### Instructions for filling in the Emission Test Template

This Information Collection Request (ICR) spreadsheet is intended to collect information about emission data from fossil fuel burning power plants and which test methods were used to do so for cases where the test methods are not currently supported by the Electronic Reporting Tool (ERT). This spreadsheet should only be used if the method is not in the ERT or if you do not have access to a lab which performs methods that are in the ERT. You must complete at least 3 separate runs or sampling events for each of the requested constituents. This spreadsheet is intended to be used for one boiler of one facility. Data for multiple boilers should be handled by using separate copies of this spreadsheet. yellow are required. All cells that are shaded in green are populated using drop

-down lists. You do not need to populate cells shaded in gray, as they are automatically populated from the Boiler Information worksheet. resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_EmisTestMethods.xls (example: 8100_Unit_2_EmisTestMethods.xls).

Please refer to the following steps when using these spreadsheets.

Boiler Information Worksheet

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the control device configuration.

Emission Data Worksheets

The emission data worksheets are provided for each constituent or constituent family required for this analysis. On each spreadsheet, you must enter boiler operating information during sampling, fuel input information, and emission test results. There are generally 1 to 3 emission test results records to be entered depending on the constituent or constituent family. For example, CO only requires 1 record with 3 sample events, while Mercury requires that you enter both Hg Hg+2

### , or if the Ontario

- Hydro Method was used, you would need to enter Hg0

### , HgP, and Hg Volatile Organic HAP and Speciated Semi

-Volatile Organic HAP worksheets allow you to use a drop Constituent field to define as many records as needed to record each HAP that you have results for. General instructions follow for these worksheets:

Boiler Operation Information

1. Please provide the values of all requested parameters for each of test run/sample. 2. Please provide any other supporting information or comments in the Other Supporting Information field.

Fuel Information

1. Please enter what types of fuel are being used in your boiler using the drop

-downs in the Fuel Type Selection field. You may enter up to 4 fuel types. If you are not burning one or more of the fuel types entered in one or more samples, then enter an input rate of zero. 2. Please enter the unit of measure using the drop down provided. 3. Please enter the test method used to determine the fuel input rate. 4. Please provide any other information that you feel may be important in the Other Supporting Information field.

Emission Data

### 1. Some constituents ask for the emission rate results of each run in two different units of measure, while others do not. If emission rate results are requested in two different units of measure (ex. lb/MMBtu (Pounds per million BTU) and ppmvd @ 7% O 2 

### (parts per million by volume dry basis at 7 percent oxygen)), you are required to provide both. 2. Please provide the test method used. This may or may not match the example given in the Test Method Used field. Please ensure that the name includes the owning organization of the test method (ex. U.S. EPA Method 0010). 3. Please provide any other information that you feel may be important in the Other Supporting Information field. 4. If data sheets and QA/QC documentation tables are provided for the test method you are entering data for please also enter these data.

### This Information Collection Request (ICR) spreadsheet is intended to collect information about emission data from fossil fuel burning power plants and which test methods were used to do so for cases where the test methods are not currently supported by the Electronic Reporting Tool (ERT). This spreadsheet should only be used if the method is not in the ERT or if you do not have access to a lab which performs methods that are in the ERT. You must complete at least 3 separate This spreadsheet is intended to be used for one boiler of one facility. Data for multiple boilers should be handled by using separate copies of this spreadsheet. Fields shaded in down lists. You do not need to populate cells shaded in gray, as they are automatically populated from the Boiler Information worksheet. Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_EmisTestMethods.xls

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

The emission data worksheets are provided for each constituent or constituent family required for this analysis. On each spreadsheet, you must enter boiler operating information during sampling, fuel input information, and emission test results. There are generally 1 to 3 emission test results records to be entered depending on the constituent or constituent family. For example, CO only requires 1 record with 3 sample events, while Mercury requires that you enter both Hg0 

### and , HgP, and Hg+2 

### . However, both the Speciated Volatile Organic HAP worksheets allow you to use a drop

-down provided in the Constituent field to define as many records as needed to record each HAP that you have results for. General instructions

2. Please provide any other supporting information or comments in the Other Supporting Information field.

downs in the Fuel Type Selection field. You may enter up to 4 fuel types. If you are not burning one or more of the fuel types entered in one or more samples,

4. Please provide any other information that you feel may be important in the Other Supporting Information field.

### 1. Some constituents ask for the emission rate results of each run in two different units of measure, while others do not. If emission rate results are requested in two different units of measure (ex. lb/MMBtu (Pounds per million BTU) and

(parts per million by volume dry basis at 7 percent oxygen)), you are required to provide both. 2. Please provide the test method used. This may or may not match the example given in the Test Method Used field. Please ensure that the name includes the owning organization of the test method (ex. U.S. EPA Method 0010). 3. Please provide any other information that you feel may be important in the Other Supporting Information field. 4. If data sheets and QA/QC documentation tables are provided for the test method you are entering data for please alsoEIA

Facility Code Facility Name Boiler ID

6639 R D Green G2Control Device Configuraton

Listed (by

boiler) in the Configuration Order Section of the Facility Unit Configurations Section of the Electronic ICRListed (by boiler) in the Configuration Order Section of the Facility Unit Configurations Section of the Electronic ICREIA

Facility Code Facility Name Boiler ID

6639 R D Green G2

Run Number Test Start Date Test Start TimeMeasured Value (ppm) Test End Time Test End DateBasis (Wet or Dry) Test Method Used Data Flag (ADL, BDL, DDL) CO Emission Test ResultsTest Method Comments lb/mmBtu ppmdv @ 7% O 2 Calculated Emission RateSteam Output (1000 lb/hr) Total Heat Input (mmBtu/hr) Flue Gas Moisture (%)Flue Gas Flow Rate (dscfm) Flue Gas CO2(%) Flue Gas O2(%)Fuel Input Rate Fuel Type

Flue Gas Temperature (F) Fuel #1Units of Measure Measurement Method Fuel Input Rate Fuel #1Fuel Type Units of Measure Measurement Method Fuel #2Fuel Input Rate Fuel Type Units of Measure Fuel #3Measurement Method Fuel Input Rate Fuel Type Fuel #4Units of Measure Measurement Method Fuel #4 Other Supporting InformationEIA

Facility Code Facility Name Boiler ID 6639 R D Green G2

1 5/18/2010 6:43 5/18/2010 2 5/20/2010 6:48 5/20/2010 3 5/20/2010 9:25 5/20/2010 Run Number Test Start Date Test Start Time Test End DateMeasured Value (ppm) Basis (Wet or Dry) Test Method Used Data Flag (ADL, BDL, DDL) 9:00 <8.24E-03 Dry U.S. EPA Method 316 BDL 9:02 <8.16E-03 Dry U.S. EPA Method 316 BDL 11:37 <7.33E-02 Dry U.S. EPA Method 316 BDL Test End Time Formaldehyde Emission Test ResultsTest Method

Comments lb/mmBtu ppmdv @ 7% O 2

<9.53E-06 <8.06E-03 1188 2171 <9.47E-06 <8.14E-03 1117 2081 <8.26E-05 <6.95E-02 1117 2081 Steam Output (1000 lb/hr) Total Heat Input

(mmBtu/hr) Calculated Emission RateFuel Input Rate Fuel Type Units of Measure 13 11.3 6.68 662506 121 1679 bitum inous ton/day 12.7 11.3 6.96 646871 123 1615 bitum inous ton/day 13.1 12 6.24 645873 123 1615 bitum inous ton/day Flue Gas Temperature (F) Fuel #1 Flue Gas Moisture (%) Flue Gas

CO2(%) Flue Gas

O2(%) Flue Gas Flow

Rate (dscfm)Measurement

Method Fuel Input

Rate Fuel Type Units of Measure Measurement

Method Fuel Input

Rate Fuel Type Units of

Measure 545 petroleum coke

ton/day 466 petroleum coke

ton/day 466 petroleum coke

ton/day Fuel #2 Fuel #3Measurement

Method Fuel Input

Rate Fuel Type Units of

Measure Measurement

Method Fuel #4 Other Supporting InformationEIA

Facility Code Facility Name Boiler ID 6639 R D Green G2

1 5/18/2010 6:43 2 5/20/2010 6:48 3 5/20/2010 9:25 Run Number Test Start Date Test Start TimeMeasured Value (ppm) Basis (Wet or Dry)

5/18/2010 9:00 0.317 Dry 5/20/2010 9:02 0.305 Dry 5/20/2010 11:37 0.337 Dry

Test End Time Test End Date Methane Emission Test ResultsTest Method Used Data Flag (ADL, BDL, DDL) Test Method Comments lb/mmBtu

U.S. EPA Method 18 ADL 0.000196 U.S. EPA Method 18 ADL 0.000189 U.S. EPA Method 18 ADL 0.000203 Methane Emission Test Results Calculated Emission Rateppmdv @ 7% O2

0.31 1188 2171 13 11.3 6.68 662506 0.304 1117 2081 12.7 11.3 6.96 646871 0.32 1117 2081 13.1 12 6.24 645873 Flue Gas O2(%) Flue Gas

Flow Rate (dscfm) Calculated Emission Rate Steam Output (1000 lb/hr) Total Heat

Input (mmBtu/hr) Flue Gas

Moisture (%) Flue Gas CO2(%)Fuel Input Rate Fuel Type Units of

Measure Measurement

Method Fuel

Input Rate Fuel Type Units of

Measure

121 1679 bitum inous ton/day 545 petroleum coke ton/day 123 1615 bitum inous ton/day 466 petroleum coke ton/day 123 1615 bitum inous ton/day 466 petroleum coke ton/day Flue Gas Temperat ure (F) Fuel #1 Fuel #2Measurement

Method Fuel

Input Rate Fuel Type Units of

Measure Measurement

Method Fuel

Input Rate Fuel Type Units of

Measure Fuel #4 Fuel #3Measurement

Method Other Supporting InformationEIA

Facility Code Facility Name Boiler ID 6639 R D Green G2

Run Number Test Start Date Test Start Time Test End DateMeasured Value (ppm) Basis (Wet or Dry) Test Method Used Test End Time SO2Emission Test ResultsData Flag (ADL,

BDL, DDL) Test Method

Comments lb/mmBtu ppmdv @ 7% O 2 Calculated Emission Rate Steam Output (1000 lb/hr)Fuel Input Rate Fuel Type Flue Gas O2(%) Flue Gas

Flow Rate (dscfm) Total Heat Input (mmBtu/hr) Flue Gas

Moisture (%) Flue Gas

CO2(%) Flue Gas Temperature (F) Fuel #1Units of

Measure Measurement

Method Fuel Input

Rate Fuel Type Units of

Measure Measurement

Method Fuel Input

Rate Fuel Type Fuel #1 Fuel #2 Fuel #3Units of

Measure Measurement

Method Fuel Input

Rate Fuel Type Units of Measure Measurement

Method Fuel #4 Fuel #3Other Supporting InformationEIA

Facility Code Facility Name Boiler ID 6639 R D Green G2

1 5/18/2010 13:05 2 5/19/2010 7:15 3 5/19/2010 12:45 Run Number Test Start Date Test Start TimePlease note QA/QC documentation starting in Column "AI"

Measured Value (μg/dscm) Basis (Wet or Dry)

5/18/2010 15:05 3.1 Dry 5/19/2010 9:15 2.48 Dry 5/19/2010 14:45 2.1 Dry

Test End Time Test End Date Total Vapor Phase Mercury Emission Test ResultsPlease note QA/QC documentation starting in Column "AI"

Test Method Used Data Flag (ADL, BDL, DDL) Test Method

Comments (lb/mmBtu)

U.S. EPA Method 30B ADL 2.86E-06 1188 U.S. EPA Method 30B ADL 2.31E-06 1048 U.S. EPA Method 30B ADL 2.02E-06 1048 Steam Output (1000 lb/hr) Total Vapor Phase Mercury Emission Test ResultsFuel Input Rate

2171 12.1 11.5 6.58 654850 122 1679 2110 9.09 11.4 6.7 664700 122 1652 2110 12.4 11 7.06 645100 123 1652 Flue Gas Flow Rate (dscfm) Flue Gas

Temperature (F) Flue Gas O2(%) Total Heat Input (mmBtu/hr) Flue Gas CO2(%) Flue Gas Moisture (%)Fuel Type Units of Measure Measurement

Method Fuel Input

Rate Fuel Type Units of

Measure Measurement

Method Fuel Input

Rate

bitum inous ton/day 545 petroleum coke ton/day bitum inous ton/day 502 petroleum coke ton/day bitum inous ton/day 502 petroleum coke ton/day Fuel #1 Fuel #2Fuel Type Units of Measure Measurement

Method Fuel Input

Rate Fuel Type Units of Measure Measurement

Method Fuel #3 Fuel #4QA /QC Documentation

Trap ID Section 1

Mass (ng) Section 2

Mass (ng) Total

Mass (ng) Initial

Spike (ng) Total NonSpike (ng)

56766 395.11 5.663 401 0 401 59797 283.61 1.496 285 0 285 59793 263.25 1.573 265 0 265 Other Supporting InformationSample

Volume (dscm) Volume

Difference (%) Volume Diff. Limit Breaktrough

(%) Breaktrough

Limit Concentration

(μg/dscm) Trap ID

122 1.7 1.433271747 0.003286885 72572 121 0.8 0.527484926 0.002355372 72575 121 0.8 0.597530864 0.002190083 72565 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!

≤10% of Section 1 Hg

mass for Hg conc. >1

μg/dscm: or ≤ 20% of Section Trap #1

≤20% of field

recovery testSection 1

Mass Section 2

Mass Total

Mass Initial

Spike Total NonSpike Sample

Volume Volume

Difference (%) Volume Diff. Limit

843.6 10.85 854 500 354 122 1.7 809.6 1.526 811 500 311 120 0 741.7 1.686 743 500 243 121 0.8 ≤20% of field

recovery test Trap #2Breaktrough (%) Breaktrough Limit Concentration

(μg/dscm) Abs. diff. RD (%) Limit C rec

1.286154576 0.002901639 0.000385 6.225166 3.69 0.188488142 0.002591667 0.000236 4.776489 4.41 0.227315626 0.002008264 0.000182 4.330709 3.97 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! Measured Spike Recovery ( R ) Paired Trap Agreement (RD)

≥ 10 % RD mass for Hg conc. >1 μg/dscm: or

≤20% RD or ≤0.2 μg/dscm abs.diff. for Hg conc. ≤1 ≤10% of Section 1 Hg mass for Hg conc. >1

μg/dscm: or ≤ 20% of Section 1 for Hg conc. ≤1R (%) by

Run Ravg(%) Limit

90.3 106 95.8 Average Recovery

, between 85 and 115% Measured Spike Recovery ( R )

97.36666667EIA

Facility Code Facility Name Boiler ID 6639 R D Green G2

Run Number Test Start Date Test Start TimeMeasured Hg 0Value (μg/dscm) Measured Hg +2Value (μg/dscm) Test End Time Test End DateMeasured Hg PValue

(μg/dscm) Basis (Wet or Dry) Test Method Used Data Flag (ADL, BDL, DDL) Total Vapor Phase Mercury Emission Test ResultsTest Method

Comments Total Mercury (lb/mmBtu) Steam Output

(1000 lb/hr) Total Heat

Input (mmBtu/hr) Flue Gas

Moisture (%) Flue Gas

CO2(%)Fuel Input Rate Fuel Type Units of Measure Measurement

Method Fuel #1 Flue Gas O2(%) Flue Gas

Flow Rate (dscfm) Flue Gas

Temperature (F)Fuel Input Rate Fuel Type Units of Measure Measurement

Method Fuel Input

Rate Fuel Type Units of Measure Measurement

Method Fuel #2 Fuel #3Fuel Input

Rate Fuel Type Units of Measure Measurement

Method Other Supporting Information Fuel #4EIA

Facility Code Facility Name Boiler ID 6639 R D Green G2

Speciated Volatile Organic HAP Emission Data

Benzene 1 5/18/2010 Benzene 2 5/20/2010 Benzene 3 5/20/2010 Methyl bromide 1 5/18/2010 Methyl bromide 2 5/20/2010 Methyl bromide 3 5/20/2010 Carbon disulfide 1 5/18/2010 Carbon disulfide 2 5/20/2010 Carbon disulfide 3 5/20/2010 Carbon tetrachloride 1 5/18/2010 Carbon tetrachloride 2 5/20/2010 Carbon tetrachloride 3 5/20/2010 Chlorobenzene 1 5/18/2010 Chlorobenzene 2 5/20/2010 Chlorobenzene 3 5/20/2010 Chloroform 1 5/18/2010 Chloroform 2 5/20/2010 Chloroform 3 5/20/2010 Methyl chloride 1 5/18/2010 Methyl chloride 2 5/20/2010 Methyl chloride 3 5/20/2010 Ethylbenzene 1 5/18/2010 Ethylbenzene 2 5/20/2010 Ethylbenzene 3 5/20/2010 Cumene (isopropylbenzene) 1 5/18/2010 Cumene (isopropylbenzene) 2 5/20/2010 Cumene (isopropylbenzene) 3 5/20/2010 Methylene chloride 1 5/18/2010 Methylene chloride 2 5/20/2010 Methylene chloride 3 5/20/2010 Styrene 1 5/18/2010 Styrene 2 5/20/2010 Styrene 3 5/20/2010 Tetrachloroethylene 1 5/18/2010 Tetrachloroethylene 2 5/20/2010 Tetrachloroethylene 3 5/20/2010 Toluene 1 5/18/2010 Toluene 2 5/20/2010 Toluene 3 5/20/2010 Methyl chloroform (1,1,1-trichloroethane) 1 5/18/2010 Methyl chloroform (1,1,1-trichloroethane) 2 5/20/2010 Methyl chloroform (1,1,1-trichloroethane) 3 5/20/2010 m-Xylene 1 5/18/2010 m-Xylene 2 5/20/2010 m-Xylene 3 5/20/2010 o-Xylene 1 5/18/2010 o-Xylene 2 5/20/2010

Compound (use drop down to define for as many rows as

needed) Run Number Test Start Dateo-Xylene 3 5/20/2010Measured Value (μg/m3) 6:43 AM 5/18/2010 8:25 AM [<0.411] 6:48 AM 5/20/2010 8:29 AM [<0.582] 9:25 AM 5/20/2010 10:38 AM [<0.671] 6:43 AM 5/18/2010 8:25 AM [<1.09] 6:48 AM 5/20/2010 8:29 AM [<1.17] 9:25 AM 5/20/2010 10:38 AM [<0.974] 6:43 AM 5/18/2010 8:25 AM [<140] 6:48 AM 5/20/2010 8:29 AM 169 9:25 AM 5/20/2010 10:38 AM 228 6:43 AM 5/18/2010 8:25 AM [<0.217] 6:48 AM 5/20/2010 8:29 AM [<0.348] 9:25 AM 5/20/2010 10:38 AM [<0.213] 6:43 AM 5/18/2010 8:25 AM <0.155 6:48 AM 5/20/2010 8:29 AM [<0.145] 9:25 AM 5/20/2010 10:38 AM [<0.162] 6:43 AM 5/18/2010 8:25 AM [<0.373] 6:48 AM 5/20/2010 8:29 AM [<0.473] 9:25 AM 5/20/2010 10:38 AM [<0.598] 6:43 AM 5/18/2010 8:25 AM [<28.1] 6:48 AM 5/20/2010 8:29 AM 15.4 9:25 AM 5/20/2010 10:38 AM [<10.9] 6:43 AM 5/18/2010 8:25 AM <0.118 6:48 AM 5/20/2010 8:29 AM [<0.184] 9:25 AM 5/20/2010 10:38 AM <0.125 6:43 AM 5/18/2010 8:25 AM <0.119 6:48 AM 5/20/2010 8:29 AM [<0.117] 9:25 AM 5/20/2010 10:38 AM <0.122 6:43 AM 5/18/2010 8:25 AM 2.22 6:48 AM 5/20/2010 8:29 AM 2.66 9:25 AM 5/20/2010 10:38 AM 2.16 6:43 AM 5/18/2010 8:25 AM <0.168 6:48 AM 5/20/2010 8:29 AM [<0.156] 9:25 AM 5/20/2010 10:38 AM [<0.162] 6:43 AM 5/18/2010 8:25 AM <0.138 6:48 AM 5/20/2010 8:29 AM [<0.167] 9:25 AM 5/20/2010 10:38 AM <0.142 6:43 AM 5/18/2010 8:25 AM [<0.304] 6:48 AM 5/20/2010 8:29 AM <0.943 9:25 AM 5/20/2010 10:38 AM 0.713 6:43 AM 5/18/2010 8:25 AM <0.140 6:48 AM 5/20/2010 8:29 AM [<0.132] 9:25 AM 5/20/2010 10:38 AM <0.143 6:43 AM 5/18/2010 8:25 AM <0.221 6:48 AM 5/20/2010 8:29 AM [<0.357] 9:25 AM 5/20/2010 10:38 AM <0.222 6:43 AM 5/18/2010 8:25 AM <0.125 6:48 AM 5/20/2010 8:29 AM <0.166 Test Start Time Test End Date Test End Time9:25 AM 5/20/2010 10:38 AM <0.128Footnotes:

* Front half fraction contains filter, cyclone, and cartridge ** Back half fraction contains condensate, solvent, impingers

Basis Test Method Used Data Flag (ADL, BDL, DDL) Front Half Mass (ng)

Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B ADL Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B BDL Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B ADL Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B BDL Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B BDL Dry U.S. EPA Method 0031 with SW -846 Method 8260B BDL Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B BDL Dry U.S. EPA Method 0031 with SW -846 Method 8260B ADL Dry U.S. EPA Method 0031 with SW -846 Method 8260B ADL Dry U.S. EPA Method 0031 with SW -846 Method 8260B ADL Dry U.S. EPA Method 0031 with SW -846 Method 8260B BDL Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B BDL Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B BDL Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B BDL Dry U.S. EPA Method 0031 with SW -846 Method 8260B ADL Dry U.S. EPA Method 0031 with SW -846 Method 8260B BDL Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B BDL Dry U.S. EPA Method 0031 with SW -846 Method 8260B BDL Dry U.S. EPA Method 0031 with SW -846 Method 8260B DLL Dry U.S. EPA Method 0031 with SW -846 Method 8260B BDL Dry U.S. EPA Method 0031 with SW -846 Method 8260B BDL Dry U.S. EPA Method 0031 with SW -846 Method 8260B BDLDry U.S. EPA Method 0031 with SW -846 Method 8260B BDLBack Half Mass (ng) Total Mass (ng) Test Method Comments lb/mmBtu

[<0.0252] <0.0035, 0.0045, 0.0056, <0.0035, 0.0037, <0.0035, <0.0009 [<3.81E-07] [<0.0473] 0.01, 0.0055, <0.0035, 0.011, 0.0059, <0.0035, <0.0035, <0.0035, <0.0009 [<5.41E-07] [<0.0403] 0.046, 0.0055, 0.01, <0.0035, 0.0096, 0.0062, <0.0009 [<6.06E-07] [<0.0668] 0.012, 0.0088, <0.0059, 0.017, 0.0087, 0.0092, <0.0052 [<1.01E-06] [<0.0950] 0.01, 0.014, <0.0059, 0.015, <0.0059, 0.017, 0.01, 0.012, <0.0052 [<1.09E-06] [<0.0585] 0.0072, 0.0092, 0.019, <0.0059, <0.0059, 0.0061, <0.0052 [<8.79E-07] [<8.61] .015, 4.3, 4.1, <0.0019, 0.041, .14, 0.0084 [<1.30E-04] 13.8 1.57E-04 13.7 2.05E-04 [<0.0133] <0.0012, .003, .0035, <0.0012, <0.0012,<0.0012,<0.002 [<2.01E-07] [<0.0283] 0.012, 0.0033, <0.0012, 0.002, 0.0042, <0.0012, <0.0012, <0.0012, <.002 [<3.23E-07] [<0.0128] .0025, 0.0023, 0.0024, <0.0012, <0.0012, <0.0012, <0.002 [<1.92E-07] <0.00950 <1.43E-07 [<0.0118] (<0.001, 0.0011, 0.0017, 0.0023, <0.0010, <0.0010, .0012, <0.0010, <0.0015) [<1.35E-07] [<0.0097] (<0.0010, 0.0018, 0.0015, <0.0010, 0.0019, <0.0010, <0.0015) [<1.46E-07] [<0.0229] (<0.0011, 0.0061, 0.0064, <0.0011, <0.0011, <0.0011, .006) [<3.46E-07] [<0.0385] (0.0086, 0.0088, <0.0011, 0.011, <0.0011, <0.0011, <0.0011, <0.0011, 0.0046) [<4.40E-07] [<0.0359] (0.0082, 0.0082, 0.012, <0.0011, <0.0011, <0.0011, 0.00420) [<5.39E-07] [<1.72] (0.008, 0.0055, 0.0064, 1.5, 0.06, 0.14, <0.0024) [<2.60E-05] 1.25 1.43E-05 [<0.656] (0.0027, 0.0044, 0.012, 0.014, 0.5, 0.12, <0.0024) [<9.85E-06] <0.0073 <1.10E-07 [<0.0150] (0.0051, <0.0010, <0.0010, 0.0013, 0.0021, <0.0010, <0.0010, <0.0010, <0.0013) [<1.71E-07] <0.0075 <1.12E-07 <0.0073 <1.10E-07 [<0.0095] (0.0012, <0.0010, <0.0010, <0.0010, <0.0010, <0.0010, <0.0010, <0.0010, <0.0013) [<1.09E-07] <0.0073 <1.10E-07 0.136 2.06E-06 0.216 2.47E-06 0.130 1.95E-06 <0.0103 1.55E-07 [<0.0127] (0.0016, <0.0013, <0.0013, 0.0018, <0.0013, <0.0013, <0.0013, <0.0013, <0.0015) [<1.45E-07] [<0.0097] (<0.0013, <0.0013, <0.0013, <0.0013, 0.0014, 0.0016, <0.0015) [<1.46E-07] <0.0085 1.28E-07 [<0.0136] (0.0037, <0.0011, <0.0011, <0.0011, 0.0014, <0.0011, <0.0011, <0.0011, <0.0019) [<1.55E-07] <0.0085 1.28E-07 [<0.0186] (0.0024, 0.004, 0.0061, 0.0017, 0.0011, 0.0016, <0.0017) [<2.81E-07] 0.0767 <8.77E-07 0.0428 6.43E-07 <0.00860 1.30E-07 [<0.0107] (0.0011, <0.0010, <0.0010, <0.0010, <0.0010, <0.0010, <0.0010, <0.0010, <0.0026) [<1.22E-07] <0.00860 1.29E-07 <0.0135 <2.04E-07 [<0.0290] (0.011, <0.0020, <0.0020, <0.0020, 0.0047, <0.0020, <0.0020, <0.0020, <0.0013) [<3.32E-07] <0.0133 2.00E-07 <0.0077 1.16E-07 <0.0135 <1.54E-07 Calculated Emission Rate<0.0077 <1.16E-07ug/dscm @ 7% O2

[<0.402] 1188 2171 12.4 [<0.580] 1117 2081 12.5 [<0.637] 1117 2081 12.5 [<1.06] 1188 2171 12.4 [<1.16] 1117 2081 12.5 [<0.924] 1117 2081 12.5 [<137] 1188 2171 12.4 169 1117 2081 12.5 216 1117 2081 12.5 [<0.212] 1188 2171 12.4 [<0.347] 1117 2081 12.5 [<0.202] 1117 2081 12.5 <0.151 1188 2171 12.4 [<0.145] 1117 2081 12.5 [<0.153] 1117 2081 12.5 [<0.365] 1188 2171 12.4 [<0.472] 1117 2081 12.5 [<0.567] 1117 2081 12.5 [<27.4] 1188 2171 12.4 15.4 1117 2081 12.5 [<10.3] 1117 2081 12.5 <0.116 1188 2171 12.4 [<0.183] 1117 2081 12.5 <0.118 1117 2081 12.5 <0.116 1188 2171 12.4 [<0.117] 1117 2081 12.5 <0.115 1117 2081 12.5 2.17 1188 2171 12.4 2.65 1117 2081 12.5 2.05 1117 2081 12.5 <0.164 1188 2171 12.4 [<0.156] 1117 2081 12.5 [<0.153] 1117 2081 12.5 <0.135 1188 2171 12.4 [<0.166] 1117 2081 12.5 <0.134 1117 2081 12.5 [<0.297] 1188 2171 12.4 <0.940 1117 2081 12.5 0.676 1117 2081 12.5 <0.137 1188 2171 12.4 [<0.131] 1117 2081 12.5 <0.136 1117 2081 12.5 <0.216 1188 2171 12.4 [<0.356] 1117 2081 12.5 <0.210 1117 2081 12.5 <0.123 1188 2171 12.4 <0.165 1117 2081 12.5 Calculated Emission Rate Steam Output (1000 lb/hr) Total Heat Input (mmBtu/hr) Flue Gas Moisture (%)<0.122 1117 2081 12.511.3 6.68 651500 123 11.3 6.96 641000 123 12 6.24 641700 123 11.3 6.68 651500 123 11.3 6.96 641000 123 12 6.24 641700 123 11.3 6.68 651500 123 11.3 6.96 641000 123 12 6.24 641700 123 11.3 6.68 651500 123 11.3 6.96 641000 123 12 6.24 641700 123 11.3 6.68 651500 123 11.3 6.96 641000 123 12 6.24 641700 123 11.3 6.68 651500 123 11.3 6.96 641000 123 12 6.24 641700 123 11.3 6.68 651500 123 11.3 6.96 641000 123 12 6.24 641700 123 11.3 6.68 651500 123 11.3 6.96 641000 123 12 6.24 641700 123 11.3 6.68 651500 123 11.3 6.96 641000 123 12 6.24 641700 123 11.3 6.68 651500 123 11.3 6.96 641000 123 12 6.24 641700 123 11.3 6.68 651500 123 11.3 6.96 641000 123 12 6.24 641700 123 11.3 6.68 651500 123 11.3 6.96 641000 123 12 6.24 641700 123 11.3 6.68 651500 123 11.3 6.96 641000 123 12 6.24 641700 123 11.3 6.68 651500 123 11.3 6.96 641000 123 12 6.24 641700 123 11.3 6.68 651500 123 11.3 6.96 641000 123 12 6.24 641700 123 11.3 6.68 651500 123 11.3 6.96 641000 123

Flue Gas O2(%) Flue Gas Flow Rate (scfm) Flue Gas Temperature (F) Flue Gas CO2(%)12 6.24 641700 123Fuel Input Rate Fuel Type Units of Measure Measurement Method

1679 bitum inous ton/day 1615 bitum inous ton/day 1615 bitum inous ton/day 1679 bitum inous ton/day 1615 bitum inous ton/day 1615 bitum inous ton/day 1679 bitum inous ton/day 1615 bitum inous ton/day 1615 bitum inous ton/day 1679 bitum inous ton/day 1615 bitum inous ton/day 1615 bitum inous ton/day 1679 bitum inous ton/day 1615 bitum inous ton/day 1615 bitum inous ton/day 1679 bitum inous ton/day 1615 bitum inous ton/day 1615 bitum inous ton/day 1679 bitum inous ton/day 1615 bitum inous ton/day 1615 bitum inous ton/day 1679 bitum inous ton/day 1615 bitum inous ton/day 1615 bitum inous ton/day 1679 bitum inous ton/day 1615 bitum inous ton/day 1615 bitum inous ton/day 1679 bitum inous ton/day 1615 bitum inous ton/day 1615 bitum inous ton/day 1679 bitum inous ton/day 1615 bitum inous ton/day 1615 bitum inous ton/day 1679 bitum inous ton/day 1615 bitum inous ton/day 1615 bitum inous ton/day 1679 bitum inous ton/day 1615 bitum inous ton/day 1615 bitum inous ton/day 1679 bitum inous ton/day 1615 bitum inous ton/day 1615 bitum inous ton/day 1679 bitum inous ton/day 1615 bitum inous ton/day 1615 bitum inous ton/day 1679 bitum inous ton/day 1615 bitum inous ton/day Fuel #11615 bitum inous ton/dayFuel Input Rate Fuel Type Units of Measure Measurement Method

545 petroleum coke ton/day 466 petroleum coke ton/day 466 petroleum coke ton/day 545 petroleum coke ton/day 466 petroleum coke ton/day 466 petroleum coke ton/day 545 petroleum coke ton/day 466 petroleum coke ton/day 466 petroleum coke ton/day 545 petroleum coke ton/day 466 petroleum coke ton/day 466 petroleum coke ton/day 545 petroleum coke ton/day 466 petroleum coke ton/day 466 petroleum coke ton/day 545 petroleum coke ton/day 466 petroleum coke ton/day 466 petroleum coke ton/day 545 petroleum coke ton/day 466 petroleum coke ton/day 466 petroleum coke ton/day 545 petroleum coke ton/day 466 petroleum coke ton/day 466 petroleum coke ton/day 545 petroleum coke ton/day 466 petroleum coke ton/day 466 petroleum coke ton/day 545 petroleum coke ton/day 466 petroleum coke ton/day 466 petroleum coke ton/day 545 petroleum coke ton/day 466 petroleum coke ton/day 466 petroleum coke ton/day 545 petroleum coke ton/day 466 petroleum coke ton/day 466 petroleum coke ton/day 545 petroleum coke ton/day 466 petroleum coke ton/day 466 petroleum coke ton/day 545 petroleum coke ton/day 466 petroleum coke ton/day 466 petroleum coke ton/day 545 petroleum coke ton/day 466 petroleum coke ton/day 466 petroleum coke ton/day 545 petroleum coke ton/day 466 petroleum coke ton/day Fuel #2466 petroleum coke ton/dayFuel Input Rate Fuel Type Units of Measure Measurement Method Fuel #3Fuel Input Rate Fuel Type Units of Measure Measurement Method Fuel #4Other Supporting

InformationEIA

Facility Code Facility Name 6639 R D Green

Speciated Semi-Volatile Organic HAP Emission Data

Acenaphthene 1 Acenaphthene 2 Acenaphthene 3 Acenaphthylene 1 Acenaphthylene 2 Acenaphthylene 3 Acetophenone 1 Acetophenone 2 Acetophenone 3 Anthracene 1 Anthracene 2 Anthracene 3 Benzo(a)anthracene 1 Benzo(a)anthracene 2 Benzo(a)anthracene 3 Benzo(b)fluoranthene 1 Benzo(b)fluoranthene 2 Benzo(b)fluoranthene 3 Benzo(k)fluoranthene 1 Benzo(k)fluoranthene 2 Benzo(k)fluoranthene 3 Benzoic acid 1 Benzoic acid 2 Benzoic acid 3 Benzo(g,h,i)perylene 1 Benzo(g,h,i)perylene 2 Benzo(g,h,i)perylene 3 Benzo(a)pyrene 1 Benzo(a)pyrene 2 Benzo(a)pyrene 3 Benzo(e)pyrene 1 Benzo(e)pyrene 2 Benzo(e)pyrene 3 Bis(2-ethylhexyl) phthalate 1 Bis(2-ethylhexyl) phthalate 2 Bis(2-ethylhexyl) phthalate 3 Chrysene 1 Chrysene 2 Chrysene 3 Di-n-octyl phthalate 1 Di-n-octyl phthalate 2 Di-n-octyl phthalate 3 Fluoranthene 1 Fluoranthene 2 Fluoranthene 3 Fluorene 1 Fluorene 2

Compound (use drop down to define for as many rows as

needed) Run NumberFluorene 3

Indeno(1,2,3-cd)pyrene 1 Indeno(1,2,3-cd)pyrene 2 Indeno(1,2,3-cd)pyrene 3 2-Methylnaphthalene 1 2-Methylnaphthalene 2 2-Methylnaphthalene 3 Naphthalene 1 Naphthalene 2 Naphthalene 3 Phenanthrene 1 Phenanthrene 2 Phenanthrene 3 Phenol 1 Phenol 2 Phenol 3 Pyrene 1 Pyrene 2 Pyrene 3Boiler ID

G2

5/18/2010 6:43 AM 5/18/2010

5/20/2010 6:48 AM 5/20/2010 5/20/2010 9:25 AM 5/20/2010 5/18/2010 6:43 AM 5/18/2010 5/20/2010 6:48 AM 5/20/2010 5/20/2010 9:25 AM 5/20/2010 5/18/2010 6:43 AM 5/18/2010 5/20/2010 6:48 AM 5/20/2010 5/20/2010 9:25 AM 5/20/2010 5/18/2010 6:43 AM 5/18/2010 5/20/2010 6:48 AM 5/20/2010 5/20/2010 9:25 AM 5/20/2010 5/18/2010 6:43 AM 5/18/2010 5/20/2010 6:48 AM 5/20/2010 5/20/2010 9:25 AM 5/20/2010 5/18/2010 6:43 AM 5/18/2010 5/20/2010 6:48 AM 5/20/2010 5/20/2010 9:25 AM 5/20/2010 5/18/2010 6:43 AM 5/18/2010 5/20/2010 6:48 AM 5/20/2010 5/20/2010 9:25 AM 5/20/2010 5/18/2010 6:43 AM 5/18/2010 5/20/2010 6:48 AM 5/20/2010 5/20/2010 9:25 AM 5/20/2010 5/18/2010 6:43 AM 5/18/2010 5/20/2010 6:48 AM 5/20/2010 5/20/2010 9:25 AM 5/20/2010 5/18/2010 6:43 AM 5/18/2010 5/20/2010 6:48 AM 5/20/2010 5/20/2010 9:25 AM 5/20/2010 5/18/2010 6:43 AM 5/18/2010 5/20/2010 6:48 AM 5/20/2010 5/20/2010 9:25 AM 5/20/2010 5/18/2010 6:43 AM 5/18/2010 5/20/2010 6:48 AM 5/20/2010 5/20/2010 9:25 AM 5/20/2010 5/18/2010 6:43 AM 5/18/2010 5/20/2010 6:48 AM 5/20/2010 5/20/2010 9:25 AM 5/20/2010 5/18/2010 6:43 AM 5/18/2010 5/20/2010 6:48 AM 5/20/2010 5/20/2010 9:25 AM 5/20/2010 5/18/2010 6:43 AM 5/18/2010 5/20/2010 6:48 AM 5/20/2010 5/20/2010 9:25 AM 5/20/2010 5/18/2010 6:43 AM 5/18/2010 5/20/2010 6:48 AM 5/20/2010 Test Start Date Test Start Time Test End Date5/20/2010 9:25 AM 5/20/2010 5/18/2010 6:43 AM 5/18/2010 5/20/2010 6:48 AM 5/20/2010 5/20/2010 9:25 AM 5/20/2010 5/18/2010 6:43 AM 5/18/2010 5/20/2010 6:48 AM 5/20/2010 5/20/2010 9:25 AM 5/20/2010 5/18/2010 6:43 AM 5/18/2010 5/20/2010 6:48 AM 5/20/2010 5/20/2010 9:25 AM 5/20/2010 5/18/2010 6:43 AM 5/18/2010 5/20/2010 6:48 AM 5/20/2010 5/20/2010 9:25 AM 5/20/2010 5/18/2010 6:43 AM 5/18/2010 5/20/2010 6:48 AM 5/20/2010 5/20/2010 9:25 AM 5/20/2010 5/18/2010 6:43 AM 5/18/2010 5/20/2010 6:48 AM 5/20/2010 5/20/2010 9:25 AM 5/20/2010Footnotes: * Front Half Composite contains particulate filter, front half of the filter holder, and probe solvent rinses ** Back Half Composite contains XAD-2 resin tube, back half of the filter holder, and coil condenser solvent rinses *** Condensate Composite contains condensate and Impinger contents and the glassware solvent rinses

Measured Value (μg/m3) Basis (Wet or Dry)

9:00 AM [<0.0150] Dry 9:02 AM [<0.0500] Dry 11:37 AM [<0.0428] Dry 9:00 AM [<0.00579] Dry 9:02 AM [<0.0121] Dry 11:37 AM [<0.0135] Dry 9:00 AM [<0.00350] Dry 9:02 AM [<0.00294] Dry 11:37 AM [<0.00429] Dry 9:00 AM [<0.0140] Dry 9:02 AM [<0.0361] Dry 11:37 AM [<0.0316] Dry 9:00 AM [<0.00621] Dry 9:02 AM [<0.01085] Dry 11:37 AM [<0.0133] Dry 9:00 AM [<0.00882] Dry 9:02 AM [<0.01064] Dry 11:37 AM [<0.01167] Dry 9:00 AM [<0.0461] Dry 9:02 AM [<0.0468] Dry 11:37 AM [<0.0474] Dry 9:00 AM [<0.0939] Dry 9:02 AM [<0.0775] Dry 11:37 AM [<0.0971] Dry 9:00 AM [<0.0144] Dry 9:02 AM [<0.00909] Dry 11:37 AM [<0.00790] Dry 9:00 AM [<0.00673] Dry 9:02 AM [<0.00842] Dry 11:37 AM [<0.01085] Dry 9:00 AM [<0.00939] Dry 9:02 AM [<0.0129] Dry 11:37 AM [<0.0206] Dry 9:00 AM <0.01127 Dry 9:02 AM [<0.0178] Dry 11:37 AM [<0.0152] Dry 9:00 AM [<0.0143] Dry 9:02 AM [<0.0261] Dry 11:37 AM [<0.0410] Dry 9:00 AM [<0.00819] Dry 9:02 AM <0.00475 Dry 11:37 AM <0.00475 Dry 9:00 AM [<0.0933] Dry 9:02 AM [<0.126] Dry 11:37 AM [<0.152] Dry 9:00 AM [<0.0464] Dry 9:02 AM [<0.128] Dry Test End Time11:37 AM [<0.1183] Dry 9:00 AM [<0.00381] Dry 9:02 AM [<0.00356] Dry 11:37 AM [<0.00367] Dry 9:00 AM [<0.0632] Dry 9:02 AM [<0.1028] Dry 11:37 AM [<0.1028] Dry 9:00 AM [<0.282] Dry 9:02 AM [<0.291] Dry 11:37 AM [<0.343] Dry 9:00 AM [<0.280] Dry 9:02 AM [<0.579] Dry 11:37 AM [<0.693] Dry 9:00 AM [<0.00397] Dry 9:02 AM [<0.00346] Dry 11:37 AM [<0.00449] Dry 9:00 AM [<0.0540] Dry 9:02 AM [<0.0828] Dry 11:37 AM [<0.0922] Dry* Front Half Composite contains particulate filter, front half of the filter holder, and probe solvent rinses ** Back Half Composite contains XAD-2 resin tube, back half of the filter holder, and coil condenser solvent rinses *** Condensate Composite contains condensate and Impinger contents and the glassware solvent rinses

Test Method Used Data Flag (ADL, BDL, DDL) Front Half mass* (ng)

U.S. EPA Method 0010 with SW -846 Method 8270C 16.0 U.S. EPA Method 0010 with SW -846 Method 8270C 81.0 U.S. EPA Method 0010 with SW -846 Method 8270C 65.0 U.S. EPA Method 0010 with SW -846 Method 8270C 7.6 U.S. EPA Method 0010 with SW -846 Method 8270C 15.0 U.S. EPA Method 0010 with SW -846 Method 8270C 18.0 U.S. EPA Method 0010 with SW -846 Method 8270C <1.1 U.S. EPA Method 0010 with SW -846 Method 8270C <1.1 U.S. EPA Method 0010 with SW -846 Method 8270C <1.1 U.S. EPA Method 0010 with SW -846 Method 8270C 21.0 U.S. EPA Method 0010 with SW -846 Method 8270C 64.0 U.S. EPA Method 0010 with SW -846 Method 8270C 52.0 U.S. EPA Method 0010 with SW -846 Method 8270C 5.9 U.S. EPA Method 0010 with SW -846 Method 8270C 15.0 U.S. EPA Method 0010 with SW -846 Method 8270C 19.0 U.S. EPA Method 0010 with SW -846 Method 8270C 7.3 U.S. EPA Method 0010 with SW -846 Method 8270C 11.0 U.S. EPA Method 0010 with SW -846 Method 8270C 13.0 U.S. EPA Method 0010 with SW -846 Method 8270C 4.4 U.S. EPA Method 0010 with SW -846 Method 8270C 6.6 U.S. EPA Method 0010 with SW -846 Method 8270C 7.8 U.S. EPA Method 0010 with SW -846 Method 8270C <30 U.S. EPA Method 0010 with SW -846 Method 8270C <30 U.S. EPA Method 0010 with SW -846 Method 8270C <30 U.S. EPA Method 0010 with SW -846 Method 8270C <5.6 U.S. EPA Method 0010 with SW -846 Method 8270C <5.6 U.S. EPA Method 0010 with SW -846 Method 8270C 6.5 U.S. EPA Method 0010 with SW -846 Method 8270C 7.1 U.S. EPA Method 0010 with SW -846 Method 8270C 11.0 U.S. EPA Method 0010 with SW -846 Method 8270C 16.0 U.S. EPA Method 0010 with SW -846 Method 8270C 6.7 U.S. EPA Method 0010 with SW -846 Method 8270C 16.0 U.S. EPA Method 0010 with SW -846 Method 8270C 23.0 U.S. EPA Method 0010 with SW -846 Method 8270C <3.4 U.S. EPA Method 0010 with SW -846 Method 8270C 6.3 U.S. EPA Method 0010 with SW -846 Method 8270C 8.2 U.S. EPA Method 0010 with SW -846 Method 8270C 14 U.S. EPA Method 0010 with SW -846 Method 8270C 30 U.S. EPA Method 0010 with SW -846 Method 8270C 41 U.S. EPA Method 0010 with SW -846 Method 8270C 9.9 U.S. EPA Method 0010 with SW -846 Method 8270C <3.4 U.S. EPA Method 0010 with SW -846 Method 8270C <3.4 U.S. EPA Method 0010 with SW -846 Method 8270C 130 U.S. EPA Method 0010 with SW -846 Method 8270C 180 U.S. EPA Method 0010 with SW -846 Method 8270C 230 U.S. EPA Method 0010 with SW -846 Method 8270C 62 U.S. EPA Method 0010 with SW -846 Method 8270C 200 Semi-Volatile Organic HAP Emission Test ResultsU.S. EPA Method 0010 with SW -846 Method 8270C 190

U.S. EPA Method 0010 with SW -846 Method 8270C 2.0 U.S. EPA Method 0010 with SW -846 Method 8270C 3.1 U.S. EPA Method 0010 with SW -846 Method 8270C 3.3 U.S. EPA Method 0010 with SW -846 Method 8270C 42 U.S. EPA Method 0010 with SW -846 Method 8270C 100 U.S. EPA Method 0010 with SW -846 Method 8270C 99 U.S. EPA Method 0010 with SW -846 Method 8270C 48 U.S. EPA Method 0010 with SW -846 Method 8270C 72 U.S. EPA Method 0010 with SW -846 Method 8270C 62 U.S. EPA Method 0010 with SW -846 Method 8270C 420 U.S. EPA Method 0010 with SW -846 Method 8270C 950 U.S. EPA Method 0010 with SW -846 Method 8270C 1100 U.S. EPA Method 0010 with SW -846 Method 8270C <2.4 U.S. EPA Method 0010 with SW -846 Method 8270C <2.4 U.S. EPA Method 0010 with SW -846 Method 8270C <2.4 U.S. EPA Method 0010 with SW -846 Method 8270C <68 U.S. EPA Method 0010 with SW -846 Method 8270C <98 U.S. EPA Method 0010 with SW -846 Method 8270C <120Back Half mass* (ng) Condensate Mass*** (ng) Total Composite (ng)

8.0 <4.8 [<28.8] 11.0 <4.8 [<96.8] 13.0 <4.8 [<82.8] 3.2 <0.30 [<11.1] 8.1 <0.30 [<23.4] 7.9 <0.30 [<26.2] 3.6 <2.0 [<6.70] 2.6 <2.0 [<5.70] <1.9 5.3 [<8.30] <4.4 <1.4 [<26.8] <4.4 <1.4 [<69.8] 7.7 <1.4 [<61.1] <3.0 <3.0 [<11.9] <3.0 <3.0 [<21.0] 3.7 <3.0 [<25.7] <6.6 <3.0 [<16.9] <6.6 <3.0 [<20.6] <6.6 <3.0 [<22.6] <82.00 <2.00 [<88.4] <82.00 <2.00 [<90.6] <82.00 <2.00 [<91.8] 100 <50 [<180] 70 <50 [<150] <38 120 [<188] 21.0 <1.0 [<27.6] 11.0 <1.0 [<17.6] 7.8 <1.0 [<15.3] 5.0 <0.8 [<12.9] 4.5 <0.8 [<16.3] 4.2 <0.8 [<21.0] 8.5 <2.8 [<18.0] 6.2 <2.8 [<25.0] 14.0 <2.8 [<39.8] <15.0 <3.2 <21.6 25 <3.2 [<34.5] 18 <3.2 [<29.4] 13 0.46 [<27.5] 20 <0.4 [<50.4] 38 <0.4 [<79.4] <3.6 <2.2 [<15.7] <3.6 <2.2 <9.20 <3.6 <2.2 <9.20 44 <4.8 [<179] 59 <4.8 [<244] 60 <4.8 [<295] 24 <3.0 [<89.0] 45 <3.0 [<248] Semi-Volatile Organic HAP Emission Test Results36 <3.0 [<229] 3.3 <2.0 [<7.30] <1.8 <2.0 [<6.90] <1.8 <2.0 [<7.10] 62 <17.0 [<121] 82 <17.0 [<199] 83 <17.0 [<199] <460 <32.0 [<540] <460 <32.0 [<564] 570 <32.0 [<664] 95 <22.0 [<537] 150 <22.0 [<1122] 220 <22.0 [<1342] 3.2 <2.0 [<7.60] 2.3 <2.0 [<6.70] 4.3 <2.0 [<8.70] 32 <3.4 [<103] 59 <3.4 [<160] 55 <3.4 [<178]Test Method Comments lb/mmBtu ug/dscm @ 7% O2

[<1.39E-08] [<0.0147] [<4.65E-08] [<0.0499] [<3.86E-08] [<0.0406] [<5.37E-09] [<0.00566] [<1.12E-08] [<0.0121] [<1.22E-08] [<0.0128] [<3.24E-09] [<0.00342] [<2.74E-09] [<0.00294] [<3.87E-09] [<0.00407] [<1.30E-08] [<0.0137] [<3.35E-08] [<0.0360] [<2.85E-08] [<0.0299] [<5.75E-09] [<0.00607] [<1.01E-08] [<0.01082] [<1.20E-08] [<0.01259] [<8.17E-09] [<0.00862] [<9.90E-09] [<0.01061] [<1.05E-08] [<0.01107] [<4.27E-08] [<0.0451] [<4.35E-08] [<0.0467] [<4.28E-08] [<0.0450] [<8.70E-08] [<0.0918] [<7.21E-08] [<0.0773] [<8.76E-08] [<0.0921] [<1.33E-08] [<0.01408] [<8.46E-09] [<0.00907] [<7.13E-09] [<0.00749] [<6.24E-09] [<0.00658] [<7.83E-09] [<0.00840] [<9.79E-09] [<0.01029] [<8.70E-09] [<0.00918] [<1.20E-08] [<0.01288] [<1.85E-08] [<0.0195] <1.04E-08 <0.01102 [<1.66E-08] [<0.0178] [<1.37E-08] [<0.0144] [<1.33E-08] [<0.01401] [<2.42E-08] [<0.0260] [<3.70E-08] [<0.0389] [<7.59E-09] [<0.00801] <4.42E-09 <0.00474 <4.29E-09 <0.00451 [<8.64E-08] [<0.0912] [<1.17E-07] [<0.1256] [<1.37E-07] [<0.144] [<4.30E-08] [<0.0454] [<1.19E-07] [<0.1278] Calculated Emission Rate[<1.07E-07] [<0.1122] [<3.53E-09] [<0.00372] [<3.31E-09] [<0.00355] [<3.31E-09] [<0.00348] [<5.85E-08] [<0.0617] [<9.56E-08] [<0.1025] [<9.27E-08] [<0.0975] [<2.61E-07] [<0.275] [<2.71E-07] [<0.291] [<3.09E-07] [<0.325] [<2.60E-07] [<0.274] [<5.39E-07] [<0.578] [<6.25E-07] [<0.657] [<3.67E-09] [<0.00388] [<3.22E-09] [<0.00345] [<4.05E-09] [<0.00426] [<5.00E-08] [<0.0527] [<7.71E-08] [<0.0826] [<8.31E-08] [<0.0874]1188 2171 12.4 1117 2081 12.5 1117 2081 12.5 1188 2171 12.4 1117 2081 12.5 1117 2081 12.5 1188 2171 12.4 1117 2081 12.5 1117 2081 12.5 1188 2171 12.4 1117 2081 12.5 1117 2081 12.5 1188 2171 12.4 1117 2081 12.5 1117 2081 12.5 1188 2171 12.4 1117 2081 12.5 1117 2081 12.5 1188 2171 12.4 1117 2081 12.5 1117 2081 12.5 1188 2171 12.4 1117 2081 12.5 1117 2081 12.5 1188 2171 12.4 1117 2081 12.5 1117 2081 12.5 1188 2171 12.4 1117 2081 12.5 1117 2081 12.5 1188 2171 12.4 1117 2081 12.5 1117 2081 12.5 1188 2171 12.4 1117 2081 12.5 1117 2081 12.5 1188 2171 12.4 1117 2081 12.5 1117 2081 12.5 1188 2171 12.4 1117 2081 12.5 1117 2081 12.5 1188 2171 12.4 1117 2081 12.5 1117 2081 12.5 1188 2171 12.4 1117 2081 12.5 Steam Output (1000 lb/hr) Total Heat Input (mmBtu/hr) Flue Gas Moisture (%)1117 2081 12.5 1188 2171 12.4 1117 2081 12.5 1117 2081 12.5 1188 2171 12.4 1117 2081 12.5 1117 2081 12.5 1188 2171 12.4 1117 2081 12.5 1117 2081 12.5 1188 2171 12.4 1117 2081 12.5 1117 2081 12.5 1188 2171 12.4 1117 2081 12.5 1117 2081 12.5 1188 2171 12.4 1117 2081 12.5 1117 2081 12.511.3 6.68 651500 11.3 6.96 641000 12 6.24 641700 11.3 6.68 651500 11.3 6.96 641000 12 6.24 641700 11.3 6.68 651500 11.3 6.96 641000 12 6.24 641700 11.3 6.68 651500 11.3 6.96 641000 12 6.24 641700 11.3 6.68 651500 11.3 6.96 641000 12 6.24 641700 11.3 6.68 651500 11.3 6.96 641000 12 6.24 641700 11.3 6.68 651500 11.3 6.96 641000 12 6.24 641700 11.3 6.68 651500 11.3 6.96 641000 12 6.24 641700 11.3 6.68 651500 11.3 6.96 641000 12 6.24 641700 11.3 6.68 651500 11.3 6.96 641000 12 6.24 641700 11.3 6.68 651500 11.3 6.96 641000 12 6.24 641700 11.3 6.68 651500 11.3 6.96 641000 12 6.24 641700 11.3 6.68 651500 11.3 6.96 641000 12 6.24 641700 11.3 6.68 651500 11.3 6.96 641000 12 6.24 641700 11.3 6.68 651500 11.3 6.96 641000 12 6.24 641700 11.3 6.68 651500 11.3 6.96 641000

Flue Gas O2(%) Flue Gas Flow Rate (scfm) Flue Gas CO2(%)12 6.24 641700 11.3 6.68 651500 11.3 6.96 641000 12 6.24 641700 11.3 6.68 651500 11.3 6.96 641000 12 6.24 641700 11.3 6.68 651500 11.3 6.96 641000 12 6.24 641700 11.3 6.68 651500 11.3 6.96 641000 12 6.24 641700 11.3 6.68 651500 11.3 6.96 641000 12 6.24 641700 11.3 6.68 651500 11.3 6.96 641000 12 6.24 641700Fuel Input Rate Fuel Type

123 1679 bitum inous 123 1615 bitum inous 123 1615 bitum inous 123 1679 bitum inous 123 1615 bitum inous 123 1615 bitum inous 123 1679 bitum inous 123 1615 bitum inous 123 1615 bitum inous 123 1679 bitum inous 123 1615 bitum inous 123 1615 bitum inous 123 1679 bitum inous 123 1615 bitum inous 123 1615 bitum inous 123 1679 bitum inous 123 1615 bitum inous 123 1615 bitum inous 123 1679 bitum inous 123 1615 bitum inous 123 1615 bitum inous 123 1679 bitum inous 123 1615 bitum inous 123 1615 bitum inous 123 1679 bitum inous 123 1615 bitum inous 123 1615 bitum inous 123 1679 bitum inous 123 1615 bitum inous 123 1615 bitum inous 123 1679 bitum inous 123 1615 bitum inous 123 1615 bitum inous 123 1679 bitum inous 123 1615 bitum inous 123 1615 bitum inous 123 1679 bitum inous 123 1615 bitum inous 123 1615 bitum inous 123 1679 bitum inous 123 1615 bitum inous 123 1615 bitum inous 123 1679 bitum inous 123 1615 bitum inous 123 1615 bitum inous 123 1679 bitum inous 123 1615 bitum inous Flue Gas Temperature (F) Fuel #1123 1615 bitum inous 123 1679 bitum inous 123 1615 bitum inous 123 1615 bitum inous 123 1679 bitum inous 123 1615 bitum inous 123 1615 bitum inous 123 1679 bitum inous 123 1615 bitum inous 123 1615 bitum inous 123 1679 bitum inous 123 1615 bitum inous 123 1615 bitum inous 123 1679 bitum inous 123 1615 bitum inous 123 1615 bitum inous 123 1679 bitum inous 123 1615 bitum inous 123 1615 bitum inousUnits of Measure Measurement Method Fuel Input Rate

ton/day 545 ton/day 466 ton/day 466 ton/day 545 ton/day 466 ton/day 466 ton/day 545 ton/day 466 ton/day 466 ton/day 545 ton/day 466 ton/day 466 ton/day 545 ton/day 466 ton/day 466 ton/day 545 ton/day 466 ton/day 466 ton/day 545 ton/day 466 ton/day 466 ton/day 545 ton/day 466 ton/day 466 ton/day 545 ton/day 466 ton/day 466 ton/day 545 ton/day 466 ton/day 466 ton/day 545 ton/day 466 ton/day 466 ton/day 545 ton/day 466 ton/day 466 ton/day 545 ton/day 466 ton/day 466 ton/day 545 ton/day 466 ton/day 466 ton/day 545 ton/day 466 ton/day 466 ton/day 545 ton/day 466 Fuel #1ton/day 466

ton/day 545 ton/day 466 ton/day 466 ton/day 545 ton/day 466 ton/day 466 ton/day 545 ton/day 466 ton/day 466 ton/day 545 ton/day 466 ton/day 466 ton/day 545 ton/day 466 ton/day 466 ton/day 545 ton/day 466 ton/day 466Fuel Type Units of Measure Measurement Method

petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day Fuel #2petroleum coke ton/day

petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/day petroleum coke ton/dayFuel Input Rate Fuel Type Units of Measure Fuel #3Measurement Method Fuel Input Rate Fuel Type Fuel #4Units of Measure Measurement Method Fuel #4 Other Supporting InformationEIA

Facility Code Facility Name Boiler ID

6639 R D Green G2

1 5/17/2010 6:58 5/17/2010 2 5/17/2010 10:15 5/17/2010 3 5/17/2010 13:43 5/17/2010 Run Number Test Start Date Test Start Time Test End DateMeasured Value (ppm) Basis (Wet or Dry) Test Method Used

10:08 <0.0178 Dry U.S. EPA Method 26A-Mod 13:27 <0.0191 Dry U.S. EPA Method 26A-Mod 16:52 <0.0174 Dry U.S. EPA Method 26A-Mod Hydrogen Cyanide Emission Test Results Test End TimeData Flag (ADL,

BDL, DDL) Test Method

Comments BDL <1.85E-05 1222 2318 14.2 11.5 BDL <1.98E-05 1222 2318 14.4 11.5 BDL <1.81E-05 1222 2318 13.6 11.5 Steam Output (1000 lb/hr) Total Heat

Input (mmBtu/hr) Calculated Emission Rate (lb/mmBtu) Flue Gas Moisture (%) Flue Gas CO2(%)Fuel Input Rate Fuel Type Units of Measure Measurement

Method Fuel Input

Rate 6.58 665156 123 1809 bitum inous ton/day 537 6.58 654276 124 1809 bitum inous ton/day 537 6.58 650977 122 1809 bitum inous ton/day 537 Flue Gas Flow Rate (dscfm) Flue Gas

Temperature (F) Fuel #1 Flue Gas O2(%)Fuel Type Units of Measure Measurement

Method Fuel Input Rate Fuel Type Units of Measure Measurement

Method Fuel Input

Rate petroleum coke

ton/day petroleum coke

ton/day petroleum coke

ton/day Fuel #2 Fuel #3Fuel Type Units of Measure Measurement

Method Fuel #4 Other Supporting InformationEIA

Facility Code Facility Name Boiler ID

6639 R D Green G2

Run Number Test Start Date Test Start Time Test End DateMeasured Value (ppm) Basis (Wet or Dry) Test Method Used Test End Time Hydrogen Chloride Emission Test ResultsData Flag (ADL,

BDL, DDL) Test Method

Comments Calculated

Emission Rate (lb/mmBtu) Flue Gas Moisture (%) Flue Gas CO2(%) Hydrogen Chloride Emission Test Results Steam Output (1000 lb/hr) Total Heat

Input (mmBtu/hr)Fuel Input Rate Fuel Type Units of Measure Measurement

Method Fuel Input

Rate Flue Gas Temperature (F) Fuel #1 Flue Gas O2(%) Flue Gas

Flow Rate (dscfm)Fuel Type Units of Measure Measurement

Method Fuel Input Rate Fuel Type Units of Measure Measurement

Method Fuel Input

Rate Fuel #2 Fuel #3Fuel Type Units of Measure Measurement

Method Fuel #4 Other Supporting InformationEIA

Facility Code Facility Name Boiler ID

6639 R D Green G2

Run Number Test Start Date Test Start Time Test End DateMeasured Value (ppm) Basis (Wet or Dry) Test Method Used Hydrogen Flouride Emission Test Results Test End TimeData Flag (ADL,

BDL, DDL) Test Method

Comments Hydrogen Flouride Emission Test Results Steam Output (1000 lb/hr) Total Heat

Input (mmBtu/hr) Calculated Emission Rate (lb/mmBtu) Flue Gas Moisture (%)Fuel Input Rate Fuel Type Units of Measure Measurement

Method Flue Gas Flow Rate (dscfm) Flue Gas

Temperature (F) Fuel #1 Flue Gas CO2(%) Flue Gas

O2(%)Fuel Input

Rate Fuel Type Units of Measure Measurement

Method Fuel Input Rate Fuel Type Units of Measure Measurement

Method Fuel #2 Fuel #3Fuel Input

Rate Fuel Type Units of Measure Measurement

Method Fuel #4 Other Supporting InformationEIA

Facility Code Facility Name Boiler ID 6639 R D Green G2

Run Number Test Start Date Test Start TimeMeasured NO (ppm) Test End Time Test End DateMeasured NO2(ppm) Basis (Wet or Dry) Test Method Used NOXEmission Test ResultsData Flag (ADL, BDL, DDL) Test Method Comments (lb/mmBtu) Total NOXCalculated Emission Rateppmdv @ 7% O 2 Flue Gas O2(%) Calculated Emission Rate Steam Output (1000 lb/hr) Total Heat Input

(mmBtu/hr) Flue Gas

Moisture (%) Flue Gas

CO2(%)Fuel Input Rate Fuel Type Units of Measure Measurement

Method Fuel Input

Rate Flue Gas Flow Rate (dscfm) Flue Gas

Temperature (F) Fuel #1Fuel Type Units of Measure Measurement

Method Fuel Input

Rate Fuel Type Units of Measure Measurement

Method Fuel Input

Rate Fuel #2 Fuel #3Fuel Type Units of Measure Measurement

Method Fuel #4 Other Supporting InformationEIA

Facility Code Facility Name Boiler ID 6639 R D Green G2

Run Number Test Start Date Test Start TimeTotal Dissolved Solids (mg solids/liter) Total Suspended Solids (mg solids/liter) Test End Time Test End DateTest Method Used Data Flag (ADL, BDL, DDL) Constisuent Emission Test ResultsTest Method Comments Fuel Input Rate Flue Gas Temperat ure (F) Flue Gas Flow Rate (dscfm) Steam Output (1000 lb/hr) Total Heat Input

(mmBtu/hr)Fuel Type Units of Measure Measurement

Method Fuel Input Rate Fuel Type Units of Measure Measurement

Method Fuel Input Rate Fuel #1 Fuel #2Fuel Type Units of Measure Measurement

Method Fuel Input

Rate Fuel Type Units of

Measure Measurement

Method Fuel #3 Fuel #4Other Supporting Information