Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop-down boxes, included. Gray fields are aut

filled from other fields.

Please name each resulting spreadsheet with the following naming convention: 

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.

3. Please choose the type of fuel being sampled using the drop-down in the fuel column of the Boiler Informatio

worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column.

4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "A

04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If t

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange 

highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksh

6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell)

7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a min

composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you ha

more.

8. Provide the results of the analyses for each constituent requested. Use the drop-down boxes to fill in the unit

measure.
Information

ormation about chemical analyses of fuels 

hlorine, fluorine, and metals, such as 

 selenium. This spreadsheet is intended to 

) fuel analyses at that specific boiler. This 

or all 4 HAP surrogates were being tested. 

Fields that are highlighted in yellow are 

xes, included. Gray fields are automatically 

 on the Boiler Information worksheet.

el column of the Boiler Information 

e Other Fuel Description column.

hods worksheet. For example: "ASTM D5865-

cklist worksheet (orange tab). If the units of

ease fill them in the blank, orange 

n the Fuels Sample Results worksheet.

range highlighted cell).

orksheet. You must provide a minimum of 3 

t limited to that number if you have collected 

down boxes to fill in the units of 
EIA Facility Code Facility Name Boiler ID Fuel Type 1

1200067 Cleary Flood 8 No.6 Fuel Oil (residual or bunker C)
Fuel Type 2 Fuel Type 3 Other Fuel Description

No.2 Fuel Oil (distillate) Note 1: separate samples were taken for No. 6 and No

Note 2: No. 2 Oil was about 7-10% of the total (combin
es were taken for No. 6 and No. 2 oil each day of testing

bout 7-10% of the total (combined No. 6 and No. 2) oil flow rate 
EIA Facility Code Facility Name Boiler ID Basis Analyte

1200067 Cleary Flood 8 As Received Higher Heating Value

1200067 Cleary Flood 8 As Received % Moisture

1200067 Cleary Flood 8 As Received % Ash

1200067 Cleary Flood 8 As Received % Sulfur

1200067 Cleary Flood 8 Dry basis Higher Heating Value

1200067 Cleary Flood 8 Dry basis % Ash

1200067 Cleary Flood 8 Dry basis % Sulfur

1200067 Cleary Flood 8 Dry basis Antimony

1200067 Cleary Flood 8 Dry basis Arsenic

1200067 Cleary Flood 8 Dry basis Beryllium

1200067 Cleary Flood 8 Dry basis Cadmium

1200067 Cleary Flood 8 Dry basis Chlorine

1200067 Cleary Flood 8 Dry basis Chromium

1200067 Cleary Flood 8 Dry basis Cobalt

1200067 Cleary Flood 8 Dry basis Fluorine

1200067 Cleary Flood 8 Dry basis Lead

1200067 Cleary Flood 8 Dry basis Manganese

1200067 Cleary Flood 8 Dry basis Mercury

1200067 Cleary Flood 8 Dry basis Nickel

1200067 Cleary Flood 8 Dry basis Selenium
Analysis Method for each Analyte 

(example: ASTM D5865-04)

D240

D482

D1552

SW6010B

SW6010B

SW6010B

SW6010B

E776/9253

SW6010B

SW6010B

D3761

SW6010B

SW6010B

SW7470

SW6010B

SW6010B
EIA Facility Code Facility Name Boiler ID

1200067 Cleary Flood 8

Sample Number (minimum 

of 3 composite samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating Value 

(HHV)

(as received)

R10090070-01 [2 Oil] 9/20/2010 9/20/2010 19240.00

R10090070-02 [6 Oil] 9/20/2010 9/20/2010 18270.00

R10090070-03 [2 Oil] 9/21/2010 9/21/2010 19200.00

R10090070-04 [6 Oil] 9/21/2010 9/21/2010 18350.00

R10090070-05 [2 Oil] 9/22/2010 9/22/2010 19430.00

R10090070-06 [6 Oil] 9/22/2010 9/22/2010 18310.00

R10090070-07 [2 Oil] 9/23/2010 9/23/2010 19380.00

R10090070-08 [6 Oil] 9/23/2010 9/23/2010 18450.00

 Fuel Testing Results


HAPs Test Group

Mercury and non-mercury metalic HAPs

HHV Units

% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis)

Btu/lb 0.1

Btu/lb 0.14

Btu/lb 0.12

Btu/lb 0.16

Btu/lb 0.11

Btu/lb 0.17

Btu/lb 0.08

Btu/lb 0.29


HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis)

