Dolan Chemical Laboratory

4001 Bixby Road

Groveport, OH 43125

T: 614-836-4221, Audinet 210-4221

F: 614-836-4168, Audinet 210-4168

http://aepenv/labs

Water Analysis

Form REP-703

Rev. 0, 4/2012

Location: Mountaineer Plant Report Date: 8/7/2013

Sample Number: 132921-001 Date Collected: 07/17/2013 11:05 Date Received: 7/17/2013

 Primary Clarifier Effluent

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 3.71 ug/L 0.050 0.010 DPC 07/24/2013 11:48 EPA 200.8

Arsenic, As 3.64 ug/L 0.10 0.030 DPC 07/24/2013 11:48 EPA 200.8

Barium, Ba 92.3 ug/L 0.10 0.020 DPC 07/24/2013 11:48 EPA 200.8

Beryllium, Be < 1.0 ug/L U 5.0 1.0 DAM 07/31/2013 15:40 EPA 200.7

Cadmium, Cd 2.20 ug/L 0.050 0.010 DPC 07/24/2013 11:48 EPA 200.8

Chromium, Cr 5.6 ug/L 0.20 0.040 DPC 07/24/2013 11:48 EPA 200.8

Cobalt, Co 42.2 ug/L 0.020 0.0040 DPC 07/24/2013 11:48 EPA 200.8

Copper, Cu 2.66 ug/L 0.050 0.010 DPC 07/24/2013 11:48 EPA 200.8

Lead, Pb 1.08 ug/L 0.010 0.0020 DPC 07/24/2013 11:48 EPA 200.8

Mercury, Hg 668 ng/L 50 20 TLT 07/29/2013 EPA 1631E

Molybdenum, Mo 311 ug/L 0.050 0.010 DPC 07/24/2013 11:48 EPA 200.8

Nickel, Ni 465 ug/L 0.20 0.050 DPC 07/24/2013 11:48 EPA 200.8

Selenium, Se 309 ug/L 0.50 0.20 DPC 07/24/2013 11:48 EPA 200.8

Silver, Ag 0.014 ug/L 0.010 0.0020 DPC 07/24/2013 11:48 EPA 200.8

Thallium, Tl 3.50 ug/L 0.050 0.0020 DPC 07/24/2013 11:48 EPA 200.8

Tin, Sn < 10 ug/L U 50 10 DAM 07/31/2013 15:40 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 07/31/2013 15:40 EPA 200.7

Zinc, Zn 74.5 ug/L 0.50 0.10 DPC 07/24/2013 11:48 EPA 200.8

Aluminum, Al 0.396 mg/L 0.0010 0.0003 DPC 07/24/2013 11:48 EPA 200.8

Boron, B 329 mg/L 0.20 0.040 DAM 07/31/2013 15:40 EPA 200.7

Calcium, Ca 740 mg/L 0.20 0.040 DAM 07/31/2013 15:40 EPA 200.7

Iron, Fe 0.842 mg/L 0.50 0.10 DAM 07/31/2013 15:40 EPA 200.7

Magnesium, Mg 2690 mg/L 0.10 0.020 DAM 07/31/2013 15:40 EPA 200.7

Manganese, Mn 34.4 mg/L 0.0050 0.0010 DAM 07/31/2013 15:40 EPA 200.7

Potassium, K 53.0 mg/L 0.50 0.070 DAM 07/31/2013 15:38 EPA 200.7

Sodium, Na 263 mg/L 0.50 0.080 DAM 07/31/2013 15:38 EPA 200.7

Strontium, Sr 8.96 mg/L 0.010 0.0030 DAM 07/31/2013 15:38 EPA 200.7

Nitrate-Nitrite, NO3-NO2, as N 38.8 mg/L 0.10 0.020 DMM 07/22/2013 SM20 4500NO3 H

Mountaineer Plant, 132921 Page 1 of 10
Location: Mountaineer Plant Report Date: 8/7/2013

Sample Number: 132921-001A Date Collected: 07/17/2013 11:05 Date Received: 7/17/2013

 Primary Clarifier Effluent Dissolved

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 3.02 ug/L 0.050 0.010 DPC 07/24/2013 11:53 EPA 200.8

