United States Environmental Protection Agency, Region 4 

 

Report 

Katrina Response 

Environmental Soil and Sediment Sampling 

Gulf Coast of Mississippi 

October, 2005 

 Science and Ecosystem Support Division 

980 College Station Road 

Athens, GA 30605 

Mississippi Department of Environmental Quality 

2380 Highway 80 West 

Jackson, Mississippi 39204

iii

Executive Summary

On August 29, 2005, Hurricane Katrina made landfall along the Gulf coast of the 

southeastern United States, causing unprecedented damage from eastern Louisiana to 

near Mobile, Alabama, due to the high winds and storm surge. During the week of 

October 3, 2005, the USEPA Region 4, Science and Ecosystem Support Division (SESD) 

collected soil and sediment samples near facilities in the affected areas in Mississippi to 

determine if flooding from the storm surge released hazardous constituents and materials. 

The facilities being investigated were located in the storm surge impacted portions of 

Hancock, Harrison and Jackson Counties in Mississippi. This investigation was 

requested by the Mississippi Department of Environmental Quality (MDEQ) and the 

USEPA, Region 4, Waste Management Division. 

The locations of these sites are shown and identified in Figure 1 (Appendix A), 

while Figures 2 through 7 show the facilities. Sample locations are shown in Figures 8

through 13, also included in Appendix A. The analytical data are presented in Section 6

and Appendix B of this report. 

 The analytical data presented in Section 6 and Appendix B of this report, was 

evaluated by the Region 4 Waste Management Division, Technical Services Section 

(TSS) to determine if there were any observable or attributable Post-Katrina impacts at 

the investigated sites. Technical Services Section staff reviewed the data presented in 

Section 6 and Appendix B. Evaluating the sampling data to determine if there was an 

off-site impact from Hurricane Katrina posed a challenge, due to the scarcity of preexisting sampling data and supporting information that could be used for data 

interpretation. 

EPA’s conclusions regarding the potential impact of the hurricane on these sites 

are based on a comparison of post-hurricane data to available past sample data collected 

during any facility investigations or routine monitoring activities. In addition, the results 

were compared to EPA Region 9 Preliminary Remediation Goals (PRGs) to determine if 

conditions at the sites might represent previously unrecognized risks to human health and 

the environment. EPA Region 9 PRGs (available at: 

http://www.epa.gov/region9/waste/sfund/prg/index.html) are conservative risk-based 

concentrations based on long-term exposures in either a residential or 

commercial/industrial setting. They are considered by EPA to be protective for people 

(including sensitive groups) over a lifetime. The PRGs are not clean up standards, but 

used to assist EPA scientists and others in initial screening-level evaluations of 

environmental measurements. The impact evaluations are presented in Section 7 of this 

report. 

The scope of the investigations at each site and the conclusions that were reached 

regarding releases or impacts from Hurricane Katrina are presented in the following site 

summaries. For the Risk Management Plan (RMP), Toxic Release Inventory (TRI) and 

Tier II Emergency Planning and Community Right-to-Know Act (EPCRA) facilities, 

PRGs based on an industrial/commercial exposure situation were utilized, except in the 

case where samples were taken in the vicinity of residential development; in which case 
iv

residential PRG soil screening values were used. The impact evaluations are presented in 

Section 7 of this report. 

 The scope of the investigations at each site and the conclusions that were reached 

regarding releases or impacts from Hurricane Katrina are presented in the following site 

summaries: 

DuPont DeLisle - Pass Christian, Mississippi

Three surface soil and two sediment samples were collected at five locations. 

These samples were analyzed for volatile organic compounds (VOCs), semi-volatile 

organic compounds (SVOCs), pesticides/PCBs, and metals. Low levels of metals, VOCs, 

pesticides, and SVOCs were detected in samples. Samples were also collected for 

dioxins. The dioxin data will be released in an addendum to this report when it is 

available. No PCBs were reported. 

From a comparison with sampling conducted pre-hurricane Katrina there is no 

clear and consistent pattern of increased contamination levels that would clearly indicate 

a potential release in the area of the DuPont DeLisle facility due to the effects of 

Hurricane Katrina. None of the reported analytes exceeded risk-based soil screening 

benchmarks for an industrial exposure scenario, or residential PRGs in the vicinity of 

residential development northeast of the facility. 

Chevron Pascagoula, First Chemical, Mississippi Phosphates - Pascagoula, Mississippi

 

Three surface soil and seven sediment samples were collected at ten locations. 

These samples were analyzed for volatile organic compounds (VOCs), semi-volatile 

organic compounds (SVOCs), pesticides/PCBs, metals, and radionuclides (samples BC2 

and BC4 were collected as part of another investigation, no radionuclide analyses were 

performed on these samples). Several metals were detected, along with low 

concentrations of VOCs, pesticides, and SVOCs. No PCBs were reported in these 

samples. 

Several metals exceeded pre-hurricane concentrations, however these elevated 

concentrations were detected in sediments in a ditch that is part of a solid waste 

management unit on site property that was previously known to contain elevated metals 

concentrations and were the site of previous industrial activity. EPA believes the 

exceedances are not significant enough to clearly indicate an impact due to hurricane 

Katrina in light of the likelihood of pre-existing metals contamination in surficial soil and 

drainage ditch sediments. Maximum detected levels of the metals arsenic and chromium 

exceeded PRGs, however were within a risk-range considered acceptable by EPA in 

other regulatory contexts. It is unlikely that frequent and prolonged human contact with 

sediments under water in drainage ditches would occur. There does not appear to be an 

indication of a potential release in the area of the facilities due to the effects of Hurricane 

Katrina. 
v

Omega Protein - Moss Point, Mississippi

Three sediment samples were collected at three locations. These samples were 

analyzed for volatile organic compounds (VOCs), semi-volatile organic compounds 

(SVOCs), pesticides/PCBs, and metals. Low concentrations of several metals were 

detected, along with several reported low concentrations of SVOCs. One PCB was 

reported. No VOCs were reported. 

There is no indication of a potential release in the area of the Omega Protein facility due 

to the effects of Hurricane Katrina. None of the reported analytes exceeded human health 

benchmarks for exposed to contaminants in soil or sediment under a 

commercial/industrial scenario. 

Port Bienville Industrial Park (Polychemie, Inc.) - Pearlington, Mississippi

Two surface soil and three sediment samples were collected at five locations. 

These samples were analyzed for volatile organic compounds (VOCs), semi-volatile 

organic compounds (SVOCs), pesticides/PCBs, and metals. Low levels of several metals 

were detected, along with low levels of ten SVOCs, along with a few VOCs, and 

pesticides. No PCBs were reported for these samples. 

Arsenic and benzo(a)pyrene exceeded PRGs but fell within a risk range of 1 in 

1,000,000 to 1 in 10,000 risk over background of an individual developing cancer over a 

lifetime from long-term exposure to those concentrations, which EPA has found 

acceptable in other regulatory and remedial contexts. None of the remaining analytes 

detected in soil or sediment exceeded industrial PRG soil screening levels. There is no 

indication of a potential release in the area of the Polychemie, Inc. facility, due to the 

effects of Hurricane Katrina. 

Ershigs Fiberglass, Inc. - Biloxi, Mississippi

Three surface soil and two sediment samples were collected at five locations. 

These samples were analyzed for volatile organic compounds (VOCs), semi-volatile 

organic compounds (SVOCs), pesticides/PCBs, and metals. Low concentrations of 

several pesticides and SVOCs were reported. No VOCs or PCBs were reported. 

Arsenic exceeded residential PRGs, however all detections were within a risk 

range of 1 in 1,000,000 to 1 in 10,000 risk over background of an individual developing 

cancer over a lifetime from long-term exposure to those concentrations, which EPA has 

found acceptable in other regulatory and remedial contexts. None of the other analytes 

exceeded residential PRG soil screening values. There does not appear to be indication of 

a potential release in the area of Ershigs Fiberglass due to the effects of Hurricane 

Katrina. 
vi

Naval Construction Battalion Center - Gulfport, Mississippi

Five sediment samples were collected from the wetland north of this installation. 

These samples were analyzed for dioxins only. At the request of MDEQ, an additional 

four sediment samples were collected in November by SESD personnel from an outfall 

that may have been contaminated from a pre-Katrina event. These samples were 

analyzed for PCBs only. This data will be released in an addendum to this report when it 

becomes available. 
vii

Acronyms 

AOC Area of Concern 

ASBLOQAM Analytical Support Branch Laboratory Operations and Quality 

Assurance Manual 

bgs below ground surface 

CERCLA Comprehensive Environmental Response, Compensation, and 

Liability Act 

CLP Contract Laboratory Program 

DAP diammonium phosphate 

DQO Data Quality Objectives 

EAB Ecological Assessment Branch 

EI Environmental Indicator 

EISOPQAM Environmental Investigations Standard Operating Procedures and 

Quality Assurance Manual 

EPCRA Emergency Planning and Community Right-to-Know Act 

ESAT Environmental Services Assistance Team 

FCC First Chemical Corporation 

GPRA Government Performance and Results Act 

GPS Global Positioning System 

HSO Health and Safety Officer 

HSWA Hazardous and Solid Waste Amendments 

IDW Investigation Derived Waste 

MDEQ Mississippi Department of Environmental Quality 

MSDS Material Safety Data Sheet 

MS/MSD Matrix Spike/Matrix Spike Duplicate 

NAREL National Air and Radiation Environmental Laboratory 

NCBC Naval Construction Battalion Center 

OSC On-Scene Coordinator 

OSWER Office of Solid Waste and Emergency Response 

PCBs Polychlorinated Biphenyls 

POTW Publicly-Owned Treatment Works 

QAPP Quality Assurance Project Plan 

QA/QC Quality Assurance/Quality Control 

RCRA Resource Conservation and Recovery Act 

RALs removal action levels 

RFA RCRA Facility Assessment 

RFI RCRA Facility Investigation 

RMP Risk Management Plan 

SESD Science and Ecosystem Support Division 

SOW Statement Of Work 

SVOC Semi-Volatile Organic Compound 

SWMU Solid Waste Management Unit 

TCL/TAL Target Compound List/Target Analyte List 

TIC Tentatively Identified Compound 

UIC Underground Injection Control 

USAF United States Air Force 

USEPA United States Environmental Protection Agency 

VOC Volatile Organic Compound 
viii

Table of Contents

Title and Approval Sheet.............................................................................................. ii 

Executive Summary..................................................................................................... iii 

Acronyms .................................................................................................................... vii 

1.0 INTRODUCTION............................................................................................. 1 

1.1 Report Outline ....................................................................................... 1 

1.2 Background/Site Locations.................................................................... 2 

1.3 Site Histories/Status Post Katrina......................................................... 2 

2.0 SAMPLING/DATA QUALITY OBJECTIVES............................................... 8 

2.1 Data Quality Objectives......................................................................... 8 

2.1.1 Problem Statement..................................................................... 8 

2.1.2 Identify the Decision................................................................... 8 

2.1.3 Decision Inputs........................................................................... 9 

2.1.4 Study Boundaries....................................................................... 9 

2.1.5 Decision Rule ............................................................................ 10 

2.1.6 Error Limits ............................................................................. 10 

2.1.7 Optimize Sampling Design....................................................... 10 

3.0 INVESTIGATION MANAGEMENT PLAN................................................. 13 

3.1 Field Project Responsibilities.............................................................. 13 

3.2 Site Control and Access....................................................................... 13 

3.3 Sample Collection and Handling Procedures..................................... 13 

3.4 Sample Analysis and Validation.......................................................... 14 

3.5 Chain of Custody ................................................................................. 14 

3.5.1 Sample Labels........................................................................... 15 

3.5.2 Sample Custody Seals .............................................................. 15 

3.5.3 Chain-of-Custody Record ........................................................ 15 

3.6 Station and Sample Identification....................................................... 15 

3.7 Site Mapping........................................................................................ 16 

3.8 Investigation Derived Waste (IDW).................................................... 16 

3.9 Sample Containers............................................................................... 16 

3.10 Investigation Schedule ......................................................................... 16 

4.0 SAMPLING DESIGN AND RATIONALE.................................................... 17 

4.1 Sampling Design .................................................................................. 17 

4.2 Data Validation/Usability .................................................................... 17 

4.3 Data Management/Document Control................................................ 17 

5.0 QUALITY ASSURANCE ............................................................................... 18 

5.1 Organization and Responsibilities....................................................... 18 

5.2 Field QA/QC Samples.......................................................................... 18 

5.2.1 Matrix Spike/Matrix Spike Duplicate ..................................... 18 

5.2.2 Population Variability - Duplicate Samples............................ 18 

5.2.3 Sample Handling - On-Site Splits............................................ 18 

5.2.4 Trip Blanks............................................................................... 19 
ix

6.0 INVESTIGATION RESULTS........................................................................ 20 

6.1 DuPont - DeLisle.................................................................................. 20 

6.2 Chevron – Pascagoula, First Chemical, Mississippi Phosphates ....... 21 

6.3 Omega Protein ..................................................................................... 21 

6.4 Port Bienville Industrial Park (Polychemie, Inc.) .............................. 21 

6.5 Ershigs Fiberglass, Inc......................................................................... 21 

6.6 Naval Construction Battalion Center.................................................. 22 

7.0 IMPACT EVALUATION............................................................................... 23 

7.1 DuPont DeLisle - Pass Christian, Mississippi..................................... 24 

7.1.1 Results....................................................................................... 24 

7.1.2 Discussion ................................................................................. 24 

7.1.3 Conclusion ................................................................................ 25 

7.2 Chevron Pascagoula, First Chemical, Mississippi Phosphate - 

Pascagoula, Mississippi........................................................................ 25 

7.2.1 Results....................................................................................... 25 

7.2.2 Discussion ................................................................................. 26 

7.2.3 Conclusion ................................................................................ 27 

7.3 Omega Protein - Moss Point, Mississippi............................................ 28 

7.3.1 Results....................................................................................... 28 

7.3.2 Discussion ................................................................................. 28 

7.3.3 Conclusion ................................................................................ 28 

7.4 Port Bienville Industrial Park (Polychemie, Inc.) - Pearlington, 

Mississippi............................................................................................ 28 

7.4.1 Results....................................................................................... 28 

7.4.2 Discussion ................................................................................. 29 

7.4.3 Conclusion ................................................................................ 29 

7.5 Ershigs Fiberglass - Biloxi, Mississippi............................................... 30 

7.5.1 Results....................................................................................... 30 

7.5.2 Discussion ................................................................................. 30 

7.5.3 Conclusion ................................................................................ 30 

7.6 Naval Construction Battalion Center - Gulfport, Mississsippi .......... 31 

8.0 REFERENCES................................................................................................ 32 

Appendix A ................................................................................................................. 33 

Appendix B.................................................................................................................. 48 

Appendix C ................................................................................................................. 86 
1

1.0 INTRODUCTION

On August 29, 2005, Hurricane Katrina made landfall along the Gulf coast of the 

southeastern United States, causing unprecedented damage from eastern Louisiana to 

near Mobile, Alabama, due to the high winds and storm surge. During the week of 

October 3, 2005, the USEPA Region 4, Science and Ecosystem Support Division (SESD) 

collected soil and sediment samples near facilities in the affected areas in Mississippi to 

determine if flooding from the storm surge released hazardous constituents and materials. 

The facilities being investigated are located in the storm surge impacted portions of 

Hancock, Harrison and Jackson Counties in Mississippi. This investigation was 

requested by the Mississippi Department of Environmental Quality (MDEQ) and the 

USEPA, Region 4, Waste Management Division. 

The Quality Assurance Project Plan Katrina Response Environmental Soil and 

Sediment Sampling Gulf Coast of Mississippi (QAPP, 2005) for the collection of 

environmental samples in the three county Gulf coastal area of Mississippi was 

developed by the United States Environmental Protection Agency (US-EPA), Region 4, 

in accordance with the EPA Guidance for Quality Assurance Project Plans (EPA QA/G5, 1998). The QAPP underwent external peer review by the Science Advisory Board, 

whose comments were incorporated. 

Soil and sediment samples were collected from RMP (Risk Management Plan), 

Tier II, and TRI (Toxic Release Inventory) facilities in the three counties. In addition, 

one facility, Naval Construction Battalion Center (NCBC) Gulfport, was selected because 

the recent flooding may have re-contaminated a partially remediated site. All samples 

were analyzed for metals (including mercury), volatile organic compounds and semivolatile organic compounds, including pesticides/PCBs (polychlorinated biphenyls), with 

the exception of one site (NCBC Gulfport) where some samples were analyzed for 

dioxins only, and others were analyzed for PCBs only. At the DuPont DeLisle facility, 

samples were also analyzed for dioxin, in addition to the parameters listed above. 

Samples from the Chevron Refinery – Pascagoula, First Chemical, and MS Phosphates 

complex were analyzed using gamma spectroscopy in addition to the parameters listed 

above. Split samples were offered to each facility. 

Where knowledge of site specific analytes was available (such as the NCBC and 

DuPont DeLisle), the analyte list was tailored for that situation. The analytical results 

were evaluated to determine if these constituents are present in soils and sediments 

adjacent to the facilities, indicating a possible release to the environment, which could 

lead to a more thorough assessment. 

1.1 Report Outline 

Section 1 provides the introduction to the report and a brief summary of the sites 

investigated. Section 2 provides the sampling data quality objectives used to develop the 

Quality Assurance Project Plan (QAPP) for the investigation. Section 3 is the 

investigation management plan detailing the field procedures used during the study. 

Section 4 is the sampling design and rationale, including data validation procedures. 
2

Section 5 presents QA/QC procedures used during the investigation. Section 6 is a 

summary of the sample data. Section 7 presents the results of the decision matrix used to 

evaluate the sampling results. Section 8 is references. Appendix A contains the figures 

referenced in the report. Appendix B contains data summary tables. Appendix C

contains the laboratory data sheets. 

1.2 Background/Site Locations

Figure 1 (Appendix A) is an area map indicating the general locations of the 

facilities investigated. Maps were also prepared showing the locations of the facilities 

and the proposed sampling locations. See Figures 2 - 7 in Appendix A. 

1.3 Site Histories/Status Post Katrina 

These facilities were selected by the Waste Management Division because they 

are located in areas of significant widespread damage, and are RMP, Tier II, or TRI 

facilities. All have reported damage from the effects of Katrina. One additional facility 

(NCBC) was included to assess the possibility of re-contamination of a wetland due to 

the flooding. It should be noted that these facilities may be covered by more than one of 

these definitions. 

Risk Management Plan (RMP) Facilities:

 Initial reports from these facilities indicated no visible releases of hazardous 

constituents beyond their perimeters. However, due to the large amounts of chemicals 

used and/or manufactured by these facilities, an off-site examination was deemed 

necessary. The following information was obtained from the South Programs Section, 

RCRA Programs Branch. 

DuPont DeLisle - Pass Christian 

 The DuPont-DeLisle plant is a titanium dioxide manufacturing operation located 

on Bay St. Louis, in the community of Pass Christian, Mississippi. The DuPont DeLisle 

facility operates two identical production lines. Line 1 began production in September 

1979, Line 2 production began in October of 1991. DuPont utilizes the Chloride 

Ilmenite process to extract titanium from ore. A hazardous waste generated on site is a 

mixture of ferrous and ferric chloride. This waste is characteristic for lead, chromium, 

and is also considered corrosive. DuPont performs deep well injection onsite through a 

Underground Injection Control (UIC) permit. 

 DuPont DeLisle has an operating RCRA Permit for onsite treatment and storage 

units. The annual quantity of D002/D007/D008 wastes for tank treatment, storage and 

UIC is listed as 1,500,000 tons per year. On April 13, 2005, DuPont submitted a Class 1 

modification package for the RCRA Part B, which proposed the addition of two splitter 

tanks which would improve the handling of the corrosive waste streams. The modified 

permit was issued August 10, 2005, and will expire on August 9, 2014. 
3

 Because MDEQ is not fully Hazardous and Solid Waste Amendment (HSWA) 

authorized, the DeLisle plant is under EPA authority for corrective action through the 

HSWA portion of the permit. 

 RCRA Facility Investigation (RFI) phase I and II have been conducted at the site, 

and an approved Corrective Action Groundwater Monitoring Plan is in place to monitor 

three areas (5 SWMUs) for arsenic, barium, beryllium, manganese, lead, cis-1,2 

dichloroethene, trans-1,2-dichloroethene, 1,1-dichloroethene, trichloroethene, 

tetrachloroethene (PCE) and vinyl chloride: 

Southeast Waste Management Area for Solid Waste Management Units 

(SWMUs) 14, 22 & 29; 

 West Waste Management Area for SWMUs 8 & 28; and 

 PCE Containment Sump downgradient. 

 The class of chemicals known as dioxins and furans (polychlorinated 

dibenzodioxins, and polychlorinated dibenzofurans, PCDD/PCDF) are present at the 

DuPont-DeLisle facility. 

 EPA received first communication from DuPont on September 7, 2005. Prior to 

that email communication, EPA was unable to establish phone or data contact with 

DuPont-DeLisle. EPA has had follow-up contact with the Environmental Office at 

DuPont-DeLisle on September 14, 2005. Much of the following information is derived 

from these exchanges. MDEQ visited the site two days after the Hurricane along with 

Florida Emergency Responders. The storm surged over the site's levee (~ 20 feet) and 

the site was under 7 to 9 feet of water. There is significant mud and sediment from Bay 

St. Louis spread across the site; DuPont reported that they did not believe there is any 

process material in the sediments. All plant process ditches, sumps and trenches were 

cleaned prior to the storm and all containment and structures faired well. DuPont has 

been in contact with MDEQ on Solid Waste issues. 

 There was nearly 100% retention in the Waste Management area; one small 

breech at WMU #11 of mostly storm water occurred; this was repaired. There have been 

no known leaks/releases to the air or water. 

Aerial imagery indicates a small area of housing immediately north of the facility. 

This facility is located in Figure 2. 

Chevron Refinery – Pascagoula 

The Pascagoula Refinery was built in the early 1960’s and went into operation in 

1963. The Facility is owned by Chevron U.S.A, Inc. and is operated by ChevronTexaco 

Products Company, a division of Chevron U.S.A., Inc. The Refinery property consists of 

approximately 3,000 acres. A total of 1,000 acres have been developed industrially. The 

refinery is ChevronTexaco’s largest with a refining capacity of 325,000 barrels per day. 

An expansion to 360,000 barrels per day was underway when Hurricane Katrina struck 

the facility. 
4

The facility is completely surrounded by a hurricane dike that has closable gates. 

The dike was not breeched, however, it was eroded in places and the facility was flooded. 

This caused a loss of power at the facility which has now been restored. Power was lost 

to the storm water pumping system and the wastewater treatment system [the units of the 

wastewater treatment system are HSWA SWMUs]. The wastewater treatment system 

was restarted about 10 days after the storm. The oil shipping terminal is back in 

operation, therefore, ChevronTexaco can distribute product which was stored in tanks or 

arrives by ship. The RCRA regulated units are at one of the highest points in the facility 

and were not flooded. The tank field was flooded, but there have been no observed 

releases inside the facility. 

The facility also had HSWA corrective action underway in August before the 

hurricane struck. A removal action at the Wharf Revetment Area in the shipping terminal 

was completed two days before the hurricane struck and the area was concreted over. 

First report is that the new, concrete revetment, [as opposed to sandbags] held up well in 

the storm, thus protecting the area that was excavated. Excavation of contaminated soil 

in the tank field was completed just before the storm struck and the Oily Dirt Pile SWMU 

80 was removed as well. A total of 38 roll off containers of removed soil were stored on 

the East Hill [near the regulated units], one of the highest areas in the facility, and were 

not affected by the storm surge. The HSWA corrective action scheduled at the North 

Canal [part of the storm water system] had not yet begun, and will have to be delayed. 

ChevronTexaco's large [140 acre, 200 million gallon] hurricane surge lagoon was 

overtopped [incoming] by the storm surge, but the dike held and there was no apparent 

release to the adjacent Grand Bay National Wildlife Refuge and the National Estuarine 

Research Reserve [NERR]. However, the large lagoon took on salt water from the surge, 

which may affect the freshwater wildlife in the lagoon. The lagoon has been 

characterized as an ‘attractive nuisance’ for wildlife and is the subject of an ongoing 

Ecological Risk Assessment. Overall, the flooding was not as bad at the facility as 

Hurricane George in 1998. 

No adjacent housing areas were located on the aerial imagery. This facility is 

located in Figure 3. 

First Chemical Corporation – Pascagoula

First Chemical Corporation (FCC) has operated since 1967, manufacturing 

numerous and sundry chemicals. A 1988 RFA identified approximately 30 SWMUs and 

Areas of Concern (AOCs). The recently completed RCRA Facility Assessment (RFA) 

expanded that number to greater than 65. FCC has conducted several investigations at 

the facility over the years, with the most recent study being completed in 2004. First 

Chemical was purchased in 2002 by DuPont, and it is operated as a wholly owned 

subsidiary. 

Shallow groundwater at the site (<15 ft bgs) has been impacted by various 

contaminants; predominantly aniline, benzene, nitrobenzene, and toluene. The primary 

sources of groundwater contamination are a former wastewater treatment pond (Pond 3) 

and associated former effluent ditch. Miscellaneous leaks and minor releases have also 
5

contributed. The facility has monitoring and recovery systems in place, and they are 

designing enhancements to the groundwater recovery system. The design should be 

completed in early 2006, with installation possibly completed within 2006. 

Hurricane Katrina Impacts

The facility did not suffer heavy damage, and there were no reported releases. 

Two tanks were damaged, but the contents are being transferred to temporary storage 

tanks. The facility will be out of operation for perhaps several weeks. A PubliclyOwned Treatment Works (POTW) to which the facility pipes its partially treated effluent 

was damaged, however, and it may be out of commission for “months”. The facility will 

require some means of disposing of its wastewater if the POTW is not online by the time 

FCC is ready to go live. 

No adjacent housing areas were located on the aerial imagery. This facility is 

located in Figure 3. 

Toxic Release Inventory (TRI) Facilities: 

 The following information is derived from the TRI website 

(http://www.epa.gov/tri/): The Toxics Release Inventory (TRI) is a publicly available 

EPA database that contains information on toxic chemical releases and other waste 

management activities reported annually by certain covered industry groups as well as 

federal facilities. This inventory was established under the Emergency Planning and 

Community Right-to-Know Act of 1986 (EPCRA) and expanded by the Pollution 

Prevention Act of 1990. 

 Information about these facilities is limited, but incidents are known to have 

occurred due to the effects of Hurricane Katrina. Region 4 On-Scene Coordinators 

(OSCs) have responded to incidents at the following facilities: 

 Omega Protein – Moss Point 

No adjacent housing areas were located on the aerial imagery. This facility is 

located in Figure 4. 

 Port Bienville Industrial Park (Polychemie, Inc.) – Pearlington 

 No adjacent housing areas were located on the aerial imagery. This facility is 

located in Figure 5. 

 Ershigs Fiberglass – Biloxi 

 Housing was noted to the northwest, west and south in the aerial imagery. This 

facility is located in Figure 6. 
6

Tier II Facility:

 The Emergency Planning and Community Right-to-Know Act of 1986 (EPCRA) 

has a requirement for facilities exceeding the EPCRA Chemicals and Reporting 

Thresholds specified in Sections 311/312 of the Act to submit a Tier II form. Tier II 

forms require basic facility identification information, employee contact information for 

both emergencies and non-emergencies, and information about chemicals stored or used 

at the facility: 

• The chemical name or the common name as indicated on the Material Safety Data 

Sheet (MSDS); 

• An estimate of the maximum amount of the chemical present at any time during 

the preceding calendar year and the average daily amount; 

• A brief description of the manner of storage of the chemical; 

• The location of the chemical at the facility; and 

• An indication of whether the owner of the facility elects to withhold location 

information from disclosure to the public. 

Mississippi Phosphates – Pascagoula 

Mississippi Phosphates Corporation is located at 601 Highway 611 Pascagoula, 

MS and employs approximately 220 people. More than 900,000 tons of diammonium 

phosphate (DAP) are produced at the complex each year. Nearly two-thirds of this 

product is exported, mainly to China and India. Mississippi Phosphates Corporation is a 

member of the Phosphate Chemical Export Association, Inc., (PhosChem) which handles 

the export sales of the company's DAP. Its deep-water port facility on the Gulf of 

Mexico allows Mississippi Phosphates to load ships for export directly from the plant 

site. MS Phosphates imports phosphate rock from the country of Morocco. 

Data from Region 4 OSCs indicates a leak of anhydrous ammonia from an above 

ground storage tank. This is a large facility that had the potential to release hazardous 

constituents beyond its’ operational perimeter. 

No adjacent housing areas were located on the aerial imagery. This facility is 

located in Figure 3. 

Naval Construction Battalion Center:

Naval Construction Battalion Center (NCBC) – Gulfport. NCBC Gulfport is 

located in the western part of the City of Gulfport, in Harrison County, Mississippi, 

approximately two miles north of the Gulf of Mexico. The off-base Area of Concern 

(AOC) is located immediately downgradient (north) of Outfall 3. 

The source area of dioxin contamination for the off-base AOC is the Herbicide 

Orange Storage Area, designated as Site 8, at NCBC Gulfport. Between 1968 and 1977, 

Site 8 was used by the United States Air Force (USAF) as a storage area for drums 

containing the herbicide Agent Orange, also known as Herbicide Orange, prior to being 

shipped to Vietnam. Occasional spills and drum ruptures occurred during storage and 
7

handling of the Herbicide Orange. Dioxin migration has occurred primarily through 

erosion of dioxin-contaminated soil and sediment from Site 8 and its transport 

downstream via ditches and canals to a small wetland area at Turkey Creek. This 

wetland was in the process of being cleaned up (80% completion) when Katrina occurred, 

and there is a possibility that flooding may re-contaminated the remediated area. 

Four sediment samples were collected by SESD in November from an outfall that 

may have been contaminated with PCBs prior to the Katrina event. 

Housing is located immediately adjacent to the wetland. This facility is located in 

Figure 7. 
8

2.0 SAMPLING/DATA QUALITY OBJECTIVES

2.1 Data Quality Objectives

The Data Quality Objectives (DQO) process for Superfund was used in 

developing the QAPP, in accordance with the Guidance for the DQO Process (EPA 

QA/G-4, 2000). DQOs are useful in identifying the study objectives and decisions to be 

made and the criteria by which the data will be assessed. These data are then used for 

decision making. 

DQOs were established prior to data collection and integrated with the project 

planning process so that sufficient data of known quality are collected to support sound 

decision making. DQOs are developed using an interactive approach to decision-making 

based on detailed EPA guidance. The steps are: 

• Problem statement 

• Identify the decisions 

• Identify the inputs into the decision 

• Define the boundaries of the study 

• Develop decision rules 

• Specify tolerable limits on decision errors 

• Optimize the design for obtaining data 

2.1.1 Problem Statement

The initial step in the DQO process is to define the problem so that the focus of 

the investigation will be clear. During the landfall of Hurricane Katrina, a massive storm 

surge flooded extensive portions of Hancock, Harrison and Jackson Counties in the Gulf 

Coast of Mississippi. Within this area are located many hazardous waste facilities. It 

was not known what effect, if any, the storm surge had on these facilities and the 

surrounding areas, with respect to release and dispersion of hazardous materials and 

chemicals, particularly to residential settings and sediment. The facilities selected for this 

investigation have had indications of a potential release to surrounding soils, or 

conditions prior to Katrina make a release to surrounding soils or sediment possible. The 

problem is identifying these potential releases to surrounding soils and sediments. It 

must be strongly emphasized that this investigation is not intended to provide a 

comprehensive assessment of potential releases beyond the operational perimeters of 

these facilities. Rather, it is intended to provide a first look at these areas post-Katrina. 

2.1.2 Identify the Decision

The purpose of this DQO step is to identify the decisions that must be supported 

with the collected data. This helped to define the objectives of the field investigation. 

The decision needed was to determine what areas of the Mississippi Gulf Coast, in 

immediate proximity to the hazardous waste facilities, may be the site of a potential 
9

release of hazardous materials to surrounding soils and\or sediments. SESD prepared this 

report detailing the results of the investigation to provide the supporting data for these 

decisions. 

2.1.3 Decision Inputs

This step is used to identify the information needed to support the decisions. The 

primary inputs needed to support the decisions are surface soil and sediment samples. 

Analytical results used in this decision making process were definitive laboratory data, 

obtained from analysis by a contract laboratory obtained through the EPA’s Contract 

Laboratory Program (CLP lab). All samples were analyzed for metals (including 

mercury), volatile organic compounds and semi-volatile organic compounds, including 

pesticides and PCBs, with the exception of samples from NCBC Gulfport where samples 

were analyzed for PCBs or dioxins only. Samples from the DuPont DeLisle facility were 

analyzed for dioxins in addition to these parameters. Samples from the Chevron Refinery 

– Pascagoula, First Chemical, and MS Phosphates complex were also analyzed using 

gamma spectroscopy in addition to the parameters listed above. 

Surface soil samples were composites comprised of soil from the 0” to 3” interval 

at each aliquot location. The sample for volatile organic compounds was collected from 

the centermost aliquot. Sediment samples were collected from ditches or other surface 

water conveyances as grab samples in the vicinity of each site to determine if releases 

occurred via these pathways. 

 

2.1.4 Study Boundaries

The purpose of this step is to identify the boundaries of the study. The media of 

interest was surface soils and sediments adjacent to the selected RMP, Tier II and TRI 

facilities, as well as the wetland north of NCBC Gulfport. The study boundaries are 

defined below. 

Study Area – The study area was the portions of Hancock, Harrison and Jackson 

counties flooded by the storm surge associated with Hurricane Katrina. Within the larger 

study area are the selected facilities. For each of the identified sites, the area to be 

investigated consisted of soils and/or sediments near the facility (but outside the 

perimeter), including ditches or storm water conveyances that were present. 

Sample Depth – Soil samples were collected from 0” to 3” below ground surface 

depth. Samples collected from ditches were from a similar interval. 

Temporal Boundaries –The field investigation was conducted the week of 

October 3, 2005. All efforts were made to obtain the quickest possible turnaround times 

on the analytical results (consistent with good laboratory practices) to expedite decision 

making. 
10

Physical Boundaries - No sampling was conducted beneath any concrete or 

asphalt paved areas or from under any structures. Also, no samples were collected in the 

immediate vicinity of any downed power lines or under any unstable structures that may 

have posed a collapse hazard to the sampling team. Several sample locations were 

moved varying distances from the original proposed locations due to on-site conditions 

(see Table 1 in Appendix B for a description and rationale of sample boundaries). 

 2.1.5 Decision Rule

The Technical Services Section in the Superfund Remedial and Technical 

Services Branch has prepared a decision matrix to be used in determining if a potential 

release has occurred (Appendix C). The results of this matrix evaluation are found in 

Section 7.0 of this report. 

2.1.6 Error Limits

Because of inherent variability introduced through sample collection, mixing, 

storage, transportation, and analysis, it is important to specify the acceptable decision 

error rates. Decision errors were reduced by using standard, published protocols for 

sampling and analytical procedures. Sampling protocols followed the Environmental 

Investigations Standard Operating Procedures and Quality Assurance Manual 

(EISOPQAM) while analytical procedures followed the current CLP Statement of Work 

(SOW), the regional SOW for dioxins, and the NAREL (National Air and Radiation 

Environmental Laboratory) GAM-01 for gamma spectroscopy. 

2.1.7 Optimize Sampling Design

The final step in the DQO process is the development of a sampling design that 

takes into account data needs, key decisions, and environmental variables, such as 

physical and site constraints, and how the spatial and temporal boundaries of the 

contamination and population at risk will be identified. The work plan, as included in the 

QAPP, was developed based on the integration of aerial imagery of the affected areas 

(pre-Katrina) and the EPA facility registry. Due to the time-critical nature of the 

investigation, a reconnaissance of each area was not practical or possible. As such, each 

sample team approached each site with generic protocols for sampling. As stated in 

Section 3.3, up to 5 samples were collected adjacent to each facility. Sediment samples 

were also collected from ditches or other conveyances that left the property. It must be 

noted that the proposed sample locations were selected using 1:24,000 topographic maps 

and quarter-quad digital orthographic quads. These maps were the most current 

available, but are still several years old. In addition, they may be inaccurate by as much 

as 20’ to 40’. 
11

Samples were collected on an authoritative basis, from areas deemed most likely 

to be impacted. Specifically, soils were sampled adjacent to facility perimeters and 

sediment samples from drainage pathways. Sampling locations are presented in Table 1 

of Appendix B. 

DuPont DeLisle, see Figure 8

Two grab sediment samples were collected from ditches draining the facility to 

St. Louis Bay. Three additional composite surface soil samples were collected between 

the facility and a residential area immediately north of the facility. 

Chevron Refinery – Pascagoula, First Chemical Corporation, and Mississippi 

Phosphates, see Figure 9

 Because these selected facilities are adjacent to each other, sampling occurred 

around these facilities as a unit. Grab sediment samples were collected from ditches 

draining to Bayou Cassotte, Bangs Lake, and the Gulf of Mexico. In addition, composite 

surface soil samples were collected north and south of the facility complex. Finally, this 

report includes data from two sediment sampling stations established in Bayou Cassotte 

by the Ecological Assessment Branch (EAB), Water Quality Studies of Bays in Coastal 

Mississippi (EPA 2005), the week prior to this investigation. 

Omega Protein, see Figure 10

 Three grab sediment samples were collected from the north bank of the 

Escatawpa River, two at the facility and one downgradient. No upland soil samples are 

proposed for this facility because Morton International (which was not listed for sampling 

in this effort) is immediately north. In addition, this report contains data from a sediment 

sampling station established by EAB the week prior to this investigation in the Escatawpa 

River downstream of Omega Protein. 

Port Bienville Industrial Park (Polychemie, Inc.), see Figure 11

Grab sediment samples were collected at the three indicated locations to 

determine if a potential release to the waterway occurred as the storm surge receded. 

Two composite surface soil samples were collected at the indicated locations to 

determine if contaminants may have moved further inland from the facility on the rising 

flood waters. 

Ershigs Fiberglass, see Figure 12

 Four composite surface soil samples were collected as shown, to determine if 

contaminants may have been deposited between the facility and nearby housing. An 

additional grab sediment sample was collected from a small inlet draining to Biloxi Bay. 
12

Naval Construction Battalion Center (NCBC) Gulfport, see Figure 13

 Five grab sediment samples were collected as shown, to determine if the wetland 

may have become re-contaminated during the storm surge. These samples were 

recollected by SESD in November due to problems with the sample analysis. At the 

same time four sediment samples were collected from an NCBC outfall that may have 

been contaminated with PCBs from an earlier, non-Katrina related incident. 
13

3.0 INVESTIGATION MANAGEMENT PLAN

3.1 Field Project Responsibilities

The overall field investigation/sampling phase of the project and any field 

decisions were the responsibility of the Field Project Leader who was responsible for the 

following field activities: 

• Ensure that all field activities were communicated and coordinated with the 

Project Leader. 

• Monitoring overall field project quality control. 

• Coordinating field scheduling of work with other Section and Division 

activities. 

• Overseeing and managing field technical resources including non-sampling 

field activities. 

The site Health and Safety Officer (HSO) was responsible for monitoring the 

health and safety of the sampling/investigative personnel. In addition to the Field Project 

Officer and HSO, five other staff persons were involved in the field operations for the 

investigation. All field investigators are required to have 40 hours of hazardous waste 

site safety training, and specific knowledge and expertise of sample collection and safety 

techniques in accordance with the Region 4 EPA Environmental Investigations Standard 

Operating Procedures and Quality Assurance Manual (EISOPQAM), November 2001. 

3.2 Site Control and Access

Access arrangements for RMP facilities were made by Lael Butler, Chief, South 

Programs Section, RCRA Programs Branch. Access arrangements for TRI and Tier II 

facilities were made by Fred Sloan. Access to the NCBC was arranged by Michelle 

Thornton. 

3.3 Sample Collection and Handling Procedures

All samples were collected, containerized, preserved, handled, and documented in 

accordance with the EISOPQAM. A copy of the manual, in addition to the site-specific 

Health and Safety Plan, was maintained by the field project leader for reference during all 

phases of the field sampling activities. 

The surface soil samples were collected as composite samples, with the number of 

aliquots and pattern determined by the site conditions, using stainless steel hand augers. 

The pattern size was appropriate to characterize the area in question. The central aliquot 

location for each sample was located using GPS to at least one meter accuracy. Each 

aliquot was comprised of the 0” to 3” below ground surface interval. All grass, roots and 

other vegetative material, as well as small rocks or stones, were removed from the sample 
14

matrix during sample mixing, prior to containerization. It should be noted that sediment 

deposited by the storm surge was present in the collected samples. 

Sediment samples were collected using stainless steel scoops, stainless steel 

spoons and/or stainless steel hand augers. 

Soil samples were collected as described in Section 2.1.7, using hand augers, 

spoons, or scoops as appropriate, and the aliquots were thoroughly mixed in glass pans. 

Samples for volatile organic compound analyses were collected prior to mixing with 

minimum disturbance from the central aliquot in Encore® sample containers using EPA 

Method 5035. After mixing, the samples were placed in the appropriate containers and 

placed on ice, as specified in Appendix A of the Region 4 EISOPQAM. 

3.4 Sample Analysis and Validation

All samples were analyzed for metals, volatiles, semi-volatiles, pesticides and 

PCBs, in accordance with the current Contract Laboratory Program Statement of Work, 

again with the exception of the NCBC Gulfport facility where samples were analyzed for 

dioxins or PCBs only. Samples from the DuPont DeLisle facility were analyzed for 

dioxins in addition to these parameters. Samples from the Chevron Refinery – 

Pascagoula, First Chemical, and MS Phosphates complex were also analyzed for 

Radium-226 and radionuclides using gamma spectroscopy in addition to the parameters 

listed above. 

By using sampling procedures as outlined in the Region 4 EISOPQAM errors 

introduced in the decision making process were minimized. 

3.5 Chain of Custody

All chain-of-custody and record keeping procedures were in accordance with the 

EISOPQAM. Chain-of-custody procedures are comprised of the following elements; 1) 

maintaining sample custody and 2) documentation of samples for evidence. 

As defined in the EISOPQAM, a sample or other physical evidence is in custody 

if: 

• it is in the actual possession of an investigator; 

• it is in the view of an investigator, after being in their physical possession; 

• it was in the physical possession of an investigator and then it was secured to 

prevent tampering; and/or 

• it is placed in a designated secure area. 
15

3.5.1 Sample Labels

Sample labels were prepared and affixed to each sample container sent to the CLP 

laboratory. The labels were prepared using waterproof, non-erasable ink as specified in 

Section 3 of the EISOPQAM. 

3.5.2 Sample Custody Seals

The samples were sealed as soon as possible following collection as specified in 

the EISOPQAM. The custody seal bears the date and the initials of the sample custodian 

at the time it was sealed. 

3.5.3 Chain-of-Custody Record

The field Chain-Of-Custody Record is used to record the custody of all samples 

sent to the laboratory. All of these samples were accompanied by a Chain-Of-Custody 

Record. The Chain-Of-Custody Record documents transfer of custody of samples from 

the sampler/sample custodian to another person, the laboratory, or other organizational 

elements. To simplify the Chain-of-Custody Record and eliminate potential litigation 

problems, as few people as possible should have custody of the samples or physical 

evidence during the investigation. 

The Chain-Of-Custody Record also serves as a sample logging mechanism for the 

laboratory sample custodian. A Chain-of-Custody Record was completed for all samples 

collected for this investigation. A separate Chain-of-Custody Record was used for each 

final destination or laboratory utilized during the investigation. 

For samples split with a facility, a Receipt for Sample form was completed and 

signed. 

3.6 Station and Sample Identification

Sample identification numbers were assigned using the following format: 

XXX##YYZ, where: 

XXX is an identifier for the RMP, Tier 2, TRI, or NCBC facility 

## indicates surface soil (SF) or sediment SD 

YY indicates the sample location number, i.e., 01 for the facility location 

Z identifies splits or duplicates: “S” is split; “D” is duplicate 

A split sample is a sample comprised of two samples, the primary sample and the 

designated split sample, that are collected from the same sample material that has been 

homogenized in a glass pan prior to filling of the sample containers. Assuming a well 

mixed sample, a split helps evaluate both the field and laboratory procedures. A 
16

duplicate sample is a co-located sample, usually collected less than six inches from the 

primary sample at a location and is collected to show variability of the matrix sampled. 

3.7 Site Mapping

The locations of all samples were logged using a GPS unit capable of one meter 

accuracy, as specified in Section 2.1.7. 

3.8 Investigation Derived Waste (IDW)

 The following identifies types of non-hazardous IDW that were generated during 

the investigation and their disposition: 

• Gloves, paper towels, and other miscellaneous trash generated during the 

investigation were bagged and placed in a dumpster for disposal at a Class D 

landfill. It is not anticipated that this material will constitute a significant 

threat to human health and the environment. 

3.9 Sample Containers

Sample containers were obtained from the SESD Field Equipment Center in 

Athens, Georgia. These containers complied with the requirements specified in 

Appendix A of the EISOPQAM. Table 2 (Appendix B) lists the container types and 

numbers used. 

 It should be noted that time constraints did not allow for the normal QA/QC 

checks for these pre-cleaned sample containers as specified in the EISOPQAM. 

3.10 Investigation Schedule

The field investigation began October 3, 2005, and ended October 7, 2005. 

During the investigation SESD: 

• Collected soil and sediment samples from the identified properties within the 

area affected by the Katrina storm surge. 

• Collected location data for sampling points using GPS techniques (Section 

3.7). 

• Collected and properly disposed non-hazardous IDW. 
17

4.0 SAMPLING DESIGN AND RATIONALE

Surface soil and sediment samples were collected during this field investigation. 

4.1 Sampling Design

Seven RMP, Tier II, and TRI facilities were selected for this investigation. In 

addition, one superfund site that had the potential to re-contaminant a remediated portion 

of the site was also selected. Three to eight sampling stations were selected for each site 

(or complex of sites). These sampling stations were selected to provide preliminary 

information on potential releases to soils and sediments beyond the perimeters of the 

facilities. 

4.2 Data Validation/Usability

Analyses for metals, Volatile Organic Compounds (VOCs), semivolatiles, 

pesticides and PCBs were performed by CLP laboratories. This data was validated 

according to the National Functional Guidelines for Organic Data Review, Office of 

Solid Waste and Emergency Response (OSWER) 9240.1-05-A-P (October 1999), the 

National Functional Guidelines for Inorganic Data Review, OSWER 9240.1-45 (October 

2004) and Region 4’s Data Validation Standard Operating Procedures for Contract 

Laboratory Program Routine Analytical Services, Revision 2.0 (January 1999). 

The dioxin/furan analyses were performed by a laboratory contracted to EPA. 

Validation of the dioxin data will be performed by ESAT, using the National Functional 

Guidelines for Dioxin Data Review, OSWER540-R-02-003 (August 2002) and Region 

4's Data Validation Standard Operating Procedures for Dioxin Data Version 3.0 (May 

2002) documents. The dioxin data will consist of a Level 4 - CLP type data package that 

contains the Chain-of-Custody paperwork, instrument raw data, initial and/or continuing 

calibration data/curves, bench sheets/sample preparation information, QA/QC 

data/information, and case narrative detailing any problems associated with this data. 

The gamma spectroscopy analyses were performed by the National Air and 

Radiation Environmental Laboratory (NAREL), using method NAREL GAM-01. 

Review and validation of all data (including screening data) from samples 

collected during this investigation was completed in an expeditious manner, utilizing 

quick turnaround times consistent with good laboratory practices. 

4.3 Data Management/Document Control

Project files will be maintained in accordance to the EISOPQAM. The field 

project leader will review the file at the conclusion of the project to ensure completeness. 

Laboratory data was released to the Chief, Technical Services Section as it became 

available.
18

5.0 QUALITY ASSURANCE

Quality assurance (QA) procedures must begin in the planning stage and continue 

through sample collection, analyses, reporting and final review. The methods that were 

used to ensure data quality are discussed below. 

5.1 Organization and Responsibilities

The field project leader has overall responsibility for field QA. Off-site 

laboratory analyses for samples collected during the investigation were conducted by the 

CLP. The precision, comparability and accuracy of sample analyses were addressed in 

accordance with the Analytical Support Branch laboratory Operations and Quality 

Assurance Manual (ASBLOQAM). 

5.2 Field QA/QC Samples

5.2.1 Matrix Spike/Matrix Spike Duplicate

Samples for laboratory quality control analyses matrix spike/matrix spike 

duplicate (MS/MSD), were designated as specified in the EISOPQAM. One MS/MSD 

sample was designated for every 20 samples split to the CLP laboratory, two total for this 

investigation. 

5.2.2 Population Variability - Duplicate Samples

Co-located duplicate samples were collected to provide data for an assessment of 

the variability of constituents within the designated areas. Following collection of the 

initial sample that is to be duplicated, the sample was re-collected with clean equipment. 

The letter ‘D’ was appended to the sample ID used for the primary sample at the 

duplicated location for the duplicate containers being sent to the laboratory (see Section 

3.6). One duplicate sample was collected per site or complex of sites. The data is located 

in the Data Summary Tables in Appendix B. There is not enough data for a valid 

statistical interpretation of this data, but examining the data indicates that some 

heterogeneity is present in these samples. This is likely a result of the samples being to 

some extent a mixture of pre-Katrina soil and sediment deposited post-Katrina. To 

answer this definitively is beyond the scope of this investigation. However, as seen 

below, the results of the split sampling indicate that this may be the case. 

5.2.3 Sample Handling - On-Site Splits

Split samples were collected to assess sample handling variability. Following 

collection and mixing of the sample that was to be split, the sample was apportioned into 

two identical sets of sample containers. The letter ‘S’ was appended to the sample ID 
19

used for the primary sample to indicate the split sample being sent to the laboratory (see 

Section 3.6). One split sample was to be collected per site, or complex of sites, two were 

inadvertently not collected. The data is located in the Data Summary Tables in 

Appendix B. As with the duplicate samples discussed above, there is not sufficient data 

for a valid statistical interpretation of this data. However, examining the data indicates 

that samples were properly mixed in the field, providing a homogenous sample for lab 

analysis. Again, a definitive answer is beyond the scope of this investigation. 

5.2.4 Trip Blanks

Four trip blanks were collected during this investigation. Trip blanks provide a 

check on the handling of soil samples collected for volatile organic compounds (VOCs) 

analyses. The results are shown in Table 8, Appendix B. Low levels (11 to 17 ug/kg) of 

acetone were reported in three of the four blanks. Acetone is a common laboratory 

contaminant. 
20

6.0 INVESTIGATION RESULTS

 The field investigation teams noted a layer of what appeared to be newly 

deposited sediment at the various sampling locations. This was apparently a result of the 

Katrina storm surge, but a factual determination of this was beyond the scope of this 

investigation. Visual estimates of the thickness of this layer of material ranged from 0” 

to approximately 2”, and was generally less than 1⁄4”. Where present, this material was 

included in the samples collected. 

 The following sections summarize the results of analysis of samples collected at 

the facilities or sites selected for the Post-Katrina soil/sediment investigation. Figures 8

through 13, contained in Appendix A of this document, show the locations of these 

samples. The analytical data summary tables provided for each facility or site are 

comprised of only the compounds or analytes that were detected (Appendix B). The 

complete data, included in Appendix C of this report, contain the detected compounds as 

well as those analyzed for but not detected, with the minimum quantitation limits for the 

undetected compounds and analytes. Appendix C also contains analytical data for 

tentatively identified compounds (TICs), unknown compounds, and petroleum products, 

where these were detected. 

 The following is a list of data qualifiers used in the analytical data summary tables 

accompanying the presentation of the investigation results. 

U Analyte not detected at or above reporting limit. 

 J Identification of analyte is acceptable; reported value is an estimate. 

 N Presumptive evidence analyte is present; analyte reported as tentative 

 identification. 

UJ Analyte not detected at or above reporting limit. Reporting limit is an 

estimate. 

NJ Presumptive evidence analyte is present; analyte reported as tentative 

identification. Reported value is an estimate.

R Presence or absence of analyte can not be determined from data due to 

severe quality control problems. Data are rejected and considered 

unusable. 

A Analyte analyzed in replicate. Reported value is “average” of replicates. 

/2 constituents or metabolites of technical chlordane.

 

 

6.1 DuPont - DeLisle 

 Three surface soil and two sediment samples were collected at five locations, as 

shown on Figure 8. These samples were analyzed for volatile organic compounds 

(VOCs), semi-volatile organic compounds (SVOCs), pesticides/PCBs, metals, and 

dioxins. Table 3 in Appendix B summarizes the results of analysis of these samples. 

Appendix C contains the data sheets with all results, including tentatively identified 

compounds (TICs) and quantitation limits for analytes that were not detected. 
21

A small diesel fuel spill was noted in the area of sample DU-SD-02 by the 

sampling team. 

 

6.2 Chevron – Pascagoula, First Chemical, Mississippi Phosphates 

 

Three surface soil and seven sediment samples were collected at ten locations, as 

shown on Figure 9. These samples were analyzed for volatile organic compounds 

(VOCs), semi-volatile organic compounds (SVOCs), pesticides/PCBs, metals, and 

radionuclides (samples BC2 and BC4 were collected as part of another investigation, no 

radionuclide analyses were performed on these samples). Table 4 in Appendix B

summarizes the results of analysis of these samples. Appendix C contains the data 

sheets with all results, including tentatively identified compounds (TICs) and quantitation 

limits for analytes that were not detected. 

6.3 Omega Protein 

Three sediment samples were collected at three locations, as shown on Figure 10. 

These samples were analyzed for volatile organic compounds (VOCs), semi-volatile 

organic compounds (SVOCs), pesticides/PCBs, and metals. Table 5 in Appendix B

summarizes the results of analysis of these samples. Appendix C contains the data 

sheets with all results, including tentatively identified compounds (TICs) and quantitation 

limits for analytes that were not detected. 

6.4 Port Bienville Industrial Park (Polychemie, Inc.) 

Two surface soil and three sediment samples were collected at five locations, as 

shown on Figure 11. These samples were analyzed for volatile organic compounds 

(VOCs), semi-volatile organic compounds (SVOCs), pesticides/PCBs, and metals. Table 

6 in Appendix B summarizes the results of analysis of these samples. Appendix C

contains the data sheets with all results, including tentatively identified compounds 

(TICs) and quantitation limits for analytes that were not detected. 

6.5 Ershigs Fiberglass, Inc.

Three surface soil and two sediment samples were collected at five locations, as 

shown on Figure 12. These samples were analyzed for volatile organic compounds 

(VOCs), semi-volatile organic compounds (SVOCs), pesticides/PCBs, and metals. Table 

7 in Appendix B summarizes the results of analysis of these samples. Appendix C

contains the data sheets with all results, including tentatively identified compounds 

(TICs) and quantitation limits for analytes that were not detected. 
22

6.6 Naval Construction Battalion Center 

 Five sediment samples were collected at the locations indicated on Figure 13. 

These samples were analyzed for dioxins only. An additional four sediment samples 

were collected in November from an outfall that may have been contaminated from a preKatrina event. These samples were analyzed for PCBs only. This data will be released in 

an addendum to this report when it is available. 
23

7.0 IMPACT EVALUATION

The Technical Services Section (TSS) of the Superfund Remedial and Technical 

Services Branch has reviewed the data for these sites, in consultation with the Regional 

programs. TSS has made a preliminary assessment regarding whether surface soil or 

sediments may have been adversely impacted by the Katrina storm surge. In particular, 

TSS was asked to evaluate whether there are any significant post-Katrina impacts from 

potential releases of hazardous substances. The question is whether or not potential 

releases of hazardous substances may have occurred or (in the case of NCBC) whether 

known environmental contamination associated with the sites has been re-distributed. It 

must be understood however, that a definitive attribution to sites cannot be made, nor can 

this study determine if observed contaminants are present due to the effects of Katrina, or 

were present prior to Katrina. 

Evaluating the sampling data to determine if there was an off-site impact from 

Hurricane Katrina posed a challenge due to the scarcity of pre-existing sampling data and 

supporting information that could be used for data interpretation. EPA’s conclusions 

regarding the potential impact of the hurricane on these sites are based on a comparison 

of post-hurricane data to available past sample data collected during facility 

investigations or routine monitoring activities. In addition, the results were compared to 

EPA Region 9 Preliminary Remediation Goals (PRGs) to determine if conditions at the 

sites might represent previously unrecognized risks to human health and the environment. 

EPA Region 9 PRGs (available at: 

http://www.epa.gov/region9/waste/sfund/prg/index.html) are conservative risk-based 

concentrations based on long-term exposures in either a residential or 

commercial/industrial setting. They are considered by EPA to be protective for people 

(including sensitive groups) over a lifetime. The PRGs are not clean up standards, but 

used to assist EPA scientists and others in initial screening-level evaluations of 

environmental measurements. 

The scope of the investigations at each site and the conclusions that were reached 

regarding releases or impacts from Hurricane Katrina are presented in the following site 

summaries. For the Risk Management Plan (RMP), Toxic Release Inventory (TRI) and 

Tier II Emergency Planning and Community Right-to-Know Act (EPCRA) facilities, 

PRGs based on an industrial/commercial exposure situation were utilized, except in the 

case where samples were taken in the vicinity of residential development; in which case 

residential PRG soil screening values were used. 

A typical background level for PAHs was based on a value of 45 mg/kg that EPA 

Region 4 considers representative of anthropogenic urban background based on a 

compilation of literature sources. For further comparison, Figure 14 (Appendix A) 

shows urban background ranges of carcinogenic PAHs from a number of literature 

sources. 

Sediments were screened against soil benchmarks because no similar benchmarks 

existed for sediments. Region 4 normally considers long-term human exposure to 

sediments that are underwater to be minimal due to limited opportunity for frequent 

contact of significant duration. Several samples contained unidentified organic 
24

compounds reported by the laboratory. Because the identities of the compounds are not 

known, they could not be screened against levels protective of human health. 

7.1 DuPont DeLisle - Pass Christian, Mississippi 

The samples for dioxin analysis were recollected due to uncertainties with the 

quality of the data from the original laboratory. This data will be issued as an addendum 

when it becomes available. 

7.1.1 Results 

Soils

Aluminum, arsenic, barium, calcium, chromium, cobalt, copper, iron, lead, 

magnesium, manganese, nickel, potassium, vanadium, and zinc were detected in the soil 

samples collected from the DuPont DeLisle facility from the dirt road and ditch. No 

semi-volatile organic compounds or PCBs were detected in soils collected from the 

DuPont DeLisle facility. Acetone was detected in several samples. Acetone is a 

common laboratory contaminant, and detections of low levels such as this one are not 

indicative of a release. Low levels of the pesticides DDD, alpha-chlordane, dieldrin, 

endrin ketone, and methoxychlor were also in these samples. 

Sediments

Aluminum, arsenic, barium, calcium, chromium, cobalt, copper, iron, lead, 

magnesium, manganese, nickel, potassium, selenium, sodium, thallium, vanadium, and 

zinc were detected in sediments collected from the DuPont DeLisle facility. No PCBs 

were detected in these samples. A few organic compounds were detected in sediments 

collected from depositional areas outside the facility (see discussion below). 

7.1.2 Discussion 

No detected metals exceeded industrial PRGs. Samples in the vicinity of 

residential development did not exceed residential soil screening values (PRGs). Facility 

specific background data was available for the metals arsenic, lead, and chromium. The 

detected concentrations of lead were slightly above the facility specific background value 

(8.7 mg/kg) taken prior to hurricane Katrina. Of the three samples the maximum value for 

lead in soil was 26 mg/kg. The maximum concentration was measured at sample location 

DU-SF-04, lower than previously detected. The maximum detected concentration of lead 

was below the preliminary remedial goal for industrial exposure of 800 mg/kg. 

Concentrations of Metals Detected in Soils Compared to Site-Specific Background 

Chemical Maximum Detected 

Concentration, mg/kg 

Site-Specific Background 

Prior to Katrina, mg/kg 

Arsenic 1.5 7.4 

Lead 26J 8.7 

Chromium 11 36.5 
25

Sediments were screened against soil benchmarks because no similar benchmarks 

exist for sediments. Region 4 normally considers long-term human exposure to sediments 

that are underwater to be minimal. The sediments in question are in a depositional area. 

They are not in an area where people are likely to come in contact with the sediments. 

A few organic compounds were detected in sample DU-SD-02, which was 

collected in a depositional area outside the facility. 1,1-Biphenyl was detected at 1100 

ug/kg, 2-methylnaphthalene was detected at 4100 ug/kg, naphthalene was detected at 

1100 ug/kg, phenanthrene was detected at 1200 ug/kg, anthracene was detected at 110 

ug/kg, and pyrene was detected at 130 ug/kg. None of the values were considered 

elevated with respect to protection of human health. Three of the chemicals (1,1-

biphenyl, naphthalene, and 2-methylnaphthalene) are volatile chemicals that are not 

expected to persist in the environment for long periods of time. These chemicals degrade 

rapidly in the environment and are not of concern for long-term exposure to people. None 

of the concentrations were greater than anthropogenic background EPA Region 4 

considers typical of industrial/urban areas. 

7.1.3 Conclusion 

From a comparison with sampling conducted pre-hurricane Katrina there is no 

clear and consistent pattern of increased contamination levels that would clearly indicate 

a potential release in the area of the DuPont DeLisle facility due to the effects of 

Hurricane Katrina. None of the reported analytes exceeded risk-based soil screening 

benchmarks for an industrial exposure scenario, or residential PRGs in the vicinity of 

residential development northeast of the facility. 

7.2 Chevron Pascagoula, First Chemical, Mississippi Phosphate - 

Pascagoula, Mississippi 

7.2.1 Results 

Soils

Aluminum, arsenic, barium, calcium, chromium, cobalt, copper, iron, lead, 

magnesium, manganese, mercury, nickel, potassium, selenium, sodium, vanadium, and 

zinc were detected in the soil samples. Low levels of pesticides heptachlor epoxide and 

methoxychlor were also detected at in soil samples. No VOCs, SVOCs or PCBs were 

reported. Samples were collected and analyzed for radionuclides. The primary 

radionuclide of concern is Radium 226 (Ra 226). 

Sediments

Aluminum, arsenic, barium, beryllium, calcium, chromium, cobalt, copper, iron, 

lead, magnesium, manganese, nickel, potassium, selenium, sodium, vanadium, and zinc 

were detected in sediment samples. Acetone and toluene were detected at low levels in 
26

two samples. Acetone and toluene are common laboratory contaminants, and detections 

of low levels such as these are not indicative of a release. Low levels of the pesticides 

DDE, gamma chlordane, heptachlor epoxide, and methoxychlor were also detected in 

sediment samples. No PCBs were reported. Samples were collected and analyzed for 

radionuclides. The primary radionuclide of concern is Ra226. 

7.2.2 Discussion 

There were no levels for Ra226 or any other radionuclide that exceeded expected 

background levels. From the data reported there were no levels that indicated a potential 

release of radioactive contamination. 

Sediments were screened against industrial PRGs. Region 4 normally considers 

long-term human exposure to sediments that are under water to be minimal. The 

sediments in question are in ditches that serve the storm water drainage and outfall areas 

of the sampled facilities. They are not in areas where people are likely to come in contact 

with the sediments. The maximum detection of total chromium (95 mg/kg) at sample 

CFM-SD-05 exceeded the industrial PRG (64 mg/kg) but was below the 1E-05 (1 in 

100,000) risk level (640 mg/kg). The maximum detected level of arsenic at sample CFMSD-06 (10 mg/kg) was above the industrial PRG (1.6 mg/kg) but below the in 1E-05 risk 

level (100 mg/kg). Both chromium and arsenic concentrations fell within a risk range of 1 

in 1,000,000 to 1 in 10,000 risk over background of an individual developing cancer over 

a lifetime from long-term exposure to those concentrations, which EPA has found 

acceptable in other regulatory and remedial contexts. None of the remaining analytes 

detected in soil or sediment exceeded industrial PRG soil screening levels. 

Baseline data collected prior to hurricane Katrina was available, including recent 

sediment data from Bayou Cassotte, sediment samples from the wetlands south of the 

Chevron Pascagoula operational area, and recent sediment sampling data from outfall 

areas of the Mississippi Phosphates Corp. 

Facility specific background data was available for the metals aluminum, arsenic, 

barium, beryllium, calcium, chromium, cobalt, iron, lead, magnesium, manganese, nickel, 

potassium, selenium and vanadium. Sediment sampling from Bayou Cassotte also 

included the metals antimony, cadmium, copper, silver, sodium, thallium, mercury and 

zinc in addition to the facility-specific metals data. Sediment and soil data were 

compared to relevant baseline data. Data that exceeded baseline sampling are shown 

below: 
27

Metals Detected in Sediment/Soils Exceeding Site-Specific Background 

Chemical Maximum detected 

concentration, 

mg/kg 

Location Site-Specific 

Background Prior to 

Katrina, mg/kg 

Aluminum 16000 CFM-SD-06 8200 (Bayou Cassotte) 

Beryllium 1.3 CFM-SD-06 1.1 (Chevron) 

Calcium 43000 CFM-SD-06 7400 (Bayou Cassotte) 

Chromium 95 CFM-SD-05 29 (Chevron) 

Cobalt 14 CFM-SD-06 8.7 (Chevron) 

Lead 63 CFM-SD-07 16 (Chevron) 

Nickel 64 CFM-SD-05/08 15 (Chevron) 

Vanadium 590 CFM-SD-05 86 (Chevron) 

Detected concentrations of aluminum, beryllium, calcium, cobalt, lead and nickel 

were above levels detected in Bayou Cassotte and the wetlands South of Chevron prior to 

hurricane Katrina. However, these samples (CFM-SD-06 and CFM-SD-07) were taken 

from a ditch that collects surface runoff drainage from the Chevron facility and an area to 

the south that had a history of industrial activity. The area where samples CFM-SD-06, 

CFM-SD-07 and CFM-SF-08 were located is currently in a solid waste management unit 

(SWMU). 

Prior to Chevron acquiring this area, it was formerly used by the HK Porter 

Company to manufacture refractory brick. During industrial activities, surface soil 

became contaminated with various metals including magnesium and calcium. Later, this 

area became part of the Owens Corning Glass Plant. Given the past history of industrial 

use in the area, and that the sample was obtained from a drainage ditch that collected 

surface runoff from areas impacted by current and previous industrial activity, it is not 

surprising to see elevated levels of metals. It is likely that these metals concentrations 

were pre-existing in the area and questionable whether they resulted from the impact of 

hurricane Katrina. 

Detected concentrations of chromium, nickel, and vanadium were identified in 

sample CFM-SD-05, which was collected from a drainage ditch southeast of the Chevron 

operational area. This ditch is part of an existing SWMU and on Chevron property. The 

SWMU that this ditch drains is a hurricane retention pond known to contain vanadium in 

soil and sludge. This is the only location where vanadium has been previously detected in 

any significant quantity. Nickel has been used as a crude oil cracking catalyst and can be 

found in the soil at several SWMUs within the plant. Therefore, it is unsurprising to 

encounter elevated levels of vanadium, nickel or other metals in this ditch, and is unlikely 

to constitute a hurricane Katrina-related impact. 

7.2.3 Conclusion

In spite of several metals exceeding local baseline sampling data, the exceedances 

are not significant enough to clearly indicate an impact due to hurricane Katrina in light 

of the likelihood of pre-existing metals contamination in surficial soil and drainage ditch 

sediments. All detected analytes were within a risk-range considered acceptable by EPA 

in other regulatory contexts. It is unlikely that frequent and prolonged human contact 
28

with sediments under water in drainage ditches would occur. There does not appear to be 

an indication of a potential release in the area of the facilities due to the effects of 

Hurricane Katrina. 

7.3 Omega Protein - Moss Point, Mississippi 

 7.3.1 Results 

Sediments

 Aluminum, antimony, arsenic, barium, beryllium, calcium, chromium, cobalt, 

copper, iron, lead, magnesium, manganese, nickel, potassium, sodium, thallium, mercury, 

vanadium and zinc were detected in these samples. Low concentrations of several semivolatile organic compounds and low levels of pesticides were also detected. One PCB, 

PCB-1260, was reported at a concentration of 21J ug/kg in sample OP-SD-02. No 

volatile organic compounds were reported. 

 7.3.2 Discussion

No pre-Katrina sampling data is available for the site, therefore there is 

uncertainty about impact of the hurricane on the surrounding environment. Detected 

analytes were compared to industrial PRG soil screening levels. Arsenic (2.2 mg/kg) 

slightly exceeded the industrial PRG (1.6 mg/kg) at sampling point OP-SD-02, but was 

below the 1E-05 risk level (16 mg/kg). Benzo(a)pyrene (1300 ug/kg) exceeded the 

industrial PRG (210 ug/kg) at sample location OP-SD-01, but was below the 1E-05 risk 

range. Both fell within a risk range of 1 in 1,000,000 to 1 in 10,000 risk over background 

of an individual developing cancer over a lifetime from long-term exposure to those 

concentrations, which EPA has found acceptable in other regulatory and remedial 

contexts. None of the remaining analytes detected in soil or sediment exceeded industrial 

PRG soil screening levels. 

 7.3.3 Conclusion

There is no clear indication of a release in the area of the Omega Protein facility 

due to the effects of Hurricane Katrina. None of the reported analytes exceeded levels of 

concern for exposure to contaminants in soil or sediment under a commercial/industrial 

scenario. 

 7.4 Port Bienville Industrial Park (Polychemie, Inc.) - Pearlington, Mississippi

 7.4.1 Results 

Soils

Aluminum, arsenic, barium, calcium, chromium, cobalt, copper, iron, lead, 

magnesium, manganese, nickel, potassium, selenium, sodium, vanadium, and zinc were 
29

detected in the soil samples collected from the Polychemie, Inc. facility from the southern 

portion of the site. No semi-volatile or volatile organic compounds were reported in 

these samples. No PCBs were reported for these samples. Gamma chlordane was 

detected in soil sample PO-SF-04 at 0.86J mg/kg. 

Sediments

Aluminum, arsenic, barium, cadmium, calcium, chromium, cobalt, copper, iron, 

lead, magnesium, manganese, nickel, potassium, sodium, vanadium, and zinc were 

detected in sediments collected from the Polychemie, Inc. facility. No pesticides or PCBs 

were reported in these samples. 

Several organic compounds were detected in sediments. One volatile organic 

compound, acetone, was detected at 140 ug/kg in sample PO-SD-01D. Acetone is a 

common laboratory contaminant, and detections of low levels such as this one are not 

suggestive of a release. Ten PAH compounds were detected in Sample PO-SD-03. These 

included benzo(a)anthracene, benzo(b)fluoranthene, benzo(ghi)perylene, 

benzo(k)fluoranthene, benzo-a-pyrene, chrysene, fluoranthene, indeno (1,2,3-cd) pyrene, 

phenanthrene, and pyrene. Levels of the PAHs ranged between 120 ug/kg for 

benzo(ghi)perylene to 400 ug/kg for fluoranthene. 

Unknown miscellaneous semi-volatile organic compounds were reported by the 

CLP laboratory. The identities of the unknown compounds were not verified by the 

laboratory. 

 7.4.2 Discussion 

No facility specific background data was available for the metals detected in soils. 

Arsenic detections exceeded the industrial PRG (1.6 mg/kg) at sample locations PO-SD01 and PO-SD-02 (18, 7.7 mg/kg), but were within a risk range of 1 in 1,000,000 to 1 in 

10,000 risk over background of an individual developing cancer over a lifetime from 

long-term exposure to those concentrations, which EPA has found acceptable in other 

regulatory and remedial contexts. None of the other metals detected exceeded industrial 

PRGs. 

None of the concentrations of organic compounds exceeded industrial PRGs and 

detected PAHs appear low relative to anthropogenic background typical of urban areas as 

shown in Figure 14. 

 7.4.3 Conclusion

Because no background data are available for the site prior to Hurricane Katrina, 

it is difficult to determine the impact of the hurricane on the surrounding environment 

with certainty. However, none of the concentrations detected were at levels of concern in 

regard to protection of human health. There is no indication of a potential release in the 

area of the Polychemie, Inc. facility due to the effects of Hurricane Katrina. 
30

7.5 Ershigs Fiberglass - Biloxi, Mississippi 

7.5.1 Results 

Soils

Aluminum, arsenic, barium, cadmium, calcium, chromium, cobalt, copper, iron, 

lead, magnesium, manganese, nickel, potassium, sodium, vanadium, and zinc were 

reported in soil samples collected for this site. No volatile organic compounds, or PCBs 

were detected in these samples. Low concentrations of six semi-volatile organic 

compounds and six pesticides were reported. 

Sediments

Aluminum, arsenic, barium, calcium, chromium, cobalt, copper, iron, lead, 

magnesium, manganese, nickel, potassium, sodium, vanadium, and zinc were reported for 

these samples. Twelve semi-volatile organic compounds and eight pesticides were 

reported at low concentrations. No volatile organic compounds or PCBs were reported. 

7.5.2 Discussion 

Because no background data are available for the site prior to Hurricane Katrina, 

it is difficult to determine the impact of the hurricane on the surrounding environment 

with certainty. Although this facility is in an industrialized area, there is evidence of 

residential development in the vicinity of the site. As an added precaution, detected 

analytes were compared to residential PRGs. 

Arsenic (1.3-14 mg/kg) was the only metal that exceeded residential PRGs (0.4 

mg/kg), however all detections were within a risk range of 1 in 1,000,000 to 1 in 10,000 

risk over background of an individual developing cancer over a lifetime from long-term 

exposure to those concentrations, which EPA has found acceptable in other regulatory 

and remedial contexts. The highest arsenic concentrations were taken in the vicinity of a 

commercial parking lot, while those samples closer to residential areas were below the 

1E-05 risk level. None of the other analytes exceeded residential PRG soil screening 

values. 

7.5.3 Conclusion 

There does not appear to be indication of a potential release in the area of Ershigs 

Fiberglass due to the effects of Hurricane Katrina. Styrene, one of the primary chemicals 

stored and used on site, was not detected in the analysis. None of the detected analytes 

were at levels of concern for excess human health risk from long term exposure. 
31

7.6 Naval Construction Battalion Center - Gulfport, Mississsippi

The data and discussion for NCBC will be issued as an addendum. Samples for 

dioxin analysis were recollected due to uncertainties with the quality of the data from the 

original laboratory. Four additional samples were collected from another portion of the 

base for PCB analysis at the request of MDEQ, and will be included in the addendum. 
32

8.0 REFERENCES 

1. Comprehensive Environmental Response, Compensation, and Liability 

Act of 1980 (CERCLA) and the Superfund Amendments and 

Reauthorization Act of 1986 (SARA). 

2. U.S. EPA, EPAQA/G-4, Guidance for the Data Quality Objectives 

Process, EPA/600/R-96/055, August 2000. 

3. U.S. EPA, EPAQA/G-5, EPA Guidance for Quality Assurance Project 

Plans, EPA/600/R-98/018, February 1998. 

4. U.S. EPA, Region 4, Analytical Support Branch Operations and Quality 

Control Manual Revision 1, (ASBLOQAM). July 2001. 

5. U.S. EPA, Region 4, Environmental Investigations Standard Operating 

Procedures and Quality Assurance Manual (EISOPQAM). November 

2001. (http://www.epa.gov/region4/sesd/sesdpub_guidance.html). 

6. USEPA Contract laboratory Program Statement of Work for Inorganic 

Analysis, ILM05.3 March 2004. 

http://www.epa.gov/superfund/programs/clp/inorg.htm 

7. USEPA Contract laboratory Program Statement of Work for Inorganic 

Analysis, OLM04.2, May, 1999. 

http://www.epa.gov/superfund/programs/clp/organic.htm 

8. USEPA Water Quality Studies of Bays in Waters of Mississippi, October, 

2005. 

9. Quality Assurance Project Plan Katrina Response Environmental Soil and 

Sediment Sampling Gulf Coast of Mississippi, September, 2005. 

10. Menzie et al. (1992) Exposure to Carcinogenic PAHs in the Environment. 

Env Sci Technol 26, 1278-1284. 

11. Saltiene et al. (2001) Contamination of Soil by Polycyclic Aromatic 

Hydrocarbons in Some Urban Areas, 

http://preprint.chemweb.com/envchem/0102001. 

12. Electric Power Research Institute (EPRI) (2000) Literature Review of 

Polycyclic Aromatic Hydrocarbons TR-114755. This source provides 

values for US and Japan background ranges, Michigan schools and 

residences and Ohio residences. 

13. ATSDR, 2002 Toxicological Profile for Polycyclic Aromatic 

Hydrocarbons. P. 262, Table 5-3. 
33

Appendix A 

Figures
34
35
36
37
38
39
40
41
42
43
44
45
46
47

 Figure 14: Comparison of background ranges of cPAHs from a variety of sources.

0.1 1 10 100 1000 10000

Eastern M agazine Area

ATSDR Background Range

EPRI US urban background

EPRI Japan background

Columbus OH residences

Michigan Schools

Michigan Residences

Saltiene et al, Int'l cities

Menzie et al. US urban background
48

Appendix B 

Data Summary Tables
Table 1 

Sample Rationale and Locations 

Facility Sample ID Grab or 

Composite

Location Rationale 

DuPont DeLisle DU-SD-01 Grab (0”-

3”) 

Dirt road and canal southwest of Site 

Evaluate potential for hazardrained from site via ditch. 

DuPont DeLisle DU-SD-02 Grab (0”-

3”) 

Dirt road at well south of site Evaluate potential for hazar

drained from site via ditch. 

DuPont DeLisle DU-SF-03 3 point 

composite (0”-3”) 

South of swale along Kiln DeLisle Rd. 

Evaluate potential for hazarmoved North with storm su

DuPont DeLisle DU-SF-04 3 point 

composite (0”-3”) 

South of swale along Kiln DeLisle Rd. 

Evaluate potential for hazarmoved North with storm su

DuPont DeLisle DU-SF-05 4 point 

composite (0”-3”) 

South of swale along Kiln DeLisle Rd. 

Evaluate potential for hazarmoved North with storm su

Chevron, First Chemical, MS Phosphates 

CFM-SF-01 3 point 

linear composite (0”-3”) 

Bank of concrete drainage structure 

Evaluate potential for hazarmoved North with storm su

Chevron, First Chemical, MS Phosphates 

CFM-SF-02 5 point 

‘Star’ composite (0”-3”) 

Chevron Ditch, South of complex 

Evaluate potential for hazarmoved drained with storm 

Chevron, First Chemical, MS Phosphates 

CFM-SD-04 Grab (0”-

3”) 

South of storm surge lagoon Evaluate potential for hazar

moved North with storm su

Chevron, First Chemical, MS Phosphates 

CFM-SD-05 Grab (0”-

3”) 

Wetlands southeast of complex Evaluate potential for hazar

moved North with storm su

Chevron, First Chemical, MS Phosphates 

CFM-SD-06 Grab (0”-

3”) 

Ditch south of complex Evaluate potential for hazar

moved North with storm su
Chevron, First Chemical, MS Phosphates 

CFM-SD-07 Grab (0”-

3”) 

Ditch south of complex Evaluate potential for hazar

moved North with storm su

Chevron, First Chemical, MS Phosphates 

CFM-SF-08 5 point 

‘Star’ composite (0”-3”) 

South of complex Evaluate potential for hazar

moved South with storm su

Chevron, First Chemical, MS Phosphates 

BC2 (Sediment) 

Grab Bayou Cassotte, West of MS 

Phosphates 

Evaluate potential for hazarmoved South with storm su

Chevron, First Chemical, MS Phosphates 

BC4 (Sediment) 

Grab Bayou Cassotte, Southwest of 

First Chemical 

Evaluate potential for hazarmoved South with storm su

Omega Protein OP-SD-01 Grab Bank of Escatawpa River, 

South of Site 

Evaluate potential for hazardrained South with storm su

Omega Protein OP-SD-02 Grab Bank of Escatawpa River, 

South of Site 

Evaluate potential for hazardrained South with storm su

Omega Protein OP-SD-03 Grab Bank of Escatawpa River, 

downstream of Site (power line right-of-way) 

Evaluate potential for hazarmoved downstream with st

Polychemie PO-SD-01 Wetland North of Site Evaluate potential for hazar

drained North with storm su

Polychemie PO-SD-02 Canal West of Site Evaluate potential for hazar

drained West with storm su

Polychemie PO-SD-03 Grab Canal at Sea Plane Rd. Evaluate potential for hazar

moved downgradient with s

Polychemie PO-SF-04 5 point 

linear composite near road 

Southeast of Site Evaluate potential for hazar

moved Southeast with storm 
Polychemie PO-SF-05 5 point 

linear composite between fence and road 

Southwest of Site Evaluate potential for hazar

moved Southwest with stor

Ershigs Fiberglass, Inc. 

ER-SF-01 5 point 

composite collected around perimeter of basketball court 

Northwest of Site Evaluate potential for hazar

moved Northwest with stor

Ershigs Fiberglass, Inc. 

ER-SF-02 5 point 

‘Star’ composite (0”-3”) 

Southwest of Site Evaluate potential for hazar

moved West with storm sur

Ershigs Fiberglass, Inc. 

ER-SF-03 5 point 

‘Star’ composite (0”-3”) 

South of Site Evaluate potential for hazar

moved Southwest with stor

Ershigs Fiberglass, Inc. 

ER-SD-04 Grab (0”-

3”) 

South of Site, Canal on west side of parking lot 

Evaluate potential for hazarmoved South with storm su

Ershigs Fiberglass, Inc. 

ER-SD-05 Grab (0”-

3”) 

Inlet southeast of Site Evaluate potential for hazar

drained Southwest with sto

NCBC Gulfport NC-SD-01 Grab (0”-

3”) 

Wetland North of NCBC Evaluate potential for TCD

remediated portion of wetla

NCBC Gulfport NC-SD-02 Grab (0”-

3”) 

Wetland North of NCBC Evaluate potential for TCD

remediated portion of wetla

NCBC Gulfport NC-SD-03 Grab (0”-

3”) sediment trap 

Wetland North of NCBC Evaluate potential for TCD

remediated portion of wetla
NCBC Gulfport NC-SD-04 Grab (0”-

3”)sediment trap 

Wetland North of NCBC Evaluate potential for TCD

remediated portion of wetla

NCBC Gulfport NC-SD-05 Grab (0”-

3”) sediment trap 

Wetland North of NCBC (Edwards tract) 

Evaluate potential for TCDremediated portion of wetla
Table 2 

Sample Containers and Holding Times 

Analytes Containers Splits Dups Holding 

Times 

Metals 1 8oz. glass 1 8oz. glass 1 8oz. glass 180 days VOCs 3 EnCoreTM 3 EnCoreTM 3 EnCoreTM 48 hours Semi-Volatiles, Pesticides, PCBs 

1 8oz. glass 1 8oz. glass 1 8oz. glass 14 days 

Dioxins 1 8oz. glass 1 8oz. glass 1 8oz. glass 30 days Radium 226 and gamma Spectroscopy 

1 8oz. glass 1 8oz. glass 1 8oz. glass 180 days 
Table 3 

Data Summary Table - Metals 

Post - Katrina Soil and Sediment Sampling 

DuPont - DeLisle 

Pass Christian, Mississippi 

October, 2005 

 DUSD01 DUSD01D DUSD02 DUSF03 DUSF04 DUS 1010 1105 1200 1405 1345  10/4/2005 10/4/2005 10/4/2005 10/4/2005 10/4/2005 10/4/2% Moisture % 55 58 24 11 12 Aluminum MG/KG 12000 9000 4800 6500 5100 4Arsenic MG/KG 53 J 35 J 1 R 1.4 1.5 Barium MG/KG 140 J 87 J 400 27 17 J Beryllium MG/KG 2 1.3 0.22 UJ 0.12 UJ 0.1 UJ Calcium MG/KG 1500 J 1400 J 330 J 1100 230 J Chromium MG/KG 22 J 18 J 7.3 J 11 J 9.1 J Cobalt MG/KG 8.3 J 7.9 J 0.83 J 1.2 J 0.74 J Copper MG/KG 33 J 22 J 2.6 J 2.7 J 2 J Iron MG/KG 13000 J 13000 J 2900 J 9900 J 7900 J 4Lead MG/KG 18 J 15 J 16 J 16 J 26 J Magnesium MG/KG 1100 1200 470 J 150 J 140 J Manganese MG/KG 96 J 130 J 12 J 380 J 180 J Nickel MG/KG 18 J 14 J 1.6 J 2.5 J 1.6 J Potassium MG/KG 1600 1200 J 240 J 88 J 82 J Selenium MG/KG 0.88 J 0.73 R 4.6 U 4 U 0.48 R Sodium MG/KG 1800 1900 630 J 110 UJ 110 UJ Thallium MG/KG 1.9 J 0.53 R 3.3 U 2.8 U 2.8 U Vanadium MG/KG 50 38 11 16 14 Zinc MG/KG 56 49 J 15 21 14 

U-Analyte not detected at or above reporting limit. J-Identification of analyte is acceptable; reported value is an estimate. UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate. R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data aunusable. 
Table 3 (Continued) 

Data Summary Table – Semi-Volatiles 

Post - Katrina Soil and Sediment Sampling 

DuPont - DeLisle 

Pass Christian, Mississippi 

October, 2005 

DUSD01 DUSD01D DUSD02 DUSF03 DUSF04 

 1010 1105 1200 1405 1345  10/4/2005 10/4/2005 10/4/2005 10/4/2005 10/4/2005 % Moisture % 50 50 24 14 12 1,1-Biphenyl UG/KG 660 U 660 U 1100 380 U 380 U 2-Methylnaphthalene UG/KG 660 U 660 U 4100 380 U 380 U Anthracene UG/KG 660 U 660 U 110 J 380 U 380 U Naphthalene UG/KG 660 U 660 U 1100 380 U 380 U Phenanthrene UG/KG 660 U 660 U 1200 380 U 380 U Pyrene UG/KG 660 U 660 U 130 J 380 U 380 U 

U-Analyte not detected at or above reporting limit. J-Identification of analyte is acceptable; reported value is an estimate. 
Table 3 (Continued) 

Data Summary Table – Pesticides/PCBs 

Post - Katrina Soil and Sediment Sampling 

DuPont - DeLisle 

Pass Christian, Mississippi 

October, 2005 

DUSD01 DUSD01D DUSD02 DUSF03 DUSF04 

 1010 1105 1200 1405 1345  10/4/2005 10/4/2005 10/4/2005 10/4/2005 10/4/2005 % Moisture % 50 50 24 14 12 4,4'-DDD (p,p'-DDD) UG/KG 6.6 UJ 6.6 UJ 4.3 UJ 3.3 UJ 0.8 J alpha-Chlordane /2 UG/KG 4.7 4 N 2.2 U 1.7 U 1.1 NDieldrin UG/KG 6.6 U 6.6 U 4.3 U 3.3 U 1 J Endosulfan I (alpha) UG/KG 3.4 U 1.1 J 2.2 U 1.7 U 1.9 U Endrin UG/KG 1.8 NJ 6.6 U 1 J 3.3 U 3.8 U Endrin Ketone UG/KG 6.6 U 6.6 U 4.3 U 3.3 U 3.8 U Methoxychlor UG/KG 34 U 34 U 22 U 5.7 J 19 U 

 U-Analyte not detected at or above reporting limit. 

J-Identification of analyte is acceptable; reported value is an estimate. UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate. NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an esti/2-constituents or metabolites of technical chlordane 
Table 3 (Continued) 

Data Summary Table – Volatile Organic Compounds 

Post - Katrina Soil and Sediment Sampling 

DuPont - DeLisle 

Pass Christian, Mississippi 

October, 2005 

DUSD01 DUSD01D DUSD02 DUSF03 DUSF04 DU

 1010 1105 1200 1405 1345  10/4/2005 10/4/2005 10/4/2005 10/4/2005 10/4/2005 10/4% Moisture % 56 55 24 14 12 Acetone UG/KG 34 UJ 50 J 68 J 12 UJ 53 J Benzene UG/KG 34 U 38 U 24 J 12 U 11 U Ethyl Benzene UG/KG 34 U 38 U 230 J 12 U 11 U Isopropylbenzene UG/KG 34 U 38 U 140 J 12 U 11 U Methylcyclohexane UG/KG 34 U 38 U 140 J 12 U 11 U Toluene UG/KG 34 U 38 U 23 J 12 U 11 U Total Xylenes UG/KG 34 U 38 U 760 J 12 U 11 U 

U-Analyte not detected at or above reporting limit. J-Identification of analyte is acceptable; reported value is an estimate. UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate. 
Table 4 

Data Summary Table – Metals 

Post - Katrina Soil and Sediment Sampling 

Chevron Refinery – Pascagoula, First Chemical, and Mississippi Phosphate 

Pascagoula, Mississippi 

October, 2005 

 CFMSF01 CFMSF02 CFMSF02S CFMSD03 CFMSD04 CFMS 1055 1130 1130 1240 1345  10/6/2005 10/6/2005 10/6/2005 10/6/2005 10/6/2005 10/6/2% Moisture % 9 22 22 58 25 Aluminum MG/KG 7500 4000 4200 6800 4000 8Arsenic MG/KG 1.7 0.64 J 0.68 R 3.3 1.5 J Barium MG/KG 13 J 8 J 8.6 J 11 J 7.3 J Beryllium MG/KG 0.13 UJ 0.08 UJ 0.08 UJ 0.32 UJ 0.06 J Calcium MG/KG 9800 660 690 1200 J 3000 5Chromium MG/KG 9.2 J 4 J 4.2 J 14 J 5.6 Cobalt MG/KG 0.69 J 0.34 J 0.38 J 1.8 J 0.66 J Copper MG/KG 3.6 2.6 J 2.7 J 6.8 2 J Iron MG/KG 5100 J 1300 J 1400 J 9200 J 5800 8Lead MG/KG 8.4 J 15 J 18 J 8 J 3 Magnesium MG/KG 300 J 190 J 190 J 2400 610 J 4Manganese MG/KG 16 J 4.6 J 5.1 J 51 J 32 J Nickel MG/KG 3.6 J 1.2 J 1.4 J 5.9 J 2.5 J Potassium MG/KG 200 J 110 J 110 J 1400 240 J Selenium MG/KG 3.9 U 0.48 R 4.5 U 8.4 U 4.7 U Sodium MG/KG 470 J 520 J 530 J 9900 2800 22Total Mercury MG/KG 0.38 0.03 UJ 0.03 UJ 0.24 U 0.13 U Vanadium MG/KG 15 7.1 7.5 28 9.8 Zinc MG/KG 18 16 16 30 9.5 

U-Analyte not detected at or above reporting limit. J-Identification of analyte is acceptable; reported value is an estimate. UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate. R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data aunusable. 
Table 4 (Continued) 

Data Summary Table – Metals 

Post - Katrina Soil and Sediment Sampling 

Chevron Refinery – Pascagoula, First Chemical, and Mississippi Phosphate 

Pascagoula, Mississippi 

October, 2005 

 CFMSD06 CFMSD07 CFMSF08  1145 1115 1035 10/6/2005 10/6/2005 10/6/2005% Moisture % 49 49 7Aluminum MG/KG 16000 11000 4300Antimony MG/KG 0.76 R 12 UJ 6.4 UJArsenic MG/KG 10 2.9 1.7Barium MG/KG 59 37 J 17 J Beryllium MG/KG 1.3 0.51 UJ 0.29 UJCadmium MG/KG 0.34 UJ 0.29 UJ 0.05 UJCalcium MG/KG 43000 7700 15000Chromium MG/KG 60 J 28 J 16 J Cobalt MG/KG 14 2.5 J 2.2 J Copper MG/KG 15 20 23Iron MG/KG 21000 J 8600 J 4300 J Lead MG/KG 26 J 63 J 6.6 J Magnesium MG/KG 11000 3200 890Manganese MG/KG 890 J 93 J 45 J Nickel MG/KG 20 8.7 64Potassium MG/KG 2300 1300 220 J Selenium MG/KG 6.8 U 3.1 J 1.5 J Sodium MG/KG 8600 7700 300 J Vanadium MG/KG 41 60 240Zinc MG/KG 130 120 95

 U-Analyte not detected at or above reporting limit. 

J-Identification of analyte is acceptable; reported value is an estimate. UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate. R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data a

unusable. 
Table 4 (Continued) 

Data Summary Table – Metals 

Post - Katrina Soil and Sediment Sampling 

Chevron Refinery – Pascagoula, First Chemical, and Mississippi Phosphate 

Pascagoula, Mississippi 

October, 2005 

BC2SD BC4DSD BC4SD 

 1130 1300 1240 9/27/2005 9/27/2005 9/27/2005% Moisture % 60 41 49 AAluminum MG/KG 8200 2600 3000Arsenic MG/KG 6.4 1.2 0.87Barium MG/KG 130 27 57Beryllium MG/KG 0.82 0.3 0.3Cadmium MG/KG 1.1 1.5 1.8Calcium MG/KG 7400 4900 4700Chromium MG/KG 21 7.2 9.7Cobalt MG/KG 4.6 0.59 0.66Copper MG/KG 20 4.7 5.5Iron MG/KG 17000 3400 3200Lead MG/KG 36 4.8 5.9Magnesium MG/KG 5100 1800 1700Manganese MG/KG 450 26 26Nickel MG/KG 8.4 2.4 2.7Potassium MG/KG 2300 510 450Sodium MG/KG 18000 8500 5900Strontium MG/KG 57 59 66Titanium MG/KG 17 12 14Vanadium MG/KG 24 6.1 7.3Yttrium MG/KG 12 2.7 2.5Zinc MG/KG 140 48 55

 A-Analyte analyzed in replicate. Reported value is 'average' of replicates. 
Table 4 (Continued) 

Data Summary Table – Semi-Volatile Organic Compounds 

Post - Katrina Soil and Sediment Sampling 

Chevron Refinery – Pascagoula, First Chemical, and Mississippi Phosphate 

Pascagoula, Mississippi 

October, 2005 

BC2SD BC4DSD BC4SD 

 1130 1300 1240 9/27/2005 9/27/2005 9/27/2005% Moisture % 63.61 29.58 33.67Fluoranthene UG/KG 900 U 66 J 500 UPyrene UG/KG 900 U 63 J 500 U

U-Analyte not detected at or above reporting limit. J-Identification of analyte is acceptable; reported value is an estimate. 
Table 4 (Continued) 

Data Summary Table – Pesticides/PCBs 

Post - Katrina Soil and Sediment Sampling 

Chevron Refinery – Pascagoula, First Chemical, and Mississippi Phosphate 

Pascagoula, Mississippi 

October, 2005 

 CFMSF01 CFMSF02 CFMSF02S CFMSD03 CFMSD04  1055 1130 1130 1240 1345  10/6/2005 10/6/2005 10/6/2005 10/6/2005 10/6/2005 % Moisture % 9 23 21 54 25 gamma-Chlordane /2 UG/KG 1.9 U 2.2 U 2.2 U 3.7 U 2.3 U Methoxychlor UG/KG 19 U 22 U 5.3 NJ 37 U 23 U  CFMSD05D CFMSD06 CFMSD07 CFMSF08  1245 1145 1115 1035 10/6/2005 10/6/2005 10/6/2005 10/6/2005% Moisture % 73 51 40 6gamma-Chlordane /2 UG/KG 3.2 NJ 3.5 U 2.8 U 1.8 U Methoxychlor UG/KG 63 U 7.8 NJ 28 U 3.7 NJ

 U-Analyte not detected at or above reporting limit. 

NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an esti/2-constituents or metabolites of technical chlordane 
Table 4 (Continued) 

Data Summary Table – VOCs 

Post - Katrina Soil and Sediment Sampling 

Chevron Refinery – Pascagoula, First Chemical, and Mississippi Phosphate 

Pascagoula, Mississippi 

October, 2005 

CFMSF01 CFMSF02 CFMSF02S CFMSD03 CFMSD04 CFM

 1055 1130 1130 1240 1345  10/6/2005 10/6/2005 10/6/2005 10/6/2005 10/6/2005 10/6/% Moisture % 9 23 21 56 25 Acetone UG/KG 11 U 13 U 13 U 35 U 13 U Toluene UG/KG 11 U 13 U 13 U 35 U 13 U  CFMSD06 CFMSD07 CFMSF08  1145 1115 1035 10/6/2005 10/6/2005 10/6/2005% Moisture % 51 40 6Acetone UG/KG 25 U 24 U 16 UToluene UG/KG 25 U 24 U 16 U

BC2SD BC4DSD BC4SD 

 1130 1300 1240 9/27/2005 9/27/2005 9/27/2005% Moisture % 60 41 501,2,3-Trichlorobenzene UG/KG 1.8 J 4.6 U 6.5 UBenzene UG/KG 0.23 J 2.3 U 3.3 UCarbon Disulfide UG/KG 4.7 J 3.2 4.4Isopropylbenzene UG/KG 14 2.3 U 3.3 Un-Butylbenzene UG/KG 50 J 4.6 U 6.5 Un-Propylbenzene UG/KG 51 J 2.3 U 3.3 Up-Isopropyltoluene UG/KG 43 J 2.3 U 3.3 Usec-Butylbenzene UG/KG 30 J 2.3 U 3.3 U

U-Analyte not detected at or above reporting limit. J-Identification of analyte is acceptable; reported value is an estimate. 
Table 4 (Continued) 

Data Summary Table – Radionuclides (CFM-SF-01) 

Post - Katrina Soil and Sediment Sampling 

Chevron Refinery – Pascagoula, First Chemical, and Mississippi Phosphate 

Pascagoula, Mississippi 

October, 2005 

Analyte Activity ± 2F

Uncertainty 

MDC Unit Date 

Ba140 

Bi212 Bi214 

Co60 

Cs137 

I131 

K40 

Pb210 Pb212 Pb214 

Ra223 Ra226 Ra228 

Tl208 

U235 

* * * *

ND 

4.72e-01 8.24e-01 

ND 

4.51e-02 

ND 

7.19e-01 

ND 

4.28e-01 8.75e-01 1.41e-01 

2.28e+00 

4.61e-01 1.34e-01 1.42e-01 

2.3e-01 6.6e-02 1.3e-02 2.2e-01 4.3e-02 6.5e-02 1.0e-01 4.1e-01 6.2e-02 2.1e-02 2.5e-02 

1.2e-01 2.7e-02 4.9e-02 

3.1e+00 

PCI/GDRY

PCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRY

10/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated. 

Analyte Activity ± 2F

Uncertainty 

MDC Unit Date 

Ra226 9.22e-01 1.5e-01 2.6e-02 PCI/GDRY 10/25/2005
Table 4 (Continued) 

Data Summary Table – Radionuclides (CFM-SF-02) 

Post - Katrina Soil and Sediment Sampling 

Chevron Refinery – Pascagoula, First Chemical, and Mississippi Phosphate 

Pascagoula, Mississippi 

October, 2005 

Analyte Activity ± 2F

Uncertainty 

MDC Unit Date 

Ba140 

Bi212 Bi214 

Co60 

Cs137 

I131 

K40 

Pb210 Pb212 Pb214 

Ra223 Ra224 Ra226 Ra228 

Tl208 

U235 

* * * *

ND 

3.99e-01 5.10e-01 

ND 

1.54e-01 

ND 

5.89e-01 

ND 

4.64e-01 5.45e-01 1.00e-01 3.93e-01 

1.20e+00 

4.67e-01 1.36e-01 7.54e-02 

2.2e-01 4.8e-02 2.0e-02 2.1e-01 4.6e-02 4.9e-02 1.0e-01 3.6e-01 3.5e-01 6.1e-02 2.1e-02 2.2e-02 

1.1e-01 2.6e-02 4.5e-02 

2.8e+00 

PCI/GDRY

PCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRY

10/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated. 

Analyte Activity ± 2F

Uncertainty 

MDC Unit Date 

Ra226 5.85e-01 1.0e-01 2.8e-02 PCI/GDRY 10/25/2005
Table 4 (Continued) 

Data Summary Table – Radionuclides (CFM-SF-02S) 

Post - Katrina Soil and Sediment Sampling 

Chevron Refinery – Pascagoula, First Chemical, and Mississippi Phosphate 

Pascagoula, Mississippi 

October, 2005 

Analyte Activity ± 2F

Uncertainty 

MDC Unit Date 

Ba140 

Bi212 Bi214 

Co60 

Cs137 

I131 

K40 

Pb210 Pb212 Pb214 

Ra223 Ra226 Ra228 

Tl208 

U235 

* * * *

ND 

3.29e-01 5.06e-01 

ND 

1.56e-01 

ND 

8.68e-01 

ND 

4.58e-01 5.59e-01 1.31e-01 

1.13e+00 

4.77e-01 1.33e-01 7.12e-02 

2.4e-01 5.2e-02 2.1e-02 2.2e-01 4.7e-02 5.2e-02 9.8e-02 4.1e-01 6.6e-02 2.2e-02 2.6e-02 

1.5e-01 2.8e-02 5.1e-02 

3.1e+00 

PCI/GDRY

PCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRY

10/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated. 

Analyte Activity ± 2F

Uncertainty 

MDC Unit Date 

Ra226 6.70e-01 1.1e-01 3.3e-02 PCI/GDRY 10/25/2005
Table 4 (Continued) 

Data Summary Table – Radionuclides (CFM-SD-03) 

Post - Katrina Soil and Sediment Sampling 

Chevron Refinery – Pascagoula, First Chemical, and Mississippi Phosphate 

Pascagoula, Mississippi 

October, 2005 

Analyte Activity ± 2F

Uncertainty 

MDC Unit Date 

Ba140 

Be7 

Bi212 Bi214 

Co60 

Cs137 

I131 

K40 

Pb210 Pb212 Pb214 

Ra223 Ra224 Ra226 Ra228 Th234 

Tl208 

U235 

* * * * * *

ND 

2.75e-01 3.51e-01 3.64e-01 

ND 

2.39e-02 

ND 

2.34e+00 

8.85e-01 4.65e-01 4.35e-01 1.53e-01 3.97e-01 

1.08e+00 

3.74e-01 6.77e-01 1.42e-01 6.75e-02 

1.5e-01 2.8e-01 6.0e-02 1.7e-02 4.2e-01 9.3e-01 4.8e-02 5.2e-02 7.5e-02 3.3e-01 4.0e-01 7.0e-02 2.3e-01 2.8e-02 2.5e-02 

1.6e-01 5.6e-02 5.1e-02 

PCI/GDRY

PCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRY

10/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/2005

 * An asterisk indicates a result whose value may be significantly over or underestimated. 

Analyte Activity ± 2F

Uncertainty 

MDC Unit Date 

Ra226 4.90e-01 8.8e-02 2.7e-02 PCI/GDRY 10/25/2005
Table 4 (Continued) 

Data Summary Table – Radionuclides (CFM-SD-04) 

Post - Katrina Soil and Sediment Sampling 

Chevron Refinery – Pascagoula, First Chemical, and Mississippi Phosphate 

Pascagoula, Mississippi 

October, 2005 

Analyte Activity ± 2F

Uncertainty 

MDC Unit Date 

Ba140 

Be7 

Bi212 Bi214 

Co60 

Cs137 

I131 

K40 

Pb210 Pb212 Pb214 

Ra224 Ra226 Ra228 

Tl208 

U235 

* * * *

ND 

5.55e-02 4.60e-01 3.84e-01 

ND ND ND 

1.11e+00 

ND 

4.38e-01 4.36e-01 4.03e-01 7.93e-01 4.13e-01 1.29e-01 4.98e-02 

5.8e-02 1.3e-01 3.3e-02 1.6e-01 3.3e-02 3.3e-02 2.0e-01 1.9e-01 3.9e-02 1.4e-02 1.2e-02 

8.7e-02 2.0e-02 2.0e-02 2.5e-02 

3.2e+00 

PCI/GDRY

PCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRY

10/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated. 

Analyte Activity ± 2F

Uncertainty 

MDC Unit Date 

Ra226 5.77e-01 1.0e-01 3.5e-02 PCI/GDRY 10/25/2005
Table 4 (Continued) 

Data Summary Table – Radionuclides (CFM-SD-05) 

Post - Katrina Soil and Sediment Sampling 

Chevron Refinery – Pascagoula, First Chemical, and Mississippi Phosphate 

Pascagoula, Mississippi 

October, 2005 

Analyte Activity ± 2F

Uncertainty 

MDC Unit Date 

Ba140 

Bi212 Bi214 

Co60 

Cs137 

I131 

K40 

Pb210 Pb212 Pb214 

Ra226 Ra228 Th234 

Tl208 

* * * * 

ND 

4.59e-01 4.74e-01 

ND 

4.28e-01 

ND 

2.32e+00 

ND 

4.93e-01 5.59e-01 

1.26e+00 

3.98e-01 

1.04e+00 

1.35e-01 

4.2e-01 9.8e-02 5.3e-02 6.7e-01 8.1e-02 8.3e-02 7.6e-01 1.2e-01 6.1e-01 4.9e-02 

6.3e-01 7.8e-02 3.2e-01 

9.4e+00 

PCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRY

10/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/2005

 * An asterisk indicates a result whose value may be significantly over or underestimated. 

Analyte Activity ± 2F

Uncertainty 

MDC Unit Date 

Ra226 7.35e-01 1.2e-01 1.9e-02 PCI/GDRY 10/25/2005
Table 4 (Continued) 

Data Summary Table – Radionuclides (CFM-SD-05D) 

Post - Katrina Soil and Sediment Sampling 

Chevron Refinery – Pascagoula, First Chemical, and Mississippi Phosphate 

Pascagoula, Mississippi 

October, 2005 

Analyte Activity ± 2F

Uncertainty 

MDC Unit Date 

Ba140 

Bi212 Bi214 

Co60 

Cs137 

I131 

K40 

Pb210 Pb212 Pb214 

Ra223 Ra226 Ra228 Th234 

Tl208 

U235 

* * * * *

ND 

6.80e-01 6.00e-01 

ND 

7.10e-01 

ND 

2.90e+00 

ND 

5.55e-01 7.32e-01 2.33e-01 

1.66e+00 

5.93e-01 

1.61e+00 

1.92e-01 1.13e-01 

3.4e-01 1.0e-01 6.2e-02 5.4e-01 7.3e-02 8.6e-02 1.4e-01 7.4e-01 1.2e-01 5.3e-01 4.4e-02 4.4e-02 

2.4e-01 6.1e-02 8.6e-02 

3.5e+00 

PCI/GDRY

PCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRY

10/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated. 

Analyte Activity ± 2F

Uncertainty 

MDC Unit Date 

Ra226 7.42e-01 1.2e-01 1.7e-02 PCI/GDRY 10/25/2005
Table 4 (Continued) 

Data Summary Table – Radionuclides (CFM-SD-06) 

Post - Katrina Soil and Sediment Sampling 

Chevron Refinery – Pascagoula, First Chemical, and Mississippi Phosphate 

Pascagoula, Mississippi 

October, 2005 

Analyte Activity ± 2F

Uncertainty 

MDC Unit Date 

Ba140 

Be7 

Bi212 Bi214 

Co60 

Cs137 

I131 

K40 

Pb210 Pb212 Pb214 

Ra223 Ra226 Ra228 

Tl208 

U235 

* * * *

ND 

3.53e-01 

1.17e+00 

7.05e-01 

ND 

5.36e-02 

ND 

6.28e+00 

ND 

9.39e-01 7.85e-01 2.97e-01 

1.82e+00 1.00e+00 

2.63e-01 1.14e-01 

1.7e-01 3.3e-01 7.6e-02 2.1e-02 6.0e-01 7.8e-02 7.3e-02 1.1e-01 5.8e-01 1.1e-01 3.6e-02 3.6e-02 

2.0e-01 4.5e-02 6.6e-02 

4.6e+00 

PCI/GDRY

PCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRY

10/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated. 

Analyte Activity ± 2F

Uncertainty 

MDC Unit Date 

Ra226 8.82e-01 1.4e-01 3.1e-02 PCI/GDRY 10/25/2005
Table 4 (Continued) 

Data Summary Table – Radionuclides (CFM-SD-07) 

Post - Katrina Soil and Sediment Sampling 

Chevron Refinery – Pascagoula, First Chemical, and Mississippi Phosphate 

Pascagoula, Mississippi 

October, 2005 

Analyte Activity ± 2F

Uncertainty 

MDC Unit Date 

Ba140 

Be7 

Bi212 Bi214 

Co60 

Cs137 

I131 

K40 

Pb210 Pb212 Pb214 

Ra224 Ra226 Ra228 Th234 

Tl208 

U235 

* * * *

ND 

3.12e-01 5.62e-01 3.64e-01 

ND 

6.30e-01 

ND 

2.25e+00 

ND 

5.01e-01 4.04e-01 4.95e-01 

ND 

5.57e-01 7.23e-01 1.66e-01 8.07e-02 

1.7e-01 2.8e-01 5.8e-02 4.8e-02 3.4e-01 5.4e-02 5.4e-02 3.8e-01 8.0e-02 3.6e-01 2.8e-02 2.8e-02 

1.8e-01 4.1e-02 6.2e-02 

4.9e+00 

5.9e-01 

PCI/GDRY

PCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRY

10/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/2005

 * An asterisk indicates a result whose value may be significantly over or underestimated. 

Analyte Activity ± 2F

Uncertainty 

MDC Unit Date 

Ra226 3.72e-01 6.9e-02 2.6e-02 PCI/GDRY 10/25/2005
Table 4 (Continued) 

Data Summary Table – Radionuclides (CFM-SF-08) 

Post - Katrina Soil and Sediment Sampling 

Chevron Refinery – Pascagoula, First Chemical, and Mississippi Phosphate 

Pascagoula, Mississippi 

October, 2005 

Analyte Activity ± 2F

Uncertainty 

MDC Unit Date 

Ba140 

Bi212 Bi214 

Co60 

Cs137 

I131 

K40 

Pb210 Pb212 Pb214 

Ra223 Ra226 Ra228 

Tl208 

U235 

* * * *

ND 

4.82e-01 4.57e-01 

ND 

1.60e-02 

ND 

1.04e+00 

ND 

4.38e-01 5.17e-01 1.14e-01 8.91e-01 4.66e-01 1.38e-01 5.59e-02 

2.9e-01 5.2e-02 1.3e-02 2.8e-01 4.9e-02 5.3e-02 1.1e-01 4.5e-01 6.9e-02 2.4e-02 2.8e-02 

1.5e-01 3.2e-02 5.4e-02 

3.4e+00 

PCI/GDRY

PCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRYPCI/GDRY

10/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/200510/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated. 

Analyte Activity ± 2F

Uncertainty 

MDC Unit Date 

Ra226 5.54e-01 9.7e-02 2.6e-02 PCI/GDRY 10/25/2005
Table 5 

Data Summary Table – Metals 

Post - Katrina Soil and Sediment Sampling 

Omega Protein 

Moss Point, Mississippi 

October, 2005 

OPSD01 OPSD02 OPSD02D OPSD03 

 950 900 925 1020 10/4/2005 10/4/2005 10/4/2005 10/4/2005% Moisture % 7 15 18 19Aluminum MG/KG 9500 5000 7800 4000Antimony MG/KG 0.45 J 1.6 J 7.4 UJ 7.4 Arsenic MG/KG 1.2 J 3.6 J 2.2 J 1.6 J Barium MG/KG 260 J 81 J 18 J 15 J Beryllium MG/KG 0.04 UJ 0.05 J 0.08 UJ 0.03 Calcium MG/KG 16000 J 970 J 2100 J 180 J Chromium MG/KG 10 J 39 J 10 J 8.5 J Cobalt MG/KG 3.3 J 4.1 J 1.1 J 0.41 J Copper MG/KG 45 J 46 J 6.5 J 13 J Iron MG/KG 8800 J 56000 J 10000 J 7700 J Lead MG/KG 80 J 130 J 8.8 J 17 J Magnesium MG/KG 1800 620 540 J 350 J Manganese MG/KG 54 J 350 J 46 J 8.9 J Nickel MG/KG 6.7 J 14 J 2.3 J 1.2 J Potassium MG/KG 270 J 260 J 240 J 290 J Sodium MG/KG 1400 1200 1100 1500Thallium MG/KG 0.47 R 0.54 J 3.1 U 3.1 Total Mercury MG/KG 0.03 UJ 0.12 U 0.12 U 0.15Vanadium MG/KG 18 11 16 12Zinc MG/KG 220 980 44 11

 U-Analyte not detected at or above reporting limit. 

J-Identification of analyte is acceptable; reported value is an estimate. UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate. R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data a

unusable. 
Table 5 (Continued) 

Data Summary Table – Metals 

Post - Katrina Soil and Sediment Sampling 

Omega Protein 

Moss Point, Mississippi 

October, 2005 

ER1DSD ER1SD

1430 1400

9/28/2005 9/28/2005

% Moisture % 23 20

Aluminum MG/KG 180 A 210

Barium MG/KG 1.7 A 1

Calcium MG/KG 71 A 50

Iron MG/KG 270 A 370

Lead MG/KG 2.1 A 1.3

Magnesium MG/KG 200 A 120

Manganese MG/KG 1.7 A 2.5

Sodium MG/KG 1300 A 540

Strontium MG/KG 1.5 A 1.1

Titanium MG/KG 2.6 AJ 2.8 J 

Zinc MG/KG 1.6 A 1.9

J-Identification of analyte is acceptable; reported value is an estimate. A-Analyte analyzed in replicate. Reported value is 'average' of replicates. 
Table 5 (Continued) 

Data Summary Table – Semi-Volatiles 

Post - Katrina Soil and Sediment Sampling 

Omega Protein 

Moss Point, Mississippi 

October, 2005 

OPSD01 OPSD02 OPSD02D OPS

 950 900 925 1 10/4/2005 10/4/2005 10/4/2005 10/4/2% Moisture % 6 14 19 Acenaphthylene UG/KG 160 J 380 U 410 U Acetophenone UG/KG 300 J 91 J 410 U 8Anthracene UG/KG 120 J 380 U 410 U Benzaldehyde UG/KG 350 UJ 380 UJ 410 UJ 1Benzo(a)Anthracene UG/KG 1200 380 U 410 U Benzo(b)Fluoranthene UG/KG 1600 380 U 410 U Benzo(ghi)Perylene UG/KG 750 J 380 UJ 410 UJ Benzo(k)Fluoranthene UG/KG 890 380 U 410 U Benzo-a-Pyrene UG/KG 1300 380 U 410 U Chrysene UG/KG 1200 380 U 410 U Dibenzo(a,h)Anthracene UG/KG 360 J 380 UJ 410 UJ Dimethyl Phthalate UG/KG 350 U 570 410 U Fluoranthene UG/KG 1900 380 U 410 U Indeno (1,2,3-cd) Pyrene UG/KG 1100 J 380 UJ 410 UJ Phenanthrene UG/KG 140 J 380 U 410 U Phenol UG/KG 350 U 380 U 410 U 11Pyrene UG/KG 2000 380 U 410 U 

 U-Analyte not detected at or above reporting limit. 

J-Identification of analyte is acceptable; reported value is an estimate. UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate. 
Table 5 (Continued) 

Data Summary Table – Pesticides/PCBs 

Post - Katrina Soil and Sediment Sampling 

Omega Protein 

Moss Point, Mississippi 

October, 2005 

OPSD01 OPSD02 OPSD02D OPSD

 950 900 925 10 10/4/2005 10/4/2005 10/4/2005 10/4/20% Moisture % 6 14 19 4,4'-DDE (p,p'-DDE) UG/KG 3.5 U 3.8 U 4.1 U 4,4'-DDT (p,p'-DDT) UG/KG 1.4 J 3.8 U 4.1 U alpha-Chlordane /2 UG/KG 1.7 NJ 2 U 2.1 U Dieldrin UG/KG 3.5 U 3.8 U 4.1 U Endrin Ketone UG/KG 3.5 U 3.8 U 2 NJ gamma-Chlordane /2 UG/KG 1.8 U 2 U 2.1 U Methoxychlor UG/KG 8 NJ 20 U 21 U PCB-1260 (Aroclor 1260) UG/KG 35 U 21 J 41 U 

 U-Analyte not detected at or above reporting limit. 

J-Identification of analyte is acceptable; reported value is an estimate. NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estiN-Presumptive evidence analyte is present; analyte reported as tentative identification. /2-constituents or metabolites of technical chlordane 
Table 6 

Data Summary Table – Metals 

Post - Katrina Soil and Sediment Sampling 

Polychemie, Inc. 

Pearlington, Mississippi 

October, 2005 

POSD01 POSD01D POSD02 POSD03 POSF04 PO

 1225 1240 1320 1320 1250  10/3/2005 10/3/2005 10/3/2005 10/3/2005 10/3/2005 10/3% Moisture % 80 79 64 26 14 Aluminum MG/KG 15000 11000 9300 1900 2600 Arsenic MG/KG 18 J 9 J 7.7 J 1 J 0.41 R Barium MG/KG 52 J 79 J 160 J 390 J 15 J Cadmium MG/KG 2.5 U 2.3 U 1.4 U 0.92 0.58 U Calcium MG/KG 2300 J 2200 J 1900 J 11000 J 2000 J Chromium MG/KG 19 J 14 J 13 J 3.6 J 2.7 J Cobalt MG/KG 5.3 J 7.8 J 7.4 J 1.2 J 0.49 J Copper MG/KG 14 J 16 J 14 J 2.9 J 2 J Iron MG/KG 41000 J 23000 J 18000 J 3500 J 1900 J Lead MG/KG 26 J 17 J 14 J 8.8 J 6.6 J Magnesium MG/KG 3400 3400 3600 460 J 160 J Manganese MG/KG 190 J 260 J 380 J 160 J 21 J Nickel MG/KG 8.1 J 9.7 J 12 J 1.6 J 1.2 J Potassium MG/KG 1400 J 1500 J 1900 200 J 89 J Selenium MG/KG 17 U 16 U 9.8 U 4.7 U 4.1 U Sodium MG/KG 9600 9400 8100 830 530 J Vanadium MG/KG 38 28 25 4.3 J 4.6 J Zinc MG/KG 85 110 74 83 21 

 U-Analyte not detected at or above reporting limit. 

J-Identification of analyte is acceptable; reported value is an estimate. R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data a

unusable. 
Table 6 (Continued) 

Data Summary Table – Semi-volatile Organic Compounds 

Post - Katrina Soil and Sediment Sampling 

Polychemie, Inc. 

Pearlington, Mississippi 

October, 2005 

POSD01 POSD01D POSD02 POSD03 POSF04 

 1225 1240 1320 1320 1250  10/3/2005 10/3/2005 10/3/2005 10/3/2005 10/3/2005 % Moisture % 78 80 58 17 12 Benzo(a)Anthracene UG/KG 1500 U 1700 U 790 U 220 J 380 U Benzo(b)Fluoranthene UG/KG 1500 U 1700 U 790 U 210 J 380 U Benzo(ghi)Perylene UG/KG 1500 UJ 1700 UJ 790 UJ 120 J 380 UJ Benzo(k)Fluoranthene UG/KG 1500 U 1700 U 790 U 230 J 380 U Benzo-a-Pyrene UG/KG 1500 U 1700 U 790 U 200 J 380 U Chrysene UG/KG 1500 U 1700 U 790 U 280 J 380 U Fluoranthene UG/KG 1500 U 1700 U 790 U 400 380 U Indeno (1,2,3-cd) Pyrene UG/KG 1500 U 1700 U 790 U 150 J 380 U Phenanthrene UG/KG 1500 U 1700 U 790 U 180 J 380 U Pyrene UG/KG 1500 U 1700 U 790 U 370 J 380 U 

U-Analyte not detected at or above reporting limit. J-Identification of analyte is acceptable; reported value is an estimate. UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate. 
Table 6 (Continued) 

Data Summary Table – Pesticides/PCBs 

Post - Katrina Soil and Sediment Sampling 

Polychemie, Inc. 

Pearlington, Mississippi 

October, 2005 

POSD01 POSD01D POSD02 POSD03 POSF04 P

 1225 1240 1320 1320 1250  10/3/2005 10/3/2005 10/3/2005 10/3/2005 10/3/2005 10% Moisture % 78 80 58 17 12 gamma-Chlordane /2 UG/KG 7.7 U 8.5 U 4 U 2 U 0.86 J 

U-Analyte not detected at or above reporting limit. J-Identification of analyte is acceptable; reported value is an estimate. /2-constituents or metabolites of technical chlordane 
Table 6 (Continued) 

Data Summary Table – Volatile Organic Compounds 

Post - Katrina Soil and Sediment Sampling 

Polychemie, Inc. 

Pearlington, Mississippi 

October, 2005 

POSD01 POSD01D POSD02 POSD03 POSF04 POSF

 1225 1240 1320 1320 1250 12 10/3/2005 10/3/2005 10/3/2005 10/3/2005 10/3/2005 10/3/20% Moisture % 78 80 58 17 12 Acetone UG/KG 96 U 140 32 U 11 U 10 UJ 

 U-Analyte not detected at or above reporting limit. 

UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate. 
Table 7 

Data Summary Table – Metals 

Post - Katrina Soil and Sediment Sampling 

Ershigs Fiberglass 

Biloxi, Mississippi 

October, 2005 

ERSF01 ERSF01S ERSF02 ERSF03 ERSD04 ERSD0

 915 915 1010 1050 1115 1 10/4/2005 10/4/2005 10/4/2005 10/4/2005 10/4/2005 10/4/2% Moisture % 45 38 9 20 49 Aluminum MG/KG 4100 5300 2600 3000 15000 3Antimony MG/KG 0.4 R 0.48 R 6.6 UJ 7.5 UJ 0.71 R 0Arsenic MG/KG 2.2 J 2.3 J 2.7 J 1.3 J 14 J Barium MG/KG 75 J 52 J 24 J 29 J 180 J Cadmium MG/KG 0.27 J 0.81 U 0.55 U 0.63 U 0.98 U 0Calcium MG/KG 19000 J 14000 J 1500 J 5900 J 3200 J 12Chromium MG/KG 8.1 J 8.7 J 3.9 J 5.9 J 16 J Cobalt MG/KG 1.5 J 1.4 J 0.47 J 0.83 J 2.5 J Copper MG/KG 48 J 32 J 11 J 9.9 J 39 J Iron MG/KG 6800 J 6500 J 2600 J 3300 J 11000 J 5Lead MG/KG 48 J 34 J 71 J 44 J 26 J Magnesium MG/KG 830 J 770 J 330 UJ 610 J 1700 2Manganese MG/KG 120 J 82 J 35 J 74 J 210 J Nickel MG/KG 4 J 3.9 J 1.4 J 4.8 J 5 J Potassium MG/KG 340 J 370 J 150 J 280 J 700 J Sodium MG/KG 1800 1400 730 900 2500 1Vanadium MG/KG 8.8 J 11 4.5 J 5.8 J 23 Zinc MG/KG 1200 580 93 78 110 

U-Analyte not detected at or above reporting limit. J-Identification of analyte is acceptable; reported value is an estimate. UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate. R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data aunusable. 
Table 7 (Continued) 

Data Summary Table – Semi-Volatile Organic Compounds 

Post - Katrina Soil and Sediment Sampling 

Ershigs Fiberglass 

Biloxi, Mississippi 

October, 2005 

ERSF01 ERSF01S ERSF02 ERSF03 ERSD04 

 915 915 1010 1050 1115  10/4/2005 10/4/2005 10/4/2005 10/4/2005 10/4/2005 % Moisture % 36 36 9 18 45 Acetophenone UG/KG 170 J 520 U 360 U 400 U 300 J Benzo(a)Anthracene UG/KG 520 U 520 U 360 U 400 U 600 U Benzo(b)Fluoranthene UG/KG 520 U 520 U 360 U 87 J 600 U Benzo(ghi)Perylene UG/KG 520 UJ 520 UJ 360 UJ 400 UJ 600 UJ Benzo(k)Fluoranthene UG/KG 520 U 520 U 80 J 400 U 600 U Benzo-a-Pyrene UG/KG 520 U 520 U 360 U 400 U 600 U bis(2-Ethylhexyl) Phthalate UG/KG 860 U 1200 U 360 U 400 U 600 U Chrysene UG/KG 520 U 520 U 81 J 400 U 600 U Fluoranthene UG/KG 520 U 520 U 110 J 100 J 600 U Indeno (1,2,3-cd) Pyrene UG/KG 520 UJ 520 UJ 360 UJ 400 UJ 600 UJ Phenanthrene UG/KG 520 U 520 U 360 U 400 U 600 U Pyrene UG/KG 520 U 520 U 150 J 96 J 600 U 

U-Analyte not detected at or above reporting limit. J-Identification of analyte is acceptable; reported value is an estimate. UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate. 
Table 7 (Continued) 

Data Summary Table – Pesticides/PCBs 

Post - Katrina Soil and Sediment Sampling 

Ershigs Fiberglass 

Biloxi, Mississippi 

October, 2005 

ERSF01 ERSF01S ERSF02 ERSF03 ERSD04 

 915 915 1010 1050 1115  10/4/2005 10/4/2005 10/4/2005 10/4/2005 10/4/2005 % Moisture % 36 36 9 18 45 4,4'-DDD (p,p'-DDD) UG/KG 5.2 UJ 5.2 UJ 3.6 UJ 4 UJ 3.3 NJ 4,4'-DDE (p,p'-DDE) UG/KG 5.2 U 1.1 NJ 6.3 5.6 6.5 4,4'-DDT (p,p'-DDT) UG/KG 5.2 U 5.2 U 6.2 N 9.9 12 Aldrin UG/KG 2.7 U 2.7 U 1.9 U 0.91 NJ 15 N alpha-Chlordane /2 UG/KG 2.7 U 3 U 17 U 18 U 24 N Dieldrin UG/KG 5.2 U 1.3 J 7.2 9.4 12 Endosulfan Sulfate UG/KG 5.2 U 1.2 J 3.6 U 4 U 6 U gamma-Chlordane /2 UG/KG 2.7 U 3.5 N 11 N 19 N 23 N Methoxychlor UG/KG 27 U 27 U 19 U 21 U 31 U 

U-Analyte not detected at or above reporting limit. J-Identification of analyte is acceptable; reported value is an estimate. UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate. N-Presumptive evidence analyte is present; analyte reported as tentative identification. NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an esti/2-constituents or metabolites of technical chlordane. 
Table 8 

Data Summary Table – Volatile Trip Blanks 

Post - Katrina Soil and Sediment Sampling 

Ershigs Fiberglass 

Biloxi, Mississippi 

October, 2005 

POTB901 TB902 TB903 TB904 

 1521 1229 1426 1427 10/3/2005 10/4/2005 10/6/2005 10/6/2005% Moisture % 0 0 0 0Acetone UG/KG 11 14 UJ 17 14

UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate. 
86

Appendix C 

Laboratory Data Sheets 
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9518 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 10:35

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AJ4 D No: 3AJ4 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSF08 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

350 U UG/KG Benzaldehyde 350 U UG/KG Dibenzofuran350 U UG/KG Phenol 350 U UG/KG 2,4-Dinitrotoluene350 U UG/KG bis(2-Chloroethyl) Ether 350 U UG/KG Diethyl Phthalate350 U UG/KG 2-Chlorophenol 350 U UG/KG Fluorene350 U UG/KG 2-Methylphenol 350 U UG/KG 4-Chlorophenyl Phenyl E350 U UG/KG bis(2-Chloroisopropyl) Ether 880 U UG/KG 4-Nitroaniline350 U UG/KG Acetophenone 880 U UG/KG 2-Methyl-4,6-Dinitrophen350 U UG/KG (3-and/or 4-)Methylphenol 350 U UG/KG n-Nitrosodiphenylamine/350 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze350 U UG/KG Hexachloroethane 350 UJ UG/KG 4-Bromophenyl Phenyl E350 U UG/KG Nitrobenzene 350 UJ UG/KG Hexachlorobenzene (HC350 U UG/KG Isophorone 350 U UG/KG Atrazine350 U UG/KG 2-Nitrophenol 880 U UG/KG Pentachlorophenol350 U UG/KG 2,4-Dimethylphenol 350 U UG/KG Phenanthrene350 U UG/KG bis(2-Chloroethoxy)Methane 350 U UG/KG Anthracene350 U UG/KG 2,4-Dichlorophenol 350 U UG/KG Carbazole350 U UG/KG Naphthalene 350 U UG/KG Di-n-Butylphthalate350 U UG/KG 4-Chloroaniline 350 U UG/KG Fluoranthene350 U UG/KG Hexachlorobutadiene 350 U UG/KG Pyrene350 U UG/KG Caprolactam 350 U UG/KG Benzyl Butyl Phthalate350 U UG/KG 4-Chloro-3-Methylphenol 350 U UG/KG 3,3'-Dichlorobenzidine350 U UG/KG 2-Methylnaphthalene 350 U UG/KG Benzo(a)Anthracene350 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 350 U UG/KG Chrysene350 U UG/KG 2,4,6-Trichlorophenol 350 U UG/KG bis(2-Ethylhexyl) Phthala880 U UG/KG 2,4,5-Trichlorophenol 350 U UG/KG Di-n-Octylphthalate350 U UG/KG 1,1-Biphenyl 350 U UG/KG Benzo(b)Fluoranthene350 U UG/KG 2-Chloronaphthalene 350 U UG/KG Benzo(k)Fluoranthene880 U UG/KG 2-Nitroaniline 350 U UG/KG Benzo-a-Pyrene350 U UG/KG Dimethyl Phthalate 350 U UG/KG Indeno (1,2,3-cd) Pyrene350 U UG/KG 2,6-Dinitrotoluene 350 U UG/KG Dibenzo(a,h)Anthracene350 U UG/KG Acenaphthylene 350 U UG/KG Benzo(ghi)Perylene880 U UG/KG 3-Nitroaniline 6 % % Moisture350 U UG/KG Acenaphthene880 U UG/KG 2,4-Dinitrophenol880 U UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9518 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 10:35

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ4 D No: 3AJ4 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSF08 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

4200 J UG/KG 22 UNKNOWNS

89 J UG/KG SUBSTITUTED PHENANTHRENE CARBOXYLIC ACID

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9519 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 11:15

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AJ5 D No: 3AJ5 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD07 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

550 U UG/KG Benzaldehyde 550 U UG/KG Dibenzofuran550 U UG/KG Phenol 550 U UG/KG 2,4-Dinitrotoluene550 U UG/KG bis(2-Chloroethyl) Ether 550 U UG/KG Diethyl Phthalate550 U UG/KG 2-Chlorophenol 550 U UG/KG Fluorene550 U UG/KG 2-Methylphenol 550 U UG/KG 4-Chlorophenyl Phenyl E550 U UG/KG bis(2-Chloroisopropyl) Ether 1400 U UG/KG 4-Nitroaniline550 U UG/KG Acetophenone 1400 U UG/KG 2-Methyl-4,6-Dinitrophen550 U UG/KG (3-and/or 4-)Methylphenol 550 U UG/KG n-Nitrosodiphenylamine/550 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze550 U UG/KG Hexachloroethane 550 UJ UG/KG 4-Bromophenyl Phenyl E550 U UG/KG Nitrobenzene 550 UJ UG/KG Hexachlorobenzene (HC550 U UG/KG Isophorone 550 U UG/KG Atrazine550 U UG/KG 2-Nitrophenol 1400 U UG/KG Pentachlorophenol550 U UG/KG 2,4-Dimethylphenol 550 U UG/KG Phenanthrene550 U UG/KG bis(2-Chloroethoxy)Methane 550 U UG/KG Anthracene550 U UG/KG 2,4-Dichlorophenol 550 U UG/KG Carbazole550 U UG/KG Naphthalene 550 U UG/KG Di-n-Butylphthalate550 U UG/KG 4-Chloroaniline 550 U UG/KG Fluoranthene550 U UG/KG Hexachlorobutadiene 550 U UG/KG Pyrene550 U UG/KG Caprolactam 550 U UG/KG Benzyl Butyl Phthalate550 U UG/KG 4-Chloro-3-Methylphenol 550 U UG/KG 3,3'-Dichlorobenzidine550 U UG/KG 2-Methylnaphthalene 550 U UG/KG Benzo(a)Anthracene550 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 550 U UG/KG Chrysene550 U UG/KG 2,4,6-Trichlorophenol 550 U UG/KG bis(2-Ethylhexyl) Phthala

1400 U UG/KG 2,4,5-Trichlorophenol 550 U UG/KG Di-n-Octylphthalate

550 U UG/KG 1,1-Biphenyl 550 U UG/KG Benzo(b)Fluoranthene550 U UG/KG 2-Chloronaphthalene 550 U UG/KG Benzo(k)Fluoranthene

1400 U UG/KG 2-Nitroaniline 550 U UG/KG Benzo-a-Pyrene

550 U UG/KG Dimethyl Phthalate 550 U UG/KG Indeno (1,2,3-cd) Pyrene550 U UG/KG 2,6-Dinitrotoluene 550 U UG/KG Dibenzo(a,h)Anthracene550 U UG/KG Acenaphthylene 550 U UG/KG Benzo(ghi)Perylene

1400 U UG/KG 3-Nitroaniline 40 % % Moisture

550 U UG/KG Acenaphthene

1400 U UG/KG 2,4-Dinitrophenol1400 U UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9519 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 11:15

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ5 D No: 3AJ5 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD07 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

8700 J UG/KG 24 UNKNOWNS

550 NJ UG/KG EUCALYPTOL210 NJ UG/KG CARYOPHYLLENE210 NJ UG/KG HEXADECANOIC ACID, METHYL ESTER210 NJ UG/KG N-HEXADECANOIC ACID

1000 NJ UG/KG STIGMASTEROL, 22,23-DIHYDRO1200 NJ UG/KG STIGMAST-4-EN-3-ONE

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9520 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 11:30

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AJ6 D No: 3AJ6 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSF02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

430 U UG/KG Benzaldehyde 430 U UG/KG Dibenzofuran430 U UG/KG Phenol 430 U UG/KG 2,4-Dinitrotoluene430 U UG/KG bis(2-Chloroethyl) Ether 430 U UG/KG Diethyl Phthalate430 U UG/KG 2-Chlorophenol 430 U UG/KG Fluorene430 U UG/KG 2-Methylphenol 430 U UG/KG 4-Chlorophenyl Phenyl E430 U UG/KG bis(2-Chloroisopropyl) Ether 1100 U UG/KG 4-Nitroaniline430 U UG/KG Acetophenone 1100 U UG/KG 2-Methyl-4,6-Dinitrophen430 U UG/KG (3-and/or 4-)Methylphenol 430 U UG/KG n-Nitrosodiphenylamine/430 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze430 U UG/KG Hexachloroethane 430 UJ UG/KG 4-Bromophenyl Phenyl E430 U UG/KG Nitrobenzene 430 UJ UG/KG Hexachlorobenzene (HC430 U UG/KG Isophorone 430 U UG/KG Atrazine430 U UG/KG 2-Nitrophenol 1100 U UG/KG Pentachlorophenol430 U UG/KG 2,4-Dimethylphenol 430 U UG/KG Phenanthrene430 U UG/KG bis(2-Chloroethoxy)Methane 430 U UG/KG Anthracene430 U UG/KG 2,4-Dichlorophenol 430 U UG/KG Carbazole430 U UG/KG Naphthalene 430 U UG/KG Di-n-Butylphthalate430 U UG/KG 4-Chloroaniline 430 U UG/KG Fluoranthene430 U UG/KG Hexachlorobutadiene 430 U UG/KG Pyrene430 U UG/KG Caprolactam 430 U UG/KG Benzyl Butyl Phthalate430 U UG/KG 4-Chloro-3-Methylphenol 430 U UG/KG 3,3'-Dichlorobenzidine430 U UG/KG 2-Methylnaphthalene 430 U UG/KG Benzo(a)Anthracene430 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 430 U UG/KG Chrysene430 U UG/KG 2,4,6-Trichlorophenol 430 U UG/KG bis(2-Ethylhexyl) Phthala

1100 U UG/KG 2,4,5-Trichlorophenol 430 U UG/KG Di-n-Octylphthalate

430 U UG/KG 1,1-Biphenyl 430 U UG/KG Benzo(b)Fluoranthene430 U UG/KG 2-Chloronaphthalene 430 U UG/KG Benzo(k)Fluoranthene

1100 U UG/KG 2-Nitroaniline 430 U UG/KG Benzo-a-Pyrene

430 U UG/KG Dimethyl Phthalate 430 U UG/KG Indeno (1,2,3-cd) Pyrene430 U UG/KG 2,6-Dinitrotoluene 430 U UG/KG Dibenzo(a,h)Anthracene430 U UG/KG Acenaphthylene 430 U UG/KG Benzo(ghi)Perylene

1100 U UG/KG 3-Nitroaniline 23 % % Moisture

430 U UG/KG Acenaphthene

1100 U UG/KG 2,4-Dinitrophenol1100 U UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9520 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 11:30

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ6 D No: 3AJ6 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSF02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

1400 J UG/KG 8 UNKNOWNS

340 NJ UG/KG .GAMMA.-SITOSTEROL800 NJ UG/KG A'-NEOGAMMACER-22(29)-EN-3-ONE

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9521 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 11:30

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AJ7 D No: 3AJ7 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSF02S / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

420 U UG/KG Benzaldehyde 420 U UG/KG Dibenzofuran420 U UG/KG Phenol 420 U UG/KG 2,4-Dinitrotoluene420 U UG/KG bis(2-Chloroethyl) Ether 420 U UG/KG Diethyl Phthalate420 U UG/KG 2-Chlorophenol 420 U UG/KG Fluorene420 U UG/KG 2-Methylphenol 420 U UG/KG 4-Chlorophenyl Phenyl E420 U UG/KG bis(2-Chloroisopropyl) Ether 1100 U UG/KG 4-Nitroaniline420 U UG/KG Acetophenone 1100 U UG/KG 2-Methyl-4,6-Dinitrophen420 U UG/KG (3-and/or 4-)Methylphenol 420 U UG/KG n-Nitrosodiphenylamine/420 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze420 U UG/KG Hexachloroethane 420 UJ UG/KG 4-Bromophenyl Phenyl E420 U UG/KG Nitrobenzene 420 UJ UG/KG Hexachlorobenzene (HC420 U UG/KG Isophorone 420 U UG/KG Atrazine420 U UG/KG 2-Nitrophenol 1100 U UG/KG Pentachlorophenol420 U UG/KG 2,4-Dimethylphenol 420 U UG/KG Phenanthrene420 U UG/KG bis(2-Chloroethoxy)Methane 420 U UG/KG Anthracene420 U UG/KG 2,4-Dichlorophenol 420 U UG/KG Carbazole420 U UG/KG Naphthalene 420 U UG/KG Di-n-Butylphthalate420 U UG/KG 4-Chloroaniline 420 U UG/KG Fluoranthene420 U UG/KG Hexachlorobutadiene 420 U UG/KG Pyrene420 U UG/KG Caprolactam 420 U UG/KG Benzyl Butyl Phthalate420 U UG/KG 4-Chloro-3-Methylphenol 420 U UG/KG 3,3'-Dichlorobenzidine420 U UG/KG 2-Methylnaphthalene 420 U UG/KG Benzo(a)Anthracene420 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 420 U UG/KG Chrysene420 U UG/KG 2,4,6-Trichlorophenol 420 U UG/KG bis(2-Ethylhexyl) Phthala

1100 U UG/KG 2,4,5-Trichlorophenol 420 U UG/KG Di-n-Octylphthalate

420 U UG/KG 1,1-Biphenyl 420 U UG/KG Benzo(b)Fluoranthene420 U UG/KG 2-Chloronaphthalene 420 U UG/KG Benzo(k)Fluoranthene

1100 U UG/KG 2-Nitroaniline 420 U UG/KG Benzo-a-Pyrene

420 U UG/KG Dimethyl Phthalate 420 U UG/KG Indeno (1,2,3-cd) Pyrene420 U UG/KG 2,6-Dinitrotoluene 420 U UG/KG Dibenzo(a,h)Anthracene420 U UG/KG Acenaphthylene 420 U UG/KG Benzo(ghi)Perylene

1100 U UG/KG 3-Nitroaniline 21 % % Moisture

420 U UG/KG Acenaphthene

1100 U UG/KG 2,4-Dinitrophenol1100 U UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9521 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 11:30

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ7 D No: 3AJ7 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSF02S / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

5300 J UG/KG 21 UNKNOWNS

100 NJ UG/KG SUBSTITUTED PHENANTHRENECARBOXYLIC ACID770 NJ UG/KG .GAMMA.-SITOSTEROL460 NJ UG/KG 2,5 -HEXANEDIONE

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9522 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 10:55

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AJ8 D No: 3AJ8 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSF01 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

360 U UG/KG Benzaldehyde 360 U UG/KG Dibenzofuran360 U UG/KG Phenol 360 U UG/KG 2,4-Dinitrotoluene360 U UG/KG bis(2-Chloroethyl) Ether 360 U UG/KG Diethyl Phthalate360 U UG/KG 2-Chlorophenol 360 U UG/KG Fluorene360 U UG/KG 2-Methylphenol 360 U UG/KG 4-Chlorophenyl Phenyl E360 U UG/KG bis(2-Chloroisopropyl) Ether 910 U UG/KG 4-Nitroaniline360 U UG/KG Acetophenone 910 U UG/KG 2-Methyl-4,6-Dinitrophen360 U UG/KG (3-and/or 4-)Methylphenol 360 U UG/KG n-Nitrosodiphenylamine/360 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze360 U UG/KG Hexachloroethane 360 UJ UG/KG 4-Bromophenyl Phenyl E360 U UG/KG Nitrobenzene 360 UJ UG/KG Hexachlorobenzene (HC360 U UG/KG Isophorone 360 U UG/KG Atrazine360 U UG/KG 2-Nitrophenol 910 U UG/KG Pentachlorophenol360 U UG/KG 2,4-Dimethylphenol 360 U UG/KG Phenanthrene360 U UG/KG bis(2-Chloroethoxy)Methane 360 U UG/KG Anthracene360 U UG/KG 2,4-Dichlorophenol 360 U UG/KG Carbazole360 U UG/KG Naphthalene 360 U UG/KG Di-n-Butylphthalate360 U UG/KG 4-Chloroaniline 360 U UG/KG Fluoranthene360 U UG/KG Hexachlorobutadiene 360 U UG/KG Pyrene360 U UG/KG Caprolactam 360 U UG/KG Benzyl Butyl Phthalate360 U UG/KG 4-Chloro-3-Methylphenol 360 U UG/KG 3,3'-Dichlorobenzidine360 U UG/KG 2-Methylnaphthalene 360 U UG/KG Benzo(a)Anthracene360 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 360 U UG/KG Chrysene360 U UG/KG 2,4,6-Trichlorophenol 360 U UG/KG bis(2-Ethylhexyl) Phthala910 U UG/KG 2,4,5-Trichlorophenol 360 U UG/KG Di-n-Octylphthalate360 U UG/KG 1,1-Biphenyl 360 U UG/KG Benzo(b)Fluoranthene360 U UG/KG 2-Chloronaphthalene 360 U UG/KG Benzo(k)Fluoranthene910 U UG/KG 2-Nitroaniline 360 U UG/KG Benzo-a-Pyrene360 U UG/KG Dimethyl Phthalate 360 U UG/KG Indeno (1,2,3-cd) Pyrene360 U UG/KG 2,6-Dinitrotoluene 360 U UG/KG Dibenzo(a,h)Anthracene360 U UG/KG Acenaphthylene 360 U UG/KG Benzo(ghi)Perylene910 U UG/KG 3-Nitroaniline 9 % % Moisture360 U UG/KG Acenaphthene910 U UG/KG 2,4-Dinitrophenol910 U UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9522 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 10:55

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ8 D No: 3AJ8 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSF01 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

1900 J UG/KG 12 UNKNOWNS

81 NJ UG/KG 1-(10-METHYLANTHRACEN-9-YL)ETHANONE

390 NJ UG/KG 1-NAPHTHALENECARBOXYLIC ACID, DECAHYDRO-

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9523 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 11:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AJ9 D No: 3AJ9 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD06 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

670 U UG/KG Benzaldehyde 670 U UG/KG Dibenzofuran670 U UG/KG Phenol 670 U UG/KG 2,4-Dinitrotoluene670 U UG/KG bis(2-Chloroethyl) Ether 670 U UG/KG Diethyl Phthalate670 U UG/KG 2-Chlorophenol 670 U UG/KG Fluorene670 U UG/KG 2-Methylphenol 670 U UG/KG 4-Chlorophenyl Phenyl E670 U UG/KG bis(2-Chloroisopropyl) Ether 1700 U UG/KG 4-Nitroaniline670 U UG/KG Acetophenone 1700 U UG/KG 2-Methyl-4,6-Dinitrophen670 U UG/KG (3-and/or 4-)Methylphenol 670 U UG/KG n-Nitrosodiphenylamine/670 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze670 U UG/KG Hexachloroethane 670 UJ UG/KG 4-Bromophenyl Phenyl E670 U UG/KG Nitrobenzene 670 UJ UG/KG Hexachlorobenzene (HC670 U UG/KG Isophorone 670 U UG/KG Atrazine670 U UG/KG 2-Nitrophenol 1700 U UG/KG Pentachlorophenol670 U UG/KG 2,4-Dimethylphenol 670 U UG/KG Phenanthrene670 U UG/KG bis(2-Chloroethoxy)Methane 670 U UG/KG Anthracene670 U UG/KG 2,4-Dichlorophenol 670 U UG/KG Carbazole670 U UG/KG Naphthalene 670 U UG/KG Di-n-Butylphthalate670 U UG/KG 4-Chloroaniline 670 U UG/KG Fluoranthene670 U UG/KG Hexachlorobutadiene 670 U UG/KG Pyrene670 U UG/KG Caprolactam 670 U UG/KG Benzyl Butyl Phthalate670 U UG/KG 4-Chloro-3-Methylphenol 670 U UG/KG 3,3'-Dichlorobenzidine670 U UG/KG 2-Methylnaphthalene 670 U UG/KG Benzo(a)Anthracene670 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 670 U UG/KG Chrysene670 U UG/KG 2,4,6-Trichlorophenol 670 U UG/KG bis(2-Ethylhexyl) Phthala

1700 U UG/KG 2,4,5-Trichlorophenol 670 U UG/KG Di-n-Octylphthalate

670 U UG/KG 1,1-Biphenyl 670 U UG/KG Benzo(b)Fluoranthene670 U UG/KG 2-Chloronaphthalene 670 U UG/KG Benzo(k)Fluoranthene

1700 U UG/KG 2-Nitroaniline 670 U UG/KG Benzo-a-Pyrene

670 U UG/KG Dimethyl Phthalate 670 U UG/KG Indeno (1,2,3-cd) Pyrene670 U UG/KG 2,6-Dinitrotoluene 670 U UG/KG Dibenzo(a,h)Anthracene670 U UG/KG Acenaphthylene 670 U UG/KG Benzo(ghi)Perylene

1700 U UG/KG 3-Nitroaniline 51 % % Moisture

670 U UG/KG Acenaphthene

1700 U UG/KG 2,4-Dinitrophenol1700 U UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9523 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 11:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ9 D No: 3AJ9 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD06 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

15000 J UG/KG 17 UNKNOWNS

310 NJ UG/KG N-HEXADECANOIC ACID280 NJ UG/KG SQUALENE

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9524 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 12:35

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AK0 D No: 3AK0 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD05 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

1400 U UG/KG Benzaldehyde 1400 U UG/KG Dibenzofuran1400 U UG/KG Phenol 1400 U UG/KG 2,4-Dinitrotoluene1400 U UG/KG bis(2-Chloroethyl) Ether 1400 U UG/KG Diethyl Phthalate1400 U UG/KG 2-Chlorophenol 1400 U UG/KG Fluorene1400 U UG/KG 2-Methylphenol 1400 U UG/KG 4-Chlorophenyl Phenyl E1400 U UG/KG bis(2-Chloroisopropyl) Ether 3600 U UG/KG 4-Nitroaniline1400 U UG/KG Acetophenone 3600 U UG/KG 2-Methyl-4,6-Dinitrophen1400 U UG/KG (3-and/or 4-)Methylphenol 1400 U UG/KG n-Nitrosodiphenylamine/1400 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze1400 U UG/KG Hexachloroethane 1400 UJ UG/KG 4-Bromophenyl Phenyl E1400 U UG/KG Nitrobenzene 1400 UJ UG/KG Hexachlorobenzene (HC1400 U UG/KG Isophorone 1400 U UG/KG Atrazine1400 U UG/KG 2-Nitrophenol 3600 U UG/KG Pentachlorophenol1400 U UG/KG 2,4-Dimethylphenol 1400 U UG/KG Phenanthrene1400 U UG/KG bis(2-Chloroethoxy)Methane 1400 U UG/KG Anthracene1400 U UG/KG 2,4-Dichlorophenol 1400 U UG/KG Carbazole1400 U UG/KG Naphthalene 1400 U UG/KG Di-n-Butylphthalate1400 U UG/KG 4-Chloroaniline 1400 U UG/KG Fluoranthene1400 U UG/KG Hexachlorobutadiene 1400 U UG/KG Pyrene1400 U UG/KG Caprolactam 1400 U UG/KG Benzyl Butyl Phthalate1400 U UG/KG 4-Chloro-3-Methylphenol 1400 U UG/KG 3,3'-Dichlorobenzidine1400 U UG/KG 2-Methylnaphthalene 1400 U UG/KG Benzo(a)Anthracene1400 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 1400 U UG/KG Chrysene1400 U UG/KG 2,4,6-Trichlorophenol 1400 U UG/KG bis(2-Ethylhexyl) Phthala3600 U UG/KG 2,4,5-Trichlorophenol 1400 U UG/KG Di-n-Octylphthalate1400 U UG/KG 1,1-Biphenyl 1400 U UG/KG Benzo(b)Fluoranthene1400 U UG/KG 2-Chloronaphthalene 1400 U UG/KG Benzo(k)Fluoranthene3600 U UG/KG 2-Nitroaniline 1400 U UG/KG Benzo-a-Pyrene1400 U UG/KG Dimethyl Phthalate 1400 U UG/KG Indeno (1,2,3-cd) Pyrene1400 U UG/KG 2,6-Dinitrotoluene 1400 U UG/KG Dibenzo(a,h)Anthracene1400 U UG/KG Acenaphthylene 1400 U UG/KG Benzo(ghi)Perylene3600 U UG/KG 3-Nitroaniline 77 % % Moisture1400 U UG/KG Acenaphthene3600 U UG/KG 2,4-Dinitrophenol3600 U UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9524 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 12:35

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AK0 D No: 3AK0 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD05 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

870 NJ UG/KG BICYCLO [3.1.1] HEPTANE, 6,6,DIMETHYL-2-METHYL74000 J UG/KG 26 UNKNOWNS

1600 NJ UG/KG N-HEXADECANOIC ACID5300 NJ UG/KG STIGMAST-4-EN-3-ONE

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9525 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 12:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AK1 D No: 3AK1 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD05D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

1200 U UG/KG Benzaldehyde 1200 U UG/KG Dibenzofuran1200 U UG/KG Phenol 1200 U UG/KG 2,4-Dinitrotoluene1200 U UG/KG bis(2-Chloroethyl) Ether 1200 U UG/KG Diethyl Phthalate1200 U UG/KG 2-Chlorophenol 1200 U UG/KG Fluorene1200 U UG/KG 2-Methylphenol 1200 U UG/KG 4-Chlorophenyl Phenyl E1200 U UG/KG bis(2-Chloroisopropyl) Ether 3100 U UG/KG 4-Nitroaniline1200 U UG/KG Acetophenone 3100 U UG/KG 2-Methyl-4,6-Dinitrophen1200 U UG/KG (3-and/or 4-)Methylphenol 1200 U UG/KG n-Nitrosodiphenylamine/1200 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze1200 U UG/KG Hexachloroethane 1200 UJ UG/KG 4-Bromophenyl Phenyl E1200 U UG/KG Nitrobenzene 1200 UJ UG/KG Hexachlorobenzene (HC1200 U UG/KG Isophorone 1200 U UG/KG Atrazine1200 U UG/KG 2-Nitrophenol 3100 U UG/KG Pentachlorophenol1200 U UG/KG 2,4-Dimethylphenol 1200 U UG/KG Phenanthrene1200 U UG/KG bis(2-Chloroethoxy)Methane 1200 U UG/KG Anthracene1200 U UG/KG 2,4-Dichlorophenol 1200 U UG/KG Carbazole1200 U UG/KG Naphthalene 1200 U UG/KG Di-n-Butylphthalate1200 U UG/KG 4-Chloroaniline 1200 U UG/KG Fluoranthene1200 U UG/KG Hexachlorobutadiene 1200 U UG/KG Pyrene1200 U UG/KG Caprolactam 1200 U UG/KG Benzyl Butyl Phthalate1200 U UG/KG 4-Chloro-3-Methylphenol 1200 U UG/KG 3,3'-Dichlorobenzidine1200 U UG/KG 2-Methylnaphthalene 1200 U UG/KG Benzo(a)Anthracene1200 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 1200 U UG/KG Chrysene1200 U UG/KG 2,4,6-Trichlorophenol 1200 U UG/KG bis(2-Ethylhexyl) Phthala3100 U UG/KG 2,4,5-Trichlorophenol 1200 U UG/KG Di-n-Octylphthalate1200 U UG/KG 1,1-Biphenyl 1200 U UG/KG Benzo(b)Fluoranthene1200 U UG/KG 2-Chloronaphthalene 1200 U UG/KG Benzo(k)Fluoranthene3100 U UG/KG 2-Nitroaniline 1200 U UG/KG Benzo-a-Pyrene1200 U UG/KG Dimethyl Phthalate 1200 U UG/KG Indeno (1,2,3-cd) Pyrene1200 U UG/KG 2,6-Dinitrotoluene 1200 U UG/KG Dibenzo(a,h)Anthracene1200 U UG/KG Acenaphthylene 1200 U UG/KG Benzo(ghi)Perylene3100 U UG/KG 3-Nitroaniline 73 % % Moisture1200 U UG/KG Acenaphthene3100 U UG/KG 2,4-Dinitrophenol3100 U UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9525 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 12:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AK1 D No: 3AK1 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD05D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

58000 J UG/KG 28 UNKNOWNS

1500 NJ UG/KG 15-ISOBUTYL-(13ALPHAH)-ISOCOPALANE4400 NJ UG/KG STIGMAST-4-EN-3-ONE

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9526 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 12:40

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AK2 D No: 3AK2 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

720 U UG/KG Benzaldehyde 720 U UG/KG Dibenzofuran720 U UG/KG Phenol 720 U UG/KG 2,4-Dinitrotoluene720 U UG/KG bis(2-Chloroethyl) Ether 720 U UG/KG Diethyl Phthalate720 U UG/KG 2-Chlorophenol 720 U UG/KG Fluorene720 U UG/KG 2-Methylphenol 720 U UG/KG 4-Chlorophenyl Phenyl E720 U UG/KG bis(2-Chloroisopropyl) Ether 1800 U UG/KG 4-Nitroaniline720 U UG/KG Acetophenone 1800 U UG/KG 2-Methyl-4,6-Dinitrophen720 U UG/KG (3-and/or 4-)Methylphenol 720 U UG/KG n-Nitrosodiphenylamine/720 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze720 U UG/KG Hexachloroethane 720 UJ UG/KG 4-Bromophenyl Phenyl E720 U UG/KG Nitrobenzene 720 UJ UG/KG Hexachlorobenzene (HC720 U UG/KG Isophorone 720 U UG/KG Atrazine720 U UG/KG 2-Nitrophenol 1800 U UG/KG Pentachlorophenol720 U UG/KG 2,4-Dimethylphenol 720 U UG/KG Phenanthrene720 U UG/KG bis(2-Chloroethoxy)Methane 720 U UG/KG Anthracene720 U UG/KG 2,4-Dichlorophenol 720 U UG/KG Carbazole720 U UG/KG Naphthalene 720 U UG/KG Di-n-Butylphthalate720 U UG/KG 4-Chloroaniline 720 U UG/KG Fluoranthene720 U UG/KG Hexachlorobutadiene 720 U UG/KG Pyrene720 U UG/KG Caprolactam 720 U UG/KG Benzyl Butyl Phthalate720 U UG/KG 4-Chloro-3-Methylphenol 720 U UG/KG 3,3'-Dichlorobenzidine720 U UG/KG 2-Methylnaphthalene 720 U UG/KG Benzo(a)Anthracene720 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 720 U UG/KG Chrysene720 U UG/KG 2,4,6-Trichlorophenol 720 U UG/KG bis(2-Ethylhexyl) Phthala

1800 U UG/KG 2,4,5-Trichlorophenol 720 U UG/KG Di-n-Octylphthalate

720 U UG/KG 1,1-Biphenyl 720 U UG/KG Benzo(b)Fluoranthene720 U UG/KG 2-Chloronaphthalene 720 U UG/KG Benzo(k)Fluoranthene

1800 U UG/KG 2-Nitroaniline 720 U UG/KG Benzo-a-Pyrene

720 U UG/KG Dimethyl Phthalate 720 U UG/KG Indeno (1,2,3-cd) Pyrene720 U UG/KG 2,6-Dinitrotoluene 720 U UG/KG Dibenzo(a,h)Anthracene720 U UG/KG Acenaphthylene 720 U UG/KG Benzo(ghi)Perylene

1800 U UG/KG 3-Nitroaniline 54 % % Moisture

720 U UG/KG Acenaphthene

1800 U UG/KG 2,4-Dinitrophenol1800 U UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9526 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 12:40

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AK2 D No: 3AK2 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

10000 J UG/KG 24 UNKNOWNS

540 NJ UG/KG HEXADECENOIC ACID, Z-11-500 NJ UG/KG N-HEXADECANOIC ACID630 NJ UG/KG 1-EICOSENE840 NJ UG/KG TESTOSTERONE

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9527 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 13:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AK5 D No: 3AK5 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD04 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

440 U UG/KG Benzaldehyde 440 U UG/KG Dibenzofuran440 U UG/KG Phenol 440 U UG/KG 2,4-Dinitrotoluene440 U UG/KG bis(2-Chloroethyl) Ether 440 U UG/KG Diethyl Phthalate440 U UG/KG 2-Chlorophenol 440 U UG/KG Fluorene440 U UG/KG 2-Methylphenol 440 UJ UG/KG 4-Chlorophenyl Phenyl E440 UJ UG/KG bis(2-Chloroisopropyl) Ether 1100 U UG/KG 4-Nitroaniline440 U UG/KG Acetophenone 1100 U UG/KG 2-Methyl-4,6-Dinitrophen440 U UG/KG (3-and/or 4-)Methylphenol 440 U UG/KG n-Nitrosodiphenylamine/440 UJ UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze440 UJ UG/KG Hexachloroethane 440 U UG/KG 4-Bromophenyl Phenyl E440 U UG/KG Nitrobenzene 440 UJ UG/KG Hexachlorobenzene (HC440 U UG/KG Isophorone 440 U UG/KG Atrazine440 U UG/KG 2-Nitrophenol 1100 U UG/KG Pentachlorophenol440 U UG/KG 2,4-Dimethylphenol 440 U UG/KG Phenanthrene440 U UG/KG bis(2-Chloroethoxy)Methane 440 U UG/KG Anthracene440 U UG/KG 2,4-Dichlorophenol 440 U UG/KG Carbazole440 U UG/KG Naphthalene 440 U UG/KG Di-n-Butylphthalate440 U UG/KG 4-Chloroaniline 440 U UG/KG Fluoranthene440 U UG/KG Hexachlorobutadiene 440 U UG/KG Pyrene440 U UG/KG Caprolactam 440 U UG/KG Benzyl Butyl Phthalate440 U UG/KG 4-Chloro-3-Methylphenol 440 U UG/KG 3,3'-Dichlorobenzidine440 U UG/KG 2-Methylnaphthalene 440 U UG/KG Benzo(a)Anthracene440 U UG/KG Hexachlorocyclopentadiene (HCCP) 440 U UG/KG Chrysene440 U UG/KG 2,4,6-Trichlorophenol 440 U UG/KG bis(2-Ethylhexyl) Phthala

1100 U UG/KG 2,4,5-Trichlorophenol 440 U UG/KG Di-n-Octylphthalate

440 U UG/KG 1,1-Biphenyl 440 U UG/KG Benzo(b)Fluoranthene440 U UG/KG 2-Chloronaphthalene 440 U UG/KG Benzo(k)Fluoranthene

1100 UJ UG/KG 2-Nitroaniline 440 U UG/KG Benzo-a-Pyrene

440 U UG/KG Dimethyl Phthalate 440 U UG/KG Indeno (1,2,3-cd) Pyrene440 U UG/KG 2,6-Dinitrotoluene 440 U UG/KG Dibenzo(a,h)Anthracene440 U UG/KG Acenaphthylene 440 U UG/KG Benzo(ghi)Perylene

1100 U UG/KG 3-Nitroaniline 25 % % Moisture

440 U UG/KG Acenaphthene

1100 U UG/KG 2,4-Dinitrophenol1100 U UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9527 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 13:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AK5 D No: 3AK5 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD04 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

4100 J UG/KG 17 UNKNOWNS

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9528 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 12:25

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AF9 D No: 3AF9 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSD01 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

1500 U UG/KG Benzaldehyde 1500 U UG/KG Dibenzofuran1500 U UG/KG Phenol 1500 U UG/KG 2,4-Dinitrotoluene1500 U UG/KG bis(2-Chloroethyl) Ether 1500 U UG/KG Diethyl Phthalate1500 U UG/KG 2-Chlorophenol 1500 U UG/KG Fluorene1500 U UG/KG 2-Methylphenol 1500 U UG/KG 4-Chlorophenyl Phenyl E1500 U UG/KG bis(2-Chloroisopropyl) Ether 3800 U UG/KG 4-Nitroaniline1500 U UG/KG Acetophenone 3800 UJ UG/KG 2-Methyl-4,6-Dinitrophen1500 U UG/KG (3-and/or 4-)Methylphenol 1500 U UG/KG n-Nitrosodiphenylamine/1500 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze1500 U UG/KG Hexachloroethane 1500 U UG/KG 4-Bromophenyl Phenyl E1500 U UG/KG Nitrobenzene 1500 U UG/KG Hexachlorobenzene (HC1500 U UG/KG Isophorone 1500 U UG/KG Atrazine1500 U UG/KG 2-Nitrophenol 3800 U UG/KG Pentachlorophenol1500 U UG/KG 2,4-Dimethylphenol 1500 U UG/KG Phenanthrene1500 U UG/KG bis(2-Chloroethoxy)Methane 1500 U UG/KG Anthracene1500 U UG/KG 2,4-Dichlorophenol 1500 U UG/KG Carbazole1500 U UG/KG Naphthalene 1500 U UG/KG Di-n-Butylphthalate1500 U UG/KG 4-Chloroaniline 1500 U UG/KG Fluoranthene1500 U UG/KG Hexachlorobutadiene 1500 U UG/KG Pyrene1500 UR UG/KG Caprolactam 1500 U UG/KG Benzyl Butyl Phthalate1500 U UG/KG 4-Chloro-3-Methylphenol 1500 U UG/KG 3,3'-Dichlorobenzidine1500 U UG/KG 2-Methylnaphthalene 1500 U UG/KG Benzo(a)Anthracene1500 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 1500 U UG/KG Chrysene1500 U UG/KG 2,4,6-Trichlorophenol 1500 U UG/KG bis(2-Ethylhexyl) Phthala3800 U UG/KG 2,4,5-Trichlorophenol 1500 U UG/KG Di-n-Octylphthalate1500 U UG/KG 1,1-Biphenyl 1500 U UG/KG Benzo(b)Fluoranthene1500 U UG/KG 2-Chloronaphthalene 1500 U UG/KG Benzo(k)Fluoranthene3800 U UG/KG 2-Nitroaniline 1500 U UG/KG Benzo-a-Pyrene1500 U UG/KG Dimethyl Phthalate 1500 U UG/KG Indeno (1,2,3-cd) Pyrene1500 U UG/KG 2,6-Dinitrotoluene 1500 U UG/KG Dibenzo(a,h)Anthracene1500 U UG/KG Acenaphthylene 1500 UJ UG/KG Benzo(ghi)Perylene3800 U UG/KG 3-Nitroaniline 78 % % Moisture1500 U UG/KG Acenaphthene3800 UJ UG/KG 2,4-Dinitrophenol3800 UJ UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9528 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 12:25

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AF9 D No: 3AF9 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSD01 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

20000 J UG/KG 19 UNKNOWNS

N UG/KG PETROLEUM PRODUCT

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9529 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 12:40

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AG0 D No: 3AG0 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSD01D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

1700 U UG/KG Benzaldehyde 1700 U UG/KG Dibenzofuran1700 U UG/KG Phenol 1700 U UG/KG 2,4-Dinitrotoluene1700 U UG/KG bis(2-Chloroethyl) Ether 1700 U UG/KG Diethyl Phthalate1700 U UG/KG 2-Chlorophenol 1700 U UG/KG Fluorene1700 U UG/KG 2-Methylphenol 1700 U UG/KG 4-Chlorophenyl Phenyl E1700 U UG/KG bis(2-Chloroisopropyl) Ether 4200 U UG/KG 4-Nitroaniline1700 U UG/KG Acetophenone 4200 UJ UG/KG 2-Methyl-4,6-Dinitrophen1700 U UG/KG (3-and/or 4-)Methylphenol 1700 U UG/KG n-Nitrosodiphenylamine/1700 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze1700 U UG/KG Hexachloroethane 1700 U UG/KG 4-Bromophenyl Phenyl E1700 U UG/KG Nitrobenzene 1700 U UG/KG Hexachlorobenzene (HC1700 U UG/KG Isophorone 1700 U UG/KG Atrazine1700 U UG/KG 2-Nitrophenol 4200 U UG/KG Pentachlorophenol1700 U UG/KG 2,4-Dimethylphenol 1700 U UG/KG Phenanthrene1700 U UG/KG bis(2-Chloroethoxy)Methane 1700 U UG/KG Anthracene1700 U UG/KG 2,4-Dichlorophenol 1700 U UG/KG Carbazole1700 U UG/KG Naphthalene 1700 U UG/KG Di-n-Butylphthalate1700 U UG/KG 4-Chloroaniline 1700 U UG/KG Fluoranthene1700 U UG/KG Hexachlorobutadiene 1700 U UG/KG Pyrene1700 UR UG/KG Caprolactam 1700 U UG/KG Benzyl Butyl Phthalate1700 U UG/KG 4-Chloro-3-Methylphenol 1700 U UG/KG 3,3'-Dichlorobenzidine1700 U UG/KG 2-Methylnaphthalene 1700 U UG/KG Benzo(a)Anthracene1700 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 1700 U UG/KG Chrysene1700 U UG/KG 2,4,6-Trichlorophenol 1700 U UG/KG bis(2-Ethylhexyl) Phthala4200 U UG/KG 2,4,5-Trichlorophenol 1700 U UG/KG Di-n-Octylphthalate1700 U UG/KG 1,1-Biphenyl 1700 U UG/KG Benzo(b)Fluoranthene1700 U UG/KG 2-Chloronaphthalene 1700 U UG/KG Benzo(k)Fluoranthene4200 U UG/KG 2-Nitroaniline 1700 U UG/KG Benzo-a-Pyrene1700 U UG/KG Dimethyl Phthalate 1700 U UG/KG Indeno (1,2,3-cd) Pyrene1700 U UG/KG 2,6-Dinitrotoluene 1700 U UG/KG Dibenzo(a,h)Anthracene1700 U UG/KG Acenaphthylene 1700 UJ UG/KG Benzo(ghi)Perylene4200 U UG/KG 3-Nitroaniline 80 % % Moisture1700 U UG/KG Acenaphthene4200 UJ UG/KG 2,4-Dinitrophenol4200 UJ UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9529 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 12:40

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG0 D No: 3AG0 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSD01D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

8900 J UG/KG 11 UNKNOWNS

N UG/KG PETROLEUM PRODUCT

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9530 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 13:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AG1 D No: 3AG1 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSD02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

790 U UG/KG Benzaldehyde 790 U UG/KG Dibenzofuran790 U UG/KG Phenol 790 U UG/KG 2,4-Dinitrotoluene790 U UG/KG bis(2-Chloroethyl) Ether 790 U UG/KG Diethyl Phthalate790 U UG/KG 2-Chlorophenol 790 U UG/KG Fluorene790 U UG/KG 2-Methylphenol 790 U UG/KG 4-Chlorophenyl Phenyl E790 U UG/KG bis(2-Chloroisopropyl) Ether 2000 U UG/KG 4-Nitroaniline170 J UG/KG Acetophenone 2000 UJ UG/KG 2-Methyl-4,6-Dinitrophen790 U UG/KG (3-and/or 4-)Methylphenol 790 U UG/KG n-Nitrosodiphenylamine/790 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze790 U UG/KG Hexachloroethane 790 U UG/KG 4-Bromophenyl Phenyl E790 U UG/KG Nitrobenzene 790 U UG/KG Hexachlorobenzene (HC790 U UG/KG Isophorone 790 U UG/KG Atrazine790 U UG/KG 2-Nitrophenol 2000 U UG/KG Pentachlorophenol790 U UG/KG 2,4-Dimethylphenol 790 U UG/KG Phenanthrene790 U UG/KG bis(2-Chloroethoxy)Methane 790 U UG/KG Anthracene790 U UG/KG 2,4-Dichlorophenol 790 U UG/KG Carbazole790 U UG/KG Naphthalene 790 U UG/KG Di-n-Butylphthalate790 U UG/KG 4-Chloroaniline 790 U UG/KG Fluoranthene790 U UG/KG Hexachlorobutadiene 790 U UG/KG Pyrene790 UR UG/KG Caprolactam 790 U UG/KG Benzyl Butyl Phthalate790 U UG/KG 4-Chloro-3-Methylphenol 790 U UG/KG 3,3'-Dichlorobenzidine790 U UG/KG 2-Methylnaphthalene 790 U UG/KG Benzo(a)Anthracene790 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 790 U UG/KG Chrysene790 U UG/KG 2,4,6-Trichlorophenol 790 U UG/KG bis(2-Ethylhexyl) Phthala

2000 U UG/KG 2,4,5-Trichlorophenol 790 U UG/KG Di-n-Octylphthalate

790 U UG/KG 1,1-Biphenyl 790 U UG/KG Benzo(b)Fluoranthene790 U UG/KG 2-Chloronaphthalene 790 U UG/KG Benzo(k)Fluoranthene

2000 U UG/KG 2-Nitroaniline 790 U UG/KG Benzo-a-Pyrene

790 U UG/KG Dimethyl Phthalate 790 U UG/KG Indeno (1,2,3-cd) Pyrene790 U UG/KG 2,6-Dinitrotoluene 790 U UG/KG Dibenzo(a,h)Anthracene790 U UG/KG Acenaphthylene 790 UJ UG/KG Benzo(ghi)Perylene

2000 U UG/KG 3-Nitroaniline 58 % % Moisture

790 U UG/KG Acenaphthene

2000 UJ UG/KG 2,4-Dinitrophenol2000 UJ UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9530 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 13:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG1 D No: 3AG1 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSD02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

25000 J UG/KG 28 UNKNOWNS

N UG/KG PETROLEUM PRODUCT

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9531 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 13:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AG2 D No: 3AG2 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSD03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

400 U UG/KG Benzaldehyde 400 U UG/KG Dibenzofuran400 U UG/KG Phenol 400 U UG/KG 2,4-Dinitrotoluene400 U UG/KG bis(2-Chloroethyl) Ether 400 U UG/KG Diethyl Phthalate400 U UG/KG 2-Chlorophenol 400 U UG/KG Fluorene400 U UG/KG 2-Methylphenol 400 U UG/KG 4-Chlorophenyl Phenyl E400 U UG/KG bis(2-Chloroisopropyl) Ether 1000 U UG/KG 4-Nitroaniline400 U UG/KG Acetophenone 1000 UJ UG/KG 2-Methyl-4,6-Dinitrophen400 U UG/KG (3-and/or 4-)Methylphenol 400 U UG/KG n-Nitrosodiphenylamine/400 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze400 U UG/KG Hexachloroethane 400 U UG/KG 4-Bromophenyl Phenyl E400 U UG/KG Nitrobenzene 400 U UG/KG Hexachlorobenzene (HC400 U UG/KG Isophorone 400 U UG/KG Atrazine400 U UG/KG 2-Nitrophenol 1000 U UG/KG Pentachlorophenol400 U UG/KG 2,4-Dimethylphenol 180 J UG/KG Phenanthrene400 U UG/KG bis(2-Chloroethoxy)Methane 400 U UG/KG Anthracene400 U UG/KG 2,4-Dichlorophenol 400 U UG/KG Carbazole400 U UG/KG Naphthalene 400 U UG/KG Di-n-Butylphthalate400 U UG/KG 4-Chloroaniline 400 UG/KG Fluoranthene400 U UG/KG Hexachlorobutadiene 370 J UG/KG Pyrene400 UR UG/KG Caprolactam 400 U UG/KG Benzyl Butyl Phthalate400 U UG/KG 4-Chloro-3-Methylphenol 400 U UG/KG 3,3'-Dichlorobenzidine400 U UG/KG 2-Methylnaphthalene 220 J UG/KG Benzo(a)Anthracene400 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 280 J UG/KG Chrysene400 U UG/KG 2,4,6-Trichlorophenol 400 U UG/KG bis(2-Ethylhexyl) Phthala

1000 U UG/KG 2,4,5-Trichlorophenol 400 U UG/KG Di-n-Octylphthalate

400 U UG/KG 1,1-Biphenyl 210 J UG/KG Benzo(b)Fluoranthene400 U UG/KG 2-Chloronaphthalene 230 J UG/KG Benzo(k)Fluoranthene

1000 U UG/KG 2-Nitroaniline 200 J UG/KG Benzo-a-Pyrene

400 U UG/KG Dimethyl Phthalate 150 J UG/KG Indeno (1,2,3-cd) Pyrene400 U UG/KG 2,6-Dinitrotoluene 400 U UG/KG Dibenzo(a,h)Anthracene400 U UG/KG Acenaphthylene 120 J UG/KG Benzo(ghi)Perylene

1000 U UG/KG 3-Nitroaniline 17 % % Moisture

400 U UG/KG Acenaphthene

1000 UJ UG/KG 2,4-Dinitrophenol1000 UJ UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9531 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 13:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG2 D No: 3AG2 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSD03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

300 J UG/KG 3 UNKNOWNS190 NJ UG/KG UNKNOWN PAH

N UG/KG PETROLEUM PRODUCT

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9532 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 12:50

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AG3 D No: 3AG3 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSF04 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

380 U UG/KG Benzaldehyde 380 U UG/KG Dibenzofuran380 U UG/KG Phenol 380 U UG/KG 2,4-Dinitrotoluene380 U UG/KG bis(2-Chloroethyl) Ether 380 U UG/KG Diethyl Phthalate380 U UG/KG 2-Chlorophenol 380 U UG/KG Fluorene380 U UG/KG 2-Methylphenol 380 U UG/KG 4-Chlorophenyl Phenyl E380 U UG/KG bis(2-Chloroisopropyl) Ether 940 U UG/KG 4-Nitroaniline380 U UG/KG Acetophenone 940 UJ UG/KG 2-Methyl-4,6-Dinitrophen380 U UG/KG (3-and/or 4-)Methylphenol 380 U UG/KG n-Nitrosodiphenylamine/380 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze380 U UG/KG Hexachloroethane 380 U UG/KG 4-Bromophenyl Phenyl E380 U UG/KG Nitrobenzene 380 U UG/KG Hexachlorobenzene (HC380 U UG/KG Isophorone 380 U UG/KG Atrazine380 U UG/KG 2-Nitrophenol 940 U UG/KG Pentachlorophenol380 U UG/KG 2,4-Dimethylphenol 380 U UG/KG Phenanthrene380 U UG/KG bis(2-Chloroethoxy)Methane 380 U UG/KG Anthracene380 U UG/KG 2,4-Dichlorophenol 380 U UG/KG Carbazole380 U UG/KG Naphthalene 380 U UG/KG Di-n-Butylphthalate380 U UG/KG 4-Chloroaniline 380 U UG/KG Fluoranthene380 U UG/KG Hexachlorobutadiene 380 U UG/KG Pyrene380 UR UG/KG Caprolactam 380 U UG/KG Benzyl Butyl Phthalate380 U UG/KG 4-Chloro-3-Methylphenol 380 U UG/KG 3,3'-Dichlorobenzidine380 U UG/KG 2-Methylnaphthalene 380 U UG/KG Benzo(a)Anthracene380 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 380 U UG/KG Chrysene380 U UG/KG 2,4,6-Trichlorophenol 380 U UG/KG bis(2-Ethylhexyl) Phthala940 U UG/KG 2,4,5-Trichlorophenol 380 U UG/KG Di-n-Octylphthalate380 U UG/KG 1,1-Biphenyl 380 U UG/KG Benzo(b)Fluoranthene380 U UG/KG 2-Chloronaphthalene 380 U UG/KG Benzo(k)Fluoranthene940 U UG/KG 2-Nitroaniline 380 U UG/KG Benzo-a-Pyrene380 U UG/KG Dimethyl Phthalate 380 U UG/KG Indeno (1,2,3-cd) Pyrene380 U UG/KG 2,6-Dinitrotoluene 380 U UG/KG Dibenzo(a,h)Anthracene380 U UG/KG Acenaphthylene 380 UJ UG/KG Benzo(ghi)Perylene940 U UG/KG 3-Nitroaniline 12 % % Moisture380 U UG/KG Acenaphthene940 UJ UG/KG 2,4-Dinitrophenol940 UJ UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9532 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 12:50

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG3 D No: 3AG3 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSF04 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

8400 J UG/KG 27 UNKNOWNS

N UG/KG PETROLEUM PRODUCT

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9533 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 12:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AG4 D No: 3AG4 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSF05 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

380 U UG/KG Benzaldehyde 380 U UG/KG Dibenzofuran380 U UG/KG Phenol 380 U UG/KG 2,4-Dinitrotoluene380 U UG/KG bis(2-Chloroethyl) Ether 380 U UG/KG Diethyl Phthalate380 U UG/KG 2-Chlorophenol 380 U UG/KG Fluorene380 U UG/KG 2-Methylphenol 380 U UG/KG 4-Chlorophenyl Phenyl E380 U UG/KG bis(2-Chloroisopropyl) Ether 950 U UG/KG 4-Nitroaniline380 U UG/KG Acetophenone 950 UJ UG/KG 2-Methyl-4,6-Dinitrophen380 U UG/KG (3-and/or 4-)Methylphenol 380 U UG/KG n-Nitrosodiphenylamine/380 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze380 U UG/KG Hexachloroethane 380 U UG/KG 4-Bromophenyl Phenyl E380 U UG/KG Nitrobenzene 380 U UG/KG Hexachlorobenzene (HC380 U UG/KG Isophorone 380 U UG/KG Atrazine380 U UG/KG 2-Nitrophenol 950 U UG/KG Pentachlorophenol380 U UG/KG 2,4-Dimethylphenol 380 U UG/KG Phenanthrene380 U UG/KG bis(2-Chloroethoxy)Methane 380 U UG/KG Anthracene380 U UG/KG 2,4-Dichlorophenol 380 U UG/KG Carbazole380 U UG/KG Naphthalene 380 U UG/KG Di-n-Butylphthalate380 U UG/KG 4-Chloroaniline 380 U UG/KG Fluoranthene380 U UG/KG Hexachlorobutadiene 380 U UG/KG Pyrene380 UR UG/KG Caprolactam 380 U UG/KG Benzyl Butyl Phthalate380 U UG/KG 4-Chloro-3-Methylphenol 380 U UG/KG 3,3'-Dichlorobenzidine380 U UG/KG 2-Methylnaphthalene 380 U UG/KG Benzo(a)Anthracene380 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 380 U UG/KG Chrysene380 U UG/KG 2,4,6-Trichlorophenol 380 U UG/KG bis(2-Ethylhexyl) Phthala950 U UG/KG 2,4,5-Trichlorophenol 380 U UG/KG Di-n-Octylphthalate380 U UG/KG 1,1-Biphenyl 380 U UG/KG Benzo(b)Fluoranthene380 U UG/KG 2-Chloronaphthalene 380 U UG/KG Benzo(k)Fluoranthene950 U UG/KG 2-Nitroaniline 380 U UG/KG Benzo-a-Pyrene380 U UG/KG Dimethyl Phthalate 380 U UG/KG Indeno (1,2,3-cd) Pyrene380 U UG/KG 2,6-Dinitrotoluene 380 U UG/KG Dibenzo(a,h)Anthracene380 U UG/KG Acenaphthylene 380 UJ UG/KG Benzo(ghi)Perylene950 U UG/KG 3-Nitroaniline 13 % % Moisture380 U UG/KG Acenaphthene950 UJ UG/KG 2,4-Dinitrophenol950 UJ UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9533 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 12:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG4 D No: 3AG4 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSF05 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

21000 J UG/KG 20 UNKNOWNS

N UG/KG PETROLEUM PRODUCT

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9534 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 12:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AG5 D No: 3AG5 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSF05S / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

380 U UG/KG Benzaldehyde 380 U UG/KG Dibenzofuran380 U UG/KG Phenol 380 U UG/KG 2,4-Dinitrotoluene380 U UG/KG bis(2-Chloroethyl) Ether 380 U UG/KG Diethyl Phthalate380 U UG/KG 2-Chlorophenol 380 U UG/KG Fluorene380 U UG/KG 2-Methylphenol 380 U UG/KG 4-Chlorophenyl Phenyl E380 U UG/KG bis(2-Chloroisopropyl) Ether 950 U UG/KG 4-Nitroaniline380 U UG/KG Acetophenone 950 UJ UG/KG 2-Methyl-4,6-Dinitrophen380 U UG/KG (3-and/or 4-)Methylphenol 380 U UG/KG n-Nitrosodiphenylamine/380 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze380 U UG/KG Hexachloroethane 380 U UG/KG 4-Bromophenyl Phenyl E380 U UG/KG Nitrobenzene 380 U UG/KG Hexachlorobenzene (HC380 U UG/KG Isophorone 380 U UG/KG Atrazine380 U UG/KG 2-Nitrophenol 950 U UG/KG Pentachlorophenol380 U UG/KG 2,4-Dimethylphenol 380 U UG/KG Phenanthrene380 U UG/KG bis(2-Chloroethoxy)Methane 380 U UG/KG Anthracene380 U UG/KG 2,4-Dichlorophenol 380 U UG/KG Carbazole380 U UG/KG Naphthalene 380 U UG/KG Di-n-Butylphthalate380 U UG/KG 4-Chloroaniline 380 U UG/KG Fluoranthene380 U UG/KG Hexachlorobutadiene 380 U UG/KG Pyrene380 UR UG/KG Caprolactam 380 U UG/KG Benzyl Butyl Phthalate380 U UG/KG 4-Chloro-3-Methylphenol 380 U UG/KG 3,3'-Dichlorobenzidine380 U UG/KG 2-Methylnaphthalene 380 U UG/KG Benzo(a)Anthracene380 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 380 U UG/KG Chrysene380 U UG/KG 2,4,6-Trichlorophenol 380 U UG/KG bis(2-Ethylhexyl) Phthala950 U UG/KG 2,4,5-Trichlorophenol 380 U UG/KG Di-n-Octylphthalate380 U UG/KG 1,1-Biphenyl 380 U UG/KG Benzo(b)Fluoranthene380 U UG/KG 2-Chloronaphthalene 380 U UG/KG Benzo(k)Fluoranthene950 U UG/KG 2-Nitroaniline 380 U UG/KG Benzo-a-Pyrene380 U UG/KG Dimethyl Phthalate 380 U UG/KG Indeno (1,2,3-cd) Pyrene380 U UG/KG 2,6-Dinitrotoluene 380 U UG/KG Dibenzo(a,h)Anthracene380 U UG/KG Acenaphthylene 380 UJ UG/KG Benzo(ghi)Perylene950 U UG/KG 3-Nitroaniline 13 % % Moisture380 U UG/KG Acenaphthene950 UJ UG/KG 2,4-Dinitrophenol950 UJ UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9534 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 12:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG5 D No: 3AG5 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSF05S / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

34000 J UG/KG 22 UNKNOWNS

N UG/KG PETROLEUM PRODUCT

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9535 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 09:00

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AG7 D No: 3AG7 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF OPSD02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

380 UJ UG/KG Benzaldehyde 380 U UG/KG Dibenzofuran380 U UG/KG Phenol 380 U UG/KG 2,4-Dinitrotoluene380 U UG/KG bis(2-Chloroethyl) Ether 380 U UG/KG Diethyl Phthalate380 U UG/KG 2-Chlorophenol 380 U UG/KG Fluorene380 U UG/KG 2-Methylphenol 380 U UG/KG 4-Chlorophenyl Phenyl E380 U UG/KG bis(2-Chloroisopropyl) Ether 970 U UG/KG 4-Nitroaniline

91 J UG/KG Acetophenone 970 UJ UG/KG 2-Methyl-4,6-Dinitrophen

380 U UG/KG (3-and/or 4-)Methylphenol 380 U UG/KG n-Nitrosodiphenylamine/380 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze380 U UG/KG Hexachloroethane 380 U UG/KG 4-Bromophenyl Phenyl E380 U UG/KG Nitrobenzene 380 U UG/KG Hexachlorobenzene (HC380 U UG/KG Isophorone 380 UJ UG/KG Atrazine380 U UG/KG 2-Nitrophenol 970 UJ UG/KG Pentachlorophenol380 U UG/KG 2,4-Dimethylphenol 380 U UG/KG Phenanthrene380 U UG/KG bis(2-Chloroethoxy)Methane 380 U UG/KG Anthracene380 U UG/KG 2,4-Dichlorophenol 380 U UG/KG Carbazole380 U UG/KG Naphthalene 380 U UG/KG Di-n-Butylphthalate380 U UG/KG 4-Chloroaniline 380 U UG/KG Fluoranthene380 U UG/KG Hexachlorobutadiene 380 U UG/KG Pyrene380 UR UG/KG Caprolactam 380 U UG/KG Benzyl Butyl Phthalate380 U UG/KG 4-Chloro-3-Methylphenol 380 UJ UG/KG 3,3'-Dichlorobenzidine380 U UG/KG 2-Methylnaphthalene 380 U UG/KG Benzo(a)Anthracene380 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 380 U UG/KG Chrysene380 U UG/KG 2,4,6-Trichlorophenol 380 U UG/KG bis(2-Ethylhexyl) Phthala970 U UG/KG 2,4,5-Trichlorophenol 380 U UG/KG Di-n-Octylphthalate380 U UG/KG 1,1-Biphenyl 380 U UG/KG Benzo(b)Fluoranthene380 U UG/KG 2-Chloronaphthalene 380 U UG/KG Benzo(k)Fluoranthene970 U UG/KG 2-Nitroaniline 380 U UG/KG Benzo-a-Pyrene570 UG/KG Dimethyl Phthalate 380 UJ UG/KG Indeno (1,2,3-cd) Pyrene380 U UG/KG 2,6-Dinitrotoluene 380 UJ UG/KG Dibenzo(a,h)Anthracene380 U UG/KG Acenaphthylene 380 UJ UG/KG Benzo(ghi)Perylene970 U UG/KG 3-Nitroaniline 14 % % Moisture380 U UG/KG Acenaphthene970 UJ UG/KG 2,4-Dinitrophenol970 UJ UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9535 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 09:00

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG7 D No: 3AG7 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF OPSD02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

7300 J UG/KG 28 UNKNOWNS

N UG/KG PETROLEUM PRODUCT

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9536 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 09:25

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AG8 D No: 3AG8 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF OPSD02D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

410 UJ UG/KG Benzaldehyde 410 U UG/KG Dibenzofuran410 U UG/KG Phenol 410 U UG/KG 2,4-Dinitrotoluene410 U UG/KG bis(2-Chloroethyl) Ether 410 U UG/KG Diethyl Phthalate410 U UG/KG 2-Chlorophenol 410 U UG/KG Fluorene410 U UG/KG 2-Methylphenol 410 U UG/KG 4-Chlorophenyl Phenyl E410 U UG/KG bis(2-Chloroisopropyl) Ether 1000 U UG/KG 4-Nitroaniline410 U UG/KG Acetophenone 1000 UJ UG/KG 2-Methyl-4,6-Dinitrophen410 U UG/KG (3-and/or 4-)Methylphenol 410 U UG/KG n-Nitrosodiphenylamine/410 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze410 U UG/KG Hexachloroethane 410 U UG/KG 4-Bromophenyl Phenyl E410 U UG/KG Nitrobenzene 410 U UG/KG Hexachlorobenzene (HC410 U UG/KG Isophorone 410 UJ UG/KG Atrazine410 U UG/KG 2-Nitrophenol 1000 UJ UG/KG Pentachlorophenol410 U UG/KG 2,4-Dimethylphenol 410 U UG/KG Phenanthrene410 U UG/KG bis(2-Chloroethoxy)Methane 410 U UG/KG Anthracene410 U UG/KG 2,4-Dichlorophenol 410 U UG/KG Carbazole410 U UG/KG Naphthalene 410 U UG/KG Di-n-Butylphthalate410 U UG/KG 4-Chloroaniline 410 U UG/KG Fluoranthene410 U UG/KG Hexachlorobutadiene 410 U UG/KG Pyrene410 UR UG/KG Caprolactam 410 U UG/KG Benzyl Butyl Phthalate410 U UG/KG 4-Chloro-3-Methylphenol 410 UJ UG/KG 3,3'-Dichlorobenzidine410 U UG/KG 2-Methylnaphthalene 410 U UG/KG Benzo(a)Anthracene410 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 410 U UG/KG Chrysene410 U UG/KG 2,4,6-Trichlorophenol 410 U UG/KG bis(2-Ethylhexyl) Phthala

1000 U UG/KG 2,4,5-Trichlorophenol 410 U UG/KG Di-n-Octylphthalate

410 U UG/KG 1,1-Biphenyl 410 U UG/KG Benzo(b)Fluoranthene410 U UG/KG 2-Chloronaphthalene 410 U UG/KG Benzo(k)Fluoranthene

1000 U UG/KG 2-Nitroaniline 410 U UG/KG Benzo-a-Pyrene

410 U UG/KG Dimethyl Phthalate 410 UJ UG/KG Indeno (1,2,3-cd) Pyrene410 U UG/KG 2,6-Dinitrotoluene 410 UJ UG/KG Dibenzo(a,h)Anthracene410 U UG/KG Acenaphthylene 410 UJ UG/KG Benzo(ghi)Perylene

1000 U UG/KG 3-Nitroaniline 19 % % Moisture

410 U UG/KG Acenaphthene

1000 UJ UG/KG 2,4-Dinitrophenol1000 UJ UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9536 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 09:25

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG8 D No: 3AG8 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF OPSD02D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

6200 J UG/KG 24 UNKNOWNS

N UG/KG PETROLEUM PRODUCT

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9537 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 09:50

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AG9 D No: 3AG9 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF OPSD01 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

350 UJ UG/KG Benzaldehyde 350 U UG/KG Dibenzofuran350 U UG/KG Phenol 350 U UG/KG 2,4-Dinitrotoluene350 U UG/KG bis(2-Chloroethyl) Ether 350 U UG/KG Diethyl Phthalate350 U UG/KG 2-Chlorophenol 350 U UG/KG Fluorene350 U UG/KG 2-Methylphenol 350 U UG/KG 4-Chlorophenyl Phenyl E350 U UG/KG bis(2-Chloroisopropyl) Ether 880 U UG/KG 4-Nitroaniline300 J UG/KG Acetophenone 880 UJ UG/KG 2-Methyl-4,6-Dinitrophen350 U UG/KG (3-and/or 4-)Methylphenol 350 U UG/KG n-Nitrosodiphenylamine/350 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze350 U UG/KG Hexachloroethane 350 U UG/KG 4-Bromophenyl Phenyl E350 U UG/KG Nitrobenzene 350 U UG/KG Hexachlorobenzene (HC350 U UG/KG Isophorone 350 UJ UG/KG Atrazine350 U UG/KG 2-Nitrophenol 880 UJ UG/KG Pentachlorophenol350 U UG/KG 2,4-Dimethylphenol 140 J UG/KG Phenanthrene350 U UG/KG bis(2-Chloroethoxy)Methane 120 J UG/KG Anthracene350 U UG/KG 2,4-Dichlorophenol 350 U UG/KG Carbazole350 U UG/KG Naphthalene 350 U UG/KG Di-n-Butylphthalate350 U UG/KG 4-Chloroaniline 1900 UG/KG Fluoranthene350 U UG/KG Hexachlorobutadiene 2000 UG/KG Pyrene350 UR UG/KG Caprolactam 350 U UG/KG Benzyl Butyl Phthalate350 U UG/KG 4-Chloro-3-Methylphenol 350 UJ UG/KG 3,3'-Dichlorobenzidine350 U UG/KG 2-Methylnaphthalene 1200 UG/KG Benzo(a)Anthracene350 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 1200 UG/KG Chrysene350 U UG/KG 2,4,6-Trichlorophenol 350 U UG/KG bis(2-Ethylhexyl) Phthala880 U UG/KG 2,4,5-Trichlorophenol 350 U UG/KG Di-n-Octylphthalate350 U UG/KG 1,1-Biphenyl 1600 UG/KG Benzo(b)Fluoranthene350 U UG/KG 2-Chloronaphthalene 890 UG/KG Benzo(k)Fluoranthene880 U UG/KG 2-Nitroaniline 1300 UG/KG Benzo-a-Pyrene350 U UG/KG Dimethyl Phthalate 1100 J UG/KG Indeno (1,2,3-cd) Pyrene350 U UG/KG 2,6-Dinitrotoluene 360 J UG/KG Dibenzo(a,h)Anthracene160 J UG/KG Acenaphthylene 750 J UG/KG Benzo(ghi)Perylene880 U UG/KG 3-Nitroaniline 6 % % Moisture350 U UG/KG Acenaphthene880 UJ UG/KG 2,4-Dinitrophenol880 UJ UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9537 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 09:50

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG9 D No: 3AG9 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF OPSD01 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

10000 J UG/KG 22 UNKNOWNS

250 NJ UG/KG CYCLOPENTA (DEF) PHENANTHRENONE550 NJ UG/KG 11H-BENZO [B] FLUORENE380 NJ UG/KG 2 PYRENE, 1-METHYL470 NJ UG/KG BENZO [E] PYRENE

N UG/KG PETROLEUM PRODUCT

1100 NJ UG/KG UNKNOWN PAH

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9538 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 10:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AH0 D No: 3AH0 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF OPSD03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

1700 J UG/KG Benzaldehyde 380 U UG/KG Dibenzofuran

11000 UG/KG Phenol 380 U UG/KG 2,4-Dinitrotoluene

380 U UG/KG bis(2-Chloroethyl) Ether 380 U UG/KG Diethyl Phthalate380 U UG/KG 2-Chlorophenol 380 U UG/KG Fluorene380 U UG/KG 2-Methylphenol 380 U UG/KG 4-Chlorophenyl Phenyl E380 U UG/KG bis(2-Chloroisopropyl) Ether 970 U UG/KG 4-Nitroaniline

8400 UG/KG Acetophenone 970 UJ UG/KG 2-Methyl-4,6-Dinitrophen

380 U UG/KG (3-and/or 4-)Methylphenol 380 U UG/KG n-Nitrosodiphenylamine/380 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze380 U UG/KG Hexachloroethane 380 U UG/KG 4-Bromophenyl Phenyl E380 U UG/KG Nitrobenzene 380 U UG/KG Hexachlorobenzene (HC380 U UG/KG Isophorone 380 UJ UG/KG Atrazine380 U UG/KG 2-Nitrophenol 970 UJ UG/KG Pentachlorophenol380 U UG/KG 2,4-Dimethylphenol 380 U UG/KG Phenanthrene380 U UG/KG bis(2-Chloroethoxy)Methane 380 U UG/KG Anthracene380 U UG/KG 2,4-Dichlorophenol 380 U UG/KG Carbazole380 U UG/KG Naphthalene 380 U UG/KG Di-n-Butylphthalate380 U UG/KG 4-Chloroaniline 320 J UG/KG Fluoranthene380 U UG/KG Hexachlorobutadiene 270 J UG/KG Pyrene380 UR UG/KG Caprolactam 380 U UG/KG Benzyl Butyl Phthalate380 U UG/KG 4-Chloro-3-Methylphenol 380 UJ UG/KG 3,3'-Dichlorobenzidine380 U UG/KG 2-Methylnaphthalene 95 J UG/KG Benzo(a)Anthracene380 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 220 J UG/KG Chrysene380 U UG/KG 2,4,6-Trichlorophenol 380 U UG/KG bis(2-Ethylhexyl) Phthala970 U UG/KG 2,4,5-Trichlorophenol 380 U UG/KG Di-n-Octylphthalate380 U UG/KG 1,1-Biphenyl 210 J UG/KG Benzo(b)Fluoranthene380 U UG/KG 2-Chloronaphthalene 130 J UG/KG Benzo(k)Fluoranthene970 U UG/KG 2-Nitroaniline 380 U UG/KG Benzo-a-Pyrene380 U UG/KG Dimethyl Phthalate 87 J UG/KG Indeno (1,2,3-cd) Pyrene380 U UG/KG 2,6-Dinitrotoluene 380 U UG/KG Dibenzo(a,h)Anthracene380 U UG/KG Acenaphthylene 380 U UG/KG Benzo(ghi)Perylene970 U UG/KG 3-Nitroaniline 14 % % Moisture380 U UG/KG Acenaphthene970 UJ UG/KG 2,4-Dinitrophenol970 UJ UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9538 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 10:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH0 D No: 3AH0 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF OPSD03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

98000 J UG/KG 24 UNKNOWNS

550 NJ UG/KG 2-BUTEN-1-ONE, 1,3-DIPHENYL480 NJ UG/KG 6,7,8,9-BENZO[B]FLUORENE

6800 NJ UG/KG 1,3-PROPANEDIONE, 1,3-DIPHENYL1700 NJ UG/KG 1,3,5-TRIPHENYL-1,5-PENTANEDIONE

370 NJ UG/KG 1,1':3',1' ':3' ',1' ' '-QUATERPHENYL

N UG/KG PETROLEUM PRODUCT

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9539 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 09:15

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AH1 D No: 3AH1 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSF01 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

520 UJ UG/KG Benzaldehyde 520 U UG/KG Dibenzofuran520 U UG/KG Phenol 520 U UG/KG 2,4-Dinitrotoluene520 U UG/KG bis(2-Chloroethyl) Ether 520 U UG/KG Diethyl Phthalate520 U UG/KG 2-Chlorophenol 520 U UG/KG Fluorene520 U UG/KG 2-Methylphenol 520 U UG/KG 4-Chlorophenyl Phenyl E520 U UG/KG bis(2-Chloroisopropyl) Ether 1300 U UG/KG 4-Nitroaniline170 J UG/KG Acetophenone 1300 UJ UG/KG 2-Methyl-4,6-Dinitrophen520 U UG/KG (3-and/or 4-)Methylphenol 520 U UG/KG n-Nitrosodiphenylamine/520 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze520 U UG/KG Hexachloroethane 520 U UG/KG 4-Bromophenyl Phenyl E520 U UG/KG Nitrobenzene 520 U UG/KG Hexachlorobenzene (HC520 U UG/KG Isophorone 520 UJ UG/KG Atrazine520 U UG/KG 2-Nitrophenol 1300 UJ UG/KG Pentachlorophenol520 U UG/KG 2,4-Dimethylphenol 520 U UG/KG Phenanthrene520 U UG/KG bis(2-Chloroethoxy)Methane 520 U UG/KG Anthracene520 U UG/KG 2,4-Dichlorophenol 520 U UG/KG Carbazole520 U UG/KG Naphthalene 520 U UG/KG Di-n-Butylphthalate520 U UG/KG 4-Chloroaniline 520 U UG/KG Fluoranthene520 U UG/KG Hexachlorobutadiene 520 U UG/KG Pyrene520 UR UG/KG Caprolactam 520 U UG/KG Benzyl Butyl Phthalate520 U UG/KG 4-Chloro-3-Methylphenol 520 UJ UG/KG 3,3'-Dichlorobenzidine520 U UG/KG 2-Methylnaphthalene 520 U UG/KG Benzo(a)Anthracene520 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 520 U UG/KG Chrysene520 U UG/KG 2,4,6-Trichlorophenol 860 U UG/KG bis(2-Ethylhexyl) Phthala

1300 U UG/KG 2,4,5-Trichlorophenol 520 U UG/KG Di-n-Octylphthalate

520 U UG/KG 1,1-Biphenyl 520 U UG/KG Benzo(b)Fluoranthene520 U UG/KG 2-Chloronaphthalene 520 U UG/KG Benzo(k)Fluoranthene

1300 U UG/KG 2-Nitroaniline 520 U UG/KG Benzo-a-Pyrene

520 U UG/KG Dimethyl Phthalate 520 UJ UG/KG Indeno (1,2,3-cd) Pyrene520 U UG/KG 2,6-Dinitrotoluene 520 UJ UG/KG Dibenzo(a,h)Anthracene520 U UG/KG Acenaphthylene 520 UJ UG/KG Benzo(ghi)Perylene

1300 U UG/KG 3-Nitroaniline 36 % % Moisture

520 U UG/KG Acenaphthene

1300 UJ UG/KG 2,4-Dinitrophenol1300 UJ UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9539 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 09:15

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH1 D No: 3AH1 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSF01 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

11000 J UG/KG 27 UNKNOWNS

N UG/KG PETROLEUM PRODUCT

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9540 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 09:15

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AH2 D No: 3AH2 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSF01S / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

520 UJ UG/KG Benzaldehyde 520 U UG/KG Dibenzofuran520 U UG/KG Phenol 520 U UG/KG 2,4-Dinitrotoluene520 U UG/KG bis(2-Chloroethyl) Ether 520 U UG/KG Diethyl Phthalate520 U UG/KG 2-Chlorophenol 520 U UG/KG Fluorene520 U UG/KG 2-Methylphenol 520 U UG/KG 4-Chlorophenyl Phenyl E520 U UG/KG bis(2-Chloroisopropyl) Ether 1300 U UG/KG 4-Nitroaniline520 U UG/KG Acetophenone 1300 UJ UG/KG 2-Methyl-4,6-Dinitrophen520 U UG/KG (3-and/or 4-)Methylphenol 520 U UG/KG n-Nitrosodiphenylamine/520 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze520 U UG/KG Hexachloroethane 520 U UG/KG 4-Bromophenyl Phenyl E520 U UG/KG Nitrobenzene 520 U UG/KG Hexachlorobenzene (HC520 U UG/KG Isophorone 520 UJ UG/KG Atrazine520 U UG/KG 2-Nitrophenol 1300 UJ UG/KG Pentachlorophenol520 U UG/KG 2,4-Dimethylphenol 520 U UG/KG Phenanthrene520 U UG/KG bis(2-Chloroethoxy)Methane 520 U UG/KG Anthracene520 U UG/KG 2,4-Dichlorophenol 520 U UG/KG Carbazole520 U UG/KG Naphthalene 520 U UG/KG Di-n-Butylphthalate520 U UG/KG 4-Chloroaniline 520 U UG/KG Fluoranthene520 U UG/KG Hexachlorobutadiene 520 U UG/KG Pyrene520 UR UG/KG Caprolactam 520 U UG/KG Benzyl Butyl Phthalate520 U UG/KG 4-Chloro-3-Methylphenol 520 UJ UG/KG 3,3'-Dichlorobenzidine520 U UG/KG 2-Methylnaphthalene 520 U UG/KG Benzo(a)Anthracene520 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 520 U UG/KG Chrysene520 U UG/KG 2,4,6-Trichlorophenol 1200 U UG/KG bis(2-Ethylhexyl) Phthala

1300 U UG/KG 2,4,5-Trichlorophenol 520 U UG/KG Di-n-Octylphthalate

520 U UG/KG 1,1-Biphenyl 520 U UG/KG Benzo(b)Fluoranthene520 U UG/KG 2-Chloronaphthalene 520 U UG/KG Benzo(k)Fluoranthene

1300 U UG/KG 2-Nitroaniline 520 U UG/KG Benzo-a-Pyrene

520 U UG/KG Dimethyl Phthalate 520 UJ UG/KG Indeno (1,2,3-cd) Pyrene520 U UG/KG 2,6-Dinitrotoluene 520 UJ UG/KG Dibenzo(a,h)Anthracene520 U UG/KG Acenaphthylene 520 UJ UG/KG Benzo(ghi)Perylene

1300 U UG/KG 3-Nitroaniline 36 % % Moisture

520 U UG/KG Acenaphthene

1300 UJ UG/KG 2,4-Dinitrophenol1300 UJ UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9540 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 09:15

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH2 D No: 3AH2 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSF01S / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

20000 J UG/KG 28 UNKNOWNS

N UG/KG PETROLEUM PRODUCT

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9541 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 10:10

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AH3 D No: 3AH3 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSF02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

360 UJ UG/KG Benzaldehyde 360 U UG/KG Dibenzofuran360 U UG/KG Phenol 360 U UG/KG 2,4-Dinitrotoluene360 U UG/KG bis(2-Chloroethyl) Ether 360 U UG/KG Diethyl Phthalate360 U UG/KG 2-Chlorophenol 360 U UG/KG Fluorene360 U UG/KG 2-Methylphenol 360 U UG/KG 4-Chlorophenyl Phenyl E360 U UG/KG bis(2-Chloroisopropyl) Ether 910 U UG/KG 4-Nitroaniline360 U UG/KG Acetophenone 910 UJ UG/KG 2-Methyl-4,6-Dinitrophen360 U UG/KG (3-and/or 4-)Methylphenol 360 U UG/KG n-Nitrosodiphenylamine/360 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze360 U UG/KG Hexachloroethane 360 U UG/KG 4-Bromophenyl Phenyl E360 U UG/KG Nitrobenzene 360 U UG/KG Hexachlorobenzene (HC360 U UG/KG Isophorone 360 UJ UG/KG Atrazine360 U UG/KG 2-Nitrophenol 910 UJ UG/KG Pentachlorophenol360 U UG/KG 2,4-Dimethylphenol 360 U UG/KG Phenanthrene360 U UG/KG bis(2-Chloroethoxy)Methane 360 U UG/KG Anthracene360 U UG/KG 2,4-Dichlorophenol 360 U UG/KG Carbazole360 U UG/KG Naphthalene 360 U UG/KG Di-n-Butylphthalate360 U UG/KG 4-Chloroaniline 110 J UG/KG Fluoranthene360 U UG/KG Hexachlorobutadiene 150 J UG/KG Pyrene360 UR UG/KG Caprolactam 360 U UG/KG Benzyl Butyl Phthalate360 U UG/KG 4-Chloro-3-Methylphenol 360 UJ UG/KG 3,3'-Dichlorobenzidine360 U UG/KG 2-Methylnaphthalene 360 U UG/KG Benzo(a)Anthracene360 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 81 J UG/KG Chrysene360 U UG/KG 2,4,6-Trichlorophenol 360 U UG/KG bis(2-Ethylhexyl) Phthala910 U UG/KG 2,4,5-Trichlorophenol 360 U UG/KG Di-n-Octylphthalate360 U UG/KG 1,1-Biphenyl 360 U UG/KG Benzo(b)Fluoranthene360 U UG/KG 2-Chloronaphthalene 80 J UG/KG Benzo(k)Fluoranthene910 U UG/KG 2-Nitroaniline 360 U UG/KG Benzo-a-Pyrene360 U UG/KG Dimethyl Phthalate 360 UJ UG/KG Indeno (1,2,3-cd) Pyrene360 U UG/KG 2,6-Dinitrotoluene 360 UJ UG/KG Dibenzo(a,h)Anthracene360 U UG/KG Acenaphthylene 360 UJ UG/KG Benzo(ghi)Perylene910 U UG/KG 3-Nitroaniline 9 % % Moisture360 U UG/KG Acenaphthene910 UJ UG/KG 2,4-Dinitrophenol910 UJ UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9541 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 10:10

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH3 D No: 3AH3 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSF02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

12000 J UG/KG 24 UNKNOWNS

N UG/KG PETROLEUM PRODUCT

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9542 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 10:50

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AH4 D No: 3AH4 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSF03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

400 UJ UG/KG Benzaldehyde 400 U UG/KG Dibenzofuran400 U UG/KG Phenol 400 U UG/KG 2,4-Dinitrotoluene400 U UG/KG bis(2-Chloroethyl) Ether 400 U UG/KG Diethyl Phthalate400 U UG/KG 2-Chlorophenol 400 U UG/KG Fluorene400 U UG/KG 2-Methylphenol 400 U UG/KG 4-Chlorophenyl Phenyl E400 U UG/KG bis(2-Chloroisopropyl) Ether 1000 U UG/KG 4-Nitroaniline400 U UG/KG Acetophenone 1000 UJ UG/KG 2-Methyl-4,6-Dinitrophen400 U UG/KG (3-and/or 4-)Methylphenol 400 U UG/KG n-Nitrosodiphenylamine/400 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze400 U UG/KG Hexachloroethane 400 U UG/KG 4-Bromophenyl Phenyl E400 U UG/KG Nitrobenzene 400 U UG/KG Hexachlorobenzene (HC400 U UG/KG Isophorone 400 UJ UG/KG Atrazine400 U UG/KG 2-Nitrophenol 1000 UJ UG/KG Pentachlorophenol400 U UG/KG 2,4-Dimethylphenol 400 U UG/KG Phenanthrene400 U UG/KG bis(2-Chloroethoxy)Methane 400 U UG/KG Anthracene400 U UG/KG 2,4-Dichlorophenol 400 U UG/KG Carbazole400 U UG/KG Naphthalene 400 U UG/KG Di-n-Butylphthalate400 U UG/KG 4-Chloroaniline 100 J UG/KG Fluoranthene400 U UG/KG Hexachlorobutadiene 96 J UG/KG Pyrene400 UR UG/KG Caprolactam 400 U UG/KG Benzyl Butyl Phthalate400 U UG/KG 4-Chloro-3-Methylphenol 400 UJ UG/KG 3,3'-Dichlorobenzidine400 U UG/KG 2-Methylnaphthalene 400 U UG/KG Benzo(a)Anthracene400 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 400 U UG/KG Chrysene400 U UG/KG 2,4,6-Trichlorophenol 400 U UG/KG bis(2-Ethylhexyl) Phthala

1000 U UG/KG 2,4,5-Trichlorophenol 400 U UG/KG Di-n-Octylphthalate

400 U UG/KG 1,1-Biphenyl 87 J UG/KG Benzo(b)Fluoranthene400 U UG/KG 2-Chloronaphthalene 400 U UG/KG Benzo(k)Fluoranthene

1000 U UG/KG 2-Nitroaniline 400 U UG/KG Benzo-a-Pyrene

400 U UG/KG Dimethyl Phthalate 400 UJ UG/KG Indeno (1,2,3-cd) Pyrene400 U UG/KG 2,6-Dinitrotoluene 400 UJ UG/KG Dibenzo(a,h)Anthracene400 U UG/KG Acenaphthylene 400 UJ UG/KG Benzo(ghi)Perylene

1000 U UG/KG 3-Nitroaniline 18 % % Moisture

400 U UG/KG Acenaphthene

1000 UJ UG/KG 2,4-Dinitrophenol1000 UJ UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9542 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 10:50

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH4 D No: 3AH4 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSF03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

15000 J UG/KG 28 UNKNOWNS

N UG/KG PETROLEUM PRODUCT

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9543 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 11:15

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AH5 D No: 3AH5 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSD04 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

600 UJ UG/KG Benzaldehyde 600 U UG/KG Dibenzofuran600 U UG/KG Phenol 600 U UG/KG 2,4-Dinitrotoluene600 U UG/KG bis(2-Chloroethyl) Ether 600 U UG/KG Diethyl Phthalate600 U UG/KG 2-Chlorophenol 600 U UG/KG Fluorene600 U UG/KG 2-Methylphenol 600 U UG/KG 4-Chlorophenyl Phenyl E600 U UG/KG bis(2-Chloroisopropyl) Ether 1500 U UG/KG 4-Nitroaniline300 J UG/KG Acetophenone 1500 UJ UG/KG 2-Methyl-4,6-Dinitrophen600 U UG/KG (3-and/or 4-)Methylphenol 600 U UG/KG n-Nitrosodiphenylamine/600 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze600 U UG/KG Hexachloroethane 600 U UG/KG 4-Bromophenyl Phenyl E600 U UG/KG Nitrobenzene 600 U UG/KG Hexachlorobenzene (HC600 U UG/KG Isophorone 600 UJ UG/KG Atrazine600 U UG/KG 2-Nitrophenol 1500 UJ UG/KG Pentachlorophenol600 U UG/KG 2,4-Dimethylphenol 600 U UG/KG Phenanthrene600 U UG/KG bis(2-Chloroethoxy)Methane 600 U UG/KG Anthracene600 U UG/KG 2,4-Dichlorophenol 600 U UG/KG Carbazole600 U UG/KG Naphthalene 600 U UG/KG Di-n-Butylphthalate600 U UG/KG 4-Chloroaniline 600 U UG/KG Fluoranthene600 U UG/KG Hexachlorobutadiene 600 U UG/KG Pyrene600 UR UG/KG Caprolactam 600 U UG/KG Benzyl Butyl Phthalate600 U UG/KG 4-Chloro-3-Methylphenol 600 UJ UG/KG 3,3'-Dichlorobenzidine600 U UG/KG 2-Methylnaphthalene 600 U UG/KG Benzo(a)Anthracene600 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 600 U UG/KG Chrysene600 U UG/KG 2,4,6-Trichlorophenol 600 U UG/KG bis(2-Ethylhexyl) Phthala

1500 U UG/KG 2,4,5-Trichlorophenol 600 U UG/KG Di-n-Octylphthalate

600 U UG/KG 1,1-Biphenyl 600 U UG/KG Benzo(b)Fluoranthene600 U UG/KG 2-Chloronaphthalene 600 U UG/KG Benzo(k)Fluoranthene

1500 U UG/KG 2-Nitroaniline 600 U UG/KG Benzo-a-Pyrene

600 U UG/KG Dimethyl Phthalate 600 UJ UG/KG Indeno (1,2,3-cd) Pyrene600 U UG/KG 2,6-Dinitrotoluene 600 UJ UG/KG Dibenzo(a,h)Anthracene600 U UG/KG Acenaphthylene 600 UJ UG/KG Benzo(ghi)Perylene

1500 U UG/KG 3-Nitroaniline 45 % % Moisture

600 U UG/KG Acenaphthene

1500 UJ UG/KG 2,4-Dinitrophenol1500 UJ UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9543 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 11:15

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH5 D No: 3AH5 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSD04 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

13000 J UG/KG 28 UNKNOWNS

N UG/KG PETROLEUM PRODUCT

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9544 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 11:25

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AH6 D No: 3AH6 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSD04D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

490 UJ UG/KG Benzaldehyde 490 U UG/KG Dibenzofuran490 U UG/KG Phenol 490 U UG/KG 2,4-Dinitrotoluene490 U UG/KG bis(2-Chloroethyl) Ether 490 U UG/KG Diethyl Phthalate490 U UG/KG 2-Chlorophenol 490 U UG/KG Fluorene490 U UG/KG 2-Methylphenol 490 U UG/KG 4-Chlorophenyl Phenyl E490 U UG/KG bis(2-Chloroisopropyl) Ether 1200 U UG/KG 4-Nitroaniline490 U UG/KG Acetophenone 1200 UJ UG/KG 2-Methyl-4,6-Dinitrophen490 U UG/KG (3-and/or 4-)Methylphenol 490 U UG/KG n-Nitrosodiphenylamine/490 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze490 U UG/KG Hexachloroethane 490 U UG/KG 4-Bromophenyl Phenyl E490 U UG/KG Nitrobenzene 490 U UG/KG Hexachlorobenzene (HC490 U UG/KG Isophorone 490 UJ UG/KG Atrazine490 U UG/KG 2-Nitrophenol 1200 UJ UG/KG Pentachlorophenol490 U UG/KG 2,4-Dimethylphenol 180 J UG/KG Phenanthrene490 U UG/KG bis(2-Chloroethoxy)Methane 490 U UG/KG Anthracene490 U UG/KG 2,4-Dichlorophenol 490 U UG/KG Carbazole490 U UG/KG Naphthalene 490 U UG/KG Di-n-Butylphthalate490 U UG/KG 4-Chloroaniline 530 UG/KG Fluoranthene490 U UG/KG Hexachlorobutadiene 460 J UG/KG Pyrene490 UR UG/KG Caprolactam 490 U UG/KG Benzyl Butyl Phthalate490 U UG/KG 4-Chloro-3-Methylphenol 490 UJ UG/KG 3,3'-Dichlorobenzidine490 U UG/KG 2-Methylnaphthalene 180 J UG/KG Benzo(a)Anthracene490 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 270 J UG/KG Chrysene490 U UG/KG 2,4,6-Trichlorophenol 490 U UG/KG bis(2-Ethylhexyl) Phthala

1200 U UG/KG 2,4,5-Trichlorophenol 490 U UG/KG Di-n-Octylphthalate

490 U UG/KG 1,1-Biphenyl 280 J UG/KG Benzo(b)Fluoranthene490 U UG/KG 2-Chloronaphthalene 200 J UG/KG Benzo(k)Fluoranthene

1200 U UG/KG 2-Nitroaniline 230 J UG/KG Benzo-a-Pyrene

490 U UG/KG Dimethyl Phthalate 210 J UG/KG Indeno (1,2,3-cd) Pyrene490 U UG/KG 2,6-Dinitrotoluene 490 UJ UG/KG Dibenzo(a,h)Anthracene490 U UG/KG Acenaphthylene 250 J UG/KG Benzo(ghi)Perylene

1200 U UG/KG 3-Nitroaniline 32 % % Moisture

490 U UG/KG Acenaphthene

1200 UJ UG/KG 2,4-Dinitrophenol1200 UJ UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9544 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 11:25

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH6 D No: 3AH6 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSD04D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

6900 J UG/KG 27 UNKNOWNS

N UG/KG PETROLEUM PRODUCT

250 NJ UG/KG BENZO [E] PYRENE

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9545 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 11:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AH7 D No: 3AH7 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSD05 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

660 UJ UG/KG Benzaldehyde 660 U UG/KG Dibenzofuran660 U UG/KG Phenol 660 U UG/KG 2,4-Dinitrotoluene660 U UG/KG bis(2-Chloroethyl) Ether 660 U UG/KG Diethyl Phthalate660 U UG/KG 2-Chlorophenol 660 U UG/KG Fluorene660 U UG/KG 2-Methylphenol 660 U UG/KG 4-Chlorophenyl Phenyl E660 U UG/KG bis(2-Chloroisopropyl) Ether 1700 U UG/KG 4-Nitroaniline660 U UG/KG Acetophenone 1700 UJ UG/KG 2-Methyl-4,6-Dinitrophen660 U UG/KG (3-and/or 4-)Methylphenol 660 U UG/KG n-Nitrosodiphenylamine/660 U UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze660 U UG/KG Hexachloroethane 660 U UG/KG 4-Bromophenyl Phenyl E660 U UG/KG Nitrobenzene 660 U UG/KG Hexachlorobenzene (HC660 U UG/KG Isophorone 660 UJ UG/KG Atrazine660 U UG/KG 2-Nitrophenol 1700 UJ UG/KG Pentachlorophenol660 U UG/KG 2,4-Dimethylphenol 660 U UG/KG Phenanthrene660 U UG/KG bis(2-Chloroethoxy)Methane 660 U UG/KG Anthracene660 U UG/KG 2,4-Dichlorophenol 660 U UG/KG Carbazole660 U UG/KG Naphthalene 660 U UG/KG Di-n-Butylphthalate660 U UG/KG 4-Chloroaniline 660 U UG/KG Fluoranthene660 U UG/KG Hexachlorobutadiene 660 U UG/KG Pyrene660 UR UG/KG Caprolactam 660 U UG/KG Benzyl Butyl Phthalate660 U UG/KG 4-Chloro-3-Methylphenol 660 U UG/KG 3,3'-Dichlorobenzidine660 U UG/KG 2-Methylnaphthalene 660 U UG/KG Benzo(a)Anthracene660 UJ UG/KG Hexachlorocyclopentadiene (HCCP) 660 U UG/KG Chrysene660 U UG/KG 2,4,6-Trichlorophenol 200 J UG/KG bis(2-Ethylhexyl) Phthala

1700 U UG/KG 2,4,5-Trichlorophenol 660 U UG/KG Di-n-Octylphthalate

660 U UG/KG 1,1-Biphenyl 660 U UG/KG Benzo(b)Fluoranthene660 U UG/KG 2-Chloronaphthalene 660 U UG/KG Benzo(k)Fluoranthene

1700 U UG/KG 2-Nitroaniline 660 U UG/KG Benzo-a-Pyrene

660 U UG/KG Dimethyl Phthalate 660 UJ UG/KG Indeno (1,2,3-cd) Pyrene660 U UG/KG 2,6-Dinitrotoluene 660 UJ UG/KG Dibenzo(a,h)Anthracene660 U UG/KG Acenaphthylene 660 UJ UG/KG Benzo(ghi)Perylene

1700 U UG/KG 3-Nitroaniline 50 % % Moisture

660 U UG/KG Acenaphthene

1700 UJ UG/KG 2,4-Dinitrophenol1700 UJ UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9545 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 11:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH7 D No: 3AH7 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSD05 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

14000 J UG/KG 26 UNKNOWNS

N UG/KG PETROLEUM PRODUCT

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9546 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 10:10

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AH8 D No: 3AH8 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSD01 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

660 U UG/KG Benzaldehyde 660 U UG/KG Dibenzofuran660 U UG/KG Phenol 660 U UG/KG 2,4-Dinitrotoluene660 U UG/KG bis(2-Chloroethyl) Ether 660 U UG/KG Diethyl Phthalate660 U UG/KG 2-Chlorophenol 660 U UG/KG Fluorene660 U UG/KG 2-Methylphenol 660 UJ UG/KG 4-Chlorophenyl Phenyl E660 UJ UG/KG bis(2-Chloroisopropyl) Ether 1700 U UG/KG 4-Nitroaniline660 U UG/KG Acetophenone 1700 U UG/KG 2-Methyl-4,6-Dinitrophen660 U UG/KG (3-and/or 4-)Methylphenol 660 U UG/KG n-Nitrosodiphenylamine/660 UJ UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze660 UJ UG/KG Hexachloroethane 660 U UG/KG 4-Bromophenyl Phenyl E660 U UG/KG Nitrobenzene 660 UJ UG/KG Hexachlorobenzene (HC660 U UG/KG Isophorone 660 U UG/KG Atrazine660 U UG/KG 2-Nitrophenol 1700 U UG/KG Pentachlorophenol660 U UG/KG 2,4-Dimethylphenol 660 U UG/KG Phenanthrene660 U UG/KG bis(2-Chloroethoxy)Methane 660 U UG/KG Anthracene660 U UG/KG 2,4-Dichlorophenol 660 U UG/KG Carbazole660 U UG/KG Naphthalene 660 U UG/KG Di-n-Butylphthalate660 U UG/KG 4-Chloroaniline 660 U UG/KG Fluoranthene660 U UG/KG Hexachlorobutadiene 660 U UG/KG Pyrene660 U UG/KG Caprolactam 660 U UG/KG Benzyl Butyl Phthalate660 U UG/KG 4-Chloro-3-Methylphenol 660 U UG/KG 3,3'-Dichlorobenzidine660 U UG/KG 2-Methylnaphthalene 660 U UG/KG Benzo(a)Anthracene660 U UG/KG Hexachlorocyclopentadiene (HCCP) 660 U UG/KG Chrysene660 U UG/KG 2,4,6-Trichlorophenol 660 U UG/KG bis(2-Ethylhexyl) Phthala

1700 U UG/KG 2,4,5-Trichlorophenol 660 U UG/KG Di-n-Octylphthalate

660 U UG/KG 1,1-Biphenyl 660 U UG/KG Benzo(b)Fluoranthene660 U UG/KG 2-Chloronaphthalene 660 U UG/KG Benzo(k)Fluoranthene

1700 UJ UG/KG 2-Nitroaniline 660 U UG/KG Benzo-a-Pyrene

660 U UG/KG Dimethyl Phthalate 660 U UG/KG Indeno (1,2,3-cd) Pyrene660 U UG/KG 2,6-Dinitrotoluene 660 U UG/KG Dibenzo(a,h)Anthracene660 U UG/KG Acenaphthylene 660 U UG/KG Benzo(ghi)Perylene

1700 U UG/KG 3-Nitroaniline 50 % % Moisture

660 U UG/KG Acenaphthene

1700 U UG/KG 2,4-Dinitrophenol1700 U UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9546 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 10:10

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH8 D No: 3AH8 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSD01 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

200 J UG/KG SUBSTITUTED NAPHTHALENE390 NJ UG/KG 1,1'-BIPHENYL, BIS(1-METHYLETHYL)-

8900 J UG/KG 27 UNKNOWNS

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9547 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 11:05

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AH9 D No: 3AH9 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSD01D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

660 U UG/KG Benzaldehyde 660 U UG/KG Dibenzofuran660 U UG/KG Phenol 660 U UG/KG 2,4-Dinitrotoluene660 U UG/KG bis(2-Chloroethyl) Ether 660 U UG/KG Diethyl Phthalate660 U UG/KG 2-Chlorophenol 660 U UG/KG Fluorene660 U UG/KG 2-Methylphenol 660 UJ UG/KG 4-Chlorophenyl Phenyl E660 UJ UG/KG bis(2-Chloroisopropyl) Ether 1700 U UG/KG 4-Nitroaniline660 U UG/KG Acetophenone 1700 U UG/KG 2-Methyl-4,6-Dinitrophen660 U UG/KG (3-and/or 4-)Methylphenol 660 U UG/KG n-Nitrosodiphenylamine/660 UJ UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze660 UJ UG/KG Hexachloroethane 660 U UG/KG 4-Bromophenyl Phenyl E660 U UG/KG Nitrobenzene 660 UJ UG/KG Hexachlorobenzene (HC660 U UG/KG Isophorone 660 U UG/KG Atrazine660 U UG/KG 2-Nitrophenol 1700 U UG/KG Pentachlorophenol660 U UG/KG 2,4-Dimethylphenol 660 U UG/KG Phenanthrene660 U UG/KG bis(2-Chloroethoxy)Methane 660 U UG/KG Anthracene660 U UG/KG 2,4-Dichlorophenol 660 U UG/KG Carbazole660 U UG/KG Naphthalene 660 U UG/KG Di-n-Butylphthalate660 U UG/KG 4-Chloroaniline 660 U UG/KG Fluoranthene660 U UG/KG Hexachlorobutadiene 660 U UG/KG Pyrene660 U UG/KG Caprolactam 660 U UG/KG Benzyl Butyl Phthalate660 U UG/KG 4-Chloro-3-Methylphenol 660 U UG/KG 3,3'-Dichlorobenzidine660 U UG/KG 2-Methylnaphthalene 660 U UG/KG Benzo(a)Anthracene660 U UG/KG Hexachlorocyclopentadiene (HCCP) 660 U UG/KG Chrysene660 U UG/KG 2,4,6-Trichlorophenol 660 U UG/KG bis(2-Ethylhexyl) Phthala

1700 U UG/KG 2,4,5-Trichlorophenol 660 U UG/KG Di-n-Octylphthalate

660 U UG/KG 1,1-Biphenyl 660 U UG/KG Benzo(b)Fluoranthene660 U UG/KG 2-Chloronaphthalene 660 U UG/KG Benzo(k)Fluoranthene

1700 UJ UG/KG 2-Nitroaniline 660 U UG/KG Benzo-a-Pyrene

660 U UG/KG Dimethyl Phthalate 660 U UG/KG Indeno (1,2,3-cd) Pyrene660 U UG/KG 2,6-Dinitrotoluene 660 U UG/KG Dibenzo(a,h)Anthracene660 U UG/KG Acenaphthylene 660 U UG/KG Benzo(ghi)Perylene

1700 U UG/KG 3-Nitroaniline 50 % % Moisture

660 U UG/KG Acenaphthene

1700 U UG/KG 2,4-Dinitrophenol1700 U UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9547 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 11:05

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH9 D No: 3AH9 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSD01D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

280 NJ UG/KG BICYCLO[3.1.1] HEPT-2-ENE, 2,6,6-TRIMETHYL240 NJ UG/KG BENZENE, 1-METHYL-4-(1-METHYLETHYL)-490 NJ UG/KG 1,1'-BIPHENYL, BIS(1-METHYLETHYL)-200 J UG/KG UNKNOWN ALDEHYDE600 NJ UG/KG ANDROSTAN-6-ONE, (5.ALPHA.)-

8400 J UG/KG 24 UNKNOWNS

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9548 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 12:00

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AJ0 D No: 3AJ0 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSD02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

430 U UG/KG Benzaldehyde 430 U UG/KG Dibenzofuran430 U UG/KG Phenol 430 U UG/KG 2,4-Dinitrotoluene430 U UG/KG bis(2-Chloroethyl) Ether 430 U UG/KG Diethyl Phthalate430 U UG/KG 2-Chlorophenol 430 U UG/KG Fluorene430 U UG/KG 2-Methylphenol 430 UJ UG/KG 4-Chlorophenyl Phenyl E430 UJ UG/KG bis(2-Chloroisopropyl) Ether 1100 U UG/KG 4-Nitroaniline430 U UG/KG Acetophenone 1100 U UG/KG 2-Methyl-4,6-Dinitrophen430 U UG/KG (3-and/or 4-)Methylphenol 430 U UG/KG n-Nitrosodiphenylamine/430 UJ UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze430 UJ UG/KG Hexachloroethane 430 U UG/KG 4-Bromophenyl Phenyl E430 U UG/KG Nitrobenzene 430 UJ UG/KG Hexachlorobenzene (HC430 U UG/KG Isophorone 430 U UG/KG Atrazine430 U UG/KG 2-Nitrophenol 1100 U UG/KG Pentachlorophenol430 U UG/KG 2,4-Dimethylphenol 1200 UG/KG Phenanthrene430 U UG/KG bis(2-Chloroethoxy)Methane 110 J UG/KG Anthracene430 U UG/KG 2,4-Dichlorophenol 430 U UG/KG Carbazole

1100 UG/KG Naphthalene 430 U UG/KG Di-n-Butylphthalate

430 U UG/KG 4-Chloroaniline 430 U UG/KG Fluoranthene430 U UG/KG Hexachlorobutadiene 130 J UG/KG Pyrene430 U UG/KG Caprolactam 430 U UG/KG Benzyl Butyl Phthalate430 U UG/KG 4-Chloro-3-Methylphenol 430 U UG/KG 3,3'-Dichlorobenzidine

4100 UG/KG 2-Methylnaphthalene 430 U UG/KG Benzo(a)Anthracene

430 U UG/KG Hexachlorocyclopentadiene (HCCP) 430 U UG/KG Chrysene430 U UG/KG 2,4,6-Trichlorophenol 430 U UG/KG bis(2-Ethylhexyl) Phthala

1100 U UG/KG 2,4,5-Trichlorophenol 430 U UG/KG Di-n-Octylphthalate1100 UG/KG 1,1-Biphenyl 430 U UG/KG Benzo(b)Fluoranthene

430 U UG/KG 2-Chloronaphthalene 430 U UG/KG Benzo(k)Fluoranthene

1100 UJ UG/KG 2-Nitroaniline 430 U UG/KG Benzo-a-Pyrene

430 U UG/KG Dimethyl Phthalate 430 U UG/KG Indeno (1,2,3-cd) Pyrene430 U UG/KG 2,6-Dinitrotoluene 430 U UG/KG Dibenzo(a,h)Anthracene430 U UG/KG Acenaphthylene 430 U UG/KG Benzo(ghi)Perylene

1100 U UG/KG 3-Nitroaniline 24 % % Moisture

430 U UG/KG Acenaphthene

1100 U UG/KG 2,4-Dinitrophenol1100 U UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9548 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 12:00

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ0 D No: 3AJ0 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSD02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

18000 J UG/KG 27 UNKNOWNS

520 NJ UG/KG NAPHTHALENE, 1-METHYL200 NJ UG/KG NAPHTHALENE, 1,2,3,4-TETRAHYDRO-5,6-DIMETHYL190 NJ UG/KG NAPHTHALENE, 1,5-DIMETHYL530 NJ UG/KG NAPHTHALENE, 2,6-DIMETHYL170 NJ UG/KG NAPHTHALENE, 2-(1-METHYLETHYL)-210 NJ UG/KG NAPHTHALENE, 1,4,6-TRIMETHYL2400 NJ UG/KG DIBENZOTHIOPHENE, 4-METHYL-

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9549 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 13:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AJ1 D No: 3AJ1 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSF05 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

370 U UG/KG Benzaldehyde 370 U UG/KG Dibenzofuran370 U UG/KG Phenol 370 U UG/KG 2,4-Dinitrotoluene370 U UG/KG bis(2-Chloroethyl) Ether 370 U UG/KG Diethyl Phthalate370 U UG/KG 2-Chlorophenol 370 U UG/KG Fluorene370 U UG/KG 2-Methylphenol 370 UJ UG/KG 4-Chlorophenyl Phenyl E370 UJ UG/KG bis(2-Chloroisopropyl) Ether 920 U UG/KG 4-Nitroaniline370 U UG/KG Acetophenone 920 U UG/KG 2-Methyl-4,6-Dinitrophen370 U UG/KG (3-and/or 4-)Methylphenol 370 U UG/KG n-Nitrosodiphenylamine/370 UJ UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze370 UJ UG/KG Hexachloroethane 370 U UG/KG 4-Bromophenyl Phenyl E370 U UG/KG Nitrobenzene 370 UJ UG/KG Hexachlorobenzene (HC370 U UG/KG Isophorone 370 U UG/KG Atrazine370 U UG/KG 2-Nitrophenol 920 U UG/KG Pentachlorophenol370 U UG/KG 2,4-Dimethylphenol 370 U UG/KG Phenanthrene370 U UG/KG bis(2-Chloroethoxy)Methane 370 U UG/KG Anthracene370 U UG/KG 2,4-Dichlorophenol 370 U UG/KG Carbazole370 U UG/KG Naphthalene 370 U UG/KG Di-n-Butylphthalate370 U UG/KG 4-Chloroaniline 370 U UG/KG Fluoranthene370 U UG/KG Hexachlorobutadiene 370 U UG/KG Pyrene370 U UG/KG Caprolactam 370 U UG/KG Benzyl Butyl Phthalate370 U UG/KG 4-Chloro-3-Methylphenol 370 U UG/KG 3,3'-Dichlorobenzidine370 U UG/KG 2-Methylnaphthalene 370 U UG/KG Benzo(a)Anthracene370 U UG/KG Hexachlorocyclopentadiene (HCCP) 370 U UG/KG Chrysene370 U UG/KG 2,4,6-Trichlorophenol 370 U UG/KG bis(2-Ethylhexyl) Phthala920 U UG/KG 2,4,5-Trichlorophenol 370 U UG/KG Di-n-Octylphthalate370 U UG/KG 1,1-Biphenyl 370 U UG/KG Benzo(b)Fluoranthene370 U UG/KG 2-Chloronaphthalene 370 U UG/KG Benzo(k)Fluoranthene920 UJ UG/KG 2-Nitroaniline 370 U UG/KG Benzo-a-Pyrene370 U UG/KG Dimethyl Phthalate 370 U UG/KG Indeno (1,2,3-cd) Pyrene370 U UG/KG 2,6-Dinitrotoluene 370 U UG/KG Dibenzo(a,h)Anthracene370 U UG/KG Acenaphthylene 370 U UG/KG Benzo(ghi)Perylene920 U UG/KG 3-Nitroaniline 10 % % Moisture370 U UG/KG Acenaphthene920 U UG/KG 2,4-Dinitrophenol920 U UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9549 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 13:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ1 D No: 3AJ1 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSF05 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

330 NJ UG/KG CYCLOHEXENE, 1-METHYL-4-(1-METHYLETHENYL)-240 NJ UG/KG N-HEXADECANOIC ACID

24000 J UG/KG 23 UNKNOWNS

700 NJ UG/KG .GAMMA.-SITOSTEROL

1200 NJ UG/KG STIGMAST-4-EN-3-ONE1700 NJ UG/KG 2 PHENANTHRENECARBOXYLIC ACIDS

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9550 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 13:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AJ2 D No: 3AJ2 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSF04 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

380 U UG/KG Benzaldehyde 380 U UG/KG Dibenzofuran380 U UG/KG Phenol 380 U UG/KG 2,4-Dinitrotoluene380 U UG/KG bis(2-Chloroethyl) Ether 380 U UG/KG Diethyl Phthalate380 U UG/KG 2-Chlorophenol 380 U UG/KG Fluorene380 U UG/KG 2-Methylphenol 380 UJ UG/KG 4-Chlorophenyl Phenyl E380 UJ UG/KG bis(2-Chloroisopropyl) Ether 940 U UG/KG 4-Nitroaniline380 U UG/KG Acetophenone 940 U UG/KG 2-Methyl-4,6-Dinitrophen380 U UG/KG (3-and/or 4-)Methylphenol 380 U UG/KG n-Nitrosodiphenylamine/380 UJ UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze380 UJ UG/KG Hexachloroethane 380 U UG/KG 4-Bromophenyl Phenyl E380 U UG/KG Nitrobenzene 380 UJ UG/KG Hexachlorobenzene (HC380 U UG/KG Isophorone 380 U UG/KG Atrazine380 U UG/KG 2-Nitrophenol 940 U UG/KG Pentachlorophenol380 U UG/KG 2,4-Dimethylphenol 380 U UG/KG Phenanthrene380 U UG/KG bis(2-Chloroethoxy)Methane 380 U UG/KG Anthracene380 U UG/KG 2,4-Dichlorophenol 380 U UG/KG Carbazole380 U UG/KG Naphthalene 380 U UG/KG Di-n-Butylphthalate380 U UG/KG 4-Chloroaniline 380 U UG/KG Fluoranthene380 U UG/KG Hexachlorobutadiene 380 U UG/KG Pyrene380 U UG/KG Caprolactam 380 U UG/KG Benzyl Butyl Phthalate380 U UG/KG 4-Chloro-3-Methylphenol 380 U UG/KG 3,3'-Dichlorobenzidine380 U UG/KG 2-Methylnaphthalene 380 U UG/KG Benzo(a)Anthracene380 U UG/KG Hexachlorocyclopentadiene (HCCP) 380 U UG/KG Chrysene380 U UG/KG 2,4,6-Trichlorophenol 380 U UG/KG bis(2-Ethylhexyl) Phthala940 U UG/KG 2,4,5-Trichlorophenol 380 U UG/KG Di-n-Octylphthalate380 U UG/KG 1,1-Biphenyl 380 U UG/KG Benzo(b)Fluoranthene380 U UG/KG 2-Chloronaphthalene 380 U UG/KG Benzo(k)Fluoranthene940 UJ UG/KG 2-Nitroaniline 380 U UG/KG Benzo-a-Pyrene380 U UG/KG Dimethyl Phthalate 380 U UG/KG Indeno (1,2,3-cd) Pyrene380 U UG/KG 2,6-Dinitrotoluene 380 U UG/KG Dibenzo(a,h)Anthracene380 U UG/KG Acenaphthylene 380 U UG/KG Benzo(ghi)Perylene940 U UG/KG 3-Nitroaniline 12 % % Moisture380 U UG/KG Acenaphthene940 U UG/KG 2,4-Dinitrophenol940 U UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9550 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 13:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ2 D No: 3AJ2 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSF04 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

10000 J UG/KG 25 UNKNOWNS

150 NJ UG/KG PHENANTHRENE, 1-METHYL-7-(1-METHYLETHYL)-360 NJ UG/KG SUBSTITUTED PHENANTHRENECARBOXYLIC ACID530 NJ UG/KG .GAMMA.-SITOSTEROL350 NJ UG/KG LONGIFOLENALDEHYDE

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9551 2005 05-0928 Produced by: Appleby, Charlie 

Extractables Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 14:05

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AJ3 D No: 3AJ3 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSF03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

380 U UG/KG Benzaldehyde 380 U UG/KG Dibenzofuran380 U UG/KG Phenol 380 U UG/KG 2,4-Dinitrotoluene380 U UG/KG bis(2-Chloroethyl) Ether 380 U UG/KG Diethyl Phthalate380 U UG/KG 2-Chlorophenol 380 U UG/KG Fluorene380 U UG/KG 2-Methylphenol 380 UJ UG/KG 4-Chlorophenyl Phenyl E380 UJ UG/KG bis(2-Chloroisopropyl) Ether 970 U UG/KG 4-Nitroaniline380 U UG/KG Acetophenone 970 U UG/KG 2-Methyl-4,6-Dinitrophen380 U UG/KG (3-and/or 4-)Methylphenol 380 U UG/KG n-Nitrosodiphenylamine/380 UJ UG/KG n-Nitroso di-n-Propylamine NA UG/KG 1,2,4,5-Tetrachlorobenze380 UJ UG/KG Hexachloroethane 380 U UG/KG 4-Bromophenyl Phenyl E380 U UG/KG Nitrobenzene 380 UJ UG/KG Hexachlorobenzene (HC380 U UG/KG Isophorone 380 U UG/KG Atrazine380 U UG/KG 2-Nitrophenol 970 U UG/KG Pentachlorophenol380 U UG/KG 2,4-Dimethylphenol 380 U UG/KG Phenanthrene380 U UG/KG bis(2-Chloroethoxy)Methane 380 U UG/KG Anthracene380 U UG/KG 2,4-Dichlorophenol 380 U UG/KG Carbazole380 U UG/KG Naphthalene 380 U UG/KG Di-n-Butylphthalate380 U UG/KG 4-Chloroaniline 380 U UG/KG Fluoranthene380 U UG/KG Hexachlorobutadiene 380 U UG/KG Pyrene380 U UG/KG Caprolactam 380 U UG/KG Benzyl Butyl Phthalate380 U UG/KG 4-Chloro-3-Methylphenol 380 U UG/KG 3,3'-Dichlorobenzidine380 U UG/KG 2-Methylnaphthalene 380 U UG/KG Benzo(a)Anthracene380 U UG/KG Hexachlorocyclopentadiene (HCCP) 380 U UG/KG Chrysene380 U UG/KG 2,4,6-Trichlorophenol 380 U UG/KG bis(2-Ethylhexyl) Phthala970 U UG/KG 2,4,5-Trichlorophenol 380 U UG/KG Di-n-Octylphthalate380 U UG/KG 1,1-Biphenyl 380 U UG/KG Benzo(b)Fluoranthene380 U UG/KG 2-Chloronaphthalene 380 U UG/KG Benzo(k)Fluoranthene970 UJ UG/KG 2-Nitroaniline 380 U UG/KG Benzo-a-Pyrene380 U UG/KG Dimethyl Phthalate 380 U UG/KG Indeno (1,2,3-cd) Pyrene380 U UG/KG 2,6-Dinitrotoluene 380 U UG/KG Dibenzo(a,h)Anthracene380 U UG/KG Acenaphthylene 380 U UG/KG Benzo(ghi)Perylene970 U UG/KG 3-Nitroaniline 14 % % Moisture380 U UG/KG Acenaphthene970 U UG/KG 2,4-Dinitrophenol970 U UG/KG 4-Nitrophenol

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9551 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 14:05

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ3 D No: 3AJ3 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSF03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

4000 J UG/KG 20 UNKNOWNS

930 NJ UG/KG SUBSTITUTED PHENANTHRENE CARBOXYLIC ACID

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9518 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 10:35

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ4 D No: 3AJ4 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSF08 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

4300 MG/KG Aluminum

6.4 UJ MG/KG Antimony1.7 MG/KG Arsenic

17 J MG/KG Barium

0.29 UJ MG/KG Beryllium0.05 UJ MG/KG Cadmium

15000 MG/KG Calcium

16 J MG/KG Chromium

2.2 J MG/KG Cobalt

23 MG/KG Copper

4300 J MG/KG Iron

6.6 J MG/KG Lead

890 MG/KG Magnesium

45 J MG/KG Manganese

0.11 U MG/KG Total Mercury

64 MG/KG Nickel

220 J MG/KG Potassium

1.5 J MG/KG Selenium1.1 U MG/KG Silver

300 J MG/KG Sodium

2.7 U MG/KG Thallium

240 MG/KG Vanadium

95 MG/KG Zinc

NA MG/KG Cyanide

7 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9519 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 11:15

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ5 D No: 3AJ5 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD07 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

11000 MG/KG Aluminum

12 UJ MG/KG Antimony

2.9 MG/KG Arsenic

37 J MG/KG Barium

0.51 UJ MG/KG Beryllium0.29 UJ MG/KG Cadmium

7700 MG/KG Calcium

28 J MG/KG Chromium

2.5 J MG/KG Cobalt

20 MG/KG Copper

8600 J MG/KG Iron

63 J MG/KG Lead

3200 MG/KG Magnesium

93 J MG/KG Manganese

0.07 UJ MG/KG Total Mercury

8.7 MG/KG Nickel

1300 MG/KG Potassium

3.1 J MG/KG Selenium1.9 U MG/KG Silver

7700 MG/KG Sodium

4.9 U MG/KG Thallium

60 MG/KG Vanadium

120 MG/KG Zinc

NA MG/KG Cyanide

49 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9520 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 11:30

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ6 D No: 3AJ6 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSF02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

4000 MG/KG Aluminum

7.7 UJ MG/KG Antimony

0.64 J MG/KG Arsenic

8.0 J MG/KG Barium

0.08 UJ MG/KG Beryllium0.07 UJ MG/KG Cadmium

660 MG/KG Calcium

4.0 J MG/KG Chromium

0.34 J MG/KG Cobalt

2.6 J MG/KG Copper

1300 J MG/KG Iron

15 J MG/KG Lead

190 J MG/KG Magnesium

4.6 J MG/KG Manganese

0.03 UJ MG/KG Total Mercury

1.2 J MG/KG Nickel

110 J MG/KG Potassium

0.48 R MG/KG Selenium

1.3 U MG/KG Silver

520 J MG/KG Sodium

3.2 U MG/KG Thallium7.1 MG/KG Vanadium

16 MG/KG Zinc

NA MG/KG Cyanide

22 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9521 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 11:30

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ7 D No: 3AJ7 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSF02S / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

4200 MG/KG Aluminum

7.7 UJ MG/KG Antimony

0.68 R MG/KG Arsenic

8.6 J MG/KG Barium

0.08 UJ MG/KG Beryllium0.04 UJ MG/KG Cadmium

690 MG/KG Calcium

4.2 J MG/KG Chromium

0.38 J MG/KG Cobalt

2.7 J MG/KG Copper

1400 J MG/KG Iron

18 J MG/KG Lead

190 J MG/KG Magnesium

5.1 J MG/KG Manganese

0.03 UJ MG/KG Total Mercury

1.4 J MG/KG Nickel

110 J MG/KG Potassium

4.5 U MG/KG Selenium1.3 U MG/KG Silver

530 J MG/KG Sodium

3.2 U MG/KG Thallium7.5 MG/KG Vanadium

16 MG/KG Zinc

NA MG/KG Cyanide

22 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9522 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 10:55

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ8 D No: 3AJ8 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSF01 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

7500 MG/KG Aluminum

0.24 R MG/KG Antimony

1.7 MG/KG Arsenic

13 J MG/KG Barium

0.13 UJ MG/KG Beryllium0.17 UJ MG/KG Cadmium

9800 MG/KG Calcium

9.2 J MG/KG Chromium

0.69 J MG/KG Cobalt

3.6 MG/KG Copper

5100 J MG/KG Iron

8.4 J MG/KG Lead

300 J MG/KG Magnesium

16 J MG/KG Manganese

0.38 MG/KG Total Mercury

3.6 J MG/KG Nickel

200 J MG/KG Potassium

3.9 U MG/KG Selenium1.1 U MG/KG Silver

470 J MG/KG Sodium

2.8 U MG/KG Thallium

15 MG/KG Vanadium18 MG/KG Zinc

NA MG/KG Cyanide

9 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9523 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 11:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ9 D No: 3AJ9 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD06 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

16000 MG/KG Aluminum

0.76 R MG/KG Antimony

10 MG/KG Arsenic59 MG/KG Barium

1.3 MG/KG Beryllium

0.34 UJ MG/KG Cadmium

43000 MG/KG Calcium

60 J MG/KG Chromium14 MG/KG Cobalt15 MG/KG Copper

21000 J MG/KG Iron

26 J MG/KG Lead

11000 MG/KG Magnesium

890 J MG/KG Manganese

0.20 U MG/KG Total Mercury

20 MG/KG Nickel

2300 MG/KG Potassium

6.8 U MG/KG Selenium2.0 U MG/KG Silver

8600 MG/KG Sodium

0.72 R MG/KG Thallium

41 MG/KG Vanadium

130 MG/KG Zinc

NA MG/KG Cyanide

49 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9524 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 12:35

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AK0 D No: 3AK0 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD05 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

8900 MG/KG Aluminum

26 UJ MG/KG Antimony

3.8 J MG/KG Arsenic

74 J MG/KG Barium

0.82 UJ MG/KG Beryllium

2.2 U MG/KG Cadmium

5100 MG/KG Calcium

95 J MG/KG Chromium

4.1 J MG/KG Cobalt

33 MG/KG Copper

8500 J MG/KG Iron

23 J MG/KG Lead

4300 MG/KG Magnesium

54 J MG/KG Manganese

0.17 UJ MG/KG Total Mercury

64 MG/KG Nickel

1400 J MG/KG Potassium

24 MG/KG Selenium

4.3 U MG/KG Silver

22000 MG/KG Sodium

11 U MG/KG Thallium

590 MG/KG Vanadium150 MG/KG Zinc

NA MG/KG Cyanide

77 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9525 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 12:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AK1 D No: 3AK1 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD05D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

8900 MG/KG Aluminum

30 UJ MG/KG Antimony

3.3 J MG/KG Arsenic

50 J MG/KG Barium

0.79 UJ MG/KG Beryllium

2.5 U MG/KG Cadmium

5000 MG/KG Calcium

80 J MG/KG Chromium

2.7 J MG/KG Cobalt

30 MG/KG Copper

6500 J MG/KG Iron

25 J MG/KG Lead

4400 MG/KG Magnesium

51 J MG/KG Manganese

0.14 UJ MG/KG Total Mercury

47 MG/KG Nickel

1500 J MG/KG Potassium

21 MG/KG Selenium

4.9 U MG/KG Silver

25000 MG/KG Sodium

12 U MG/KG Thallium

500 MG/KG Vanadium130 MG/KG Zinc

NA MG/KG Cyanide

80 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9526 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 12:40

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AK2 D No: 3AK2 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

6800 MG/KG Aluminum

14 UJ MG/KG Antimony

3.3 MG/KG Arsenic

11 J MG/KG Barium

0.32 UJ MG/KG Beryllium

1.2 U MG/KG Cadmium

1200 J MG/KG Calcium

14 J MG/KG Chromium

1.8 J MG/KG Cobalt6.8 MG/KG Copper

9200 J MG/KG Iron

8.0 J MG/KG Lead

2400 MG/KG Magnesium

51 J MG/KG Manganese

0.24 U MG/KG Total Mercury

5.9 J MG/KG Nickel

1400 MG/KG Potassium

8.4 U MG/KG Selenium2.4 U MG/KG Silver

9900 MG/KG Sodium

6.0 U MG/KG Thallium

28 MG/KG Vanadium30 MG/KG Zinc

NA MG/KG Cyanide

58 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9527 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 13:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AK5 D No: 3AK5 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD04 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

4000 MG/KG Aluminum

0.49 R MG/KG Antimony

1.5 J MG/KG Arsenic7.3 J MG/KG Barium

0.06 J MG/KG Beryllium0.67 U MG/KG Cadmium

3000 MG/KG Calcium

5.6 MG/KG Chromium

0.66 J MG/KG Cobalt

2.0 J MG/KG Copper

5800 MG/KG Iron

3.0 MG/KG Lead

610 J MG/KG Magnesium

32 J MG/KG Manganese

0.13 U MG/KG Total Mercury

2.5 J MG/KG Nickel

240 J MG/KG Potassium

4.7 U MG/KG Selenium1.3 U MG/KG Silver

2800 MG/KG Sodium

3.3 U MG/KG Thallium9.8 MG/KG Vanadium9.5 MG/KG Zinc

NA MG/KG Cyanide

25 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9528 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 12:25

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AF9 D No: 3AF9 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSD01 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

15000 MG/KG Aluminum

1.1 R MG/KG Antimony

18 J MG/KG Arsenic52 J MG/KG Barium

0.97 UJ MG/KG Beryllium

2.5 U MG/KG Cadmium

2300 J MG/KG Calcium

19 J MG/KG Chromium

5.3 J MG/KG Cobalt

14 J MG/KG Copper

41000 J MG/KG Iron

26 J MG/KG Lead

3400 MG/KG Magnesium

190 J MG/KG Manganese

0.50 U MG/KG Total Mercury

8.1 J MG/KG Nickel

1400 J MG/KG Potassium

17 U MG/KG Selenium

5.0 U MG/KG Silver

9600 MG/KG Sodium

12 U MG/KG Thallium38 MG/KG Vanadium85 MG/KG Zinc

NA MG/KG Cyanide

80 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9529 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 12:40

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG0 D No: 3AG0 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSD01D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

11000 MG/KG Aluminum

28 UJ MG/KG Antimony

9.0 J MG/KG Arsenic

79 J MG/KG Barium

0.84 UJ MG/KG Beryllium

2.3 U MG/KG Cadmium

2200 J MG/KG Calcium

14 J MG/KG Chromium

7.8 J MG/KG Cobalt

16 J MG/KG Copper

23000 J MG/KG Iron

17 J MG/KG Lead

3400 MG/KG Magnesium

260 J MG/KG Manganese

0.47 U MG/KG Total Mercury

9.7 J MG/KG Nickel

1500 J MG/KG Potassium

16 U MG/KG Selenium

4.7 U MG/KG Silver

9400 MG/KG Sodium

12 U MG/KG Thallium28 MG/KG Vanadium

110 MG/KG Zinc

NA MG/KG Cyanide

79 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9530 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 13:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG1 D No: 3AG1 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSD02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

9300 MG/KG Aluminum

17 UJ MG/KG Antimony

7.7 J MG/KG Arsenic

160 J MG/KG Barium

0.74 UJ MG/KG Beryllium

1.4 U MG/KG Cadmium

1900 J MG/KG Calcium

13 J MG/KG Chromium

7.4 J MG/KG Cobalt

14 J MG/KG Copper

18000 J MG/KG Iron

14 J MG/KG Lead

3600 MG/KG Magnesium

380 J MG/KG Manganese

0.09 UJ MG/KG Total Mercury

12 J MG/KG Nickel

1900 MG/KG Potassium

9.8 U MG/KG Selenium2.8 U MG/KG Silver

8100 MG/KG Sodium

7.0 U MG/KG Thallium

25 MG/KG Vanadium74 MG/KG Zinc

NA MG/KG Cyanide

64 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9531 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 13:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG2 D No: 3AG2 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSD03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

1900 MG/KG Aluminum

8.1 UJ MG/KG Antimony1.0 J MG/KG Arsenic

390 J MG/KG Barium

0.15 UJ MG/KG Beryllium0.92 MG/KG Cadmium

11000 J MG/KG Calcium

3.6 J MG/KG Chromium1.2 J MG/KG Cobalt2.9 J MG/KG Copper

3500 J MG/KG Iron

8.8 J MG/KG Lead

460 J MG/KG Magnesium160 J MG/KG Manganese

0.14 U MG/KG Total Mercury

1.6 J MG/KG Nickel

200 J MG/KG Potassium

4.7 U MG/KG Selenium1.4 U MG/KG Silver

830 MG/KG Sodium

3.4 U MG/KG Thallium4.3 J MG/KG Vanadium

83 MG/KG Zinc

NA MG/KG Cyanide

26 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9532 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 12:50

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG3 D No: 3AG3 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSF04 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

2600 MG/KG Aluminum

6.9 UJ MG/KG Antimony

0.41 R MG/KG Arsenic

15 J MG/KG Barium

0.03 UJ MG/KG Beryllium0.58 U MG/KG Cadmium

2000 J MG/KG Calcium

2.7 J MG/KG Chromium

0.49 J MG/KG Cobalt

2.0 J MG/KG Copper

1900 J MG/KG Iron

6.6 J MG/KG Lead

160 J MG/KG Magnesium

21 J MG/KG Manganese

0.03 UJ MG/KG Total Mercury

1.2 J MG/KG Nickel

89 J MG/KG Potassium

4.1 U MG/KG Selenium1.2 U MG/KG Silver

530 J MG/KG Sodium

2.9 U MG/KG Thallium4.6 J MG/KG Vanadium

21 MG/KG Zinc

NA MG/KG Cyanide

14 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9533 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 12:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG4 D No: 3AG4 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSF05 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

5400 MG/KG Aluminum

6.9 UJ MG/KG Antimony1.3 J MG/KG Arsenic

16 J MG/KG Barium

0.03 UJ MG/KG Beryllium0.57 U MG/KG Cadmium

320 J MG/KG Calcium

5.3 J MG/KG Chromium

0.87 J MG/KG Cobalt

2.5 J MG/KG Copper

5200 J MG/KG Iron

6.0 J MG/KG Lead

210 J MG/KG Magnesium160 J MG/KG Manganese

0.04 UJ MG/KG Total Mercury

1.6 J MG/KG Nickel

120 J MG/KG Potassium

0.27 R MG/KG Selenium

1.2 U MG/KG Silver

440 J MG/KG Sodium

2.9 U MG/KG Thallium9.8 MG/KG Vanadium6.3 J MG/KG Zinc

NA MG/KG Cyanide

13 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9534 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 12:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG5 D No: 3AG5 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSF05S / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

5500 MG/KG Aluminum

7.0 UJ MG/KG Antimony1.3 J MG/KG Arsenic

16 J MG/KG Barium

0.04 UJ MG/KG Beryllium0.58 U MG/KG Cadmium

380 J MG/KG Calcium

5.1 J MG/KG Chromium

0.91 J MG/KG Cobalt

2.6 J MG/KG Copper

5000 J MG/KG Iron

6.5 J MG/KG Lead

220 J MG/KG Magnesium170 J MG/KG Manganese

0.05 UJ MG/KG Total Mercury

1.6 J MG/KG Nickel

120 J MG/KG Potassium

0.58 J MG/KG Selenium

1.2 U MG/KG Silver

590 MG/KG Sodium

2.9 U MG/KG Thallium9.7 MG/KG Vanadium6.5 J MG/KG Zinc

NA MG/KG Cyanide

14 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9535 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 09:00

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG7 D No: 3AG7 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF OPSD02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

5000 MG/KG Aluminum

1.6 J MG/KG Antimony3.6 J MG/KG Arsenic

81 J MG/KG Barium

0.05 J MG/KG Beryllium0.58 U MG/KG Cadmium

970 J MG/KG Calcium

39 J MG/KG Chromium

4.1 J MG/KG Cobalt

46 J MG/KG Copper

56000 J MG/KG Iron

130 J MG/KG Lead620 MG/KG Magnesium350 J MG/KG Manganese

0.12 U MG/KG Total Mercury

14 J MG/KG Nickel

260 J MG/KG Potassium

4.1 U MG/KG Selenium1.2 U MG/KG Silver

1200 MG/KG Sodium

0.54 J MG/KG Thallium

11 MG/KG Vanadium

980 MG/KG Zinc

NA MG/KG Cyanide

15 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9536 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 09:25

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG8 D No: 3AG8 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF OPSD02D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

7800 MG/KG Aluminum

7.4 UJ MG/KG Antimony2.2 J MG/KG Arsenic

18 J MG/KG Barium

0.08 UJ MG/KG Beryllium0.61 U MG/KG Cadmium

2100 J MG/KG Calcium

10 J MG/KG Chromium

1.1 J MG/KG Cobalt6.5 J MG/KG Copper

10000 J MG/KG Iron

8.8 J MG/KG Lead

540 J MG/KG Magnesium

46 J MG/KG Manganese

0.12 U MG/KG Total Mercury

2.3 J MG/KG Nickel

240 J MG/KG Potassium

0.47 R MG/KG Selenium

1.2 U MG/KG Silver

1100 MG/KG Sodium

3.1 U MG/KG Thallium

16 MG/KG Vanadium44 MG/KG Zinc

NA MG/KG Cyanide

18 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9537 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 09:50

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG9 D No: 3AG9 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF OPSD01 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

9500 MG/KG Aluminum

0.45 J MG/KG Antimony

1.2 J MG/KG Arsenic

260 J MG/KG Barium

0.04 UJ MG/KG Beryllium0.54 U MG/KG Cadmium

16000 J MG/KG Calcium

10 J MG/KG Chromium

3.3 J MG/KG Cobalt

45 J MG/KG Copper

8800 J MG/KG Iron

80 J MG/KG Lead

1800 MG/KG Magnesium

54 J MG/KG Manganese

0.03 UJ MG/KG Total Mercury

6.7 J MG/KG Nickel

270 J MG/KG Potassium

3.8 U MG/KG Selenium1.1 U MG/KG Silver

1400 MG/KG Sodium

0.47 R MG/KG Thallium

18 MG/KG Vanadium

220 MG/KG Zinc

NA MG/KG Cyanide

7 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9538 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 10:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH0 D No: 3AH0 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF OPSD03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

4000 MG/KG Aluminum

7.4 UJ MG/KG Antimony1.6 J MG/KG Arsenic

15 J MG/KG Barium

0.03 UJ MG/KG Beryllium0.62 U MG/KG Cadmium

180 J MG/KG Calcium

8.5 J MG/KG Chromium

0.41 J MG/KG Cobalt

13 J MG/KG Copper

7700 J MG/KG Iron

17 J MG/KG Lead

350 J MG/KG Magnesium

8.9 J MG/KG Manganese

0.15 MG/KG Total Mercury

1.2 J MG/KG Nickel

290 J MG/KG Potassium

4.3 U MG/KG Selenium1.2 U MG/KG Silver

1500 MG/KG Sodium

3.1 U MG/KG Thallium

12 MG/KG Vanadium11 MG/KG Zinc

NA MG/KG Cyanide

19 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9539 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 09:15

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH1 D No: 3AH1 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSF01 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

4100 MG/KG Aluminum

0.40 R MG/KG Antimony

2.2 J MG/KG Arsenic

75 J MG/KG Barium

0.17 UJ MG/KG Beryllium0.27 J MG/KG Cadmium

19000 J MG/KG Calcium

8.1 J MG/KG Chromium1.5 J MG/KG Cobalt

48 J MG/KG Copper

6800 J MG/KG Iron

48 J MG/KG Lead

830 J MG/KG Magnesium120 J MG/KG Manganese

0.07 UJ MG/KG Total Mercury

4.0 J MG/KG Nickel

340 J MG/KG Potassium

6.4 U MG/KG Selenium1.8 U MG/KG Silver

1800 MG/KG Sodium

4.6 U MG/KG Thallium8.8 J MG/KG Vanadium

1200 MG/KG Zinc

NA MG/KG Cyanide

45 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9540 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 09:15

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH2 D No: 3AH2 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSF01S / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

5300 MG/KG Aluminum

0.48 R MG/KG Antimony

2.3 J MG/KG Arsenic

52 J MG/KG Barium

0.15 UJ MG/KG Beryllium0.81 U MG/KG Cadmium

14000 J MG/KG Calcium

8.7 J MG/KG Chromium1.4 J MG/KG Cobalt

32 J MG/KG Copper

6500 J MG/KG Iron

34 J MG/KG Lead

770 J MG/KG Magnesium

82 J MG/KG Manganese

0.07 UJ MG/KG Total Mercury

3.9 J MG/KG Nickel

370 J MG/KG Potassium

5.6 U MG/KG Selenium1.6 U MG/KG Silver

1400 MG/KG Sodium

4.0 U MG/KG Thallium

11 MG/KG Vanadium

580 MG/KG Zinc

NA MG/KG Cyanide

38 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9541 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 10:10

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH3 D No: 3AH3 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSF02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

2600 MG/KG Aluminum

6.6 UJ MG/KG Antimony2.7 J MG/KG Arsenic

24 J MG/KG Barium

0.06 UJ MG/KG Beryllium0.55 U MG/KG Cadmium

1500 J MG/KG Calcium

3.9 J MG/KG Chromium

0.47 J MG/KG Cobalt

11 J MG/KG Copper

2600 J MG/KG Iron

71 J MG/KG Lead

330 UJ MG/KG Magnesium

35 J MG/KG Manganese

0.13 MG/KG Total Mercury

1.4 J MG/KG Nickel

150 J MG/KG Potassium

0.24 R MG/KG Selenium

1.1 U MG/KG Silver

730 MG/KG Sodium

2.8 U MG/KG Thallium4.5 J MG/KG Vanadium

93 MG/KG Zinc

NA MG/KG Cyanide

9 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9542 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 10:50

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH4 D No: 3AH4 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSF03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

3000 MG/KG Aluminum

7.5 UJ MG/KG Antimony1.3 J MG/KG Arsenic

29 J MG/KG Barium

0.08 UJ MG/KG Beryllium0.63 U MG/KG Cadmium

5900 J MG/KG Calcium

5.9 J MG/KG Chromium

0.83 J MG/KG Cobalt

9.9 J MG/KG Copper

3300 J MG/KG Iron

44 J MG/KG Lead

610 J MG/KG Magnesium

74 J MG/KG Manganese

0.07 UJ MG/KG Total Mercury

4.8 J MG/KG Nickel

280 J MG/KG Potassium

4.4 U MG/KG Selenium1.3 U MG/KG Silver

900 MG/KG Sodium

3.1 U MG/KG Thallium5.8 J MG/KG Vanadium

78 MG/KG Zinc

NA MG/KG Cyanide

20 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9543 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 11:15

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH5 D No: 3AH5 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSD04 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

15000 MG/KG Aluminum

0.71 R MG/KG Antimony

14 J MG/KG Arsenic

180 J MG/KG Barium

0.31 UJ MG/KG Beryllium0.98 U MG/KG Cadmium

3200 J MG/KG Calcium

16 J MG/KG Chromium

2.5 J MG/KG Cobalt

39 J MG/KG Copper

11000 J MG/KG Iron

26 J MG/KG Lead

1700 MG/KG Magnesium

210 J MG/KG Manganese

0.08 UJ MG/KG Total Mercury

5.0 J MG/KG Nickel

700 J MG/KG Potassium

6.8 U MG/KG Selenium2.0 U MG/KG Silver

2500 MG/KG Sodium

4.9 U MG/KG Thallium

23 MG/KG Vanadium

110 MG/KG Zinc

NA MG/KG Cyanide

49 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9544 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 11:25

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH6 D No: 3AH6 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSD04D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

3500 MG/KG Aluminum

0.55 R MG/KG Antimony

2.1 J MG/KG Arsenic

97 J MG/KG Barium

0.14 UJ MG/KG Beryllium0.71 U MG/KG Cadmium

12000 J MG/KG Calcium

8.3 J MG/KG Chromium1.3 J MG/KG Cobalt

18 J MG/KG Copper

5400 J MG/KG Iron

91 J MG/KG Lead

2300 MG/KG Magnesium

85 J MG/KG Manganese

0.12 UJ MG/KG Total Mercury

2.6 J MG/KG Nickel

280 J MG/KG Potassium

5.0 U MG/KG Selenium1.4 U MG/KG Silver

1300 MG/KG Sodium

0.35 R MG/KG Thallium

8.2 MG/KG Vanadium

130 MG/KG Zinc

NA MG/KG Cyanide

29 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9545 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 11:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH7 D No: 3AH7 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSD05 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

4300 MG/KG Aluminum

1.2 J MG/KG Antimony4.5 J MG/KG Arsenic

430 J MG/KG Barium

0.30 UJ MG/KG Beryllium

1.1 U MG/KG Cadmium

2900 J MG/KG Calcium

9.2 J MG/KG Chromium2.2 J MG/KG Cobalt

120 J MG/KG Copper

8300 J MG/KG Iron

21 J MG/KG Lead

1700 MG/KG Magnesium

73 J MG/KG Manganese

0.05 UJ MG/KG Total Mercury

3.0 J MG/KG Nickel

730 J MG/KG Potassium

7.4 U MG/KG Selenium2.1 U MG/KG Silver

4300 MG/KG Sodium

5.3 U MG/KG Thallium

11 J MG/KG Vanadium

100 MG/KG Zinc

NA MG/KG Cyanide

52 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9546 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 10:10

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH8 D No: 3AH8 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSD01 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

12000 MG/KG Aluminum

1.1 R MG/KG Antimony

53 J MG/KG Arsenic

140 J MG/KG Barium

2.0 MG/KG Beryllium1.1 U MG/KG Cadmium

1500 J MG/KG Calcium

22 J MG/KG Chromium

8.3 J MG/KG Cobalt

33 J MG/KG Copper

13000 J MG/KG Iron

18 J MG/KG Lead

1100 MG/KG Magnesium

96 J MG/KG Manganese

0.13 UJ MG/KG Total Mercury

18 J MG/KG Nickel

1600 MG/KG Potassium

0.88 J MG/KG Selenium

2.2 U MG/KG Silver

1800 MG/KG Sodium

1.9 J MG/KG Thallium

50 MG/KG Vanadium56 MG/KG Zinc

NA MG/KG Cyanide

55 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9547 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 11:05

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH9 D No: 3AH9 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSD01D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

9000 MG/KG Aluminum

0.59 R MG/KG Antimony

35 J MG/KG Arsenic87 J MG/KG Barium

1.3 MG/KG Beryllium1.2 U MG/KG Cadmium

1400 J MG/KG Calcium

18 J MG/KG Chromium

7.9 J MG/KG Cobalt

22 J MG/KG Copper

13000 J MG/KG Iron

15 J MG/KG Lead

1200 MG/KG Magnesium

130 J MG/KG Manganese

0.15 UJ MG/KG Total Mercury

14 J MG/KG Nickel

1200 J MG/KG Potassium

0.73 R MG/KG Selenium

2.4 U MG/KG Silver

1900 MG/KG Sodium

0.53 R MG/KG Thallium

38 MG/KG Vanadium49 J MG/KG Zinc

NA MG/KG Cyanide

58 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9548 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 12:00

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ0 D No: 3AJ0 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSD02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

4800 MG/KG Aluminum

7.9 UJ MG/KG Antimony1.0 R MG/KG Arsenic

400 MG/KG Barium

0.22 UJ MG/KG Beryllium0.65 U MG/KG Cadmium

330 J MG/KG Calcium

7.3 J MG/KG Chromium

0.83 J MG/KG Cobalt

2.6 J MG/KG Copper

2900 J MG/KG Iron

16 J MG/KG Lead

470 J MG/KG Magnesium

12 J MG/KG Manganese

0.13 U MG/KG Total Mercury

1.6 J MG/KG Nickel

240 J MG/KG Potassium

4.6 U MG/KG Selenium1.3 U MG/KG Silver

630 J MG/KG Sodium

3.3 U MG/KG Thallium

11 MG/KG Vanadium15 MG/KG Zinc

NA MG/KG Cyanide

24 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9549 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 13:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ1 D No: 3AJ1 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSF05 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

4000 MG/KG Aluminum

6.8 UJ MG/KG Antimony1.0 R MG/KG Arsenic

15 J MG/KG Barium

0.04 UJ MG/KG Beryllium0.57 U MG/KG Cadmium

540 J MG/KG Calcium

5.6 J MG/KG Chromium

0.45 J MG/KG Cobalt

1.9 J MG/KG Copper

4300 J MG/KG Iron

13 J MG/KG Lead

140 J MG/KG Magnesium

36 J MG/KG Manganese

0.03 UJ MG/KG Total Mercury

1.3 J MG/KG Nickel

85 J MG/KG Potassium

4.0 U MG/KG Selenium1.1 U MG/KG Silver

96 UJ MG/KG Sodium

2.8 U MG/KG Thallium9.2 MG/KG Vanadium

11 MG/KG Zinc

NA MG/KG Cyanide

12 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9550 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 13:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ2 D No: 3AJ2 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSF04 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

5100 MG/KG Aluminum

0.28 R MG/KG Antimony

1.5 MG/KG Arsenic

17 J MG/KG Barium

0.10 UJ MG/KG Beryllium0.57 U MG/KG Cadmium

230 J MG/KG Calcium

9.1 J MG/KG Chromium

0.74 J MG/KG Cobalt

2.0 J MG/KG Copper

7900 J MG/KG Iron

26 J MG/KG Lead

140 J MG/KG Magnesium180 J MG/KG Manganese

0.04 UJ MG/KG Total Mercury

1.6 J MG/KG Nickel

82 J MG/KG Potassium

0.48 R MG/KG Selenium

1.1 U MG/KG Silver

110 UJ MG/KG Sodium

2.8 U MG/KG Thallium

14 MG/KG Vanadium14 MG/KG Zinc

NA MG/KG Cyanide

12 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9551 2005 05-0928 Produced by: Goddard, Denise 

Metals Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 14:05

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ3 D No: 3AJ3 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSF03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

6500 MG/KG Aluminum

0.24 R MG/KG Antimony

1.4 MG/KG Arsenic

27 MG/KG Barium

0.12 UJ MG/KG Beryllium0.56 U MG/KG Cadmium

1100 MG/KG Calcium

11 J MG/KG Chromium

1.2 J MG/KG Cobalt2.7 J MG/KG Copper

9900 J MG/KG Iron

16 J MG/KG Lead

150 J MG/KG Magnesium380 J MG/KG Manganese

0.11 U MG/KG Total Mercury

2.5 J MG/KG Nickel

88 J MG/KG Potassium

4.0 U MG/KG Selenium1.1 U MG/KG Silver

110 UJ MG/KG Sodium

2.8 U MG/KG Thallium

16 MG/KG Vanadium21 MG/KG Zinc

NA MG/KG Cyanide

11 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Cyanide Analysis Not RequestedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9518 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 10:35

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ4 D No: 3AJ4 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSF08 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

1.8 UJ UG/KG alpha-BHC1.8 U UG/KG beta-BHC1.8 U UG/KG delta-BHC1.8 UJ UG/KG gamma-BHC (Lindane)1.8 U UG/KG Heptachlor1.8 U UG/KG Aldrin1.8 U UG/KG Heptachlor Epoxide1.8 U UG/KG Endosulfan I (alpha)3.5 U UG/KG Dieldrin3.5 U UG/KG 4,4'-DDE (p,p'-DDE)3.5 U UG/KG Endrin3.5 U UG/KG Endosulfan II (beta)3.5 UJ UG/KG 4,4'-DDD (p,p'-DDD)3.5 U UG/KG Endosulfan Sulfate3.5 U UG/KG 4,4'-DDT (p,p'-DDT)3.7 NJ UG/KG Methoxychlor3.5 U UG/KG Endrin Ketone3.5 U UG/KG Endrin Aldehyde1.8 U UG/KG alpha-Chlordane /21.8 U UG/KG gamma-Chlordane /2

180 U UG/KG Toxaphene

35 U UG/KG PCB-1016 (Aroclor 1016)71 U UG/KG PCB-1221 (Aroclor 1221)35 U UG/KG PCB-1232 (Aroclor 1232)35 U UG/KG PCB-1242 (Aroclor 1242)35 U UG/KG PCB-1248 (Aroclor 1248)35 U UG/KG PCB-1254 (Aroclor 1254)35 U UG/KG PCB-1260 (Aroclor 1260)

6 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9519 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 11:15

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ5 D No: 3AJ5 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD07 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

2.8 UJ UG/KG alpha-BHC2.8 U UG/KG beta-BHC2.8 U UG/KG delta-BHC2.8 UJ UG/KG gamma-BHC (Lindane)2.8 U UG/KG Heptachlor2.8 U UG/KG Aldrin2.8 U UG/KG Heptachlor Epoxide2.8 U UG/KG Endosulfan I (alpha)5.5 U UG/KG Dieldrin5.5 U UG/KG 4,4'-DDE (p,p'-DDE)5.5 U UG/KG Endrin5.5 U UG/KG Endosulfan II (beta)5.5 UJ UG/KG 4,4'-DDD (p,p'-DDD)5.5 U UG/KG Endosulfan Sulfate5.5 U UG/KG 4,4'-DDT (p,p'-DDT)

28 U UG/KG Methoxychlor

5.5 U UG/KG Endrin Ketone5.5 U UG/KG Endrin Aldehyde2.8 U UG/KG alpha-Chlordane /22.8 U UG/KG gamma-Chlordane /2

280 U UG/KG Toxaphene

55 U UG/KG PCB-1016 (Aroclor 1016)

110 U UG/KG PCB-1221 (Aroclor 1221)

55 U UG/KG PCB-1232 (Aroclor 1232)55 U UG/KG PCB-1242 (Aroclor 1242)55 U UG/KG PCB-1248 (Aroclor 1248)55 U UG/KG PCB-1254 (Aroclor 1254)55 U UG/KG PCB-1260 (Aroclor 1260)40 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9520 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 11:30

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ6 D No: 3AJ6 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSF02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

2.2 UJ UG/KG alpha-BHC2.2 U UG/KG beta-BHC2.2 U UG/KG delta-BHC2.2 UJ UG/KG gamma-BHC (Lindane)2.2 U UG/KG Heptachlor2.2 U UG/KG Aldrin2.2 U UG/KG Heptachlor Epoxide2.2 U UG/KG Endosulfan I (alpha)4.3 U UG/KG Dieldrin4.3 U UG/KG 4,4'-DDE (p,p'-DDE)4.3 U UG/KG Endrin4.3 U UG/KG Endosulfan II (beta)4.3 UJ UG/KG 4,4'-DDD (p,p'-DDD)4.3 U UG/KG Endosulfan Sulfate4.3 U UG/KG 4,4'-DDT (p,p'-DDT)

22 U UG/KG Methoxychlor

4.3 U UG/KG Endrin Ketone4.3 U UG/KG Endrin Aldehyde2.2 U UG/KG alpha-Chlordane /22.2 U UG/KG gamma-Chlordane /2

220 U UG/KG Toxaphene

43 U UG/KG PCB-1016 (Aroclor 1016)87 U UG/KG PCB-1221 (Aroclor 1221)43 U UG/KG PCB-1232 (Aroclor 1232)43 U UG/KG PCB-1242 (Aroclor 1242)43 U UG/KG PCB-1248 (Aroclor 1248)43 U UG/KG PCB-1254 (Aroclor 1254)43 U UG/KG PCB-1260 (Aroclor 1260)23 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9521 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 11:30

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ7 D No: 3AJ7 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSF02S / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

2.2 UJ UG/KG alpha-BHC2.2 U UG/KG beta-BHC2.2 U UG/KG delta-BHC2.2 UJ UG/KG gamma-BHC (Lindane)2.2 U UG/KG Heptachlor2.2 U UG/KG Aldrin2.2 U UG/KG Heptachlor Epoxide2.2 U UG/KG Endosulfan I (alpha)4.2 U UG/KG Dieldrin4.2 U UG/KG 4,4'-DDE (p,p'-DDE)4.2 U UG/KG Endrin4.2 U UG/KG Endosulfan II (beta)4.2 UJ UG/KG 4,4'-DDD (p,p'-DDD)4.2 U UG/KG Endosulfan Sulfate4.2 U UG/KG 4,4'-DDT (p,p'-DDT)5.3 NJ UG/KG Methoxychlor4.2 U UG/KG Endrin Ketone4.2 U UG/KG Endrin Aldehyde2.2 U UG/KG alpha-Chlordane /22.2 U UG/KG gamma-Chlordane /2

220 U UG/KG Toxaphene

42 U UG/KG PCB-1016 (Aroclor 1016)85 U UG/KG PCB-1221 (Aroclor 1221)42 U UG/KG PCB-1232 (Aroclor 1232)42 U UG/KG PCB-1242 (Aroclor 1242)42 U UG/KG PCB-1248 (Aroclor 1248)42 U UG/KG PCB-1254 (Aroclor 1254)42 U UG/KG PCB-1260 (Aroclor 1260)21 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9522 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 10:55

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ8 D No: 3AJ8 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSF01 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

1.9 UJ UG/KG alpha-BHC1.8 U UG/KG beta-BHC1.9 U UG/KG delta-BHC1.9 UJ UG/KG gamma-BHC (Lindane)1.9 U UG/KG Heptachlor1.9 U UG/KG Aldrin1.9 U UG/KG Heptachlor Epoxide1.9 U UG/KG Endosulfan I (alpha)3.6 U UG/KG Dieldrin3.6 U UG/KG 4,4'-DDE (p,p'-DDE)3.6 U UG/KG Endrin3.6 U UG/KG Endosulfan II (beta)3.6 UJ UG/KG 4,4'-DDD (p,p'-DDD)3.6 U UG/KG Endosulfan Sulfate3.6 U UG/KG 4,4'-DDT (p,p'-DDT)

19 U UG/KG Methoxychlor

3.6 U UG/KG Endrin Ketone3.6 U UG/KG Endrin Aldehyde1.9 U UG/KG alpha-Chlordane /21.9 U UG/KG gamma-Chlordane /2

190 U UG/KG Toxaphene

36 U UG/KG PCB-1016 (Aroclor 1016)74 U UG/KG PCB-1221 (Aroclor 1221)36 U UG/KG PCB-1232 (Aroclor 1232)36 U UG/KG PCB-1242 (Aroclor 1242)36 U UG/KG PCB-1248 (Aroclor 1248)36 U UG/KG PCB-1254 (Aroclor 1254)36 U UG/KG PCB-1260 (Aroclor 1260)

9 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9523 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 11:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ9 D No: 3AJ9 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD06 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

3.5 UJ UG/KG alpha-BHC3.5 U UG/KG beta-BHC3.5 U UG/KG delta-BHC3.5 UJ UG/KG gamma-BHC (Lindane)3.5 U UG/KG Heptachlor3.5 U UG/KG Aldrin3.5 U UG/KG Heptachlor Epoxide3.5 U UG/KG Endosulfan I (alpha)6.7 U UG/KG Dieldrin6.7 U UG/KG 4,4'-DDE (p,p'-DDE)6.7 U UG/KG Endrin6.7 U UG/KG Endosulfan II (beta)6.7 UJ UG/KG 4,4'-DDD (p,p'-DDD)6.7 U UG/KG Endosulfan Sulfate6.7 U UG/KG 4,4'-DDT (p,p'-DDT)7.8 NJ UG/KG Methoxychlor6.7 U UG/KG Endrin Ketone6.7 U UG/KG Endrin Aldehyde3.5 U UG/KG alpha-Chlordane /23.5 U UG/KG gamma-Chlordane /2

350 U UG/KG Toxaphene

67 U UG/KG PCB-1016 (Aroclor 1016)

140 U UG/KG PCB-1221 (Aroclor 1221)

67 U UG/KG PCB-1232 (Aroclor 1232)67 U UG/KG PCB-1242 (Aroclor 1242)67 U UG/KG PCB-1248 (Aroclor 1248)67 U UG/KG PCB-1254 (Aroclor 1254)67 U UG/KG PCB-1260 (Aroclor 1260)51 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9524 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 12:35

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AK0 D No: 3AK0 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD05 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

7.4 UJ UG/KG alpha-BHC7.4 U UG/KG beta-BHC7.4 U UG/KG delta-BHC7.4 UJ UG/KG gamma-BHC (Lindane)7.4 U UG/KG Heptachlor7.4 U UG/KG Aldrin7.4 U UG/KG Heptachlor Epoxide7.4 U UG/KG Endosulfan I (alpha)

14 U UG/KG Dieldrin14 U UG/KG 4,4'-DDE (p,p'-DDE)14 U UG/KG Endrin14 U UG/KG Endosulfan II (beta)14 UJ UG/KG 4,4'-DDD (p,p'-DDD)14 U UG/KG Endosulfan Sulfate14 U UG/KG 4,4'-DDT (p,p'-DDT)74 U UG/KG Methoxychlor14 U UG/KG Endrin Ketone14 U UG/KG Endrin Aldehyde

7.4 U UG/KG alpha-Chlordane /23.8 NJ UG/KG gamma-Chlordane /2

740 U UG/KG Toxaphene140 U UG/KG PCB-1016 (Aroclor 1016)290 U UG/KG PCB-1221 (Aroclor 1221)140 U UG/KG PCB-1232 (Aroclor 1232)140 U UG/KG PCB-1242 (Aroclor 1242)140 U UG/KG PCB-1248 (Aroclor 1248)140 U UG/KG PCB-1254 (Aroclor 1254)140 U UG/KG PCB-1260 (Aroclor 1260)

77 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9525 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 12:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AK1 D No: 3AK1 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD05D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

6.3 UJ UG/KG alpha-BHC6.3 U UG/KG beta-BHC6.3 U UG/KG delta-BHC6.3 UJ UG/KG gamma-BHC (Lindane)6.3 U UG/KG Heptachlor6.3 U UG/KG Aldrin6.3 U UG/KG Heptachlor Epoxide6.3 U UG/KG Endosulfan I (alpha)

12 U UG/KG Dieldrin12 U UG/KG 4,4'-DDE (p,p'-DDE)12 U UG/KG Endrin12 U UG/KG Endosulfan II (beta)12 UJ UG/KG 4,4'-DDD (p,p'-DDD)12 U UG/KG Endosulfan Sulfate12 U UG/KG 4,4'-DDT (p,p'-DDT)63 U UG/KG Methoxychlor12 U UG/KG Endrin Ketone12 U UG/KG Endrin Aldehyde

6.3 U UG/KG alpha-Chlordane /23.2 NJ UG/KG gamma-Chlordane /2

630 U UG/KG Toxaphene120 U UG/KG PCB-1016 (Aroclor 1016)250 U UG/KG PCB-1221 (Aroclor 1221)120 U UG/KG PCB-1232 (Aroclor 1232)120 U UG/KG PCB-1242 (Aroclor 1242)120 U UG/KG PCB-1248 (Aroclor 1248)120 U UG/KG PCB-1254 (Aroclor 1254)120 U UG/KG PCB-1260 (Aroclor 1260)

73 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9526 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 12:40

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AK2 D No: 3AK2 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

3.7 UJ UG/KG alpha-BHC3.7 U UG/KG beta-BHC3.7 U UG/KG delta-BHC3.7 UJ UG/KG gamma-BHC (Lindane)3.7 U UG/KG Heptachlor3.7 U UG/KG Aldrin3.7 U UG/KG Heptachlor Epoxide3.7 U UG/KG Endosulfan I (alpha)7.2 U UG/KG Dieldrin7.2 U UG/KG 4,4'-DDE (p,p'-DDE)7.2 U UG/KG Endrin7.2 U UG/KG Endosulfan II (beta)7.2 UJ UG/KG 4,4'-DDD (p,p'-DDD)7.2 U UG/KG Endosulfan Sulfate7.2 U UG/KG 4,4'-DDT (p,p'-DDT)

37 U UG/KG Methoxychlor

7.2 U UG/KG Endrin Ketone7.2 U UG/KG Endrin Aldehyde3.7 U UG/KG alpha-Chlordane /23.7 U UG/KG gamma-Chlordane /2

370 U UG/KG Toxaphene

72 U UG/KG PCB-1016 (Aroclor 1016)

150 U UG/KG PCB-1221 (Aroclor 1221)

72 U UG/KG PCB-1232 (Aroclor 1232)72 U UG/KG PCB-1242 (Aroclor 1242)72 U UG/KG PCB-1248 (Aroclor 1248)72 U UG/KG PCB-1254 (Aroclor 1254)72 U UG/KG PCB-1260 (Aroclor 1260)54 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9527 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 13:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AK5 D No: 3AK5 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD04 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

2.3 UJ UG/KG alpha-BHC2.3 U UG/KG beta-BHC2.3 U UG/KG delta-BHC2.3 UJ UG/KG gamma-BHC (Lindane)2.3 U UG/KG Heptachlor2.3 U UG/KG Aldrin2.3 U UG/KG Heptachlor Epoxide2.3 U UG/KG Endosulfan I (alpha)4.4 U UG/KG Dieldrin4.4 U UG/KG 4,4'-DDE (p,p'-DDE)4.4 U UG/KG Endrin4.4 U UG/KG Endosulfan II (beta)4.4 UJ UG/KG 4,4'-DDD (p,p'-DDD)4.4 U UG/KG Endosulfan Sulfate4.4 U UG/KG 4,4'-DDT (p,p'-DDT)

23 U UG/KG Methoxychlor

4.4 U UG/KG Endrin Ketone4.4 U UG/KG Endrin Aldehyde2.3 U UG/KG alpha-Chlordane /22.3 U UG/KG gamma-Chlordane /2

230 U UG/KG Toxaphene

44 U UG/KG PCB-1016 (Aroclor 1016)89 U UG/KG PCB-1221 (Aroclor 1221)44 U UG/KG PCB-1232 (Aroclor 1232)44 U UG/KG PCB-1242 (Aroclor 1242)44 U UG/KG PCB-1248 (Aroclor 1248)44 U UG/KG PCB-1254 (Aroclor 1254)44 U UG/KG PCB-1260 (Aroclor 1260)25 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9528 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 12:25

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AF9 D No: 3AF9 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSD01 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

7.7 UJ UG/KG alpha-BHC7.7 U UG/KG beta-BHC7.7 U UG/KG delta-BHC7.7 UJ UG/KG gamma-BHC (Lindane)7.7 U UG/KG Heptachlor7.7 U UG/KG Aldrin7.7 U UG/KG Heptachlor Epoxide7.7 U UG/KG Endosulfan I (alpha)

15 U UG/KG Dieldrin15 U UG/KG 4,4'-DDE (p,p'-DDE)15 U UG/KG Endrin15 U UG/KG Endosulfan II (beta)15 UJ UG/KG 4,4'-DDD (p,p'-DDD)15 U UG/KG Endosulfan Sulfate15 U UG/KG 4,4'-DDT (p,p'-DDT)77 U UG/KG Methoxychlor15 U UG/KG Endrin Ketone15 U UG/KG Endrin Aldehyde

7.7 U UG/KG alpha-Chlordane /27.7 U UG/KG gamma-Chlordane /2

770 U UG/KG Toxaphene150 U UG/KG PCB-1016 (Aroclor 1016)300 U UG/KG PCB-1221 (Aroclor 1221)150 U UG/KG PCB-1232 (Aroclor 1232)150 U UG/KG PCB-1242 (Aroclor 1242)150 U UG/KG PCB-1248 (Aroclor 1248)150 U UG/KG PCB-1254 (Aroclor 1254)150 U UG/KG PCB-1260 (Aroclor 1260)

78 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9529 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 12:40

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG0 D No: 3AG0 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSD01D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

8.5 UJ UG/KG alpha-BHC8.5 U UG/KG beta-BHC8.5 U UG/KG delta-BHC8.5 UJ UG/KG gamma-BHC (Lindane)8.5 U UG/KG Heptachlor8.5 U UG/KG Aldrin8.5 U UG/KG Heptachlor Epoxide8.5 U UG/KG Endosulfan I (alpha)

17 U UG/KG Dieldrin17 U UG/KG 4,4'-DDE (p,p'-DDE)17 U UG/KG Endrin17 U UG/KG Endosulfan II (beta)17 UJ UG/KG 4,4'-DDD (p,p'-DDD)17 U UG/KG Endosulfan Sulfate17 U UG/KG 4,4'-DDT (p,p'-DDT)85 U UG/KG Methoxychlor17 U UG/KG Endrin Ketone17 U UG/KG Endrin Aldehyde

8.5 U UG/KG alpha-Chlordane /28.5 U UG/KG gamma-Chlordane /2

850 U UG/KG Toxaphene170 U UG/KG PCB-1016 (Aroclor 1016)340 U UG/KG PCB-1221 (Aroclor 1221)170 U UG/KG PCB-1232 (Aroclor 1232)170 U UG/KG PCB-1242 (Aroclor 1242)170 U UG/KG PCB-1248 (Aroclor 1248)170 U UG/KG PCB-1254 (Aroclor 1254)170 U UG/KG PCB-1260 (Aroclor 1260)

80 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9530 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 13:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG1 D No: 3AG1 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSD02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

4.0 UJ UG/KG alpha-BHC4.0 U UG/KG beta-BHC4.0 U UG/KG delta-BHC4.0 UJ UG/KG gamma-BHC (Lindane)4.0 U UG/KG Heptachlor4.0 U UG/KG Aldrin4.0 U UG/KG Heptachlor Epoxide4.0 U UG/KG Endosulfan I (alpha)7.9 U UG/KG Dieldrin7.9 U UG/KG 4,4'-DDE (p,p'-DDE)7.9 U UG/KG Endrin7.9 U UG/KG Endosulfan II (beta)7.9 UJ UG/KG 4,4'-DDD (p,p'-DDD)7.9 U UG/KG Endosulfan Sulfate7.9 U UG/KG 4,4'-DDT (p,p'-DDT)

40 U UG/KG Methoxychlor

7.9 U UG/KG Endrin Ketone7.9 U UG/KG Endrin Aldehyde4.0 U UG/KG alpha-Chlordane /24.0 U UG/KG gamma-Chlordane /2

400 U UG/KG Toxaphene

79 U UG/KG PCB-1016 (Aroclor 1016)

160 U UG/KG PCB-1221 (Aroclor 1221)

79 U UG/KG PCB-1232 (Aroclor 1232)79 U UG/KG PCB-1242 (Aroclor 1242)79 U UG/KG PCB-1248 (Aroclor 1248)79 U UG/KG PCB-1254 (Aroclor 1254)79 U UG/KG PCB-1260 (Aroclor 1260)58 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9531 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 13:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG2 D No: 3AG2 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSD03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

2.0 UJ UG/KG alpha-BHC2.0 U UG/KG beta-BHC2.0 U UG/KG delta-BHC2.0 UJ UG/KG gamma-BHC (Lindane)2.0 U UG/KG Heptachlor2.0 U UG/KG Aldrin2.0 U UG/KG Heptachlor Epoxide2.0 U UG/KG Endosulfan I (alpha)4.0 U UG/KG Dieldrin4.0 U UG/KG 4,4'-DDE (p,p'-DDE)4.0 U UG/KG Endrin4.0 U UG/KG Endosulfan II (beta)4.0 UJ UG/KG 4,4'-DDD (p,p'-DDD)4.0 U UG/KG Endosulfan Sulfate4.0 U UG/KG 4,4'-DDT (p,p'-DDT)

20 U UG/KG Methoxychlor

4.0 U UG/KG Endrin Ketone4.0 U UG/KG Endrin Aldehyde2.0 U UG/KG alpha-Chlordane /22.0 U UG/KG gamma-Chlordane /2

200 U UG/KG Toxaphene

40 U UG/KG PCB-1016 (Aroclor 1016)81 U UG/KG PCB-1221 (Aroclor 1221)40 U UG/KG PCB-1232 (Aroclor 1232)40 U UG/KG PCB-1242 (Aroclor 1242)40 U UG/KG PCB-1248 (Aroclor 1248)40 U UG/KG PCB-1254 (Aroclor 1254)40 U UG/KG PCB-1260 (Aroclor 1260)17 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9532 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 12:50

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG3 D No: 3AG3 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSF04 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

1.9 UJ UG/KG alpha-BHC1.9 U UG/KG beta-BHC1.9 U UG/KG delta-BHC1.9 UJ UG/KG gamma-BHC (Lindane)1.9 U UG/KG Heptachlor1.9 U UG/KG Aldrin2.5 U UG/KG Heptachlor Epoxide1.9 U UG/KG Endosulfan I (alpha)3.8 U UG/KG Dieldrin3.8 U UG/KG 4,4'-DDE (p,p'-DDE)3.8 U UG/KG Endrin3.8 U UG/KG Endosulfan II (beta)3.8 UJ UG/KG 4,4'-DDD (p,p'-DDD)3.8 U UG/KG Endosulfan Sulfate3.8 U UG/KG 4,4'-DDT (p,p'-DDT)

19 U UG/KG Methoxychlor

3.8 U UG/KG Endrin Ketone3.8 U UG/KG Endrin Aldehyde1.9 U UG/KG alpha-Chlordane /2

0.86 J UG/KG gamma-Chlordane /2

190 U UG/KG Toxaphene

38 U UG/KG PCB-1016 (Aroclor 1016)76 U UG/KG PCB-1221 (Aroclor 1221)38 U UG/KG PCB-1232 (Aroclor 1232)38 U UG/KG PCB-1242 (Aroclor 1242)38 U UG/KG PCB-1248 (Aroclor 1248)38 U UG/KG PCB-1254 (Aroclor 1254)38 U UG/KG PCB-1260 (Aroclor 1260)12 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9533 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 12:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG4 D No: 3AG4 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSF05 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

2.0 UJ UG/KG alpha-BHC2.0 U UG/KG beta-BHC2.0 U UG/KG delta-BHC2.0 UJ UG/KG gamma-BHC (Lindane)2.0 U UG/KG Heptachlor2.0 U UG/KG Aldrin2.0 U UG/KG Heptachlor Epoxide2.0 U UG/KG Endosulfan I (alpha)3.8 U UG/KG Dieldrin3.8 U UG/KG 4,4'-DDE (p,p'-DDE)3.8 U UG/KG Endrin3.8 U UG/KG Endosulfan II (beta)3.8 UJ UG/KG 4,4'-DDD (p,p'-DDD)3.8 U UG/KG Endosulfan Sulfate3.8 U UG/KG 4,4'-DDT (p,p'-DDT)

20 U UG/KG Methoxychlor

3.8 U UG/KG Endrin Ketone3.8 U UG/KG Endrin Aldehyde2.0 U UG/KG alpha-Chlordane /22.0 U UG/KG gamma-Chlordane /2

200 U UG/KG Toxaphene

38 U UG/KG PCB-1016 (Aroclor 1016)77 U UG/KG PCB-1221 (Aroclor 1221)38 U UG/KG PCB-1232 (Aroclor 1232)38 U UG/KG PCB-1242 (Aroclor 1242)38 U UG/KG PCB-1248 (Aroclor 1248)38 U UG/KG PCB-1254 (Aroclor 1254)38 U UG/KG PCB-1260 (Aroclor 1260)13 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9534 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 12:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG5 D No: 3AG5 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSF05S / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

2.0 UJ UG/KG alpha-BHC2.0 U UG/KG beta-BHC2.0 U UG/KG delta-BHC2.0 UJ UG/KG gamma-BHC (Lindane)2.0 U UG/KG Heptachlor2.0 U UG/KG Aldrin2.0 U UG/KG Heptachlor Epoxide2.0 U UG/KG Endosulfan I (alpha)3.8 U UG/KG Dieldrin3.8 U UG/KG 4,4'-DDE (p,p'-DDE)3.8 U UG/KG Endrin3.8 U UG/KG Endosulfan II (beta)3.8 U UG/KG 4,4'-DDD (p,p'-DDD)3.8 U UG/KG Endosulfan Sulfate3.8 U UG/KG 4,4'-DDT (p,p'-DDT)

20 U UG/KG Methoxychlor

3.8 U UG/KG Endrin Ketone3.8 U UG/KG Endrin Aldehyde2.0 U UG/KG alpha-Chlordane /22.0 U UG/KG gamma-Chlordane /2

200 U UG/KG Toxaphene

38 U UG/KG PCB-1016 (Aroclor 1016)77 U UG/KG PCB-1221 (Aroclor 1221)38 U UG/KG PCB-1232 (Aroclor 1232)38 U UG/KG PCB-1242 (Aroclor 1242)38 U UG/KG PCB-1248 (Aroclor 1248)38 U UG/KG PCB-1254 (Aroclor 1254)38 U UG/KG PCB-1260 (Aroclor 1260)13 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9535 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 09:00

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG7 D No: 3AG7 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF OPSD02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

2.0 UJ UG/KG alpha-BHC2.0 U UG/KG beta-BHC2.0 U UG/KG delta-BHC2.0 UJ UG/KG gamma-BHC (Lindane)2.0 U UG/KG Heptachlor2.0 U UG/KG Aldrin2.0 U UG/KG Heptachlor Epoxide2.0 U UG/KG Endosulfan I (alpha)3.8 U UG/KG Dieldrin3.8 U UG/KG 4,4'-DDE (p,p'-DDE)3.8 U UG/KG Endrin3.8 U UG/KG Endosulfan II (beta)3.8 UJ UG/KG 4,4'-DDD (p,p'-DDD)3.8 U UG/KG Endosulfan Sulfate3.8 U UG/KG 4,4'-DDT (p,p'-DDT)

20 U UG/KG Methoxychlor

3.8 U UG/KG Endrin Ketone3.8 U UG/KG Endrin Aldehyde2.0 U UG/KG alpha-Chlordane /22.0 U UG/KG gamma-Chlordane /2

200 U UG/KG Toxaphene

38 U UG/KG PCB-1016 (Aroclor 1016)78 U UG/KG PCB-1221 (Aroclor 1221)38 U UG/KG PCB-1232 (Aroclor 1232)38 U UG/KG PCB-1242 (Aroclor 1242)38 U UG/KG PCB-1248 (Aroclor 1248)38 U UG/KG PCB-1254 (Aroclor 1254)21 J UG/KG PCB-1260 (Aroclor 1260)14 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9536 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 09:25

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG8 D No: 3AG8 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF OPSD02D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

2.1 UJ UG/KG alpha-BHC2.1 U UG/KG beta-BHC2.1 U UG/KG delta-BHC2.1 UJ UG/KG gamma-BHC (Lindane)2.1 U UG/KG Heptachlor2.1 U UG/KG Aldrin2.1 U UG/KG Heptachlor Epoxide2.1 U UG/KG Endosulfan I (alpha)4.1 U UG/KG Dieldrin4.1 U UG/KG 4,4'-DDE (p,p'-DDE)4.1 U UG/KG Endrin4.1 U UG/KG Endosulfan II (beta)4.1 UJ UG/KG 4,4'-DDD (p,p'-DDD)4.1 U UG/KG Endosulfan Sulfate4.1 U UG/KG 4,4'-DDT (p,p'-DDT)

21 U UG/KG Methoxychlor

2.0 NJ UG/KG Endrin Ketone4.1 U UG/KG Endrin Aldehyde2.1 U UG/KG alpha-Chlordane /22.1 U UG/KG gamma-Chlordane /2

210 U UG/KG Toxaphene

41 U UG/KG PCB-1016 (Aroclor 1016)83 U UG/KG PCB-1221 (Aroclor 1221)41 U UG/KG PCB-1232 (Aroclor 1232)41 U UG/KG PCB-1242 (Aroclor 1242)41 U UG/KG PCB-1248 (Aroclor 1248)41 U UG/KG PCB-1254 (Aroclor 1254)41 U UG/KG PCB-1260 (Aroclor 1260)19 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9537 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 09:50

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AG9 D No: 3AG9 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF OPSD01 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

1.8 UJ UG/KG alpha-BHC1.8 U UG/KG beta-BHC1.8 U UG/KG delta-BHC1.8 UJ UG/KG gamma-BHC (Lindane)1.8 U UG/KG Heptachlor1.8 U UG/KG Aldrin1.8 U UG/KG Heptachlor Epoxide1.8 U UG/KG Endosulfan I (alpha)3.5 U UG/KG Dieldrin3.5 U UG/KG 4,4'-DDE (p,p'-DDE)3.5 U UG/KG Endrin3.5 U UG/KG Endosulfan II (beta)3.5 UJ UG/KG 4,4'-DDD (p,p'-DDD)3.5 U UG/KG Endosulfan Sulfate1.4 J UG/KG 4,4'-DDT (p,p'-DDT)8.0 NJ UG/KG Methoxychlor3.5 U UG/KG Endrin Ketone3.5 U UG/KG Endrin Aldehyde1.7 NJ UG/KG alpha-Chlordane /21.8 U UG/KG gamma-Chlordane /2

180 U UG/KG Toxaphene

35 U UG/KG PCB-1016 (Aroclor 1016)71 U UG/KG PCB-1221 (Aroclor 1221)35 U UG/KG PCB-1232 (Aroclor 1232)35 U UG/KG PCB-1242 (Aroclor 1242)35 U UG/KG PCB-1248 (Aroclor 1248)35 U UG/KG PCB-1254 (Aroclor 1254)35 U UG/KG PCB-1260 (Aroclor 1260)

6 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9538 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 10:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH0 D No: 3AH0 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF OPSD03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

2.0 UJ UG/KG alpha-BHC2.0 U UG/KG beta-BHC2.0 U UG/KG delta-BHC2.0 UJ UG/KG gamma-BHC (Lindane)2.0 U UG/KG Heptachlor2.0 U UG/KG Aldrin8.3 U UG/KG Heptachlor Epoxide2.0 U UG/KG Endosulfan I (alpha)9.7 UG/KG Dieldrin

19 N UG/KG 4,4'-DDE (p,p'-DDE)

3.9 U UG/KG Endrin3.8 U UG/KG Endosulfan II (beta)3.8 UJ UG/KG 4,4'-DDD (p,p'-DDD)3.8 U UG/KG Endosulfan Sulfate

12 N UG/KG 4,4'-DDT (p,p'-DDT)20 U UG/KG Methoxychlor

2.7 NJ UG/KG Endrin Ketone3.8 U UG/KG Endrin Aldehyde2.0 U UG/KG alpha-Chlordane /25.8 UG/KG gamma-Chlordane /2

200 U UG/KG Toxaphene

38 U UG/KG PCB-1016 (Aroclor 1016)78 U UG/KG PCB-1221 (Aroclor 1221)38 U UG/KG PCB-1232 (Aroclor 1232)38 U UG/KG PCB-1242 (Aroclor 1242)38 U UG/KG PCB-1248 (Aroclor 1248)38 U UG/KG PCB-1254 (Aroclor 1254)38 U UG/KG PCB-1260 (Aroclor 1260)14 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9539 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 09:15

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH1 D No: 3AH1 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSF01 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

2.7 UJ UG/KG alpha-BHC2.7 U UG/KG beta-BHC2.7 U UG/KG delta-BHC2.7 UJ UG/KG gamma-BHC (Lindane)2.7 U UG/KG Heptachlor2.7 U UG/KG Aldrin2.7 U UG/KG Heptachlor Epoxide2.7 U UG/KG Endosulfan I (alpha)5.2 U UG/KG Dieldrin5.2 U UG/KG 4,4'-DDE (p,p'-DDE)5.2 U UG/KG Endrin5.2 U UG/KG Endosulfan II (beta)5.2 UJ UG/KG 4,4'-DDD (p,p'-DDD)5.2 U UG/KG Endosulfan Sulfate5.2 U UG/KG 4,4'-DDT (p,p'-DDT)

27 U UG/KG Methoxychlor

5.2 U UG/KG Endrin Ketone5.2 U UG/KG Endrin Aldehyde2.7 U UG/KG alpha-Chlordane /22.7 U UG/KG gamma-Chlordane /2

270 U UG/KG Toxaphene

52 U UG/KG PCB-1016 (Aroclor 1016)

100 U UG/KG PCB-1221 (Aroclor 1221)

52 U UG/KG PCB-1232 (Aroclor 1232)52 U UG/KG PCB-1242 (Aroclor 1242)52 U UG/KG PCB-1248 (Aroclor 1248)52 U UG/KG PCB-1254 (Aroclor 1254)52 U UG/KG PCB-1260 (Aroclor 1260)36 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9540 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 09:15

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH2 D No: 3AH2 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSF01S / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

2.7 UJ UG/KG alpha-BHC2.7 U UG/KG beta-BHC2.7 U UG/KG delta-BHC2.7 UJ UG/KG gamma-BHC (Lindane)2.7 U UG/KG Heptachlor2.7 U UG/KG Aldrin2.7 U UG/KG Heptachlor Epoxide2.7 U UG/KG Endosulfan I (alpha)1.3 J UG/KG Dieldrin1.1 NJ UG/KG 4,4'-DDE (p,p'-DDE)5.2 U UG/KG Endrin5.2 U UG/KG Endosulfan II (beta)5.2 UJ UG/KG 4,4'-DDD (p,p'-DDD)1.2 J UG/KG Endosulfan Sulfate5.2 U UG/KG 4,4'-DDT (p,p'-DDT)

27 U UG/KG Methoxychlor

5.2 U UG/KG Endrin Ketone5.2 U UG/KG Endrin Aldehyde3.0 U UG/KG alpha-Chlordane /23.5 N UG/KG gamma-Chlordane /2

270 U UG/KG Toxaphene

52 U UG/KG PCB-1016 (Aroclor 1016)

100 U UG/KG PCB-1221 (Aroclor 1221)

52 U UG/KG PCB-1232 (Aroclor 1232)52 U UG/KG PCB-1242 (Aroclor 1242)52 U UG/KG PCB-1248 (Aroclor 1248)52 U UG/KG PCB-1254 (Aroclor 1254)52 U UG/KG PCB-1260 (Aroclor 1260)36 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9541 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 10:10

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH3 D No: 3AH3 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSF02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

1.9 UJ UG/KG alpha-BHC1.9 U UG/KG beta-BHC1.9 U UG/KG delta-BHC1.9 UJ UG/KG gamma-BHC (Lindane)1.9 U UG/KG Heptachlor1.9 U UG/KG Aldrin5.0 U UG/KG Heptachlor Epoxide1.9 U UG/KG Endosulfan I (alpha)7.2 UG/KG Dieldrin6.3 UG/KG 4,4'-DDE (p,p'-DDE)3.6 U UG/KG Endrin3.6 U UG/KG Endosulfan II (beta)3.6 UJ UG/KG 4,4'-DDD (p,p'-DDD)3.6 U UG/KG Endosulfan Sulfate6.2 N UG/KG 4,4'-DDT (p,p'-DDT)

19 U UG/KG Methoxychlor

3.6 U UG/KG Endrin Ketone3.6 U UG/KG Endrin Aldehyde

17 U UG/KG alpha-Chlordane /211 N UG/KG gamma-Chlordane /2

190 U UG/KG Toxaphene

36 U UG/KG PCB-1016 (Aroclor 1016)74 U UG/KG PCB-1221 (Aroclor 1221)36 U UG/KG PCB-1232 (Aroclor 1232)36 U UG/KG PCB-1242 (Aroclor 1242)36 U UG/KG PCB-1248 (Aroclor 1248)36 U UG/KG PCB-1254 (Aroclor 1254)36 U UG/KG PCB-1260 (Aroclor 1260)

9 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9542 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 10:50

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH4 D No: 3AH4 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSF03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

2.1 UJ UG/KG alpha-BHC2.1 U UG/KG beta-BHC2.1 U UG/KG delta-BHC2.1 UJ UG/KG gamma-BHC (Lindane)2.1 U UG/KG Heptachlor

0.91 NJ UG/KG Aldrin

2.9 U UG/KG Heptachlor Epoxide2.1 U UG/KG Endosulfan I (alpha)9.4 UG/KG Dieldrin5.6 UG/KG 4,4'-DDE (p,p'-DDE)4.0 U UG/KG Endrin4.0 U UG/KG Endosulfan II (beta)4.0 UJ UG/KG 4,4'-DDD (p,p'-DDD)4.0 U UG/KG Endosulfan Sulfate9.9 UG/KG 4,4'-DDT (p,p'-DDT)

21 U UG/KG Methoxychlor

4.0 U UG/KG Endrin Ketone4.0 U UG/KG Endrin Aldehyde

18 U UG/KG alpha-Chlordane /219 N UG/KG gamma-Chlordane /2

210 U UG/KG Toxaphene

40 U UG/KG PCB-1016 (Aroclor 1016)82 U UG/KG PCB-1221 (Aroclor 1221)40 U UG/KG PCB-1232 (Aroclor 1232)40 U UG/KG PCB-1242 (Aroclor 1242)40 U UG/KG PCB-1248 (Aroclor 1248)40 U UG/KG PCB-1254 (Aroclor 1254)40 U UG/KG PCB-1260 (Aroclor 1260)18 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9543 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 11:15

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH5 D No: 3AH5 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSD04 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

3.1 UJ UG/KG alpha-BHC3.1 U UG/KG beta-BHC3.1 U UG/KG delta-BHC3.1 UJ UG/KG gamma-BHC (Lindane)3.1 U UG/KG Heptachlor

15 N UG/KG Aldrin

3.1 U UG/KG Heptachlor Epoxide3.1 U UG/KG Endosulfan I (alpha)

12 UG/KG Dieldrin

6.5 UG/KG 4,4'-DDE (p,p'-DDE)6.0 U UG/KG Endrin6.0 U UG/KG Endosulfan II (beta)3.3 NJ UG/KG 4,4'-DDD (p,p'-DDD)6.0 U UG/KG Endosulfan Sulfate

12 UG/KG 4,4'-DDT (p,p'-DDT)31 U UG/KG Methoxychlor

6.0 U UG/KG Endrin Ketone6.0 U UG/KG Endrin Aldehyde

24 N UG/KG alpha-Chlordane /223 N UG/KG gamma-Chlordane /2

310 U UG/KG Toxaphene

60 U UG/KG PCB-1016 (Aroclor 1016)

120 U UG/KG PCB-1221 (Aroclor 1221)

60 U UG/KG PCB-1232 (Aroclor 1232)60 U UG/KG PCB-1242 (Aroclor 1242)60 U UG/KG PCB-1248 (Aroclor 1248)60 U UG/KG PCB-1254 (Aroclor 1254)60 U UG/KG PCB-1260 (Aroclor 1260)45 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9544 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 11:25

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH6 D No: 3AH6 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSD04D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

2.5 UJ UG/KG alpha-BHC2.5 U UG/KG beta-BHC2.5 U UG/KG delta-BHC2.5 UJ UG/KG gamma-BHC (Lindane)2.5 U UG/KG Heptachlor2.5 U UG/KG Aldrin2.5 U UG/KG Heptachlor Epoxide2.5 U UG/KG Endosulfan I (alpha)7.1 UG/KG Dieldrin4.9 N UG/KG 4,4'-DDE (p,p'-DDE)4.9 U UG/KG Endrin4.9 U UG/KG Endosulfan II (beta)2.0 J UG/KG 4,4'-DDD (p,p'-DDD)4.9 U UG/KG Endosulfan Sulfate3.9 J UG/KG 4,4'-DDT (p,p'-DDT)6.8 J UG/KG Methoxychlor2.3 U UG/KG Endrin Ketone4.9 U UG/KG Endrin Aldehyde8.4 N UG/KG alpha-Chlordane /26.6 U UG/KG gamma-Chlordane /2

250 U UG/KG Toxaphene

49 U UG/KG PCB-1016 (Aroclor 1016)99 U UG/KG PCB-1221 (Aroclor 1221)49 U UG/KG PCB-1232 (Aroclor 1232)49 U UG/KG PCB-1242 (Aroclor 1242)49 U UG/KG PCB-1248 (Aroclor 1248)49 U UG/KG PCB-1254 (Aroclor 1254)49 U UG/KG PCB-1260 (Aroclor 1260)32 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9545 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 11:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH7 D No: 3AH7 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSD05 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

3.4 UJ UG/KG alpha-BHC3.4 U UG/KG beta-BHC3.4 U UG/KG delta-BHC3.4 UJ UG/KG gamma-BHC (Lindane)3.4 U UG/KG Heptachlor3.4 U UG/KG Aldrin3.4 U UG/KG Heptachlor Epoxide3.4 U UG/KG Endosulfan I (alpha)4.6 NJ UG/KG Dieldrin2.0 J UG/KG 4,4'-DDE (p,p'-DDE)6.6 U UG/KG Endrin6.6 U UG/KG Endosulfan II (beta)6.6 UJ UG/KG 4,4'-DDD (p,p'-DDD)6.6 U UG/KG Endosulfan Sulfate2.7 J UG/KG 4,4'-DDT (p,p'-DDT)

34 U UG/KG Methoxychlor

6.6 U UG/KG Endrin Ketone6.6 U UG/KG Endrin Aldehyde6.5 U UG/KG alpha-Chlordane /28.4 UG/KG gamma-Chlordane /2

340 U UG/KG Toxaphene

66 U UG/KG PCB-1016 (Aroclor 1016)

130 U UG/KG PCB-1221 (Aroclor 1221)

66 U UG/KG PCB-1232 (Aroclor 1232)66 U UG/KG PCB-1242 (Aroclor 1242)66 U UG/KG PCB-1248 (Aroclor 1248)66 U UG/KG PCB-1254 (Aroclor 1254)66 U UG/KG PCB-1260 (Aroclor 1260)50 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9546 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 10:10

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH8 D No: 3AH8 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSD01 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

3.4 UJ UG/KG alpha-BHC3.4 U UG/KG beta-BHC3.4 U UG/KG delta-BHC3.4 UJ UG/KG gamma-BHC (Lindane)3.4 U UG/KG Heptachlor3.4 U UG/KG Aldrin3.4 U UG/KG Heptachlor Epoxide3.4 U UG/KG Endosulfan I (alpha)6.6 U UG/KG Dieldrin6.6 U UG/KG 4,4'-DDE (p,p'-DDE)1.8 NJ UG/KG Endrin6.6 U UG/KG Endosulfan II (beta)6.6 UJ UG/KG 4,4'-DDD (p,p'-DDD)6.6 U UG/KG Endosulfan Sulfate6.6 U UG/KG 4,4'-DDT (p,p'-DDT)

34 U UG/KG Methoxychlor

6.6 U UG/KG Endrin Ketone6.6 U UG/KG Endrin Aldehyde4.7 UG/KG alpha-Chlordane /23.4 U UG/KG gamma-Chlordane /2

340 U UG/KG Toxaphene

66 U UG/KG PCB-1016 (Aroclor 1016)

130 U UG/KG PCB-1221 (Aroclor 1221)

66 U UG/KG PCB-1232 (Aroclor 1232)66 U UG/KG PCB-1242 (Aroclor 1242)66 U UG/KG PCB-1248 (Aroclor 1248)66 U UG/KG PCB-1254 (Aroclor 1254)66 U UG/KG PCB-1260 (Aroclor 1260)50 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9547 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 11:05

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH9 D No: 3AH9 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSD01D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

3.4 UJ UG/KG alpha-BHC3.4 U UG/KG beta-BHC3.4 U UG/KG delta-BHC3.4 UJ UG/KG gamma-BHC (Lindane)3.4 U UG/KG Heptachlor3.4 U UG/KG Aldrin3.4 U UG/KG Heptachlor Epoxide1.1 J UG/KG Endosulfan I (alpha)6.6 U UG/KG Dieldrin6.6 U UG/KG 4,4'-DDE (p,p'-DDE)6.6 U UG/KG Endrin6.6 U UG/KG Endosulfan II (beta)6.6 UJ UG/KG 4,4'-DDD (p,p'-DDD)6.6 U UG/KG Endosulfan Sulfate6.6 U UG/KG 4,4'-DDT (p,p'-DDT)

34 U UG/KG Methoxychlor

6.6 U UG/KG Endrin Ketone6.6 U UG/KG Endrin Aldehyde4.0 N UG/KG alpha-Chlordane /23.4 U UG/KG gamma-Chlordane /2

340 U UG/KG Toxaphene

66 U UG/KG PCB-1016 (Aroclor 1016)

130 U UG/KG PCB-1221 (Aroclor 1221)

66 U UG/KG PCB-1232 (Aroclor 1232)66 U UG/KG PCB-1242 (Aroclor 1242)66 U UG/KG PCB-1248 (Aroclor 1248)66 U UG/KG PCB-1254 (Aroclor 1254)66 U UG/KG PCB-1260 (Aroclor 1260)50 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9548 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 12:00

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ0 D No: 3AJ0 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSD02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

2.2 UJ UG/KG alpha-BHC2.2 U UG/KG beta-BHC2.2 U UG/KG delta-BHC2.2 UJ UG/KG gamma-BHC (Lindane)2.2 U UG/KG Heptachlor2.2 U UG/KG Aldrin2.2 U UG/KG Heptachlor Epoxide2.2 U UG/KG Endosulfan I (alpha)4.3 U UG/KG Dieldrin4.3 U UG/KG 4,4'-DDE (p,p'-DDE)1.0 J UG/KG Endrin4.3 U UG/KG Endosulfan II (beta)4.3 UJ UG/KG 4,4'-DDD (p,p'-DDD)4.3 U UG/KG Endosulfan Sulfate4.3 U UG/KG 4,4'-DDT (p,p'-DDT)

22 U UG/KG Methoxychlor

4.3 U UG/KG Endrin Ketone4.3 U UG/KG Endrin Aldehyde2.2 U UG/KG alpha-Chlordane /22.2 U UG/KG gamma-Chlordane /2

220 U UG/KG Toxaphene

43 U UG/KG PCB-1016 (Aroclor 1016)88 U UG/KG PCB-1221 (Aroclor 1221)43 U UG/KG PCB-1232 (Aroclor 1232)43 U UG/KG PCB-1242 (Aroclor 1242)43 U UG/KG PCB-1248 (Aroclor 1248)43 U UG/KG PCB-1254 (Aroclor 1254)43 U UG/KG PCB-1260 (Aroclor 1260)24 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9549 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 13:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ1 D No: 3AJ1 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSF05 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

1.9 UJ UG/KG alpha-BHC1.9 U UG/KG beta-BHC1.9 U UG/KG delta-BHC1.9 UJ UG/KG gamma-BHC (Lindane)1.9 U UG/KG Heptachlor1.9 U UG/KG Aldrin

13 U UG/KG Heptachlor Epoxide

1.9 U UG/KG Endosulfan I (alpha)

0.86 NJ UG/KG Dieldrin

3.7 U UG/KG 4,4'-DDE (p,p'-DDE)3.7 U UG/KG Endrin3.7 U UG/KG Endosulfan II (beta)3.7 UJ UG/KG 4,4'-DDD (p,p'-DDD)3.7 U UG/KG Endosulfan Sulfate3.7 U UG/KG 4,4'-DDT (p,p'-DDT)

19 U UG/KG Methoxychlor

1.7 NJ UG/KG Endrin Ketone3.7 U UG/KG Endrin Aldehyde1.9 U UG/KG alpha-Chlordane /21.9 U UG/KG gamma-Chlordane /2

190 U UG/KG Toxaphene

37 U UG/KG PCB-1016 (Aroclor 1016)74 U UG/KG PCB-1221 (Aroclor 1221)37 U UG/KG PCB-1232 (Aroclor 1232)37 U UG/KG PCB-1242 (Aroclor 1242)37 U UG/KG PCB-1248 (Aroclor 1248)37 U UG/KG PCB-1254 (Aroclor 1254)37 U UG/KG PCB-1260 (Aroclor 1260)10 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9550 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 13:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ2 D No: 3AJ2 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSF04 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

1.9 UJ UG/KG alpha-BHC1.9 U UG/KG beta-BHC1.9 U UG/KG delta-BHC1.9 UJ UG/KG gamma-BHC (Lindane)1.9 U UG/KG Heptachlor1.9 U UG/KG Aldrin1.9 U UG/KG Heptachlor Epoxide1.9 U UG/KG Endosulfan I (alpha)1.0 J UG/KG Dieldrin3.8 U UG/KG 4,4'-DDE (p,p'-DDE)3.8 U UG/KG Endrin3.8 U UG/KG Endosulfan II (beta)

0.80 J UG/KG 4,4'-DDD (p,p'-DDD)

3.8 U UG/KG Endosulfan Sulfate3.8 U UG/KG 4,4'-DDT (p,p'-DDT)

19 U UG/KG Methoxychlor

3.8 U UG/KG Endrin Ketone3.8 U UG/KG Endrin Aldehyde1.1 NJ UG/KG alpha-Chlordane /21.9 U UG/KG gamma-Chlordane /2

190 U UG/KG Toxaphene

38 U UG/KG PCB-1016 (Aroclor 1016)76 U UG/KG PCB-1221 (Aroclor 1221)38 U UG/KG PCB-1232 (Aroclor 1232)38 U UG/KG PCB-1242 (Aroclor 1242)38 U UG/KG PCB-1248 (Aroclor 1248)38 U UG/KG PCB-1254 (Aroclor 1254)38 U UG/KG PCB-1260 (Aroclor 1260)12 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9551 2005 05-0928 Produced by: Appleby, Charlie 

Pesticides & Aroclors Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 14:05

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ3 D No: 3AJ3 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSF03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

1.7 UJ UG/KG alpha-BHC1.7 U UG/KG beta-BHC1.7 U UG/KG delta-BHC1.7 UJ UG/KG gamma-BHC (Lindane)1.7 U UG/KG Heptachlor1.7 U UG/KG Aldrin1.7 U UG/KG Heptachlor Epoxide1.7 U UG/KG Endosulfan I (alpha)3.3 U UG/KG Dieldrin3.3 U UG/KG 4,4'-DDE (p,p'-DDE)3.3 U UG/KG Endrin3.3 U UG/KG Endosulfan II (beta)3.3 UJ UG/KG 4,4'-DDD (p,p'-DDD)3.3 U UG/KG Endosulfan Sulfate3.3 U UG/KG 4,4'-DDT (p,p'-DDT)5.7 J UG/KG Methoxychlor3.3 U UG/KG Endrin Ketone3.3 U UG/KG Endrin Aldehyde1.7 U UG/KG alpha-Chlordane /21.7 U UG/KG gamma-Chlordane /2

170 U UG/KG Toxaphene

33 U UG/KG PCB-1016 (Aroclor 1016)67 U UG/KG PCB-1221 (Aroclor 1221)33 U UG/KG PCB-1232 (Aroclor 1232)33 U UG/KG PCB-1242 (Aroclor 1242)33 U UG/KG PCB-1248 (Aroclor 1248)33 U UG/KG PCB-1254 (Aroclor 1254)33 U UG/KG PCB-1260 (Aroclor 1260)14 % % Moisture

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9518 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 10:35

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AJ4 D No: 3AJ4 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSF08 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

16 U UG/KG Dichlorodifluoromethane 16 U UG/KG Dibromochloromethane16 U UG/KG Chloromethane 16 U UG/KG 1,2-Dibromoethane (EDB16 U UG/KG Vinyl Chloride 16 U UG/KG Chlorobenzene16 U UG/KG Bromomethane 16 U UG/KG Ethyl Benzene16 UJ UG/KG Chloroethane 16 U UG/KG Total Xylenes16 U UG/KG Trichlorofluoromethane (Freon 11) 16 U UG/KG Styrene16 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 16 U UG/KG Bromoform16 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 16 U UG/KG Isopropylbenzene16 U UG/KG Acetone 16 U UG/KG 1,1,2,2-Tetrachloroethan16 U UG/KG Carbon Disulfide 16 U UG/KG 1,3-Dichlorobenzene16 U UG/KG Methyl Acetate 16 U UG/KG 1,4-Dichlorobenzene16 U UG/KG Methylene Chloride 16 U UG/KG 1,2-Dichlorobenzene16 U UG/KG trans-1,2-Dichloroethene 16 U UG/KG 1,2-Dibromo-3-Chloropro16 U UG/KG Methyl T-Butyl Ether (MTBE) 16 U UG/KG 1,2,4-Trichlorobenzene16 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene16 U UG/KG cis-1,2-Dichloroethene 6 % % Moisture16 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

16 U UG/KG Chloroform16 U UG/KG 1,1,1-Trichloroethane16 U UG/KG Cyclohexane16 U UG/KG Carbon Tetrachloride16 U UG/KG Benzene16 U UG/KG 1,2-Dichloroethane16 U UG/KG Trichloroethene (Trichloroethylene)16 U UG/KG Methylcyclohexane16 U UG/KG 1,2-Dichloropropane16 U UG/KG Bromodichloromethane16 U UG/KG cis-1,3-Dichloropropene16 U UG/KG Methyl Isobutyl Ketone16 U UG/KG Toluene16 U UG/KG trans-1,3-Dichloropropene16 U UG/KG 1,1,2-Trichloroethane16 U UG/KG Tetrachloroethene (Tetrachloroethylene)16 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9519 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 11:15

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AJ5 D No: 3AJ5 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD07 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

24 U UG/KG Dichlorodifluoromethane 24 U UG/KG Dibromochloromethane24 U UG/KG Chloromethane 24 U UG/KG 1,2-Dibromoethane (EDB24 U UG/KG Vinyl Chloride 24 U UG/KG Chlorobenzene24 U UG/KG Bromomethane 24 U UG/KG Ethyl Benzene24 UJ UG/KG Chloroethane 24 U UG/KG Total Xylenes24 U UG/KG Trichlorofluoromethane (Freon 11) 24 U UG/KG Styrene24 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 24 U UG/KG Bromoform24 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 24 U UG/KG Isopropylbenzene24 U UG/KG Acetone 24 U UG/KG 1,1,2,2-Tetrachloroethan24 U UG/KG Carbon Disulfide 24 U UG/KG 1,3-Dichlorobenzene24 U UG/KG Methyl Acetate 24 U UG/KG 1,4-Dichlorobenzene24 U UG/KG Methylene Chloride 24 U UG/KG 1,2-Dichlorobenzene24 U UG/KG trans-1,2-Dichloroethene 24 U UG/KG 1,2-Dibromo-3-Chloropro24 U UG/KG Methyl T-Butyl Ether (MTBE) 24 U UG/KG 1,2,4-Trichlorobenzene24 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene24 U UG/KG cis-1,2-Dichloroethene 40 % % Moisture24 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

24 U UG/KG Chloroform24 U UG/KG 1,1,1-Trichloroethane24 U UG/KG Cyclohexane24 U UG/KG Carbon Tetrachloride24 U UG/KG Benzene24 U UG/KG 1,2-Dichloroethane24 U UG/KG Trichloroethene (Trichloroethylene)24 U UG/KG Methylcyclohexane24 U UG/KG 1,2-Dichloropropane24 U UG/KG Bromodichloromethane24 U UG/KG cis-1,3-Dichloropropene24 U UG/KG Methyl Isobutyl Ketone24 U UG/KG Toluene24 U UG/KG trans-1,3-Dichloropropene24 U UG/KG 1,1,2-Trichloroethane24 U UG/KG Tetrachloroethene (Tetrachloroethylene)24 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9520 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 11:30

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AJ6 D No: 3AJ6 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSF02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

13 U UG/KG Dichlorodifluoromethane 13 U UG/KG Dibromochloromethane13 U UG/KG Chloromethane 13 U UG/KG 1,2-Dibromoethane (EDB13 U UG/KG Vinyl Chloride 13 U UG/KG Chlorobenzene13 U UG/KG Bromomethane 13 U UG/KG Ethyl Benzene13 UJ UG/KG Chloroethane 13 U UG/KG Total Xylenes13 U UG/KG Trichlorofluoromethane (Freon 11) 13 U UG/KG Styrene13 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 13 U UG/KG Bromoform13 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 13 U UG/KG Isopropylbenzene13 U UG/KG Acetone 13 U UG/KG 1,1,2,2-Tetrachloroethan13 U UG/KG Carbon Disulfide 13 U UG/KG 1,3-Dichlorobenzene13 U UG/KG Methyl Acetate 13 U UG/KG 1,4-Dichlorobenzene13 U UG/KG Methylene Chloride 13 U UG/KG 1,2-Dichlorobenzene13 U UG/KG trans-1,2-Dichloroethene 13 U UG/KG 1,2-Dibromo-3-Chloropro13 U UG/KG Methyl T-Butyl Ether (MTBE) 13 U UG/KG 1,2,4-Trichlorobenzene13 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene13 U UG/KG cis-1,2-Dichloroethene 23 % % Moisture13 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

13 U UG/KG Chloroform13 U UG/KG 1,1,1-Trichloroethane13 U UG/KG Cyclohexane13 U UG/KG Carbon Tetrachloride13 U UG/KG Benzene13 U UG/KG 1,2-Dichloroethane13 U UG/KG Trichloroethene (Trichloroethylene)13 U UG/KG Methylcyclohexane13 U UG/KG 1,2-Dichloropropane13 U UG/KG Bromodichloromethane13 U UG/KG cis-1,3-Dichloropropene13 U UG/KG Methyl Isobutyl Ketone13 U UG/KG Toluene13 U UG/KG trans-1,3-Dichloropropene13 U UG/KG 1,1,2-Trichloroethane13 U UG/KG Tetrachloroethene (Tetrachloroethylene)13 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9521 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 11:30

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AJ7 D No: 3AJ7 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSF02S / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

13 U UG/KG Dichlorodifluoromethane 13 U UG/KG Dibromochloromethane13 U UG/KG Chloromethane 13 U UG/KG 1,2-Dibromoethane (EDB13 U UG/KG Vinyl Chloride 13 U UG/KG Chlorobenzene13 U UG/KG Bromomethane 13 U UG/KG Ethyl Benzene13 UJ UG/KG Chloroethane 13 U UG/KG Total Xylenes13 U UG/KG Trichlorofluoromethane (Freon 11) 13 U UG/KG Styrene13 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 13 U UG/KG Bromoform13 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 13 U UG/KG Isopropylbenzene13 U UG/KG Acetone 13 U UG/KG 1,1,2,2-Tetrachloroethan13 U UG/KG Carbon Disulfide 13 U UG/KG 1,3-Dichlorobenzene13 U UG/KG Methyl Acetate 13 U UG/KG 1,4-Dichlorobenzene13 U UG/KG Methylene Chloride 13 U UG/KG 1,2-Dichlorobenzene13 U UG/KG trans-1,2-Dichloroethene 13 U UG/KG 1,2-Dibromo-3-Chloropro13 U UG/KG Methyl T-Butyl Ether (MTBE) 13 U UG/KG 1,2,4-Trichlorobenzene13 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene13 U UG/KG cis-1,2-Dichloroethene 21 % % Moisture13 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

13 U UG/KG Chloroform13 U UG/KG 1,1,1-Trichloroethane13 U UG/KG Cyclohexane13 U UG/KG Carbon Tetrachloride13 U UG/KG Benzene13 U UG/KG 1,2-Dichloroethane13 U UG/KG Trichloroethene (Trichloroethylene)13 U UG/KG Methylcyclohexane13 U UG/KG 1,2-Dichloropropane13 U UG/KG Bromodichloromethane13 U UG/KG cis-1,3-Dichloropropene13 U UG/KG Methyl Isobutyl Ketone13 U UG/KG Toluene13 U UG/KG trans-1,3-Dichloropropene13 U UG/KG 1,1,2-Trichloroethane13 U UG/KG Tetrachloroethene (Tetrachloroethylene)13 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9522 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 10:55

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AJ8 D No: 3AJ8 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSF01 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

11 U UG/KG Dichlorodifluoromethane 11 U UG/KG Dibromochloromethane11 U UG/KG Chloromethane 11 U UG/KG 1,2-Dibromoethane (EDB11 U UG/KG Vinyl Chloride 11 U UG/KG Chlorobenzene11 U UG/KG Bromomethane 11 U UG/KG Ethyl Benzene11 UJ UG/KG Chloroethane 11 U UG/KG Total Xylenes11 U UG/KG Trichlorofluoromethane (Freon 11) 11 U UG/KG Styrene11 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 11 U UG/KG Bromoform11 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 11 U UG/KG Isopropylbenzene11 U UG/KG Acetone 11 U UG/KG 1,1,2,2-Tetrachloroethan11 U UG/KG Carbon Disulfide 11 U UG/KG 1,3-Dichlorobenzene11 U UG/KG Methyl Acetate 11 U UG/KG 1,4-Dichlorobenzene11 U UG/KG Methylene Chloride 11 U UG/KG 1,2-Dichlorobenzene11 U UG/KG trans-1,2-Dichloroethene 11 U UG/KG 1,2-Dibromo-3-Chloropro11 U UG/KG Methyl T-Butyl Ether (MTBE) 11 U UG/KG 1,2,4-Trichlorobenzene11 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene11 U UG/KG cis-1,2-Dichloroethene 9 % % Moisture11 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

11 U UG/KG Chloroform11 U UG/KG 1,1,1-Trichloroethane11 U UG/KG Cyclohexane11 U UG/KG Carbon Tetrachloride11 U UG/KG Benzene11 U UG/KG 1,2-Dichloroethane11 U UG/KG Trichloroethene (Trichloroethylene)11 U UG/KG Methylcyclohexane11 U UG/KG 1,2-Dichloropropane11 U UG/KG Bromodichloromethane11 U UG/KG cis-1,3-Dichloropropene11 U UG/KG Methyl Isobutyl Ketone11 U UG/KG Toluene11 U UG/KG trans-1,3-Dichloropropene11 U UG/KG 1,1,2-Trichloroethane11 U UG/KG Tetrachloroethene (Tetrachloroethylene)11 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9523 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 11:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AJ9 D No: 3AJ9 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD06 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

25 U UG/KG Dichlorodifluoromethane 25 U UG/KG Dibromochloromethane25 U UG/KG Chloromethane 25 U UG/KG 1,2-Dibromoethane (EDB25 U UG/KG Vinyl Chloride 25 U UG/KG Chlorobenzene25 U UG/KG Bromomethane 25 U UG/KG Ethyl Benzene25 UJ UG/KG Chloroethane 25 U UG/KG Total Xylenes25 U UG/KG Trichlorofluoromethane (Freon 11) 25 U UG/KG Styrene25 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 25 U UG/KG Bromoform25 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 25 U UG/KG Isopropylbenzene25 U UG/KG Acetone 25 U UG/KG 1,1,2,2-Tetrachloroethan25 U UG/KG Carbon Disulfide 25 U UG/KG 1,3-Dichlorobenzene25 U UG/KG Methyl Acetate 25 U UG/KG 1,4-Dichlorobenzene25 U UG/KG Methylene Chloride 25 U UG/KG 1,2-Dichlorobenzene25 U UG/KG trans-1,2-Dichloroethene 25 U UG/KG 1,2-Dibromo-3-Chloropro25 U UG/KG Methyl T-Butyl Ether (MTBE) 25 U UG/KG 1,2,4-Trichlorobenzene25 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene25 U UG/KG cis-1,2-Dichloroethene 51 % % Moisture25 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

25 U UG/KG Chloroform25 U UG/KG 1,1,1-Trichloroethane25 U UG/KG Cyclohexane25 U UG/KG Carbon Tetrachloride25 U UG/KG Benzene25 U UG/KG 1,2-Dichloroethane25 U UG/KG Trichloroethene (Trichloroethylene)25 U UG/KG Methylcyclohexane25 U UG/KG 1,2-Dichloropropane25 U UG/KG Bromodichloromethane25 U UG/KG cis-1,3-Dichloropropene25 U UG/KG Methyl Isobutyl Ketone25 U UG/KG Toluene25 U UG/KG trans-1,3-Dichloropropene25 U UG/KG 1,1,2-Trichloroethane25 U UG/KG Tetrachloroethene (Tetrachloroethylene)25 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9523 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 11:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ9 D No: 3AJ9 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD06 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

50 NJ UG/KG DIMETHYL SULFIDE

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9524 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 12:35

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AK0 D No: 3AK0 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD05 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

67 U UG/KG Dichlorodifluoromethane 67 U UG/KG Dibromochloromethane67 U UG/KG Chloromethane 67 U UG/KG 1,2-Dibromoethane (EDB67 U UG/KG Vinyl Chloride 67 U UG/KG Chlorobenzene67 U UG/KG Bromomethane 67 U UG/KG Ethyl Benzene67 UJ UG/KG Chloroethane 67 U UG/KG Total Xylenes67 U UG/KG Trichlorofluoromethane (Freon 11) 67 U UG/KG Styrene67 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 67 U UG/KG Bromoform67 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 67 U UG/KG Isopropylbenzene

180 UG/KG Acetone 67 U UG/KG 1,1,2,2-Tetrachloroethan

67 U UG/KG Carbon Disulfide 67 U UG/KG 1,3-Dichlorobenzene67 U UG/KG Methyl Acetate 67 U UG/KG 1,4-Dichlorobenzene67 U UG/KG Methylene Chloride 67 U UG/KG 1,2-Dichlorobenzene67 U UG/KG trans-1,2-Dichloroethene 67 U UG/KG 1,2-Dibromo-3-Chloropro67 U UG/KG Methyl T-Butyl Ether (MTBE) 67 U UG/KG 1,2,4-Trichlorobenzene67 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene67 U UG/KG cis-1,2-Dichloroethene 77 % % Moisture67 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

67 U UG/KG Chloroform67 U UG/KG 1,1,1-Trichloroethane67 U UG/KG Cyclohexane67 U UG/KG Carbon Tetrachloride67 U UG/KG Benzene67 U UG/KG 1,2-Dichloroethane67 U UG/KG Trichloroethene (Trichloroethylene)67 U UG/KG Methylcyclohexane67 U UG/KG 1,2-Dichloropropane67 U UG/KG Bromodichloromethane67 U UG/KG cis-1,3-Dichloropropene67 U UG/KG Methyl Isobutyl Ketone24 J UG/KG Toluene67 U UG/KG trans-1,3-Dichloropropene67 U UG/KG 1,1,2-Trichloroethane67 U UG/KG Tetrachloroethene (Tetrachloroethylene)67 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9524 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 12:35

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AK0 D No: 3AK0 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD05 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

120 NJ UG/KG (1R)-2,6,6-TRIMETHYLBICYCLO[3,1,1] HEPT-2-ENE

57 NJ UG/KG CAMPHENE

130 NJ UG/KG BENZENE, 1-METHYL-3-(1-METHYLETHYL)-

N UG/KG PETROLEUM PRODUCT

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9525 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 12:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AK1 D No: 3AK1 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD05D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

59 U UG/KG Dichlorodifluoromethane 59 U UG/KG Dibromochloromethane59 U UG/KG Chloromethane 59 U UG/KG 1,2-Dibromoethane (EDB59 U UG/KG Vinyl Chloride 59 U UG/KG Chlorobenzene59 U UG/KG Bromomethane 59 U UG/KG Ethyl Benzene59 UJ UG/KG Chloroethane 59 U UG/KG Total Xylenes59 U UG/KG Trichlorofluoromethane (Freon 11) 59 U UG/KG Styrene59 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 59 U UG/KG Bromoform59 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 59 U UG/KG Isopropylbenzene81 UG/KG Acetone 59 U UG/KG 1,1,2,2-Tetrachloroethan59 U UG/KG Carbon Disulfide 59 U UG/KG 1,3-Dichlorobenzene59 U UG/KG Methyl Acetate 59 U UG/KG 1,4-Dichlorobenzene59 U UG/KG Methylene Chloride 59 U UG/KG 1,2-Dichlorobenzene59 U UG/KG trans-1,2-Dichloroethene 59 U UG/KG 1,2-Dibromo-3-Chloropro59 U UG/KG Methyl T-Butyl Ether (MTBE) 59 U UG/KG 1,2,4-Trichlorobenzene59 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene59 U UG/KG cis-1,2-Dichloroethene 78 % % Moisture59 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

59 U UG/KG Chloroform59 U UG/KG 1,1,1-Trichloroethane59 U UG/KG Cyclohexane59 U UG/KG Carbon Tetrachloride59 U UG/KG Benzene59 U UG/KG 1,2-Dichloroethane59 U UG/KG Trichloroethene (Trichloroethylene)59 U UG/KG Methylcyclohexane59 U UG/KG 1,2-Dichloropropane59 U UG/KG Bromodichloromethane59 U UG/KG cis-1,3-Dichloropropene59 U UG/KG Methyl Isobutyl Ketone59 U UG/KG Toluene59 U UG/KG trans-1,3-Dichloropropene59 U UG/KG 1,1,2-Trichloroethane59 U UG/KG Tetrachloroethene (Tetrachloroethylene)59 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9526 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 12:40

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AK2 D No: 3AK2 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

35 U UG/KG Dichlorodifluoromethane 35 U UG/KG Dibromochloromethane35 U UG/KG Chloromethane 35 U UG/KG 1,2-Dibromoethane (EDB35 U UG/KG Vinyl Chloride 35 U UG/KG Chlorobenzene35 U UG/KG Bromomethane 35 U UG/KG Ethyl Benzene35 UJ UG/KG Chloroethane 35 U UG/KG Total Xylenes35 U UG/KG Trichlorofluoromethane (Freon 11) 35 U UG/KG Styrene35 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 35 U UG/KG Bromoform35 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 35 U UG/KG Isopropylbenzene35 U UG/KG Acetone 35 U UG/KG 1,1,2,2-Tetrachloroethan35 U UG/KG Carbon Disulfide 35 U UG/KG 1,3-Dichlorobenzene35 U UG/KG Methyl Acetate 35 U UG/KG 1,4-Dichlorobenzene35 U UG/KG Methylene Chloride 35 U UG/KG 1,2-Dichlorobenzene35 U UG/KG trans-1,2-Dichloroethene 35 U UG/KG 1,2-Dibromo-3-Chloropro35 U UG/KG Methyl T-Butyl Ether (MTBE) 35 U UG/KG 1,2,4-Trichlorobenzene35 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene35 U UG/KG cis-1,2-Dichloroethene 56 % % Moisture35 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

35 U UG/KG Chloroform35 U UG/KG 1,1,1-Trichloroethane35 U UG/KG Cyclohexane35 U UG/KG Carbon Tetrachloride35 U UG/KG Benzene35 U UG/KG 1,2-Dichloroethane35 U UG/KG Trichloroethene (Trichloroethylene)35 U UG/KG Methylcyclohexane35 U UG/KG 1,2-Dichloropropane35 U UG/KG Bromodichloromethane35 U UG/KG cis-1,3-Dichloropropene35 U UG/KG Methyl Isobutyl Ketone35 U UG/KG Toluene35 U UG/KG trans-1,3-Dichloropropene35 U UG/KG 1,1,2-Trichloroethane35 U UG/KG Tetrachloroethene (Tetrachloroethylene)35 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9527 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 13:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AK5 D No: 3AK5 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD04 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

13 U UG/KG Dichlorodifluoromethane 13 U UG/KG Dibromochloromethane13 U UG/KG Chloromethane 13 U UG/KG 1,2-Dibromoethane (EDB13 U UG/KG Vinyl Chloride 13 U UG/KG Chlorobenzene13 U UG/KG Bromomethane 13 U UG/KG Ethyl Benzene13 UJ UG/KG Chloroethane 13 U UG/KG Total Xylenes13 U UG/KG Trichlorofluoromethane (Freon 11) 13 U UG/KG Styrene13 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 13 U UG/KG Bromoform13 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 13 U UG/KG Isopropylbenzene13 U UG/KG Acetone 13 U UG/KG 1,1,2,2-Tetrachloroethan13 U UG/KG Carbon Disulfide 13 U UG/KG 1,3-Dichlorobenzene13 U UG/KG Methyl Acetate 13 U UG/KG 1,4-Dichlorobenzene13 U UG/KG Methylene Chloride 13 U UG/KG 1,2-Dichlorobenzene13 U UG/KG trans-1,2-Dichloroethene 13 U UG/KG 1,2-Dibromo-3-Chloropro13 U UG/KG Methyl T-Butyl Ether (MTBE) 13 U UG/KG 1,2,4-Trichlorobenzene13 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene13 U UG/KG cis-1,2-Dichloroethene 25 % % Moisture13 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

13 U UG/KG Chloroform13 U UG/KG 1,1,1-Trichloroethane13 U UG/KG Cyclohexane13 U UG/KG Carbon Tetrachloride13 U UG/KG Benzene13 U UG/KG 1,2-Dichloroethane13 U UG/KG Trichloroethene (Trichloroethylene)13 U UG/KG Methylcyclohexane13 U UG/KG 1,2-Dichloropropane13 U UG/KG Bromodichloromethane13 U UG/KG cis-1,3-Dichloropropene13 U UG/KG Methyl Isobutyl Ketone13 U UG/KG Toluene13 U UG/KG trans-1,3-Dichloropropene13 U UG/KG 1,1,2-Trichloroethane13 U UG/KG Tetrachloroethene (Tetrachloroethylene)13 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9527 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 13:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AK5 D No: 3AK5 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF CFMSD04 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

21 J UG/KG 1 UNKNOWN

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9528 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 12:25

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AF9 D No: 3AF9 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSD01 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

96 U UG/KG Dichlorodifluoromethane 96 U UG/KG Dibromochloromethane96 U UG/KG Chloromethane 96 U UG/KG 1,2-Dibromoethane (EDB96 U UG/KG Vinyl Chloride 96 U UG/KG Chlorobenzene96 U UG/KG Bromomethane 96 U UG/KG Ethyl Benzene96 UJ UG/KG Chloroethane 96 U UG/KG Total Xylenes96 U UG/KG Trichlorofluoromethane (Freon 11) 96 U UG/KG Styrene96 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 96 U UG/KG Bromoform96 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 96 U UG/KG Isopropylbenzene96 U UG/KG Acetone 96 U UG/KG 1,1,2,2-Tetrachloroethan96 U UG/KG Carbon Disulfide 96 U UG/KG 1,3-Dichlorobenzene96 U UG/KG Methyl Acetate 96 U UG/KG 1,4-Dichlorobenzene96 U UG/KG Methylene Chloride 96 U UG/KG 1,2-Dichlorobenzene96 U UG/KG trans-1,2-Dichloroethene 96 U UG/KG 1,2-Dibromo-3-Chloropro96 U UG/KG Methyl T-Butyl Ether (MTBE) 96 U UG/KG 1,2,4-Trichlorobenzene96 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene96 U UG/KG cis-1,2-Dichloroethene 78 % % Moisture96 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

96 U UG/KG Chloroform96 U UG/KG 1,1,1-Trichloroethane96 U UG/KG Cyclohexane96 U UG/KG Carbon Tetrachloride96 U UG/KG Benzene96 U UG/KG 1,2-Dichloroethane96 U UG/KG Trichloroethene (Trichloroethylene)96 U UG/KG Methylcyclohexane96 U UG/KG 1,2-Dichloropropane96 U UG/KG Bromodichloromethane96 U UG/KG cis-1,3-Dichloropropene96 U UG/KG Methyl Isobutyl Ketone96 U UG/KG Toluene96 U UG/KG trans-1,3-Dichloropropene96 U UG/KG 1,1,2-Trichloroethane96 U UG/KG Tetrachloroethene (Tetrachloroethylene)96 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9529 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 12:40

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AG0 D No: 3AG0 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSD01D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

110 U UG/KG Dichlorodifluoromethane 110 U UG/KG Dibromochloromethane110 U UG/KG Chloromethane 110 U UG/KG 1,2-Dibromoethane (EDB110 U UG/KG Vinyl Chloride 110 U UG/KG Chlorobenzene110 U UG/KG Bromomethane 110 U UG/KG Ethyl Benzene110 UJ UG/KG Chloroethane 110 U UG/KG Total Xylenes110 U UG/KG Trichlorofluoromethane (Freon 11) 110 U UG/KG Styrene110 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 110 U UG/KG Bromoform110 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 110 U UG/KG Isopropylbenzene140 UG/KG Acetone 110 U UG/KG 1,1,2,2-Tetrachloroethan110 U UG/KG Carbon Disulfide 110 U UG/KG 1,3-Dichlorobenzene110 U UG/KG Methyl Acetate 110 U UG/KG 1,4-Dichlorobenzene110 U UG/KG Methylene Chloride 110 U UG/KG 1,2-Dichlorobenzene110 U UG/KG trans-1,2-Dichloroethene 110 U UG/KG 1,2-Dibromo-3-Chloropro110 U UG/KG Methyl T-Butyl Ether (MTBE) 110 U UG/KG 1,2,4-Trichlorobenzene110 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene110 U UG/KG cis-1,2-Dichloroethene 80 % % Moisture110 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

110 U UG/KG Chloroform110 U UG/KG 1,1,1-Trichloroethane110 U UG/KG Cyclohexane110 U UG/KG Carbon Tetrachloride110 U UG/KG Benzene110 U UG/KG 1,2-Dichloroethane110 U UG/KG Trichloroethene (Trichloroethylene)110 U UG/KG Methylcyclohexane110 U UG/KG 1,2-Dichloropropane110 U UG/KG Bromodichloromethane110 U UG/KG cis-1,3-Dichloropropene110 U UG/KG Methyl Isobutyl Ketone110 U UG/KG Toluene110 U UG/KG trans-1,3-Dichloropropene110 U UG/KG 1,1,2-Trichloroethane110 U UG/KG Tetrachloroethene (Tetrachloroethylene)110 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9530 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 13:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AG1 D No: 3AG1 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSD02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

32 U UG/KG Dichlorodifluoromethane 32 U UG/KG Dibromochloromethane32 U UG/KG Chloromethane 32 U UG/KG 1,2-Dibromoethane (EDB32 U UG/KG Vinyl Chloride 32 U UG/KG Chlorobenzene32 U UG/KG Bromomethane 32 U UG/KG Ethyl Benzene32 UJ UG/KG Chloroethane 32 U UG/KG Total Xylenes32 U UG/KG Trichlorofluoromethane (Freon 11) 32 U UG/KG Styrene32 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 32 U UG/KG Bromoform32 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 32 U UG/KG Isopropylbenzene32 U UG/KG Acetone 32 U UG/KG 1,1,2,2-Tetrachloroethan32 U UG/KG Carbon Disulfide 32 U UG/KG 1,3-Dichlorobenzene32 U UG/KG Methyl Acetate 32 U UG/KG 1,4-Dichlorobenzene32 U UG/KG Methylene Chloride 32 U UG/KG 1,2-Dichlorobenzene32 U UG/KG trans-1,2-Dichloroethene 32 U UG/KG 1,2-Dibromo-3-Chloropro32 U UG/KG Methyl T-Butyl Ether (MTBE) 32 U UG/KG 1,2,4-Trichlorobenzene32 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene32 U UG/KG cis-1,2-Dichloroethene 58 % % Moisture32 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

32 U UG/KG Chloroform32 U UG/KG 1,1,1-Trichloroethane32 U UG/KG Cyclohexane32 U UG/KG Carbon Tetrachloride32 U UG/KG Benzene32 U UG/KG 1,2-Dichloroethane32 U UG/KG Trichloroethene (Trichloroethylene)32 U UG/KG Methylcyclohexane32 U UG/KG 1,2-Dichloropropane32 U UG/KG Bromodichloromethane32 U UG/KG cis-1,3-Dichloropropene32 U UG/KG Methyl Isobutyl Ketone32 U UG/KG Toluene32 U UG/KG trans-1,3-Dichloropropene32 U UG/KG 1,1,2-Trichloroethane32 U UG/KG Tetrachloroethene (Tetrachloroethylene)32 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9531 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 13:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AG2 D No: 3AG2 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSD03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

11 U UG/KG Dichlorodifluoromethane 11 U UG/KG Dibromochloromethane11 U UG/KG Chloromethane 11 U UG/KG 1,2-Dibromoethane (EDB11 U UG/KG Vinyl Chloride 11 U UG/KG Chlorobenzene11 U UG/KG Bromomethane 11 U UG/KG Ethyl Benzene11 UJ UG/KG Chloroethane 11 U UG/KG Total Xylenes11 U UG/KG Trichlorofluoromethane (Freon 11) 11 U UG/KG Styrene11 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 11 U UG/KG Bromoform11 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 11 U UG/KG Isopropylbenzene11 U UG/KG Acetone 11 U UG/KG 1,1,2,2-Tetrachloroethan11 U UG/KG Carbon Disulfide 11 U UG/KG 1,3-Dichlorobenzene11 U UG/KG Methyl Acetate 11 U UG/KG 1,4-Dichlorobenzene11 U UG/KG Methylene Chloride 11 U UG/KG 1,2-Dichlorobenzene11 U UG/KG trans-1,2-Dichloroethene 11 U UG/KG 1,2-Dibromo-3-Chloropro11 U UG/KG Methyl T-Butyl Ether (MTBE) 11 U UG/KG 1,2,4-Trichlorobenzene11 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene11 U UG/KG cis-1,2-Dichloroethene 17 % % Moisture11 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

11 U UG/KG Chloroform11 U UG/KG 1,1,1-Trichloroethane11 U UG/KG Cyclohexane11 U UG/KG Carbon Tetrachloride11 U UG/KG Benzene11 U UG/KG 1,2-Dichloroethane11 U UG/KG Trichloroethene (Trichloroethylene)11 U UG/KG Methylcyclohexane11 U UG/KG 1,2-Dichloropropane11 U UG/KG Bromodichloromethane11 U UG/KG cis-1,3-Dichloropropene11 U UG/KG Methyl Isobutyl Ketone11 U UG/KG Toluene11 U UG/KG trans-1,3-Dichloropropene11 U UG/KG 1,1,2-Trichloroethane11 U UG/KG Tetrachloroethene (Tetrachloroethylene)11 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9532 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 12:50

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AG3 D No: 3AG3 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSF04 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

10 U UG/KG Dichlorodifluoromethane 10 U UG/KG Dibromochloromethane10 U UG/KG Chloromethane 10 U UG/KG 1,2-Dibromoethane (EDB10 U UG/KG Vinyl Chloride 10 U UG/KG Chlorobenzene10 U UG/KG Bromomethane 10 U UG/KG Ethyl Benzene10 UJ UG/KG Chloroethane 10 U UG/KG Total Xylenes10 U UG/KG Trichlorofluoromethane (Freon 11) 10 U UG/KG Styrene10 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 10 U UG/KG Bromoform10 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 10 U UG/KG Isopropylbenzene10 UJ UG/KG Acetone 10 U UG/KG 1,1,2,2-Tetrachloroethan10 U UG/KG Carbon Disulfide 10 U UG/KG 1,3-Dichlorobenzene10 UJ UG/KG Methyl Acetate 10 U UG/KG 1,4-Dichlorobenzene10 U UG/KG Methylene Chloride 10 U UG/KG 1,2-Dichlorobenzene10 U UG/KG trans-1,2-Dichloroethene 10 U UG/KG 1,2-Dibromo-3-Chloropro10 U UG/KG Methyl T-Butyl Ether (MTBE) 10 U UG/KG 1,2,4-Trichlorobenzene10 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene10 U UG/KG cis-1,2-Dichloroethene 12 % % Moisture10 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

10 U UG/KG Chloroform10 U UG/KG 1,1,1-Trichloroethane10 U UG/KG Cyclohexane10 U UG/KG Carbon Tetrachloride10 U UG/KG Benzene10 U UG/KG 1,2-Dichloroethane10 U UG/KG Trichloroethene (Trichloroethylene)10 U UG/KG Methylcyclohexane10 U UG/KG 1,2-Dichloropropane10 U UG/KG Bromodichloromethane10 U UG/KG cis-1,3-Dichloropropene10 U UG/KG Methyl Isobutyl Ketone10 U UG/KG Toluene10 U UG/KG trans-1,3-Dichloropropene10 U UG/KG 1,1,2-Trichloroethane10 U UG/KG Tetrachloroethene (Tetrachloroethylene)10 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9533 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 12:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AG4 D No: 3AG4 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSF05 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

10 U UG/KG Dichlorodifluoromethane 10 U UG/KG Dibromochloromethane10 U UG/KG Chloromethane 10 U UG/KG 1,2-Dibromoethane (EDB10 U UG/KG Vinyl Chloride 10 U UG/KG Chlorobenzene10 U UG/KG Bromomethane 10 U UG/KG Ethyl Benzene10 UJ UG/KG Chloroethane 10 U UG/KG Total Xylenes10 U UG/KG Trichlorofluoromethane (Freon 11) 10 U UG/KG Styrene10 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 10 U UG/KG Bromoform10 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 10 U UG/KG Isopropylbenzene10 UJ UG/KG Acetone 10 U UG/KG 1,1,2,2-Tetrachloroethan10 U UG/KG Carbon Disulfide 10 U UG/KG 1,3-Dichlorobenzene10 UJ UG/KG Methyl Acetate 10 U UG/KG 1,4-Dichlorobenzene10 U UG/KG Methylene Chloride 10 U UG/KG 1,2-Dichlorobenzene10 U UG/KG trans-1,2-Dichloroethene 10 U UG/KG 1,2-Dibromo-3-Chloropro10 U UG/KG Methyl T-Butyl Ether (MTBE) 10 U UG/KG 1,2,4-Trichlorobenzene10 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene10 U UG/KG cis-1,2-Dichloroethene 13 % % Moisture10 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

10 U UG/KG Chloroform10 U UG/KG 1,1,1-Trichloroethane10 U UG/KG Cyclohexane10 U UG/KG Carbon Tetrachloride10 U UG/KG Benzene10 U UG/KG 1,2-Dichloroethane10 U UG/KG Trichloroethene (Trichloroethylene)10 U UG/KG Methylcyclohexane10 U UG/KG 1,2-Dichloropropane10 U UG/KG Bromodichloromethane10 U UG/KG cis-1,3-Dichloropropene10 U UG/KG Methyl Isobutyl Ketone10 U UG/KG Toluene10 U UG/KG trans-1,3-Dichloropropene10 U UG/KG 1,1,2-Trichloroethane10 U UG/KG Tetrachloroethene (Tetrachloroethylene)10 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9534 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 12:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AG5 D No: 3AG5 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POSF05S / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

10 U UG/KG Dichlorodifluoromethane 10 U UG/KG Dibromochloromethane10 U UG/KG Chloromethane 10 U UG/KG 1,2-Dibromoethane (EDB10 U UG/KG Vinyl Chloride 10 U UG/KG Chlorobenzene10 U UG/KG Bromomethane 10 U UG/KG Ethyl Benzene10 UJ UG/KG Chloroethane 10 U UG/KG Total Xylenes10 U UG/KG Trichlorofluoromethane (Freon 11) 10 U UG/KG Styrene10 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 10 U UG/KG Bromoform10 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 10 U UG/KG Isopropylbenzene10 UJ UG/KG Acetone 10 U UG/KG 1,1,2,2-Tetrachloroethan10 U UG/KG Carbon Disulfide 10 U UG/KG 1,3-Dichlorobenzene10 UJ UG/KG Methyl Acetate 10 U UG/KG 1,4-Dichlorobenzene10 U UG/KG Methylene Chloride 10 U UG/KG 1,2-Dichlorobenzene10 U UG/KG trans-1,2-Dichloroethene 10 U UG/KG 1,2-Dibromo-3-Chloropro10 U UG/KG Methyl T-Butyl Ether (MTBE) 10 U UG/KG 1,2,4-Trichlorobenzene10 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene10 U UG/KG cis-1,2-Dichloroethene 13 % % Moisture10 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

10 U UG/KG Chloroform10 U UG/KG 1,1,1-Trichloroethane10 U UG/KG Cyclohexane10 U UG/KG Carbon Tetrachloride10 U UG/KG Benzene10 U UG/KG 1,2-Dichloroethane10 U UG/KG Trichloroethene (Trichloroethylene)10 U UG/KG Methylcyclohexane10 U UG/KG 1,2-Dichloropropane10 U UG/KG Bromodichloromethane10 U UG/KG cis-1,3-Dichloropropene10 U UG/KG Methyl Isobutyl Ketone10 U UG/KG Toluene10 U UG/KG trans-1,3-Dichloropropene10 U UG/KG 1,1,2-Trichloroethane10 U UG/KG Tetrachloroethene (Tetrachloroethylene)10 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9535 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 09:00

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AG7 D No: 3AG7 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF OPSD02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

10 U UG/KG Dichlorodifluoromethane 10 U UG/KG Dibromochloromethane10 U UG/KG Chloromethane 10 U UG/KG 1,2-Dibromoethane (EDB10 U UG/KG Vinyl Chloride 10 U UG/KG Chlorobenzene10 UJ UG/KG Bromomethane 10 U UG/KG Ethyl Benzene10 U UG/KG Chloroethane 10 U UG/KG Total Xylenes10 U UG/KG Trichlorofluoromethane (Freon 11) 10 U UG/KG Styrene10 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 10 U UG/KG Bromoform10 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 10 U UG/KG Isopropylbenzene10 UJ UG/KG Acetone 10 U UG/KG 1,1,2,2-Tetrachloroethan10 U UG/KG Carbon Disulfide 10 U UG/KG 1,3-Dichlorobenzene10 U UG/KG Methyl Acetate 10 U UG/KG 1,4-Dichlorobenzene10 UJ UG/KG Methylene Chloride 10 U UG/KG 1,2-Dichlorobenzene10 U UG/KG trans-1,2-Dichloroethene 10 U UG/KG 1,2-Dibromo-3-Chloropro10 U UG/KG Methyl T-Butyl Ether (MTBE) 10 U UG/KG 1,2,4-Trichlorobenzene10 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene10 U UG/KG cis-1,2-Dichloroethene 14 % % Moisture10 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

10 U UG/KG Chloroform10 U UG/KG 1,1,1-Trichloroethane10 U UG/KG Cyclohexane10 U UG/KG Carbon Tetrachloride10 U UG/KG Benzene10 U UG/KG 1,2-Dichloroethane10 U UG/KG Trichloroethene (Trichloroethylene)10 U UG/KG Methylcyclohexane10 U UG/KG 1,2-Dichloropropane10 U UG/KG Bromodichloromethane10 U UG/KG cis-1,3-Dichloropropene10 U UG/KG Methyl Isobutyl Ketone10 U UG/KG Toluene10 U UG/KG trans-1,3-Dichloropropene10 U UG/KG 1,1,2-Trichloroethane10 U UG/KG Tetrachloroethene (Tetrachloroethylene)10 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9536 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 09:25

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AG8 D No: 3AG8 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF OPSD02D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

11 U UG/KG Dichlorodifluoromethane 11 U UG/KG Dibromochloromethane11 U UG/KG Chloromethane 11 U UG/KG 1,2-Dibromoethane (EDB11 U UG/KG Vinyl Chloride 11 U UG/KG Chlorobenzene11 UJ UG/KG Bromomethane 11 U UG/KG Ethyl Benzene11 U UG/KG Chloroethane 11 U UG/KG Total Xylenes11 U UG/KG Trichlorofluoromethane (Freon 11) 11 U UG/KG Styrene11 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 11 U UG/KG Bromoform11 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 11 U UG/KG Isopropylbenzene11 UJ UG/KG Acetone 11 U UG/KG 1,1,2,2-Tetrachloroethan11 U UG/KG Carbon Disulfide 11 U UG/KG 1,3-Dichlorobenzene11 U UG/KG Methyl Acetate 11 U UG/KG 1,4-Dichlorobenzene11 UJ UG/KG Methylene Chloride 11 U UG/KG 1,2-Dichlorobenzene11 U UG/KG trans-1,2-Dichloroethene 11 U UG/KG 1,2-Dibromo-3-Chloropro11 U UG/KG Methyl T-Butyl Ether (MTBE) 11 U UG/KG 1,2,4-Trichlorobenzene11 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene11 U UG/KG cis-1,2-Dichloroethene 19 % % Moisture11 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

11 U UG/KG Chloroform11 U UG/KG 1,1,1-Trichloroethane11 U UG/KG Cyclohexane11 U UG/KG Carbon Tetrachloride11 U UG/KG Benzene11 U UG/KG 1,2-Dichloroethane11 U UG/KG Trichloroethene (Trichloroethylene)11 U UG/KG Methylcyclohexane11 U UG/KG 1,2-Dichloropropane11 U UG/KG Bromodichloromethane11 U UG/KG cis-1,3-Dichloropropene11 U UG/KG Methyl Isobutyl Ketone11 U UG/KG Toluene11 U UG/KG trans-1,3-Dichloropropene11 U UG/KG 1,1,2-Trichloroethane11 U UG/KG Tetrachloroethene (Tetrachloroethylene)11 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9537 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 09:50

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AG9 D No: 3AG9 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF OPSD01 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

10 U UG/KG Dichlorodifluoromethane 10 U UG/KG Dibromochloromethane10 U UG/KG Chloromethane 10 U UG/KG 1,2-Dibromoethane (EDB10 U UG/KG Vinyl Chloride 10 U UG/KG Chlorobenzene10 UJ UG/KG Bromomethane 10 U UG/KG Ethyl Benzene10 U UG/KG Chloroethane 10 U UG/KG Total Xylenes10 U UG/KG Trichlorofluoromethane (Freon 11) 10 U UG/KG Styrene10 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 10 U UG/KG Bromoform10 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 10 U UG/KG Isopropylbenzene10 UJ UG/KG Acetone 10 U UG/KG 1,1,2,2-Tetrachloroethan10 U UG/KG Carbon Disulfide 10 U UG/KG 1,3-Dichlorobenzene10 U UG/KG Methyl Acetate 10 U UG/KG 1,4-Dichlorobenzene10 UJ UG/KG Methylene Chloride 10 U UG/KG 1,2-Dichlorobenzene10 U UG/KG trans-1,2-Dichloroethene 10 U UG/KG 1,2-Dibromo-3-Chloropro10 U UG/KG Methyl T-Butyl Ether (MTBE) 10 U UG/KG 1,2,4-Trichlorobenzene10 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene10 U UG/KG cis-1,2-Dichloroethene 6 % % Moisture10 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

10 U UG/KG Chloroform10 U UG/KG 1,1,1-Trichloroethane10 U UG/KG Cyclohexane10 U UG/KG Carbon Tetrachloride10 U UG/KG Benzene10 U UG/KG 1,2-Dichloroethane10 U UG/KG Trichloroethene (Trichloroethylene)10 U UG/KG Methylcyclohexane10 U UG/KG 1,2-Dichloropropane10 U UG/KG Bromodichloromethane10 U UG/KG cis-1,3-Dichloropropene10 U UG/KG Methyl Isobutyl Ketone10 U UG/KG Toluene10 U UG/KG trans-1,3-Dichloropropene10 U UG/KG 1,1,2-Trichloroethane10 U UG/KG Tetrachloroethene (Tetrachloroethylene)10 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9538 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 10:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AH0 D No: 3AH0 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF OPSD03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

11 U UG/KG Dichlorodifluoromethane 11 U UG/KG Dibromochloromethane11 U UG/KG Chloromethane 11 U UG/KG 1,2-Dibromoethane (EDB11 U UG/KG Vinyl Chloride 11 U UG/KG Chlorobenzene11 UJ UG/KG Bromomethane 11 U UG/KG Ethyl Benzene11 U UG/KG Chloroethane 11 U UG/KG Total Xylenes11 U UG/KG Trichlorofluoromethane (Freon 11) 11 U UG/KG Styrene11 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 11 U UG/KG Bromoform11 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 11 U UG/KG Isopropylbenzene11 UJ UG/KG Acetone 11 U UG/KG 1,1,2,2-Tetrachloroethan11 U UG/KG Carbon Disulfide 11 U UG/KG 1,3-Dichlorobenzene11 U UG/KG Methyl Acetate 11 U UG/KG 1,4-Dichlorobenzene11 UJ UG/KG Methylene Chloride 11 U UG/KG 1,2-Dichlorobenzene11 U UG/KG trans-1,2-Dichloroethene 11 U UG/KG 1,2-Dibromo-3-Chloropro11 U UG/KG Methyl T-Butyl Ether (MTBE) 11 U UG/KG 1,2,4-Trichlorobenzene11 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene11 U UG/KG cis-1,2-Dichloroethene 14 % % Moisture11 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

11 U UG/KG Chloroform11 U UG/KG 1,1,1-Trichloroethane11 U UG/KG Cyclohexane11 U UG/KG Carbon Tetrachloride11 U UG/KG Benzene11 U UG/KG 1,2-Dichloroethane11 U UG/KG Trichloroethene (Trichloroethylene)11 U UG/KG Methylcyclohexane11 U UG/KG 1,2-Dichloropropane11 U UG/KG Bromodichloromethane11 U UG/KG cis-1,3-Dichloropropene11 U UG/KG Methyl Isobutyl Ketone11 U UG/KG Toluene11 U UG/KG trans-1,3-Dichloropropene11 U UG/KG 1,1,2-Trichloroethane11 U UG/KG Tetrachloroethene (Tetrachloroethylene)11 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9539 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 09:15

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AH1 D No: 3AH1 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSF01 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

18 U UG/KG Dichlorodifluoromethane 18 U UG/KG Dibromochloromethane18 U UG/KG Chloromethane 18 U UG/KG 1,2-Dibromoethane (EDB18 U UG/KG Vinyl Chloride 18 U UG/KG Chlorobenzene18 UJ UG/KG Bromomethane 18 U UG/KG Ethyl Benzene18 U UG/KG Chloroethane 18 U UG/KG Total Xylenes18 U UG/KG Trichlorofluoromethane (Freon 11) 18 U UG/KG Styrene18 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 18 U UG/KG Bromoform18 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 18 U UG/KG Isopropylbenzene18 UJ UG/KG Acetone 18 U UG/KG 1,1,2,2-Tetrachloroethan18 U UG/KG Carbon Disulfide 18 U UG/KG 1,3-Dichlorobenzene18 U UG/KG Methyl Acetate 18 U UG/KG 1,4-Dichlorobenzene18 UJ UG/KG Methylene Chloride 18 U UG/KG 1,2-Dichlorobenzene18 U UG/KG trans-1,2-Dichloroethene 18 U UG/KG 1,2-Dibromo-3-Chloropro18 U UG/KG Methyl T-Butyl Ether (MTBE) 18 U UG/KG 1,2,4-Trichlorobenzene18 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene18 U UG/KG cis-1,2-Dichloroethene 36 % % Moisture18 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

18 U UG/KG Chloroform18 U UG/KG 1,1,1-Trichloroethane18 U UG/KG Cyclohexane18 U UG/KG Carbon Tetrachloride18 U UG/KG Benzene18 U UG/KG 1,2-Dichloroethane18 U UG/KG Trichloroethene (Trichloroethylene)18 U UG/KG Methylcyclohexane18 U UG/KG 1,2-Dichloropropane18 U UG/KG Bromodichloromethane18 U UG/KG cis-1,3-Dichloropropene18 U UG/KG Methyl Isobutyl Ketone18 U UG/KG Toluene18 U UG/KG trans-1,3-Dichloropropene18 U UG/KG 1,1,2-Trichloroethane18 U UG/KG Tetrachloroethene (Tetrachloroethylene)18 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9540 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 09:15

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AH2 D No: 3AH2 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSF01S / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

15 U UG/KG Dichlorodifluoromethane 15 U UG/KG Dibromochloromethane15 U UG/KG Chloromethane 15 U UG/KG 1,2-Dibromoethane (EDB15 U UG/KG Vinyl Chloride 15 U UG/KG Chlorobenzene15 UJ UG/KG Bromomethane 15 U UG/KG Ethyl Benzene15 U UG/KG Chloroethane 15 U UG/KG Total Xylenes15 U UG/KG Trichlorofluoromethane (Freon 11) 15 U UG/KG Styrene15 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 15 U UG/KG Bromoform15 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 15 U UG/KG Isopropylbenzene15 UJ UG/KG Acetone 15 U UG/KG 1,1,2,2-Tetrachloroethan15 U UG/KG Carbon Disulfide 15 U UG/KG 1,3-Dichlorobenzene15 U UG/KG Methyl Acetate 15 U UG/KG 1,4-Dichlorobenzene15 UJ UG/KG Methylene Chloride 15 U UG/KG 1,2-Dichlorobenzene15 U UG/KG trans-1,2-Dichloroethene 15 U UG/KG 1,2-Dibromo-3-Chloropro15 U UG/KG Methyl T-Butyl Ether (MTBE) 15 U UG/KG 1,2,4-Trichlorobenzene15 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene15 U UG/KG cis-1,2-Dichloroethene 36 % % Moisture15 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

15 U UG/KG Chloroform15 U UG/KG 1,1,1-Trichloroethane15 U UG/KG Cyclohexane15 U UG/KG Carbon Tetrachloride15 U UG/KG Benzene15 U UG/KG 1,2-Dichloroethane15 U UG/KG Trichloroethene (Trichloroethylene)15 U UG/KG Methylcyclohexane15 U UG/KG 1,2-Dichloropropane15 U UG/KG Bromodichloromethane15 U UG/KG cis-1,3-Dichloropropene15 U UG/KG Methyl Isobutyl Ketone15 U UG/KG Toluene15 U UG/KG trans-1,3-Dichloropropene15 U UG/KG 1,1,2-Trichloroethane15 U UG/KG Tetrachloroethene (Tetrachloroethylene)15 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9541 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 10:10

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AH3 D No: 3AH3 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSF02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

11 U UG/KG Dichlorodifluoromethane 11 U UG/KG Dibromochloromethane11 U UG/KG Chloromethane 11 U UG/KG 1,2-Dibromoethane (EDB11 U UG/KG Vinyl Chloride 11 U UG/KG Chlorobenzene11 UJ UG/KG Bromomethane 11 U UG/KG Ethyl Benzene11 U UG/KG Chloroethane 11 U UG/KG Total Xylenes11 U UG/KG Trichlorofluoromethane (Freon 11) 11 U UG/KG Styrene11 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 11 U UG/KG Bromoform11 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 11 U UG/KG Isopropylbenzene11 UJ UG/KG Acetone 11 U UG/KG 1,1,2,2-Tetrachloroethan11 U UG/KG Carbon Disulfide 11 U UG/KG 1,3-Dichlorobenzene11 U UG/KG Methyl Acetate 11 U UG/KG 1,4-Dichlorobenzene11 UJ UG/KG Methylene Chloride 11 U UG/KG 1,2-Dichlorobenzene11 U UG/KG trans-1,2-Dichloroethene 11 U UG/KG 1,2-Dibromo-3-Chloropro11 U UG/KG Methyl T-Butyl Ether (MTBE) 11 U UG/KG 1,2,4-Trichlorobenzene11 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene11 U UG/KG cis-1,2-Dichloroethene 9 % % Moisture11 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

11 U UG/KG Chloroform11 U UG/KG 1,1,1-Trichloroethane11 U UG/KG Cyclohexane11 U UG/KG Carbon Tetrachloride11 U UG/KG Benzene11 U UG/KG 1,2-Dichloroethane11 U UG/KG Trichloroethene (Trichloroethylene)11 U UG/KG Methylcyclohexane11 U UG/KG 1,2-Dichloropropane11 U UG/KG Bromodichloromethane11 U UG/KG cis-1,3-Dichloropropene11 U UG/KG Methyl Isobutyl Ketone11 U UG/KG Toluene11 U UG/KG trans-1,3-Dichloropropene11 U UG/KG 1,1,2-Trichloroethane11 U UG/KG Tetrachloroethene (Tetrachloroethylene)11 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9542 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 10:50

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AH4 D No: 3AH4 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSF03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

11 U UG/KG Dichlorodifluoromethane 11 U UG/KG Dibromochloromethane11 U UG/KG Chloromethane 11 U UG/KG 1,2-Dibromoethane (EDB11 U UG/KG Vinyl Chloride 11 U UG/KG Chlorobenzene11 UJ UG/KG Bromomethane 11 U UG/KG Ethyl Benzene11 U UG/KG Chloroethane 11 U UG/KG Total Xylenes11 U UG/KG Trichlorofluoromethane (Freon 11) 11 U UG/KG Styrene11 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 11 U UG/KG Bromoform11 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 11 U UG/KG Isopropylbenzene11 UJ UG/KG Acetone 11 U UG/KG 1,1,2,2-Tetrachloroethan11 U UG/KG Carbon Disulfide 11 U UG/KG 1,3-Dichlorobenzene11 U UG/KG Methyl Acetate 11 U UG/KG 1,4-Dichlorobenzene11 UJ UG/KG Methylene Chloride 11 U UG/KG 1,2-Dichlorobenzene11 U UG/KG trans-1,2-Dichloroethene 11 U UG/KG 1,2-Dibromo-3-Chloropro11 U UG/KG Methyl T-Butyl Ether (MTBE) 11 U UG/KG 1,2,4-Trichlorobenzene11 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene11 U UG/KG cis-1,2-Dichloroethene 18 % % Moisture11 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

11 U UG/KG Chloroform11 U UG/KG 1,1,1-Trichloroethane11 U UG/KG Cyclohexane11 U UG/KG Carbon Tetrachloride11 U UG/KG Benzene11 U UG/KG 1,2-Dichloroethane11 U UG/KG Trichloroethene (Trichloroethylene)11 U UG/KG Methylcyclohexane11 U UG/KG 1,2-Dichloropropane11 U UG/KG Bromodichloromethane11 U UG/KG cis-1,3-Dichloropropene11 U UG/KG Methyl Isobutyl Ketone11 U UG/KG Toluene11 U UG/KG trans-1,3-Dichloropropene11 U UG/KG 1,1,2-Trichloroethane11 U UG/KG Tetrachloroethene (Tetrachloroethylene)11 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9542 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 10:50

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH4 D No: 3AH4 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSF03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

41 J UG/KG UNKNOWN

N UG/KG PETROLEUM PRODUCT

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9543 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 11:15

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AH5 D No: 3AH5 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSD04 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

22 U UG/KG Dichlorodifluoromethane 22 U UG/KG Dibromochloromethane22 U UG/KG Chloromethane 22 U UG/KG 1,2-Dibromoethane (EDB22 U UG/KG Vinyl Chloride 22 U UG/KG Chlorobenzene22 UJ UG/KG Bromomethane 22 U UG/KG Ethyl Benzene22 U UG/KG Chloroethane 22 U UG/KG Total Xylenes22 U UG/KG Trichlorofluoromethane (Freon 11) 22 U UG/KG Styrene22 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 22 U UG/KG Bromoform22 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 22 U UG/KG Isopropylbenzene22 UJ UG/KG Acetone 22 U UG/KG 1,1,2,2-Tetrachloroethan22 U UG/KG Carbon Disulfide 22 U UG/KG 1,3-Dichlorobenzene22 U UG/KG Methyl Acetate 22 U UG/KG 1,4-Dichlorobenzene22 UJ UG/KG Methylene Chloride 22 U UG/KG 1,2-Dichlorobenzene22 U UG/KG trans-1,2-Dichloroethene 22 U UG/KG 1,2-Dibromo-3-Chloropro22 U UG/KG Methyl T-Butyl Ether (MTBE) 22 U UG/KG 1,2,4-Trichlorobenzene22 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene22 U UG/KG cis-1,2-Dichloroethene 45 % % Moisture22 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

22 U UG/KG Chloroform22 U UG/KG 1,1,1-Trichloroethane22 U UG/KG Cyclohexane22 U UG/KG Carbon Tetrachloride22 U UG/KG Benzene22 U UG/KG 1,2-Dichloroethane22 U UG/KG Trichloroethene (Trichloroethylene)22 U UG/KG Methylcyclohexane22 U UG/KG 1,2-Dichloropropane22 U UG/KG Bromodichloromethane22 U UG/KG cis-1,3-Dichloropropene22 U UG/KG Methyl Isobutyl Ketone22 U UG/KG Toluene22 U UG/KG trans-1,3-Dichloropropene22 U UG/KG 1,1,2-Trichloroethane22 U UG/KG Tetrachloroethene (Tetrachloroethylene)22 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9544 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 11:25

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AH6 D No: 3AH6 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSD04D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

16 U UG/KG Dichlorodifluoromethane 16 U UG/KG Dibromochloromethane16 U UG/KG Chloromethane 16 U UG/KG 1,2-Dibromoethane (EDB16 U UG/KG Vinyl Chloride 16 U UG/KG Chlorobenzene16 UJ UG/KG Bromomethane 16 U UG/KG Ethyl Benzene16 U UG/KG Chloroethane 16 U UG/KG Total Xylenes16 U UG/KG Trichlorofluoromethane (Freon 11) 16 U UG/KG Styrene16 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 16 U UG/KG Bromoform16 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 16 U UG/KG Isopropylbenzene16 UJ UG/KG Acetone 16 U UG/KG 1,1,2,2-Tetrachloroethan16 U UG/KG Carbon Disulfide 16 U UG/KG 1,3-Dichlorobenzene16 U UG/KG Methyl Acetate 16 U UG/KG 1,4-Dichlorobenzene16 UJ UG/KG Methylene Chloride 16 U UG/KG 1,2-Dichlorobenzene16 U UG/KG trans-1,2-Dichloroethene 16 U UG/KG 1,2-Dibromo-3-Chloropro16 U UG/KG Methyl T-Butyl Ether (MTBE) 16 U UG/KG 1,2,4-Trichlorobenzene16 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene16 U UG/KG cis-1,2-Dichloroethene 32 % % Moisture16 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

16 U UG/KG Chloroform16 U UG/KG 1,1,1-Trichloroethane16 U UG/KG Cyclohexane16 U UG/KG Carbon Tetrachloride16 U UG/KG Benzene16 U UG/KG 1,2-Dichloroethane16 U UG/KG Trichloroethene (Trichloroethylene)16 U UG/KG Methylcyclohexane16 U UG/KG 1,2-Dichloropropane16 U UG/KG Bromodichloromethane16 U UG/KG cis-1,3-Dichloropropene16 U UG/KG Methyl Isobutyl Ketone16 U UG/KG Toluene16 U UG/KG trans-1,3-Dichloropropene16 U UG/KG 1,1,2-Trichloroethane16 U UG/KG Tetrachloroethene (Tetrachloroethylene)16 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9545 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 11:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AH7 D No: 3AH7 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF ERSD05 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

21 U UG/KG Dichlorodifluoromethane 21 U UG/KG Dibromochloromethane21 U UG/KG Chloromethane 21 U UG/KG 1,2-Dibromoethane (EDB21 U UG/KG Vinyl Chloride 21 U UG/KG Chlorobenzene21 UJ UG/KG Bromomethane 21 U UG/KG Ethyl Benzene21 U UG/KG Chloroethane 21 U UG/KG Total Xylenes21 U UG/KG Trichlorofluoromethane (Freon 11) 21 U UG/KG Styrene21 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 21 U UG/KG Bromoform21 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 21 U UG/KG Isopropylbenzene21 UJ UG/KG Acetone 21 U UG/KG 1,1,2,2-Tetrachloroethan21 U UG/KG Carbon Disulfide 21 U UG/KG 1,3-Dichlorobenzene21 U UG/KG Methyl Acetate 21 U UG/KG 1,4-Dichlorobenzene21 UJ UG/KG Methylene Chloride 21 U UG/KG 1,2-Dichlorobenzene21 U UG/KG trans-1,2-Dichloroethene 21 U UG/KG 1,2-Dibromo-3-Chloropro21 U UG/KG Methyl T-Butyl Ether (MTBE) 21 U UG/KG 1,2,4-Trichlorobenzene21 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene21 U UG/KG cis-1,2-Dichloroethene 51 % % Moisture21 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

21 U UG/KG Chloroform21 U UG/KG 1,1,1-Trichloroethane21 U UG/KG Cyclohexane21 U UG/KG Carbon Tetrachloride21 U UG/KG Benzene21 U UG/KG 1,2-Dichloroethane21 U UG/KG Trichloroethene (Trichloroethylene)21 U UG/KG Methylcyclohexane21 U UG/KG 1,2-Dichloropropane21 U UG/KG Bromodichloromethane21 U UG/KG cis-1,3-Dichloropropene21 U UG/KG Methyl Isobutyl Ketone21 U UG/KG Toluene21 U UG/KG trans-1,3-Dichloropropene21 U UG/KG 1,1,2-Trichloroethane21 U UG/KG Tetrachloroethene (Tetrachloroethylene)21 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9546 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 10:10

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AH8 D No: 3AH8 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSD01 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

34 U UG/KG Dichlorodifluoromethane 34 U UG/KG Dibromochloromethane34 U UG/KG Chloromethane 34 U UG/KG 1,2-Dibromoethane (EDB34 U UG/KG Vinyl Chloride 34 U UG/KG Chlorobenzene34 UJ UG/KG Bromomethane 34 U UG/KG Ethyl Benzene34 U UG/KG Chloroethane 34 U UG/KG Total Xylenes34 U UG/KG Trichlorofluoromethane (Freon 11) 34 U UG/KG Styrene34 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 34 U UG/KG Bromoform34 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 34 U UG/KG Isopropylbenzene34 UJ UG/KG Acetone 34 U UG/KG 1,1,2,2-Tetrachloroethan34 U UG/KG Carbon Disulfide 34 U UG/KG 1,3-Dichlorobenzene34 U UG/KG Methyl Acetate 34 U UG/KG 1,4-Dichlorobenzene34 UJ UG/KG Methylene Chloride 34 U UG/KG 1,2-Dichlorobenzene34 U UG/KG trans-1,2-Dichloroethene 34 U UG/KG 1,2-Dibromo-3-Chloropro34 U UG/KG Methyl T-Butyl Ether (MTBE) 34 U UG/KG 1,2,4-Trichlorobenzene34 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene34 U UG/KG cis-1,2-Dichloroethene 56 % % Moisture34 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

34 U UG/KG Chloroform34 U UG/KG 1,1,1-Trichloroethane34 U UG/KG Cyclohexane34 U UG/KG Carbon Tetrachloride34 U UG/KG Benzene34 U UG/KG 1,2-Dichloroethane34 U UG/KG Trichloroethene (Trichloroethylene)34 U UG/KG Methylcyclohexane34 U UG/KG 1,2-Dichloropropane34 U UG/KG Bromodichloromethane34 U UG/KG cis-1,3-Dichloropropene34 U UG/KG Methyl Isobutyl Ketone34 U UG/KG Toluene34 U UG/KG trans-1,3-Dichloropropene34 U UG/KG 1,1,2-Trichloroethane34 U UG/KG Tetrachloroethene (Tetrachloroethylene)34 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9547 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 11:05

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AH9 D No: 3AH9 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSD01D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

38 U UG/KG Dichlorodifluoromethane 38 U UG/KG Dibromochloromethane38 UJ UG/KG Chloromethane 38 U UG/KG 1,2-Dibromoethane (EDB38 U UG/KG Vinyl Chloride 38 U UG/KG Chlorobenzene38 U UG/KG Bromomethane 38 U UG/KG Ethyl Benzene38 UJ UG/KG Chloroethane 38 U UG/KG Total Xylenes38 U UG/KG Trichlorofluoromethane (Freon 11) 38 U UG/KG Styrene38 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 38 U UG/KG Bromoform38 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 38 U UG/KG Isopropylbenzene50 J UG/KG Acetone 38 U UG/KG 1,1,2,2-Tetrachloroethan38 U UG/KG Carbon Disulfide 38 U UG/KG 1,3-Dichlorobenzene38 U UG/KG Methyl Acetate 38 U UG/KG 1,4-Dichlorobenzene38 U UG/KG Methylene Chloride 38 U UG/KG 1,2-Dichlorobenzene38 U UG/KG trans-1,2-Dichloroethene 38 U UG/KG 1,2-Dibromo-3-Chloropro38 U UG/KG Methyl T-Butyl Ether (MTBE) 38 U UG/KG 1,2,4-Trichlorobenzene38 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene38 U UG/KG cis-1,2-Dichloroethene 55 % % Moisture38 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

38 U UG/KG Chloroform38 U UG/KG 1,1,1-Trichloroethane38 U UG/KG Cyclohexane38 U UG/KG Carbon Tetrachloride38 U UG/KG Benzene38 U UG/KG 1,2-Dichloroethane38 U UG/KG Trichloroethene (Trichloroethylene)38 U UG/KG Methylcyclohexane38 U UG/KG 1,2-Dichloropropane38 U UG/KG Bromodichloromethane38 U UG/KG cis-1,3-Dichloropropene38 U UG/KG Methyl Isobutyl Ketone38 U UG/KG Toluene38 U UG/KG trans-1,3-Dichloropropene38 U UG/KG 1,1,2-Trichloroethane38 U UG/KG Tetrachloroethene (Tetrachloroethylene)38 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9547 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 11:05

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AH9 D No: 3AH9 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSD01D / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

36 NJ UG/KG BENZENE, 1-METHYL-3-(1-METHYLETHYL)-

N UG/KG PETROLEUM PRODUCT

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9548 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 12:00

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AJ0 D No: 3AJ0 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSD02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

66 UJ UG/KG Dichlorodifluoromethane 66 U UG/KG Dibromochloromethane66 UJ UG/KG Chloromethane 66 U UG/KG 1,2-Dibromoethane (EDB66 UJ UG/KG Vinyl Chloride 66 U UG/KG Chlorobenzene66 UJ UG/KG Bromomethane 230 J UG/KG Ethyl Benzene66 UJ UG/KG Chloroethane 760 J UG/KG Total Xylenes66 UJ UG/KG Trichlorofluoromethane (Freon 11) 66 U UG/KG Styrene66 UJ UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 66 U UG/KG Bromoform66 UJ UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 140 J UG/KG Isopropylbenzene68 J UG/KG Acetone 66 U UG/KG 1,1,2,2-Tetrachloroethan66 UJ UG/KG Carbon Disulfide 66 U UG/KG 1,3-Dichlorobenzene66 UJ UG/KG Methyl Acetate 66 U UG/KG 1,4-Dichlorobenzene66 UJ UG/KG Methylene Chloride 66 U UG/KG 1,2-Dichlorobenzene66 UJ UG/KG trans-1,2-Dichloroethene 66 U UG/KG 1,2-Dibromo-3-Chloropro66 UJ UG/KG Methyl T-Butyl Ether (MTBE) 66 U UG/KG 1,2,4-Trichlorobenzene66 UJ UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene66 UJ UG/KG cis-1,2-Dichloroethene 24 % % Moisture66 UJ UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

66 UJ UG/KG Chloroform66 U UG/KG 1,1,1-Trichloroethane66 U UG/KG Cyclohexane66 U UG/KG Carbon Tetrachloride24 J UG/KG Benzene66 UJ UG/KG 1,2-Dichloroethane66 U UG/KG Trichloroethene (Trichloroethylene)

140 J UG/KG Methylcyclohexane

66 UJ UG/KG 1,2-Dichloropropane66 UJ UG/KG Bromodichloromethane66 UJ UG/KG cis-1,3-Dichloropropene66 U UG/KG Methyl Isobutyl Ketone23 J UG/KG Toluene66 U UG/KG trans-1,3-Dichloropropene66 U UG/KG 1,1,2-Trichloroethane66 U UG/KG Tetrachloroethene (Tetrachloroethylene)66 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9548 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 12:00

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ0 D No: 3AJ0 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSD02 / 

_________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

22000 NJ UG/KG 6 SUBSTITUTED BENZENES37000 J UG/KG 12 UNKNOWNS

3300 NJ UG/KG BENZENE, 1-ETHYL-2,3-DIMETHYL3200 NJ UG/KG BENZENE, 1-METHYL-2-(1-METHYLETHYL)-2700 NJ UG/KG BENZENE, 1,4-DIETHYL2000 NJ UG/KG 1H-INDENE, 2,3-DIHYDRO-4,7-DIMETHYL2900 NJ UG/KG BENZENE, 1-ETHYL-2,4,5-TRIMETHYL4900 NJ UG/KG 1H-INDENE, 2,3-DIHYDRO-1,2-DIMETHYL2200 NJ UG/KG 1H-INDENE, 2,3-DIHYDRO-1,1-DIMETHYL2000 NJ UG/KG NAPHTHALENE, 1,2,3,4-TETRAHYDRO-5-METHYL2100 NJ UG/KG 1H-INDENE, 2,3-DIHYDRO-1,1,5-TRIMETHYL4000 NJ UG/KG BENZOCYCLOHEPTATRIENE3200 NJ UG/KG NAPHTHALENE, 1-METHYL2000 NJ UG/KG BENZENE, 1,3,5-TRIMETHYL-2-(1-METHYLETHYL)-

N UG/KG PETROLEUM PRODUCT

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9549 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 13:20

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AJ1 D No: 3AJ1 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSF05 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

12 U UG/KG Dichlorodifluoromethane 12 U UG/KG Dibromochloromethane12 UJ UG/KG Chloromethane 12 U UG/KG 1,2-Dibromoethane (EDB12 U UG/KG Vinyl Chloride 12 U UG/KG Chlorobenzene12 U UG/KG Bromomethane 12 U UG/KG Ethyl Benzene12 UJ UG/KG Chloroethane 12 U UG/KG Total Xylenes12 U UG/KG Trichlorofluoromethane (Freon 11) 12 U UG/KG Styrene12 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 12 U UG/KG Bromoform12 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 12 U UG/KG Isopropylbenzene95 J UG/KG Acetone 12 U UG/KG 1,1,2,2-Tetrachloroethan12 U UG/KG Carbon Disulfide 12 U UG/KG 1,3-Dichlorobenzene12 U UG/KG Methyl Acetate 12 U UG/KG 1,4-Dichlorobenzene12 U UG/KG Methylene Chloride 12 U UG/KG 1,2-Dichlorobenzene12 U UG/KG trans-1,2-Dichloroethene 12 U UG/KG 1,2-Dibromo-3-Chloropro12 U UG/KG Methyl T-Butyl Ether (MTBE) 12 U UG/KG 1,2,4-Trichlorobenzene12 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene12 U UG/KG cis-1,2-Dichloroethene 10 % % Moisture12 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

12 U UG/KG Chloroform12 U UG/KG 1,1,1-Trichloroethane12 U UG/KG Cyclohexane12 U UG/KG Carbon Tetrachloride12 U UG/KG Benzene12 U UG/KG 1,2-Dichloroethane12 U UG/KG Trichloroethene (Trichloroethylene)12 U UG/KG Methylcyclohexane12 U UG/KG 1,2-Dichloropropane12 U UG/KG Bromodichloromethane12 U UG/KG cis-1,3-Dichloropropene12 U UG/KG Methyl Isobutyl Ketone12 U UG/KG Toluene12 U UG/KG trans-1,3-Dichloropropene12 U UG/KG 1,1,2-Trichloroethane12 U UG/KG Tetrachloroethene (Tetrachloroethylene)12 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9550 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 13:45

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AJ2 D No: 3AJ2 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSF04 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

11 U UG/KG Dichlorodifluoromethane 11 U UG/KG Dibromochloromethane11 UJ UG/KG Chloromethane 11 U UG/KG 1,2-Dibromoethane (EDB11 U UG/KG Vinyl Chloride 11 U UG/KG Chlorobenzene11 U UG/KG Bromomethane 11 U UG/KG Ethyl Benzene11 UJ UG/KG Chloroethane 11 U UG/KG Total Xylenes11 U UG/KG Trichlorofluoromethane (Freon 11) 11 U UG/KG Styrene11 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 11 U UG/KG Bromoform11 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 11 U UG/KG Isopropylbenzene53 J UG/KG Acetone 11 U UG/KG 1,1,2,2-Tetrachloroethan11 U UG/KG Carbon Disulfide 11 U UG/KG 1,3-Dichlorobenzene11 U UG/KG Methyl Acetate 11 U UG/KG 1,4-Dichlorobenzene11 U UG/KG Methylene Chloride 11 U UG/KG 1,2-Dichlorobenzene11 U UG/KG trans-1,2-Dichloroethene 11 U UG/KG 1,2-Dibromo-3-Chloropro11 U UG/KG Methyl T-Butyl Ether (MTBE) 11 U UG/KG 1,2,4-Trichlorobenzene11 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene11 U UG/KG cis-1,2-Dichloroethene 12 % % Moisture11 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

11 U UG/KG Chloroform11 U UG/KG 1,1,1-Trichloroethane11 U UG/KG Cyclohexane11 U UG/KG Carbon Tetrachloride11 U UG/KG Benzene11 U UG/KG 1,2-Dichloroethane11 U UG/KG Trichloroethene (Trichloroethylene)11 U UG/KG Methylcyclohexane11 U UG/KG 1,2-Dichloropropane11 U UG/KG Bromodichloromethane11 U UG/KG cis-1,3-Dichloropropene11 U UG/KG Methyl Isobutyl Ketone11 U UG/KG Toluene11 U UG/KG trans-1,3-Dichloropropene11 U UG/KG 1,1,2-Trichloroethane11 U UG/KG Tetrachloroethene (Tetrachloroethylene)11 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9551 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 14:05

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717MD No: 3AJ3 D No: 3AJ3 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSF03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

12 U UG/KG Dichlorodifluoromethane 12 U UG/KG Dibromochloromethane12 U UG/KG Chloromethane 12 U UG/KG 1,2-Dibromoethane (EDB12 U UG/KG Vinyl Chloride 12 U UG/KG Chlorobenzene12 UJ UG/KG Bromomethane 12 U UG/KG Ethyl Benzene12 U UG/KG Chloroethane 12 U UG/KG Total Xylenes12 U UG/KG Trichlorofluoromethane (Freon 11) 12 U UG/KG Styrene12 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 12 U UG/KG Bromoform12 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 12 U UG/KG Isopropylbenzene12 UJ UG/KG Acetone 12 U UG/KG 1,1,2,2-Tetrachloroethan12 U UG/KG Carbon Disulfide 12 U UG/KG 1,3-Dichlorobenzene12 U UG/KG Methyl Acetate 12 U UG/KG 1,4-Dichlorobenzene12 UJ UG/KG Methylene Chloride 12 U UG/KG 1,2-Dichlorobenzene12 U UG/KG trans-1,2-Dichloroethene 12 U UG/KG 1,2-Dibromo-3-Chloropro12 U UG/KG Methyl T-Butyl Ether (MTBE) 12 U UG/KG 1,2,4-Trichlorobenzene12 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene12 U UG/KG cis-1,2-Dichloroethene 14 % % Moisture12 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

12 U UG/KG Chloroform12 U UG/KG 1,1,1-Trichloroethane12 U UG/KG Cyclohexane12 U UG/KG Carbon Tetrachloride12 U UG/KG Benzene12 U UG/KG 1,2-Dichloroethane12 U UG/KG Trichloroethene (Trichloroethylene)12 U UG/KG Methylcyclohexane12 U UG/KG 1,2-Dichloropropane12 U UG/KG Bromodichloromethane12 U UG/KG cis-1,3-Dichloropropene12 U UG/KG Methyl Isobutyl Ketone12 U UG/KG Toluene12 U UG/KG trans-1,3-Dichloropropene12 U UG/KG 1,1,2-Trichloroethane12 U UG/KG Tetrachloroethene (Tetrachloroethylene)12 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9551 2005 05-0928 Produced by: Appleby, Charlie 

MISCELLANEOUS COMPOUNDS Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 14:05

Inorg Contractor: LIBRTY 

Ending: 

Org Contractor: LIBRTY 

Case No: 34717MD No: 3AJ3 D No: 3AJ3 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF DUSF03 / 

_________________________________________________________________________________________________________________________________________________________________________________

SURFACE SOIL 

6 J UG/KG UNKNOWN

N UG/KG PETROLEUM PRODUCT

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Data Reported as Identified by CLP Lab - IDs Not VerifiedR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9552 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 14:26Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717D No: 3AK3 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF TB903 / 

_________________________________________________________________________________________________________________________________________________________________________________

TRIP BLANK - SOIL 

12 U UG/KG Dichlorodifluoromethane 12 U UG/KG Dibromochloromethane12 U UG/KG Chloromethane 12 U UG/KG 1,2-Dibromoethane (EDB12 U UG/KG Vinyl Chloride 12 U UG/KG Chlorobenzene12 U UG/KG Bromomethane 12 U UG/KG Ethyl Benzene12 UJ UG/KG Chloroethane 12 U UG/KG Total Xylenes12 U UG/KG Trichlorofluoromethane (Freon 11) 12 U UG/KG Styrene12 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 12 U UG/KG Bromoform12 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 12 U UG/KG Isopropylbenzene17 UG/KG Acetone 12 U UG/KG 1,1,2,2-Tetrachloroethan12 U UG/KG Carbon Disulfide 12 U UG/KG 1,3-Dichlorobenzene12 U UG/KG Methyl Acetate 12 U UG/KG 1,4-Dichlorobenzene12 U UG/KG Methylene Chloride 12 U UG/KG 1,2-Dichlorobenzene12 U UG/KG trans-1,2-Dichloroethene 12 U UG/KG 1,2-Dibromo-3-Chloropro12 U UG/KG Methyl T-Butyl Ether (MTBE) 12 U UG/KG 1,2,4-Trichlorobenzene12 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene12 U UG/KG cis-1,2-Dichloroethene 0 % % Moisture12 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

12 U UG/KG Chloroform12 U UG/KG 1,1,1-Trichloroethane12 U UG/KG Cyclohexane12 U UG/KG Carbon Tetrachloride12 U UG/KG Benzene12 U UG/KG 1,2-Dichloroethane12 U UG/KG Trichloroethene (Trichloroethylene)12 U UG/KG Methylcyclohexane12 U UG/KG 1,2-Dichloropropane12 U UG/KG Bromodichloromethane12 U UG/KG cis-1,3-Dichloropropene12 U UG/KG Methyl Isobutyl Ketone12 U UG/KG Toluene12 U UG/KG trans-1,3-Dichloropropene12 U UG/KG 1,1,2-Trichloroethane12 U UG/KG Tetrachloroethene (Tetrachloroethylene)12 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9553 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/06/2005 14:27Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717D No: 3AK4 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF TB904 / 

_________________________________________________________________________________________________________________________________________________________________________________

TRIP BLANK - SOIL 

13 U UG/KG Dichlorodifluoromethane 13 U UG/KG Dibromochloromethane13 U UG/KG Chloromethane 13 U UG/KG 1,2-Dibromoethane (EDB13 U UG/KG Vinyl Chloride 13 U UG/KG Chlorobenzene13 U UG/KG Bromomethane 13 U UG/KG Ethyl Benzene13 UJ UG/KG Chloroethane 13 U UG/KG Total Xylenes13 U UG/KG Trichlorofluoromethane (Freon 11) 13 U UG/KG Styrene13 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 13 U UG/KG Bromoform13 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 13 U UG/KG Isopropylbenzene14 UG/KG Acetone 13 U UG/KG 1,1,2,2-Tetrachloroethan13 U UG/KG Carbon Disulfide 13 U UG/KG 1,3-Dichlorobenzene13 U UG/KG Methyl Acetate 13 U UG/KG 1,4-Dichlorobenzene13 U UG/KG Methylene Chloride 13 U UG/KG 1,2-Dichlorobenzene13 U UG/KG trans-1,2-Dichloroethene 13 U UG/KG 1,2-Dibromo-3-Chloropro13 U UG/KG Methyl T-Butyl Ether (MTBE) 13 U UG/KG 1,2,4-Trichlorobenzene13 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene13 U UG/KG cis-1,2-Dichloroethene 0 % % Moisture13 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

13 U UG/KG Chloroform13 U UG/KG 1,1,1-Trichloroethane13 U UG/KG Cyclohexane13 U UG/KG Carbon Tetrachloride13 U UG/KG Benzene13 U UG/KG 1,2-Dichloroethane13 U UG/KG Trichloroethene (Trichloroethylene)13 U UG/KG Methylcyclohexane13 U UG/KG 1,2-Dichloropropane13 U UG/KG Bromodichloromethane13 U UG/KG cis-1,3-Dichloropropene13 U UG/KG Methyl Isobutyl Ketone13 U UG/KG Toluene13 U UG/KG trans-1,3-Dichloropropene13 U UG/KG 1,1,2-Trichloroethane13 U UG/KG Tetrachloroethene (Tetrachloroethylene)13 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9554 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/03/2005 15:21Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717D No: 3AF8 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF POTB901 / 

_________________________________________________________________________________________________________________________________________________________________________________

TRIP BLANK - SOIL 

11 U UG/KG Dichlorodifluoromethane 11 U UG/KG Dibromochloromethane11 U UG/KG Chloromethane 11 U UG/KG 1,2-Dibromoethane (EDB11 U UG/KG Vinyl Chloride 11 U UG/KG Chlorobenzene11 U UG/KG Bromomethane 11 U UG/KG Ethyl Benzene11 UJ UG/KG Chloroethane 11 U UG/KG Total Xylenes11 U UG/KG Trichlorofluoromethane (Freon 11) 11 U UG/KG Styrene11 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 11 U UG/KG Bromoform11 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 11 U UG/KG Isopropylbenzene11 UG/KG Acetone 11 U UG/KG 1,1,2,2-Tetrachloroethan11 U UG/KG Carbon Disulfide 11 U UG/KG 1,3-Dichlorobenzene11 U UG/KG Methyl Acetate 11 U UG/KG 1,4-Dichlorobenzene11 U UG/KG Methylene Chloride 11 U UG/KG 1,2-Dichlorobenzene11 U UG/KG trans-1,2-Dichloroethene 11 U UG/KG 1,2-Dibromo-3-Chloropro11 U UG/KG Methyl T-Butyl Ether (MTBE) 11 U UG/KG 1,2,4-Trichlorobenzene11 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene11 U UG/KG cis-1,2-Dichloroethene 0 % % Moisture11 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

11 U UG/KG Chloroform11 U UG/KG 1,1,1-Trichloroethane11 U UG/KG Cyclohexane11 U UG/KG Carbon Tetrachloride11 U UG/KG Benzene11 U UG/KG 1,2-Dichloroethane11 U UG/KG Trichloroethene (Trichloroethylene)11 U UG/KG Methylcyclohexane11 U UG/KG 1,2-Dichloropropane11 U UG/KG Bromodichloromethane11 U UG/KG cis-1,3-Dichloropropene11 U UG/KG Methyl Isobutyl Ketone11 U UG/KG Toluene11 U UG/KG trans-1,3-Dichloropropene11 U UG/KG 1,1,2-Trichloroethane11 U UG/KG Tetrachloroethene (Tetrachloroethylene)11 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WE

______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9555 2005 05-0928 Produced by: Appleby, Charlie 

Volatiles Scan Requestor: Project Leader: FSLOAN

Beginning: 10/04/2005 12:29Ending: 

Org Contractor: LIBRTY 

 RESULTS UNITS ANALYTE

Case No: 34717D No: 3AG6 

 RESULTS UNITS ANALYTE

Hurricane Katrina Response 

SF TB902 / 

_________________________________________________________________________________________________________________________________________________________________________________

TRIP BLANK - SOIL 

14 U UG/KG Dichlorodifluoromethane 14 U UG/KG Dibromochloromethane14 U UG/KG Chloromethane 14 U UG/KG 1,2-Dibromoethane (EDB14 U UG/KG Vinyl Chloride 14 U UG/KG Chlorobenzene14 UJ UG/KG Bromomethane 14 U UG/KG Ethyl Benzene14 U UG/KG Chloroethane 14 U UG/KG Total Xylenes14 U UG/KG Trichlorofluoromethane (Freon 11) 14 U UG/KG Styrene14 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 14 U UG/KG Bromoform14 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 14 U UG/KG Isopropylbenzene14 UJ UG/KG Acetone 14 U UG/KG 1,1,2,2-Tetrachloroethan14 U UG/KG Carbon Disulfide 14 U UG/KG 1,3-Dichlorobenzene14 U UG/KG Methyl Acetate 14 U UG/KG 1,4-Dichlorobenzene14 UJ UG/KG Methylene Chloride 14 U UG/KG 1,2-Dichlorobenzene14 U UG/KG trans-1,2-Dichloroethene 14 U UG/KG 1,2-Dibromo-3-Chloropro14 U UG/KG Methyl T-Butyl Ether (MTBE) 14 U UG/KG 1,2,4-Trichlorobenzene14 U UG/KG 1,1-Dichloroethane NA UG/KG 1,2,3-Trichlorobenzene14 U UG/KG cis-1,2-Dichloroethene 0 % % Moisture14 U UG/KG Methyl Ethyl Ketone

NA UG/KG Bromochloromethane

14 U UG/KG Chloroform14 U UG/KG 1,1,1-Trichloroethane14 U UG/KG Cyclohexane14 U UG/KG Carbon Tetrachloride14 U UG/KG Benzene14 U UG/KG 1,2-Dichloroethane14 U UG/KG Trichloroethene (Trichloroethylene)14 U UG/KG Methylcyclohexane14 U UG/KG 1,2-Dichloropropane14 U UG/KG Bromodichloromethane14 U UG/KG cis-1,3-Dichloropropene14 U UG/KG Methyl Isobutyl Ketone14 U UG/KG Toluene14 U UG/KG trans-1,3-Dichloropropene14 U UG/KG 1,1,2-Trichloroethane14 U UG/KG Tetrachloroethene (Tetrachloroethylene)14 U UG/KG Methyl Butyl Ketone

_________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative ideK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repo
DATA REPORTED ON DRY WEI

_______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9397 2005 05-0926 Produced by: Muse, Janet 

Extractables Scan Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/27/2005 11:30Ending: 

 RESULTS UNITS ANALYTE RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU BC2SD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

900 U UG/KG bis(2-Chloroethyl) Ether 900 U UG/KG Anthracene900 UJ UG/KG Benzaldehyde 900 U UG/KG Carbazole900 U UG/KG Hexachloroethane 900 U UG/KG Di-n-Butylphthalate900 U UG/KG bis(2-Chloroisopropyl) Ether 900 U UG/KG Fluoranthene900 U UG/KG n-Nitroso di-n-Propylamine 900 U UG/KG Pyrene900 U UG/KG Acetophenone 900 U UG/KG Benzyl Butyl Phthalate900 U UG/KG Nitrobenzene 900 U UG/KG bis(2-Ethylhexyl) Phthala900 U UG/KG Hexachlorobutadiene 900 U UG/KG Benzo(a)Anthracene900 U UG/KG Caprolactam 900 U UG/KG Chrysene900 U UG/KG 2-Methylnaphthalene 900 U UG/KG 3,3'-Dichlorobenzidine900 U UG/KG 1,2,4-Trichlorobenzene 900 U UG/KG Di-n-Octylphthalate900 U UG/KG Naphthalene 900 U UG/KG Benzo(b)Fluoranthene900 U UG/KG 4-Chloroaniline 900 U UG/KG Benzo(k)Fluoranthene900 U UG/KG bis(2-Chloroethoxy)Methane 900 U UG/KG Benzo-a-Pyrene900 U UG/KG Isophorone 900 U UG/KG Indeno (1,2,3-cd) Pyrene900 U UG/KG Hexachlorocyclopentadiene (HCCP) 900 U UG/KG Dibenzo(a,h)Anthracene900 U UG/KG 1,1-Biphenyl 900 U UG/KG Benzo(ghi)Perylene900 U UG/KG 2-Chloronaphthalene 900 U UG/KG 2-Chlorophenol900 U UG/KG 2-Nitroaniline 900 U UG/KG 2-Methylphenol900 U UG/KG Acenaphthylene 900 U UG/KG (3-and/or 4-)Methylpheno900 U UG/KG Acenaphthene 900 U UG/KG 2-Nitrophenol900 U UG/KG Dimethyl Phthalate 900 U UG/KG Phenol900 U UG/KG Dibenzofuran 900 U UG/KG 2,4-Dimethylphenol900 U UG/KG 2,4-Dinitrotoluene 900 U UG/KG 2,4-Dichlorophenol900 U UG/KG 2,6-Dinitrotoluene 900 U UG/KG 2,4,6-Trichlorophenol900 U UG/KG 3-Nitroaniline 900 U UG/KG 2,4,5-Trichlorophenol900 U UG/KG 4-Chlorophenyl Phenyl Ether 900 U UG/KG 4-Chloro-3-Methylphenol900 U UG/KG 4-Nitroaniline 1800 UJ UG/KG 2,4-Dinitrophenol900 U UG/KG Fluorene 1800 U UG/KG 2-Methyl-4,6-Dinitrophen900 U UG/KG Diethyl Phthalate 1800 U UG/KG Pentachlorophenol900 U UG/KG n-Nitrosodiphenylamine/Diphenylamine 1800 U UG/KG 4-Nitrophenol900 U UG/KG Hexachlorobenzene (HCB) 900 U UG/KG 2,3,4,6-Tetrachloropheno900 U UG/KG Atrazine 63.61 % % Moisture900 U UG/KG 4-Bromophenyl Phenyl Ether900 U UG/KG Phenanthrene

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

J- due to RSD >20% on ICAL for BenzaldehydeJ-qualified due to QC Limits Exceeded for 2,4-DinitrophenolR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
DATA REPORTED ON DRY WEI

_______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9400 2005 05-0926 Produced by: Muse, Janet 

Extractables Scan Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/27/2005 13:00Ending: 

 RESULTS UNITS ANALYTE RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU BC4DSD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

460 U UG/KG bis(2-Chloroethyl) Ether 460 U UG/KG Anthracene460 UJ UG/KG Benzaldehyde 460 U UG/KG Carbazole460 U UG/KG Hexachloroethane 460 U UG/KG Di-n-Butylphthalate460 U UG/KG bis(2-Chloroisopropyl) Ether 66 J UG/KG Fluoranthene460 U UG/KG n-Nitroso di-n-Propylamine 63 J UG/KG Pyrene460 U UG/KG Acetophenone 460 U UG/KG Benzyl Butyl Phthalate460 U UG/KG Nitrobenzene 460 U UG/KG bis(2-Ethylhexyl) Phthala460 U UG/KG Hexachlorobutadiene 460 U UG/KG Benzo(a)Anthracene460 U UG/KG Caprolactam 460 U UG/KG Chrysene460 U UG/KG 2-Methylnaphthalene 460 U UG/KG 3,3'-Dichlorobenzidine460 U UG/KG 1,2,4-Trichlorobenzene 460 U UG/KG Di-n-Octylphthalate460 U UG/KG Naphthalene 460 U UG/KG Benzo(b)Fluoranthene460 U UG/KG 4-Chloroaniline 460 U UG/KG Benzo(k)Fluoranthene460 U UG/KG bis(2-Chloroethoxy)Methane 460 U UG/KG Benzo-a-Pyrene460 U UG/KG Isophorone 460 U UG/KG Indeno (1,2,3-cd) Pyrene460 U UG/KG Hexachlorocyclopentadiene (HCCP) 460 U UG/KG Dibenzo(a,h)Anthracene460 U UG/KG 1,1-Biphenyl 460 U UG/KG Benzo(ghi)Perylene460 U UG/KG 2-Chloronaphthalene 460 U UG/KG 2-Chlorophenol460 U UG/KG 2-Nitroaniline 460 U UG/KG 2-Methylphenol460 U UG/KG Acenaphthylene 460 U UG/KG (3-and/or 4-)Methylpheno460 U UG/KG Acenaphthene 460 U UG/KG 2-Nitrophenol460 U UG/KG Dimethyl Phthalate 460 U UG/KG Phenol460 U UG/KG Dibenzofuran 460 U UG/KG 2,4-Dimethylphenol460 U UG/KG 2,4-Dinitrotoluene 460 U UG/KG 2,4-Dichlorophenol460 U UG/KG 2,6-Dinitrotoluene 460 U UG/KG 2,4,6-Trichlorophenol460 U UG/KG 3-Nitroaniline 460 U UG/KG 2,4,5-Trichlorophenol460 U UG/KG 4-Chlorophenyl Phenyl Ether 460 U UG/KG 4-Chloro-3-Methylphenol460 U UG/KG 4-Nitroaniline 930 UJ UG/KG 2,4-Dinitrophenol460 U UG/KG Fluorene 930 U UG/KG 2-Methyl-4,6-Dinitrophen460 U UG/KG Diethyl Phthalate 930 U UG/KG Pentachlorophenol460 U UG/KG n-Nitrosodiphenylamine/Diphenylamine 930 U UG/KG 4-Nitrophenol460 U UG/KG Hexachlorobenzene (HCB) 460 U UG/KG 2,3,4,6-Tetrachloropheno460 U UG/KG Atrazine 29.58 % % Moisture460 U UG/KG 4-Bromophenyl Phenyl Ether460 U UG/KG Phenanthrene

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

J- due to RSD >20% on ICAL for Benzaldehyde J-qualified due to QC Limits Exceeded for 2,4-DinitropJ-qualified: value <MQL for Fluoranthene and PyreneR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
DATA REPORTED ON DRY WEI

_______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9401 2005 05-0926 Produced by: Muse, Janet 

Extractables Scan Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/27/2005 12:40Ending: 

 RESULTS UNITS ANALYTE RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU BC4SD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

500 U UG/KG bis(2-Chloroethyl) Ether 500 U UG/KG Anthracene500 UJ UG/KG Benzaldehyde 500 U UG/KG Carbazole500 U UG/KG Hexachloroethane 500 U UG/KG Di-n-Butylphthalate500 U UG/KG bis(2-Chloroisopropyl) Ether 500 U UG/KG Fluoranthene500 U UG/KG n-Nitroso di-n-Propylamine 500 U UG/KG Pyrene500 U UG/KG Acetophenone 500 U UG/KG Benzyl Butyl Phthalate500 U UG/KG Nitrobenzene 500 U UG/KG bis(2-Ethylhexyl) Phthala500 U UG/KG Hexachlorobutadiene 500 U UG/KG Benzo(a)Anthracene500 U UG/KG Caprolactam 500 U UG/KG Chrysene500 U UG/KG 2-Methylnaphthalene 500 U UG/KG 3,3'-Dichlorobenzidine500 U UG/KG 1,2,4-Trichlorobenzene 500 U UG/KG Di-n-Octylphthalate500 U UG/KG Naphthalene 500 U UG/KG Benzo(b)Fluoranthene500 U UG/KG 4-Chloroaniline 500 U UG/KG Benzo(k)Fluoranthene500 U UG/KG bis(2-Chloroethoxy)Methane 500 U UG/KG Benzo-a-Pyrene500 U UG/KG Isophorone 500 U UG/KG Indeno (1,2,3-cd) Pyrene500 U UG/KG Hexachlorocyclopentadiene (HCCP) 500 U UG/KG Dibenzo(a,h)Anthracene500 U UG/KG 1,1-Biphenyl 500 U UG/KG Benzo(ghi)Perylene500 U UG/KG 2-Chloronaphthalene 500 U UG/KG 2-Chlorophenol500 U UG/KG 2-Nitroaniline 500 U UG/KG 2-Methylphenol500 U UG/KG Acenaphthylene 500 U UG/KG (3-and/or 4-)Methylpheno500 U UG/KG Acenaphthene 500 U UG/KG 2-Nitrophenol500 U UG/KG Dimethyl Phthalate 500 U UG/KG Phenol500 U UG/KG Dibenzofuran 500 U UG/KG 2,4-Dimethylphenol500 U UG/KG 2,4-Dinitrotoluene 500 U UG/KG 2,4-Dichlorophenol500 U UG/KG 2,6-Dinitrotoluene 500 U UG/KG 2,4,6-Trichlorophenol500 U UG/KG 3-Nitroaniline 500 U UG/KG 2,4,5-Trichlorophenol500 U UG/KG 4-Chlorophenyl Phenyl Ether 500 U UG/KG 4-Chloro-3-Methylphenol500 U UG/KG 4-Nitroaniline 990 UJ UG/KG 2,4-Dinitrophenol500 U UG/KG Fluorene 990 U UG/KG 2-Methyl-4,6-Dinitrophen500 U UG/KG Diethyl Phthalate 990 U UG/KG Pentachlorophenol500 U UG/KG n-Nitrosodiphenylamine/Diphenylamine 990 U UG/KG 4-Nitrophenol500 U UG/KG Hexachlorobenzene (HCB) 500 U UG/KG 2,3,4,6-Tetrachloropheno500 U UG/KG Atrazine 33.67 % % Moisture500 U UG/KG 4-Bromophenyl Phenyl Ether500 U UG/KG Phenanthrene

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

J- due to RSD >20% on ICAL for BenzaldehydeJ-qualified due to QC Limits Exceeded for 2,4-DinitrophenolR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
DATA REPORTED ON DRY WEI

_______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9443 2005 05-0926 Produced by: Revell, Dennis 

Extractables Scan Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/28/2005 14:30Ending: 

 RESULTS UNITS ANALYTE RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU ER1DSD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

400 U UG/KG bis(2-Chloroethyl) Ether 400 U UG/KG Anthracene400 U UG/KG Benzaldehyde 400 UJ UG/KG Carbazole400 U UG/KG Hexachloroethane 400 U UG/KG Di-n-Butylphthalate400 U UG/KG bis(2-Chloroisopropyl) Ether 400 U UG/KG Fluoranthene400 U UG/KG n-Nitroso di-n-Propylamine 400 U UG/KG Pyrene400 U UG/KG Acetophenone 400 U UG/KG Benzyl Butyl Phthalate400 U UG/KG Nitrobenzene 400 U UG/KG bis(2-Ethylhexyl) Phthala400 U UG/KG Hexachlorobutadiene 400 U UG/KG Benzo(a)Anthracene400 U UG/KG Caprolactam 400 U UG/KG Chrysene400 U UG/KG 2-Methylnaphthalene 400 U UG/KG 3,3'-Dichlorobenzidine400 U UG/KG 1,2,4-Trichlorobenzene 400 U UG/KG Di-n-Octylphthalate400 U UG/KG Naphthalene 400 U UG/KG Benzo(b)Fluoranthene400 U UG/KG 4-Chloroaniline 400 U UG/KG Benzo(k)Fluoranthene400 U UG/KG bis(2-Chloroethoxy)Methane 400 U UG/KG Benzo-a-Pyrene400 U UG/KG Isophorone 400 U UG/KG Indeno (1,2,3-cd) Pyrene400 U UG/KG Hexachlorocyclopentadiene (HCCP) 400 U UG/KG Dibenzo(a,h)Anthracene400 U UG/KG 1,1-Biphenyl 400 U UG/KG Benzo(ghi)Perylene400 U UG/KG 2-Chloronaphthalene 400 U UG/KG 2-Chlorophenol400 U UG/KG 2-Nitroaniline 400 U UG/KG 2-Methylphenol400 U UG/KG Acenaphthylene 400 U UG/KG (3-and/or 4-)Methylpheno400 U UG/KG Acenaphthene 400 U UG/KG 2-Nitrophenol400 UJ UG/KG Dimethyl Phthalate 400 U UG/KG Phenol400 U UG/KG Dibenzofuran 400 U UG/KG 2,4-Dimethylphenol400 U UG/KG 2,4-Dinitrotoluene 400 U UG/KG 2,4-Dichlorophenol400 U UG/KG 2,6-Dinitrotoluene 400 U UG/KG 2,4,6-Trichlorophenol400 U UG/KG 3-Nitroaniline 400 U UG/KG 2,4,5-Trichlorophenol400 U UG/KG 4-Chlorophenyl Phenyl Ether 400 U UG/KG 4-Chloro-3-Methylphenol400 U UG/KG 4-Nitroaniline 790 UJ UG/KG 2,4-Dinitrophenol400 U UG/KG Fluorene 790 U UG/KG 2-Methyl-4,6-Dinitrophen400 U UG/KG Diethyl Phthalate 790 U UG/KG Pentachlorophenol400 U UG/KG n-Nitrosodiphenylamine/Diphenylamine 790 U UG/KG 4-Nitrophenol400 U UG/KG Hexachlorobenzene (HCB) 400 U UG/KG 2,3,4,6-Tetrachloropheno400 UJ UG/KG Atrazine 20.62 % % Moisture400 U UG/KG 4-Bromophenyl Phenyl Ether400 U UG/KG Phenanthrene

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

J-qualified for low recovery in CCV for Dimethylphthalate, Atrazine, CarbazoleJ-qualified due to QC Limits Exceeded for 2,4-DinitrophenolR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
DATA REPORTED ON DRY WEI

_______________________________________________________________________________________________________________________

EXTRACTABLES SAMPLE ANALYSIS Production 

9445 2005 05-0926 Produced by: Revell, Dennis 

Extractables Scan Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/28/2005 14:00Ending: 

 RESULTS UNITS ANALYTE RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU ER1SD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

410 U UG/KG bis(2-Chloroethyl) Ether 410 U UG/KG Anthracene410 U UG/KG Benzaldehyde 410 UJ UG/KG Carbazole410 U UG/KG Hexachloroethane 410 U UG/KG Di-n-Butylphthalate410 U UG/KG bis(2-Chloroisopropyl) Ether 410 U UG/KG Fluoranthene410 U UG/KG n-Nitroso di-n-Propylamine 410 U UG/KG Pyrene410 U UG/KG Acetophenone 410 U UG/KG Benzyl Butyl Phthalate410 U UG/KG Nitrobenzene 410 U UG/KG bis(2-Ethylhexyl) Phthala410 U UG/KG Hexachlorobutadiene 410 U UG/KG Benzo(a)Anthracene410 U UG/KG Caprolactam 410 U UG/KG Chrysene410 U UG/KG 2-Methylnaphthalene 410 U UG/KG 3,3'-Dichlorobenzidine410 U UG/KG 1,2,4-Trichlorobenzene 410 U UG/KG Di-n-Octylphthalate410 U UG/KG Naphthalene 410 U UG/KG Benzo(b)Fluoranthene410 U UG/KG 4-Chloroaniline 410 U UG/KG Benzo(k)Fluoranthene410 U UG/KG bis(2-Chloroethoxy)Methane 410 U UG/KG Benzo-a-Pyrene410 U UG/KG Isophorone 410 U UG/KG Indeno (1,2,3-cd) Pyrene410 U UG/KG Hexachlorocyclopentadiene (HCCP) 410 U UG/KG Dibenzo(a,h)Anthracene410 U UG/KG 1,1-Biphenyl 410 U UG/KG Benzo(ghi)Perylene410 U UG/KG 2-Chloronaphthalene 410 U UG/KG 2-Chlorophenol410 U UG/KG 2-Nitroaniline 410 U UG/KG 2-Methylphenol410 U UG/KG Acenaphthylene 410 U UG/KG (3-and/or 4-)Methylpheno410 U UG/KG Acenaphthene 410 U UG/KG 2-Nitrophenol410 UJ UG/KG Dimethyl Phthalate 410 U UG/KG Phenol410 U UG/KG Dibenzofuran 410 U UG/KG 2,4-Dimethylphenol410 U UG/KG 2,4-Dinitrotoluene 410 U UG/KG 2,4-Dichlorophenol410 U UG/KG 2,6-Dinitrotoluene 410 U UG/KG 2,4,6-Trichlorophenol410 U UG/KG 3-Nitroaniline 410 U UG/KG 2,4,5-Trichlorophenol410 U UG/KG 4-Chlorophenyl Phenyl Ether 410 U UG/KG 4-Chloro-3-Methylphenol410 U UG/KG 4-Nitroaniline 820 UJ UG/KG 2,4-Dinitrophenol410 U UG/KG Fluorene 820 U UG/KG 2-Methyl-4,6-Dinitrophen410 U UG/KG Diethyl Phthalate 820 U UG/KG Pentachlorophenol410 U UG/KG n-Nitrosodiphenylamine/Diphenylamine 820 U UG/KG 4-Nitrophenol410 U UG/KG Hexachlorobenzene (HCB) 410 U UG/KG 2,3,4,6-Tetrachloropheno410 UJ UG/KG Atrazine 19.98 % % Moisture410 U UG/KG 4-Bromophenyl Phenyl Ether410 U UG/KG Phenanthrene

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

J-qualified for low recovery in CCV for Dimethylphthalate, Atrazine, CarbazoleJ-qualified due to QC Limits Exceeded for 2,4-DinitrophenolR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
DATA REPORTED ON DRY WEI

_______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9397 2005 05-0926 Produced by: Scifres, Jenny 

Metals Scan Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/27/2005 11:30Ending: 

 RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU BC2SD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

0.50 U MG/KG Silver

6.4 MG/KG Arsenic

130 MG/KG Barium

0.82 MG/KG Beryllium

1.1 MG/KG Cadmium4.6 MG/KG Cobalt

21 MG/KG Chromium20 MG/KG Copper

1.6 U MG/KG Molybdenum8.4 MG/KG Nickel

36 MG/KG Lead

0.50 U MG/KG Antimony

1.0 U MG/KG Selenium

NA MG/KG Tin

57 MG/KG Strontium17 MG/KG Titanium

0.50 U MG/KG Thallium

24 MG/KG Vanadium12 MG/KG Yttrium

140 MG/KG Zinc

0.078 MG/KG Total Mercury

8200 MG/KG Aluminum

450 MG/KG Manganese

7400 MG/KG Calcium5100 MG/KG Magnesium

17000 MG/KG Iron18000 MG/KG Sodium

2300 MG/KG Potassium

60 % % Moisture

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Per Cent Moisture Determined at 60 Degrees Celsius.R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
DATA REPORTED ON DRY WEI

_______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9400 2005 05-0926 Produced by: Scifres, Jenny 

Metals Scan Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/27/2005 13:00Ending: 

 RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU BC4DSD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

0.50 U MG/KG Silver

1.2 MG/KG Arsenic

27 MG/KG Barium

0.30 MG/KG Beryllium

1.5 MG/KG Cadmium

0.59 MG/KG Cobalt

7.2 MG/KG Chromium4.7 MG/KG Copper1.6 U MG/KG Molybdenum2.4 MG/KG Nickel4.8 MG/KG Lead

0.50 U MG/KG Antimony

1.0 U MG/KG Selenium

NA MG/KG Tin

59 MG/KG Strontium12 MG/KG Titanium

0.50 U MG/KG Thallium

6.1 MG/KG Vanadium2.7 MG/KG Yttrium

48 MG/KG Zinc

0.044 U MG/KG Total Mercury

2600 MG/KG Aluminum

26 MG/KG Manganese

4900 MG/KG Calcium1800 MG/KG Magnesium3400 MG/KG Iron8500 MG/KG Sodium

510 MG/KG Potassium

41 % % Moisture

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Per Cent Moisture Determined at 60 Degrees Celsius.R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
DATA REPORTED ON DRY WEI

_______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9401 2005 05-0926 Produced by: Scifres, Jenny 

Metals Scan Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/27/2005 12:40Ending: 

 RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU BC4SD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

0.50 U MG/KG Silver0.87 MG/KG Arsenic

57 MG/KG Barium

0.30 MG/KG Beryllium

1.8 MG/KG Cadmium

0.66 MG/KG Cobalt

9.7 MG/KG Chromium5.5 MG/KG Copper1.6 U MG/KG Molybdenum2.7 MG/KG Nickel5.9 MG/KG Lead

0.50 U MG/KG Antimony

1.0 U MG/KG Selenium

NA MG/KG Tin

66 MG/KG Strontium14 MG/KG Titanium

0.50 U MG/KG Thallium

7.3 MG/KG Vanadium2.5 MG/KG Yttrium

55 MG/KG Zinc

0.044 U MG/KG Total Mercury

3000 MG/KG Aluminum

26 MG/KG Manganese

4700 MG/KG Calcium1700 MG/KG Magnesium3200 MG/KG Iron5900 MG/KG Sodium

450 MG/KG Potassium

49 A % % Moisture

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Per Cent Moisture Determined at 60 Degrees Celsius.R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
DATA REPORTED ON DRY WEI

_______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9443 2005 05-0926 Produced by: Scifres, Jenny 

Metals Scan Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/28/2005 14:30Ending: 

 RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU ER1DSD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

0.50 U MG/KG Silver0.25 U MG/KG Arsenic

1.7 A MG/KG Barium

0.30 U MG/KG Beryllium0.12 U MG/KG Cadmium0.50 U MG/KG Cobalt0.50 U MG/KG Chromium

2.0 UJ MG/KG Copper5.2 U MG/KG Molybdenum

0.99 U MG/KG Nickel

2.1 A MG/KG Lead

0.25 U MG/KG Antimony0.50 U MG/KG Selenium

NA MG/KG Tin

1.5 A MG/KG Strontium2.6 AJ MG/KG Titanium

0.25 U MG/KG Thallium

2.0 UJ MG/KG Vanadium

0.30 U MG/KG Yttrium

1.6 A MG/KG Zinc

0.045 U MG/KG Total Mercury

180 A MG/KG Aluminum

1.7 A MG/KG Manganese

71 A MG/KG Calcium

200 A MG/KG Magnesium270 A MG/KG Iron

1300 A MG/KG Sodium

99 U MG/KG Potassium23 % % Moisture

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Per Cent Moisture Determined at 60 Degrees Celsius. Quantitation limit estimated for Cu and VLCS Precision outside Method Acceptance Criteria for Ti. R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
DATA REPORTED ON DRY WEI

_______________________________________________________________________________________________________________________

METALS SAMPLE ANALYSIS Production 

9445 2005 05-0926 Produced by: Scifres, Jenny 

Metals Scan Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/28/2005 14:00Ending: 

 RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU ER1SD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

0.50 U MG/KG Silver0.25 U MG/KG Arsenic

1.0 MG/KG Barium

0.30 U MG/KG Beryllium0.12 U MG/KG Cadmium0.50 U MG/KG Cobalt0.50 U MG/KG Chromium

2.0 UJ MG/KG Copper5.2 U MG/KG Molybdenum1.0 U MG/KG Nickel1.3 MG/KG Lead

0.25 U MG/KG Antimony0.50 U MG/KG Selenium

NA MG/KG Tin

1.1 MG/KG Strontium2.8 J MG/KG Titanium

0.25 U MG/KG Thallium

2.0 UJ MG/KG Vanadium

0.30 U MG/KG Yttrium

1.9 MG/KG Zinc

0.044 U MG/KG Total Mercury

210 MG/KG Aluminum

2.5 MG/KG Manganese

50 MG/KG Calcium

120 MG/KG Magnesium370 MG/KG Iron540 MG/KG Sodium100 U MG/KG Potassium

20 % % Moisture

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Per Cent Moisture Determined at 60 Degrees Celsius. Quantitation limit estimated for Cu and VLCS Precision outside Method Acceptance Criteria for Ti. R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
DATA REPORTED ON DRY WEI

_______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9397 2005 05-0926 Produced by: Revells, Lavon 

Pesticides Scan Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/27/2005 11:30Ending: 

 RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU BC2SD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

11 U UG/KG Aldrin11 U UG/KG Heptachlor11 U UG/KG Heptachlor Epoxide11 U UG/KG alpha-BHC28 U UG/KG beta-BHC11 U UG/KG gamma-BHC (Lindane)11 U UG/KG delta-BHC11 U UG/KG Endosulfan I (alpha)11 U UG/KG Dieldrin41 U UG/KG 4,4'-DDT (p,p'-DDT)11 U UG/KG 4,4'-DDE (p,p'-DDE)27 U UG/KG 4,4'-DDD (p,p'-DDD)27 U UG/KG Endrin27 U UG/KG Endosulfan II (beta)27 U UG/KG Endosulfan Sulfate

1080 U UG/KG Toxaphene

11 U UG/KG Chlordene /211 U UG/KG gamma-Chlordane /211 U UG/KG trans-Nonachlor /211 U UG/KG alpha-Chlordane /211 U UG/KG cis-Nonachlor /254 U UG/KG Methoxychlor35 U UG/KG Endrin Ketone64 % % Moisture

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

P,P-DDT reported MQL raised above requested MQL because of Matrix interferenceOther pesticide results above requested MQL due to low sample dry weightR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
DATA REPORTED ON DRY WEI

_______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9397 2005 05-0926 Produced by: Revells, Lavon 

PCB Scan Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/27/2005 11:30Ending: 

 RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU BC2SD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

100 UJ UG/KG PCB-1242 (Aroclor 1242)100 UJ UG/KG PCB-1254 (Aroclor 1254)100 UJ UG/KG PCB-1221 (Aroclor 1221)100 UJ UG/KG PCB-1232 (Aroclor 1232)100 UJ UG/KG PCB-1248 (Aroclor 1248)100 UJ UG/KG PCB-1260 (Aroclor 1260)100 UJ UG/KG PCB-1016 (Aroclor 1016)

64 % % Moisture

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

QC limits for surrogate exceededR-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
DATA REPORTED ON DRY WEI

_______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9400 2005 05-0926 Produced by: Revells, Lavon 

Pesticides Scan Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/27/2005 13:00Ending: 

 RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU BC4DSD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

5.7 U UG/KG Aldrin6.8 U UG/KG Heptachlor5.7 U UG/KG Heptachlor Epoxide5.7 U UG/KG alpha-BHC5.7 U UG/KG beta-BHC5.7 U UG/KG gamma-BHC (Lindane)5.7 U UG/KG delta-BHC5.7 U UG/KG Endosulfan I (alpha)5.7 U UG/KG Dieldrin

14 U UG/KG 4,4'-DDT (p,p'-DDT)

5.7 U UG/KG 4,4'-DDE (p,p'-DDE)

14 U UG/KG 4,4'-DDD (p,p'-DDD)14 U UG/KG Endrin14 U UG/KG Endosulfan II (beta)14 U UG/KG Endosulfan Sulfate

570 U UG/KG Toxaphene

5.7 U UG/KG Chlordene /25.7 U UG/KG gamma-Chlordane /25.7 U UG/KG trans-Nonachlor /25.7 U UG/KG alpha-Chlordane /25.7 U UG/KG cis-Nonachlor /2

28 U UG/KG Methoxychlor18 U UG/KG Endrin Ketone30 % % Moisture

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
DATA REPORTED ON DRY WEI

_______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9400 2005 05-0926 Produced by: Revells, Lavon 

PCB Scan Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/27/2005 13:00Ending: 

 RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU BC4DSD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

100 U UG/KG PCB-1242 (Aroclor 1242)100 U UG/KG PCB-1254 (Aroclor 1254)100 U UG/KG PCB-1221 (Aroclor 1221)100 U UG/KG PCB-1232 (Aroclor 1232)100 U UG/KG PCB-1248 (Aroclor 1248)100 U UG/KG PCB-1260 (Aroclor 1260)100 U UG/KG PCB-1016 (Aroclor 1016)

30 % % Moisture

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
DATA REPORTED ON DRY WEI

_______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9401 2005 05-0926 Produced by: Revells, Lavon 

Pesticides Scan Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/27/2005 12:40Ending: 

 RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU BC4SD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

6.0 U UG/KG Aldrin6.8 U UG/KG Heptachlor6.0 U UG/KG Heptachlor Epoxide6.0 U UG/KG alpha-BHC6.0 U UG/KG beta-BHC6.0 U UG/KG gamma-BHC (Lindane)6.0 U UG/KG delta-BHC6.0 U UG/KG Endosulfan I (alpha)6.0 U UG/KG Dieldrin

15 U UG/KG 4,4'-DDT (p,p'-DDT)

6.0 U UG/KG 4,4'-DDE (p,p'-DDE)

15 U UG/KG 4,4'-DDD (p,p'-DDD)15 U UG/KG Endrin15 U UG/KG Endosulfan II (beta)15 U UG/KG Endosulfan Sulfate

600 U UG/KG Toxaphene

6.0 U UG/KG Chlordene /26.0 U UG/KG gamma-Chlordane /26.0 U UG/KG trans-Nonachlor /26.0 U UG/KG alpha-Chlordane /26.0 U UG/KG cis-Nonachlor /2

30 U UG/KG Methoxychlor19 U UG/KG Endrin Ketone34 % % Moisture

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
DATA REPORTED ON DRY WEI

_______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9401 2005 05-0926 Produced by: Revells, Lavon 

PCB Scan Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/27/2005 12:40Ending: 

 RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU BC4SD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

100 U UG/KG PCB-1242 (Aroclor 1242)100 U UG/KG PCB-1254 (Aroclor 1254)100 U UG/KG PCB-1221 (Aroclor 1221)100 U UG/KG PCB-1232 (Aroclor 1232)100 U UG/KG PCB-1248 (Aroclor 1248)100 U UG/KG PCB-1260 (Aroclor 1260)100 U UG/KG PCB-1016 (Aroclor 1016)

34 % % Moisture

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
DATA REPORTED ON DRY WEI

_______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9443 2005 05-0926 Produced by: Revells, Lavon 

PCB Scan Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/28/2005 14:30Ending: 

 RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU ER1DSD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

100 U UG/KG PCB-1242 (Aroclor 1242)100 U UG/KG PCB-1254 (Aroclor 1254)100 U UG/KG PCB-1221 (Aroclor 1221)100 U UG/KG PCB-1232 (Aroclor 1232)100 U UG/KG PCB-1248 (Aroclor 1248)100 U UG/KG PCB-1260 (Aroclor 1260)100 U UG/KG PCB-1016 (Aroclor 1016)

21 % % Moisture

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
DATA REPORTED ON DRY WEI

_______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9443 2005 05-0926 Produced by: Revells, Lavon 

Pesticides Scan Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/28/2005 14:30Ending: 

 RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU ER1DSD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

4.1 U UG/KG Aldrin4.1 U UG/KG Heptachlor4.1 U UG/KG Heptachlor Epoxide4.1 U UG/KG alpha-BHC4.1 U UG/KG beta-BHC4.1 U UG/KG gamma-BHC (Lindane)4.1 U UG/KG delta-BHC4.1 U UG/KG Endosulfan I (alpha)4.1 U UG/KG Dieldrin

10 U UG/KG 4,4'-DDT (p,p'-DDT)

4.1 U UG/KG 4,4'-DDE (p,p'-DDE)

10 U UG/KG 4,4'-DDD (p,p'-DDD)10 U UG/KG Endrin10 U UG/KG Endosulfan II (beta)10 U UG/KG Endosulfan Sulfate

410 U UG/KG Toxaphene

4.1 U UG/KG Chlordene /24.1 U UG/KG gamma-Chlordane /24.1 U UG/KG trans-Nonachlor /24.1 U UG/KG alpha-Chlordane /24.1 U UG/KG cis-Nonachlor /2

23 U UG/KG Methoxychlor10 U UG/KG Endrin Ketone21 % % Moisture

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
DATA REPORTED ON DRY WEI

_______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9445 2005 05-0926 Produced by: Revells, Lavon 

PCB Scan Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/28/2005 14:00Ending: 

 RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU ER1SD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

100 U UG/KG PCB-1242 (Aroclor 1242)100 U UG/KG PCB-1254 (Aroclor 1254)100 U UG/KG PCB-1221 (Aroclor 1221)100 U UG/KG PCB-1232 (Aroclor 1232)100 U UG/KG PCB-1248 (Aroclor 1248)100 U UG/KG PCB-1260 (Aroclor 1260)100 U UG/KG PCB-1016 (Aroclor 1016)

20 % % Moisture

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
DATA REPORTED ON DRY WEI

_______________________________________________________________________________________________________________________

PESTICIDES/PCB SAMPLE ANALYSIS Production 

9445 2005 05-0926 Produced by: Revells, Lavon 

Pesticides Scan Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/28/2005 14:00Ending: 

 RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU ER1SD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

4.1 U UG/KG Aldrin4.1 U UG/KG Heptachlor4.1 U UG/KG Heptachlor Epoxide4.1 U UG/KG alpha-BHC4.1 U UG/KG beta-BHC4.1 U UG/KG gamma-BHC (Lindane)4.1 U UG/KG delta-BHC4.1 U UG/KG Endosulfan I (alpha)4.1 U UG/KG Dieldrin

10 U UG/KG 4,4'-DDT (p,p'-DDT)

4.1 U UG/KG 4,4'-DDE (p,p'-DDE)

10 U UG/KG 4,4'-DDD (p,p'-DDD)10 U UG/KG Endrin10 U UG/KG Endosulfan II (beta)10 U UG/KG Endosulfan Sulfate

410 U UG/KG Toxaphene

4.1 U UG/KG Chlordene /24.1 U UG/KG gamma-Chlordane /24.1 U UG/KG trans-Nonachlor /24.1 U UG/KG alpha-Chlordane /24.1 U UG/KG cis-Nonachlor /2

21 U UG/KG Methoxychlor10 U UG/KG Endrin Ketone20 % % Moisture

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordaneU-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
DATA REPORTED ON DRY WEI

_______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9397 2005 05-0926 Produced by: Hale, Sallie 

Volatiles Scan Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/27/2005 11:30Ending: 

 RESULTS UNITS ANALYTE RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU BC2SD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

3.9 U UG/KG Dichlorodifluoromethane 3.9 U UG/KG cis-1,3-Dichloropropene3.9 U UG/KG Chloromethane 19 U UG/KG Bromoform3.9 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 3.9 U UG/KG Bromobenzene3.9 U UG/KG Methyl T-Butyl Ether (MTBE) 3.9 U UG/KG 1,1,2,2-Tetrachloroethan3.9 U UG/KG Bromomethane 3.9 U UG/KG Tetrachloroethene (Tetra3.9 U UG/KG Cyclohexane 3.9 U UG/KG 1,3-Dichloropropane3.9 U UG/KG Vinyl Chloride 3.9 U UG/KG Methyl Butyl Ketone3.9 U UG/KG Chloroethane 3.9 U UG/KG Toluene3.9 U UG/KG Trichlorofluoromethane (Freon 11) 3.9 U UG/KG Chlorobenzene3.9 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 3.9 U UG/KG 1,1,1,2-Tetrachloroethan3.9 U UG/KG Methylene Chloride 3.9 U UG/KG Ethyl Benzene

39 U UG/KG Acetone 7.7 U UG/KG (m- and/or p-)Xylene

4.7 J UG/KG Carbon Disulfide 3.9 U UG/KG o-Xylene3.9 U UG/KG Methyl Acetate 3.9 U UG/KG Styrene3.9 U UG/KG 1,1-Dichloroethane 7.7 U UG/KG 1,2,3-Trichloropropane3.9 U UG/KG cis-1,2-Dichloroethene 3.9 U UG/KG o-Chlorotoluene3.9 U UG/KG 2,2-Dichloropropane 7.7 U UG/KG p-Chlorotoluene7.7 U UG/KG Methyl Ethyl Ketone 7.7 U UG/KG 1,3-Dichlorobenzene3.9 U UG/KG Bromochloromethane 7.7 U UG/KG 1,4-Dichlorobenzene

19 U UG/KG trans-1,2-Dichloroethene 3.9 U UG/KG 1,2-Dichlorobenzene

3.9 U UG/KG Chloroform 3.9 U UG/KG 1,2-Dibromoethane (EDB3.9 U UG/KG 1,2-Dichloroethane 14 UG/KG Isopropylbenzene3.9 U UG/KG 1,1,1-Trichloroethane 51 J UG/KG n-Propylbenzene3.9 U UG/KG 1,1-Dichloropropene 3.9 U UG/KG 1,3,5-Trimethylbenzene3.9 U UG/KG Carbon Tetrachloride 3.9 U UG/KG tert-Butylbenzene3.9 U UG/KG Bromodichloromethane 3.9 U UG/KG 1,2,4-Trimethylbenzene3.9 U UG/KG Methyl Isobutyl Ketone 30 J UG/KG sec-Butylbenzene3.9 U UG/KG 1,2-Dichloropropane 43 J UG/KG p-Isopropyltoluene3.9 U UG/KG Methylcyclohexane 50 J UG/KG n-Butylbenzene3.9 U UG/KG Dibromomethane 19 U UG/KG 1,2-Dibromo-3-Chloropro3.9 U UG/KG trans-1,3-Dichloropropene 7.7 U UG/KG 1,2,4-Trichlorobenzene3.9 U UG/KG Trichloroethene (Trichloroethylene) 3.9 U UG/KG Hexachloro-1,3-Butadien

0.23 J UG/KG Benzene 1.8 J UG/KG 1,2,3-Trichlorobenzene

3.9 U UG/KG Dibromochloromethane 60 % % Moisture3.9 U UG/KG 1,1,2-Trichloroethane

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

Benzene and 1,2,3-trichlorobenzene results >MDL but <MQL.Other results reported as J due to low recovery in MS/MSD.R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
_______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9397 2005 05-0926 Produced by: Hale, Sallie 

MISCELLANEOUS COMPOUNDS Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/27/2005 11:30Ending: 

 RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU BC2SD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

N UG/KG Petroleum Products

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
DATA REPORTED ON DRY WEI

_______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9400 2005 05-0926 Produced by: Hale, Sallie 

Volatiles Scan Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/27/2005 13:00Ending: 

 RESULTS UNITS ANALYTE RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU BC4DSD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

2.3 U UG/KG Dichlorodifluoromethane 2.3 U UG/KG cis-1,3-Dichloropropene2.3 U UG/KG Chloromethane 11 U UG/KG Bromoform2.3 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 2.3 U UG/KG Bromobenzene2.3 U UG/KG Methyl T-Butyl Ether (MTBE) 2.3 U UG/KG 1,1,2,2-Tetrachloroethan2.3 U UG/KG Bromomethane 2.3 U UG/KG Tetrachloroethene (Tetra2.3 U UG/KG Cyclohexane 2.3 U UG/KG 1,3-Dichloropropane2.3 U UG/KG Vinyl Chloride 2.3 U UG/KG Methyl Butyl Ketone2.3 U UG/KG Chloroethane 2.3 U UG/KG Toluene2.3 U UG/KG Trichlorofluoromethane (Freon 11) 2.3 U UG/KG Chlorobenzene2.3 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 2.3 U UG/KG 1,1,1,2-Tetrachloroethan2.3 U UG/KG Methylene Chloride 2.3 U UG/KG Ethyl Benzene

23 U UG/KG Acetone 4.6 U UG/KG (m- and/or p-)Xylene

3.2 UG/KG Carbon Disulfide 2.3 U UG/KG o-Xylene2.3 U UG/KG Methyl Acetate 2.3 U UG/KG Styrene2.3 U UG/KG 1,1-Dichloroethane 4.6 U UG/KG 1,2,3-Trichloropropane2.3 U UG/KG cis-1,2-Dichloroethene 2.3 U UG/KG o-Chlorotoluene2.3 U UG/KG 2,2-Dichloropropane 4.6 U UG/KG p-Chlorotoluene4.6 U UG/KG Methyl Ethyl Ketone 4.6 U UG/KG 1,3-Dichlorobenzene2.3 U UG/KG Bromochloromethane 4.6 U UG/KG 1,4-Dichlorobenzene

11 U UG/KG trans-1,2-Dichloroethene 2.3 U UG/KG 1,2-Dichlorobenzene

2.3 U UG/KG Chloroform 2.3 U UG/KG 1,2-Dibromoethane (EDB2.3 U UG/KG 1,2-Dichloroethane 2.3 U UG/KG Isopropylbenzene2.3 U UG/KG 1,1,1-Trichloroethane 2.3 U UG/KG n-Propylbenzene2.3 U UG/KG 1,1-Dichloropropene 2.3 U UG/KG 1,3,5-Trimethylbenzene2.3 U UG/KG Carbon Tetrachloride 2.3 U UG/KG tert-Butylbenzene2.3 U UG/KG Bromodichloromethane 2.3 U UG/KG 1,2,4-Trimethylbenzene2.3 U UG/KG Methyl Isobutyl Ketone 2.3 U UG/KG sec-Butylbenzene2.3 U UG/KG 1,2-Dichloropropane 2.3 U UG/KG p-Isopropyltoluene2.3 U UG/KG Methylcyclohexane 4.6 U UG/KG n-Butylbenzene2.3 U UG/KG Dibromomethane 11 U UG/KG 1,2-Dibromo-3-Chloropro2.3 U UG/KG trans-1,3-Dichloropropene 4.6 U UG/KG 1,2,4-Trichlorobenzene2.3 U UG/KG Trichloroethene (Trichloroethylene) 2.3 U UG/KG Hexachloro-1,3-Butadien2.3 U UG/KG Benzene 4.6 U UG/KG 1,2,3-Trichlorobenzene2.3 U UG/KG Dibromochloromethane 41 % % Moisture2.3 U UG/KG 1,1,2-Trichloroethane

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
_______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9400 2005 05-0926 Produced by: Hale, Sallie 

MISCELLANEOUS COMPOUNDS Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/27/2005 13:00Ending: 

 RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU BC4DSD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

200 NJ UG/KG Thiobismethane

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
DATA REPORTED ON DRY WEI

_______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9401 2005 05-0926 Produced by: Hale, Sallie 

Volatiles Scan Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/27/2005 12:40Ending: 

 RESULTS UNITS ANALYTE RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU BC4SD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

3.3 U UG/KG Dichlorodifluoromethane 3.3 U UG/KG cis-1,3-Dichloropropene3.3 U UG/KG Chloromethane 16 U UG/KG Bromoform3.3 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 3.3 U UG/KG Bromobenzene3.3 U UG/KG Methyl T-Butyl Ether (MTBE) 3.3 U UG/KG 1,1,2,2-Tetrachloroethan3.3 U UG/KG Bromomethane 3.3 U UG/KG Tetrachloroethene (Tetra3.3 U UG/KG Cyclohexane 3.3 U UG/KG 1,3-Dichloropropane3.3 U UG/KG Vinyl Chloride 3.3 U UG/KG Methyl Butyl Ketone3.3 U UG/KG Chloroethane 3.3 U UG/KG Toluene3.3 U UG/KG Trichlorofluoromethane (Freon 11) 3.3 U UG/KG Chlorobenzene3.3 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 3.3 U UG/KG 1,1,1,2-Tetrachloroethan3.3 U UG/KG Methylene Chloride 3.3 U UG/KG Ethyl Benzene

33 U UG/KG Acetone 6.5 U UG/KG (m- and/or p-)Xylene

4.4 UG/KG Carbon Disulfide 3.3 U UG/KG o-Xylene3.3 U UG/KG Methyl Acetate 3.3 U UG/KG Styrene3.3 U UG/KG 1,1-Dichloroethane 6.5 U UG/KG 1,2,3-Trichloropropane3.3 U UG/KG cis-1,2-Dichloroethene 3.3 U UG/KG o-Chlorotoluene3.3 U UG/KG 2,2-Dichloropropane 6.5 U UG/KG p-Chlorotoluene6.5 U UG/KG Methyl Ethyl Ketone 6.5 U UG/KG 1,3-Dichlorobenzene3.3 U UG/KG Bromochloromethane 6.5 U UG/KG 1,4-Dichlorobenzene

16 U UG/KG trans-1,2-Dichloroethene 3.3 U UG/KG 1,2-Dichlorobenzene

3.3 U UG/KG Chloroform 3.3 U UG/KG 1,2-Dibromoethane (EDB3.3 U UG/KG 1,2-Dichloroethane 3.3 U UG/KG Isopropylbenzene3.3 U UG/KG 1,1,1-Trichloroethane 3.3 U UG/KG n-Propylbenzene3.3 U UG/KG 1,1-Dichloropropene 3.3 U UG/KG 1,3,5-Trimethylbenzene3.3 U UG/KG Carbon Tetrachloride 3.3 U UG/KG tert-Butylbenzene3.3 U UG/KG Bromodichloromethane 3.3 U UG/KG 1,2,4-Trimethylbenzene3.3 U UG/KG Methyl Isobutyl Ketone 3.3 U UG/KG sec-Butylbenzene3.3 U UG/KG 1,2-Dichloropropane 3.3 U UG/KG p-Isopropyltoluene3.3 U UG/KG Methylcyclohexane 6.5 U UG/KG n-Butylbenzene3.3 U UG/KG Dibromomethane 16 U UG/KG 1,2-Dibromo-3-Chloropro3.3 U UG/KG trans-1,3-Dichloropropene 6.5 U UG/KG 1,2,4-Trichlorobenzene3.3 U UG/KG Trichloroethene (Trichloroethylene) 3.3 U UG/KG Hexachloro-1,3-Butadien3.3 U UG/KG Benzene 6.5 U UG/KG 1,2,3-Trichlorobenzene3.3 U UG/KG Dibromochloromethane 50 % % Moisture3.3 U UG/KG 1,1,2-Trichloroethane

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
DATA REPORTED ON DRY WEI

_______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9443 2005 05-0926 Produced by: Hale, Sallie 

Volatiles Scan Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/28/2005 14:30Ending: 

 RESULTS UNITS ANALYTE RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU ER1DSD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

1.2 U UG/KG Dichlorodifluoromethane 1.2 U UG/KG cis-1,3-Dichloropropene1.2 U UG/KG Chloromethane 5.9 U UG/KG Bromoform1.2 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 1.2 U UG/KG Bromobenzene1.2 U UG/KG Methyl T-Butyl Ether (MTBE) 1.2 U UG/KG 1,1,2,2-Tetrachloroethan1.2 U UG/KG Bromomethane 1.2 U UG/KG Tetrachloroethene (Tetra1.2 U UG/KG Cyclohexane 1.2 U UG/KG 1,3-Dichloropropane1.2 U UG/KG Vinyl Chloride 1.2 U UG/KG Methyl Butyl Ketone1.2 U UG/KG Chloroethane 1.2 U UG/KG Toluene1.2 U UG/KG Trichlorofluoromethane (Freon 11) 1.2 U UG/KG Chlorobenzene1.2 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 1.2 U UG/KG 1,1,1,2-Tetrachloroethan1.2 U UG/KG Methylene Chloride 1.2 U UG/KG Ethyl Benzene

12 U UG/KG Acetone 2.4 U UG/KG (m- and/or p-)Xylene

1.2 U UG/KG Carbon Disulfide 1.2 U UG/KG o-Xylene1.2 U UG/KG Methyl Acetate 1.2 U UG/KG Styrene1.2 U UG/KG 1,1-Dichloroethane 2.4 U UG/KG 1,2,3-Trichloropropane1.2 U UG/KG cis-1,2-Dichloroethene 1.2 U UG/KG o-Chlorotoluene1.2 U UG/KG 2,2-Dichloropropane 2.4 U UG/KG p-Chlorotoluene2.4 U UG/KG Methyl Ethyl Ketone 2.4 U UG/KG 1,3-Dichlorobenzene1.2 U UG/KG Bromochloromethane 2.4 U UG/KG 1,4-Dichlorobenzene5.9 U UG/KG trans-1,2-Dichloroethene 1.2 U UG/KG 1,2-Dichlorobenzene1.2 U UG/KG Chloroform 1.2 U UG/KG 1,2-Dibromoethane (EDB1.2 U UG/KG 1,2-Dichloroethane 1.2 U UG/KG Isopropylbenzene1.2 U UG/KG 1,1,1-Trichloroethane 1.2 U UG/KG n-Propylbenzene1.2 U UG/KG 1,1-Dichloropropene 1.2 U UG/KG 1,3,5-Trimethylbenzene1.2 U UG/KG Carbon Tetrachloride 1.2 U UG/KG tert-Butylbenzene1.2 U UG/KG Bromodichloromethane 1.2 U UG/KG 1,2,4-Trimethylbenzene1.2 U UG/KG Methyl Isobutyl Ketone 1.2 U UG/KG sec-Butylbenzene1.2 U UG/KG 1,2-Dichloropropane 1.2 U UG/KG p-Isopropyltoluene1.2 U UG/KG Methylcyclohexane 2.4 U UG/KG n-Butylbenzene1.2 U UG/KG Dibromomethane 5.9 U UG/KG 1,2-Dibromo-3-Chloropro1.2 U UG/KG trans-1,3-Dichloropropene 2.4 U UG/KG 1,2,4-Trichlorobenzene1.2 U UG/KG Trichloroethene (Trichloroethylene) 1.2 U UG/KG Hexachloro-1,3-Butadien1.2 U UG/KG Benzene 2.4 U UG/KG 1,2,3-Trichlorobenzene1.2 U UG/KG Dibromochloromethane 23 % % Moisture1.2 U UG/KG 1,1,2-Trichloroethane

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
DATA REPORTED ON DRY WEI

_______________________________________________________________________________________________________________________

VOLATILES SAMPLE ANALYSIS Production 

9445 2005 05-0926 Produced by: Hale, Sallie 

Volatiles Scan Requestor: MDEQ Project Leader: MKOENIG

Beginning: 09/28/2005 14:00Ending: 

 RESULTS UNITS ANALYTE RESULTS UNITS ANALYTE

Mississippi Gulf Coast Monitoring Study 

WQU ER1SD / 

__________________________________________________________________________________________________________________________________________________________________________________

SEDIMENT 

1.2 U UG/KG Dichlorodifluoromethane 1.2 U UG/KG cis-1,3-Dichloropropene1.2 U UG/KG Chloromethane 6.3 U UG/KG Bromoform1.2 U UG/KG 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) 1.2 U UG/KG Bromobenzene1.2 U UG/KG Methyl T-Butyl Ether (MTBE) 1.2 U UG/KG 1,1,2,2-Tetrachloroethan1.2 U UG/KG Bromomethane 1.2 U UG/KG Tetrachloroethene (Tetra1.2 U UG/KG Cyclohexane 1.2 U UG/KG 1,3-Dichloropropane1.2 U UG/KG Vinyl Chloride 1.2 U UG/KG Methyl Butyl Ketone1.2 U UG/KG Chloroethane 1.2 U UG/KG Toluene1.2 U UG/KG Trichlorofluoromethane (Freon 11) 1.2 U UG/KG Chlorobenzene1.2 U UG/KG 1,1-Dichloroethene (1,1-Dichloroethylene) 1.2 U UG/KG 1,1,1,2-Tetrachloroethan1.2 U UG/KG Methylene Chloride 1.2 U UG/KG Ethyl Benzene

12 U UG/KG Acetone 2.5 U UG/KG (m- and/or p-)Xylene

1.2 U UG/KG Carbon Disulfide 1.2 U UG/KG o-Xylene1.2 U UG/KG Methyl Acetate 1.2 U UG/KG Styrene1.2 U UG/KG 1,1-Dichloroethane 2.5 U UG/KG 1,2,3-Trichloropropane1.2 U UG/KG cis-1,2-Dichloroethene 1.2 U UG/KG o-Chlorotoluene1.2 U UG/KG 2,2-Dichloropropane 2.5 U UG/KG p-Chlorotoluene2.5 U UG/KG Methyl Ethyl Ketone 2.5 U UG/KG 1,3-Dichlorobenzene1.2 U UG/KG Bromochloromethane 2.5 U UG/KG 1,4-Dichlorobenzene6.3 U UG/KG trans-1,2-Dichloroethene 1.2 U UG/KG 1,2-Dichlorobenzene1.2 U UG/KG Chloroform 1.2 U UG/KG 1,2-Dibromoethane (EDB1.2 U UG/KG 1,2-Dichloroethane 1.2 U UG/KG Isopropylbenzene1.2 U UG/KG 1,1,1-Trichloroethane 1.2 U UG/KG n-Propylbenzene1.2 U UG/KG 1,1-Dichloropropene 1.2 U UG/KG 1,3,5-Trimethylbenzene1.2 U UG/KG Carbon Tetrachloride 1.2 U UG/KG tert-Butylbenzene1.2 U UG/KG Bromodichloromethane 1.2 U UG/KG 1,2,4-Trimethylbenzene1.2 U UG/KG Methyl Isobutyl Ketone 1.2 U UG/KG sec-Butylbenzene1.2 U UG/KG 1,2-Dichloropropane 1.2 U UG/KG p-Isopropyltoluene1.2 U UG/KG Methylcyclohexane 2.5 U UG/KG n-Butylbenzene1.2 U UG/KG Dibromomethane 6.3 U UG/KG 1,2-Dibromo-3-Chloropro1.2 U UG/KG trans-1,3-Dichloropropene 2.5 U UG/KG 1,2,4-Trichlorobenzene1.2 U UG/KG Trichloroethene (Trichloroethylene) 1.2 U UG/KG Hexachloro-1,3-Butadien1.2 U UG/KG Benzene 2.5 U UG/KG 1,2,3-Trichlorobenzene1.2 U UG/KG Dibromochloromethane 20 % % Moisture1.2 U UG/KG 1,1,2-Trichloroethane

__________________________________________________________________________________________________________________________________________________________________________________

EPA - REGION IV SESD, ATHENS, GA

Sample FY Project:Facility:Program:Id/Station:Media:

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative idenK-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value. L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.U-Analyte not detected at or above reporting limit. | J-Identification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above repor
Data Package Checklist Reviewer Initials Date 

(Initials do not signify approval) MASB QA Officer 

 NAREL QA Coordinator 

 MASB Chief 

Project: KATRINA RESPONSE-MS

Date due:

SDG Number: #0500067

Analysis: NAREL RA-04

Type of Package: 9 Data Summary Package 9 Complete Package

Y N N/A Comments

9 9 9 All samples in the SDG are reported

9 9 9 All results are the ones intended

9 9 9 Printed results match the raw data

9 9 9 Error report forms are attached

9 9 9 SDG Form is attached

9 9 9 Analyst’s checklist is attached

9 9 9 Original prep batch forms are attached

9 9 9 All supporting data sheets are attached

9 9 9 All raw data sheets appear to be correct

9 9 9 All handwritten notes are initialed and dated

9 9 9 Package is arranged correctly

9 9 9 Package appears to be complete

Were holding times met? 9 Yes 9 No 9 N/A

Were all QC results acceptable? 9 Yes 9 No

Are there any exceptions to report? 9 Yes 9 No

Prepared by: 

QAO Review

Y N N/A

9 9 9 All QC failures are noted Note: If changes to the case

9 9 9 Raw data look reasonable narrative are suggested, please

9 9 9 All exceptions have been noted provide the necessary language.

Comments: 
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES 

REPORT OF SAMPLE DELIVERY GROUP #0500067

Project: KATRINA RESPONSE-MS

Analysis Procedure: Radium-226 in Environmental Matrices

Date Reported: 11/17/2005

SAMPLES

NAREL

Sample # Client Sample ID Type Matrix DateCollected

Date

Received

A5.04976C

A5.04977D

A5.04978E

A5.04979F

A5.04980Y

A5.04981Z

CFMSD03

CFMSD04

CFMSD05

CFMSD05D

CFMSD06

CFMSD07

SAM

SAM

SAM

SAM

SAM

SAM

SEDIMENT

SEDIMENT

SEDIMENT

SEDIMENT

SEDIMENT

SEDIMENT

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

EXCEPTIONS

1. Packaging and Shipping - No problems were observed.

2. Documentation - No problems were observed.

3. Sample Preparation - No problems were encountered.

4. Analysis - No problems were encountered.

5. Holding Times - All holding times were met.

QUALITY CONTROL

1. QC samples - All QC analysis results met NAREL acceptance criteria except the matrix spike result.

2. Instruments - Response and background checks for all instruments used in these analyses met NAREL

acceptance criteria.

CERTIFICATION

I certify that this data report complies with the terms and conditions of the Quality Assurance Project Plan, except as

noted above. Release of the data contained in this report has been authorized by the Chief of the Monitoring and

Analytical Services Branch and the NAREL Quality Assurance Coordinator, or their designees, as verified by the

following signatures.

___________________________________________________

Mary F. Wisdom Date 

Quality Assurance Coordinator

___________________________________________________

John Griggs, Ph.D. Date 

Chief, Monitoring and Analytical Services Branch
GENERAL INFORMATION

SAMPLE TYPES

BLD Blind sample

FBK Field blank

SAM Normal sample

ANALYSIS QC TYPES

ANA Normal analysis

DUP Laboratory duplicate

LCS Laboratory control sample (blank spike)

MS Matrix spike

MSD Matrix spike duplicate

RBK Reagent blank

QUALITY INDICATORS

RPD Relative Percent Difference

%R Percent Recovery

Z Number of standard deviations by which a QC measurement differs from the expected value

EVALUATION OF QC ANALYSES

A reagent blank result is considered unacceptable if it is more than 3 standard deviations below zero or more than 3

standard deviations above a predetermined upper control limit. For some analyses NAREL has set the upper control

limit at zero. For others the control limit is a small positive number.

NAREL evaluates the results of duplicate and spike analyses using "Z scores." A Z score is the number of standard

deviations by which the QC result differs from its ideal value. The score is considered acceptable if its absolute value

is not greater than 3.

The Z score for a spiked sample is computed by dividing the difference between the measured value and the target value

by the combined standard uncertainty of the difference.

The Z score for a duplicate analysis is computed by dividing the difference between the two measured values by the

combined standard uncertainty of the difference. When the precision of paired MS/MSD analyses is evaluated, the

native sample activity is subtracted from each measured value and the net concentrations are then converted to total

activities before the Z score is computed.

Each standard uncertainty used to compute a Z score includes an additional fixed term to represent sources of

measurement error other than counting error. This additional term is not used in the evaluation of reagent blanks.

NAREL reports the "relative percent difference," or RPD, between duplicate results and the "percent recovery," or %R,

for spiked analyses, but does not use these values for evaluation.
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500067

ANALYSIS SUMMARY

Analysis Procedure: NAREL RA-04 

Title: Radium-226 in Environmental Matrices 

NAREL Sample # QC

Type Preparation Procedure Date

Completed

Prep

Batch #

QC

Batch #

A5.04976C

A5.04976C

A5.04977D

A5.04977D

A5.04977D

A5.04978E

A5.04979F

A5.04980Y

A5.04981Z

RBK-00496346B *

DUP

MS

MSD

RBK

NAREL RA-01

NAREL RA-01

NAREL RA-01

NAREL RA-01

NAREL RA-01

NAREL RA-01

NAREL RA-01

NAREL RA-01

NAREL RA-01

NAREL RA-01

11/10/2005

11/10/2005

11/10/2005

11/10/2005

11/10/2005

11/17/2005

11/17/2005

11/17/2005

11/17/2005

11/10/2005

0010184F

0010184F

0010184F

0010184F

0010184F

0010197L

0010197L

0010197L

0010197L

0010184F

0003928W

0003928W

0003928W

0003928W

0003928W

0003928W

0003928W

0003928W

0003928W

0003928W

* Samples marked with an asterisk are not in this sample delivery group but were analyzed with it for QC purposes.

PREPARATION METHOD(S) USED

Procedure ID Title

NAREL RA-01 Preparing Solid Samples for Ra-226 and Ra-228 Analysis
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #: A5.04976C

Matrix: SEDIMENT

Sample type: SAM

Amount analyzed: 4.935e-01 GASH

Dry/wet weight: 44.22 %

Ash/dry weight: 92.00 %

QC batch #: 0003928W

Prep batch #: 0010184F

Prep procedure: NAREL RA-01

Analysis procedure: NAREL RA-04

Analyst: CHD

QC type: ANA

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

11/09/2005 18:25 1000.0 LC4E DPG

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ra226 4.90e-01 8.8e-02 2.7e-02 PCI/GDRY 10/25/2005
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #: A5.04976C

Matrix: SEDIMENT

Sample type: SAM

Amount analyzed: 5.034e-01 GASH

Dry/wet weight: 44.22 %

Ash/dry weight: 92.00 %

QC batch #: 0003928W

Prep batch #: 0010184F

Prep procedure: NAREL RA-01

Analysis procedure: NAREL RA-04

Analyst: CHD

QC type: DUP

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

11/09/2005 18:25 1000.0 LC4F DPG

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ra226 6.06e-01 1.1e-01 3.9e-02 PCI/GDRY 10/25/2005
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #: A5.04977D

Matrix: SEDIMENT

Sample type: SAM

Amount analyzed: 4.977e-01 GASH

Dry/wet weight: 75.62 %

Ash/dry weight: 96.80 %

QC batch #: 0003928W

Prep batch #: 0010184F

Prep procedure: NAREL RA-01

Analysis procedure: NAREL RA-04

Analyst: CHD

QC type: ANA

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

11/09/2005 18:25 1000.0 LC4G DPG

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ra226 5.77e-01 1.0e-01 3.5e-02 PCI/GDRY 10/25/2005
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #: A5.04977D

Matrix: SEDIMENT

Sample type: SAM

Amount analyzed: 4.977e-01 GASH

Dry/wet weight: 75.62 %

Ash/dry weight: 96.80 %

QC batch #: 0003928W

Prep batch #: 0010184F

Prep procedure: NAREL RA-01

Analysis procedure: NAREL RA-04

Analyst: CHD

QC type: MS

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

11/09/2005 18:25 1000.0 LC4I DPG

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ra226 2.31e+01 3.5e+00 2.7e-02 PCI/GDRY 10/25/2005
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #: A5.04977D

Matrix: SEDIMENT

Sample type: SAM

Amount analyzed: 4.977e-01 GASH

Dry/wet weight: 75.62 %

Ash/dry weight: 96.80 %

QC batch #: 0003928W

Prep batch #: 0010184F

Prep procedure: NAREL RA-01

Analysis procedure: NAREL RA-04

Analyst: CHD

QC type: MSD

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

11/09/2005 18:25 1000.0 LC4K DPG

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ra226 3.25e+01 4.8e+00 3.4e-02 PCI/GDRY 10/25/2005
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #: A5.04978E

Matrix: SEDIMENT

Sample type: SAM

Amount analyzed: 4.937e-01 GASH

Dry/wet weight: 22.28 %

Ash/dry weight: 56.40 %

QC batch #: 0003928W

Prep batch #: 0010197L

Prep procedure: NAREL RA-01

Analysis procedure: NAREL RA-04

Analyst: CHD

QC type: ANA

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

11/16/2005 18:15 1000.0 LC4D CHD

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ra226 7.35e-01 1.2e-01 1.9e-02 PCI/GDRY 10/25/2005
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #: A5.04979F

Matrix: SEDIMENT

Sample type: SAM

Amount analyzed: 4.973e-01 GASH

Dry/wet weight: 23.14 %

Ash/dry weight: 66.40 %

QC batch #: 0003928W

Prep batch #: 0010197L

Prep procedure: NAREL RA-01

Analysis procedure: NAREL RA-04

Analyst: CHD

QC type: ANA

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

11/16/2005 18:15 1000.0 LC4E CHD

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ra226 7.42e-01 1.2e-01 1.7e-02 PCI/GDRY 10/25/2005
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #: A5.04980Y

Matrix: SEDIMENT

Sample type: SAM

Amount analyzed: 4.974e-01 GASH

Dry/wet weight: 50.08 %

Ash/dry weight: 82.40 %

QC batch #: 0003928W

Prep batch #: 0010197L

Prep procedure: NAREL RA-01

Analysis procedure: NAREL RA-04

Analyst: CHD

QC type: ANA

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

11/16/2005 18:15 1000.0 LC4G CHD

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ra226 8.82e-01 1.4e-01 3.1e-02 PCI/GDRY 10/25/2005
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #: A5.04981Z

Matrix: SEDIMENT

Sample type: SAM

Amount analyzed: 4.981e-01 GASH

Dry/wet weight: 59.53 %

Ash/dry weight: 85.20 %

QC batch #: 0003928W

Prep batch #: 0010197L

Prep procedure: NAREL RA-01

Analysis procedure: NAREL RA-04

Analyst: CHD

QC type: ANA

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

11/16/2005 18:15 1000.0 LC4I CHD

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ra226 3.72e-01 6.9e-02 2.6e-02 PCI/GDRY 10/25/2005
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500067

SAMPLE ANALYSIS REPORT

QC Sample #: RBK-00496346B QC batch #: 0003928W

Prep batch #: 0010184F

Prep procedure: NAREL RA-01

Analysis procedure: NAREL RA-04

Analyst: CHD

QC type: RBK

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

11/09/2005 18:25 1000.0 LC4M DPG

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ra226 3.83e-02 1.3e-02 1.4e-02 PCI 10/25/2005
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500067

QC BATCH SUMMARY

QC batch #: 0003928W

Preparation procedure: NAREL RA-01

Analysis procedure: NAREL RA-04

NAREL Sample # QC

Type Yield (%) ± 2σ Uncertainty (%) Analyst

A5.04976C

A5.04976C

A5.04977D

A5.04977D

A5.04977D

A5.04978E

A5.04979F

A5.04980Y

A5.04981Z

RBK-00496346B *

DUP

MS

MSD

RBK

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

CHD

CHD

CHD

CHD

CHD

CHD

CHD

CHD

CHD

CHD

* Samples marked with an asterisk are not in this sample delivery group but were analyzed with it for QC purposes.
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500067

PREPARATION BATCH SUMMARY

SAMPLES ANALYZED

NAREL

Sample #

QC

Type Aliquot Size Completion

Date Prep Batch

A5.04976C

A5.04976C

A5.04977D

A5.04977D

A5.04977D

A5.04978E

A5.04979F

A5.04980Y

A5.04981Z

RBK-00496346B *

DUP

MS

MSD

RBK

4.94e-01 GASH

5.03e-01 GASH

4.98e-01 GASH

4.98e-01 GASH

4.98e-01 GASH

4.94e-01 GASH

4.97e-01 GASH

4.97e-01 GASH

4.98e-01 GASH

1.00e+00 SAMP

11/10/2005

11/10/2005

11/10/2005

11/10/2005

11/10/2005

11/17/2005

11/17/2005

11/17/2005

11/17/2005

11/10/2005

0010184F

0010184F

0010184F

0010184F

0010184F

0010197L

0010197L

0010197L

0010197L

0010184F

* Samples marked with an asterisk are not in this sample delivery group but were analyzed with it for QC purposes.
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500067

DETECTOR REPORT

The following were used for samples in the SDG

LC4D 11/16/2005 18:15 00495553C A5.04978E

LC4E 11/09/2005 18:25 00495547E A5.04976C

LC4E 11/16/2005 18:15 00495556F A5.04979F

LC4F 11/09/2005 18:25 00496343Y A5.04976C

LC4G 11/09/2005 18:25 00495550Z A5.04977D

LC4G 11/16/2005 18:15 00495559J A5.04980Y

LC4I 11/09/2005 18:25 00496344Z A5.04977D

LC4I 11/16/2005 18:15 00495563E A5.04981Z

LC4K 11/09/2005 18:25 00496345A A5.04977D

The following were used for other samples in the QC batches

LC4M 11/09/2005 18:25 00496346B 
Data Package Checklist Reviewer Initials Date 

(Initials do not signify approval) MASB QA Officer 

 NAREL QA Coordinator 

 MASB Chief 

Project: KATRINA RESPONSE-MS

Date due:

SDG Number: #0500068

Analysis: NAREL RA-04

Type of Package: 9 Data Summary Package 9 Complete Package

Y N N/A Comments

9 9 9 All samples in the SDG are reported

9 9 9 All results are the ones intended

9 9 9 Printed results match the raw data

9 9 9 Error report forms are attached

9 9 9 SDG Form is attached

9 9 9 Analyst’s checklist is attached

9 9 9 Original prep batch forms are attached

9 9 9 All supporting data sheets are attached

9 9 9 All raw data sheets appear to be correct

9 9 9 All handwritten notes are initialed and dated

9 9 9 Package is arranged correctly

9 9 9 Package appears to be complete

Were holding times met? 9 Yes 9 No 9 N/A

Were all QC results acceptable? 9 Yes 9 No

Are there any exceptions to report? 9 Yes 9 No

Prepared by: 

QAO Review

Y N N/A

9 9 9 All QC failures are noted Note: If changes to the case

9 9 9 Raw data look reasonable narrative are suggested, please

9 9 9 All exceptions have been noted provide the necessary language.

Comments: 
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES 

REPORT OF SAMPLE DELIVERY GROUP #0500068

Project: KATRINA RESPONSE-MS

Analysis Procedure: Radium-226 in Environmental Matrices

Date Reported: 11/17/2005

SAMPLES

NAREL

Sample # Client Sample ID Type Matrix DateCollected

Date

Received

A5.04982A

A5.04983B

A5.04984C

A5.04985D

CFMSF01

CFMSF02

CFMSF02S

CFMSF08

SAM

SAM

SAM

SAM

SOIL

SOIL

SOIL

SOIL

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

EXCEPTIONS

1. Packaging and Shipping - No problems were observed.

2. Documentation - No problems were observed.

3. Sample Preparation - No problems were encountered.

4. Analysis - No problems were encountered.

5. Holding Times - All holding times were met.

QUALITY CONTROL

1. QC samples - All QC analysis results met NAREL acceptance criteria.

2. Instruments - Response and background checks for all instruments used in these analyses met NAREL

acceptance criteria.

CERTIFICATION

I certify that this data report complies with the terms and conditions of the Quality Assurance Project Plan, except as

noted above. Release of the data contained in this report has been authorized by the Chief of the Monitoring and

Analytical Services Branch and the NAREL Quality Assurance Coordinator, or their designees, as verified by the

following signatures.

___________________________________________________

Mary F. Wisdom Date 

Quality Assurance Coordinator

___________________________________________________

John Griggs, Ph.D. Date 

Chief, Monitoring and Analytical Services Branch
GENERAL INFORMATION

SAMPLE TYPES

BLD Blind sample

FBK Field blank

SAM Normal sample

ANALYSIS QC TYPES

ANA Normal analysis

DUP Laboratory duplicate

LCS Laboratory control sample (blank spike)

MS Matrix spike

MSD Matrix spike duplicate

RBK Reagent blank

QUALITY INDICATORS

RPD Relative Percent Difference

%R Percent Recovery

Z Number of standard deviations by which a QC measurement differs from the expected value

EVALUATION OF QC ANALYSES

A reagent blank result is considered unacceptable if it is more than 3 standard deviations below zero or more than 3

standard deviations above a predetermined upper control limit. For some analyses NAREL has set the upper control

limit at zero. For others the control limit is a small positive number.

NAREL evaluates the results of duplicate and spike analyses using "Z scores." A Z score is the number of standard

deviations by which the QC result differs from its ideal value. The score is considered acceptable if its absolute value

is not greater than 3.

The Z score for a spiked sample is computed by dividing the difference between the measured value and the target value

by the combined standard uncertainty of the difference.

The Z score for a duplicate analysis is computed by dividing the difference between the two measured values by the

combined standard uncertainty of the difference. When the precision of paired MS/MSD analyses is evaluated, the

native sample activity is subtracted from each measured value and the net concentrations are then converted to total

activities before the Z score is computed.

Each standard uncertainty used to compute a Z score includes an additional fixed term to represent sources of

measurement error other than counting error. This additional term is not used in the evaluation of reagent blanks.

NAREL reports the "relative percent difference," or RPD, between duplicate results and the "percent recovery," or %R,

for spiked analyses, but does not use these values for evaluation.
(Blank page)
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500068

ANALYSIS SUMMARY

Analysis Procedure: NAREL RA-04 

Title: Radium-226 in Environmental Matrices 

NAREL Sample # QC

Type Preparation Procedure Date

Completed

Prep

Batch #

QC

Batch #

A5.04982A

A5.04982A

A5.04982A

A5.04983B

A5.04983B

A5.04984C

A5.04985D

RBK-00496350X *

MS

MSD

DUP

RBK

NAREL RA-01

NAREL RA-01

NAREL RA-01

NAREL RA-01

NAREL RA-01

NAREL RA-01

NAREL RA-01

NAREL RA-01

11/15/2005

11/15/2005

11/15/2005

11/15/2005

11/15/2005

11/17/2005

11/17/2005

11/15/2005

0010188K

0010188K

0010188K

0010188K

0010188K

0010198M

0010198M

0010188K

0003929X

0003929X

0003929X

0003929X

0003929X

0003929X

0003929X

0003929X

* Samples marked with an asterisk are not in this sample delivery group but were analyzed with it for QC purposes.

PREPARATION METHOD(S) USED

Procedure ID Title

NAREL RA-01 Preparing Solid Samples for Ra-226 and Ra-228 Analysis
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500068

SAMPLE ANALYSIS REPORT

Sample #: A5.04982A

Matrix: SOIL

Sample type: SAM

Amount analyzed: 5.022e-01 GASH

Dry/wet weight: 91.12 %

Ash/dry weight: 96.80 %

QC batch #: 0003929X

Prep batch #: 0010188K

Prep procedure: NAREL RA-01

Analysis procedure: NAREL RA-04

Analyst: CHD

QC type: ANA

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

11/14/2005 18:30 1000.0 LC4E DPG

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ra226 9.22e-01 1.5e-01 2.6e-02 PCI/GDRY 10/25/2005
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500068

SAMPLE ANALYSIS REPORT

Sample #: A5.04982A

Matrix: SOIL

Sample type: SAM

Amount analyzed: 4.981e-01 GASH

Dry/wet weight: 91.12 %

Ash/dry weight: 96.80 %

QC batch #: 0003929X

Prep batch #: 0010188K

Prep procedure: NAREL RA-01

Analysis procedure: NAREL RA-04

Analyst: CHD

QC type: MS

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

11/14/2005 18:30 1000.0 LC4F DPG

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ra226 3.68e+01 5.5e+00 3.6e-02 PCI/GDRY 10/25/2005
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500068

SAMPLE ANALYSIS REPORT

Sample #: A5.04982A

Matrix: SOIL

Sample type: SAM

Amount analyzed: 5.022e-01 GASH

Dry/wet weight: 91.12 %

Ash/dry weight: 96.80 %

QC batch #: 0003929X

Prep batch #: 0010188K

Prep procedure: NAREL RA-01

Analysis procedure: NAREL RA-04

Analyst: CHD

QC type: MSD

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

11/14/2005 18:30 1000.0 LC4G DPG

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ra226 3.09e+01 4.6e+00 3.2e-02 PCI/GDRY 10/25/2005
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500068

SAMPLE ANALYSIS REPORT

Sample #: A5.04983B

Matrix: SOIL

Sample type: SAM

Amount analyzed: 4.931e-01 GASH

Dry/wet weight: 77.88 %

Ash/dry weight: 95.20 %

QC batch #: 0003929X

Prep batch #: 0010188K

Prep procedure: NAREL RA-01

Analysis procedure: NAREL RA-04

Analyst: CHD

QC type: ANA

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

11/14/2005 18:30 1000.0 LC4I DPG

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ra226 5.85e-01 1.0e-01 2.8e-02 PCI/GDRY 10/25/2005
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500068

SAMPLE ANALYSIS REPORT

Sample #: A5.04983B

Matrix: SOIL

Sample type: SAM

Amount analyzed: 4.982e-01 GASH

Dry/wet weight: 77.88 %

Ash/dry weight: 95.20 %

QC batch #: 0003929X

Prep batch #: 0010188K

Prep procedure: NAREL RA-01

Analysis procedure: NAREL RA-04

Analyst: CHD

QC type: DUP

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

11/14/2005 18:30 1000.0 LC4K DPG

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ra226 6.92e-01 1.2e-01 3.2e-02 PCI/GDRY 10/25/2005
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500068

SAMPLE ANALYSIS REPORT

Sample #: A5.04984C

Matrix: SOIL

Sample type: SAM

Amount analyzed: 5.005e-01 GASH

Dry/wet weight: 77.37 %

Ash/dry weight: 95.20 %

QC batch #: 0003929X

Prep batch #: 0010198M

Prep procedure: NAREL RA-01

Analysis procedure: NAREL RA-04

Analyst: CHD

QC type: ANA

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

11/16/2005 18:15 1000.0 LC4K CHD

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ra226 6.70e-01 1.1e-01 3.3e-02 PCI/GDRY 10/25/2005
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500068

SAMPLE ANALYSIS REPORT

Sample #: A5.04985D

Matrix: SOIL

Sample type: SAM

Amount analyzed: 4.960e-01 GASH

Dry/wet weight: 93.22 %

Ash/dry weight: 97.20 %

QC batch #: 0003929X

Prep batch #: 0010198M

Prep procedure: NAREL RA-01

Analysis procedure: NAREL RA-04

Analyst: CHD

QC type: ANA

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

11/16/2005 18:15 1000.0 LC4M CHD

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ra226 5.54e-01 9.7e-02 2.6e-02 PCI/GDRY 10/25/2005
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500068

SAMPLE ANALYSIS REPORT

QC Sample #: RBK-00496350X QC batch #: 0003929X

Prep batch #: 0010188K

Prep procedure: NAREL RA-01

Analysis procedure: NAREL RA-04

Analyst: CHD

QC type: RBK

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

11/14/2005 18:30 1000.0 LC4M DPG

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ra226 7.54e-02 1.7e-02 1.4e-02 PCI 10/25/2005
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500068

QC BATCH SUMMARY

QC batch #: 0003929X

Preparation procedure: NAREL RA-01

Analysis procedure: NAREL RA-04

NAREL Sample # QC

Type Yield (%) ± 2σ Uncertainty (%) Analyst

A5.04982A

A5.04982A

A5.04982A

A5.04983B

A5.04983B

A5.04984C

A5.04985D

RBK-00496350X *

MS

MSD

DUP

RBK

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

CHD

CHD

CHD

CHD

CHD

CHD

CHD

CHD

* Samples marked with an asterisk are not in this sample delivery group but were analyzed with it for QC purposes.
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500068

PREPARATION BATCH SUMMARY

SAMPLES ANALYZED

NAREL

Sample #

QC

Type Aliquot Size Completion

Date Prep Batch

A5.04982A

A5.04982A

A5.04982A

A5.04983B

A5.04983B

A5.04984C

A5.04985D

RBK-00496350X *

MS

MSD

DUP

RBK

5.02e-01 GASH

4.98e-01 GASH

5.02e-01 GASH

4.93e-01 GASH

4.98e-01 GASH

5.01e-01 GASH

4.96e-01 GASH

1.00e+00 SAMP

11/15/2005

11/15/2005

11/15/2005

11/15/2005

11/15/2005

11/17/2005

11/17/2005

11/15/2005

0010188K

0010188K

0010188K

0010188K

0010188K

0010198M

0010198M

0010188K

* Samples marked with an asterisk are not in this sample delivery group but were analyzed with it for QC purposes.
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

SDG #0500068

DETECTOR REPORT

The following were used for samples in the SDG

LC4E 11/14/2005 18:30 00495566H A5.04982A

LC4F 11/14/2005 18:30 00496347C A5.04982A

LC4G 11/14/2005 18:30 00496348D A5.04982A

LC4I 11/14/2005 18:30 00495569L A5.04983B

LC4K 11/14/2005 18:30 00496349E A5.04983B

LC4K 11/16/2005 18:15 00495572F A5.04984C

LC4M 11/16/2005 18:15 00495575J A5.04985D

The following were used for other samples in the QC batches

LC4M 11/14/2005 18:30 00496350X 
Data Package Checklist Reviewer Initials Date 

(Initials do not signify approval) MASB QA Officer 

 NAREL QA Coordinator 

 MASB Chief 

Project: KATRINA RESPONSE-MS

Date due:

SDG Number: #0500067

Analysis: NAREL GAM-01

Type of Package: 9 Data Summary Package 9 Complete Package

Y N N/A Comments

9 9 9 All samples in the SDG are reported

9 9 9 All results are the ones intended

9 9 9 Printed results match the raw data

9 9 9 Error report forms are attached

9 9 9 SDG Form is attached

9 9 9 Analyst’s checklist is attached

9 9 9 Original prep batch forms are attached

9 9 9 All supporting data sheets are attached

9 9 9 All raw data sheets appear to be correct

9 9 9 All handwritten notes are initialed and dated

9 9 9 Package is arranged correctly

9 9 9 Package appears to be complete

Were holding times met? 9 Yes 9 No 9 N/A

Were all QC results acceptable? 9 Yes 9 No

Are there any exceptions to report? 9 Yes 9 No

Prepared by: 

QAO Review

Y N N/A

9 9 9 All QC failures are noted Note: If changes to the case

9 9 9 Raw data look reasonable narrative are suggested, please

9 9 9 All exceptions have been noted provide the necessary language.

Comments: 
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES 

REPORT OF SAMPLE DELIVERY GROUP #0500067

Project: KATRINA RESPONSE-MS

Analysis Procedure: Gamma Spectrometry

Date Reported: 10/27/2005

SAMPLES

NAREL

Sample # Client Sample ID Type Matrix DateCollected

Date

Received

A5.04976C

A5.04977D

A5.04978E

A5.04979F

A5.04980Y

A5.04981Z

CFMSD03

CFMSD04

CFMSD05

CFMSD05D

CFMSD06

CFMSD07

SAM

SAM

SAM

SAM

SAM

SAM

SEDIMENT

SEDIMENT

SEDIMENT

SEDIMENT

SEDIMENT

SEDIMENT

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

EXCEPTIONS

1. Packaging and Shipping - No problems were observed.

2. Documentation - No problems were observed.

3. Sample Preparation - No problems were encountered.

4. Analysis - NAREL sample A5.04978 was originally counted on a detector that failed its daily QC. The

sample was recounted on a different detector. The results of the recount are reported in this data package.

5. Holding Times - All holding times were met.

QUALITY CONTROL

1. QC samples - All QC analysis results met NAREL acceptance criteria.

2. Instruments - Response and background checks for all instruments used in these analyses met NAREL

acceptance criteria.
CERTIFICATION

I certify that this data report complies with the terms and conditions of the Quality Assurance Project Plan, except as

noted above. Release of the data contained in this report has been authorized by the Chief of the Monitoring and

Analytical Services Branch and the NAREL Quality Assurance Coordinator, or their designees, as verified by the

following signatures.

___________________________________________________

Mary F. Wisdom Date 

Quality Assurance Coordinator

___________________________________________________

John Griggs, Ph.D. Date 

Chief, Monitoring and Analytical Services Branch
GENERAL INFORMATION

SAMPLE TYPES

BLD Blind sample

FBK Field blank

SAM Normal sample

ANALYSIS QC TYPES

ANA Normal analysis

DUP Laboratory duplicate

LCS Laboratory control sample (blank spike)

MS Matrix spike

MSD Matrix spike duplicate

RBK Reagent blank

QUALITY INDICATORS

RPD Relative Percent Difference

%R Percent Recovery

Z Number of standard deviations by which a QC measurement differs from the expected value

EVALUATION OF QC ANALYSES

A reagent blank result is considered unacceptable if it is more than 3 standard deviations below zero or more than 3

standard deviations above a predetermined upper control limit. For some analyses NAREL has set the upper control

limit at zero. For others the control limit is a small positive number.

NAREL evaluates the results of duplicate and spike analyses using "Z scores." A Z score is the number of standard

deviations by which the QC result differs from its ideal value. The score is considered acceptable if its absolute value

is not greater than 3.

The Z score for a spiked sample is computed by dividing the difference between the measured value and the target value

by the combined standard uncertainty of the difference.

The Z score for a duplicate analysis is computed by dividing the difference between the two measured values by the

combined standard uncertainty of the difference. When the precision of paired MS/MSD analyses is evaluated, the

native sample activity is subtracted from each measured value and the net concentrations are then converted to total

activities before the Z score is computed.

Each standard uncertainty used to compute a Z score includes an additional fixed term to represent sources of

measurement error other than counting error. This additional term is not used in the evaluation of reagent blanks.

NAREL reports the "relative percent difference," or RPD, between duplicate results and the "percent recovery," or %R,

for spiked analyses, but does not use these values for evaluation.

U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES

SDG #0500067

ANALYSIS SUMMARY

Analysis Procedure: NAREL GAM-01 

Title: Gamma Spectrometry 

NAREL Sample # QC

Type Preparation Procedure Date

Completed

Prep

Batch #

QC

Batch #

A5.04976C

A5.04977D

A5.04978E

A5.04979F

A5.04980Y

A5.04980Y

A5.04981Z

DUP

N/A

N/A

N/A

N/A

N/A

N/A

N/A

10/13/2005

10/13/2005

10/27/2005

10/13/2005

10/13/2005

10/14/2005

10/13/2005

0010113P

0010113P

0010151W

0010113P

0010113P

0010113P

0010113P

0003916R

0003916R

0003916R

0003916R

0003916R

0003916R

0003916R

* Samples marked with an asterisk are not in this sample delivery group but were analyzed with it for QC purposes.
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES

SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #: A5.04976C

Matrix: SEDIMENT

Sample type: SAM

Amount analyzed: 1.150e+02 GDRY

Dry/wet weight: 44.22 %

Ash/dry weight: 92.00 %

QC batch #: 0003916R

Prep batch #: 0010113P

Prep procedure: N/A

Analysis procedure: NAREL GAM-01

Analyst: DPS

QC type: ANA

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

10/12/2005 15:21 1000.0 GE02 NSS

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ba140

Be7

Bi212

Bi214

Co60

Cs137

I131

K40

Pb210

Pb212

Pb214

Ra223

Ra224

Ra226

Ra228

Th234

Tl208

U235

*

*

*

*

*

*

ND

2.75e-01

3.51e-01

3.64e-01

ND

2.39e-02

ND

2.34e+00

8.85e-01

4.65e-01

4.35e-01

1.53e-01

3.97e-01

1.08e+00

3.74e-01

6.77e-01

1.42e-01

6.75e-02

1.5e-01

2.8e-01

6.0e-02

1.7e-02

4.2e-01

9.3e-01

4.8e-02

5.2e-02

7.5e-02

3.3e-01

4.0e-01

7.0e-02

2.3e-01

2.8e-02

2.5e-02

1.6e-01

5.6e-02

5.1e-02

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated.
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES

SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #: A5.04977D

Matrix: SEDIMENT

Sample type: SAM

Amount analyzed: 2.440e+02 GDRY

Dry/wet weight: 75.62 %

Ash/dry weight: 96.80 %

QC batch #: 0003916R

Prep batch #: 0010113P

Prep procedure: N/A

Analysis procedure: NAREL GAM-01

Analyst: DPS

QC type: ANA

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

10/12/2005 15:22 1000.0 GE04 NSS

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ba140

Be7

Bi212

Bi214

Co60

Cs137

I131

K40

Pb210

Pb212

Pb214

Ra224

Ra226

Ra228

Tl208

U235

*

*

*

*

ND

5.55e-02

4.60e-01

3.84e-01

ND

ND

ND

1.11e+00

ND

4.38e-01

4.36e-01

4.03e-01

7.93e-01

4.13e-01

1.29e-01

4.98e-02

5.8e-02

1.3e-01

3.3e-02

1.6e-01

3.3e-02

3.3e-02

2.0e-01

1.9e-01

3.9e-02

1.4e-02

1.2e-02

8.7e-02

2.0e-02

2.0e-02

2.5e-02

3.2e+00

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated.
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES

SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #: A5.04978E

Matrix: SEDIMENT

Sample type: SAM

Amount analyzed: 1.340e+01 GASH

Dry/wet weight: 22.28 %

Ash/dry weight: 56.40 %

QC batch #: 0003916R

Prep batch #: 0010151W

Prep procedure: N/A

Analysis procedure: NAREL GAM-01

Analyst: DPS

QC type: ANA

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

10/26/2005 14:15 1000.0 GE04 NSS

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ba140

Bi212

Bi214

Co60

Cs137

I131

K40

Pb210

Pb212

Pb214

Ra226

Ra228

Th234

Tl208

*

*

*

*

ND

4.59e-01

4.74e-01

ND

4.28e-01

ND

2.32e+00

ND

4.93e-01

5.59e-01

1.26e+00

3.98e-01

1.04e+00

1.35e-01

4.2e-01

9.8e-02

5.3e-02

6.7e-01

8.1e-02

8.3e-02

7.6e-01

1.2e-01

6.1e-01

4.9e-02

6.3e-01

7.8e-02

3.2e-01

9.4e+00

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated.
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES

SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #: A5.04979F

Matrix: SEDIMENT

Sample type: SAM

Amount analyzed: 4.060e+01 GDRY

Dry/wet weight: 23.14 %

Ash/dry weight: 66.40 %

QC batch #: 0003916R

Prep batch #: 0010113P

Prep procedure: N/A

Analysis procedure: NAREL GAM-01

Analyst: DPS

QC type: ANA

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

10/12/2005 15:23 1000.0 GE06 NSS

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ba140

Bi212

Bi214

Co60

Cs137

I131

K40

Pb210

Pb212

Pb214

Ra223

Ra226

Ra228

Th234

Tl208

U235

*

*

*

*

*

ND

6.80e-01

6.00e-01

ND

7.10e-01

ND

2.90e+00

ND

5.55e-01

7.32e-01

2.33e-01

1.66e+00

5.93e-01

1.61e+00

1.92e-01

1.13e-01

3.4e-01

1.0e-01

6.2e-02

5.4e-01

7.3e-02

8.6e-02

1.4e-01

7.4e-01

1.2e-01

5.3e-01

4.4e-02

4.4e-02

2.4e-01

6.1e-02

8.6e-02

3.5e+00

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated.
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES

SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #: A5.04980Y

Matrix: SEDIMENT

Sample type: SAM

Amount analyzed: 7.390e+01 GDRY

Dry/wet weight: 50.08 %

Ash/dry weight: 82.40 %

QC batch #: 0003916R

Prep batch #: 0010113P

Prep procedure: N/A

Analysis procedure: NAREL GAM-01

Analyst: DPS

QC type: ANA

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

10/12/2005 15:23 1000.0 GE07 NSS

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ba140

Be7

Bi212

Bi214

Co60

Cs137

I131

K40

Pb210

Pb212

Pb214

Ra223

Ra226

Ra228

Tl208

U235

*

*

*

*

ND

3.53e-01

1.17e+00

7.05e-01

ND

5.36e-02

ND

6.28e+00

ND

9.39e-01

7.85e-01

2.97e-01

1.82e+00

1.00e+00

2.63e-01

1.14e-01

1.7e-01

3.3e-01

7.6e-02

2.1e-02

6.0e-01

7.8e-02

7.3e-02

1.1e-01

5.8e-01

1.1e-01

3.6e-02

3.6e-02

2.0e-01

4.5e-02

6.6e-02

4.6e+00

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated.
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES

SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #: A5.04980Y

Matrix: SEDIMENT

Sample type: SAM

Amount analyzed: 7.390e+01 GDRY

Dry/wet weight: 50.08 %

Ash/dry weight: 82.40 %

QC batch #: 0003916R

Prep batch #: 0010113P

Prep procedure: N/A

Analysis procedure: NAREL GAM-01

Analyst: DPS

QC type: DUP

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

10/13/2005 12:52 1000.0 GE02 NSS

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ba140

Be7

Bi212

Bi214

Co60

Cs137

I131

K40

Pb210

Pb212

Pb214

Ra223

Ra224

Ra226

Ra228

Th234

Tl208

*

*

*

*

ND

1.50e-01

9.95e-01

6.45e-01

ND

4.26e-02

ND

5.81e+00

ND

9.68e-01

7.51e-01

3.24e-01

8.66e-01

1.89e+00

8.66e-01

1.55e+00

3.00e-01

1.5e-01

3.8e-01

9.1e-02

3.0e-02

7.7e-01

8.3e-02

7.8e-02

1.4e-01

5.4e-01

5.5e-01

1.2e-01

3.9e-01

4.4e-02

2.7e-01

7.8e-02

7.3e-02

2.0e+00

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated.
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES

SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #: A5.04981Z

Matrix: SEDIMENT

Sample type: SAM

Amount analyzed: 7.540e+01 GDRY

Dry/wet weight: 59.53 %

Ash/dry weight: 85.20 %

QC batch #: 0003916R

Prep batch #: 0010113P

Prep procedure: N/A

Analysis procedure: NAREL GAM-01

Analyst: DPS

QC type: ANA

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

10/12/2005 15:22 1000.0 GE09 NSS

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ba140

Be7

Bi212

Bi214

Co60

Cs137

I131

K40

Pb210

Pb212

Pb214

Ra224

Ra226

Ra228

Th234

Tl208

U235

*

*

*

*

ND

3.12e-01

5.62e-01

3.64e-01

ND

6.30e-01

ND

2.25e+00

ND

5.01e-01

4.04e-01

4.95e-01

ND

5.57e-01

7.23e-01

1.66e-01

8.07e-02

1.7e-01

2.8e-01

5.8e-02

4.8e-02

3.4e-01

5.4e-02

5.4e-02

3.8e-01

8.0e-02

3.6e-01

2.8e-02

2.8e-02

1.8e-01

4.1e-02

6.2e-02

4.9e+00

5.9e-01

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated.
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES

SDG #0500067

QC BATCH SUMMARY

QC batch #: 0003916R

Preparation procedure: N/A

Analysis procedure: NAREL GAM-01

NAREL Sample # QC

Type Yield (%) ± 2σ Uncertainty (%) Analyst

A5.04976C

A5.04977D

A5.04978E

A5.04979F

A5.04980Y

A5.04980Y

A5.04981Z

DUP

N/A

N/A

N/A

N/A

N/A

N/A

N/A

DPS

DPS

DPS

DPS

DPS

DPS

DPS

* Samples marked with an asterisk are not in this sample delivery group but were analyzed with it for QC purposes.
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES

SDG #0500067

PREPARATION BATCH SUMMARY

SAMPLES ANALYZED

NAREL

Sample #

QC

Type Aliquot Size Completion

Date Prep Batch

A5.04976C

A5.04977D

A5.04978E

A5.04979F

A5.04980Y

A5.04980Y

A5.04981Z

DUP

1.15e+02 GDRY

2.44e+02 GDRY

1.34e+01 GASH

4.06e+01 GDRY

7.39e+01 GDRY

7.39e+01 GDRY

7.54e+01 GDRY

10/13/2005

10/13/2005

10/27/2005

10/13/2005

10/13/2005

10/14/2005

10/13/2005

0010113P

0010113P

0010151W

0010113P

0010113P

0010113P

0010113P

* Samples marked with an asterisk are not in this sample delivery group but were analyzed with it for QC purposes.
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES

SDG #0500067

DETECTOR REPORT

The following were used for samples in the SDG

GE02 10/12/2005 15:21 00495545C A5.04976C

GE02 10/13/2005 12:52 00495560B A5.04980Y

GE04 10/12/2005 15:22 00495548F A5.04977D

GE04 10/26/2005 14:15 00496380D A5.04978E

GE06 10/12/2005 15:23 00495554D A5.04979F

GE07 10/12/2005 15:23 00495557G A5.04980Y

GE09 10/12/2005 15:22 00495561C A5.04981Z

The following were used for other samples in the QC batches

None found
Data Package Checklist Reviewer Initials Date 

(Initials do not signify approval) MASB QA Officer 

 NAREL QA Coordinator 

 MASB Chief 

Project: KATRINA RESPONSE-MS

Date due:

SDG Number: #0500068

Analysis: NAREL GAM-01

Type of Package: 9 Data Summary Package 9 Complete Package

Y N N/A Comments

9 9 9 All samples in the SDG are reported

9 9 9 All results are the ones intended

9 9 9 Printed results match the raw data

9 9 9 Error report forms are attached

9 9 9 SDG Form is attached

9 9 9 Analyst’s checklist is attached

9 9 9 Original prep batch forms are attached

9 9 9 All supporting data sheets are attached

9 9 9 All raw data sheets appear to be correct

9 9 9 All handwritten notes are initialed and dated

9 9 9 Package is arranged correctly

9 9 9 Package appears to be complete

Were holding times met? 9 Yes 9 No 9 N/A

Were all QC results acceptable? 9 Yes 9 No

Are there any exceptions to report? 9 Yes 9 No

Prepared by: 

QAO Review

Y N N/A

9 9 9 All QC failures are noted Note: If changes to the case

9 9 9 Raw data look reasonable narrative are suggested, please

9 9 9 All exceptions have been noted provide the necessary language.

Comments: 
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES 

REPORT OF SAMPLE DELIVERY GROUP #0500068

Project: KATRINA RESPONSE-MS

Analysis Procedure: Gamma Spectrometry

Date Reported: 10/19/2005

SAMPLES

NAREL

Sample # Client Sample ID Type Matrix DateCollected

Date

Received

A5.04982A

A5.04983B

A5.04984C

A5.04985D

CFMSF01

CFMSF02

CFMSF02S

CFMSF08

SAM

SAM

SAM

SAM

SOIL

SOIL

SOIL

SOIL

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

EXCEPTIONS

1. Packaging and Shipping - No problems were observed.

2. Documentation - No problems were observed.

3. Sample Preparation - No problems were encountered.

4. Analysis - No problems were encountered.

5. Holding Times - All holding times were met.

QUALITY CONTROL

1. QC samples - All QC analysis results met NAREL acceptance criteria.

2. Instruments - Response and background checks for all instruments used in these analyses met NAREL

acceptance criteria.

CERTIFICATION

I certify that this data report complies with the terms and conditions of the Quality Assurance Project Plan, except as

noted above. Release of the data contained in this report has been authorized by the Chief of the Monitoring and

Analytical Services Branch and the NAREL Quality Assurance Coordinator, or their designees, as verified by the

following signatures.

___________________________________________________

Mary F. Wisdom Date 

Quality Assurance Coordinator

___________________________________________________

John Griggs, Ph.D. Date 

Chief, Monitoring and Analytical Services Branch
GENERAL INFORMATION

SAMPLE TYPES

BLD Blind sample

FBK Field blank

SAM Normal sample

ANALYSIS QC TYPES

ANA Normal analysis

DUP Laboratory duplicate

LCS Laboratory control sample (blank spike)

MS Matrix spike

MSD Matrix spike duplicate

RBK Reagent blank

QUALITY INDICATORS

RPD Relative Percent Difference

%R Percent Recovery

Z Number of standard deviations by which a QC measurement differs from the expected value

EVALUATION OF QC ANALYSES

A reagent blank result is considered unacceptable if it is more than 3 standard deviations below zero or more than 3

standard deviations above a predetermined upper control limit. For some analyses NAREL has set the upper control

limit at zero. For others the control limit is a small positive number.

NAREL evaluates the results of duplicate and spike analyses using "Z scores." A Z score is the number of standard

deviations by which the QC result differs from its ideal value. The score is considered acceptable if its absolute value

is not greater than 3.

The Z score for a spiked sample is computed by dividing the difference between the measured value and the target value

by the combined standard uncertainty of the difference.

The Z score for a duplicate analysis is computed by dividing the difference between the two measured values by the

combined standard uncertainty of the difference. When the precision of paired MS/MSD analyses is evaluated, the

native sample activity is subtracted from each measured value and the net concentrations are then converted to total

activities before the Z score is computed.

Each standard uncertainty used to compute a Z score includes an additional fixed term to represent sources of

measurement error other than counting error. This additional term is not used in the evaluation of reagent blanks.

NAREL reports the "relative percent difference," or RPD, between duplicate results and the "percent recovery," or %R,

for spiked analyses, but does not use these values for evaluation.
GENERAL INFORMATION (CONTINUED)

GAMMA ANALYSIS

The reporting format lists the gamma emitters in alphabetical order. The activity and 2-sigma uncertainty for

radionuclides measured by gamma spectroscopy are reported only if the nuclide is detected. Nuclides that are not

detected do not appear in the report, with the exception of Ba-140, Co-60, Cs-137, I-131, K-40, Ra-226 and Ra-228.

If one of these seven nuclides is undetected, NAREL reports it as “Not Detected” or “ND”, and provides a samplespecific estimate of the MDC.

Due to potential spectral interferences and other possible problems associated with the determination of the activity

of certain radionuclides, the activities for Bi-214, Pb-214, Th-234, Pa-234m, Ra-226, Th-231, and U-235 are subject

to greater possible uncertainty than other commonly reported radionuclides. It should be noted that this potential

uncertainty is not included in the two-sigma counting uncertainty which is reported with each activity. Although in

this report we do provide the calculated activities for these radionuclides, we recommend that the results be used only

as a qualitative means of indicating the presence of these radionuclides and not as a quantitative measure of their

concentration. The results for these nuclides are not used in the evaluation of quality control samples. Furthermore,

because of mutual interference between Ra-226 and U-235, NAREL’s gamma analysis software tends to overestimate

the amounts of these nuclides whenever both are present in a sample. Lower estimates for Ra-226 activities can be

obtained from the reported activities of its decay products, Pb-214 and Bi-214, which are likely to be somewhat less

than the Ra-226 activity because of the potential escape of radon gas.

NAREL’s gamma spectroscopy software corrects activities and MDCs for decay between collection and analysis, but

only up to a limit of ten half-lives. So, if the decay time for a sample is more than ten half-lives of a radionuclide, that

nuclide will almost always be undetected and the reported MDC will be meaningless. This is usually a problem only

for short-lived radionuclides, such as I-131 and Ba-140, when there is a long delay between collection and analysis.
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES

SDG #0500068

ANALYSIS SUMMARY

Analysis Procedure: NAREL GAM-01 

Title: Gamma Spectrometry 

NAREL Sample # QC

Type Preparation Procedure Date

Completed

Prep

Batch #

QC

Batch #

A5.04982A

A5.04983B

A5.04984C

A5.04985D

A5.04985D DUP

N/A

N/A

N/A

N/A

N/A

10/13/2005

10/14/2005

10/14/2005

10/14/2005

10/18/2005

0010113P

0010113P

0010113P

0010113P

0010113P

0003917T

0003917T

0003917T

0003917T

0003917T

* Samples marked with an asterisk are not in this sample delivery group but were analyzed with it for QC purposes.
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES

SDG #0500068

SAMPLE ANALYSIS REPORT

Sample #: A5.04982A

Matrix: SOIL

Sample type: SAM

Amount analyzed: 1.510e+02 GDRY

Dry/wet weight: 91.12 %

Ash/dry weight: N/A

QC batch #: 0003917T

Prep batch #: 0010113P

Prep procedure: N/A

Analysis procedure: NAREL GAM-01

Analyst: DPS

QC type: ANA

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

10/13/2005 12:47 500.0 GE13 NSS

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ba140

Bi212

Bi214

Co60

Cs137

I131

K40

Pb210

Pb212

Pb214

Ra223

Ra226

Ra228

Tl208

U235

*

*

*

*

ND

4.72e-01

8.24e-01

ND

4.51e-02

ND

7.19e-01

ND

4.28e-01

8.75e-01

1.41e-01

2.28e+00

4.61e-01

1.34e-01

1.42e-01

2.3e-01

6.6e-02

1.3e-02

2.2e-01

4.3e-02

6.5e-02

1.0e-01

4.1e-01

6.2e-02

2.1e-02

2.5e-02

1.2e-01

2.7e-02

4.9e-02

3.1e+00

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated.
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES

SDG #0500068

SAMPLE ANALYSIS REPORT

Sample #: A5.04983B

Matrix: SOIL

Sample type: SAM

Amount analyzed: 1.560e+02 GDRY

Dry/wet weight: 77.88 %

Ash/dry weight: N/A

QC batch #: 0003917T

Prep batch #: 0010113P

Prep procedure: N/A

Analysis procedure: NAREL GAM-01

Analyst: DPS

QC type: ANA

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

10/13/2005 21:09 500.0 GE13 NSS

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ba140

Bi212

Bi214

Co60

Cs137

I131

K40

Pb210

Pb212

Pb214

Ra223

Ra224

Ra226

Ra228

Tl208

U235

*

*

*

*

ND

3.99e-01

5.10e-01

ND

1.54e-01

ND

5.89e-01

ND

4.64e-01

5.45e-01

1.00e-01

3.93e-01

1.20e+00

4.67e-01

1.36e-01

7.54e-02

2.2e-01

4.8e-02

2.0e-02

2.1e-01

4.6e-02

4.9e-02

1.0e-01

3.6e-01

3.5e-01

6.1e-02

2.1e-02

2.2e-02

1.1e-01

2.6e-02

4.5e-02

2.8e+00

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated.
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES

SDG #0500068

SAMPLE ANALYSIS REPORT

Sample #: A5.04984C

Matrix: SOIL

Sample type: SAM

Amount analyzed: 1.380e+02 GDRY

Dry/wet weight: 77.37 %

Ash/dry weight: N/A

QC batch #: 0003917T

Prep batch #: 0010113P

Prep procedure: N/A

Analysis procedure: NAREL GAM-01

Analyst: DPS

QC type: ANA

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

10/14/2005 05:32 500.0 GE13 NSS

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ba140

Bi212

Bi214

Co60

Cs137

I131

K40

Pb210

Pb212

Pb214

Ra223

Ra226

Ra228

Tl208

U235

*

*

*

*

ND

3.29e-01

5.06e-01

ND

1.56e-01

ND

8.68e-01

ND

4.58e-01

5.59e-01

1.31e-01

1.13e+00

4.77e-01

1.33e-01

7.12e-02

2.4e-01

5.2e-02

2.1e-02

2.2e-01

4.7e-02

5.2e-02

9.8e-02

4.1e-01

6.6e-02

2.2e-02

2.6e-02

1.5e-01

2.8e-02

5.1e-02

3.1e+00

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated.
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES

SDG #0500068

SAMPLE ANALYSIS REPORT

Sample #: A5.04985D

Matrix: SOIL

Sample type: SAM

Amount analyzed: 1.230e+02 GDRY

Dry/wet weight: 93.22 %

Ash/dry weight: N/A

QC batch #: 0003917T

Prep batch #: 0010113P

Prep procedure: N/A

Analysis procedure: NAREL GAM-01

Analyst: DPS

QC type: ANA

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

10/14/2005 13:55 500.0 GE13 NSS

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ba140

Bi212

Bi214

Co60

Cs137

I131

K40

Pb210

Pb212

Pb214

Ra223

Ra226

Ra228

Tl208

U235

*

*

*

*

ND

4.82e-01

4.57e-01

ND

1.60e-02

ND

1.04e+00

ND

4.38e-01

5.17e-01

1.14e-01

8.91e-01

4.66e-01

1.38e-01

5.59e-02

2.9e-01

5.2e-02

1.3e-02

2.8e-01

4.9e-02

5.3e-02

1.1e-01

4.5e-01

6.9e-02

2.4e-02

2.8e-02

1.5e-01

3.2e-02

5.4e-02

3.4e+00

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated.
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES

SDG #0500068

SAMPLE ANALYSIS REPORT

Sample #: A5.04985D

Matrix: SOIL

Sample type: SAM

Amount analyzed: 1.230e+02 GDRY

Dry/wet weight: 93.22 %

Ash/dry weight: N/A

QC batch #: 0003917T

Prep batch #: 0010113P

Prep procedure: N/A

Analysis procedure: NAREL GAM-01

Analyst: DPS

QC type: DUP

COUNTING INFORMATION

Date and time Duration (min) Detector ID Operator

10/17/2005 15:10 1000.0 GE02 DPS

ANALYTICAL RESULTS

Analyte Activity ± 2σ Uncertainty MDC Unit Date

Ba140

Be7

Bi212

Bi214

Co60

Cs137

I131

K40

Pb210

Pb212

Pb214

Ra223

Ra226

Ra228

Th234

Tl208

U235

*

*

*

*

*

ND

2.12e-01

2.79e-01

4.26e-01

ND

ND

ND

1.16e+00

ND

4.06e-01

5.25e-01

1.06e-01

1.07e+00

4.67e-01

5.20e-01

1.37e-01

6.74e-02

1.4e-01

2.6e-01

6.3e-02

3.6e-01

4.4e-02

5.5e-02

7.6e-02

3.7e-01

7.2e-02

2.6e-01

2.7e-02

2.3e-02

2.2e-01

4.8e-02

4.2e-02

7.1e-02

1.4e+00

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

PCI/GDRY

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated.
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES

SDG #0500068

QC BATCH SUMMARY

QC batch #: 0003917T

Preparation procedure: N/A

Analysis procedure: NAREL GAM-01

NAREL Sample # QC

Type Yield (%) ± 2σ Uncertainty (%) Analyst

A5.04982A

A5.04983B

A5.04984C

A5.04985D

A5.04985D DUP

N/A

N/A

N/A

N/A

N/A

DPS

DPS

DPS

DPS

DPS

* Samples marked with an asterisk are not in this sample delivery group but were analyzed with it for QC purposes.
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES

SDG #0500068

PREPARATION BATCH SUMMARY

SAMPLES ANALYZED

NAREL

Sample #

QC

Type Aliquot Size Completion

Date Prep Batch

A5.04982A

A5.04983B

A5.04984C

A5.04985D

A5.04985D DUP

1.51e+02 GDRY

1.56e+02 GDRY

1.38e+02 GDRY

1.23e+02 GDRY

1.23e+02 GDRY

10/13/2005

10/14/2005

10/14/2005

10/14/2005

10/18/2005

0010113P

0010113P

0010113P

0010113P

0010113P

* Samples marked with an asterisk are not in this sample delivery group but were analyzed with it for QC purposes.
U.S. ENVIRONMENTAL PROTECTION AGENCY

NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES

SDG #0500068

DETECTOR REPORT

The following were used for samples in the SDG

GE02 10/17/2005 15:10 00495576K A5.04985D

GE13 10/13/2005 12:47 00495564F A5.04982A

GE13 10/13/2005 21:09 00495567J A5.04983B

GE13 10/14/2005 05:32 00495570D A5.04984C

GE13 10/14/2005 13:55 00495573G A5.04985D

The following were used for other samples in the QC batches

None found