Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

-down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

-down boxes to fill in the units of

measure.Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

-
5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

3181 Mitchell Power Station 1_3 No.6 Fuel Oil (residual or bunker C)Fuel Type 2 Fuel Type 3 Other Fuel Description No.6 Fuel Oil (residual or bunker C)EIA

Facility Code Facility Name Boiler ID Basis An alyte

3181 Mitchell Power Station 1_3 As Received Heat of Combustion 3181 Mitchell Power Station 1_3 As Received Water by Distillation 3181 Mitchell Power Station 1_3 As Received Metals 3181 Mitchell Power Station 1_3 As Received Anions 3181 Mitchell Power Station 1_3 As Received Mercury 3181 Mitchell Power Station 1_3 As Received Carbon, Hydrogen, Nitrogen 3181 Mitchell Power Station 1_3 As Received Oxygen 3181 Mitchell Power Station 1_3 As Received SulfurAn alysis M ethod for each Analyte

(example: ASTM D5865-04)
ASTM D240 ASTM D95 EPA 3040A 6010B EPA 5050 9056 EPA 245.1 ASTM D5291 ASTM D5291_MOD ASTM D4294EIA Facility Code Facility Name Boiler ID 3181 Mitchell Power Station 1_3

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) A-OIL-1A 7/20/2010 7/20/2010 19053 A-OIL-2A 7/21/2010 7/21/2010 19035 A-OIL-3A 7/22/2010 7/22/2010 19073 A-OIL-4A 7/23/2010 7/23/2010 19061 Fuel Testing ResultsHAPs Test Group

Acid gas HAPs

HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) Btu/lb N/A N/A 0.1208 Btu/lb N/A N/A 0.1137 Btu/lb N/A N/A 0.1067 Btu/lb N/A N/A 0.1069HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) N/A N/A 0.0008 % 0.000488 N/A N/A 0.0008 % 0.000513 N/A N/A 0.0007 % 0.001180 N/A N/A 0.0008 % 0.000954Mercury

Units Antimony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] μg/gChromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) [<0.5] μg/g [<1] μg/g [<0.5] μg/g [<0.5] μg/g [<1] [<0.5] μg/g [<1] μg/g [<0.5] μg/g [<0.5] μg/g [<1] [<0.5] μg/g [<1] μg/g [<0.5] μg/g [<0.5] μg/g [<1] [<0.5] μg/g [<1] μg/g [<0.5] μg/g [<0.5] μg/g [<1]Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Selenium Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h μg/g 17 ppm [<0.5] μg/g μg/g 12 ppm [<0.5] μg/g μg/g 15 ppm [<0.5] μg/g μg/g 11 ppm [<0.5] μg/g Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Ultimate Analy

ses, % by

wtEIA Facility Code Facility Name Boiler ID 3181 Mitchell Power Station 1_3

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) A-OIL-1A 7/20/2010 7/20/2010 19053 A-OIL-2A 7/21/2010 7/21/2010 19035 A-OIL-3A 7/22/2010 7/22/2010 19073 A-OIL-4A 7/23/2010 7/23/2010 19061 Fuel Testing ResultsHAPs Test Group

Mercury and non-mercury metalic HAPs

HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) Btu/lb N/A N/A 0.1208 Btu/lb N/A N/A 0.1137 Btu/lb N/A N/A 0.1067 Btu/lb N/A N/A 0.1069HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units N/A N/A 0.0008 % 0.000488 μg/g N/A N/A 0.0008 % 0.000513 μg/g N/A N/A 0.0007 % 0.001180 μg/g N/A N/A 0.0008 % 0.000954 μg/gAn timony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5]Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units μg/g [<1] μg/g [<0.5] μg/g [<0.5] μg/g [<1] μg/g μg/g [<1] μg/g [<0.5] μg/g [<0.5] μg/g [<1] μg/g μg/g [<1] μg/g [<0.5] μg/g [<0.5] μg/g [<1] μg/g μg/g [<1] μg/g [<0.5] μg/g [<0.5] μg/g [<1] μg/gNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Fluorine (Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h Fixed Carbon 17 ppm [<0.5] μg/g 12 ppm [<0.5] μg/g 15 ppm [<0.5] μg/g 11 ppm [<0.5] μg/g Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen

Ultimate Analy

ses, % by

wtEIA Facility Code Facility Name Boiler ID 3181 Mitchell Power Station 1_3

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) A-OIL-1A 7/20/2010 7/20/2010 19053 A-OIL-2A 7/21/2010 7/21/2010 19035 A-OIL-3A 7/22/2010 7/22/2010 19073 A-OIL-4A 7/23/2010 7/23/2010 19061 Fuel Testing ResultsHAPs Test Group

Non-dioxin/furan organic HAPs

HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) Btu/lb N/A N/A 0.1208 Btu/lb N/A N/A 0.1137 Btu/lb N/A N/A 0.1067 Btu/lb N/A N/A 0.1069HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units N/A N/A 0.0008 % 0.000488 μg/g N/A N/A 0.0008 % 0.000513 μg/g N/A N/A 0.0007 % 0.001180 μg/g N/A N/A 0.0008 % 0.000954 μg/gAn timony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5]Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units μg/g [<1] μg/g [<0.5] μg/g [<0.5] μg/g [<1] μg/g μg/g [<1] μg/g [<0.5] μg/g [<0.5] μg/g [<1] μg/g μg/g [<1] μg/g [<0.5] μg/g [<0.5] μg/g [<1] μg/g μg/g [<1] μg/g [<0.5] μg/g [<0.5] μg/g [<1] μg/gNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Fluorine (Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h Fixed Carbon 17 ppm [<0.5] μg/g 12 ppm [<0.5] μg/g 15 ppm [<0.5] μg/g 11 ppm [<0.5] μg/g Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen

Ultimate Analy

ses, % by

wtEIA Facility Code Facility Name Boiler ID 3181 Mitchell Power Station 1_3

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) A-OIL-1A 7/20/2010 7/20/2010 19053 A-OIL-2A 7/21/2010 7/21/2010 19035 A-OIL-3A 7/22/2010 7/22/2010 19073 A-OIL-4A 7/23/2010 7/23/2010 19061 Fuel Testing ResultsHAPs Test Group

Dioxin/furan HAPs

HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) Btu/lb N/A N/A 0.1208 Btu/lb N/A N/A 0.1137 Btu/lb N/A N/A 0.1067 Btu/lb N/A N/A 0.1069HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units N/A N/A 0.0008 % 0.000488 μg/g N/A N/A 0.0008 % 0.000513 μg/g N/A N/A 0.0007 % 0.001180 μg/g N/A N/A 0.0008 % 0.000954 μg/gAn timony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5] μg/g [<0.5]Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units μg/g [<1] μg/g [<0.5] μg/g [<0.5] μg/g [<1] μg/g μg/g [<1] μg/g [<0.5] μg/g [<0.5] μg/g [<1] μg/g μg/g [<1] μg/g [<0.5] μg/g [<0.5] μg/g [<1] μg/g μg/g [<1] μg/g [<0.5] μg/g [<0.5] μg/g [<1] μg/gNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Fluorine (Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h Fixed Carbon 17 ppm [<0.5] μg/g 12 ppm [<0.5] μg/g 15 ppm [<0.5] μg/g 11 ppm [<0.5] μg/g Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen

Ultimate Analy

ses, % by

wt