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Exhaust Emissions Sampling 

Daltile, Conroe, TX 

Kiln Scrubber Inlet and Exhaust 

August 23, 2005 

TCEQ Permit No. 21283 

Armstrong Environmental, Inc. 

Project W-2471-05 

Report Prepared For: 

Bob Hurt 

Daltile 

7834 C.F. Hawn Freeway 

Dallas, TX 75217 

Report Prepared August 26, 2005 By: 

Armstrong Environmental, Inc. 

7715 Sovereign Row 

Dallas, Texas 75247 

(214) 631-0021 
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I. Introduction 

II. Summary 

III. Procedures 

IV. Appendices 

TABLE OF CONTENTS 

A. Calculation Summaries 

B. Continuous Emissions Monitor Summaries 

C. Analytical Summaries 

D. Field Data Sheets 

E. Equipment Calibrations 

F. Standard Gas Certifications 

G. S02 Interference Check 

H. Resumes 

Page 

I 

2- 5 

6- II 

12- 17 

18- 51 

52- 114 

115-125 

126- 138 

139- 147 

148-187 

188-191 
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I. INTRODUCTION 

A series of tests was performed on the inlet and exhaust ducts associated with the Kiln 

Scrubber (EPN 29) at the Daltile facility in Conroe, TX on August 23, 2005. 

The purpose of this test series was to determine the exhaust emission rate of Particulate, 

CO, NOx, VOC, S02, HF, HCJ, and Opacity, and the removal efficiency ofHF and HCl 

as required by the Special Condition 13 of TCEQ Permit 21283. 

Testing followed procedures detailed in Title 40: Code of Federal Regulations ( 40:CFR). 

Sampling was performed by Richard Taylor, Dan Barrera and Tom Armstrong of 

Armstrong Environmental, Inc. using two Apex Method 5 sampling trains, an EcoPhysics 

70S continuous NOx analyzer, a Fuji 3300 continuous CO analyzer, a Western Research 

721-AT continuous S02 analyzer, and a ThermoEnvironmental 51 continuous FID 

analyzer. 

Present during the test series was Cedric Flemming and Thomas J. Bill of TCEQ. 

Three one hour test repetitions were performed, commencing at 12:05 PM and ending at 

3:15PM. 

om Armstrong 

President 

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II. SUMMARY 

A series of tests was performed on the inlet and exhaust ducts associated with the Kiln 

Scrubber (EPN 29) at the Daltile facility in Conroe, TX on August 23, 2005. 

Sampling was performed following procedures detailed in Title 40: Code of Federal 

Regulations. 

Results of this test series are summarized in Tables I & 2. 

Results indicate the following emission rates: 

Run# 1 2 3 Averae;e 

Exhaust PM, lbs/hr 3.186 2.793 2.295 2.758 

Permit Allowable, 4.43 4.43 4.43 4.43 

lbs!hr 

Exhaust CO, lbs!hr 7.332 8.151 8.603 8.029 

Permit Allowable, 9.59 9.59 9.59 9.59 

lbs!hr 

Exhaust NOx, 3.319 3.175 3.025 3.173 

lbs/hr 

Permit Allowable, 1.72 1.72 1.72 1.72 

lbs!hr 

Exhaust VOC as 0.664 0.695 0.765 0.708 

C3H8, lbs!hr 

Permit Allowable, 0.42 0.42 0.42 0.42 

lbs/hr 

Exhaust S02, 0.197 0.080 0.11 7 0.131 

lbs!hr 

Permit Allowable, 9.67 9.67 9.67 9.67 

lbslhr 

Inlet HF, lbslhr 5.704 6.732 5.135 5.857 

Exhaust HF, lbs!hr 0.0155 0.0128 0.0163 0.0!49 

Permit Allowable, 0.56 0.56 0.56 0.56 

lbslhr 

Removal 99.73 99.81 99.68 99.75 

Efficiencv, % 

Permit Allowable, % 95 95 95 95 

Inlet HCl, lbs!hr 10.028 I 0.955 9.076 I 0.020 

Exhaust HCI, 0.0200 0.0240 0.0271 0.0237 

!bs/hr 

Pemlit Allowable, 0.41 0.41 0.41 0.41 

!bs!hr 

Removal 99.80 99.78 99.70 99.76 

Efficiency, % 

Permit Allowable,% 95 95 95 95 

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Results indicate this source to be in compliance with the emission requirements of Permit 

21283 with the exception ofNOx and VOC. 

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SUMMARY OF EMISSIONS TEST DATA 

Table: 1 

Plant : Daltile, Conroe, TX 

Location : Scrubber Inlet 

Operator : T. Armstrong, D. Barrera 

Test Date : 23·Aug·05 

Repetition : 1 2 

STACK GAS 

Temperature, F 379.3 368.4 

Velocity, fps 46.71 47.08 

Volume Flow, acfm 35220.2 35496.5 

scfm 19816.5 20074.8 

scfh 1188989 1204489 

Moisture, % 7 92% 865% 

C02,% 2.00 2.00 

02,% 18.00 18.00 

SAMPLE 

Start Time, hrs:min 9:30AM 11:45 AM 

Finish Time, hrs:min 10:40 AM 12:56 PM 

Sample Volume, set 36.106 36.101 

lsokinetic Ratio,% 102.5384 101.2037 

HYDROGEN FLUORIDE 

Sample Weight, mg 78.55 91.51 

Concentration, ppm 92.3907 107.6506 

Emissions, lbs/hr 5 70361 6. 7.32291 

HYDROGEN CHLORIDE 

Sample Weight, mg 138.11 148.91 

Concentration, ppm 89.01!13 95.98621 

Emissions, lbs/hr )0.02833 10.95515 

4 

3 

367.8 

46.63 

35156.5 

19999.2 

ll99953 

820% 

2.00 

18.00 

1:35 PM 

2:44PM 

35.604 

100.1869 

69.10 

82.42318 

5.135199 

122.13 

79.82351 

9.076149 
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SUMMARY OF EMISSIONS TEST DATA 

Table : 2 

Plant : Daltile, Conroe, TX 

Location : Kiln Scrubber Exhaust 

Operator: R. Taylor, T Armstrong 

Test Date : 23-Aug-05 

Repetition : 

STACK GAS 

Temperature, F 

Velocity, fps 

Volume Flow, acfm 

Moisture, % 

C02,% 

02,% 

Opacity, % 

SAMPLE 

scfm 

seth 

Start Time, hrs:min 

Finish Time, hrs:m1n 

Sample Volume, scf 

lsokinetic Ratio,% 

PARTICULATE 

Front Half ;~ 

Sample Weight, mg 

Concentration, gr/scf 

Emiss·lons, lbs/hr 

Back Half 

Sample Weight, mg 

Concentration, gr/scf 

Emissions, lbs/hr 

Total Particulate, lbs/hr 

CARBON MONOXIDE 

Concentration, ppm 

Emissions, lbs/hr 

NITROGEN OXIDE AS N02 

Concentration, ppm 

Emss1ons, lbs/hr 

VOC AS C3H8 

Concentration, ppm as C3H8, WET 

Concentration, ppm as C3H8, DRY 

Emissions as C3H8, lbs/hr 

Emissions as Carbon, lbs/hr 

SULFUR DIOXIDE 

Concentration, ppm 

Emissions, lbs/hr 

HYDROGEN FLUORIDE 

Sample We1ght, mg 

Concentration, ppm 

Emissions, lbs/hr 

HYDROGEN CHLORIDE 

Sample Weight, mg 

Concentration, ppm 

Em1ss1ons, lbs/hr 

138.0 

29.41 

28065.5 

20407.1 

1224428 

17.02% 

),50 

18.50 

0.00 

9:30AM 

10:35 AM 

4!.328 

100.9787 

47.88 

0.017876 

3.127912 

0.89 

0.000332 

0.058142 

3.186054 

82.38 

7.332075 

22.7 

3.31918 

3.94 

4.748188 

0.664091 

0.543347 

0.969 

0.197!29 

0.237 

0.243541 

0.015483 

0.307 

Q, 172862 

0.020056 

2 

137,8 

30.30 

28909.6 

20973.3 

1258397 

17.24% 

),50 

18.50 

0.00 

1!:45 AM 

12:50 PM 

42.735 

10),599 

39.28 

0.014182 

2.550425 

3.74 

0.00135 

0.242836 

2 79326 

89.11 

8.151096 

2U3 

3 17533 

4.00 

4.833125 

0.694724 

0 568411 

0.383 

0.080077 

0.197 

0.19577 

0.012791 

0.369 

0.200929 

0.023959 

5 

3 

137,2 

30.25 

28862.9 

211730 

1270380 

16.40% 

),50 

18.50 

0.00 

!35 PM 

2 40 PM 

42.679 

100.5079 

34.13 

0.012339 

2.240091 

0.84 

0.000304 

0.055133 

2.295223 

93.16 

8.602703 

19.94 

3 025035 

4.41 

5.275258 

0,765498 

0626316 

0.552 

0.1165ll 

0.248 

0.246776 

0.016277 

0.413 

0.225185 

0 027!07 
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III. PROCEDURES 

The procedure for emissions sampling followed USEPA test methods as detailed in Title 

40: Code of Federal Regulations. The following methods were used: 

Method 

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2 

3 

5 

6C 

7E 

9 

10 

25A 

26A 

Title 

Sample and Velocity Traverses for Stationary Sources 

Determination of Stack Gas Velocity and Volumetric Flow Rate (TypeS 

Pitot Tube) 

Gas Analysis for the Determination of Dry Molecular Weight 

Determination of Particulate Emissions from Stationary Sources 

Determination of Sulfur Dioxide Emissions from Stationary Sources 

(Instrumental Analyzer Procedure) 

Determination of Nitrogen Oxides Emissions from Stationary Sources 

(Instrumental Analyzer Procedure) 

Visual Determination of the Opacity of Emissions from Stationary 

Sources 

Determination of Carbon Monoxide Emissions from Stationary Sources 

Determination of Total Gaseous Organic Concentration using a Flame 

Ionization Analyzer 

Determination of Hydrogen Halides and Halogens Emissions from 

Stationary Sources 

02 and C02 were determined using PyRite Analyzers. A single grab sample was taken 

on the inlet location during each run. An integrated bag sample was taken on the exhaust 

via a peristaltic pump from the CEMS pump for each run (the pump was turned off 

during port changes). 

PM. HF and HCl sampling was performed on the scrubber exhaust for 2.5 minutes at 

each of 24 points, 12 points per traverse, making a total run duration of 60 minutes. A 

schematic ofthe sampling location is shown in Figure 2. The sampling train was 

configured as follows: 

Glass Sampling Nozzle 

Heated Glass Lined Probe 

Heated teflon filter 

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lmpinger #1 - 100 mls H20 

Impinger #2 - I 00 mls 0.1 N H2S04 

Impinger #3 - I 00 mls 0.1 N H2S04 

lmpinger #4 - Empty 

lmpinger #5 - 200 grams silica Gel 

Analysis for PM was performed on the probe wash, filter, and solution from the first 

impinger. HF and HCl analysis was performed on an aliquot from the first impinger, and 

the solution from the 2nd and 3rd impingers. Analysis was performed using a Dwnex 

LC20 IC/HPLC. 

HF sampling was performed on the scrubber inlet for 4 minutes at each of 16 points, 8 

points per traverse, making a total run duration of64 minutes. A schematic of the inlet 

sampling location is shown in Figure 1. The sampling train was configured as follows: 

Glass Sampling Nozzle 

Heated Teflon Lined Probe 

Heated Flexible Teflon Sample line 

Heated Teflon Filter 

Impinger #I - I 00 mls 0.1 N H2S04 

lmpinger #2- I 00 mls 0.1 N H2S04 

lmpinger #3 - Empty 

Impinger #4- 200 grams silica gel 

HF and HCl analysis was performed on the solutions from the 1st and 2nd impingers. 

Continuous emission monitors were operated according to the following parameters: 

Component Monitor Actual Scale . Calculation Standards 

Scale 

co Fuji 3300 SN 0 -500 0-200 99J ppm, 200 

MC0303 ppmCOinN2 

EPA Protocol I 

NOx EcoPhysics 70S 0- 100 0- 60 25.5 ppm, 51 ppm 

SN 8350095 NOx mN2 EPA 

Protocol 1 

voc TECO 51 0- 100 0- 60 15.2 ppm, 28.8 

SN 5!-39764-261 ppm, 48.8 ppm 

C3H8 in Air EPA 

Protocol I 

S02 Western Research 0- 110 0- II 0 50.1 ppm, 101 

721- AT ppm S02 in N2 

SN W72!-8846-l EPA Protocol I 

A schematic of CEM configuration is shown in Figure 3. Actual scale is the scale the 

monitor 'vas operated at. Calculation scale is the scale used in Equat1on 6C and to 

calculate drift and bias. The CO monitor was operated following the calibration and 

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operating parameters given in Method 6C, with no ascarite or silica gel used up front of 

the analyzer. This deviation was addressed in the sampling protocol and the pretest 

meeting. 

A S02 interference check was performed on the same process (Roller Kiln Scrubber) at 

the Dallas facility ofDaltile on July 9, 2003 using the same S02 monitor. The 

interference check in included in Appendix G. 

A NOx converter check was performed the morning of 8/23/05 using the 51 ppm NOx in 

N2 gas standard and is included in Appendix B. 

Opacity readings were taken over 6 minute intervals between each test repetition. 

8 
ure 1 - Kiln Scrubber Inlet 

// 

. \ 

0 " (, ' 

0 - 3 4 6 7 s\ 

24ft. 17 ft. 

- - -·- -

J 

stack Diameter - 48 inches 

Point #1 - 1 .5 inches Point #2 - 5.0 inches 

Point #3- 9.3 inclies Point #4 -15.5 inches 

Point #5 - 32.5 inches 

Point #6- 38.7 inches 

Point #7 - 43 inches Point #8 - 46.5 incties 

- - - -

0' 

- - - - - -
 - Scrubber Exhaust 

- - - -

CEMS Traverse 

/ ""-.. / 

/ \ ,/ ,, \ 

\ 

/-

/ 7 i.l 9 10 11 1 

\ . I / \ \ / \ \ / .. , 

"'"'-...._ / . / "'..._ 

Stack Diameter - 54 

Point Atl - 9 inches Point #:2 - 27 inches Point #3 - 45 inches 

stack Diameter - 54 inches 

Poin11t1 - ·1.-1 inches 

Point tt-2 - 3.6 inches 

Poirrt #3 - 6 A inches 

Poirrt #4- 9.6 inct·1es 

Point #S- B.5 inches 

Point #6- inches 

Point #7- 24 7 inches 

Point ttf1 - 4(1 .5 inches Point #9 - 44.4 inches 

Pointlt10- 47.6 inches 

Point lt11 . 50.4 inches Point #-12 - 52 inches 

_/_ .. /· 

- - - - - -

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- - - -

0 

.--< 

-
 3- CEM Configuration 

Heated Prob 

Heated 

Sample 

e 

Line ::=_ l 

1 n 

FlO Analyzer 

Pump 

t J Heated Manifold I 

Pump J 

Sample 

Processor 

pan Line 

I 

Pump micron filter 

- - - - - -

rCO Analyzer 

NOx Analyzer 

S02 Analyzer 

Flowmet er 

Calibration Poin1 

prng owed by a 0.3 

- - - - - - - - -
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I Appendix A 

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PLANT: 

DATE: 

PLACE: 

RUN#· 

EMISSION TEST SUMMARY 

':2:7-:c,_ ::::-')11 ''"' -y 

:::3-,::,ur~-o~ 

Srrul"Jh"' lniP.i 

64 LIQUID COLLECTED (mls) TEST DURATION (MINUTES)· 

NOZZLE DIAMETER (INCH.) 

METER COEFFICIENT (Y) 

PiTOT COEFFICIENT (Cp) 

GAS METER VOL.(Cu.Ft.) 

BAROMETRIC PRESSURE 

0.253 PARTICULATE WEIGHT (Front halt mg): 

0.991 PARTICULATE WEIGHT (Back hall mg) 

8.8'1 STATIC PRESSURE (1n H20) 

33.152 PERCENT C02 

29 :-' PERCENT 02 

PERCENT CD 

FOR CIRCULAR STACK 

STACK DIAMETER (inch)· 

STACK AREA (Sq.Ft.) 

NOZZLE AREA (teet): 

FOR RECTANGULAR STACK 

48 STACK LENGTH(1nchs) 

12.56637 STACK WIOTH(inchs) 

0 000349 STACK AREA (Sq ft.) 

ENTER THE STACK AREA SHOWN ABOVE· 

FLOWS 

SAMPLED VOLUME (STD. CU.FT.): 

VOLUME OF WATER VAPOR (STD. CU. FT.) 

FRACTIONAL MOISTURE CONTENT(%) 

DRY BASE 

MOLECULAR WT OF STACK GAS (DRY BASE): 

MOLECULAR WT. OF STACK GAS (WET BASE)· 

STACK PRESSURE (mch Hg)· 

STACK GAS VELOCITY (It/sec.): 

ACTUAL STACK GAS FLOW RATE (ACFM): 

STANDARD STACK GAS FLOW RATE (SCFH): 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF). 

PARTICULATE CONCENTRATION (LBS/SCF)· 

PARTICULATE EMISSION (LBS/HR) 

BACK HALF 

PARTICULATE CONCENTRATION (GR.!SCF): 

PARTICULATE CONCENTRATION (LBS/SCF)· 

PARTICULATE EMISSION (LBS/HR) 

ISOKII~ETIC RATIO(%)· 

POiiHS STACK T DELTA P SQUAR D_P 

der; F 

382 0 40 0.632456 

2 385 0.53 0.728011 

3 386 C.SC 0.707107 4 384 0 46 0.678233 

5 38:! C Li I 0.685565 

6 38C CJ .;_5 0.67082 

7 383 0 43 0.655744 

8 352 c•.27 0.519615 

9 381 C•.32 0.565685 

10 386 0.41 0.640312 

11 385 G' 49 0.7 

12 384 J 46 0.678233 

13 383 0 3S 0.616441 

14 379 0.3E 0.6 

15 37S 0.36 0.6 

!6 355 c- 36 0.6 

379 25 0 6424 

12 56637 

DELTA H 

:::. 90 

J .2Q 

i 10 

l GO 1 . 0 

~ DC 

Q07 

0.6'-

0 72 

0 92 

1 l ~:;. 

; 00 

0.86 

0.81 

0.2J 

o s; 

0.9319 

36.1063 

3 1066 

0 0792 

80.0000 

29 0400 

28.1654 

29.0603 

46.7122 

35220.1985 

1188988.98 

0.0000 

0 OOE+OO 

0.0000 

0.0000 

O_OQE ... QO 

0 0000 

102 5384 

METER T 

INLET 

5~ 

86 

89 

90 

91 

92 

92 

93 

89 

93 

95 

96 

96 

96 

96 

9~-

92 1250 

METER T. 

OUTLET 

34 

84 

34 

85 

25 

86 

87 

27 

29 

89 

89 

90 

90 

91 

:?1 

g, 

87.6250 

66 

0 

8 7 

0 

Meter 

Volume 

695.9 

698.2 

700.9 

703.6 

706.1 

708.4 

711.1 

713.6 

715.49 

717.6 

719 9 

722.6 

725.1 

727.4 

729.6 

731.8 

7 34 052 

89.8750 

Po1nt 

VMSTO 

2 2 

2.5798 

2.5721 

2.3766 

2.185 

2.5597 

2 3678 

]_ 7868 

1 999 

2.1722 

2.5464 

2.353 

2 164 

2 0678 

2.0678 

2.1167 

Pomt Po1nt Point I so 

Velocrty Mo,sture 

ml' 

46.0652 4.02686 101.7121 

53.1194 4.72201 103 7999 

51.6246 4. 70789 106.6119 

49.4581 4.35012 102.5824 

49.9335 3.99945 93 1937 

48.8015 4.68529 111.4422 

47.7898 4.33397 105.6439 

37.1661 3.27059 98 7419 

41.1775 3.65894 103.2660 

46.7481 3.9759 99.4279 

51.0756 4 66098 106.5582 

49 4581 4.30685 101.5621 

44.9255 3. 96094 102 7068 

43.6234 3. 78483 100 5902 

43.5974 3.78483 :t 00 5302 

43 074 3 87429 101 6710 

1" (... 
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PLANT · 

JATE 

PLACE 

RUN# 

2.3-i,._;g 'J:i 

s::~. , :),. .. ·. ,_,t 

EMISSION TEST SUMMARY 

TEST DURATION 64 LIQUID COLLECTED (mls) {MINUTES) 

NOZZLE DIAMETER (INCH.) 

METER COEFFI Cl ENT (Y) 

PITOT CDEFFICI ENT (Cp) 

GAS METER VOL.(Cu.Ft) 

BAROMETRIC PRESSURE 

CL253 PARTICULATE WEIGHT (Front half mg) 

:; 991 PARTICULATE WEIGHT (Sack halt mg). 

0.84 STATIC PRESSURE (In H20) 

33 6LS PERCENT C02 

29 7 PERCENT 02 

PERCENT CO 

FOR CIRCULAR STACK 

STACK DIAMETER (inch): 

STACK AREA {Sq Ft.) 

NOZZLE AREA (feet) 

FOR RECTANGULAR STACK 

<:8 STACK LENGTH(Inches) 

12.56637 STACK WIDTH(inches) 

0.000349 STACK AREA (Sq Ft.) 

ENTER THE STACK AREA SHOWN ABOVE 

FLOWS 

SAMPLED VOLUME (STD CU FT) 

VOLUME OF WATER VAPOR (STD. CU.FT) 

FRACTIONAL MOISTURE CONTENT(%): 

DRY BASE: 

MOLECULAR WT_ OF STACK GAS (DRY BASE): 

MOLECULAR WT. OF STACK GAS (WET BASE): 

STACK PRESSURE (inch Hg): 

STACK GAS VELOCITY (ft/sec.): 

ACTUAL STACK GAS FLOW RATE (ACFM): 

STANDARD STACK GAS FLOW RATE (SCFH) 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR /SCF): 

PARTICULATE CONCENTRATION (L8S/SCF) 

PARTICULATE EMISSION (LBS/HR) 

BACK HALF 

PARTICULATE CONCENTRATION (GR./SCF): 

PARTICULATE CONCENTRATION (LBS!SCF)· 

PARTICULATE EMISSION (lBS/HR) 

!SOKINETIC RATIO(%)· 

POINTS STACK T DELTA P SQUAR D.P 

deg F 

1 373 0 49 0.7 

2 373 0 51 0.714143 

3 373 0 48 0.69282 

4 373 0 44 0.663325 

5 37~ 0 -"13 0.655744 

6 373 0.41 0 640312 

7 366 0.42 0.640312 

8 3CO 0.26 0.509902 

9 361 0 .',.6 0.678233 

10 370 i) 52 0.72111 

11 370 c 47 0.685565 

12 370 0 4-3 0.655744 

13 368 0.4] 0 640312 

14 369 (Hl 0.640312 

15 366 c ::07 0.608276 

16 352 c·.32 0.565685 

368.375 0 6507 

DELTA H 

LO 

:.20 

lW 

LOO 

0.97 

0.92 

0 02 

c 55-

LOC· 

~ 2C 

; 

0 97 " 

0 92 

0 92 

C· S4 

C. 72 

0 9669 

36.1008 

3 4173 

0.0865 

80.0000 

29_0400 

28.0853 

29.0603 

47.0787 

35496 473 

1204488.88 

0.0000 

0 OOE+OO 

0.0000 

0 0000 

0.00£+00 

0.0000 

101.2037 

METER T 

INLET 

S3 

?5 

?7 

93 

£•9 

99 

JOG 

1GC' 

98 

100 

lO! 

!OJ 

iOl 

101 

lG1 

1C 1 

99 0625 

METER T 

OUTLET 

~13 

93 

93 

9¢ 

94 

95 

S5 

os 

96 

96 

% 

90-

97 

'?I' 

97 

97 

95 2500 

2 7 

18 

0 

Meter Po,nt Point PoH:t Po:r~t ! so 

Volume VMSTD VelOCity Mo1sture 

m!s 

734.1B8 2 459 50 7838 4_951754 102 B311 

736.8 2 4439 51.8099 4.921323 100.1752 

739.4 2.43B9 50.2629 4.911243 103.0467 

742 2.3403 4B.1231 4.712692 103.2776 

744.5 2.2445 47.516 4 5197B4 100_Q74B 

746.9 2.2422 46 4536 4.515169 102.5051 

749.3 2.2402 46.258 4.51112 101.98!9 

751 7 1.7273 36 7027 3 47B243 98.3B32 

753.552 2.3B09 48.B49 4. 794552 102.0191 

756_] 2.4264 52.221 4 88604¢ 9831B6 

758.7 2 4236 49 647 4.B80465 103.2980 

761 3 2.2364 47.4874 4 503599 99.6564 

763 7 2.2342 46 314 4 499015 101 B313 

766.1 2 2342 46.3419 4.499015 101 8928 

768.5 2 0476 43.9436 4.123282 9R1235 

770.7 1 9874 40.6683 4 002145 102 9143 

772.B36 

97.1563 

13 
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I 

I 

I 

I 

I 

I 

I 

I 

I 

I 

I 

I 

I 

PLANT· 

DATE: 

PLACE 

RUN;<~ 

Da';~l,~ (;,')11• Ct' 

23-IA'-\ C5 

EMISSION TEST SUMMARY 

64 LIQUID COLLECTED (mls) TEST DURATION (MINUTES) 

NOZZLE DIAMETER (INCH.) 

METER COEFFICIENT (Y) 

PITOT COEFFICIENT {Cp) 

GAS METER VOL_(Cu.Ft.) 

BAROMETRIC PRESSURE 

C253 PARTICULATE WEIGHT {Front half mg) 

D.99!. PARTICULATE WEIGH-:- (Sack halt mg} 

0.84 STATIC PRESSURE (in H20) 

33 363 PERCENT C02 

29 7 PERCENT 02 

PERCENT CO 

FOR CIRCULAR STACK 

STACK DIAMETER (inch) 

STACK AREA (Sq_Ft.) 

NOZZLE AREA (feet) 

48 

12.56637 

0 000349 

ENTER THE STACK AREA SHOWN ABOVE 

FLOWS 

SAMPLED VOLUME (STD. CU_FT.)· 

VOLUME OF WATER VAPOR {STD. CU. FT.) 

FRACTIONAL MOISTURE CONTENT(%)· 

DRY BASE 

MOLECULAR WT. OF STACK GAS (DRY BAS::): 

MOLECULAR WT. OF STACK GAS (WET BASE) 

STACK PRESSURE (inch H~o::): 

STACK GAS VELOCITY (ttl sec.)· 

ACTUAL STACK GAS FLOW RATE (ACFM): 

STANDARD STACK GAS FLOW RATE (SCFH) 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF): 

PARTICULATE CONCENTRATION (LBS/SCF) 

PARTICULATE EMISSION (LBS/HR) 

BACK HALF 

PARTICULATE CONCENTRATION (GR./SCF)· 

PARTICULATE CONCENTRATION (LBS/SCF) 

PARTICULATE EMISSION (LBS/HR)· 

ISOKINETIC RATIO(%) 

POINTS STACK T DELTA P SQUAR D P 

deg F 

365 0.43 0.655744 

2 372 J.48 0.69282 

3 371 0.47 0.685565 

4 37: 0.45 0.67082 

5 371 0 45 0.670B2 

6 372 = 43 0.655744 

7 367 G 4-l 0 640312 

8 352 '::'.?7 0 519615 

9 3G7 Ci 49 0. 7 

10 37? C.51 0 714143 

11 37? 8.19 0.7 12 ~~- c £: 0.640312 

13 373 0.39 0.6245 

14 37! -:us 0.6245 

15 365 G.32 0.565685 

16 3:: ~ C.3? 0.565685 

367.75 0 6454 

fOR RECTANGULAR STACK 

STACK LENGTH{mches) 

STACK WIUTH(1nches) 

STACK AREA (Sq.F! l 

12 ')6h37 

DELTA H 

0 97 

l lJ 

1.10 

1.00 

i 00 

0.97 

0 92 

c 6~ 

J 18 

: ;_)(-

J J.C 

:J 92 

0 33 

c 8.'3 

() 7:; 

:; 72 

0 9513 

35.6036 

3.1819 

0.0820 

80.0000 

29.0400 

28.1343 

29.0676 

46.6278 

35156.515 

1199952 96 

0.0000 

0 OOE+OO 

0.0000 

0.0000 

0 OOE+OO 

0 0000 

100 1869 

METER T 

IN LEi 

96 

93 

;oo 

101 

102 

102 

1C3 

iQj 

; 02 

105 

:o5 

JC{) 

lOS 

206 

~:)6 

l:Jf 

102 9375 

METER T 

OUTLET 

96 

96 

96 

97 

97 

97 

93 

93 

~«;. 

99 

~OJ 

]00 

JQ1 

;c:c 

lOl 

lJ: 

98 5625 

67 

0 

8 6 

0 

Meter 

Volume 

772.955 

775.4 

777.9 

780.5 

783 

785.8 

787.9 

790.3 

792 225 

794.8 

797.5 

800 

802.4 

804.8 

807 1 

809 2 

811.318 

t:##ti#t:-:;;; 

Po1n1 

VMSTJ 

2.2886 

2.3367 

2.4258 

2.3277 

2 6047 

1.9534 

2.2282 

1 7858 

2.3917 

2.5018 

2.3138 

2.2183 

2.2161 

2.1238 

1 9385 

1.9549 

Point Po:nt Pc;,nt isc.-

Veloctty MOISture 

ml; 

4 7 2969 4 351202 101.2573 

50.1827 4 44252 98.2641 

49.6274 4.611941 103 0290 

48.56 4 425533 101.0378 

48.56 4 952167 123 0613 

47 4972 3 71385 86.7913 

46 2398 4.236305 101.0816 

37 1819 3.395267 98 9223 

50 ::502 4.547223 99.2488 

51 7271 4 75641 102 0658 

so. 7027 4.399082 96.3053 

46 3515 4.2~ 7493 100.8759 

45.2612 4.213335 103 4524 

45.2069 4 037779 99.G228 

40 826 3.685484 99 4796 

40 4536 3 716798 99 4097 

11 
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PLANT: 

DATE: 

PLACE . 

RUN#: 

EMISSION TEST SUMMARY 

C)Cl!t;i", Cow<::-P TY 

L.:J·klf.;-05 

~.il:' Sc~unlw' Exh<,ust 

1 

TEST DURATION (MINUTES): 60 LIQUID COLLECTED (mls) 

NOZZLE DIAMETER (INCH.): 

METER COEFFICIENT (Y) 

PITOT COEFFICIENT (Cp) 

GAS METER VOL.(Cu.Ft.) 

BAROMETRIC PRESSURE 

0 3123 PARTICULATE WEIGHT (Front hall mg) 

0 995 PARTICULATE WEIGHT (Back hall mg): 

0.84 STATIC PRESSURE (in H20): 

4.3.89 PERCENT C02 

29 7 PERCENT 02 

PERCENT CD 

FOR CIRCULAR STACK 

STACK DIAMETER (Inch)· 

STACK AREA (Sq Ft.) 

NOZZLE AREA (feet): 

FOR RECTANGULAR STACK 

54 STACK LENGTH(inchs) · 

15 90431 STACK WIDTH(inchs) 

0.000532 STACK AREA (Sq. Ft.) 

ENTER THE STACK AREA SHOWN ABOVE· 

FLOWS 

SAMPLED VOLUME (STO CU.FT) 

VOLUME OF WATER VAPOR (STD. CU_FT_) 

FRACTIONAL MOISTURE CONTENT(%) 

DRY BASE 

MOLECULAR WT. OF STACK GAS (DRY BASE): 

MOLECULAR WT. OF STACK GAS (WET BASE)· 

STACK PRESSURE (inch Hg): 

STACK GAS VELOCITY (ft!sec.)· 

ACTUAL STACK GAS FLOW RATE (ACFM): 

STANDARD STACK GAS FLOW RATE (SCFH)· 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR_!SCF): 

PARTICULATE CONCENTRATION (LBS/SCF) 

PARTICULATE EMISSION (LBS/HR): 

BACK HALF 

PARTICULATE CONCENTRATION (GR_ISCF)· 

PARTICULATE CONCENTRATION (LBS/SCF): 

PARTICULATE EMISSION (LBS/HR): 

ISOKINETIC RAT!O (%)· 

POINTS STACK T. DELTA P SQUAR D_P 

deg F 

1 137 .]_31 0 556776 

2 138 0_33 0.574456 

3 139 0.32 0.565685 

4 139 0 29 0.538516 

5 ]39 C' 28 0.52915 

6 138 0 21 0.458258 

7 :38 0.20 0.447214 

8 ~ 38 0.19 0.43589 

9 138 0 lS 0.424264 

10 138 0 14 0.374166 

11 138 0.10 0.316228 

12 Ll3 o_os 0.282843 

13 138 0 20 0.447214 

14 137 0.2; 0.458258 

15 138 0.20 0.447214 

16 135 0.19 0.43589 

17 138 0 2C 0.447214 

18 138 0.20 0_447214 

19 138 J 2S 0.5 

20 ; 32 0_30 0.547723 

21 J 38 o_ 32 0.565685 

22 ~ 38 J 34 0.583095 

23 138 0.33 0.574456 

24 137 DZl 0 447214 

138 o.,;752 

:s 9043:. 

DELTA H 

1.80 

:.90 

l 90 

1 70 

1.60 

~-20 

l 2C 

1 ~0 

1 10 

0 82 

0 58 

0 ·~7 

1 20 

1.20 

' 20 

~ l G 

j_ 20 

1.2C 

1.50 

; 2J 

9·2 

')DC 

; 9C 

: 2S 

1 3654 

41.3277 

8 4773 

0.1702 

80.0000 

28.9800 

27.1111 

29.6941 

29.4107 

28065.4642 

1224428.24 

0.0179 

2 55E·06 

3.1279 

0.0003 

4.75E-08 

0.0581 

100.9787 

METER T 

INLET 

85 

91 

93 

94 

os 

96 

98 

99 

99 

99 

100 

99 

98 

:02 

103 

104 

j J4 

; ::14 

;c;l.. 

]·J5 

1 J:O 

:or; 

: rJ'S 

iOS 

99_7917 

METER T 

OUTLET 

85 

36 

87 

87 

88 

88 

89 

90 

90 

90 

91 

9l 

92 

92 

93 

93 

93 

94 

gc; 

9"-

?5 

?5 

0~, 

96 

91.1667 

Meter 

.LSC • 

47.88 

:JB9 

::-08 

1 5 

18 5 

0 

0 

Volume 

257_9 

260 

262.2 

264_4 

266.4 

268.5 

270.2 

271 9 

273.6 

275.3 

276.8 

278 

279.05 

280.8 

282.5 

284 3 

285.9 

287.7 

289_4 

291.3 

293 4 

295.6 

297.9 

300 1 

301 791 

95.4792 

Po1nt 

VMSTO 

2.0176 

2 1007 

2.095 

1.9018 

1.9928 

1.6102 

1.6058 

1.6025 

1.6025 

1.413 

l.l277 

0 0874 

1.6486 

1.5957 

1.6866 

1.4975 

1.6851 

1.59 

1 77811 

1 9653 

2.0576 

2.1497 

2 0557 

J .576 

Po1nt Po1nt Pomt I so 

Velocity Mo1sture 

ml; 

34.4313 8.80412 100.9151 

35.5544 9.16676 101.9233 

35.0408 9.14176 103.3076 

33_3579 8.29905 985160 

32.7777 8 69606 105.0560 

28.3626 7 02636 97.9343 

27.6791 7.00731 100 0809 

26.9782 6.99295 102 4703 

26.2587 6.99295 105.2782 

23.158 6.16598 105.2575 

19.5721 4 92099 99.3955 

17.5058 4.30857 97.2977 

27.6791 7_19392 102 7460 

28.3389 6.96328 96.9740 

27.679! 7.35967 105.1134 

26.9782 6.53446 95.7519 

27.6791 7.35309 105.0] 93 

27.6791 6_93837 99 0962 

30.9461 7 76039 99.1352 

33.8998 8 57595 ]00.0083 

350116 8.97852 101 3781 

36.0891 9_38057 -;o2 7553 

35.5544 8.97051 99_7412 

27 6559 6 87703 98 1380 

15 
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I 

PLANT 

DATE: 

PLACE . 

RUN#· 

EMISSION TEST SUMMARY 

D;!ltrle. Corl'nt'. TY 

23-;..wg-·JS 

Krl; Sr•ubtJc>r Erhnu<;: 

2 

TEST DURATION (MINUTES): 60 LIQUID COLLECTED (mls) 

NOZZLE DIAMETER (INCH.): 

METER COEFFICIENT (Y) 

PITOT COEFFICIENT (Cp) 

GAS METER VDL(Cu.Ft.) 

BAROMETRIC PRESSURE 

CJ.3l23 PARTICULATE WEIGHT (Front halt mg) 

0 995 PARTICULATE WEIGHT (Back hall mg): 

0.84 STATIC PRESSURE(m H20): 

46_0 l PERCENT C02 

29 7 PERCENT 02 

PERCENT CO 

FOR CIRCULAR STACK 

STACK DIAMETER (mch): 

STACK AREA (Sq. Ft.) 

NOZZLE AREA (teet): 

FOR RECTANGULAR STACK 

54 STACK LENGTH(rnches) 

15.90431 STACK WIDTH(mches) 

0.000532 STACK AREA (Sq.Ft) 

ENTER THE STACK AREA SHOWN ABOVE· j~ 90tl3l 

FLOWS 

SAMPLED VOLUME (STD. CU.FT_)' 42.7352 VOLUME OF WATER VAPOR (STD. CU.FT_), 8 9009 FRACTIONAL MOISTURE CONTENT(%) 0.1724 

DRY BASE: 80.0000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 28.9800 

MOLECULAR WT OF STACK GAS (WET BASE): 27 0873 

STACK PRESSURE (mch Hg): 29.6941 

STACK GAS VELOCITY (ftlsec.): 30.2953 ACTUAL STACK GAS FLOW RATE (ACFM) 28909.577 

STANDARD STACK GAS FLOW RATE (SCFH): 1258397.44 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF): 0.0142 

PARTICULATE CONCENTRATION (L8S/SCF) 2.03E·06 PARTICULATE EMISSION (L8S/HR)· 2.55D4 

BACK HALF 

PARTICULATE CONCENTRATION (GR/SCF): 0.0014 

PARTICULATE CONCENTRATION (LBS/SCF) L93E·07 

PARTICULATE EMISSION (L8S/HR)· 0 2428 

ISOKINETIC RATIO(%)· 101.5990 

POINTS STACK T DELTA P SQUAR O.P DELTAH METER T 

deg F INLET 

137 0 35 0.591608 2.10 96 2 133 0 33 0.574456 2 OG 99 3 138 0 32 0.565685 1.90 102 4 138 0.30 0.547723 1.80 104 5 138 0.26 0.509902 ~ 60 .i.OS 

6 138 0 22 0.469042 l .30 1C7 

7 138 0.20 0.447214 1.20 107 8 138 0.19 0 43589 1.20 lOS 9 138 0.20 0.447214 1.20 108 

10 137 0.21 0.458258 1.30 109 

11 138 0.20 0.447214 1 20 l09 

12 137 Q. ~ 5 0.387298 c 92 109 

13 l37 c 18 0 424264 uo 102 

14 138 0.19 0 43589 : 20 lOS 

15 !38 0 20 0.447214 1.20 108 

16 138 0.20 0.447214 L20 108 17 J38 0.20 0 447214 i 2G 188 18 i38 0 19 0.43589 l 20 i09 

19 138 0.24 0.489898 ~.50 109 20 138 0.29 0.538516 1 83 110 21 138 ':;_3! 0.556776 1.% ClC 

22 :38 0.33 0.574456 2 JO j;· 

23 ;33 0.32 0.565685 2.00 1:1 24 :37 0.2'3 0.5 52 ; ~ l 

137 79167 0 4894 1.4800 107 0000 

METER T. 

OUTLET 

96 

'96 

97 

37 

97 

98 

99 

99 

99 

100 

100 

:o-; 

lOl 

100 

:c: 

l01 

!C~ 

J.C2 

lOO 

:ol 

101 

!Ol 

;~. 

J'l: 

99 5833 

189.1 

39.28 

3_74 

1.5 

13.5 

0 

0 

Meter 

Volume 

303.8 

306.1 

308.4 

310.6 

312.7 

314_7 

316.5 

318.3 

319.9 

321.7 

323.5 

325.3 

326.809 

328.5 

330.2 

331 9 

333.7 

335 4 

337.1 

339.1 

341 2 

343_4 

345.6 

347.8 

349.81 

l03.2917 

Point Po1nt 

VMSTD VelOCity 

2.1676 36.6014 

2.1613 35.57 

2.0594 35 0269 

1.9618 339147 

1 8658 31.5729 

1.6735 29.0428 

1.6716 27.6912 

1.4845 26.9901 

1.6701 27.6912 

1.6676 28.3513 

1.6672 27.6912 

1.3954 23.9612 

l. 57 42 26.2482 

1.5759 26.9901 

1.5745 27 6912 

1.6672 27.6912 

1.5745 27.5912 

1 5717 26.9901 

1.8538 30 3342 

1.9444 33.3447 

2.0375 34.4753 

2.0362 35.5 7 

2.0362 35.0269 

1 8581 30 9338 

Pomt Point I so 

Moisture 

ml' 

9 604417 102.2589 

9.576216 105.0908 

9.124868 101 6902 

8 692419 100 0478 

8_267038 102.2094 

7.415004 99.6615 

7.406591 104_4073 

6.577794 95.1330 

7.400019 104 3147 

7.388733 101.5604 

7.38691 104 1299 

6.182936 100.5572 

6.974946 103.5544 

6.982711 100.9892 

6.976526 98.3449 

7 38691 104 1299 

6.976526 98.3449 

6.964189 100.7213 

8.213755 105.6972 

8 615563 100 8584 

9 028052 102 2211 

9.0223 99.0120 

9.0223 100 5472 

8.232947 103 7i69 

lC 
I 

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I 

I 

I 

I 

I 

I 

I 

I 

PLANT : 

DATE 

PLACE· 

RUN# 

EMISSION TEST SUMMARY 

82ll·'·' Cc'W02 -y 

23-F.e~g JS 

r:,!: S:: _;:J~J"~ fxh;1ust 

TEST DURATION (MINUTES): 60 LIQUID COLLECTED (mls) 

NOZZLE DIAMETER (INCH.)· 

METER COEFFICIENT (Y) 

PITOT COEFFICIENT (Cp) 

GAS METER VOL.(Cu.Ft.) 

BAROMETRIC PRESSURE 

0.3123 PARTICULATE WEIGHT (Front half mg): 

0 995 PARTICULATE WEIGHT (Back halt mg) · 

0.84 STATIC PRESSURE (irl H20) 

46.26 PERCENT C02 

29 7 PERCENT 02 

PERCENT CO 

FOR CIRCULAR STACK 

STACK DIAMETER (irKh) 

STACK AREA (Sq.Ft.) 

NOZZLE AREA (feet) 

FOR RECTANGULAR STACK 

54 STACK LENGTH(inches): 

15.90431 STACK WIDTH(inches) 

0.000532 STACK AREA (Sq Ft.) 

ENTER THE STACK AREA SHOWN ABOVE· J 5 9Qt,;q 

FLOWS 

SAMPLED VOLUME (STD CU.FT.) 42.6789 

VOLUME OF WATER VAPOR (STD_ CU. FT.) 8.3738 

FRACTIONAL MO\STURE CONTENT(%) 0.1640 

DRY BASE 80.0000 

MOLECULAR WT. OF STACK GAS (DRY BASE) 28.9800 

MOLECULAR WT OF STACK GAS (WET BASE)· 27 1790 

STACK PRESSURE (mch Hg): 29.6941 

STACK GAS VELOCITY (ftlsec.): 30.2464 

ACTUAL STACK GAS FLOW RATE (ACFM)· 28862.9271 

STANDARD STACK GAS FLOW RATE (SCFH): 1270380.11 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF): 0.0123 

PARTICULATE CONCENTRATION (LBS/SCF) 1 76E-06 

PARTICULATE EMISSION (LBS/HR)· 2.2401 

BACK HALF 

PARTICULATE CONCENTRATION (GR./SCF): 0.0003 

PARTICULATE CONCENTRATION (LBS/SCF)· 4.34£-08 

PARTICULATE EMISSION (LBS/HR): 0.0551 

ISOKINETIC RATIO(%): 100.5079 

POINTS STACK T DELTA P SQUAR O.P DELTA H METER T 

deg F INLET 

1 137 0 34 0.583095 2 10 201 

2 137 0 33 0.574456 ? OC· 107 

3 ~37 Cl.32 0.565685 ?.00 109 

4 :;:3;' 0.30 0.547723 1.80 llO 

5 137 0.27 0.519615 1 60 ill 

6 137 0 25 0.5 1.50 :ll 

7 137 0 20 0.447214 1.20 111 

8 137 0.19 0.43589 1 20 111 

9 137 0_19 0.43589 1 20 111 

10 137 0.20 0.447214 1.20 112 

11 137 0.!8 0.424264 1 10 ;.I 

12 136 0 14 0.374166 0 86 -·· 13 137 c 17 0.412311 i.OO i06 

14 137 0.19 0.43589 1 20 jlQ 

15 138 0.19 0.43589 1.20 111 

16 138 0 20 0 447214 1.20 l-'2 

17 138 0.19 0.43589 ; .20 : i2 

18 138 0.20 0.447214 1.20 113 

19 136 0.27 0.519615 1 70 113 

20 ~37 0.30 0.547723 1 90 ]1L 

21 137 c .;:3 0.574456 :?.80 _,;:, 

22 137 J.33 0_574456 2.J:::; il3 

23 131 0 32 0.565685 2 00 ll3 

24 : 37 J 25 0.5 ; 5C- . :3 

137.16667 0.4896 1 4983 110 7917 

METER T. 

OUTLET 

101 

101 

lC:" 

102 

102 

102 

10:2 

i03 

103 

104 

104 

:o; 

;o4 

104 

104 

10C. 

104 

104 

:05 

l05 

1:5 

,c5 

l05 

W'S 

103.4583 

~ 77 9 

34.l 3 

C· 84 

0 08 

1.5 

~85 

0 

Meter 

Volume 

350.3 

352.6 

354.8 

357.1 

359.2 

361.2 

363.2 

365 

366.7 

368.4 

370_1 

371.8 

373.278 

374 9 

376.6 

378.3 

380.1 

381.8 

383.6 

385.6 

387.8 

390.1 

392.3 

394.6 

396.56 

107 1250 

Po1nl Point 

VMSTD VelOCity 

2.1483 36.0138 

2.0435 35 4802 

2.1326 34.9385 

1.9427 33 8291 

1 8477 32.0931 

1.8472 30.8816 

1.6613 27.6213 

1.5676 26 9219 

1.5676 26.9219 

1.5648 27.6213 

1.5658 26.2039 

1.3605 23.0903 

1 5002 25.4656 

1.5676 26.9219 

1.5662 26.9445 

1.6569 27.6444 

l. 5648 26.9445 

1 .6554 27.6444 

1.84 32.1199 

2.0232 33.8291 

2.1176 35.4802 

2.0255 35.4802 

2.1176 34.9385 

1 8028 308816 

Po1nt Po1nt I so 

Mo1sture 

ml' 

8.966848 101.9702 

8_529261 98 4526 

8.901173 104.3386 

8 108802 98.1678 

7.712048 98.4149 

7_710147 102.2505 

6.933997 102.8115 

6.543 99 5344 

6.543 99_5344 

6.531481 96.8433 

6.535622 102.1465 

5.678779 100 5541 

6 261798 100.7042 

6.543 99 5344 

6.537236 99.5299 

6.915686 102.6258 

6.531481 99.4423 

6.9096C3 102.5355 

7.680058 98.0887 

8.444808 102 2356 

8.838599 102.0233 

8 454312 97.5875 

8.838599 103.6051 

7 524602 99 7599 

l'i' 
I 

I 

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I 

I 

I 

I 

I 

I 

I Appendix B 

I 

I 

I 

I 

I 

I 

I 

I 

I 
I 

8123105 NOx Converter Check 

I Date/Time NOx 

I mmlddlyy hh:mm:ss ppm 

08/23105 07:36:45 0.266266 

08123105 07:37:45 23.06641 

08123105 07:38:45 51.60451 51.0 ppm NOx 

I 08123105 07:39:45 11.40576 

08123105 07:40:45 6.772583 

08123105 07:41:45 30.10938 Start Converter Check 

I 08123105 07:42:45 30.32276 

08123105 07:43:45 30.34033 

08123105 07:44:45 30.37696 

I 08/23105 07:45:45 30.4087 

08123105 07:46:45 30.38184 

08123105 07:47:45 30.41162 

08123105 07:48:45 30.44288 

I 08123105 07:49:45 30.44581 

08123105 07:50:45 30.4546 

08123105 07:51:45 30.47657 

I 08123105 07:52:45 30.47657 

08123105 07:53:45 30.47999 

08123105 07:54:45 30.4961 

I 08/23105 07:55:45 30.53516 

08123105 07:56:45 30.50587 

08123105 07:57:45 30.53907 

I 08123105 07 58:45 30.52296 

08123105 07:59:45 30.50831 

08123105 08:00:45 30.52638 

08123105 08:01:45 30.48487 

I 08123105 08:02:45 30.50929 

08123105 08:03:45 30.52198 

08123105 08:04:45 30.53419 

I 08123105 08:05:45 30.51759 

08123105 08:06:45 30.51808 

08123105 08:07:45 30.48536 

I 08123105 08:08:45 30.52492 

08123105 08:09:45 30.47951 

08123105 08:10:45 30.5 

I 08123105 08:11:45 30.4541 Stop Converter Check, Bag Off 

08123105 08: 12:45 6.982544 

08123105 08: 13:45 0.403427 

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Sheet1 

Summary of CO Analyzer Calibrations and Bias 

Plant: 

Source: 

Date: 

Run #1 

Run #2 

Run #3 

Daltile, Conroe, TX 

Kiln Scrubber Exhaust 

8/23/05 

Analyzer Calibratrion Data 

Cylinder Analyzer Absolute %Span 

Value Response Difference 

Zero Gas 0 2.53 2.53 1.265 

Mid Range 99.1 101.38 2.28 1.14 

High Range 200 196.33 -3.67 -1.835 

System Calibration Bias and Drift Data 

Analyzer Initial Values Final Values 

Calibration System System System System 

Response Calibration Calibration Calibration Calibration 

Response Bias Response Bias 

Zero Gas 2.53 2.48 -0.025 5.13 1.3 

Upscale 101.38 101.05 -0.165 102.33 0.475 

Average CO Concentration: 85.18 

Corrected CO Concentration: 82.38507 

(Equation 6C-1) 

Zero Gas 2.53 5.13 1.3 4.8 1.135 

Upscale 101.38 102.33 0.475 100.6 -0.39 

Average CO Concentration: 91.74 

Corrected CO Concentration: 89.11298 

(Equation 6C-1) 

Zero Gas 2.53 4.8 1.135 3.43 0.45 

Upscale 101.38 100.6 -0.39 100.48 -0.45 

Average CO Concentration: 94.76 

Corrected CO Concentration: 93.15965 

(Equation 6C-1) 

Page 1 

Drift Average 

Calibration 

Values 

1.325 3.805 

0.64 101 .69 

-0.165 4.965 

-0.865 101.465 

-0.685 4.115 

-0.06 100.54 

20 
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Sheet1 

Summary of NOx Analyzer Calibrations and Bias 

Plant: 

Source: 

Date: 

Run #1 

Run #2 

Run #3 

Daltile, Conroe, TX 

Kiln Scrubber Exhaust 

8/23/05 

Analyzer Calibratrion Data 

Cylinder 

Value 

Zero Gas 0 

Mid Range 25.5 

High Range 51 

Analyzer 

Response 

0.1 

24.9 

5U3 

System Calibration Bias and Drift Data 

Analyzer Initial Values 

Calibration System System 

Absolute %Span 

Difference 

0.1 0.166667 

-0.6 -1 

0.13 0.216667 

Final Values 

System System 

Response Calibration Calibration Calibration Calibration 

Response Bias Response Bias 

Zero Gas 0.1 0.13 0.05 0.45 0.583333 

Upscale 24.9 24.4 -0.83333 24.35 -0.91667 

Average NOx Concentration· 21.73 

Corrected NOx Concentration: 22.69961 

(Equation 6C-1) 

Zero Gas 0.1 0.45 0.583333 0.58 0.8 

Upscale 24.9 24.35 -0.91667 24.4 -0.83333 

Average NOx Concentration: 20.29 

Corrected NOx Concentration: 2113422 

(Equation 6C-1) 

Zero Gas 0.1 0.58 0.8 0.7 

Upscale 24.9 24.4 -0.83333 24.35 -0.91667 

Average NOx Concentration: 19.2 

Corrected NOx Concentration: 19.94017 

(Equation 6C-1) 

Page 1 

Drift Average 

Calibration 

Values 

0.533333 0.29 

-0.08333 24.375 

0.216667 0.515 

0.083333 24.375 

0.2 0.64 

-0.08333 24.375 

21 
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Sheet1 

Summary of Sulfur Dioxide Analyzer Calibrations and Bias 

Plant: 

Source: 

Date: 

Run #1 

Run #2 

Run #3 

Daltile, Conroe, TX 

Kiln Scrubber Exhaust 

8/23/05 

Analyzer Calibratrion Data 

Cylinder 

Value 

Zero Gas 0 

Mid Range 50.1 

High Range 101 

Analyzer 

Response 

0.1 

50.13 

101.65 

System Calibration Bias and Drift Data 

Analyzer Initial Values 

Calibration System System 

Absolute % Span 

Difference 

0.1 0 090909 

0.03 0.027273 

0.65 0.590909 

Final Values 

System System 

Response Calibration Calibration Calibration Calibration 

Response Bias Response Bias 

Zero Gas 0.1 0.78 0.618182 2.43 2.118182 

Upscale 50.13 47.95 -1.98182 48.8 -1.20909 

Average S02 Concentration: 2.51 

Corrected S02 Concentration: 0.969436 

(Equation 6C-1) 

Zero Gas 0.1 2.43 2.118182 0.58 0.436364 

Upscale 50.13 48.8 -1.20909 46.88 -2.95455 

Average S02 Concentration: 1.86 

Corrected S02 Concentration: 0.383846 

(Equation 6C-1) 

Zero Gas 0.1 0.58 0.436364 0 -0.09091 

Upscale 50.13 46.88 -2.95455 46.35 -3.43636 

Average S02 Concentration: 0.8 

Corrected S02 Concentration: 0.55156 

(Equation 6C-1) 

Page 1 

Drift Average 

Calibration 

Values 

1.5 1.605 

0.772727 48.375 

-1.68182 1.505 

-1.74545 47.84 

-0.52727 0.29 

-0.48182 46.615 

22 
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Date/Time VOC co 

mmlddlyy hh:mm.ss ppm ppm 

08/23105 08.25:42 0.1 

08/23105 08.25:52 0.1 

08123105 08 26:02 0.1 

08/23/0508:26"12 0_1 

08/23/05 08'26.22 0_1 

08/23/05 08:26'32 0_1 

08123105 08:26:42 0 1 

08/23/05 08:26'52 0.1 

08/23/05 08:27:02 

08/23/05 08:27"12 

08/23105 08:27:22 

08123105 08.27:32 

08123105 08:27:42 

08123105 08:27:52 

08/23/05 08:28:02 

08/23/05 08.28:12 

08123105 08:28:22 

08/23/05 08:28:32 

08/23/05 08:28:42 

08/23/05 08:28:52 

08/23/05 08:29:02 

08/23/05 08:29:12 

08123105 08:29:22 

08123/05 08:29:32 

08/23/05 08:29:42 

08/23/05 08:29:52 

08123/05 08:30:02 

08123105 08:30:12 

08/23/05 08:30:22 

08/23/05 08:30'32 

08/23/05 08:30:42 

08123/05 08:30:52 

08/23/05 08:31:02 

08123/05 08:3'1 :12 

08123/05 08:31:22 

08123105 08:31 :32 

08123105 08:31'42 

08/23/05 08:31"52 

08123105 08:32:02 

08/23105 08:32:12 

08/23105 08:32:22 

08/23/05 08'32:32 

08!23/05 08:32:42 

08/23/05 08.32:52 

08/23/05 08:33:02 

08123105 08:33:12 

08123/05 08.33:22 

08123/05 08:33:32 

08/23/05 08"33:42 

08123/05 08:33:52 

08/23/05 08:34:02 

08123/05 08:34:12 

08123105 08'34:22 

08123/05 08"34'32 

08/23/05 08:34:42 

08123105 08:34:52 

08123105 08:35:02 

08123105 08:35:12 

08123105 08.35:22 

08123105 08:35:32 

08/23/05 08:35.42 

08/23105 08:35:52 

08123105 08·36:02 

08/23105 08 36' 12 

08.'23/05 08:36:22 

08.'23105 08-36.32 

08/23.105 08:36:42 

08/23105 08:36:52 

08/23105 08·37:02 

08123/05 08 37:12 

0.1 

0.2 

0.2 

0.2 

0.2 

0.2 

0.2 

0.2 

0 2 

0.2 

0.2 

02 

0.2 

0.1 

0.1 

0.1 

0.1 

0 1 

0.1 

0 1 

01 

0.1 

0 1 

0.1 

02 

0.2 

0.2 

0.2 

02 

0.2 

0 1 

0 1 

0.1 

0.1 

0.1 

0.1 

0.1 

0 1 

0.1 

00 

0.1 

00 

0.1 

0.1 

02 

0 1 

01 

0.0 

0.1 

0.1 

0 0 

0 1 

0.1 

0 0 

00 

00 

0 1 

0 1 

IJ: 

0.0 

0 0 

0 1 

1.2 

1.5 

1.5 

1 4 

1.5 

1.4 

1.5 

1.7 

1 5 

1 4 

1.6 

1.9 

20 

2.4 

2 7 

2.7 

2.6 

27 

2.6 

2.8 

3.1 

2.6 

2.3 

2.0 

1.6 

1 9 

1.7 

1 6 

1 4 

1.6 

2.0 

2.0 

2.2 

2.6 

2.5 

2.6 

2.5 

2.5 

2.8 

2.9 

26 

23 

2 2 

2.2 

2.2 

2.0 

2.1 

24.6 

96.8 

100.9 

101.0 

101.3 

101.3 

101.3 

101.6 

101.4 

51.7 

2.4 

1 9 

1 8 

1 8 

"1.8 

1 6 

1 7 

1.8 

2.0 

: 9 

2.1 

39 3 

185.6 

NO' 

ppm 

802 

ppm 

0.2 -0.1 

0.3 -0.1 

0.2 -0.2 

0_2 -0_1 

0 3 0.0 

0.3 0.0 

0 3 -0.1 

0 3 0.0 

2.2 

48.7 

49.6 

50.0 

50.2 

50.7 

51.0 

51_0 

51.0 

51.1 

51.2 

51.2 

22.2 

0.4 

0.3 

0.3 

0.3 

02 

0.3 

28 

24.2 

24.6 

24.7 

24.7 

24_8 

24_8 

24.9 

24.9 

24.9 

24.9 

24 9 

7.8 

0.3 

0.3 

0.3 

0.3 

0.2 

0.2 

0.3 

02 

0.1 

0.1 

0 1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.2 

0.2 

0.2 

0 2 

0 2 

0 2 

0.2 

0.2 

0.2 

0.2 

0.2 

0.3 

0.2 

00 

0 0 

0.0 

0.0 

0.0 

0.0 

0.0 

00 

00 

00 

00 

0.0 

00 

0.0 

0.0 

0.0 

0.0 

0 0 

0 0 

0 0 

0.0 

0.0 

0.0 

0.0 

0.0 

01 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.0 

00 

0 1 

01 

0.1 

0.1 

01 

0 1 

0 1 

0.1 

0 1 

0.2 

0.2 

01 

0.1 

0.1 

0.1 

0_1 

0 1 

0 1 

0 1 

0 1 

0: 

0 1 

0.1 

0 1 

8/23/05 Calibrations 

51 ppm NOx 

25 5 ppm NOx 

Zero CO, S02 

99.1 ppm CO 

Zero NOx 

Page 1 
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08/23/05 08 37:22 

08/23/05 08 37:32 

08/23105 08'37:42 

08/23105 08:37'52 

08123105 08.38.02 

08/23/05 08:38.12 

08/23/05 08:38.22 

08/23/05 08:38:32 

08123/05 08:38.42 

08123/05 08:38:52 

08/23/05 08:39:02 

08123105 08:39:12 

08/23/05 08.39:22 

08/23105 08:39:32 

08123105 08:39:42 

08123105 08:39:52 

08123/05 08'40:02 

08/23/05 08'40:12 

08/23/05 08:40:22 

08/23105 08:40:32 

08/23/05 08:40'42 

08/23/05 08:40:52 

08/23105 08:41 :02 

08/23105 08:41 '12 

08/23/05 08 41 :22 

08/23/05 08:41 :32 

08123/05 08:41.42 

08/23/05 08 41-52 

08/23/05 08.42.02 

08/23/05 08'42'12 

08/23/05 08'42'22 

08/23/05 08:42.32 

08/23/05 08:42.42 

08/23/05 08:42:52 

08/23/05 08:43:02 

08/23/05 08:43:12 

08/23/05 08:43:22 

08/23/05 08:43.32 

08/23/05 08:43:42 

08/23/05 08:43.52 

08/23/05 08:44:02 

08/23/05 08:44'12 

08/23/05 08'44:22 

08/23/05 08:44.32 

08/23/05 08:44.42 

08/23/0:S 08:44:52 

08/23/05 08:45:02 

08/23/05 08:45:12 

08/23/05 08:45:22 

08/23/05 08:45:32 

08/23/05 08:45:42 

08/23/05 08"45:52 

08/23/05 08'46:02 

08/23/05 08:46:12 

08/23/05 08"46:22 

08/23/05 08:46'32 

08/23/05 08'46'42 

08/23/05 08:46.52 

08/23/05 08:47:02 

08123105 08:47:12 

08/23/05 08:47.22 

08/23/05 08.47.32 

08123105 08:4 7:42 

08/23105 08:47:52 

08/23/05 08:48:02 

08/23/05 08:48:12 

08/23/05 08:48:22 

08/23105 08:48:32 

03/23/05 08:48:42 

08/23/05 08:48:52 

08/23/05 08:49:02 

08/23105 08:49.12 

0.1 

0.1 

0 1 

0.1 

01 

0.1 

01 

0.0 

01 

01 

0.1 

0 1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.2 

0.1 

0.2 

0.2 

0.1 

0.1 

0.1 

0.2 

0.2 

0.4 

02 

0.1 

01 

01 

0 1 

01 

0 1 

01 

01 

0.1 

0.1 

0.0 

0.0 

0.1 

0.1 

01 

DO 

0.0 

00 

00 

00 

00 

00 

00 

DO 

01 

0.1 

00 

0 1 

00 

0.2 

0.1 

0.1 

0.2 

0 3 

0.2 

0.3 

0.1 

0.2 

0.0 

0.0 

0.0 

0.0 

00 

0.6 

194.9 

195.3 

195.7 

196.2 

196.2 

196.3 

196.4 

196.3 

196.3 

138_3 

5.9 

2.6 

2.5 

2.3 

2.1 

23 

1.9 

2.1 

2.4 

2.6 

2.4 

2.8 

26 

2.7 

2.7 

2 8 

3.1 

3 1 

3.2 

3 1 

3.3 

3.3 

34 

31 

2.6 

24 

21 

20 

2 1 

1.9 

2.0 

2.0 

1.8 

24 

26 

3.2 

3.3 

3.2 

3.2 

3.1 

3.4 

3.4 

34 

3.5 

3.2 

34 

33 

3.3 

3.3 

34 

3.4 

3 3 

34 

34 

3 1 

3.2 

3.0 

3.1 

29 

30 

30 

3.0 

0.1 

0.1 

0.1 

01 

01 

0.1 

0.1 

01 

0.1 

0.1 

0.2 

0.2 

0.2 

0.2 

0.2 

02 

0.3 

0.5 

04 

04 

04 

04 

04 

04 

04 

04 

04 

04 

04 

04 

04 

04 

04 

02 

0.2 

02 

02 

02 

02 

0.3 

02 

02 

0.2 

0.2 

02 

02 

02 

0.2 

02 

0.2 

0.2 

02 

0.2 

0.3 

0 2 

0.2 

0.3 

0.3 

0 3 

0.3 

0 3 

0 3 

0.3 

03 

03 

0.3 

0.2 

0.2 

0.2 

0.2 

02 

0.2 

01 

0 1 

01 

0 1 

0.2 

0.2 

0.2 

0.1 

0.2 

0.3 

0.2 

0.1 

0.1 

0.3 

0.2 

0.2 

3.1 

22.8 

39.8 

46.4 

48.4 

49.0 

49.4 

49.5 

49.7 

49_8 

50 0 

50.1 

50.1 

50.1 

50.1 

50.2 

47.7 

28 2 

11.2 

4.4 

22 

1.3 

1.0 

0.8 

0.6 

0.6 

0.7 

17 2 

62.6 

88.7 

97.2 

99.7 

100.4 

100_7 

100.9 

101.1 

101_2 

101_2 

101.3 

101.4 

101.4 

101.5 

101.6 

101.6 

101.6 

101.7 

101.7 

91.9 

47 1 

16.6 

59 

2.9 

2.0 

1.7 

1.5 

1 3 

8123105 Calibrations 

200 ppm CO 

50 1 ppm S02 

101 ppm S02 

24 

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08/23/05 08:49:22 

08/23/05 08:49.32 

08/23/05 08:49:42 

08/23/05 08:49:52 

08/23105 08:50:02 

OB/23105 oe-so:12 

08/23/05 08.50.22 

OB/23/05 oe-so:32 

08/23/05 08:50:42 

08/23/05 08:50:52 

08/23/05 08:51:02 

08/23/05 08'51:12 

08/23/05 08:51:22 

08/23/05 08:51:32 

08/23/05 08:51:42 

08/23/05 08'51 :52 

08/23/05 08:52:02 

08/23/05 08:52:12 

08/23/05 08:52:22 

08/23/05 08:52:32 

08/23/05 08.52:42 

08/23/05 08 52'52 

08/23/05 08 53.02 

08/23/05 08:53:12 

08/23/05 08:53:22 

08/23/05 08:53:32 

08/23/05 08:53:42 

08/23/05 08'53:52 

08/23/05 08:54:02 

08/23/05 08:54:12 

08/23/05 08'54:22 

08/23/05 08:54:32 

08/23/05 08.54.42 

08/23/05 08:54:52 

08/23/05 08'55:02 

08/23/05 08:55:12 

08/23/05 08:55:22 

08/23/05 08:55:32 

08/23/05 08:55:42 

08/23/05 08:55:52 

08123105 08:56:02 

08123105 08:56:12 

08/23/05 08:56:22 

08/23/05 08:56:32 

08/23/05 08:56:42 

08123105 08:56:52 

08123105 08:57:02 

08123105 08:57-12 

08123105 08:57:22 

08/23105 08:57:32 

08/23/05 08:57:42 

08123105 08:57:52 

08/23/05 08'58:02 

08/23105 08:58:12 

08/23/05 08:58:22 

08/23/05 08:58:32 

08.

123/05 08:58:42 

08/23105 08:58:52 

08/23/05 08'59"02 

08/23/05 08:59:12 

08/23/05 08:59.22 

08/23/05 08'59'32 

08/23/05 08:59:42 

08/23/05 08:59:52 

08123105 09:00:02 

08123105 09:00:12 

08123105 09:00:22 

08/23/05 09_00'32 

08/23/05 09:00 42 

08/23/05 09:00:52 

08/23/05 09'01 :02 

08/23/05 09'01 12 

1.0 

1.2 

0.9 

0.1 

0.1 

0.1 

0.2 

0.0 

00 

00 

0.0 

0.0 

09 

00 

0.0 

0.0 

0.0 

0.0 

00 

00 

01 

00 

0.1 

01 

01 

0.0 

0.0 

0.0 

0.0 

00 

00 

0.1 

0.1 

0.5 

O_i 

0.1 

0.0 

0.0 

0.0 

0.0 

00 

00 

00 

00 

0.0 

00 

00 

00 

00 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

09 

1.0 

1 0 

11 

1.0 

0.1 

0 0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

00 

0.0 

2.9 

2.9 

2.7 

2.8 

2.5 

2.6 

2.7 

2.9 

2.7 

2.7 

2.7 

2.5 

2.5 

2.4 

2.5 

2.4 

24 

24 

2.5 

2.5 

2.4 

2.6 

2.5 

2.4 

2.3 

2.6 

2.6 

2.7 

2.4 

2.5 

2.4 

2.4 

2.4 

2.4 

2.6 

2.6 

19.2 

52.9 

68.7 

77.6 

84.7 

88_6 

91_6 

94.0 

95.7 

97_1 

97_9 

99_1 

99.7 

100.3 

100.3 

100.6 

100.3 

100.7 

100.6 

101.2 

101.2 

101.2 

100.9 

95.5 

78.1 

47.3 

25.7 

14.3 

9.6 

7.5 

6.3 

54 

4.8 

44 

4.3 

3 9 

0.2 

0.2 

0.2 

0.2 

0.2 

0.2 

0.2 

0.2 

0.2 

4.2 

9 7 

13.7 

16.9 

19.2 

20.9 

21.9 

22.7 

23.1 

23.4 

23_7 

23.8 

23.9 

24 0 

24.1 

24.2 

24.2 

24 3 

24.4 

24 3 

24.4 

24.4 

24.4 

24.4 

24.3 

24.4 

24.2 

20.7 

10.8 

6.7 

4.9 

3.5 

2_5 

1.8 

1.4 

1.1 

0.9 

0 7 

0.5 

0.4 

0.3 

0.3 

0.2 

0.2 

0.2 

0.1 

0.2 

0.1 

0.1 

0.1 

01 

0.1 

0.2 

02 

0.2 

0.4 

04 

04 

04 

04 

04 

04 

04 

1.2 

1.1 

1 0 

11 

1 0 

1.0 

1.0 

0 9 

0.8 

0.8 

0.8 

0.8 

0.8 

0.8 

0.8 

0.9 

0 9 

0 9 

0 9 

0 9 

1.0 

0 9 

0.9 

0.8 

0 8 

0.7 

0.7 

0.7 

0.8 

0.8 

0.7 

0.8 

0.8 

0.8 

0.8 

0.9 

0.8 

0.8 

0.8 

0 9 

1 0 

1 0 

1 0 

0.9 

0 9 

1 0 

1.0 

0.9 

0.8 

0 9 

0.9 

0.8 

0.8 

0 9 

0.9 

0.9 

1 0 

0.9 

0.9 

0.8 

07 

0.7 

0.9 

11 

3.2 

8.2 

14 4 

19_8 

24 2 

28 1 

31 4 

34 2 

8/23/05 Cal1brat1ons 

25_5 ppm NOx Bias 

Zero CO, S02 Bias 

99 1 ppm CO Bias 

Zero VOC, NOx B1as 

Page 3 

25 
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08123105 09:01 22 

08123/05 09 01 :32 

08123/05 09'01 :42 

08/23/05 09:01 :52 

08/23/05 09.02:02 

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08/23/05 09:02:22 

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08/23/05 09:05.02 

08/23105 09:05:12 

08/23/05 09:05:22 

08123/05 09:05'32 

08/23/05 09:05.42 

08123!05 09:05:52 

08123105 09:06:02 

08123105 09:06.12 

08/23/05 09:06:22 

08/23/05 09:06'32 

08/23/05 09:06'42 

08/23/05 09:06:52 

08/23/05 09:07'02 

08/23/05 08:07' 12 

08/23/05 09:07.22 

08123/05 09:07:32 

08/23/05 09:07'42 

08/23/05 09:07"52 

08/23/05 09:08:02 

08/23/05 09:08:12 

08123/05 09:08:22 

08/23/05 09:08:32 

08123/05 09:08:42 

08/23/05 09:08:52 

08/23/05 09:09:02 

08/23/05 09:09:12 

08/23/05 09:09:22 

08/23/05 09:09:32 

08123105 09:09:42 

08123/05 09:09:52 

08/23/05 09:10:02 

08123/05 09:10.12 

08/23/05 09:10:22 

08/23/05 09:10:32 

08123105 09:10:42 

08/23/05 09:10:52 

08123/05 09:11:02 

08/23/05 09:11 :12 

08/23/05 09.11 :22 

08/23/05 09:11:32 

08123/05 09:11 :42 

08/23/05 09:11 :52 

08123/05 09:12:02 

08123/05 09:12"12 

08/23/05 09:12:22 

08123105 09:12:32 

08/23/05 09:12:42 

08123/05 09:12:52 

08123/05 09:13:02 

0.0 

0.0 

0.0 

DO 

0.0 

0.0 

0.0 

0 0 

0 0 

0.0 

0.0 

00 

-0.1 

0.0 

0.0 

0.0 

DO 

DO 

0.0 

00 

DO 

0.0 

DO 

DO 

DO 

0.0 

0.0 

DO 

DO 

DO 

0.0 

0.6 

1.0 

1.0 

1 0 

1ee 

28.6 

28.6 

28.6 

28.6 

28_7 

28.7 

28.7 

28.8 

28.8 

28.7 

28_6 

10.5 

1.2 

12 

11 

20.0 

49.1 

49.2 

49.1 

49.1 

49.2 

49.3 

47.1 

4.6 

1.3 

1.3 

6.6 

14_7 

14_7 

14.7 

14.7 

14.7 

14.7 

14.8 

14.7 

4.0 

3.7 

3 7 

3.8 

3.7 

38 

3 7 

3.8 

3.6 

3.8 

3.7 

3.9 

3.7 

4.0 

4.0 

4.1 

4.0 

4.2 

4.0 

3.7 

3.6 

3.4 

3.3 

3.5 

3.4 

3.4 

3.4 

3.8 

3.3 

3.4 

3.3 

3.3 

3.2 

3.6 

3.8 

4.2 

4 0 

4.2 

4.0 

4.1 

3.7 

3.8 

3.8 

3.9 

3_7 

3.9 

39 

39 

3.8 

39 

4.1 

3 7 

41 

4.0 

·1 6 

-5_8 

39 

3.7 

3.7 

3.7 

3.4 

3.6 

3.8 

4.0 

3.9 

4.0 

3.9 

4.1 

4.0 

4 2 

4 3 

04 

04 

0.4 

0.4 

0.4 

0.4 

0.4 

0.4 

0.4 

0.4 

0.4 

0.4 

04 

04 

0.4 

0.4 

0.4 

0.4 

04 

0.4 

0.4 

0.4 

0.4 

0.4 

0.4 

04 

0.4 

0.4 

04 

0.4 

0.4 

0.4 

0.4 

0.4 

0.3 

03 

03 

0.2 

0.2 

0.2 

0.2 

0.1 

01 

02 

02 

0.1 

0.1 

0.1 

0.1 

0.1 

01 

0.2 

0.2 

0.3 

02 

01 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0 1 

0.2 

0.2 

0.2 

0.2 

0 1 

0.1 

0 1 

01 

36.4 

38.7 

40.4 

41_5 

42_5 

43.2 

43.8 

44.5 

45_1 

45_5 

45.9 

46 1 

46 3 

46.5 

46.6 

46.8 

47.1 

47 4 

47.5 

47.5 

47.5 

47.6 

47.7 

47.8 

47.9 

48.0 

48.0 

47.9 

47.9 

48.0 

47.8 

46.3 

44 7 

43.6 

42 0 

38.6 

32 6 

26_0 

20.8 

17.0 

14.4 

12.4 

11 0 

9.6 

8.5 

7.7 

7.0 

6 3 

5.7 

5.3 

51 

5.0 

5.0 

5.0 

4.9 

52 

5.1 

4.8 

4.5 

4.2 

40 

3.9 

3.9 

39 

40 

40 

3.9 

39 

3.8 

3.6 

35 

8/23/05 Calibrations 

50_1 ppm 802 Bias 

28 8 ppm C3H8 

48 8 ppm C3H8 

2r .l 

Page 4 
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8/23/05 Calibrations 

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08/23/05 09:13:12 14.7 4 2 0.1 34 

08/23/05 09.13:22 14.3 40 0 1 3.3 

I 08/23/05 09:13'32 2.6 39 0.1 3.3 

08/23/05 09:13:42 1.2 4 1 0 1 3.2 

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DatefTime 

mm/dd/yy hh:mm·ss 

08/23/05 09.28.22 

08/23/05 09.28:32 

08/23/05 09:28:42 

08/23/05 09:28:52 

08/23/05 09:29:02 

08/23/05 09:29:12 

08123/05 09'29 22 

08/23/05 09'29:32 

08/23/05 09:29:42 

08/23/05 09.29:52 

Start Run t'1 

08/23/05 09:30:02 

08/23/05 09.30:12 

08/23/05 09:30:22 

08/23/05 09:30.32 

08/23/05 09:30.42 

08/23/05 09.30:52 

08/23/05 09:31:02 

08/23/05 09:31 '12 

08/23/05 09:31:22 

08/23/05 09:31 .32 

08/23/05 09:31:42 

08/23/05 09:31:52 

08123105 09:32:02 

08/23/05 09:32:12 

08/23/05 09:32:22 

08/23/05 09:32:32 

08/23/05 09.32.42 

08/23/05 09:32.52 

08/23/05 09:33:02 

08/23/05 09:33:12 

08/23/05 09_33:22 

08/23/05 09:33:32 

08/23/05 09:33:42 

08/23/05 09:33:52 

08/23/05 09:34:02 

08/23/05 09:34:12 

08/23/05 09:34:22 

08/23/05 09:34:32 

08/23105 09:34.42 

08/23/05 09:34:52 

08/23/05 09:35:02 

08/23105 09:35:12 

08123/05 09:35:22 

08/23/05 09:35:32 

08123105 09:35:42 

08123/05 09:35:52 

08/23/05 09:36:02 

08/23/05 09:36:12 

08/23/05 09:36:22 

08/23/05 09:36:32 

08/23/05 09:36:42 

08/23/05 09:36:52 

08/23/05 09:37:02 

08/23/05 09:37:12 

08/23/05 09:37:22 

08/23/05 09:37:32 

08/23/05 09"37.42 

08/23/05 09:37:52 

08/23/05 09:38:02 

08/23/05 09:38.12 

08/23/05 09:38:22 

08/23/05 09:38:32 

08/23/05 09"38:42 

08/23/05 09:38:52 

08/23/05 09:39:02 

08/23/05 09'39:12 

08/23/05 09:39:22 

08/23/05 09.39"32 

08/23.105 09·39'42 

08/23/05 09'39'52 

VOC CO NOx 502 

ppm ppm ppm ppm 

4.4 83.8 21 5 2.8 

4.2 85.1 21.5 2.7 

4.2 86.3 21.5 2.6 

42 

4.1 

4.2 

42 

4.2 

4.2 

4.4 

4.5 

4.5 

4.4 

3.8 

3.8 

4.0 

4.0 

39 

4.0 

3.8 

4.1 

4.0 

39 

3.6 

3.3 

36 

3.3 

3.4 

3.6 

3.8 

3.6 

3.8 

3.9 

3.5 

3.6 

3.3 

3.5 

34 

3.9 

3.5 

36 

4 1 

3 7 

37 

39 

39 

3.8 

38 

40 

4.5 

4.3 

41 

4.0 

3.9 

3.8 

3.8 

3.9 

3.8 

3.9 

42 

4.6 

4 2 

4.3 

4.2 

4.2 

4.2 

4.1 

4 3 

46 

45 

84.9 

84.4 

84.4 

84.5 

85.4 

86_5 

87.2 

88.0 

89.3 

90.1 

90 9 

92 4 

92.0 

91 4 

92_3 

90_9 

88_0 

86.2 

85.5 

84.7 

86.1 

87.5 

87.4 

88.2 

95.0 

97.9 

92.9 

88.3 

84.4 

79.8 

77.6 

75.2 

728 

70_9 

38_7 

69_1 

67_5 

66_5 

65.7 

65_5 

65_1 

65.2 

65 3 

65_8 

66.7 

674 

69 1 

70 1 

71_2 

73 1 

74_9 

76_9 

78.4 

79_9 

80_9 

81.3 

81.7 

81.5 

81.3 

81 3 

81 1 

81.3 

81_5 

81_5 

82 ~ 

82 6 

83 6 

21.6 

21_7 

21.6 

21_6 

21.5 

21.5 

21.6 

21.7 

21.6 

21.8 

22 0 

21 9 

22.0 

222 

22 1 

22.2 

22.3 

22.1 

22.1 

22.0 

22.0 

21.7 

21.7 

21.8 

21.6 

21.5 

21.7 

21.6 

21.5 

21.6 

21.7 

21 7 

22_0 

22_2 

22_2 

22_3 

22 4 

22_5 

22_5 

22_6 

22_6 

22.4 

22.3 

22.2 

22.0 

222 

22 1 

221 

22 1 

220 

22_0 

21.9 

21_7 

21_6 

21_6 

21.6 

21.7 

21 8 

21.9 

221 

221 

221 

22 0 

21.8 

21_8 

220 

21 9 

2.6 

2.6 

2.5 

2.4 

2.4 

23 

2 3 

2.3 

2.3 

2.3 

24 

2.3 

2.3 

2 2 

2.2 

2.3 

2.3 

2.3 

2.2 

22 

22 

22 

2.3 

22 

2.3 

2.3 

2.3 

2.2 

22 

2.2 

2.1 

21 

2.1 

21 

1 9 

2 1 

21 

2 1 

21 

21 

21 

21 

2.2 

2.1 

2.2 

21 

21 

2.3 

22 

21 

21 

22 

21 

2.2 

2.2 

22 

22 

2.3 

2.3 

2.3 

2 1 

21 

22 

22 

20 

2.1 

22 

8/23/05 Run #1 

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08123105 09:40:02 

08/23105 09:40.12 

08/23/05 09:40:22 

08123105 09:40:32 

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08123105 09:41 :12 

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08/23/05 09:44.12 

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08/23/05 09:44.32 

08/23/05 09.44:42 

08/23/05 09:44:52 

08/23/05 09.45:02 

08/23/05 09.45:12 

08123105 09:45:22 

08/23/05 09:45:32 

08/23/05 09:45.42 

08/23/05 09 45.52 

08/23/05 09 46-02 

08/23/05 09 46-12 

08/23/05 09 46:22 

08/23/05 09'46:32 

08/23/05 09 46:42 

08/23/05 09:46.52 

08123105 09:47:02 

08123105 09:47:12 

08123105 09:47:22 

08/23/05 09.47:32 

08123105 09.47:42 

08123105 09:47:52 

08/23/05 09.48:02 

08123105 09 48:12 

08123105 09:48.22 

08/23/05 09:48:32 

08/23/05 09.48:42 

08/23/05 09:48:52 

08123105 09:49:02 

08/23/05 09:49.12 

08/23/05 09:49"22 

08/23/05 09'49:32 

08/23/05 09:49:42 

08/23/05 09'49:52 

08/23/05 09:50:02 

08/23105 09:50:12 

08123/05 09:50'.22 

08/23/05 09:50:32 

08/23/05 09:50:42 

08/23/05 09:50.52 

08/23/05 09 51:02 

08123105 09:51:12 

08123105 09:51:22 

08/23105 09'51 '32 

08/23105 09 51:42 

08/23105 09 51:52 

08/23/05 09.52:02 

08/23/05 09·52: 12 

4.5 

4.4 

4.4 

4.4 

43 

4.5 

4.3 

4.4 

4.6 

4.6 

4.6 

4.9 

4.9 

5.0 

4.5 

45 

4.8 

4.6 

5.0 

4.8 

4.5 

4.5 

4.5 

4.8 

4.6 

46 

4.5 

4.6 

4.5 

44 

4.4 

4.3 

4.6 

4.3 

4.6 

4.8 

45 

4.7 

4.6 

5.1 

4.5 

44 

4.5 

4.6 

4.4 

44 

46 

4.6 

4.8 

4.6 

4.5 

4.3 

4.4 

4 5 

46 

45 

5.2 

4 9 

4.6 

4 6 

4.7 

4.8 

4.7 

4 9 

5.0 

4.7 

4.6 

4.8 

45 

4.4 

4.0 

3.8 

37 

3 6 

84.4 

85.4 

86.9 

87_7 

88.2 

88_8 

89 1 

89.8 

90.5 

91.2 

91_9 

92_2 

92_6 

93_0 

92_9 

93.0 

93.3 

93.5 

93.9 

93.9 

93.9 

94.4 

93.9 

93.6 

93.0 

92.2 

92.0 

91 _7 

91.8 

92.3 

92 1 

92 3 

92.6 

92.4 

92.7 

92.8 

92.3 

92_3 

92 1 

921 

92_9 

93_5 

93.7 

93.8 

93.9 

94.2 

94 4 

95_0 

95_6 

95_8 

95_9 

95.8 

95_9 

96.1 

96.4 

96.8 

96.9 

97.0 

96.9 

96 5 

96_2 

96_2 

96_1 

96.2 

96.7 

96.8 

96 9 

97_3 

97_6 

98.3 

99.3 

gg 6 

100_1 

100.4 

21.9 

22.1 

22.1 

22.0 

22 0 

22_0 

22.2 

22_2 

22.3 

22.3 

22.3 

22.2 

22.3 

22.3 

22.3 

22.3 

22.3 

22.3 

22.3 

22.4 

22.3 

22.4 

22_4 

22.4 

22.5 

22.6 

22.7 

22.7 

22.7 

22.6 

22.4 

22.4 

22.7 

227 

23.0 

23 1 

23.1 

23.0 

23.1 

23.2 

23.2 

23.3 

23.4 

23.4 

23.4 

23.5 

23.3 

23.2 

23.2 

23.2 

23.1 

23.0 

22_9 

22.7 

22.8 

22_7 

22_6 

22.6 

22.7 

22.7 

22.7 

22.7 

22.7 

22.6 

22_7 

22.4 

221 

21.9 

21.8 

21.9 

221 

221 

22.4 

22_5 

2.3 

2.3 

2.2 

21 

21 

22 

23 

2.3 

2.3 

2 3 

2.3 

2.2 

2.2 

2.3 

23 

2 3 

2.3 

2.4 

2.4 

24 

2.4 

2.3 

2.3 

2.3 

22 

22 

22 

2.2 

2.2 

2.3 

2.3 

23 

2.3 

2.4 

2.4 

24 

24 

2.3 

2.3 

24 

2.5 

2.4 

2.4 

2.4 

2.4 

2.5 

2.3 

23 

2.3 

2.3 

2.3 

2.4 

2.4 

2.4 

2 5 

2.4 

24 

24 

24 

25 

2.6 

26 

24 

24 

25 

26 

2_5 

2.5 

2.4 

24 

2.3 

24 

2.4 

2.5 

8/23/05 Run #1 

2CI 

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08/23/05 09-52:22 

08123105 09:52·32 

08/23/05 09:52:42 

08/23105 09:52:52 

08/23/05 09:53-02 

08/23/05 09'53:12 

08123105 09:53:22 

08/23/05 09:53:32 

08/23/05 09:53:42 

08/23/05 09:53:52 

08/23/05 09:54:02 

08123105 09:54:12 

08/23/05 09:54:22 

08/23/05 09:54:32 

08/23/05 09:54:42 

08123105 09:54:52 

08/23105 09"55:02 

08123105 09:55·. 12 

08/23/05 09:55:22 

08/23/05 09:55:32 

08/23/05 09:55'42 

08123105 09:55:52 

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08123/05 09.59'12 

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Port Change 

08123105 10:00:02 

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08123105 1 o·o3 12 

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08123/05 10·.03:42 

08/23/05 10:03:52 

08/23/05 10:04:02 

08123105 10.04:12 

08/23/05 10:04:22 

3.7 

3 9 

39 

3.6 

3.4 

3.4 

3.4 

3.4 

3.4 

3.7 

3.7 

3.4 

3.4 

3.5 

3.4 

3.4 

3.5 

3.6 

3.6 

3.6 

3.7 

36 

3.5 

3.5 

3.5 

3.4 

3.4 

3.3 

3.2 

33 

3 4 

3.4 

3.5 

3.8 

3.5 

3.6 

39 

3.7 

4.2 

4.4 

4 0 

3 7 

3.6 

3.6 

3.6 

34 

3.4 

1.7 

1.3 

1.4 

1 4 

1.4 

1.5 

1.5 

1.5 

1.4 

1.3 

1.2 

1.3 

1.4 

1.3 

1 3 

1.2 

1 2 

1 3 

1.2 

1 3 

1.3 

1.3 

1 5 

1.4 

1.3 

30 

99.8 

98.4 

97.1 

95.3 

93 4 

91.3 

89.1 

87.8 

85.8 

84.1 

82.5 

80.5 

78.5 

77.3 

77.0 

78.1 

79.8 

80.6 

81.7 

83.3 

84.6 

85.9 

86.2 

86 8 

87.3 

87.8 

88.2 

88.0 

87.7 

87.4 

86.7 

85.5 

85.4 

85.2 

84.2 

84.3 

8" 

84.0 

84.2 

84.2 

83.7 

84.7 

86.9 

88.2 

88.5 

89.4 

90.5 

90.8 

88.8 

62.9 

37.2 

22.3 

15.0 

11.1 

8 9 

7.2 

6.2 

57 

55 

5.1 

5.2 

5.1 

50 

48 

4.6 

4 9 

4.8 

4.8 

52 

53 

54 

5.6 

53 

22.7 

23.0 

23 2 

23.2 

23 3 

23.4 

23.3 

23 4 

23.5 

23.5 

23.6 

23.5 

22.9 

227 

22.7 

22.4 

22.3 

22.3 

22.1 

22.1 

22.1 

22.0 

22.0 

22.0 

21.9 

21.9 

21.8 

21 8 

21.9 

21.9 

22.0 

22.2 

22 2 

22.3 

22.6 

22.5 

22.4 

22.5 

22.3 

22.3 

22.2 

21.8 

21.7 

21.8 

21.8 

21.6 

21.5 

21.5 

212 

17.0 

10.8 

72 

51 

40 

3.4 

3.0 

27 

24 

23 

2.2 

20 

1.9 

1 8 

1 7 

1 6 

1 5 

1 5 

1.4 

14 

1.3 

1.2 

1 2 

12 

2.5 

24 

2 5 

24 

2.4 

2 4 

2 5 

2.4 

2.4 

2.3 

2.4 

25 

2.5 

2.4 

2.5 

25 

25 

2 5 

2.5 

2.5 

24 

25 

25 

2.5 

2.4 

2.4 

24 

2.4 

2.5 

2.5 

2.6 

2.5 

2.4 

2.4 

2.5 

25 

2.5 

2.5 

2.5 

2.5 

25 

2.5 

25 

2.5 

2.5 

2.4 

2.4 

2.4 

2.5 

2.6 

2.5 

2 4 

2.4 

23 

22 

2.2 

2.2 

2.2 

2.3 

22 

22 

2.2 

2.3 

2.3 

2.3 

2.3 

23 

22 

2 3 

2.3 

2.3 

23 

22 

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08!23!05 10:04:32 

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08/23/05 10.04.52 

Resume Sampling 

08/23/05 10:05:02 

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08/23/05 10"10:02 

08/23/0510'10'12 

08!23105 10:10·22 

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08/23/0510:11:02 

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08/23/0510"12.22 

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08123/05 10.16.02 

08123/0510"16·12 

08123/0510"16:22 

08/23/05 10.16.32 

3.9 

3.9 

3.8 

35 

34 

33 

3.3 

3.2 

3.4 

3.3 

3.3 

33 

3.4 

3.6 

38 

3 7 

3.9 

34 

3.4 

3.2 

3.2 

3.2 

3.4 

3.3 

3.2 

3.3 

3.8 

3.6 

3.8 

4.1 

38 

35 

3.5 

3.6 

3 7 

3.5 

3.5 

3.4 

3.5 

3.6 

3.6 

3.6 

3.6 

3.7 

38 

4.0 

4.1 

4.1 

4.5 

4.5 

4.3 

4.3 

4 1 

40 

4.1 

4.4 

4.1 

40 

4.0 

43 

4.3 

44 

4.7 

4.3 

4.1 

4.1 

4 2 

42 

41 

4.1 

4.1 

4.0 

3.9 

5.6 

19.8 

41.8 

54.7 

59.7 

60.6 

59.1 

56.4 

53 7 

51.9 

50.9 

50.4 

50 8 

52.2 

52.8 

54 1 

56 5 

57.7 

60.1 

61.8 

64.3 

66.4 

67.2 

68.1 

68.9 

68.1 

68.3 

68.0 

69.0 

70.5 

71.5 

73.9 

76.3 

78.4 

80.5 

82 1 

83.3 

84 2 

84 6 

84.8 

85 0 

84.7 

84.6 

84.6 

84.8 

85.1 

84.8 

84.5 

84.6 

84.9 

85.6 

86.9 

87.7 

88.3 

88.4 

88 1 

88.0 

88.0 

88.1 

88.2 

88.2 

88.4 

88 7 

88 4 

88.5 

89 1 

89 4 

89 1 

89.1 

89.1 

90 1 

90.9 

91.4 

11 

2.9 

91 

13.9 

16.3 

177 

18.8 

19.2 

19.6 

20.0 

20.0 

20.2 

20.6 

20.4 

20.2 

20.3 

20.1 

19.8 

20.0 

19.9 

19.6 

19.8 

20.0 

20.2 

20.0 

19 6 

19.5 

19.5 

19.3 

19 4 

19.5 

19.8 

19.9 

19.8 

19.9 

19 7 

19.6 

19 8 

19.9 

20.0 

20.3 

20.7 

20 8 

20.9 

20.6 

20.5 

20.6 

20.6 

20.8 

20.8 

20.7 

20.5 

20.4 

20.4 

20.7 

20.9 

21.1 

21.4 

214 

21.5 

21.2 

21.0 

213 

21.4 

21 4 

215 

21.5 

215 

21.4 

21.5 

21 5 

217 

21 7 

2.2 

2.2 

23 

23 

2.3 

2.4 

24 

24 

2.6 

2.6 

2.5 

24 

2.5 

2.5 

2.6 

26 

2 5 

25 

25 

2.5 

2.6 

2.6 

2.4 

24 

2.5 

2.5 

2.6 

2.5 

2.5 

25 

26 

26 

2.5 

2.5 

2.5 

25 

2.5 

2.5 

2.6 

2.7 

2.7 

2.8 

2.7 

26 

2.7 

26 

2.7 

2.7 

27 

2.6 

2.5 

2.6 

2.7 

2.6 

2.5 

26 

2.6 

2.6 

27 

28 

2.8 

2.8 

2.7 

2.7 

2.6 

2.6 

2 6 

2.6 

27 

28 

2.8 

27 

28 

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08/23/05 10:27:02 

08/23/0510.27"12 

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08/23105 10:28:02 

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08/23/05 10'28'32 

08/23/05 10:28:42 

08123105 10'28.52 

38 

3 7 

3 7 

3.6 

3 7 

3.9 

3 7 

39 

3.6 

3.8 

4.1 

3 7 

3.8 

3.9 

3.8 

3.6 

3.7 

35 

3.5 

3.6 

3.5 

3.5 

3.3 

3.4 

3.8 

36 

3.4 

3.3 

3.5 

3.5 

3.7 

3.4 

3.6 

3.6 

3.5 

3.6 

3.7 

3.9 

3.9 

3.8 

3.8 

38 

39 

4.0 

4.0 

4.0 

42 

4.3 

4.3 

4.2 

4.0 

4.0 

40 

4.2 

4.0 

4.2 

4.3 

4.2 

42 

4.1 

3.9 

4.2 

41 

4.2 

40 

4.0 

4.2 

4.3 

4.3 

4.4 

4.5 

4.3 

42 

4.4 

92_3 

91_3 

89.5 

88.3 

87 1 

85.6 

84.6 

83.3 

82 4 

81 6 

79.7 

78.6 

78_5 

78.4 

79 2 

80.6 

81.3 

82.3 

83.1 

83.3 

84.4 

85.1 

85.5 

86.5 

86.8 

87 1 

87 4 

86.9 

87.0 

86.4 

85.7 

85.6 

85_3 

85.5 

85 6 

85.2 

86 0 

86.2 

86.3 

87.1 

87.8 

87.8 

88.5 

89.1 

89.7 

90 6 

91 _4 

91 9 

92_8 

93.5 

93.9 

94_8 

95.4 

95.6 

95.9 

95.1 

94.8 

94_4 

93 8 

93 7 

93.2 

92.8 

93.0 

92.7 

91.4 

90 8 

90 2 

89 5 

90 5 

91 2 

92.0 

92.9 

93.1 

93 5 

21 8 

21 7 

21.6 

21.6 

21 4 

21.4 

21.6 

21.5 

21 6 

21 6 

21.5 

214 

21.4 

21 3 

21.6 

21.7 

21.9 

22.0 

22.1 

22.1 

22.2 

22.1 

22.0 

221 

223 

22.2 

22.2 

22.2 

22.3 

22.5 

22.5 

22.6 

22_5 

22_3 

22.3 

22.1 

22.2 

22.2 

21.9 

21.8 

21_9 

21_8 

21.5 

21.6 

21.6 

21_6 

21.6 

21_6 

21.4 

21.2 

21.2 

21.0 

21 1 

21.2 

21.3 

21.3 

21.4 

21.5 

21.5 

21_6 

21_6 

21.6 

21.6 

21.5 

21.6 

21.5 

21_6 

21 5 

21 4 

21_3 

21 1 

21 1 

21.1 

21 0 

28 

2.8 

2.8 

28 

2.8 

2.8 

28 

2.7 

28 

2.8 

2.8 

2.8 

28 

2.7 

2.7 

2.8 

2.8 

2.7 

2.7 

2.7 

2.7 

27 

2.7 

2.6 

2.6 

2.5 

2.6 

26 

27 

27 

26 

2.5 

2.6 

2.7 

28 

2.8 

2.7 

2.7 

2.8 

27 

2 7 

2.6 

2.7 

2.7 

2.8 

2.8 

2.8 

2.8 

2.8 

28 

2.8 

2.7 

2.8 

2.8 

2.8 

27 

27 

2.8 

2.8 

2.8 

28 

2.8 

2.8 

2.9 

2.8 

28 

2.9 

2.8 

28 

2.8 

2.8 

2_9 

2.9 

29 

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08123105 10:29.22 

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08123105 10.29'.42 

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08/23/0510:34.52 

Stop Run #1 

08/23/05 10.35•02 

08123105 10:35:12 

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08123105 10:35:42 

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08/23/05 10 36·.22 

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08/23/05 1 0'.3 7A2 

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08/23/0510:38:02 

08123105 10:38 12 

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08/23/05 10 40'02 

08/23/0510-40:12 

08123/05 10:40:22 

08123105 10:40.32 

08/23/05 10 40:42 

4.2 

4 1 

41 

41 

4.2 

40 

38 

39 

41 

4.3 

4.2 

4.1 

39 

38 

3.9 

3.7 

3.6 

36 

33 

32 

3.2 

3.1 

3 1 

31 

3.1 

3.1 

3.2 

3.0 

3.1 

3.2 

3.2 

3.6 

3.6 

3.3 

33 

33 

3.94 

3 2 

27 

1 4 

1 3 

1.3 

12 

1.3 

1.2 

12 

12 

1.2 

12 

1.3 

1.3 

1.2 

12 

1.2 

12 

12 

12 

11 

1.2 

11 

11 

1 2 

12 

11 

11 

12 

11 

1.1 

11 

11 

11 

11 

94.2 

95.9 

96.3 

95.4 

94 1 

93 6 

93.1 

93 7 

93.6 

92.2 

91.6 

91.8 

91.8 

92.1 

92.6 

92.4 

93 2 

94.5 

95.9 

97.7 

97.1 

94.6 

92.8 

90.3 

87.5 

86.0 

82.4 

78 6 

75.6 

73.1 

71.3 

70.9 

70.4 

70.3 

70.9 

71 1 

85.18 

70.8 

72.5 

70.8 

64.6 

44.7 

30.9 

21.5 

16.3 

12.9 

10 7 

95 

8.8 

8.1 

7.6 

7.7 

75 

72 

7.2 

7.1 

7 1 

74 

7.0 

7 1 

70 

6.2 

6.3 

6 1 

6.1 

6 1 

6.1 

6 0 

6 1 

6 1 

60 

6.3 

21.2 

21 0 

20.9 

20.9 

20.9 

21 0 

21.2 

21 1 

21.3 

21.4 

21.1 

21.2 

21.2 

21.0 

21.2 

21 3 

21.2 

21 3 

21.5 

21 3 

21 .5 

21.7 

21.8 

22.2 

22.4 

22.5 

22.6 

22.7 

224 

22.3 

22.2 

22.1 

22.0 

22.0 

22.1 

22.2 

21.73 

22 2 

21.9 

20.9 

19.8 

14.9 

11.0 

8.6 

7.0 

5.8 

4.9 

4.3 

3.9 

35 

3.3 

3.2 

3.0 

2.9 

2.9 

3.2 

31 

29 

27 

24 

2.3 

22 

2 1 

2.0 

20 

1.9 

18 

1.8 

17 

1.7 

1.6 

1 6 

2.9 

2.9 

29 

2.9 

2.8 

27 

2.7 

2.9 

3.0 

2.9 

2.9 

2.8 

2.8 

2.8 

2.8 

2.7 

2.8 

27 

28 

2.8 

29 

30 

2.9 

2.9 

3.0 

2.9 

29 

2.8 

2.8 

2.8 

2.7 

27 

2.8 

2.7 

2.7 

2.8 

2.51 

2 9 

2.9 

29 

2.8 

2.7 

2.7 

28 

27 

2.5 

2.6 

2.7 

2.7 

2.6 

2.6 

2.5 

2.5 

2.5 

2.6 

2.7 

2.6 

2.6 

2.6 

2.5 

2.6 

2.6 

25 

2.5 

2.5 

2.5 

26 

2.6 

2.6 

2.5 

2.5 

25 

8123/05 Run #1 

33 

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08123/05 "10.40.52 

08123105 10.41:02 

08/23105 1 0:41:12 

08/23/05 10:41'.22 

08/23/05 10:41:32 

08/23/05 10:41:42 

08123105 10:41.52 

08/23/05 10:42:02 

08/23/05 10:42:12 

08/23/05 10:42:22 

08123105 10:42'32 

08123105 10.42'42 

08/23/05 10:42:52 

08/23/05 10:43:02 

08/23/0510:43:12 

08/23/05 10.43:22 

08/23/05 10:43:32 

08/23/05 10:43:42 

08/23/05 10.43:52 

08/23/05 10:44:02 

08/23/0510:44:12 

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08/23/05 10:44:32 

08/23/05 10:44:42 

08/23/05 10:44'52 

08/23/05 10.45:02 

08/23/0510:45:12 

08/23/05 10.45:22 

08/23/05 10:45:32 

08/23/05 10:45:42 

08123105 10:45:52 

08123105 10.46:02 

08/23/05 10:46:12 

08/23/05 10:46'22 

08123105 10.46:32 

08123105 10:46:42 

08123/05 10:46:52 

08/23/0510:47:02 

08/23/05 10:47:12 

08/23/0510:47:22 

08/23/0510:47:32 

08/23/0510:47:42 

08/23/05 10:47:52 

08/23/05 10:48:02 

08/23/05 10:48:12 

08/23/05 10:48:22 

08/23/05 10:48:32 

08/23/05 10:48:42 

08/23/05 10:48:52 

08/23/05 10:49:02 

08/23/05 10:49:12 

08/23/05 10 49:22 

08123/05 10:49:32 

08/23105 10:49'42 

08123/05 10 49:52 

08/23/05 10:50'02 

08/23/0510:50.12 

08123/05 1 0'50:22 

08/23/0510:50'32 

08123/05 10"50:42 

08/23/05 10·.50:52 

08/23/05 10:51:02 

08/23/0510·51·12 

08123105 1 0:51 .22 

08/23/0510:51:32 

08/23/05 10:51.42 

08/23105 10'51:52 

08/23/05 10:52:02 

08/23/0510:52:12 

08123/05 10'52:22 

08/23/05 10:52:32 

08/23/05 10·52'42 

08/23105 10:52:52 

11 

1 2 

1.1 

1.1 

1.1 

11 

1.1 

1.2 

1.1 

1.1 

1.1 

1.2 

1.1 

1.1 

1.1 

1.1 

1.1 

1.1 

1.1 

1.0 

1.0 

1.0 

1.0 

1.1 

1 0 

1.1 

1.1 

11 

1.1 

1.1 

11 

1.1 

04 

0.1 

0.1 

0.1 

0.0 

01 

0 0 

0.0 

0.1 

00 

0.1 

0 1 

0 1 

0 1 

00 

0 1 

0 1 

00 

0 0 

00 

00 

00 

00 

0 3 

00 

0 0 

0.0 

0.0 

0 0 

00 

0.0 

0.0 

0.0 

0.0 

00 

00 

0.0 

00 

o.o 

o.o 

o.o 

6.0 

6 0 

6.3 

6.1 

6.2 

6.0 

6.1 

62 

59 

6.0 

5.9 

5.8 

6.1 

5.8 

6.0 

6.0 

5.9 

6.1 

5.9 

59 

5.9 

6.0 

6.1 

6.0 

5.9 

6.1 

5.7 

60 

59 

5.8 

5.9 

6.2 

6.0 

6.0 

6.0 

5.8 

5.9 

6.0 

5.9 

5.8 

5.8 

56 

56 

57 

5.7 

5.7 

5.7 

5.6 

55 

54 

54 

53 

5.1 

5.2 

5.2 

5.0 

49 

6 9 

27.0 

53.5 

69.6 

82.1 

88.6 

93.1 

96.8 

98.8 

100 2 

100.9 

101.7 

102.1 

102.3 

102.3 

102.3 

16 

1 5 

1.5 

1 4 

1.5 

14 

1.4 

1 4 

1.4 

1 4 

1.3 

1.2 

1 3 

10 

1.2 

1.2 

1.1 

1.1 

1.1 

1.1 

1.0 

1.0 

1.0 

09 

0.9 

0.9 

0.9 

09 

0.9 

0.8 

0.8 

0 8 

08 

0.8 

3.7 

9.3 

14.0 

17.8 

20.4 

21.9 

22.8 

23 2 

23.6 

23 8 

24.0 

24.0 

24.1 

24.1 

24.1 

24.3 

24.3 

24.3 

24.4 

24.4 

24.4 

24.2 

24 3 

23 6 

18.5 

11.4 

7.7 

4 9 

33 

2 3 

1.6 

11 

09 

0.7 

06 

05 

0.5 

0.5 

0.4 

26 

2.5 

24 

2.4 

2.4 

2.4 

24 

2.4 

2 5 

24 

2.5 

25 

24 

24 

2.5 

25 

2.6 

2.6 

2.5 

2.4 

2.4 

25 

2.5 

2.6 

2.5 

2.5 

2.4 

2.4 

26 

25 

2.5 

2.6 

26 

27 

2.5 

2.6 

2.6 

2.5 

25 

2.6 

2.6 

2.5 

2.4 

24 

2.5 

26 

25 

2.5 

2 5 

25 

2.5 

26 

2.5 

2.4 

2.4 

2.4 

24 

2.4 

24 

25 

2.6 

26 

2.6 

25 

2.5 

2.5 

2.5 

2.5 

2.5 

2.5 

2.4 

25 

26 

8/23/05 Run #1 

25.5 ppm NOx 

Zero CO, S02 

99.1 ppm CO 

Zero VOC, NOx 

Page 7 

34 
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I 08/23/05 10:53:02 0.0 102.4 0.4 26 

08/23/0510:53:12 0.0 102.0 04 2.5 

I 08/23/05 10:53:22 0.7 102.0 0.4 2.6 

08123105 10"53:32 0.9 101.4 0.5 2.5 

08/23/05 10:53:42 1.0 95.7 0.4 2.6 

08/23/05 10:53.52 1.0 77.8 0.4 2.6 

08/23/05 10'54:02 0.8 50.2 0.4 25 

I 08/23/05 10:54:12 0.1 28.9 0.5 2.5 

08/23/0510:54'22 0.1 16.4 0 5 2.5 

08/23/05 10:54:32 0.1 11.4 06 2.6 

08/23/05 10:54:42 00 8.7 0.7 2.8 

I 08/23/05 10 54:52 0 0 7.2 0.7 3.4 

08/23/05 10:55:02 0.0 6.5 0.8 4.2 

08/23/0510:55.12 0.0 6.2 0.8 5.0 

08/23/05 10'55:22 0.0 6.0 0.8 76 

08123105 10"55:32 0.0 6.0 0.8 10.2 

I 08123105 10:55:42 0.0 5.8 08 12 7 08/23/05 10·55"52 00 5.7 0.8 15.7 

08/23/05 10-56:02 00 5.7 0.8 18 8 

08123105 10:56:12 0 0 60 0.8 21 8 08123105 10:56:22 0.0 60 0.8 24.3 

I 08123105 10:56-32 0.0 58 0.8 26 7 08123105 10:56'42 0.0 5.8 0.8 28 9 

08/23/05 10:56"52 0.0 5.8 0.8 31 1 08123105 10:57:02 0.0 5.7 0 8 33.2 

I 08/23/05 10:57:12 0.0 5.7 0.8 34.9 

08/23/05 10:57:22 0.0 5.4 07 36.4 

08/23/05 10:57:32 0.0 5.5 0.8 37.8 

08/23/05 10:57.42 0.0 5.5 0.7 38.9 

08123105 10:57:52 00 5.5 0.7 40.0 

I 08/23/05 10:58:02 00 5.6 0.7 41.1 

08/23/0510:58:12 00 55 0.7 42.0 

08/23/05 10:58:22 00 54 0.7 42.7 

08/23/05 10:58:32 00 5.7 0.7 43.4 

08/23/05 10:58:42 0.0 5.9 0.7 44 1 

I 08/23/05 10·58:52 00 59 0.7 44.8 

08/23/05 10:59:02 0.0 5.9 0.7 45.3 

08/23/0510:59:12 00 60 0.6 45.8 

08/23/05 10:59:22 0.0 5.9 0.6 46.2 

08/23/05 10:59:32 0.0 5.5 06 46.5 I 08/23/05 10:59:42 0.0 5.5 06 46.7 

08/23/05 10:59.52 00 5.3 0.6 47.0 

08123/05 11 :00.02 00 5.3 0.7 47.3 

08/23/0511:00:12 0.0 5.8 06 47.6 

I 08/23/05 11:00:22 0.0 5.8 0.6 47.8 

08/23/05 11 :00:32 00 5.8 0.6 481 

08123105 11 :00:42 00 6 0 0.6 48.2 

08/23/05 11 :00:52 00 55 06 48.4 

08/23/05 11:01:02 00 57 0 6 48.6 I 08/23/0511:01:12 0 0 5.6 0.6 48.8 50.1 ppm S02 

08/23/05 11:01:22 00 5.5 0.6 48.9 

08/23/05 11:01:32 00 5.6 0.5 48.9 

08/23/05 11:01:42 0.1 5.8 05 48 4 I 08/23/05 11:01:52 11.7 59 0.5 47.0 

08/23/05 11:02:02 14.6 6.0 0.5 47.0 

08/23/05 11:0212 14.6 5.9 0.5 47.1 15.2 ppm C3H8 

08/23/05 11:02:22 14.7 59 04 46.4 I 08/23/0511.0232 14.7 6.1 0.3 44 1 

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08/23/05 11 '44:02 

08/23/0511 44:12 

08/23/05 11:44:22 

08/23/05 11:44:32 

08123105 11:44:42 

08/23/05 11:44:52 

Start Run #2 

08/23/05 11:45:02 

08/23/05 11'45:12 

08/23/05 11 '45:22 

08/23/05 11:45 32 

08123/05 11:45 42 

08123105 11:45:52 

08123105 11 '46:02 

08/23/05 11 :46'12 

08/23/05 11 :46:22 

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08/23/05 11 :46'42 

08/23/05 11 '46:52 

08/23/0511:47:02 

08/23/05 11 :4 7:12 

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08123105 11:47:52 

08/23/0511:48"02 

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08123105 11:48:52 

08/23/05 11 :49:02 

08/23/0511:49:12 

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08/23/05 11:49:32 

08/23/05 11:49:42 

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08/23/05 11:50:02 

08/23/05 11 .50.12 

08/23/05 11.50:22 

08/23/05 11:50:32 

08/23/05 11:50.42 

08/23/05 11:50:52 

08/23/05 11:51 :02 

08/23/0511:51:12 

08/23/05 11:51.22 

08/23/05 11'51 :32 

08/23/0511:51:42 

08/23/05 11:51 :52 

08/23/05 11:52:02 

08/23/0511:52:12 

08/23/05 11:52:22 

08/23/05 11:52:32 

08/23/05 11:52:42 

08/23/05 11 .52:52 

08/23/05 11:53:02 

08/23/05 11:53:12 

08/23/05 11 .53:22 

08/23/05 11:53:32 

08/23/05 11:53:42 

08/23/05 11:53:52 

08/23/05 11 .54:02 

08123105 11:54:12 

08/23/05 11 :54"22 

08/23/05 11 '54:32 

08/23/05 11-54.42 

08123105 11:54:52 

08/23/05 11 ·5s-oz 

08/23/05 11:55 12 

08/23/05 11:55:22 

08/23/05 11"55:32 

VOC CO NOx 502 

ppm ppm ppm ppm 

4.0 91.9 20.4 2.5 

4.0 92.2 20.2 2.6 

4.0 92.9 19.9 2.5 

4.0 

4.3 

4.4 

4.2 

4.0 

4.1 

41 

4.2 

4.0 

4.0 

4.1 

4.0 

3 9 

3.8 

3 7 

3.6 

35 

3.8 

3.9 

3.8 

3.6 

3.6 

3 4 

3.7 

3 7 

3.5 

3.7 

3.9 

4.1 

40 

38 

4.1 

38 

3.8 

3 9 

3 9 

3.9 

4.0 

3.8 

3.7 

3.7 

3.9 

3.9 

3.8 

4.0 

4.4 

4 5 

4.1 

3.9 

3.8 

3.8 

3.8 

3.8 

38 

3.7 

3 7 

3.7 

3.6 

3.5 

3.5 

3 3 

33 

34 

34 

35 

3.5 

3.4 

93.2 

93_4 

94.2 

95.1 

95.5 

96.2 

96.0 

96.0 

96.7 

97.8 

98 1 

97 8 

97_3 

97.1 

96 6 

95_4 

93_6 

91_8 

891 

87.3 

85_3 

82_1 

79 9 

79.0 

78.2 

78.0 

78 6 

79.5 

80.4 

810 

81_7 

82_0 

82 6 

83.0 

84 3 

85.6 

86.7 

88.0 

88.5 

89.4 

90.6 

90.6 

91.5 

92 5 

92.4 

93.3 

94.0 

94.2 

94.9 

95 7 

95.4 

95.4 

95.9 

95.4 

95.5 

96.0 

95.7 

96.5 

97.3 

97.3 

97 4 

97_1 

95 7 

94 7 

93_7 

91 5 

90 0 

19_8 

19 6 

19.5 

19.8 

19 9 

20.0 

20 1 

20.2 

20 0 

20_1 

19_8 

19.8 

19.9 

20 1 

20_2 

20.4 

20.7 

20.8 

20.9 

21.0 

20.9 

20_9 

20_8 

20.5 

20.6 

20_7 

20.6 

20.9 

20.8 

?0 6 

20_7 

20.6 

20.7 

20_8 

20.9 

21 0 

21 3 

21.5 

21 5 

21.4 

21.3 

21_2 

21 0 

21.0 

20_9 

21.0 

21.0 

20.9 

20.9 

211 

21 2 

21_1 

211 

21 1 

21_0 

20 9 

20 9 

20 9 

20 7 

20.6 

20 5 

20 5 

20.5 

20.8 

20_8 

20 8 

20_9 

2.4 

25 

24 

2.5 

25 

2.4 

2.4 

2.5 

26 

2.6 

25 

2.5 

2.5 

2 4 

2.6 

26 

2.5 

2.5 

2.4 

2.4 

2.4 

2.4 

2.3 

2.3 

24 

2.4 

24 

2.3 

2.3 

2.4 

2.4 

2.3 

2.4 

2.4 

2 3 

23 

2.5 

24 

23 

2.3 

2.3 

2.3 

2.4 

25 

2.4 

2.5 

2.6 

2.4 

2.4 

24 

23 

23 

2.3 

2.4 

2.4 

24 

2.3 

2.4 

24 

2.4 

2.4 

23 

2_3 

2.3 

2.3 

24 

2.3 

8123!05 Run #2 

36 

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08123105 12:00:32 

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08/23/0512:01:12 

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08/23/0512:01:32 

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08/23/05 12:02'02 

08/23/05 12:02:12 

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08123105 12:02:32 

08/23/05 12:02:42 

08/23/05 12:02:52 

08/23/05 12:03:02 

08/23/05 12:03'12 

06/23/05 12:03:22 

08/23/0512.03:32 

08/23/05 12:03:42 

08/23/05 12:03:52 

08/23/05 12-04:02 

08/23/0512.04:12 

08/23/05 12-04:22 

08/23/05 12:04:32 

08/23/05 12:04'42 

08/23/05 12'04:52 

08/23/05 12:05.02 

08/23/05 12.05:12 

08/23/05 12:05:22 

08123105 12:05:32 

08/23/05 12:05.42 

08123105 12:05:52 

08123105 12.06:02 

08/23/0512'06.12 

08/23/05 12:06:22 

08/23/05 12:06:32 

08/23/05 12:06:42 

08/23/05 12:06:52 

08123105 12'07:02 

08/23/05 12:07:12 

08/23/05 12:07:22 

08/23/05 12:07"32 

08/23/05 12"07:42 

08123105 12.07:52 

36 

37 

3.8 

3.9 

3.9 

3.9 

3.9 

3.9 

3.9 

4.0 

4.0 

4.4 

4.3 

41 

4.1 

4.1 

4.0 

41 

4.1 

4.0 

4.0 

42 

4.3 

4.3 

4.1 

4.3 

4.2 

4.1 

4.1 

4.0 

40 

40 

3.9 

3.8 

4.0 

3.9 

3.9 

3.9 

4.0 

39 

39 

4.0 

3.9 

3.7 

3.8 

3 7 

3.5 

3.3 

3.2 

3.2 

3.2 

3.2 

3.3 

3.9 

38 

3.6 

3.5 

3.5 

38 

3.7 

3 8 

3 7 

3 5 

35 

34 

3.5 

3.4 

34 

34 

3.5 

36 

3.6 

36 

3.7 

89_3 

88.2 

87 8 

88.0 

88.0 

88.4 

88 9 

89.4 

90.4 

91.0 

91.0 

91.5 

91.7 

91.8 

92.3 

92.6 

92.3 

92.5 

92.6 

92.7 

92.8 

93_0 

93.1 

93.6 

93 6 

93.7 

94.1 

94.8 

94.7 

95.0 

95.4 

95:2 

95 7 

95.9 

951 

95.2 

97.5 

96.7 

95.5 

95.2 

94_5 

94.3 

94.6 

94.6 

94.6 

94.9 

94.9 

94.2 

93_6 

91_4 

89 0 

87_2 

84 1 

81.1 

79.2 

778 

76 9 

77_8 

79.0 

80.1 

82.1 

83.9 

84.8 

86.0 

86.2 

86.6 

86.9 

86.5 

86 8 

87.0 

86 3 

86.4 

87.4 

874 

21.0 

21 0 

21.0 

21 1 

21.0 

21 0 

21_1 

21.1 

21 1 

21.2 

21.1 

21.1 

21.2 

21.2 

21.1 

21_3 

21 3 

21 1 

21_0 

21_1 

21.0 

21_0 

20.9 

20.8 

20 9 

20.8 

20.9 

20 8 

20.6 

20.4 

20.2 

20.2 

20.2 

20.3 

20.7 

20.8 

20 6 

20.6 

20 4 

20.3 

20.4 

20.4 

20.7 

20.7 

20.6 

20.6 

20.5 

20.5 

20_7 

20 9 

21_0 

21.3 

21 5 

21.2 

21.1 

21.2 

21 1 

20.8 

20.8 

20.8 

20.6 

20.4 

20.4 

20.3 

20.4 

20.5 

20.6 

20.7 

20.6 

20 6 

20.7 

20 6 

20.5 

20 4 

2.3 

23 

24 

24 

2.3 

2.3 

23 

2.3 

24 

2.3 

2.2 

2.3 

2.2 

2.2 

2.3 

2.3 

23 

23 

2.3 

22 

2.1 

21 

2.3 

2 4 

23 

2.2 

2.2 

2.2 

2.2 

2.2 

2.2 

21 

2.2 

2.2 

2.3 

23 

23 

2.3 

2.2 

2.2 

2.2 

22 

2.2 

21 

2.1 

2.1 

2.3 

2.2 

2.2 

22 

23 

2.3 

24 

23 

2.3 

2.1 

21 

2 1 

22 

22 

22 

2.2 

2.1 

2.1 

22 

22 

21 

2.0 

2.1 

2 1 

2.0 

20 

20 

2.0 

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Port Change 

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Resume Sampling 

3.9 

3 8 

3.8 

3.9 

4.2 

40 

44 

4.2 

4.0 

3.9 

3.9 

4.0 

4.2 

44 

4.5 

43 

44 

42 

4.2 

41 

4.2 

4.3 

4.2 

4.2 

42 

4.2 

4.1 

4.1 

4.1 

4.2 

4.3 

4.5 

43 

4.2 

4.1 

44 

4.5 

4.3 

4.2 

4.3 

4.2 

4.2 

4 1 

3.2 

1.3 

1.3 

1 3 

1.3 

14 

1.4 

1.2 

12 

1 2 

11 

12 

1.3 

14 

1.2 

1.2 

1.1 

1.2 

1.2 

1.3 

27 

4 5 

4 4 

4.3 

4.5 

4 7 

4 7 

4 5 

44 

87.2 

87.2 

87.7 

88.3 

88_7 

89.9 

91.6 

92.3 

93.7 

94_1 

94 0 

93.5 

93.6 

94.1 

93.5 

93.2 

92.5 

92.3 

92.2 

92 3 

93_6 

93 8 

93.8 

94.7 

94.9 

94.6 

94 4 

94.2 

94.3 

95.0 

95_1 

95.3 

94.7 

93.9 

94 7 

95_1 

94 6 

95 0 

95.1 

94.6 

94 6 

95 8 

96_1 

96 2 

95.6 

78 7 

47_1 

28 9 

17.2 

11 8 

8.6 

70 

6.1 

5.7 

5.5 

5.3 

5.7 

5.7 

54 

56 

56 

58 

5.6 

5.0 

6.1 

25.5 

61 1 

78.3 

86 7 

91 9 

94 0 

94_5 

20.4 

20 3 

20.4 

20.6 

20.7 

20.7 

20.6 

20_5 

20 2 

20.1 

20.2 

20.4 

20.2 

20.2 

20 4 

20.2 

20.0 

201 

20_2 

20 1 

19 9 

19_9 

19 9 

19_8 

19.9 

20.0 

20.0 

20 1 

20.0 

20_0 

19.9 

19.7 

19.9 

20.0 

20.0 

20.1 

20.1 

20.1 

20.1 

20_1 

20.3 

20.3 

20 3 

20 4 

20.4 

18.7 

12.1 

7.7 

5.0 

3.7 

2.9 

2.5 

2.2 

20 

1 9 

1.8 

17 

1.7 

1.6 

1.6 

1.6 

1.5 

1.5 

1.5 

1.5 

29 

8 9 

13 5 

15.8 

17.4 

18_3 

18 8 

2.0 

2.0 

2.0 

2.1 

21 

2.0 

1.9 

20 

2.0 

1 9 

2.1 

2.1 

2.0 

2.0 

2.1 

2.0 

2.0 

2.0 

20 

1.9 

1 9 

1.9 

2.0 

2.1 

2.0 

1.9 

1.9 

1.9 

1.9 

1.9 

2.0 

2.0 

2 1 

2.0 

2.0 

2.0 

19 

1.9 

1.9 

2.1 

2.1 

20 

2.0 

1 9 

2.0 

1.9 

1 9 

1 8 

1.8 

1.7 

1.6 

1.5 

14 

1.5 

1.5 

1.5 

1.5 

1.5 

1.5 

1.5 

1.5 

1.5 

14 

14 

1.5 

1.5 

1.6 

1.7 

17 

1 g 

1 g 

1 8 

8123/05 Run #2 

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08/23/0512:31:52 

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08/23/0512:32'12 

4.5 

4.4 

4.4 

4.3 

4.3 

4.3 

43 

4.3 

4.4 

4.2 

4.2 

42 

4.1 

4 2 

4 3 

4.4 

4.2 

4.0 

41 

3.9 

4.0 

4.1 

4.1 

4.1 

4.1 

4.1 

3.9 

3.8 

36 

3.6 

3.6 

3.6 

36 

39 

39 

3.8 

39 

39 

3.9 

4.0 

40 

4.2 

4.1 

4.1 

4.1 

4.3 

4.2 

4 5 

4.6 

3.9 

3.9 

3.8 

3.8 

38 

3 7 

36 

40 

3.8 

3.9 

3.8 

3.8 

3.9 

3.9 

40 

41 

4.1 

4.0 

41 

4.0 

4.0 

4.1 

4.2 

43 

4.3 

95.2 

94 9 

94.6 

94.4 

93 4 

93.9 

96.0 

96.3 

95.8 

95 4 

94 9 

94.9 

95.3 

95.2 

95.0 

94.8 

94.7 

97.9 

99.5 

98.1 

96.4 

95.5 

94.2 

92.2 

91.4 

90.3 

89.8 

90.3 

89.7 

89.9 

90.0 

89.2 

88.6 

88.6 

88.0 

877 

874 

86.9 

87.3 

87.5 

87.6 

88.3 

89.0 

89.6 

90.5 

91.7 

92.0 

92.7 

93.3 

94.0 

94.6 

94.7 

94.1 

93.9 

93.7 

92 5 

91.5 

90 5 

89 7 

89 3 

89.3 

89.5 

90.2 

91.8 

91 6 

91 7 

92.2 

92.1 

91.8 

92 2 

92.8 

93.3 

93.6 

94.0 

19.0 

19 1 

19.1 

19.2 

19.3 

19.3 

19.2 

19.2 

19.4 

19.4 

19.2 

19.2 

19.3 

19.1 

19.1 

19.3 

19.2 

19.2 

19.2 

19.3 

19.3 

19.5 

19.5 

19.5 

19.8 

19 8 

19.8 

20.1 

20.1 

19.9 

20.0 

20.3 

20.5 

20 4 

20.4 

20.4 

20.5 

20.4 

20.4 

20.5 

20.6 

20.5 

20.5 

20.4 

20.0 

19 8 

19.9 

19.7 

19.7 

19 7 

19.6 

19.9 

19.9 

19.9 

20 1 

20.1 

20.0 

20.0 

20.1 

20 1 

20 1 

20 2 

20.1 

19.8 

19.8 

19.6 

19 4 

19.5 

19.7 

19.9 

19 9 

20.1 

20.2 

20.1 

1.8 

"1.8 

1 8 

1.8 

1.8 

1.7 

1.7 

1.8 

1 7 

1.7 

1.7 

1.7 

1 7 

1.7 

1.7 

1.7 

1.7 

1.7 

1.8 

1.8 

1.7 

1.7 

1.8 

1.8 

1.8 

1 8 

1 8 

1.7 

1.7 

1.7 

1.7 

1.6 

1.6 

1.6 

1.5 

1.6 

1.6 

1.7 

1.7 

1.6 

1.7 

1.7 

1.6 

1 6 

1 5 

1.6 

1.7 

1.7 

1 6 

1.6 

1.6 

1 5 

1 5 

1.5 

1.6 

1.7 

1.7 

1.7 

1.7 

1.7 

1.6 

1 5 

1.6 

1.5 

1 6 

1.6 

1.6 

1.5 

1.6 

1.6 

1.6 

1.5 

1.5 

1.5 

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08123105 12:42:02 

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08/23/05 12:42 42 

08/23/05 12:42:52 

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08123105 12.44 22 

08/23/05 12:44:32 

4.2 

4.1 

4.2 

4.1 

4.1 

4.1 

4.4 

4.1 

3.9 

4.0 

39 

3.8 

36 

3.6 

3.6 

3.7 

3.6 

3.7 

4.1 

4.0 

4.2 

4.2 

4.2 

4.0 

4.1 

4.1 

4.1 

42 

4.2 

4.0 

40 

4.0 

4.3 

4.3 

42 

4 1 

4.7 

4.3 

4.1 

4.1 

4.1 

42 

4 3 

3.9 

40 

4.0 

4.0 

45 

46 

4.6 

4.4 

4.3 

4.3 

4.2 

4.5 

4.3 

4.5 

4.4 

43 

4.1 

42 

4.1 

4.0 

4.0 

4.0 

4.0 

4.0 

40 

39 

4.1 

4.3 

4.1 

4.1 

4.1 

94 7 

95_3 

95.8 

96.2 

96.9 

97.2 

96.7 

96.0 

96 1 

95_8 

95.8 

95.9 

95.6 

95.3 

94.8 

93.3 

91_2 

89 4 

88.0 

87.3 

87.3 

86.8 

86 7 

87_3 

87.7 

88.0 

88.2 

88.3 

88.4 

88 8 

88.8 

89.2 

90.0 

89.9 

90_4 

91.0 

90 6 

90.9 

91_6 

91 7 

91.9 

92.5 

92.4 

92.7 

92.9 

92.6 

92.0 

91.1 

90 0 

89_1 

88 2 

87_9 

88.4 

89.0 

89 6 

91 1 

92.6 

93.6 

95 4 

96.0 

95.0 

94.9 

94 9 

94_4 

94 4 

94_1 

92 6 

91.5 

91.6 

91 '1 

90.9 

91 5 

91.4 

91.3 

20.1 

20.1 

20.1 

20.0 

20.0 

20.0 

20.2 

20.2 

20.0 

20.1 

20_1 

20.2 

20.2 

20.1 

20.0 

20.1 

20.0 

20.0 

20.1 

20.1 

20 0 

20.2 

20 4 

20.1 

19.9 

19 9 

19.9 

19.8 

19.8 

19.9 

19.8 

20.0 

20.2 

20_1 

20.1 

20.0 

20_0 

20.0 

20.1 

20.3 

20.6 

20.3 

201 

20 0 

20 0 

20_1 

20.1 

20 2 

20 2 

20.1 

20.0 

19.9 

19.9 

19.7 

19.7 

19.8 

19.8 

19.7 

19.9 

20.2 

20_2 

20.2 

20.2 

20.3 

20.3 

20.3 

20.2 

20.2 

201 

20 0 

20 1 

20 1 

201 

20 2 

1.6 

1 6 

1.6 

1.6 

1.5 

1.5 

1.5 

1.5 

1.5 

1.6 

1 7 

1.6 

1.6 

1.5 

1.5 

1.5 

1 5 

1.5 

1 5 

1.4 

1 4 

1.5 

1.6 

1 5 

1.5 

1.6 

1.6 

1.6 

1.5 

1.4 

14 

1.5 

1.4 

1.4 

1.4 

1.5 

1.5 

1.5 

1.5 

1 5 

1.5 

1.5 

1.3 

1.4 

1.5 

1.5 

1 4 

1.4 

1.3 

1.4 

1.4 

1.5 

1.5 

1.5 

1.5 

1.3 

1.3 

1.4 

1.5 

1 4 

1.4 

1.4 

1 5 

1 4 

1.2 

1 3 

i_3 

1 3 

1.3 

1.3 

1.2 

1.2 

1.3 

1.2 

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Stop Run #2 

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08/23/05 12:55' 32 

08/23/05 12:55:42 

08/23/05 12:55:52 

08/23/0512.56:02 

08/23/05 12.56:12 

08/23/05 12:56'22 

43 

41 

41 

4.0 

4.0 

4.3 

42 

4.3 

4 7 

44 

4.3 

43 

44 

4.6 

4.3 

4.6 

4.3 

4.3 

42 

41 

42 

4.3 

43 

46 

4.3 

44 

4.3 

41 

4 1 

4.2 

4 1 

43 

4 00 

3.2 

1.6 

14 

14 

1.3 

1.3 

1.3 

1.3 

1.3 

1.2 

1.3 

1.2 

1 3 

1.3 

13 

1.2 

12 

1 2 

1 2 

1 2 

1.2 

1 2 

12 

1.2 

1.2 

12 

1 2 

1 2 

1.2 

1 2 

12 

12 

1.2 

1.2 

12 

1 2 

12 

1.2 

11 

92.1 

92.1 

91_5 

92.1 

92.2 

92.1 

92.4 

92_6 

92 5 

92_9 

93_5 

93.3 

93.5 

94.9 

95 6 

95.5 

95.7 

95.1 

94.5 

95.2 

95.2 

95.2 

96.4 

97.1 

95.7 

94.3 

93 0 

92.2 

92.1 

91_6 

91.9 

93 6 

91.74 

92 5 

89 0 

79.3 

56.0 

38.3 

26.7 

19.3 

15.4 

124 

10.9 

9.8 

8.7 

8.2 

76 

6.7 

65 

64 

6.1 

6.1 

6.3 

6.1 

5.9 

5.8 

5.7 

5.6 

52 

5.2 

5.2 

54 

51 

5.1 

55 

5.8 

5.6 

5.7 

59 

5.8 

5.5 

5.5 

20.4 

20.4 

20.3 

20.3 

20.3 

20.4 

20.2 

20.0 

20.0 

20.1 

20.2 

20 2 

20.2 

20.2 

20.2 

20 1 

20 1 

20.1 

20.0 

19.8 

20.0 

20.2 

20.1 

19.9 

19.7 

19.6 

19.8 

19.9 

20.0 

20.3 

20.4 

201 

20.29 

20.0 

19.1 

18.2 

13.8 

10.5 

6.1 

64 

52 

44 

38 

34 

32 

3.0 

27 

26 

2.4 

23 

2.2 

22 

2 1 

2.0 

1 9 

1 9 

1 8 

1.8 

1 8 

1 8 

1 9 

1 9 

20 

2 1 

2.3 

2 3 

2.0 

1 8 

1.6 

1 6 

1.5 

1 5 

1.1 

11 

1.2 

1 3 

1.3 

1.4 

1 4 

1 4 

1.3 

1 2 

1.3 

1.4 

1.3 

1.2 

1.2 

1.3 

1.3 

1 3 

1 4 

1.3 

1.3 

1.4 

1.3 

1.3 

1.4 

1.3 

1.2 

11 

1.1 

1.2 

1 2 

1.2 

1.86 

1.2 

11 

11 

11 

11 

1.2 

1.1 

1.1 

1 0 

0.9 

0.8 

0.9 

0.9 

1.0 

1.1 

1.2 

1.0 

09 

0.8 

0.9 

0.9 

0 9 

08 

0.8 

0 8 

0.9 

0.8 

08 

0.8 

0.8 

0.8 

0.8 

0 9 

09 

0.8 

08 

0.8 

0.8 

0 8 

8/23/05 Run #2 

41 

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08123105 12:59.22 

08/23/05 12:59:32 

08123!05 12:59:42 

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08123105 13:02:22 

08/23/0513:02:32 

08123105 13:02:42 

08123105 13.02:52 

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08123!05 13:04:32 

08123105 13.04:42 

08123105 13'04:52 

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08123105 13.05:52 

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08/23/05 13:07"22 

08/23/0513:07:32 

08123105 13.07:42 

08123105 13:07:52 

08/23/05 13:08:02 

08'23/0513:08:12 

08123105 13:08:22 

08123105 13-08:32 

1 2 

1.2 

12 

1_2 

1.2 

1.2 

1.2 

1.2 

1.2 

1.2 

1.2 

1 2 

1.2 

1.1 

1.2 

1.2 

1.2 

1.2 

1 2 

1.2 

12 

1.2 

1.2 

1.2 

1.1 

1.0 

03 

0.2 

0.2 

0.2 

0.2 

0.2 

0.2 

0.2 

0.3 

0.2 

02 

0.3 

03 

0.2 

0.2 

0.2 

02 

0 3 

02 

0.2 

0.4 

06 

02 

0.2 

0.2 

0.2 

0.2 

0.2 

0.2 

0.2 

0.2 

0.2 

0.2 

0.1 

0.2 

0.2 

0.2 

0.2 

0.2 

0.1 

0.1 

0.1 

0.1 

02 

0 7 

11 

11 

59 

58 

5.8 

6 1 

6.2 

6.0 

6.0 

6.0 

6.1 

5.6 

56 

5.3 

5.2 

5.1 

5.3 

5.7 

5.6 

5.3 

5.7 

5.9 

5.8 

5.6 

56 

5.4 

5.4 

5.7 

55 

5.2 

5.1 

5.0 

4.6 

4.3 

4.2 

4.4 

45 

42 

4.6 

46 

4.4 

4.3 

45 

4.8 

4.8 

4.6 

4.9 

4.9 

4.8 

4.2 

4.6 

8 8 

32 5 

58.2 

75.8 

86.1 

90.8 

94.0 

96.0 

97.3 

97.9 

98.2 

98 7 

99_4 

99_6 

100.0 

100.5 

100.6 

100.7 

100.6 

100.5 

100 4 

W0.2 

99.9 

94.3 

1 5 

1.5 

15 

1.5 

1.4 

1.4 

1.3 

1 3 

1.3 

1.2 

1.1 

11 

1.1 

11 

11 

1.1 

1.0 

1.1 

1 0 

1.0 

1.0 

1.0 

1.0 

0.9 

0.9 

0.9 

09 

1.1 

4.8 

11.5 

16.3 

19.4 

21 4 

22.5 

23_1 

23.6 

23.8 

24.0 

24.1 

24.2 

24.3 

24.3 

24.4 

24.4 

24.4 

24.4 

24_1 

24_0 

23.8 

20.5 

13 0 

8 0 

4 8 

3.0 

2.0 

1.6 

1.3 

1.1 

1 0 

09 

0.8 

0 7 

0 7 

07 

0.6 

0.6 

0.6 

0.6 

0.5 

05 

0.5 

0.5 

05 

0_7 

0.6 

0 7 

0.8 

0.9 

0.8 

0.8 

0.8 

0.8 

0.7 

08 

0.8 

0.8 

0.7 

0.7 

0.8 

0.8 

0.8 

0.7 

0.7 

0 7 

0.6 

0.7 

0.7 

0 7 

0.7 

0.7 

0.6 

06 

0.7 

0.7 

0.7 

0.7 

0.7 

0.7 

0.7 

06 

0.6 

0.7 

0 7 

06 

0.7 

0.7 

0.6 

0.5 

0.5 

0.5 

0.6 

0.6 

0.7 

0.6 

0.5 

0.5 

0.6 

0.7 

06 

0.5 

0.6 

05 

05 

0.6 

07 

07 

0.7 

0.7 

0.6 

0.5 

0.5 

0.5 

04 

0.4 

04 

8/23/05 Run #2 

25_5 ppm NOx 

Zero CO, S02 

99.1 ppm CO 

Zero VOC, NOx 

Page 7 

42 
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08123105 13:10:12 

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08/23/05 13:10:32 

08/23/0513'10.42 

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08/23/0513:11:02 

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08/23/05 1 3 11 '32 

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08!23/05 13:14.42 

08123/05 13:14:52 

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08123105 13:15'12 

08/23/05 13:15:22 

08/23/0513:15:32 

08/23/0513:15:42 

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08/23/05 13:16.02 

08/23/05 13:16:12 

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08/23105 13" 17:52 

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08/23/05 13:18 32 

08/23/05 13:18:42 

08123105 13:18:52 

08/23/05 13.19:02 

08/23/0513:19'12 

08/23/0513 19.22 

08/23/05 13"19:32 

08/23/05 13:19:42 

08/23/0513:19.52 

1.1 

1.0 

0.3 

0.2 

0.2 

0.2 

0.2 

0 2 

0.2 

0.2 

0.1 

0.1 

0.1 

0 2 

0 1 

01 

0.1 

0.1 

01 

0.2 

0.2 

0.2 

0.1 

0.2 

0.2 

0.2 

02 

0.1 

0.1 

0.2 

0.2 

0.1 

0.2 

0.2 

0.1 

01 

0 1 

0.2 

0.2 

0.2 

0.2 

0.2 

01 

0.1 

0.1 

0.2 

0.1 

0.1 

0.1 

0.1 

0.1 

01 

0 1 

0.1 

0.1 

0.2 

0 1 

0 1 

0 1 

0.1 

0.1 

70 

14_9 

14.9 

14.9 

14.9 

14.9 

14_9 

73.0 

47.3 

29.8 

17.6 

12.2 

8.7 

6.4 

5.4 

51 

4.7 

4.5 

4.6 

4.8 

50 

48 

47 

49 

4 9 

4.8 

4.6 

4.5 

4.5 

4.3 

4.5 

4.3 

4.5 

4.5 

4.8 

4.8 

49 

4.9 

4.9 

4.9 

4.9 

4.7 

4.7 

4.9 

46 

45 

4.1 

4.1 

4.2 

4.3 

4.2 

4 5 

4.6 

4.6 

4.7 

53 

4.2 

4.3 

4.2 

4.6 

4.7 

4.6 

4.4 

3.9 

39 

4.1 

44 

4.7 

4.5 

4.7 

4.9 

4.7 

4 5 

4.5 

44 

05 

0.5 

0.6 

0.6 

0.7 

0.7 

0.8 

0 8 

0.8 

0.8 

0.8 

0.8 

0.8 

0.8 

0.8 

0.8 

0.8 

0.8 

0.8 

0.8 

0.8 

0.8 

0.8 

0.8 

0.8 

0.8 

0.8 

08 

0.7 

0.7 

0.7 

0.7 

0.7 

0.7 

0 7 

0.7 

0.7 

0.7 

0.7 

07 

0.7 

0 7 

0 7 

0.6 

0.7 

0.6 

0.6 

0.6 

0.6 

0.6 

0.6 

0.6 

0.6 

0.6 

06 

0.6 

0.6 

06 

0.6 

0 6 

0.5 

0.5 

05 

0.5 

05 

04 

0.3 

03 

0.4 

0.5 

0.5 

0.4 

0.5 

0 7 

1.3 

2.6 

4.5 

7.1 

9.6 

11.9 

144 

17_1 

19.8 

22.1 

23.9 

25.8 

27.3 

28.8 

30.3 

31.6 

33_0 

34.3 

35.2 

36_2 

37.1 

37_9 

38_5 

39_1 

40.0 

40.6 

41.2 

41.7 

42_1 

42.5 

42.8 

43_1 

43_5 

43.9 

44_1 

44_4 

44.6 

44.9 

45 0 

45.3 

45.3 

45 4 

45.6 

45.9 

46.1 

46.2 

46.3 

46 4 

46 5 

46_6 

46.7 

46.7 

46.9 

47.0 

46.9 

45.7 

45 2 

45.4 

44_8 

43.1 

40 4 

37_3 

8/23/05 Run #2 

50.1 ppm S02 

15 2 ppm C3H8 

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DaterTime VOC CO NOx S02 

mm/dd/yy hh:mm:ss ppm ppm ppm ppm 

08/23/05 13:33:52 4.3 85.3 18.5 3.5 

08/23/05 13.34:02 

08/23/0513'34:12 

08/23/05 13:34:22 

08/23/05 13:34:32 

08123105 13:34:42 

08/23/05 13:34:52 

Start Run #3 

08123105 13:35:02 

08123105 13:35:12 

08123105 13:35:22 

08/23/05 13:35:32 

08/23/05 13:35:42 

08123105 13:35:52 

08123105 13:36:02 

08/23/0513.36.12 

08123105 13:36:22 

08123105 13 36.32 

08123105 13:36:42 

08/23/0513:36:52 

08123105 13:37.02 

08123105 13:37:12 

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08/23/0513.37:32 

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08123105 13:39:52 

08/23/05 13".40:02 

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08123105 13:40:42 

08123105 13:40:52 

08123105 13"41 :02 

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08123105 13:41 :32 

08/23/0513:41 42 

08123105 13:41.52 

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08123105 13"42:32 

08123105 13:42:42 

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08123105 13:43:12 

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08123105 13:43:42 

08/23/0513:43"52 

08/23/05 13.44:02 

08123!05 13:44:12 

08123105 13:44:22 

08/23/05 13:44:32 

08/23/0513:44:42 

08/23/0513:44:52 

08123105 13.45"02 

08/23105 ; 3:45.12 

08/23/05 13:45:22 

4.4 

4.3 

4.2 

4.3 

4.1 

4.0 

39 

40 

3.9 

3.9 

3.9 

3.7 

3.7 

3.7 

36 

3.6 

3.6 

36 

3 7 

3.8 

3.8 

3.8 

4.1 

3.8 

3.8 

37 

3.9 

42 

4.2 

4.5 

4.4 

4.5 

4.7 

48 

4.6 

4.5 

4.5 

4.6 

45 

4.6 

4.4 

4.3 

4.3 

4.3 

4.3 

4.3 

4.2 

4.2 

4.3 

4.3 

4.2 

4.4 

4.5 

4.4 

4.2 

4.2 

4 2 

4.3 

4.3 

4.3 

4.4 

4.4 

44 

44 

44 

42 

4.2 

4.3 

4.7 

85.9 

86.5 

87.7 

88.1 

88.4 

88 4 

88.8 

88.9 

89.0 

90.2 

90.7 

91.7 

93.6 

94.9 

95.1 

95.2 

94.5 

92.8 

91.7 

90.6 

89.3 

88.6 

88.0 

87.8 

86.7 

84 9 

83.7 

81.0 

78.5 

77.4 

75 7 

74.9 

75.7 

77.2 

79.0 

81.4 

84 3 

86 7 

87.8 

89 4 

91.0 

91.0 

91 3 

91.9 

92 0 

92.3 

93.1 

93.3 

92.9 

93.1 

93.8 

93.8 

94.2 

95.6 

95.9 

95.2 

95.2 

94.4 

94.1 

94 7 

95.7 

96.5 

97.3 

98.3 

98.1 

98 1 

98.6 

98.2 

98.2 

18.5 

18.3 

18.5 

18.7 

18.9 

19.0 

18 8 

18.8 

19.1 

19.0 

18.9 

18.9 

18.8 

18 8 

19.0 

19.1 

19.2 

19 3 

19.2 

19.2 

19.2 

18.9 

18.8 

18.9 

18.9 

19.1 

19.3 

19.4 

19.4 

19.4 

19.4 

19.3 

19.2 

19.3 

19.4 

19.3 

19.3 

19.4 

19.2 

19.2 

19 3 

19.1 

19.2 

19 4 

19 4 

19.4 

19.4 

19 4 

19.3 

19.4 

19.6 

19.9 

19.8 

19.7 

19.5 

19.5 

19 4 

19 7 

19.7 

19 5 

19 5 

19.4 

19.3 

19.2 

19.3 

19.3 

19.3 

19.3 

19.2 

34 

3.3 

3.2 

3.2 

3.1 

3.1 

30 

29 

2.8 

2.7 

2.7 

2.6 

2.5 

2.5 

24 

23 

2.3 

2.4 

23 

2.1 

2.0 

2.0 

21 

2.0 

2.0 

2.0 

1.9 

1 9 

1.8 

1.8 

1.6 

1.6 

1.7 

1 7 

1.7 

1.7 

1.7 

1.7 

1.7 

1.7 

1 6 

1.6 

1.5 

1.5 

1 4 

1.4 

1 4 

1 4 

1 4 

1 4 

1 5 

1 5 

1.4 

1.4 

1 4 

1.4 

1.3 

1 3 

1.3 

1.3 

1 3 

1.4 

1.4 

1.4 

1.4 

1.3 

1.2 

i.3 

1 3 

8/23105 Run #3 

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08123105 13:45:32 

08/23/05 13.45:42 

08123105 13:45.52 

08123105 13:46:02 

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08123105 13:57'42 

4.3 

4.1 

4.0 

4 1 

4.0 

4.1 

4 1 

41 

4.3 

42 

42 

4.3 

44 

44 

4.5 

4.5 

43 

4.3 

43 

4.3 

4.3 

4.3 

44 

44 

44 

4 7 

47 

4.7 

48 

5.0 

5.0 

50 

4.8 

5.0 

52 

5.0 

5.1 

5.0 

52 

5.0 

52 

5.1 

5.1 

4.9 

4.9 

4.8 

46 

4.6 

47 

4.9 

50 

5.1 

4.8 

4.8 

5.2 

4 7 

4 8 

48 

4 7 

4.8 

48 

4 7 

4.6 

47 

4 7 

46 

4.6 

45 

4.4 

44 

4.6 

4.5 

4.5 

4.5 

96 7 

94_3 

91.8 

89.9 

89.4 

89.3 

88.4 

88_7 

89.0 

88_3 

88.3 

88.2 

87.6 

87.8 

88.5 

89.3 

91.5 

93.3 

94.4 

95.7 

96.9 

96.9 

96_3 

94.9 

93.9 

93.7 

93.9 

94.1 

94.9 

96.8 

97.9 

99 0 

100_0 

101.9 

1021 

101_9 

101.8 

102.9 

103.8 

107.1 

112.9 

109.9 

106.7 

104.2 

100.9 

97.9 

96.3 

95 9 

94.5 

95.8 

98_6 

98.0 

97_4 

98 5 

100_0 

103_0 

107_6 

105.8 

103.0 

101_3 

101.6 

102.5 

104.6 

105.4 

105.4 

106.7 

111.4 

112.2 

110 2 

108_0 

105 2 

103.4 

102.5 

100.7 

19.2 

19 2 

19_1 

19.1 

19.2 

19.2 

19_3 

19 3 

19.3 

19.4 

19.4 

19 6 

19_8 

19.9 

1!:1.!:1 

20_1 

20.1 

19.9 

20_1 

20.1 

19.9 

20_1 

19 8 

19 5 

19.6 

19.4 

19.4 

19_6 

19_5 

19.3 

19.3 

19.4 

19_3 

19.2 

19.2 

19.2 

19_2 

19.2 

19.2 

19.2 

19.0 

19.3 

19.4 

19_3 

19.6 

19.8 

19.6 

19 6 

19.7 

19.5 

19.3 

19.6 

19.6 

19 4 

19.6 

19.6 

19.5 

19.6 

19 7 

19 5 

19_3 

19.4 

19.3 

19.3 

19.4 

19.3 

19_2 

19 2 

19.2 

19.2 

19.2 

19.4 

18.5 

19_5 

1.2 

1.2 

1.2 

'1.2 

12 

1.2 

1 2 

12 

11 

1.2 

1.3 

1 2 

11 

12 

1 2 

12 

11 

11 

11 

12 

12 

1 2 

1.3 

12 

11 

11 

1.0 

1.0 

11 

12 

11 

11 

11 

11 

1.2 

11 

1.0 

11 

11 

11 

11 

1 0 

1 0 

'1.0 

1.0 

1.0 

11 

1.1 

1 0 

0.9 

08 

1.0 

0.9 

1.0 

1.0 

11 

09 

0 9 

09 

0.9 

09 

1.0 

0 9 

08 

0.8 

08 

0.8 

08 

08 

08 

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08123105 13:58:02 

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Port Change 

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4.5 

4.5 

4.4 

4.3 

4.2 

42 

4.2 

4.3 

4.3 

46 

4.6 

4.4 

45 

4.2 

40 

4.0 

39 

40 

40 

4.0 

4.1 

4.1 

4.2 

4.2 

43 

4.5 

4.7 

4.4 

4.3 

45 

43 

43 

4.3 

4.4 

4.4 

45 

46 

4.5 

4.7 

50 

46 

46 

4.2 

1.5 

1.4 

14 

1.4 

1.4 

1.4 

1.4 

1.4 

i.4 

14 

1.4 

13 

1.3 

1.4 

14 

1.4 

1.5 

14 

4.4 

45 

4.5 

4.5 

4.7 

4 9 

4.8 

4.7 

4.8 

51 

50 

48 

99 0 

99.7 

98.7 

96 2 

95_7 

95 6 

95.5 

96.5 

98.0 

98.0 

97_6 

97.6 

97.9 

97.4 

97.0 

95.8 

94.4 

92.1 

89.8 

87_6 

86.1 

85_4 

84.6 

84.7 

85_7 

86_8 

87.5 

88.1 

88 6 

89.2 

89 9 

91 2 

92.0 

92_0 

92 4 

93 6 

94 1 

94.2 

95.2 

95.6 

95.7 

96.8 

97.3 

96_9 

84_8 

52.8 

31_2 

18.7 

12 2 

8 5 

6.4 

5.7 

56 

5.3 

5.2 

54 

56 

5.4 

5.2 

5.3 

54 

5.4 

121 

45_9 

71.8 

84_0 

88.6 

91.3 

93.3 

94_1 

94.2 

94 8 

95.8 

19 6 

19.8 

19.6 

19.7 

19.9 

20.0 

20.0 

20.1 

20.1 

20.0 

20.2 

20.3 

19.9 

19.8 

19.9 

19.8 

19.9 

19.9 

20.0 

19.8 

19.6 

19 7 

19.6 

19.4 

19.5 

19.5 

19.6 

19.7 

19.9 

19.8 

19 7 

19.7 

19.8 

19.5 

19.3 

19.3 

19.3 

19.6 

19.6 

19 8 

20.1 

20.0 

20.0 

20.0 

18.8 

12.8 

78 

5.1 

35 

2.8 

2.3 

20 

1.9 

18 

1 7 

1.6 

1.6 

1.6 

1 5 

15 

1 5 

1.5 

1.6 

5.8 

111 

14.3 

16.1 

17.1 

17.8 

182 

18.5 

18.6 

18.8 

08 

0 8 

08 

0 8 

0 8 

07 

0.7 

0.8 

08 

0.8 

0.8 

0.8 

0.8 

0.8 

0.8 

0 7 

09 

0.8 

08 

0.8 

0.7 

0.8 

06 

0 7 

0.8 

0.6 

0.6 

06 

0.6 

0.7 

0 7 

0.7 

07 

0.7 

0.6 

06 

0.7 

0.7 

0.6 

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06 

0.7 

0.7 

0.5 

0.6 

0.6 

0.5 

05 

0 5 

0.5 

0.4 

0.3 

03 

0.4 

0.5 

0.5 

04 

0.4 

04 

0.3 

0.3 

03 

04 

0.4 

0.4 

0.4 

0.4 

05 

0.5 

0.5 

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0.4 

8/23105 Run #3 

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Resume Sampling 

08/23/0514 10:02 

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08/23/0514'2~:52 

08123105 14.22:02 

4.7 

4.6 

4.6 

4.5 

4.6 

4.6 

4.6 

4.6 

4 7 

4.8 

4.6 

5.0 

5.0 

5.1 

5.0 

4.8 

4.7 

4 7 

4.6 

4.6 

4.9 

4.7 

4.7 

4.9 

5.1 

5.1 

5.0 

4.8 

5.0 

5.1 

5.3 

4.9 

4.7 

4.8 

4 7 

46 

4.7 

48 

5.0 

5.1 

5.0 

5.2 

5.2 

5.4 

5.2 

4.8 

4.6 

4.6 

4.6 

4.7 

4 7 

4.6 

4.7 

4.7 

4 7 

4.6 

4.6 

4.5 

4.5 

4.7 

4.8 

4.6 

4.7 

4.7 

46 

4 7 

46 

4.5 

4.5 

4.5 

4.5 

4.6 

4.6 

96 3 

95.9 

95.3 

94.9 

94.9 

95.3 

97 6 

99.9 

99.6 

99.1 

96.5 

98.5 

99 0 

99.6 

100.3 

101 1 

100.6 

100.2 

99.2 

98.9 

99.4 

99.0 

99.2 

100.5 

100 7 

101.0 

102.5 

101.7 

100.1 

99.6 

99.3 

99 8 

106.2 

107.1 

103.9 

101.3 

101.1 

100 5 

100 0 

100.9 

101.4 

100.4 

101.9 

103.1 

101.3 

100.8 

103.5 

104.2 

102.4 

101.9 

101.4 

103.2 

103.6 

104.1 

105.1 

104.7 

104.8 

105.4 

105.6 

104.9 

104.3 

105.0 

104 5 

103.9 

104 9 

105 4 

104.3 

103.2 

102.9 

102 2 

102.1 

102 4 

103.6 

18.6 

18.5 

18.6 

16.9 

18.9 

19.1 

19.4 

19.2 

19.0 

19.1 

19.1 

18 9 

19.2 

19 4 

19 2 

19.1 

19.2 

19.0 

16.9 

18.8 

18.9 

19.3 

19.3 

19.2 

19.2 

19.2 

19.0 

19.0 

19.2 

19.1 

19.0 

19.1 

16.9 

19.0 

19 1 

19.1 

19.2 

19 2 

19.3 

19.3 

19 4 

19.4 

19.4 

19.3 

19.5 

19 5 

19.2 

19.2 

19.2 

19.2 

19.2 

18.9 

16.6 

18.8 

18.6 

18.7 

18.8 

16.8 

18.6 

16.8 

19.0 

18 8 

18 7 

18 9 

18.8 

18 6 

18 7 

18.7 

18 6 

18.8 

19 1 

19.2 

19.2 

05 

0.4 

04 

0.6 

0.7 

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0.4 

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0.5 

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06 

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04 

0.5 

04 

05 

05 

04 

03 

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0.3 

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08123!05 14:29:02 

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08123105 14·30:52 

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08/23/05 14'34.02 

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4.5 

4 7 

4.6 

4.6 

4.6 

4.6 

4.7 

50 

48 

4.7 

45 

4.6 

4.5 

4.3 

4.1 

4.1 

4.0 

4.0 

3.9 

4.0 

4.1 

42 

43 

4 1 

4.2 

4.1 

41 

4.3 

4.5 

4.4 

4.6 

4.5 

51 

4.8 

4.8 

4.7 

4.5 

4.4 

4.5 

4.4 

44 

4.4 

45 

4.5 

4.5 

4.5 

4.5 

4.5 

4.5 

4.5 

4.4 

4.3 

44 

4.3 

43 

43 

43 

4.3 

4.3 

4.4 

4.3 

4.3 

4.2 

4.1 

3.9 

4.0 

39 

39 

4.0 

4.1 

42 

4.2 

4 3 " 

103.4 

103.3 

102 2 

100.6 

98 4 

96.2 

95.5 

95.5 

95.0 

95.6 

98.7 

100.0 

99.4 

100.5 

102.4 

102.2 

101.3 

99.8 

97.3 

95.5 

93 7 

91.9 

90.6 

89.8 

89.2 

88.9 

88.6 

88.9 

88.8 

89.1 

90.4 

90.4 

90.9 

91.9 

92.8 

93.1 

93.6 

94.4 

94.8 

95 0 

95.5 

95.5 

95.2 

95.8 

95.9 

95.4 

95.1 

95.7 

95.5 

95.8 

96.5 

97.4 

97.6 

97.5 

97.8 

97.3 

96.9 

96.5 

95.9 

94.9 

94.5 

94.4 

93.9 

93.8 

94 3 

94.0 

93.1 

91.7 

90.2 

88.5 

87.2 

86.5 

86.2 

86.6 

19.1 

19.1 

19.0 

19.1 

19.0 

19.1 

19.1 

19 1 

19.3 

19.4 

19.2 

19.2 

19.3 

19.1 

18.9 

18.8 

18.8 

18.9 

19.1 

19.2 

19.3 

19.3 

19.2 

19.2 

19.2 

19.1 

19.1 

191 

19.4 

19.2 

19.2 

19.3 

19.3 

19.4 

19.3 

19.3 

19.3 

19.4 

19.5 

19.7 

19.9 

19 8 

19.7 

19.7 

19.7 

19.5 

19 2 

19.2 

19.0 

18.9 

19 1 

19 3 

19 1 

19.1 

19.1 

19.1 

19.1 

19.0 

19.0 

19.2 

19.4 

19.4 

19.5 

19.4 

19.4 

19.3 

19.3 

19.3 

19.4 

19.6 

19.7 

19 8 

18 7 

19 6 

0.4 

0.4 

04 

0.5 

0.4 

0.3 

0.4 

0.5 

0.4 

04 

0.4 

0.4 

0.3 

03 

03 

0.4 

0.3 

0.2 

0.3 

0.4 

0.4 

0.4 

0.4 

0.4 

0.4 

0.4 

0.4 

0.3 

02 

02 

0.3 

0.5 

0.5 

0.5 

0.5 

0.3 

0.4 

04 

0.5 

0.5 

0.4 

0.4 

0.4 

0.4 

0.4 

0.3 

0.3 

04 

0.3 

04 

0.4 

0.4 

0.5 

04 

0.3 

0.4 

04 

0.4 

0.4 

0.4 

0.4 

0.5 

0.4 

0.3 

03 

0.3 

0.3 

0.4 

0.5 

0.5 

04 

04 

0.3 

02 

8/23/05 Run #3 

Page 5 48 
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08123105 14:34:32 

08123105 14:34:42 

08123/05 14.3452 

08/23/05 14:35:02 

08123/0514:35.12 

08123105 14:35:22 

08123105 14:35'32 

08123105 14:35:42 

08/23/05 14:35:52 

08123105 14:36:02 

08123105 14:36:12 

08/23/05 14:36:22 

08123105 14:36 32 

08123105 14:36:42 

08/23/05 14:36:52 

08123105 14:37-02 

08123105 14.37:12 

08/23/05 14:37:22 

08123105 14:37:32 

08123105 14'37.42 

08/23/05 14:37:52 

08123105 14:38:02 

08/23/0514:38:12 

08123105 14:38:22 

08123105 14:38:32 

08123105 14'38:42 

08123105 14:38:52 

08/23/05 14:39:02 

08/23/0514:39'12 

08/23/05 14'.39:22 

08123105 14:39:32 

08123105 14:39:42 

08123105 14:39:52 

Stop Run #3 

08123105 14:40:02 

08/23/05 14:40:12 

08/23/05 14:40.22 

08123105 14:40_32 

08/23/05 14:40:42 

08123105 14.40:52 

08/23/0514:41:02 

08/23/0514:41"12 

08/23/0514:41.22 

08123105 14:41:32 

08123105 14:41 :42 

08/23/0514'41:52 

08123105 14'42:02 

08123105 14:42:12 

08123105 14:42.22 

08123105 14:42:32 

08123105 14:42:42 

08123105 14:42:52 

08123105 14:43:02 

08123105 14:43:12 

08123105 14:43:22 

08123105 14:43:32 

08123105 14.43:42 

08123105 14:43:52 

08/23/05 14.44:02 

08123!05 14:44:12 

08123105 14:44:22 

08123105 14:44:32 

08/23/05 14:44:42 

08123105 14.44:52 

08/23/05 14:45:02 

08/23/0514.45:12 

08/23/05 14:45.22 

08/23/05 14:45:32 

08/23105 14 45:42 

08/23/05 14:45:52 

08123105 14'.46:02 

08/23105 14:46:12 

44 

4.4 

4.5 

46 

46 

4.5 

4.7 

4.6 

4.9 

4.7 

45 

4.5 

43 

4.5 

48 

4 3 

4.1 

40 

3.8 

3.5 

34 

3.5 

3.7 

39 

3.8 

3.9 

4.0 

42 

4.3 

4 7 

4.8 

5.0 

4 7 

4.41 

5.3 

49 

31 

17 

14 

1 3 

1.4 

14 

1 4 

1 4 

1 4 

1.4 

1.3 

14 

1.3 

1 3 

1.3 

1.3 

1.3 

1 3 

1.3 

1.3 

1.3 

1.3 

1.3 

1 3 

1 3 

1 3 

1.3 

1.3 

1.3 

1 2 

1.3 

1 3 

1.3 

1.3 

1.3 

1.3 

87.9 

88_5 

88_9 

89_8 

91.3 

92.5 

93.1 

94.1 

95.2 

95.8 

96 1 

96.9 

97 6 

98.1 

98.2 

97 9 

97.4 

96.5 

95.9 

95.4 

94.1 

92.2 

90.4 

88.4 

86.4 

84.0 

82_5 

81.0 

79.2 

78_9 

78.9 

80.1 

82.7 

94.76 

84.5 

86.7 

87.9 

87.8 

75.0 

51.4 

35.0 

23.3 

16.5 

120 

8.9 

7.2 

64 

5.9 

5.3 

52 

4.8 

4.8 

4.6 

4.7 

4.5 

4.3 

4.3 

4.1 

42 

4.5 

4.6 

4.6 

44 

44 

4.3 

44 

4.5 

4.3 

4.3 

42 

38 

36 

19.4 

19.3 

19.2 

19 3 

19.3 

19.3 

19 5 

19.4 

19.3 

19.4 

19.2 

19.1 

19.2 

19.4 

19.3 

19.4 

19.4 

19.4 

19.4 

19.3 

19.2 

19.2 

19.3 

19.3 

19.5 

19.7 

19.6 

19.6 

19.6 

19.5 

19.5 

19.4 

19 3 

19.20 

19.2 

19.2 

19 2 

18.4 

16 9 

12.3 

9.0 

66 

50 

4.0 

3.4 

3 0 

2 7 

2.5 

2.3 

22 

22 

2.1 

1 9 

1 9 

1 8 

1.8 

17 

1 7 

1 7 

1.6 

1.6 

1.6 

1.6 

1.5 

1.5 

1 5 

1 5 

1.5 

1 5 

15 

1.5 

14 

0.2 

0.2 

0.2 

03 

0.3 

0.3 

0.4 

02 

0.2 

0.2 

0.3 

0.3 

0 3 

04 

04 

04 

04 

04 

0.4 

0.3 

04 

0.4 

0.3 

0.3 

0.2 

0.3 

0.3 

0.3 

0 1 

0.1 

0.2 

02 

02 

0_80 

0.3 

0.3 

0.3 

0 3 

04 

0.3 

0.3 

0.1 

0.1 

0 1 

0.1 

0.1 

0 1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0 1 

0.0 

00 

0.0 

0.0 

0.1 

0 1 

0 0 

00 

0.0 

0 1 

0.1 

0.1 

0: 

01 

8/23/05 Run #3 

Page 6 49 
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08/23/05 14:46:22 

08/23/05 14 46 32 

08/23/05 14:46:42 

08/23/05 14 46.52 

08/23/05 14:47•02 

08/23/05 14:47:12 

08/23/05 14:47:22 

08/23/05 14:47:32 

08/23/05 14:47:42 

08/23/05 14:47:52 

08/23/05 14:48:02 

08/23/05 14:48:12 

08/23/05 14:48:22 

08173/05 14:48:32 

08123105 14:48:42 

08123!05 14:48:52 

08123!05 14:49:02 

08/23/05 14:49:12 

08/23/05 14:49:22 

08/23/05 14:49:32 

08123105 14:49:42 

08/23/05 14:49'52 

08/23/05 14:50_02 

08/23/0514:50:12 

08/23/05 14:50:22 

08/23/05 14 50:32 

08/23/05 14:50:42 

08/23/05 14 50:52 

08/23/0514:51:02 

08/23/0514:51:12 

08/23/05 14:51:22 

08/23/0514:51:32 

08/23/05 14:51 :42 

08/23/05 14:51 :52 

08/23/05 14:52:02 

08/23/05 14:52:12 

08/23/05 14:52:22 

08/23/05 14:52 32 

08/23/05 14:52:42 

08/23/05 14:52:52 

08/23/05 14:53 02 

08/23/05 14:53:12 

08/23/05 14:53:22 

08/23/05 14:53:32 

08/23/05 14:53:42 

08123105 14:53:52 

08/23/05 14:54:02 

08/23/0514:54:12 

08/23/05 14:54:22 

08/23/05 14:54:32 

08/23/05 14.54:42 

08/23/0514:54:52 

08/23/05 14:55:02 

08/23/0514:55·12 

08/23/05 14:55:22 

08/23/05 14"55:32 

08/23105 14:55:42 

ORI?::l/05 14·55·57 

08/23/05 14:56'02 

08/23/05 14:56:12 

08/23/05 14:56.22 

08/23/05 14:56.32 

08/23/05 14:56:42 

08/23/05 14:56:52 

08/23/05 14.57:02 

08/23/05 14:57:12 

08/23/05 14:57:22 

08/23/05 14:57:32 

08/23/05 14:57:42 

08/23/05 14.57:52 

08/23/05 14.58:02 

08/23/05 14'58:12 

08/23/05 14:58:22 

1.2 

13 

1 3 

1.3 

1 3 

1.3 

1.2 

1.2 

1 3 

1.3 

1.2 

0.7 

0.5 

04 

0.5 

0.4 

0.5 

0.5 

0.4 

0.4 

0.4 

0.3 

03 

04 

04 

0.4 

0.4 

0.4 

0.4 

0.3 

0.3 

0.4 

0.4 

0.4 

0.4 

04 

0.4 

0.4 

03 

03 

0.3 

0.3 

0.3 

0 3 

0.3 

03 

0.3 

0.3 

0.3 

0.3 

03 

0.3 

0.3 

0.3 

0.3 

1.0 

1.2 

1 ' 

0.8 

0.4 

0.3 

0.3 

0.3 

0.3 

0.3 

0.3 

0.3 

0.3 

0.3 

03 

0.3 

0 3 

0.3 

3.8 

4.0 

3 g 

3.9 

4.1 

4.3 

4.4 

4.7 

4.7 

4.3 

4.3 

44 

4.4 

43 

4.0 

3.8 

3.9 

3.9 

4.0 

3.7 

3.5 

3.5 

3.4 

3.4 

33 

3.0 

3.0 

3.0 

30 

3.1 

3.5 

3.5 

3.6 

3.5 

3.4 

3.6 

51 

25.1 

53.5 

73_3 

84.9 

90_9 

94_6 

96 8 

98_2 

98.9 

99.0 

99.4 

99.8 

100.1 

100.1 

100.3 

100.4 

100.6 

100.6 

1001 

99_8 

91 9 

67.2 

37.2 

18_5 

10_5 

6.6 

4.7 

3.8 

36 

3 5 

3.3 

3.3 

3.2 

2.9 

2.7 

2.8 

1 4 

1 4 

1.3 

1.4 

13 

1.3 

1.3 

1.3 

1.3 

1.3 

1.3 

1.3 

1.2 

28 

9.1 

14.8 

18.5 

20.9 

22.1 

22.9 

23_3 

23.7 

23.9 

23.9 

23_9 

24.0 

24.1 

24.2 

24.3 

24.3 

24.4 

24.3 

24.4 

24.3 

24.1 

24.2 

239 

19.6 

12.5 

76 

4.7 

3.1 

2.1 

1.6 

1.3 

1.1 

0.9 

0.9 

08 

08 

07 

0.7 

0.7 

0.7 

0.7 

0.7 

06 

07 

0.7 

0.7 

0.8 

0.8 

0 9 

09 

0.9 

1.0 

0.9 

1.0 

0.9 

0.9 

09 

0.9 

0.9 

0.0 

0 0 

0.0 

00 

0 0 

0.0 

0.0 

0.1 

0 1 

0 1 

0.1 

01 

0.1 

00 

00 

0.1 

0.1 

0.1 

0.0 

0.0 

00 

0.0 

0.0 

0.0 

0.0 

00 

0.0 

0.0 

0 0 

0.0 

0.0 

0.0 

0.0 

0.0 

-0.1 

00 

00 

0 0 

0.1 

0.1 

0.1 

0.0 

0.0 

00 

0.0 

-0.1 

0.0 

00 

0 0 

0 0 

00 

00 

0 0 

0 0 

0.0 

-0.1 

-0.1 

00 

0.0 

0.0 

00 

0 2 

13 

36 

66 

96 

12_7 

15.4 

17.9 

20.3 

22.8 

25 0 

26_9 

8/23/05 Run #3 

25_5 ppm NOx 

Zero CO, S02 

99 1 ppm CO 

Zero VOC, NOx 

Page 7 50 
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I 08/23/05 14:58-32 0.3 3.1 09 28.5 

08/23/0514:58:42 0.3 3.1 0.9 30_0 

I 08/23/05 14-58:52 0 3 2.8 09 31.3 

08/23/05 14:59:02 0.3 31 09 32.5 

08/23/05 14:59:12 02 3.4 09 33_9 

08/23/05 14:59:22 03 3.5 0.8 34.9 

08/23/05 14 59:32 0.3 3.5 0 9 35.6 

I 08/23/05 14:59:42 0.3 3.4 0 8 36.5 

08/23/05 14:59:52 03 3.6 0.8 37.4 

08/23/05 15:00:02 0.3 3.6 0.8 38.2 

08/23/05 15:00:12 0.3 3.5 0.8 38.7 

I 

08/23/05 15:00:22 02 3.2 0.8 39.1 

08/23/05 15:00:32 03 28 08 39.6 

08/23/05 15:00 42 0.3 2.8 08 40 0 

08/23/05 15:00:52 0.3 2.9 0.8 40_4 

08/23/05 15:01 :02 0.3 29 08 40.8 

I 08/23/0515:01'12 0.3 29 0.8 41.2 

08/23/05 15:01 :22 03 3.1 07 41.7 

08/23/05 15:01:32 0.3 3.3 07 42.1 

08/23/05 15:01 '42 0.3 34 0.7 42 4 

08/23/0515:01:52 0.3 3.2 07 42.5 

I 08/23/05 15:02:02 0.3 3.2 0.7 43.6 

08/23/05 15:02:12 0.3 34 0.7 44.8 

08/23/05 15:02:22 0.3 3.3 0.7 45.0 

08/23/05 15:02'32 0 3 3.3 0.7 46.2 

I 08/23/05 15:02.42 0.3 3.1 0.6 46.3 50.1 ppm 802 

08/23/0515:02•52 0.3 2.7 0.7 46.4 

08/23/05 15:03:02 1.4 2.4 0.6 46.5 

08/23/0515'03:12 14.2 2.7 0.6 45.2 

I 08/23/0515·03:22 15_0 2.6 0.6 42.2 

08/23/05 15:03:32 15.0 2 7 0.6 42.1 

08/23/05 15:03'42 15.0 29 0.6 41.1 15 2 ppm C3H8 

08/23/05 15:03:52 15.0 3.2 05 38.9 

I 08/23/05 15:04:02 15.0 3.2 04 36_1 

08/23/0515:0412 14 9 3? 04 Cl:l::l 

08/23/0515-04:22 5.2 3 1 04 30 6 

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Summary of Analytical Procedures 

1. Particulate 

Samples were transported to the office of Armstrong Environmental, Inc. by Tom Armstrong and delivered 

to Tom Annstrong on 8/24/05. After insuring no leakage had occurred in transport, probe washes and 

impinger solutions were measured with a glass measuring cylinder. Probe washes were transferred to glass 

beakers, rinsing both the sample bottle and m;:asuring cylinder with acetone and adding this rinse to the 

total sample volume. Impinger #1 on the scrubber exhaust was diluted to 300 rnls wrth H20. After 

evaporating the probe washes on a hot plate, samples were desiccated for 24 hrs and weighed to a constant 

weight. Filters were desiccated for 24hrs and weighed to a constant weight. A I 0 rn1 aliquot was taken 

from the impinger #1 solution and analyzed for HF and HCl, the balance transferred to glass beakers and 

evaporated in a oven, desiccated for 24 hrs and weighed to a constant weight. The analytical balance 

(Ohaus Explorer digital) was calibrated with an internal 100 gr. standard. Filters were handled with 

tweezers, beakers were handled with latex gloves and tongs. 

2. HFand HCl 

The ion chromatograph was calibrated using certified standards of 992 mg/hter fluoride and 986 mg/liter 

chloride. Working standards were made by adding 0.5 rnls, 1.0 rnl, 2.0 mls, and 4.0 rnls to a 100 rnl 

volumetric flask and diluting to the mark with either H20 or H2S04. The second standard for H20 

calibration was made twice, the second set of injections used in the calibration curve. Standards were 

injected into the IC using a manual injection valve. After insuring no leakage had occurred to the remaining 

samples (impingers 2,3 & 4 on the exhaust, impingers 1,2 & 3 on the inlet) each sample was diluted to a 

constant volume (300 rnls for the exhaust, 500 rnls for the inlet) and injected into the !C. Each sample was 

injected twice into the IC with the exception of Run #2 from the exhaust on impinger 2,3 & 4 sample which 

was injected four times. 

52 
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FILTER ANALITICAL DATA 

Company: Daltile, Conroe, TX 

Date: 8/23/05 

Location: Kiln Scrubber Exhaust 

Run 1 

Filter ID Number 

Date of Weighing 

Time 

Gross Filter Wt. 

Date of Weighing 

Time 

Gross Filter Wt. 

Ave, Gross Filter Wt. 

Date of Weighing 

Time 

Filter Tare Wt. 

Date of Weighing 

Time 

Filter Tare Wt. 

Ave. Filter Tare Wt. 

Wt. of PM on Filter (grams) 

Total Weight of Particulate (mg) 

44T 

8126/05 

7:03AM 

OAD54 

8126105 

2J4PM 

OAD57 

0:4056 

8/3105 

12'30PM 

03736 

8/4!05 

9:37AM 

0,3736 

0.3736 

0.0320 

32.0 

Run 2 

45T 

B/26/05 

7:02AM 

04106 

8/26/05 

2'15PM 

0.4108 

0:4107 

813105 

12:33 PM 

0:3812 

814/05 

9:39AM 

0:3814 

0.3813 

0.0294 

29.4 

Run 3 

46T 

8/26105 

7:01AM 

0:4050 

8126105 

2'16PM 

oAb51 

0:4051 

8/3105 

12:35PM 

0,3755 

8{4/05 

:40AM 

0.3766 

0.3766 

0.0285 

28.5 

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PARTICULATE ANALYTICAL DATA FORM 

Company: Dalt1le, Conroe, TX 

Date: 8/23/05 

Location: K1ln Scrubber Exhaust 

Run 1 

Density (Pa) 

Blank Concentration (Ca) 

Rinse Volume (Vaw) 

Residue in Rinse (Wa) = Ca·x-vaw-x-pa 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Average Gross Weight 

Less Blank Residue (Wa) 

Average Beaker Tare Weight 

Weight of Particulate in Rinse (mg) 

0.7851 

0:0005095 

178 

0.0001 

8/26105 

2:19PM 

98:3918 

7/6/05 

7:11AM 

98.3769 

7/6/05 

2.33PM 

98.3759 

98.3919 

0.0001 

98.3759 

15.88 

Run 2 

0.7851 

0.0005095 

165 

0.0001 

8126/05 

6:59AM 

107A852 

8/26/05 

2:!S~M 

107:4852 

7/6/05 

7'12AM 

107.475:2 

716/05 

2:32PM 

1074753 

107.4852 

0.0001 

107.4753 

9.88 

ACETONE BLANK ANALYTICAL DATA FORM 

Blank Volume (Va) 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Average Gross Weight 

Date of Weighing 

Time 

Tare Weight 

Date of Weighing 

Time 

Tare Weight 

Average Tare Weight 

Weight of Blank (Ma) 

Ca= Ma/(Va'Pa) = mg/g 

250 · 8/26105 

6:56AM 

.•:· \OS:2903 

sn6io:; 

2:21 F'M 

103.2904 

103 29035 

716!05 

7•!7AM 

!032904. 

7/6i05 

. 2:29PM 

!03.2901 

103.29025 

0 00010 

0 00051 

Note: In no case should a blank residue greater than 0.01 mg/g or 0_001% of the blank 

wei ht be subtracted from the sam le wei ht. 

Run 3 

0:7851 

0 0005095 

182 

0.0001 

8/26/05 

6:53AM 

99:1614 

8/26105 

2:24PM 

99.1611 

7/6/05 

7:13AM 

99.1556 

716105 

2:31PM 

99.1555 

99.1613 

0.0001 

99.1556 

5.63 

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PARTICULATE ANALYTICAL DATA FORM 

Company: Daltile. Conroe. TX 

Date: 8/23105 

Location: Kiln Scrubber Exhaust 

Run 1 

DenSity (Pa) l 

Blank Concentration (Ca) 

Rinse Volume (Vaw) 

Residue in Rinse (Wa) :::: ca-lfvaw·K-Pa 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Average Gross Weight 

Less Blank Residue (Wa) 

Average Beaker Tare Weight 

Weight of Particulate in Rinse (mg) 

ZE.Q7 

'300 

0.0001 

8!26105 

6:52AM 

106.6855 

8126/05 

2:25PM 

!05.6853 

716105 

7:14AM 

1066845 

7/6/05 

2:30PM 

!06.6844 

106.6854 

0.0001 

106.6845 

0.89 

H20 BLANK ANALYTICAL DATA FORM 

Blank Volume (Va) 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Average Gross Weight 

Date of Weighing 

Time 

Tare Weight 

Date of Weighing 

Time 

Tare Weight 

Average Tare Weight 

Weight of Blank (Ma) 

Ca= Mai(Va'Pa) =gig 

250 

8/2610~ 

6:57AM 

101Hll8 

s/26105 

2:20PM 

!OO.Ul9 

100.11185 

716!05 

T18AM 

!DO:)Tl9 

716105 

2:28PM 

100.!H7 

100.1118 

5E·05 

2E·07 

Run 2 

l 

2EcQ7 

300 

0.0001 

8/26/05 

6:54AM 

1()7:4510 

8126/05 

2:23PM 

107.4509 

7/6/05. 

7:15AM 

107:4472 

7./6/05 

2:29PM 

10?.4471 

107.4510 

0.0001 

107.4472 

3.74 

Note: In no case should a blank residue greater than 0 01 mg/g or 0.001% of the blank 

wei ht be subtracted from the sam le wei ht. 

Run 3 

1 

2£•07 

300 

0 0001 

8/26/05 

.6:55AM 

100]654 

8/26105 

2:22PM 

100.7652 

7/6105 

7:16AM 

100.7645 

7/6/05 

2:28PM 

100:7643 

100.7653 

0.0001 

100.7644 

0.84 

.I 55 
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Company: 

Date: 

Location: 

Run#: 

Filter lD Number 

Date of Weighing 

Time 

Gross Filter Wt 

Date of Weighing 

Time 

Gross Filter Wt 

Ave. Gross Filter Wt 

Date of Weighing 

Time 

Filter Tare Wt 

Date of Weighing 

Time 

Filter Tare Wt 

Ave. Filter Tare Wt 

Wt of PM on Filter (grams) 

Wt. of PM in Rinse (grams) 

Total Weight of Particulate (mg) 

F! L TER AN ALIT I CAL DAT P. 

Cliff 

!J(u('O.C 

7'.03 

' 'P ~""{ 

f(u(o! 

r<.f:rY 

''-/:0 £'7 

/' 

( OrA!O e.__ ~ 

vs-r 

tlvdor 

71: 0~}__--

·' lfl o& 

<g(u/o! 

I '{ i I.'> 

,"flcg 

I 

?/J/ o:;-

' /- '-(to I 

i{1k/oi-

' .·o I 

, '-to s-o 

?fu.(v-1 

I'/', 10 

,'f'D)i 

;; /3 ;,,~­

i~:::/s.­

o.3 .. :rt."::;-

;; ;c-r/ /' s·~ 

"'-( : '-ft) 

6 ?,-:t-tf? 

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Dote: 

3:;nk C~n:.:ent1ation (C2) 

~insf \'-,lume (Vaw) 

Resd•./e h .=::-i.:-Jse (\,.,

1

::;) ~ C?"""\i?vl'?a 

7im-e 

lime 

Averag:; Sr-:=tss Wel.sht 

Less 3i3.n.~ ?esi·j~..Je (\'1

1a) 

Jwer'i:?e 3;3ker T-E3J;; Weight 

!t:lft.ti 

iB;moy 

t> 2- I 

?-tin 3 

.r;f:~;~r;; li:tUi1111> 

.,m~~~~mJ; tMiH17 

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3:z:~tk Co7!c~r.t~::.'ckm (C:3) 

,=:i~:tse VJliJiTle (Vaw) 

;::es!:J: ... /e i;; R·i-nse (Wa) ~ C:o .... \ia\.'1~"'"-?a 

Ti;ne 

Time 

Ave:-a_ge Gr:..ss VVeig~t 

l_~s.s 31:::-n.i.:·Resd'Je (I:Va) 

A'':;-.;~, 3oa~.o- ~---, \~loj-7{1"- '-'-:::.- - '.-'tor_ -s '' 

~.·· 

'',qz; 

~!!~~0: t67: '(g$2-

TJ{t;/p;iy 

DJWt:< 

ji;)U/)@ 

','J~~'~j f\ft41$J 

?.u n 3 

.~mW0 'tf;tW"lf 

',~~.~~) '•oo•Vtitr:••: 

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?.b?Ti·:ULA_T:: ~_1\,_!.LYT·:.L.L )P.iA 02f\~ 

Com?acy Do, l+. \C. 

Dcte: 

3io;nk Conc::n:r:::tion (C:a) 

F-Ci~se Volu~e (Vcw) 

Resi-j:.._,·e in ~-lnse (W?.)::: Ca""'V:::v.~"?3 

Dote:;~ W::ighing 

lime 

.ll..verage Gmss Vv'eight 

Le~s 3Ja'n~:-?=si·::l!.Je CYh) 

P.ve.-:-2ge 3eof:~r Tar:: W:=ignt 

D rb 

?. u n l 

......... ::::::: 

*~~·········· 

····-····~·-····· 

• 

! ;t~ltJ-N! fb''N 'i'QJ<f 

~rf~4tf!J. W/7it.ii.F1>' 

·:!~t~;J 

5Q 
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Summary of HF and HCI Analysis 

Plant: Daltile, Conroe, TX -- - ---- ---

Location: Kiln Scrubber Exhaust: --- --- ----- - Date: 8/23/05 

Run# 

2 

2 

3 

3 

,_ --

---- -----

1 2,3"& 4 

1 .2,3,& 4 

2 ],3,8.~ .. 

2 2,:>,& 4 

2 2,3,& 4 

22,3,&4 

--- - --

3 2,3,& 4 

3],3,& 4-

_:VolumE! . _[)jlution 

300'--

300' 

1 , 300 

300 

300 

1 ' 300 

300; 

:loo[ 

300 

300 

300 

:loa·· 

300 

300 -

Sheet1 

--- - --

FI-, ug/ml HF, mg Cl-, ug/ml HCI, mg 

. 6.27: 6:08529:3_- Q62 0 191]0!l 

1, 0.28 0.088452 0.65 0.20046 ---- - ------

Average 0.086873 0.195834 

0.22 0.069498 0.71 0.218964 

0.23. 0.072657 0.68 0.209712 

Average 0.071078 0.214338 

0.26 0.082134 0.9 0.27756 ---------------- - - - ---

0.27 0.085293 0.94 0.289896 ----- --- ------ -----

J;ver<Jge 0.083714 0.283728 ----- . 

048 0.151632 0.35 0.10794 ---- -

1 : 047 0.148473 0.37 0.114108 -· ------ ------

)\.verage 0.150053 0.111024 .. -

043 0.135837 0.56 0.172704 

0.38' 0.120042 044 0.135696 

048 0.151632 0.52 0.160368 

0.31 0.097929 048 0.148032 

Average 0.12636 0 1542 

0.5 0.15795 042 0.129528 

0.54 0.170586 042 0.129528 . -

,Average 0.164268 0.129528 

Totals 

Run #1 0.236925 0.306858 

Run #2 0.197438 0.368538 - , ---- -

Run #3 0.247982 0413256 

60 

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Sheet1 

Summary of HF and f:l(;l Jl.nalysis 

Plant: Daltile, Conroe, TX 

Location: Kiln Scrubber Inlet - -----

Date: 8/23/05 

Run# Imp# Volume Dilution Fl-, ug/ml HF, mg (;l:,u~/ml HCI, mg 

1 1 ,2 & 3 - -- ------ --

1 1 ,2 & 3 

2 1,2 & 3 

2 1,2 & 3 

3 1,2 & 3 

3 1,2 & 3 

500 10 14.65 77.13225 26.76 137.5464 

500 

500 

500 

500 

500 

10 15.19 79.97535 

Average 78.5538 

10 17.39 91.55835 

10 17.37 91.45305 

Average 91.5057 

10' ----------

10 i 

13.31 70.07715 

12.94 68.1291 

Average 69.10313 

Page 1 

------------------

26.98 138.6772 

138.1118 

28.55 146.747 

29.39 151.0646 

148.9058 

23.88 122.7432 

-- ----

23.64. 121.5096 

122.1264 

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Conditions 

Date 

Time 

Component i (> 

Fl· 1. 1 ......... 

Cl· 1 666 

2 '' 

........ 

6 ' 

Component 

FlCl2 

4.96 ug/!nl Fl- in H20 

4.93 ug/ml Cl- in H20 

08/24/2005 

09:30:02 

Number Retention 

1 1 .050 

2 1.666 

Area 

403 .. 80 ~1 

301.75 M 

705.55 

1 0/A .. 000!1'\! 

External Units 

4.54 ug/ml 

4.b9 ug/ml 

''' ) 

Area external 

403.80 M 4 '54 

30i.75 M 4 '59 

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c:ond5. tic.ns 

D.ste 

TimE~ 

Co11ponent 

Fl- 1. ' ......... 

Cl- 1. 6 

2 ......... 

3i .. 

4 ......... . 

\ ..... 

6 ........ . 

Component 

Fl~ 

Cl-.. 

2 

6 -~ '76 ug_/ml 

4 . 93 ug_/m l 

08/24/200S 

09:33:04 

!.:: :: 

t::' ]_-

ClNumber Retention 

1 1"050 

2 1 .. 666 

i.n H2Cl 

in H20 

1 C)2 4 . 00()rn\J 

Area Ex.~ernal 

403.50 M 4 . 54 

315.65 M 4.79 

Area External Units 

403 ".50 f"l 4.54 ug/rnl 

315.65 M 4.79 ug/mJ 

719 .. 15 9 .. 33 

.. : 63 
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FlClFl~ 

Clc:or!ditions 

Date 

Time 

1. H 

Component 

2 

9.92 ug;'ml Fl- in H20 

9.86 ug/ml ~~- irf H20 

08/24/2005 

09:36:'54 

Number Retention Area 

1 1. .050 795.75 

2 1 666 579,12 

1374.87 

l '~J2Ll . OOC'trr\/ 

795.75 M 9.42 

579.12 M 8.48 

External Units 

~1 9A2 ug/ml 

M 8 Ji8 ug/mJ 

17.89 

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Conditions 

Date 

Time 

9~92 ug/ml 

9~86 ug/ml. 

08/24/2005 

09:40:23 

F.lComponsnt 

-· J ()2 , li (.;Om\/ 

?stentio',,J ... ''I'"'' 

' 

fl- 1 . ;.:::::::::::"·::":: .... , ............ ''""'"""""''"'''. .11'''" 

I 

1 '666! Cl- ; ..... , ........ ,::·:,,,,,,,,,,,,, .. . 

Component Number Retention 

n- 1 1 .. 050 

c .l -- 2 1 .666 

2 

in 

in 

H20 

H20 

Area 

873" 15 

560.00 

1433.15 

External 

~·1 10.30 

M 8 _41 

18.71 

~rte~ na.l 

873.15 M 10.30 

560.00 M 8.41 

Units 

ug/rnl 

ug/rnJ 

65 
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FlClFlClConditions 

Date 

Time 

1 . ; .• 

1.700 

Component 

2 

19_84 ug/ml Fl- ~n H20 

19.72 ug/ml Cl- in H20 

08/24/2005 

09:45:00 

Number Retention Area 

1 1.066 1692.90 

2 1 .700 1.380.90 

3073.80 

~.rea External 

1692.90H 19. 39 

1380. 90 M 21 . 35 

External Units 

1"1 19.39 ug/ml 

M 21.35 ug/m.l 

40.74 

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FlClFlClConditions 

Date 

Time 

Component 

2 

19_84 ug/ml ~·1- in H20 

19.72 ug/ml Cl- ln H2G 

08./24/2005 

09048,11 

Number Retention Area 

1 1.066 1.690.15 ,, 

/, 1.700 1346.30 

3036.45 

Area 

1690.15 M 19.36 

1346.30 M 20.86 

External Units 

~1 19.36 ug/rnl ~1 20.86 ug/mJ 

40.22 

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Date 

Time 

39.68 ug/ml Fl- in H20 

39.44 ug/ml Cl- in H20 

08./24/2005 

09:53:14 

~ompDnt'n:. Ret.enti"i' . . , .................................................................. . 

Fl- 1. 

ClComponent Number Retention Area 

F 1 ·-· .c ' 1.066 3245.20 

Cl- 2 1 "716 287-5,30 

2 6120.50 

l 02.6. ,_ OOOm\J 

Area ::xtsrnal 

3245.20 M 37.82 

2875.30 38.49 

External Units 

~~ 37.82 ug/ml 

38 .. 49 ug./rnl 

76.31 

68 
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Condi t.ions 

Date 

Time 

CCI~IPOflt'ilt 

FlClComponent 

f7 .lCl2 

39.68 ug/ml Fl- irr H20 

39.44 ug/ml Cl- 1n H20 

08/24/2005 

09:56~02 

Number Retention Area 

1 1.083 3426.80 

2 1 .716 2827.75 

6254.55 

Ex~~rnal 

3426.80 M 39 '92 

2827.75 39 .12 

External Units 

M 39.92 """ /rv,l w.:;:} I '""" 39.12 ug/rnJ 

79.05 

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FlClConditions ~ 

ct. 5(-; 

Date 

Time ~ 

Component 

L !· 

8' 

i 

' ......... 

s, .... 

{.1. Cr ?.-

- ug/ml Fl- in H20 

X 11 ug/n1l Cl- in H20 

08/24/2005 

10:04:06 

! 

Component Number Retention Area 

FJ- 1 1.050 869.20 Cl- 2 1"683 644.53 

2 1513.73 

lrr ea b:ter Gal 

869.20 M 10. 32 

644.53 M 10.79 

External Units 

~,, 10.32 ug/m] 

r·1 10.79 ug/ml 

21.11 

70 
--------------------------------- --------------- -------------- ---------------- ------------ - ---------

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Ccndi t~i<.)fl~; 

Date 

Time 

9.92 ug/ml Fl- in H2C 

9.86 ug/ml Cl- ln H20 

08/24/2005 

10::07:06 

~-1 0/ , 40(Jrn\t 

Comoonent 

FlClComponent Number Retention Area 

rJ ' ,050 910.45 

Cl- " ) 1.683 634.74 

~ 

L 1545.19 

Area 

910.45 M 

634.74 M 

External Units 

M 10.80 ug/nil 

1'1 9.79 ug/ml 

20.59 

.. ) 71 

External 

10.80 

9.79 
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Cali.brst.i_on file 

AMOUNT INJECTED 

AREA 0,000 ................................................ 

3336. 

Avg slope of C\Jrve: 85.78 

Y-axis intercept: 0,00 

Coeff of lin regr: 0.88 

~lo. Area Amount 

0: 0 .000 0 .000 

.1 : t~03 650 4 ,960 

2: 889 .825 9.920 

3: 1691 .525 19.840 

{j.: 3336 .000 ~::Jo 

~~ .680 

CF 

0 .000 

81 .381 

89.700 

85,2.58 

8/~ r,-;'") 

• "-'' ,j 

2 

3 

4 

5 

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AI10UNT INJECTED 

ARE?\ 0 0()0 39 <~O 

I-' 

2851.52 

slope of curve: 69.65 

Y-axis intercept· 0.00 

Coeff of lin regr: 0.92 

f'-lo ~1rea r:imOtJ nt 

0 : 0 .000 0 000 

1 : 308 700 ,q .930 

2 ' 639 36.:, 9 860 

3 : 1363 600 19 720 :'~ : 2851 b2S ?,9 <'1, !1 () 

('C 

~' 

0 .000 

62 .617 

6•1 .844 

69 148 -7 ,.., 

; ,,::: 300 

1 

2 

3 

4 

5 

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Date 

Time 

Daltilc ScT·ubber Exhaus~ 

Run #1 I!Hf:.- :ttl 

Volume 300 DiJ.ution 1/1 

08/24/2005 

10:2';;:34 

-·1 Ci2 .. o:;.oom\i 

Component 

(unknown) 

FlClComponent 

FlCl2 

Number 

1 

2 

Retention Area 

1.033 21 .71 

1 .. 650 38"40 

60.11 

102l; "OOOml ./ 

External Units 

r1 0.27 ug/ml 

M 0_62 ug/m1 

0.89 

Area 

45.25 

21.71 M 

38.40 M 

74 

External 

N/A 

0.27 

0.62 
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Component 

r unkno~<n) 

(unknown) 

FlClDate 

Time 

Component 

F l·-

Cl2 

Dsltil2 Scrubber Exhaust r~:un #1 Imp #1 

Volume 300 Di!utic~l 1/1 

08/24/2005 

10:25:42 

Number Retention 

1 1.050 

2 1 .666 

Area 

22.50 

40.40 

62·.90 

External Uni t.s 

M 0.28 ug,/ml 

M 0.65 ug/ml 

0.93 

Area 

32.60 

47 .00 

22.50 M 

40.40 M 

75 

Ext.s•nal 

N/A 

N/A 

0.28 

0.65 
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Date 

Time 

Run #2 In,p #1 

Volume 300 Dilution 1/1 

08/24/2005 

10:32:26 

-102 ."~OOm\..' 

Component 

(unknown) 

FlCJComponent 

Flc l2 

Number 

1 

2 

Retention Area 

1.033 17.95 

1 "6!50 43 60 

61.55 

1 rJ2.(t , OOOrn\/ 

External Units 

M 0.22 us/ml 

M 0.71 ug/ml 

0.93 

76 

Area 

43.90 

17.95 M 

43.60 M 

External 

N/A 

uz 

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Component 

I unknown) 

F lClDat~e 

Time 

O<ile SCil1bbe7 E:~haust 

Run #2 Imp :H1 

VolumE: 300 Di li.~t .. ion L/'1 

08/24/2005 

10:35:43 

-- :J C:2 . 4 00rn'v' 

Retention 

: 

0. 2161 

1 . 11 ! 

sj ..... 

! ...... . &i 

•, 

r 

Component Number Retention Area 

Fl- 1 1.033 18.40 

Cl- 2 1.6h6 /:1.75 

2 60.15 

1024.000mV 

Area External 

34.30 N/A 

18.40 M 0.23 

41.75 M 0.68 

External Units 

M 0.23 ug/ml ~1 0 "()8 ug/rnl 

0.90 

77 
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Component 

(unknown) 

(unknown) 

FlClRun :ff3 Imp 

\/oJume 300 

Date 08/24/2005 

Time 10:40:19 

~,:tJ2 .. 40()rn\.i 

Retention 

I 

1.666/ F'' 

2i' 

! 

, 

3] .. ··· 

i.. ... 4i 

I 

Si · 

' 

! 

I····· 6· ! 

Dilution 1/1 

Component Number Retention Area 

Fl- 1 1,050 20.90 Cl- 2 J ,666 5:) "50 

2 76.40 

102r{ ,OOOrn\J 

External Units 

M 0.26 ug/ml 

M 0.90 ug/ml 

1 .16 

Area 

513.20 

25.70 

20.90 M 

55.50 M 

78 

External 

!UA 

N/A 

0.26 

0.90 
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Date 

Time 

Da_l"t-ils s~~Tubt>~; '--· :-.eu:st 

Run .ft3 Imt.:o #1 

Volume 300 DilLttion 1/1 

08/24/2005 

10:44:28 

-~ 102, '~ OOm'v' 

Component 

(unknown) 

lunknol~n) 

( unkr,own I 

FlClComponent 

FlC1-· 

2 

Number 

1 

2 

Retention Area 

1 ()":>0 "•,_, ..J,,) 22 .27 

:i_ 650 c -, ,j I _fJe 

80.15 

Area External 

61.00 N/A 

32.90 N/A 

65.80 N/A 

22.27 M 0.27 

57.88 M 0.94 

External Units 

!~i 0 "27 ug/m1 ~1 0 .94 ug/ml 

1 .21 

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(i)f!ditions 

Compnnert. 

(unknown) 

Date 

T j nvsComponent 

0 

H20 Blank 

08/24/2005 

10:53:20 

Numbe• Retention ATe a 

0.00 

1024. OOOm\/ 

Exteonal Units 

0.00 

Area E!:ternal 

3L60 N/A 

80 
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I 

(unknown) 

FlClDa_te 

Time 

Component 

2 

08/24/2005 

11:01:28 

Number Retention 

1 

2 

1.033 

1 "666 

Area 

334"20 M 

270 . 70 r1 

604.90 

External Units 

4"11 ug/rnJ 

4.38 ug/ml 

8.49 

105.85 

334.20 M 

270.70 H 

81 

N/A 

4 '11 

4.38 
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Cornpont:nt 

(unknown) 

(unknown) 

FlCl· 

Time 

I 

0. 8331 

1 . 11"·""' 

I 

I 

1. 633! ; 

zl·· .. · · 

Component 

Fl~ 

Cl-· 

2 

,; "96 ug/ml F l- :. r· H2S04 

4.~3 ug/"1l Cl- in H2S04 

08/24/2005 

11:04:06 

Number Retention Area 

1 1 .016 354.65 

2 1 .633 265.75 

620.40 

Area Ext.t>rnal 

75.05 N/A 

103.90 N/A 

354.65 M 4.36 

265.75 M 4.30 

External Units 

r>,,', 4.36 ug/ml '' M 4.30 ug/ml 

8.66 

82 
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Compon&nt 

(unknown) 

FlClDate 

Time 

Component 

FlCl2 

9.92 ug/ml Fl- ~-r1 ~2S04 

9.66 ug/ml Cl- in H2S04 

08.-'"24/2005 

11::14:25 

Number Retention Area 

1 1 .033 839" 10 

1 .683 E.l~9 _40 

1388_50 

~L 0/'/l . OOOrn\/ 

External Units 

~1 10 -~~2 ug/ml ~1 8"66 ug/rnJ 

19_09 

Area 

106.20 

83UO M 

549.40 M 

83 

N/A 

10.42 

8.66 
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Component ( unho~m) 

(unknown) 

FlClComponent 

Flc 1--

2 

Date 

Time 

9~£6 ug/ml 

08/24/2005 

11:16:56 

Number Retention 

1 1 .033 

2 1 .650 

H2SC4 

Area External 

8L!4 ,55 r~1 10 /j 0 ",,,,_, 

54/) .10 ~1 8 .66 

1393.65 19.15 

Units 

u_g/rnl 

U9/m1 

Area 

57.60 

106.95 

844.55 H 

549.10 M 

84 

Exler nai 

N/A 

N/A 

10.48 

8.66 
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Date 

Time 

19. 8tt- ug/ml 

1 S. 72 ug/inl 

08/24/-2005 

11:26:52 

-J 02 • .:::!O()rn\1 

Component ( unknowri) 

(unknown) 

Flc 1-

F;etention 

0.166' 

0.8501 

1. H 

l 

' I 

1.716\ 

i 2. 

i 

Component 

,c- 1 ,. 

Cl2 

Number Retention 

1 1 .050 

~2 J .716 

l_ i1 f-12504 

Area 

~ 7 r:::, 1 _L ' ,_ .~ .10 M 

1:218 " -:~ s 11 

2969.45 

J024.00Um\/ 

External Units 

20"77 ug/ml 

17 .96 ug_,/m1 

38.73 

-· ./ 

Area 

31.10 

106.90 

1751.10M 

1218.35 H 

85 

External 

N/A 

N/A 

20 '77 

17 '96 
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Compont>nt (unknown) 

(unknown) 

FlClDate 

Time 

Component 

Fl 

Cl2 

19.84 LC;i/rnl Fl- lfi H2SQ:.} 

19.72 ug/rnl Cl- 1r1 H2S04 

08/24/2005 

11:29:24 

1(!~? -~-OOmV 

Number Retention Area 

1 1 050 176[~ "05 

2 l .683 1.J 62 s:·, 

2926.60 

:1.024 .OOO~n\i 

External Units 

i"1 20 Q~ ./L ug/ml ~-~ 17 />0 

- t:.. / ug/rnl 

38.21 

Area 

72 '35 

107.50 

1764.05 M 

1162.55 M 

86 

External 

N/A 

N/A 

20.92 

17 '29 
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Condi t.l.ons 

Date 

Time 

39_68 ug/ml Fl- 1n H2S04 

39.44 ug/ml Sl- 1n H2S04 

08/24/2005 

11:39:18 

-~·1()2 .1.!-00rn\/ 

Component (onknown) 

(unknown) 

FlClComponent 

Fl--

C1-

2 

Number 

1 

., 

·' 

Retention Area 

1 "066 3522 . 11-0 

1 "76(, 2712 . 2'' ~ 

6234 .60 

1024 "OOOm\! 

External Units 

!'4 38 "96 u.g/rn1 

1'1 37 .79 U-J/m1 

76.74 

Area 

18.40 

112.60 

3522.40 M 

2712.20 M 

87 

Erternd 

N/A 

N/A 

38.96 

37.79 
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Compone~t 

(unknown) 

I unknown) 

flClDate 

Time 

39.68 119/ml Fl- in H2S04 

39.44 ug/ml Cl- in H2S04 

08;-"24/2005 

11:41:51 

--102 _4C<Om') 

Retentior1 

0' 116['' . 

' 

' 

0 .850•1' 

1. 1 

! 

Component Number Retention Area 

FJ .• 1 1 .066 3645 "'" .. .._;,._,< 

c 1·- 2 1 "766 2731 .80 

2 6377.10 

l024.000mV 

Area External 

72 .J:, N/ A 

116.45 N/A 

3645.30 40.19 

2731.80 M 38.01 

External Uni t.s 

40 "29 ug/ml 

1'1 38 .02 u.g./ml 

78.31 

-· 88 
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I 

I 

F l·- . col 

At'\OUNT INJECTED 

AREA 

')' 

3583.8 

slope of curve: 88 52 

xis inte)·cept: 0.00 

Coef·f of lin rAgr: 0.88 

!',10 /'~I ea r.:,m()U r1t 

0 : 0 .000 0 000 

1 : ::;4li 425 4 .960 

2 : 841 .8:c.::8 9 .920 

3 : 1757 575 l 9 .840 

4 : 3583 850 /?;9 680 

CF 

0 000 

69 .441 

84 861 

88 ,587 

90 ::.:19 

2 

3 

4 

5 

89 
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I 

AI~OUNT INJECTED 

AREA 

2722, t)OU! ........................................................... . 

Avg slope of cur\Je: 63.53 Y-a,~is intercept~ 0.00 

Coeff of lin regr: 0.82 

~lo Ar·en Amount 

0 ' 0 .000 0 .000 

1 : 268 .225 4 .930 

2' ~' 549 _250 9 ,860 

'>· -'" 1190 .450 19 J20 

4 2722 ,0()() 39 "~~ 40 

39.440 

CF 

0 "00() 

54 .. 4-07 

::,5 .705 

60 .368 

69 .016 

l 

2 

3 

4 

5 

90 
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I 

I 

I 

I 

I 

I 

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Conditions 

Date 

Time 

Daltile Scrubbe1- Exhaust 

Run #1 Imps 2,3 & 4 

Volume 300 Dilution 1/1 

08/24/2005 

11:51=4-4 

--1.J2 "4 OOm\i 

Component (unknown) 

(unknown) 

F!-

C]-

Component 

FlCl--

2 

Nurnbe)· 

1 

-, 

"-

Retent.ion Area 

1 .200 33_25 

1 .700 18.90 

52.15 

1024.000mV 

External Units 

1'1 0.48 ug/ml ~·r 0"?-5 ug/m.l 

0.83 

91 

Area 

31.10 

47.90 

33.25 M 

18.90 fl 

External 

N/A 

N/A 

0.48 

0.35 
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Concii Lions 

Date 

Time 

Daltile Scrubber Ext1aust 

Run #1 Imps 2,3 & 4 

Volume 300 Dilution 1/1 

08/24/2005 

12:03:48 

-102.400mV 

Component 

(unknown) 

FlClComponent 

FlCl2 

Number 

1 

0 

Retention Area 

1"200 32.40 

1 .716 20.35 

52.75 

~1 

1024 .OOOnW 

External 

0.47 

0.37 

0.84 

Units 

ug/rnl 

ug/rnl 

Area 

53.80 

32.40 

20.35 M 

n 9,., -' -· . .. {_, 

External 

N/A 

0. 47 

0.37 
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I 

Date 

Time 

Daltile Scrubber Exhaust 

Run #2 Imps 2,3 & 4 

Volume 300 Dilution 1/1 

08/24/2005 

12:06:36 

--1 ()2. 400m\' 

Component 

(unknown) 

( unkrro~1n) 

Fl· 

ClComponent 

Fl-· 

Cl·· 

2 

Number- Retention Area 

1 1 "183 29.60 

2 1.700 :30.:30 

59.90 

:L02~.000mV 

Exter-nal Units 

0.43 ug/ml ~1 0.56 ug/ml 

0.98 

Area 

21 . 25 

110.80 

29.60 

30.30 M 

93 

External 

NiA 

N/A 

0.43 

0.56 
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I 

I 

Component 

(unknown) 

(unknown) 

Flc 1-

Date 

Time 

Daltils Scrubber Exhaust 

Run #2 Imps 2,3 & 4 

Volume 300 Dilution 1/1 

08/24/2005 

12=16=1.3 

-102 .400m\i 

Retention 

0 '1 i 6j 

1 0 ,850! 

1! 

1.200! 

! 

716! 

2i"'''' 

i 

3!······· I 

' 

! 

I 

4("' 

Component Number Retention Area 

FlCl2 

1 

2 

1.200 

1 "716 

26 .. 65 M 

:24 .. l 0 1'·1 

50.75 

1024 . OOOm\i 

External Units 

0.38 ug/ml 

0. il-L~ ug/m.l 

0.83 

Area External 

21,00 N/A 

53.90 N/A 

26.65 H 0.38 

24.10 11 0.44 

94 
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Condi t_i CHIS 

Date 

Time 

Oaltile Sct·ubber Exhaust 

Run #2 Imps 2,3 & 4 

Volume 300 Dilution 1/1 

08/24/2005 

12=18:47 

-102 .400m\" 

Component 

(unknown I 

(unknown) 

FlClRetention 

0.0161 

0. 8331 

1 i .. 

1.083i I 

1.700! 

Component 

F l --- Cl2 

Number Retention Area 

1 1.083 33.35 

2 1.700 28,35 

61.70 

Area External 

53.60 ri!A 

39.70 M N/ A 

33.35 M 0.48 

28.35 fl 0.52 

External Units 

r1 0.48 ug/mJ 

1•1 0,52 u g,/rn 1 

1 .00 

95 
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Date 

Time 

Daltile Scrubber Exhaust 

Run fi2 Imps 2,3 & 4 

Volume 300 Dilution 1/1 

08/24/2005 

12:28:10 

-102 ,400rn\/ 

Component (unknown) 

(unknown) 

FlClComponent 

~' 1--

Cl 

2 

Number 

1 

2 

Retention Area 

1,200 21 AO 

1.716 26"50 

47.90 

l 02Ll OOOm\/ 

External Units 

M 0.31 ug/ml ~-1 0.49 ug/rnl 

0.80 

Area 

17.80 

52.30 

21.40 M 

26.50 M 

96 

External 

N/A 

N/A 

0.31 
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C.:)nditions 

Date 

Time 

Daltile Scrubber Exhaust 

Run #3 Imps 2}3 & 4 

Volume 300 Dilution 1/1 

08/24/2005 

12:37:39 

-102 . 400rn\i 

Component 

(unknown) 

nClComponent Number Retention Area 

Fl- 1 1.200 311.90 

Cl- 2 1 .716 22.85 

2 57.75 

~1 

M 

1024 "OOOm\J 

External 

o.so 

0.42 

0.92 

Units 

ug/rnl 

ug/ml 

Area 

47.90 

34.90 II 

22.85 M 

' ' 9 '7 -' -' I 

External 

N/A 

0.50 

0.42 
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I 

Condit ic•ns 

Component 

(unknown) 

(unknown) 

FlClDat.e 

Time 

Component 

FlCl2 

Deltile Scr·lJbber Exhaust 

Run #3 Imps 2,3 & 4 

Volume 300 Dilution 1/1 

08/24/2005 

12=49:23 

Number Retention Area 

1 1 .. 200 37.60 

2 1.733 22.80 

60.40 

1024 "OOOm') 

External Units 

M 0.54 ug/ml 

11 0- (l2 ug/rn.l. 

0_96 

98 

Area 

33.45 

51.55 

37.60 M 

22.80 M 

External 

N/A 

N/A 

0.54 

0.42 
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C<>nditions 

Date 

Time 

Daltlls Scrubber Inlet 

Run #1 Imps 1 & 2 

Volume 500 Dilution 1.110 

08/24/2005 

12:59:04 

-~ 102 "400!~1\/ 

Component 

(unknown) 

(unknown) 

FlClComponent 

Flc l·· 

2 

!~umber 

1 

2 

Retention Area 

1 .083 1278.70 

1.766 1736 . ()8 

3015.68 

1024.000mV 

Area External 

21 .00 N/A 

27.65 N/A 

1278.70 H 14 . 6S 

1736.98 M 2& .76 

External Units 

1•1 14.65 ug/rnl 

M 26,76 uq/ml 

41.41 

99 
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Condi t.ion2:; 

Da.te 

Time 

Daltile Scrubber Inlet 

Run #1 Imps 1 & 2 

Volume 500 Dilution 1/10 

08/24/2005 

13=01=35 

-102"400m\J 

Component 

(unknown) 

FlClComponent 

Flc 1--

2 

Number 

1 

2 

Retention Area 

1 ,066 1328.05 

1.750 1754"61 

3082.66 

M 

;j 

1024,000m\/ 

External 

15 "19 

26"98 

42.17 

Units 

ug/ml 

ug/mJ 

Area 

41.20 

1328,05 H 

1754.61 M 

100 

External 

N/A 

15 ,)9 

26_98 
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Date 

Time 

Daltile Scrubber Inlet 

Run #2 Imps 1 & 2 

Volume 500 Dilution 1/10 

08/24/2005 

13=10:52 

-102"400m\J 

Component 

(unknown) 

FlClComponent Number Retention Area 

Fl- 1 1_0(,6 1531 .30 

Cl- 2 1.766 1875,94 

2 3407.24 

M 

M 

1024.000m'J 

External Units 

17.39 ug/rnl 

::::8 "55 ug./m1 

45.94 

Area 

69.60 

1531.30 M 

1875.94 M 

101 

External 

N/A 

17 '39 

28 '55 
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I 

Date 

Time 

Run #2 Imps 1 & 2 

Volume 500 Dilution 1/10 

08/24/2005 

13:16:03 

-102.400rn\/ 

Compor!ent 

(unknown) 

FlClComponent 

FlC.l2 

Numbeo Retention Aoea 

1 1.066 1530.00 

2 1 ""766 1941.76 

3471.76 

J 024, OOOm\/ 

Exteonal Units 

~1 17.37 ug/rnl 

t1 29.39 ug/mJ 

46.77 

Area 

75 '80 

1530.00 M 

1941.76 H 

102 

External 

N/A 

17.37 

29.39 
---------

I 

I 

ConcH tio ns 

Date 

Time 

Run #3 Imps 1 & 2 

Volume 500 Dilution 1/10 

08/24/2005 

13:25=21 

I -1<)2 .400m\l 

I 

I 

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I 

Component 

( llnknown) 

FlClCompon,2nt 

Flc 1-· 

2 

Number Retention Area 

1 1 "06() 1154 .60 

2 1.750 1513.29 

2667.89 

'l 024. _ OOOm\/ 

External Units 

~1 13.31 ug/ml 

11 ;?3.88 ug/rnl 

37.19 

Area 

62.80 

115UO M 

1513.29 M 

103 

External 

N/A 

13. 31 

23.88 
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Date 

Time 

Daltile ScrLtbber Inlet 

Run #3 Imps 1 & 2 

Volume 500 Dilution 1/10 

08/24/2005 

13:27=45 

~· 1 02 . 4()0m\J 

Component 

(unknown) 

f]-

ClComponent 

F l--

Cl2 

Number 

1 

2 

Retention Area 

1 066 1120.40 

1.750 1495.26 

2615.66 

~1 

M 

1024 . OOOm\1 

Extel-nal 

12.94 

23 64 

36.58 

Units 

ug/ml 

ug/rnl 

Area 

82.05 

1120,40 M 

1495.26 M 

104 

External 

N/A 

12,94 

23,64 
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Condit-ion:=:~ 

Date 

Time 

Daltile Scrubber InlBtH2S04 alank 

08/24/2005 

13:39:32 

1024.000mV 

Component (unknown) 

Rete P t~ ~~~' .. ............ , ........................................................................................................................................................................................................................................................ , 0. 

(unknown) 0. 

(unknown) 2. 

Component Number Retention Area External Units 

0 0 .. 00 0 .. 00 

Ar&a 

64 .19 

119.00 

93.25 

105 

External 

N/A 

N/ A 
I 

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I 

I 

Condi t.i..(.•ns 

Date 

Time 

Daltile Scrubber Inlet 

19.84 ug/ml Fl- in H2S04 

19.72 ug/ml Cl- in H2S04 

08/24/2005 

13:49:22 

"¥ :1 C2, 400m') 

Component 

(unknown) 

( unknofln) 

FlClComponent 

f' 1--

Cl2 

Number 

1 

~. 

< 

Retention Area 

1 .050 1.763.25 

1 .. 716 1240.:35 

3003.60 

1. •)21 0 OOCrml) 

Area External 

2UO N/A 

116.30 fl N/A 

1763.25 M 19.90 

1240.35 M 20.36 

External Units 

I~ 19 .. 90 ug/ml 

M 20 .. 36 ug/m] 

40.26 

106 
NVIRONMENTAL, INC 

reign How 

TX 75247 CHAIN OF CUSTODY RECORD 

PHONE NO .. (214)•631-0021 

FAX NO. (214) 905-0634 

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N VI RON MENTAL~ INC 

PHONE NO .. (214)•631-00~~1 

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Copy to Clion11flrojnc1 Coordin;llor 

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THllO 

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NVIRONMENTAL, INC PHONE NO.~ (214)•631-0021 

FAX NO. { 214) 905-0634 

reign Row 

TX 75247 

CHAIN OF CUSTODY RECORD 

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Fluoride Standard 

Product Number 037158 

Certificate of Analysis 

Lot Number 050607 

Expiration of Certification 

December 2006 

The Fluoride Standard was developed to aid the analysis of anions by Ion Chromatography (IC). 

The single-ion standard was prepared by the dissolution of high-purity salt in 2:18.2 megohm· 

deionized water, which was tested by IC for ionic contaminants. The bottle label states the 

nominal concentration value of the ionic component for informational purposes only. The ion 

concentration value was detcnnined by Ion Chromatography. Tbe system was standardized using 

the National Institute of Standards & Teclmology (NIST), Standard Reference .Material, SRM 

3183 (Fluoride Standard Solution). T11e actual concentration value determined for the 

component ion is listed below. 

Fluoride Standard 

Component 

Fluoride 

Concrntration 

(mg/L) 

992 ± 4 

The concentration -value is based on proven reliable metl1ods of analysis. The estimated 

uncertainties are two standard de,·iations of the concentration ,·alues. The concentration value is 

''-'ananted to be stable for three montbs from the date of shipment 

Tbe preparation and analyses of tbe Fluoride Standard was perfom1ed with extreme care by 

DlONEX Corporation Consumablcs l\1anufacturing Department. 

Dione~ U.S. Regional ou;ces 

S,n,·.~·o·o. c; V,\oirr-~:r; I·_ 

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Dione~ International Subsidiaries 

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Chloride Standard 

Product Number 037159 

Certificate of Analysis 

Lot Number 041210 

Expiration of Certification 

June 2006 

The Chloride Standard was developed to aid the analysis of anions by Ion Chromatography (I C). 

The single-ion standard was prepared by the dissolution of high-purity salt in :::18.2 megohm 

deionized water, which was tested by IC for ionic contaminants. The bottle label states the 

nominal concentration value of the ionic component for informational purposes only. The ion 

concentration value was determined by Ion Chromatography. The system was standardized using 

the National Institute of Standards & Technology (NIST), Standard Reference Material, SRM 

3182 (Chloride Standard Solution). The actual concentration value determined for the single-ion 

is listed below. 

Chloride Standard 

Component 

Chloride 

Concentration 

(mg/L) 

986± 4 

The concentration value is based on proven reliable methods of analysis. The estimated 

uncertainties are two standard deviations of the concentration values. The concentration value is 

warranted to be stable for three months from the date of shipment. 

The preparation and analyses of the Chloride Standard was performed with extreme care by the 

DIONEX Corporation Consumables Manufactunng Department. 

Document No. 03~ 1 S4-25 

Oionex U.S. Regional 01frt:es 

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- - - - - - - - - - - - -

Meter 

Seri<JI/1-

jlllljljl 

11 

/3 

Armstrong Envnonmenlnllnc 

EPA Mel hod 5 

522 Series Meter Box Calibration 

Pre-Test Orifice Method 

English Meter Box Units, English K' Factor 

Dale -------------

B<lrornelric Pressure·---------> 

Theoretical Critical Vacuum---> 

08/04/05 

29.75 (in. H!J) 

14.03 (in Hg) 

IMPORT AI\ I' or Vdlid lest rt:sulls, the Vcu:uum should be 1lo 2 in. Hu greater !han the Theorelical Critical Vacuum shown above. 

IMPORT AI\ The Critical Orifice Coelficiont, !<', rnu::;l Ue c·1lered in English units, (ft)"3.(deo R)hQ 5/((in Hg)'(rnin)) !!11!!11' 

DIW GAS METER READINGS 

-CHITICAL ORIFICE READINGSV"lorrw Volunw Volume lniha/ Temps. Final Ternps Orifice I<' Orifice Actual dl I Time lnilicil final Total Inlet Oullel Inlet Oullel Serial# Coefficient Vacuum (111 H20) (l!llfl) (Cll ft) (cu fl) (Cii fl) (deg F) (deg F) (deg F) (deg F) (number) (see above) (in Hg) 0.25 6.00 661.1300 063.132 1.932 89.0 89_0 89_0 89_0 40 0.242 23.0 0 51 7.(10 564.0fJ0 667 230 3.230 89.0 89.0 90_0 90.0 48 0_344 21.0 0_94 6_00 667.100 670.1319 3.719 90.0 90.0 91.0 90.0 55 0.464 19.0 1.55 10 no 671_300 619.274 7.974 91_0 90.0 93_0 91_0 63 0 593 17.0 ::1.00 6.00 6H0.200 686.809 6_609 93.0 91.0 95,0 9'1 0 73 0.824 14.5 

................................................... RESULTS ................................................. .. 

--· DRY GAS METER· --·-.,·--ORIFICE---------

-- DRY GAS MEl ER -- -ORIFICE ---------

VOI.UME VOLUME VOLUME VOLUME VOLUME 

-Ambient Tempera!taelnilin) Final Averaoe 

(deg f) (de9 f) (dog f) 

90 0 90.0 90_0 

90.0 90 0 90.0 

91_0 

92.0 92.0 

92.0 92.0 

93 0 

91.5 

92.0 

92 5 

CORRECT CORRECTED CORRECT CORRECT NOMINAL 

Vm(sld) Vrn(sld) VL:r(sld) Vcr(si(J) Vee 

CALIBRATION FACTOR 

y 

Valiu!ion 

CALIBRATION FACTOR 

dH@ 

(i)IJ fl) (tilers) (cu fl) (liters) (cu It) 1.848 0.-1 1.84·1 0.1 1.933 3.089 0.1 3_057 0.1 3,204 3 555 0.1 3.526 01 3.705 7.620 0.3 /.514 0.3 7.903 6.32-'1 0.2 6.256 0.2 6.586 (nurnber) (n11mber) 0.998 0.007 0.990 -0.001 0_992 0.001 0.986 -0.005 0.989 -0.002 Value (in H20) 1.423 1.437 1 461 1 473 1.479 V<Hiation (in H20) -0.0313 -0.018 0.007 0.018 0.024 

-

Average Y -------> 0.991 1.455 <-------Average dH@ 

NoJe: F()! C<Jiibralion f

0

at:lor Y, I lie r<llio of the 10<-1ding of tl1e calibration Jlleter to lhe dry gas meier, 

<ICCeptable tolerance of Individual v<Jiiws from the averaoe is ·+-0 02. 

for Orifice CaiJbialiOII FddOt dl-l@, llw orifice dirferentiul pressure in inches or H20 I hal equales lo 0. 75 cfrn of air 

"' 68 F "'"' 29 92 "oepl,<b• of iodi'ji'J"l 'aloe' rwm I he "e"ge" ' 0 2 /. , / 

'-· 

1-" 

t\ ') 

(j) 

SIGNCO __ _ D'le, ___ 'ifi_'/./_!_0 s:=_ 

- 

CO

1 n1 e

1 IT

i C

-Average 

DGM D

Outlet O

(deg H) (d

549.0 549_5 

550.0 550.5 

551.0 
I 

I Tempe1ature l\f;eter Calibrations 

I 

Meter Box#: 11 

I Date: 08/04/05 

Calibrated By: RT 

Emtech Thenno I Degrees F Checker Probe Stack Oven Exit Auxiliary 

Point 1 32 30 30 30 31 31 

Point 2 212 211 211 211 211 212 I 

I Point 3 752 751 751 751 751 752 

I Emtech Thermo 

Degrees R Checker Probe Stack Oven Exit Auxiliary 

I Point 1 492 490 490 490 491 491 

Point 2 672 671 671 671 671 672 

I Point 3 1212 1211 1211 1211 1211 1212 

Percent Difference 

Probe Stack Oven Exit Auxiliary 

I 

I Point 1 0.406504 0406504 0406504 0.203252 0.203252 

Point 2 0 14881 0.14881 0.14881 0.14881 0 

I Point 3 0.082508 0.082508 0.082508 0 082508 0 

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I 1 ') ,.., ~ I 
Armstrong Environmental Inc. 

EPA Method 5 

APEX INSTRUMENTS 

511 Series Meter Box Calibration 

Post-Test Orifice Method 

English Meter Box Units, English K' Factor 

Date: ---·---------------------> 

Barometric Pressure: ----------> 

Theoretical Critical Vacuum:---> 

08/24/05 

29.65 (in Hg) 

13 99 (in. Hg) 

Vacuum should be 1 to 2 in. Hg greater than the Theoretical Critical Vacuum shown above. 

K', must be entered in English units, (ft)"3.(deg R)"O.S/((in.Hg)•(min)). 

S METER READINGS -CRITICAL ORIFICE READINGSTheoretical Critical Vacuum:---> 13.99 (in Hg) 

Volume Initial Temps. 

Total Inlet Outlet 

Final Temps. Orifice K' Orifice Actual --Ambient Temperature--

Inlet Outlet Serial# Coefficient Vacuum Initial 

(cu fl) (deg F) (deg F) 

5 003 900 89.0 

(deg F) (deg F) (number) (see above) (in Hg) (deg F) 

91.0 900 55 0.464 19.5 90.0 

3.127 90.0 90.0 91.0 91 0 55 0.464 19.5 91.0 

3 747 91.0 91 0 92 0 91.0 55 0.464 19.5 91.0 

RESULTS ..... H ................................... *'**•···· 

FICE--------

VOLUME VOLUME 

CORRECT NOMINAL 

Vcr(std) Vcr 

(liters) (cu fl) 

0.2 4.934 

0.1 0.1 

3.087 3.706 

--DRY GAS METERCALIBRATION FACTOR 

y 

Value Variation 

(number) (number) 

0.984 -0.001 0.984 -0.001 0.986 0.002 

---------ORIFICE---

CALIBRATION FACTOR 

dH@ 

Value Variation 

(in H20) (in H20) 

1464 0.0000 

1.464 -0.000 1.464 -0 000 

Final Average 

(deg F) (deg F) 

900 90.0 

91.0 910 

92.0 91.5 

Average Y -------> 0.985 1.464 <-------Average dH@ 

he reading of the calibration meter to the dry gas meter, 

 from the average is +-0.02 

orifice differential pressure in inches of H20 that equates to 0.75 cfm of air 

abl;rtolerance values from the average is +-0.2. 

-....__t,'J"{VI I Dale 6 /z. I/o s-

- - - - - - - - - - -

DGM 

Outlet 

(deg R) 

549 5 550.5 551.0 

-

CONVERSIOI\1 FACTORS 

1 mm Hg = 0.13330 kPa 

1 em "" 0.39370 inch 

1 rnm ::o 0.03937 inch 

1 cu ft = 28.32 liters 

DGM Ambient 

Overall Temp 

(deg R) (deg R) 

550.0 550.0 550.5 551.0 551,3 551.5 

co 

C'-l 

,...; 

- - -
I 

I Temperature Meter Calibrations 

I Meter Box#: 11 

Date: 08/24/05 

I Calibrated By: RT 

Emtech Thermo 

I Degrees F Checker Probe Stack Oven Exit Auxiliary 

Point 1 32 30 30 30 30 30 

I Point 2 212 211 212 211 212 211 

Point 3 752 751 751 751 751 751 

I 

I Emtech Thermo 

Degrees R Checker Probe Stack Oven Exit Auxiliary 

I Point 1 492 490 490 490 490 490 

Point 2 672 671 672 671 672 671 

I Point 3 1212 1211 1211 1211 1211 1211 

I Percent Difference 

Probe Stack Oven Exit Auxiliary 

I Poini 1 0.406504 0.406504 0.406504 0.406504 0.406504 

Point 2 0.14881 0 0.14881 0 0.14881 

I Point 3 0 082508 0 082508 0.082508 0.082508 0.082508 

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Mete( Box 1. 

Scncrl # 

!!1!!11]1 

10 

30272 

APE Anns110il\J Environrnenlallnc 

EPA Mel hod 5 

522 Series Meier Box Calibralion 

Pre-Test Orifice Mel hod 

English Meier Box Unils, English K' Faclor 

Dale:-----,.·---------

BcHornetric Pressure:--··· ----"' 

Theoretical Critical Va()lllHn ---> 

08/04/05 

29.75 (in. Hg) 

14.03 (in Hg) 

IMPORlAh F-or valid lr.J::>lrc-Jsulb, the Aclu<JI Vncuum should be 1 to 2 in. Hg greater I han tJw Theoretical Critical Vacuum shown above 

IMPORTA/\ Cliihll Codfidenl, K', must be entered in English units, 5/((in.Hg)'(min)) 11!!11!11 

DRY GAS METER READINGS ------- -------

-CRITICAl ORIFICE READINGSVolurrre Votun1e Voliune lnihal Temps. dH Final Temps. Time lllili;il Fin<il Total Inlet Outlet (in 1120) Inlet Outlet (111in) (ell II) (cult) (cu II) (deu F) (deg F) 0.24 (deg F) (deg F) 

U.49 

7.00 22,1 900 227.162 2.262 90 0 90.0 91 0 91_0 

0.9"1 10 

8.00 

00 

227.'100 231.095 3_695 91.0 91.0 93.0 92.0 

·1 .50 5.no 252_1()0 

231 ,SOO 237_712 6.212 93.0 92.0 94.0 93.0 

2_90 

256 085 3.985 94.0 94_0 95_0 94.0 fi 00 2<1,1.600 25"1.162 6_562 95.0 94_0 98.0 94_0 

................................................... RESULTS .................................................. . 

- ORY GAS METER- --------ORIFICE · 

-- DRY GAS METER -

VOLUME VOLUME VOI.UME VOLUME VOLUME 

Orifice K' Orifice Aclual 

Serial# Coeffrcient Va(:UUm 

(number) (see above) (in Hg) 

40 0.242 22.0 48 0.344 20.5 

55 0.464 19 0 

63 0.593 18.0 

73 0 824 16.0 

.... 

__ ORIFICE ---

· Alllbienl Ternperalwe -· 

Initial final Average 

(deg F) (deo f) (deo F) 

90.0 91.0 90.5 91.0 92.0 91.5 

92.0 

9•1.0 

94.0 

93_0 94.0 94.0 

92.5 

94.0 

94.0 

CALIBRATION FACTOR CORRECT CORRECTED COJ<RECT CORRECT NOMINAl CALIBRATION FACTOR y Vm(sld) Vm(sltl) Ver(shl) Vcr(sld) Ve< Value Varialion (cu II) (liters) ((:ll fl) (lilers) ((:ufj) 2.153 (nwnber) (number) 01 2. 15"1 0.1 2.256 3.519 0.1 0.997 0.002 3.489 0 1 3 667 0.992 5.908 0.2 ·0.003 5.871 0.2 6.181 0 994 1-" ·000'1 3. 78 7 0.1 3.750 0.1 3.959 6.2•16 02 0 990 -0.004 6.247 02 6.595 (.;.) 1.000 0 006 

0 Average Y -------> 0.995 

Nule: for Calibmlion Faclor Y, !lw r<llio of the reading of tile (:alibiulion meter lo !he dry gas meter, 

<l(:Gept8ble toi&IaJl(:e !!I illdividual values from the average is 1·-0.02. 

dH@ 

Value Variation 

(it1 H20) (in H20) 

1.364 -0 0363 

1.379 -0.021 

1.411 0.011 

1 421 0.02'1 

1.426 0.026 

1.400 <-------Average dH@ 

Fm Orifice Calibration Fi!dor dH@, tile orifice (flfferentiaJ pressure in i ::; of H20 thai equates to 0."/5 dm of air 

"' 

68 

F '"' lmm I he a""9" ;, +0 2. Dale. ____ (? J __ ._ 

- - 

CON

1 rnm 

1 em 

1mm 

1 Cli 

·Average Tamp

DGM DG

Outlet Ov

(deg R) (de

550 5 555'1.5 55

552 5 55554.0 55554 0 55
I 

I leG~ Perature Meter Calibrations 

I 

lv1eter Box#: 10 

I Date: 08/04/05 

Calibrated By: .RT 

I Emtech Thermo 

Degrees F Checker Probe Stack Oven Exit Auxiliary 

Point 1 32 31 31 31 31 31 I Point 2 212 211 211 211 211 211 

I Point 3 752 751 751 751 751 751 

I Emtech Thermo 

Degrees R Checker Probe Stack Oven Exit Auxiliary 

I ?oint 1 492 491 491 491 491 491 

Point 2 672 671 671 671 671 671 

I Point 3 1212 1211 1 211 1211 1211 1211 

I Percent Difference 

Probe Stack Oven Exit Auxiliary 

I Point 1 0.203252 0.203252 0.203252 0.203252 0.203252 

Point 2 0 14881 0.14881 0 14881 0.14881 0 14881 I Point 3 0.082508 0 082508 0.082508 0 082508 0.082508 

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Meter Box II 

Serial#. 

1!!!!1!11 

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10 

30272 

- - - - -

Armstrong Environmental Inc. 

EPA Method 5 

511 Series Meter Box Calibration 

Post-Test Orifice Method 

English Meter Box Units, English K' Factor 

Date:------------------------> 

Barometric Pressure: ----------> 

Theoretical Critical Vacuum:---> 

- -

08/24/05 

29.65 (in. Hg) 

13.99 (in. Hg) 

- -

IMPORT Ar-. For valid test results, the Actual Vacuum should be 1 to 2 in. Hg greater than the Theoretical Critical Vacuum shown abovo 

IMPORT AI\ The Critical Orifice Coefficient. K', must be entered in English units, (ft)"3'(deg R)h0.5/((in.Hg)"(min)). 

!!!!!!I!! 

--------------DRY GAS METER READINGS--------------- -CRITICAL ORIFICE READINGS-

- - - -

Volume Volume Volume Initial Temps. Final Temps. 

Theoretical Critical Vacuum:---> 13_gg (in. Hg) 

Orifice K' Orifice dfl Time Initial Final Total Inlet Outlet Inlet Actual --Ambient Temperature- Oul!et 

(in H20) (min) (cu ft) (cu ft) (cu ft) (deg F) (deg F) (deg F) (deg F) 0.90 6.50 <100.600 404.619 4.019 88.0 87.0 90.0 89.0 

0.90 7.00 <105.100 409.435 4.335 90.0 89.0 92.0 91.0 

0.90 g_oo •109,800 415.354 5.554 g2,0 g1_0 93.0 92.0 

'''"'''"'''''•••••••·•••••••••• .. ••• .............. RESULTS ................................................. .. 

---DRY GAS METER--· 

VOLUME VOLUME 

COR RECTI CORRECTED 

Vm(std) Vm(sld) 

(cu ft) (liters) 

3.841 0.2 

4.128 

f-"5274 

w 

0.2 

0.2 

--- ORIFICE ------

VOLUME VOLUME VOLUME 

COR RECTI COR RECTI NOMINAL 

Vcr(std) Vcr(std) Ve< 

(cu ft) (liters) (cu ft) 

3.8og 01 4.012 

4.100 0.2 4.323 

5.267 0.2 5.563 

--DRY GAS METER·-

CALIBRATION FACTOR 

y 

Value 

(number) 

0.992 

0.9g3 

0.9gg 

Variation 

(number) 

-0.003 

-0.001 

0.004 

Serial# Coefficient Vacuum Initial 

(number) (see above) (in Hg) (deg F) 

55 

55 

55 

0.464 19.5 

0.464 19.5 

0.464 19.5 

---------ORIFICE---------

CALIBRATION FACTOR 

dH@ 

Value 

(in H20) 

1.408 

1.404 

1.403 

Variation 

(in H20) 

0.0030 

-0.001 

-0.002 

g1_0 

91.0 

92.0 

Final Average 

(deg F) (deg F) 

91.0 91.0 

92.0 91.5 

g3_0 92.5 {'~ Average Y -------> 0.994 1.405 <-------Average dH@ 

Note: For Calibration FactorY, the ratio of the reading of the calibration meter to the dry gas meter, 

acceptable tolerance of individual values from the average is +-0.02. 

For Orifice Calibration Factor dH@, the orifice differential pressure in inches of H20 that equates to 0.75 cfm of air 

at 68 F and 29.g2_jn!.<b.~~g, accepta tolezance t individual values from the average is +-0.2. / ~- 7 '>/f"r/- SIGNED: 5\ a _.,_...... Date cJ ~LdS 

D

Ou
I 

I Temperature Meter Calibrations 

I Meter Box#: 10 

Date: 08/24/05 

I Calibrated By: RT 

Emtech Thermo 

I Degrees F Checker Probe Stack Oven Exit Auxiliary 

Point 1 32 31 31 31 31 31 

I Point 2 212 210 211 210 210 211 

Point 3 752 750 750 750 750 751 

I 

I Emtech Thermo 

Degrees R Checker Probe Stack Oven Exit Auxiliary 

Point 1 492 491 491 491 491 491 I Point 2 672 670 671 670 670 671 

I Point 3 1212 1210 1210 1210 1210 1211 

I Percent Difference 

Probe Stack Oven Exit Auxiliary 

Point 1 0.203252 0.203252 0.203252 0.203252 0.203252 I Point 2 0.297619 0.14881 0.297619 0.297619 0.14881 

I Point 3 0.165017 0.165017 0.165017 0.165017 0.082508 

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NOZZLE :NS?ECTION AND MEASUREMENT OATA SHEET 

?resam~l e Inspect ion 

Ja:e Mecsu~ed ---~-

re:ord 

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Presample Inspectia~ 

I here)y cer:·ify that t'ne .a~ov::: ref2r2nced nozzi e ci;Jpea.:-s to be 

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Post Samole 

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Corrrnents: 

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criteria tube/probe numb-er IJ 6 meets or exceeds all specifications 

pitat tube 

and/or 

calibration 

applicable des1gn features* and is hereby assigned a __ 

factor of 0.84. ·- ______ .c------c--,/~--__ --- #"-- - -~ -/- _/ /''' ~ _, 

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Appendix F 
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Specialty Gas Products 

Date: 6/27/2005 

Customer: Matheson- Trigas 

Description: NO 1n N2- EPA Protocol 

Cylinder No. EB0001164 

Component 

N1tnc Oxide 

Nitrogen, Balance 

Reference Standard 

Description 

GMIS 

Instrumentation 

Description 

Honba Process Analyzer 

Requested 

Concentration 

50 ppm 

Expiration date 

11/22/2006 

Model# 

CLA-51 0-NO 

3106 Pasadena Freeway 

Pasadena, Texas 77503 

!713) 534-8217 "ax!713) 5348133 

Project: 16015 

Exp. Date: 6/27/2007 

Cyl'1nder Pressure: 1900psig 

Certified 

Concentration 

50.4 ppm 

NOx: 51 ppm 

Cylinder Number 

ND22557 

Date Last Clibrated 

6/16/2005 

Accuracy 

1% 

Concentration 

99 8 PPM no 

Principle 

CHEMI 

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I Anaylsis Results: Z =zero gas, S =standard gas, X= sample gas 

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First Triad- NO 

Z1- -1.20 

S2= 994.10 

Z3= -1 10 

S1= 994.80 

Z2= -1.30 

X3= 499.80 

Average= 50.3ppm 

Curve: Y = 0. 33645 + 0. 099857'X 

X1= 498.30 

X2= 498.40 

S3= 997.40 

I Analyst~~~ ?- .. = 

Second Triad - NO 

Z1 -1.10 

S2= 998.20 

Z3= -0.80 

S1= 998.50 

Z2= -0.70 

X3= 500.80 

Average = 50.53ppm 

X1= 

X2= 

S3= 

502.80 

502.40 

994.20 

. 

~HIS STANDARD 

~ 

IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

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Specialty Gas Products 

Date: 6/27/2005 

Customer Matheson - Trig as 

Description NO in N2 - EPA Protocol 

Cylinder No EB0001156 

Component 

N1tnc Ox1de 

Nitrogen, Balance 

Reference Standard 

Description 

GMIS 

Instrumentation 

Description 

Honba Process Analyzer 

Requested 

Concentration 

25 ppm 

Expiration date 

11/22/2006 

Model# 

CLA-510-NO 

3106 Pasadena Freeway 

Pasadena, Texas 77503 

1713) 534-82'7 Faxl713) 534-3133 

Project: 16014 

Exp. Date 6/27/2007 

Cylinder Pressure: 1900psig 

Certified 

Concentration 

25.0 ppm 

NOx 25.5 ppm 

Cylinder Number 

ND22557 

Date Last Clibrated 

6/16/2005 

Accuracy 

1% 

Concentration 

99.8 PPM no 

Principle 

CHEMI 

Anaylsis Results: Z =zero gas, S =standard gas, X= sample gas 

First Triad- NO 

Z1- -1.20 

S2= 994.10 

Z3= -1.10 

S1= 994.80 

Z2= -1 30 

X3= 246.10 

Average= 24.90ppm 

Curve Y = 0.33645 + 0.099857·x 

X1= 244.50 

X2= 244.80 

53= 997.40 

Second Triad- NO 

Z1- -1.10 S1= 

S2= 998.20 Z2= 

Z3= -0.80 X3= 

Average= 25.00ppm 

998.50 

-0.70 

246.40 

X1= 247.10 

X2= 247.00 

53= 994.20 

Analys~~ --,~ 

I THIS STAN ~RD IS NIST TRACEABLE. IT WAS CERTiFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

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DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

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Specialty Gas Products 

Date: 6/27/2005 

Customer: Trigas 

Description: COm N2- EPA Protocol 

Cylinder No: EB0000761 

Component 

Carbon Monoxide 

Nitrogen, Balance 

Reference Standard 

Description 

NTRM 

Instrumentation 

Description 

Horiba Process Analyzer 

3106 Pasadena Freeway 

Pasadena, Texas 77503 

(713) 534-8217 Fax(713) 534-8133 

Requested 

Concentration 

100 ppm 

Expiration date 

5/29/2006 

Model# 

VIA-510-CO 

Project: 16018 

Exp. Date: 6/27/2008 

Cylinder Pressure: 1 900psig 

Certified 

Concentration 

99.1 ppm 

Cylinder Number 

SX1 9190 

Date Last Clibrated 

6/10/2005 

Anaylsis Results: Z =zero gas, S =standard gas, X= sample gas 

First Triad- CO 

Z1= -0.90 S1= 

S2= 204.80 Z2= 

Z3= -0.80 X3= 

Y=028607+0250309'X 

Average= 9945ppm 

204.90 

-0.80 

396 50 

X1= 

X2= 

S3= 

396.60 

396.60 

204.90 

Second Triad -CO 

Z1- -040 S1= 513.30 

S2= 513.20 Z2= -040 

Z3= -040 X3= 98520 

Y=O 031031+0.100163'X 

Average= 98.74ppm 

~· -- --~ 

I Analysf· 

/ 

~~ 

--~-

. ~-.. -··· :.:," 

~-:; __ ~ 

~ 

Accuracy 

1% 

Concentration 

994.2 ppm CO 

Principle 

NDIR 

X1= 

X2= 

S3= 

985.70 

98540 

513.20 

I 

TH!S STA~4DARD IS NIST TRACEABLE. iT 'vVAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

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Specialty Gas Products 

Date: 8/16/2004 

Customer: Matheson- Trigas 

3106 Pasadena Freeway 

Pasadena, Texas 77503 

(713) 534~8217 Fax(713) 534-8133 

ProJect: 10548 

Description: CO, 02 in N2- EPA Protocol Exp. Date: 8/162007 

Cylinder No: CC187154 

Component 

Carbon Monoxide 

Nitrogen, Balance 

Reference Standard 

Description 

GMIS 

Instrumentation 

Description 

Horiba Process Analyzer 

Requested 

Concentration 

200ppm 

Expiration date 

4/6/2006 

Model# 

VIA-510-CO 

Anaylsis Results· Z"" zero gas, S :: standard gas, X:: sample gas 

First Triad -CO 

Z1- -0.3 

S2= 993~20 

Z3= -0.30 

S1 = 993.5 

Z2= -0.30 

X3= 199.90 

Curve: Y=-0.6893+1 001139X 

Average =199.6ppm 

X1= 199.9 

X2= 200.00 

S3= 993.00 

Cylinder Pressure: 1900psig 

Certified 

Concentration 

200ppm 

Cylinder Number 

CC177636 

Date Last Clibrated 

8/6/2004 

Second Triad . CO 

Z1 -0.4 S1 = 995.5 

S2= 995~80 Z2= -0.30 

Z3= -0.30 X3= 200 60 

Average= 199 Bppm 

I 

Anaiyst: L- --~~-~:____ __ {___ I Ling Wen ...----~ 

Accuracy 

1% 

Concentration 

994.2 ppm CO 

Principle 

NDIR 

X1= 200.6 

X2= 200.60 

S3= 995.60 

THIS STANDARD IS NIST TRACEABLE IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES 

I 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

142 
MATHESON CERTIFICATE OF Ai'IALYSIS- EPA PROTOCOL MIXTURE 

TRI·GAS 

I 

Customer: MATHESON TRI-GAS - OALLAS 

•

Cylinder Number: 

Cylinder pressure: 

SX-36727 

2000 

8/7/2003 

8/7/06 

Last Analysis date: 

IExp·~ration Date· 

I Component: Propane 

Protocol· 

G1 

Reference# 

262579 

Lot# 

1 09-36-31 020 

DO NOT USE THIS CYLINDER WHEN THE 

PRESSURE FALLS BELOW 150 PSIG 

REPLICATE RESPONSES 

Date: 8/7/2003 Date: 

15.2 PPM 

15.2 PPM Certified Cone: 15.2 ± 0.15 PPM 

• 15.1 PPM 

.._____,=-. --------------------

rALANCE GAS: Air 

•

REFERENCE STANDARDS 

Component: Propane 

SRM #: SRM-1666b 

I Cylinder# Cal-0 11826 

Concentration: 9.73 ppm 

~ERTIFICATION INSTRUMENTS 

Component: Propane 

Make/Model: Varian 3800 GC I Seri2! Number: LR-92489 

Measurement Principle: TC, FlO 

Last Calibration: 8/7/2003 (_ __________________________________ _ 

I i-.Joles: 

I This certification was performed according to EPA Traceability Protocol for Assay & Certification of Gaseous 

Calibration Standards September 1997, using procedure G1 and/or G2. 

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.'"1 I f /' ~ 

fi--L J · i/> \,._.::[~' ~~-~~~----- Date ___ _,8"'-/"'8/'-"2""0.,0,.,_3 

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I Specialty Gas Products 

I Date: 6rrl2004 

Customer: Trigas 

3106 Pasadena Freeway 

Pasadena, Texas 77503 

(713) 534-8217 Fax(713) 534-8133 

I Description: Propane in Air- EPA Protocol 

Project: 9210-01 

Exp. Date: 61712007 

I 

I 

Cylinder No: SX41680 

Component 

Propane 

Air, Balance 

I Reference Standard 

Description 

NTRM I Instrumentation 

Description 

Horiba Process Analyzer 

Requested 

Concentration 

30 ppm 

Expiration date 

71212004 

Model# 

FIA-51 0 

Cylinder Pressure: 1 900psig 

Certified 

Concentration 

28.8 ppm 

Cylinder Number 

SG9183302 

Date Last Glib rated 

512412004 I Anaylsis Results: Z =zero gas, S =standard gas, X= sample gas 

I First Triad - Propane 

Z1 = 0.60 S1 = 207.90 

S2= 207.70 Z2= 0.60 

I Z3= 0.60 X3= 57.40 

Curve: Y=-0.05085+0.501149·x 

Average= 28.77pm 

I 

I . /- Analys~ 

X1= 57.60 

X2= 57.50 

S3= 208 00 

Accuracy 

1% 

Concentration 

103.6 ppm Propane 

Principle 

FIA 

// 

<HIS STANDARD IS NiST TRACEABLE. iT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. I DO NOT USE THIS STANDARD IF THE CYLINDER P?ESSURE IS LESS THAN 150 PSIG 

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Specialty Gas Products 

Date: 6{//2004 

Customer: Trigas 

3106 Pasadena Freeway 

Pasadena, Texas 77503 

(713) 534-8217 Fax(713) 534-8133 

Description· Propane in Air- EPA Protocol 

ProJect: 9211-01 

Exp. Date 6/7/2007 

Cylinder No: CC177391 

Component 

Propane 

Air, Balance 

Requested 

Concentration 

50 ppm 

Cylinder Pressure: 1 900psig 

Certified 

Concentration 

48.8 ppm 

I Reference Standard 

Description Expiration date 

7/2/2004 

Cylinder Number 

SG9183302 I 

I 

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I 

NTRM 

Instrumentation 

Description 

Horiba Process Analyzer 

Model# 

FIA-51 0 

Anaylsis Results: Z =zero gas, S =standard gas, X= sample gas 

First Triad - Propane 

Z1- 0.60 S1 ~ 207.90 

S2~ 207.70 Z2~ 0.60 

Z3~ 0.60 X3~ 97.50 

Curve: Y~-0.05085+0.501149'X 

Average~ 48.78pm 

X1 ~ 97.60 

X2~ 97.20 

S3~ 208.00 

./ ---~------ 1 // ~--z..- -~ '--------= Analyst: L------·- ____ -( ----~ 

~-- . 

Date Last Clibrated 

5/24/2004 

Accuracy 

1% 

Concentration 

103.6 ppm Propane 

Principle 

FIA 

THIS STANDARD IS NISI TRACEABLE. IT VvAS CE'RTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES I DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE iS LESS THAN 150 PSIG 

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Specialty Gas Products 

Date 7/13/2004 

Customer: Matheson-Trigas 

3106 Pasadena Freeway 

Pasadena, Texas 77503 

(713) 534-8217 Fax(713) 534-8133 

Description: S02 in N2 - EPA Protocol 

Project No· 9970 

Exp. Date: 7/13/2006 

Cylinder No CC88735 

Component 

Sulfur Dioxide 

Nitrogen, Balance 

Reference Standard 

Description 

GMIS 

• GMIS CC177157 Tracebility 

Description 

NTRM 

Instrumentation 

Description 

Horiba Process Analyzer 

Requested 

Concentration 

100ppm 

Expiration date 

1/19/2006 

Expiration date 

6/1/2006 

Model# 

VIA-51 O-S02 

Cylinder Pressure: 1900psig 

Certified 

Concentration 

101 ppm 

C)llinder Number 

CC177157 

C)llinder Number 

SG9199568 

Date Last Clibrated 

6/15/2004 

Accuracy 

1% 

Concentration 

793.8ppm S02 

Concentration 

1997ppm S02 

Principle 

NDIR 

I Anaylsis Results: Z =zero gas, S =standard gas, X= sample gas 

I 

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I 

First Triad - S02 

Z1- -0.90 S1= 791.9 

S2= 794.0 Z2= -0.70 

Z3= -0.90 X3= 99.2 

Curve Y=1.971+0.999869•X 

Average= 1 00.6ppm 

~ -- ------;o. 

/ ~--7 ---------- ~~- Analyst: / _L ' ~~ ~---------

X1= 98.7 

X2= 99.0 

S3= 792.6 

Second Triad - S02 

Z1- -0.90 S1= 794 

S2= 793.2 Z2= -0.60 

Z3= -0.60 X3= 99.30 

Average =100.9ppm 

X1= 99.0 

X2= 99.2 

S3= 793.4 

~- Ling WJJ~--- ?---

THIS STANDARD IS r'iST TRACEABLE. IT WAS CERTIFIED ,LI.CCORDING TO THE EPA PROTOCOL PROCEDURES 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

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Specialty Gas Products 

Date: 7/13/2004 

Customer: Matheson-Trig as 

3106 Pasadena Freeway 

Pasadena, Texas 77503 

(713) 534-8217 Fax(713) 534-8133 

Project No: 9969 

Description: S02 in N2 - EPA Protocol Exp. Date 7/13/2006 

Cylinder Pressure: 1900psig Cylinder No CC 177 434 

Component 

Sulfur Dioxide 

Nitrogen, Balance 

Reference Standard 

Description 

NTRM 

Instrumentation 

Description 

Horiba Process Analyzer 

Requested 

Concentration 

50 ppm 

Expiration date 

6/1/2006 

Model# 

VIA-51 0-S02 

Certified 

Concentration 

50.1 ppm 

Cylinder Number 

Sg9135833 

Date Last Clibrated 

7/7/2004 

Anaylsis Results: Z = zero gas, S = standard gas, X = sample gas 

First Triad - S02 

Z1- -1.30 S1= 999.90 

S2= 999.90 Z2= -0.70 

Z3= 0.00 X3= 503.60 

Curve: Y=0.0064+0.09986·x 

Average = 50.15ppm 

//- -- ,/ ~ _, AnalySt:.o:----'~· i c-·~-c> .------

Ling_ Werf/ c.-

X1= 502.60 

X2= 503.60 

S3= 999.90 

Second Triad - S02 

Z1- -0.80 S1= 997.90 

S2= 998.70 Z2= -0.10 

Z3= -0.20 X3= 501.60 

Average =49.98ppm 

Accuracy 

1% 

Concentration 

99.8ppm S02 

Principle 

NDIR 

X1= 500.30 

X2= 500.30 

S3= 999.30 

THIS STANDARD IS NIST TRACEABLE IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

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Appendix G 
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Summary()! 802 lnteriE>rncE>_ Check 

Plant: Dalt1ie, Dallas, TX 

Location: Plant 4 Scrubber - -

Monitor: Western Research 721-AT 

Run# 

-- --------

Monitor _802, ppm 

Modified Method 6 S02 

% Difference 

0 

0 

0 

Sheet1 

.... 

2 ' 3 ----- -----

0 

o: 

0 

Page 1 

0 -----------

0 

0 

148 
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Sulfur Dioxide Barium-Thorin Analysis 

Plant: Calt;le. Daiias, iX 

Location: Pi ant #4 Scrubber 

Date: 20 Jul 03 

Standardizati n Ba (CI02)4 

Titration (mls 

l0.5 10.5 10:5 

Blank Titration (mls) 

0.1 0.1 0.1 

Volume of Standard Sulfuric Acid (mls) 

Normality of Standard Sulfuric Acid 

Normality: 0.009524 

Run# Location Volume 

(mls) 

1 lrop l 2 50 

2 imp 1·2 

3 Imp l 2 50 

Run# Location 

1 lrop2&3 

2 Imp 2 & 3 

3 Imp 2 & 3 

Dilution 

(mls) 

1 

S02 

S02 

S02 

Avg. Titration (mls) 

10.5 

Avg. Blank (mls) 

0.1 

Aliquot 

Volume 

(mls) 

Total Grams 

0 

0 

0 

Titration 

(mls) 

0 1 0 l 

Total Mg 

0.00 

0.00 

0.00 

149 

Average 

Titration 

(mls) 

0.1 

0.1 

0 1 
I 

I 

I -

. -- -- h_ -") "{),, ~ J: - t:-~: \:. ..... i • (4. 

lc 

--~ .. !( ' ----:-~I_;-

! i : 

--~~. T-

-=~- :·rr 

• ! 

-~--·-----'-----'-

~~- i ' .. _)__ )' 

! 

1--i-i··' 

---'----.-.!. __ 

t-·- I __ .!_-

I 

' 

-_-_--~!- _L_ .L 

1-

. !. 

L 

___ i 

:59: 

.! 

I 

I ' ! 

_-_1319'_-_ 

.i 

' I -

i_ 

! 

L •... L. 

. ~--

i i ;i _\!._-,,~ 

in ! .I~· 

{!Q -- ! .. L 

_o ,c_! L' , :t ; o~ 1 

i ' 

---- ;_ __ ~ ____ _J..__ 

Jni(rt:JI'·. ( __ v ·-~-J~u .. '-) uf),: _ < ; ' ' : 

--,- . --~ ---

! 

--~------- -------~-----'----- --

LD ,:\;: q , !. r §_,JJ, I, ___ [ ____ L __ :_~- _ ' : ~ : i ! 1 1 r -~-------i.-- .~ ____ f ---~- +--

. -=c-JC5~-() _[Q_j z:):~;cr :----~-- --: I ' 

! 

-f ----! --- i __ . r---

j- . -,---

1 

• j --- ·[-··. ~-

_L 

! ' ' -;----l- +--~ I 

_J.,_ ___ __J _____ _ 

! 

. ' 

r-- 1.~_1 L 

_T ___ -~~ t, ---+-----~-- __ :,_ -·t·· ___ (_ --•---,-' ----

.. _.L. ~- I 

. _L __ : ____ /_ : : --i-----'----l--

1 I - _______ L __ --~-:- ···----

L--

j_- _I : -~_}. __ +--- ] ---~ 

-- _: ______ -~-- -~--!--

--l 

:, __ ' 

' . -~-- c-- --! 

' '150 -- L-

_; ___ _ 

i ___ ,_ --~-

' L---'---

---1--------

i L_ _ 
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EMISSION TEST SUMMARY 

PLANT • 

DATE • 

PLACE • 

RUN# • 

8a!tile. Ca: ::jS IX 

9·JUl·03 

TEST DURATION (MINUTES) • 

NOZZL[ DIAMETER (INCH.). 

METER COEFFICIENT (Y) 

PITOT COEFFICIENT (Cp) 

GAS METER VOL.(Cu.Ft.) 

BAROMETRIC PRESSURE 

FLOWS 

50 LIQUID COLLECTED (mls) 

0 S02 Sample We1ght, mg• 

0.944 

0 STATIC PRESSURE (in H20) • 

1.818 PERCENT C02 

29.5 PERCENT 02 

PERCENT CO 

SAMPLED VOLUME (STD CU.FT.)• 1.6737 

S02, ppm• 0.0000 

POINTS STACK T DELTA P SQUAR D P DELTA H METER T. 

deg F INLET 

1 0 0.00 72 

2 0 72 

3 0 72 

4 0 73 

5 0 73 

6 0 73 

7 0 73 

8 0 74 

9 0 75 

10 0 75 

11 0 75 

12 0 76 

#DIV/01 0 0000 0.0000 73.5833 

151 

METERT. 

OUTLET 

72 

72 

72 

73 

73 

73 

73 

74 

75 

75 

75 

76 

73.5833 

0 

0 

0 

0 

0 

0 

0 

73.5833 
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EMISSION TEST SUMMARY 

PL~.NT : 

DATE: 9 Jul 03 

PLACE : ?la:~t 4 Scrubber 

RUN#: 2 

TEST DURATION (MINUTES): 

NOZZLE DIAMETER (INCH.): 

METER COEFFICIENT (Y) 

PITOT COEFFICIENT (Cp) 

GAS METER VOL.(Cu. Ft) 

BAROMETRIC PRESSURE 

FLOWS 

60 LIQUID COLLECTED (mls) 

0 S02 Sample We;ght, mg: 

0 944 

0 STATIC PRESSURE (In H20): 

1 843 PERCENT C02 

29.5 PERCENT 02 

PERCENT CO 

SAMPLED VOLUME (STD CU. FT.): 1.6694 

S02, ppm: 0.0000 

POINTS STACK T. DELTA P SQUAR D P DELTA H METER T. 

deg F INLET 

1 0 0.00 82 

2 0 81 

3 0 81 

4 0 82 

5 0 82 

6 0 82 

7 0 82 

8 0 83 

9 0 83 

10 0 83 

11 0 83 

12 0 84 

#DIV/01 0 0000 0.0000 82 3333 

152 

METER T. 

OUTLET 

82 

81 

81 

82 

82 

82 

82 

83 

83 

33 

83 

34 

32 3333 82.3333 

0 

0 

0 

D 

0 

0 

0 
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EMISSION TEST SUMMARY 

PLANT • 

DATE• 

PLACE • 

RUN# • 

9-Jul 03 

Plant 4 Scrubber 

3 

TEST DURATIDN (MINUTES) • 

NOZZLE DIAMETER (INCH.) • 

METER CDEFFICI ENT (Y) 

PITDT CD EFFICIENT (Cp) 

GAS METER VDL.(Cu.Ft.) 

BAROMETRIC PRESSURE 

FLOWS 

60 LIQUID COLLECTED (mls) 

0 S02 Sample Weight. mg• 

8.944 

0 STATIC PRESSURE (in H20) • 

!.857 PERCENT C02 

29 5 PERCENT 02 

PERCENT CO 

SAMPLED VOLUME (STD CU. FT.)• 1.6818 

SD2, ppm. 0.0000 

POINTS STACK T. DELTA P SQUAR D P DELTA H METER T. 

deg F INLET 

1 0 0.00 86 

2 0 83 

3 0 82 

4 0 82 

5 0 82 

6 0 82 

7 0 82 

8 0 82 

9 0 82 

lO 0 82 

1 1 0 82 

12 0 82 

#DIV/01 0.0000 0.0000 82.4167 

153 

METER T. 

OUTLET 

86 

83 

82 

82 

82 

82 

82 

82 

82 

82 

82 

82 

82.4167 

0 

0 

0 

0 

0 

0 

0 

82.4167 
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"" , .., \ I 

. 

P L'-\....!_~ "'T _: rc)~f.L, 1 -.c f \c .. "----\! f 1 t._ '·-~ ,! I·~ , - 'I , .a .. DATe: . . . ... c> , f , 

RE?ETITIO~: l ·'' 

LOCATION (SOURCE#): f/ 

oPEMToR -r+ , · . SA-MPLE TRAIN #c: /;\: O'_s .::. 7-

!J 

' 

METER BOX#: ~ v· ,--

BAROMETRIC PRESSURE:';:J';<:c 

A.MBJENT TElvlPEMTURE: /e--

ASSUMED MOISTURE: -

PROBE LENGTH: -

NOZZLE DLJJI1ETER: --

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Box 1 Dry Gos Meter 

al#: 3909 

!I! 

Arn1slronq Environmental h1c. 

EPA Method G 

Orifice Method 

English Meter Box Units, English f<' Factm 

Dale. Bnrometdc Pressure;- ------ -> 

Theoretical Crilical VacuumJuly l 1. 2003 29.78 13.91 (in. Hg) 

JRTAf'. For valid test results, tt1e Aclll<ll Vacuum should be 1 to 2 in. Hg greater lhanl11e Theoretical Critical Vacuum shown above JRTAf'. The Crilic81 Orifice Codficier1t, 1\', rnust lle entered in English units, (ft)"J.(deg R)"0.5/((in.Hg)"(rnin)). !I! 

- - DI\Y GAS METEH READINGS-------------- -CRITICAL ORIFICE READINGSVolu111e Volume Theoretical Critical Vacuum:---> Volrune 14.05 (in. Hg) Initial Temps. Final T elllps. Orifice K' Olifice Actual --Ambient Temperature-- JH Ti111e llliti<ll i"il1ill Total Inlet Outlet 20) (ITllll) (cu ft) Inlet OLillet Serial# Coefficient Vacuum Initial (cu It) (cu H) (deg F) (deg F) (deg F) (deg F) (number) (see above) (in Hg) (deg F) 0.00 5.00 16.716 16_91/ 0.201 87.0 87.0 87.0 87.0 16907 0.029 230 87.0 

000 

0.00 

5.00 

5.00 

17.1 

IG 917 

18 17.320 

17.118 0.20 I 87.0 87.0 87.0 87.0 16907 0.029 23.0 87.0 0.202 87 0 87.0 87.0 87.0 16907 0.029 19.5 87.0 

......................... , .................... HCSUL TS ..................... ............ ,.,, .. .. '* 

RY GAS MElER ---

UME VOLUME 

RECT CORRCCTEIJ 

n(std) V111(std) 

(cu rt) (liters) 

o.19J o_o 

0.193 0.0 

0.194 0.0 

-ORIFICE------

VOLUMt:: VOLUME VOLUME 

CORr-\EC r CORf\ECT NOMINAL 

Vcr(sld) Vcr(std) Vcr 

(cu ft) (liters) (curt) 

0. 18?. 0.0 0.190 

0.182 0.0 0.190 

0.182 0.0 0.190 

Ave1 C"lQe Y - -----> 

--DRY GAS METER--

CALIIJRATION FACTOR 

y 

Value 

(number) 

0.945 0.945 0.941 

Variation 

(number) 

0.002 

0.002 

-0.003 

· OR!f'ICF --- --·· 

CALIBRATION FACTOR 

dH@ 

Value 

(in 1-120) 

0.000 0.000 

0.000 

Variation 

(in H20) 

00000 

0.000 

0.000 

Final 

(deg F) 

87.0 87.0 87.0 

f-" 

CJl 

"">.1 

0.944 0.000 <--- ---Average dH@ 

For· Calibrati011 FactorY, l!1e IClliO of the reading of the c<:rlibralion meier to the dry gas meter, 

lcceptable tolerance of individual values frorn tile average is +-0.02. 

or Oilflce Calrbrat1on F8clor r1H@, tile orrf1ce d!ffelen.!J.al...-p;;}sure m rnches of H20 that equates !o 0 75 cfm uf a1r 

11 68 F and 29 92 1nclles off lg, tdler<mceor rr Nld;zal v lues from lhe average rs +-0 2 / 6 

A' / (/ --;; , -·-· SIGNED / ' :;" Date I /I 0 ) 

,, ... ,/ 

/ """ 

Average 

(deg F) 

87.0 

87.0 

87.0 

-

DGM 

Outlet 

(deg 

547547547
- - - - - - - - - - - - - - - 

APEX INSTRUMENTS VUA ORIFICE ADAPTER CALIBRATION 

--1 

WTM Moclcl NLnuber l 1\L 11 

Condlllons 

!Time 07110103 16:30 

_____ l'. -· 1G907 P<essu•e .] ____ __ 

______ 

353.5 

Technlciarl RM 

'n,., h', I" ICnglisll unils, 

'Th, Crilrcal Oril1ce I<' '"Mel ric u01ils (l'l<'")l(mmllg'min) NOTE· VOLUME IN LITERS 

----------

Wt'l Test Meier 

-----

""" ,.;;;;- Volumr VoiUhle Volume Tempera tum 

lniliJI Final To\31 nnat 

((-)) (V.,.;) (V,.,) (Vm) (t,.,,) 

I : 111"1 L L L 'C •c H-03 G 306.025 312.500 6.475 30 30 6 312.500 310.960 6.460 30 30 

·----· 

6 318.%0 325.420 6.460 30 30 

I ucJ!Ify 1111\ nr•l'l" A.'--__"-r:_-(/1'::._0..:.7__ tested rn occortlance wdh \he US EPA Me\l1od 5 standards 

lhP Col'e ol l•llr. 40 60 Appemhx A Mblhod S, Item 7 2 

S1p,na\\ne ',.//, ___ _ 

c.n 

co 

(/ 

mm Hg 

Arnb Temp 

Initial 

\1..,>'(1)) 

--- "c 

29 

29 29 

'"'""'c""'""""' 

• I 

Sid Temp 

«, 0.386 I 

I 

AmbTemp Coef!lclenl 

Vacuum Metric Unl1s E

K' 

•c fllrll llg see above' 

29 597 0.0239 

29 610 0.0233 

30 6<0 0.0230 

nonA 

---7' --------------------------- . - ----- -

•[quatmn to Calculate Standardized Flowrate 

Pressure and Absolu

lemperature Condtttuns: Pbor & Tamb(ab•J): 

* Pb,.IT,mb(•b,,U

2 
I 

I 

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--· ' -------~ ' ' 

'-

~--_:__--~--~-- ' 

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!____ _ __ L___ '-----l---

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Sheet1 

Summary of Sulfur Dioxide Analyzer Calibrations and Bias 

Plant: Daltile 

Source: Plant 4 Scrubber 

Date: 7/9/03 

Run #1 

Run #2 

Run #3 

Analyzer Calibratrion Data 

Cylinder Analyzer Absolute % Span 

Value Response Difference 

Zero Gas 

Mid Range 

High Range 

0 0.15 0.15 0.25 

25.7 25.7 0 0 

50.7 50.65 -0.05 -0 08333 

System Calibration Bias and Drift Data 

Analyzer Initial Values Final Values 

Calibration System System System System 

Response Calibration Calibration Calibration Calibration 

Response Bias Response Bias 

Zero Gas 0.15 0.18 0.005 0.23 0.133333 

Upscale 25.7 24.85 -0.14167 23.53 -3.61667 

Average S02 Concentration: 0.17 

Corrected S02 Concentration: -0 0375 

(Equation 6C-1) 

Zero Gas 0.15 0.23 0 013333 -0.13 -046667 

Upscale 25.7 23.53 -0.36167 23.9 -3 

Average S02 Concentration: -0.13 

Corrected S02 Concentration: -0.19548 

(Equation 6C-1) 

Zero Gas 0.15 -0.13 -0.04667 -0.05 -0.33333 

Upscale 25.7 23.9 -0.3 23.5 -3 66667 

Average S02 Concentration: -0.1 

Corrected S02 Concentration: -00108 

(Equation 6C-1) 

Drift 

0 083333 

-2.2 

-0.6 

0.616667 

0 133333 

-0 66667 

Page 1 160 

Average 

Calibration 

Values 

0.205 

24.19 

0.05 

23.715 

-0.09 

23.7 
I 

7/HJ·'G3 C::aiibrcticns 

I 

Date:Time co S02 

I mm--ddiYJ' :Oh:r:1rr::ss :)pr' ;Jb~ 

Q7iQ9r'03 09:32:3~ c i 0.2 

07109}03 09:33:45 0.1 0.2 :.>-'·o r-;2 

07/09/03 09:33:55 0.0 0.1 

I 07/09/03 09:34:05 0.1 0.1 

07/09/03 09.34:15 0.1 30.2 

07/09/03 09:34:25 0.1 35.5 

07/09/03 09:34:35 0.1 43.2 

07/09/03 09:34:45 0.0 47.1 

I 07/09/03 09:34:55 ·0.3 47.8 

07/09/03 09:35:05 ~0.3 48.3 

07/09/03 09:35:15 -0.4 48.8 

07/09103 09:35:25 -0.3 49.1 

I 07/09/03 09.35:35 -0.4 49.4 

07/09/03 09:35:45 -0.4 49.6 

07/09/03 09:35:55 -0.2 49.7 

07/09/03 09:35:05 -0.3 49.9 

07/09/03 09:36:15 -0.2 50.1 

I 07/09/03 09:36:25 -0.2 50.1 

07/09/03 09:36:35 -0.2 50.1 

07/09/03 09:36:45 -0.2 50.2 

07/09/03 09:36:55 -0.1 50.3 

07/09/03 09:37:05 -0.1 50.5 

I 07/09/03 09:37:15 -0.1 50.4 

07109/03 09:37:25 -0.1 50.6 

07/09/03 09:37:35 -0.1 "'·6 

07/09/03 09:37:45 -0.2 50.6 

I 07/09/03 09:37:55 -0.3 50.7 50.7 ppm S02 

07/09/03 09:38:05 -0.2 50.7 

07/09/03 09.38:15 -0.3 50.6 

07/09/03 09:38:25 -0.3 50.7 

I 07/09/03 09:38:35 -0.3 50.a 

07/09/03 09:38:45 -0.1 50.0 

07/09/03 09:38:55 -0.2 47.9 

07/09/03 09:39:05 0.0 43.5 

07/09/03 09:39:15 00 37.7 

I 07/09/03 09:39:25 0.0 31.6 

07/09/03 09:39:35 0.0 26.4 

07/09/03 09:39:45 0.1 22.5 

07/09/03 09:39:55 O.l L9.5 

07109.103 09:40:05 0.1 17.0 

I 07/09/03 09:40:15 -0.1 15.5 

07/09/03 09:40:25 ·0.1 15.0 

07/09/03 09:40:35 -0.1 15.1 

07/09/03 09:40:45 -0.2 15.7 

I 07/09/03 09"40:55 0.0 16.6 

07/09/03 09:41:05 -0.1 17.5 

07/09/03 09:41:15 -0.2 184 

07/09/03 09:41:25 -0.1 19.3 

07/09/03 09:41:35 -0.2 20.2 

I 07/09/03 09:~1 :45 ·0.1 21.0 

07/09/03 09:41:55 -0.3 21.4 

07/09103 09:42:05 -0.2 22.0 

07/09/03 09:42:15 -0.2 22.5 

07/09/03 09:42:25 -0.2 23.1 

I 07/09/03 09:~2:35 -0 2 23.6 

07/09/03 09"42:45 -0.1 24.0 

07/09/03 09:42:55 00 24.3 

07/09/03 09"43:05 0.1 24.5 

07/09/03 09.~3 15 0.1 24.7 

I 07/09103 09 ~3:25 0.1 24.8 

07/09/03 09:43:35 0.2 24.9 

07/09/03 09:43:45 0.3 25.0 

C//09/03 09:~3:55 0.2 25.2 

I 07/09/03 09:44:05 00 25.3 

07/09103 09:44:15 0."1 25.4 

07/09/03 09:44:25 'J.2 25.5 

07/09/03 09:44:35 0.1 25.6 

C.7/G9:'03 09;44:45 D.2 25.7 

I 07/09/03 09:44:55 0.2 25.7 25 7 tJPrn S02 

07i09f03 09:45:05 0.2 25.7 

I Page 1 161 
I 

iii CoCi3 Caiibrai.ions 

I 

07/09/03 09:45:15 0.2 25.7 

I 81'09.'03 J9:45:25 ]_3 25.7 

07109/03 09:45:35 0.3 25.6 

07/0S/03 09:45:45 0.2 25.5 

07/09/03 09:45:55 D.2 25.6 

07/09103 09:46:05 0.2 25.6 

I 07/09!03 09:46:15 0.2 25.5 

07109!03 09-46:25 0.1 25.5 

07/09/03 09.46:35 00 252 

07/09/03 09:46:45 0.1 24.6 

I 07/09/03 09:46:55 0.2 23.2 

07/09/03 09:47:05 0.1 21.3 

07/09/03 09:47:15 0.3 19.3 

07109/03 09:47.25 0.3 17.5 

07109103 09:47:35 0.3 15.8 

I 07!09103 09:47:45 0.3 14.3 

07/09/03 09:47:55 0.2 12.9 

07/09103 09:48:05 0.3 11 _s 

07/09/03 09:48:15 0.3 10.5 

07/09/03 09:48:25 0.3 9.6 

I 07/09/03 09:48:35 0.2 8.7 

07/09!03 09:48:45 0.3 7.8 

07/09/03 09:48:55 0.2 7.2 

07/09/03 09:49:05 0.2 6.8 

07/09/03 09:49·15 0.2 6.3 

I 07/09/03 09:49:25 0.2 5.8 

07109/03 09:49:35 0.2 5.3 

07/09/03 09:49:45 0.2 4.9 

07/09/03 09:49;55 0.2 4.5 

I 07109!03 09:50:05 0.1 4.1 

07/09/03 09:50:15 0.1 3.8 

07/09/03 09:50:25 0.2 3.6 

07/09103 09:50:35 00 3.3 

07/09/03 09:50:45 0.0 3_1 

I 07109/03 09:50:55 0.1 3.0 

07!09/03 09:51:05 0.1 2.9 

07/09/03 09:51:15 0.0 2.8 

07/09/03 09:51:25 0.2 2.7 

07/09103 09:51:35 0.0 2.3 

I 07/09/03 09:51:45 0.1 2.1 

07/09/03 09:51:55 0.1 2.0 

07109103 09:52:05 0.1 1.9 

07/09/03 09:52:15 0.1 1.9 

I 07/09/03 09:52:25 0.1 1.8 

07/09103 09:52:35 0.2 1.7 

07/09/03 09:52:<15 0.3 1.6 

07/09/03 09:52:55 0.3 1.5 

07109/03 09:53:05 0.3 14 

I 07109103 09:53:15 0.3 14 

07/09!03 09:53:25 0.2 1.3 

07/09/03 09:53:35 0.3 1.2 

07/09/03 09:53:<15 0.2 1.1 

:J7/09/03 09:53:55 0.2 1.2 

I Oi/09103 09:54:05 0.2 1.2 

07109/03 09:54:15 0.2 1.1 

07/09/03 09:54:25 0.1 1.0 

07109103 09:54:35 0.1 0.9 

07/09/03 09:54:45 00 0.5 

I 07/09/03 09.54:55 0.0 0.3 

07109103 09:55:05 0.0 0.2 

07/09,103 09:55:15 -C.1 0.2 Zero Bias 

07109103 09:55:25 00 0.2 

I 07i09/03 09:55:35 0 0 0.1 

07/09/03 09_55:45 -0.1 1.8 

07/09..'03 09:55:55 0.0 3.1 

87/09.'03 89:56:05 -C.i 4.7 

I 07/09.103 09:56:15 -0.2 6.7 

07/09/03 09:56:25 -0_1 5.7 

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07/09/03 09:59:55 -0.2 24.5 

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Stop Run #1 0.17 

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07/09/03 11:33:05 -0.3 17.5 

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I 07109/0311:45:15 34.5 4.0 

0/109!03 '! '1 :45:25 34.9 3.S· 

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I 07/09/03 1 ~ .46:05 34.5 3.3 

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I 07/09/03 11:46:55 34.1 2.6 

07/09/03 t 1 :47:05 34.0 2.4 

07109/03 11:47:15 33.5 2.3 

07109/0311:47:25 33.3 2.1 

I 07/09/:13 11·47:35 33.4 2.0 

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07/09/0311:47:55 33.8 1.8 

07/09/03 11:48:05 34.6 1.8 

07109/0311:48:15 34.9 1.6 

I 07/09/03 11:48:25 35.5 1.5 

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07109/03 '11 :48:55 37.4 14 

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I 07/09/03 11:49:15 42.6 1.2 

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07/09/03 11:49:45 46.2 1.0 

I 07/09.10311:49:55 47.2 0.8 

Start Run #2 

07/09/03 11·.50:05 47.8 0.8 

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I 07/09/03 11:50:25 47.0 0.7 

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I 07/09/03 11:51:15 32.5 0.3 

07/09/03 11:51:25 28.4 02 

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I 07/09/0311:52:05 20.6 0.0 

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07109103 12:'02:05 17_1 ·0.2 

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I 07/09103 '12:10·.25 18.5 O.C 

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Customer: 

MATHESON 

TRI·GAS 

MATHESON TRI·GAS ·IRVING 

Cylinder Number; 

Cyli~der pressure: 

SX-32146 

2000 

4-17-2003 

10/17/03 

Last Analysis date; 

Expiration Date: 

Component : Sulfur Dioxide 

Certified Cone: 25.7 ± 0.2 PPM 

BALANCE GAS Nitrogen 

REFERENCE STANDARDS 

Component Sulfur Dioxide 

SRM # SRM-.1693a 

Cylinder#: CAL-01 0596 

Concentration: 49.9 ppm 

I CERTIFICATION INSTRUMENTS .· 

Component: Sulfur Dioxide 

I 

Make/Model: Nicolet 550 

Serial Numbec: ACN-9402192 

Measurement Principle: FTIR 

r;J~,:·~-. ;:..,, __ . I' ,, 

I 

I Protocol 

G1 

87 

Reference# Lot ¢= 

249290 109-36-28491 

,98NQ,ic0JsEJ(1!S,9YLI~DERW(-1Et(l)J-iE ·. 

c ''C.~f'E.~~U.REf;Abli;:>;BECOW<l50P?JG· · :· · 

REPLICATE RESPONSES 

Date: 4-10-2003 Date: 4-17-2003 

25.6 PPM 25.9 PPM 

25.5 PPM 25.4 PPM 

25.5 PPM 25.8 PPM 

Last Calibration· 4-3-2003 

1~----------------------------------

I ~Jote.sI This certification was performed according to EPA Traceability Protocol for Assay & Certification o"f Gaseous 

Calioration Standards Sep~ember 1997, us1ng procedure G1 and/or G2. 

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~AIR LIQUIDE I I . .. CERTIFICATE of ANALYSIS 

I [li~:~f~~~~~:~;o~~~~~,'~='-'-----~r~~~~~-~~~.~:te?\~~:~u"~~:~,·~,.:---'-n_t_e_rf_e~:~:~~~~su~::~~~=m~~~~~~~:~m-M __ bu_~'_t:i_·_c_o_m_~n~f~f~,:arol Gases 

I _o9/03/02 o9to2/04 1 

jCustomer: P.O. Number: i'Joies: 

!Armstrong 

il~~-~~;~::;~~'~i:~:i~ ;;,r;; ... • REEERENCESTANDARD 

IF.-J~~~~:'['t -~F: ~~,~~:~:;~~~:-i~c,~~-~~u~--~~~,~~:~~'~;'~~-~,)~-~\~-~~-~~,:~N~t~s~,~~~~\;::;:~1~=,_ G~~= 1#~ 5 

I 

tra-::eability are in compliance with 

C PA-500/R-971123 

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Model Number: 

Serial Number: 

Analytical Principle 

MPC Calibrated: 

Component 1 

Suli'Jr D1oxicie 

fl 

A~alyst: 

I 11.!25 .~ai;mont .Parkv-1,;y, Lc Porte. Texas 77571 S')JJ 

Pilor:e: 128~) <F4-C.4QC· Fax: (23J) .0:74-St:'S 

I 

REQUESTED 

f~i{~~~d~tl~_ri: 50 ppr:J 

Serial Number 

Analytical Principle: 

MPC Calibrated: 

0.09 

51 12 

I , I 

-0.1 0 

50.87 

1:// / v 

! -~ 

187 

:~~SAY• 

C_?_~~ntr.atf?·~-

so 7 ::o.9 pp:T, 
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fArmstrong I Environmental, " Inc .. 

RESuME OF 

EDUCATION 

Thomas Armstrong 

College ofDupage 

Glen Ellyn, Illinois 

WORK EXPERIENCE 

2/91 - Present President 

Armstrong Environmental, Inc. 

Dallas, TX 

4/84 - 2/91 Vice-President 

Turner Engineering, Inc. 

Dallas, TX 

1976- 1984 Project Manager 

The Almega Corporation 

Bensenville, I!linocs 

1975- 1976 Environn1ental SpeciaEst 

Particle Data Labs, Ltd 

Elmhurst, Illinois 

Mr .. t\rmstrong has 15 years experience in performing field and laboratory analysis of air 

pollutants !'vir Armstrong has tested for air pollutants in a variety of industries, including 

chemical, steel) food) power generation, pharmaceutical; ceramics, petrocbemica1 and 

cemer1t Mr Armstrong has performed ambient and stack tests for particulate, SOx, NOx, 

h:-)"d:-o:::arbo71S, TRS and o:hers using vinually all cune:1t test methods and pros~dures. 

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fAcmstr-ong 

~ Environmental, Inc* 

(2" L') 63" -8S2" ==-:::x (2~ 4) 905·0534 

RESTJME OF 

EDUCATION 

Richard Taylor 

Southwest Texas State University 

BS -Environmental Studies 

San Marcos, TX 

WORK EXPERIENCE 

2/91 - Present 

4/88- 2/91 

Project Manager 

Armstrong Environmental, Inc. 

Dallas, TX 

Project Manager 

Turner Engineering, Inc. 

Dallas, TX 

Mr. Taylor has widespread technical experience sampling for hydrocarbons, carbon 

monoxide, nitrogen oxides, sulfur oxides, particulate matter, TRS, acids, oxygen, carbon 

dioxide, metals, fluorides, chlorides among other compounds. He has performed emission 

testing on boilers, scrubbers, baghouses, incinerators, kilns, tank vents and various other 

processes. He specializes in gas chromatography, monitor certification and efficiency 

testing. 1v1i. Taylor communicates effectively \vith plant supen:isors and state inspectors. 

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,4=Armstrong 

1 1 Environmental, Inc .. 7715 Sove:-eig:"'. Rovi • ·Ja!le.s, IX 752L7 • (2",4; 631.ClC21 • i=ax (2"L; 905-D63L • E-nail Arn:st@.lx_netcorr COrT 

RESUME OF: 

EDUCA TIO:\': 

Dan Barrera 

Houston Community College 

1983- 1987 

Houston, TX 

WORK EXPERIENCE: 

1!101 To Present 

8/97- 11/01 

10/91- 8/97 

4/87 - I 1/91 

1984- 1997 

1983-1984 

I 976 - 1982 

Stack Tester 

Armstrong Environmental, Inc 

Beer Store Manager 

Grand Prairie, TX 

Stack Tester 

Armstrong Environmental, Inc 

Computer Operator 

Alexanders, Inc. 

New York, NY 

Laser Printer Operator 

Compass Micromation, Inc 

Houston, TX 

Microfilm Production Manager 

AJlacomp 

Houston, TX 

Production Supervisor 

US Data Corporation 

Dallas, TX 

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, , • ~ • lfllll!tl 111 - llfl'JIIIli 1\ r . ~ ,.. I ~ N ~ 

Vl~ltsLt: t:lvii::S::S U :::S 

EVALUATOR 

This is to certify that 

met the specifications of Federal Reference Method 9 

and qualified as a visible emissions evaluator. 

Maximum deviation on white and black smoke did not 

exceed 7.5% opociiy and no single error exceeding 

l 5% opociiy was incurred during the certification test 

conducted bv Eastern Technical Associates of Roleioh, . '--' 

North Carolina. This certificate is valid for six months 

from dote of issue. 

326861 

Pres!dent 

191