### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

3845 TransAlta Centralia Generation LLC BW 21 

### subbituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte



### 3845 TransAlta Centralia Generation LLC BW21 As Received Higher Heating Value 

### 3845 TransAlta Centralia Generation LLC BW21 As Received % Moisture 

### 3845 TransAlta Centralia Generation LLC BW21 As Received % Ash 

### 3845 TransAlta Centralia Generation LLC BW21 As Received % Sulfur 

### 3845 TransAlta Centralia Generation LLC BW21 Dry

basis Higher Heating Value 

### 3845 TransAlta Centralia Generation LLC BW21 Dry

basis % Ash 

### 3845 TransAlta Centralia Generation LLC BW21 Dry

basis % Sulfur 

### 3845 TransAlta Centralia Generation LLC BW21 Dry

basis Antim ony 

### 3845 TransAlta Centralia Generation LLC BW21 Dry

basis Arsenic 

### 3845 TransAlta Centralia Generation LLC BW21 Dry

basis Beryllium 

### 3845 TransAlta Centralia Generation LLC BW21 Dry

basis Cadmium 

### 3845 TransAlta Centralia Generation LLC BW21 Dry

basis Chlorine 

### 3845 TransAlta Centralia Generation LLC BW21 Dry

basis Chromium 

### 3845 TransAlta Centralia Generation LLC BW21 Dry

basis Cobalt 

### 3845 TransAlta Centralia Generation LLC BW21 Dry

basis Fluorine 

### 3845 TransAlta Centralia Generation LLC BW21 Dry

basis Lead 

### 3845 TransAlta Centralia Generation LLC BW21 Dry

basis Manganese 

### 3845 TransAlta Centralia Generation LLC BW21 Dry

basis Mercury 

### 3845 TransAlta Centralia Generation LLC BW21 Dry

basis Nickel 

### 3845 TransAlta Centralia Generation LLC BW21 Dry

basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) 

### ASTM D 5865 ASTM D 3302 ASTM D 3174/5142 ASTM D 4239 ASTM D 5865 ASTM D 3174/5142 ASTM D 4239 ASTM D 6357 ASTM D 6357 ASTM D 6357 ASTM D 6357 ASTM D 6721 ASTM D 6357 ASTM D 6357 ASTM D 3761 ASTM D 6357 ASTM D 6357 ASTM D 6722 ASTM D 6357 SW7740EIA Facility Code Facility Name Boiler ID HAPs Test Group 

### 3845 TransAlta Centralia Generation LLC BW21 Dioxin/furan HAPs

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY ) Test Stop

Date (MM/DD/YYY Y) Higher

Heating Value (HHV) (as received ) HHV Units % Moistur
e (as receive d) % A

sh (as receive d) 

### 1-0600-032310-U1-TEMA (1-fuel-1) 3/22/2010 3/23/2010 8002 Btu/lb 28.21 10.08 2-2045-032310-U1-TEMA (2-fuel-1) 3/23/2010 3/23/2010 8143 Btu/lb 26.83 10.78 3-0530-032410-U1-TEMA (3-fuel-2) * see note on analysis sheet 3/23/2010 3/24/2010 7796 Btu/lb 26.98 13.17 4-1800-032410-U1-TEMA (4-fuel-1) 3/24/2010 3/24/2010 8024 Btu/lb 25.84 12.53 5-0600-032510-U1-TEMA (5-fuel-1) 3/24/2010 3/25/2010 8142 Btu/lb 26.32 11.18 6-1800-032510-U1-TEMA (6-fuel-1) 3/25/2010 3/25/2010 7921 Btu/lb 27.18 11.93 Fuel Testing Results%

Sulfur (as receiv ed) Higher Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) %

Sulfur (Dry Basis) Chlo rine (Dry Basi s) Chlorin e Units Mercu

ry (Dry Basis) Mercu

ry Units An tim
on y (Dr y Ba sis ) An tim ony Units Ars enic (Dry Basi s) Arseni c Units Bery

lliu

m (Dry Basi s) Beryll ium Units Cad mium (Dry Basis ) Cadm ium Units Chr

om iu

m (Dr y Ba sis) 

### 0.35 11147 Btu/lb 14.04 0.48 77 ppm 0.07 μg/g 1 μg/g 3 μg/g 0.4 μg/g 0.3 μg/g 12 0.3 11129 Btu/lb 14.74 0.42 46 ppm 0.11 μg/g 1 μg/g 2 μg/g 0.4 μg/g 0.4 μg/g 15 0.31 10676 Btu/lb 18.03 0.42 57 ppm 0.1 μg/g 2 μg/g 3 μg/g 0.4 μg/g 0.4 μg/g 16 0.34 10819 Btu/lb 16.9 0.45 53 ppm 0.06 μg/g 2 μg/g 3 μg/g 0.4 μg/g 0.4 μg/g 16 0.32 11051 Btu/lb 15.17 0.44 53 ppm 0.07 μg/g 2 μg/g 3 μg/g 0.4 μg/g 0.4 μg/g 13 0.31 10878 Btu/lb 16.39 0.42 55 ppm 0.09 μg/g 2 μg/g 3 μg/g 0.4 μg/g 0.4 μg/g 16Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Chro mium Units Lea d (Dr y Ba sis) Lead Units Mang
anese (Dry Basis ) Mang
anese Units Nic kel (Dry Bas is) Nickel Units Se le ni

u m (D ry Ba sis ) Selen ium Units Fluor ine (Dry Basi s) Fluor ine Units Cob alt (Dry Basi s) Cobalt Units Total Moisture

Volatiles As h

Fixed Carbon

Carbon Hydrogen 

### μg/g 4 μg/g 77 μg/g 11 μg/g 1 μg/g 87 ppm 2 μg/g 28.21 40.4 14 45.5 62.8 4.57 μg/g 4 μg/g 90 μg/g 12 μg/g 1 μg/g 86 ppm 2 μg/g 26.83 39.8 14.7 45.4 63.7 4.51 μg/g 4 μg/g 119 μg/g 17 μg/g 1 μg/g 90 ppm 2 μg/g 26.98 38.5 18 43.4 61.1 4.34 μg/g 4 μg/g 115 μg/g 13 μg/g 1 μg/g 86 ppm 2 μg/g 25.84 38.7 16.9 44.4 62 4.44 μg/g 4 μg/g 100 μg/g 10 μg/g 1 μg/g 98 ppm 2 μg/g 26.32 39.5 15.2 45.3 63.7 4.55 μg/g 4 μg/g 110 μg/g 12 μg/g 1 μg/g 95 ppm 2 μg/g 27.18 39 16.4 44.6 62.2 4.47 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Nitrogen Total Sulfur

Oxygen 

### 0.91 0.48 16.18 0.89 0.42 15.77 0.86 0.42 15.23 0.87 0.45 15.36 0.88 0.44 15.29 0.86 0.42 15.65 Ultimate Analy

ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 3845 TransAlta Centralia Generation LLC BW21 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 

### 4-1800-032410-U1-TEMA (4-fuel-1)

3/24/2010 3/24/2010 8024 Btu/lb 5-0600-032510-U1-TEMA (5-fuel-1)

3/24/2010 3/25/2010 8142 Btu/lb 6-1800-032510-U1-TEMA (6-fuel-1)

3/25/2010 3/25/2010 7921 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 25.84 12.53 0.34 10819 Btu/lb 16.9 0.45 26.32 11.18 0.32 11051 Btu/lb 15.17 0.44 27.18 11.93 0.31 10878 Btu/lb 16.39 0.42Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 53 ppm 0.06 μg/g 2 μg/g 3 μg/g 0.4 53 ppm 0.07 μg/g 2 μg/g 3 μg/g 0.4 55 ppm 0.09 μg/g 2 μg/g 3 μg/g 0.4Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### μg/g 0.4 μg/g 16 μg/g 4 μg/g 115 μg/g μg/g 0.4 μg/g 13 μg/g 4 μg/g 100 μg/g μg/g 0.4 μg/g 16 μg/g 4 μg/g 110 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 

### 13 μg/g 1 μg/g 86 ppm 2 μg/g 10 μg/g 1 μg/g 98 ppm 2 μg/g 12 μg/g 1 μg/g 95 ppm 2 μg/gNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur



### 25.84 38.7 16.9 44.4 61.98 4.44 0.87 0.45 26.32 39.53 15.17 45.3 63.67 4.55 0.88 0.44 27.18 39.02 16.39 44.59 62.21 4.47 0.86 0.42 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 

### 15.36 15.29 15.65EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 3845 TransAlta Centralia Generation LLC BW21 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### 4-1800-032410-U1-TEMA (4-fuel-1)

3/24/2010 3/24/2010 8024 Btu/lb 5-0600-032510-U1-TEMA (5-fuel-1)

3/24/2010 3/25/2010 8142 Btu/lb 6-1800-032510-U1-TEMA (6-fuel-1)

3/25/2010 3/25/2010 7921 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 25.84 12.53 0.34 10819 Btu/lb 16.9 0.45 26.32 11.18 0.32 11051 Btu/lb 15.17 0.44 27.18 11.93 0.31 10878 Btu/lb 16.39 0.42Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 53 ppm 0.06 μg/g 2 μg/g 3 μg/g 0.4 53 ppm 0.07 μg/g 2 μg/g 3 μg/g 0.4 55 ppm 0.09 μg/g 2 μg/g 3 μg/g 0.4Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### μg/g 0.4 μg/g 16 μg/g 4 μg/g 115 μg/g μg/g 0.4 μg/g 13 μg/g 4 μg/g 100 μg/g μg/g 0.4 μg/g 16 μg/g 4 μg/g 110 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 13 μg/g 1 μg/g 86 ppm 2 μg/g 25.84 10 μg/g 1 μg/g 98 ppm 2 μg/g 26.32 12 μg/g 1 μg/g 95 ppm 2 μg/g 27.18 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

### 38.7 16.9 44.4 61.98 4.44 0.87 0.45 15.36 39.53 15.17 45.3 63.67 4.55 0.88 0.44 15.29 39.02 16.39 44.59 62.21 4.47 0.86 0.42 15.65 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 3845 TransAlta Centralia Generation LLCBW21

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm