# N E S H A P I CR - E x i d e V er n o n

M r . F r e n c h , W e h av e p os t e d t h e E x i d e T e c hn o l o g i e s (V e r n o n , C

A ) F i n a l R e p o rt s f o r t h e I C R te s t i n g f o r t h e S e c o nd ar y L e a d S m e l te r I ndu s t r y . T h e p os t e d l o c a t i o n i s f t p : // f t p . e r g. c o m / o u t g o i n g / S e c o nd ary L e a d D a t a . P l e as e b e aw ar e t h a t : • T h e p r

e l i m i n ar y d a ta f o r m e r c u r y (Hg ) s ub m i t te d a t t h e e nd o f S

e p t e m b e r h as b ee n r

e v i s e d d u e t o a l a b o ra t o r y r e p o rt i n g e rr

o r . T h e m e r

c u r y (H g ) e m i ss i o n s s h o u l d b e r

e du c e d by a fa c

t o r of 1 , 00 0 . • T h e f i n a l r e p o rt w as n o t e n te r

e d i n to t h e E R T s i n c e a p r e d o m i n a n c

e of t h e t e s t m e t h o d s ar

e n o t s upp o rte d by E R T . T h e t e s t m e t h o d s u t i l i z e d we r

e p r i m ar i l y C

A RB t e s t m e t h o d s s

i n c e t h e t e s t i n g p r o v i d e d a du a l pu r p os

e of sa t i sf y i n g t h e r e q u i r e m e n t s of A B 25 8 8 , t h e A i r T ox i c s “ H o t Sp o t

s ” I n f o r m a t i o n a nd A ss

e ss m e n t A c t . P l e as e c o n t a c t m e i f y o u n ee d a dd i t i o n a l i n f

o r m a t i o n . T h a n ks Cha r l e s M. F i gue r oa 

# A lm e ga P (71 4 ) 88 9 - 4000 C (7 1 4 ) 6 7 9 - 59 80 c f i gue r oa @ al m egae n v i r on m en t a l . c om 

# F r o m: " C h ar l e s F i gu e r o a " < c f i gu e r o a @ a lm e g a e nv i r on m e n t a l . c o m> T o: f

r e n c h . c hu c k@ e p a . gov D a t e: 10 / 18 / 2010 6 : 40 PM Su bj ec t: N E S H A P I CR - E x i d e V e r non CC: j ohn@ a lm e g ae nv i r on m e n t a l . c o m; s a d h i k a ri @ a lm e g a e nv i r on m e n t a l . c o m; E d . M op a s @ e x i d e . c o m;

D a nny . G r ee n e @ e r g . c om P a g e 1 o f 1

# S ec o nd a r y L e a d S m e l t i n g - I C R E x i d e ( V er n o n )

D a nn y , A tt a c h e d i s t h e s u m m ar y o f r e s u l t s fr o m t h e r e c e n t l y c o ndu c t e d I C R t e s t i n g c o ndu c t e d a t t h e Ex i d e fa c

i l i t y l o c a t e d i n V e r n o n , C

a l i f o r n i a . I t i s o u r und e rs

t a nd i n g t h a t t h e p r

e l i m i n ar y d a ta / r e s u l t s ar e to b e s e n t t o t h e a t t e n t i o n of C

h u c k F r e n c h (E P A ) a nd y o u rs e l f by t o d ay . T h e f i n a l r e p o rt a nd r

e s u l t s w i l l u t i l i z e t h e E R T s y s t e m a nd w

i l l b e s ub m i tt e d i n a c o up l e o f w

e e ks ( du e 10 /18 /10 ) . T h e fa c i l i t y d a t a w as t oo l ar g e a f i l e to b e i n c

l ud e d i n t h i s e - m a i l , a nd w i l l b e p os te d o n t h e F T P . E RG . c om / o u t g o i n g / S e c o nd ar y L e a d D a t a w e b l o c a t i o n . I m a y n e e d t o c o n tac t y o u t o m o rr o w , as to d ay ’ s p ass w o r d w as n o t a l l ow

i n g m e t o a c c e ss . P l e as e c o n t a c t u s i f y o u h av e a n y qu e s

t i o n s . T h a n ks Cha r l e s M. F i gue r oa 

# A lm e ga P (71 4 ) 88 9 - 4000 C (7 1 4 ) 6 7 9 - 59 80 c f i gue r oa @ al m egae n v i r on m en t a l . c om 

# F r o m: " C h ar l e s F i gu e r o a " < c f i gu e r o a @ a lm e g a e nv i r on m e n t a l . c o m> T o: D a nny . G r ee n e @ e r g . c om D a t e: 9 / 30 / 2010 9 : 04 PM Su bj ec t: S ec ond ar y L ea d S m e lt i ng - I CR E x i d e ( V e r non) CC: E d .M op a s @ e x i d e . c o m; j ohn@ a lm e g a e nv i r on m e n t a l . c o m; fr e n c h . c hu c k@ e p a . gov A t t a c h m e n t s: N S S u mm ar y . x l s x ; D r y e r S u mm ar y . x l sx P a g e 1 o f 1F a c ility : E x i d e T ec hno l og i es

C ity: V er non , CA S o u r ce: F ee d D r y er TE S T D A TA u n its T e s t R e s u l ts A v er a ge R u n N u m b er - R un 1 R un 2 R un 2 ( m e a n) T e s t D a te m / d /y 09 / 14 / 10 09 / 16 / 10 09 / 17 / 10 T e s t T i me h /m 7 : 09 - 15 : 44 7 : 00 - 15 : 25 5 : 43 - 14 : 10 S am p li n g D a t a* M o i s tu re % 10 .6 12 .7 14 .1 12 .5 O xyg e n ** % v/v 17 .3 18 .3 18 .7 18 .1 C a rbon D i ox i d e ** % v/v 1 .4 1 .4 1 .3 1 .4 G a s S a m p l e V o l u me , V m s td d s cm 8 . 80 8 . 78 8 . 93 8 . 84 S t a c k F l o w R a te d s cm /m in 299 293 291 294 C AR B M e t h o d 436 C O NC E N T RA T I ON m g / d s cm T o t al T o t al T o t al A l u m i n u m , Al m g/ d s cm ADL 1 . 36 E + 00 ADL 1 . 59 E - 03 ADL 1 . 57 E + 00 A DL 9 . 78 E- 01 An ti m ony , Sb m g/ d s cm ADL 1 . 05 E - 03 ADL 8 . 20 E - 04 ADL 1 . 46 E - 03 A DL 1 . 11 E- 03 A r s e n i c , As m g/ d s cm ADL 5 . 75 E - 04 ADL 1 . 55 E - 04 ADL 1 . 32 E - 03 A DL 6 . 82 E- 04 B a r i u m , Ba m g/ d s cm ADL 8 . 87 E - 04 ADL 1 . 49 E - 03 ADL 1 . 32 E - 02 A DL 5 . 20 E- 03 B er y lli u m , Be m g/ d s cm B DL < 5 . 68 E - 05 B DL < 5 . 69 E - 05 B DL < 5 . 60 E - 05 B DL < 5 . 66 E- 05 C a d m i u m , Cd m g/ d s cm ADL 2 . 05 E - 04 ADL 2 . 28 E - 04 ADL 4 . 03 E - 04 A DL 2 . 79 E- 04 C hr o m i u m , Cr( T) m g/ d s cm B D Lb < 6 . 14 E - 05 ADL 1 . 82 E - 04 ADL 4 . 48 E - 05 B D Lb < 9 . 61 E- 05 C ob a lt, Co m g/ d s cm ADL 4 . 09 E - 05 ADL 5 . 58 E - 05 ADL 2 . 58 E - 05 A DL 4 . 08 E- 05 C opp er , Cu m g/ d s cm ADL 4 . 21 E - 04 ADL 2 . 85 E - 04 ADL 3 . 70 E - 04 A DL 3 . 58 E- 04 L e a d , Pb m g/ d s cm ADL 1 . 93 E - 01 ADL 2 . 85 E - 01 ADL 3 . 36 E - 01 A DL 2 . 71 E- 01 M a ng a n e s e , Mn m g/ d s cm ADL 2 . 74 E - 03 ADL 5 . 93 E - 0 3 B D Lb < 2 . 24 E - 05 B D Lb < 2 . 90 E- 03 M er c u r y , H g m g/ d s cm ADL 2 . 05 E - 03 ADL 1 . 48 E - 03 ADL 2 . 80 E - 03 A DL 2 . 11 E- 03 N i c k e l, Ni m g/ d s cm ADL 1 . 82 E - 04 ADL 2 . 16 E - 04 ADL 3 . 36 E - 04 A DL 2 . 45 E- 04 P ho s pho ru s , P m g/ d s cm B DL < 3 . 07 E - 03 B DL < 3 . 07 E - 03 B DL < 3 . 02 E - 03 B DL < 3 . 06 E- 03 S e l e n i u m , Se m g/ d s cm ADL 3 . 87 E - 05 ADL 4 . 44 E - 05 ADL 4 . 37 E - 05 A DL 4 . 22 E- 05 S il v er , Ag m g/ d s cm ADL 8 . 41 E - 05 ADL 1 . 14 E - 04 ADL 4 . 26 E - 05 A DL 8 . 02 E- 05 T h a lli u m , Tl m g/ d s cm B DL < 2 . 27 E - 05 B DL < 2 . 28 E - 05 B DL < 2 . 24 E - 05 B DL < 2 . 26 E- 05 V a n a d i u m , V , ( a s V - p e n t ox i d e) m g/ d s cm B DL < 1 . 14 E - 04 B DL < 1 . 25 E - 04 B DL < 1 . 46 E - 04 B DL < 1 . 28 E- 04 Zi n c , Zn m g/ d s cm ADL 9 . 78 E - 04 ADL 6 . 60 E - 04 ADL 1 . 64 E - 03 A DL 1 . 09 E- 03 Ir on , Fe m g/ d s cm ADL 1 . 18 E - 04 ADL 1 . 30 E - 04 ADL 1 . 54 E - 04 A DL 1 . 34 E- 04 C AR B M e t h o d 436 m g / d s cm C O NC E N T RA T I O N @ 7 %O 2 C o rr . a t 7 % O2 T o t al T o t al T o t al A l u m i n u m , Al m g/ d s cm , C o rr. ADL 5 . 29 E + 00 ADL 8 . 48 E - 03 ADL 1 . 01 E + 01 A DL 5 . 12 E + 00 An ti m ony , Sb m g/ d s cm , C o rr. ADL 4 . 05 E - 03 ADL 4 . 36 E - 03 ADL 9 . 36 E - 03 A DL 5 . 92 E- 03 A r s e n i c , As m g/ d s cm , C o rr. ADL 2 . 23 E - 03 ADL 8 . 24 E - 04 ADL 8 . 47 E - 03 A DL 3 . 84 E- 03 B a r i u m , Ba m g/ d s cm , C o rr. ADL 3 . 44 E - 03 ADL 7 . 94 E - 03 ADL 8 . 50 E - 02 A DL 3 . 21 E- 02 B er y lli u m , Be m g/ d s cm , C o rr. B DL < 2 . 20 E - 04 B DL < 3 . 03 E - 04 B DL < 3 . 60 E - 04 B DL < 2 . 94 E- 04 C a d m i u m , Cd m g/ d s cm , C o rr. ADL 7 . 93 E - 04 ADL 1 . 21 E - 03 ADL 2 . 59 E - 03 A DL 1 . 53 E- 03 C hr o m i u m , Cr( T) m g/ d s cm , C o rr. B D Lb < 2 . 38 E - 04 ADL 9 . 69 E - 04 ADL 2 . 88 E - 04 B D Lb < 4 . 98 E- 04 C ob a lt, Co m g/ d s cm , C o rr. ADL 1 . 59 E - 04 ADL 2 . 97 E - 04 ADL 1 . 66 E - 04 A DL 2 . 07 E- 04 C opp er , Cu m g/ d s cm , C o rr. ADL 1 . 63 E - 03 ADL 1 . 51 E - 03 ADL 2 . 38 E - 03 A DL 1 . 84 E- 03 L e a d , Pb m g/ d s cm , C o rr. ADL 7 . 49 E - 01 ADL 1 . 51 E + 00 ADL 2 . 16 E + 00 A DL 1 . 47 E + 00 M a ng a n e s e , Mn m g/ d s cm , C o rr. ADL 1 . 06 E - 02 ADL 3 . 16 E - 0 2 B D Lb < 1 . 44 E - 04 B D Lb < 1 . 41 E- 02 M er c u r y , H g m g/ d s cm , C o rr. ADL 7 . 93 E - 03 ADL 7 . 88 E - 03 ADL 1 . 80 E - 02 A DL 1 . 13 E- 02 N i c k e l, Ni m g/ d s cm , C o rr. ADL 7 . 05 E - 04 ADL 1 . 15 E - 03 ADL 2 . 16 E - 03 A DL 1 . 34 E- 03 P ho s pho ru s , P m g/ d s cm , C o rr. B DL < 1 . 19 E - 02 B DL < 1 . 64 E - 02 B DL < 1 . 94 E - 02 B DL < 1 . 59 E- 02 S e l e n i u m , Se m g/ d s cm , C o rr. ADL 1 . 50 E - 04 ADL 2 . 36 E - 04 ADL 2 . 81 E - 04 A DL 2 . 22 E- 04 S il v er , Ag m g/ d s cm , C o rr. ADL 3 . 26 E - 04 ADL 6 . 06 E - 04 ADL 2 . 74 E - 04 A DL 4 . 02 E- 04 T h a lli u m , Tl m g/ d s cm , C o rr. B DL < 8 . 81 E - 05 B DL < 1 . 21 E - 04 B DL < 1 . 44 E - 04 B DL < 1 . 18 E- 04 V a n a d i u m , V , ( a s V - p e n t ox i d e) m g/ d s cm , C o rr. B DL < 4 . 41 E - 04 B DL < 6 . 66 E - 04 B DL < 9 . 36 E - 04 B DL < 6 . 81 E- 04 Zi n c , Zn m g/ d s cm , C o rr. ADL 3 . 79 E - 03 ADL 3 . 51 E - 03 ADL 1 . 05 E - 02 A DL 5 . 94 E- 03 Ir on , Fe m g/ d s cm , C o rr. ADL 4 . 58 E - 04 ADL 6 . 91 E - 04 ADL 9 . 87 E - 04 A DL 7 . 12 E- 04 ##### * P er f o r me d du r i ng i s o k i n e ti c s a m p li ng ( e . g . C A RB M e thod 436 ). ** M e a s u r e d v i a S C A Q M D M e thod 10 .1 B D L - B e l o w D e t ec ti on L e v e l, M R L i s r epo r t e d. AD L - A bov e D e t ec ti on L e v el B D L b - R e a g e n t b l a nk c o rr ec t e d r e s u lt s i s l e ss th a n B D L , B D L i s s u b s titu t e d. 

## M u l t i - M et a ls CARB 436

## S u mm a r y o f S ou r c e T e s t s f o r E x i de T e c hno l o g i e s - V e r non

D i scha r ge Po i nt Pe r m it P age

# S t ack

H e i gh t, ft D eg F Es ti m a t ed S t ack F l o w DSC FM S t ack

D i a m e t er U ps tr ea m /

do w ns tr eam S t ack D esc r i p ti on F ee d D ry e r B a ghou se / C y c l one C 144 / C 143 S 145 3 69 221 11 , 000 36 840 / 84 ( 23 /2 . 3) 4 " d i a po rt s x 4 C on tr o l D ev i ce D ev i ce IDF a c ility : E x i d e T ec hno l og i es

C ity: V er non , CA S o u r ce: F ee d D r y er E xh a u s t S t a ck TE S T D A TA u n its T e s t R e s u l ts A v er a ge R u n N u m b er - R un 1 R un 2 R un 2 ( m e a n) T e s t D a te m / d /y 09 / 14 / 10 09 / 16 / 10 09 / 17 / 10 T e s t T i me h /m 7 : 09 - 16 : 02 7 : 00 - 16 : 00 5 : 43 - 14 : 10 S am p li n g D a t a* M o i s tu re % 8 .5 14 .6 12 .2 11 .8 O xyg e n ** % v/v 17 .3 18 .3 18 .7 18 .1 C a rbon D i ox i d e ** % v/v 1 .4 1 .4 1 .3 1 .4 G a s S a m p l e V o l u me , V m s td d s cm 8 . 73 8 . 80 8 . 74 8 . 76 S t a c k F l o w R a te d s cm /m in 303 289 293 295 C AR B M e t h o d 425 C O NC E N T RA T I ON T o t al T o t al T o t al C hr o m i u m V I ( t o t a l) u g/ d s cm B DL < 0 . 0463 ADL 0 . 1489 ADL 0 . 1912 B DL < 0 . 1288 C O NC E N T RA T I O N @ 7 %O 2 T o t al T o t al T o t al C hr o m i u m V I ( t o t a l) u g/ d s cm , C o rr. B DL < 0 . 1793 ADL 0 . 7925 ADL 1 . 229 B DL < 0 . 7335 * P er f o r me d du r i ng i s o k i n e ti c s a m p li ng ( e . g . C A RB M e thod 425 ). ** M e a s u r e d v i a S C A Q M D M e thod 10 .1 B D L - B e l o w D e t ec ti on L e v e l, M R L i s r epo r t e d. AD L - A bov e D e t ec ti on L e v el 

## H e xa v a l e n t C h r o um i um CAR B 425

### R un N u m ber 1 2 3

R un D a te 09 /20 / 10 09 /20 / 10 09 /20 / 10 R un S t ar t T i me 8 : 55 11 : 30 14 : 00 R un S t op T i me 11 : 04 13 : 42 16 : 19 T est T r a i n P a r a m ete rs A VE R A GE V o l u m e o f D ry

G a s S a m p l e , S C F* 78 . 187 77 . 323 77 . 725 77 . 745 V o l u m e o f D ry

G a s S a m p l e , d s cm 2 . 214 2 . 190 2 . 201 2 . 201 F l u e G as P a r a m ete rs C O 2 , P er c e n t B y V o l u m e , D ry 0 . 30 0 . 80 1 .2 0 . 77 O 2 , P er c e n t B y V o l u m e , D ry 20 . 20 19 .0 18 .5 19 . 23 T e m pera t u re , D egree s F 210 .5 209 .8 210 .1 210 .1 Mo i s t u re , % 5 . 92 4 . 33 7 . 62 5 . 96 A i r F l o w R a t e , W e t A C FM 15 , 358 15 , 147 15 , 286 15 , 264 A i r F l o w R a t e , D ry S C F M* 11 , 316 11 , 362 11 , 066 11 , 248 A i r F l o w R a t e , d s c m / m in 320 .4 321 .7 313 .4 319 To ta l F il te r a b l e P a r t i c u l ate T o t a l c a t c h , mg 3 . 00 3 . 55 0 . 60 2 . 38 C o n c e n t ra t i o n @ 7 % O2 0 . 0118 0 . 0052 0 . 0007 0 . 0059 C o n c e n t ra t i o n m g / D S CM 1 . 355 1 . 621 0 . 273 1 . 083 C o n c e n t ra t i o n @ 7 % O 2 , m g / D S CM 26 . 90 11 . 86 1 . 58 13 . 45

* 68 D egree s F a n d 29 . 92 I n c h e s o f Mer c u ry 

# T o t a l F ilt e r ab l e P a rt i cu l a te EP A M e t hod 5 ( F ilt e r T e m p @ 250 deg F) Ex i de , V e r non , Feed D r y er

## D i sc h arg e P oint P erm i t P a g e # St ack

He igh t , ft De g F E s t i ma te d St ack Flow D S C FM St ack

D i ame t er U p s t ream

/ down s t re am St ack Descr ip ti on Nep t une Scr ubbe r/ No r t h & S ou t h Re v e r b B aghou s e (B aghou s e s e x hau s t to scr

ubbe r and a r

e pa r t o f t he e m i ss ion c on t

r ol t r ain) C42 / C43/

C40 / C41 S 139 23 112 137 22 , 000 45 .5 672 / 420 ( 15 / 9) 4 " d i a .

po r t s x 2 C on t r ol Dev i ce Dev i ce ID Dev i ce ID

# P C Bs CARB 428 F a c ilit y : E x i d e Tec hn o l o g i es C it y: V ern o n, CA S o u r ce: N ep tun e S c r

ubb er E xh a u s t S t a ck TE S T DA TA un its Te s t R e s u l ts A v er age R un N u mb er - R un 1 R un

2 R un

3 ( m e a n) Te s t D a te m/ d/y 09 / 01 / 10 09 / 02 / 10 09 / 03 / 10 Te s t T i me h/m 7 : 45 - 16 : 02 7 : 30 - 15 : 50 7 : 30 - 16 : 05 S a m p li n g D a t a* M o i s tu re % 17.2 14.5 14.7 15.5 O x yg e n ** % v /v 18.0 17.3 19.9 18.4 Ca r b o n D i ox i d e ** % v /v 2.7 3.8 < 0.3 2.3 G a s S a mp l e V o l u m e , V m s td d s cm 9.57 9.60 9.55 9.57 S t a c k F l o w Ra te d s c m/min 530 544 542 539 CAR B Me t h o d 428 - P C Bs C O NC E N T RA T I ON ng / d s cm T o t a l m o n o CB ng / d s cm ADL 0.426 ADL 0.442 ADL 0.480 ADL 0.449 T o t a l d i CB ng / d s cm ADL 8.548 ADL 4.780 ADL 3.646 ADL 5.66 T o t a l tri CB ng / d s cm ADL 16.303 ADL 8.519 ADL 5.731 ADL 10.18 T o t a l t e tr aCB ng / d s cm ADL 27.171 ADL 14.373 ADL 10.214 ADL 17.25 T o t a l p e n t aCB ng / d s cm ADL 32.501 ADL 20.934 ADL 16.029 ADL 23.15 T o t a l h e x aCB ng / d s cm ADL 8.507 ADL 5.676 ADL 5.217 ADL 6.47 T o t a l h ep t aCB ng / d s cm ADL 1.703 ADL 0.970 ADL 1.016 ADL 1.23 T o t a l o c t aCB ng / d s cm ADL 0.166 B DL < 0.104 ADL 0.036 B DL < 0.102 T o t a l n o n aCB ng / d s cm ADL 0.0123 ADL 0.0107 B DL < 0.105 B DL < 0.0426 T o t a l d ec aCB ng / d s cm B DL < 0.105 B DL < 0.104 B DL < 0.105 B DL < 0.104 T o t a l P C B s , a s M o n o C B ng / d s cm ADL 95.307 ADL 55.616 ADL 42.325 ADL 64.42 CAR B Me t h o d 428 - P C Bs n g / d s cm C O NC E N T RA T I O N @ 7 %O 2 

### C o rr .a t7 % O2 T o t a l m o n o CB ng / d s c m , C o rr. ADL 2.04 4 ADL 1.71 1 ADL 6.352 ADL 3.369 T o t a l d i CB ng / d s c m , C o rr. ADL 40.97 3 ADL 18.52 2 ADL 48.263 ADL 35.920 T o t a l tri CB ng / d s c m , C o rr. ADL 78.14 0 ADL 33.00 9 ADL 75.862 ADL 62.337 T o t a l t e tr aCB ng / d s c m , C o rr. ADL 130.23 3 ADL 55.68 7 ADL 135.220 ADL 107.047 T o t a l p e n t aCB ng / d s c m , C o rr. ADL 155.77 8 ADL 81.11 0 ADL 212.191 ADL 149.693 T o t a l h e x aCB ng / d s c m , C o rr. ADL 40.77 3 ADL 21.99 3 ADL 69.066 ADL 43.944 T o t a l h ep t aCB ng / d s c m , C o rr. ADL 8.16 5 ADL 3.75 7 ADL 13.453 ADL 8.458 T o t a l o c t aCB ng / d s c m , C o rr. ADL 0.79 6 B DL < 0.40 4 ADL 0.4701 B DL < 0.557 T o t a l n o n aCB ng / d s c m , C o rr. ADL 0.059 1 ADL 0.041 6 B DL < 1.387 B DL < 0.496 T o t a l d ec aCB ng / d s c m , C o rr. B DL < 0.50 1 B DL < 0.403 5 B DL < 1.387 B DL < 0.764 T o t a l P C B s , a s M o n o C B ng / d s c m , C o rr. ADL 456.81 7 ADL 215.48 6 ADL < 560.296 ADL 410.866 * P er f o rm e d du ri ng i s o k i n e ti c s a mp li ng ( e .g. C A R B M e th o d 428 ). ** M e a s u r e d v i a S C AQ M D M e th o d 10.1 B D L - Be l o w D e t ec ti o n Le v e l , M R L i s r ep o rt e d. AD L - A b ov e D e t ec ti o n Le v e l.F a c ility : E x i d e T ec hno l og i es

C ity: V er non , CA S o u r ce: N ep tu n e S c ru bb er E xh a u s t S t a ck TE S T D A TA u n its T e s t R e s u l ts A v er a ge R u n N u m b er - R un 1 R un 2 R un 3 ( m e a n) T e s t D a te mm / dd / yy 09 / 01 / 10 09 / 02 / 10 09 / 03 / 10 T e s t T i me h /m 7 : 45 - 16 : 02 7 : 30 - 15 : 50 7 : 30 - 16 : 05 S am p li n g D a t a* M o i s tu re % 17 .2 14 .5 14 .7 15 .5 O xyg e n ** % v/v 18 .0 17 .3 19 .9 18 .4 C a rbon D i ox i d e ** % v/v 2 .7 3 .8 < 0 .3 2 .3 G a s S a m p l e V o l u me , V m s td d s cm 9 . 57 9 . 60 9 . 55 9 . 57 S t a c k F l o w R a te d s cm /m in 530 544 542 539 C AR B M e t h o d 428 C O NC E N T RA T I ON n g / d s cm 2 , 3 , 7 , 8 - T C DD ng/ d s cm B DL < 1 . 71 E - 4 ADL 4 . 50 E - 4 B DL < 4 . 25 E -4 B DL < 3 . 49 E- 04 1 , 2 , 3 , 7 , 8 - P e C DD ng/ d s cm ADL 2 . 24 E - 4 ADL 4 . 92 E - 4 B DL < 6 . 38 E -4 B DL < 4 . 51 E- 04 1 , 2 , 3 , 4 , 7 , 8 - H x C DD ng/ d s cm B D L < 3 . 73 E - 4 B D L < 2 . 18 E - 4 ADL 2 . 66 E -4 B DL < 2 . 86 E- 04 1 , 2 , 3 , 6 , 7 , 8 - H x C DD ng/ d s cm B D L < 3 . 48 E - 4 ADL 2 . 30 E - 4 ADL 3 . 71 E -4 B DL < 3 . 16 E- 04 1 , 2 , 3 , 7 , 8 , 9 - H x C DD ng/ d s cm B D L < 3 . 31 E - 4 B D L < 1 . 94 E - 4 ADL 2 . 59 E -4 B DL < 2 . 61 E- 04 1 , 2 , 3 , 4 , 6 , 7 , 8 , - H p C DD ng/ d s cm ADL 4 . 98 E - 4 B DL < 3 . 69 E - 4 ADL 4 . 20 E -4 B DL < 4 . 29 E- 04 O C DD ng/ d s cm ADL 2 . 23 E - 3 B DL < 1 . 48 E - 3 ADL 1 . 39 E -3 B DL < 1 . 70 E- 03 2 , 3 , 7 , 8 - T C DF ng/ d s cm ADL 4 . 55 E - 3 ADL 1 . 23 E - 2 ADL 1 . 12 E -2 A DL 9 . 35 E- 03 1 , 2 , 3 , 7 , 8 - P e C DF ng/ d s cm ADL 3 . 76 E - 3 ADL 1 . 36 E - 2 ADL 1 . 32 E -2 A DL 1 . 02 E- 02 2 , 3 , 4 , 7 , 8 - P e C DF ng/ d s cm ADL 2 . 78 E - 3 ADL 1 . 05 E - 2 ADL 1 . 02 E -2 A DL 7 . 82 E- 03 1 , 2 , 3 , 4 , 7 , 8 - H x C DF ng/ d s cm B DL < 9 . 39 E - 4 ADL 4 . 82 E - 3 ADL 4 . 75 E -3 B DL < 3 . 50 E- 03 1 , 2 , 3 , 6 , 7 , 8 - H x C DF ng/ d s cm ADL 1 . 22 E - 3 ADL 5 . 08 E - 3 ADL 5 . 22 E -3 A DL 3 . 84 E- 03 2 , 3 , 4 , 6 , 7 , 8 - H x C DF ng/ d s cm ADL 6 . 50 E - 4 ADL 2 . 34 E - 3 ADL 2 . 57 E -3 A DL 1 . 85 E- 03 1 , 2 , 3 , 7 , 8 , 9 - H x C DF ng/ d s cm B D L < 6 . 98 E - 5 ADL 4 . 25 E - 4 ADL 9 . 00 E -4 B DL < 4 . 65 E- 04 1 , 2 , 3 , 4 , 6 , 7 , 8 - H p C DF ng/ d s cm ADL 7 . 79 E - 4 ADL 2 . 86 E - 3 ADL 2 . 89 E -3 A DL 2 . 18 E- 03 1 , 2 , 3 , 4 , 7 , 8 , 9 - H p C DF ng/ d s cm B D L < 1 . 96 E - 4 B D L < 2 . 86 E - 4 ADL 4 . 31 E -4 B DL < 3 . 04 E- 04 O C DF ng/ d s cm ADL 3 . 00 E - 4 B DL < 4 . 09 E - 4 B DL < 5 . 09 E -4 B DL < 4 . 06 E- 04 T o t a l T C DD ng/ d s cm ADL 1 . 11 E - 2 ADL 1 . 90 E - 2 ADL 1 . 82 E -2 A DL 1 . 61 E- 02 T o t a l P e C DD ng/ d s cm ADL 4 . 17 E - 3 ADL 6 . 53 E - 3 ADL 9 . 73 E -3 A DL 6 . 81 E- 03 T o t a l H x C DD ng/ d s cm ADL 2 . 12 E - 3 ADL 4 . 24 E - 3 ADL 3 . 95 E -3 A DL 3 . 44 E- 03 T o t a l H p C DD ng/ d s cm ADL 1 . 86 E - 3 ADL 8 . 01 E - 4 ADL 1 . 32 E -3 A DL 1 . 33 E- 03 T o t a l T C DF ng/ d s cm ADL 1 . 48 E - 1 ADL 3 . 45 E - 1 ADL 3 . 37 E -1 A DL 2 . 77 E- 01 T o t a l P e C DF ng/ d s cm ADL 4 . 88 E - 2 ADL 1 . 68 E - 1 ADL 1 . 55 E -1 A DL 1 . 24 E- 01 T o t a l H x C DF ng/ d s cm ADL 7 . 20 E - 3 ADL 3 . 95 E - 2 ADL 4 . 06 E -2 A DL 2 . 91 E- 02 T o t a l H p C DF ng/ d s cm ADL 7 . 79 E - 4 ADL 3 . 50 E - 3 ADL 4 . 08 E -3 A DL 2 . 79 E- 03 C AR B M e t h o d 428 n g / d s cm C O NC E N T RA T I O N @ 7 %O 2 C o rr . a t 7 % O2 2 , 3 , 7 , 8 - T C DD ng/ d s cm , C o rr. B DL < 8 . 21 E - 0 4 ADL 1 . 74 E - 0 3 B DL < 5 . 63 E - 03 B DL < 2 . 73 E- 03 1 , 2 , 3 , 7 , 8 - P e C DD ng/ d s cm , C o rr. ADL 1 . 07 E - 0 3 ADL 1 . 90 E - 0 3 B DL < 8 . 45 E - 03 B DL < 3 . 81 E- 03 1 , 2 , 3 , 4 , 7 , 8 - H x C DD ng/ d s cm , C o rr. B D L < 1 . 79 E - 0 3 B D L < 8 . 43 E - 0 4 ADL 3 . 52 E - 03 B DL < 2 . 05 E- 03 1 , 2 , 3 , 6 , 7 , 8 - H x C DD ng/ d s cm , C o rr. B D L < 1 . 67 E - 0 3 ADL 8 . 92 E - 0 4 ADL 4 . 91 E - 03 B DL < 2 . 49 E- 03 1 , 2 , 3 , 7 , 8 , 9 - H x C DD ng/ d s cm , C o rr. B D L < 1 . 59 E - 0 3 B D L < 7 . 51 E - 0 4 ADL 3 . 43 E - 03 B DL < 1 . 92 E- 03 1 , 2 , 3 , 4 , 6 , 7 , 8 , - H p C DD ng/ d s cm , C o rr. ADL 2 . 39 E - 0 3 B DL < 1 . 43 E - 0 3 ADL 5 . 56 E - 03 B DL < 3 . 13 E- 03 O C DD ng/ d s cm , C o rr. ADL 1 . 07 E - 0 2 B DL < 5 . 73 E - 0 3 ADL 1 . 84 E - 02 B DL < 1 . 16 E- 02 2 , 3 , 7 , 8 - T C DF ng/ d s cm , C o rr. ADL 2 . 18 E - 0 2 ADL 4 . 76 E - 0 2 ADL 1 . 48 E - 01 A DL 7 . 26 E- 02 1 , 2 , 3 , 7 , 8 - P e C DF ng/ d s cm , C o rr. ADL 1 . 80 E - 0 2 ADL 5 . 29 E - 0 2 ADL 1 . 75 E - 01 A DL 8 . 19 E- 02 2 , 3 , 4 , 7 , 8 - P e C DF ng/ d s cm , C o rr. ADL 1 . 33 E - 0 2 ADL 4 . 08 E - 0 2 ADL 1 . 34 E - 01 A DL 6 . 28 E- 02 1 , 2 , 3 , 4 , 7 , 8 - H x C DF ng/ d s cm , C o rr. B DL < 4 . 50 E - 0 3 ADL 1 . 87 E - 0 2 ADL 6 . 28 E - 02 B DL < 2 . 87 E- 02 1 , 2 , 3 , 6 , 7 , 8 - H x C DF ng/ d s cm , C o rr. ADL 5 . 86 E - 0 3 ADL 1 . 97 E - 0 2 ADL 6 . 91 E - 02 A DL 3 . 15 E- 02 2 , 3 , 4 , 6 , 7 , 8 - H x C DF ng/ d s cm , C o rr. ADL 3 . 12 E - 0 3 ADL 9 . 08 E - 0 3 ADL 3 . 40 E - 02 A DL 1 . 54 E- 02 1 , 2 , 3 , 7 , 8 , 9 - H x C DF ng/ d s cm , C o rr. B D L < 3 . 35 E - 0 4 ADL 1 . 65 E - 0 3 ADL 1 . 19 E - 02 B DL < 4 . 63 E- 03 1 , 2 , 3 , 4 , 6 , 7 , 8 - H p C DF ng/ d s cm , C o rr. ADL 3 . 73 E - 0 3 ADL 1 . 11 E - 0 2 ADL 3 . 82 E - 02 A DL 1 . 77 E- 02 1 , 2 , 3 , 4 , 7 , 8 , 9 - H p C DF ng/ d s cm , C o rr. B D L < 9 . 42 E - 0 4 B D L < 1 . 11 E - 0 3 ADL 5 . 70 E - 03 B DL < 2 . 58 E- 03 O C DF ng/ d s cm , C o rr. ADL 1 . 44 E - 0 3 B DL < 1 . 59 E - 0 3 B DL < 6 . 74 E - 03 B DL < 3 . 25 E- 03 T o t a l T C DD ng/ d s cm , C o rr. ADL 5 . 31 E - 0 2 ADL 7 . 34 E - 0 2 ADL 2 . 41 E - 01 A DL 1 . 23 E- 01 T o t a l P e C DD ng/ d s cm , C o rr. ADL 2 . 00 E - 0 2 ADL 2 . 53 E - 0 2 ADL 1 . 29 E - 01 A DL 5 . 80 E- 02 T o t a l H x C DD ng/ d s cm , C o rr. ADL 1 . 02 E - 0 2 ADL 1 . 64 E - 0 2 ADL 5 . 23 E - 02 A DL 2 . 63 E- 02 T o t a l H p C DD ng/ d s cm , C o rr. ADL 8 . 91 E - 0 3 ADL 3 . 10 E - 0 3 ADL 1 . 74 E - 02 A DL 9 . 82 E- 03 T o t a l T C DF ng/ d s cm , C o rr. ADL 7 . 11 E - 0 1 ADL 1 . 34 E + 0 0 ADL 4 . 47 E + 00 A DL 2 . 17 E + 00 T o t a l P e C DF ng/ d s cm , C o rr. ADL 2 . 34 E - 0 1 ADL 6 . 50 E - 0 1 ADL 2 . 05 E + 00 A DL 9 . 79 E- 01 T o t a l H x C DF ng/ d s cm , C o rr. ADL 3 . 45 E - 0 2 ADL 1 . 53 E - 0 1 ADL 5 . 38 E - 01 A DL 2 . 42 E- 01 T o t a l H p C DF ng/ d s cm , C o rr. ADL 3 . 73 E - 0 3 ADL 1 . 35 E - 0 2 ADL 5 . 40 E - 02 A DL 2 . 38 E- 02 * P er f o r me d du r i ng i s o k i n e ti c s a m p li ng ( e . g . C A RB M e thod 428 ). ** M e a s u r e d v i a S C A Q M D M e thod 10 .1 B D L - B e l o w D e t ec ti on L e v e l, R L i s r epo r t e d. AD L - A bov e D e t ec ti on L e v e l. 

## D i o x i n / F u r a ns CARB 428

## F a c ilit y: E x i d e T ec hn o l o g i es

L o c ati o n: V e rn o n , CA S o u r ce: N e p t u n e S c r u bb er T e s t: E PA M 25A R un T e st S ta rt E nd C O2 d ry d r y ppm N o. D ate Time Time d r y % d r y

% ppm @ 7% O2 1 09 / 01 / 10 7 : 11 16 : 07 18 . 00 2 . 66 1 . 27 6 . 07 2 09 / 02 / 10 7 : 17 15 : 47 17 . 31 3 . 81 0 . 68 2 . 81 3 09 / 03 / 10 7 : 47 16 : 05 19 . 85 0 . 30 0 . 41 7 . 05 * O 2 / C O 2 w a s m e a s u r e d v ia S C AQMD M e t h o d 10 . 1. N o t e : E PA M e t h o d 25 A i n s t r u m e n t off - li n e e v e r y 2- h o u r s fo r c ali b r ati o n s. S am p l e d du r i n g t h e C A RB M e t h o d 428 s am p li n g e v e n t. O2 

# T o t a l H y d r o c a r b o ns U S E P A M e t h o d 25A

R u n I n fo r mati on F l u e G a s C o m p o s iti o n* T H C a s P r o p a n e ( M W : 44 . 1 l b/l b - m o l e)

### F a c ili t y : E x i d e T ec hn o l og i es

C i t y: V e r n o n , CA So u r ce: N e p t un e Sc r ubb e r E x hau s t S t a ck TE S T DATA un i ts T es t R es u l ts A v erage Run N u m b er - R un 1 R un 2 R un 2 ( mea n) T es t D a te m / d /y 09 / 13 / 10 09 / 14 / 10 09 / 14 / 10 T es t T i me h /m 10 : 50 - 15 : 02 6 : 09 - 10 : 23 10 : 57 - 15 : 10 S a m p li n g D a t a* M o i s t u re % 16 .7 17 .8 17 .5 17 .3 O xyge n ** % v /v 16 .4 15 .9 15 .3 15 .9 C a r b o n D i ox i d e** % v /v 4 .9 5 .9 6 .8 5 .8 G as S a mp l e V o l u m e , Vm s td d s cm 4 . 77 4 . 78 4 . 77 4 . 78 S t a c k F l o w R a te d s c m / m in 527 523 523 524 CARB M e t h o d 421 CONCENTRAT I ON mg / d scm H y d r oge n C h l o r i d e ( HC L) m g / d s cm BDL < 0 . 0241 BDL < 0 . 0253 BDL < 0 . 0260 BDL < 0 . 0251 H y d r oge n F l u o r i d e ( H F) m g / d s cm BDL < 0 . 0247 BDL < 0 . 0259 BDL < 0 . 0266 BDL < 0 . 0258 CARB M e t h o d 421 mg / d scm CONCENTRAT I ON @7 %O 2 

### C orr . a t 7 % O2 H y d r oge n C h l o r i d e ( HC L) m g / d s c m , C o rr. BDL < 0 . 0749 BDL < 0 . 0703 BDL < 0 . 0645 BDL < 0 . 0699 H y d r oge n F l u o r i d e ( H F) m g / d s c m , C o rr. BDL < 0 . 0768 BDL < 0 . 0720 BDL < 0 . 0660 BDL < 0 . 0716 * P e r f o r m e d du r i n g i s o k i n e t i c sa mp li n g ( e . g . C A RB M e t h o d 421 ). ** M e asu r e d v

i a S C A Q M D M e t h o d 10 .1 BDL - B e l o w D e t ec t i o n L e ve l , M RL i s r e p o rt e d. 

# H CL CAR B 421

### R un N u m ber R1 2 3

R un D a te 09 / 13 / 10 09 / 14 / 10 09 / 14 / 10 R un S t ar t T i me 10 : 50 6 : 09 10 : 57 R un S t op T i me 15 : 05 10 : 23 15 : 10 T est T r a i n P a r a m ete rs A VE R A GE V o l u m e o f D ry

G a s S a m p l e , S C F* 167 . 520 162 . 621 159 . 747 163 . 296 V o l u m e o f D ry

G a s S a m p l e , d s cm 4 . 744 4 . 605 4 . 523 4 . 624 F l u e G as P a r a m ete rs C O 2 , P er c e n t B y V o l u m e , D ry 4 . 88 5 . 90 6 . 75 5 . 84 O 2 , P er c e n t B y V o l u m e , D ry 16 . 43 15 .9 15 .3 15 . 88 T e m pera t u re , D egree s F 139 .4 139 .4 140 .5 139 .8 Mo i s t u re , % 17 . 58 18 . 26 17 . 83 17 . 89 A i r F l o w R a t e , D ry S C F M* 18 , 465 17 , 635 17 , 399 17 , 833 A i r F l o w R a t e , d s c m / m in 522 .9 499 .4 492 .7 505 .0 To ta l F il te r a b l e P a r t i c u l ate T o t a l c a t c h , mg 23 . 30 20 . 40 26 . 95 23 . 55 C o n c e n t ra t i o n m g / D S CM 4 . 91 4 . 43 5 . 96 5 . 10 C o n c e n t ra t i o n @ 7 % O 2 , m g / D S CM 15 . 26 12 . 31 14 . 79 14 . 12

* 68 D egree s F a n d 29 . 92 I n c h e s o f Mer c u ry 

# T o t a l F ilt e r ab l e P a rt i cu l a te EP A M e t hod 5 ( F ilt e r T e m p @ 250 deg F) Ex i de , V e r non , N ep t une S c r ubberF a c ility : E x i d e T ec hno l og i es

C ity: V er non , CA S o u r ce: N ep tu n e S c ru bb er E xh a u s t S t a ck TE S T D A TA u n its T e s t R e s u l ts A v er a ge R u n N u m b er - R un 1 R un 2 R un 2 ( m e a n) T e s t D a te m / d /y 09 / 08 / 10 09 / 09 / 10 09 / 10 / 10 T e s t T i me h /m 8 : 25 - 16 : 45 8 : 06 - 16 : 29 5 : 37 - 14 : 09 S am p li n g D a t a* M o i s tu re % 15 .3 17 .9 18 .3 17 .2 O xyg e n ** % v/v 16 .6 16 .7 16 .2 16 .5 C a rbon D i ox i d e ** % v/v 4 .5 3 .8 5 .1 4 .5 G a s S a m p l e V o l u me , V m s td d s cm 8 . 46 9 . 59 9 . 21 9 . 09 S t a c k F l o w R a te d s cm /m in 510 524 501 512 C AR B M e t h o d 436 C O NC E N T RA T I ON m g / d s cm T o t al T o t al T o t al A l u m i n u m , Al m g/ d s cm ADL 1 . 11 E - 02 ADL 1 . 04 E - 02 ADL 9 . 23 E - 02 A DL 3 . 80 E- 02 An ti m ony , Sb m g/ d s cm ADL 6 . 97 E - 05 ADL 1 . 36 E - 04 ADL 7 . 60 E - 05 A DL 9 . 38 E- 05 A r s e n i c , As m g/ d s cm ADL 4 . 73 E - 06 ADL 1 . 11 E - 04 ADL 5 . 87 E - 05 A DL 5 . 80 E- 05 B a r i u m , Ba m g/ d s cm ADL 3 . 66 E - 04 ADL 2 . 19 E - 04 ADL 1 . 63 E - 04 A DL 2 . 49 E- 04 B er y lli u m , Be m g/ d s cm B DL < 5 . 91 E - 05 B DL < 5 . 22 E - 05 B DL < 5 . 43 E - 05 B DL < 5 . 52 E- 05 C a d m i u m , Cd m g/ d s cm ADL 8 . 15 E - 05 ADL 3 . 65 E - 05 ADL 9 . 02 E - 05 A DL 6 . 94 E- 05 C hr o m i u m , Cr( T) m g/ d s cm ADL 9 . 45 E - 05 ADL 7 . 30 E - 05 ADL 1 . 19 E - 04 A DL 9 . 57 E- 05 C ob a lt, Co m g/ d s cm ADL 6 . 26 E - 05 ADL 2 . 40 E - 05 ADL 3 . 80 E - 05 A DL 4 . 15 E- 05 C opp er , Cu m g/ d s cm ADL 3 . 43 E - 04 ADL 2 . 30 E - 04 ADL 2 . 28 E - 04 A DL 2 . 67 E- 04 L e a d , Pb m g/ d s cm ADL 2 . 77 E - 03 ADL 2 . 86 E - 03 ADL 2 . 11 E - 03 A DL 2 . 58 E- 03 M a ng a n e s e , Mn m g/ d s cm B D Lb < 2 . 36 E - 0 5 B D Lb < 2 . 09 E - 0 5 B D Lb < 2 . 17 E - 05 B D Lb < 2 . 21 E- 05 M er c u r y , H g m g/ d s cm ADL 1 . 30 E + 00 ADL 9 . 18 E - 01 ADL 3 . 48 E + 00 A DL 1 . 90 E + 00 N i c k e l, Ni m g/ d s cm ADL 1 . 18 E - 05 ADL 6 . 47 E - 04 ADL 3 . 26 E - 04 A DL 3 . 28 E- 04 P ho s pho ru s , P m g/ d s cm ADL 3 . 19 E - 03 ADL 5 . 53 E - 03 ADL 4 . 02 E - 03 A DL 4 . 25 E- 03 S e l e n i u m , Se m g/ d s cm B DL < 2 . 36 E - 05 B DL < 2 . 09 E - 05 ADL 4 . 02 E - 04 B DL < 1 . 49 E- 04 S il v er , Ag m g/ d s cm B DL < 2 . 36 E - 05 B DL < 2 . 09 E - 05 B DL < 2 . 17 E - 05 B DL < 2 . 21 E- 05 T h a lli u m , Tl m g/ d s cm B DL < 2 . 36 E - 05 B DL < 2 . 09 E - 05 B DL < 2 . 17 E - 05 B DL < 2 . 21 E- 05 V a n a d i u m , V , ( a s V - p e n t ox i d e) m g/ d s cm B DL < 1 . 18 E - 04 B DL < 1 . 04 E - 04 B DL < 1 . 09 E - 04 B DL < 1 . 10 E- 04 Zi n c , Zn m g/ d s cm ADL 7 . 09 E - 05 ADL 1 . 31 E - 03 ADL 1 . 15 E - 03 A DL 8 . 46 E- 04 Ir on , Fe m g/ d s cm ADL 1 . 54 E - 03 ADL 9 . 57 E - 03 ADL 7 . 21 E - 03 A DL 6 . 10 E- 03 C AR B M e t h o d 436 m g / d s cm C O NC E N T RA T I O N @ 7 %O 2 C o rr . a t 7 % O2 T o t al T o t al T o t al A l u m i n u m , Al m g/ d s cm , C o rr. ADL 3 . 56 E - 02 ADL 3 . 46 E - 02 ADL 2 . 74 E - 01 A DL 1 . 15 E- 01 An ti m ony , Sb m g/ d s cm , C o rr. ADL 2 . 23 E - 04 ADL 4 . 50 E - 04 ADL 2 . 25 E - 04 A DL 3 . 00 E- 04 A r s e n i c , As m g/ d s cm , C o rr. ADL 1 . 51 E - 05 ADL 3 . 67 E - 04 ADL 1 . 74 E - 04 A DL 1 . 85 E- 04 B a r i u m , Ba m g/ d s cm , C o rr. ADL 1 . 17 E - 03 ADL 7 . 27 E - 04 ADL 4 . 83 E - 04 A DL 7 . 95 E- 04 B er y lli u m , Be m g/ d s cm , C o rr. B DL < 1 . 89 E - 04 B DL < 1 . 73 E - 04 B DL < 1 . 61 E - 04 B DL < 1 . 74 E- 04 C a d m i u m , Cd m g/ d s cm , C o rr. ADL 2 . 61 E - 04 ADL 1 . 21 E - 04 ADL 2 . 67 E - 04 A DL 2 . 17 E- 04 C hr o m i u m , Cr( T) m g/ d s cm , C o rr. ADL 3 . 03 E - 04 ADL 2 . 42 E - 04 ADL 3 . 54 E - 04 A DL 3 . 00 E- 04 C ob a lt, Co m g/ d s cm , C o rr. ADL 2 . 01 E - 04 ADL 7 . 96 E - 05 ADL 1 . 13 E - 04 A DL 1 . 31 E- 04 C opp er , Cu m g/ d s cm , C o rr. ADL 1 . 10 E - 03 ADL 7 . 62 E - 04 ADL 6 . 76 E - 04 A DL 8 . 45 E- 04 L e a d , Pb m g/ d s cm , C o rr. ADL 8 . 88 E - 03 ADL 9 . 51 E - 03 ADL 6 . 27 E - 03 A DL 8 . 22 E- 03 M a ng a n e s e , Mn m g/ d s cm , C o rr. B D Lb < 7 . 57 E - 0 5 B D Lb < 6 . 93 E - 0 5 B D Lb < 6 . 44 E - 05 B D Lb < 6 . 98 E- 05 M er c u r y , H g m g/ d s cm , C o rr. ADL 4 . 17 E + 00 ADL 3 . 05 E + 00 ADL 1 . 03 E + 01 A DL 5 . 84 E + 00 N i c k e l, Ni m g/ d s cm , C o rr. ADL 3 . 79 E - 05 ADL 2 . 15 E - 03 ADL 9 . 66 E - 04 A DL 1 . 05 E- 03 P ho s pho ru s , P m g/ d s cm , C o rr. ADL 1 . 02 E - 02 ADL 1 . 84 E - 02 ADL 1 . 19 E - 02 A DL 1 . 35 E- 02 S e l e n i u m , Se m g/ d s cm , C o rr. B DL < 7 . 57 E - 05 B DL < 6 . 93 E - 05 ADL 1 . 19 E - 03 B DL < 4 . 46 E- 04 S il v er , Ag m g/ d s cm , C o rr. B DL < 7 . 57 E - 05 B DL < 6 . 93 E - 05 B DL < 6 . 44 E - 05 B DL < 6 . 98 E- 05 T h a lli u m , Tl m g/ d s cm , C o rr. B DL < 7 . 57 E - 05 B DL < 6 . 93 E - 05 B DL < 6 . 44 E - 05 B DL < 6 . 98 E- 05 V a n a d i u m , V , ( a s V - p e n t ox i d e) m g/ d s cm , C o rr. B DL < 3 . 79 E - 04 B DL < 3 . 46 E - 04 B DL < 3 . 22 E - 04 B DL < 3 . 49 E- 04 Zi n c , Zn m g/ d s cm , C o rr. ADL 2 . 27 E - 04 ADL 4 . 36 E - 03 ADL 3 . 41 E - 03 A DL 2 . 67 E- 03 Ir on , Fe m g/ d s cm , C o rr. ADL 4 . 92 E - 03 ADL 3 . 18 E - 02 ADL 2 . 14 E - 02 A DL 1 . 94 E- 02 * P er f o r me d du r i ng i s o k i n e ti c s a m p li ng ( e . g . C A RB M e thod 436 ). ** M e a s u r e d v i a S C A Q M D M e thod 10 .1 B D L - B e l o w D e t ec ti on L e v e l, M R L i s r epo r t e d. AD L - A bov e D e t ec ti on L e v el B D L b - R e a g e n t b l a nk c o rr ec t e d r e s u lt s i s l e ss th a n B D L , B D L i s s u b s titu t e d. 

## M u l t i - M e t a l s CAR B 436

# Sp ec i a t e d T ox i c O rga n i c s T O - 15 F a c ilit y : E x i d e T e c hn o l og i es C it y : V e r n o n , CA S o u r c e : N e p t un e S c r ubb er T e s t D a t e : 9 / 14 / 2010 P ARA M ETER U n its D a ta D a ta D a ta R un N u m b er R un1 R un2 R un3 T e s t D a te m / d/y 9 / 14 / 2010 9 / 14 / 2010 9 / 14 / 2010 T e s t T i me h/m 12 : 38 : 12 : 58 13 : 15 : 13 : 45 13 : 56 - 14 : 26 S a m p li n g C o nd iti o ns S a m p li n g D a ta O x yg e n* % 15 .3 15 .3 15 .3 C a r b o n D i o x i d e* % 6 .8 6 .8 6 .8 S t a nd a r d T e m

p e r a t u r e , T s td o 

### C 25 25 25 S t a nd a r d P r e ss u r e , P s td A tm 1 1 1 S t a c k G a s F l o w R a t e * D S C FM 19 , 782 19 , 782 19 , 782 L a b o r a t o r y D a ta U n its R un3 B e n z e ne ppbv B DL 0 . 78 B DL 0 . 78 B DL 0 . 81 B DL 0 . 79 1 , 3 - B u t ad i e ne ppbv B DL 2 .4 B DL 2 .4 B DL 2 .4 B DL 2 . 40 N aph t ha l e ne ppbv B DL 16 B DL 16 B DL 16 B DL 16 . 00 C on ce n t r a t i on m g / d s cm B e n z e ne m g / d s cm B DL < 0 . 002490 B DL < 0 . 002490 B DL < 0 . 002586 B DL < 0 . 00252 1 , 3 - B u t ad i e ne m g / d s cm B DL < 0 . 005306 B DL < 0 . 005306 B DL < 0 . 005306 B DL < 0 . 00531 N aph t ha l e ne m g / d s cm B DL < 0 . 083817 B DL < 0 . 083817 B DL < 0 . 083817 B DL < 0 . 08382 C on ce n t r a t i on a t 7 %O2 m g / d s cm B e n z e ne m g / d s cm B DL < 0 . 006181 B DL < 0 . 006181 B DL < 0 . 006419 B DL < 0 . 00626 1 , 3 - B u t ad i e ne m g / d s cm B DL < 0 . 013171 B DL < 0 . 013171 B DL < 0 . 013171 B DL < 0 . 01317 N aph t ha l e ne m g / d s cm B DL < 0 . 208047 B DL < 0 . 208047 B DL < 0 . 208047 B DL < 0 . 20805 B D L - B e l o w D e t e c ti o n Le v e l, R L i s r e p o r t e d. * O 2 / C O 2 w a s m ea s u r e d v i a S C A Q M D M e t h o d 10 . 1. m g / d s c m = ( ppb v

/ 1000 ) * ( 12 . 187 ) * ( M W ) / ( 273 . 15+ o 

### C) S t a c k f l o w f r o m H C l t e s t R un #3 R un1 R un2 AV E R G AE