### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.
1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected
more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of
measure.

### Information
This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

50776 Panther Creek Energy Facility BLR1 BLR2 

### coal refuse (culm or gob)Fuel Type 2 Fuel Type 3 Other Fuel Description



### No.2 Fuel Oil (distillate)EIA

Facility Code Facility Name Boiler ID Basis An alyte



### 50776 Panther Creek Energy Facility BLR1 BLR2 As Received Higher Heating Value 

### 50776 Panther Creek Energy Facility BLR1 BLR2 As Received % Moisture 

### 50776 Panther Creek Energy Facility BLR1 BLR2 As Received % Ash 

### 50776 Panther Creek Energy Facility BLR1 BLR2 As Received % Sulfur 

### 50776 Panther Creek Energy Facility BLR1 BLR2 Dry

basis Higher Heating Value 

### 50776 Panther Creek Energy Facility BLR1 BLR2 Dry

basis % Ash 

### 50776 Panther Creek Energy Facility BLR1 BLR2 Dry

basis % Sulfur 

### 50776 Panther Creek Energy Facility BLR1 BLR2 Dry

basis Antim ony 

### 50776 Panther Creek Energy Facility BLR1 BLR2 Dry

basis Arsenic 

### 50776 Panther Creek Energy Facility BLR1 BLR2 Dry

basis Beryllium 

### 50776 Panther Creek Energy Facility BLR1 BLR2 Dry

basis Cadmium 

### 50776 Panther Creek Energy Facility BLR1 BLR2 Dry

basis Chlorine 

### 50776 Panther Creek Energy Facility BLR1 BLR2 Dry

basis Chromium 

### 50776 Panther Creek Energy Facility BLR1 BLR2 Dry

basis Cobalt 

### 50776 Panther Creek Energy Facility BLR1 BLR2 Dry

basis Fluorine 

### 50776 Panther Creek Energy Facility BLR1 BLR2 Dry

basis Lead 

### 50776 Panther Creek Energy Facility BLR1 BLR2 Dry

basis Manganese 

### 50776 Panther Creek Energy Facility BLR1 BLR2 Dry

basis Mercury 

### 50776 Panther Creek Energy Facility BLR1 BLR2 Dry

basis Nickel 

### 50776 Panther Creek Energy Facility BLR1 BLR2 Dry

basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) 

### ASTM D5865 ASTM D5142 ASTM D5142 ASTM D4239 ASTM D5865 ASTM D5142 ASTM D4239 SW846-6020 SW846-6020 SW846-6020 SW846-6020 ASTM D6721 SW846-6020 SW846-6020 ASTM D3761 SW846-6020 SW846-6020 ASTM D6722 SW846-6020 SW846-6020EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 50776 Panther Creek Energy Facility BLR1 BLR2 Dioxin/furan HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### DF RUN 1 7/6/2010 7/6/2010 6276.00 Btu/lb DF RUN 2 7/7/2010 7/7/2010 6538.00 Btu/lb DF RUN 3 7/8/2010 7/8/2010 6200.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 11.87 42.1 0.4 7121 Btu/lb 47.77 0.46 10.2 42.52 0.41 7281 Btu/lb 47.35 0.45 10.92 43.59 0.37 6960 Btu/lb 48.93 0.41Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 145 μg/g 163 μg/g 147 μg/gBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 

### 6.71 47.77 45.52 45.67 1.23 0.61 0.46 6.68 47.35 45.97 46.97 1.26 0.65 0.45 7.21 48.93 43.86 44.62 1.2 0.61 0.41 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen



### 4.26 3.32 4.23EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 50776 Panther Creek Energy Facility BLR1 BLR2 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 

### M RUN 1 7/15/2010 7/15/2010 6599.00 Btu/lb M RUN 2 7/16/2010 7/16/2010 6713.00 Btu/lb M RUN 3 7/19/2010 7/19/2010 6811.00 Btu/lb

HG RUN 1 7/19/2010 7/19/2010 6771.00 Btu/lb HG RUN 2 7/19/2010 7/19/2010 6765.00 Btu/lb HG RUN 3 7/19/2010 7/19/2010 6760.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 12.65 39.18 0.38 7556 Btu/lb 44.85 0.44 12.47 39.19 0.39 7669 Btu/lb 44.78 0.45 12.85 37.93 0.38 7816 Btu/lb 43.52 0.44

12.56 38.73 0.39 7744 Btu/lb 44.29 0.45 12.48 38.63 0.4 7729 Btu/lb 44.14 0.46 12.66 38.34 0.39 7740 Btu/lb 43.9 0.45Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 174 μg/g 0.287 μg/g 1.54 mg/Kg 14.8 mg/Kg 1.68 151 μg/g 0.271 μg/g <1.0 mg/Kg 10.6 mg/Kg 1.69 148 μg/g 0.272 μg/g 1.04 mg/Kg 12.1 mg/Kg 1.51

150 μg/g 0.265 μg/g 1.04 mg/Kg 12.4 mg/Kg 1.57 139 μg/g 0.257 μg/g 1.03 mg/Kg 12.4 mg/Kg 1.73 149 μg/g 0.257 μg/g 1.03 mg/Kg 11.9 mg/Kg 2.58Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### mg/Kg 0.51 mg/Kg 24.3 mg/Kg 27.9 mg/Kg 76.4 mg/Kg mg/Kg 1.64 mg/Kg 16 mg/Kg 8.37 mg/Kg 104 mg/Kg mg/Kg 1.6 mg/Kg 18 mg/Kg 22.3 mg/Kg 93.5 mg/Kg
mg/Kg 1.55 mg/Kg 17 mg/Kg 21.1 mg/Kg 59.8 mg/Kg mg/Kg 1.63 mg/Kg 18.5 mg/Kg 23 mg/Kg 72.2 mg/Kg mg/Kg 1.6 mg/Kg 18.2 mg/Kg 22.9 mg/Kg 82.2 mg/KgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 

### 20.8 mg/Kg 10.9 mg/Kg 10.7 mg/Kg 18.8 mg/Kg 9.52 mg/Kg 19 mg/Kg 18.7 mg/Kg 9.37 mg/Kg 8.42 mg/Kg

17.8 mg/Kg 9.45 mg/Kg 8.22 mg/Kg 19 mg/Kg 9.47 mg/Kg 8.53 mg/Kg 18.3 mg/Kg 9.8 mg/Kg 8.47 mg/KgNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 

### 7.44 44.85 47.7 49.48 1.29 0.68 0.44 6.92 44.78 48.31 50.46 1.31 0.71 0.45 7.2 43.52 49.28 51.55 1.33 0.71 0.44

6.76 44.29 48.94 50.19 1.31 0.74 0.45 6.73 44.14 49.13 50.98 1.32 0.72 0.46 7.08 73.9 49.02 49.52 1.31 0.7 0.45 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 

### 3.26 2.31 2.44

3.02 2.38 4.13EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 50776 Panther Creek Energy Facility BLR1 BLR2 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### AG RUN 1 7/20/2010 7/20/2010 6391.00 Btu/lb AG RUN 2 7/20/2010 7/20/2010 6342.00 Btu/lb AG RUN 3 7/20/2010 7/20/2010 6170.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 12.38 41.1 0.36 7294 Btu/lb 46.9 0.41 11.03 43.64 0.35 7128 Btu/lb 49.05 0.4 13.52 41.54 0.33 7135 Btu/lb 48.03 0.39Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 143 μg/g 138 μg/g 129 μg/gBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 44 μg/g <40.0 μg/g 42 μg/g Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

### 7.1 46.9 46 47.44 1.29 0.64 0.41 3.32 6.95 49.05 44 46.53 1.29 0.67 0.4 2.06 7.14 48.03 44.83 46.51 1.3 0.66 0.39 3.11 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 50776 Panther Creek Energy Facility BLR1 BLR2

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### ORG RUN 1 7/21/2010 7/21/2010 6432.00 Btu/lb ORG RUN 2 7/21/2010 7/21/2010 6111.00 Btu/lb ORG RUN 3 7/21/2010 7/21/2010 6170.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 12.85 39.52 0.38 7380 Btu/lb 45.35 0.44 12.4 41.85 0.37 6976 Btu/lb 47.77 0.43 12.63 41.9 0.36 7062 Btu/lb 47.95 0.41Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

### 6.92 45.35 47.73 48.91 1.26 0.7 0.44 3.34 7.49 47.77 44.74 46.05 1.26 0.66 0.43 3.83 7.16 47.95 44.88 46.46 1.24 0.68 0.41 3.25 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg /g petroleum coke μg/g other mg /KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm 

### μg/g