### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1 6147 Monticello 2 

### ligniteFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte



### 6147 Monticello 2 As Received Higher Heating Value 

### 6147 Monticello 2 As Received % Moisture 

### 6147 Monticello 2 As Received % Ash 

### 6147 Monticello 2 As Received % Sulfur 

### 6147 Monticello 2 Dry basis Higher Heating Value 

### 6147 Monticello 2 Dry basis % Ash 

### 6147 Monticello 2 Dry basis % Sulfur 

### 6147 Monticello 2 Dry basis Antim ony 

### 6147 Monticello 2 Dry basis Arsenic 

### 6147 Monticello 2 Dry basis Beryllium 

### 6147 Monticello 2 Dry basis Cadmium 

### 6147 Monticello 2 Dry basis Chlorine 

### 6147 Monticello 2 Dry basis Chromium 

### 6147 Monticello 2 Dry basis Cobalt 

### 6147 Monticello 2 Dry basis Fluorine 

### 6147 Monticello 2 Dry basis Lead 

### 6147 Monticello 2 Dry basis Manganese 

### 6147 Monticello 2 Dry basis Mercury 

### 6147 Monticello 2 Dry basis Nickel 

### 6147 Monticello 2 Dry basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) 

### ASTM D 5865 ASTM D 3302 ASTM D 3174/5142 ASTM D 4239 ASTM D 5865 ASTM D 3174/5142 ASTM D 4239 ASTM D 6357 ASTM D 6357 ASTM D 6357 ASTM D 6357 ASTM D 6721 ASTM D 6357 ASTM D 6357 ASTM D 3761 ASTM D 6357 ASTM D 6357 ASTM D 6722 ASTM D 6357 SW7740EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 6147 Monticello 2

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 1A 

### 4/27/2010 4/27/2010 7699.00 Btu/lb 1B 4/27/2010 4/27/2010 7935.00 Btu/lb 1C 4/27/2010 4/27/2010 7992.00 Btu/lb 2A 4/28/2010 4/28/2010 7804.00 Btu/lb 2B 4/28/2010 4/28/2010 7385.00 Btu/lb 2C 4/29/2010 4/29/2010 7676.00 Btu/lb 3A 4/29/2010 4/29/2010 7774.00 Btu/lb 3B 4/29/2010 4/29/2010 7766.00 Btu/lb 3C 4/29/2010 4/29/2010 7642.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 31.03 8.86 0.33 11162 Btu/lb 12.85 0.47 31.3 6.74 0.33 11549 Btu/lb 9.81 0.47 31.39 6.72 0.3 11649 Btu/lb 9.8 0.44 30.25 9.22 0.36 11189 Btu/lb 13.22 0.51 32.08 10.5 0.39 10873 Btu/lb 15.46 0.58 31.65 8.86 0.42 11231 Btu/lb 12.96 0.62 31.45 8.61 0.5 11341 Btu/lb 12.56 0.73 31.29 8.42 0.36 11303 Btu/lb 8.42 0.36 30.89 9.42 0.41 11058 Btu/lb 13.63 0.59Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 20 ppm 0.16 μg/g [<2] μg/g 2 μg/g 0.4 [<10] ppm 0.1 μg/g [<2] μg/g 2 μg/g [<0.4] 12 ppm 0.07 μg/g [<2] μg/g 1 μg/g 0.4 11 ppm 0.15 μg/g [<2] μg/g 1 μg/g 0.5 13 ppm 0.18 μg/g [<2] μg/g 2 μg/g 0.7 17 ppm 0.15 μg/g [<2] μg/g 2 μg/g 0.5 11 ppm 0.2 μg/g [<2] μg/g 2 μg/g 0.5 13 ppm 0.16 μg/g [<2] μg/g 2 μg/g 0.4 13 ppm 0.17 μg/g [<2] μg/g 1 μg/g 0.5Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### μg/g [<0.4] μg/g 11 μg/g 5 μg/g 32 μg/g μg/g [<0.4] μg/g 8 μg/g [<4] μg/g 28 μg/g μg/g [<0.4] μg/g 8 μg/g [<4] μg/g 21 μg/g μg/g [<0.4] μg/g 10 μg/g 5 μg/g 36 μg/g μg/g [<0.4] μg/g 12 μg/g 6 μg/g 57 μg/g μg/g [<0.4] μg/g 11 μg/g 5 μg/g 49 μg/g μg/g [<0.4] μg/g 10 μg/g 4 μg/g 41 μg/g μg/g [<0.4] μg/g 9 μg/g 4 μg/g 32 μg/g μg/g [<0.4] μg/g 13 μg/g 6 μg/g 38 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 7 μg/g 2 μg/g 56 ppm [<2] μg/g 31.03 6 μg/g 2 μg/g 62 ppm [<2] μg/g 31.3 6 μg/g 2 μg/g 59 ppm [<2] μg/g 31.39 6 μg/g 2 μg/g 61 ppm [<2] μg/g 30.25 7 μg/g 3 μg/g 89 ppm [<2] μg/g 32.08 7 μg/g 3 μg/g 76 ppm [<2] μg/g 31.65 7 μg/g 3 μg/g 63 ppm [<2] μg/g 31.45 6 μg/g 2 μg/g 84 ppm [<2] μg/g 31.29 7 μg/g 3 μg/g 85 ppm [<2] μg/g 30.89 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 

### 42.38 12.85 44.77 64.04 4.54 0.88 0.47 43.28 9.81 46.91 66.34 4.62 0.92 0.47 43.65 9.8 46.55 66.7 4.63 1 0.44 42.47 13.22 44.31 63.97 4.61 0.98 0.51 42.16 15.46 42.38 62.12 4.53 0.97 0.58 42.77 12.96 44.27 64.15 4.6 0.97 0.62 43.17 12.56 44.27 64.64 4.6 1.01 0.73 43.41 12.26 44.33 64.94 4.6 0.95 0.53 42.11 13.63 44.26 63.29 4.54 0.95 0.59 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen



### 17.22 17.84 17.43 16.71 16.34 16.7 16.46 16.72 17EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 6147 Monticello 2

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt UnitsNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur

Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

OxygenEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 6147 Monticello 2

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 6147 Monticello 2

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg /g petroleum coke μg/g other mg /KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm