# I

I I I I I I I I I I I I I I I I I I Exhaust Emissions Sampling 

# Daltile, Conroe, TX Kiln Scrubber Inlet and Exhaust August 23, 2005 TCEQ Permit No. 21283 

# Armstrong Environmental, Inc. Project W-2471-05

Report Prepared For: Bob Hurt

Daltile 7834 C.F. Hawn Freeway Dallas, TX 75217

Report Prepared August 26, 2005 By: Armstrong Environmental, Inc. 7715 Sovereign Row Dallas, Texas 75247 (214) 631-0021

# I

I I I I I I I I I I I I I I I I I I I. 

# Introduction

II. Summary

III. Procedures

IV. Appendices 

# TABLE OF CONTENTS

A. Calculation Summaries

B. Continuous Emissions Monitor Summaries

C. Analytical Summaries

D. Field Data Sheets

E. Equipment Calibrations

F. Standard Gas Certifications

G. S02 Interference Check

H. Resumes Page

I



# 2- 5

6- II



# 12- 17

18- 51

52- 114

115-125

126- 138

139- 147

148-187

188-191

# I

I I I I I I I 

# I I I I I I I I I I I I. 

# INTRODUCTION

A series of tests was performed on the inlet and exhaust ducts associated with the Kiln Scrubber (EPN 29) at the Daltile facility in Conroe, TX on August 23, 2005.

The purpose of this test series was to determine the exhaust emission rate of Particulate, CO, NOx, VOC, S02, HF, HCJ, 

# and Opacity, and the removal efficiency ofHF and HCl
as required by the Special Condition 13 of TCEQ Permit 21283. Testing followed procedures detailed in Title 40: Code of Federal Regulations ( 40:CFR). Sampling was performed by Richard Taylor, Dan Barrera and Tom Armstrong of Armstrong Environmental, Inc. using two Apex Method 5 sampling trains, an EcoPhysics 70S continuous NOx analyzer, a Fuji 3300 continuous CO analyzer, a Western Research 721-AT continuous S02 analyzer, and a ThermoEnvironmental 51 continuous FID analyzer.

Present during the test series was Cedric Flemming and Thomas J. 

# Bill of TCEQ.

Three one hour test repetitions were performed, commencing at 12:05 PM and ending at 3:15PM.

om Armstrong President

l

# I

I I I I I I I 

# I I 

# I I I I I I 

# I I I II. SUMMARY

A series of tests was performed on the inlet and exhaust ducts associated with the Kiln Scrubber (EPN 29) at the Daltile facility in Conroe, TX on August 23, 2005.
Sampling was performed following procedures detailed in Title 40: Code of Federal Regulations.

Results of this test series are summarized in Tables I & 

# 2.

Results indicate the following emission rates:



# Run# 1 

# 2 

# 3 Averae;e Exhaust PM, lbs/hr 

# 3.186 2.793 2.295 2.758 Permit Allowable, 

# 4.43 4.43 4.43 4.43 lbs!hr Exhaust CO, lbs!hr 

# 7.332 8.151 8.603 8.029 Permit Allowable, 

# 9.59 9.59 9.59 9.59 lbs!hr Exhaust NOx, 

# 3.319 3.175 3.025 3.173 lbs/hr Permit Allowable, 

# 1.72 1.72 1.72 1.72 lbs!hr Exhaust VOC as 

# 0.664 0.695 0.765 0.708

C3H8, lbs!hr Permit Allowable, 

# 0.42 0.42 0.42 0.42 lbs/hr Exhaust S02, 

# 0.197 0.080 0.11 7 0.131 lbs!hr Permit Allowable, 

# 9.67 9.67 9.67 9.67 lbslhr Inlet HF, lbslhr 

# 5.704 6.732 5.135 5.857 Exhaust HF, lbs!hr 

# 0.0155 0.0128 0.0163 0.0!49 Permit Allowable, 

# 0.56 0.56 0.56 0.56 lbslhr Removal 

# 99.73 99.81 99.68 99.75 Efficiencv, % Permit Allowable, 

### % 

# 95 95 95 95

Inlet HCl, lbs!hr 

# 10.028 I 0.955 9.076 I 0.020

Exhaust HCI, 

# 0.0200 0.0240 0.0271 0.0237 !bs/hr Pemlit Allowable, 

# 0.41 0.41 0.41 0.41 !bs!hr Removal 

# 99.80 99.78 99.70 99.76 Efficiency, 

## % Permit Allowable,% 

# 95 95 95 95

2

# I

I I I I I I I I I I I I I I I I 

# I I Results indicate this source to be in compliance with the emission requirements of Permit 21283 with the exception ofNOx and VOC.

3

# I

I I I I I I I I I I I I I I I I I I SUMMARY OF EMISSIONS TEST DATA



## Table: 1 Plant : Daltile, Conroe, TX Location : Scrubber Inlet Operator : T. Armstrong, D. Barrera Test Date : 23·Aug·05 Repetition : 1 2

STACK GAS 

## Temperature, F 379.3 368.4 Velocity, fps 46.71 47.08 Volume Flow, acfm 35220.2 35496.5 scfm 19816.5 20074.8 scfh 1188989 1204489 Moisture, % 7 92% 865% C02,% 2.00 2.00 02,% 18.00 18.00

SAMPLE 

## Start Time, hrs:min 9:30AM 11:45 AM Finish Time, hrs:min 10:40 AM 12:56 PM Sample Volume, set 36.106 36.101 lsokinetic Ratio,% 102.5384 101.2037

HYDROGEN FLUORIDE 

## Sample Weight, mg 78.55 91.51 Concentration, ppm 92.3907 107.6506 Emissions, lbs/hr 5 70361 6. 7.32291

HYDROGEN CHLORIDE 

## Sample Weight, mg 138.11 148.91 Concentration, ppm 89.01!13 95.98621 Emissions, lbs/hr 

# )0.02833 10.95515



# 4 3

367.8 46.63 35156.5 19999.2 ll99953 820%

2.00 18.00

1:35 PM 2:44PM

35.604 100.1869

69.10 82.42318 5.135199

122.13 79.82351 9.076149

# I

I I I I I I I I I 

# I I I I I I I I 

# I SUMMARY OF EMISSIONS TEST DATA



### Table : 2 Plant : Daltile, Conroe, TX Location : Kiln Scrubber Exhaust Operator: R. Taylor, T Armstrong Test Date : 23-Aug-05 Repetition :

STACK GAS 

### Temperature, F Velocity, fps Volume Flow, acfm

Moisture, 

## % C02,% 02,% Opacity, 

## %

SAMPLE 

### scfm seth

Start Time, hrs:min Finish Time, hrs:m1n Sample Volume, scf lsokinetic Ratio,%

PARTICULATE 

### Front Half

**;~** 

### Sample Weight, mg Concentration, gr/scf Emiss·lons, lbs/hr

Back Half Sample Weight, mg Concentration, gr/scf Emissions, lbs/hr

Total Particulate, lbs/hr

CARBON MONOXIDE 

### Concentration, ppm Emissions, lbs/hr

NITROGEN OXIDE AS N02 

### Concentration, ppm Emss1ons, lbs/hr

VOC AS C3H8 

### Concentration, ppm as C3H8, WET Concentration, ppm as C3H8, DRY Emissions as C3H8, lbs/hr Emissions as Carbon, lbs/hr

SULFUR DIOXIDE 

### Concentration, ppm Emissions, lbs/hr

HYDROGEN FLUORIDE 

### Sample We1ght, mg Concentration, ppm Emissions, lbs/hr

HYDROGEN CHLORIDE 

### Sample Weight, mg Concentration, ppm Em1ss1ons, lbs/hr 

### 138.0 29.41 28065.5 20407.1 1224428

17.02% ),50 18.50 0.00

9:30AM 10:35 AM

4!.328 100.9787

47.88 0.017876 3.127912

0.89 0.000332 0.058142

3.186054

82.38 7.332075

22.7 3.31918

3.94 4.748188 0.664091 0.543347

0.969 0.197!29

0.237 0.243541 0.015483

0.307 Q, 

### 172862 0.020056 2



### 137,8 30.30 28909.6 20973.3 1258397

17.24% ),50 18.50 0.00

1!:45 AM 12:50 PM

42.735 10),599

39.28 0.014182 2.550425

3.74 0.00135 0.242836

2 79326

89.11 8.151096



### 2U3 3 17533

4.00 4.833125 0.694724 0 568411

0.383 0.080077

0.197 0.19577 

### 0.012791

0.369 0.200929 0.023959



## 5 3



### 137,2 30.25 28862.9 211730 1270380

16.40% ),50 18.50 0.00

!35 PM 

### 2 40 PM 42.679 100.5079

34.13 0.012339 2.240091

0.84 0.000304 0.055133

2.295223

93.16 8.602703



### 19.94 3 025035

4.41 5.275258 0,765498 0626316

0.552 0.1165ll

0.248 0.246776 0.016277

0.413 0.225185 0 027!07

# I

I I I I I I I I I I I I I I I I I I III. 

# PROCEDURES

The procedure for emissions sampling followed USEPA test methods as detailed in Title 40: Code of Federal Regulations. The following methods were used:

Method I



# 2

3



# 5

6C

7E



# 9

10

25A

26A Title Sample and Velocity Traverses for Stationary Sources

Determination of Stack Gas Velocity and Volumetric Flow Rate (TypeS Pitot Tube)

Gas Analysis for the Determination of Dry Molecular Weight

Determination of Particulate Emissions from Stationary Sources

Determination of Sulfur Dioxide Emissions from Stationary Sources (Instrumental Analyzer Procedure)

Determination of Nitrogen Oxides Emissions from Stationary Sources (Instrumental Analyzer Procedure)

Visual Determination of the Opacity of Emissions from Stationary Sources

Determination of Carbon Monoxide Emissions from Stationary Sources

Determination of Total Gaseous Organic Concentration using a Flame Ionization Analyzer

Determination of Hydrogen Halides and Halogens Emissions from Stationary Sources

02 and C02 were determined using PyRite Analyzers. A single grab sample was taken
on the inlet location during each run. An integrated bag sample was taken on the exhaust via a peristaltic pump from the CEMS pump for each run (the pump was turned off during port changes).

PM. HF and HCl sampling was performed on the scrubber exhaust for 2.5 minutes at each of 24 points, 12 points per traverse, making a total run duration of 60 minutes. A schematic ofthe sampling location is shown in Figure 2. The sampling train was configured as follows:

Glass Sampling Nozzle Heated Glass Lined Probe Heated teflon filter

6

# I

I I I I I I I I I I I I I I I I I I lmpinger #1

- 100 mls H20 Impinger #2

- I 00 mls 0.1 N H2S04 Impinger #3

- I 00 mls 0.1 N H2S04 lmpinger #4

- Empty lmpinger #5

- 200 grams silica Gel Analysis for PM was performed on the probe wash, filter, and solution from the first impinger. HF and HCl analysis was performed on an aliquot from the first impinger, and the solution from the 2nd and 3rd impingers. Analysis was performed using a Dwnex LC20 IC/HPLC.

HF sampling was performed on the scrubber inlet for 4 minutes at each of 16 points, 8 points per traverse, making a total run duration of64 minutes. A schematic of the inlet sampling location is shown in Figure 1. The sampling train was configured as follows:

Glass Sampling Nozzle Heated Teflon Lined Probe Heated Flexible Teflon Sample line Heated Teflon Filter Impinger #I

- I 00 mls 0.1 N H2S04 lmpinger #2- I 00 mls 0.1 N H2S04 lmpinger #3

- Empty Impinger #4- 200 grams silica gel

HF and HCl analysis was performed on the solutions from the 1st and 2nd impingers.

Continuous emission monitors were operated according to the following parameters:

Component Monitor Actual Scale

. Calculation Standards Scale 

# co Fuji 3300 SN 

# 0 -500 0-200 99J ppm, 200 MC0303 ppmCOinN2 EPA Protocol I 

# NOx EcoPhysics 70S 

# 0- 100 0- 60 25.5 ppm, 51 ppm SN 8350095 NOx mN2 EPA Protocol 1 

# voc TECO 51 

# 0- 100 0- 60 15.2 ppm, 28.8 SN 5!-39764-261 ppm, 48.8 ppm C3H8 in Air EPA Protocol I 

# S02 Western Research 

# 0- 110 0- II 0 50.1 ppm, 101 721- AT ppm S02 in N2 SN W72!-8846-l EPA Protocol I



# A schematic of CEM configuration is shown in Figure 3. Actual scale is the scale the monitor 'vas operated at. Calculation scale is the scale used in Equat1on 6C and to 

# calculate drift and bias. The CO monitor was operated following the calibration and

7

# I

I I I I I I I I I I I I I I 

# I I I I operating parameters given in Method 6C, with no ascarite or silica gel used up front of the analyzer. This deviation was addressed in the sampling protocol and the pretest meeting.

A S02 interference check was performed on the same process (Roller Kiln Scrubber) at the Dallas facility ofDaltile on July 9, 2003 using the same S02 monitor. The interference check in included in Appendix G.

A NOx converter check was performed the morning of 8/23/05 using the 51 ppm NOx in N2 gas standard and is included in Appendix B.
Opacity readings were taken over 6 minute intervals between each test repetition.

8- -Figure1 -KilnScrubberInlet////.\0"(,'.!:0-3467s\24ft.17ft.- - ---·--JstackDiameter-48inchesPoint#1- 1.5inchesPoint#2-5.0inchesPoint#3-9.3incliesPoint#4-15.5inchesPoint#5-32.5inchesPoint#6-38.7inchesPoint#7-43inchesPoint#8-46.5incties- - --0'- --- - -Figure2 -ScrubberExhaust16ft0tJ*16ft.- - - - -- --CEMSTraverse/""-..//\,/,,\\/-/7i.l910111\.I/\\/\\/..,"'"'-...._/./"'..._StackDiameter-54PointAtl-9inchesPoint#:2-27inchesPoint#3-45inchesstackDiameter-54inchesPoin11t1-·1.-1inchesPointtt-2-3.6inchesPoirrt#3-6AinchesPoirrt#4-9.6inct·1esPoint#S-B.5inchesPoint#6-inchesPoint#7-247inchesPointttf1-4(1.5inchesPoint#9-44.4inchesPointlt10-47.6inchesPointlt11.50.4inchesPoint#-12-52inches_/_../·----- -II/-- --0.--<-Figure3-CEMConfigurationlnstackFilter,HeatedProbHeatedSampleeLine::=_ln1FlOAnalyzerPumptJHeatedManifoldIPumpJSampleProcessorBiasCalibrationSpanLineIPumpmicronfilter-- -- - --- - -rCOAnalyzerNOxAnalyzerS02AnalyzerFlowmeterCalibrationPoin1prngowedbya0.3- - - --- - --

# I

I I I I I I I I I Appendix A 

# I I I I I I I I I

# I

I I I I I I I I I I I I I I I I I I PLANT: DATE: PLACE: RUN#· 

### EMISSION TEST SUMMARY

':2:7-:c,_ 

### ::::-')11 ''"' -y**:::3-,::,ur~-o~** Srrul"Jh"' lniP.i

64 LIQUID COLLECTED (mls) TEST DURATION (MINUTES)· NOZZLE DIAMETER (INCH.) METER COEFFICIENT (Y) PiTOT COEFFICIENT (Cp) GAS METER VOL.(Cu.Ft.) BAROMETRIC PRESSURE 0.253 PARTICULATE WEIGHT (Front halt mg): 0.991 PARTICULATE WEIGHT (Back hall mg) 8.8'1 STATIC PRESSURE (1n H20) 33.152 PERCENT C02

29 :-' PERCENT 02 PERCENT CD

FOR CIRCULAR STACK STACK DIAMETER (inch)· STACK AREA (Sq.Ft.) NOZZLE AREA (teet): FOR RECTANGULAR STACK 48 STACK LENGTH(1nchs) 12.56637 STACK WIOTH(inchs) 0 000349 STACK AREA (Sq ft.)

ENTER THE STACK AREA SHOWN ABOVE·



### FLOWS SAMPLED VOLUME (STD. CU.FT.): VOLUME OF WATER VAPOR (STD. CU. FT.)

FRACTIONAL MOISTURE CONTENT(%) DRY BASE MOLECULAR WT OF STACK GAS (DRY BASE): MOLECULAR WT. OF STACK GAS (WET BASE)·

STACK PRESSURE (mch Hg)· STACK GAS VELOCITY (It/sec.): ACTUAL STACK GAS FLOW RATE (ACFM): STANDARD STACK GAS FLOW RATE (SCFH):

PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR./SCF). PARTICULATE CONCENTRATION (LBS/SCF)· PARTICULATE EMISSION (LBS/HR)

BACK HALF PARTICULATE CONCENTRATION (GR.!SCF): PARTICULATE CONCENTRATION (LBS/SCF)· PARTICULATE EMISSION (LBS/HR)**ISOKII~ETIC** RATIO(%)·

POiiHS STACK T DELTA P SQUAR D_P der; F

382 0 40 0.632456 2 385 0.53 0.728011 3 386 C.SC 0.707107 4 384 0 46 0.678233 5 38:! C Li I 0.685565 6 38C CJ .;_5 0.67082 7 383 0 43 0.655744 8 352 c•.27 0.519615 9 381 C•.32 0.565685 10 

### 386 0.41 0.640312 11 385 G' 49 0.7 12 384 J 46 0.678233 13 383 0 3S 0.616441 14 

### 379 0.3E 0.6 15 

### 37S 0.36 0.6 !6 355 

### c- 36 0.6

379 25 0 6424 12 56637

DELTA H

:::. 90
J .2Q i 10 l GO 1 . 0**~** DC Q07 0.6'- 0 72 0 92 1 l**~:;.** ; 00 0.86 0.81 0.2J 

## o s;

0.9319 36.1063 3 1066 0 0792 80.0000 29 0400 28.1654

29.0603 46.7122 35220.1985 1188988.98

0.0000 0 OOE+OO

0.0000

0.0000 O_OQE

... QO

0 0000

102 5384

METER T

INLET**5~** 

### 86 89 90 91 

### 92 92 93 89 93 

### 95 

### 96 96 96 96**9~-** 92 1250 METER T. OUTLET

34 84 34 85 

### 25 

### 86 87 27 

### 29 89 

### 89 90 90 91 :?1 g,

87.6250 66 0

8 7

0

Meter Volume

695.9 698.2 700.9 703.6 706.1 708.4 711.1 713.6 715.49 717.6 719 9 722.6 725.1 727.4 729.6 731.8 7 34 052 89.8750 Po1nt VMSTO

2 2 2.5798 2.5721 2.3766 2.185 2.5597 2 3678 ]_ 7868

1 999 2.1722 2.5464 2.353 2 164 2 0678 2.0678 2.1167 Pomt Po1nt Point I so Velocrty Mo,sture ml' 46.0652 4.02686 101.7121 53.1194 4.72201 103 7999 51.6246 4. 70789 106.6119 49.4581 4.35012 102.5824 49.9335 3.99945 93 1937 48.8015 4.68529 111.4422 47.7898 4.33397 105.6439 37.1661 3.27059 98 7419 41.1775 3.65894 103.2660 46.7481 3.9759 99.4279 51.0756 4 66098 106.5582 49 4581 4.30685 101.5621 44.9255 3. 96094 102 7068 43.6234 3. 78483 100 5902 43.5974 3.78483 :t 00 5302 43 074 3 87429 101 6710



# 1 " (...

# I

I I I I I I I I I I I I I I I I I I PLANT · 

### JATE PLACE RUN# 2.3-i,._;g 'J:i**s::~.** 

## , :),.

.. ·. ,_,t 

### EMISSION TEST SUMMARY

64 LIQUID COLLECTED (mls) TEST DURATION {MINUTES) NOZZLE DIAMETER (INCH.) METER COEFFI Cl ENT (Y) PITOT CDEFFICI ENT (Cp) GAS METER VOL.(Cu.Ft) BAROMETRIC PRESSURE CL253 PARTICULATE WEIGHT (Front half mg) :; 991 PARTICULATE WEIGHT (Sack halt mg). 0.84 STATIC PRESSURE (In H20) 33 6LS PERCENT C02

29 7 PERCENT 02 PERCENT CO

FOR CIRCULAR STACK STACK DIAMETER (inch): STACK AREA {Sq Ft.) NOZZLE AREA (feet) FOR RECTANGULAR STACK <:8 STACK LENGTH(Inches) 12.56637 STACK WIDTH(inches) 0.000349 STACK AREA (Sq Ft.)

ENTER THE STACK AREA SHOWN ABOVE



### FLOWS SAMPLED VOLUME (STD CU FT) VOLUME OF WATER VAPOR (STD. CU.FT)

FRACTIONAL MOISTURE CONTENT(%): DRY BASE: MOLECULAR WT_ OF STACK GAS (DRY BASE): MOLECULAR WT. OF STACK GAS (WET BASE):

STACK PRESSURE (inch Hg): STACK GAS VELOCITY (ft/sec.): ACTUAL STACK GAS FLOW RATE (ACFM): STANDARD STACK GAS FLOW RATE (SCFH)

PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR /SCF): PARTICULATE CONCENTRATION (L8S/SCF) PARTICULATE EMISSION (LBS/HR)

BACK HALF PARTICULATE CONCENTRATION (GR./SCF): PARTICULATE CONCENTRATION (LBS!SCF)· PARTICULATE EMISSION (lBS/HR)

!SOKINETIC RATIO(%)·

POINTS STACK T DELTA P SQUAR D.P deg F

1 373 0 49 0.7 2 373 0 51 0.714143 3 373 0 48 0.69282 4 373 0 44 0.663325 5**37~** 0 -"13 0.655744 6 373 0.41 0 640312 7 366 0.42 0.640312 8 3CO 0.26 0.509902 9 361 0 .',.6 0.678233 10 370 i) 52 0.72111 11 370 c 47 0.685565 12 370 0 4-3 0.655744 13 368 0.4] 0 640312 14 

### 369 (Hl 0.640312 15 366 

## c ::07 0.608276 16 352 c·.32 0.565685

368.375 0 6507 DELTA H



### LO :.20 lW LOO 0.97 0.92 0 02 

## c 55- LOC·**~** 2C ; 

# " 0 97 0 92 0 92 C· S4 C. 72

0 9669 36.1008 3 4173 0.0865 80.0000 29_0400 28.0853

29.0603 47.0787 35496 473 1204488.88

0.0000 0 OOE+OO

0.0000

0 0000 0.00£+00

0.0000

101.2037

METER T

INLET

S3 ?5 ?7 93 £•9 99 

### JOG 1GC' 98 100 lO! !OJ iOl 101 lG1 1C 1

99 0625 METER T OUTLET**~13** 93 93 9¢ 94 95 S5 

## os 96 96 % 90- 97 '?I' 97 97

95 2500 2 7

18

0

Meter Po,nt Point PoH:t**Po:r~t** ! so Volume VMSTD VelOCity Mo1sture m!s 734.1B8 2 459 50 7838 4_951754 102 B311

736.8 2 4439 51.8099 4.921323 100.1752 739.4 2.43B9 50.2629 4.911243 103.0467

742 2.3403 4B.1231 4.712692 103.2776 744.5 2.2445 47.516 4 5197B4 100_Q74B 746.9 2.2422 46 4536 4.515169 102.5051 749.3 2.2402 46.258 4.51112 101.98!9 751 7 1.7273 36 7027 3 47B243 98.3B32 753.552 2.3B09 48.B49 4. 794552 102.0191

756_] 2.4264 52.221 4 88604¢ 9831B6 758.7 2 4236 49 647 4.B80465 103.2980 761 3 2.2364 47.4874 4 503599 99.6564 763 7 2.2342 46 314 4 499015 101 B313 766.1 2 2342 46.3419 4.499015 101 8928 768.5 2 0476 43.9436 4.123282 9R1235 770.7 1 9874 40.6683 4 002145 102 9143 772.B36 97.1563



# 13

# I

I I I I I I I I I I I I I I I I I I PLANT· DATE: PLACE**RUN;<~ Da';~l,~**  (;,')11• Ct' 23-IA'-\ C5 

### EMISSION TEST SUMMARY

64 LIQUID COLLECTED (mls) TEST DURATION (MINUTES) NOZZLE DIAMETER (INCH.) METER COEFFICIENT (Y) PITOT COEFFICIENT {Cp) GAS METER VOL_(Cu.Ft.) BAROMETRIC PRESSURE C253 PARTICULATE WEIGHT {Front half mg) D.99!. PARTICULATE WEIGH-:- (Sack halt mg} 0.84 STATIC PRESSURE (in H20) 33 363 PERCENT C02

29 7 PERCENT 02 PERCENT CO

FOR CIRCULAR STACK STACK DIAMETER (inch) STACK AREA (Sq_Ft.) NOZZLE AREA (feet) 48 12.56637 0 000349

ENTER THE STACK AREA SHOWN ABOVE


### FLOWS
SAMPLED VOLUME (STD. CU_FT.)· VOLUME OF WATER VAPOR {STD. CU. FT.)

FRACTIONAL MOISTURE CONTENT(%)· DRY BASE MOLECULAR WT. OF STACK GAS (DRY BAS::): MOLECULAR WT. OF STACK GAS (WET BASE)

STACK PRESSURE (inch**H~o::):** STACK GAS VELOCITY (ttl sec.)· ACTUAL STACK GAS FLOW RATE (ACFM): STANDARD STACK GAS FLOW RATE (SCFH)

PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR./SCF): PARTICULATE CONCENTRATION (LBS/SCF) PARTICULATE EMISSION (LBS/HR)

BACK HALF PARTICULATE CONCENTRATION (GR./SCF)· PARTICULATE CONCENTRATION (LBS/SCF) PARTICULATE EMISSION (LBS/HR)·

ISOKINETIC RATIO(%)

POINTS STACK T DELTA P SQUAR D P deg F

365 0.43 0.655744 2 

### 372 J.48 0.69282 3 371 0.47 0.685565 4 37: 0.45 0.67082 5 371 0 45 0.670B2 6 372 

# = 43 0.655744 7 367 G 4-l 0 640312 8 352 '::'.?7 0 519615 9 3G7 Ci 49 0. 7 10 37? C.51 0 714143 11 37? 8.19 0.7 12**~~-** 

## c 

## £: 0.640312 13 373 0.39 0.6245 14 

### 37! 

## -:us 0.6245 15 365 G.32 0.565685 16 

### 3::**~** C.3? 0.565685

367.75 0 6454 fOR RECTANGULAR STACK STACK LENGTH{mches) STACK WIUTH(1nches) STACK AREA (Sq.F! l

12 ')6h37

DELTA H

0 97 l lJ 1.10 1.00 i 00 0.97 0 92 

## c**6~** J 18 

### : ;_)(-

J J.C :J 92 0 33 

## c 8.'3 () 7:;
:; 72

0 9513 35.6036 3.1819 0.0820 80.0000 29.0400 28.1343

29.0676 46.6278 35156.515 1199952 96

0.0000 0 OOE+OO

0.0000

0.0000 0 OOE+OO

0 0000

100 1869

METER T

IN LEi

96 93 

## ;oo 101 102 102 1C3 iQj
; 02 105 :o5 JC{) lOS 206**~:)6** l:Jf

102 9375 METER T OUTLET

96 96 96 97 97 97 93 93**~«;.** 

### 99**~OJ** ]00 JQ1 

## ;c:c lOl lJ:

98 5625 67

0 8 6

0

Meter Volume

772.955

775.4 777.9 780.5

783 785.8 787.9 790.3 792 225

794.8 797.5

800 802.4 804.8 807 1 809 2 811.318 t:##ti#t:-:;;; Po1n1 VMSTJ

2.2886 2.3367 2.4258 2.3277 2 6047 1.9534 2.2282 1 7858 2.3917 2.5018 2.3138 2.2183 2.2161 2.1238 1 9385 1.9549 Point Po:nt Pc;,nt isc.- Veloctty MOISture ml; 4 7 2969 4 351202 101.2573 50.1827 4 44252 98.2641 49.6274 4.611941 103 0290

48.56 4 425533 101.0378 48.56 4 952167 123 0613 47 4972 3 71385 86.7913 46 2398 4.236305 101.0816 37 1819 3.395267 98 9223 50 ::502 4.547223 99.2488 51 7271 4 75641 102 0658
so. 7027 4.399082 96.3053 46 3515**4.2~** 7493 100.8759 45.2612 4.213335 103 4524 45.2069 4 037779 99.G228 40 826 3.685484 99 4796 40 4536 3 716798 99 4097



# 11

# I

I I I I I I I I I I I I I I I I I I PLANT: DATE: PLACE

. RUN#: 

### EMISSION TEST SUMMARY

C)Cl!t;i", Cow<::-P TY L.:J·klf.;-05**~.il:' Sc~unlw'**  Exh<,ust 1

TEST DURATION (MINUTES): 60 LIQUID COLLECTED (mls) NOZZLE DIAMETER (INCH.): METER COEFFICIENT (Y) PITOT COEFFICIENT (Cp) GAS METER VOL.(Cu.Ft.) BAROMETRIC PRESSURE 0 3123 PARTICULATE WEIGHT (Front hall mg) 0 995 PARTICULATE WEIGHT (Back hall mg): 0.84 STATIC PRESSURE (in H20): 4.3.89 PERCENT C02

29 7 PERCENT 02 PERCENT CD

FOR CIRCULAR STACK STACK DIAMETER (Inch)· STACK AREA (Sq Ft.) NOZZLE AREA (feet): FOR RECTANGULAR STACK 54 STACK LENGTH(inchs) · 15 90431 STACK WIDTH(inchs) 0.000532 STACK AREA (Sq. Ft.)

ENTER THE STACK AREA SHOWN ABOVE·


### FLOWS SAMPLED VOLUME (STO CU.FT) VOLUME OF WATER VAPOR (STD. CU_FT_)

FRACTIONAL MOISTURE CONTENT(%) DRY BASE MOLECULAR WT. OF STACK GAS (DRY BASE): MOLECULAR WT. OF STACK GAS (WET BASE)·

STACK PRESSURE (inch Hg): STACK GAS VELOCITY (ft!sec.)· ACTUAL STACK GAS FLOW RATE (ACFM): STANDARD STACK GAS FLOW RATE (SCFH)·

PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR_!SCF): PARTICULATE CONCENTRATION (LBS/SCF) PARTICULATE EMISSION (LBS/HR):

BACK HALF PARTICULATE CONCENTRATION (GR_ISCF)· PARTICULATE CONCENTRATION (LBS/SCF): PARTICULATE EMISSION (LBS/HR):

ISOKINETIC RAT!O (%)·

POINTS STACK T. DELTA P SQUAR D_P deg F



### 1 137 .]_31 0 556776 

### 2 138 0_33 0.574456 3 

### 139 0.32 0.565685 

### 4 139 0 29 0.538516 

### 5 ]39 C' 28 0.52915 

### 6 138 0 21 0.458258 

### 7 :38 0.20 0.447214 

### 8**~** 38 0.19 0.43589 9 

### 138 0 lS 0.424264 

### 10 138 0 14 0.374166 

### 11 138 0.10 0.316228 

### 12 Ll3 

## o_os 0.282843 

### 13 138 0 20 0.447214 

### 14 137 0.2; 0.458258 

### 15 138 0.20 0.447214 

### 16 135 0.19 0.43589 

### 17 138 0 2C 0.447214 

### 18 138 0.20 0_447214 

### 19 138 J 2S 0.5 20 ; 32 0_30 0.547723 

### 21 J 38 

### o_ 32 0.565685 22**~** 38 J 34 0.583095 

### 23 138 0.33 0.574456 

### 24 137 DZl 0 447214



### 138 o.,;752 

## :s 9043:.

DELTA H

1.80 :.90 l 90 

### 1 70 1.60**~-20** l 2C 1**~0** 

### 1 10 0 82 

### 0 58 0**·~7** 1 20 1.20 ' 20**~** l G

j_ 20 1.2C 1.50 ; 2J

9·2 ')DC ; 9C

: 2S

1 3654 41.3277 

### 8 4773 0.1702 80.0000 28.9800 27.1111

29.6941 29.4107 28065.4642 1224428.24

0.0179 2 55E·06

3.1279

0.0003 4.75E-08

0.0581

100.9787

METER T

INLET



### 85 91 

### 93 94 

## os 96 

### 98 99 99 99 

### 100 99 

### 98 :02 103 104 j J4 

## ; ::14 ;c;l.. ]·J5 1 J:O 

### :or;

: rJ'S iOS

99_7917 METER T OUTLET



### 85 36 87 87 

### 88 88 89 90 90 

### 90 91 9l 

### 92 92 93 93 93 94 gc; 9"- ?5 ?5**0~,** 

### 96

91.1667 Meter .LSC • 47.88

:JB9 ::-08

1 5 18 5

0

0

Volume

257_9



### 260 262.2 264_4 266.4 268.5 270.2 271 9 273.6 275.3 276.8

278 279.05 280.8 282.5 284 3 285.9 287.7 289_4 291.3 293 4 295.6 297.9 300 1 301 791 95.4792 Po1nt VMSTO

2.0176 2 1007 2.095 1.9018 1.9928 1.6102 1.6058 1.6025 1.6025 1.413 l.l277 0 0874 1.6486 1.5957 1.6866 1.4975 1.6851

1.59 1 77811 1 9653 2.0576 2.1497 2 0557

J .576 Po1nt Po1nt Pomt I so Velocity Mo1sture ml; 34.4313 8.80412 100.9151 35.5544 9.16676 101.9233 35.0408 9.14176 103.3076 33_3579 8.29905 985160 32.7777 8 69606 105.0560 28.3626 7 02636 97.9343 27.6791 7.00731 100 0809 26.9782 6.99295 102 4703 26.2587 6.99295 105.2782 23.158 6.16598 105.2575 19.5721 4 92099 99.3955 17.5058 4.30857 97.2977 27.6791 7_19392 102 7460 28.3389 6.96328 96.9740 27.679! 7.35967 105.1134 26.9782 6.53446 95.7519 27.6791 7.35309 105.0] 93 27.6791 6_93837 99 0962 30.9461 7 76039 99.1352 33.8998 8 57595 ]00.0083 350116 8.97852 101 3781 36.0891 9_38057 -;o2 7553 35.5544 8.97051 99_7412 27 6559 6 87703 98 1380



# 15

# I

I I I I I I I I I I I I I I I I I I PLANT DATE: PLACE

. RUN#· 

### EMISSION TEST SUMMARY

D;!ltrle. Corl'nt'. TY 23-;..wg-·JS Krl; Sr•ubtJc>r Erhnu<;: 2

TEST DURATION (MINUTES): 60 LIQUID COLLECTED (mls) NOZZLE DIAMETER (INCH.): METER COEFFICIENT (Y) PITOT COEFFICIENT (Cp) GAS METER VDL(Cu.Ft.) BAROMETRIC PRESSURE CJ.3l23 PARTICULATE WEIGHT (Front halt mg) 0 995 PARTICULATE WEIGHT (Back hall mg): 0.84 STATIC PRESSURE(m H20): 46_0 l PERCENT C02 29 7 PERCENT 02 PERCENT CO

FOR CIRCULAR STACK STACK DIAMETER (mch): STACK AREA (Sq. Ft.) NOZZLE AREA (teet): FOR RECTANGULAR STACK 54 STACK LENGTH(rnches) 15.90431 STACK WIDTH(mches) 0.000532 STACK AREA (Sq.Ft)

ENTER THE STACK AREA SHOWN ABOVE·**j~** 90tl3l


### FLOWS SAMPLED VOLUME (STD. CU.FT_)' 42.7352 VOLUME OF WATER VAPOR (STD. CU.FT_), 8 9009

FRACTIONAL MOISTURE CONTENT(%) 0.1724 DRY BASE: 80.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 28.9800 MOLECULAR WT OF STACK GAS (WET BASE): 27 0873

STACK PRESSURE (mch Hg): 29.6941 STACK GAS VELOCITY (ftlsec.): 30.2953 ACTUAL STACK GAS FLOW RATE (ACFM) 28909.577 STANDARD STACK GAS FLOW RATE (SCFH): 1258397.44

PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0142 PARTICULATE CONCENTRATION (L8S/SCF) 2.03E·06 PARTICULATE EMISSION (L8S/HR)· 2.55D4

BACK HALF PARTICULATE CONCENTRATION (GR/SCF): 0.0014 PARTICULATE CONCENTRATION (LBS/SCF) L93E·07 PARTICULATE EMISSION (L8S/HR)· 0 2428

ISOKINETIC RATIO(%)· 101.5990

POINTS STACK T DELTA P SQUAR O.P DELTAH METER T deg F INLET

137 0 35 0.591608 2.10 96 2 133 0 33 0.574456 2 OG 99 3 138 0 32 0.565685 1.90 102 

### 4 138 0.30 0.547723 1.80 

### 104 5 138 0.26 0.509902**~** 60 .i.OS 

### 6 138 0 22 0.469042 l .30 1C7 

### 7 138 0.20 0.447214 1.20 107 

### 8 138 0.19 0 43589 1.20 lOS 9 

### 138 0.20 0.447214 1.20 

### 108 10 137 0.21 0.458258 1.30 

### 109 11 138 0.20 0.447214 1 20 l09 

### 12 137 Q.**~** 5 0.387298 

## c 92 109 

### 13 l37 c 18 0 424264 

## uo 102 

### 14 138 0.19 0 43589 : 20 lOS 

### 15 !38 0 20 0.447214 1.20 

### 108 16 138 0.20 0.447214 L20 108 

### 17 J38 0.20 0 447214 i 2G 188 

### 18 i38 0 19 0.43589 l 20 i09 

### 19 138 0.24 0.489898**~.50** 109 

### 20 138 0.29 0.538516 

### 1 83 110 

### 21 138 ':;_3! 0.556776 1.% ClC 

### 22 

### :38 0.33 0.574456 2 JO j;· 

### 23 ;33 0.32 0.565685 2.00 1:1 24 

### :37 0.2'3 

### 0.5 52 ;**~** l

137 79167 0 4894 1.4800 107 0000 METER T. OUTLET

96 '96 97 37 

### 97 98 99 99 99 

### 100 100 :o-; lOl 100 

## :c: l01**!C~** J.C2 lOO 

### :ol 101 !Ol**;~.** J'l:

99 5833 189.1 39.28 3_74

1.5 13.5

0

0

Meter Volume

303.8 306.1 308.4 310.6 312.7 314_7 316.5 318.3 319.9 321.7 323.5 325.3 326.809

328.5 330.2 331 9 333.7 335 4 337.1 339.1 341 2 343_4 345.6 347.8 349.81 l03.2917 Point Po1nt VMSTD VelOCity

2.1676 36.6014 2.1613 35.57 2.0594 35 0269 1.9618 339147 1 8658 31.5729 1.6735 29.0428 1.6716 27.6912 1.4845 26.9901 1.6701 27.6912 1.6676 28.3513 1.6672 27.6912 1.3954 23.9612 l. 57 42 26.2482 1.5759 26.9901 1.5745 27 6912 1.6672 27.6912 1.5745 27.5912 1 5717 26.9901 1.8538 30 3342 1.9444 33.3447 2.0375 34.4753 2.0362 35.5 7 2.0362 35.0269 1 8581 30 9338 Pomt Point I so Moisture ml' 9 604417 102.2589 9.576216 105.0908 9.124868 101 6902 8 692419 100 0478 8_267038 102.2094 7.415004 99.6615 7.406591 104_4073 6.577794 95.1330 7.400019 104 3147 7.388733 101.5604 7.38691 104 1299 6.182936 100.5572 6.974946 103.5544 6.982711 100.9892 6.976526 98.3449 7 38691 104 1299 6.976526 98.3449 6.964189 100.7213 8.213755 105.6972 8 615563 100 8584 9 028052 102 2211

9.0223 99.0120 9.0223 100 5472 8.232947 103 7i69



# lC

# I

I I I I I I I I I I I I I I I I I I PLANT : 

### DATE PLACE· RUN# 

### EMISSION TEST SUMMARY

82ll·'·' Cc'W02 -y

**23-F.e~g** JS r:,!: S::

**_;:J~J"~** fxh;1ust

TEST DURATION (MINUTES): 60 LIQUID COLLECTED (mls) NOZZLE DIAMETER (INCH.)· METER COEFFICIENT (Y) PITOT COEFFICIENT (Cp) GAS METER VOL.(Cu.Ft.) BAROMETRIC PRESSURE 0.3123 PARTICULATE WEIGHT (Front half mg): 0 995 PARTICULATE WEIGHT (Back halt mg) · 0.84 STATIC PRESSURE (irl H20) 46.26 PERCENT C02 29 7 PERCENT 02 PERCENT CO

FOR CIRCULAR STACK STACK DIAMETER (irKh) STACK AREA (Sq.Ft.) NOZZLE AREA (feet) FOR RECTANGULAR STACK 54 STACK LENGTH(inches): 15.90431 STACK WIDTH(inches) 0.000532 STACK AREA (Sq Ft.)

ENTER THE STACK AREA SHOWN ABOVE· J 5 9Qt,;q


### FLOWS SAMPLED VOLUME (STD CU.FT.) 42.6789 VOLUME OF WATER VAPOR (STD_ CU. FT.) 8.3738

FRACTIONAL MO\STURE CONTENT(%) 0.1640 DRY BASE 80.0000 MOLECULAR WT. OF STACK GAS (DRY BASE) 28.9800 MOLECULAR WT OF STACK GAS (WET BASE)· 27 1790

STACK PRESSURE (mch Hg): 29.6941 STACK GAS VELOCITY (ftlsec.): 30.2464 ACTUAL STACK GAS FLOW RATE (ACFM)· 28862.9271 STANDARD STACK GAS FLOW RATE (SCFH): 1270380.11

PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0123 PARTICULATE CONCENTRATION (LBS/SCF) 1 76E-06 PARTICULATE EMISSION (LBS/HR)· 2.2401

BACK HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0003 PARTICULATE CONCENTRATION (LBS/SCF)· 4.34£-08 PARTICULATE EMISSION (LBS/HR): 0.0551

ISOKINETIC RATIO(%): 100.5079

POINTS STACK T DELTA P SQUAR O.P DELTA H METER T deg F INLET



### 1 137 0 34 0.583095 2 10 201 

### 2 137 0 33 0.574456 ? OC· 107 

### 3

**~37** Cl.32 0.565685 ?.00 109 

### 4 :;:3;' 0.30 0.547723 1.80 llO 

### 5 137 0.27 0.519615 1 60 ill 6 

### 137 0 25 0.5 1.50 :ll 

### 7 137 0 20 0.447214 1.20 111 

### 8 137 0.19 0.43589 1 20 

### 111 9 137 0_19 0.43589 1 20 

### 111 10 137 0.20 0.447214 1.20 112 

### 11 137 0.!8 0.424264 1 10 ;.I 

### 12 136 0 14 0.374166 0 86 

# -·· 13 137 

## c 17 0.412311 i.OO i06 

### 14 137 0.19 0.43589 1 20 jlQ 

### 15 138 0.19 0.43589 1.20 111 

### 16 138 0 20 0 447214 1.20 l-'2 

### 17 138 0.19 0.43589 ; .20 : i2 

### 18 138 0.20 0.447214 1.20 113 

### 19 136 0.27 0.519615 1 70 

### 113 20

**~37** 0.30 0.547723 1 90 ]1L 

### 21 137 

## c .;:3 0.574456 :?.80 

## _,;:, 22 137 J.33 0_574456 2.J:::; il3 

### 23 131 0 32 0.565685 2 00 ll3 

### 24 : 37 J 25 

### 0.5 ; 5C-



### . :3

137.16667 0.4896 1 4983 110 7917 METER T. OUTLET



### 101 101 lC:" 102 102 102 10:2 i03 103 

### 104 104 

## :o; ;o4 104 

### 104 10C. 104 104 :05 l05 1:5 

### ,c5 l05 W'S

103.4583 **~** 77 9 34.l 3 C· 84 0 08

1.5

**~85**

0

Meter Volume

350.3 352.6 354.8 357.1 359.2 361.2 363.2



### 365 366.7 368.4 370_1 371.8 373.278

374 9 376.6 378.3 380.1 381.8 383.6 385.6 387.8 390.1 392.3 394.6 396.56 107 1250 Po1nl Point VMSTD VelOCity

2.1483 36.0138 2.0435 35 4802 2.1326 34.9385 1.9427 33 8291 1 8477 32.0931 1.8472 30.8816 1.6613 27.6213 1.5676 26 9219 1.5676 26.9219 1.5648 27.6213 1.5658 26.2039 1.3605 23.0903 1 5002 25.4656 1.5676 26.9219 1.5662 26.9445 1.6569 27.6444 l. 5648 26.9445 1 .6554 27.6444

1.84 32.1199 2.0232 33.8291 2.1176 35.4802 2.0255 35.4802 2.1176 34.9385 1 8028 308816 Po1nt Po1nt I so Mo1sture ml' 8.966848 101.9702 8_529261 98 4526 8.901173 104.3386 8 108802 98.1678 7.712048 98.4149 7_710147 102.2505 6.933997 102.8115 6.543 99 5344 6.543 99_5344 6.531481 96.8433 6.535622 102.1465 5.678779 100 5541 6 261798 100.7042 6.543 99 5344 6.537236 99.5299 6.915686 102.6258 6.531481 99.4423 6.9096C3 102.5355 7.680058 98.0887 8.444808 102 2356 8.838599 102.0233 8 454312 97.5875 8.838599 103.6051 7 524602 99 7599



# l'i'

# I

I I I I I I I I I Appendix B 

# I I I I I I I I I

# I

8123105 NOx Converter Check



# I
Date/Time NOx 

# I mmlddlyy hh:mm:ss ppm 08/23105 07:36:45 0.266266 08123105 07:37:45 23.06641 08123105 07:38:45 51.60451 51.0 ppm NOx 

# I 08123105 07:39:45 11.40576 08123105 07:40:45 6.772583 08123105 07:41:45 30.10938 Start Converter Check 

# I 08123105 07:42:45 30.32276 08123105 07:43:45 30.34033 08123105 07:44:45 30.37696 

# I 08/23105 07:45:45 30.4087 08123105 07:46:45 30.38184 08123105 07:47:45 30.41162 08123105 07:48:45 30.44288 

# I 08123105 07:49:45 30.44581 08123105 07:50:45 30.4546 08123105 07:51:45 30.47657 

# I 08123105 07:52:45 30.47657 08123105 07:53:45 30.47999 08123105 07:54:45 30.4961 

# I 08/23105 07:55:45 30.53516 08123105 07:56:45 30.50587 08123105 07:57:45 30.53907 

# I 08123105 07 58:45 30.52296 08123105 07:59:45 30.50831 08123105 08:00:45 30.52638 08123105 08:01:45 30.48487 

# I 08123105 08:02:45 30.50929 08123105 08:03:45 30.52198 08123105 08:04:45 30.53419 

# I 08123105 08:05:45 30.51759 08123105 08:06:45 30.51808 08123105 08:07:45 30.48536 

# I 08123105 08:08:45 30.52492 08123105 08:09:45 30.47951 08123105 08:10:45 30.5 

# I 08123105 08:11:45 30.4541 Stop Converter Check, Bag Off 08123105 08: 12:45 6.982544 08123105 08: 13:45 0.403427 

# I I I I I Page 1 

# 13

# I

I I I

I

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# lB

# I

I I I I I I I I I I I I I I I I I I Sheet1

Summary of CO Analyzer Calibrations and Bias

Plant: Source: Date:

Run #1

Run #2

Run #3 Daltile, Conroe, TX Kiln Scrubber Exhaust 8/23/05
Analyzer Calibratrion Data
Cylinder Analyzer Absolute %Span Value Response Difference Zero Gas 0 2.53 2.53 1.265 Mid Range 99.1 101.38 2.28 1.14 High Range 200 196.33 -3.67 -1.835

System Calibration Bias and Drift Data
Analyzer Initial Values Final Values Calibration System System System System Response Calibration Calibration Calibration Calibration Response Bias Response Bias

Zero Gas 2.53 2.48 -0.025 5.13 1.3 Upscale 101.38 101.05 -0.165 102.33 0.475
Average CO Concentration: 85.18 Corrected CO Concentration: 82.38507 (Equation 6C-1)

Zero Gas 2.53 5.13 1.3 4.8 1.135 Upscale 101.38 102.33 0.475 100.6 -0.39
Average CO Concentration: 91.74 Corrected CO Concentration: 89.11298 (Equation 6C-1)

Zero Gas 2.53 4.8 1.135 3.43 0.45 Upscale 101.38 100.6 -0.39 100.48 -0.45
Average CO Concentration: 94.76 Corrected CO Concentration: 93.15965 (Equation 6C-1)

Page 1 Drift Average Calibration Values

1.325 3.805 0.64 101 .69

-0.165 4.965 -0.865 101.465

-0.685 4.115

-0.06 100.54



# 20

# I

I I I I I I I I I I I I I I I I I I Sheet1

Summary of NOx Analyzer Calibrations and Bias

Plant: Source: Date:

Run #1

Run #2

Run #3 Daltile, Conroe, TX Kiln Scrubber Exhaust 8/23/05
Analyzer Calibratrion Data
Cylinder Value Zero Gas 0 Mid Range 25.5 High Range 51 Analyzer Response 0.1 24.9 5U3

System Calibration Bias and Drift Data
Analyzer Initial Values Calibration System System Absolute %Span Difference 0.1 0.166667 -0.6 -1 0.13 0.216667

Final Values System System Response Calibration Calibration Calibration Calibration Response Bias Response Bias

Zero Gas 0.1 0.13 0.05 0.45 0.583333 Upscale 24.9 24.4 -0.83333 24.35 -0.91667

Average NOx Concentration· 

## 21.73 Corrected NOx Concentration: 22.69961 (Equation 6C-1)

Zero Gas 0.1 0.45 0.583333 0.58 0.8 Upscale 24.9 24.35 -0.91667 24.4 -0.83333
Average NOx Concentration: 20.29 Corrected NOx Concentration: 2113422 (Equation 6C-1)

Zero Gas 0.1 0.58 0.8 0.7 Upscale 24.9 24.4 -0.83333 24.35 -0.91667
Average NOx Concentration: 19.2 Corrected NOx Concentration: 19.94017 (Equation 6C-1)

Page 1 Drift Average Calibration Values

0.533333 0.29 -0.08333 24.375

0.216667 0.515 0.083333 24.375

0.2 0.64 -0.08333 24.375



# 21

# I

I I I I I I I I I I I I I I I I I I Sheet1

Summary of Sulfur Dioxide Analyzer Calibrations and Bias

Plant: Source: Date:



## Run #1

Run #2

Run #3 Daltile, Conroe, TX Kiln Scrubber Exhaust 8/23/05

Analyzer Calibratrion Data


## Cylinder Value Zero Gas 0 Mid Range 50.1 High Range 101 Analyzer Response 0.1 50.13 101.65

System Calibration Bias and Drift Data


## Analyzer Initial Values Calibration System System Absolute 

# % Span Difference 0.1 0 090909 0.03 0.027273 0.65 0.590909

Final Values System System Response Calibration Calibration Calibration Calibration Response Bias Response Bias

Zero Gas 0.1 0.78 0.618182 2.43 2.118182 Upscale 50.13 47.95 -1.98182 48.8 -1.20909
Average S02 Concentration: 2.51 Corrected S02 Concentration: 0.969436 (Equation 6C-1)

Zero Gas 0.1 2.43 2.118182 0.58 0.436364 Upscale 50.13 48.8 -1.20909 46.88 -2.95455
Average S02 Concentration: 1.86 Corrected S02 Concentration: 0.383846 (Equation 6C-1)

Zero Gas 0.1 0.58 0.436364 0 -0.09091 Upscale 50.13 46.88 -2.95455 46.35 -3.43636
Average S02 Concentration: 0.8 Corrected S02 Concentration: 0.55156 (Equation 6C-1)

Page 1 Drift Average Calibration Values

1.5 1.605 0.772727 48.375

-1.68182 1.505 -1.74545 47.84

-0.52727 0.29 -0.48182 46.615



# 22

# I

I I I I I I 

# I I I I 

# I 

# I I I I 

# I I 

# I Date/Time VOC co mmlddlyy hh:mm.ss ppm ppm 08/23105 08.25:42 0.1 08/23105 08.25:52 0.1 08123105 08 26:02 0.1 08/23/0508:26"12 0_1 08/23/05 08'26.22 0_1 08/23/05 08:26'32 0_1 08123105 08:26:42 0 1 08/23/05 08:26'52 0.1 08/23/05 08:27:02 08/23/05 08:27"12 08/23105 08:27:22 08123105 08.27:32 08123105 08:27:42 08123105 08:27:52 08/23/05 08:28:02 08/23/05 08.28:12 08123105 08:28:22 08/23/05 08:28:32 08/23/05 08:28:42 08/23/05 08:28:52 08/23/05 08:29:02 08/23/05 08:29:12 08123105 08:29:22 08123/05 08:29:32 08/23/05 08:29:42 08/23/05 08:29:52 08123/05 08:30:02 08123105 08:30:12 08/23/05 08:30:22 08/23/05 08:30'32 08/23/05 08:30:42 08123/05 08:30:52 08/23/05 08:31:02 08123/05 08:3'1 :12 08123/05 08:31:22 08123105 08:31 :32 08123105 08:31'42
08/23/05 08:31"52 08123105 08:32:02 08/23105 08:32:12 08/23105 08:32:22 08/23/05 08'32:32 08!23/05 08:32:42 08/23/05 08.32:52 08/23/05 08:33:02 08123105 08:33:12 08123/05 08.33:22 08123/05 08:33:32 08/23/05 08"33:42 08123/05 08:33:52 08/23/05 08:34:02 08123/05 08:34:12
08123105 08'34:22 08123/05 08"34'32 08/23/05 08:34:42 08123105 08:34:52 08123105 08:35:02 08123105 08:35:12 08123105 08.35:22 08123105 08:35:32 08/23/05 08:35.42 08/23105 08:35:52 08123105 08·36:02 08/23105 08 36' 12 08.'23/05 08:36:22 08.'23105 08-36.32 08/23.105 08:36:42 08/23105 08:36:52 08/23105 08·37:02 08123/05 08 37:12 0.1 

### 0.2 0.2 0.2 0.2 0.2 

### 0.2 0.2 0 2 

### 0.2
0.2 

### 02 

### 0.2 0.1 0.1 0.1 0.1 

### 0 1 0.1 0 1 01 0.1 0 1 0.1 02 0.2 

### 0.2 

### 0.2 02 0.2 0 1 0 1 0.1 0.1 0.1 0.1 0.1 0 1 0.1 00 0.1 00 0.1 0.1 

### 02 0 1 01 

### 0.0 0.1 0.1 0 0 0 1 0.1 0 0 00 00 0 1 0 1 

### IJ: 0.0 0 0 0 1 1.2 1.5 1.5 1 4 1.5 1.4 1.5 1.7 1 5 1 4 1.6 1.9 

### 20 2.4 2 7 2.7 2.6 27 2.6 2.8 3.1 2.6 

### 2.3 

### 2.0 1.6 1 9 1.7 1 6 1 4 1.6 

### 2.0 2.0 2.2 2.6 

### 2.5 2.6 2.5 2.5 2.8 

### 2.9 26 

### 23 2 2 

### 2.2 2.2 2.0 2.1 24.6 96.8 100.9 101.0 

### 101.3 101.3 101.3 101.6 101.4 51.7

2.4 1 9 

### 1 8 1 8 "1.8 1 6 1 7 1.8 2.0

: 9 2.1 39 3 185.6 

### NO' ppm 

### 802 ppm 0.2 -0.1 0.3 -0.1 0.2 -0.2 0_2 -0_1 0 3 0.0 0.3 0.0 0 3 -0.1 0 3 0.0 2.2 48.7 49.6 50.0 50.2 50.7 51.0 51_0 

### 51.0 51.1 51.2 51.2 22.2 0.4 

### 0.3 0.3 0.3 02 

### 0.3 28 24.2 24.6 24.7 24.7 24_8 24_8 

### 24.9 24.9 24.9 24.9 24 9 7.8 

### 0.3 0.3 0.3 0.3 

### 0.2 0.2 0.3 

### 02 0.1 0.1 0 1 

### 0.1 0.1 0.1 0.1 0.1 0.1 

### 0.2 0.2 0.2 0 2 0 2 

### 0 2 

### 0.2 0.2 

### 0.2 0.2 

### 0.2 0.3 0.2 00 0 0 0.0 0.0 0.0 0.0 0.0 00 00 

### 00
00 0.0 

### 00 0.0 0.0 

### 0.0 0.0 0 0 0 0 0 0 

### 0.0 0.0 

### 0.0 0.0 0.0 01 

### 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.0 00 0 1 01 0.1 0.1 01 0 1 

### 0 1
0.1 0 1 

### 0.2 

### 0.2 01 0.1 0.1 0.1 0_1 0 1 0 1 0 1 0 1 

### 0: 0 1 0.1 0 1 8/23/05 Calibrations

51 ppm NOx

25 5 ppm NOx
Zero CO, S02

99.1 ppm CO
Zero NOx



### Page 1

# I

I I I I I I I I I I I I I I I I I I 08/23/05 08 37:22 08/23/05 08 37:32 08/23105 08'37:42 08/23105 08:37'52 

### 08123105 08.38.02 08/23/05 08:38.12 08/23/05 08:38.22 08/23/05 08:38:32 08123/05 08:38.42 08123/05 08:38:52 08/23/05 08:39:02 08123105 08:39:12 08/23/05 08.39:22 08/23105 08:39:32 

### 08123105 08:39:42 08123105 08:39:52 08123/05 08'40:02 08/23/05 08'40:12 08/23/05 08:40:22 08/23105 08:40:32 08/23/05 08:40'42 08/23/05 08:40:52 08/23105 08:41 :02 08/23105 08:41 '12 08/23/05 08 41 :22 08/23/05 08:41 :32 08123/05 08:41.42 08/23/05 08 41-52 08/23/05 08.42.02 08/23/05 08'42'12 08/23/05 08'42'22 08/23/05 08:42.32 08/23/05 08:42.42 08/23/05 08:42:52 08/23/05 08:43:02 08/23/05 08:43:12 08/23/05 08:43:22 08/23/05 08:43.32 08/23/05 08:43:42 08/23/05 08:43.52 08/23/05 08:44:02 08/23/05 08:44'12 08/23/05 08'44:22 08/23/05 08:44.32 08/23/05 08:44.42 08/23/0:S 08:44:52 08/23/05 08:45:02 08/23/05 08:45:12 08/23/05 08:45:22 08/23/05 08:45:32 08/23/05 08:45:42 08/23/05 08"45:52 08/23/05 08'46:02 08/23/05 08:46:12 08/23/05 08"46:22 08/23/05 08:46'32 08/23/05 08'46'42 08/23/05 08:46.52 08/23/05 08:47:02
08123105 08:47:12 08/23/05 08:47.22 08/23/05 08.47.32
08123105 08:4 7:42 08/23105 08:47:52 08/23/05 08:48:02 08/23/05 08:48:12 08/23/05 08:48:22 08/23105 08:48:32 03/23/05 08:48:42 08/23/05 08:48:52 08/23/05 08:49:02 08/23105 08:49.12 0.1 0.1 0 1 0.1 01 0.1 01 0.0 01 01 0.1 0 1 0.1 0.1 0.1 0.1 0.1 0.2 0.1 0.2 0.2 0.1 0.1 0.1 

### 0.2 0.2 

### 0.4 02 0.1 01 01 0 1 01 0 1 01 01 0.1 0.1 0.0 

### 0.0 0.1 0.1 01 

### DO 0.0 

### 00 00 

### 00 

### 00 00 00 

### DO 01 0.1 

### 00 0 1 00 0.2 0.1 0.1 0.2 0 3 0.2 

### 0.3 0.1 

### 0.2 0.0 0.0 0.0 

### 0.0 00 0.6 194.9 195.3 195.7 196.2 196.2 

### 196.3 196.4 196.3 196.3 138_3

5.9 

### 2.6 2.5 

### 2.3 2.1 

### 23 1.9 2.1 

### 2.4 2.6 

### 2.4 2.8 

### 26 2.7 2.7 2 8 3.1 3 1 

### 3.2
3 1 

### 3.3 3.3 

### 34 31 2.6 

### 24 21 20 2 1 1.9 2.0 

### 2.0 1.8 

### 24 26 

### 3.2 3.3 3.2 3.2 3.1 

### 3.4 3.4 34 3.5 

### 3.2 34 33 

### 3.3 3.3 34 3.4 3 3 

### 34 34 3 1 

### 3.2 3.0 3.1 29 

### 30 30 3.0 0.1 0.1 0.1 01 01 0.1 0.1 01 0.1 0.1 

### 0.2 0.2 0.2 0.2 0.2 02 0.3 0.5 

### 04 04 04 

### 04 04 04 

### 04 04 04 

### 04 04 

### 04 04 04 

### 04 02 0.2 

### 02 02 02 02 0.3 

### 02 02 0.2 0.2 

### 02 02 02 

### 0.2 02 

### 0.2 0.2 02 0.2 

### 0.3 0 2 

### 0.2 

### 0.3 0.3 0 3 

### 0.3
0 3 0 3 

### 0.3 

### 03 03 

### 0.3 

### 0.2 0.2 0.2 0.2 

### 02 0.2 01 0 1 01 0 1 0.2 0.2 0.2 0.1 0.2 

### 0.3 0.2 0.1 0.1 

### 0.3 0.2 0.2 3.1 22.8 39.8 46.4 48.4 49.0 49.4 49.5 49.7 49_8 

### 50 0 50.1 

### 50.1 50.1 50.1 50.2 47.7 28 2 11.2 

### 4.4 22 1.3 1.0 

### 0.8 0.6 0.6 0.7 17 2 62.6 88.7 97.2 99.7 100.4 100_7 100.9 101.1 101_2 101_2 101.3 101.4 101.4 101.5 101.6 

### 101.6 101.6 101.7 101.7

91.9 47 1 16.6 59 2.9 2.0 1.7 1.5 1 3 8123105 Calibrations

200 ppm CO

50 1 ppm S02

101 ppm S02



# 24

Page 2

# I

I I I I I I I I I I I I I I I I I I 08/23/05 08:49:22 08/23/05 08:49.32 08/23/05 08:49:42 

### 08/23/05 08:49:52 08/23105 08:50:02 OB/23105 

## oe-so:12 08/23/05 08.50.22 OB/23/05 oe-so:32 

### 08/23/05 08:50:42 08/23/05 08:50:52 08/23/05 08:51:02 08/23/05 08'51:12 08/23/05 08:51:22 08/23/05 08:51:32 

### 08/23/05 08:51:42 08/23/05 08'51 :52 08/23/05 08:52:02 08/23/05 08:52:12 08/23/05 08:52:22 

### 08/23/05 08:52:32 08/23/05 08.52:42 08/23/05 08 52'52 

### 08/23/05 08 53.02 08/23/05 08:53:12 08/23/05 08:53:22 08/23/05 08:53:32 08/23/05 08:53:42 08/23/05 08'53:52 08/23/05 08:54:02 08/23/05 08:54:12 08/23/05 08'54:22 

### 08/23/05 08:54:32 08/23/05 08.54.42 08/23/05 08:54:52 08/23/05 08'55:02 

### 08/23/05 08:55:12 08/23/05 08:55:22 08/23/05 08:55:32 08/23/05 08:55:42 08/23/05 08:55:52 

### 08123105 08:56:02 

### 08123105 08:56:12 08/23/05 08:56:22 08/23/05 08:56:32 08/23/05 08:56:42 

### 08123105 08:56:52 

### 08123105 08:57:02 

### 08123105 08:57-12 

### 08123105 08:57:22 08/23105 08:57:32 08/23/05 08:57:42 

### 08123105 08:57:52 08/23/05 08'58:02 08/23105 08:58:12 08/23/05 08:58:22 08/23/05 08:58:32 08. 1 23/05 08:58:42 08/23105 08:58:52 08/23/05 08'59"02 08/23/05 08:59:12 08/23/05 08:59.22 08/23/05 08'59'32 08/23/05 08:59:42 08/23/05 08:59:52 

### 08123105 09:00:02 

### 08123105 09:00:12 

### 08123105 09:00:22 08/23/05 09_00'32 08/23/05 09:00 42 08/23/05 09:00:52 08/23/05 09'01 :02 08/23/05 09'01 12 1.0 1.2 0.9 0.1 0.1 0.1 0.2 0.0 00 00 0.0 0.0 

### 09 00 

### 0.0 0.0 0.0 

### 0.0 00 00 01 

### 00 0.1 01 01 0.0 

### 0.0 0.0 

### 0.0 

### 00 00 0.1 0.1 0.5 O_i 0.1 0.0 

### 0.0 0.0 

### 0.0 

### 00 00 00 00 

### 0.0 00 00 00 00 

### 0.0 

### 0.0 0.0 

### 0.0 

### 0.0 0.0 0.0 0.0 09 1.0 1 0 11 1.0 0.1 0 0 

### 0.0 0.0 

### 0.0 

### 0.0 0.0 0.0 

### 00 0.0 2.9 2.9 

### 2.7 2.8 2.5 2.6 

### 2.7 2.9 

### 2.7 2.7 2.7 2.5 2.5 

### 2.4 2.5 

### 2.4 

### 24 24 

### 2.5 2.5 2.4 2.6 

### 2.5 

### 2.4 2.3 2.6 2.6 

### 2.7 

### 2.4 

### 2.5 2.4 2.4 2.4 2.4 2.6 

### 2.6 19.2 52.9 68.7 

### 77.6 84.7 88_6 91_6 94.0 95.7 97_1 97_9 99_1 99.7 100.3 100.3 100.6 100.3 100.7 

### 100.6 101.2 101.2 101.2

100.9 95.5 78.1 47.3 25.7 14.3 

### 9.6 7.5 

### 6.3 

### 54 4.8 44 4.3 

### 3 9 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 4.2 

### 9 7 13.7 16.9 19.2 20.9 21.9 22.7 23.1 23.4 23_7 23.8 23.9 24 

### 0 24.1 24.2 24.2 24 3 24.4 24 

### 3 

### 24.4 24.4 24.4 24.4 24.3 24.4 24.2 20.7 10.8 

### 6.7 4.9 3.5 2_5 1.8 1.4 1.1 

### 0.9 0 7 0.5 0.4 

### 0.3 0.3 0.2 0.2 0.2 

### 0.1 0.2 0.1 0.1 0.1 01 0.1 0.2 

### 02 0.2 

### 0.4 04 04 04 04 

### 04 04 04 1.2 1.1 1 0 11 

### 1 0 1.0 1.0 

### 0 9 

### 0.8 0.8 0.8 0.8 0.8 0.8 0.8 0.9 0 9 

### 0 9 0 9 0 9 1.0 

### 0 9 

### 0.9 0.8 0 8 0.7 0.7 0.7 

### 0.8 

### 0.8 0.7 0.8 0.8 0.8 0.8 0.9 0.8 0.8 0.8 0 9 1 0 1 0 1 0 0.9 

### 0 9 1 0 1.0 0.9 

### 0.8 0 9 

### 0.9 0.8 0.8 0 9 0.9 

### 0.9
1 0 0.9 0.9 

### 0.8 07 0.7 

### 0.9 11 3.2 

### 8.2 14 4 19_8 24 2 28 1 31 4 34 2 8/23/05 Cal1brat1ons

25_5 ppm NOx Bias Zero CO, S02 Bias

99 1 ppm CO Bias Zero VOC, NOx B1as

Page 3 

# 25

# I



# I I 

# I I I I I I I I I 

# I I I I I I 

# I 08123105 09:01 22 08123/05 09 01 :32 08123/05 09'01 :42 08/23/05 09:01 :52 

### 08/23/05 09.02:02 08/23/05 09:02:12 08/23/05 09:02:22 08/23/05 09:02:32 

### 08/23/05 09:02.42 08/23105 09:02.52 08/23105 09:03•02 08/23/05 09:03'12 08/23/05 09:03:22 

### 08/23/05 09:03.32 08/23/05 09:03.42 08/23/05 09:03:52 08/23/05 09:04:02 

### 08/23/05 09:04:12 08/23/05 09:04:22 08/23/05 09:04:32 

### 08/23/05 09:04:42 08/23105 09:04:52 

### 08/23/05 09:05.02 08/23105 09:05:12 08/23/05 09:05:22 08123/05 09:05'32 08/23/05 09:05.42 08123!05 

### 09:05:52 08123105 09:06:02 08123105 09:06.12 08/23/05 09:06:22 08/23/05 09:06'32 08/23/05 09:06'42 08/23/05 09:06:52 08/23/05 09:07'02 08/23/05 08:07' 12 

### 08/23/05 09:07.22 08123/05 09:07:32 08/23/05 09:07'42 08/23/05 09:07"52 08/23/05 09:08:02 08/23/05 09:08:12 08123/05 09:08:22 08/23/05 09:08:32 08123/05 09:08:42 08/23/05 09:08:52 08/23/05 09:09:02 08/23/05 09:09:12 08/23/05 09:09:22 08/23/05 09:09:32 

### 08123105 09:09:42 08123/05 09:09:52 08/23/05 09:10:02 08123/05 09:10.12 08/23/05 09:10:22 08/23/05 09:10:32 

### 08123105 09:10:42 08/23/05 09:10:52 08123/05 09:11:02 08/23/05 09:11 :12 08/23/05 09.11 :22 08/23/05 09:11:32 08123/05 09:11 :42 08/23/05 09:11 :52 08123/05 09:12:02 08123/05 09:12"12 08/23/05 09:12:22 

### 08123105 09:12:32 08/23/05 09:12:42 08123/05 09:12:52 08123/05 09:13:02 0.0 0.0 0.0 

### DO 0.0 0.0 0.0 0 0 0 0 

### 0.0 0.0 00 -0.1 

### 0.0 0.0 0.0 

### DO DO 0.0 00 

### DO 0.0 

### DO DO DO 0.0
0.0 

### DO DO DO 0.0 0.6 1.0 1.0 1 0 1ee 28.6 28.6 28.6 28.6 28_7 

### 28.7 28.7 28.8 28.8 28.7 28_6 10.5 1.2 12 11 20.0 49.1 

### 49.2 49.1 49.1 49.2 49.3 47.1 4.6 1.3 1.3 6.6 14_7 14_7 14.7 

### 14.7 14.7 14.7 14.8
14.7 4.0 3.7 3 7 3.8 3.7 38 3 7 3.8 

### 3.6 3.8 3.7 

### 3.9 3.7 4.0 4.0 4.1 4.0 4.2 4.0 3.7 

### 3.6 

### 3.4 3.3 3.5 

### 3.4 3.4 3.4 3.8 3.3 

### 3.4 3.3 3.3 3.2 3.6 3.8 4.2 4 0 4.2 4.0 4.1 3.7 

### 3.8 3.8 

### 3.9 

### 3_7 3.9 39 39 3.8 39 4.1 

### 3 7 41 4.0
·1 6 -5_8 

### 39 3.7 3.7 3.7 

### 3.4 3.6 3.8 4.0 

### 3.9 4.0 3.9 4.1 4.0 

### 4 2 4 3 04 04 

### 0.4 0.4 0.4 0.4 0.4 0.4 0.4 0.4 0.4 0.4 04 04 

### 0.4 0.4 0.4 0.4 04 

### 0.4 0.4 0.4 0.4 0.4 0.4
04 

### 0.4 0.4 04 

### 0.4 0.4 0.4 0.4 0.4 0.3 03 

### 03 0.2 0.2 0.2 

### 0.2 0.1 01 02 

### 02 0.1 0.1 0.1 0.1 0.1 01 0.2 0.2 

### 0.3
02 01 0.1 0.1 0.1 0.1 0.1 0.1 0 1 0.2 0.2 0.2 0.2 0 1
0.1 0 1 01 36.4 38.7 40.4 41_5 42_5 43.2 43.8 44.5 45_1 45_5 45.9 46 1 46 

### 3 46.5 46.6 46.8 47.1 47 4 47.5 47.5 47.5 47.6 47.7 47.8 

### 47.9 48.0 48.0 47.9 47.9 48.0 47.8 46.3 44 7 43.6 42 0 38.6 

### 32 6 26_0 20.8 17.0 14.4 12.4 11 0 

### 9.6 8.5 7.7 

### 7.0 6 3 5.7 

### 5.3 51 5.0 5.0 5.0 4.9 

### 52 5.1 4.8 4.5 4.2 40 

### 3.9 3.9 39 40 40 3.9 

### 39 3.8 3.6 35 8/23/05 Calibrations

50_1 ppm 802 Bias

28 8 ppm C3H8

48 8 ppm C3H8



# 2 

# r .l Page 4

# I

8/23/05 Calibrations



# I

08/23/05 09:13:12 14.7 4 2 0.1 

### 34 08/23/05 09.13:22 14.3 40 0 1 

### 3.3 

# I 08/23/05 09:13'32 

### 2.6 39 0.1 

### 3.3 08/23/05 09:13:42 

### 1.2 4 1 0 1 

### 3.2 

# I I I I I I I I I I I I I I I 27 

# I Page 5

# I

I I I I I I I I I I I I I I I I I I DatefTime mm/dd/yy hh:mm·ss 08/23/05 09.28.22 08/23/05 09.28:32 08/23/05 09:28:42 08/23/05 09:28:52 08/23/05 09:29:02 08/23/05 09:29:12 08123/05 09'29 22 08/23/05 09'29:32 08/23/05 09:29:42 08/23/05 09.29:52

Start Run t'1 08/23/05 09:30:02 08/23/05 09.30:12 08/23/05 09:30:22 08/23/05 09:30.32 08/23/05 09:30.42 08/23/05 09.30:52 08/23/05 09:31:02 08/23/05 09:31 '12 08/23/05 09:31:22 08/23/05 09:31 .32 08/23/05 09:31:42 08/23/05 09:31:52 08123105 09:32:02 08/23/05 09:32:12 08/23/05 09:32:22 08/23/05 09:32:32 08/23/05 09.32.42 08/23/05 09:32.52 08/23/05 09:33:02 08/23/05 09:33:12 08/23/05 09_33:22 08/23/05 09:33:32 08/23/05 09:33:42 08/23/05 09:33:52 08/23/05 09:34:02 08/23/05 09:34:12 08/23/05 09:34:22 08/23/05 09:34:32 08/23105 09:34.42 08/23/05 09:34:52 08/23/05 09:35:02 08/23105 09:35:12 08123/05 09:35:22 08/23/05 09:35:32 08123105 09:35:42 08123/05 09:35:52 08/23/05 09:36:02 08/23/05 09:36:12 08/23/05 09:36:22 08/23/05 09:36:32 08/23/05 09:36:42 08/23/05 09:36:52 08/23/05 09:37:02 08/23/05 09:37:12 08/23/05 09:37:22 08/23/05 09:37:32 08/23/05 09"37.42 08/23/05 09:37:52 08/23/05 09:38:02 08/23/05 09:38.12 08/23/05 09:38:22 08/23/05 09:38:32 08/23/05 09"38:42 08/23/05 09:38:52 08/23/05 09:39:02 08/23/05 09'39:12 08/23/05 09:39:22 08/23/05 09.39"32 08/23.105 09·39'42 08/23/05 09'39'52 VOC CO NOx 502 ppm ppm ppm ppm 4.4 83.8 21 5 2.8 4.2 85.1 21.5 2.7 4.2 86.3 21.5 2.6 42 4.1 4.2 42 4.2 4.2 4.4

4.5 4.5 4.4 3.8 3.8 4.0 4.0 39 4.0 3.8 4.1 4.0 39 

### 3.6 3.3 

### 36 3.3 3.4 

### 3.6 3.8 

### 3.6 3.8 3.9 3.5 

### 3.6 3.3 3.5 34 3.9 3.5 

### 36 4 1 3 7 37 39 39 3.8 38 40 4.5 4.3 41 4.0 3.9 3.8 3.8 3.9 3.8 3.9 

### 42 4.6 4 2 4.3 4.2 4.2 4.2 4.1 4 3 46 45 84.9 84.4 84.4 84.5 85.4 86_5 87.2

88.0 89.3 90.1 90 9 92 4 92.0 91 4 92_3 90_9 88_0 86.2 85.5 84.7 86.1 87.5 87.4 88.2 95.0 97.9 92.9 88.3 84.4 79.8 77.6 75.2 728 70_9 38_7 69_1 67_5 66_5 65.7 65_5 65_1 65.2 

### 65 3 65_8 66.7 674 69 1 70 1 71_2 73 1 74_9 76_9 78.4 79_9 80_9 81.3 81.7 81.5 81.3 81 3 81 1 81.3 81_5 81_5 82

**~** 82 6 83 6 21.6 21_7 21.6 21_6 21.5 21.5 21.6

21.7 21.6 21.8 22 0 21 9 22.0 222 22 1 22.2 22.3 22.1 22.1 22.0 22.0 21.7 21.7 21.8 21.6 21.5 21.7 21.6 21.5 21.6 21.7 21 7 22_0 22_2 22_2 22_3 22 4 22_5 22_5 22_6 22_6 22.4 22.3 22.2 22.0 

### 222 22 1 221 22 1 220 22_0 21.9 21_7 21_6 21_6 21.6 21.7 21 8 21.9 221 221 221 22 0 21.8 21_8 220 21 9 2.6 2.6 2.5 2.4 2.4 23 

### 2 3

2.3 2.3 2.3 24 2.3 2.3 2 2 2.2 2.3 2.3 2.3 2.2 

### 22 22 22 2.3 

### 22 2.3 2.3 2.3 2.2 

### 22 2.2 2.1 21 2.1 21 1 9 2 1 21 2 1 21 21 21 21 2.2 2.1 2.2 21 

### 21 2.3 

### 22 21 21 

### 22 21 2.2 2.2 22 

### 22 2.3 2.3 2.3 2 1 21 

### 22 22 

### 20 2.1 22 8/23/05 Run #1

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### 09:40:02 08/23105 09:40.12 

### 08/23/05 09:40:22 08123105 

### 09:40:32 08/23/05 09:40:42 08/23105 09:40:52 08/23/05 09:41:02 08123105 09:41 :12 08/23/05 09:41 :22 08/23/05 09 41:32 08/23/05 09:41:42 08/23105 09:41:52 08/23/05 09:42:02 08/23/05 09:42:12 08/23105 09:42'22 

### 08/23/05 09:42:32 08/23/05 09'42.42 08/23/05 09:42:52 08/23/05 09'43"02 08/23/05 09:43:12 

### 08/23/05 09:43:22 08123/05 09:43:32 08/23/05 09:43:42 08/23/05 09:43:52 08/23/05 09:44:02 08/23/05 09:44.12 08/23/05 09:44:22 08/23/05 09:44.32 08/23/05 09.44:42 08/23/05 09:44:52 08/23/05 09.45:02 08/23/05 09.45:12 08123105 09:45:22 

### 08/23/05 09:45:32 08/23/05 09:45.42 08/23/05 09 45.52 08/23/05 09 46-02 08/23/05 09 46-12 08/23/05 09 46:22 08/23/05 09'46:32 08/23/05 09 46:42 08/23/05 09:46.52 

### 08123105 09:47:02 

### 08123105 09:47:12 

### 08123105 09:47:22 08/23/05 09.47:32 

### 08123105 09.47:42 

### 08123105 09:47:52 08/23/05 09.48:02 

### 08123105 09 48:12 

### 08123105 09:48.22 08/23/05 09:48:32 08/23/05 09.48:42 08/23/05 09:48:52 

### 08123105 09:49:02 08/23/05 09:49.12 08/23/05 09:49"22 08/23/05 09'49:32 08/23/05 09:49:42 08/23/05 09'49:52 08/23/05 09:50:02 08/23105 09:50:12 08123/05 09:50'.22 08/23/05 09:50:32 08/23/05 09:50:42 08/23/05 09:50.52 08/23/05 09 51:02 

### 08123105 09:51:12 

### 08123105 09:51:22 

### 08/23105 09'51 '32 08/23105 09 51:42 08/23105 09 51:52 08/23/05 09.52:02 08/23/05 09·52: 12 4.5 

### 4.4 4.4 4.4 43 4.5 4.3 

### 4.4 4.6 4.6 4.6 4.9 4.9 

### 5.0 4.5 45 4.8 4.6 

### 5.0 4.8 4.5 4.5 4.5 4.8 4.6 46 4.5 4.6 4.5 44 

### 4.4 4.3 4.6 4.3 4.6 4.8 45 4.7 4.6 5.1 4.5 44 4.5 4.6 4.4 44 46 4.6 4.8 4.6 4.5 4.3 

### 4.4 4 5 46 45 

### 5.2 4 9 4.6 4 6 4.7 4.8 4.7 4 9 

### 5.0 4.7 4.6 4.8 45 4.4 4.0 

### 3.8 

### 37 3 6 84.4 85.4 86.9 87_7 88.2 88_8 89 1 89.8 90.5 91.2 91_9 92_2 92_6 93_0 92_9 93.0 93.3 93.5 93.9 93.9 93.9 94.4 93.9 93.6 93.0 92.2 92.0 91 _7 91.8 92.3 92 1 92 3 92.6 92.4 92.7 92.8 92.3 92_3 92 1 921 92_9 93_5 93.7 93.8 93.9 94.2 94 4 95_0 95_6 95_8 95_9 95.8 95_9 96.1 96.4 96.8 96.9 97.0 96.9 96 5 96_2 96_2 96_1 96.2 96.7 96.8 96 9 97_3 97_6 98.3 99.3 gg 

### 6 100_1 100.4 21.9 22.1 22.1 22.0 

### 22 0 22_0 22.2 22_2 22.3 22.3 22.3 22.2 22.3 22.3 22.3 22.3 22.3 22.3 22.3 22.4 22.3 22.4 22_4 22.4 22.5 22.6 22.7 22.7 22.7 22.6 22.4 22.4 22.7 

### 227 23.0 23 1 23.1 23.0 23.1 23.2 23.2 23.3 23.4 23.4 23.4 23.5 23.3 23.2 23.2 23.2 23.1 23.0 22_9 22.7 22.8 22_7 22_6 22.6 22.7 22.7 22.7 22.7 22.7 22.6 22_7 22.4 221 21.9 21.8 21.9 221 221 22.4 22_5 2.3 2.3 2.2 

### 21 21 22 23 2.3 2.3 2 3 2.3 

### 2.2 2.2 2.3 23 2 3 2.3 

### 2.4 2.4 24 2.4 2.3 2.3 2.3 22 22 

### 22 2.2 2.2 2.3 2.3 23 2.3 

### 2.4 2.4 24 24 2.3 2.3 

### 24 2.5 

### 2.4 2.4 2.4 2.4 2.5 2.3 23 2.3 2.3 2.3 

### 2.4 2.4 2.4 2 5 

### 2.4 24 24 

### 24 25 2.6 

### 26 

### 24 24 25 26 2_5 2.5 

### 2.4 24 2.3 

### 24 

### 2.4 2.5 8/23/05 Run #1



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# I I I I I I 08/23/05 09-52:22 

### 08123105 09:52·32 08/23/05 09:52:42 08/23105 09:52:52 08/23/05 09:53-02 08/23/05 09'53:12 08123105 09:53:22 08/23/05 09:53:32 08/23/05 09:53:42 08/23/05 09:53:52 08/23/05 09:54:02 08123105 09:54:12 08/23/05 09:54:22 08/23/05 09:54:32 08/23/05 09:54:42 08123105 09:54:52 08/23105 09"55:02 

### 08123105 

### 09:55·. 12 08/23/05 09:55:22 08/23/05 09:55:32 08/23/05 09:55'42 08123105 09:55:52 08123105 09.56:02 08/23/05 09:56:12 08/23/05 09:56:22 08/23/05 09:56:32 08/23/05 09:56:42 08123105 09-56:52 08123105 09:57:02 08123105 09:57:12 08/23/05 09:57:22 08/23/05 09:57.32 08/23/05 09:57:42 08/23/05 09:57:52 08123105 09:58:02 08/23105 09:58:12 08/23/05 09_58•.27 08/23/05 09:58:32 08/23/05 09:58:42 08/23/05 09:58:52 08/23/05 09:59:02 08123/05 09.59'12 08/23/05 09:59:22 

### 08/23105 09:59:32 

### 08123105 09:59:42 08/23/05 09"59:52 Port Change 

### 08123105 10:00:02 08/23/05 10:00:12 08/23/05 10:00:22 08/23/05 10'00:32 08/23/05 10:00.42 08/23/05 10:00:52 

### 08123105 10'01:02 08123/0510:01:12 08123/05 10:0122 08/23/05 10.01:32 

### 08123105 10:01:42 08/23/05 10.01:52 08/23/0510:02'02 08/23/05 10'02.12 08/23/0510:02:22 08/23/05 10:02:32 08/23/05 10.02:42 08123/05 10:02:52 08/23/05 10'03:02 

### 08123105 1 o·o3 12 08/23105 1 0'03:22 08123/05 10:03:32 

### 08123/05 10·.03:42 08/23/05 10:03:52 08/23/05 10:04:02 

### 08123105 10.04:12 08/23/05 10:04:22 3.7 3 9 39 3.6 

### 3.4 3.4 3.4 3.4 3.4 3.7 3.7 

### 3.4 3.4 3.5 

### 3.4 3.4 3.5 3.6 3.6 3.6 3.7 36 

### 3.5 3.5 3.5 3.4 

### 3.4 3.3 3.2 33 3 4 

### 3.4 3.5 3.8 

### 3.5 3.6 39 3.7 4.2 

### 4.4 4 0 3 7 3.6 3.6 3.6 34



### 3.4 1.7 1.3 

### 1.4 1 4 

### 1.4 1.5 1.5 1.5 1.4 1.3 1.2 1.3 1.4 1.3 1 3 1.2 1 2 1 3 1.2 1 3 1.3 1.3 1 5 1.4 1.3 

### 30 99.8 98.4 97.1 95.3 93 4 91.3 89.1 87.8 85.8 84.1 82.5 80.5 78.5 77.3 77.0 78.1 79.8 80.6 81.7 83.3 84.6 85.9 86.2 86 8 87.3 87.8 88.2 88.0 87.7 87.4 86.7 85.5 85.4 85.2 84.2 84.3 

### 8" 84.0 84.2 84.2 83.7 84.7 86.9 88.2 88.5 89.4

90.5 90.8 88.8 62.9 37.2 22.3 15.0 11.1 8 9 7.2 6.2 57 55 5.1 5.2 5.1 

### 50 48 4.6 4 9 4.8 4.8 

### 52 53 54 5.6 

### 53 22.7 23.0 

### 23 2 23.2 23 3 

### 23.4 23.3 23 4 23.5 23.5 23.6 23.5 22.9 

### 227 22.7 22.4 22.3 22.3 22.1 22.1 22.1 22.0 22.0 22.0 21.9 21.9 21.8 21 8 21.9 21.9 22.0 22.2 22 2 22.3 22.6 22.5 22.4 22.5 22.3 22.3 22.2 21.8 21.7 21.8 21.8 21.6

21.5 21.5 212 17.0 10.8 72 51 40 3.4 

### 3.0 

### 27 24 23 2.2 

### 20 1.9 1 8 1 7 1 6 

### 1 5 1 5 1.4 

### 14 

### 1.3 1.2 1 2 12 2.5 

### 24 2 5 

### 24 

### 2.4 2 4 2 5 

### 2.4 2.4 2.3 2.4 25 2.5 

### 2.4 2.5 25 25 2 5 2.5 2.5 

### 24 25 25 2.5 

### 2.4 2.4 24 

### 2.4 2.5 2.5 2.6 2.5 

### 2.4 2.4 2.5 25 2.5 2.5 2.5 2.5 25 2.5 25 2.5 2.5 

### 2.4

2.4 2.4 2.5 2.6 2.5 2 4 

### 2.4 23 22 

### 2.2 2.2 2.2 

### 2.3 22 

### 22 2.2 

### 2.3 2.3 

### 2.3 2.3 

### 23 22 2 3 2.3 2.3 23 22 8/23/05 Run #1



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I I I I I I I I I I I I I I I I I I 08!23!05 10:04:32 08!23105 10'04:42 08/23/05 10.04.52 Resume Sampling 08/23/05 10:05:02 08/2310510:05:12 08/23/05 10:05:22 08/23/05 10:05:32 08/23/05 10:05:42 08/23/05 10:05:52 08/23/05 10:06:02 08/23/05 10:06:12 08123/05 10:06:22 08/23/0510.06:32 08/23/05 10'06 42 08/23105 10:06:52 08123105 10:07'02 08/23/05 10:07:12 08/23105 10:07:22 08123/05 10:07:32 08/23/05 10:07:42 08/23/0510:07:52 08!23105 10:08:02 08/23/05 10:08:12 08/23/0510:08:22 08!23!05 10:08:32 08/23/05 10:08:42 08!23105 10:08 52 08/23105 10:09·02 08/23/0510:09:12 08/23/05 10:09:22 

### 08/23/0510:09·32 08/23105 10:09'42 08/23/05 10:09:52 08/23/05 10"10:02 08/23/0510'10'12 08!23105 10:10·22 08/23/0510:10'32 08/23/05 10:10:42 08/23/05 10 10:52 08/23/0510:11:02 08/23/05 10:11.12 08/23/05 10:11.22 08/23/05 10:11:32 08/23/05 10:11:42 08/23/05 10:11:52 08/23/0510:12:02 08/23/0510:12:12 08/23/0510"12.22 08/23/0510"12:32 08/23/05 10:12:42 08/23/05 10:12:52 08!23105 10:13:02 08/23/0510:13:12 08/23/05 10:13:22 08/23/0510:13:32 08/23/05 10:13:42 08/23/0510:13:52 08/23/05 10:14:02 08/23105 10:14:12 08/23/05 10.14:22 08/23/0510:14:32 08/23/05 10:14:42 08/23/0510:14"52 08/23/05 10:15:02 08/23105 10"15:12 08/23105 10:15:22 08/23/05 10"15:32 08/23/0510"15:42 08/23/05 10:15.52 08123/05 10.16.02 08123/0510"16·12 08123/0510"16:22 08/23/05 10.16.32 3.9 3.9 3.8



### 35 34 33 3.3 

### 3.2 3.4 

### 3.3 3.3 33 3.4 3.6 38 3 7 3.9 

### 34 

### 3.4 3.2 3.2 3.2 3.4 3.3 

### 3.2 3.3 3.8 3.6 3.8 4.1 38 35 3.5 3.6 3 7 3.5 3.5 

### 3.4 3.5 3.6 3.6 3.6 3.6 3.7 38 4.0 4.1 4.1 4.5 4.5 4.3 4.3 4 1 40 4.1 

### 4.4 4.1 40 4.0 

### 43 4.3 44 4.7 4.3 4.1 4.1 4 2 42 41 4.1 4.1 4.0 3.9 5.6 19.8 41.8

54.7 59.7 60.6 59.1 56.4 

### 53 7 51.9 50.9 50.4 50 8 52.2 52.8 54 1 56 5 57.7 60.1 61.8 64.3 66.4 67.2 68.1 68.9 68.1 68.3 68.0 69.0 70.5 71.5 73.9 76.3 78.4 80.5 82 1 83.3 84 2 84 6 84.8 85 0 84.7 84.6 84.6 84.8 85.1 84.8 84.5 84.6 84.9 85.6 86.9 87.7 88.3 88.4 88 1 88.0 88.0 88.1 88.2 88.2 88.4 88 7 88 4 88.5 89 1 89 4 89 1 89.1 89.1 90 1 90.9 91.4 11 2.9 91

13.9 16.3 177 18.8 19.2 19.6 20.0 20.0 20.2 20.6 20.4 20.2 20.3 20.1 19.8 20.0 19.9 19.6 19.8 20.0 20.2 20.0 19 6 19.5 19.5 19.3 19 4 19.5 19.8 19.9 19.8 19.9 19 7 19.6 19 8 19.9 20.0 20.3 20.7 20 8 20.9 20.6 20.5 20.6 20.6 20.8 20.8 20.7 20.5 20.4 20.4 20.7 20.9 21.1 21.4 214 21.5 21.2 21.0 213 21.4 21 4 215 21.5 215 21.4 21.5 21 5 

### 217 21 7 2.2 2.2 

### 23

23 

### 2.3 2.4 24 24 2.6 2.6 2.5 24 2.5 2.5 2.6 26 2 5 25 25 2.5 2.6 2.6 

### 2.4 24 2.5 2.5 2.6 2.5 2.5 25 26 26 2.5 2.5 2.5 

### 25 2.5 2.5 2.6 2.7 2.7 2.8 2.7 26 2.7 26 2.7 2.7 27 2.6 2.5 2.6 2.7 2.6 2.5 26 2.6 2.6 27 

### 28 2.8 2.8 2.7 2.7 2.6 2.6 2 6 2.6 27 

### 28 2.8 27 

### 28 8/23105 Run #1



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### 08123105 10:17:22 08/23/0510:17:32 08/23/0510:17:42 

### 08/23/0510:17:52 08/23/0510:18:02 08/23/0510:18.12 

### 08/23/05 10:18:22 08/23/0510:18:32 08/23/05 10:18:42 08/23/05 10:18:52 08/23/05 10:19:02 08/23/0510.19.12 08/23/05 10.19:22 

### 08/23/05 10:19:32 08/23/05 10:19'42 08/23/0510'19:52 08/23/05 10:20:02 

### 08/23/0510:20:12 08/23/05 10'20:22 08/23/05 10:20.32 08123105 10:20:42 08/23/05 10:20.52 08123105 10:21.02 08/23/05 10:21:12 08/23/05 10:21:22 

### 08/23/05 10:21:32 08/23/05 10:21 42 08/23/05 10:21:52 

### 08/23/05 10:22:02 08/23/0510:22:12 

### 08/23/05 10:22:22 08/23/05 10:22:32 08/23/0510:22:'12 08/23/05 10:22:52 08/23/05 10:23:02 08/23/05 10:23:12 08/23/0510:23:22 08/23/05 10:23:32 08/23/05 10.23.42 08/23/05 10.23:52 08/23/05 10:24:02 08/23/0510.24:12 08/23/05 10:24:22 08/23/05 10:24:32 08/23/05 10:24:42 08/23/05 10:24:52 08/23/05 10:25:02 08/23/0510:25:12 08/23/05 10.25:22 08/23/05 10:25.32 08/23/05 10:25 42 08/23/05 10.25:52 08/23/05 10.26:02 08/23/05 10:26.12 08/23/05 10:26:22 08/23/05 10:26:32 08/23/05 10:26:42 08/23/0510:26:52 08/23/05 10:27:02 08/23/0510.27"12 08/23/05 10:27:22 08/23/05 10'27:32 08/23/05 10:27'42 08/23/05 10:27:52 08/23105 10:28:02 08/23/05 10:28:12 08/23/05 10'28:22 08/23/05 10'28'32 08/23/05 10:28:42 

### 08123105 10'28.52 38 3 7 

### 3 7 3.6 

### 3 7 3.9 

### 3 7 39 3.6 3.8 4.1 

### 3 7 3.8 3.9 3.8 3.6 3.7 

### 35 3.5 3.6 

### 3.5 3.5 3.3 3.4 

### 3.8 36 3.4 3.3 

### 3.5 3.5 3.7 3.4 3.6 3.6 

### 3.5 3.6 3.7 3.9 3.9 

### 3.8 3.8 38 39 4.0 4.0 4.0 

### 42 4.3 4.3 4.2 4.0 4.0 40 4.2 4.0 4.2 4.3 4.2 42 4.1 3.9 4.2 41 4.2 40 4.0 4.2 4.3 4.3 4.4 4.5 4.3 42 4.4 92_3 

### 91_3 89.5 88.3 

### 87 1 85.6 84.6 83.3 

### 82 4 81 6 79.7 78.6 78_5 78.4 79 2 80.6 81.3 82.3 83.1 

### 83.3 84.4 85.1 85.5 86.5 86.8 87 1 87 4 86.9 87.0 86.4 85.7 85.6 85_3 85.5 

### 85 6 85.2 86 0 86.2 

### 86.3 87.1 87.8 87.8 88.5 89.1 

### 89.7 90 6 91 _4 91 9 92_8 93.5 

### 93.9 94_8 95.4 

### 95.6 95.9 95.1 

### 94.8 94_4 93 8 93 

### 7 93.2 92.8 

### 93.0 92.7 91.4 90 8 90 2 89 5 90 5 91 2 92.0 

### 92.9 93.1 93 5 21 8 21 7 21.6 21.6 21 4 21.4 21.6 21.5 21 6 21 6 21.5 

### 214 21.4 21 3 21.6 21.7 21.9 22.0 22.1 22.1 22.2 22.1 22.0 221 223 22.2 22.2 22.2 22.3 22.5 22.5 22.6 22_5 22_3 22.3 22.1 22.2 22.2 21.9 21.8 21_9 21_8 21.5 21.6 21.6 21_6 21.6 21_6 21.4 21.2 21.2 21.0 21 1 21.2 21.3 21.3 21.4 21.5 21.5 21_6 21_6 21.6 21.6 21.5 21.6 21.5 21_6 21 5 21 4 21_3 21 1 21 1 21.1 21 0 

### 28 2.8 2.8 28 2.8 2.8 28 2.7 28 2.8 2.8 2.8 28 2.7 2.7 2.8 2.8 2.7 2.7 2.7 2.7 27 2.7 2.6 2.6 2.5 2.6 

### 26 27 27 

### 26 2.5 2.6 

### 2.7 28 2.8 2.7 2.7 2.8 27 2 7 2.6 

### 2.7 2.7 2.8 2.8 2.8 2.8 2.8 28 2.8 2.7 2.8 2.8 2.8 27 27 2.8 2.8 2.8 28 2.8 2.8 2.9 2.8 28 2.9 2.8 28 2.8 2.8 2_9 

### 2.9 29 8/23/05 Run #1



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### 10:29.22 08/23/05 10.29:32 

### 08123105 10.29'.42 08123105 10.29.52 

### 08/23/0510'30:02 08/23/0510:30:12 08/23/05 10:30.22 08123105 10'30:32 

### 08/23/05 10'30:42 08/23/05 10:30.52 08/23/0510:31:02 08/23/0510.31:12 08123105 10:31.22 08/23/0510'.31:32 08/23/0510:31:42 08123105 10:31 :52 

### 08123105 10:32:02 08/23/0510 32:12 08/23/05 10:32:22 08/23/05 10:32.32 

### 08123105 10:32:42 

### 08/23/05 10:32:52 08123105 

### 10:33:02 08/23/05 10:33:12 08123105 

### 10:33:22 08123105 10:33:32 08/23/05 10:33:42 

### 08/23/05 10:33:52 08/23105 10:34:02 08/23/0510.34:12 08/23/05 10:34:22 08/23/05 10'34:32 08123105 10:34:42 08/23/0510:34.52
Stop Run #1

08/23/05 10.35•02 

### 08123105 10:35:12 08/23/05 10:35:22 08/23/05 10:35.32 08123105 

### 10:35:42 08/23/05 10'35:52 08/23/05 10:36:02 08/23/05 10:36.12 08/23/05 10 36·.22 08/23/05 10:36:32 08/23/05 10:36:42 08/23/05 10:36:52 08/23/05 10:37:02 08/23/0510:37:12 08123105 

### 10.37:22 08/23/05 10:37:32 08/23/05 1 

### 0'.3 

### 7A2 08/23/05 10:37'52 08/23/0510:38:02 08123105 

### 10:38 12 08/23/05 10:38:22 08/23/05 10:38:32 08/23/05 10:38:42 08/23/05 10:38:52 08/23/05 10:39.02 08/23/05 10.39:12 08/23/05 10:39:22 08/23/0510'39:32 08/23/05 10:39.42 08/23/05 10 39:52 08/23/05 10 40'02 08/23/0510-40:12 08123/05 10:40:22 08123105 

### 10:40.32 08/23/05 10 40:42 4.2 4 1 41 41 4.2 

### 40 38 39 41 4.3 4.2 4.1 

### 39 38 3.9 3.7 3.6 36 

### 33 32 3.2 3.1 3 1 31 3.1 3.1 

### 3.2 3.0 3.1 

### 3.2 3.2 3.6 3.6 3.3 33 

### 33

3.94

3 2 

### 27 1 4 1 3 1.3 

### 12 1.3 1.2 

### 12 12 1.2 12 1.3 1.3 1.2 12 1.2 

### 12 12 

### 12 11 1.2 11 11 

### 1 2 12 11 11 

### 12 11 1.1 11 11 11 11 

### 94.2 95.9 96.3 95.4 94 1 

### 93 6 93.1 93 7 93.6 92.2 91.6 91.8 91.8 92.1 92.6 92.4 93 2 94.5 95.9 97.7 97.1 94.6 92.8 90.3 87.5 86.0 82.4 78 6 

### 75.6 73.1 71.3 70.9 70.4 70.3 70.9 71 1



### 85.18

70.8 72.5 70.8 64.6 44.7 30.9 21.5 16.3 12.9 10 7 

### 95 8.8 8.1 7.6 

### 7.7 

### 75 72 7.2 7.1 7 1 

### 74 7.0 

### 7 1 70 6.2 6.3 6 1 6.1 6 1 6.1 

### 6 0 6 1 6 1 

### 60 6.3 

### 21.2 21 0 

### 20.9 20.9 20.9 21 0 

### 21.2 21 1 

### 21.3 21.4 21.1 21.2 21.2 21.0 21.2 21 

### 3 21.2 21 3 

### 21.5 21 3 

### 21 .5 

### 21.7 21.8 22.2 22.4 22.5 22.6 22.7 

### 224 22.3 22.2 22.1 22.0 22.0 22.1 22.2

21.73

22 2 

### 21.9 20.9 19.8 14.9 11.0 8.6 7.0 5.8 4.9 4.3 

### 3.9 35 3.3 

### 3.2 3.0 2.9 2.9 3.2 31 29 

### 27 24 

### 2.3 22 

### 2 1 2.0 

### 20 1.9 18 1.8 

### 17 1.7 1.6 1 6 2.9 2.9 29 2.9 

### 2.8 27 2.7 2.9 3.0 2.9 2.9 

### 2.8 2.8 2.8 2.8 2.7 2.8 27 28 2.8 29 30 2.9 2.9 3.0 2.9 29 

### 2.8 2.8 2.8 2.7 27 

### 2.8 2.7 2.7 

### 2.8

2.51

2 9 2.9 29 

### 2.8 2.7 2.7 28 27 

### 2.5 2.6 2.7 2.7 2.6 2.6 2.5 2.5 2.5 2.6 2.7 2.6 2.6 2.6 2.5 

### 2.6 2.6 

### 25 2.5 2.5 2.5 26 2.6 2.6 2.5 2.5 25 8123/05 Run #1



# 33

Page 6

# I



# I I 

# I I I 

# I I I I I I 

# I I I I I 

# I I 08123/05 "10.40.52 08123105 10.41:02 08/23105 1 0:41:12 08/23/05 10:41'.22 08/23/05 10:41:32 08/23/05 10:41:42 

### 08123105 10:41.52 

### 08/23/05 10:42:02 08/23/05 10:42:12 08/23/05 10:42:22 

### 08123105 10:42'32 

### 08123105 10.42'42 08/23/05 10:42:52 08/23/05 10:43:02 08/23/0510:43:12 08/23/05 10.43:22 

### 08/23/05 10:43:32 08/23/05 10:43:42 08/23/05 10.43:52 08/23/05 10:44:02 08/23/0510:44:12 08/23/05 10:44.22 08/23/05 10:44:32 08/23/05 10:44:42 08/23/05 10:44'52 08/23/05 10.45:02 08/23/0510:45:12 08/23/05 10.45:22 08/23/05 10:45:32 08/23/05 10:45:42 08123105 10:45:52 08123105 10.46:02 08/23/05 10:46:12 08/23/05 10:46'22 08123105 

### 10.46:32 08123105 10:46:42 08123/05 10:46:52 

### 08/23/0510:47:02 08/23/05 10:47:12 08/23/0510:47:22 08/23/0510:47:32 08/23/0510:47:42 08/23/05 10:47:52 08/23/05 10:48:02 08/23/05 10:48:12 08/23/05 10:48:22 08/23/05 10:48:32 08/23/05 10:48:42 08/23/05 10:48:52 08/23/05 10:49:02 08/23/05 10:49:12 08/23/05 10 49:22 08123/05 10:49:32 08/23105 10:49'42 08123/05 10 49:52 08/23/05 10:50'02 08/23/0510:50.12 08123/05 1 0'50:22 08/23/0510:50'32 08123/05 10"50:42 08/23/05 10·.50:52 08/23/05 10:51:02 08/23/0510·51·12 

### 08123105 1 0:51 .22 08/23/0510:51:32 08/23/05 10:51.42 08/23105 10'51:52 08/23/05 10:52:02 08/23/0510:52:12 08123/05 10'52:22 08/23/05 10:52:32 08/23/05 10·52'42 08/23105 10:52:52 11 1 2 1.1 1.1 1.1 11 1.1 1.2 1.1 

### 1.1 1.1 1.2 1.1 1.1 1.1 1.1 1.1 1.1 1.1 1.0 1.0 1.0 1.0 1.1 1 0 1.1 1.1 11 1.1 1.1 11 

### 1.1 04 0.1 0.1 0.1 0.0 01 

### 0 0 

### 0.0 0.1 

### 00 0.1 0 1 0 1 0 1 00 0 1 0 1 

### 00 0 0 00 

### 00 

### 00 00 0 3 

### 00 0 0 0.0 

### 0.0 0 0 00 0.0 0.0 0.0 

### 0.0 00 00 

### 0.0 

### 00 

# o.o o.o o.o 6.0 

### 6 0 6.3 6.1 6.2 6.0 6.1 62 

### 59 6.0 

### 5.9 5.8 6.1 

### 5.8 6.0 6.0 

### 5.9 6.1 

### 5.9 59 5.9 6.0 6.1 6.0 

### 5.9 6.1 5.7 60 

### 59 5.8 5.9 6.2 6.0 6.0 6.0 

### 5.8 5.9 6.0 

### 5.9 5.8 5.8 56 56 57 5.7 5.7 5.7 5.6 55 

### 54 54 

### 53 

### 5.1 5.2 5.2 

### 5.0 49 6 9 27.0 53.5 69.6 82.1 88.6 93.1 96.8 98.8 100 2 100.9 101.7 102.1 

### 102.3 102.3 102.3 16 1 5 1.5 1 4 1.5 14 1.4 1 4 1.4 1 4 1.3 1.2 1 3 10 1.2 1.2 1.1 1.1 

### 1.1 1.1 1.0 1.0 1.0 

### 09 0.9 0.9 0.9 

### 09 0.9 0.8 0.8 0 8 

### 08 0.8 

### 3.7 9.3 14.0 17.8 20.4 21.9 22.8 23 2 23.6 23 8 24.0 24.0 24.1 24.1 24.1 24.3 24.3 24.3 

### 24.4 24.4 24.4 24.2 24 3 23 6 18.5 11.4 

### 7.7 4 9 33 

### 2 3 1.6 11 

### 09 0.7 06 

### 05 0.5 

### 0.5 0.4 26 2.5 

### 24 2.4 2.4 2.4 24 2.4 2 5 

### 24 2.5 25 

### 24 24 2.5 25 2.6 2.6 2.5 2.4 

### 2.4 25 2.5 2.6 

### 2.5 2.5 

### 2.4 2.4 26 

### 25 2.5 2.6 

### 26 

### 27 2.5 

### 2.6 2.6 

### 2.5 25 

### 2.6 2.6 

### 2.5 2.4 

### 24 2.5 

### 26 25 2.5 2 5 

### 25 2.5 26 

### 2.5 

### 2.4 2.4 2.4 24 2.4 24 25 2.6 26 

### 2.6 25 

### 2.5 2.5 

### 2.5 2.5 

### 2.5 2.5 2.4 

### 25 26 8/23/05 Run #1

25.5 ppm NOx Zero CO, S02

99.1 ppm CO Zero VOC, NOx

Page 7 

# 34

# I

8/23/05 Run #1



# I

08/23/05 10:53:02 

### 0.0 102.4 0.4 26 08/23/0510:53:12 0.0 102.0 04 2.5 

# I 08/23/05 10:53:22 0.7 102.0 0.4 2.6 08123105 10"53:32 0.9 101.4 0.5 2.5 08/23/05 10:53:42 1.0 

### 95.7 0.4 2.6 08/23/05 10:53.52 1.0 77.8 0.4 2.6 08/23/05 10'54:02 0.8 

### 50.2 0.4 25 

# I 08/23/05 10:54:12 0.1 

### 28.9 0.5 2.5 08/23/0510:54'22 0.1 16.4 0 5 2.5 08/23/05 10:54:32 0.1 11.4 06 2.6 08/23/05 10:54:42 00 8.7 0.7 2.8 

# I 08/23/05 10 54:52 0 0 7.2 0.7 3.4 08/23/05 10:55:02 0.0 6.5 0.8 4.2 08/23/0510:55.12 0.0 6.2 0.8 5.0 08/23/05 10'55:22 0.0 6.0 0.8 76 

### 08123105 10"55:32 0.0 6.0 0.8 10.2 

# I 08123105 

### 10:55:42 0.0 5.8 08 12 7 08/23/05 10·55"52 00 5.7 0.8 15.7 08/23/05 10-56:02 00 5.7 0.8 18 8 08123105 10:56:12 0 0 60 0.8 21 8 08123105 

### 10:56:22 0.0 60 0.8 24.3 

# I 08123105 10:56-32 0.0 58 0.8 26 7 08123105 10:56'42 0.0 5.8 0.8 28 9 08/23/05 10:56"52 0.0 5.8 0.8 31 1 

### 08123105 10:57:02 0.0 5.7 0 8 33.2 

# I 08/23/05 10:57:12 0.0 5.7 0.8 34.9 08/23/05 10:57:22 0.0 5.4 07 36.4 08/23/05 10:57:32 0.0 5.5 0.8 37.8 08/23/05 10:57.42 0.0 5.5 0.7 

### 38.9 08123105 10:57:52 00 5.5 0.7 40.0 

# I 08/23/05 10:58:02 00 5.6 0.7 41.1 08/23/0510:58:12 00 55 0.7 42.0 08/23/05 10:58:22 00 54 0.7 42.7 08/23/05 10:58:32 00 5.7 0.7 43.4 08/23/05 10:58:42 0.0 5.9 0.7 44 1 

# I 08/23/05 10·58:52 00 59 0.7 44.8 08/23/05 10:59:02 0.0 5.9 0.7 45.3 08/23/0510:59:12 00 60 0.6 45.8 08/23/05 10:59:22 0.0 5.9 0.6 46.2 08/23/05 10:59:32 0.0 5.5 06 46.5 

# I 08/23/05 10:59:42 0.0 5.5 06 46.7 08/23/05 10:59.52 00 5.3 0.6 47.0 08123/05 11 :00.02 00 5.3 0.7 47.3 08/23/0511:00:12 0.0 5.8 06 47.6 

# I 08/23/05 11:00:22 0.0 5.8 0.6 47.8 08/23/05 11 :00:32 00 5.8 0.6 481 08123105 11 :00:42 00 6 0 0.6 48.2 08/23/05 11 :00:52 00 55 06 48.4 08/23/05 11:01:02 00 57 0 6 

### 48.6 

# I 08/23/0511:01:12 0 0 5.6 0.6 

### 48.8 50.1 ppm S02 08/23/05 11:01:22 00 5.5 0.6 

### 48.9 08/23/05 11:01:32 00 5.6 0.5 

### 48.9 08/23/05 11:01:42 0.1 5.8 05 48 4 

# I 08/23/05 11:01:52 11.7 59 0.5 47.0 08/23/05 11:02:02 

### 14.6 6.0 0.5 47.0 08/23/05 11:0212 

### 14.6 5.9 0.5 47.1 15.2 ppm C3H8 08/23/05 11:02:22 

### 14.7 59 04 46.4 

# I 08/23/0511.0232 

### 14.7 6.1 0.3 44 1 

# I I I 35 

# I Page 8

# I

I I I I I I I I I I I I I I I I I I Date/Time mm/dd/yy hh:mm·ss 08/23/05 11 '44:02 08/23/0511 44:12 08/23/05 11:44:22 08/23/05 11:44:32 08123105 11:44:42 08/23/05 11:44:52

Start Run #2 08/23/05 11:45:02 08/23/05 11'45:12 08/23/05 11 '45:22 08/23/05 11:45 32 08123/05 11:45 42 08123105 11:45:52 08123105 11 '46:02 08/23/05 11 :46'12 08/23/05 11 :46:22 08/23/05 11.46:32 08/23/05 11 :46'42 08/23/05 11 '46:52 08/23/0511:47:02 08/23/05 11 :4 7:12 

### 08123105 11:47:22 08123105 11:4 7:32 08/23/05 11:47:42 08123105 11:47:52 08/23/0511:48"02 08/23/05 11:48:12 08/23/05 11 :48:22 08/23/05 11:48:32 08/23/05 11:48:42 08123105 11:48:52 08/23/05 11 :49:02 08/23/0511:49:12 08/23/05 11:49:22 08/23/05 11:49:32 08/23/05 11:49:42 08/23/05 11:49:52 08/23/05 11:50:02 08/23/05 11 .50.12 08/23/05 11.50:22 08/23/05 11:50:32 08/23/05 11:50.42 08/23/05 11:50:52 08/23/05 11:51 :02 08/23/0511:51:12 08/23/05 11:51.22 08/23/05 11'51 :32 08/23/0511:51:42 08/23/05 11:51 :52 08/23/05 11:52:02 08/23/0511:52:12 08/23/05 11:52:22 08/23/05 11:52:32 08/23/05 11:52:42 08/23/05 11 .52:52 08/23/05 11:53:02 08/23/05 11:53:12 08/23/05 11 .53:22 08/23/05 11:53:32 08/23/05 11:53:42 08/23/05 11:53:52 08/23/05 11 .54:02 08123105 11:54:12 08/23/05 11 :54"22 08/23/05 11 '54:32 08/23/05 11-54.42 08123105 11:54:52 08/23/05 11 ·5s-oz 08/23/05 11:55 12 08/23/05 11:55:22 08/23/05 11"55:32 VOC CO NOx 502 ppm ppm ppm ppm 4.0 91.9 20.4 2.5 4.0 92.2 20.2 2.6 4.0 92.9 19.9 2.5 4.0 

### 4.3 4.4

4.2 4.0 4.1 41 4.2 4.0 4.0 4.1 4.0 3 9 

### 3.8 3 7 3.6 

### 35 3.8 3.9 

### 3.8 3.6 3.6 3 4 3.7 3 7 

### 3.5 3.7 3.9 4.1 40 

### 38 4.1 

### 38 3.8 3 9 3 9 3.9 4.0 

### 3.8 3.7 3.7 3.9 3.9 

### 3.8 4.0 4.4 4 5 4.1 3.9 

### 3.8 3.8 3.8 3.8 38 3.7 3 7 3.7 3.6 

### 3.5 3.5 3 3 

### 33 34 34 

### 35 3.5 3.4 93.2 93_4 94.2

95.1 95.5 96.2 96.0 96.0 96.7 97.8 98 1 97 8 97_3 97.1 96 6 95_4 93_6 91_8 891 87.3 85_3 82_1 79 9 79.0 78.2 78.0 78 6 79.5 80.4 

### 810 81_7 82_0 82 6 83.0 

### 84 3 85.6 86.7 88.0 88.5 89.4 90.6 90.6 91.5 92 5 92.4 93.3 94.0 94.2 94.9 95 7 95.4 95.4 95.9 95.4 95.5 96.0 95.7 96.5 97.3 97.3 97 4 97_1 95 7 94 7 93_7 91 5 90 0 19_8 19 6 19.5

19.8 19 9 20.0 20 1 20.2 20 0 20_1 19_8 19.8 19.9 20 1 20_2 20.4 20.7 20.8 20.9 21.0 20.9 20_9 20_8 20.5 20.6 20_7 20.6 20.9 20.8 ?0 6 20_7 20.6 20.7 20_8 20.9 21 0 21 

### 3 21.5 21 5 21.4 21.3 21_2 21 0 21.0 20_9 21.0 21.0 20.9 20.9 211 21 2 21_1 211 21 1 21_0 20 9 20 9 20 9 20 7 20.6 20 

### 5 20 5 20.5 20.8 20_8 20 8 20_9 2.4 25 24

2.5 25 

### 2.4 2.4 2.5 26 2.6 25 2.5 2.5 2 4 2.6 26 2.5 2.5 

### 2.4 2.4 2.4 

### 2.4 2.3 

### 2.3 24 2.4 24 

### 2.3 2.3 2.4 2.4 

### 2.3 

### 2.4 2.4 2 3 23 2.5 24 

### 23 2.3 2.3 

### 2.3 

### 2.4 25 

### 2.4 2.5 2.6 

### 2.4 2.4 24 23 

### 23 2.3 2.4 2.4 24 

### 2.3 2.4 24 

### 2.4 2.4 23 2_3 2.3 2.3 24 

### 2.3 8123!05 Run #2



# 36

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I I I I I I I I I I I I I I I I I I 08/23/05 11:55:42 08/23/05 11.55:52 08/23/05 11:56:02 08/23/0511:56:12 08/23/05 11:56.22 08/23/05 11:56:32 08/23/05 11"56:42 08/23/05 11 :56'52 08/23/05 11:57:02 08/23/05 11"57:12 08/23/0511:57:22 08/23/05 11 :57"32 

### 08/23/05 11.57:42 08/23/05 11:57:52 08/23/05 11:58:02 08/23/05 11:58:12 08123105 11:58.22 08123105 

### 11:58:32 08/23/05 11:58:42 08/23/05 11:58:52 08/23/05 11:59:02 08/23/0511:59:12 08/23/05 11 :59:22 08/23/05 11 :59· 32 08/23/05 11:59:42 08/23/05 11:59:52 08/23/05 12.00:02 08/23/05 12:00:12 08/23/05 12:00:22 

### 08123105 12:00:32 08/23/0512:00:42 08/23/05 12:00:52 08/23/05 12:01.02 08/23/0512:01:12 08/23/05 12:01.22 08/23/0512:01:32 08/23/05 12:01:42 08/23/05 12:01:52 

### 08/23/05 12:02'02 08/23/05 12:02:12 08/23/05 12:02.22 08123105 12:02:32 08/23/05 12:02:42 08/23/05 12:02:52 08/23/05 12:03:02 08/23/05 12:03'12 06/23/05 12:03:22 08/23/0512.03:32 08/23/05 12:03:42 08/23/05 12:03:52 08/23/05 12-04:02 08/23/0512.04:12 08/23/05 12-04:22 08/23/05 12:04:32 08/23/05 12:04'42 08/23/05 12'04:52 08/23/05 12:05.02 08/23/05 12.05:12 08/23/05 12:05:22 08123105 12:05:32 08/23/05 12:05.42 08123105 12:05:52 08123105 12.06:02 08/23/0512'06.12 08/23/05 12:06:22 08/23/05 12:06:32 08/23/05 12:06:42 08/23/05 12:06:52 08123105 12'07:02 08/23/05 12:07:12 08/23/05 12:07:22 08/23/05 12:07"32 08/23/05 12"07:42 08123105 12.07:52 36 37 3.8 3.9 3.9 3.9 3.9 3.9 3.9 4.0 4.0 4.4 4.3 41 4.1 4.1 4.0 41 4.1 4.0 4.0 

### 42 4.3 4.3 4.1 4.3 4.2 4.1 4.1 4.0 40 40 3.9 3.8 4.0 3.9 

### 3.9 3.9 4.0 

### 39 39 4.0 3.9 3.7 

### 3.8 3 7 

### 3.5 3.3 3.2 3.2 3.2 

### 3.2 3.3 

### 3.9 38 3.6 3.5 3.5 38 3.7 3 8 3 7 

### 3 5 35 34 

### 3.5 3.4 34 34 

### 3.5 36 3.6 36 3.7 

### 89_3 88.2 87 8 

### 88.0 88.0 88.4 88 9 

### 89.4 90.4 91.0 91.0 91.5 91.7 91.8 92.3 92.6 92.3 92.5 92.6 92.7 92.8 93_0 93.1 93.6 93 6 93.7 94.1 94.8 94.7 95.0 95.4 95:2 95 7 

### 95.9 951 

### 95.2 97.5 96.7 95.5 95.2 94_5 94.3 94.6 94.6 94.6 94.9 94.9 94.2 93_6 91_4 89 0 87_2 84 1 81.1 

### 79.2 778 76 9 

### 77_8 79.0 80.1 82.1 83.9 84.8 86.0 86.2 86.6 86.9 86.5 86 8 87.0 86 3 86.4 87.4 874 21.0 21 0 

### 21.0 21 1 

### 21.0 21 0 

### 21_1 21.1 21 1 

### 21.2 21.1 21.1 21.2 21.2 21.1 21_3 21 3 21 1 

### 21_0 21_1 21.0 21_0 20.9 20.8 20 9 

### 20.8 20.9 20 

### 8 20.6 20.4 20.2 20.2 20.2 20.3 20.7 20.8 20 6 

### 20.6 20 4 20.3 20.4 20.4 20.7 20.7 20.6 20.6 20.5 20.5 20_7 20 9 

### 21_0 21.3 21 5 

### 21.2 21.1 21.2 21 1 

### 20.8 20.8 20.8 20.6 20.4 20.4 20.3 20.4 20.5 20.6 20.7 20.6 20 6 

### 20.7 20 6 

### 20.5 20 4 2.3 23 24 

### 24 2.3 

### 2.3 23 2.3 24 

### 2.3 

### 2.2 2.3 

### 2.2 2.2 

### 2.3 2.3 

### 23 23 2.3 

### 22 2.1 21 

### 2.3 2 4 

### 23 

### 2.2 2.2 2.2 2.2 2.2 2.2 21 

### 2.2 2.2 2.3 23 23 

### 2.3 2.2 2.2 2.2 

### 22 2.2 21 2.1 2.1 

### 2.3 

### 2.2 2.2 22 

### 23 2.3 24 

### 23 2.3 2.1 21 

### 2 1 22 22 22 2.2 2.1 2.1 22 22 21 2.0 2.1 2 1 2.0 

### 20 20 2.0 

### 8/23/05 Run #2

Page 2

# I

I I I I I I I I I I I I 

# I I I I 

# I I 08/23/05 12.08:02 08/23/0512:08'12 08/23/05 12"08.22 

### 08/23/05 12:08:32 08/23/05 12:08.42 08/23105 12'08:52 08/23/05 12:09:02 08/23/0512:09'12 08/23/05 12:09:22 08123105 12:09:32 

### 08123105 12:09.42 08/23/05 12:09:52 08/23/0512:10.02 08/23/0512:10:12 08/23/05 12:10:22 08/2310512:10:32 08/23/0512:10:42 08/23/05 12:10:52 08/23/05 12'11 02 08/23/0512'11:12 08/23/05 12: 11'22 08/23/05 12'11.32 08/23/05 12:11:42 

### 08/23/05 12:11 :52 08/23/05 12:12:02 08/23/05 12:12:12 08/23/05 12:12:22 08/23/0512:12.32 08/23105 

### 12:12:42 08/23/0512:12:52 08/23/0512'13:02 08/23/05 12:13"12 08/23/0512.13:22 08/23/05 12:13:32 08123/05 12:13:42 08123/05 

### 12:13:52 08/23/0512:14:02 08/23/0512.14:12 08/23/05 12:14:22 08/23/0512-14:32 08/23/05 12:14:42 08/23/05 12:14-52 Port Change 08123/05 12:15'02 08/23/0512"15:12 08/23/05 12:15:22 08123105 12-15:32 08/23/0512.15:42 08/23/05 12:15:52 08/23/0512:16:02 08/23/05 12:16:12 08/23/05 12:16:22 08/23/0512'16:32 08/23105 12:16.42 08/23/0512:16:52 08/23/05 12:17:02 08/23/0512:17:12 08/23/0512:17.22 08/23/05 12:17.32 08/23/0512.17'42 08/23/05 12:17:52 08/23105 12.18:02 08/23/0512:18:12 08/23/05 12.18:22 08/23/05 12:18.32 08/23/0512'18:42 08/23/05 12:18:52 08/23/0512'19:02 08/23/05 12-19'12 08/23/0512:19:22 08123105 12_19'32 08/23/0512'19-42 08/23/05 12-19.52 Resume Sampling 3.9 3 8 3.8 3.9 4.2 40 44 4.2 4.0 3.9 3.9 4.0 4.2 44 4.5 43 44 42 4.2 41 4.2 4.3 4.2 4.2 42 4.2 4.1 4.1 4.1 4.2 4.3 4.5 43 4.2 4.1 

### 44 4.5 4.3 4.2 4.3 4.2 4.2

4 1 3.2 1.3 1.3 

### 1 3 1.3 

### 14 1.4 1.2 12 

### 1 2 11 12 1.3 

### 14 1.2 1.2 1.1 1.2 1.2 1.3 

### 27 4 5 4 4 4.3 4.5 

### 4 7 4 7 4 5 

### 44 87.2 87.2 87.7 88.3 88_7 89.9 91.6 92.3 93.7 94_1 94 0 93.5 93.6 94.1 93.5 93.2 92.5 92.3 92.2 92 3 93_6 93 8 93.8 94.7 94.9 94.6 94 4 94.2 94.3 95.0 95_1 95.3 94.7 93.9 94 7 95_1 94 

### 6 95 0 95.1 94.6 94 6 95 8

96_1 96 2 95.6 78 7 47_1 28 9 17.2 11 8 8.6 

### 70 6.1 

### 5.7 5.5 5.3 

### 5.7 5.7 

### 54 56 56 

### 58 5.6 5.0 6.1 25.5 61 1 78.3 86 7 91 9 94 0 94_5 20.4 

### 20 3 20.4 20.6 20.7 20.7 20.6 20_5 20 2 20.1 20.2 20.4 20.2 20.2 

### 20 4 20.2 20.0 201 20_2 20 1 19 9 19_9 19 9 19_8 19.9 20.0 20.0 20 1 20.0 20_0 19.9 19.7 19.9 20.0 20.0 20.1 20.1 20.1 20.1 20_1 20.3 20.3

20 3 20 4 20.4 18.7 12.1 7.7 5.0 3.7 2.9 2.5 2.2 20 1 9 1.8 

### 17 1.7 1.6 1.6 1.6 

### 1.5 1.5 1.5 1.5 29 8 9 13 5 15.8 17.4 18_3 18 8 2.0 2.0 

### 2.0 2.1 21 

### 2.0 1.9 20 

### 2.0 1 9 2.1 2.1 

### 2.0 2.0 2.1 2.0 

### 2.0 2.0 

### 20 1.9 1 9 1.9 2.0 2.1 

### 2.0 1.9 1.9 1.9 1.9 1.9 2.0 

### 2.0 2 1 2.0 2.0 

### 2.0 19 1.9 1.9 2.1 2.1 20



### 2.0 1 9 

### 2.0 1.9 1 9 1 8 1.8 1.7 1.6 1.5 

### 14 1.5 1.5 1.5 

### 1.5 1.5 1.5 

### 1.5 1.5 1.5 

### 14 14 1.5 1.5 1.6 1.7 

### 17 1 g 1 g 

### 1 8 8123/05 Run #2



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# I I I I 

# I I I I I I I 08/23/05 12.20:02 08123!05 12:20:12 08/23/0512:20:22 08/23/05 12:20:32 08/23/05 12:20'42 08/23/05 12.20:52 08/23/05 12:21:02 08/23/0512:21:12 08/23/0512:21.22 08123105 

### 12 21:32 08123105 12'21.42 08/23/05 12"21:52 08/23/05 12".22:02 08/23/0512:22·12 

### 08/23/05 12:22:22 08/23/05 12:22·32 08/23/05 12:22'42 08/23/05 12:22:52 08/23/05 12:23:02 08/23/0512:23:12 08!23105 

### 12:23:22 08!23105 

### 12.23:32 08123105 12:23:42 08/23/05 12:23:52 08!23105 12:24:02 08!23105 12.24".12 08123105 12.24.22 08/23/0512:24:32 08/23/05 12:24:42 08/23/0512:24·52 08!23105 

### 12:25:02 08/23/0512:25:12 08123105 

### 12:25:22 08/23/05 12:25:32 08/23/05 12:25:42 08/23/0512:25:52 08/23/0512:26:02 

### 08/23/0512:26:12 08/23/05 12:26:22 08!23105 

### 12:26:32 08/23/05 12:26:42 08/23/05 12:26·52 08123105 

### 12:27:02 08/23/0512:27:12 08123!05 

### 12:27:22 08/23/05 12:27:32 08/23/05 12:27:42 08/23/0512:27:52 08/23/05 12:28:02 08!23105 

### 12.28:12 08/23/05 12:28:22 08123105 

### 12:28:32 08/23/05 12:28:42 08/23/05 12:28:52 08/23/05 12:29:02 08/23/05 12:29:12 08/23/05 12:29:22 08/23/05 12:29:32 08123105 

### 12:29:42 08/23/05 12:29:52 08!23105 

### 12.30:02 08/23105 12:30:12 08/23/05 12:30:22 08/23/05 12:30:32 08/23/05 12:30:42 08/23/0512 30:52 08/23/05 12.31.02 08/23/05 12:31:12 08!23105 

### 12:31 :22 08/23/0512'31:32 08!23105 

### 12 31 :42 08/23/0512:31:52 08/23/0512:32:02 08/23/0512:32'12 4.5 4.4 4.4 4.3 4.3 4.3 43 4.3 4.4 4.2 4.2 

### 42 4.1 

### 4 2 4 3 4.4 

### 4.2 4.0 41 

### 3.9 4.0 4.1 4.1 4.1 4.1 4.1 

### 3.9 3.8 36 3.6 3.6 3.6 36 

### 39 39 3.8 39 39 3.9 4.0 40 

### 4.2 4.1 4.1 4.1 

### 4.3 4.2 4 5 4.6 

### 3.9 3.9 3.8 3.8 38 3 7 36 40 

### 3.8 3.9 3.8 

### 3.8 3.9 3.9 40 41 4.1 4.0 41 4.0 4.0 4.1 

### 4.2 43 

### 4.3 95.2 94 9 

### 94.6 94.4 93 4 93.9 96.0 96.3 95.8 95 4 94 9 

### 94.9 95.3 95.2 95.0 94.8 94.7 97.9 99.5 98.1 96.4 95.5 94.2 92.2 91.4 90.3 89.8 

### 90.3 89.7 89.9 90.0 89.2 88.6 88.6 88.0 877 874 

### 86.9 87.3 87.5 87.6 88.3 89.0 89.6 90.5 91.7 92.0 92.7 93.3 94.0 94.6 94.7 94.1 93.9 93.7 92 5 91.5 90 5 89 7 89 3 

### 89.3 89.5 90.2 91.8 91 

### 6 91 7 

### 92.2 92.1 91.8 92 2 92.8 93.3 93.6 94.0 19.0 19 1 

### 19.1 19.2 19.3 19.3 19.2 19.2 19.4 19.4 19.2 19.2 19.3 19.1 19.1 19.3 19.2 19.2 19.2 19.3 19.3 19.5 19.5 19.5 19.8 19 8 

### 19.8 20.1 20.1 19.9 20.0 20.3 20.5 20 4 

### 20.4 20.4 20.5 20.4 20.4 20.5 20.6 20.5 20.5 20.4 20.0 19 8 

### 19.9 19.7 19.7 19 7 

### 19.6 19.9 19.9 19.9 20 1 

### 20.1 20.0 20.0 20.1 20 1 20 1 20 2 

### 20.1 19.8 19.8 19.6 19 4 

### 19.5 19.7 19.9 19 9 

### 20.1 20.2 20.1 1.8 "1.8 

### 1 8 1.8 1.8 1.7 1.7 1.8 1 7 1.7 1.7 1.7 1 7 1.7 1.7 1.7 1.7 1.7 1.8 1.8 1.7 1.7 1.8 1.8 1.8 1 8 1 8 1.7 1.7 1.7 1.7 1.6 1.6 1.6 1.5 1.6 1.6 1.7 1.7 1.6 1.7 1.7 1.6 1 6 1 5 1.6 

### 1.7 1.7 1 6 1.6 1.6 1 5 1 5 1.5 1.6 1.7 1.7 1.7 1.7 1.7 1.6 

### 1 5 1.6 1.5 1 6 1.6 1.6 1.5 1.6 1.6 1.6 

### 1.5 1.5 

### 1.5 8/23/05 Run #2

Page 4 

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# I I I 08/23/05 12.32:22 08123/05 12:32:32 08/23105 12:32:42 08/23/05 12:32:52 08123!05 12:33:02 08/23/0512'33:12 08/23/0512:33:22 08/23/05 12'33:32 08/23/05 12'33:42 08/23/05 12:33'52 

### 08123105 12:34:02 08/23/0512:34:12 08/23/05 12:34:22 08/23/05 12:34:32 08/23/05 12:34:42 08/23/05 12:34:52 08/23105 12:35:02 08/23/05 12:35:12 08/23105 12.35:22 08/23/05 12:35:32 08123105 12:35:42 08/23/05 12:35:52 08/23/05 12:36.02 08/23/0512:36:12 08/23/05 12:36:22 

### 08123105 12:36:32 08/23/05 12.36:42 08/23105 12:36:52 08/23/05 12"37.02 08/23/0512'37:12 08/23/05 12:37:22 08/23/05 12.37:32 08/23/05 12.37:42 

### 08123105 12:37:52 

### 08123105 12:38"02 08/23/05 12:38:12 08/23/05 12:38:22 08/23/05 12:38:32 08/23/05 12'38:42 08/23/05 12:38:52 08/23/05 12:39:02 08/23/0512.39:12 08/23/05 12:39:22 08/23/05 12:39:32 08/23/05 12:39:42 08/23/0512:39:52 

### 08123105 12:40:02 08/23/05 12'40:12 08/23/05 12.40 22 08/23/05 12'40:32 08/23/05 12'40:42 08/23/05 12:40'52 08/23/0512'41:02 08/23/0512:41:12 08/23/0512'41:22 08/23/0512:41:32 08/23/0512:41:42 08/23/0512:41'52 

### 08123105 12:42:02 08/23/05 12.42.12 08/23/05 12.42:22 08/23/05 12'42:32 08/23/05 12:42 42 08/23/05 12:42:52 08/23/05 12 43:02 08/23/05 12:43:12 08/23/05 12:43:22 08/23/05 12:43:32 08/23/05 12:43:42 08/23/05 12:43:52 08/23/05 12:44:02 08/23/05 12:44:12 

### 08123105 12.44 22 08/23/05 12:44:32 4.2 4.1 4.2 4.1 4.1 4.1 4.4 4.1 3.9 4.0 39 3.8 36 3.6 3.6 3.7 3.6 3.7 4.1 4.0 4.2 4.2 4.2 4.0 4.1 4.1 4.1 42 4.2 4.0 40 4.0 4.3 4.3 42 4 1 4.7 4.3 4.1 4.1 4.1 42 4 3 3.9 40 4.0 4.0 45 46 4.6 4.4 4.3 4.3 4.2 4.5 4.3 4.5 4.4 43 4.1 

### 42 4.1 4.0 4.0 4.0 4.0 4.0 40 39 4.1 4.3 4.1 4.1 4.1 94 7 95_3 95.8 96.2 96.9 97.2 96.7 96.0 96 1 95_8 95.8 95.9 95.6 95.3 94.8 93.3 91_2 89 4 88.0 87.3 87.3 86.8 86 7 87_3 87.7 88.0 88.2 88.3 88.4 88 8 88.8 89.2 90.0 89.9 90_4 91.0 90 6 90.9 91_6 91 7 91.9 92.5 92.4 92.7 92.9 92.6 92.0 91.1 90 0 89_1 88 2 87_9 88.4 89.0 89 6 91 1 92.6 93.6 95 4 96.0 95.0 94.9 94 9 94_4 94 4 94_1 92 6 91.5 91.6 91 '1 90.9 91 5 91.4 91.3 20.1 20.1 20.1 20.0 20.0 20.0 20.2 20.2 20.0 20.1 20_1 20.2 20.2 20.1 20.0 20.1 20.0 20.0 20.1 20.1 20 0 20.2 20 4 20.1 19.9 19 9 19.9 19.8 19.8 19.9 19.8 20.0 20.2 20_1 20.1 20.0 20_0 20.0 20.1 20.3 20.6 20.3 201 20 0 20 0 20_1 20.1 20 2 20 2 20.1 20.0 19.9 19.9 19.7 19.7 19.8 19.8 19.7 19.9 20.2 20_2 20.2 20.2 20.3 20.3 20.3 20.2 20.2 201 20 0 20 1 20 1 201 20 2 1.6 1 6 1.6 1.6 1.5 1.5 1.5 1.5 1.5 1.6 1 7 1.6 1.6 1.5 1.5 1.5 1 5 1.5 1 5 1.4 1 4 1.5 1.6 1 5 1.5 1.6 1.6 1.6 1.5 1.4 

### 14 1.5 1.4 1.4 1.4 1.5 1.5 1.5 1.5 1 5 1.5 1.5 1.3 1.4 1.5 1.5 1 4 1.4 1.3 1.4 1.4 1.5 1.5 1.5 1.5 1.3 1.3 1.4 1.5 1 4 1.4 1.4 1 5 1 4 1.2 1 3 i_3 1 3 1.3 1.3 1.2 1.2 1.3 1.2 8123/05 Run #2



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# I I I I I I I I I I I I I I 08/23/05 i 

### 2:44:42 08/23/05 12:44:52 08/23/05 12:45:02 08/23/05 12:45' 12 08/23/05 12:45:22 08/23/05 12:45:32 08/23/05 12:45:42 

### 08/23/0512.45:52 08/23/05 12.46:02 08/23/05 12:46:12 

### 08/23/0512:46:22 08/23/05 12'46:32 08/23/05 12:46.42 08/23/05 12:46:52 08/23/05 12.47:02 08123105 12:47·.12 08123105 12:47:22 08/23/05 12:47:32 08/23/05 12:47:42 

### 08/23/05 12:47:52 08/23/05 12:48:02 08/23/0512:48:12 

### 08123105 12:48:22 08123105 12:48.32 08/23/05 12:48:42 08/23/05 12:48'52 08123105 12:49:02 08/23/05 12:49:12 08/23/05 12:49:22 08/23/05 12:49:32 08/23/05 12:49:42 08123/05 12 49:52
Stop Run #2



### 08/23/05 12:50:02 08/23/05 12.50:12 08/23/05 12:50:22 08/23/05 12:50.32 08123105 

### 12:50:42 08/23/05 12:50:52 

### 08/23/0512:51:02 08/23/05 12:51-12 08/23/05 12:51 '22 08/23/0512:51:32 08/23/05 12:51.42 08/23/05 12 51.52 08/23/05 12:52:02 08/23/0512:52:12 08/23/05 12:52:22 08/23/05 12:52:32 08/23/05 12:52.42 08/23/05 12:52:52 08/23/05 12'53:02 08/23/05 12:53:12 08/23/0512:53:22 08/23/05 12'53:32 08/23/05 12'53:42 08/23/05 12'53:52 08/23/05 17-54-02 08/23/05 12:54:12 08/23/05 12:54:22 08/23/05 12:54:32 08/23/05 12:54:42 08/23/0512:54:52 08/23/05 12:55:02 08/23/05 12:55:12 08/23/05 12:55:22 08/23/05 12:55' 32 08/23/05 12:55:42 08/23/05 12:55:52 08/23/0512.56:02 08/23/05 12.56:12 08/23/05 12:56'22 43 41 41 4.0 4.0 4.3 

### 42 4.3 

### 4 7 

### 44 4.3 43 

### 44 4.6 4.3 4.6 4.3 4.3 

### 42 41 

### 42 4.3 43 46 4.3 44 4.3 41 4 1 

### 4.2 4 1 43



### 4 00

3.2 1.6 14 

### 14 1.3 1.3 1.3 1.3 1.3 

### 1.2 1.3 1.2 1 3 1.3 13 

### 1.2 12 

### 1 2 1 2 1 2 

### 1.2 1 2 12 

### 1.2 1.2 12 

### 1 2 1 2 1.2 1 2 12 

### 12 1.2 

### 1.2 12 

### 1 2 

### 12 1.2 11 

### 92.1 92.1 91_5 92.1 92.2 92.1 92.4 92_6 92 5 

### 92_9 93_5 93.3 93.5 94.9 95 6 95.5 95.7 95.1 94.5 95.2 95.2 95.2 96.4 97.1 95.7 94.3 93 0 

### 92.2 92.1 91_6 91.9 93 6



### 91.74

92 5 89 0 

### 79.3 56.0 38.3 26.7 19.3 15.4 124 

### 10.9 9.8 8.7 

### 8.2 76 6.7 65 64 6.1 6.1 

### 6.3 6.1 

### 5.9 5.8 5.7 5.6 

### 52 5.2 5.2 

### 54 51 5.1 55 5.8 5.6 

### 5.7 59 5.8 5.5 

### 5.5 20.4 20.4 20.3 20.3 20.3 20.4 20.2 20.0 20.0 20.1 20.2 20 2 

### 20.2 20.2 20.2 20 1 

### 20 1 

### 20.1 20.0 19.8 20.0 20.2 20.1 19.9 19.7 19.6 19.8 19.9 20.0 20.3 20.4 201



### 20.29

20.0 19.1 18.2 13.8 10.5 6.1 64 

### 52 

### 44 38 34 

### 32 3.0 

### 27 26 2.4 23 2.2 22 2 1 2.0 1 9 1 9 1 8 

### 1.8 1 8 1 8 1 9 1 9 

### 20 2 1 

### 2.3 2 3 2.0 1 8 1.6 1 6 1.5 

### 1 5 1.1 11 1.2 1 3 1.3 

### 1.4 1 4 1 4 1.3 1 2 1.3 

### 1.4 1.3 1.2 

### 1.2 1.3 1.3 1 3 1 4 1.3 

### 1.3 

### 1.4 1.3 1.3 

### 1.4 1.3 

### 1.2 11 1.1 

### 1.2 1 2 1.2

1.86

1.2 

### 11 11 11 11 1.2 1.1 1.1 1 0 0.9 

### 0.8 0.9 

### 0.9 1.0 1.1 

### 1.2 1.0 

### 09 0.8 0.9 0.9 0 9 

### 08 0.8 0 8 0.9 

### 0.8 08 0.8 0.8 0.8 0.8 0 9 09 0.8 08 0.8 

### 0.8 0 8 8/23/05 Run #2



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# I I I I I I I I I 08/23/05 12.56:32 08123105 

### 12'56:42 08/23/05 12:56'52 08/23105 12:57:02 08123105 12:57:12 

### 08123105 12:57:22 

### 08/23/05 12:57:32 08123/05 12:57:42 08123105 12:57:52 08/23105 12'58:02 08/23/05 12:58:12 

### 08/23/05 12:58:22 08123105 12:58.32 08/23105 12:58:42 08!23105 

### 12:58:52 08123105 

### 12:59:02 08123105 

### 12:59:12 08123105 

### 12:59.22 08/23/05 12:59:32 08123!05 

### 12:59:42 08/23/05 12:59:52 08/23/05 13:00:02 08/23/05 13:00:12 08123105 13:00:22 08/23/05 13:00.32 08!23105 13:00'42 08/23/05 13:00:52 08/23/05 13:01:02 08/2310513:01-12 08/23/0513:01:22 08/23/0513'01:32 08/23/0513:01:42 08/23/05 13:01:52 08123/0513:02:02 08/23/0513:02:12 08123105 

### 13:02:22 08/23/0513:02:32 08123105 13:02:42 

### 08123105 13.02:52 

### 08123105 13:03:02 08/23/0513:03:12 

### 08123105 13:03:22 

### 08123105 13:03:32 

### 08123105 13:03:42 08/23/05 13:03:52 08/23105 13:04:02 08/23/05 13:04:12 08/23/05 13:04:22 

### 08123!05 13:04:32 

### 08123105 13.04:42 

### 08123105 13'04:52 

### 08123105 13 05:02 

### 08123105 13.05:12 

### 08123105 13.05:22 

### 08123105 13:05.32 08/23105 13:05:42 

### 08123105 13.05:52 

### 08123105 13:06:02 08i23/0513:06:12 08/23105 13:06:22 08/23/05 13:06:32 08/23/05 13:06:42 08/23105 13:06:52 08/23/05 13:07'02 08/23/0513:07:12 08/23/05 13:07"22 08/23/0513:07:32 

### 08123105 13.07:42 

### 08123105 13:07:52 08/23/05 13:08:02 08'23/0513:08:12 

### 08123105 13:08:22 

### 08123105 13-08:32 1 2 1.2 12 1_2 1.2 1.2 1.2 1.2 1.2 1.2 1.2 1 2 1.2 1.1 1.2 1.2 1.2 1.2 

### 1 2 1.2 12 1.2 1.2 1.2 1.1 1.0 03 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.3 0.2 02 0.3 03 0.2 0.2 0.2 02 0 3 02 0.2 0.4 06 02 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.1 0.2 0.2 0.2 0.2 0.2 

### 0.1 0.1 0.1 0.1 02 0 7 11 11 59 58 5.8 6 1 6.2 6.0 6.0 6.0 6.1 

### 5.6 56 5.3 5.2 5.1 5.3 5.7 5.6 5.3 5.7 5.9 5.8 5.6 

### 56 5.4 5.4 5.7 

### 55 5.2 5.1 

### 5.0 4.6 4.3 4.2 4.4 45 42 4.6 46 4.4 4.3 

### 45 4.8 

### 4.8 4.6 

### 4.9 4.9 4.8 4.2 4.6 8 8 

### 32 5 58.2 75.8 86.1 90.8 94.0 96.0 97.3 97.9 98.2 98 7 99_4 99_6 100.0 100.5 

### 100.6 100.7 100.6 100.5 100 4 W0.2 99.9 94.3 1 5 1.5 15 1.5 1.4 1.4 1.3 1 3 1.3 1.2 1.1 11 1.1 11 11 1.1 1.0 1.1 1 0 1.0 1.0 1.0 1.0 0.9 0.9 0.9 09 1.1 4.8 11.5 16.3 19.4 21 4 22.5 23_1 23.6 23.8 24.0 24.1 24.2 24.3 24.3 

### 24.4 24.4 24.4 24.4 24_1 24_0 23.8 20.5 13 0 

### 8 0 4 8 3.0 2.0 1.6 1.3 1.1 1 0 09 0.8 0 7 0 7 07 0.6 

### 0.6 0.6 0.6 0.5 05 0.5 

### 0.5 05 0_7 0.6 0 7 0.8 0.9 0.8 0.8 0.8 0.8 0.7 08 0.8 0.8 0.7 0.7 0.8 0.8 0.8 0.7 0.7 0 7 0.6 0.7 0.7 0 7 0.7 0.7 0.6 06 0.7 0.7 0.7 0.7 0.7 0.7 0.7 06 0.6 0.7 

### 0 7 06 0.7 

### 0.7 0.6 0.5 0.5 0.5 0.6 0.6 0.7 0.6 

### 0.5 0.5 0.6 0.7 06 

### 0.5 0.6 

### 05 05 0.6 07 07 0.7 0.7 0.6 

### 0.5 0.5 0.5 

### 04

0.4 

### 04 8/23/05 Run #2

25_5 ppm NOx Zero CO, S02

99.1 ppm CO Zero VOC, NOx

Page 7 

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I I I I I I I I I I I I I I I I I I 08/23/05 13:08:42 08/23/05 13:08:52 08/23/05 13:09:02 08/23/05 13:09:12 08/23/05 13:09.22 08123105 13'09:32 08123105 13:09:42 08/23/05 13:09:52 08123105 13:10:02 08123105 13:10:12 08123105 13:10:22 08/23/05 13:10:32 08/23/0513'10.42 08/23/05 13' 1 0 52 08/23/0513:11:02 08/23/0513:11:12 08/23/05 13:11 :22 08/23/05 1 3 11 '32 08/23/0513:11:42 08/23/0513:11:52 08/23/05 13:12:02 08/23/05 13:12:12 08/23/0513:12:22 08/23/0513:12:32 08/23/0513:12:42 08/23/0513:12:52 08/23/05 13:13:02 08/23/05 13'13-12 08/23/0513:13'22 08/23/05 13:13:32 08/23/0513:13:42 08/23/0513:13:52 08/23/05 13:14:02 08/23/05 13:14:12 08/23/05 13:14:22 08/23/0513:14:32 08!23/05 13:14.42 08123/05 13:14:52 08/23/0513:15:02 08123105 13:15'12 08/23/05 13:15:22 08/23/0513:15:32 08/23/0513:15:42 08/23/0513:15:52 08/23/05 13:16.02 08/23/05 13:16:12 08/23/0513:16:22 08/23/0513:16:32 08/23/0513:16:42 08/23/0513:16:52 08/23/05 13.17:02 08/23/0513:17:12 08/23/0513'17:22 08/23/05 13:17'32 08/23/0513:17:42 08/23105 

### 13" 17:52 08/23/05 13:18:02 08/23/05 13:18:12 08/23/0513:18:22 08/23/05 13:18 32
08/23/05 13:18:42 08123105 13:18:52 08/23/05 13.19:02 08/23/0513:19'12 08/23/0513 19.22 08/23/05 13"19:32
08/23/05 13:19:42 08/23/0513:19.52 1.1 1.0 0.3 0.2 

### 0.2 0.2 0.2 0 2 

### 0.2 0.2 0.1 0.1 0.1 0 2 0 1 01 0.1 0.1 01 0.2 0.2 

### 0.2 0.1 

### 0.2 0.2 0.2 02 0.1 0.1 0.2 

### 0.2 0.1 0.2 0.2 0.1 01 0 1 0.2 

### 0.2 0.2 0.2 0.2 01 0.1 0.1 0.2 0.1 0.1 0.1 0.1 0.1 01 0 1 0.1 0.1 

### 0.2 0 1 0 1 0 1 0.1
0.1 70 14_9 

### 14.9 14.9 14.9 14.9 14_9 73.0 47.3 29.8 17.6 12.2 8.7 6.4 5.4 51 4.7 4.5 4.6 4.8 

### 50 48 47 49 4 9 4.8 4.6 4.5 4.5 4.3 4.5 4.3 4.5 4.5 4.8 4.8 49 4.9 4.9 4.9 4.9 4.7 4.7 4.9 46 45 4.1 4.1 4.2 4.3 4.2 4 5 4.6 4.6 4.7 

### 53 4.2 4.3 4.2 4.6 4.7 4.6 4.4 3.9 39
4.1 44 4.7 4.5 4.7 4.9 4.7 4 5
4.5 44 

### 05 0.5 0.6 0.6 0.7 

### 0.7 0.8 0 8 0.8 0.8 0.8 0.8 0.8 0.8 0.8 0.8 0.8 0.8 0.8 0.8 0.8 0.8 0.8 0.8 0.8 0.8 0.8 08 0.7 0.7 0.7 0.7 0.7 0.7 0 7 0.7 0.7 0.7 0.7 07 0.7 0 7 

### 0 7 0.6 0.7 0.6 0.6 0.6 0.6 0.6 0.6 0.6 0.6 0.6 06 0.6 0.6 06 0.6
0 6 

### 0.5 0.5 

### 05
0.5 

### 05 

### 04
0.3 03 0.4 

### 0.5 0.5 0.4 

### 0.5 0 7 1.3 2.6 4.5 7.1 9.6 11.9 144 17_1 19.8 22.1 23.9 25.8 27.3 28.8 30.3 31.6 33_0 34.3 35.2 36_2 37.1 37_9 38_5 39_1 40.0 40.6 41.2 41.7 42_1 42.5 42.8 43_1 43_5 43.9 44_1 44_4 44.6 44.9 45 0 45.3 45.3 45 4 45.6 45.9 46.1 46.2 46.3 46 4 46 5 46_6 46.7 

### 46.7 46.9 47.0 46.9 45.7 45 2 45.4 44_8
43.1
40 4 37_3 8/23/05 Run #2

50.1 ppm 

### S02

15 2 ppm C3H8

Page 8 

# 43

# I

I 

# I I I 

# I I I I I I I I I I I I I 

# I DaterTime VOC CO NOx S02 mm/dd/yy hh:mm:ss ppm ppm ppm ppm 08/23/05 13:33:52 4.3 85.3 18.5 3.5 08/23/05 13.34:02 08/23/0513'34:12 08/23/05 13:34:22 08/23/05 13:34:32 

### 08123105 13:34:42 08/23/05 13:34:52

Start Run #3 08123105 13:35:02 08123105 13:35:12 08123105 

### 13:35:22 08/23/05 13:35:32 

### 08/23/05 13:35:42 08123105 13:35:52 08123105 13:36:02 08/23/0513.36.12 08123105 13:36:22 08123105 13 36.32 08123105 13:36:42 08/23/0513:36:52 08123105 13:37.02 08123105 13:37:12 08/23/05 13:37:22 08/23/0513.37:32 08/23/0513 37:42 

### 08/23/05 13:37:52 08123105 13:38:02 08/23/0513:38:12 08123105 13:38:22 08123105 

### 13:38:32 08123105 

### 13:38:42 08/23/0513:38:52 08123105 13:39:02 08123105 

### 13:39:12 08/23/05 13:39.22 08/23/05 13:39:32 08/23/05 13"39:42 

### 08123105 13:39:52 08/23/05 13".40:02 08/23/0513:40:12 08/23/05 13:40.22 08/23/05 13:40:32 

### 08123105 13:40:42 

### 08123105 13:40:52 

### 08123105 13"41 :02 08/23/0513:41:12 

### 08123105 13:41:22 

### 08123105 13:41 :32 08/23/0513:41 42 

### 08123105 13:41.52 08/23/05 13:42:02 08/23/0513:42:12 

### 08123105 13:42:22 

### 08123105 13"42:32 

### 08123105 13:42:42 08/23/05 13:42:52 08/23/05 13:43:02 

### 08123105 13:43:12 08/23/05 13:43:22 08/23/05 13"43:32 

### 08123105 13:43:42 08/23/0513:43"52 08/23/05 13.44:02 

### 08123!05 13:44:12 

### 08123105 13:44:22 08/23/05 13:44:32 08/23/0513:44:42 08/23/0513:44:52 

### 08123105 13.45"02 08/23105 ; 3:45.12 08/23/05 13:45:22 

### 4.4 4.3 4.2 

### 4.3 

### 4.1 4.0

39 40 3.9 3.9 3.9 3.7 3.7 3.7 36 3.6 3.6 36 3 7 3.8 3.8 

### 3.8 

### 4.1 3.8 3.8 37 3.9 42 

### 4.2 4.5 

### 4.4 4.5 4.7 48 4.6 4.5 4.5 4.6 45 4.6 

### 4.4 4.3 4.3 

### 4.3 4.3 4.3 4.2 4.2 

### 4.3 4.3 4.2 

### 4.4 4.5 

### 4.4 4.2 4.2 4 2 

### 4.3 4.3 

### 4.3 

### 4.4 4.4 

### 44 44 44 

### 42 4.2 4.3 4.7 85.9 86.5 87.7 88.1 88.4 88 4

88.8 88.9 89.0 90.2 90.7 91.7 93.6 94.9 95.1 95.2 94.5 92.8 91.7 90.6 89.3 88.6 88.0 87.8 86.7 84 9 83.7 81.0 78.5 77.4 75 7 74.9 75.7 77.2 79.0 81.4 84 3 86 7 87.8 89 4 91.0 91.0 91 

### 3 91.9 92 0 92.3 93.1 93.3 92.9 93.1 93.8 93.8 94.2 95.6 95.9 95.2 95.2 94.4 94.1 94 7 95.7 96.5 97.3 98.3 98.1 98 1 98.6 98.2 98.2 18.5 18.3 18.5 18.7 18.9 19.0

18 8 18.8 19.1 19.0 18.9 18.9 18.8 18 

### 8 19.0 19.1 19.2 19 3 19.2 19.2 19.2 18.9 18.8 18.9 18.9 19.1 19.3 19.4 19.4 19.4 19.4 19.3 19.2 19.3 19.4 19.3 19.3 19.4 19.2 19.2 19 3 19.1 19.2 19 4 19 4 19.4 19.4 19 4 19.3 19.4 19.6 19.9 19.8 19.7 19.5 19.5 19 4 19 7 19.7 19 5 19 5 19.4 19.3 19.2 19.3 19.3 19.3 19.3 19.2 34 3.3 3.2 3.2 3.1 3.1



### 30 29 

### 2.8 2.7 2.7 2.6 2.5 2.5 24 23 2.3 

### 2.4 23 2.1 2.0 2.0 21 2.0 2.0 2.0 1.9 1 9 1.8 1.8 1.6 1.6 1.7 1 7 1.7 1.7 1.7 1.7 1.7 1.7 1 6 1.6 1.5 1.5 1 4 

### 1.4 1 4 1 4 1 4 1 4 1 5 1 5 

### 1.4 1.4 1 4 

### 1.4 1.3 1 3 1.3 1.3 1 3 

### 1.4 1.4 1.4 1.4 1.3 1.2 i.3 

### 1 3 8/23105 Run #3

Page 1 

# 44

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I I I I I I I I I I I I I I I I I I 08123105 

### 13:45:32 08/23/05 13.45:42 08123105 

### 13:45.52 08123105 13:46:02 08/23/05 13:46:12 08/2310513:46:22 08123105 13:46.32 08/23/05 13:46:42 08123105 13:46:52 08123105 13'47:02 08/23/05 13 4 7:12 

### 08/23/0513:47:22 08/23/0513:47:32 08/23/05 13:47:42 08/23/0513:47.52 

### 08123105 13.48:02 08/23/05 13:48:12 08123105 13:48:22 08/23/05 13:48:32 

### 08/23/05 13:48:42 08/23/05 13:48:52 08123105 

### 13:49:02 08/23/0513:49'12 08123105 13:49:22 08123105 13:49:32 08123105 13:49.42 

### 08/23/05 13:49:52 08/23/05 13:50:02 

### 08/23/0513:50'.12 08/23105 

### 13:50:22 08123105 

### 13:50:32 08123105 13:50:42 08123105 13:50:52 08/23/0513:51:02 08!23/0513'51:12 08123105 13"51:22 08/2310513:51:32 08/23/05 13:51 '.42 

### 08123105 13.51:52 08123105 13:52:02 08123105 13:52".12 08123105 13:52:22 08123105 13:52:32 08/23105 13:52:42 08123105 13:52:52 08123105 13:53:02 08123105 13:53:12 08123105 13:53:22 08123105 13:53:32 08123105 13:53:42 08123105 13:53:52 08123105 13:54:02 08123105 13:54:12 08/23/0513:54:22 08/23/05 13:54:32 08123105 13:54:42 08123105 13:54:52 08123105 13:55:02 08/23/0513:55:12 08123/05 13:55:22 08/23/05 13:55:32 08/23/05 13:55'42 08123105 13:55:52 08/23/05 13:56:02 08/23/05 13:56:12 08/23/05 13:56:22 08/23/05 13:56:32 08/23/05 13:56:42 08/23/05 13:56:52 08/23/05 13:57.02 08123105 13:57:12 08/23/05 13:57:22 0812310.5 13:57:32 08123105 13:57'42 4.3 4.1 4.0 4 1 4.0 4.1 4 1 41 4.3 

### 42 42 4.3 

### 44 44 4.5 4.5 43 4.3 43 4.3 4.3 4.3 

### 44 

### 44 44 4 7 

### 47 4.7 48 5.0 5.0 50 4.8 5.0 

### 52 5.0 5.1 5.0 

### 52 5.0 

### 52 5.1 5.1 4.9 4.9 4.8 46 4.6 

### 47 4.9 50 5.1 4.8 4.8 5.2 4 7 4 8 48 

### 4 7 4.8 

### 48 4 7 4.6 

### 47 4 7 46 4.6 45 4.4 

### 44 4.6 4.5 4.5 4.5 96 7 94_3 91.8 89.9 89.4 89.3 88.4 88_7 89.0 88_3 88.3 88.2 87.6 87.8 88.5 89.3 91.5 93.3 94.4 95.7 96.9 96.9 96_3 94.9 93.9 93.7 93.9 94.1 94.9 96.8 97.9 99 0 100_0 101.9 1021 101_9 101.8 102.9 103.8 107.1 112.9 109.9 106.7 104.2 100.9 97.9 96.3 95 9 94.5 95.8 98_6 98.0 97_4 98 5 100_0 103_0 107_6 105.8 103.0 101_3 101.6 102.5 104.6 105.4 105.4 106.7 111.4 112.2 110 2 108_0 105 2 103.4 102.5 100.7 19.2 19 2 19_1 19.1 19.2 19.2 19_3 19 3 19.3 19.4 19.4 19 6 19_8 19.9 1!:1.!:1 20_1 20.1 19.9 20_1 20.1 19.9 20_1 19 

### 8 19 5 19.6 19.4 19.4 19_6 19_5 19.3 19.3 19.4 19_3 19.2 19.2 19.2 19_2 19.2 19.2 19.2 19.0 19.3 19.4 19_3 19.6 19.8 19.6 19 6 19.7 19.5 19.3 19.6 19.6 19 4 19.6 19.6 19.5 19.6 19 7 19 5 19_3 19.4 19.3 19.3 19.4 19.3 19_2 19 2 19.2 19.2 19.2 19.4 

### 18.5 19_5 1.2 1.2 1.2 '1.2 

### 12 1.2 1 2 

### 12 11 1.2 1.3 1 2 11 

### 12 1 2 12 11 11 11 

### 12 12 1 2 1.3 

### 12 11 11 1.0 1.0 11 12 11 11 11 11 1.2 11 1.0 11 11 11 11 1 0 1 0 '1.0 1.0 1.0 11 1.1 1 0 

### 0.9 

### 08 1.0 

### 0.9 1.0 1.0 11 

### 09 0 9 09 0.9 09 1.0 0 9 

### 08 0.8 

### 08 0.8 08 

### 08 08 

### o8 

### 08 0.9 0.8 8/23/05 Run #3



### Page 2 

# 45

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# I I I I I I 08/23/05 13:57_52 08123105 13:58:02 08/23/05 13:58.12 08/23/05 13'58:22 

### 08123105 13:58:32 08/23/05 13:58:42 

### 08/23/0513:58:52 08/23/05 13:59:02 08/23/05 13:59.12 08/23/05 13:59:22 08/23/05 13:59:32 08/23105 13:59:42 08123105 13:59:52 OB/23105 14:00:02 08123105 14:00:12 08/23/05 14:00:22 08123105 14:00:32 08/23/05 14:00:42 08/23/05 14"00:52 08123105 14-01:02 08/23/05 14:01:12 08123105 14:01:22 08/23/0514:01:32 08/23/05 14:01:42 08123105 14:01:52 OB/23105 14:02:02 08/23/05 14'.02:12 08/23/05 14:02:22 08123105 14:02:32 08/23/05 14:02:42 08/23/05 14:02:52 

### 08/23/05 14:03:02 08/23/0514:03:12 08/23/0514:03'22 08123105 14:03:32 08/23/05 14:03-42 08/23/05 14:03:52 08/23/05 14'.04:02 08/23/05 14:0412 08/23/05 14:04:22 08/23/05 14:04:32 08/23/05 14.04"42 08/23/05 14:04:52 Port Change 08/23/05 14:05:02 08/23/05 14:05'_12 08123105 14:05:22 08/23/05 14:05:32 08/23/05 14:05:42 08123105 14:05:52 08/23.105 14:06:02 08/23/05 14:06:12 08/23/05 14:06:22 08123105 14:06:32 08/23/05 14:06'42 08123105 14:06:52 08123105 14:07:02 08/23/0514:07:12 08123105 14:07:22 08/23/05 14:07:32 08/23/05 14:07:42 08123105 14'.07:52 08123105 14:08:02 08/23/05 14:08· 12 08/23/05 14:08:22 08/23/05 14:08:32 08/23/05 14'08:42 08/23/05 14:08 52 08/23/05 14:09:02 08123105 14:09:12 08/23/05 14:09:22 08/23/05 14:09· 32 08/23/05 14:09:42 08/23/05 14'09:52 4.5 4.5 

### 4.4 4.3 4.2 42 4.2 4.3 4.3 46 4.6 

### 4.4 45 4.2 

### 40 4.0 39 

### 40 40 

### 4.0 4.1 4.1 4.2 4.2 43 4.5 4.7 

### 4.4 4.3 45 43 43 4.3 

### 4.4 4.4 45 46 4.5 4.7 50 46 46 4.2

1.5 

### 1.4 14 1.4 

### 1.4 1.4 1.4 

### 1.4 i.4 

### 14 1.4 13 

### 1.3 1.4 

### 14 1.4 1.5 

### 14 

### 4.4 45 4.5 

### 4.5 4.7 4 9 4.8 

### 4.7 4.8 51 

### 50 48 99 0 99.7 98.7 96 2 95_7 

### 95 6 95.5 96.5 98.0 98.0 97_6 97.6 97.9 97.4 97.0 95.8 94.4 92.1 89.8 87_6 86.1 85_4 84.6 84.7 85_7 86_8 87.5 88.1 88 6 89.2 89 9 91 2 92.0 92_0 

### 92 4 93 6 94 1 94.2 95.2 95.6 95.7 96.8 97.3

96_9 84_8 52.8 31_2 18.7 12 2 8 5 

### 6.4 5.7 

### 56 5.3 5.2 54 

### 56 

### 5.4 5.2 5.3 54 

### 5.4 121 45_9 71.8 84_0 88.6 91.3 93.3 94_1 94.2 94 8 95.8 19 6 19.8 19.6 19.7 19.9 20.0 20.0 20.1 20.1 20.0 20.2 20.3 19.9 19.8 19.9 19.8 19.9 19.9 20.0 19.8 19.6 19 7 19.6 19.4 19.5 19.5 19.6 19.7 19.9 19.8 

### 19 7 19.7 19.8 19.5 19.3 19.3 19.3 19.6 19.6 19 

### 8 20.1 20.0 20.0

20.0 18.8 12.8 

### 78 5.1 

### 35 2.8 2.3 

### 20 1.9 18 

### 1 7 

### 1.6 1.6 1.6 1 5 15 

### 1 5 1.5 

### 1.6 5.8 111 14.3 16.1 17.1 17.8 

### 182 18.5 

### 18.6 18.8 08 0 8 08 0 8 0 8 07 0.7 0.8 08 0.8 0.8 0.8 0.8 0.8 0.8 0 7 

### 09 0.8 08 0.8 0.7 0.8 06 0 7 0.8 0.6 0.6 06 0.6 0.7 0 7 0.7 07 0.7 0.6 06 0.7 0.7 0.6 0.6 06 0.7 0.7

0.5 0.6 0.6 

### 0.5 05 0 5 0.5 

### 0.4 0.3 03 

### 0.4 0.5 

### 0.5 04 

### 0.4 04 0.3 0.3 03 

### 04 0.4 

### 0.4 0.4 0.4 05 0.5 

### 0.5 0 4 04 

### 0.4 8/23105 Run #3



# 4G
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I I I I I I I I I I 

# I I I I I I I I Resume Sampling 08/23/0514 10:02 08/23/0514:10:12 08/23/0514:10.22 08/23/0514:10:32 08/23/05 14:10:42 08/23/0514:10:52 08/23/0514:11:02 08/23/0514:11:12 08/23/05 14:11.22 08/23/05 14:11:32 08/23/05 14:11-42 08/23/05 14:11 '52 08/23/05 14'12:02 06/23/05 14:12:12 08/23/05 14:12.22 08/23/0514:12:32 06/23/05 14:12:42 

### 08123105 14:12:52 08/23/0514:13'02 06/23/05 14:13:12 08/23/05 14.13:22 08/23/05 14:13:32 08/23/0514:13'42 08/23/0514:13:52 08/23/05 14.14:02 08/23/05 14:14:12 08/23/05 14.14:22 08123105 14:14:32 08/23/05 14:14:42 08/23/05 14:14:52 08/23/05 14:15:02 08/23/0514'15:12 08/23/0514:15.22 08/23/05 14:15:32 08/23/05 14:15:42 08123105 14:15:52 08/23/05 14.16:02 08/23/051416:12 08/23/0514:16.22 08/23/0514:16:32 06/23/05 14:16:42 08/23/05 14:16:52 08123105 14:17:02 06/23/0514.17:12 08123105 14:17:22 08/23/05 14:17:32 08/23/05 14:17:42 08/23/0514:17:52 08/23/0514:18:02 08/23/0514:18:12 08/23/0514:18:22 08/23/051418.32 08/23/05 14:18:42 08/23/0514'18:52 08/23/05 14:19:02 08/23/0514:19:12 08/23/0514:19'22 08123105 14:19:32 08/23/0514:19:42 08/23/05 14.19.52 08123105 14:20:02 08/23/0514:20:12 08/23/05 14:20:22 08/23/05 14:20-32 08/23/05 14 20:42 08123105 14:20-52 08/23/05 14:21.02 08/23/05 14:21:12 08/23/0514:21:22 08/23/05 14'21:32 08/23/0514:21:42**08/23/0514'2~:52** 08123105 14.22:02 4.7 4.6 4.6 4.5 4.6 4.6 4.6 4.6 4 7 4.8 4.6 5.0 5.0 5.1 5.0 4.8 

### 4.7 4 7 4.6 4.6 4.9 

### 4.7 4.7 4.9 5.1 5.1 5.0 4.8 5.0 5.1 5.3 4.9 

### 4.7 4.8 4 7 46 

### 4.7 48 5.0 5.1 5.0 5.2 5.2 

### 5.4 5.2 4.8 4.6 4.6 4.6 

### 4.7 4 7 4.6 

### 4.7 4.7 4 7 4.6 4.6 4.5 4.5 4.7 4.8 4.6 

### 4.7 4.7 46 4 7 46 4.5 4.5 4.5 4.5 4.6 4.6 96 3 95.9 95.3 94.9 94.9 95.3 97 6 99.9 99.6 99.1 96.5 98.5 99 0 99.6 100.3 101 1 100.6 100.2 99.2 98.9 99.4 99.0 99.2 100.5 100 7 101.0 102.5 101.7 100.1 99.6 99.3 99 8 106.2 107.1 103.9 101.3 101.1 100 5 100 0 100.9 101.4 100.4 101.9 103.1 101.3 100.8 103.5 104.2 102.4 101.9 101.4 103.2 103.6 104.1 105.1 104.7 104.8 105.4 105.6 104.9 104.3 105.0 104 5 103.9 104 9 105 4 104.3 103.2 102.9 102 2 102.1 102 4 103.6 18.6 18.5 18.6 16.9 18.9 19.1 19.4 19.2 19.0 19.1 19.1 18 9 19.2 19 4 19 2 19.1 19.2 19.0 16.9 18.8 18.9 19.3 19.3 19.2 19.2 19.2 19.0 19.0 19.2 19.1 19.0 19.1 16.9 19.0 19 1 19.1 19.2 19 2 19.3 19.3 19 4 19.4 19.4 19.3 19.5 19 5 19.2 19.2 19.2 19.2 19.2 18.9 16.6 18.8 18.6 18.7 18.8 16.8 18.6 16.8 19.0 18 8 18 7 18 9 18.8 18 6 18 7 18.7 18 6 18.8 19 1 19.2 19.2 05 

### 0.4 04 0.6 

### 0.7 0.6 0.5 

### 0.4 0.5 0.5 0.5 0.5 0.5 0.5 05 06 0.6 0.5 

### 0.4 0.5 0.5 

### 0.4 0.5 0.5 

### 0.4 0.5 0.5 0.6 05 0.5 

### 0.4 05 0.6 0.6 0.5 0.5 0.5 0.5 

### 0.4 0.4 0.4 0.4 04 0.3 0.3 

### 0.4 0.4 05 

### 0.5 06 0.6 0.6 0.5 

### 0.5 0.5 04 

### 0.5 04 05 

### 05 04 03 0.3 

### 04 0.3 0.3 0.3 0.3 

### 0.4 0.4 0.3 0.3 0 3 8/23/05 Run #3

Page 4 

# 4?

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I I I I I 

# I I I I 

# I I I I I 

# I I I I 08/23/05 14:22:12 08123/05 14:22:22 08123105 14.22:32 08/23105 14:22:42 08!23105 14:22:52 

### 08123105 14:23:02 08/23/05 14:23:12 08/23/05 14:23:22 08/23/05 14:23:32 08/23/05 14:23:42 08/23/05 14:23:52 08/23/05 14:24:02 08/23/05 14:24:12 08/23/05 14:24:22 08/23/05 14:24:32 

### 08/23/05 14:24:42 08123105 14:24:52 08123105 14:25:02 08/23/05 14:25-12 08/23/05 14:25:22 08/23/05 14.25:32 08123105 14:25:42 08/23105 14:25:52 08/23/05 14:26:02 08/23/0514:26:12 

### 08/23/05 14:26:22 08/23/05 14:26:32 08/23/05 14:26:42 08/23/05 14:26:52 08!23105 

### 14:27:02 08/23/05 14:27:12 08/23/05 14:27:22 08123105 14:27:32 08/23105 14:27:42 08/23/05 14:27:52 08123105 14:28:02 08/23/05 14:28:12 08/23/05 14:28:22 08!23!05 14.28:32 08/23/05 14:28:42 08/23/0514:28.52 08123!05 14:29:02 08!23!05 14:29:12 08/23/05 14:29.22 08123105 14:29:32 08/23/05 14:29:42 08/23/05 14:29:52 08/23/05 14:30'02 08/23/0514:30:12 08/23/05 14.30:22 08!23!05 14:30:32 08/23/05 14.30:42 08123105 14·30:52 08/23/0514:31:02 08/23/05 14"31 12 08/23/0514'31:22 08/23/0514:31:32 08/23/0514:31:42 08/23/0514:31:52 08/23/05 14:32:02 08/23/0514.32:12 08/23/05 14:32:22 08/23105 14:32:32 08123105 14:32.42 08/23105 14:32:52 08123105 14:33"02 08/23/05 14.33:12 08/23/05 14.33:22 08/23/05 14"33:32 08/23/05 14:33'42 08/23/05 14"33:52 08/23/05 14'34.02 08/23/05 14:34:12 08/23105 14:34:22 4.5 4 7 4.6 4.6 4.6 4.6 4.7 

### 50 48 4.7 45 4.6 4.5 4.3 4.1 4.1 4.0 

### 4.0 3.9 4.0 4.1 

### 42 43 4 1 

### 4.2 4.1 41 4.3 4.5 

### 4.4 4.6 4.5 51 4.8 4.8 4.7 4.5 

### 4.4 4.5 

### 4.4 44 

### 4.4 45 4.5 4.5 4.5 4.5 4.5 4.5 4.5 

### 4.4 4.3 44 4.3 43 43 

### 43 4.3 

### 4.3 

### 4.4 4.3 

### 4.3 

### 4.2 4.1 

### 3.9 4.0 

### 39 39 4.0 4.1 

### 42 4.2 

# " 4 3 103.4 103.3 102 2 100.6 98 4 96.2 95.5 95.5 95.0 95.6 98.7 100.0 99.4 100.5 102.4 102.2 101.3 99.8 97.3 95.5 

### 93 7 91.9 90.6 89.8 89.2 88.9 88.6 88.9 88.8 89.1 90.4 90.4 90.9 91.9 92.8 93.1 93.6 94.4 94.8 

### 95 0 95.5 95.5 95.2 95.8 95.9 95.4 95.1 95.7 95.5 95.8 96.5 97.4 97.6 97.5 97.8 97.3 96.9 96.5 95.9 94.9 94.5 94.4 93.9 93.8 94 3 94.0 93.1 91.7 90.2 88.5 87.2 86.5 86.2 86.6 19.1 19.1 19.0 19.1 19.0 19.1 19.1 19 1 19.3 19.4 19.2 19.2 19.3 19.1 18.9 18.8 18.8 18.9 19.1 19.2 19.3 19.3 19.2 19.2 19.2 19.1 19.1 191 19.4 19.2 19.2 19.3 19.3 19.4 19.3 19.3 19.3 19.4 19.5 19.7 19.9 19 8 19.7 19.7 19.7 19.5 19 2 19.2 19.0 18.9 19 1 19 3 19 1 19.1 19.1 19.1 19.1 19.0 19.0 19.2 19.4 19.4 19.5 19.4 19.4 19.3 19.3 19.3 19.4 19.6 19.7 19 8 18 7 19 6 0.4 

### 0.4 04 

### 0.5 0.4 0.3 

### 0.4 0.5 

### 0.4 04 

### 0.4 0.4 0.3 03 03 

### 0.4 0.3 

### 0.2 0.3 

### 0.4 0.4 0.4 0.4 0.4 0.4 0.4 0.4 0.3 

### 02 02 0.3 

### 0.5 0.5 0.5 0.5 0.3 

### 0.4 04 

### 0.5 0.5 

### 0.4 0.4 0.4 0.4 0.4 0.3 0.3 

### 04 0.3 04 

### 0.4 0.4 0.5 

### 04 0.3 

### 0.4 

### 04 0.4 0.4 0.4 0.4 0.5 

### 0.4 0.3 03 0.3 0.3 

### 0.4 0.5 0.5 

### 04 04 0.3 

### 02 8/23/05 Run #3



### Page 5 

# 48

# I

I I I I I I I I I I I I I I I I I I 08123105 14:34:32 08123105 14:34:42 08123/05 14.3452 08/23/05 14:35:02 08123/0514:35.12 08123105 

### 14:35:22 08123105 14:35'32 08123105 14:35:42 08/23/05 14:35:52 08123105 14:36:02 08123105 14:36:12 08/23/05 14:36:22 08123105 14:36 32 08123105 14:36:42 08/23/05 14:36:52 08123105 14:37-02 08123105 14.37:12 08/23/05 14:37:22 08123105 14:37:32 08123105 14'37.42 08/23/05 14:37:52 08123105 

### 14:38:02 08/23/0514:38:12 08123105 14:38:22 08123105 14:38:32 08123105 14'38:42 08123105 14:38:52 08/23/05 14:39:02 08/23/0514:39'12 08/23/05 14'.39:22 08123105 14:39:32 08123105 14:39:42 08123105 

### 14:39:52
Stop Run #3

08123105 14:40:02 08/23/05 14:40:12 08/23/05 14:40.22 08123105 14:40_32 08/23/05 14:40:42 08123105 14.40:52 08/23/0514:41:02 08/23/0514:41"12 08/23/0514:41.22 08123105 14:41:32 08123105 14:41 :42 08/23/0514'41:52 08123105 14'42:02 08123105 14:42:12 08123105 14:42.22 08123105 14:42:32 08123105 14:42:42 08123105 14:42:52 08123105 14:43:02 08123105 14:43:12 08123105 14:43:22 08123105 14:43:32 08123105 14.43:42 08123105 14:43:52 08/23/05 14.44:02 08123!05 14:44:12 08123105 14:44:22 08123105 14:44:32 08/23/05 14:44:42 08123105 14.44:52 08/23/05 14:45:02 08/23/0514.45:12 08/23/05 14:45.22 08/23/05 14:45:32 08/23105 14 45:42 08/23/05 14:45:52 08123105 14'.46:02 08/23105 14:46:12 44 4.4 4.5 46 46 4.5 

### 4.7 4.6 4.9 

### 4.7 45 4.5 43 4.5 48 4 3 4.1 

### 40 3.8 

### 3.5 34 

### 3.5 3.7 39 3.8 3.9 

### 4.0 

### 42 4.3 

### 4 7 4.8 

### 5.0 4 7

4.41



### 5.3 49 31 

### 17 14 1 3 1.4 14 1 4 1 4 1 4 1.4 1.3 

### 14 1.3 1 3 1.3 

### 1.3 1.3 1 3 1.3 1.3 1.3 1.3 1.3 

### 1 3 1 3 1 3 1.3 1.3 

### 1.3 1 2 1.3 1 3 1.3 1.3 1.3 

### 1.3 87.9 88_5 88_9 89_8 91.3 92.5 93.1 94.1 95.2 95.8 96 1 96.9 97 6 98.1 98.2 97 9 97.4 96.5 95.9 95.4 94.1 92.2 90.4 88.4 86.4 84.0 82_5 81.0 79.2 78_9 78.9 80.1 82.7

94.76

84.5 86.7 87.9 87.8 75.0 51.4 35.0 23.3 16.5 120 8.9 7.2 

### 64 5.9 5.3 52 4.8 4.8 4.6 4.7 4.5 4.3 

### 4.3 4.1 

### 42 4.5 4.6 4.6 

### 44 44 4.3 

### 44 4.5 4.3 

### 4.3 

### 42 38 

### 36 19.4 19.3 19.2 19 3 19.3 19.3 19 

### 5 19.4 19.3 19.4 19.2 19.1 19.2 19.4 19.3 19.4 19.4 19.4 19.4 19.3 19.2 19.2 19.3 19.3 19.5 19.7 19.6 19.6 19.6 19.5 19.5 19.4 19 3

19.20

19.2 19.2 19 2 18.4 16 9 12.3 9.0 66 

### 50 4.0 3.4 

### 3 0 2 7 2.5 2.3 

### 22 22 2.1 1 9 1 9 1 8 1.8 

### 17 1 7 1 7 1.6 1.6 

### 1.6 1.6 1.5 1.5 1 5 1 5 

### 1.5 1 5 15 

### 1.5 14 

### 0.2 0.2 0.2 

### 03 0.3 0.3 0.4 

### 02 0.2 0.2 0.3 0.3 0 3 

### 04 04 

### 04 04 

### 04 0.4 0.3 04 0.4 0.3 0.3 0.2 0.3 0.3 0.3 0 1 0.1 0.2 

### 02 02

0_80

0.3 0.3 0.3 0 3 

### 04 0.3 0.3 0.1 0.1 0 1 0.1 0.1 0 1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0 1 0.0 00 0.0 

### 0.0 0.1 0 1 0 0 00 0.0 0 1 0.1 0.1 

### 0: 01 8/23/05 Run #3

Page 6 

# 49

# I

I I I I 

# I 

# I I I I I 

# I I 

# I I I I 

# I I 08/23/05 14:46:22 08/23/05 14 46 32 08/23/05 14:46:42 08/23/05 14 46.52 08/23/05 14:47•02 08/23/05 14:47:12 

### 08/23/05 14:47:22 08/23/05 14:47:32 08/23/05 14:47:42 08/23/05 14:47:52 08/23/05 14:48:02 08/23/05 14:48:12 08/23/05 14:48:22 08173/05 14:48:32 

### 08123105 14:48:42 08123!05 14:48:52 

### 08123!05 14:49:02 08/23/05 14:49:12 08/23/05 14:49:22 08/23/05 14:49:32 

### 08123105 14:49:42 08/23/05 14:49'52 08/23/05 14:50_02 08/23/0514:50:12 

### 08/23/05 14:50:22 08/23/05 14 

### 50:32 08/23/05 14:50:42 08/23/05 14 50:52 08/23/0514:51:02 08/23/0514:51:12 08/23/05 14:51:22 

### 08/23/0514:51:32 08/23/05 14:51 :42 08/23/05 14:51 :52 

### 08/23/05 14:52:02 08/23/05 14:52:12 08/23/05 14:52:22 08/23/05 14:52 32 08/23/05 14:52:42 

### 08/23/05 14:52:52 08/23/05 14:53 02 08/23/05 14:53:12 08/23/05 14:53:22 08/23/05 14:53:32 08/23/05 14:53:42 

### 08123105 14:53:52 08/23/05 14:54:02 08/23/0514:54:12 08/23/05 14:54:22 08/23/05 14:54:32 08/23/05 14.54:42 08/23/0514:54:52 08/23/05 14:55:02 08/23/0514:55·12 08/23/05 14:55:22 08/23/05 14"55:32 08/23105 14:55:42 ORI?::l/05 14·55·57 08/23/05 14:56'02 08/23/05 14:56:12 08/23/05 14:56.22 08/23/05 14:56.32 08/23/05 14:56:42 08/23/05 14:56:52 08/23/05 14.57:02 08/23/05 14:57:12 08/23/05 14:57:22 08/23/05 14:57:32 08/23/05 14:57:42 08/23/05 14.57:52 08/23/05 14.58:02 08/23/05 14'58:12 08/23/05 14:58:22 1.2 13 1 3 1.3 1 3 1.3 1.2 1.2 1 3 1.3 1.2 

### 0.7 0.5 04 

### 0.5 0.4 0.5 

### 0.5 0.4 0.4 0.4 0.3 03 04 04 0.4 0.4 0.4 0.4 0.3 0.3 0.4 0.4 0.4 0.4 04 0.4 0.4 03 03 0.3 0.3 0.3 0 3 0.3 03 0.3 0.3 0.3 0.3 03 

### 0.3 0.3 0.3 0.3 1.0 1.2
1 ' 0.8 0.4 0.3 0.3 0.3 0.3 0.3 0.3 0.3 0.3 0.3 03 0.3 0 3 0.3 3.8 4.0 

### 3 g 3.9 4.1 4.3 4.4 4.7 4.7 4.3 4.3 44 4.4 43 4.0 3.8 3.9 3.9 4.0 

### 3.7 3.5 3.5 3.4 3.4 33 3.0 3.0 3.0 30 

### 3.1 

### 3.5 3.5 3.6 3.5 3.4 

### 3.6 

### 51 25.1 53.5 73_3 84.9 90_9 94_6 96 8 98_2 98.9 99.0 99.4 99.8 100.1 100.1 

### 100.3 100.4 100.6 100.6 1001 99_8 91 9 67.2 37.2 18_5 10_5 

### 6.6 4.7 3.8 

### 36 3 5 3.3 

### 3.3 3.2 2.9 2.7 2.8 1 4 1 4 1.3 1.4 13 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1.2 

### 28 9.1 14.8 18.5 20.9 22.1 22.9 23_3 23.7 23.9 23.9 23_9 24.0 24.1 24.2 24.3 

### 24.3 24.4 24.3 24.4 24.3 24.1 24.2 239 19.6 12.5 76 4.7 3.1 2.1 1.6 1.3 1.1 0.9 0.9 

### 08 08 

### 07 

### 0.7 0.7 0.7 0.7 0.7 

### 06 07 0.7 0.7 0.8 0.8 

### 0 9 09 0.9 1.0 0.9 1.0 0.9 0.9 09 0.9 0.9 0.0 0 0 

### 0.0 00 

### 0 0 0.0 

### 0.0 0.1 0 1 0 1 0.1 01 0.1 00 

### 00 0.1 0.1 0.1 

### 0.0 0.0 00 

### 0.0 0.0 

### 0.0 0.0 

### 00 0.0 0.0 0 0 

### 0.0 0.0 0.0 0.0 0.0 -0.1 

### 00 00 0 0 0.1 0.1 0.1 

### 0.0 0.0 

### 00 0.0 -0.1 0.0 00 0 0 0 0 00 

### 00 0 0 0 0 0.0 -0.1 -0.1 00 0.0 0.0 

### 00 0 2 13 

### 36 

### 66 96 12_7 15.4 17.9 20.3 

### 22.8 25 0 26_9 8/23/05 Run #3

25_5 ppm NOx Zero CO, S02

99 1 ppm CO Zero VOC, NOx

Page 7 

# 50

# I

8/23/05 Run #3



# I

08/23/05 14:58-32 0.3 3.1 09 

### 28.5 08/23/0514:58:42 0.3 3.1 0.9 30_0 

# I 08/23/05 14-58:52 0 3 2.8 09 31.3 08/23/05 14:59:02 0.3 31 09 32.5 08/23/05 14:59:12 02 3.4 09 33_9 08/23/05 14:59:22 03 3.5 0.8 

### 34.9 08/23/05 14 59:32 0.3 3.5 0 9 35.6 

# I 08/23/05 14:59:42 0.3 3.4 0 8 36.5 08/23/05 14:59:52 03 3.6 0.8 37.4 

### 08/23/05 15:00:02 0.3 3.6 0.8 38.2 

### 08/23/05 15:00:12 0.3 3.5 0.8 

### 38.7 

# I 08/23/05 15:00:22 02 3.2 0.8 

### 39.1 

### 08/23/05 15:00:32 03 28 08 

### 39.6 08/23/05 15:00 42 0.3 2.8 08 40 0 08/23/05 15:00:52 0.3 2.9 0.8 40_4 

### 08/23/05 15:01 :02 0.3 29 08 

### 40.8 

# I 08/23/0515:01'12 0.3 29 0.8 41.2 

### 08/23/05 15:01 :22 03 3.1 07 41.7 08/23/05 15:01:32 0.3 3.3 07 42.1 08/23/05 15:01 '42 0.3 34 0.7 42 4 

### 08/23/0515:01:52 0.3 3.2 07 

### 42.5 

# I 08/23/05 15:02:02 0.3 3.2 0.7 

### 43.6 08/23/05 15:02:12 0.3 34 0.7 44.8 

### 08/23/05 15:02:22 0.3 3.3 0.7 

### 45.0 08/23/05 15:02'32 0 3 3.3 0.7 

### 46.2 

# I 08/23/05 15:02.42 0.3 3.1 0.6 

### 46.3 50.1 ppm 

### 802 08/23/0515:02•52 0.3 2.7 0.7 

### 46.4 08/23/05 15:03:02 1.4 2.4 0.6 

### 46.5 08/23/0515'03:12 14.2 2.7 0.6 45.2 

# I 08/23/0515·03:22 15_0 2.6 0.6 42.2 08/23/05 15:03:32 

### 15.0 2 7 0.6 42.1 08/23/05 15:03'42 

### 15.0 29 0.6 41.1 15 2 ppm C3H8 08/23/05 15:03:52 

### 15.0 3.2 05 38.9 

# I 08/23/05 15:04:02 

### 15.0 3.2 04 36_1 08/23/0515:0412 14 9 3? 04 Cl:l::l 08/23/0515-04:22 5.2 3 1 04 30 6 

# I I I I I I I I I 51

Page 8

# I

I I I I I I I I I Appendix C 

# I I I I I I I I I

# I

I I I I I I I I I I I I I I I I I I Summary of Analytical Procedures

1. 

## Particulate
Samples were transported to the office of Armstrong Environmental, Inc. by Tom Armstrong and delivered to Tom Annstrong on 8/24/05. After insuring no leakage had occurred in transport, probe washes and impinger solutions were measured with a glass measuring cylinder. Probe washes were transferred to glass beakers, rinsing both the sample bottle and m;:asuring cylinder with acetone and adding this rinse to the total sample volume. Impinger #1 on the scrubber exhaust was diluted to 300 rnls wrth H20. After evaporating the probe washes on a hot plate, samples were desiccated for 24 hrs and weighed to a constant weight. Filters were desiccated for 24hrs and weighed to a constant weight. A I 0 

## rn1 aliquot was taken from the impinger #1 solution and analyzed for HF and HCl, the balance transferred to glass beakers and evaporated in a oven, desiccated for 24 hrs and weighed to a constant weight. The analytical balance (Ohaus Explorer digital) was calibrated with an internal 100 gr. standard. Filters were handled with tweezers, beakers were handled with latex gloves and tongs.

2. HFand HCl

The ion chromatograph was calibrated using certified standards of 992 mg/hter fluoride and 986 mg/liter chloride. Working standards were made by adding 0.5 rnls, 1.0 rnl, 2.0 mls, and 4.0 rnls to a 100 rnl volumetric flask and diluting to the mark with either H20 or H2S04. The second standard for H20 calibration was made twice, the second set of injections used in the calibration curve. Standards were injected into the IC using a manual injection valve. After insuring no leakage had occurred to the remaining samples (impingers 2,3 & 

## 4 on the exhaust, impingers 1,2 & 

## 3 on the inlet) each sample was diluted to a constant volume (300 rnls for the exhaust, 500 rnls for the inlet) and injected into the !C. Each sample was injected twice into the IC with the exception of Run #2 from the exhaust on impinger 2,3 & 

## 4 sample which
was injected four times.



# 52

# I

I I I I I I I I I I I I I I 

# I I I I FILTER ANALITICAL DATA

Company: Daltile, Conroe, TX Date: 

## 8/23/05 Location: Kiln Scrubber Exhaust Run 

## 1

Filter ID Number

Date of Weighing Time 

## Gross Filter Wt.

Date of Weighing Time Gross Filter Wt.

Ave, Gross Filter Wt.

Date of Weighing Time Filter Tare Wt.

Date of Weighing Time Filter Tare Wt.

Ave. Filter Tare Wt.

Wt. of PM on Filter (grams)

Total Weight of Particulate (mg) 44T



# 8126/05 7:03AM



## OAD54

8126105 

# 2J4PM

OAD57

0:4056



# 8/3105 12'30PM 

# 03736

8/4!05 9:37AM



# 0,3736

0.3736

0.0320

32.0 Run 2



## 45T



# B/26/05 7:02AM

04106



# 8/26/05 2'15PM



# 0.4108

0:4107

813105 

## 12:33 

# PM 0:3812

814/05 9:39AM



# 0:3814

0.3813

0.0294

29.4 Run 

# 3

46T



## 8/26105 7:01AM

0:4050



# 8126105 2'16PM



# oAb51

0:4051

8/3105 12:35PM 

## 0,3755

8{4/05 

## :40AM 

# 0.3766

0.3766

0.0285

28.5



# 53

# I

I I 

# I I I I 

# I I I I 

# I I I I I 

# I I 

# I PARTICULATE ANALYTICAL DATA FORM

Company: 

### Dalt1le, Conroe, TX 

## Date: 8/23/05 Location: 

### K1ln Scrubber Exhaust 

## Run 1

Density (Pa)

Blank Concentration (Ca) Rinse Volume (Vaw) 

### Residue in Rinse (Wa) 

### = Ca·x-vaw-x-pa



### Date of Weighing Time Gross Weight



### Date of Weighing 

### Time Gross Weight

Date of Weighing 

## Time Beaker Tare Weight

Date of Weighing Time Beaker Tare Weight
Average Gross Weight Less Blank Residue (Wa) Average Beaker Tare Weight

Weight of Particulate in Rinse (mg) 

## 0.7851

0:0005095 178 

## 0.0001

8/26105 2:19PM 98:3918

7/6/05 

## 7:11AM 98.3769

7/6/05 2.33PM 

## 98.3759

98.3919

0.0001 98.3759

15.88 Run 2



## 0.7851

0.0005095 165 0.0001

8126/05 6:59AM 107A852



## 8/26/05

**2:!S~M** 

## 107:4852

7/6/05 7'12AM 107.475:2

716/05 2:32PM 1074753

107.4852

0.0001 107.4753

9.88



## ACETONE BLANK ANALYTICAL DATA FORM

Blank Volume (Va)

Date of Weighing Time Gross Weight

Date of Weighing Time Gross Weight
Average Gross Weight

Date of Weighing Time Tare Weight

Date of Weighing Time Tare Weight
Average Tare Weight

Weight of Blank (Ma) Ca= Ma/(Va'Pa) = mg/g 

## 250

· 8/26105

6:56AM


## .•:· \OS:2903 

# sn6io:; 2:21 F'M 

## 103.2904

103 29035

716!05 7•!7AM 

## !032904.

7/6i05

. 2:29PM 

## !03.2901

103.29025

0 00010 0 00051

Note: In no case should a blank residue greater than 0.01 mg/g or 0_001% of the blank wei ht be subtracted from the sam le wei ht. Run 3



## 0:7851



## 0 0005095 182 0.0001



## 8/26/05 6:53AM 99:1614

8/26105 2:24PM 99.1611

7/6/05 7:13AM 

## 99.1556

716105 2:31PM 99.1555

99.1613

0.0001 99.1556

5.63



# 54

# I

I I I I I I I I I I I I I I I I I I PARTICULATE ANALYTICAL DATA FORM

Company: 

### Daltile. Conroe. TX 

## Date: 8/23105 Location: 

### Kiln Scrubber Exhaust 

## Run 1
DenSity 

### (Pa) l



### Blank Concentration (Ca) Rinse Volume (Vaw) Residue in Rinse (Wa) :::: 

### ca-lfvaw·K-Pa

Date of Weighing 

## Time Gross Weight



### Date of Weighing 

## Time Gross Weight



### Date of Weighing 

## Time Beaker Tare Weight

Date of Weighing 

### Time Beaker Tare Weight
Average Gross Weight 

### Less Blank Residue (Wa) Average Beaker Tare Weight


### Weight of Particulate in Rinse (mg) 

## ZE.Q7 '300 0.0001



## 8!26105 6:52AM 106.6855

8126/05 2:25PM !05.6853

716105 7:14AM 

## 1066845

7/6/05 2:30PM !06.6844

106.6854

0.0001 106.6845

0.89



## H20 BLANK ANALYTICAL DATA FORM

Blank Volume (Va)

Date of Weighing Time Gross Weight

Date of Weighing Time Gross Weight
Average Gross Weight

Date of Weighing Time Tare Weight

Date of Weighing Time Tare Weight
Average Tare Weight
Weight of 

### Blank (Ma) Ca= Mai(Va'Pa) 

### =gig 

## 250**8/2610~** 

### 6:57AM 101Hll8

s/26105 2:20PM 

## !OO.Ul9

100.11185



## 716!05 T18AM !DO:)Tl9

716105 2:28PM 100.!H7

100.1118

5E·05 2E·07 Run 2



### l


## 2EcQ7



## 300 0.0001

8/26/05 6:54AM 1()7:4510

8126/05 2:23PM 107.4509

7/6/05. 7:15AM 

## 107:4472

7./6/05 2:29PM 10?.4471

107.4510

0.0001 107.4472

3.74

Note: In no case should a blank residue greater than 0 01 mg/g or 0.001% of the blank wei ht be subtracted from the sam le wei ht. Run 3



### 1



## 2£•07

300 0 0001

8/26/05 .6:55AM 100]654

8/26105 2:22PM 100.7652

7/6105 7:16AM 100.7645

7/6/05 2:28PM 100:7643

100.7653

0.0001 100.7644

0.84



## .I 

# 55

# I

I I 

# I I I I I I I 

# I I I 

# I I I I I I Company: 

## Date: Location: Run#:

Filter lD Number

Date of Weighing Time Gross Filter Wt

Date of Weighing Time Gross Filter Wt

Ave. Gross Filter Wt

Date of Weighing Time Filter Tare Wt

Date of Weighing Time Filter Tare Wt

Ave. Filter Tare Wt

Wt of PM on Filter (grams)

Wt. 

## of PM 

## in Rinse (grams)



## Total Weight of Particulate (mg) F! L TER AN ALIT I CAL DAT 

## P.



# Cliff 

# !J(u('O.C
7'.03 

# ' 'P

**~""{** 

# f(u(o! r<.f:rY ''-/:0 

# £'7 

# /' ( OrA!O 

# e.__

**~**



# vs-r tlvdor 71:

**0~}__--** 

# ·' lfl o&



# <g(u/o!
I '{ 

# i I.'> 

# ,"flcg

I 

# ?/J/ o:;- ' /- 

# '-(to I 

# i{1k/oi- ' .·o I



## , '-to 

# s-o ?fu.(v-1 I'/', 10 

# ,'f'D)i



# ;; /3

**;,,~­**

**i~:::/s.­** 

# o.3

.. 

# :rt."::;-



# ;; ;c-r/ /'

**s·~** "'-( : '-ft) 

# 6 ?,-:t-tf?



# 56

# I

I I I I I I I I I I I I I I I I I I Dote:

3:;nk**C~n:.:ent1ation** 

### (C2)**~insf** 

### \'-,lume (Vaw) 

### Resd•./e h .=::-i.:-Jse (\,., 1 ::;)

### ~ 

### C?"""\i?vl'?a

7im-e



## lime

Averag:; Sr-:=tss Wel.sht Less

## 3i3.n.~**?esi·j~..Je** (\'1 1 

### a) 

## Jwer'i:?e 3;3ker T-E3J;; 

## Weight 

# !t:lft.ti iB;moy 

# t> 2- 

# I ?-tin 3

# .r;f:~;~r;; li:tUi1111>

# .,m~~~~mJ; tMiH17



# 57

# I

I I I I I I I I I I I I 

# I I I I I I**3:z:~tk Co7!c~r.t~::.'ckm**  

### (C:3)**,=:i~:tse** 

### VJliJiTle (Vaw) 

### ;::es!:J:

... /e i;; R·i-nse (Wa)**~** 

### C:o

....**\ia\.'1~"'"-?a**



### Ti;ne



## Time

Ave:-a_ge 

## Gr:..ss**VVeig~t l_~s.s**  

### 31:::-n.i.:·Resd'Je (I:Va)**A'':;-.;~, 3oa~.o-** **~---, \~loj-7{1"-**  '-'-:::.-

- '.-'tor_ -s ''

# ~.·· '',qz;

# ~!!~~0: t67: '(g$2-



# TJ{t;/p;iy DJWt:< ji;)U/)@

# ','J~~'~j f\ft41$J ?.u 

## n 3

# .~mW0 'tf;tW"lf

# ',~~.~~) '•oo•Vtitr:••:



# 58

# I

I I I I I I I I I I I I I I I I I I ?.b?Ti·:ULA_T::

**~_1\,_!.LYT·:.L.L** 

## )P.iA

**02f\~** 

## Com?acy 

# Do, 

# l+. \C.

Dcte:



### 3io;nk Conc::n:r:::tion (C:a)

**F-Ci~se Volu~e**  

### (Vcw) 

### Resi-j:.._,·e in

**~-lnse** 

### (W?.):::

**Ca""'V:::v.~"?3**

**Dote:;~** 

### W::ighing 

## lime

.ll..verage Gmss Vv'eight



## Le~s **3Ja'n~:-?=si·::l!.Je** 

## CYh) P.ve.-:-2ge

**3eof:~r** 

## Tar:: W:=ignt 

# D rb

?. u n 

### l

......... :::::::



# *~~··········

**····-····~·-·····** 

# •

!



# ;t~ltJ-N! fb''N 

# 'i'QJ<f



# ~rf~4tf!J. W/7it.ii.F1>'



# ·:!~t~;J

5Q

# I



# I I 

# I I 

# I I I I I I 

# I I 

# I I 

# I I I 

# I Summary of HF and HCI Analysis

Plant: 

## Daltile, Conroe, TX

-- - ---- --- 

## Location: 

## Kiln Scrubber Exhaust:

--- --- ----- 

## - 

## Date: 

## 8/23/05

Run#



## 2 2

3 3

,_ --

---- ----- 

## 1 2,3"& 4 1 .2,3,& 4

2

**],3,8.~** 

# .. 2 2,:>,& 4 2 2,3,& 4 22,3,&4

--- - -- 

## 3 2,3,& 4 3],3,& 4- _:VolumE!

. _[)jlution 

## 300'-- 300'

1 , 300 300

300 1 ' 300

300; 

# :loo[

300 300 300 

# :loa··

300 300

- 

## Sheet1

--- - -- 

## FI-, ug/ml HF, mg Cl-, ug/ml HCI, mg



# . 6.27: 6:08529:3_- Q62 0 191]0!l 1, 0.28 0.088452 0.65 0.20046

---- - ------ 

## Average 0.086873 0.195834

0.22 0.069498 0.71 0.218964 0.23. 0.072657 0.68 0.209712 Average 0.071078 0.214338

0.26 0.082134 0.9 0.27756

---------------- - - - --- 

## 0.27 0.085293 0.94 0.289896

----- --- ------ ----- 

## J;ver<Jge 0.083714 0.283728

----- . 

## 048 0.151632 0.35 0.10794

---- - 

## 1 : 

## 047 0.148473 0.37 0.114108

-· ------ ------ 

## )\.verage 0.150053 0.111024

.. - 

## 043 0.135837 0.56 0.172704 0.38' 0.120042 044 0.135696 048 0.151632 0.52 0.160368 0.31 0.097929 048 0.148032 Average 0.12636 0 1542

0.5 0.15795 042 0.129528 0.54 0.170586 042 0.129528

. - 

## ,Average 0.164268 0.129528

Totals 

## Run #1 0.236925 0.306858 Run #2 0.197438 0.368538

- 

# , ---- - 

## Run #3 0.247982 0413256



# 60

Page 1

# I

I I I I I I I 

# I I I I I I I I I I I Sheet1

Summary of HF and f:l(;l Jl.nalysis

Plant: Daltile, Conroe, TX Location: Kiln Scrubber Inlet

- ----- 

## Date: 8/23/05

Run# Imp# Volume Dilution Fl-, ug/ml HF, mg**(;l:,u~/ml** 

## HCI, mg 1 1 ,2 

## & 3

- -- ------ -- 

## 1 1 ,2 & 

## 3

2 1,2 & 

## 3 

## 2 1,2 & 

## 3

3 1,2 & 

## 3 3 1,2 & 

## 3 500 10 14.65 77.13225 26.76 137.5464 500

500 500

500 500 10 15.19 79.97535 Average 78.5538

10 17.39 91.55835 10 17.37 91.45305 Average 91.5057

10'

---------- 

## 10 i 

## 13.31 70.07715 12.94 68.1291 Average 69.10313

Page 1 ------------------ 

## 26.98 138.6772 138.1118

28.55 146.747 29.39 151.0646 148.9058

23.88 122.7432

-- ---- 

## 23.64. 121.5096 122.1264



# 61

# I

I I I I I I I I I I I I I I I I I I Conditions
Date Time

Component i (>



## Fl· 

## 1. 1


## .........



## Cl· 1 666


## 2 ''



## ........



## 6 '



# Component


# FlCl2 

# 4.96 ug/!nl Fl- 

# in H20 4.93 ug/ml Cl- in H20 08/24/2005 09:30:02



# Number Retention

1 

## 1 .050 2 

## 1.666 

# Area

403

.. 80**~1** 

## 301.75 M

705.55 1 0/A

.. 000!1'\!



# External Units

4.54 ug/ml 4.b9 ug/ml

'''

) 

# Area external

403.80 M 4 '54

30i.75 M 4 '59



# 62

# I

I I I I I I I I I I I I I I I I I I c:ond5. 

# tic.ns



# D.ste**TimE~**



## Co11ponent



## Fl- 1. 

# '

.........


# Cl- 1. 6 

## 2

.........

3i

..



## 4

......... .

\



### .....



## 6

........ .



# Component**Fl~** 

## Cl-

..

2 6

### -~ 

## '76 ug_/ml 

## 4

. 93 ug_/m 

## l 

## 08/24/200S 09:33:04



# !.:: :: t::' ]_-

## Cl

# Number Retention

1 1"050 

## 2 

## 1

.. 666 

# i.n H2Cl 

# in H20

1 C)2 4

. 00()rn\J 

# Area**Ex.~ernal**



## 403.50 M 4

. 54

315.65 M 

## 4.79



# Area External Units

403 ".50 

## f"l 

# 4.54 

# ug/rnl 315.65 M 

# 4.79 

# ug/mJ

719

.. 15 9

.. 33

.. : 

# 63

# I

I I I I 

# I I I I I 

# I I I I 

# I I I 

# I I FlCl**Fl~**

# Clc:or!ditions


# Date Time

1. 

# H

Component

2 

# 9.92 ug;'ml Fl- in H20 9.86 ug/ml**~~-** 

# irf H20 08/24/2005 09:36:'54



# Number Retention Area

1 1. 

## .050 

## 795.75 2 1 

## 666 579,12



## 1374.87 l**'~J2Ll** 

## . OOC'trr\/



# 795.75 M 9.42

579.12 M 8.48



# External Units**~1** 

## 9A2 

# ug/ml M 

## 8 Ji8 

# ug/mJ

17.89



# 64

# I

I I I I I I I I I I I I I I I I I I Conditions

Date Time**9~92** 

# ug/ml**9~86** 

## ug/ml. 

## 08/24/2005 09:40:23 F.l

# Componsnt -· J ()2
, li 

### (.;Om\/ 

# ?stentio',,J

... ''I'"''
'



# fl- ;.:::::::::::"·::"::

.... , 

## ............ ''""'"""""''"'''. 

## 1 . 

## .11'''" 

# I 1 '666! ; 

### ..... , ........ 

### ,::·:,,,,,,,,,,,,,

.. . 

# Cl-

Component Number Retention


# n- 1 1

.. 050 

# c .l

-- 2 1 .666



## 2 

# in 

# in H20 H20



# Area

873" 15 560.00



## 1433.15 

# External**~·1** 

## 10.30 M 

## 8 _41



## 18.71**~rte~** 

# na.l

873.15 M 10.30

560.00 M 

## 8.41



# Units ug/rnl ug/rnJ



# 65

# I

I I I I I I I I I 

# I I I I I I I I I Fl

# ClFlClConditions

Date 

# Time

1 . ; .•

1.700



# Component

2 19_84 

## ug/ml Fl-**~n** 

## H20 

# 19.72 ug/ml Cl- in H20 08/24/2005 09:45:00

Number Retention Area

1 1.066 

## 1692.90 

# 2 1 

# .700 1.380.90

3073.80**~.rea** 

# External

1692.90H 19. 39

1380. 90 M 21

. 35



# External Units

1"1 

## 19.39 

# ug/ml M 

# 21.35 ug/m.l



# 40.74



# 66

# I

I I 

# I I I I 

# I I I 

# I I I 

# I I I I 

# I I Fl

# ClFl# ClConditions

Date 

# Time

Component

2 

# 19_84 ug/ml**~·1-** 

# in H20 

# 19.72 ug/ml Cl- ln H2G 08./24/2005 

## 09048,11



# Number Retention Area

1 

## 1.066 1.690.15


# ,, 1.700 1346.30 /,



## 3036.45 

# Area

1690.15 M 19.36



## 1346.30 M 

## 20.86



# External Units**~1** 

## 19.36 

# ug/rnl**~1** 

## 20.86 ug/mJ



## 40.22



# 67

# I

I I I I I I I I I I I I I I I I I I Date Time 39.68 ug/ml Fl- in H20 39.44 ug/ml Cl- in H20 08./24/2005 09:53:14**~ompDnt'n:.** 

## Ret.enti"i'

. . , .................................................................. .



# Fl- 1.



# ClComponent Number Retention Area

F 1 ·-· 

# ' 1.066 3245.20 .c 

# Cl- 2 1 "716 287-5,30



## 2 

## 6120.50 l 02.6. ,_ OOOm\J 

## Area 

# ::xtsrnal

3245.20 M 37.82

2875.30 38.49



# External Units**~~** 

# 37.82 

# ug/ml 38

.. 49 

# ug./rnl

76.31



# 68---------------------------------------



# I I I I I I I I I I I I I I I I I I I Condi t.ions



# Date Time**CCI~IPOflt'ilt**



## Fl# ClComponent

f7 

## .l# Cl2 

# 39.68 ug/ml Fl- irr H20 39.44 ug/ml Cl- 1n H20 08/24/2005**09:56~02**



# Number Retention Area

1 

# 1.083 3426.80 2 1 .716 

# 2827.75

6254.55**Ex~~rnal**



# 3426.80 M 39 '92


# 2827.75 39 .12



# External Units

M 

# 39.92 """ /rv,l w.:;:} I 

## '""" 

# 39.12 ug/rnJ



# 79.05



# 69

# I

I I I I 

# I I I I I I I I I I 

# I I I I FlClConditions**~** 

# ct. 5(-; 

# Date Time**~**



# Component

L !·



## 8'
i



# '

.........



# s,

.... 

# {.1. Cr ?.-



# - ug/ml Fl- in H20 X 11 

## ug/n1l Cl- 

# in H20 

## 08/24/2005 10:04:06

!



# Component Number Retention Area 

# FJ- 1 

## 1.050 869.20 

# Cl- 2 1"683 

## 644.53

2 1513.73 

# lrr ea b:ter Gal

869.20 M 10. 32

644.53 M 

## 10.79



# External Units**~,,** 

## 10.32 ug/m] 

# r·1 10.79 

# ug/ml

21.11



# 70-------------------------- ------- --------------- -------------- ---------------- ------------ - ---------



# I I I I I 

# I I I I I 

# I I I I I 

# I I 

# I I Ccndi**t~i<.)fl~;** 

# Date Time 9.92 ug/ml Fl- in H2C 

# 9.86 ug/ml Cl- ln 

# H20 08/24/2005 10::07:06**~-1** 

## 0/ , 40(Jrn\t Comoonent



# Fl

# Cl

# Component Number Retention Area

rJ 

# ' ,050 

# 910.45 

# " Cl- ) 

# 1.683 634.74**~** 

## 1545.19 L 

# Area

910.45 M

634.74 M



# External Units

M 

## 10.80 

## ug/nil 1'1 

## 9.79 

# ug/ml

20.59



# .. ) 71 External

10.80

9.79

# I

I I I I 

# I I I I I I I I I I I I I I Cali.brst.i_on file



# AMOUNT INJECTED AREA 0,000

................................................



## 3336.



# Avg slope of C\Jrve: 

# 85.78 Y-axis intercept: 0,00 Coeff of lin regr: 0.88**~lo.** 

## Area 

# Amount

0: 0 .000 0 .000 .1 :**t~03** 

# 650 4 

# ,960 2: 889 .825 9.920 3: 1691 .525 19.840
{j.: 

## 3336 .000**~::Jo** 

# .680**~~** 

# CF

0 .000 81 .381 89.700 85,2.58**8/~** r,-;'")

• "-'' ,j 

## 2

3



## 4

5



# 72

# I

I I I I I I I I I I I I I I I I I I AI10UNT 

## INJECTED ARE?\ 

## 0 0()0 39**<~O**
I-'



# 2851.52



# slope of curve: 69.65 Y-axis intercept· 0.00 Coeff of lin regr: 0.92

f'-lo**~1rea** 

### r:imOtJ 

## nt



## 0 : 

## 0 .000 0 000 1 : 

## 308 700 

## ,q .930 

## 2 

# ' 639 36.:, 9 

## 860 3 : 

# 1363 600 19 

## 720**:'~** 

### : 

## 2851 

## b2S ?,9 <'1, 

### !1 () ('C**~'** 

## 0 .000 62 .617 6•1 

## .844 69 

# 148

-7 ,.., ; ,,::: 

## 300 1


# 2

3



## 4

5



# 73

# I

I I I I I I I I I I I I I I I I I I Date Time Daltilc ScT·ubber**Exhaus~** 

## Run #1 I!Hf:.- :ttl 

# Volume 300 DiJ.ution 1/1 08/24/2005 10:2';;:34

-·1 Ci2

.. 

## o:;.oom\i Component

(unknown)

# FlClComponent
Fl# Cl2 

# Number

1 2 

# Retention Area
1.033 21 .71 1

.. 650 38"40



# 60.11 102l; "OOOml

. /



# External Units

r1 

# 0.27 

# ug/ml M 

## 0_62 

# ug/m1

0.89 

# Area

45.25 21.71 M



# 38.40 M



# 74 External



# N/A 0.27

0.62

# I

I I I I 

# I I I I I I I 

# I I I I I I I Component



# r**unkno~<n)** 

## (unknown)

# Fl

# ClDate Time

Component
F l·-

# Cl2 

# Dsltil2 Scrubber Exhaust**r~:un** 

# #1 Imp 

# #1 

# Volume 300**Di!utic~l** 

# 1/1 08/24/2005 

# 10:25:42



# Number Retention

1 

# 1.050 2 1 

## .666 

# Area

22.50 40.40



# 62·.90 

# External Uni t.s

M 

# 0.28 ug,/ml M 

# 0.65 

# ug/ml

0.93 

# Area

32.60 47 .00 22.50 M



# 40.40 M



# 75 Ext.s•nal



# N/A 

# N/A 0.28



# 0.65

# I

I I I I I I I I I I I I I I I I I I Date Time Run #2 In,p #1 

# Volume 300 Dilution 1/1 08/24/2005 10:32:26

-102**."~OOm\..'** 

## Component

(unknown)

## Fl

# CJComponent
Fl

# c l2 

# Number

1 2 

# Retention Area

1.033 17.95 1 "6!50 

# 43 60



# 61.55 1 rJ2.(t
, OOOrn\/



# External Units

M 

## 0.22 

# us/ml M 

# 0.71 

# ug/ml

0.93



# 76 Area

43.90 17.95 M



## 43.60 M 

## External

N/A 

# uz

Ul

# I

I I I I I I I I I 

# I I I I I I I I I Component 

# I unknown)

F

l

# Cl**Dat~e** 

# Time O<ile SCil1bbe7

**E:~haust** 

## Run #2 Imp :H1 

# VolumE: 300 

# Di

**li.~t** 

## .. 

# ion L/'1 08/24/2005 10:35:43

-- :J 

## C:2

. 4 00rn'v' 

# Retention 

# : 0. 

# 2161

1 . 

# 11 !



# sj

.....

!

...... . &i •, 

# r

Component Number Retention Area
Fl- 1 1.033 

## 18.40 

# Cl- 2 

## 1.6h6 /:1.75

2 

## 60.15 1024.000mV Area 

# External
34.30 N/A



# 18.40 M 0.23

41.75 M 0.68



# External Units

M 

## 0.23 

# ug/ml

**~1** 

### 0 "()8 

# ug/rnl

0.90



# 77

# I

I I I I 

# I I I I I I I I I I I I I I Component (unknown) (unknown)

## Fl

# ClRun :ff3 

## Imp \/oJume 300 

# Date 08/24/2005 Time 10:40:19

**~,:tJ2** 

## .. 40()rn\.i 

# Retention



# I 1.666/ 

# F''
2i'

! 

# ,
3]

.. ···

i..

... 4i

I



## Si ·

'

! I····· 

## 6·

! 

# Dilution 1/1



# Component Number Retention Area 

# Fl- 1 1,050 

# 20.90 

# Cl- 2 J ,666 5:) "50



## 2 

# 76.40 102r{ ,OOOrn\J



# External Units

M 

# 0.26 ug/ml M 

# 0.90 ug/ml



# 1 .16 Area
513.20

25.70 20.90 M

55.50 M



# 78 External



## !UA 

# N/A 0.26

0.90

# I

I I 

# I I I I I I I I I I I I I 

# I I 

# I Date 

# Time Da_l"t-ils

**s~~Tubt>~;** 

## '--· 

# :-.eu:st Run .ft3 Imt.:o #1 

# Volume 300 DilLttion 1/1 08/24/2005 10:44:28

**-~** 

## 102,

**'~** 

## OOm'v' 

## Component (unknown)



## lunknol~n) ( unkr,own I

# Fl

# ClComponent


# FlC1-·

2 

# Number

1 2 

# Retention Area

1 ()":>0

"•,_, ..J,,) 

# 22 .27
:i_ 

## 650 c -, 

# _fJe

,j I



## 80.15 

# Area External 61.00 N/A 32.90 N/A



## 65.80 N/A 

## 22.27 M 0.27



# 57.88 M 0.94



# External Units

**!~i** 

## 0 "27 

# ug/m1

**~1** 

## 0 

# .94 

# ug/ml

1 .21



# 79

# I

I I I I I I I I I 

# I I I I I I I I I (i)f!ditions



# Compnnert.

(unknown) 

# Date T j 

# nvsComponent

0 

# H20 Blank 08/24/2005 10:53:20



# Numbe• Retention ATe a

0.00 1024. OOOm\/



# Exteonal Units

0.00 

# Area E!:ternal

3L60 

# N/A



# 80

# I

I I 

# I I I 

# I I I I I 

# I I I I 

# I I I I (unknown)

# FlClDa_te 

# Time

Component

2 08/24/2005 11:01:28



# Number Retention

1 2 

## 1.033 1 "666 

# Area

334"20 M 270

. 70 r1



## 604.90 

# External Units

4"11 

## ug/rnJ 

# 4.38 ug/ml

8.49 

# 105.85 

# 334.20 M

270.70 H



# 81 N/A 4 '11



# 4.38

# I

I I I I I I I I I I I I I I I I I I Cornpont:nt (unknown)

(unknown)

## FlCl· 

# Time



# I 0. 8331 1

. 

## 11"·""' I 

# I 1. 

## 633! ; 

# zl··

.. · ·

Component**Fl~** 

## Cl-·

2 ,; "96 

## ug/ml F l- :. 

## r· H2S04**4.~3** 

# ug/"1l Cl- in H2S04 08/24/2005 11:04:06



# Number Retention Area

1 

## 1 .016 

## 354.65 2 1 .633 

## 265.75



## 620.40 

# Area Ext.t>rnal 75.05 

# N/A

103.90 

# N/A 354.65 M 4.36

265.75 M 4.30



# External Units

r>,,', 

# 4.36 

# ug/ml 

# '' M 

## 4.30 

# ug/ml

8.66



# 82

# I

I I I I I I I I I I I I I I 

# I I I I Compon&nt

(unknown)

# FlCl

# Date Time

Component
Fl# Cl2 

# 9.92 ug/ml Fl-**~-r1 ~2S04**  

# 9.66 ug/ml 

# Cl- in H2S04 08.-'"24/2005 

## 11::14:25



# Number Retention Area

1 1 

## .033 839" 10 

## 1 .683**E.l~9** 

## _40



## 1388_50**~L** 

### 0/'/l

. 

### OOOrn\/



# External Units**~1** 

## 10**-~~2** 

# ug/ml**~1** 

## 8"66 

## ug/rnJ



## 19_09 

# Area

106.20 83UO M



# 549.40 M



# 83 N/A 10.42

8.66

# I

I I I I I I I I I I I I I I I I I I Component (

**unho~m)** 

## (unknown)

# FlClComponent
Fl

# c 1--

2 

# Date Time **9~£6** 

# ug/ml 08/24/2005 11:16:56



# Number Retention

1 1 

## .033 

## 2 1 .650 

# H2SC4



# Area External

8L!4 

## ,55

**r~1** 

## 10 /j 0 

## ",,,,_, 

## 54/) .10

**~1** 

## 8 

## .66



# 1393.65 19.15 

# Units u_g/rnl U9/m1 

# Area 57.60

106.95 844.55 H



## 549.10 M



# 84 Exler nai 

# N/A

N/A 10.48



## 8.66

# I

I I I I I 

# I I I 

# I I 

# I I I I I I I I Date 

# Time 19. 8tt- ug/ml 

## 1 S. 72 ug/inl 08/24/-2005 

## 11:26:52

-J 02 • .:::!O()rn\1 

## Component 

## ( unknowri)

(unknown)

## Fl

# c

1- 

# F;etention 0.166'



## 0.8501 1. H 

## l ' I 

## 1.716\ 

# i 2.



## i



# Component

,c- 

## 1 ,.

# Cl2 

# Number Retention

1 1 

## .050**~2** 

## J 

## .716 l_ i1 

## f-12504



# Area**~** 7 r:::, 1 _L ' ,_**.~** 

## .10 M 

## 1:218 

# "**-:~** 

# s 11



## 2969.45 J024.00Um\/



# External Units

20"77 

# ug/ml 17 .96 ug_,/m1



## 38.73



# -· ./ 

## Area 

## 31.10

106.90 1751.10M



# 1218.35 H



# 85 External N/A

N/A 

## 20 '77

17 '96

# I

I I I I I I I I I I I I I I I I I I Compont>nt (unknown)

(unknown)

## Fl

# ClDate Time

Component

Fl

# Cl2 19.84 LC;i/rnl Fl- lfi 

## H2SQ:.} 

# 19.72 ug/rnl Cl- 1r1 

# H2S04 08/24/2005 11:29:24

**1(!~? -~-OOmV** 



# Number Retention Area

1 1 

## 050

**176[~** 

## "05 

## 2 l 

## .683 1.J 

## 62 

# s:·,

2926.60 :1.024

**.OOO~n\i**



# External Units

i"1 

# 20

**Q~** ./L 

# ug/ml

**~-~** 

## 17 />0

- t:.. / 

# ug/rnl

38.21 

## Area 72 '35



# 107.50 1764.05 M

1162.55 M



# 86 External N/A

N/A 

# 20.92

17 '29

# I

I I 

# I I I 

# I I I I I I 

# I I I 

# I I I I Condi t.l.ons



# Date Time 39_68 ug/ml Fl- 1n 

# H2S04 39.44 ug/ml Sl- 1n 

# H2S04 08/24/2005 11:39:18

**-~·1()2** 

### .1.!-00rn\/ 

## Component (onknown)

(unknown)

# FlClComponent
Fl-- 

# C1-

2 

# Number

1



# ., ·' 

# Retention Area

1 "066 

## 3522

. 11-0 

## 1 "76(, 

## 2712 2''



# .

**~**



## 6234 .60 1024 "OOOm\!



# External Units

!'4 

## 38 "96 u.g/rn1 

## 1'1 

## 37 

# .79 U-J/m1



## 76.74 

# Area 18.40

112.60 3522.40 M

2712.20 M



# 87 Erternd 

# N/A

N/A 38.96

37.79

# I



# I I I I I 

# I I 

# I I I I I 

# I I 

# I I I I **Compone~t** 

## (unknown)



# I unknown)

# flClDate 

# Time 39.68 119/ml Fl- in H2S04 39.44 ug/ml 

# Cl- in H2S04 08;-"24/2005 

# 11:41:51

--102 _4C<Om') 

# Retentior1 0' 116[''

.

' ' 

## 0 

## .850•1' 1. 1 !



# Component Number Retention Area

FJ .• 1 

## 1 

## .066 3645 

# "'"

.. .._;,._,< 

# c 1·- 2 1 "766 

# 2731 .80



## 2 

# 6377.10 

# l024.000mV Area External 72 

## .J:, N/ A



## 116.45 N/A 3645.30 40.19

2731.80 M 38.01



# External Uni t.s

40 "29 

# ug/ml 1'1 

## 38 .02 

# u.g./ml

78.31



# -· 

# 88

# I

I I I I I I I I I I I I I I 

# I I 

# I I F 

# l·-

. col



## At'\OUNT INJECTED AREA ')'



## 3583.8



# slope of curve: 88 52

xis inte)·cept: 0.00 

# Coef·f of lin 

# rAgr: 0.88
!',10

**/'~I** 

## ea 

# r.:,m()U r1t



## 0 

## : 0 

## .000 0 000 1 

## : 

# ::;4li 

# 425 4 

## .960 2 : 

## 841 .8:c.::8 

## 9 

## .920 3 : 

## 1757 575 l 

## 9 

## .840 4 : 3583 

## 850 /?;9 

## 680 

# CF

0 000 69 

# .441 84 861 88 ,587 90 

# ::.:19 2

3



## 4

5



# 89

# I

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## INJECTED 

# AREA

2722, t)OU!

........................................................... .


# Avg slope of cur\Je: 63.53

**Y-a,~is intercept~**  

# 0.00 Coeff of lin regr: 0.82

**~lo** 

## Ar·en 

# Amount

0 

# ' 0 

## .000 0 

## .000 

# 1 : 

# 268 .225 

# 4 .930 

# 2'

**~'** 

## 549 _250 9 

## ,860
'>· 

## -'" 

# 1190 .450 19 J20 4 

## 2722 ,0()() 

## 39

**"~~** 

## 40 

## 39.440



# CF

0 "00() 

# 54

.. 4-07 ::,5 

## .705 

## 60 

# .368 69 .016 

## l


## 2

3



## 4

5



# 90

# I I I I I I I I I I I I I I I I I I I Conditions

Date Time Daltile Scrubbe1- Exhaust Run #1 Imps 2,3 

# & 4 Volume 300 

# Dilution 1/1 

# 08/24/2005 11:51=4-4



## --1.J2 "4 OOm\i 

# Component (unknown)


# (unknown)
F!- C]-



# Component


# FlCl--

2 

# Nurnbe)·

1

-, 

## "- 

# Retent.ion Area

1 

## .200 33_25 1 .700 18.90



## 52.15 

# 1024.000mV



# External Units

1'1 

## 0.48 

# ug/ml

**~·r** 

## 0"?-5 

## ug/m.l



## 0.83



# 91 Area 31.10

47.90
33.25 M



## 18.90 fl 

# External N/A

N/A


# 0.48
0.35

# I

I I I I I I I I I I I I I I I I I I Concii Lions



# Date Time Daltile Scrubber Ext1aust 

# Run #1 Imps 2,3 

# & 4 Volume 300 

# Dilution 1/1 

# 08/24/2005 12:03:48



# -102.400mV Component

(unknown)

# FlClComponent


# Fl# Cl2 

# Number

1

0 

# Retention Area

1"200 

# 32.40 1 

# .716 20.35

52.75**~1** 

# 1024 .OOOnW



# External

0.47 0.37

0.84 

# Units ug/rnl ug/rnl Area

53.80
32.40
20.35 M



# n 

# 9,., -' 

# -·

. 

# .. {_, 

# External



# N/A

0. 47

0.37

# I

I I I I I I I I I I I I I I I I I I Date Time Daltile Scrubber Exhaust Run #2 Imps 2,3 

# & 4 

# Volume 300 Dilution 1/1 

## 08/24/2005 

## 12:06:36

--1 ()2. 400m\' 

# Component (unknown)

(**unkrro~1n)** 

# Fl·

# ClComponent

Fl-· 

# Cl··

2 

# Number- Retention 

# Area

1 1 "183 

## 29.60 2 1.700 

## :30.:30

59.90**:L02~.000mV**



# Exter-nal Units

0.43 

# ug/ml**~1** 

## 0.56 

# ug/ml

0.98 

# Area 21

. 25

110.80
29.60
30.30 M



# 93 External NiA

N/A


## 0.43

0.56

# I

I I I I I I I I I I I I I I I I I I Component (unknown)


# (unknown)
Fl

# c

1- 

# Date Time 

# Daltils Scrubber Exhaust Run #2 Imps 2,3 

# & 4 

# Volume 300 Dilution 1/1 08/24/2005 

# 12=16=1.3

-102 .400m\i 

# Retention 0 '1 i 

## 6j

1 

## 0 ,850! 

# 1! 

# 1.200! !

716!

2i"''''

i 

## 3!·······

I ' ! 

# I 4("'



# Component Number Retention Area
Fl# Cl2 

## 1 

## 2 

# 1.200 1 "716 26

.. 65 M :24

.. l 0 1'·1



# 50.75 1024

. OOOm\i



# External Units

0.38 ug/ml 0.**il-L~** 

## ug/m.l



## 0.83 

# Area External 21,00 N/A

53.90 N/A



## 26.65 H 0.38

24.10 11 0.44



# 94

# I

I I I I I I I I I I I I I I I I I I Condi 

# t_i CHIS



# Date Time Oaltile 

# Sct·ubber Exhaust Run #2 Imps 2,3 

# & 4 Volume 300 

# Dilution 1/1 

## 08/24/2005 

# 12=18:47

-102 .400m\" 

# Component (unknown 

# I

(unknown)

# FlClRetention 0.0161

0. 8331 1 

# i

.. 1.083i

I 

## 1.700!



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F l

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# Cl2 

# Number Retention Area

1 

# 1.083 33.35 

## 2 1.700 28,35



## 61.70 

# Area External 53.60 ri!A



## 39.70 M N/ A


## 33.35 M 0.48

28.35 fl 0.52



# External Units

r1 0.48 ug/mJ 1•1 

## 0,52 u g,/rn 

## 1

1 .00



# 95

# I

I I I I I I I I I I I I I I I I I I Date Time Daltile Scrubber Exhaust Run fi2 Imps 2,3 

# & 4 Volume 300 Dilution 1/1 08/24/2005 12:28:10

-102 ,400rn\/ 

# Component (unknown)

(unknown)

# FlClComponent**~'** 

# 1-- 

# Cl

2 Number

1 

## 2 

# Retention Area
1,200 

# 21 AO 1.716 26"50



# 47.90 l 02Ll OOOm\/



# External Units

M 0.31 

# ug/ml**~-1** 

## 0.49 

# ug/rnl

0.80 

# Area 17.80

52.30
21.40 M

26.50 M



# 96 External N/A

N/A



## 0.31

# I

I I I I I I I I I I I I I I I I I I C.:)nditions



# Date 

# Time Daltile 

# Scrubber Exhaust Run #3 Imps 2}3 

# & 4 

# Volume 300 Dilution 1/1 08/24/2005 12:37:39

-102

. 400rn\i 

# Component

(unknown)


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# Component Number Retention Area


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# 1.200 311.90 

# Cl- 2 1 .716 

# 22.85



# 2 

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## 1024 "OOOm\J



# External



# o.so 0.42

0.92 

# Units ug/rnl 

# ug/ml 

# Area

47.90
34.90 II
22.85 M



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# External



# N/A
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0.42

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(unknown)

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Component
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# Deltile 

# Scr·lJbber Exhaust Run #3 Imps 

# 2,3 

# & 4 

# Volume 300 Dilution 1/1 08/24/2005 12=49:23

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1 

## 1

.. 200 

# 37.60 2 1.733 

# 22.80

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M 

# 0.54 ug/ml 11 0- (l2 

## ug/rn.l.



# 0_96



# 98 Area 33.45

51.55


## 37.60 M


# 22.80 M 

# External N/A



# N/A

0.54


## 0.42

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I 

# I I I I I I I I 

# I I I 

# I I 

# I I I 

# I C<>nditions



# Date 

# Time Daltlls Scrubber Inlet Run #1 Imps 1 

# & 2 Volume 500 Dilution 1.110 08/24/2005 12:59:04**-~** 

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(unknown)


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2**!~umber** 

## 1 2 

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1 .083 1278.70 

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. ()8



# 3015.68 1024.000mV 

# Area External 21 .00 

# N/A

27.65 

# N/A
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# 1736.98 M 2& .76



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1•1 

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## 26,76 

# uq/ml

41.41



# 99

# I

I 

# I I 

# I I I I 

# I I 

# I I I 

# I I I 

# I I I Condi t.ion2:;



# Da.te Time Daltile Scrubber Inlet Run #1 Imps 1 

# & 2 Volume 500 

# Dilution 1/10 08/24/2005 13=01=35

-102"400m\J 

# Component

(unknown)Fl

# ClComponent
Fl

# c 1--

2 

# Number

1 2 

# Retention Area

1 

# ,066 1328.05 1.750 1754"61



# 3082.66 M ;j 

## 1024,000m\/



# External

15 "19 26"98



# 42.17 

# Units
ug/ml ug/mJ 

# Area

41.20 1328,05 H

1754.61 M



# 100 External

N/A 

## 15 ,)9

26_98

# I

I I I I I I I I I I I I I I I I I I Date 

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# & 2 Volume 500 Dilution 1/10 08/24/2005 13=10:52

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(unknown)


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# Number Retention Area


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# 1531 .30 

# Cl- 2 

## 1.766 1875,94



# 2 3407.24 M M 

# 1024.000m'J

External Units

17.39 ug/rnl ::::8 "55 

## ug./m1



# 45.94 Area

69.60

1531.30 M

1875.94 M



# 101 External

N/A

17 '39

28 '55

# I

I I 

# I I I 

# I I 

# I I 

# I I 

# I I I I I I I Date Time Run #2 Imps 1 

# & 2 Volume 500 Dilution 1/10 08/24/2005 13:16:03

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## (unknown)

# FlClComponent


# FlC.l

## 2 

# Numbeo Retention Aoea

1 

## 1.066 

# 1530.00 2 1 ""766 

# 1941.76



# 3471.76 J 024, OOOm\/



# Exteonal Units**~1** 

## 17.37 

# ug/rnl t1 

# 29.39 ug/mJ



# 46.77 Area

75 '80 1530.00 M

1941.76 H



# 102 External



# N/A 17.37



## 29.39---------



# I I ConcH tio ns

Date Time Run #3 Imps 1 

# & 2 Volume 500 Dilution 1/10 08/24/2005 13:25=21 

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# I I I I I I I I I I I I I I I I Component

( llnknown)

# FlClCompon,2nt

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2 

# Number Retention Area

1 1 "06() 

# 1154 .60 2 1.750 1513.29



# 2667.89 'l 024.

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## 13.31 

# ug/ml 11 

## ;?3.88 

# ug/rnl

37.19 Area



## 62.80 115UO M

1513.29 M



# 103 External

N/A 

## 13. 31



## 23.88

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I I I I I I I I I 

# I I I I I I I I I Date Time 

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# Run #3 Imps 1 

# & 2 Volume 500 Dilution 1/10 08/24/2005 13:27=45

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1 2 

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1 066 1120.40 1.750 

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# 36.58 

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82.05 1120,40 M

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N/A 12,94

23,64

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I I I I I I I I I I I I I I 

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# InlBtH2S04 alank 08/24/2005 13:39:32



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## 2.



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# External Units

0 

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119.00



# 93.25



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# Date 

# Time Daltile Scrubber Inlet 19.84 ug/ml Fl- in H2S04 

# 19.72 ug/ml Cl- in H2S04 08/24/2005 13:49:22

"¥ 

## :1 C2, 400m') 

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f' 

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1**~.** < 

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1 

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116.30 fl N/A 1763.25 M 19.90

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Certificate of Analysis

Lot Number 050607
Expiration of Certification December 2006

The Fluoride Standard was developed to aid the analysis of anions by Ion Chromatography (IC). The single-ion standard was prepared by the dissolution of high-purity salt in 

# 2:18.2 megohm· deionized water, which was tested by IC for ionic contaminants. The bottle label states the nominal concentration value of the ionic component for informational purposes only. The ion concentration value was detcnnined by Ion Chromatography. Tbe system was standardized using the National Institute of Standards & 

# Teclmology (NIST), Standard Reference .Material, SRM 3183 (Fluoride Standard Solution). T11e actual concentration value determined for the component ion is listed below.

Fluoride Standard
Component

Fluoride Concrntration (mg/L) 992 ± 

# 4

The concentration -value is based on proven reliable metl1ods of analysis. The estimated uncertainties are two standard de,·iations of the concentration ,·alues. The concentration value is ''-'ananted to be stable for three montbs from the date of shipment

Tbe preparation and analyses of tbe Fluoride Standard was perfom1ed with extreme care by DlONEX Corporation Consumablcs l\1anufacturing Department.

**Dione~** U.S. Regional ou;ces

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Certificate of Analysis

Lot Number 041210
Expiration of Certification June 2006

The Chloride Standard was developed to aid the analysis of anions by Ion Chromatography (I C). 

# The single-ion standard was prepared by the dissolution of high-purity salt in :::18.2 

# megohm deionized water, which was tested by IC for ionic contaminants. The bottle label states the nominal concentration value of the ionic component for informational purposes only. The ion concentration value was determined by Ion Chromatography. The system was standardized using the National Institute of Standards & 

# Technology (NIST), Standard Reference Material, SRM 3182 

# (Chloride Standard Solution). The actual concentration value determined for the single-ion is listed below.

Chloride Standard Component

Chloride Concentration (mg/L) 986± 4

The concentration value is based on proven reliable methods of analysis. The estimated uncertainties are two standard deviations of the concentration values. The concentration value is warranted to be stable for three months from the date of shipment.

The preparation and analyses of the Chloride Standard was performed with extreme care by the DIONEX Corporation Consumables Manufactunng Department.

Document No.

**03~** 

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I I I I I I I I I Appendix E 

# I I I I I I I I I- -- -- - - - - - - - -MeterSeri<JI/1-jlllljljl11/3ArmstrongEnvnonmenlnllncEPAMelhod5522SeriesMeterBoxCalibrationPre-TestOrificeMethodEnglishMeterBoxUnits,EnglishK'FactorDale-------------B<lrornelricPressure·--------->TheoreticalCriticalVacuum--->08/04/0529.75(in.H!J)14.03(inHg)IMPORTAI\I'orVdlidlestrt:sulls,theVcu:uumshouldbe1lo2in.Hugreater!hantheTheorelicalCriticalVacuumshownabove.IMPORTAI\TheCriticalOrificeCoelficiont,!<',rnu::;lUec·1leredinEnglishunits,(ft)"3.(deoR)hQ5/((inHg)'(rnin))!!11!!11'DIWGASMETERREADINGS-CHITICALORIFICEREADINGSV"lorrwVolunwVolumelniha/Temps.FinalTernpsOrificeI<'OrificeActualdlITimelnilicilfinalTotalInletOullelInletOullelSerial#CoefficientVacuum(111H20)(l!llfl)(Cllft)(cufl)(Ciifl)(degF)(degF)(degF)(degF)(number)(seeabove)(inHg)0.256.00661.1300063.1321.93289.089_089_089_0400.24223.00517.(10564.0fJ06672303.23089.089.090_090.0480_34421.00_946_00667.100670.13193.71990.090.091.090.0550.46419.01.5510no671_300619.2747.97491_090.093_091_063059317.0::1.006.006H0.200686.8096_60993.091.095,09'10730.82414.5...................................................RESULTS...................................................--·DRYGASMETER·--·-.,·--ORIFICE-----------DRYGASMElER---ORIFICE---------VOI.UMEVOLUMEVOLUMEVOLUMEVOLUME-AmbientTempera!taelnilin)FinalAveraoe(degf)(de9f)(dogf)90090.090_090.090090.091_092.092.092.092.093091.592.0925CORRECTCORRECTEDCORRECTCORRECTNOMINALVm(sld)Vrn(sld)VL:r(sld)Vcr(si(J)VeeCALIBRATIONFACTORyValiu!ionCALIBRATIONFACTORdH@(i)IJfl)(tilers)(cufl)(liters)(cuIt)1.8480.-11.84·10.11.9333.0890.13_0570.13,20435550.13.526013.7057.6200.3/.5140.37.9036.32-'10.26.2560.26.586(nurnber)(n11mber)0.9980.0070.990-0.0010_9920.0010.986-0.0050.989-0.002Value(inH20)1.4231.437146114731.479V<Hiation(inH20)-0.0313-0.0180.0070.0180.024-AverageY------->0.9911.455<-------AveragedH@NoJe:F()!C<Jiibralionf0at:lorY,Ilier<llioofthe10<-1dingoftl1ecalibrationJlletertolhedrygasmeier,<ICCeptabletoleranceofIndividualv<Jiiwsfromtheaveraoeis·+-002.forOrificeCaiJbialiOIIFddOtdl-l@,llworificedirferentiulpressureininchesorH20Ihalequaleslo0.75cfrnofair"'68F"'"'2992"oepl,<b•ofiodi'ji'J"l'aloe'rwmIhe"e"ge"'02/.,/'-·1-"t\')(j)SIGNCO___D'le,___'ifi_'/./_!_0s:=_-- -- -CONVERSIONf-'ACf'OHS1n1rnHo'0.13330kPd1em"'0.39370inch1ITIITJ00393/ittchiCUIt"'2832III<JIS-AverageDGMDGMArnbienlOutletOveJallTomp(degH)(deo(degR)549.0549.0550.0549_5549_5550_0550.0550.3551.S550.5551.3552,0551.0552.55525

# I

I Tempe1ature l\f;eter Calibrations 

# I

Meter Box#: 

# 11 

# I Date: 08/04/05 Calibrated By: RT

Emtech Thenno Degrees 

# F Checker Probe Stack 

## Oven Exit Auxiliary 

# I

Point 1 32 30 30 30 31 31
Point 2 212 211 211 211 211 212 

# I I Point 3 752 751 751 751 751 752 

# I Emtech Thermo Degrees R Checker Probe Stack Oven Exit Auxiliary 

# I Point 1 492 490 490 490 491 491
Point 2 672 671 671 671 671 672
Point 3 1212 1211 1211 1211 1211 1212 

# I

Percent Difference
Probe 

## Stack 

## Oven Exit Auxiliary 

# I I Point 1 0.406504 0406504 0406504 0.203252 0.203252
Point 2 0 14881 0.14881 0.14881 0.14881 0
Point 3 0.082508 0.082508 0.082508 0 082508 0 

# I I I I I I I 1 ')
,..,**~** 

## IMeterBox1Serial#!!11!1!111173ArmstrongEnvironmentalInc.EPAMethod5APEXINSTRUMENTS511SeriesMeterBoxCalibrationPost-TestOrificeMethodEnglishMeterBoxUnits,EnglishK'FactorDate:---·--------------------->BarometricPressure:---------->TheoreticalCriticalVacuum:--->08/24/0529.65(inHg)1399(in.Hg)IMPORTForvalidtestresults,theActualVacuumshouldbe1to2in.HggreaterthantheTheoreticalCriticalVacuumshownabove.IMPORTMTileCriticalOrif1ceCoefficient,K',mustbeenteredinEnglishunits,(ft)"3.(degR)"O.S/((in.Hg)•(min)).IIJ11JijlDRYGASMETERREADINGS-CRITICALORIFICEREADINGSTheoreticalCriticalVacuum:--->13.99(inHg)VolumeVolumeVolumeInitialTemps.dHTimeInitialFinalTotalInletOutletFinalTemps.OrificeK'OrificeActual--AmbientTemperature--InletOutletSerial#CoefficientVacuumInitial(inH20)(min)(cuft)(cufl)(cufl)(degF)(degF)0.948.00815.800820.803500390089.0(degF)(degF)(number)(seeabove)(inHg)(degF)91.0900550.46419.590.00.945.00821.100824.2273.12790.090.091.0910550.46419.591.00.94600824.600828.347374791.091092091.0550.46419.591.0...........Hd•*''*'Hh••·--·······..............RESULTS.....H...................................*'**•····---DRYGAS---VOLUMEVOLUMECORRECTCORRECTEDVm(std) Vm(std)(cuft)(liters)4.7690.229780.13.5630.1---------ORIFICE--------VOLUMEVOLUMEVOLUMECORRECTCORRECTNOMINALVcr(std)Vcr(std)Vcr(cuft)(liters)(cufl)4.6920.24.9342.9303.5140.10.13.0873.706--DRYGASMETERCALIBRATIONFACTORyValueVariation(number)(number)0.984-0.0010.984-0.0010.9860.002---------ORIFICE---CALIBRATIONFACTORdH@ValueVariation(inH20)(inH20)14640.00001.464-0.0001.464-0000FinalAverage(degF)(degF)90090.091.091092.091.5AverageY------->0.9851.464<-------AveragedH@NoteForCalibrationF<:lctorY,theratioofthereadingofthecalibrationmetertothedrygasmeter,acceptabletoleranceofindividualvaluesfromtheaverageis+-0.02ForOrificeCalibrationFactordH@,theorificedifferentialpressureininchesofH20thatequatesto0.75cfmofairat68Fand29.92InchesofHg,acceptabl;rtolerancevaluesfromtheaverageis+-0.2.-....__t,'J"{VIIDale6/z.I/os--- - - --- - - ----- -DGMOutlet(degR)5495550.5551.0-CONVERSIOI\1FACTORS1mmHg=0.13330kPa1em""0.39370inch1rnm::o0.03937inch1cuft=28.32litersDGMAmbientOverallTemp(degR)(degR)550.0550.0550.5551.0551,3551.5coC'-l,...;-- -

# I

I Temperature Meter Calibrations 

# I Meter Box#: 

# 11 Date: 08/24/05 

# I Calibrated By: RT

Emtech Thermo 

# I Degrees F Checker Probe Stack Oven Exit Auxiliary
Point 1 32 30 30 30 30 30 

# I Point 2 212 211 212 211 212 211
Point 3 752 751 751 751 751 751 

# I I Emtech Thermo 

## Degrees R Checker Probe Stack Oven Exit Auxiliary 

# I Point 1 492 490 490 490 490 490

Point 2 672 671 672 671 672 671 

# I Point 3 1212 1211 1211 1211 1211 1211 

# I Percent Difference Probe Stack Oven Exit Auxiliary 

# I Poini 1 0.406504 0.406504 0.406504 0.406504 0.406504
Point 2 0.14881 0 0.14881 

## 0 0.14881 

# I Point 3 0 082508 0 082508 0.082508 0.082508 0.082508 

# I I I I I I 129- - - - - ---- - - - -Mete(Box1.Scncrl#!!1!!11]11030272APEAnns110il\JEnvironrnenlallncEPAMelhod5522SeriesMeierBoxCalibralionPre-TestOrificeMelhodEnglishMeierBoxUnils,EnglishK'FaclorDale:-----,.·---------BcHornetricPressure:--···----"'TheoreticalCriticalVa()lllHn--->08/04/0529.75(in.Hg)14.03(inHg)IMPORlAhF-orvalidlr.J::>lrc-Jsulb,theAclu<JIVncuumshouldbe1to2in.HggreaterIhantJwTheoreticalCriticalVacuumshownaboveIMPORTA/\CliihllCodfidenl,K',mustbeenteredinEnglishunits,5/((in.Hg)'(min))11!!11!11DRYGASMETERREADINGS---------------CRITICAlORIFICEREADINGSVolurrreVotun1eVoliunelnihalTemps.FinalTemps.dHTimelllili;ilFin<ilTotalInletOutletInletOutlet(in1120)(111in)(ellII)(cult)(cuII)(deuF)(degF)(degF)(degF)0.247.0022,1900227.1622.26290090.091091_0U.498.00227.'100231.0953_69591.091.093.092.00.9"11000231,SOO237_7126.21293.092.094.093.0·1.505.no252_1()02560853.98594.094_095_094.02_90fi002<1,1.60025"1.1626_56295.094_098.094_0...................................................RESULTS...................................................-ORYGASMETER---------ORIFICE·--DRYGASMETER-VOLUMEVOLUMEVOI.UMEVOLUMEVOLUMEOrificeK'OrificeAclualSerial#CoeffrcientVa(:UUm(number)(seeabove)(inHg)400.24222.0480.34420.5550.464190630.59318.073082416.0....__ORIFICE---·AlllbienlTernperalwe-·InitialfinalAverage(degF)(deof)(deoF)90.091.090.591.092.091.592.09•1.094.093_094.094.092.594.094.0CALIBRATIONFACTORCALIBRATIONFACTORCORRECTCORRECTEDCOJ<RECTCORRECTNOMINAlyVm(sld)Vm(sltl)Ver(shl)Vcr(sld)Ve<ValueVarialion(cuII)(liters)((:llfl)(lilers)((:ufj)(nwnber)(number)2.153012.15"10.12.2560.9970.0023.5190.13.4890136670.992·0.0035.9080.25.8710.26.1810994·000'11-"3.7870.13.7500.13.9590990-0.0046.2•16026.247026.5951.0000006(.;.)0AverageY------->0.995Nule:forCalibmlionFaclorY,!lwr<llioofthereadingoftile(:alibiulionmeterlo!hedrygasmeter,<l(:Gept8bletoi&IaJl(:e!!Iilldividualvaluesfromtheaverageis1·-0.02.dH@ValueVariation(it1H20)(inH20)1.364-003631.379-0.0211.4110.01114210.02'11.4260.0261.400<-------AveragedH@FmOrificeCalibrationFi!dordH@,tileorifice(flfferentiaJpressureini::;ofH20thaiequatesto0."/5dmofair"'68F'"'lmmIhea""9";,+02.Dale.____(?J__._-- - -CONVERSION1rnmHu,1em1mm1Clifl=0.'13330kfJ<J.0.39370inr:h0.03937inch28.32lllors·AverageTampe1aturesDGMDGMArnbie11!OutletOverallTelllp(degR)(deuR)(degR)55055505550.555'1.555'1.8551_55525553.0552_5554.0554.3S540554055535540- -

# I

I**leG~** 

## Perature Meter Calibrations 

# I

lv1eter Box#: 10 

# I Date: 08/04/05 Calibrated 

# By: .RT 

# I Emtech Thermo Degrees 

## F Checker Probe Stack Oven Exit Auxiliary

Point 1 32 31 31 31 31 31 

# I Point 2 212 211 211 211 211 211 

# I Point 3 752 751 751 751 751 751 

# I Emtech Thermo Degrees R Checker Probe Stack Oven Exit 

## Auxiliary 

# I ?oint 1 492 491 491 491 491 491
Point 2 672 671 671 671 671 671 

# I Point 3 1212 1211 1 211 1211 1211 1211 

# I Percent Difference Probe Stack Oven Exit Auxiliary 

# I Point 1 0.203252 0.203252 0.203252 0.203252 0.203252
Point 2 0 14881 0.14881 0 14881 0.14881 0 14881 

# I Point 3 0.082508 0 082508 0.082508 0 082508 0.082508 

# I I I I I I 131- Meter Box II

Serial#. 1!!!!1!11 - 10

30272 - - - - -
Armstrong Environmental Inc.

EPA Method 5

511 Series Meter Box Calibration

Post- Test Orifice Method

English Meter Box Units, English K' Factor Date:------------------------> Barometric Pressure: ---------->

Theoretical Critical Vacuum:---> - - 08/24/05

29.65 (in. Hg)

13.99 (in. Hg) - -

IMPORT Ar-. For valid test results, the Actual Vacuum should be 1 to 2 in. Hg greater than the Theoretical Critical Vacuum shown abovo

IMPORT AI\ The Critical Orifice Coefficient. K', must be entered in English units, (ft)"3'(deg R)h0.5/((in.Hg)"(min)).

!!!!!!I!! --------------DRY GAS METER READINGS--------------- -CRITICAL ORIFICE READINGS- - - - -

Volume Volume Volume Initial Temps. Final Temps. Theoretical Critical Vacuum:---> 13_gg (in. Hg)

Orifice K' Orifice

dfl Time Initial Final Total Inlet Outlet Inlet Actual --Ambient Temperature-

Oul!et

(in H20) (min) (cu ft) (cu ft) (cu ft) (deg F) (deg F) (deg F) (deg F)

0.90 6.50 <100.600 404.619 4.019 88.0 87.0 90.0 89.0

0.90 7.00 <105.100 409.435 4.335 90.0 89.0 92.0 91.0

0.90 g_oo •109,800 415.354 5.554 g2,0 g1_0 93.0 92.0
'''"'''"'''''•••••••·•••••••••• .. ••• .............. RESULTS ................................................. ..

---DRY GAS METER--· VOLUME VOLUME

COR RECTI CORRECTED

Vm(std) Vm(sld)

(cu ft) (liters)

3.841 0.2

4.128 f-"5274 w 0.2 0.2 --- ORIFICE ------ VOLUME VOLUME VOLUME

COR RECTI COR RECTI NOMINAL

Vcr(std) Vcr(std) Ve<

(cu ft) (liters) (cu ft)

3.8og 01 4.012

4.100 0.2 4.323

5.267 0.2 5.563 --DRY GAS METER·- CALIBRATION FACTOR

y

Value

(number)

0.992

0.9g3

0.9gg Variation (number)

-0.003

-0.001

0.004 Serial# Coefficient Vacuum Initial

(number) (see above) (in Hg) (deg F)

55

55

55 0.464 19.5
0.464 19.5

0.464 19.5 ---------ORIFICE--------- CALIBRATION FACTOR

dH@

Value

(in H20)

1.408

1.404

1.403 Variation

(in H20)

0.0030

-0.001

-0.002 g1_0 91.0

92.0 Final Average

(deg F) (deg F)

91.0 91.0

92.0 91.5

g3_0 92.5

**{'~** Average Y -------> 0.994 1.405 <-------Average dH@

Note: For Calibration FactorY, the ratio of the reading of the calibration meter to the dry gas meter,

acceptable tolerance of individual values from the average is +-0.02.

For Orifice Calibration Factor dH@, the orifice differential pressure in inches of H20 that equates to 0.75 cfm of air

at 68 F and **29.g2_jn!.<b.~~g,** accepta tolezance t individual values from the average is +-0.2. /

**~-** 7 '>/f"r/-

SIGNED: 5\ a _.,_...... Date cJ **~LdS** - - -

DGM

Outlet

(deg R)

548.0

550.0

551.5 CONVERSION FACTORS

1 mm Hg , 0. "13330 kPa

1 em

1 rnm

1 cu ft"' DGM

Overall

(deg R)

548.5

550.5

552.0 0.:19370 inch 0.03937 inch

28.32 liters Ambient

Temp

(deg R)

551.0

551.5

552.5 -

# I

I Temperature Meter Calibrations 

# I Meter Box#: 10 Date: 08/24/05 

# I Calibrated By: RT

Emtech Thermo 

# I Degrees 

## F Checker Probe Stack Oven Exit Auxiliary

Point 1 32 31 31 31 31 31 

# I Point 2 212 210 211 210 210 211

Point 3 752 750 750 750 750 751 

# I I Emtech Thermo Degrees R Checker Probe Stack Oven Exit Auxiliary

Point 1 492 491 491 491 491 491 

# I Point 2 672 670 671 670 670 671 

# I Point 3 1212 1210 1210 1210 1210 1211 

# I Percent Difference Probe Stack Oven Exit Auxiliary

Point 1 0.203252 0.203252 0.203252 0.203252 0.203252 

# I
Point 2 0.297619 0.14881 0.297619 0.297619 0.14881 

# I Point 3 0.165017 0.165017 0.165017 0.165017 0.082508 

# I I I I I I 133

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# 138

# I

I I I I I I I I I I I I I I I I I I Appendix F

# I

I I I I I I Specialty Gas Products

Date: 6/27/2005
Customer: Matheson- Trigas Description: NO 1n N2- EPA Protocol Cylinder No. EB0001164

Component 

## N1tnc Oxide Nitrogen, Balance

Reference Standard Description 

## GMIS Instrumentation Description 

## Honba Process Analyzer Requested Concentration 

## 50 ppm

Expiration date 

## 11/22/2006

Model# 

## CLA-51 0-NO 3106 Pasadena Freeway Pasadena, Texas 77503 !713) 534-8217 "ax!713) 5348133

Project: 16015 Exp. Date: 6/27/2007 Cyl'1nder Pressure: 1900psig
Certified Concentration 

## 50.4 ppm

NOx: 51 ppm

Cylinder Number 

## ND22557

Date Last Clibrated 

## 6/16/2005 Accuracy 

## 1%

Concentration 

## 99 8 PPM no

Principle 

## CHEMI 

# I I 

# I Anaylsis Results: Z =zero gas, S =standard gas, X= sample gas 

# I I I First Triad- NO 

## Z1- -1.20 S2= 994.10 Z3= -1 10 S1= 994.80 Z2= -1.30 X3= 499.80 Average= 50.3ppm Curve: Y = 0. 33645 + 

## 0. 099857'X X1= 498.30 X2= 498.40 S3= 997.40



# I ?-

.. =



# Analyst~~~ Second Triad

- NO 

## Z1 -1.10 S2= 998.20 Z3= -0.80 S1= 998.50 Z2= -0.70 X3= 500.80 Average = 50.53ppm X1= X2= S3= 502.80 502.40 994.20



# .

**~**

**~HIS** STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

# I I I I 139

# I

I I I I I I I I 

# I I I I 

# I Specialty Gas Products

Date: 6/27/2005

Customer Matheson

- Trig as Description NO in N2

- EPA Protocol Cylinder No EB0001156

Component N1tnc Ox1de Nitrogen, Balance

Reference Standard Description GMIS Instrumentation Description Honba Process Analyzer Requested Concentration 25 ppm

Expiration date 11/22/2006

Model# CLA-510-NO 3106 Pasadena Freeway Pasadena, Texas 77503 1713) 534-82'7 Faxl713) 534-3133

Project: 16014 Exp. Date 6/27/2007 Cylinder Pressure: 1900psig
Certified Concentration 25.0 ppm

NOx 25.5 ppm

Cylinder Number ND22557

Date Last Clibrated 6/16/2005 Accuracy 1%



## Concentration 99.8 PPM no

Principle CHEMI Anaylsis Results: Z =zero gas, S =standard gas, X= sample gas

First Triad- NO Z1- -1.20 S2= 994.10 Z3= -1.10 S1= 994.80 Z2= 

## -1 30 X3= 246.10 Average= 24.90ppm Curve Y = 0.33645 + 

## 0.099857·x X1= 244.50 X2= 244.80 53= 997.40 Second Triad- NO Z1- -1.10 S1= S2= 998.20 Z2= Z3= -0.80 X3= Average= 25.00ppm 998.50 -0.70 246.40 X1= 247.10 X2= 247.00 53= 994.20



# Analys~~

**--,~** 

# I THIS STAN



# ~RD IS NIST TRACEABLE. IT WAS CERTiFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

# I I 

# I I DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG



# 140

# I

I I 

# I I I I I I I I 

# I I I I I Specialty Gas Products

Date: 6/27/2005
Customer: Trigas Description: COm N2- EPA Protocol Cylinder No: EB0000761

Component 

## Carbon Monoxide Nitrogen, Balance

Reference Standard Description 

## NTRM Instrumentation
Description 

## Horiba Process Analyzer 3106 Pasadena Freeway Pasadena, Texas 77503 (713) 534-8217 Fax(713) 534-8133

Requested Concentration 

## 100 ppm

Expiration date 

## 5/29/2006

Model# VIA-510-CO Project: 16018 Exp. Date: 6/27/2008 Cylinder Pressure: 1 900psig
Certified Concentration 

## 99.1 ppm

Cylinder Number SX1 9190

Date Last Clibrated 6/10/2005 Anaylsis Results: Z =zero gas, S =standard gas, X= sample gas
First Triad- CO Z1= -0.90 S1= S2= 204.80 Z2= Z3= -0.80 X3=
Y=028607+0250309'X Average= 9945ppm 204.90 -0.80 396 50 X1= X2= S3= 396.60 396.60 204.90 Second Triad -CO Z1- -040 S1= 513.30 S2= 513.20 Z2= -040 Z3= -040 X3= 98520
Y=O 031031+0.100163'X Average= 98.74ppm

**~·** 

## --

**--~** 

# I /

.

**~-** 

# :.:,"

__ **~**

**~~** .. -···

**~-:;** 

## Analysf·



# --~-



# ~ Accuracy 

## 1%

Concentration 

## 994.2 ppm CO

Principle 

## NDIR

X1= X2= S3= 985.70 98540 513.20



# I TH!S

**STA~4DARD** 

## IS NIST TRACEABLE. iT 'vVAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

# I 141

# I

I I 

# I I I I I I I I I I I 

# I I Specialty Gas Products

Date: 8/16/2004

Customer: Matheson- Trigas 3106 Pasadena Freeway Pasadena, Texas 77503 

### (713)

**534~8217** 

### Fax(713) 534-8133

ProJect: 10548
Description: CO, 02 in N2- EPA Protocol Exp. Date: 8/162007
Cylinder No: CC187154

Component

Carbon Monoxide Nitrogen, Balance

Reference Standard 

### Description

GMIS

Instrumentation 

### Description

Horiba Process Analyzer 

### Requested Concentration
200ppm

Expiration date
4/6/2006

Model#
VIA-510-CO
Anaylsis Results· Z"" zero gas, S :: standard gas, X:: sample gas


### First Triad -CO Z1- -0.3 S2=

**993~20** 

### Z3= -0.30 S1 = 993.5 Z2= -0.30 X3= 199.90

Curve: Y=-0.6893+1 001139X Average =199.6ppm X1= 199.9 X2= 200.00 S3= 993.00 Cylinder Pressure: 1900psig

Certified 

### Concentration
200ppm

Cylinder Number


### CC177636

Date Last Clibrated

8/6/2004

Second Triad

. CO Z1 -0.4 S1 = 995.5 S2=

**995~80** 

### Z2= -0.30 Z3= -0.30 X3= 200 60

Average= 199 Bppm



# I

Anaiyst: 

# L-

**--~~-~:____** 

# __ {___ 

# I Ling Wen



## ...----~ Accuracy

1%

Concentration



### 994.2 ppm CO

Principle

NDIR

X1= 200.6 X2= 200.60 S3= 995.60

THIS STANDARD IS NIST TRACEABLE IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES 

# I DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

# 142

# MATHESON CERTIFICATE OF Ai'IALYSIS- EPA PROTOCOL MIXTURE 

# TRI·GAS 

# I

Customer: MATHESON TRI-GAS

- OALLAS

• Cylinder Number: Cylinder pressure: SX-36727 2000 8/7/2003 8/7/06 Last Analysis date:



# IExp·~ration Date· 

# I Component: Propane Protocol· G1 Reference# 262579 Lot#


## 1 09-36-31 020



## DO NOT USE THIS CYLINDER WHEN THE PRESSURE FALLS BELOW 150 PSIG

REPLICATE RESPONSES

Date: 8/7/2003 Date: 15.2 PPM 15.2 PPM Certified Cone: 15.2 

## ± 0.15 PPM • 15.1 PPM 

# .._____,=-. --------------------

rALANCE GAS: Air

• REFERENCE STANDARDS Component: Propane SRM #: SRM-1666b 

# I Cylinder# Cal-0 11826 Concentration: 9.73 ppm



# ~ERTIFICATION INSTRUMENTS Component: Propane Make/Model: Varian 3800 GC 

# I Seri2! Number: LR-92489 Measurement Principle: TC, FlO Last Calibration: 8/7/2003 

# (_


# __________________________________ _ 

# I i-.Joles:



## I This certification was performed according to EPA Traceability Protocol for Assay 

## & Certification of Gaseous Calibration Standards September 1997, using procedure G1 and/or G2. 

# I

I I .'"1 I f /'

**~** 

# fi--L 

# J · i/>



# \,._.::[~' **~~-~~~-----** Date

___ 

# _,8"'-/"'8/'-"2""0.,0,.,_3



# 143

# I

I I I I Specialty Gas Products


# I
Date: 6rrl2004

Customer: Trigas 3106 Pasadena Freeway Pasadena, Texas 77503 (713) 534-8217 Fax(713) 534-8133 

# I Description: Propane in Air- EPA Protocol Project: 9210-01
Exp. Date: 61712007 

# I I Cylinder No: SX41680

Component 

## Propane Air, Balance 

# I Reference Standard Description 

## NTRM 

# I Instrumentation
Description 

## Horiba Process Analyzer Requested Concentration 

## 30 ppm

Expiration date 71212004

Model# 

## FIA-51 0 Cylinder Pressure: 1 900psig

Certified Concentration 

## 28.8 ppm

Cylinder Number SG9183302

Date Last Glib rated 512412004 

# I Anaylsis Results: Z =zero gas, S =standard gas, X= sample gas 

# I First Triad

- Propane Z1 = 0.60 S1 = 207.90 S2= 207.70 Z2= 0.60 

# I Z3= 0.60 X3= 57.40 Curve: Y=-0.05085+0.501149·x Average= 28.77pm 

# I I . /-

**Analys~** 

## X1= 57.60 X2= 57.50 S3= 208 00 Accuracy 

## 1%

Concentration 

## 103.6 ppm Propane

Principle 

## FIA



# // <HIS STANDARD IS NiST TRACEABLE. iT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

# I DO NOT USE THIS STANDARD IF THE CYLINDER P?ESSURE IS LESS THAN 150 PSIG 

# I I 144

# I

I I I I I 

# I I I Specialty Gas Products

Date: 6{//2004

Customer: Trigas 3106 Pasadena Freeway Pasadena, Texas 77503 

## (713) 534-8217 Fax(713) 534-8133

Description· Propane in Air- EPA Protocol ProJect: 9211-01
Exp. Date 6/7/2007 Cylinder No: CC177391

Component 

## Propane Air, Balance Requested Concentration 

## 50 ppm Cylinder Pressure: 1 900psig
Certified Concentration 

## 48.8 ppm 

# I Reference Standard
Description Expiration date 

## 7/2/2004 Cylinder Number SG9183302 

# I I I I I NTRM Instrumentation
Description 

## Horiba Process Analyzer Model# FIA-51 0 Anaylsis Results: Z =zero gas, S =standard gas, X= sample gas

First Triad

- Propane Z1- 0.60 S1

**~** 

## 207.90

**S2~** 

## 207.70

**Z2~** 

## 0.60

**Z3~** 

## 0.60

**X3~** 

## 97.50 Curve:

**Y~-0.05085+0.501149'X**

**Average~** 

## 48.78pm X1

**~** 

## 97.60

**X2~** 

## 97.20

**S3~** 

## 208.00

./



## ---~------ 

# 1 //

**~--z..- -~**  

# '--------= Analyst: 

## L------·-

____ - (

**----~**

**~--** . 

## Date Last Clibrated 5/24/2004 Accuracy 

## 1%

Concentration 

## 103.6 ppm Propane



## Principle FIA

THIS STANDARD IS NISI TRACEABLE. IT VvAS CE'RTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES 

# I DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE iS LESS THAN 150 PSIG 

# I I 145

# I

I 

# I I 

# I I I 

# I I I I I 

# I Specialty Gas Products

Date 7/13/2004
Customer: Matheson-Trigas 3106 Pasadena Freeway Pasadena, Texas 77503 (713) 534-8217 Fax(713) 534-8133

Description: S02 in N2

- EPA Protocol Project No· 9970
Exp. Date: 7/13/2006
Cylinder No CC88735

Component Sulfur Dioxide Nitrogen, Balance

Reference Standard Description GMIS

• GMIS CC177157 Tracebility Description NTRM Instrumentation Description Horiba Process Analyzer Requested Concentration 100ppm

Expiration date 1/19/2006

Expiration date 6/1/2006

Model# VIA-51 O-S02 Cylinder Pressure: 1900psig
Certified Concentration 101 ppm

C)llinder Number CC177157

C)llinder Number SG9199568

Date Last Clibrated 6/15/2004 Accuracy 

## 1%

Concentration 793.8ppm S02

Concentration 1997ppm S02

Principle NDIR 

# I Anaylsis Results: Z =zero gas, S =standard gas, X= sample gas 

# I I I I 

# I First Triad

- S02 Z1- -0.90 S1= 791.9 S2= 794.0 Z2= -0.70 Z3= -0.90 X3= 99.2 Curve Y=1.971+0.999869•X Average= 1 00.6ppm

**~** -- ------;o. /



## ~--7 ----------



## ~~- 

## Analyst: / _L '

**~~ ~---------**  

## X1= 98.7 X2= 99.0 S3= 792.6 Second Triad

- S02 Z1- -0.90 S1= 794 S2= 793.2 Z2= -0.60 Z3= -0.60 X3= 99.30 Average =100.9ppm X1= 99.0 X2= 99.2 S3= 793.4

**~-** 

## Ling

**WJJ~---** ?--- 

## THIS STANDARD IS r'iST TRACEABLE. IT WAS CERTIFIED ,LI.CCORDING TO THE EPA PROTOCOL PROCEDURES
DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG


# 146

# I

I I I I I I I I I 

# I I I I I I I I I Specialty Gas Products

Date: 7/13/2004
Customer: Matheson- Trig as 3106 Pasadena Freeway Pasadena, Texas 77503 (713) 534-8217 Fax(713) 534-8133

Project No: 9969
Description: S02 in N2

- EPA Protocol Exp. Date 7/13/2006 Cylinder Pressure: 1900psig Cylinder No CC 177 434

Component Sulfur Dioxide Nitrogen, Balance

Reference Standard Description NTRM Instrumentation Description Horiba Process Analyzer Requested Concentration 50 ppm

Expiration date 6/1/2006

Model# VIA-51 0-S02 Certified Concentration 50.1 ppm

Cylinder Number Sg9135833

Date Last Clibrated 7/7/2004
Anaylsis Results: Z 

## = zero gas, S 

## = standard gas, X 

## = sample gas

First Triad

- S02 Z1- -1.30 S1= 999.90 S2= 999.90 Z2= -0.70 Z3= 0.00 X3= 503.60 Curve: Y=0.0064+0.09986·x Average = 50.15ppm

//-



## -- ,/

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## AnalySt:.o:----'~· i



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## Werf/ c.- 

## X1= 502.60 X2= 503.60 S3= 999.90 Second Triad

- S02 Z1- -0.80 S1= 997.90 S2= 998.70 Z2= 

## -0.10 Z3= -0.20 X3= 501.60 Average =49.98ppm Accuracy 1%



## Concentration 99.8ppm S02

Principle NDIR

X1= 500.30 X2= 500.30 S3= 999.30

THIS STANDARD IS NIST TRACEABLE IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES.
DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG



# 147

# I

I I I I I I I I I I I I I I I I I I Appendix G

# I

I I I I I I I I I I I I I I I I I I Summary()! 802 lnteriE>rncE>_ Check

Plant: Dalt1ie, Dallas, TX Location: Plant 4 Scrubber

- - 

## Monitor: Western Research 721-AT

Run#

-- -------- 

## Monitor _802, ppm Modified Method 6 S02 % Difference 

## 0 0 0 Sheet1

....



# 2 ' 3

----- ----- 

## 0 

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Page 1 

## 0

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## 0 0



# 148

# I

I I I I I I I I I 

# I I I I I I I 

# I I Sulfur Dioxide Barium- Thorin Analysis

Plant: Calt;le. Daiias, 

## iX Location: Pi ant #4 Scrubber Date: 

## 20 Jul 03

Standardizati n Ba (CI02)4 

### Titration (mls 

## l0.5 10.5 10:5

Blank Titration (mls) 

## 0.1 0.1 

## 0.1

Volume of Standard Sulfuric Acid (mls) 

## Normality of Standard Sulfuric Acid

Normality: 0.009524

Run# Location Volume 

### (mls)



## 1 lrop l 2 

## 50

2 imp 

## 1·2



## 3 Imp l 2 

## 50

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## 1 lrop2&3



## 2 Imp 2 & 

### 3



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### 3 Dilution (mls)



## 1

S02

S02

S02 Avg. Titration (mls) 

## 10.5
Avg. Blank (mls) 

## 0.1

Aliquot Volume



### (mls)



## Total Grams



## 0

0

0 Titration (mls)



## 0 1 

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## 0.00

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# 149 Average 

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PLANT • DATE • PLACE • RUN# • 8a!tile. Ca: ::jS 

## IX 

## 9·JUl·03

TEST DURATION (MINUTES) • NOZZL[ DIAMETER (INCH.). METER COEFFICIENT (Y) 

## PITOT COEFFICIENT (Cp) GAS METER VOL.(Cu.Ft.) BAROMETRIC PRESSURE



# FLOWS 50 LIQUID COLLECTED (mls) 0 S02 Sample We1ght, mg• 0.944 0 STATIC PRESSURE (in H20) • 1.818 PERCENT C02

29.5 PERCENT 02 PERCENT CO

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1 

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#DIV/01 0 0000 0.0000 73.5833



# 151 METERT. OUTLET

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# I I I I I I I I I I I I I I I I I I I EMISSION TEST SUMMARY

**PL~.NT** 

## : DATE: 9 Jul 03 PLACE :

**?la:~t** 

## 4 Scrubber 

## RUN#: 

## 2

TEST DURATION (MINUTES): NOZZLE DIAMETER (INCH.): METER COEFFICIENT (Y) PITOT COEFFICIENT (Cp) GAS METER VOL.(Cu. Ft) BAROMETRIC PRESSURE



# FLOWS 60 LIQUID COLLECTED (mls) 

## 0 S02 Sample We;ght, mg: 

## 0 944 0 STATIC PRESSURE (In H20): 1 843 PERCENT C02

29.5 PERCENT 02 PERCENT CO

SAMPLED VOLUME (STD CU. FT.): 1.6694 S02, ppm: 0.0000
POINTS STACK T. DELTA P SQUAR D P DELTA H METER T. deg F INLET

1 0 0.00 82 2 0 81 3 0 81 4 0 82 5 0 82 

## 6 0 82 

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## 0 84
#DIV/01 0 0000 0.0000 82 3333



# 152 METER T. OUTLET

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PLANT • DATE• PLACE • RUN# • 9-Jul 03 Plant 4 Scrubber 

## 3

TEST DURATIDN (MINUTES) • NOZZLE DIAMETER (INCH.) • METER CDEFFICI ENT (Y) PITDT CD EFFICIENT (Cp) GAS METER VDL.(Cu.Ft.) BAROMETRIC PRESSURE



# FLOWS 60 LIQUID COLLECTED (mls) 0 S02 Sample Weight. mg• 8.944 0 STATIC PRESSURE (in H20) • !.857 PERCENT C02

29 5 PERCENT 02 PERCENT CO

SAMPLED VOLUME (STD CU. FT.)• 1.6818 SD2, ppm. 0.0000

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#DIV/01 0.0000 0.0000 82.4167



# 153 METER T. OUTLET

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I I I I I I I I I I I I I I I I I I Sheet1

Summary of Sulfur Dioxide Analyzer Calibrations and Bias

Plant: Daltile Source: Plant 4 Scrubber Date: 7/9/03

Run #1

Run #2

Run #3 

## Analyzer Calibratrion Data

Cylinder Analyzer Absolute % 

## Span Value Response Difference Zero Gas Mid Range High Range 0 0.15 0.15 0.25 25.7 25.7 0 0 50.7 50.65 -0.05 -0 08333

System Calibration Bias and Drift Data
Analyzer Initial Values Final Values Calibration System System System System Response Calibration Calibration Calibration Calibration Response Bias Response Bias

Zero Gas 0.15 0.18 0.005 0.23 0.133333 Upscale 25.7 24.85 -0.14167 23.53 -3.61667
Average S02 Concentration: 0.17 Corrected S02 Concentration: -0 0375 (Equation 6C-1)

Zero Gas 

## 0.15 0.23 0 013333 -0.13 -046667 Upscale 25.7 23.53 -0.36167 23.9 -3
Average S02 Concentration: -0.13 Corrected S02 Concentration: -0.19548 (Equation 6C-1)

Zero Gas 0.15 -0.13 -0.04667 -0.05 -0.33333 Upscale 25.7 23.9 -0.3 23.5 -3 66667
Average S02 Concentration: -0.1 Corrected S02 Concentration: -00108 (Equation 6C-1) Drift

0 083333 -2.2

-0.6 0.616667

0 133333 -0 66667

Page 1 

# 160 Average Calibration Values

0.205 24.19

0.05 23.715

-0.09 23.7

# I

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### 0.2 

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### 0.1 

# I 07/09/03 09:34:05 0.1 

### 0.1 07/09/03 09.34:15 0.1 30.2 07/09/03 09:34:25 0.1 35.5 

### 07/09/03 09:34:35 0.1 43.2 

### 07/09/03 09:34:45 0.0 47.1 

# I 07/09/03 09:34:55 ·0.3 47.8 07/09/03 09:35:05**~0.3** 

### 48.3 07/09/03 09:35:15 -0.4 48.8 07/09103 09:35:25 -0.3 49.1 

# I 07/09/03 09.35:35 -0.4 49.4 07/09/03 09:35:45 -0.4 49.6 07/09/03 09:35:55 -0.2 49.7 

### 07/09/03 09:35:05 -0.3 49.9 

### 07/09/03 09:36:15 -0.2 50.1 

# I 07/09/03 09:36:25 -0.2 50.1 07/09/03 09:36:35 -0.2 50.1 07/09/03 09:36:45 -0.2 50.2 07/09/03 09:36:55 -0.1 50.3 07/09/03 09:37:05 -0.1 

### 50.5 

# I 07/09/03 09:37:15 -0.1 

### 50.4 07109/03 09:37:25 -0.1 50.6 07/09/03 09:37:35 -0.1 

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# I 07/09/03 09:37:55 -0.3 

### 50.7 50.7 ppm S02 07/09/03 09:38:05 -0.2 

### 50.7
07/09/03 09.38:15 -0.3 

### 50.6 07/09/03 09:38:25 -0.3 50.7 

# I 07/09/03 09:38:35 -0.3 50.a 07/09/03 09:38:45 -0.1 50.0 07/09/03 09:38:55 -0.2 47.9 07/09/03 09:39:05 0.0 43.5 07/09/03 09:39:15 00 37.7 

# I 07/09/03 09:39:25 0.0 31.6 07/09/03 09:39:35 0.0 26.4 07/09/03 09:39:45 0.1 22.5 07/09/03 09:39:55 O.l L9.5 07109.103 09:40:05 0.1 17.0 

# I 07/09/03 09:40:15 -0.1 15.5 07/09/03 09:40:25 ·0.1 15.0 07/09/03 09:40:35 -0.1 15.1 07/09/03 09:40:45 -0.2 15.7 

# I 07/09/03 09"40:55 0.0 16.6 07/09/03 09:41:05 -0.1 17.5 07/09/03 09:41:15 -0.2 184 07/09/03 09:41:25 -0.1 19.3 07/09/03 09:41:35 -0.2 20.2 

# I 07/09/03**09:~1** :45 ·0.1 21.0 07/09/03 09:41:55 -0.3 21.4 07/09103 09:42:05 -0.2 22.0 07/09/03 09:42:15 -0.2 22.5 07/09/03 09:42:25 -0.2 23.1 

# I 07/09/03**09:~2:35** -0 2 23.6 07/09/03 09"42:45 -0.1 24.0 07/09/03 09:42:55 00 24.3 07/09/03 09"43:05 0.1 24.5 07/09/03**09.~3** 15 0.1 24.7 

# I 07/09103 09**~3:25** 0.1 24.8 07/09/03 09:43:35 

### 0.2 24.9 07/09/03 09:43:45 0.3 25.0 C//09/03**09:~3:55** 0.2 25.2 

# I 07/09/03 09:44:05 00 25.3 07/09103 09:44:15 0."1 25.4 07/09/03 09:44:25 'J.2 25.5 07/09/03 09:44:35 0.1 25.6 C.7/G9:'03 09;44:45 D.2 

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### 07/09103 09:46:05 0.2 25.6 

# I 07/09!03 09:46:15 0.2 25.5 07109!03 09-46:25 0.1 

### 25.5 07/09/03 09.46:35 00 

### 252 07/09/03 09:46:45 0.1 24.6 

# I 07/09/03 09:46:55 0.2 23.2 07/09/03 09:47:05 0.1 21.3 

### 07/09/03 09:47:15 0.3 19.3 

### 07109/03 09:47.25 0.3 

### 17.5 07109103 09:47:35 0.3 15.8 

# I 07!09103 09:47:45 0.3 14.3 

### 07/09/03 09:47:55 0.2 12.9 07/09103 09:48:05 0.3 11 

### _s 07/09/03 09:48:15 0.3 

### 10.5 07/09/03 09:48:25 0.3 9.6 

# I 07/09/03 09:48:35 0.2 8.7 07/09!03 09:48:45 0.3 7.8 

### 07/09/03 09:48:55 0.2 7.2 07/09/03 09:49:05 0.2 6.8 07/09/03 09:49·15 0.2 6.3 

# I 07/09/03 09:49:25 0.2 5.8 07109/03 09:49:35 0.2 5.3 

### 07/09/03 09:49:45 0.2 4.9 

### 07/09/03 09:49;55 0.2 

### 4.5 

# I 07109!03 09:50:05 0.1 4.1 07/09/03 09:50:15 0.1 3.8 07/09/03 09:50:25 0.2 3.6 07/09103 09:50:35 00 3.3 07/09/03 09:50:45 0.0 3_1 

# I 07109/03 09:50:55 0.1 3.0 07!09/03 09:51:05 0.1 2.9 07/09/03 09:51:15 0.0 2.8 07/09/03 09:51:25 0.2 2.7 07/09103 09:51:35 0.0 2.3 

# I 07/09/03 09:51:45 0.1 2.1 07/09/03 09:51:55 0.1 2.0 07109103 09:52:05 0.1 1.9 07/09/03 09:52:15 0.1 1.9 

# I 07/09/03 09:52:25 0.1 1.8 07/09103 09:52:35 0.2 1.7 07/09/03 09:52:<15 0.3 1.6 07/09/03 09:52:55 0.3 1.5 07109/03 09:53:05 0.3 14 

# I 07109103 09:53:15 0.3 14 07/09!03 09:53:25 0.2 1.3 07/09/03 09:53:35 0.3 1.2 07/09/03 09:53:<15 0.2 1.1 :J7/09/03 09:53:55 0.2 1.2 

# I Oi/09103 09:54:05 0.2 1.2 07109/03 09:54:15 0.2 1.1 07/09/03 09:54:25 0.1 1.0 07109103 09:54:35 0.1 0.9 07/09/03 09:54:45 00 0.5 

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### 0.2 

# I 07i09/03 09:55:35 0 0 

### 0.1 07/09/03 09_55:45 -0.1 1.8 07/09..'03 09:55:55 0.0 3.1 87/09.'03 89:56:05 -C.i 4.7 

# I 07/09.103 09:56:15 -0.2 6.7 07/09/03 09:56:25 -0_1 5.7 07/89/03 89:55:35 -0.1 10.7 07/09/03 09:56:45 -0.1 12_6 07/09.'0::, 09:56:55 ·U.i 1.:.2 

# I 07,'09/03 09:57:05 8.0 15_6 07/09103 09·57·15 Q_O "16_9 

# I Page 2 

# 162

# I

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### 07/09/03 09:58:05 0.2 2i .2 

### 07/09i03 09:58:15 0.1 218 

# I 07109/03 09:58:L5 0.1 

### 22.3 07/09/03 09:58:35 00 22.8 

### 07/09/03 09:58:45 0.1 23.1 07/09/03 09:58:55 0.1 23.5 07109103 

### 09:59:05 0.1 23.7 

# I 07/09/03 09:59:15 0.0 24.0 07109/03 09"59:25 -0.2 24.2 

### 07/09/03 09:59:35 -0.2 24.4 07/09/03 09:59:45 -0.3 24.5 

# I 07/09/03 09:59:55 -0.2 24.5 07/09/03 10:00:05 

### -0.3 24.6 07/09/03 10:00:15 -0.2 24.7 07/09/03 10:00:25 -0.1 24.8 

### 07/09/03 10:00:35 -0.1 

### 24.8 

# I 07/09/03 10:00:45 -0.1 24.8 

### 07/09/03 10:00:55 -0.2 

### 24.9 07/09/03 10:01:05 -0.3 25.0 

### 07/09/03 10:01:15 

### -0.3 24.8 07/09/03 10:01:25 -0.1 24.7 

# I 07/09/03 10:01:35 -0.1 24_7 07/09/03 10:01:45 -0.2 

### 24.8 07/09103 10:01:55 -0.2 

### 24.8 25.7 ppm $02 Bias 07/09/03 10:02:05 ·0.4 

### 24.9 

# I 07/09/03 10:02:15 -0.4 

### 24.9 07/09/03 10:02:25 -0.2 24.9 07/09/03 10:02:35 -0.1 24.7 07109/03 10:02:45 0.1 23.9 

# I 07/09/03 10:02:55 0.2 22.6 07/09/03 10:03:05 0.1 21.0 07/09/03 10:03:15 0.1 18.9 07/09/03 10:03:25 0.1 17.0 07109/03 10:03:35 0.1 15.4 

# I 07/09/03 10:03:45 0.1 14.2 07/09/03 10:03:55 0.0 13.1 07/09/03 10:04:05 0.0 12.1 07/09.103 10:04:15 0.1**~** 1.2 07/09/03 10:04:25 00 10.5 

# I 07/09/03 10:04:35 0.0 9.7 07/09/03 10:04:45 0.1 9.1 07/09/03 10:04:55 0.1 8.4 07/09!03 10:05:05 0.0 7.7 07/09/03 10:05:15 0.0 7_2 

# I 07/09/03 10:05:25 0.1 7.0 07/09/03 10:05:35 0.0 6.5 07/09/03 10:05:45 0.0 6.1 07/09/03 10:05:55 0.0 58 

# I 07/09/03 10:06:05 ·0_1 5.5 07/09/03 10:06:15 0.1 5.1 07/09/03 10:06:25 00 4.8 07/09/03 10:06:35 0.0 4.5 07/09/03 10:06:45 0.0 4.3 

# I 07/09103 10·06·55 0.0 4.0 07/09/03 10:07:05 0.0 3.8 07/09/0310:07:15 0.0 3.6 07/09/03 10:07:25 0.0 3.5 07/09/03 10:07:35 0.1 3.5 

# I 07/09/03 10:07:45 0.2 3.3 07/09/03 10:07:55 0.2 3.2 07/09/03 10:08:05 0.0 3 1 0?.'09/03 10:08:15 0.0 3.0 

# I D7/09/C·3 10:08:25 -0_1 2.9 

# I I Page 3 

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# I**7/~0::2::** Rur, :;'1



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### 07/09.'03 10:'12:15 Cl.9 i 0 07/09/0310:12:25 3.7 1.0 

# I 07!09!03 10:12:35 8.8 1.0 07/09/03 10:i2:45 9.2 i.O 07/09/03 10:12:55 10.8 1.0 07/09/03 10:13:05 11 7 09**07/09/0310:~3:15** 

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# I 07/09/03 10:13:25 13.7 0.8 07/09/03 10:13:35 i4.5 

### OS 07/09/03 10:13:45 15.3 0.8 07/09/0310:13:55 16.0 0.8 07/09/0310:14:05 16.5 0.8 

# I 07/09/03 10:14:15 16.5 0.7 07/09/0310;14:25 18_7 0,7 07109/0310:14:35 17.0 0.7 

### 07/09/03**10:14:~5** 

### 17.1 0.7 

# I 07/09/0310:14:55 17.2 0.7 07!09/0310:15:05 17.2 0.7

Start Run :;'1 07/09/0310:15:15 17.0 0.7 

# I 07/09/0310:15:25 17.0 0.7 07/09/03 10:15:35 17.1 0.6 07!09/0310:15:45 17.2 0.5 07/09/0310:15:55 17.5 0.6 07/09/03 10:16:05 17.6 

### 0.7 

# I 07/0910310:16:15 

### "17.5 0 8 07/0910310:18:25 17.5 0.6 07109103 10'16:35 17.3 0.6 07109!0310:16:45 17.3 0.6 

# I 07109103 10:16:55 17.1 0.5 07109103 10:17:05 17.1 0.5 0710910310:17:15 17.3 04 07109/0310:17.25 17.4 04 0710910310.17:35 17.5 0.4 

# I 07109103 10:17:45 17.2 0.4 07109/0310:17:55 17.1 0.5 07109/03 10:18:05 17.0 0.5 07!09/0310:18:15 17.2 0.5 0710910310:18:25 17.3 0.5 

# I 07!09!03 10:18:35 17.3 0.5 07/09103**10:18:~5** 17.6 0.3 07/09!03 10:18:55 17.7 0.3 07109103 10:19:05 17.7 0.3 07!09!0310:19:15 18.0 0.4 

# I 07109/03 10'19:25 18.1 0.4 07109/0310:19:35 18.1 0.3**07109/0310:19·~5** 18.3 0.3 07!09103 10:19:55 18.5 0.2 

# I 07i09103 10:20:05 18.4 0.2 07/0910310.20·15 18_2 0.2 07109/03 10:20:25 18.1 0.2 07109/03 10:20.35 17.9 0.3 07109/03 10:20:45 17.8 0.3 

# I 07109/03 10:20:55 17.6 04 07!09!03 10.21·05 17.5 0.3 07/0910"310:21:15 17.3 0.3 07/0910310:21:25 17.3 0.3 07/09103 10:21:35 17.3 03 

# I 07/09/03 10:21:45 17.4 

# " 07109/0310:21:55 17.4 0.4 07/0910310:22:05 17.4 0.3 07/09-'03 10.22:15 17.4 0.2 

# I 07!J9/03 10:22:25 17.6 0.2 07109!03**~0:22:35** 'r7 8 0.2 C?/09/03 10:22:45 17.9 0_3 07i09/03 10.22:55 18.2 0.2 07/o9'-J3 10:23·05 "17 9 0.3 

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### 0.2 07/09/03 10:24:35 22.5 

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# I 07/09/03 10:24:45 22.3 

### C.2 07/09/0310:24:55 21.8 

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### 0.2 07/09/0310:27;15 17.0 

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### 0.2 

# I 07/09/03 10:27:55 15.5 

### 0 2 07/09/03 10:28:05 15.4 

### 0.3 07109103 10:28:15 15_3 0.2 07/09/03 10:28:25 15_1 

### 0.2 

# I 07/09/03 10;28:35 15.0 

### 0.3 07/09/03 10:28:45 14.8 

### 0.3 07/09103 10:28:55 15.0 

### 0.2 07/09/03 10:29:05 14.9 

### 0.2 07!09103 10:29:15 

### 15.0 0.2 

# I 07!09!03 10:29:25 15_0 

### 0.2 07/09/03 10-79·35 15.0 

### 0.1 07/09/03 10:29:45 14.9 

### 0.2 07/09/03 10:29:55 15.1 

### 0.3 07/09/03 10:30:05 15.3 

### 0 2 

# I 07/09/03 10:30:15 15.3 

### 0.2 07/09/03 10:30:25 15.5 

### 0.2 07/09/03 10:30;35 15.5 

### 0.2 07/09/03 10:30:45 15.3 

### 0.2 07/09/03 10:30:55 15.2 

### 0.1 

# I 07/09/0310:31:05 14.9 

### 0.2 07/09/03 10:31:15 14.8 

### 0.1 07/09/03 10:31:25 14.7 

## o.--: 07/09/0310:31:35 14.6 

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# I 07/09/03 10:31:-45 14.7 

### 0 1 07/09/03 10:31:55 14.6 

### 0.2 07/09/03 10:32:05 14.6 

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### 02 07/0.9/03 10.32:25 i4.9 

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# I 07/09/03 10:32.35 15.

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# I 07/09/03 10:33:25 14.8 

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# I 07/09/03 13_13:55 1_8 07!09!0313-14:05 1.6 07109103 13:14 15 1 6 07/09/0313:14'25 1 4 07/09/0313:14:35 1 4 

# I 07109/03 13'14:45 1.3 07/09/03 13:"14:55 1 2

Stari Run #3 

# I 07!09!03 13:15:05 1.1 07!09103 13"15:15 1 0 

### 07109/03 13:15:25 0.9 07/09/0313'15:35 09 07!09103 13'15:45 0 9 

# I 07/09/03 13:15:55 07 07!09103 13:16:05 0.6 07/09103 13:16'15 06 07/09103 i3:16:25 0.5 07/09/03 13·16:35 04 

# I 07/09/03 13-16:45 0.3 07109/03 13'16 55 0.2 07/0910313:17 05 0 2 07109/03 13:17.15 

### 01 07109/0313'17:25 0 1 

# I 07109/0313:17.35 0.1 07/09/0313:17:45 01 0710910313:17:55 0.0 07109103 13:18:05 0 0 

# I 07/09/0313'18.15 00 07/09/0313-18.25 -0 1 07109/03 13"18'35 -0.2 07109103 13:18:45 -0.1 07109/03 13:18:55 0 0 

# I 07/09/0313:19:05 

### 00 07109/03 13 19:15 -0_< 07109!03 13:19.25 -0 1 07109103 13'19 35 -0 1 07109/0313:19.45 -0.2 

# I 07109!03 13-19:55 -0 1 07/09/03 13:20:05 -0 2 07/09103 13:20:15 -0_3 07/09/03 13:20'25 -0 3 

# I 07/09/03 13:20:35 -0_3 07109/03 13:20.45 -0 4 07/09/03 13'20:55 -0 4 07/09/03

**~3:21:05** -0_3 07!09103 13.21-15 -0.3 

# I 07!09/C3 i3'21:25 -0' 07109!03 13.21 .35 -0 4 07/09/03 13'2'1 45 -0 4 07iCJ9/C3 12:21.55


# - ' 07/091D313 22:05 -0 5 

# I 07109/0313:22.15 -0_3 D?/09103 13:22:25 -0_1 07/09/G3 ";3:22"35 0.0 C//[]9103 13:22·4-5 

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# I

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### J71091G3

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### 2 

# I 07/09/03

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# I 07/09/03 13:24.25 ·D 1 07109103 13:24:35 0 0 07/09/03 13.24"45 0.0 07109103 13:24:55 -0.1 07/09/03 13:25:05 .Q 1 

# I 07/09/0313:25:15 -0.

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# I 07/09/03 13.25:55 -0.1 07109/03 13:26.05 .Q 1 07/09/0313:26-15 ·0 1 07109/03 13:26:25 -0.2 07/09/0313:26:35 

### -0.3 

# I 07/09/03 13:26-45 -0.2 07/09/03 13:26:55 -0.1 07109103 13:27-05 .Q 1 07/09/03 13:27:15 -0.1 07/09/03 13:27:25 -0.1 

# I 07109103 13.27.35 -0.1 07109103 

### 13:27:45 -0.2 07/09/0313:27:55 -0.2 07/09/03 13:28:05 -0.2 

# I 07/09/0313:28.15 -0

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# I 07/09/03 :3:29:05 ·0 1 07/09/03 13_29:15 ·0 2 07/09/03 13 29 25 -0_3 07/09/03 13:29.35 -0.2 07109103 13:29:45 -0.2 

# I 07/09/03 13:29:55 -0.2 07/09/03 13:30:05 -0.2 07/09/03 13_30:15 -0_2 07/09/03 13:30:25 -0.2 

# I 07109103 13'30.35 

## .o 3 07/09/03 13:30 45 -0.2 07109103 13:30:55 -0.2 07/09/0313:31:05 -0.2 07109103 13.31:15 -0_2 

# I 07/09/03 13:31.25 .Q 3 07/09/03 13 31:35 -0_2 07/09/03 13:31 45 -0.2 07/09/03 13.31:55 -0_3 07/09/C313:32 05 -0.3 

# I 07/09/0313:32:15 -0.3 07/09/03 13:32_ 25 D D 07/09/03 13.32:35 0 0 07/09/0313.32.45 .Q 1 

# I 07/09/0313.32:55 0 0 07/09/0313.33·05 0 0 07/09/03

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### DO 07/09/03 13:33·25 00 07/09/03 13"33:35 0 0 

# I 07/09/03 13.33'45 0 0 07/09103 03'33:55 0 0 07/09/03 13.34'05 0.0 :'7/09/'J313·3-U5 -0 1 C7/'J9iC3 13:34:25 -0 I 

# I 07/09/03

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# I 07/09/03 13:35.15 

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# I ?age 2 

# 180

# I

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# I

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# I 07/09103 13.35:55 -0 2 (,7109/03

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# I 07/09/03 13:36:45 

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# I 07/09/03 13 37_25 0.0 07/09103 13:37:35 0.0 07/09/0313:37:45 0.0 07/09/03 13:37:55 0 0 07/09/03 13:38·05 0.0 

# I 07109/0313:38•15 00 07109/0313-38.25 00 07/0910313:38.35 0.0 07/09103 13:38:45 00 07/09!03 13 38:55 0.0 

# I 07/09103 13_39:05 0.0 07/09/03 <3:39:15 0 0 07109/03 13_39:25 -0_1 07109/03 13:39:35 -0.1 

# I 07/0910313:39:45 -0_1 07/09/03 13:39:55 0.0 07!09103 13:40:05 00 07109/03 13.40:15 -0 1 07109/0313:40:25 -0 1 

# I 07/0910313-40"35 0 0 07109/0313.40:45 0 0 07109/0313 40:55 -0_1 07/0910313:41 05 -0 1 07/0910313:41:15 -0.1 

# I 07/09/0313:41:25 0.0 07/09/0313:41:35 -0.1 07/09/03 13:41:45 -0. 1 07109103 13:41:55 -0.1 

# I 07!09103 13-42:05 -0.1 07/09/031342.15 0.0 07/09/03 13:42 25 0.0 07/09/03 13'42.35 -0 1 07109103 13-42:45 -0.1 

# I 07109103 13·42:55 -01 07109103 13:43:05 -0 1 07/09/03 13:43:15 0.0 07/09/0313'43:25 0.0 07/09/03 -.3'43:35 -0.1 

# I 07109103 13"43:45 -0 1 0710910313:43:55 -0_1 07109103 13'44:05 0 0 07/09/03 13'44:15 0 0 07/09/03 13'44'25 -0 1 

# I 07/09/03 13'44:35 -0_1 07/09/03 13:44:45 -01 07/09/03 13.44:55 -0_1 07_/09/03 13'45:05 -0_1 

# I 07109103 13'45: 15 -01 07109!03 13:45:25 -01 07/09/03 13:45:35 -0 1 07/09/03 13:45:45 -01 07/09/03 13:45:55 -01 

# I 07/09103 13'46:05 

### -02 07/09/03 13'46· 15 -0.2 07109/0313'46.25 -0.2 0710910313 46:35 -0.2 07.'09/0313'46:45 -0_2 

# I 07109/0313:46:55 

### -02 07/09/03

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# I 07109/0313:47 35 -0 1 [,710910313:47 45 -0 1 

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# I 07/09/03 13:49'05 

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### 07/09/03 13:49.35 -0.2 

# I 07/09/03 13:49:45 -0.3 07109/0313:49:55 -0.2 

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### 07/09/03 13:50:15 -0.2 07109/03 13:50:25 -0.3 

# I 07109/03 13:50:35 

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# I 07/09/03 13:51 25 0.0 07/0910313:51:35 -0.1 07/09/0313:51:45 -0.1 07/09/03 13:51 :55 0 0 

# I 07/09/03 13:52:05 0.0 07/09/03 13:52:15 0 0 071:)9/0313.52:25 00 07109/03 13:52:35 00 

### 07109/03 13:52:45 0.0 

# I 07/09/03 13:52·55 -0.1 07/09/03 13:53-05 -0 1 07109103 13:53.

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# I 07109103 13:53"45 0 0 07109/03 13:53:55

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# I 07109/03 13.54:35

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# I 07109/03 13:55:15 -0.2 07/09/03 13:55:25 -0.1 07/09/0313:55"35 -0_1 07/09103 13:55 45 -0 1 07/09/03 "o3:55:55 -0.2 

# I 07/09103 13:56:05 -0_2 07/09103 13:56:15 -0.3 07/09103 "!3:56.25 -0_2 07/09103 13:56-35 -0.2 07/09103 13-56'45 -0.3 

# I 07/09103 13:56 55 -0.2 07/09/03 13.57·05 -0.2 07/09/03 "13:57_15 -0.2 07/09103 '13-57_25 -0.2 

# I 07/09103 13:57:35 -0.2 07/09103 13:57'45 -0.2 07/09/03 13-57"55 -0.1 07/0910313:58'05

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# I 07/09/03 13'58.25

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# I 07/09103 13:59:55 -0 3 07/09/03 't4·0C•.05 -0 3 

# I Page 4 

# 182

# I

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# I

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# I 07109/03 14:01:25 -O.i 07109/03 14:01.35 -0 2 07/09/03 14'01:45 

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# I 07/Q9103 14:02:05 -0.1 07/09103 14:02:15 -0.2 07/09/03 14:02:25 -0.2 07109103 14:02:35 -0 1 07/09/03 14:02:45 -0.2 

# I 07/09103 14:02:55 -0.2 07109/03 14:03:05 -0.2 07/09/03 14:03:15 -0.2 07/09/03 14:03.25 -0.1 07/09103 14'03 35 -0.1 

# I 07/09/03 14.03:45 -0.2 07/09/03 14:03:55 -0.3 07109/03 14:04:05 -0.2 07/09/03 14:04:15 -0.2 

# I 07/09103 14:04:25 -0 2 07/09/03 14:04:35 -0.2 07109!03 14:04:45 

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# I 07/09103 14:05:15 -0.2 07/09103 14'05:25 -0.2 07/09/03 14:05:35 -0.2 07/09103 14:05:45 -0.2 07/09/03 14:05:55 -0. i 

# I 07/09103 14:06:05 -0.1 07109/0314:06:15 -0.1 07/09103 14'06:25 -0 2 07/09/03 14"06.35 -0 1 

# I 07/09/03 14'06.45 -0_2 07/09/03 14:06:55 -0.2 07/09/03 14:07_·05 -0_1 07/09103 14:07 15 0_0 07/09/03 14-o7:25 -0_1 

# I 07109!03 14"07'35 00 07109103 14:07.45 00 07109103 14:07:55 00 0710910314:08:05 -01 07/0910314.08:15 -0 2 

# I 07/09/0314:08:25 -0 1 07/09/03 14.08.35 -0 1 07/09/03 14:08:45 -0 1 07/09/0314 08:55 0.0 

# I 07/09103 14:09:05 -0.1 07/0910314:09-15 -0.1 07109103 14:09 25 -0_1 07/09/03 14:09_35 -0 1 07109/03 14:09 45 

### 00 

# I ()(!09103 14:09:55 -0 1 07109/03 14:10_05 -0_1 07!09!03 '14"10'15 -0 1 07!09!03 14-10:25

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# I 07109/0314.10'45 -0 1 07.109.103 ';4'10.55 -0.1 07109/03 'i4'11"05 -C.2 C·7t09!03 '•4.11"15 -0.2 

# I 87/09/0314:11.25 -0_2 07/09/0314:1135 -0.2 07/0£/03 14'1

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# I D7/09/0314·12:15 -0.2 G//09103 14 12.25 -0 1 

# I 18.3

Page 5

# I

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# I

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# I 07/09/03 14"12:55 -0 i 'J7109i03 14:13:05 :J.O :J71091:J3 14 13'15 8 0 07/09/03 14-13:25 -0 1 

### 07/09103 14:13:35 -0.1 

# I 07109103 14:13:45 -0.1 

### 07109103 14:13"55 -0.1 07/0910314:14:05 0.0 07/09/03 14:14:15 00 07/09/03 14:14:25 

### DO 

# I 07/09/03 14 14'35 -0 1 07/09/03 14'14'45 -0.1 07/09/03 14'04 55 -0.1 

# I Stop Run #3 -0 10

07/0910314.15:05 -01 07/09/0314:15:15 -01 

### 07/09/0314:15:25 -0.1 

# I 07/09/03 14:15:35 -0.1 07/09/03 14:15:45 -0.1 07/09/0314:15:55 -0.1 07/09/03 14:16'05 -0.2 07109103 14:16:15 -0.2 

# I 07/09/03 14.16.25 -0 2 07/09/03 14"16:35 -0 2 07/09/0314:16:45 -0.1 07/09/03 14:16'55 -0.2 

# I 07/09/03 14:17:05 

### -0_2 07109/03 14.17:15 -0.2 07/09/031417:25 -0.2 07/09/03 14:17'35 -0.2 07/09/0314:17 45 -01 

# I 07/09/0314.17.55 -0_2 07/09/0314.18.05 -0.2 07109/03 14'18:15 -0_1 07/0910314:18.25 

### 0.0 

# I 0710910314:18:35 

### -0.1 Zero N2 07109103 14:18'45 

### -0.1 07109103 14:18:55 

### 0.0 07/09/0314'19:05 -0.1 

# I 07/09/0314'19:15 -0_1 0710910314:19:25 -0_1 07/09/03 14-19:35 -0_1 07/09/03 14:19.45 00 07/09/03 14:19:55 0 2 

# I 07/09/03 14:20'05 0.6 07/09/03 14:20'15 1.3 07/09/03 14:20:25 2.0 07/09/03 14:20:35 

### 28 07/09103 14:20:45 36 

# I 07109/03 14:20:55 4 4 

### 07109103 14:21 :05 54 07/09/0314.21:15 64 07/09103 14"21:25 72 07/09103 14:21:35 8_2 

# I 07/09103 14:21:45 9 0 07/09/03 14:21:55 

### 98 07/09/03 14:22:05 10.6 07109/03 14.22'15 11_3 

# I 07/09/03 14:22:25 12 0 07/09103 i4:22:35 12.7 07/09/03 14:22:45 13.3 C7 1 09/03 14.22:55 13_8 07109103 14:23·05 14 2 

# I 07i09l03 't-4:23:15 '.4 6 07109/03 14.23 25 15 1 07109/03 14.23'35 15_6 07/09/03 14'23:45 15 8 07/09/0314:23:55 16_1 

# I 07/09103 14:24 05 16_5 

# I 184

Pcge 6

# I

7/10103 Run '#3 

# I

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### 17- 

# I 07/09/03 "14:24'35 17 4 07/0910314:24:45 17 5 ·J7109/C3 14 24·55 17.7 07109/03 14.25"05 17.8 07/09/03 14:25:15 18.0 

# I 07/0910314.25:25 18.1 07109103 14:25.35 

### 18.2 07109103 14:25 45 18 4 07/09/0314:25.55 18.9 

# I 07/09/03 14:26.05 

### 19.2 07/09103 14 26 15 19.5 07109103 14:26.25 

### 19.9 07109103 14:26-35 

### 20.3 07/09/03 14:26:45 20.5 

# I 07109/03 14:26.55 20 9 07/09/03 14:27 ·05 21.2 07/09/0314:27:15 21.6 07/0910314 27'25 21.9 07/09/03 14:27:35 

### 22.3 

# I 07109103 14:27"45 22.6 07109/03 14:27:55 

### 22 9 07109/03 14:28:05 

### 23.2 07/09/03 14:28:15 23 4 

# I 07109/03 14:28:25 

### 23.5
07/09/03 14 28.35 

### 23.5 25 7 ppm 

### S02 07/09/0314:28:45 

### 23.6
07/09103 14:28 55 

### 23.6 

# I I I I I I I I I I I Page 7 

# 185

# I I I I I 

# I I I I I Customer: 

# MATHESON TRI·GAS

MATHESON TRI·GAS ·IRVING Cylinder Number;**Cyli~der** 

## pressure: SX-32146 2000 4-17-2003 10/17/03 Last Analysis date; Expiration Date:

Component : Sulfur Dioxide

Certified Cone: 25.7 

## ± 0.2 PPM

BALANCE GAS Nitrogen

REFERENCE STANDARDS Component Sulfur Dioxide SRM 

## # SRM-.1693a Cylinder#: CAL-01 0596 Concentration: 49.9 ppm 

# I CERTIFICATION INSTRUMENTS .· Component: Sulfur Dioxide 

# I Make/Model: Nicolet 550 Serial Numbec: ACN-9402192 Measurement Principle: FTIR**r;J~,:·~-.** 

## ;:..,,

__



# . I'
,,

I

I 

## Protocol

G1 

# 87

Reference# Lot ¢= 

## 249290 109-36-28491

# ,98NQ,ic0JsEJ(1!S,9YLI~DERW(-1Et(l)J-iE ·. c**''C.~f'E.~~U.REf;Abli;:>;BECOW<l50P?JG·** 

# · :· ·

REPLICATE RESPONSES

Date: 4-10-2003 Date: 4-17-2003 25.6 PPM 25.9 PPM 25.5 PPM 25.4 PPM 25.5 PPM 25.8 PPM

Last Calibration· 4-3-2003

# 1~---------------------------------- I**~Jote.s** 

# I This certification was performed according to EPA Traceability Protocol for Assay & 

## Certification o"f Gaseous Calioration Standards**Sep~ember** 

## 1997, us1ng procedure G1 and/or G2. 

# I



# I I 18fl

# I I '



# ~AIR 

# LIQUIDE I 

# I

. .. CERTIFICATE of 

# ANALYSIS 

# I



# [li~:~f~~~~~:~;o~~~~~,'~='-'-----~r~~~~~-~~~.~:te?\~~:~u"~~:~,·~,.:---'-n_t_e_rf_e~:~:~~~~su~::~~~=m~~~~~~~:~m-M __ 

# bu_~'_t:i_·_c_o_m_~n~f~f~,:arol Gases 

# I _o9/03/02 o9to2/04 1 

### jCustomer: P.O. Number: i'Joies: !Armstrong



# il~~-~~;~::;~~'~i:~:i~

**;;,r;;** 

# ... • REEERENCESTANDARD



# IF.-J~~~~:'['t **-~F:**

**~~,~~:~:;~~~:- i~c,~~-~~u~--~~**  **~,~~:~~'~;'~~-~,)~-~\~-~~-~~,:~N~t~s~,~~~~\;::;:~1~=,_**

**G~~=**

**1#~** 

# 5 

# I tra-::eability are in compliance with C PA-500/R-971123



# I I 

# I I I 

# I I Model Number: Serial Number: Analytical Principle MPC Calibrated:

Component 1

Suli'Jr D1oxicie



# fl

**A~alyst:** 

# I 11.!25

**.~ai;mont** .Parkv-1,;y, Lc Porte. Texas 77571 S')JJ Pilor:e:

**128~)** <F4-C.4QC· 

### Fax: (23J) .0:74-St:'S 

# I REQUESTED



## f~i{~~~d~tl~_ri:

50 ppr:J

Serial Number Analytical Principle: MPC Calibrated:



### 0.09 51 12



# I

, I -0.1 0 50.87



# 1 ://

/ v 

# !

**-~**



# 187 **:~~SAY•**



## C_?_~~ntr.atf?·~-

so 7 

## ::o.9 pp:T,

# I I I I I I I I I I Appendix H 

# I I I I I I I I I

# I I I I I I I I I I 

# I I I I 

# I I 

# I I I fArmstrong 

# I Environmental, " 

# Inc

..

RESuME OF

EDUCATION Thomas Armstrong

College ofDupage Glen Ellyn, Illinois

WORK EXPERIENCE



# 2/91

- Present President Armstrong Environmental, Inc. Dallas, TX



# 4/84

- 2/91 Vice-President Turner Engineering, Inc. Dallas, TX



# 1976- 1984 Project Manager The Almega Corporation Bensenville, I!linocs



# 1975- 1976 Environn1ental SpeciaEst Particle Data Labs, Ltd Elmhurst, Illinois

Mr

.. t\rmstrong has 

# 15 years experience in performing field and laboratory analysis of air pollutants !'vir Armstrong has tested for air pollutants in a variety of industries, including chemical, steel) food) power generation, pharmaceutical; ceramics, petrocbemica1 and cemer1t Mr Armstrong has performed ambient and stack tests for particulate, SOx, NOx, 

# h:-)"d:-o:::arbo71S, TRS 

# and o:hers using vinually 

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# test methods and

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# 188

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# RESTJME OF

EDUCATION Richard Taylor

Southwest Texas State University BS -Environmental Studies San Marcos, TX

WORK EXPERIENCE

2/91

- Present



# 4/88- 2/91 Project Manager Armstrong Environmental, Inc. Dallas, TX
Project Manager Turner Engineering, Inc. Dallas, TX

Mr. Taylor has widespread technical experience sampling for hydrocarbons, carbon monoxide, nitrogen oxides, sulfur oxides, particulate matter, TRS, acids, oxygen, carbon dioxide, metals, fluorides, chlorides among other compounds. He has performed emission testing on boilers, scrubbers, baghouses, incinerators, kilns, tank vents and various other processes. He specializes in gas chromatography, monitor certification and efficiency testing. 1v1i. 

# Taylor communicates effectively \vith plant supen:isors and state inspectors.



# 189

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# RESUME OF:



# EDUCA TIO:\': Dan Barrera

Houston Community College 1983- 1987 Houston, TX



# WORK EXPERIENCE:

1!101 

# To Present

8/97- 11/01

10/91- 8/97

4/87

- I 

# 1/91

1984- 1997

1983-1984



# I 976

- 1982 Stack Tester Armstrong Environmental, Inc

Beer Store Manager Grand Prairie, TX

Stack Tester Armstrong Environmental, Inc

Computer Operator Alexanders, Inc. New York, NY

Laser Printer Operator Compass Micromation, Inc Houston, TX

Microfilm Production Manager AJlacomp Houston, TX

Production Supervisor US Data Corporation Dallas, TX



# 190

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# EVALUATOR

This is to certify that

met the specifications of Federal Reference Method 9 and qualified as a visible emissions evaluator. Maximum deviation on white and black smoke did not exceed 7.5% opociiy and no single error exceeding l 

# 5% opociiy was incurred during the certification test conducted bv Eastern Technical Associates of Roleioh,

. '--' 

# North Carolina. This certificate is valid for six months from dote of issue.

326861

Pres!dent 

# 191