Arsenic, As 2.65 ug/L 0.10 0.030 DPC 07/24/2013 11:53 EPA 200.8

Barium, Ba 81.4 ug/L 0.10 0.020 DPC 07/24/2013 11:53 EPA 200.8

Beryllium, Be < 1.0 ug/L U 5.0 1.0 DAM 07/31/2013 16:27 EPA 200.7

Cadmium, Cd 1.28 ug/L 0.050 0.010 DPC 07/24/2013 11:53 EPA 200.8

Chromium, Cr 1.5 ug/L 0.20 0.040 DPC 07/24/2013 11:53 EPA 200.8

Cobalt, Co 40.0 ug/L 0.020 0.0040 DPC 07/24/2013 11:53 EPA 200.8

Copper, Cu 0.81 ug/L 0.050 0.010 DPC 07/24/2013 11:53 EPA 200.8

Lead, Pb 0.052 ug/L 0.010 0.0020 DPC 07/24/2013 11:53 EPA 200.8

Molybdenum, Mo 298 ug/L 0.050 0.010 DPC 07/24/2013 11:53 EPA 200.8

Nickel, Ni 446 ug/L 0.20 0.050 DPC 07/24/2013 11:53 EPA 200.8

Selenium, Se 292 ug/L 0.50 0.20 DPC 07/24/2013 11:53 EPA 200.8

Selenite, Se+4 (Hydride) 183 ug/L 20 4.0 TLT 08/05/2013 AEP Method

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 07/24/2013 11:53 EPA 200.8

Thallium, Tl 3.43 ug/L 0.050 0.0020 DPC 07/24/2013 11:53 EPA 200.8

Tin, Sn < 10 ug/L U 50 10 DAM 07/31/2013 16:28 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 07/31/2013 16:27 EPA 200.7

Zinc, Zn 60.2 ug/L 0.50 0.10 DPC 07/24/2013 11:53 EPA 200.8

Aluminum, Al 0.0337 mg/L 0.0010 0.0003 DPC 07/24/2013 11:53 EPA 200.8

Boron, B 325 mg/L 0.20 0.040 DAM 07/31/2013 16:27 EPA 200.7

Calcium, Ca 722 mg/L 0.20 0.040 DAM 07/31/2013 16:27 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 07/31/2013 16:28 EPA 200.7

Magnesium, Mg 2630 mg/L 0.10 0.020 DAM 07/31/2013 16:27 EPA 200.7

Manganese, Mn 33.7 mg/L 0.0050 0.0010 DAM 07/31/2013 16:27 EPA 200.7

Potassium, K 51.7 mg/L 0.50 0.070 DAM 07/31/2013 16:26 EPA 200.7

Sodium, Na 261 mg/L 0.50 0.080 DAM 07/31/2013 16:26 EPA 200.7

Strontium, Sr 8.76 mg/L 0.010 0.0030 DAM 07/31/2013 16:26 EPA 200.7

Mountaineer Plant, 132921 Page 2 of 10
Location: Mountaineer Plant Report Date: 8/7/2013

Sample Number: 132921-002 Date Collected: 07/17/2013 10:36 Date Received: 7/17/2013

CPS Effluent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 2.60 ug/L 0.050 0.010 DPC 07/24/2013 11:58 EPA 200.8

Arsenic, As 1.85 ug/L 0.10 0.030 DPC 07/24/2013 11:58 EPA 200.8

Barium, Ba 79.6 ug/L 0.10 0.020 DPC 07/24/2013 11:58 EPA 200.8

Beryllium, Be < 1.0 ug/L U 5.0 1.0 DAM 07/31/2013 16:03 EPA 200.7

Cadmium, Cd 0.30 ug/L 0.050 0.010 DPC 07/24/2013 11:58 EPA 200.8

Chromium, Cr 2.2 ug/L 0.20 0.040 DPC 07/24/2013 11:58 EPA 200.8

Cobalt, Co 5.10 ug/L 0.020 0.0040 DPC 07/24/2013 11:58 EPA 200.8

Copper, Cu 0.81 ug/L 0.050 0.010 DPC 07/24/2013 11:58 EPA 200.8

Lead, Pb 0.127 ug/L 0.010 0.0020 DPC 07/24/2013 11:58 EPA 200.8

Mercury, Hg 89.5 ng/L 20 8.0 TLT 07/29/2013 EPA 1631E

Molybdenum, Mo 275 ug/L 0.050 0.010 DPC 07/24/2013 11:58 EPA 200.8

Nickel, Ni 132 ug/L 0.20 0.050 DPC 07/24/2013 11:58 EPA 200.8

Selenium, Se 255 ug/L 0.50 0.20 DPC 07/24/2013 11:58 EPA 200.8

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 07/24/2013 11:58 EPA 200.8

Thallium, Tl 1.84 ug/L 0.050 0.0020 DPC 07/24/2013 11:58 EPA 200.8

Tin, Sn < 10 ug/L U 50 10 DAM 07/31/2013 16:03 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 07/31/2013 16:03 EPA 200.7

Zinc, Zn 13.5 ug/L 0.50 0.10 DPC 07/24/2013 11:58 EPA 200.8

Aluminum, Al 0.100 mg/L 0.0010 0.0003 DPC 07/24/2013 11:58 EPA 200.8

Boron, B 288 mg/L 0.20 0.040 DAM 07/31/2013 16:03 EPA 200.7

Calcium, Ca 649 mg/L 0.20 0.040 DAM 07/31/2013 16:03 EPA 200.7

Iron, Fe 0.523 mg/L 0.50 0.10 DAM 07/31/2013 16:03 EPA 200.7

Magnesium, Mg 2400 mg/L 0.10 0.020 DAM 07/31/2013 16:03 EPA 200.7

Manganese, Mn 27.3 mg/L 0.0050 0.0010 DAM 07/31/2013 16:03 EPA 200.7

Potassium, K 46.0 mg/L 0.50 0.070 DAM 07/31/2013 16:01 EPA 200.7

Sodium, Na 232 mg/L 0.50 0.080 DAM 07/31/2013 16:01 EPA 200.7

Strontium, Sr 7.93 mg/L 0.010 0.0030 DAM 07/31/2013 16:01 EPA 200.7

Nitrate-Nitrite, NO3-NO2, as N 33.7 mg/L 0.10 0.020 DMM 07/22/2013 SM20 4500NO3 H

Mountaineer Plant, 132921 Page 3 of 10
Location: Mountaineer Plant Report Date: 8/7/2013

Sample Number: 132921-002A Date Collected: 07/17/2013 10:36 Date Received: 7/17/2013

CPS Effluent Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 2.41 ug/L 0.050 0.010 DPC 07/24/2013 12:03 EPA 200.8

Arsenic, As 1.76 ug/L 0.10 0.030 DPC 07/24/2013 12:03 EPA 200.8

Barium, Ba 76.9 ug/L 0.10 0.020 DPC 07/24/2013 12:03 EPA 200.8

Beryllium, Be < 1.0 ug/L U 5.0 1.0 DAM 07/31/2013 16:36 EPA 200.7

Cadmium, Cd < 0.010 ug/L U 0.050 0.010 DPC 07/24/2013 12:03 EPA 200.8

Chromium, Cr 1.3 ug/L 0.20 0.040 DPC 07/24/2013 12:03 EPA 200.8

Cobalt, Co 3.76 ug/L 0.020 0.0040 DPC 07/24/2013 12:03 EPA 200.8

Copper, Cu 0.47 ug/L 0.050 0.010 DPC 07/24/2013 12:03 EPA 200.8

Lead, Pb 0.029 ug/L 0.010 0.0020 DPC 07/24/2013 12:03 EPA 200.8

Molybdenum, Mo 269 ug/L 0.050 0.010 DPC 07/24/2013 12:03 EPA 200.8

Nickel, Ni 115 ug/L 0.20 0.050 DPC 07/24/2013 12:03 EPA 200.8

Selenium, Se 245 ug/L 0.50 0.20 DPC 07/24/2013 12:03 EPA 200.8

Selenite, Se+4 (Hydride) 153 ug/L 20 4.0 TLT 08/05/2013 AEP Method

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 07/24/2013 12:03 EPA 200.8

Thallium, Tl 1.68 ug/L 0.050 0.0020 DPC 07/24/2013 12:03 EPA 200.8

Tin, Sn < 10 ug/L U 50 10 DAM 07/31/2013 16:36 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 07/31/2013 16:36 EPA 200.7

Zinc, Zn 9.2 ug/L 0.50 0.10 DPC 07/24/2013 12:03 EPA 200.8

Aluminum, Al 0.0204 mg/L 0.0010 0.0003 DPC 07/24/2013 12:03 EPA 200.8

Boron, B 288 mg/L 0.20 0.040 DAM 07/31/2013 16:36 EPA 200.7

Calcium, Ca 649 mg/L 0.20 0.040 DAM 07/31/2013 16:36 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 07/31/2013 16:36 EPA 200.7

Magnesium, Mg 2370 mg/L 0.10 0.020 DAM 07/31/2013 16:36 EPA 200.7

Manganese, Mn 27.2 mg/L 0.0050 0.0010 DAM 07/31/2013 16:36 EPA 200.7

Potassium, K 46.0 mg/L 0.50 0.070 DAM 07/31/2013 16:34 EPA 200.7

Sodium, Na 231 mg/L 0.50 0.080 DAM 07/31/2013 16:34 EPA 200.7

Strontium, Sr 7.95 mg/L 0.010 0.0030 DAM 07/31/2013 16:34 EPA 200.7

Mountaineer Plant, 132921 Page 4 of 10
Location: Mountaineer Plant Report Date: 8/7/2013

Sample Number: 132921-003 Date Collected: 07/17/2013 10:52 Date Received: 7/17/2013

 Landfill Leachate

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 9.60 ug/L 0.050 0.010 DPC 07/24/2013 12:07 EPA 200.8

Arsenic, As 40.1 ug/L 0.10 0.030 DPC 07/24/2013 12:07 EPA 200.8

Barium, Ba 37.1 ug/L 0.10 0.020 DPC 07/24/2013 12:07 EPA 200.8

Beryllium, Be < 1.0 ug/L U 5.0 1.0 DAM 07/31/2013 16:11 EPA 200.7

Cadmium, Cd 0.10 ug/L 0.050 0.010 DPC 07/24/2013 12:07 EPA 200.8

Chromium, Cr 0.7 ug/L 0.20 0.040 DPC 07/24/2013 12:07 EPA 200.8

Cobalt, Co 3.03 ug/L 0.020 0.0040 DPC 07/24/2013 12:07 EPA 200.8

Copper, Cu 0.88 ug/L 0.050 0.010 DPC 07/24/2013 12:07 EPA 200.8

Lead, Pb 0.063 ug/L 0.010 0.0020 DPC 07/24/2013 12:07 EPA 200.8

Mercury, Hg 62.8 ng/L 10 4.0 TLT 07/29/2013 EPA 1631E

Molybdenum, Mo 5550 ug/L 0.050 0.010 DPC 07/24/2013 12:07 EPA 200.8

Nickel, Ni 11.1 ug/L 0.20 0.050 DPC 07/24/2013 12:07 EPA 200.8

Selenium, Se 198 ug/L 0.50 0.20 DPC 07/24/2013 12:07 EPA 200.8

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 07/24/2013 12:07 EPA 200.8

Thallium, Tl 1.98 ug/L 0.050 0.0020 DPC 07/24/2013 12:07 EPA 200.8

Tin, Sn < 10 ug/L U 50 10 DAM 07/31/2013 16:12 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 07/31/2013 16:11 EPA 200.7

Zinc, Zn 3.6 ug/L 0.50 0.10 DPC 07/24/2013 12:07 EPA 200.8

Aluminum, Al 0.0203 mg/L 0.0010 0.0003 DPC 07/24/2013 12:07 EPA 200.8

Boron, B 43.9 mg/L 0.20 0.040 DAM 07/31/2013 16:11 EPA 200.7

Calcium, Ca 365 mg/L 0.20 0.040 DAM 07/31/2013 16:11 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 07/31/2013 16:12 EPA 200.7

Magnesium, Mg 340 mg/L 0.10 0.020 DAM 07/31/2013 16:11 EPA 200.7

Manganese, Mn 1.76 mg/L 0.0050 0.0010 DAM 07/31/2013 16:11 EPA 200.7

Potassium, K 87.8 mg/L 0.50 0.070 DAM 07/31/2013 16:10 EPA 200.7

Sodium, Na 1440 mg/L 0.50 0.080 DAM 07/31/2013 16:10 EPA 200.7

Strontium, Sr 4.60 mg/L 0.010 0.0030 DAM 07/31/2013 16:10 EPA 200.7

Nitrate-Nitrite, NO3-NO2, as N 31.5 mg/L 0.10 0.020 DMM 07/22/2013 SM20 4500NO3 H

Mountaineer Plant, 132921 Page 5 of 10
Location: Mountaineer Plant Report Date: 8/7/2013

Sample Number: 132921-003A Date Collected: 07/17/2013 10:52 Date Received: 7/17/2013

 Landfill Leachate Dissolved

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 8.73 ug/L 0.050 0.010 DPC 07/24/2013 12:12 EPA 200.8

Arsenic, As 35.6 ug/L 0.10 0.030 DPC 07/24/2013 12:12 EPA 200.8

Barium, Ba 34.3 ug/L 0.10 0.020 DPC 07/24/2013 12:12 EPA 200.8

Beryllium, Be < 1.0 ug/L U 5.0 1.0 DAM 07/31/2013 16:44 EPA 200.7

Cadmium, Cd 0.09 ug/L 0.050 0.010 DPC 07/24/2013 12:12 EPA 200.8

Chromium, Cr 0.3 ug/L 0.20 0.040 DPC 07/24/2013 12:12 EPA 200.8

Cobalt, Co 2.30 ug/L 0.020 0.0040 DPC 07/24/2013 12:12 EPA 200.8

Copper, Cu 0.34 ug/L 0.050 0.010 DPC 07/24/2013 12:12 EPA 200.8

Lead, Pb 0.021 ug/L 0.010 0.0020 DPC 07/24/2013 12:12 EPA 200.8

Molybdenum, Mo 5150 ug/L 0.050 0.010 DPC 07/24/2013 12:12 EPA 200.8

Nickel, Ni 9.66 ug/L 0.20 0.050 DPC 07/24/2013 12:12 EPA 200.8

Selenium, Se 157 ug/L 0.50 0.20 DPC 07/24/2013 12:12 EPA 200.8

Selenite, Se+4 (Hydride) 71.8 ug/L 20 4.0 TLT 08/05/2013 AEP Method

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 07/24/2013 12:12 EPA 200.8

Thallium, Tl 1.81 ug/L 0.050 0.0020 DPC 07/24/2013 12:12 EPA 200.8

Tin, Sn < 10 ug/L U 50 10 DAM 07/31/2013 16:45 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 07/31/2013 16:44 EPA 200.7

Zinc, Zn 3.9 ug/L 0.50 0.10 DPC 07/24/2013 12:12 EPA 200.8

Aluminum, Al 0.0055 mg/L 0.0010 0.0003 DPC 07/24/2013 12:12 EPA 200.8

Boron, B 43.7 mg/L 0.20 0.040 DAM 07/31/2013 16:44 EPA 200.7

Calcium, Ca 363 mg/L 0.20 0.040 DAM 07/31/2013 16:44 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 07/31/2013 16:45 EPA 200.7

Magnesium, Mg 337 mg/L 0.10 0.020 DAM 07/31/2013 16:44 EPA 200.7

Manganese, Mn 1.71 mg/L 0.0050 0.0010 DAM 07/31/2013 16:44 EPA 200.7

Potassium, K 87.8 mg/L 0.50 0.070 DAM 07/31/2013 16:43 EPA 200.7

Sodium, Na 1440 mg/L 0.50 0.080 DAM 07/31/2013 16:43 EPA 200.7

Strontium, Sr 4.60 mg/L 0.010 0.0030 DAM 07/31/2013 16:43 EPA 200.7

Mountaineer Plant, 132921 Page 6 of 10
Location: Mountaineer Plant Report Date: 8/7/2013

Sample Number: 132921-004 Date Collected: 07/17/2013 10:49 Date Received: 7/17/2013

1st Stage Feed 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 5.41 ug/L 0.050 0.010 DPC 07/24/2013 12:17 EPA 200.8

Arsenic, As 16.8 ug/L 0.10 0.030 DPC 07/24/2013 12:17 EPA 200.8

Barium, Ba 65.3 ug/L 0.10 0.020 DPC 07/24/2013 12:17 EPA 200.8

Beryllium, Be < 1.0 ug/L U 5.0 1.0 DAM 07/31/2013 16:15 EPA 200.7

Cadmium, Cd 0.48 ug/L 0.050 0.010 DPC 07/24/2013 12:17 EPA 200.8

Chromium, Cr 2.5 ug/L 0.20 0.040 DPC 07/24/2013 12:17 EPA 200.8

Cobalt, Co 5.90 ug/L 0.020 0.0040 DPC 07/24/2013 12:17 EPA 200.8

Copper, Cu 1.25 ug/L 0.050 0.010 DPC 07/24/2013 12:17 EPA 200.8

Lead, Pb 0.211 ug/L 0.010 0.0020 DPC 07/24/2013 12:17 EPA 200.8

Mercury, Hg 137 ng/L 10 4.0 TLT 07/29/2013 EPA 1631E

Molybdenum, Mo 2280 ug/L 0.050 0.010 DPC 07/24/2013 12:17 EPA 200.8

Nickel, Ni 109 ug/L 0.20 0.050 DPC 07/24/2013 12:17 EPA 200.8

Selenium, Se 245 ug/L 0.50 0.20 DPC 07/24/2013 12:17 EPA 200.8

Silver, Ag 0.0020 ug/L J 0.010 0.0020 DPC 07/24/2013 12:17 EPA 200.8

Thallium, Tl 2.13 ug/L 0.050 0.0020 DPC 07/24/2013 12:17 EPA 200.8

Tin, Sn < 10 ug/L U 50 10 DAM 07/31/2013 16:15 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 07/31/2013 16:15 EPA 200.7

Zinc, Zn 15.6 ug/L 0.50 0.10 DPC 07/24/2013 12:17 EPA 200.8

Aluminum, Al 0.143 mg/L 0.0010 0.0003 DPC 07/24/2013 12:17 EPA 200.8

Boron, B 201 mg/L 0.20 0.040 DAM 07/31/2013 16:15 EPA 200.7

Calcium, Ca 549 mg/L 0.20 0.040 DAM 07/31/2013 16:15 EPA 200.7

Iron, Fe 0.825 mg/L 0.50 0.10 DAM 07/31/2013 16:15 EPA 200.7

Magnesium, Mg 1610 mg/L 0.10 0.020 DAM 07/31/2013 16:15 EPA 200.7

Manganese, Mn 18.1 mg/L 0.0050 0.0010 DAM 07/31/2013 16:15 EPA 200.7

Potassium, K 62.3 mg/L 0.50 0.070 DAM 07/31/2013 16:13 EPA 200.7

Sodium, Na 701 mg/L 0.50 0.080 DAM 07/31/2013 16:13 EPA 200.7

Strontium, Sr 6.70 mg/L 0.010 0.0030 DAM 07/31/2013 16:13 EPA 200.7

Nitrate-Nitrite, NO3-NO2, as N 23.3 mg/L 0.10 0.020 DMM 07/22/2013 SM20 4500NO3 H

Mountaineer Plant, 132921 Page 7 of 10
Location: Mountaineer Plant Report Date: 8/7/2013

Sample Number: 132921-004A Date Collected: 07/17/2013 10:49 Date Received: 7/17/2013

1st Stage Feed Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 4.77 ug/L 0.050 0.010 DPC 07/24/2013 12:22 EPA 200.8

Arsenic, As 14.3 ug/L 0.10 0.030 DPC 07/24/2013 12:22 EPA 200.8

Barium, Ba 59.4 ug/L 0.10 0.020 DPC 07/24/2013 12:22 EPA 200.8

Beryllium, Be < 1.0 ug/L U 5.0 1.0 DAM 07/31/2013 16:48 EPA 200.7

Cadmium, Cd < 0.010 ug/L U 0.050 0.010 DPC 07/24/2013 12:22 EPA 200.8

Chromium, Cr 0.8 ug/L 0.20 0.040 DPC 07/24/2013 12:22 EPA 200.8

Cobalt, Co 3.41 ug/L 0.020 0.0040 DPC 07/24/2013 12:22 EPA 200.8

Copper, Cu 0.45 ug/L 0.050 0.010 DPC 07/24/2013 12:22 EPA 200.8

Lead, Pb 0.021 ug/L 0.010 0.0020 DPC 07/24/2013 12:22 EPA 200.8

Molybdenum, Mo 2220 ug/L 0.050 0.010 DPC 07/24/2013 12:22 EPA 200.8

Nickel, Ni 79.9 ug/L 0.20 0.050 DPC 07/24/2013 12:22 EPA 200.8

Selenium, Se 214 ug/L 0.50 0.20 DPC 07/24/2013 12:22 EPA 200.8

Selenite, Se+4 (Hydride) 119 ug/L 20 4.0 TLT 08/05/2013 AEP Method

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 07/24/2013 12:22 EPA 200.8

Thallium, Tl 1.81 ug/L 0.050 0.0020 DPC 07/24/2013 12:22 EPA 200.8

Tin, Sn < 10 ug/L U 50 10 DAM 07/31/2013 16:48 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 07/31/2013 16:48 EPA 200.7

Zinc, Zn 7.7 ug/L 0.50 0.10 DPC 07/24/2013 12:22 EPA 200.8

Aluminum, Al 0.0144 mg/L 0.0010 0.0003 DPC 07/24/2013 12:22 EPA 200.8

Boron, B 189 mg/L 0.20 0.040 DAM 07/31/2013 16:48 EPA 200.7

Calcium, Ca 528 mg/L 0.20 0.040 DAM 07/31/2013 16:48 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 07/31/2013 16:48 EPA 200.7

Magnesium, Mg 1520 mg/L 0.10 0.020 DAM 07/31/2013 16:48 EPA 200.7

Manganese, Mn 16.9 mg/L 0.0050 0.0010 DAM 07/31/2013 16:48 EPA 200.7

Potassium, K 61.0 mg/L 0.50 0.070 DAM 07/31/2013 16:46 EPA 200.7

Sodium, Na 692 mg/L 0.50 0.080 DAM 07/31/2013 16:46 EPA 200.7

Strontium, Sr 6.37 mg/L 0.010 0.0030 DAM 07/31/2013 16:46 EPA 200.7

Mountaineer Plant, 132921 Page 8 of 10
Location: Mountaineer Plant Report Date: 8/7/2013

Sample Number: 132921-005 Date Collected: 07/17/2013 10:44 Date Received: 7/17/2013

Bioreactor Effluent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 0.12 ug/L 0.050 0.010 DPC 07/24/2013 12:27 EPA 200.8

Arsenic, As 0.57 ug/L 0.10 0.030 DPC 07/24/2013 12:27 EPA 200.8

Barium, Ba 80.5 ug/L 0.10 0.020 DPC 07/24/2013 12:27 EPA 200.8

Beryllium, Be < 1.0 ug/L U 5.0 1.0 DAM 07/31/2013 16:24 EPA 200.7

Cadmium, Cd < 0.010 ug/L U 0.050 0.010 DPC 07/24/2013 12:27 EPA 200.8

Chromium, Cr 2.1 ug/L 0.20 0.040 DPC 07/24/2013 12:27 EPA 200.8

Cobalt, Co 0.051 ug/L 0.020 0.0040 DPC 07/24/2013 12:27 EPA 200.8

Copper, Cu 0.40 ug/L 0.050 0.010 DPC 07/24/2013 12:27 EPA 200.8

Lead, Pb 0.020 ug/L 0.010 0.0020 DPC 07/24/2013 12:27 EPA 200.8

Mercury, Hg 5.6 ng/L 1.0 0.40 TLT 07/29/2013 EPA 1631E

Molybdenum, Mo 7.33 ug/L 0.050 0.010 DPC 07/24/2013 12:27 EPA 200.8

Nickel, Ni 2.18 ug/L 0.20 0.050 DPC 07/24/2013 12:27 EPA 200.8

Selenium, Se 2.2 ug/L 0.50 0.20 DPC 07/24/2013 12:27 EPA 200.8

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 07/24/2013 12:27 EPA 200.8

Thallium, Tl 0.0090 ug/L J 0.050 0.0020 DPC 07/24/2013 12:27 EPA 200.8

Tin, Sn < 10 ug/L U 50 10 DAM 07/31/2013 16:24 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 07/31/2013 16:24 EPA 200.7

Zinc, Zn 1.3 ug/L 0.50 0.10 DPC 07/24/2013 12:27 EPA 200.8

Aluminum, Al 3.76 mg/L 0.0010 0.0003 DPC 07/24/2013 12:27 EPA 200.8

Boron, B 179 mg/L 0.20 0.040 DAM 07/31/2013 16:24 EPA 200.7

Calcium, Ca 553 mg/L 0.20 0.040 DAM 07/31/2013 16:24 EPA 200.7

Iron, Fe 1.01 mg/L 0.50 0.10 DAM 07/31/2013 16:24 EPA 200.7

Magnesium, Mg 1480 mg/L 0.10 0.020 DAM 07/31/2013 16:24 EPA 200.7

Manganese, Mn 13.3 mg/L 0.0050 0.0010 DAM 07/31/2013 16:24 EPA 200.7

Potassium, K 59.1 mg/L 0.50 0.070 DAM 07/31/2013 16:22 EPA 200.7

Sodium, Na 682 mg/L 0.50 0.080 DAM 07/31/2013 16:22 EPA 200.7

Strontium, Sr 6.59 mg/L 0.010 0.0030 DAM 07/31/2013 16:22 EPA 200.7

Nitrate-Nitrite, NO3-NO2, as N 1.66 mg/L 0.10 0.020 DMM 07/22/2013 SM20 4500NO3 H

Mountaineer Plant, 132921 Page 9 of 10
Location: Mountaineer Plant Report Date: 8/7/2013

Sample Number: 132921-005A Date Collected: 07/17/2013 10:44 Date Received: 7/17/2013

Bioreactor Effluent Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 0.07 ug/L 0.050 0.010 DPC 07/24/2013 12:31 EPA 200.8

Arsenic, As 0.51 ug/L 0.10 0.030 DPC 07/24/2013 12:31 EPA 200.8

Barium, Ba 72.4 ug/L 0.10 0.020 DPC 07/24/2013 12:31 EPA 200.8

Beryllium, Be < 1.0 ug/L U 5.0 1.0 DAM 07/31/2013 16:52 EPA 200.7

Cadmium, Cd < 0.010 ug/L U 0.050 0.010 DPC 07/24/2013 12:31 EPA 200.8

Chromium, Cr 1.8 ug/L 0.20 0.040 DPC 07/24/2013 12:31 EPA 200.8

Cobalt, Co 0.051 ug/L 0.020 0.0040 DPC 07/24/2013 12:31 EPA 200.8

Copper, Cu 0.12 ug/L 0.050 0.010 DPC 07/24/2013 12:31 EPA 200.8

Lead, Pb 0.0070 ug/L J 0.010 0.0020 DPC 07/24/2013 12:31 EPA 200.8

Molybdenum, Mo 5.38 ug/L 0.050 0.010 DPC 07/24/2013 12:31 EPA 200.8

Nickel, Ni 2.08 ug/L 0.20 0.050 DPC 07/24/2013 12:31 EPA 200.8

Selenium, Se 2.0 ug/L 0.50 0.20 DPC 07/24/2013 12:31 EPA 200.8

Selenite, Se+4 (Hydride) < 0.080 ug/L U 0.40 0.080 TLT 08/05/2013 AEP Method

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 07/24/2013 12:31 EPA 200.8

Thallium, Tl 0.0020 ug/L J 0.050 0.0020 DPC 07/24/2013 12:31 EPA 200.8

Tin, Sn < 10 ug/L U 50 10 DAM 07/31/2013 16:52 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 07/31/2013 16:52 EPA 200.7

Zinc, Zn 2.8 ug/L 0.50 0.10 DPC 07/24/2013 12:31 EPA 200.8

Aluminum, Al 3.29 mg/L 0.0010 0.0003 DPC 07/24/2013 12:31 EPA 200.8

Boron, B 176 mg/L 0.20 0.040 DAM 07/31/2013 16:51 EPA 200.7

Calcium, Ca 531 mg/L 0.20 0.040 DAM 07/31/2013 16:51 EPA 200.7

Iron, Fe 0.924 mg/L 0.50 0.10 DAM 07/31/2013 16:52 EPA 200.7

Magnesium, Mg 1430 mg/L 0.10 0.020 DAM 07/31/2013 16:51 EPA 200.7

Manganese, Mn 12.9 mg/L 0.0050 0.0010 DAM 07/31/2013 16:51 EPA 200.7

Potassium, K 59.0 mg/L 0.50 0.070 DAM 07/31/2013 16:50 EPA 200.7

Sodium, Na 680 mg/L 0.50 0.080 DAM 07/31/2013 16:50 EPA 200.7

Strontium, Sr 6.45 mg/L 0.010 0.0030 DAM 07/31/2013 16:50 EPA 200.7

Sample Number: 132921-006 Date Collected: 07/17/2013 10:53 Date Received: 7/17/2013

Field Blank 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Mercury, Hg 0.28 ng/L J 0.50 0.20 TLT 07/29/2013 EPA 1631E

THIS TEST REPORT RELATES ONLY TO THE ITEMS TESTED AND SHALL NOT BE REPRODUCED EXCEPT IN FULL WITHOUT WRITTEN 

APPROVAL OF THE LABORATORY. ALL TEST RESULTS MEET ALL OF THE REQUIREMENTS OF THE ACCREDITING AUTHORITY, 

UNLESS OTHERWISE NOTED.

U: Analyte was analyzed and not detected at or above adjusted Method Detection Limit

J: Analyte was positively identified, though the quantitation was below Reporting Limit.

Brian Snyder, Chemist II

Email bssnyder@aep.com Tel. 614-836-4224

Fax 614-836-4168 Audinet 210-4224

Mountaineer Plant, 132921 Page 10 of 10