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# OAR Box 1672 Prepped by Charmelle Mathews



### Document

Number:

Docket Number: 

# A-98-1 3

Printed 9/30/2008 11:01:00 AM Sheet 40 of 132P. 2 

## A 9 8 1 3 ll?C- H Dat e sent : Mon # 

### 0 9 Fe b199 8 15:44:1 2 -050 0 From : STEV E SHED D<SHEDD.STEVEOEPAMAIL.EPA.GOV> To : rlwright@ashland . co m Subject : IC R Rick , Thank s fo r th e cal l an d th e informatio n o n packagin g and blendin g operation s a t Ashland Chemica l Corporation . Someon e fromPE S wil l b e following-up o n thos e facilities . W e wil l als o add yo u t o th e lis t t o receiv e E-mail s o n upcomin g meeting s an d material s o n thi s project , etc . Attache d i s a draf t ICR targete d mor e a t terminal s and pipelin e facilities . W e wil l likel yd o anothe r IC R i n th e futur e fo r stand-alon e packagin g an d blendin g facilitie s and adjus t th e attache d t o reflec t thos e operation s and lesse n unnecessaryinformation . Th e attache d doe s contai n some packagin g an d blendin g question s fo r terminal s and pipelin e facilitie s tha t hav e thos e type s o f operation s collocate d o n site . Agai n thank s fo r th e information ! Stev e Stephe n Shedd U.S . EP A Offic e o f Ai r Qualit yPlanning and Standard s Researc hTriangl e Park , N C 2771 1 voice : (919 ) 541-539 7 fax : (919 ) 541-024 6 E-mail : Shedd.SteveOEPAMAIL.EPA.GOV



# C O Bernd Hanek e - - 1 - - Tue , 1 0 Fe b199 8 11:49:1 7P. 3



### MAXIMU M ACHIEVABL E CONTRO L TECHNOLOG Y(MACT ) STANDARD S DEVELOPMENT INFORMATIO N REQUES T 

## Instruction s Thi s informatio n reques t i s t o b e complete d fo r operation s tha t compris e th e organi c liquid s distribution(non gasoline ) sourc e categor ya t you r plant . Th e sourc e categor yi s thos e activitie s associate d wit hth e storag e an d distributio n o f organi c liquid s othe r tha n gasoline , a t site s whic hserv e a s distributio n point s fro mwhic horgani c liquid s ma yb e obtaine d fo r furthe r us e an d processing . Thi s reques t cover s th e storag e and transfe r o f organi c liquid s (including equipmen t leaks ) , and als o consider s wast e an d wastewate r treatmen t and disposa l practices . W e ar e requestin g informatio n regarding eac hcompoun d identifie d a s a hazardou s ai r pollutan t (HAP ) tha t i s use d i n o r emitte d byanyoperations , including fugitiv e emissio n sources , tha t ar e par t o f th e organi c liquid s distributio n (non-gasoline ) sourc e categor ya t you r facility . Not e that , fo r thi s survey , w e woul d als o lik e informatio n o n an

ygasolin e storag e and distributio n activitie s a t eac hfacilit yi n orde r t o completel y characteriz e th e operation s and t o understan d th e tota l emission s pictur e a t th e facility . Fil l ou t thi s informatio n reques t a s completel ya s possibl e fro mexistin g information . A t a minimum , provid e (1 ) informatio n o n th e presenc e o f HA P emission s and (2 ) HA P emissio n estimate s base d o n previousl yobtaine d tes t dat a o r o n engineerin g calculations , provide d ther e i s a basi s fo r suc h calculations . Attachmen t Ainclude s th e EPA' s lis t o f hazardou s ai r pollutant s tha t yo u shoul d refe r t o whe n completin g th e survey . Al l dat a and response s shoul d b e base d o n calenda r yea r 199 7 emissions , material s handled , and emissio n contro l equipmen t (unles s yo u ca n justif yselectio n o f a n alternat e bas e year ) . Pleas e b e sur e t o keep a copyo f th e complete d surve yfo r you r records . Yo u shoul d als o kee p copie s o f anynote s o r calculation s yo u performi n completin g th e survey . I f yo u nee d mor e spac e t o complet e you r response ,



# t .P. 4



### pleas e includ e th e additiona l informatio n i n a clearl y labele d attachment . I f yo u believ e ther e i s additiona l informatio n tha t i s no t requeste d i n th e surve ytha t ma yb e helpfu l t o th e EP Ai n developin g HA P emissio n standard s fo r thi s industry , pleas e includ e thi s informatio n i n a separat e attachment . I f yo u hav e anyquestion s regardin g thi s request , pleas e contac t Mr . Stephe n Shedd , U.S . EPA , Emissio n Standard s Division , a t (919 ) 541-5397 . Retur n thi s informatio n reques t and anyadditiona l informatio n to : Bruc e C . Jordan , Directo r

Emissio n Standard s Divisio n (MD-13 ) U . S . Environmenta l Protectio n Agenc y Offic e o f Ai r Qualit yPlannin g an d Standard s Researc hTriangl e Park , N C 2771 1 Attention : Stephe n Shed d II . ftenara l Informatio n A . Nam e o f lega l owne r o f plant :

B . Nam e o f lega l operato r o f plant , i f differen t fro m lega l owner : C . Addres s o f lega l owner/operato r (pleas e specif y which) : D . Siz e o f company :

Approximat e numbe r o f employee s o f th e busines s enterpris e tha t own s thi s plant , includin g wher e applicable , th e paren t companyand al l subsidiaries , branches , and unrelate d establishment s owne d b yth e paren t compan y(answe r ma yb e give n using th e followin g ranges : 0-100 ; 

# 3P. 5



### 101-250 ; 251-500 ; 501-750 ; 751-1,000 ; 1,001-1,500 ; an d >1,500) :

Numbe r o f plan t employee s associate d wit hth e organi c liquid s distributio n (non-gasoline ) operation :

E . Nam e o f plant : F . Stree t addres s o f plant : G . Latitud e and longitud e coordinate s o f plant ;

H . Nam e o f contact(s ) abl e t o answe r technica l question s abou t th e complete d survey : Nam e Nam e Titl e Titl e Telephon e Telephon e III . Plan t Operation s A . Provid e a n plo t pla n o f th e entir e facilit ywithi n th e fenceline . Thi s figur e shoul d clearl yindicat e al l storag e tank s an d thei r identifie r codes , produc t loadin g o r transfe r areas , produc t flo wlines , an d wastewate r drain s an d treatmen t areas . Us e th e sam e terminology/code s i n identifying facilit yequipmen t a s yo u wil l us e i n completin g Table s 1 throug h9 i n Sectio n IV . B . Provid e a brie f writte n descriptio n o f th e facility' s operations . Lis t th e categorie s (gasoline , refine d petroleum , solvents , glycols , etc. ) o f organi c liqui d material s handle d durin g th e bas e year , an d th e approximat e volum e throughpu t o f eac htyp e o f material . Als o describ e al l activitie s tha t generat e HA P emissions , includin g th e storage , transfer , handling ,



# * 

# yP. 6



### and processin g (sucha s blendin g o r packaging ) o f th e materials , a s wel l a s wastewate r and othe r wast e handling . Again , us e consisten t terminologyan d code s betwee n th e plo t plan , th e writte n description , an d Table s 1 throug h9 i n Sectio n IV . IV . HAPs--Emission s and Control s A . Complet e Table s 1 throug h9 fo r th e HA P emissio n point s an d contro l technique s tha t exis t a t th e facility . Sampl e entrie s ar e shown (i n bol dprint ) i n severa l o f th e tables . Wher e necessary , mak e sufficien t copie s o f blan k table s t o provid e spac e fo r complet e responses . Guidanc e t o hel p yo u fil l ou t thes e table s i s provide d below : 1 . Tabl e 1- -Ente r a cod e fo r eac horgani c liqui d stored , handled , o r loade d a t th e facility . Thi s include s bot hpur e liquid s (e.g. , benzene , methanol ) an d anyliqui d mixture s wit ha n organi c liqui d content , suc ha s wastewater . Code s ar e give n fo r severa l potentia l liquids . Wher e known , includ e th e requeste d liqui d propertie s and th e identit yan d concentratio n o f HAP s presen t i n th e liquid . 2 . Tabl e 2 --Ente r a cod e fo r eac hstorag e tan k wit h greate r tha n 10,000-gallo n («250-barrel ) capacity . Sho weac horgani c liqui d store d i n eac htank durin g th e bas e year , usin g th e same liqui d code s a s use d fo r Tabl e 1 . Fo r eac hadd-o n contro l devic e use d t o contro l vapo r emission s from.storag e tanks , fil l ou t Tabl e 8 fo r tha t typ e o f device . 3 . Tabl e 3 --Ente r eac hloading rack/loadin g armtha t transfer s organi c liquid s t o tank trucks , railcars , barges , o r tanke r ships . W e ar e als o intereste d i n operation s tha t packag e thes e liquid s int o smalle r containers , suc ha s 55-gallo n drums , 1-gallo n o r 1

- quar t cans , etc . A s i n Tabl e 2 , fil l ou t Tabl e 8 fo r eac hcontro l devic e use d t o contro l vapo r emission s fromliqui d transfers .P. 7



### Tabl e 4 --Lis t th e principa l source s o f wastewate r generation , usin g th e supplie d code s o r you r ow n description . Estimat e th e annua l flo wrat e fro m eac hsource . Drain s ar e th e individua l entryway s t o conduit s tha t mov e wate r t o storag e o r treatment . Tabl e 5 --I n thi s tabl e w e wis ht o lear n ho w wastewate r i s collecte d an d treate d a t you r facility(ies) . Fo r eac hwastewate r sourc e a s liste d i n Tabl e 4 , lis t th e numbe r o f collectio n unit s o r treatmen t approache s applicabl e t o eac h source . Th e las t fou r column s reques t informatio n o n whethe r and ho wai r emission s from eac hare a ar e controlled . A s i n Table s 2 and 3 , fil l ou t Tabl e 8 fo r eac hcontro l devic e use d t o contro l vapo r emission s fromwastewater . Tabl e 6 --Non-aqueou s wast e (semi-soli d material , o r sludge ) ma ycontai n an d emi t HA P durin g storage , handling , o r treatment . Identif yeac hindividua l typ e o f waste , an d provid e informatio n o n ho wth e wast e i s collecte d and treated . A s i n Table s 2 , 3 , an d 5 , fil l ou t Tabl e 8 fo r eac hcontro l devic e use d t o contro l ai r emission s fromnon-aqueou s waste . Tabl e 7 --Identif yth e numbe r o f eac htyp e o f equipmen t componen t bytyp e o f servic e (selectin g th e mos t prevalen t servic e fo r eac hcomponent) . LDAR program s involv e a forma l lea k surve yo f component s o n a fixe d schedul e (an d ma yinclud e a non-instrument , visua l program) . A s i n Table s 2 , 3 , 5 , an d 6 , fil l ou t Tabl e 8 fo r eac hcontro l devic e use d t o contro l vapo r emission s from equipmen t components . Tabl e 8- -Complet e th e applicabl e sectio n o f Tabl e 8 fo r eac hai r pollutio n contro l devic e i n us e a t th e facility . Fil l i n th e requeste d parameter s i f known , bu t eve n i f yo u d o no t kno wth e values , a t leas t identif yth e presenc e o f th e devic e by returnin g a tabl e showin g th e typ e o f devic e an d th e emissio n source s tha t i t controls . B e specifi c



# cP. 8



### whe n listin

g the emission sources ; e.g. , Tank s 1 , 2 , 3 , an

d 7 ; Loadin

g Rack s 1- 5 an

d 11-15 ; al l Oil

Wate r Separators ; an d s o forth .

* \P. 9



### TABL E 1 . ORGANI C LIQUID S H-ANDLED AN D HA P CONTENT (a )

Organi cLiqui d Cod e(b) : J T O Liqui d Molecula rWeigh t(lb/lb-mole) : , 9 2

Vapo rMolecula rWeight , 9 2

(lb/lb-mole) : Averag eTrueVapo rPressureo f Liqui d (psia) : , 0. 3

O R Reid Vapo rPressureo f

Liqui d (RVP) : . Averag eLiqui d Density(Lb/Gal) : . 7. 3 Avg . Temperatur

eo f Liqui d Transferred (°F) : , 6 0 Nam eo f HAP s Presen ti nLiqui d . Avg . HA PConcentratio ninLiqui d (ppm wo rpercent )

1,3-Butadiene. Acrylonitril e, Benzen e. Cumen e. Ethylbenzen e. Ethylen edichlorid e. Ethylen eglyco l , Ethyleneoxid e. Formaldehyd e. Methanol . m-Xylen e. o-Xylen e. Phenol . p-Xylen e. Styrene. 

# HP.1 0

8 TABL E 1 . ORGANI C LIQUID S HANDLE D AN D HA P CONTENT(a ) (Continued )
Toluen e Viny l chlorid e (c) . 

## 100 %

_ L
a ) Fo r anyliqui d propert yo r HA P conten t tha t i s unknown , ente r tt UK" o n the correspondin g blank . b ) Selec t th e organi c liqui d nam e tha t describe s th e materia l stored : A S = asphal t A V = aviatio n gasolin e B Z = benzen e CR = crud e oi l D I = diesel/distillat e fue l J F = je t fue l (JP-4 , etc. ) J K = je t kerosene/kerosen e L O = lub e oi l M G = moto r vehicl e gasolin e



# °\P.1 1

9 TABLE1
. ORGANIC LIQUID S HANDLE D AN D HA PCONTENT(a ) (Concluded )

N A= naphth a O G = oxygenate s (MTBE , other ) R F = residua l fue l oi l B U= 1,3-butadien e A C = acrylonitril e C U= cumen e E B = ethy l benzen e E D = ethylen e dichlorid e E G = ethylen e glyco l E O = ethylen e oxid e F O = formaldehyd e M E = methano l M X = m-Xylen e O X = o-Xylen e P H = pheno l P X = p-Xylen e S T = styren e T O = toluen e VA= viny l acetat e V C = viny l chlorid e X X = slo p oil/transmix/wast e produc t O = other , pleas e specif y
c ) Provid e the name s o f anyadditiona l HAP s no t listed .



# lo

### 1 0 TABL E 2 . STORAG E TAN K CONTRO L DAT A

Tan k I D Cod e (a) 1- A 1- A 1- B 1- B 1- C Tan

k Capacit y (Bbl ) (b ) 20,00 0

w 24,00 0

4 4 12,50 0 Nameof

Store d Liqui d (c ) AG J F T X L Annua

l Throughput (Bbl/Yr) 60,00 0 120,00 0 40,00 0 50,00 0 50,00 0 Roo f

Configuratio n (d ) CE F

u IFR

u FX R Floatin g

Roo f Tank s Only : Sea l Typ e (e) MS 3

4 4 LM 3

a

— Tank Roo f Fitting s 

### ( 0 AHBG , GFWBG , VB G

u

u

u

— Add-o n

Contro l Devic e (g ) C

u

u ( 4

—P.1 3



### 1 1 TABL E 2 . STORAG E TAN K CONTRO L DAT A(Continued )

a ) Provid e a uniqu e identifie r cod e fo r eac htan k (e.g. , A-l , B-1) . b ) Provid e th e maximu mcapacit yfo r eac htank . c ) Us e th e sam e organi c liqui d code s a s i n footnot e bo f Tabl e 1 . d ) Selec t th e storag e tan k roo f configuration : FX R «• fixe d roo f IF R = interna l floatin g roo f EF R = externa l floatin g roo f CE F = externa l floatin g roo f converte d t o a n interna l floatin g

roof . e ) Fo r floatin g roo f tanks , ente r th e floatin g dec k sea l type : VM l = vapor-mounte d primar ysea l onl y VM 2 = vapor-mounte d primar ysea l wit hweathe r shiel d VM 3 = vapor-mounte d primar ysea l wit hrim-mounte d secondar yseal . LM l » liquid-mounte d primar ysea l onl y LM 2 = liquid-mounte d primar ysea l wit hweathe r shiel d LM 3 = liquid-mounte d primar ysea l wit hrim-mounte d secondarysea l MS I = mechanica l sho e primar ysea l onl y MS 2 = mechanica l sho e primar ysea l wit hweathe r shiel d MS 3 = mechanica l sho e primar ysea l wit hrim-mounte d secondarysea l 0 = othe r (pleas e specif ytype) . f ) Fo r floatin g roo f tanks , selec t th e code s tha t bes t describ e th e type s o f roo f fitting s i n place : GPWU U= guid e pol e well , unslotted , ungaskete d slidin g coverGPWUG =

guid e pol e well , unslotted , gaskete d slidin g cove r GPSWSU N= guid e pole/sampl e well , slotted , ungaskete d slidin g cover ,

withou t floa t GPSWSU F = guid e pole/sampl e well , slotted , ungaskete d slidin g

cover , wit hfloa t GPSWSG N= guid e pole/sampl e well , slotted , gasketed slidin g cover ,

withou t floa t GPSWSG F = guid e pole/sampl e well , slotted , gaskete d slidin g cover ,

wit hfloa t AHB G= acces s hatch , bolted , gaskete d AHU U= acces s hatch , unbolted , ungaskete d MKJG= acces s hatch , unbolted , gaskete d GFWU U= gauge-floa t well , unbolted , ungaskete d 

# 12-P.1 4

1 2 TABL E 2 . STORAG E TAN K CONTRO L DAT A(Concluded )

GFWU G = gauge-floa t well , unbolted , gaskete d GFWB G = gauge-floa t well , bolted , gaskete d GHSW G = gauge-hatch/sampl e well , gaskete d GHSWU= gauge-hatch/sampl e well , ungaskete d VB G = vacuumbreaker , gaskete d VB U= vacuumbreaker , ungaskete d g ) Selec t th e code(s ) tha t bes t describ e contro l systems , i f any , use d t o contro l vapor s emitte d fromanypar t o f th e tank , includin g ri mseals , fittings , etc. : VCS 1 = vapo r collectio n systemventin g t o a vapor/liqui d absorptio n

uni t (scrubber ) VCS 2 = vapo r collectio n systemventin g t o a n incinerator/boile r VCS 3 = vapo r collectio n systemventin g t o a flar e VCS 4 = vapo r collectio n systemventin g t o a vapor/soli d adsorptio n

uni t VCS 5 = vapo r collectio n systemventin g t o a condense r B = groun d leve l burne r o r therma l oxidize r C = catalyti c oxidize r 0 o other , pleas e provid e a ful l descriptio n (us e extr a sheet ) N= none .



# 12

)1 3 TABLE 3 . LIQUI D TRANSFEROPERATION S

- ^ Rac

k ID Cod e(a ) 1 1 1 2 Ar

m I D Cod e(b ) 1- 1 1- 2 1- 2 2- 1 Organi c Liqui d

Transferred ThroughAr

m(c ) B Z T O M X M G Typ eo f

Transpor t Vehicl eo r Container Fille d(d ) T T T R Annua

l Volumeo f Transferre d Liqui d (Gal/Yr) 500,00 0 400,00 0 600,00 0 1,000,00 0 Metho do f

Loadin g (e ) SUB
u
u
u

• Averag e

Loadin g Rat e (Gal/Min ) 50 0 50 0 500 20 0 Vapo r

Contro l Devic e (f

) VCS 1

u
u VCS 2 Contro l

Devic e Efficiency (g ) 95(EJ) 95(EJ ) 95(EJ ) 90(ST )P.1 6

14 TABL E 3 . LIQUI D TRANSFE R OPERATION S (Concluded )

a ) Provid e a uniqu e identifie r cod e fo r eac hloading rac k o r othe r fillin g equipment . b ) Provid e a uniqu e identifie r cod e fo r eac hloading armi n a rac k o r equipmen t unit . c ) Us e th e same organi c liqui d code s a s i n footnot e bo f Tabl e l . d ) Selec t th e typ e o f transpor t vehicl e loade d o r containe r filled : T = tan k truc k R = tan k ca r (railroad ) B = barg e T = tanke r shi p S C = smal l containe r ( 1 gallo n o r less ; specif ysize ) M C = medium

containe r (> 1 gal. , <5 5 gal. ; specif ysize ) L C = larg e containe r (5 5 gal . drumo r larger ; specif ysize) . e ) Selec t th e metho d o f loading material : SP L = splas h(top ) SUB = to p submerge d BTM t

s botto m

loading . f ) Us e th e sam e contro l devic e code s a s i n footnot e g o f Tabl e 2 . g ) Basi s fo r contro l devic e efficienc yestimate : S A= samplin g and analysi s E J = engineerin g judgmen t S T = sourc e test .



# If cP.1 7



### 1 5 TABL E 4 . WASTEWATE R FLO WRATE S AN D DRAI NCONTROL S

Sourc eo f Wastewate r (a ) Organi cLiqui d Content (b ) Total Flo w Rat e (Gal/Yr) Numbe ro f

Drain s with Emissio n Suppressio n (c ) Numbe ro f

Drains without Emissio n Suppression (c )

a ) Selec t th e code s tha t bes t describ e th e point s o f wastewate r generation : T D S R L R L B O tank drain s (identif yth e specifi c tank s usin g th e same

tank code s a s i n footnot e a o f Tabl e 2 ) stormwate r runof f loadin g rack s (identif yth e specifi c rack s usin g th e same rac k code s a s i n footnot e a o f Tabl e 3 liqui d blending/packagin g operation s other , pleas e provid e ful l descriptio n (us e extr a sheet , i f necessary) . b ) Lis t th e principa l organi c liquid s typicall ypresen t i n eac h wastewate r stream . c ) Emissio n suppressio n control s reduc e emission s fromdrai n pipe s and include , bu t ar e no t limite d to , wate r sea l pot s an d p-traps .



# K

### 1 6 TABL E 5 . WASTEWATE R COLLECTIO NAND TREATMEN

T CONTROL(a )

S> Wastewate rTreatmen

tUni t CollectionUnits : Manhole s Junctio nBoxes Sumps/Catc

h Basins Lif tStation s Storag eTank s ( 0

Treatmen

tApproaches : Oil/Wate rSeparator

s Ai rFlotatio nSystems Coagulation

/ Precipitatio

n Unit s San d Filtratio nUnit Sourc

eo f Wastewate

r (b ) Tota l Numbe r o f Unit s (c ) No . o f

Uncovered Units tha t Ven tt o the Atmospher

e (d ) No . o f

Covere d Units tha t Ventto the Atmospher

e (d ) No . o f

Unit s tha tVent Emissions t

o aContro l Device Contro

l Devic e (e )

o o1 7 TABLE5
. WASTEWATE RCOLLECTIO NAN

D TREATMEN

TCONTROL(a ) (Continued )

O Q Wastewate rTreatmen

tUni t Equalizatio

nUnit s Treatmen tApproaches : Oxidatio nPond s Activate d Sludg eUnit s Tricklin gFilter s Clarifier s Filte rPresse s Stripper s Stormwate rRetentio n Effluent / RecyclePon

d Rotatin gBiologica

l Contactor s Shi p Of f Sit e 

### ( 0 Tota l Numbe r Sourc eo f Wastewate

ro f

Unit s (b ) (c ) No . o f Uncovere d Unit s tha t Ven tt o th e Atmospher

e (d) No . o f

Covere d Unit s tha t Ven tt o the Atmospher

e (d) No . o f

Unit s tha tVent Emissions t

o aContro l Devic e Contro

l Devic e (e )

C OP.2 0

1 8 TABL E 5 . WASTEWATE R COLLECTIO NAN D TREATMEN T CONTROL(a ) (Concluded )

a ) Includ e al l wastewate r collectio n and treatmen t unit s an d an ycontro l device s controllin g vapo r emission s fromsuc hunits . D o no t repor t informatio n o n drain s i n thi s table ; repor t drai n informatio n i n Tabl e 4 . b ) Ente r th e source s o f wastewate r i n th e sam e ro wa s th e collectio n unit s an d treatmen t system s i n us e a t th e facility . Us e th e sam e code s a s i n footnot e a o f Tabl e 4 , o r you r own description . c ) Ente r th e tota l numbe r o f eac htyp e o f collectio n uni t and treatmen t syste m fo r eac hwastewate r source . d ) Auni t shoul d b e considere d covered i f i t ha s emissio n suppressio n device s i n place . e ) Fo r eac hcollectio n uni t o r treatmen t systemvente d t o a contro l device , lis t th e devic e an d fil l ou t th e applicabl e sectio n o f Tabl e 8 . Us e th e sam e contro l devic e code s a s i n footnot e g o f Tabl e 2: f ) Provid e the name(s ) an d othe r informatio n fo r anyadditiona l wastewate r collectio n unit(s ) presen t a t th e facility . g ) Provid e th e name(s ) an d othe r informatio n fo r anyadditiona l wastewate r treatmen t approach(es ) use d a t th e facility .



# V\

### 1 9 TABL E 6 . NON-AQUEOU S WAST E COLLECTIO NAN D CONTROL(a )

Typeo f Wast e (b ) Wast

eGeneratio

n Rat e (Tons/Yr ) (c ) Wast

eCollected in ; Closed System ? (Yes/No ) (d) . Metho d o f On Sit eStorag e (e ) Wast

eTreate d or Disposed o f

OnSite ? (Yes/No ) (f ) Method o f OnSit eTreatemen

t orDisposal (g ) Contro

l Device o nTreatmen

tor Disposa l Unit (h )

^ ^

u hoP.2 2

2 0 TABL E 6 . NON-AQUEOU S WAST E COLLECTIO NAN D CONTRO L (Continued )

a ) Non-aqueou s wast e i s considere d t o contai n betwee n 1 0 an d 9 0 percen t solids . b ) Selec t th e wast e cod e tha t bes t describe s th e non-aqueou s wast e type : A P = oil-wate r separato r sludg e B l = biotreatmen t sludg e H C = contaminate d soi l O T = oil ytras han d debri s S O = slo p oi l emulsion s S S = sump/sewe r clean-ou t sludg e B = tan k bottom s Z Z = other , pleas e specif y(us e extr a sheet , i f necessary) . c ) Lis t th e annua l non-aqueou s wast e generatio n rat e i n ton s pe r year . d ) Identif y(Ye s o r No ) whethe r th e wast e i s collecte d i n a close d vapo r collectio n system . Aclose d syste mha s equipmen t t o preven t o r minimiz e wast e contac t wit hth e atmosphere , suc has : vapo r recover y systems , enclose d pipes , o r collectio n unit s wit hcovers . e ) Selec t th e storag e cod e tha t bes t describe s th e metho d b ywhic hnon aqueou s wast e i s store d on-sit e prio r t o treatmen t o r disposal : A A= ope n tank s B B = fixe d roo f tank s C C = floatin g roo f tank s D D = seale d DO T container s (5 5 gallo n drums , 11 0 gallo n bins ,

etc. ) E E = ope n roll-of f boxe s F F = covere d roll-of f boxe s G G = ope n pond s H H = covere d pond s I I = ope n pil e J J = covere d pil e KK = other , pleas e specif y(us e extr a sheet , i f necessary) . f ) Identif ywhethe r wast e i s treate d o r dispose d o f On-Sit e (Yes ) o r transporte d Off-Sit e fo r treatmen t and/o r disposa l withi n 9 0 day s o f generatio n (No) . 

# 0 \P.2 3

2 1 TABL E 6 . NON-AQUEOU S WAST E COLLECTIO NAN D CONTRO L (Concluded )

g ) I f wast e i s treate d o r dispose d o f On-Site , selec t th e treatmen t and/o r disposa l code(s ) tha t bes t describe(s ) ho wth e wast e i s manage d (i f mor e tha n on e cod e i s applicable , separat e multipl e code s wit ha comma ) : L F = lan

d buria l L T = lan

d treatment/farmin g D W= dewaterin g S T = solidification/stabilizatio n B l » biotreatmen t I N= incineration/therma l destructio n R E = recycle d 0 = other , pleas e specif y(us e extr a sheet , i f necessary) . h ) Us e th e same contro l devic e code s a s i n footnot e g o f Tabl e 2 .



# Z ^

### 2 2 TABL E 7 . EQUIPMEN T LEAK CONTRO L DAT A

Lea k Definition(a )

Equipmen t Componen

t HA

P Equipmen t Service (b ) Tota l

Equipmen t Coun t Equipmen

t Coun ti n LDA R Progra m Lea

k Repai r Response Time (c ) LDA

R Monitorin g Frequenc y (Times/Yr ) Equipmen

tCount s wit h Mechanica

l Contro l Device s (d ) Equipmen t Count s wit h aClosed Ven t System(e) Closed Vent

SystemContro

l Devic e 

### ( 0 Valves 

### S> 

# s

Compressor

s

Flange s2 3 TABL E 7 . EQUIPMEN T LEA K CONTRO L DAT A(Continued )

Equipment Component HAP Equipment Servic e (b ) Tota l

Equipment Count Equipmen t

Coun ti n LDA R Program Leak

Repai r Respons e Tim e (c ) LDA R

Monitorin g Frequenc y (Times/Yr ) EquipmentCounts

with Mechanical Control Device s (d ) Equipmen t

Count s with aClose d Ven t System(e ) Close d Ven t Syste mContro l Devic e 

### ( 0 Open-ende d line s

Samplin g connection s

Pressur erelie f valve sP.2 6

2 4 TABL E 7 . EQUIPMEN T LEA K CONTRO L DAT A(Concluded )

a ) Th e VO C concentratio n leve l (ppmv ) a t whic hequipmen t component s ar e considere d t o b e leakin g i n th e facility' s lea k detectio n an d repai r (LDAR ) program(i f applicable ) . Ente r "VISUAL " i f yo u hav e a visua l lea k inspectio n program . Ente r "NONE " i f yo u d o no t hav e a forma l lea k program . b ) Selec t th e equipmen t servic e definitio n tha t bes t describe s th e physica l stat e o f liquid s a t operatin g conditions : Ga s = proces s fluids , containin g HAP s i n a gaseou s stat e a t

operatin g condition s L L = proces s fluid s containin g HAP s i n a liqui d stat e a t

operatin g condition s wit ha vapo r pressur e greate r tha n kerosen e (0.0 4 psi a a t 6 8 degree s F ) H L = proces s fluid s containin g HAP s i n a liqui d stat e a t

operatin g condition s wit ha vapo r pressur e les s tha n kerosene . c ) Indicate s th e averag e repai r respons e tim e (i n days ) onc e a lea k ha s bee n discovered . d ) Provid e equipmen t count s fo r equipmen t wit hmechanica l contro l device s suc has : sealles s valves , pump s wit hdua l mechanica l seal s an d a barrie r fluid , compressor s wit hmechanica l seal s and a barrie r fluid , open-ende d line s wit hcaps/plugs/blind flanges , and pressur e relie f valve s wit hruptur e disks . e ) Provid e equipmen t count s fo r equipmen t wit ha vapo r collectio n an d recover y(close d vent ) system . f ) Us e th e same contro l devic e code s a s i n footnot e g o f Tabl e 2 .

• ^P.2 7



### 2 5 TABL E 8 . AI R POLLUTIONCONTRO L EQUIPMENT PARAMETER S (a ) Contro l Device : Scrubber Identifie rCode : Typ eo f scrubber , ventur i packe d be d impineemen t othe r(specify ) Gas inle ttemperature , * F Pressuredrop , i nH„ 0

r2 " " "" ~ '"

3 Liquid-to-ga s ratio , gal/1 0 acfin Inle tscrubbin gliquo r

D H percen tsolid s tvp eo f alkal i added , i f

any rat e(lbs/gal ) Wastewate rgeneratio nrate , gal/mi n HA Pcompositio no f

wastewater , mg/

t 

### Emissio nSource s (b )



### TsloP.2 8



### 2 6 TABL E 8 . AI R POLLUTIO NCONTRO L EQUIPMENT PARAMETERS(a ) (Continued ) Contro l Device : Incinerato r Identifie rCode : Type : therma

l catalytic Combustionchambe

r temperature , ° F (pleas enot

eif temperatur

emeasuremen

t i s not i nchamber ) Exces s air
. % Nominal residenc etime , s Hea t recovery : recuperative , percent

hea t recover y regenerative, percent

hea t recover y Emissio nSource s (b )

Contro l Device : Flar e Identifie rCode : . Type : n o assis t stea massis t air assist pressur eassis t Location : ground elevated Hea t conten t of ventedstream , Btu/sc f Flarega s exit

velocity , ft/s Flar eti p diameter, in
. Flar eheight , ft Supplementar

y fue l for : pilot , scf m combustionpurposes , scf

m Stea mrequirement , lb/h

r Emissio nSource s (b )



# sP.2 9

2 7 TABL E 8 . AI R POLLUTIONCONTRO L EQUIPMENT PARAMETER S (a ) (Concluded ) Control Device : CarbonAdsorbe r IdentifierCode : Typ eo f carbonbe d and number, fixe d fluidize d Ho wman ypound s o f

carbonperbe d

_ Configuration : parallel serial Numbe ro f

bed s on-lin e Numbe ro f

bed s desorbin g Pressuredrop , in . IC O Gas inle ttemperature , ° F

_ Typ eo f regeneratio n Regeneratio ntim e Adsorptio ntim e Emissio n Source s (b )

Control Device : Condenser Identifie rCode : Typ eo f condenser , surfac e contac tTi

f contact, se escrubber] Ga s inle ttemperature , ° F Ga s outle ttemperature , ° F Emissio nSource s (b )

a ) Aseparat e tabl e shoul d b e fille d ou t (afte r makin g copie s o f th e blan k table ) fo r eac hindividua l scrubber , incinerator , flare , carbo n adsorber , o r condense r a t th e facility . Fo r othe r type s o f contro l device , provid e th e mos t importan t parameter s o f operatio n o n a separat e sheet . b ) Lis t specifi c storag e tanks , loading racks/arms , and wastewate r an d non-aqueou s wast e treatmen t o r disposa l processes , usin g I D code s an d name s from

Table s 2 , 3 , 5 , and 6 .



# iV