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.. Field Sheets and Calculations 

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VES 003200 
. . ( .. . 

Week of August 11, 2008 

VES 003201 
( ... 

. · • 

veoua EST< 

FIXed Hearth Incinerator 12 

Method 2 Parameters 

Run No. . 1 2 3 

-

in. Ha 0.1137 0~. O.f127 ~ 

- 0.1172 ,;-. ~ 

Avn llolbH · 

OOM t Factor 

{) 

VES 003202 
< m 

(/) 

§ 

0 

w 

(' 

., (1 -'\ ·' 

·~- cl29 

RUN I AVGS - MJ:TALS RUNl AVGS-1 

PT I O.P I $CRT I OOM. J OGM I O...H IIT,tQ( I OlbP 

o.bP__ tf . OUT . ___ · . lQW . :=p I o:' I:;; """'"I STACK 

,.... 

.1 I o.1s I o.3813 I 89 I 87 I 1. 8 !8! 

o1 I 0.18 I o.AOOO I aa I 87 I 1• • * o2 I o.1e I O.lUl I n I 88 I ' ' Me 

.. I 0.18 I O.AOOO I .. I &9 I 1.70 I S01 I 0.18 I O.AOOO I 18 I 80 I I. 388 

I··• I o.14_l_0.3742 I 06 I 90 I uo I >!18_ I o.t4 I o.o742 I ee _l ~ I_ t.eo 387 

-.. I o.t4 I u1•2 I as I 90 I t.oo I 3e8 I o.t5 I o.oe73 I 87 I so I t.eo ... .. I o.t8 To.4ooo I ..--1 eo TI.7013Gi I o:to I oAOoo I IJii I a2 I 1.10 

"' I o.ts I OAOOO I ee I at I 1.70 I 381 I 0.18 I 0.4000 I ee I 11 I t .70 

.. I o.14 I 0.3742 I M I 91 I 1.80 I aea a o;ts I o.387s I 90 I 82 I uo 

RUN3 AVGS-1 

...... :I _ c:J: ~ 

O.U73 

~ 

I o.to I 11.4000 

I o.t5 I 0,3873 __ 

I o.t2 I o.!l4ac 

o.is I o.3 

82 17 

go 88 

97 89 

-H 

1. 

,, 

1.• 

1.70 

.1

1.3 

STACK 

19.1' 

357 

359 

e6 O.t4 0.3742 07 92 1.&0 - 380 0.16 0.4000 88 82 1.70 370 0.18 0.4000 102 514 1.70 36e 

.. 0.14 0.3742 W 92 1.50 '370 0.18 0,0000 90 83 1.70 371 0.13 0.3808 103 9S MO 358 

.a O.t& 0.3173 It 9S ' t.80 3et 0.15 0.3873 • 82 1AO 370 0.13 0..3808 103 Q5 tAO 357 

•1 o.ts 0.3873 01 .. t.eo * o.1e o.AOOO 88 8:3 t .70 370 0.15 0.3813 too 118 t.ao 352 

., 0.18 0.3873 88 .. 1.60 :leo 0.17 0..123 88 83 1.90 371 -0.15 0.3813 ••• · - • - ·-

b2 O.te 0.4000 aG 9oC 1.70 380 0.17 0 ... 123 88 a. 1.00 372 0.15 0.3373 102 D7 1,60 356 

~ 0.18 0.4000 101 $16 1.70 HI 0.17 OA123 to 85 1.80 312 0.15 0.3873 103 88 1.SU 358 

~~a o.ts o.3873 101 lil6 t.to . 370 o..ts 0..3173 t1 ss t.eo an o.ts ·o.sen 106 te t.eo ssa 

.. 0.15 G.387! 101 98 1.60 370 0.15 0.3873 01 8$ uo 372 0.15 0.3873 106 99 1.80 358 

.. 0.15 G.3873 102 t7 1.80 371 0.18 OAOOO 92 88 1.70 372 0.16 0.3873 106 98 1.80 358 

.. o.t8 G.3873 103 97 1.eo 372 o.t& o.-.ooo 12 ae 1.10 sn o.t& o.ws toe ee uo 380 

ae o.t• 0.3742 tOi se 1.50 nt o.t5 0..3873 tf ar uo n• 0.3805 101 too tAO sst 

0.3742 ee 372 o.soae 360 

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ENSR I. AECOM 

I(FHBS...._Ot.lUiq .. w..t ..... Cli:ICniCI 

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Molti-Metalo lllallk C«r«lloa 

PIIOiffiiAll 

KFRI> 11711la lhn -i.e ..... rofJJ,7l Norlbe ._.,wllae~ nm orS9,ot1RS . 

• • v*e wed tor bflllll ~- (~ .-.;CIII a 3S4·1ia.fiii..-A 

MERa1RY1 

- - ,. .. 

.._,.IVU Ul ... , 

BACKllALf IO.It 0.09 

(I Fa it,. .. ~ ... e~. .... ,. ..WU.QCIOII'OCl 

ltFB It ,. Ill u. 111M lf'MIIC' ol elllllu 6 Ill or '% tdlH 

.... 

.... o.u .... us 80.89 

( )Noe Dellctcd ~t~Liolit 

• 1114k:wf ..._ ..S Cor bW' eom:cioa 

~ 

li'BKIIt)Q ... <-1 !llle..w.c,_BH8.,.,._1oc:wmtd 

tfiiHB II > l H ... ctr. VCih=' ot tllhr I N " "' ofBH 

( )l"oo I atporM.b&o ~ Utnk 

CLIENT: Voollia ES Tecbko!Solutlono 

PROGRAM: Uolt J 

RUN NO. R1 

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< m 

(/) 

0 

0 

w 

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0 

(11 

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ENSR I 1\ECOM 

0 

ltfatfi..Melall Blank Corrtd:lon 

noHT HALl' a.r.CK HAI.If 

IWiilllll "" fll c.c.nc..! o.&aM: "' fll Oxnclt4 Sap~~ fld. Blt Vtfte (•) ~ hoc: &If s-par f14 Bllt V.... s...,k s.ct Hfllt 

... ~~· .. " • • ~ u - •• •• -"'-

SI1"ff'CM\ 0.00 0.00 IU8 - 0.00 t .OO 0.00 1.00 ·• Q.OO UO 

Ahl.-j .. _M_ 0. 0.00 ).18 - 0.00 0.00 1.00 - t..OO 

t:~A~-~o{/~A>~;:::t:~IO~.lO~::t:~O~A~·~ I ·11 QJII 9.$2 IM 0.10 " JJ.IO O.QJ o.Ui lUI f- G.OD d.CO 11.'11 - 11.00 OJID O.CO 1.00 - 1101 UD 

a.yii~ (Bt_) IUS O..OS • •111 llCl OJO 0JU OJJ • 1.00 0.01 .01 l.ll 

c.-a.~ l.ll O.OJ • 1),11 0.11 2.06 O.Q) 0.8l • 1.00 0.00 l.ff 

c.MII Co 0.00 0.00 1!.71 - 0.00 0.00 t.OO 1.80 - 0.00 t.OO I 

CtwMWtn (Cf) 76.00 US • 1).?1 UO 1.US _9.._1) OA2 " 1.00 G.04 M 'HM ! 

-"-•lC.l 0.00 00 1).11 - o.oo _MO 0.00 1.00 - 0.'!11 ... :n} 0..00 0..03 11.71 - 0.00 t.m Q.OO 1.00 - 0.00 G.tl 

lfiCibl Of!) 0.00 O.Ol 11.11 - 0.00 UO 0..00 1.00 - 0.00 Ul 

..... (P l6UO CUl • 11.11 l l..S J&l.11 • I.S1' 0.1<4 • 1,00 Q.OJ QA,) MJ.l1 

1.01 o.oo 11.11 - o.oo t.oo llOO t .• co - o.oo ...., 

Sdnl111n 

,.., O.DO 0. 0.00 0.00 l).,,. 11 -- 0.00 0.00 0.00 0,00 G.OO 1.00 I.CO •• ... ==o

~O.OO~= . =~t.IO~~ V-.dtMn 0.00 0.00 IU - 0.00 0,00 G.OO I.CKI - 0.00 1.01 

lJM(.tl.) 0.00 0.00 lU I - 0.00 0.00 0.00 LOO - O.GCI 1M 

!fFTIB i1 .. ,.... 0 1Dil.71 .... w.t ...a.., CICMftld 

JtfHB > tl.71 p.a lkft ... m. .,.....,ott:ua ,., or h a..cr "-'-~ "FHB « " ' orms. 

• • nho liNd &'!It Wek comclion (•) • btatd on • U 4 • ia. flttcf ._ 

MUCUaV1 

flOHT HAI.I' 2.97 0.1)1 • 

lffBII>Ollllil"""lllllil::l:l .... fl ... toCIQIOOCt 

liFBII>fq._ikpMCu~.-.flll.otS"'oiFlf 

""' O,IS ..,. 

( )...,_ ,. __ ...... ......................... "'* .. 

lfBKB!. >GIMo-1 "Ol.eo 111o1 OW BH'I ,.._ 1D comet 

lfBMBil :>l~o~t•lkpa;rQftiiiMf •.S~ otBH 

(. )lt:ll R~o.&.cdo1 Llmill 

CLIENT: v .. Ho iS Tedlnleol Solodo., 

PROGRAM : Uoll3 

l tUN NO. lU 

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Jtrt(B »- U.78 PI dn...,. lhe r::-t oiiJ.11 fl8 or l1!c ,_. ~- ~ llC8 ot ""of PHS. 

• • value -.cl for bl•\: OCH1'.cit'- (•) • btMd on • J.$4 • ift.. ftltw liM 

MUCUaY: 

..._, $..,.. Pkl BJir: 

f RONT HALf J.7S ... , . BACK HALF 115.21 .... . 

tf'n 11 loG •111 <root ,.. t~:eo Ilk .. fl v.,.._to eorms 

lflai1>6N'*II'A .... rl.._fN•JKoiF1f 

uo cu• • ..,. 

.... .... • l l.l!l 

( )Noio.M/ ___ Uooll 

....... .,... ........... ~ 

lf8HB ii>O._ - ·1 H._ .. .,_ 8HB ..... •CIOne:t 

lttiHB 11 >1 ,.,, .. 'ill: putcfrlt61wt qors.% •!8M 

( )No<llolodoci/ .... --Liooll 

CLIENT1 

PROGRAM: 

RVN NO. 

Veollo ES Todoalcal SoluUn113 

RJ 

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• ENSR AECOM 

SAMPLE TRAIN MOISTURE RECOVERY DATA SHEET 

' 

I 1/ ....... : ft7q 

• ..,, rr . I ,..,, jl. ~~J " :r:' \ 

1-He. I _,all-~-..-. 1-N.- :J - · ~ ....... o 1 ...... 1 _, ........... IXAD: ' : ..... IXAD-He.: ..1" .: o.lll. 

~_He._:_ iD12n:t 1-No. i'Ol "'1' • 1 iD1.,tUO 

·---- •No.oncfV'*-

No. •:, :.-: = No. ~ ~: = No. = ~~ = .-

1 0 ~l) 1 0 ~'f) 1 0 /030 

( ' }) 2 /ro )15 2 loo J'J.D 2 100 ~10 

3 loo 115 3 Ito 1/5 3 lor.> .11S 

4 0 3 4 - 0 (> -.4 () r 

6 loo . ~ 5 100 ~ It!-

!. loo too 

e 100 

100 v 

Pf 8 • )$.-- IO<:> 6 loo IDO 

7 ~ 7 S6 7 S<r 

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~ ~I ': ' lnllol A: .,,, ·;;. 'J';• 

DIFF: (g) DII'F: ":!"' ":: ~ ~ Gel Qi,.s :l&f.7 l:I.Q ~ lJI.J .,._..,, ~ 

J'Z. • .:3 s:- :.121.1 3'11. '2. 1<1.1 

Flnolllot-Gain: IAIM <> flnllllot-Ooln: &-a. F1nlll Not-Ooln: ·n,.l 

-t .m•r )t' P ·-

VES 003210 
( 

Week of September 8, 2008 '· 

( ': 

' • 

( ; 

VES 003211 
. " """' .. ES I' 

Fixed Hearth Incinerator~~~~ 

••. ~ 29 . 

( I 

1111 ~ ')4, VIV n~ ~ 100.6 11 

Dry Mole I ..!!!!!::!!!!. - ..o~ ~ O.G816 0.585 

co. ;olstadr . %dry·.. ----uo· 4.50 4.50 4.50 

0,81Siack %dry 11.21 10.91 -11.35 11.18 

~()_+Nz %dry 64.~ _!4.59_ 64.15 64.34 

Dry l ~17 ~ 9. 29.17 

~ 

Wet I rWei!ltrt 24.54 * 24.64 

· ·..!. ~ tO :.o O.S 

SQ.In. ~ 14.6 1194.6 1 .6 

Stackl inH,O 0.16 0.11 0.13 

~'llad<~~,;;----+ ln."1' .!....- Hg -f--;~ ~29.760, 14.;;;· ~ .. :--lf-,~ ~ qroot0flleli3 p - lffii3- ~ ~ 0.359 

- s.na 10~ 1D.412 

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VES 003212 
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- .... .... 1111 - .... .... ll> .... . lUI .... 020 ..., 

.,.... .... IUS a.os • l-l.71 • t,OI IUO ..,, Olllall CG) .... 0.00 ll.11 - .... .. .. Clltof!Wift CJ) :J..IO 0.61 . lUI O.lf U9 U7 

"(0.) 0.00 .... 1).11 - .... 0.00 

0 .... . .... J.UI - 0.00 .... -· .... .... ,..,, - .... .... 

~ IJ-90 

·~· . 1111 ..... 11$ ..., .... 0.00 1111 - .... . ... 0.00 ..... 1111 - 0.00 ..... .... .... I - .... o.oo 

v...-cYl .... . ... lUI - .... .... .... ~ .... o.ao 11.11 - ..... . ... ..... --------

JffH8 .. blew- 0 liD 1.3.11 ,. ........ 'fdllle., canct 

rfPJII> l.7t t~c--.C~epueer ri1.11!1&«11M:..._vlflle~ f11B• mwm:s. 

• • vM-. "'td fw bill* <Omectoa (1) ·but40.•U4· ierl. tiJI.r•l.., 

MUCURVI 

JJTa lt>tN<CIOIIS N ..... ,. ._.._IOCCII'I'=" 

t.'TBa>4111 ., ....... fii.,.,H«»>iolm 

( ) ... _, __ ..... ...... --...... till:*~ 

IACXIIAU 

"""" "'" "'"""" "'""' v ... ._,, "":..lf.olt .. PI ... ~ .. 1.00 - . ... .... 1.00 - 0.00. 

0.10 . 1.00 ... , - co.lol 

0.00 1.00 - .... ..., . 1.00 ... fi.jjjl 

..., . .... lt.U .... .... .. ... - 0.00 

0.11 • '·"' Ml .. ,. .... .. ... - •• .... 1.00 - . ... .... , ... - .... ..., . '·"' 0.01 ll.2l 

.. 1.00 - 0.00 

.... 1.00 - 0.00 

1.00 - o.co .. .. 1.00 - 0.00 

.... I.OQ - 0.00 

lfBHBfi>OtM•I ,.._._ ... IKB ..... ttcomct 

1/BHBI-. >t lll .... .,.._orctctwrl ~~&otS%oiBK 

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CLIENT : V10Ua £S TecblcalSoluPROGRAM : Uoll3 

RUN 11'0: 1U 

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EPA ISOKJNETic< SAMPUNG-FIELD DATA SHEET 

11atkli'f'N~~ l + o. \' , ........ Nib. .-

---·-

PW.IM1'CHo . 

............ .... HO 

·--

. . 

JAN< CHICQ 1ft "HH 

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. 

. .-: 

VES 003219 
( .' ,. ~ 

ENSR I AECOM 

PREUMINARY SAMPLE TRAIN RECOVERY DATA SHEET 

FOR MOISTURE DETERMINATION 

-. 

VES 003220 
c. 

' -' 

.. 

0 . 

C' 

. . 

ENSR I AECOM . 

1 

2 

3 

4 

5 

8 

PRELIMINARY SAMPLE TRAIN RECOVERY DATA SHEET 

FOR MOISTUR.E DETERMINATION 

0 It>~ 1 

100 zso 2 

loo · (15 3 

0 0 4 

S& 5 

6 

VES 003221 
( 

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( ... , ' ·, 

' ' ' 

Facility Oxygen Data 

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VES 003222 
(. 

Week of August 11,2008 

( "'1 

.. 

VES 003223 
; 

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VES 003224 
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VES 003226 
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VES 003227 
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VE$003228 
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VES 003229 
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VES 003230 
( , 

Week of September 8, 2008 

C) 

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VES 003231 
2Run1 

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; 

VES 003232 
( 

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I. 

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VES003233 
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6.57 

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VES 003239 
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i 

-2008 

• 

VES 003241 
( . .. 

(

.,, 

; ' .. 

September 10. 2008 

14:36-16:46 

Unit 2: Retest Run 1 . 

ENSR II AECOM 

I 

1 

2-6 Molecular Weight of the Stack Gas I 

1 

M.= ((4.501bllb-mole'0.44)+(11.211bllb-mole'0.32)+(84.291bllb-mole"0.28t(1· I 

0.414))+18' 0.414 : 

M.= 24.54 lbllb-mole 

2·7 Average Stack Gas Velocity ! 

v. = 85.49 ftlsec [((lbnb-mole)(in Hg))/(~)(in ! 

H:P))]112•(0.84)(0.3363)-1{(384.6'lf+460)/((29.6 in Hg+0.0969 in Hg)'(24.57 bll~o e)) 

v. = 26.037 ft/sec • 60 sec/min 

V • = 1562 ftlmln 

2-8 Average Stack Gas Dry Volumetric Flow Rate l 

a = (1·0.414)(1562 ft/min)(1194.6 in2)(1 1\'/144 in )1(528~'29.61 in Hg)/(29.92jin 

Hg'(384.6'lf+460))) 

a = 4698 ftltmin l . 

3-1 Dry Molecular Weight 

M• = 0.440 (4.50 %)+0.320(11.21%)+0.280(100-{4.50%+11.2 1%)) 

Mo = 29.171b11b-mole . 

4-1 Volume of Water Vapor Condensed 

Vwc(11cl)= 0.04715 ftltmt • ((930 mt+260 ml+125 ml+360.3 g)-(200 ml+346.7g)) 

V-.s1cl)" 53.213 ftl 

+2 Volume of Water Collected in Silica Gel 

V-= ((360.3 g .-346.7 g (0.06236 mmHg)m gmole (~(293 Oj{))/(760 mmg H9)(18.0 

g/gmole)(1.0g/pl · 

V-=0.018m 

V._= 0.636 ttl 

4-3 Sample Gas Volume 

v.-=1.021 • ((653.131 rr- 575.565 ftl- (616.044 ttl- 615.86 ttll<29.ao in Hgi-+().0969 

in Hg)(528 ~))1~29.92 in Hg'(89.9 "F+460) 

V,....= 75.295 It 

VES 003242 
c 

( "''· : 

.. ~··· -' 

4-4 Moisture Content 

Bw.= (52.213 11"+0.636 ft")/(52.213 11"+0.636 ft3+75.296 II") Bw.= 0.412.100(%) 

Bw.= 41.2% 

5-8 lsoklnetic Variation from Raw Data or lntennedlate Values 

ENSR il AECOM 

I ,;, 144in iff•4111"(100 (~.6"F+460)(75.296 11")'29.92 In Hg))/((52e0R)(1562 ] 

fthnin)(0.435 ln)'(29.61 in Hg)(120 min)(1-.414)) · 

I= 106.97% I 

29-1 In-Stack Detection Limits 

A'BIC=D 

Front-Half 

D = 0.00013'(30012.13) 

D = 0.018 ug/rri3 

Back-Half 

D = 0.00013.(15012.13) 

D = 0.0092 ugJm3 

Be 

Front-Half 

D = 0.000033.(30012.13) 

D = 0.0046 ugtm; 

Back-Half 

0 = 0.000033.(150/2.13) 

0 = 0.0023 ugtm' 

Front-Half 

. 0..:..... 2008 

r· 

VES 003243 
( ENS~ IAECOM 

0 = 0.000033*(30012. 13} 

D = 

0.0046 ug/m3 

Back-Half D = 0.000033*

(15012.13} 

D = 0.0023 ug/m3 

Cr 

Front-HtJif 

D = 0.0001*(30012.13} 

D = 0.014 ug/m3 

Back-Half 

D = 0.0001*(15012.13) 

D = 0.0070 ug/m3 

~ 

,, c Front-Half 

D = 0.000066*(30012.13} 

D = 0.0093 ug/m3 

Back-Half 

D = 0.()()0()66"(15012.13) 

D = 0.0046 ug/m3 

.!jg 

Front-Hatf 

18 

D = 0.00005*(30012.13} 

D = 0.0070 ug/m3 

Back-Half 

28 

(,_ Oooemboo 2008 

VES 003244 
c· ' 

\;.. ' 

D = 0.00005.(1500/2.13) 

D = 0.035 ug/m3 

3A 

0 = 0.00005*(10012.13) 

D = 0.0023 ug/m3 

38 

0 = 0.0001*(50012.13) 

D = 0.023 ug!m3 

3C 

0 = 0.0001*(25012.13)· 

D = 0.012 uglm3 

29-2 Analytical Fraction 1A, Front-Half, Metals _(Except Mercury) 

Mw> = c,, F6 v-., 

M 

Me.= 0.202*50*0.3 

M., = 3.0ug 

!!:! 

Me. = -0.004*50*0.3 

Me. = ..{).006 ug (NO) 

Cd 

Mt. = 0.005*50*0.3 

M., = O.D75 ug (NO) 

Cr 

Mo. = 0.830*50*·0.3 

Me. = 12.45 ug 

o.c..- 2DOt 

VES 003245 
( 

ENSRII AECOM 

fll 

Mo, = 3.033"50"0.3 

Mo, = 45.5 ug ~ 

29-3 Analytical Fraction 2A, Back·Half, Metals (Except Mercury) 

Mot. = c .. F. v-., ~ 

A! :• 

Mot. = 0.055*1 0*0.15 

Mt.,= 0.10ug 

Be 

Mt.t. = 0.001*10"0.15 

Mot, = 0.015 ug (NO) 

Cd 

c· .\ 1\.\o. = 1.697'10*0.15 

Mot. = 2.55 ug {NO) 

~ 

Mot.= 0.290*10*0.15 

Mt..=0.44 ug 

Pb 

""""= 0.218"10*0.15 

Mot. =·0.33 ug 

29-4 Total Train, ~atals (Except Mercury) 

Mt = (M~t~·Mt~~>) + (Mt..-Mt,) ,. 

As 

Mt = (3.0 - 0.2) + (0.1 - 0.10) 

Mt = 2.8 ug 

L· 

Oooltnbol 2001 

VES 003246 
( 

{ 

Be 

Mt = (0.25- 0.05) + (0.025- 0.025) 

Mt = 0.20 ug 

M1 = (0.25 - 0.05) + (2.55- 0.03) 

Mt = 2.73ug 

Mt = (12.5-0.61) + (0.44- 0.17) 

Mt = 12.16 ug 

Pb 

. Mt = (83.3-0.22) + (0.59- 0.14) 

Mt = 83.5 ug 

Unit 2: Run 1 

29-5 AnaJYtlcal Fraction 18; Front-Half Mercury 

Hg., =o.,F.v....,, 

HQftl= 8.687 '1'0.3 

H9111 = 2.61 ug 

29-6 Amount of Mercury Collected In Samp" Fraction .2 

H!Jot,2= Ow F•V-.2 

Hgl>ll2 = 4.712' 10'1.365 

H9l>ll2 = 64.3 ug 

ENSR\1 AECOM 

29-7 Back-Half Mercury Values for Analytical Fractions 3A, 38, and 3C 

HQI>h3 (A)= 3.52B-10'0.1 

Hg,.,.tA>= 3.74 ug 

~(B) = 5.539'1"0.5 

VES 003247 
c H9ons (8) = 5.13 ug 

Hgbll3(C) = 3.125'1'0.25 

H!lw<Cl= 7.81 U9 

Owc-..e.c> = 3.74+5.13+7.81 = 16.68 ug 

1 

ENSRIIAECOM . 

29-8 Total Amount of Mercury Collected In the Back-Hatf of the Sampling Train 

' 

HQb! = Hg,z + H!lot>lA + Ho- + Hgwc 

HQb! = 64.3 + 3.74 + 5.13 + 7.81 

H901 = 80.98 ug . . ~ 

29-9 Total Amount of Mercury Collected In the Back-Half of the Samplln~ Train 

Hg, = (Hg., ~ Hg,.) + (Hg,. - H!Jbhb) 

Hg, = (2.61 - 0.01) + (80.98-0.09) 

Hg,= 83.5 ug 

Unit 2: Retest 1 

29-10 Individual Metal Concentrations in Staek Gas 

Ca=(K. MiJN.w.uJ> 

As 

c.= (1o-&2.8)1(75.296"0.2832) 

c.= 0.0013 mglm3 

!!! 

c.= (1o-3' 0.20)1(75.296'0.2832) 

C.= 0.0001 mglm3 

. Be corrected for 7% Oa 

c.= (0.20'35.314'14)1((75.296'21-11.21)) 

C.= 0.13 uglm3 . 

Cd 

C.= (10'3o2.73)/(75.296'0.2832) 

c.= 0.0013 mgtm3 

VES 003248 
( 

Cd coqected for 7% Oa 

c.= (2.73"35.314"14)/((75.296.21-11 .21)) 

C.= 1.83 ug/m3 

9: c.= (10-3.12.16)1(75.296"0.2832) 

C.= 0.0057 mg/m3 

Pb 

c.= (1o·•·45.57)1(75.296*0.2832) 

c .= 0.021 mg/m3 

.!::!.9 

(

... c.= (10'3"83.5)1(75.296"0.2832) 

' . C.= 0.038 mglm3 

~ ..... 

-1 1.72)) 

ENSR l AECOM . 

; 

• 

VES 003249 
· .. .ENSR 

: 

!'ppend~ C . . I . . • . . . . . . . . I 

Reference. Method Calibrations, Verifications, and Certiftcrttlon~ 

) ·I 

' . 

... 

• i . ' 

: 

! . : 

; 

' 

.; 

., 

' 

. • 

·• ; 

. ' 

' 

' 

VES 003250 
) 

) 

, .. 

Reference Method Manual Equipment 

Pretast CalibrationS, Veriflc:ationS and Checks 

' • 

VES 003251 
'') 

\ 

ENSR i-\ECOi'vi 

DRY GAS METER CAUBRAltON .., .. Me.: 8I')S03 

---- - -- • • - "' - ~ - Clft'"UI..,_D4TA 

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.. I 

--. .. .. -... .. . ..... 

.. 

. ' 

VES 003252 
) 

ENSR AECOM 

.... _ 

--

-

... 

...... - --;;;;-

... .. 

-

• ' • ' 

..... "' --

" 11 141 .. 

DRY GAS METER CAUBRAnON 

--- tclT$5 

p. .. 

..... 

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. 

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~ ............. ,., • .__... ........... :. t.A'J 

8T.._ ........ ~ ....... ..-.: .2'J 

.. ~· 

VES 003253 
=t:: ._ -....r::-... 

~ ¥' ~ f.WS:.,s:•11"1 • .. .. .,._ .... '" • .. ..... , •• $) 

. ' Zi28l .. ........ ., • :~ 

• 

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W.,A

--

CU~ 

·..., -.... .. ..,..Q, • ., .... ---}++± ~ 

~I.,.,.-;;;;;;; . 

-

~ 

~ 

._

;:;.__ .. 

A ... Af.!t\ .05$. PA ' t.11 .... 

'· 

--- · 

' -

- -· • 

- -"-

VES 003254 
ENSR I .1-\ECOM 

) 

) 

VES 003255 
.. . · . 

) ENSR I AECOM 

_,, .. __ ., 

!!1!/!!!!!! 

.... 1 ... .... ;,1 ~-~~ ... ·- ~~ "' - , I """'I " .. = 

· on.:· f 

liii ... . I· ~· .. ~r ... r ... . ... -;-

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~ 

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~I 2 

.I 

" )4 I 

• 

VES 003256 
.. , 

' .I 

) 

ENSRI AECOM 

BAROMETERCAT.ffiRATION DATA FORM 

Field Barometer 10#: Serial No. 51111291 

Reference Barometer 10 t1: Settal No. 188841 

Pre-Test calibration data 

Calibration Pedo!rned ~ : Ryan Bums 

~ r~Erl Reid Barometer 

~ 3~~ ~ . .1 6 ~ in. Hg 29.16 

Post-Test calibration data 

Calibration Pedonned By : 

I 

R. Bums 

I AocAJracy 

. in. Hg 

.!:. +/- 0.10 ln. Hg 

Note: The field barometer Is~ to agree IMth the reference barometer 

after each calibration. The rellwence barometer is rlled<ed and re-calibnrted 

by the vendor on an annual basis. 

I 

• r. 

·' 

VES 003257 
' ) 

) 

Reference Method Manual Equipment 

Post-Test caJJbration C~ks 

.. 

VES 003258 
' »UIIISiRuME>ITS EPA~5 

522 s.tlt Milot Box Cellntian --8oocu.b._K'_ -.T ... ~-

..aMNfiGrwfd_,..... .. /IIJJflll'll'lo.lo.M ........ 1.2h. Ho....,ra.ahl'NMiclll~ ................ 

-..oM"Ain.CW.Citei».~I(.---...... " ........ "*'WI't .. ~ 

,..... 

r,t,!!Bjjl!l!O@. I 

"* ,_~F--Y h .. ofb ..... ofW. ......... ID'*-.,._~ ~....,.d......,...,.... .......... ..o.02. 

FwO*-c:.liiWidoaf__...._ ..._._...,....,.......,_..,._dHZOfW..-'oO.l'SdlldW ••Fna..atlld'lellfll.__..,.......,.._.otlrdroilillll....,.._._._.,......a. . 

-

-· .. . .. . ... 

.. . 

.. 

VES 003259 
) 

,. 

-"'EX~ 

EP~Mdlod5 

522--l!oi<~ 

PoM-Tf:SI Orh Mdlod 

.Etlglbh ....... ~ EtiQiislh J5:' ,. .... 

M'ORJN-F..-..... wa.-... .. ,a.;')laowM.....w .. t ~~~o 2k Ho_....,tr.nf'lt ~CIWIIIIIV.U.*---. 

U'OfttN~c.-~c..-....: -..t.; ...... W.IEillglilll--.~~~ 

•• 

: ~ ,._~,__v ._,.. .... ~., .. ~.,...., .. c~~y ... --. 

--------lndMdull . ..._tlofll .. .-.111~ . 

t:ofO!IIc:l.~,._.lllfO hoo6»dllterwCIIal.--tlrl..,_ti.W'*~"'o.75<*d* 

atM n~~d ... ~.....__.,~ ...... .._ ............ -.cu. 

-~ 1 • 

I'· <-) M.,=1~J "<(of) 

.. s.w• I eoc .. ...... .. 0.<%7 

.. ..... ,. . ..., 

:: 

i ,. .. 

VES 003260 
ENSR 

Appendix D 

Laboratory Data 

(

. . 

' 

1 

: . 

' . 

. •' 

l 

' 

~ 

.. ; . 

i 

' 

. 

' ' 

VES 003261 
..... 

., 

\ 

.. 

f 

Method 29 Results -~ 

.· .· 

VES 003262 
~ ··. I 

Week.of August 11,2008 

. . 

(

'"'-: . 

.. ~ 

._ . 

. . 

·c ' . . . ; . '. . •' 

VES 003263 
MaR.arn ~ ........... ... -:-------::-------------;.;.~ ~.,~.-~~ r~~~ .. ij;, ;:;_;;_ 

5015 Campuswood 0. 

SUMII104 

East Syracuse. NY 

USA 13057-4232 

y.,.... Pl1ljed II: 10002.()22 

Sile:CPT·VEOI.IA 

CMIIfiC6D OF ANALVSII 

(l)_..., ___ by_.......,., I Ill' 

(2) 'nlll ...... tl w..n I 2 + 'liJIP....,....., ......_, SC:CAL:o*s s I 

MAXicAM AHAL YTlCS IHC. Digitally 

signed by Mike 

Challis 

Date: 

2008.09.03 

16:09:00 

-&$'00' 

Plge I ollt 

---·--..-.c... --·-.----·-ln.- ... -

VES 003264 
M a a~.!!! ------------------"'--~!';;:;:-~$~$<>;;;;·"";;-:.if;i:$5.;;;, •• ;, ENSR~I 

(

. • Maxxam Job II:AIIQ1833 

' Report Dolo: 2008III8IZ7 . . Client Pn>joctll: 10002~ 

ProjecS - VEOLIA 

IIEIICURY BY COLD VAPOUR M (SAMPLING 11IMq 

! ( "' 

t" l 

· 

"'I 2.f1 2.35 

"'I ..... NIA 

"'I NIA NIA 

1111 N/A NIA 

1111 NIA NIA 

..... 

• Rl;»oelltllt 

~ 

Dllldon l.nl 

-. o..-.CioiOrdUll 85.7 

Ull U1 

1111 S.11 

"'I 1.87 

_____ .._,_ IA!IH7 

ur ,2.15 ..... 

""' NIA 114.3 

NIA .., .. :u• 

NIA .., .. 5.13 

...... NIA 7.11 0.25 

'1'5.4 0.73 

,_ 

3.15 . 0151 1-

:Z.11 

-15110110 

7.82 0.25 U8 0.13 '""2S7 

VES 003265 
M a ~~ .. r.T.! ---------------'-- -;!'~~;;-~;..ti;i!:'iii; .• ~'"'L;;;~~-~·-;· ENSR intemational 

l': j ~ 

Clonl l'lqoc:t #: 10002-022.()g()(): 

Projo<t '*""' VEOLIA 

ELEIIElfTS BY ICP/1111 (8AMPUifG TRAIN) 

.... -~) .. """ l!er)lluol48o) .. 0001 ~ICc!) .. INI~ICI) tG 

-Loocl~) tG 

·.Mol- ............ o.c:li:nl.id 

8illllc:h • OAity Ccr'*ci 8lllc:b 

. ,.....c..., 

,...... ..... ~ l.i'll 

- · '-1C<rnl8ot:ll 

18.1 

liD 

2.t5 

11$.3 

,... 

_____ ........ ,__ L7LiiiH1 

·n.r u IW 2.0 t_.,OO 

NO NO NO .M IIIIZ700 

2.38 2..22 1.88 .60 lal2700 

au 811.1 80A 1.5 ISIIQ700 

,.. - 31t 1.0 INZTOO 

Pago3ol10 

r 

r 

VES 003266 
·c\ .. ' 

Tests-JY 

-DI<FTZM> 

- D M28-U2-R1 FH 

---

-D AF7237 

- D loi29-IJ2.R2 FH - SAIIPUNG lRAIN 

_.,_ 

-'" D M2$.\12-R1 Bit 

. -SAAFI.INGTRAIN 

.-Dmmo.c. · -D~IBH 

- -..NGTRAOI 

_____ .._C... L7L11<7 

- ·200MIM1 

8hWod 

. - 21l0Ml8114 

~-· Shlppod 

- 200MIM4 

.. 

. 

VES 003267 
M a a~,!T.! ------------- --~!';;: . ....J~>z!i;•;;··;;-;-:ijt:r'ii;*;;:; ·_;;;.:;: ENSR .... iiOibiOI · 1 

, ~ P>ojoCI it. 1~.0000 : 

Pillje<I-VEOI.IA 

C} 

, 

' 

(:) Pogo Sot10 

VES 003268 
. II&RCUR'I'IIYCOI.DY-M~.,._, 

-..y1BinRiot +. -(loi29):TeoiHGFIW',.W8tl~ 

-~-ClOIAdnolbo--duolaNgh........,....-ln .. 'ftii!'O'""'*-

--. .. In~""-'M29~--.,a-y-nolbo..........,_ ..... Ngh __ ln ........ . . . · ... · .

. · fi..EIENl'8 IY ~ ,......utO TltAIIIIJ 

-F.H.In-•-~M.-Sl< _._....,..,.._lnll ___ on __ ___ OIIol ...... duola .. -

T--CR--111110-- • 

..__cr -e.H.Intc1071HN03~ __ .,,. __ ---Inllic>b-doneon-AF7231. ......_ 

------.,_...,~ Ln.l>l1 

. . ~ 

., 

VES 003269 
M a a::;! !!! --------------~~;; ENSRIIHmotional 

AllonCion:JelfGonnan 

~ :· -· 

c·I 

W.TRIX Sl'll<l! 

1Af72311) 

MATRIX SI'I(E 

TOIII~ 

DUP 1Af72311) TOIII """"Y-39 

-- TOOIIIAon:uly-38 --1)\.f' TOIIIUon:\lry-38 

-- TOOIIRPO TOIIIUon:ury-38 

1seo:I84FFS fAA TRIX SI'I<E 

1Af72311) Totai...._.2B 

W.TRIX SI'I<E DUP~) Total~ 

-- TolaiUomry-28 

--DUPTolll~ 

-- ToiiiUomry-28 

~ T-Uomry-28 

1510394 FFS 1M TRIX SI'I<E 

(Af723$) T-~ 

MATRIX SPJ<E DUP~) TOIII-

-- TDIIII~ 

--DUPT-~ 

--

IV'!) T-~ ...... _ 1591237 FfS ~ BC.AHK Total t.loft:urto3C 

""TRIX Sl'll<l! 

(Af723$) COII~ 

""TRIX SPliCE 

DUP (Af7239) TCOII~ -- TOIIII~ 

--DUPT-~ 

Moiled ,._;. . Tolll t.1oft:urto3C 

RPD TCOII.......,..OO 

15927'00 N_R MATRIX SPIKE 

(AF7236) Tdii...-(A&) 

MATRIX SI'I<E 

DUP (AF7236) 

W.TRIX SP1I<E 

Tdii-(Aa) 

(AI'7238) TOOII ~ (lloj 

W.TRIX~ 

·DUP (Af7238) OIIII~(Bo) 

MATRIX SPI<I! 

W7238) 

MATRIX SPIKE 

TCOII Cdnlum (C4) 

DUP (AF7236) T .... CNrium (Cd) 

MATRIX SPti<E 

W'723S) 'T0411 Clwomlum ((>) 

W.TRIXSPII<I! 

DUP (.01'7238) T-a.omum ((>) 

MATRIX Sl'tKE 

(AF7236) 

WilRilCSPJ<E T*~Cf'l>) 

llUP (N'7236) TOIII LeaO (PI>) 

-- TOiii-(Aa) 

PaQo 7ol10 

Clont Pn>joct II: 10002.()22.oooQ 

P;O. II: 

Projocl noma: VEOIJA 

200Ml8l21 127 127 til 

- 100 100 

200&'05121 101 101 

- 103 103 

2C081011Qt NO. ADLaO.OS 

200Mllll21 0.8 

2C08/0IIQ1 98.0 86 

200Mllln1 98.0 118 

200&'05121 112.0. 112 

200&'05121 118.0 98 

200&'05121 . NO. RDI.oO.OI 

- 2.1 

2000!/08121 92.0 92 

JZOOMll/21 911.0 01 

2006101QI w.o e7 

2C081011Qt tOt • t01 

200&'0512t NO. Rl1o0.005 

200&'0512t 0.7 

200&'05121 NO, Rtlt.oO.Q2S 

200&'05121 . 80.0 80 

200810812t 113.0 113 

200&'0512t 118.0 86 

200&'05121 llti.O ll9 

200&'05121 HD,Ina0.025 

200&'05121 o.T 

2008IOIIl28 47.5 05 

20011108128 47.5 05 

-- 50.5 tOt 

2008105128 50j) 100 

2IIClMI8I28 25.0 100 

200MJ&I2lS 24.8 89 

- 50.5 101 

2008105128 62.0 ' 104 

2008105128 51.0 102 

- 50.0 100 

- 51.5 103 

ug 86 ·116 

ug 85. 115 

ug 80·110 

ug 80 · 110 

ug 

% 20 

ug 85· t115 

ug 15 .. 115 

ug 80. 110 

"" 80·110 

ug 

% 20 

ug 85. t15 

ug 86 ·115 

ug 

ug 

ug 

% 

ug 

ug 

ug 

ug 

ug 

ug 

% 

ug 

ug 

ug TO· t30 

ug TO· t30 

ug 70·130 

ug 70·130 

ug 70-130 

ug 70 · 130 

ug 70 · 130 

ug 70 - 130 

•uo as. us 

__ .... ___ """',._""_ 

SSM ____ ,_""-* L7l-

" "' II"I')MH110 

T .. ____ 

F.: (lOS)~ 

VES 003270 
M a a~ . ':!! ------:-----------------~rs;.;.~ !!"";;:;;;:-;; ;o;;-:"~,;=~·;:;.:;: ENSRtram-.ol 

c - Je« Gormon Ciani Pooject II: 1 00012.o22Al90<t 

P.O.#: 

Pn>joCf ....,., VEOUA 

T'*' :zooMJ8Q6 51.5 103 11!1 85-115 

lliJP T<*l 200Ml8l2tS = 104 "'I 15·115 

T<*l 

- 24.5 118 11!1 115-115 

llU' TOOII 

- 25.0 100 "'I 115- 115 

- 200IICI&2e 60.6 101 .. 115-116 

-lliJP 

- 110.0 100 .. 115-Ill 

TOallood.ll'bl 

- . 61.0 to2 ' "" 115-115 

DUI' TOOII Uod (Pb) 

- 52.0 ""' ... 15- 115 

- T""'-IAOl 

- Ioiii. Rlll.>o0.40 "'I 

--DUI' T .... _IAO) 

-- 11).-- "'I 

-- T .... ...,.....tllol - I'D. RCI..0.10 "'I 

- -DUI' T .... _,(Bel 

-- Ioiii. RCI..0.10 "'I 

-- r .... CodNim CCdl 

- I'D. Rlllo0.10 1111. 

--DUI' Tolll Cilo**lm (Cd) 

,....,.,.. II), RCI.o0.10 .... . --k Toiii~(CIJ 

-- 0.30. --*' 11!1 

- Blonll DUI' Tolll Clvl>oUn(CIJ 

- 0.!13. -.o-30 Ull 

-- T'*'lood!l'b) 2008/1181211 NO, ROIJo0.2D 11!1 

--DUP T .... lood(Pb) 

- NO, .RDL-0.20 Ull 

""" TOOII-(Aa) 

-- " % :w 

T""'-(llol 

- NC % :w 

T .... ~!Cd) 

-- NC % 20 

T<*I~(CIJ 

- ... % :w 

Tellllood (Pb) 

- 11.1 % 20 

15112702 FF$ AEAOe<T l!l.foNK r .... -...•• 200MIBI22 Ioiii. RDI.o0.015 .. IU<TRIXSI'I<E 

!AF723II) T .... ~1B 2!XI8IOia2 221 2211(0 1111 85·1tS 

... TRIX SPliCE I 

CUP !AF723II) r...,.......,..,a 2008101122 254 254(0 1111 85-115 

-- r...,.......,.1a 1001A"em 98.0 Ill · "'I 110-110 

$Piioq-DUI' Ta411-1B 200Mlll22 104 104 1111 90·110 

-- T .... .......,. .. 20tMiel22 NO, RCI.o0.015 'II 

""" rc.o~-...1& 200Ml8l22 10.2 % 20 

t 592707 N _R MATRIX SPIKE 

(AF723t) """-lAO) 2008108125 48.5 113 Ull 70-130 

MATRIX SPIKE 

D\P(N'm8l 

MATRIX SPIO<I! 

TCIII-lAO) 2000108125 45.6 11 'II 70 · 130 

(AF723t) T""'-(lie) 

- 4U to Ull 70-130 

... 'IRIX 11'1<1! 

OUP (loF72II) T .... llof)hon (lie) 

- u.s .. "'I 70-130 .... TRIX_ 

(AF723!I) 

MATRIX SPUa! -~!Cd) 

- 22.1 t1 'II 70-130 

DUP CAFrnll) Tclll ~ !Cd) 

- 22.5 to Ull 70·130 

MATRIX SPICE 

(N'1238) Tclll Clworriln (0) 

- eo.o 100 Ull 70 -130 

.... TRlX &PM<I! 

DIP (AI'7231) Tolll Clwn-lln (CIJ 

- 48.0 oe 'II 70-130 

MATRIX SI"'KE 

(AI'7238) T""'Lead(Pb) 2008108125 4$.5 r7 'II 70-.130 

MATRIX SPIKE 

OUP (N'7239) T""'lood(Pb) 

- 4U V1 'II 70- 130 

Spllood- T...,_INJ 

- .v.o oe 11!1 85· 115 

--OUP'r..,._IAO) 

- ..... 118 11!1 as-n15 

( i . h008ol10 tlio-lslo ___ _, .. - ... ,..._ 

............. -.... ~~ c:..dl L7l.SH1 ot~$02--- T .. ____ .Fe (a'l5) sn.et• 

VES 003271 
lVI a a~.!.T.! ---------------...-.:-- ~!"""";;· ~'!;; .... 5 ... ;;_;;-i; ,_~s;; .. :;:;;-: . ENSR-..... 

-JolfGo<mOn ( 

{ .. 

< 

QMlC 

Htn

-

O>i QC 1'foo 

1592701 N_.R ~ !""'* -TCIIII....,..,. (So) 

· Sj>llooci-OUP TOIII~(llo) 

. . S!*td- ...... Ca<hb!l (Cd) 

S!*td-OUP TCIIII ~ (QI) 

Sj>lloociBiri .,.... OWnUtt (QI 

Sj>lloocl-k CUP TOIII aw.nvo (QI 

~- TOCIIL*~ 

• S!>llod - OUP 'Ioiii L* (PI>) 

-- TOOti-(,Oo) 

--OUPTOIII-(Ao} 

-- ,.,..,..,... (llo) 

--OUP TOOtl-(llo) 

-- TOOti~(QI) 

--OUPTOIII~(Cd) 

-- TOIII~(Cr) 

·--OUP TOIII Ctwon-. {CI) -- .,...,....., (I'll) 

--OUP TOOtllood (!'!>) Rl'O TOIII-(Ao) 

TOOti-(Bol 

TOIII~(QI) 

!.~~(QI 

.... 

Mal -r teHe 

~:--- 1 ) 

·

~...-

--to Gwletll eon-a P9 for spec:A:: c:t.ifii I ' 

Plgotofto 

qlont Plojod If: 1 DOCJ2.022A)8I)Q 

P.O. If: 

POojod- VEOUA 

Dolo 

......,.,... ~ 

--47.0 M 

47.0 M 

200MIII25 :M.O 118 

- :M.O 118 

- 4U liT 

- 50.5 101 

- 52.0 104 

- 4t.5 II ..._,., NO. RDV0.2D :Ill- HD.Ra.o0.20 

- ICI.--

2IX**?5 HD.RilloO.olO 

- ICI. RDIJoO.G$0 

- HD.Rill>O.OOO 

- O.t7, RDL>0.1$ 

- 0. tT, R00o0. t5 

- N0.~.10 

2008108125 NO. ROI.oO. tO 

2008108125 , we 

- NC 

- NC 

2008108125 ~ 

. 

__ ,., ___ _,,._ .... _ 

·- ""'lmls uo 85· tt& 

uo es. 11s 

"" 15· t16 

ug 85- n o 

"" 115· ,, 

ug .. ,, 

ug 15·115 . 

119 . ·as- us 

ug 

ug 

ug 

"'I 

uo 

ug 

ug 

"" "" ug 

% 20 

% 20 

% 20 

~ ~ 

VES 003272 
M a .../0 a m --------------------;"':;;:;"=~,..~·;;;;;·'""F-.-if;is;;:;' ;m . ......... .....p 4 ... 

V.Mdatton lia"PD page 

Maicum ~ob f: AAIII1833 

0 

__,..,,_...,._ .. __ ....__.,h_•...,_...s~oovo.,......,.....,......, ... -sJlll"' 

ISOOilC lmJ"""'('!).oiploo ,.,._., SCCoodCAML .... o.,...,...t"" _..._ ... ,_ --

Pogo to otto 

-----()ooboo!lo,c:..- L7!.817 

VES 003273 
Alt!ntjon; .Jtff Gorman 

EHSRin5015 Campuswood Or 

Sulle 104 

ENI Syno:use, NY 

USA 13C57-4232 

"'Y!A.I qt; Hilt+! 

~~19:33 

Simple Malri>c SAMPUNG TIWN 

II Samples Rec*Yed: 6 

-F.H.II>,_.•-(eo20)A 

YQ!K Project I: 10002-022.0000 

Slle:VEOUA 

CEBI fJCATE Of ANALYSIS 

200ei08I29 :!OOMillo2 S()P.(l010D:II MLII!PA GO®ISOf'.0011YL 

, . (

..,.. 

.. (1),.11Mtwaperlt:wmildb't...__~,, · 'Ot (2)-..,. .:..l*f<m*l r. -·· . 'II"..---sec"""""""_.,. 

MA)()(.A Ill ANAL Y11CS INC. 

.. .. . ... ~_~ .. ·. . 

Digitally 

signed by ~ Mike Challis 

"7- i%:-- Date: · 

~·&-•ro 2008.09.03 

12;52:33 

·04'00' 

oClllcove<~1 

_.,.,..._,. .. _____ ....... . .._ .. __ _ ....., ___ .,._._ L"-11147 

\ 

. 

' 

. ~ 

VES 003274 
.. M a a~!f.! -:-----------------:----~!';:;~;;·-;::.;:t;;t:;"";;;;;-;ii-;;;;_;;, ENSR .... ,_ ... 

C

. \ 

r. , \,:..1 

Clloo1t PltljeCIII: 1()()02.022.090( 

PTcjod .-:VEOUA 

· E~!HTS. BY ICPIIIIS (SAMPUNO ~ 

........... (MI ... ,,. ... 17.8 .10.8 8.7 • 2.0 -1 

<t~~""'-(Boj "" <aiiO 

- <0.60 <0).50 ·o.oo 18111831 

.... c.tiUo ICdl ... I .liZ 2.03 '2.00 1:113 0.00 

.... 10) ... 7$.5 77.4 eu tf12 u ,

-

_1 

..... ~~. ... SIS Sit m !ISS 1.0 18111831 

~r·~--.u.e 8llr:tl a:~~ 8llll:b . . . 

I 

I 

~ I~ 1:1'~ ~ I;;E-1' 

<ooi-(NI · ug .0.82 0.11 o:ro <0)20 OJIIJ 1-

--(Be) .. <0.0150 

- <0.050 <O.o60 p.050 -)2 

.... ceor.un ICdl ... <4.o60 <0.050 <0.050' <0.050 ~ 1- I .... ~fCt) ... ~ 0>1 o.ee ~ 0.15 1- I .... lood(Pb) . "'I (1.38 o.sa o.ss 11..16 0.10 1-

RCI._•--_,Uool ii:--• a,olly Ccna- . 

. . 

Ple02d8 

VES 003275 
. M a a~.~ ___________ ..;..__________ -....;.;.;;.~'.. ._,._;;;:;.;.; ;i~i;.,...~ .... :; .. :; .. ;;·:;-

ENSR 1n1i1m11iona1 1 

CloniPrcjocU: 11J002.a22- l 

0 

-IDA13040 

-ID -.u2.ft1 R1 

- IWAJNG TRAIN 

-ID AD04S 

-I>~R< 

- -.MGTRAIO 

_., AI300I 

-I>~IIH 

- So\NI'IMG 1IWN 

-ID -0.., 

-D~IIH --TRAit 

-ID AI3045 

- D M29-U2.fi211H --TRAit 

PlOjoct-VWI.IA. 

-........ 

--

-

--

-

-

--

-

. . Tot (ICI5)SOU7tl T .. ,_ (1100)_,_ ----

VES 003276 
M a ~.:1;!.~--- ----------· -;~~.".;;;t!:~i;;;;;:.':~'Sf~'!;:;':::;: EHSRiniB..-.al 

Ctool Projecl II: 10002.(122~ 

Projecl-VEOI.IA 

• I 

: 

VES 003277 
lVI a --4 a rn ----------------..-----~-;;;·~.,.~-=· :Gt~ .... ;: .. IR;;;-

. ~..... . ... ,...+ ;;... - ENSR lnle!NIIIonal • 1

. 

(

<··,.

1

Maxxom•Job t:Ail&7144 Clltoll'rojectfll: 10002.o22.(J900 ! 

Roport 0118: 2008/0!1103 Projeclnome: VEOLlA 

!I.EIRHTS 8YICI'IMS (SAIIPUNO 1llloiiQ 

_ 

-F.H.In-• i&.-($120):M .... 6>t ___ onei..,P. ...... IIo--cf0oolon_......,....,... _ ......... - ' 

. ~ 

- B.H. Io H202>t<N031mp.(e020~ -~....- ond - --on """"'"AI3044 . 

.... _ __. 

_____ .,_,c..- Ln.6H7 

VES 003278 
"1 a a~ .. ':!:! ~!%:~-"'~ 

"" .. ,.. ...... , eo• 

ENSRI- ( ' Al!lnlllln: Jell Gonnan 

Client PlOjod II< 1(1002-a22~ 

P.O. f; 

Pn:>foclnaroe: VEOI.IA 

• QIJally ..........,_Report 

Uloocam Job NmltJer: GM9T144' 

= 0.. 

-,m ......... \(- OCUmla 

1....,1 """ "-" 

~- TobiiAIMdc~) 

- !0.0 1CO ug 10·130 

t.IATRIX!IPI<E 

OUPIIU*CI 

toiATRIXSPOaii 

T .... _IA&l - !0.5 101 ug 10·130. 

lAJ30401 Tobii~(Be) - 53.0 100 . uu 70·130 

W.l>IXDUPIIU*CI 

'W.TRIX SPIKE 

Tobll Bot,6.m (!to) 

- ~ 100 "'I 70· 130 

(At3CNOI T .... Oodmbn (Od) 200eii>M2 2U 11<1 ug 10- 1-30 

toiATRIXSI'I<E 

.OUP (AI3040) 

IMTRIXSI'II<E 

Tobll ~ (Cd) ' 200MlOoOl :00 · 91 ug 10-t30 

lAJ3040) 

MAlRIXIIPII<E 

T .... o.omu..p) - 52.0 104' ug 70· 130 

DUP<m040) TOIII CI>R>n*.om (()) 

- e3J) ""' ug 70.130 

Mo\TRIXSAKE 

_, T .... IAod (I'll) - .. ., ill · og 70· 130 

lolo\l'RtXIIPII<E OUP (AI3040) TOIIIIAod ll'bl 

-

_..,.._ 

51Al 102 ug 70 · 130 

TCOII-IA&l 

- 48..5 at ug . 86-1t5 

0 llpbd-DIJP TCOII-~) 2001101102 su til) ug 15-115 

-- Tobll..,.._ (Bo) 

- 112.0 104 ug IS · 114 --OUP TCOII..,.... IJ!o) -2 114.0 :tOe ug es -ue 

-- Taloi~(Cd) - 2U 112 "'I 85-115 

- .81"" OUP T .... Oodmbn (Cd) 2001101102 21JI 915 ... 15·115 

-- T...,~(Q) 

- 51.5 103 ug &5·115 --DUP T .... a-..(0! 

- 52.0 104 ug 86-115 

-- TobiiiAod(Pb) - ~.5 11<1 .. 85-115 --DUP T .... IAod(Pb) 2001101102 .a.s llG ug 15·115 

-- TOIII-IA&l "''MtMi2 qj.AQ ug 

--DUPTotll-~) 2C-

- .. --· TCOII~(Be) 

- .oco.to ug 

--OUP TCOII-(1101 

- <0.10 ' ug 

-- obii~ (Od) · 200Ml8IQZ ..,.10 ug 

--DUPT .... Cdnium(Od) 2006IOem <0. 10 ug 

--· TOIII~(Q! - ..,.30 ug 

- -OUP TOOII Qwri.ooo (Q! 

- <0.30 ug 

-- TCOII Lood (AI) 2Ciolwllow qj.21) ug 

--OUP loW Lood (Pb) 

- <0.21) "'I "!'0 . ""'-~

- 2..5 ,. 20 

T""' 8or)6orl (!to) 

- NC " 20 

obii~(Cd) 200IIIOGI02 NC ,. 20 

Tobll.,.,...... (Q) - 2.6 ,. 20 

T-Lood (I'll) 

- OJI ,. 20 

1500032 N_R MAi'RoX'a..<E 

(AI3044) TOiai-CA>I ·- 60.5 101 ug 10. 130 

MATIIIXIPIICE 

DU!' (o'I304A) TOIII-CA>l· 

- . .., • ug 70·130 

WITRtX SPII<E. CN30'4) T .... .._(Be) 

- $1.0 102 ug 70· 130 

MATRIX SPtt<E 

DUP !AI304") 

W.lRtXSPI<E 

Tobii-(Bo) 

- $0.0 100 ug 70·130 

(N.!O<A) T .... Coohi.m (C4 . - 24.5 • ug 70 . 130 

c: • . -i 

__ 

' ... ___ • . Pt.goeora """''"_'"' _ _ __ ...,_,_,~ 1.71.- TC: (10<11:1>M710 TOO---- FIIIC~ 33.241 .. 

VES 003279 
( " \ 

.I 

() 

... . 

Ou.-y Assurance Report (Ccntlnued) 

......,.. Job Nllllrillr. GA817t4ol 

llUP IAI:I0<4) T-~(Cd) 

-

W.T'RIXSPI<E 

) T-~{CII) -

llUPIAI30<4) 

WI'TNXWITRIXSPt<E 

T-a.-..(Or) 

- -

WITRIXSPICE ) T*t.MCI'b) 

-

llUPIAI30<4) T*t.M(Pb) 

-

SplloadSplload-DUP T*-t'ol TGOII-t'o) 

-

- ----OU> r......,.....(llo) 

T .... ..,...{llo) 

-

-

- -~· ,...,-.,.(Cd) 

-----OU> 

S!lltod-OU> , Talli~ 

, 

.... .... ~(Ccl) ~101 

(Or) 

-

-

-

-

-- T-IAod Cl'bl 

------

--llUPT 

OUP Talli-(Ao) 

T 

TGOIIIAod 

.... 

.... 

_(Ao) 

..,...(lo) 

Cl'bl 

-

-

-

-

--CUP T .... llo!yiUn (llo) 

-

- -- , .... ~(Ccl) 

----

--llUPT-C.O.....(Cd) 

OU> 

' 

T

TobiiAod

TOIOI~{CII) 

OIOI Cl1tomiuln .(A>) (Or) 

-

-

-

-

20011011102 

--OUPT-IAod(l'l>) RPO Toiiii-(Ao) 

Talol 

Tolllllor)4bn(llo) 

~ (Ccl) 

-

-

- .... TOIOia...u.{CII) 

-

- ~ 

-

,'• 

23.1 85 

-.s ., 

oe.o 118 

4!.5 97 

<~e:O 112 

53.0 106 

53.5 101 

54.5 

51.0 

25.0 --

100 

25.0 100 

52.0 100 

$1.$ 107 

SI.O 1CI2 

!50.5 101 

~.:Ill 

~ 

4060 

~.060 

4060 

-

415 

415 

410 

410 

NC 

NC 

NC 

NC 

119 

... 

... 

... 

... 

... 

... 

"" ·"" "" uo 

'ug 

uo 

... "" 

.. 

... 

011 

uo 

"'I 

uo 

ug 

ug 

... 

"'I 

" " % 

" 

, • 130 

, • 130 

, _ 130 

, ·,130 

, ·130 

85 · 115 

85 · 115 

a5·11S 

15· 11S 

15· 115 

e5 · 115 ., .. 115 

85 · H5 

M - 115 

86 · 115 

20 

20 

20 

20 

., 

VES 003280 
M a ~~.IT.!-..:.....:.- -:-------- --------;"";:;::;;:=;;±:!1;; .... ;;'*"~;;-~.~-;- · 

c 

Maxxam Job 1: ABJI7144 

c • ' 

[ i ""' -----..-c..- L71.SK1. 

Pogo a ... • To* --T·.---- FlOC_.....,_ 

VES 003281 
c 

t' ; 

· 

Week of September 8, 2008 ., 

VES 003282 
'M a -;§1.~!:f.! --- - - -----"'----------......!""!!!!:'- !!!.!. ~ .... !':!!:l:'!!'"~_,!!!!.i!!""~'"="~ 

.Your Project#: 10002-022 

. Sile:CPT·VEOUA 

Atl!ntSon; Jeff Gorman 

ENSR lntamalional 

5015 Cempuswood Dr 

$o118104 

Ea$t Syracuse. NY 

USA 13057-4232 

Sample Mnl>c SAMPLING TRAIN 

II Sample& ReQeived:'8 

- F.H.In-+ -(6020)111 

~ERTFtcAJE OF NW.'(S!S 

• 

(1) This ...... pll'fclrmld by NII:JDrlt'D Anaf'(6c::a I 5 I ... 

(2)1tllstnt .. perfcmwdll'l.._t, 5 O''"*Ma:~ocam~scc ... : en 5 

Digitally 

signed by 

Mike Challis 

Date: 

2008.09.18 

15:23:50 

.()4'00' 

Tolal oover pages: 1 

~ ~tda 

Report Date: 20011M118 

--lsjo _...._ hlldCili'YII- an....- 50<15·----.,._- L71.11H7 Tot _,..,_711 TolfiM: --- Fooc:--11 

-

VES 003283 
0 

M a 6£;:;,~r;!;! --------------------- -"'"'"'"'H"-"'i'V'-' .... ='"'·eo:"'-="'·,·= 

ENSR. IIUmatlonal 

Clont PICjod II' 1 0002,(122 

P1ujec:l namo: CPT ·VEOUA 

EU!IIIEHJS BY ICPIIIS (SAMPU NG TRAIN) 

.... _(lie) Ull NO , a.o 2.9 2.3 111525i: 

*S.,...(Bo) Ull NO NO NO NO 1&15251j 

.... CocMJon (OdJ ug NO ND NO NO 181G25li 

.... ~(Q) Ull 0.81 125 14A 3.1 1.$ 18 

*'-'CPI>l .. D.21 45.5 4-5.1 . 1U 1.0 1815257; 

•Nol-

• ~latlt)o DNdlon Uml 

-· CoN!doOoi-(Aoj Ull 2.3 NO NO 

... ..,...,!Be) Ull NO NO ND 

*~PO Ull ND NO 2..$$ 

'""~Pl Ull 9.4 1.5 1&15257 0.17 0.44 0.15 1&1Sl70 

*'-(l'b) Ull 38.9 .1,0 1615257 NO 0.33 0.10 1&162'10 

·• Not- Rs;u..-o.cton Lhl 

-- Col*al-

..,_!All Ull NO .., 10 o.lO 1tiSZ10 

.... ..,...,(Bo) Ull NO NO ND .060 1815210 

oOolc..ium(C<I) Ull 2.81 2.601 2.02 .oeo 18162.70 

.... """"*"" (Q) I'll OM OA1 0.56 0.15 t01Q.1'0 

.... , "!J 0.32 0:0 0.40 0.10 1815210 

. ..,._ 

8llld'l ·-----~ • Clutllty Cc:JrM:II 8lk:tl 

Pogo2ofl 

-- --o.!o,C... L1LIH7 

VES 003284 
( 

•. Maxxam Job ., A8o'.2896 

. ~Detr. 20CNl109118 • 

TeStSu-.y 

-10 AU158 

-D-FH 

- SNoiPI.lNG l1WN 

-D Al3180 

S..,O.«> ~2-R1 fH 

. - SAMPUNG 1RAIN 

ua..n 1D AU181 

-D~FH 

-~TIWN 

_., AL3163 

-ID ~BBH 

- SA-.ING TRAIN 

~ ~3d8 

ENSR lnlematiooal 

Cleot Pn>joct., 1\)002-022 

Pn>joclnamo: CPT·VEOUA 

------~ L7LIIH7 T .. _._.. Tal.._ _____ ........ 

-; 

VES 003285 
(

- .. Ma>ocam Job #: A8A2896 

. ·Report 0.: 2008109118 

·. 

C"l 

.~· 

TestS......-y. 

- II A1..31114 oi., .......... M29-U2-R18H 

· .- SMIPUNO"IIWN 

ENSR~ 

Chnl Pn>jec:ll: 10002-o22 

Project ....,., CI'T·WOUA 

~-Slllppttl · -~· 

VES 003286 
'· 

• 

fv1 Ci~n~Y~--~----------------------------------------~a~·~~w~~~~~"~~~~s2'~ 

'. ENSR~ 

Clionl Pftlject ft. 10002-422 

~ .. me:CI'T-~ 

( ·· .

.. 

I!LI!M&IITS BY ICI'IMS jWIPUIG'11WN) 

-f.lt. nfllor+ RfnMis(I020):M_& __ -on-AU1tO-Q<lltO>I!O- Poot.---n~--on~AU~ · Tho-BIIdSjllto_.,lttow.&poot~--on 1!0-. .,... .... _.,.s • .,.~. 

Some--'$"'"-~ . . . . . . -e.tt.n~""".(t020t-Poot_...,_n~--"'...-po..uPbiW'IdCd ............. ~ ..... ~ '*"*-

. . 

. ( ; Pogo Sail 

___ ,_ ___ l'I\.IHI Tot -S1<M788 ·T .. - : (~Cq ......... _)3MIOI 

.· 

VES 003287 
M a.~.~ .. '!! ,..,.......,.~.-~~ . 

---·- : 

c Allenlian:Jei!Goiman 

Cllentf'IOjl<:t II: 10002~22 

P.O. I: Projod -=·CPT-VEOLIA 

Quaity Assurance RepOrt 

-JoO--~ CWQC 0.. 

::: .. CC'I'Yoo ~ - ~ cc~ 

1615257 N_R ""!~~$PIKE (AUIIIOI · T"""-(Aa! _,, 51.5 103 ug 70-100 

MA'IRX SPICE 

OU' jiiU180) ... ..__ T .... _(Aa) 200110a't7 51.0 10:1 "" . 70 ·100 

(AUIIO) 

... miXSPI<E 

y...,a.,._~) -1 1$3.5 107 "II 70-130 

DUP(AU110) TCIII ~ (llo) _,, 11:!1.5 107 "II 10-1!10 

IM'IlaXSPI<E 

IAUifO) 

... miX SPliCE 

T .... c.:onMo lCill 2Cl01101117 25.5 102 ug 10 - 1!10 

OU' (Al.3180) 

... 1101)( SPti<E T-~(C4) -17 .... 911 ug 7tl- t30 

(AUIIO) 

.... miXSPI<E 

TOOOI CIYoriMI (Ct) 200MIII17 41.5 · 81 ug 70-100 

DUP (AUIIO) 

MA.1RDC SPR 

TOIII Clwcmin tori -17 47.0 1M "" T0-1!10 

IAUIIO) T-I.Md~) 200110a't7 58.0 112 ug 10· uo ... TRI)( SPikE 

CUP (,'1.3180) T .... I.Md(pb) ~ ... 5 109 ug 70·130 

S!>bd- TOOOI-(Aa) _,, 38.0 71111> ug 811-IIS 

Sjlltod-Dl.P T .... - (A&) -.r 48.5 • "" !115-115 

0 8jlbd- TOIII-(IN) 20011011t7 3LO 711(1) "" 811-111 ---TOIII ....... (IN) 

_,, 41.0 • "" 15· 115 

-- TOIII CodmOon (Cdl 20CliiiOWt1 111.5 74 (1) ug 15- 115 

- -DI.P TOIOI ~(Cifl ' -7 23.8 1ICS ug 55·115 

-- Toooto.-ntor~ 200MIIIt7 37.0 74 (1) ug 85· 115 

---T-~torl 200M111117 47.5 !IS ug 811-115 

-- TOIIII.Md~) -17 37.5 711(1) "" 15- 115 --tllU' TOOOII.Md~) _.., 41.0 .. ug 15 - 115 

-- TOOII-(1.1) 200MIIIt7 NO, ROI."OAO ug 

--DUP TOIII-(Aa) 200M111117 NO,.RDV(IAO ug 

-- TOOOI...,...(Bo) _,, NO, RDloO.IO ua 

--OIJ>TOIII-(Bo) 20011011t7 NO. Rlll.ioo.IO ua 

-- TOIII~(I:d) 20011011t7 HD. Fll:)l.llll0.10 ua - -llU' TOOII Cad-(a! -1 NO, AOL=O.tO 

-- T""" etwoo;om~ tori "" 200M18117' NO, RDlo0-30 

--011' TOOOI Clwoniunl tori -17 "" NO. RDI.=O.:!O ug 

-- TOOOII.Md~) 20Q11101117 NO, RDloO.» ug --llU' OIIII.Md~) - 7 NO, f0.o0.20 ua 

RPO TOIII-(Aa) :!OI*M7 NC ' lO 

.,...._(llo) _,, NC ' 20 TCIII~(Cd) 200Ml8111 NC " 20 T-~(Cr) -17 14.8 " 20 

TOOOIL-(pb) 2110t109111 0.9 " 20 

1515210 NJI ... TRIX SI'I<E 

IAUI&I) 

MATRIX SPII<E 

TOIIINMnlc (Aa) -7 1$3.5 107 ua 10·130 

CUP (Al.3154) 

MATRIX SP1I<E T000l-(~) -11 eGA 101 ua TO · 130 

(AUISC) 

.... TRIX SPliCE 

TOIII!Ieo)lbo (8o) _.., 52.0 104 ug 70 .. 1.30 

OU' (Al.3154) 

W.TRI)( SPI<E 

TOOOI lleo)lbo (Bo) _., eGA 101 "" 70- 130 

(AL3154) TOIOI~(Cd) 20Clfl/08117 25.8 103 "" ro- 130 

() . __ ..... ___PlOt lol8 _ _,,._..,_ 

---R-.-..-,,_c..- 1.71.11H7 Tet: 4106)~711 TeiFN« (WCI),.....,. F.: (8015) .s.sM1e8 

VES 003288 
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(AUI&I) T*'~G'I>) 

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TOIOI-(,tot) 

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- - ou> Tolol llryiUn (ae) -- Tolll Cod!-. (Cdl • --DUP T .... __ (Cdl 

-- Tolol OW<nilm (Q) 

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--

~od-kOU' Tolol'-G'l>f Taiii'-(PI>) 

-- Talof-(,\0) 

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- -IU' T*...,..,. (llo) 

-- T*~!Cd) 

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--ou> TOIIIQwonbn(Q) 

-- Talll'-1(1'1>) 

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Page7,ol8 

ENSR....,...._ 

Ahon11on:Jd!Go<man 

CIOn! Pn>joct fl: IOOOM22 

P.O. fl: 

Project nne: CPT.VEOIJA 

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VES 003291 
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Week of August 11,2008 · 

VES 003292 
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(lel)llsma!S(fo>c)215-m-1293 Certillcate of Alialytlcal Resalts 

.CLI£NT: 

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Project: 

M.tuul Aa.lydt.J Sonit.eo 

55S5- s.nv. ... B..,._ o.tariO L7L 5111 

R030800SI 

A891648 

- PQL Ualts 

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lAb ID: . 'R0808005J.·OlA 

Date Sa.pled: OSIIJJ2008 0:00 Dale II«.Wed:. 08I26I200a 

Af73J+OtR\ HBIU-U2-R2 

lAb ID:: . R08080051-o2A 

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Date Soaplod: 01/1112001 0:00 Datc-..s: OII26IM08 

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HEATIIG VALUIIIl\M.B · 

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VES 003294 
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M a a~!!:! ------------''----_.:.--~!;;:;;=1:;.~'!ii.::iii.;''::os~-~;:;;-;-

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Al!!nt!on; Jt!f Goonan 

ENSR International 

11015 Campuswaod Dr. Sutte104 

East Syracuse, NY 

USA 130574232 

• 

Yoor Projecl ft. 1002-022 

~\/EOLIA 

. ~rt Dole: 20011'08125 

This report~ al pnMous repor!s wilh tile ..... M8xxam job .......... 

ceRifiCATJ! OfAHAL'tSIS · 

(1) TN~• .. ptrfcrmed by Maxa~M~Mllt1fca 'h'vP'Ip 

(2) ~~does 1'01: hdd .,....tdla:liui l:Jr .....-af n'IMIII., .,...~ '*'0 tw IC'P Adll rlllllt""**'Vf. 

Tolal.....,_l 

Digitally 

signed by Mike 

~~0\allis M~-"'-m 

~ Date: 20080825 

10:19:15 .()4'00' 

nil~ iiJ '! efllc:ttonil: toan.t. IWd wvt is aYliletlle Cn ...-sl 

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VES 003298 
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(

. Muxom Job 11: A8911148. · . Report o.te: 2008100125 . 

Ciont PYojed It; 1 OQ2.0Z! 

Pnijod name: VEOUA 

RESULTS OF ANAL YSJiS Of LIQUID 

- . a..yConi!OIr .. 

l 

· ... 

Pogo2ol14 

.. , 

VES 003299 
SES Standards 

CE 1: Leading Change 

ARD Branch Chiefs' Quarterly Report 

FY2015, I" Quarter Update 

• Successfully assumed responsibility for air sub-lead Region for tribes, leading an effort 

with OAR to include tribal air quality goals comprehensively in National Program 

Guidance and establishing new processes and procedures for the Regional Tribal Air 

Coordinators group to better support OAR and the tribal air program. (APB) 

• 

CE 2: Leading People 

• 

• 

CE 3: Business Acumen 

• 

• 

CE 4: Building Coalitions 

• 

• 

CE 5: Results Driven [an)1hing not already covered by SES measures in ARD Workplan] 

• Manages .thnding such that ARD provided over 25% of the FY 2015 air grant allocation 

to states to support their air pollution control programs without interruption in flow of 

funds, despite uncertainty of available funds and funding levels (APB) . 

• 

Organizational Assessment 

Key Events/Issues/Challenges and. Management Actions 

.. 

• 

Accomplishments that Support FY2014 Cross-Agency Strategy Action Pla11S 

-A New Era of State, Tribal, Local, and International Partnerships: