### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.
1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected
more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of
measure.

### Information
This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

892 Hennepin Power Station 1_2 

### subbituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte



### 892 Hennepin Power Station

1_2 As Received Higher Heating Value 

### 892 Hennepin Power Station

1_2 As Received % Moisture 

### 892 Hennepin Power Station

1_2 As Received % Ash 

### 892 Hennepin Power Station

1_2 As Received % Sulfur 

### 892 Hennepin Power Station

1_2 Dry

basis Higher Heating Value 

### 892 Hennepin Power Station

1_2 Dry

basis % Ash 

### 892 Hennepin Power Station

1_2 Dry

basis % Sulfur 

### 892 Hennepin Power Station

1_2 Dry

basis Antim ony 

### 892 Hennepin Power Station

1_2 Dry

basis Arsenic 

### 892 Hennepin Power Station

1_2 Dry

basis Bery llium 

### 892 Hennepin Power Station

1_2 Dry

basis Cadmium 

### 892 Hennepin Power Station

1_2 Dry

basis Chlorine 

### 892 Hennepin Power Station

1_2 Dry

basis Chromium 

### 892 Hennepin Power Station

1_2 Dry

basis Cobalt 

### 892 Hennepin Power Station

1_2 Dry

basis Fluorine 

### 892 Hennepin Power Station

1_2 Dry

basis Lead 

### 892 Hennepin Power Station

1_2 Dry

basis Manganese 

### 892 Hennepin Power Station

1_2 Dry

basis Mercury 

### 892 Hennepin Power Station

1_2 Dry

basis Nickel 

### 892 Hennepin Power Station

1_2 Dry

basis SeleniumAn alysis M ethod for each A nalyte

(example: ASTM D5865-04) 

### ASTM D5865 ASTM D3302 ASTM D3174 ASTM D4239B ASTM D5865 ASTM D3174 ASTM D4239B ASTM D6357 ASTM D6357 ASTM D6357 ASTM D6357 ASTM D6721 ASTM D6357 ASTM D6357 ASTM D5987 ASTM D6357 ASTM D6357 ASTM D6722-01 ASTM D6357 ASTM D4606EIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 892 Hennepin Power Station 1_2 Dioxin/furan HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Run 1 

### 4/13/2010 4/13/2010 8698.00 Btu/lb Run 2 4/14/2010 4/14/2010 8684.00 Btu/lb Run 3 4/15/2010 4/15/2010 8679.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 28.65 4.53 0.29 12190 Btu/lb 6.35 0.40 28.67 4.51 0.26 12174 Btu/lb 6.32 0.37 28.37 4.95 0.29 12116 Btu/lb 6.91 0.41Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis) 

### 20 ppm 0.076 μg/g 0.13 μg/g 1.0 μg/g 0.2 14 ppm 0.094 μg/g 0.12 μg/g 1.4 μg/g 0.2 16 ppm 0.084 μg/g 0.15 μg/g 1.3 μg/g 0.2Bery llium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### μg/g 0.06 μg/g 4 μg/g 2.0 μg/g 11 μg/g μg/g 0.06 μg/g 4 μg/g 2.2 μg/g 10 μg/g μg/g 0.09 μg/g 5 μg/g 2.3 μg/g 12 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 4 μg/g 0.7 μg/g 61 ppm 1.9 μg/g 4 μg/g 0.6 μg/g 62 ppm 1.9 μg/g 4 μg/g 0.9 μg/g 64 ppm 1.8 μg/g Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 

### 43.77 6.35 49.88 70.50 4.96 0.90 0.40 42.82 6.32 50.86 70.11 4.91 0.89 0.37 42.49 6.91 50.60 69.48 4.96 0.89 0.41 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen



### 16.89 17.40 17.35EIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 892 Hennepin Power Station 1_2 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units Run 1 

### 8/24/2010 8/25/2010 8357 Btu/lb Run 2 8/25/2010 8/25/2010 8563 Btu/lb Run 3 8/25/2010 8/25/2010 8609 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 29.88 5.70 0.21 11918 Btu/lb 8.13 0.30 29.10 4.91 0.21 12078 Btu/lb 6.92 0.30 28.53 5.18 0.23 12046 Btu/lb 7.25 0.32Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis) 

### 16 ppm 0.080 μg/g 0.15 μg/g 1.5 μg/g 0.3 11 ppm 0.073 μg/g 0.15 μg/g 1.6 μg/g 0.3 15 ppm 0.086 μg/g 0.15 μg/g 1.5 μg/g 0.3Bery llium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### μg/g 0.10 μg/g 7 μg/g 2.8 μg/g 12 μg/g μg/g 0.08 μg/g 6 μg/g 2.4 μg/g 11 μg/g μg/g 0.11 μg/g 6 μg/g 2.6 μg/g 14 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 

### 6 μg/g 0.7 μg/g 82 ppm 2.3 μg/g 6 μg/g 0.7 μg/g 68 ppm 2.6 μg/g 6 μg/g 0.6 μg/g 74 ppm 2.6 μg/gNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur



### 42.86 8.13 49.01 68.38 4.62 0.83 0.30 44.02 6.92 49.06 69.22 4.63 0.82 0.30 43.70 7.25 49.05 68.88 4.61 0.83 0.32 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 

### 17.74 18.11 18.11EIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 892 Hennepin Power Station 1_2

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis)Bery llium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 892 Hennepin Power Station 1_2

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis)Bery llium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals sy nfuel mg /g petroleum coke μg/g other mg /KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm