propyl- 70 (42 - 107) (42 - 107) SW846 8270C SW846 8270C

amine

59 (42 - 107) (42 - 107) 17 (0-43) SW846 8270C SW846 8270C

Pentachlorophenol Pentachlorophenol 57 (17 - 122) (17 - 122) SW846 8270C SW846 8270C

51 (17 - 122) (17 - 122) 11 (0-52) SW846 8270C SW846 8270C

Phenol 60 (41 - 102) (41 - 102) SW846 8270C SW846 8270C

55 (41 - 102) (41 - 102) 8.6 (0-39) SW846 8270C SW846 8270C

Pyrene 64 (41 - 115) (41 - 115) SW846 8270C SW846 8270C

59 (41 - 115) (41 - 115) 6.8 (0-43) SW846 8270C SW846 8270C

(Continued on next page)

C9K180557 96 of 161
MATRIX SPIKE SAMPLE EVALUATION REPORT

GC/MS Semivolatiles

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPPHK1A7-MS Matrix.........: Matrix.........: SOLID

MS Lot-Sample #: MS Lot-Sample #: C9K180557-012 LPPHK1A8-MSD

PERCENT RECOVERY

SURROGATE _________________________ RECOVERY ________ LIMITS __________

2,4,6-Tribromophenol 67 (35 - 124)

59 (35 - 124)

2-Fluorobiphenyl 68 (35 - 105)

60 (35 - 105)

2-Fluorophenol 74 (39 - 103)

65 (39 - 103)

Nitrobenzene-d5 74 (25 - 104)

65 (25 - 104)

Phenol-d5 72 (25 - 105)

63 (25 - 105)

Terphenyl-d14 64 (25 - 127)

58 (25 - 127)

NOTE(S): ___________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

Bold print denotes control parameters

Results and reporting limits have been adjusted for dry weight.

C9K180557 97 of 161
Clean Sites Environmental Services Inc

Client Sample ID: MW-1S

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9K180557-001 Matrix.......: Matrix.......: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Prep Batch #...: Prep Batch #...: 9328355

Mercury ND 0.20 ug/L SW846 7470A 11/24/09 LPPF51A6

Dilution Factor: 1 Analysis Time..: 15:02 MS Run #.......: 9328186

Prep Batch #...: Prep Batch #...: 9331296

Silver ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPF51AF

Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144

Aluminum Aluminum 1730 30.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51AG LPPF51AG

Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144

Arsenic ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPF51AH

Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144

Barium 47.0 10.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51AJ LPPF51AJ

Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144

Beryllium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPF51AK

Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144

Calcium Calcium 10500 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51AL LPPF51AL

Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144

Cadmium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPF51AM

Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144

Cobalt 3.5 0.50 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51AN LPPF51AN

Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144

Chromium Chromium 6.5 2.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51AP LPPF51AP

Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144

Copper 2.5 2.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51AQ LPPF51AQ

Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144

Iron 1520 50.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51AR LPPF51AR

Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144

(Continued on next page)

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Clean Sites Environmental Services Inc

Client Sample ID: MW-1S

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9K180557-001 Matrix.........: Matrix.........: WATER

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Potassium Potassium 995 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51AT LPPF51AT

Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144

Magnesium Magnesium 3140 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51AU LPPF51AU

Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144

Manganese Manganese 162 0.50 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51AV LPPF51AV

Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144

Sodium 3760 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51AW LPPF51AW

Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144

Nickel 2.6 1.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51AX LPPF51AX

Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144

Lead 1.4 1.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51A0 LPPF51A0

Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144

Selenium ND 5.0 ug/L SW846 6020 11/27-11/29/09 LPPF51A1

Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144

Thallium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPF51A2

Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144

Antimony ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPF51A3

Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144

Vanadium Vanadium 2.9 1.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51A4 LPPF51A4

Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144

Zinc 9.6 5.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPF51A5 LPPF51A5

Dilution Factor: 1 Analysis Time..: 00:34 MS Run #.......: 9331144

C9K180557 99 of 161
Clean Sites Environmental Services Inc

Client Sample ID: MW-3S

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9K180557-002 Matrix.......: Matrix.......: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Prep Batch #...: Prep Batch #...: 9328355

Mercury ND 0.20 ug/L SW846 7470A 11/24/09 LPPGN1AH

Dilution Factor: 1 Analysis Time..: 15:07 MS Run #.......: 9328186

Prep Batch #...: Prep Batch #...: 9331296

Silver ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPGN1AN

Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144

Aluminum Aluminum 2880 30.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1AP LPPGN1AP

Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144

Arsenic ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPGN1AQ

Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144

Barium 134 10.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1AR LPPGN1AR

Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144

Beryllium Beryllium 2.2 1.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1AT LPPGN1AT

Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144

Calcium Calcium 8770 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1AU LPPGN1AU

Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144

Cadmium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPGN1AV

Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144

Cobalt 4.1 0.50 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1AW LPPGN1AW

Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144

Chromium Chromium 6.4 2.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1AX LPPGN1AX

Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144

Copper 2.1 2.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1A0 LPPGN1A0

Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144

Iron 2280 50.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1A1 LPPGN1A1

Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144

(Continued on next page)

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Clean Sites Environmental Services Inc

Client Sample ID: MW-3S

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9K180557-002 Matrix.........: Matrix.........: WATER

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Potassium Potassium 1240 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1A2 LPPGN1A2

Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144

Magnesium Magnesium 5900 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1A3 LPPGN1A3

Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144

Manganese Manganese 163 0.50 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1A4 LPPGN1A4

Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144

Sodium 4720 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1A5 LPPGN1A5

Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144

Nickel 3.9 1.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1A6 LPPGN1A6

Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144

Lead 2.0 1.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1AA LPPGN1AA

Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144

Selenium ND 5.0 ug/L SW846 6020 11/27-11/29/09 LPPGN1AC

Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144

Thallium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPGN1AD

Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144

Antimony ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPGN1AE

Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144

Vanadium Vanadium 6.0 1.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1AF LPPGN1AF

Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144

Zinc 15.3 5.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGN1AG LPPGN1AG

Dilution Factor: 1 Analysis Time..: 01:05 MS Run #.......: 9331144

C9K180557 101 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L2-S1

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9K180557-003 Matrix.......: Matrix.......: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Prep Batch #...: Prep Batch #...: 9328355

Mercury ND 0.20 ug/L SW846 7470A 11/24/09 LPPGP1AH

Dilution Factor: 1 Analysis Time..: 15:10 MS Run #.......: 9328186

Prep Batch #...: Prep Batch #...: 9331296

Silver ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPGP1AN

Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144

Aluminum Aluminum 2110 30.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1AP LPPGP1AP

Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144

Arsenic ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPGP1AQ

Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144

Barium 95.4 10.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1AR LPPGP1AR

Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144

Beryllium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPGP1AT

Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144

Calcium Calcium 4150 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1AU LPPGP1AU

Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144

Cadmium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPGP1AV

Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144

Cobalt 2.9 0.50 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1AW LPPGP1AW

Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144

Chromium Chromium 7.1 2.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1AX LPPGP1AX

Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144

Copper ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPGP1A0

Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144

Iron 5950 50.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1A1 LPPGP1A1

Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144

(Continued on next page)

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Clean Sites Environmental Services Inc

Client Sample ID: L2-S1

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9K180557-003 Matrix.........: Matrix.........: WATER

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Potassium Potassium 1040 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1A2 LPPGP1A2

Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144

Magnesium Magnesium 2420 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1A3 LPPGP1A3

Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144

Manganese Manganese 104 0.50 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1A4 LPPGP1A4

Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144

Sodium 4990 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1A5 LPPGP1A5

Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144

Nickel 4.2 1.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1A6 LPPGP1A6

Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144

Lead 1.3 1.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1AA LPPGP1AA

Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144

Selenium ND 5.0 ug/L SW846 6020 11/27-11/29/09 LPPGP1AC

Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144

Thallium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPGP1AD

Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144

Antimony ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPGP1AE

Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144

Vanadium Vanadium 6.3 1.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1AF LPPGP1AF

Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144

Zinc 11.0 5.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPGP1AG LPPGP1AG

Dilution Factor: 1 Analysis Time..: 01:09 MS Run #.......: 9331144

C9K180557 103 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L1-S1

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9K180557-006 Matrix.......: Matrix.......: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Prep Batch #...: Prep Batch #...: 9328355

Mercury ND 0.20 ug/L SW846 7470A 11/24/09 LPPG11A5

Dilution Factor: 1 Analysis Time..: 15:12 MS Run #.......: 9328186

Prep Batch #...: Prep Batch #...: 9331296

Silver ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG11AE

Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144

Aluminum Aluminum 486 30.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG11AF LPPG11AF

Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144

Arsenic ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG11AG

Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144

Barium 18.7 10.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG11AH LPPG11AH

Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144

Beryllium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG11AJ

Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144

Calcium Calcium 3930 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG11AK LPPG11AK

Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144

Cadmium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG11AL

Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144

Cobalt 1.3 0.50 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG11AM LPPG11AM

Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144

Chromium Chromium 35.1 2.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG11AN LPPG11AN

Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144

Copper ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPG11AP

Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144

Iron 922 50.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG11AQ LPPG11AQ

Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144

(Continued on next page)

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Clean Sites Environmental Services Inc

Client Sample ID: L1-S1

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9K180557-006 Matrix.........: Matrix.........: WATER

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Potassium Potassium 633 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG11AR LPPG11AR

Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144

Magnesium Magnesium 2350 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG11AT LPPG11AT

Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144

Manganese Manganese 11.9 0.50 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG11AU LPPG11AU

Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144

Sodium 5830 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG11AV LPPG11AV

Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144

Nickel 5.1 1.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG11AW LPPG11AW

Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144

Lead ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG11AX

Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144

Selenium ND 5.0 ug/L SW846 6020 11/27-11/29/09 LPPG11A0

Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144

Thallium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG11A1

Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144

Antimony ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPG11A2

Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144

Vanadium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG11A3

Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144

Zinc 7.7 5.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG11A4 LPPG11A4

Dilution Factor: 1 Analysis Time..: 01:14 MS Run #.......: 9331144

C9K180557 105 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L1-S3

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9K180557-007 Matrix.......: Matrix.......: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Prep Batch #...: Prep Batch #...: 9328355

Mercury ND 0.20 ug/L SW846 7470A 11/24/09 LPPG61AG

Dilution Factor: 1 Analysis Time..: 15:13 MS Run #.......: 9328186

Prep Batch #...: Prep Batch #...: 9331296

Silver ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG61AL

Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144

Aluminum Aluminum 597 30.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61AM LPPG61AM

Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144

Arsenic Arsenic 1.9 1.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61AN LPPG61AN

Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144

Barium 65.4 10.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61AP LPPG61AP

Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144

Beryllium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG61AQ

Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144

Calcium Calcium 31600 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61AR LPPG61AR

Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144

Cadmium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG61AT

Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144

Cobalt 2.8 0.50 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61AU LPPG61AU

Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144

Chromium Chromium 3.0 2.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61AV LPPG61AV

Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144

Copper ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPG61AW

Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144

Iron 10200 50.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61AX LPPG61AX

Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144

(Continued on next page)

C9K180557 106 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L1-S3

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9K180557-007 Matrix.........: Matrix.........: WATER

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Potassium Potassium 2360 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61A0 LPPG61A0

Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144

Magnesium Magnesium 18500 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61A1 LPPG61A1

Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144

Manganese Manganese 277 0.50 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61A2 LPPG61A2

Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144

Sodium 4640 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61A3 LPPG61A3

Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144

Nickel 1.7 1.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61A4 LPPG61A4

Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144

Lead ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG61A5

Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144

Selenium ND 5.0 ug/L SW846 6020 11/27-11/29/09 LPPG61AA

Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144

Thallium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG61AC

Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144

Antimony ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPG61AD

Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144

Vanadium Vanadium 2.2 1.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61AE LPPG61AE

Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144

Zinc 10.3 5.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG61AF LPPG61AF

Dilution Factor: 1 Analysis Time..: 01:18 MS Run #.......: 9331144

C9K180557 107 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L1-S4

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9K180557-008 Matrix.......: Matrix.......: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Prep Batch #...: Prep Batch #...: 9328355

Mercury ND 0.20 ug/L SW846 7470A 11/24/09 LPPG81AN

Dilution Factor: 1 Analysis Time..: 15:16 MS Run #.......: 9328186

Prep Batch #...: Prep Batch #...: 9331296

Silver ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG81AT

Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144

Aluminum Aluminum 145 30.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG81AU LPPG81AU

Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144

Arsenic ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG81AV

Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144

Barium 33.6 10.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG81AW LPPG81AW

Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144

Beryllium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG81AX

Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144

Calcium Calcium 45100 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG81A0 LPPG81A0

Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144

Cadmium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG81A1

Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144

Cobalt ND 0.50 ug/L SW846 6020 11/27-11/29/09 LPPG81A2

Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144

Chromium Chromium 3.9 2.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG81A3 LPPG81A3

Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144

Copper ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPG81A4

Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144

Iron 3420 50.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG81A5 LPPG81A5

Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144

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Clean Sites Environmental Services Inc

Client Sample ID: L1-S4

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9K180557-008 Matrix.........: Matrix.........: WATER

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Potassium Potassium 1910 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG81AA LPPG81AA

Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144

Magnesium Magnesium 3500 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG81AC LPPG81AC

Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144

Manganese Manganese 194 0.50 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG81AD LPPG81AD

Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144

Sodium 7050 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG81AE LPPG81AE

Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144

Nickel 3.1 1.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG81AF LPPG81AF

Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144

Lead ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG81AG

Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144

Selenium ND 5.0 ug/L SW846 6020 11/27-11/29/09 LPPG81AH

Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144

Thallium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPG81AJ

Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144

Antimony ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPG81AK

Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144

Vanadium Vanadium 9.9 1.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG81AL LPPG81AL

Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144

Zinc 5.1 5.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPG81AM LPPG81AM

Dilution Factor: 1 Analysis Time..: 01:22 MS Run #.......: 9331144

C9K180557 109 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SW-1

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9K180557-009 Matrix.......: Matrix.......: WATER

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Prep Batch #...: Prep Batch #...: 9328355

Mercury ND 0.20 ug/L SW846 7470A 11/24/09 LPPHA1AV

Dilution Factor: 1 Analysis Time..: 15:22 MS Run #.......: 9328186

Prep Batch #...: Prep Batch #...: 9331296

Silver ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHA1A1

Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144

Aluminum Aluminum 446 30.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1A2 LPPHA1A2

Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144

Arsenic ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHA1A3

Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144

Barium 65.8 10.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1A4 LPPHA1A4

Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144

Beryllium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHA1A5

Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144

Calcium Calcium 16500 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1AA LPPHA1AA

Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144

Cadmium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHA1AC

Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144

Cobalt 1.1 0.50 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1AD LPPHA1AD

Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144

Chromium Chromium 4.1 2.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1AE LPPHA1AE

Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144

Copper ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPHA1AF

Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144

Iron 1000 50.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1AG LPPHA1AG

Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144

(Continued on next page)

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Clean Sites Environmental Services Inc

Client Sample ID: SW-1

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9K180557-009 Matrix.........: Matrix.........: WATER

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Potassium Potassium 3700 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1AH LPPHA1AH

Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144

Magnesium Magnesium 5120 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1AJ LPPHA1AJ

Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144

Manganese Manganese 102 0.50 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1AK LPPHA1AK

Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144

Sodium 6170 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1AL LPPHA1AL

Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144

Nickel 2.2 1.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1AM LPPHA1AM

Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144

Lead ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHA1AN

Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144

Selenium ND 5.0 ug/L SW846 6020 11/27-11/29/09 LPPHA1AP

Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144

Thallium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHA1AQ

Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144

Antimony ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPHA1AR

Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144

Vanadium Vanadium 2.5 1.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1AT LPPHA1AT

Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144

Zinc 15.4 5.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHA1AU LPPHA1AU

Dilution Factor: 1 Analysis Time..: 01:26 MS Run #.......: 9331144

C9K180557 111 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SW-2

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9K180557-010 Matrix.......: Matrix.......: WATER

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Prep Batch #...: Prep Batch #...: 9328355

Mercury ND 0.20 ug/L SW846 7470A 11/24/09 LPPHF1A3

Dilution Factor: 1 Analysis Time..: 15:24 MS Run #.......: 9328186

Prep Batch #...: Prep Batch #...: 9331296

Silver ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHF1AC

Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144

Aluminum Aluminum 448 30.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1AD LPPHF1AD

Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144

Arsenic ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHF1AE

Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144

Barium 61.5 10.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1AF LPPHF1AF

Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144

Beryllium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHF1AG

Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144

Calcium Calcium 16000 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1AH LPPHF1AH

Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144

Cadmium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHF1AJ

Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144

Cobalt 0.98 0.50 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1AK LPPHF1AK

Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144

Chromium Chromium 3.7 2.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1AL LPPHF1AL

Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144

Copper ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPHF1AM

Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144

Iron 994 50.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1AN LPPHF1AN

Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144

(Continued on next page)

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Clean Sites Environmental Services Inc

Client Sample ID: SW-2

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9K180557-010 Matrix.........: Matrix.........: WATER

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Potassium Potassium 3480 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1AP LPPHF1AP

Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144

Magnesium Magnesium 5120 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1AQ LPPHF1AQ

Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144

Manganese Manganese 89.9 0.50 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1AR LPPHF1AR

Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144

Sodium 5850 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1AT LPPHF1AT

Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144

Nickel 2.1 1.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1AU LPPHF1AU

Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144

Lead ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHF1AV

Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144

Selenium ND 5.0 ug/L SW846 6020 11/27-11/29/09 LPPHF1AW

Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144

Thallium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHF1AX

Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144

Antimony ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPHF1A0

Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144

Vanadium Vanadium 1.9 1.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1A1 LPPHF1A1

Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144

Zinc 11.4 5.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHF1A2 LPPHF1A2

Dilution Factor: 1 Analysis Time..: 01:31 MS Run #.......: 9331144

C9K180557 113 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SW-3

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9K180557-011 Matrix.......: Matrix.......: WATER

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Prep Batch #...: Prep Batch #...: 9328355

Mercury ND 0.20 ug/L SW846 7470A 11/24/09 LPPHG1A3

Dilution Factor: 1 Analysis Time..: 15:25 MS Run #.......: 9328186

Prep Batch #...: Prep Batch #...: 9331296

Silver ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHG1AC

Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144

Aluminum Aluminum 415 30.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1AD LPPHG1AD

Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144

Arsenic ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHG1AE

Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144

Barium 60.0 10.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1AF LPPHG1AF

Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144

Beryllium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHG1AG

Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144

Calcium Calcium 16300 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1AH LPPHG1AH

Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144

Cadmium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHG1AJ

Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144

Cobalt 0.91 0.50 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1AK LPPHG1AK

Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144

Chromium Chromium 3.9 2.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1AL LPPHG1AL

Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144

Copper ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPHG1AM

Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144

Iron 1040 50.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1AN LPPHG1AN

Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144

(Continued on next page)

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Clean Sites Environmental Services Inc

Client Sample ID: SW-3

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9K180557-011 Matrix.........: Matrix.........: WATER

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Potassium Potassium 3440 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1AP LPPHG1AP

Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144

Magnesium Magnesium 5140 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1AQ LPPHG1AQ

Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144

Manganese Manganese 92.2 0.50 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1AR LPPHG1AR

Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144

Sodium 5700 100 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1AT LPPHG1AT

Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144

Nickel 2.1 1.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1AU LPPHG1AU

Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144

Lead ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHG1AV

Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144

Selenium ND 5.0 ug/L SW846 6020 11/27-11/29/09 LPPHG1AW

Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144

Thallium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LPPHG1AX

Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144

Antimony ND 2.0 ug/L SW846 6020 11/27-11/29/09 LPPHG1A0

Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144

Vanadium Vanadium 2.5 1.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1A1 LPPHG1A1

Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144

Zinc 12.2 5.0 ug/L SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHG1A2 LPPHG1A2

Dilution Factor: 1 Analysis Time..: 01:35 MS Run #.......: 9331144

C9K180557 115 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SED-1

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9K180557-012 Matrix.......: Matrix.......: SOLID

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09

% Moisture.....: % Moisture.....: 20

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Prep Batch #...: Prep Batch #...: 9327175

Mercury ND 0.041 mg/kg SW846 7471A 11/23/09 LPPHK1A6

Dilution Factor: 1 Analysis Time..: 17:57 MS Run #.......: 9327086

Prep Batch #...: Prep Batch #...: 9331299

Silver ND 0.12 mg/kg SW846 6020 11/27-11/29/09 LPPHK1AF

Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147

Aluminum Aluminum 1470 3.7 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AG LPPHK1AG

Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147

Arsenic Arsenic 0.17 0.12 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AH LPPHK1AH

Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147

Barium 14.5 1.2 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AJ LPPHK1AJ

Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147

Beryllium Beryllium 0.75 0.12 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AK LPPHK1AK

Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147

Calcium Calcium 885 12.4 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AL LPPHK1AL

Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147

Cadmium ND 0.12 mg/kg SW846 6020 11/27-11/29/09 LPPHK1AM

Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147

Cobalt 3.5 0.062 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AN LPPHK1AN

Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147

Chromium Chromium 2.4 0.25 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AP LPPHK1AP

Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147

Copper 0.60 0.25 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AQ LPPHK1AQ

Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147

Iron 10900 6.2 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AR LPPHK1AR

Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147

(Continued on next page)

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Clean Sites Environmental Services Inc

Client Sample ID: SED-1

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9K180557-012 Matrix.........: Matrix.........: SOLID

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Potassium Potassium 72.9 12.4 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AT LPPHK1AT

Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147

Magnesium Magnesium 293 12.4 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AU LPPHK1AU

Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147

Manganese Manganese 94.5 0.062 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AV LPPHK1AV

Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147

Sodium 29.3 12.4 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AW LPPHK1AW

Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147

Nickel 1.2 0.12 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1AX LPPHK1AX

Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147

Lead 2.1 0.12 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1A0 LPPHK1A0

Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147

Selenium ND 0.62 mg/kg SW846 6020 11/27-11/29/09 LPPHK1A1

Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147

Thallium ND 0.12 mg/kg SW846 6020 11/27-11/29/09 LPPHK1A2

Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147

Antimony ND 0.25 mg/kg SW846 6020 11/27-11/29/09 LPPHK1A3

Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147

Vanadium Vanadium 4.6 0.12 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1A4 LPPHK1A4

Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147

Zinc 16.8 0.62 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHK1A5 LPPHK1A5

Dilution Factor: 1 Analysis Time..: 02:05 MS Run #.......: 9331147

NOTE(S): ___________________________________________________________________________________________

Results and reporting limits have been adjusted for dry weight.

C9K180557 117 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SED-2

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9K180557-013 Matrix.......: Matrix.......: SOLID

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09

% Moisture.....: % Moisture.....: 20

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Prep Batch #...: Prep Batch #...: 9327175

Mercury ND 0.041 mg/kg SW846 7471A 11/23/09 LPPHM1AH

Dilution Factor: 1 Analysis Time..: 18:03 MS Run #.......: 9327086

Prep Batch #...: Prep Batch #...: 9331299

Silver ND 0.12 mg/kg SW846 6020 11/27-11/29/09 LPPHM1AN

Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147

Aluminum Aluminum 1080 3.7 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1AP LPPHM1AP

Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147

Arsenic Arsenic 0.43 0.12 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1AQ LPPHM1AQ

Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147

Barium 12.5 1.2 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1AR LPPHM1AR

Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147

Beryllium ND 0.12 mg/kg SW846 6020 11/27-11/29/09 LPPHM1AT

Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147

Calcium Calcium 386 12.5 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1AU LPPHM1AU

Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147

Cadmium ND 0.12 mg/kg SW846 6020 11/27-11/29/09 LPPHM1AV

Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147

Cobalt 0.93 0.062 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1AW LPPHM1AW

Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147

Chromium Chromium 2.2 0.25 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1AX LPPHM1AX

Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147

Copper 0.47 0.25 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1A0 LPPHM1A0

Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147

Iron 2430 6.2 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1A1 LPPHM1A1

Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147

(Continued on next page)

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Clean Sites Environmental Services Inc

Client Sample ID: SED-2

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9K180557-013 Matrix.........: Matrix.........: SOLID

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Potassium Potassium 82.5 12.5 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1A2 LPPHM1A2

Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147

Magnesium Magnesium 121 12.5 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1A3 LPPHM1A3

Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147

Manganese Manganese 32.0 0.062 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1A4 LPPHM1A4

Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147

Sodium 25.9 12.5 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1A5 LPPHM1A5

Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147

Nickel 0.75 0.12 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1A6 LPPHM1A6

Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147

Lead 2.1 0.12 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1AA LPPHM1AA

Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147

Selenium ND 0.62 mg/kg SW846 6020 11/27-11/29/09 LPPHM1AC

Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147

Thallium ND 0.12 mg/kg SW846 6020 11/27-11/29/09 LPPHM1AD

Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147

Antimony ND 0.25 mg/kg SW846 6020 11/27-11/29/09 LPPHM1AE

Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147

Vanadium Vanadium 2.7 0.12 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1AF LPPHM1AF

Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147

Zinc 10.2 0.62 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHM1AG LPPHM1AG

Dilution Factor: 1 Analysis Time..: 02:22 MS Run #.......: 9331147

NOTE(S): ___________________________________________________________________________________________

Results and reporting limits have been adjusted for dry weight.

C9K180557 119 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SED-3

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9K180557-014 Matrix.......: Matrix.......: SOLID

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09

% Moisture.....: % Moisture.....: 23

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Prep Batch #...: Prep Batch #...: 9327175

Mercury ND 0.043 mg/kg SW846 7471A 11/23/09 LPPHN1AQ

Dilution Factor: 1 Analysis Time..: 18:09 MS Run #.......: 9327086

Prep Batch #...: Prep Batch #...: 9331299

Silver ND 0.13 mg/kg SW846 6020 11/27-11/29/09 LPPHN1AW

Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147

Aluminum Aluminum 2080 3.9 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1AX LPPHN1AX

Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147

Arsenic Arsenic 0.28 0.13 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1A0 LPPHN1A0

Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147

Barium 23.0 1.3 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1A1 LPPHN1A1

Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147

Beryllium Beryllium 0.19 0.13 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1A2 LPPHN1A2

Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147

Calcium Calcium 631 12.9 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1A3 LPPHN1A3

Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147

Cadmium ND 0.13 mg/kg SW846 6020 11/27-11/29/09 LPPHN1A4

Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147

Cobalt 1.6 0.065 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1A5 LPPHN1A5

Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147

Chromium Chromium 3.3 0.26 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1A6 LPPHN1A6

Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147

Copper 0.78 0.26 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1AA LPPHN1AA

Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147

Iron 2780 6.5 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1AC LPPHN1AC

Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147

(Continued on next page)

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Clean Sites Environmental Services Inc

Client Sample ID: SED-3

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9K180557-014 Matrix.........: Matrix.........: SOLID

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Potassium Potassium 114 12.9 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1AD LPPHN1AD

Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147

Magnesium Magnesium 252 12.9 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1AE LPPHN1AE

Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147

Manganese Manganese 57.5 0.065 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1AF LPPHN1AF

Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147

Sodium 29.9 12.9 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1AG LPPHN1AG

Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147

Nickel 1.3 0.13 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1AH LPPHN1AH

Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147

Lead 3.1 0.13 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1AJ LPPHN1AJ

Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147

Selenium ND 0.65 mg/kg SW846 6020 11/27-11/29/09 LPPHN1AK

Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147

Thallium ND 0.13 mg/kg SW846 6020 11/27-11/29/09 LPPHN1AL

Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147

Antimony ND 0.26 mg/kg SW846 6020 11/27-11/29/09 LPPHN1AM

Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147

Vanadium Vanadium 2.5 0.13 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1AN LPPHN1AN

Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147

Zinc 16.0 0.65 mg/kg SW846 6020 SW846 6020 11/27-11/29/09 11/27-11/29/09 LPPHN1AP LPPHN1AP

Dilution Factor: 1 Analysis Time..: 02:26 MS Run #.......: 9331147

NOTE(S): ___________________________________________________________________________________________

Results and reporting limits have been adjusted for dry weight.

C9K180557 121 of 161
METHOD BLANK REPORT

TOTAL Metals

Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: SOLID

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

MB Lot-Sample #: MB Lot-Sample #: C9K230000-175 Prep Batch #...: Prep Batch #...: 9327175

Mercury ND 0.033 mg/kg SW846 7471A 11/23/09 LP05J1AA

Dilution Factor: 1

Analysis Time..: 17:40

MB Lot-Sample #: MB Lot-Sample #: C9K270000-299 Prep Batch #...: Prep Batch #...: 9331299

Silver ND 0.10 mg/kg SW846 6020 11/27-11/29/09 LP72P1AA

Dilution Factor: 1

Analysis Time..: 01:42

Aluminum ND 3.0 mg/kg SW846 6020 11/27-11/29/09 LP72P1AC

Dilution Factor: 1

Analysis Time..: 01:42

Arsenic ND 0.10 mg/kg SW846 6020 11/27-11/29/09 LP72P1AD

Dilution Factor: 1

Analysis Time..: 01:42

Barium ND 1.0 mg/kg SW846 6020 11/27-11/29/09 LP72P1AE

Dilution Factor: 1

Analysis Time..: 01:42

Beryllium ND 0.10 mg/kg SW846 6020 11/27-11/29/09 LP72P1AF

Dilution Factor: 1

Analysis Time..: 01:42

Calcium ND 10.0 mg/kg SW846 6020 11/27-11/29/09 LP72P1AG

Dilution Factor: 1

Analysis Time..: 01:42

Cadmium ND 0.10 mg/kg SW846 6020 11/27-11/29/09 LP72P1AH

Dilution Factor: 1

Analysis Time..: 01:42

Cobalt ND 0.050 mg/kg SW846 6020 11/27-11/29/09 LP72P1AJ

Dilution Factor: 1

Analysis Time..: 01:42

Chromium ND 0.20 mg/kg SW846 6020 11/27-11/29/09 LP72P1AK

Dilution Factor: 1

Analysis Time..: 01:42

(Continued on next page)

C9K180557 122 of 161
METHOD BLANK REPORT

TOTAL Metals

Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: SOLID

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Copper ND 0.20 mg/kg SW846 6020 11/27-11/29/09 LP72P1AL

Dilution Factor: 1

Analysis Time..: 01:42

Iron ND 5.0 mg/kg SW846 6020 11/27-11/29/09 LP72P1AM

Dilution Factor: 1

Analysis Time..: 01:42

Potassium ND 10.0 mg/kg SW846 6020 11/27-11/29/09 LP72P1AN

Dilution Factor: 1

Analysis Time..: 01:42

Magnesium ND 10.0 mg/kg SW846 6020 11/27-11/29/09 LP72P1AP

Dilution Factor: 1

Analysis Time..: 01:42

Manganese ND 0.050 mg/kg SW846 6020 11/27-11/29/09 LP72P1AQ

Dilution Factor: 1

Analysis Time..: 01:42

Sodium ND 10.0 mg/kg SW846 6020 11/27-11/29/09 LP72P1AR

Dilution Factor: 1

Analysis Time..: 01:42

Nickel ND 0.10 mg/kg SW846 6020 11/27-11/29/09 LP72P1AT

Dilution Factor: 1

Analysis Time..: 01:42

Lead ND 0.10 mg/kg SW846 6020 11/27-11/29/09 LP72P1AU

Dilution Factor: 1

Analysis Time..: 01:42

Selenium ND 0.50 mg/kg SW846 6020 11/27-11/29/09 LP72P1AV

Dilution Factor: 1

Analysis Time..: 01:42

Thallium ND 0.10 mg/kg SW846 6020 11/27-11/29/09 LP72P1AW

Dilution Factor: 1

Analysis Time..: 01:42

Antimony ND 0.20 mg/kg SW846 6020 11/27-11/29/09 LP72P1AX

Dilution Factor: 1

Analysis Time..: 01:42

Vanadium ND 0.10 mg/kg SW846 6020 11/27-11/29/09 LP72P1A0

Dilution Factor: 1

Analysis Time..: 01:42

(Continued on next page)

C9K180557 123 of 161
METHOD BLANK REPORT

TOTAL Metals

Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: SOLID

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Zinc ND 0.50 mg/kg SW846 6020 11/27-11/29/09 LP72P1A1

Dilution Factor: 1

Analysis Time..: 01:42

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

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METHOD BLANK REPORT

TOTAL Metals

Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: WATER

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

MB Lot-Sample #: MB Lot-Sample #: C9K240000-355 Prep Batch #...: Prep Batch #...: 9328355

Mercury ND 0.20 ug/L SW846 7470A 11/24/09 LP2861AA

Dilution Factor: 1

Analysis Time..: 14:58

MB Lot-Sample #: MB Lot-Sample #: C9K270000-296 Prep Batch #...: Prep Batch #...: 9331296

Silver ND 1.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AA

Dilution Factor: 1

Analysis Time..: 00:25

Aluminum ND 30.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AC

Dilution Factor: 1

Analysis Time..: 00:25

Arsenic ND 1.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AD

Dilution Factor: 1

Analysis Time..: 00:25

Barium ND 10.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AE

Dilution Factor: 1

Analysis Time..: 00:25

Beryllium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AF

Dilution Factor: 1

Analysis Time..: 00:25

Calcium ND 100 ug/L SW846 6020 11/27-11/29/09 LP72G1AG

Dilution Factor: 1

Analysis Time..: 00:25

Cadmium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AH

Dilution Factor: 1

Analysis Time..: 00:25

Cobalt ND 0.50 ug/L SW846 6020 11/27-11/29/09 LP72G1AJ

Dilution Factor: 1

Analysis Time..: 00:25

Chromium ND 2.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AK

Dilution Factor: 1

Analysis Time..: 00:25

(Continued on next page)

C9K180557 125 of 161
METHOD BLANK REPORT

TOTAL Metals

Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: WATER

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Copper ND 2.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AL

Dilution Factor: 1

Analysis Time..: 00:25

Iron ND 50.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AM

Dilution Factor: 1

Analysis Time..: 00:25

Potassium ND 100 ug/L SW846 6020 11/27-11/29/09 LP72G1AN

Dilution Factor: 1

Analysis Time..: 00:25

Magnesium ND 100 ug/L SW846 6020 11/27-11/29/09 LP72G1AP

Dilution Factor: 1

Analysis Time..: 00:25

Manganese ND 0.50 ug/L SW846 6020 11/27-11/29/09 LP72G1AQ

Dilution Factor: 1

Analysis Time..: 00:25

Sodium ND 100 ug/L SW846 6020 11/27-11/29/09 LP72G1AR

Dilution Factor: 1

Analysis Time..: 00:25

Nickel ND 1.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AT

Dilution Factor: 1

Analysis Time..: 00:25

Lead ND 1.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AU

Dilution Factor: 1

Analysis Time..: 00:25

Selenium ND 5.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AV

Dilution Factor: 1

Analysis Time..: 00:25

Thallium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AW

Dilution Factor: 1

Analysis Time..: 00:25

Antimony ND 2.0 ug/L SW846 6020 11/27-11/29/09 LP72G1AX

Dilution Factor: 1

Analysis Time..: 00:25

Vanadium ND 1.0 ug/L SW846 6020 11/27-11/29/09 LP72G1A0

Dilution Factor: 1

Analysis Time..: 00:25

(Continued on next page)

C9K180557 126 of 161
METHOD BLANK REPORT

TOTAL Metals

Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: WATER

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Zinc ND 5.0 ug/L SW846 6020 11/27-11/29/09 LP72G1A1

Dilution Factor: 1

Analysis Time..: 00:25

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

C9K180557 127 of 161
LABORATORY CONTROL SAMPLE EVALUATION REPORT

TOTAL Metals

Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: SOLID

PERCENT RECOVERY PREPARATIONPARAMETER ___________ RECOVERY ________ LIMITS __________ METHOD _________________ ANALYSIS DATE ______________ WORK ORDER # ____________

LCS Lot-Sample#: LCS Lot-Sample#: C9K230000-175 Prep Batch #...: Prep Batch #...: 9327175

Mercury 99 (80 - 120) SW846 7471A 11/23/09 LP05J1AC

Dilution Factor: 1 Analysis Time..: 17:46

LCS Lot-Sample#: LCS Lot-Sample#: C9K270000-299 Prep Batch #...: Prep Batch #...: 9331299

Silver 98 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1A2

Dilution Factor: 1 Analysis Time..: 01:46

Aluminum 107 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1A3

Dilution Factor: 1 Analysis Time..: 01:46

Arsenic 87 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1A4

Dilution Factor: 1 Analysis Time..: 01:46

Barium 93 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1A5

Dilution Factor: 1 Analysis Time..: 01:46

Beryllium 83 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1A6

Dilution Factor: 1 Analysis Time..: 01:46

Calcium 99 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1A7

Dilution Factor: 1 Analysis Time..: 01:46

Cadmium 95 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1A8

Dilution Factor: 1 Analysis Time..: 01:46

Cobalt 86 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1A9

Dilution Factor: 1 Analysis Time..: 01:46

Chromium 96 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CA

Dilution Factor: 1 Analysis Time..: 01:46

Copper 87 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CC

Dilution Factor: 1 Analysis Time..: 01:46

Iron 97 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CD

Dilution Factor: 1 Analysis Time..: 01:46

Potassium 87 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CE

Dilution Factor: 1 Analysis Time..: 01:46

(Continued on next page)

C9K180557 128 of 161
LABORATORY CONTROL SAMPLE EVALUATION REPORT

TOTAL Metals

Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: SOLID

PERCENT RECOVERY PREPARATIONPARAMETER ___________ RECOVERY ________ LIMITS __________ METHOD _________________ ANALYSIS DATE ______________ WORK ORDER # ____________

Magnesium 108 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CF

Dilution Factor: 1 Analysis Time..: 01:46

Manganese 93 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CG

Dilution Factor: 1 Analysis Time..: 01:46

Sodium 83 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CH

Dilution Factor: 1 Analysis Time..: 01:46

Nickel 84 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CJ

Dilution Factor: 1 Analysis Time..: 01:46

Lead 107 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CK

Dilution Factor: 1 Analysis Time..: 01:46

Selenium 98 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CL

Dilution Factor: 1 Analysis Time..: 01:46

Thallium 104 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CM

Dilution Factor: 1 Analysis Time..: 01:46

Antimony 95 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CN

Dilution Factor: 1 Analysis Time..: 01:46

Vanadium 96 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CP

Dilution Factor: 1 Analysis Time..: 01:46

Zinc 87 (80 - 120) SW846 6020 11/27-11/29/09 LP72P1CQ

Dilution Factor: 1 Analysis Time..: 01:46

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

C9K180557 129 of 161
LABORATORY CONTROL SAMPLE EVALUATION REPORT

TOTAL Metals

Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: WATER

PERCENT RECOVERY PREPARATIONPARAMETER ___________ RECOVERY ________ LIMITS __________ METHOD _________________ ANALYSIS DATE ______________ WORK ORDER # ____________

LCS Lot-Sample#: LCS Lot-Sample#: C9K240000-355 Prep Batch #...: Prep Batch #...: 9328355

Mercury 108 (80 - 120) SW846 7470A 11/24/09 LP2861AC

Dilution Factor: 1 Analysis Time..: 15:00

LCS Lot-Sample#: LCS Lot-Sample#: C9K270000-296 Prep Batch #...: Prep Batch #...: 9331296

Silver 97 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1A2

Dilution Factor: 1 Analysis Time..: 00:30

Aluminum 106 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1A3

Dilution Factor: 1 Analysis Time..: 00:30

Arsenic 91 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1A4

Dilution Factor: 1 Analysis Time..: 00:30

Barium 93 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1A5

Dilution Factor: 1 Analysis Time..: 00:30

Beryllium 86 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1A6

Dilution Factor: 1 Analysis Time..: 00:30

Calcium 99 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1A7

Dilution Factor: 1 Analysis Time..: 00:30

Cadmium 94 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1A8

Dilution Factor: 1 Analysis Time..: 00:30

Cobalt 86 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1A9

Dilution Factor: 1 Analysis Time..: 00:30

Chromium 95 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CA

Dilution Factor: 1 Analysis Time..: 00:30

Copper 87 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CC

Dilution Factor: 1 Analysis Time..: 00:30

Iron 97 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CD

Dilution Factor: 1 Analysis Time..: 00:30

Potassium 88 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CE

Dilution Factor: 1 Analysis Time..: 00:30

(Continued on next page)

C9K180557 130 of 161
LABORATORY CONTROL SAMPLE EVALUATION REPORT

TOTAL Metals

Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: WATER

PERCENT RECOVERY PREPARATIONPARAMETER ___________ RECOVERY ________ LIMITS __________ METHOD _________________ ANALYSIS DATE ______________ WORK ORDER # ____________

Magnesium 106 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CF

Dilution Factor: 1 Analysis Time..: 00:30

Manganese 93 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CG

Dilution Factor: 1 Analysis Time..: 00:30

Sodium 83 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CH

Dilution Factor: 1 Analysis Time..: 00:30

Nickel 84 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CJ

Dilution Factor: 1 Analysis Time..: 00:30

Lead 105 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CK

Dilution Factor: 1 Analysis Time..: 00:30

Selenium 101 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CL

Dilution Factor: 1 Analysis Time..: 00:30

Thallium 102 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CM

Dilution Factor: 1 Analysis Time..: 00:30

Antimony 95 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CN

Dilution Factor: 1 Analysis Time..: 00:30

Vanadium 96 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CP

Dilution Factor: 1 Analysis Time..: 00:30

Zinc 88 (80 - 120) SW846 6020 11/27-11/29/09 LP72G1CQ

Dilution Factor: 1 Analysis Time..: 00:30

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

C9K180557 131 of 161
MATRIX SPIKE SAMPLE EVALUATION REPORT

TOTAL Metals

Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09

PERCENT RECOVERY RPD PREPARATION- WORK

PARAMETER ___________ RECOVERY ________ LIMITS __________ RPD ____ LIMITS ______ METHOD _________________ ANALYSIS DATE ______________ ORDER # _______

MS Lot-Sample #: MS Lot-Sample #: C9K180557-001 Prep Batch #...: Prep Batch #...: 9328355

Mercury 106 (75 - 125) SW846 7470A 11/24/09 LPPF51A7

107 (75 - 125) 0.93 (0-20) SW846 7470A 11/24/09 LPPF51A8

Dilution Factor: 1

Analysis Time..: 15:04

MS Run #.......: 9328186

MS Lot-Sample #: MS Lot-Sample #: C9K180557-001 Prep Batch #...: Prep Batch #...: 9331296

Silver 100 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51CC

99 (75 - 125) 1.2 (0-20) SW846 6020 11/27-11/29/09 LPPF51CD

Dilution Factor: 1

Analysis Time..: 00:42

MS Run #.......: 9331144

Aluminum 135 N (75 - 125) SW846 6020 11/27-11/29/09 LPPF51CE

137 N (75 - 125) 0.87 (0-20) SW846 6020 11/27-11/29/09 LPPF51CF

Dilution Factor: 1

Analysis Time..: 00:42

MS Run #.......: 9331144

Arsenic 89 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51CG

88 (75 - 125) 0.81 (0-20) SW846 6020 11/27-11/29/09 LPPF51CH

Dilution Factor: 1

Analysis Time..: 00:42

MS Run #.......: 9331144

Barium 96 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51CJ

95 (75 - 125) 0.92 (0-20) SW846 6020 11/27-11/29/09 LPPF51CK

Dilution Factor: 1

Analysis Time..: 00:42

MS Run #.......: 9331144

Beryllium 84 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51CL

81 (75 - 125) 3.6 (0-20) SW846 6020 11/27-11/29/09 LPPF51CM

Dilution Factor: 1

Analysis Time..: 00:42

MS Run #.......: 9331144

Calcium 98 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51CN

97 (75 - 125) 0.59 (0-20) SW846 6020 11/27-11/29/09 LPPF51CP

Dilution Factor: 1

Analysis Time..: 00:42

MS Run #.......: 9331144

(Continued on next page)

C9K180557 132 of 161
MATRIX SPIKE SAMPLE EVALUATION REPORT

TOTAL Metals

Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09

PERCENT RECOVERY RPD PREPARATION- WORK

PARAMETER ___________ RECOVERY ________ LIMITS __________ RPD ____ LIMITS ______ METHOD _________________ ANALYSIS DATE ______________ ORDER # _______

Cadmium 97 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51CQ

97 (75 - 125) 0.12 (0-20) SW846 6020 11/27-11/29/09 LPPF51CR

Dilution Factor: 1

Analysis Time..: 00:42

MS Run #.......: 9331144

Cobalt 84 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51CT

84 (75 - 125) 0.82 (0-20) SW846 6020 11/27-11/29/09 LPPF51CU

Dilution Factor: 1

Analysis Time..: 00:42

MS Run #.......: 9331144

Chromium 92 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51CV

91 (75 - 125) 0.58 (0-20) SW846 6020 11/27-11/29/09 LPPF51CW

Dilution Factor: 1

Analysis Time..: 00:42

MS Run #.......: 9331144

Copper 85 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51CX

84 (75 - 125) 1.1 (0-20) SW846 6020 11/27-11/29/09 LPPF51C0

Dilution Factor: 1

Analysis Time..: 00:42

MS Run #.......: 9331144

Iron 93 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51C1

92 (75 - 125) 0.61 (0-20) SW846 6020 11/27-11/29/09 LPPF51C2

Dilution Factor: 1

Analysis Time..: 00:42

MS Run #.......: 9331144

Potassium 86 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51C3

86 (75 - 125) 0.56 (0-20) SW846 6020 11/27-11/29/09 LPPF51C4

Dilution Factor: 1

Analysis Time..: 00:42

MS Run #.......: 9331144

Magnesium 105 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51C5

105 (75 - 125) 0.23 (0-20) SW846 6020 11/27-11/29/09 LPPF51C6

Dilution Factor: 1

Analysis Time..: 00:42

MS Run #.......: 9331144

(Continued on next page)

C9K180557 133 of 161
MATRIX SPIKE SAMPLE EVALUATION REPORT

TOTAL Metals

Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09

PERCENT RECOVERY RPD PREPARATION- WORK

PARAMETER ___________ RECOVERY ________ LIMITS __________ RPD ____ LIMITS ______ METHOD _________________ ANALYSIS DATE ______________ ORDER # _______

Manganese 90 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51C7

90 (75 - 125) 0.45 (0-20) SW846 6020 11/27-11/29/09 LPPF51C8

Dilution Factor: 1

Analysis Time..: 00:42

MS Run #.......: 9331144

Sodium 81 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51C9

81 (75 - 125) 0.51 (0-20) SW846 6020 11/27-11/29/09 LPPF51DA

Dilution Factor: 1

Analysis Time..: 00:42

MS Run #.......: 9331144

Nickel 82 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51DC

97 (75 - 125) 17 (0-20) SW846 6020 11/27-11/29/09 LPPF51DD

Dilution Factor: 1

Analysis Time..: 00:42

MS Run #.......: 9331144

Lead 109 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51DE

109 (75 - 125) 0.64 (0-20) SW846 6020 11/27-11/29/09 LPPF51DF

Dilution Factor: 1

Analysis Time..: 00:42

MS Run #.......: 9331144

Selenium 93 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51DG

94 (75 - 125) 1.1 (0-20) SW846 6020 11/27-11/29/09 LPPF51DH

Dilution Factor: 1

Analysis Time..: 00:42

MS Run #.......: 9331144

Thallium 106 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51DJ

105 (75 - 125) 0.11 (0-20) SW846 6020 11/27-11/29/09 LPPF51DK

Dilution Factor: 1

Analysis Time..: 00:42

MS Run #.......: 9331144

Antimony 99 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51DL

99 (75 - 125) 0.30 (0-20) SW846 6020 11/27-11/29/09 LPPF51DM

Dilution Factor: 1

Analysis Time..: 00:42

MS Run #.......: 9331144

(Continued on next page)

C9K180557 134 of 161
MATRIX SPIKE SAMPLE EVALUATION REPORT

TOTAL Metals

Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09

PERCENT RECOVERY RPD PREPARATION- WORK

PARAMETER ___________ RECOVERY ________ LIMITS __________ RPD ____ LIMITS ______ METHOD _________________ ANALYSIS DATE ______________ ORDER # _______

Vanadium 95 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51DN

94 (75 - 125) 0.33 (0-20) SW846 6020 11/27-11/29/09 LPPF51DP

Dilution Factor: 1

Analysis Time..: 00:42

MS Run #.......: 9331144

Zinc 84 (75 - 125) SW846 6020 11/27-11/29/09 LPPF51DQ

84 (75 - 125) 0.23 (0-20) SW846 6020 11/27-11/29/09 LPPF51DR

Dilution Factor: 1

Analysis Time..: 00:42

MS Run #.......: 9331144

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

N Spiked analyte recovery is outside stated control limits.

C9K180557 135 of 161
MATRIX SPIKE SAMPLE EVALUATION REPORT

TOTAL Metals

Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: SOLID

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09

PERCENT RECOVERY RPD PREPARATION- WORK

PARAMETER ___________ RECOVERY ________ LIMITS __________ RPD ____ LIMITS ______ METHOD _________________ ANALYSIS DATE ______________ ORDER # _______

MS Lot-Sample #: MS Lot-Sample #: C9K180557-012 Prep Batch #...: Prep Batch #...: 9327175

% Moisture.....: % Moisture.....: 20

Mercury 107 (75 - 125) SW846 7471A 11/23/09 LPPHK1CD

106 (75 - 125) 0.93 (0-20) SW846 7471A 11/23/09 LPPHK1CE

Dilution Factor: 1

Analysis Time..: 17:59

MS Run #.......: 9327086

MS Lot-Sample #: MS Lot-Sample #: C9K180557-012 Prep Batch #...: Prep Batch #...: 9331299

% Moisture.....: % Moisture.....: 20

Silver 95 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1CF

96 (75 - 125) 1.3 (0-20) SW846 6020 11/27-11/29/09 LPPHK1CG

Dilution Factor: 1

Analysis Time..: 02:13

MS Run #.......: 9331147

Aluminum NC (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1CH

NC (75 - 125) (0-20) SW846 6020 11/27-11/29/09 LPPHK1CJ

Dilution Factor: 1

Analysis Time..: 02:13

MS Run #.......: 9331147

Arsenic 83 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1CK

86 (75 - 125) 4.1 (0-20) SW846 6020 11/27-11/29/09 LPPHK1CL

Dilution Factor: 1

Analysis Time..: 02:13

MS Run #.......: 9331147

Barium 90 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1CM

92 (75 - 125) 2.0 (0-20) SW846 6020 11/27-11/29/09 LPPHK1CN

Dilution Factor: 1

Analysis Time..: 02:13

MS Run #.......: 9331147

Beryllium 71 N (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1CP

76 (75 - 125) 5.7 (0-20) SW846 6020 11/27-11/29/09 LPPHK1CQ

Dilution Factor: 1

Analysis Time..: 02:13

MS Run #.......: 9331147

(Continued on next page)

C9K180557 136 of 161
MATRIX SPIKE SAMPLE EVALUATION REPORT

TOTAL Metals

Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: SOLID

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09

PERCENT RECOVERY RPD PREPARATION- WORK

PARAMETER ___________ RECOVERY ________ LIMITS __________ RPD ____ LIMITS ______ METHOD _________________ ANALYSIS DATE ______________ ORDER # _______

Calcium 85 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1CR

91 (75 - 125) 6.4 (0-20) SW846 6020 11/27-11/29/09 LPPHK1CT

Dilution Factor: 1

Analysis Time..: 02:13

MS Run #.......: 9331147

Cadmium 93 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1CU

95 (75 - 125) 2.2 (0-20) SW846 6020 11/27-11/29/09 LPPHK1CV

Dilution Factor: 1

Analysis Time..: 02:13

MS Run #.......: 9331147

Cobalt 78 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1CW

79 (75 - 125) 1.6 (0-20) SW846 6020 11/27-11/29/09 LPPHK1CX

Dilution Factor: 1

Analysis Time..: 02:13

MS Run #.......: 9331147

Chromium 89 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1C0

116 * (75 - 125) 24 (0-20) SW846 6020 11/27-11/29/09 LPPHK1C1

Dilution Factor: 1

Analysis Time..: 02:13

MS Run #.......: 9331147

Copper 81 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1C2

83 (75 - 125) 1.8 (0-20) SW846 6020 11/27-11/29/09 LPPHK1C3

Dilution Factor: 1

Analysis Time..: 02:13

MS Run #.......: 9331147

Iron NC (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1C4

NC (75 - 125) (0-20) SW846 6020 11/27-11/29/09 LPPHK1C5

Dilution Factor: 1

Analysis Time..: 02:13

MS Run #.......: 9331147

Potassium 83 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1C6

85 (75 - 125) 2.0 (0-20) SW846 6020 11/27-11/29/09 LPPHK1C7

Dilution Factor: 1

Analysis Time..: 02:13

MS Run #.......: 9331147

(Continued on next page)

C9K180557 137 of 161
MATRIX SPIKE SAMPLE EVALUATION REPORT

TOTAL Metals

Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: SOLID

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09

PERCENT RECOVERY RPD PREPARATION- WORK

PARAMETER ___________ RECOVERY ________ LIMITS __________ RPD ____ LIMITS ______ METHOD _________________ ANALYSIS DATE ______________ ORDER # _______

Magnesium 102 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1C8

110 (75 - 125) 7.2 (0-20) SW846 6020 11/27-11/29/09 LPPHK1C9

Dilution Factor: 1

Analysis Time..: 02:13

MS Run #.......: 9331147

Manganese 18 N (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1DA

54 N (75 - 125) 19 (0-20) SW846 6020 11/27-11/29/09 LPPHK1DC

Dilution Factor: 1

Analysis Time..: 02:13

MS Run #.......: 9331147

Sodium 79 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1DD

79 (75 - 125) 0.83 (0-20) SW846 6020 11/27-11/29/09 LPPHK1DE

Dilution Factor: 1

Analysis Time..: 02:13

MS Run #.......: 9331147

Nickel 79 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1DF

82 (75 - 125) 3.9 (0-20) SW846 6020 11/27-11/29/09 LPPHK1DG

Dilution Factor: 1

Analysis Time..: 02:13

MS Run #.......: 9331147

Lead 100 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1DH

113 (75 - 125) 6.6 (0-20) SW846 6020 11/27-11/29/09 LPPHK1DJ

Dilution Factor: 1

Analysis Time..: 02:13

MS Run #.......: 9331147

Selenium 77 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1DK

92 (75 - 125) 16 (0-20) SW846 6020 11/27-11/29/09 LPPHK1DL

Dilution Factor: 1

Analysis Time..: 02:13

MS Run #.......: 9331147

Thallium 101 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1DM

103 (75 - 125) 1.9 (0-20) SW846 6020 11/27-11/29/09 LPPHK1DN

Dilution Factor: 1

Analysis Time..: 02:13

MS Run #.......: 9331147

(Continued on next page)

C9K180557 138 of 161
MATRIX SPIKE SAMPLE EVALUATION REPORT

TOTAL Metals

Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: SOLID

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09

PERCENT RECOVERY RPD PREPARATION- WORK

PARAMETER ___________ RECOVERY ________ LIMITS __________ RPD ____ LIMITS ______ METHOD _________________ ANALYSIS DATE ______________ ORDER # _______

Antimony 88 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1DP

88 (75 - 125) 0.40 (0-20) SW846 6020 11/27-11/29/09 LPPHK1DQ

Dilution Factor: 1

Analysis Time..: 02:13

MS Run #.......: 9331147

Vanadium 88 (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1DR

91 (75 - 125) 3.3 (0-20) SW846 6020 11/27-11/29/09 LPPHK1DT

Dilution Factor: 1

Analysis Time..: 02:13

MS Run #.......: 9331147

Zinc 73 N (75 - 125) SW846 6020 11/27-11/29/09 LPPHK1DU

96 (75 - 125) 20 (0-20) SW846 6020 11/27-11/29/09 LPPHK1DV

Dilution Factor: 1

Analysis Time..: 02:13

MS Run #.......: 9331147

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

Results and reporting limits have been adjusted for dry weight.

NC The recovery and/or RPD were not calculated.

* Relative percent difference (RPD) is outside stated control limits.

N Spiked analyte recovery is outside stated control limits.

C9K180557 139 of 161
Clean Sites Environmental Services Inc

Client Sample ID: MW-1S

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9K180557-001 Work Order #...: Work Order #...: LPPF5 Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Recoverable ND 0.010 mg/L SW846 9066 11/19-11/20/09 9323286

Phenolics

Dilution Factor: 1 Analysis Time..: 08:36 MS Run #.......: 9323208

Total Organic Carbon Total Organic Carbon 10.2 1.0 mg/L SM20 5310B SM20 5310B 11/20/09 11/20/09 9324028 9324028

(TOC)

Dilution Factor: 1 Analysis Time..: 14:06 MS Run #.......:

C9K180557 140 of 161
Clean Sites Environmental Services Inc

Client Sample ID: MW-3S

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9K180557-002 Work Order #...: Work Order #...: LPPGN Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Recoverable ND 0.010 mg/L SW846 9066 11/19-11/20/09 9323286

Phenolics

Dilution Factor: 1 Analysis Time..: 08:11 MS Run #.......: 9323208

Total Organic Carbon Total Organic Carbon 6.3 1.0 mg/L SM20 5310B SM20 5310B 11/20/09 11/20/09 9324028 9324028

(TOC)

Dilution Factor: 1 Analysis Time..: 14:14 MS Run #.......:

C9K180557 141 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L2-S1

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9K180557-003 Work Order #...: Work Order #...: LPPGP Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Recoverable ND 0.010 mg/L SW846 9066 11/19-11/20/09 9323286

Phenolics

Dilution Factor: 1 Analysis Time..: 08:11 MS Run #.......: 9323208

Total Organic Carbon Total Organic Carbon 2.3 1.0 mg/L SM20 5310B SM20 5310B 11/20/09 11/20/09 9324028 9324028

(TOC)

Dilution Factor: 1 Analysis Time..: 14:44 MS Run #.......:

C9K180557 142 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L1-S1

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9K180557-006 Work Order #...: Work Order #...: LPPG1 Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Organic Carbon Total Organic Carbon 1.3 1.0 mg/L SM20 5310B SM20 5310B 11/20/09 11/20/09 9324028 9324028

(TOC)

Dilution Factor: 1 Analysis Time..: 14:52 MS Run #.......:

C9K180557 143 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L1-S3

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9K180557-007 Work Order #...: Work Order #...: LPPG6 Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Organic Carbon Total Organic Carbon 4.6 1.0 mg/L SM20 5310B SM20 5310B 11/20/09 11/20/09 9324028 9324028

(TOC)

Dilution Factor: 1 Analysis Time..: 15:01 MS Run #.......:

C9K180557 144 of 161
Clean Sites Environmental Services Inc

Client Sample ID: L1-S4

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9K180557-008 Work Order #...: Work Order #...: LPPG8 Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/14/09 Date Received..: Date Received..: 11/18/09

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Organic Carbon Total Organic Carbon 7.3 1.0 mg/L SM20 5310B SM20 5310B 11/20/09 11/20/09 9324028 9324028

(TOC)

Dilution Factor: 1 Analysis Time..: 15:10 MS Run #.......:

C9K180557 145 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SW-1

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9K180557-009 Work Order #...: Work Order #...: LPPHA Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Organic Carbon Total Organic Carbon 19.6 1.0 mg/L SM20 5310B SM20 5310B 11/20/09 11/20/09 9324028 9324028

(TOC)

Dilution Factor: 1 Analysis Time..: 15:19 MS Run #.......:

C9K180557 146 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SW-2

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9K180557-010 Work Order #...: Work Order #...: LPPHF Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Organic Carbon Total Organic Carbon 19.0 1.0 mg/L SM20 5310B SM20 5310B 11/20/09 11/20/09 9324028 9324028

(TOC)

Dilution Factor: 1 Analysis Time..: 15:27 MS Run #.......:

C9K180557 147 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SW-3

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9K180557-011 Work Order #...: Work Order #...: LPPHG Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Organic Carbon Total Organic Carbon 19.4 1.0 mg/L SM20 5310B SM20 5310B 11/20/09 11/20/09 9324028 9324028

(TOC)

Dilution Factor: 1 Analysis Time..: 15:36 MS Run #.......:

C9K180557 148 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SED-1

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9K180557-012 Work Order #...: Work Order #...: LPPHK Matrix.........: Matrix.........: SOLID

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09

% Moisture.....: % Moisture.....: 20

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Percent Solids Percent Solids 80.4 1.0 % SM20 2540G SM20 2540G 11/24-11/25/09 11/24-11/25/09 9328026 9328026

Dilution Factor: 1 Analysis Time..: 09:35 MS Run #.......: 9328015

Total Organic Carbon ND 622 mg/kg EPA Lloyd Kahn 11/25-11/27/09 9329104

(TOC)

Dilution Factor: 1 Analysis Time..: 00:00 MS Run #.......: 9329086

NOTE(S): ___________________________________________________________________________________________

RL Reporting Limit

Results and reporting limits have been adjusted for dry weight.

C9K180557 149 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SED-2

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9K180557-013 Work Order #...: Work Order #...: LPPHM Matrix.........: Matrix.........: SOLID

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09

% Moisture.....: % Moisture.....: 20

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Percent Solids Percent Solids 80.3 1.0 % SM20 2540G SM20 2540G 11/24-11/25/09 11/24-11/25/09 9328026 9328026

Dilution Factor: 1 Analysis Time..: 09:35 MS Run #.......: 9328015

Total Organic Carbon Total Organic Carbon 817 623 mg/kg EPA Lloyd Kahn EPA Lloyd Kahn 11/27/09 11/27/09 9331165 9331165

(TOC)

Dilution Factor: 1 Analysis Time..: 15:46 MS Run #.......: 9331072

NOTE(S): ___________________________________________________________________________________________

RL Reporting Limit

Results and reporting limits have been adjusted for dry weight.

C9K180557 150 of 161
Clean Sites Environmental Services Inc

Client Sample ID: SED-3

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9K180557-014 Work Order #...: Work Order #...: LPPHN Matrix.........: Matrix.........: SOLID

Date Sampled...: Date Sampled...: 11/15/09 Date Received..: Date Received..: 11/18/09

% Moisture.....: % Moisture.....: 23

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Percent Solids Percent Solids 77.3 1.0 % SM20 2540G SM20 2540G 11/24-11/25/09 11/24-11/25/09 9328026 9328026

Dilution Factor: 1 Analysis Time..: 09:35 MS Run #.......: 9328015

Total Organic Carbon Total Organic Carbon 2810 647 mg/kg EPA Lloyd Kahn EPA Lloyd Kahn 11/27/09 11/27/09 9331165 9331165

(TOC)

Dilution Factor: 1 Analysis Time..: 00:00 MS Run #.......: 9331072

NOTE(S): ___________________________________________________________________________________________

RL Reporting Limit

Results and reporting limits have been adjusted for dry weight.

C9K180557 151 of 161
METHOD BLANK REPORT

General Chemistry

Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: WATER

REPORTING PREPARATION- PREP

PARAMETER __________________ RESULT __________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Organic Carbon Work Order #: LPTQ81AA MB Lot-Sample #: C9K200000-028

(TOC)

ND 1.0 mg/L SM20 5310B 11/20/09 9324028

Dilution Factor: 1

Analysis Time..: 13:33

Total Recoverable Work Order #: LPRH61AA MB Lot-Sample #: C9K190000-286

Phenolics

ND 0.010 mg/L SW846 9066 11/19-11/20/09 9323286

Dilution Factor: 1

Analysis Time..: 08:05

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

C9K180557 152 of 161
METHOD BLANK REPORT

General Chemistry

Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: SOLID

REPORTING PREPARATION- PREP

PARAMETER __________________ RESULT __________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Organic Carbon Work Order #: LP4W51AA MB Lot-Sample #: C9K250000-104

(TOC)

ND 500 mg/kg EPA Lloyd Kahn 11/25/09 9329104

Dilution Factor: 1

Analysis Time..: 15:48

Total Organic Carbon Work Order #: LP7ME1AA MB Lot-Sample #: C9K270000-165

(TOC)

ND 500 mg/kg EPA Lloyd Kahn 11/27/09 9331165

Dilution Factor: 1

Analysis Time..: 15:02

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

C9K180557 153 of 161
LABORATORY CONTROL SAMPLE EVALUATION REPORT

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9K180557 Matrix.........: Matrix.........: WATER

PERCENT RECOVERY RPD PREPARATION- PREP

PARAMETER ___________ RECOVERY ________ LIMITS __________ RPD ____ LIMITS ______ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Organic Carbon WO#:LPTQ81AC-LCS/LPTQ81AD-LCSD LCS Lot-Sample#: C9K200000-028

(TOC)

99 (80 - 120) SM20 5310B 11/20/09 9324028

100 (80 - 120) 0.63 (0-10) SM20 5310B 11/20/09 9324028

Dilution Factor: 1 Analysis Time..: 13:05

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

C9K180557 154 of 161
LABORATORY CONTROL SAMPLE EVALUATION REPORT

General Chemistry

Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: WATER

PERCENT RECOVERY PREPARATION- PREP

PARAMETER ___________ RECOVERY ________ LIMITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Recoverable Work Order #: LPRH61AC LCS Lot-Sample#: C9K190000-286

Phenolics

93 (75 - 125) SW846 9066 11/19-11/20/09 9323286

Dilution Factor: 1 Analysis Time..: 08:05

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

C9K180557 155 of 161
LABORATORY CONTROL SAMPLE EVALUATION REPORT

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9K180557 Matrix.........: Matrix.........: SOLID

PERCENT RECOVERY RPD PREPARATION- PREP

PARAMETER ___________ RECOVERY ________ LIMITS __________ RPD ____ LIMITS ______ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Organic Carbon WO#:LP4W51AC-LCS/LP4W51AD-LCSD LCS Lot-Sample#: C9K250000-104

(TOC)

96 (75 - 125) EPA Lloyd Kahn 11/25/09 9329104

87 (75 - 125) 9.1 (0-20) EPA Lloyd Kahn 11/25/09 9329104

Dilution Factor: 1.79 Analysis Time..: 16:03

Total Organic Carbon WO#:LP7ME1AC-LCS/LP7ME1AD-LCSD LCS Lot-Sample#: C9K270000-165

(TOC)

97 (75 - 125) EPA Lloyd Kahn 11/27/09 9331165

96 (75 - 125) 1.3 (0-20) EPA Lloyd Kahn 11/27/09 9331165

Dilution Factor: 1.8 Analysis Time..: 15:17

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

C9K180557 156 of 161
MATRIX SPIKE SAMPLE EVALUATION REPORT

General Chemistry

Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 11/17/09 Date Received..: Date Received..: 11/18/09

PERCENT RECOVERY RPD PREPARATION- PREP

PARAMETER ___________ RECOVERY ________ LIMITS __________ RPD ____ LIMITS ______ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Recoverable WO#: LPNN11AF-MS/LPNN11AG-MSD MS Lot-Sample #: C9K180471-002

Phenolics

81 (75 - 125) SW846 9066 11/19-11/20/09 9323284

87 (75 - 125) 7.1 (0-20) SW846 9066 11/19-11/20/09 9323284

Dilution Factor: 1

Analysis Time..: 08:05

MS Run #.......: 9323208

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

C9K180557 157 of 161
MATRIX SPIKE SAMPLE EVALUATION REPORT

General Chemistry

Client Lot #...: Client Lot #...: C9K180557 Matrix.........: Matrix.........: SOLID

Date Sampled...: Date Sampled...: 11/23/09 Date Received..: Date Received..: 11/25/09

PERCENT RECOVERY RPD PREPARATION- PREP

PARAMETER ___________ RECOVERY ________ LIMITS __________ RPD ____ LIMITS ______ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

% Moisture.....: % Moisture.....: 100

Total Organic Carbon WO#: LPTNR1DF-MS/LPTNR1DG-MSD MS Lot-Sample #: C9K190670-015

(TOC)

96 (75 - 125) EPA Lloyd Kahn 11/25/09 9329104

104 (75 - 125) 8.3 (0-20) EPA Lloyd Kahn 11/25/09 9329104

Dilution Factor: 1.74

Analysis Time..: 20:52

MS Run #.......: 9329086

% Moisture.....: % Moisture.....: 100

Total Organic Carbon WO#: LP59K1AH-MS/LP59K1AJ-MSD MS Lot-Sample #: C9K250536-001

(TOC)

96 (75 - 125) EPA Lloyd Kahn 11/27/09 9331165

94 (75 - 125) 4.9 (0-20) EPA Lloyd Kahn 11/27/09 9331165

Dilution Factor: 1.74

Analysis Time..: 19:23

MS Run #.......: 9331072

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

Results and reporting limits have been adjusted for dry weight.

C9K180557 158 of 161
SAMPLE DUPLICATE EVALUATION REPORT

General Chemistry

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPHK9-SMP Matrix.......: Matrix.......: SOLID

LPHK9-DUP

Date Sampled...: Date Sampled...: 11/12/09 Date Received..: Date Received..: 11/14/09

% Moisture.....: % Moisture.....: 9.8

DUPLICATE RPD PREPARATION- PREP

PARAM_____ RESULT ___________ RESULT ___________ UNITS ________ RPD _____ LIMIT _______ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Percent Solids SD Lot-Sample #: C9K140458-001

90.2 87.7 % 2.8 (0-20) SM20 2540G 11/24-11/25/09 9328026

Dilution Factor: 1 Analysis Time..: 09:35 MS Run Number..: 9328015

C9K180557 159 of 161
SAMPLE DUPLICATE EVALUATION REPORT

General Chemistry

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LPTNR-SMP Matrix.......: Matrix.......: SOLID

LPTNR-DUP

Date Sampled...: Date Sampled...: 11/18/09 Date Received..: Date Received..: 11/19/09

% Moisture.....: % Moisture.....: 53

DUPLICATE RPD PREPARATION- PREP

PARAM_____ RESULT ___________ RESULT ___________ UNITS ________ RPD _____ LIMIT _______ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Organic Carbon SD Lot-Sample #: C9K190670-015

(TOC)

8980 8210 mg/kg 8.9 (0-20) EPA Lloyd Kahn 11/25/09 9329104

Dilution Factor: 1.8 Analysis Time..: 20:09 MS Run Number..: 9329086

NOTE(S): ___________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

Results and reporting limits have been adjusted for dry weight.

C9K180557 160 of 161
SAMPLE DUPLICATE EVALUATION REPORT

General Chemistry

Client Lot #...: Client Lot #...: C9K180557 Work Order #...: Work Order #...: LP59K-SMP Matrix.......: Matrix.......: SOLID

LP59K-DUP

Date Sampled...: Date Sampled...: 11/23/09 Date Received..: Date Received..: 11/25/09

DUPLICATE RPD PREPARATION- PREP

PARAM_____ RESULT ___________ RESULT ___________ UNITS ________ RPD _____ LIMIT _______ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Organic Carbon SD Lot-Sample #: C9K250536-001

(TOC)

12600 11700 mg/kg 8.0 (0-20) EPA Lloyd Kahn 11/27/09 9331165

Dilution Factor: 1.77 Analysis Time..: 18:25 MS Run Number..: 9331072

NOTE(S): ___________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

Results and reporting limits have been adjusted for dry weight.

C9K180557 161 of 161