### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.EIA

Facility Code Facility Name Boiler ID Fuel Type 1

113 Cholla 3 bitum inousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte

113 Cholla 3 As Received Higher Heating Value 113 Cholla 3 As Received % Moisture 113 Cholla 3 As Received % Ash 113 Cholla 3 As Received % Sulfur 113 Cholla 3 Dry basis Higher Heating Value 113 Cholla 3 Dry basis % Ash 113 Cholla 3 Dry basis % Sulfur 113 Cholla 3 Dry basis Antim ony 113 Cholla 3 Dry basis Arsenic 113 Cholla 3 Dry basis Beryllium 113 Cholla 3 Dry basis Cadmium 113 Cholla 3 Dry basis Chlorine 113 Cholla 3 Dry basis Chromium 113 Cholla 3 Dry basis Cobalt 113 Cholla 3 Dry basis Fluorine 113 Cholla 3 Dry basis Lead 113 Cholla 3 Dry basis Manganese 113 Cholla 3 Dry basis Mercury 113 Cholla 3 Dry basis Nickel 113 Cholla 3 Dry basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) ASTM D5865 ASTM D3302 ASTM D3174/5142 ASTM D4239 ASTM D5865 ASTM D3174/5142 ASTM D4239 ASTM D6357 ASTM D6357 ASTM D6357 ASTM D6357 ASTM D6721 ASTM D6357 ASTM D6357 ASTM D3761 ASTM D6357 ASTM D6357 ASTM D6722 ASTM D6357 SW 7740EIA Facility Code Facility Name Boiler ID HAPs Test Group 113 Cholla 3 Mercury and non-mercury

metalic HAPs

Fuel Testing Results

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop

Date (MM/DD/YY YY) Higher

Heating Value (HHV) (as received) HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) LRMJCC10011 4/20/2010 4/20/2010 9215 Btu/lb 13.72 19.19 1.14 10680 ESMJCC10069 4/21/2010 4/22/2010 9403 Btu/lb 17.48 13.09 1.19 11395 ESMJCC10070 4/23/2010 4/23/2010 9225 Btu/lb 18.58 14.25 1.09 11330HHV Units % Moisture (Dry Basis) % A

sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic

(Dry Basis) Arsenic

Units Beryllium (Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Btu/lb 22.24 1.32 [<10] ug/g 0.16 μg/g [<2] μg/g 8 μg/g 1.2 μg/g [<0.4] Btu/lb 15.87 1.44 15 μg/g 0.15 μg/g [<2] μg/g 6 μg/g 1.2 μg/g [<0.4] Btu/lb 17.51 1.34 [<10] μg/g 0.14 μg/g [<2] μg/g 6 μg/g 0.6 μg/g [<0.4]Cadmium

Units Chromiu

m (Dry Basis) Chromiu

m Units Lead (Dry

Basis) Lead

Units Manganese (Dry Basis) Manganese

Units Nickel

(Dry Basis) Nickel

Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt

(Dry Basis) Cobalt

Units μg/g 11 μg/g 11 μg/g 83 μg/g 6 μg/g 2 μg/g 68 ug/g 3 μg/g μg/g 8 μg/g 6 μg/g 37 μg/g 4 μg/g 2 μg/g 62 μg/g [<2] μg/g μg/g 9 μg/g 8 μg/g 32 μg/g 4 μg/g 2 μg/g 69 μg/g [<2] μg/gEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 113 Cholla 3 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop

Date (MM/DD/YY YY) Higher

Heating Value (HHV) (as received) HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) LRMJCC10011 4/20/2010 4/20/2010 9215 Btu/lb 13.72 19.19 1.14 10680 ESMJCC10069 4/21/2010 4/22/2010 9403 Btu/lb 17.48 13.09 1.19 11395 ESMJCC10070 4/23/2010 4/23/2010 9225 Btu/lb 18.58 14.25 1.09 11330 Fuel Testing ResultsHHV Units % Moisture (Dry Basis) % A

sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic

(Dry Basis) Arsenic

Units Btu/lb 22.24 1.32 [<10] ug/g 0.16 μg/g [<2] μg/g 8 μg/g Btu/lb 15.87 1.44 15 μg/g 0.15 μg/g [<2] μg/g 6 μg/g Btu/lb 17.51 1.34 [<10] μg/g 0.14 μg/g [<2] μg/g 6 μg/gBeryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromiu

m (Dry Basis) Chromiu

m Units Lead (Dry

Basis) Lead

Units Manganese (Dry Basis) Manganese

Units Nickel

(Dry Basis) 1.2 μg/g [<0.4] μg/g 11 μg/g 11 μg/g 83 μg/g 6 1.2 μg/g [<0.4] μg/g 8 μg/g 6 μg/g 37 μg/g 4 0.6 μg/g [<0.4] μg/g 9 μg/g 8 μg/g 32 μg/g 4Nickel

Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt

(Dry Basis) Cobalt

Units μg/g 2 μg/g 68 ug/g 3 μg/g μg/g 2 μg/g 62 μg/g [<2] μg/g μg/g 2 μg/g 69 μg/g [<2] μg/gUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg /g petroleum coke μg/g other mg /KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm ug/g