Mercury

Units

0.01% BRL mg/Kg

0.02% BRL mg/Kg

0.07% BRL mg/Kg

0.01% BRL mg/Kg

0.02% BRL mg/Kg

0.02% BRL mg/Kg

0.03% BRL mg/Kg

0.01% BRL


Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL

BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL

BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL

BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL mg/Kg 0.567

BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL

BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL

BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL

BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL


Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

mg/Kg BRL mg/Kg 0.582 mg/Kg BRL mg/Kg BRL mg/Kg

mg/Kg BRL mg/Kg 0.62 mg/Kg 2.51 mg/Kg BRL mg/Kg

mg/Kg BRL mg/Kg 0.592 mg/Kg BRL mg/Kg BRL mg/Kg

mg/Kg 0.824 mg/Kg 0.706 mg/Kg 1.5 mg/Kg BRL mg/Kg

mg/Kg BRL mg/Kg 0.558 mg/Kg BRL mg/Kg BRL mg/Kg

mg/Kg BRL mg/Kg 0.672 mg/Kg 2.22 mg/Kg BRL mg/Kg

mg/Kg BRL mg/Kg 0.55 mg/Kg 1.81 mg/Kg BRL mg/Kg

mg/Kg BRL mg/Kg 0.641 mg/Kg 2.2 mg/Kg BRL mg/Kg


Note the Proximate/Ultimate data below should be recor

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon

BRL mg/Kg

BRL mg/Kg

BRL mg/Kg

0.126 mg/Kg

BRL mg/Kg

0.182 mg/Kg

0.152 mg/Kg

0.166 mg/Kg

Proximate Analyses, % by wt


e data below should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen

86.3 12.9 0.01 0.25 0.45

87.6 10.9 0.45 0.91 0.01

86.3 13.2 0.03 0.23 0.12

87.5 10.8 0.41 0.93 0.2

86.2 13.2 0.02 0.24 0.2

87.9 10.8 0.44 0.85 0.01

86.7 13.2 0.03 0.25 0.01

87.6 10.9 0.43 0.95 0.01

Ultimate Analyses, % by wt


EIA Facility Code Facility Name Boiler ID

1200067 Cleary Flood 8

Sample Number 

(minimum of 3 composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received)

R10090070-03 [2 Oil] 9/21/2010 9/21/2010 19200.00

R10090070-04 [6 Oil] 9/21/2010 9/21/2010 18350.00

R10090070-05 [2 Oil] 9/22/2010 9/22/2010 19430.00

R10090070-06 [6 Oil] 9/22/2010 9/22/2010 18310.00

R10090070-07 [2 Oil] 9/23/2010 9/23/2010 19380.00

R10090070-08 [6 Oil] 9/23/2010 9/23/2010 18450.00

 Fuel Testing Results


HAPs Test Group

Dioxin/furan HAPs

HHV Units

% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis)

Btu/lb 0.12 0.23

Btu/lb 0.16 0.93

Btu/lb 0.11 0.24

Btu/lb 0.17 0.85

Btu/lb 0.08 0.25

Btu/lb 0.29 0.95


HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis)

Mercury

Units

0.07 %

0.01 %

0.02 %

0.02 %

0.03 %

0.01 %


Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)


Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units


Note the Proximate/Ultimate data below should be 

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon

Proximate Analyses, % by wt


ltimate data below should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen

86.3 13.2 0.03 0.23 0.12

87.5 10.8 0.41 0.93 0.2

86.2 13.2 0.02 0.24 0.2

87.9 10.8 0.44 0.85 0.01

86.7 13.2 0.03 0.25 0.01

87.6 10.9 0.43 0.95 0.01

Ultimate Analyses, % by wt


EIA Facility Code Facility Name Boiler ID

1200067 Cleary Flood 8

Sample Number (minimum 

of 3 composite samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher 

Heating 

Value (HHV)

(as 

received)

R10090070-01 [2 Oil] 9/20/2010 9/20/2010 19240.00

R10090070-02 [6 Oil] 9/20/2010 9/20/2010 18270.00

R10090070-03 [2 Oil] 9/21/2010 9/21/2010 19200.00

R10090070-04 [6 Oil] 9/21/2010 9/21/2010 18350.00

R10090070-05 [2 Oil] 9/22/2010 9/22/2010 19430.00

R10090070-06 [6 Oil] 9/22/2010 9/22/2010 18310.00

R10090070-09 [2 Oil] 9/24/2010 9/24/2010 19340.00

R10090070-10 [6 Oil] 9/24/2010 9/24/2010 18340.00

 Fuel Testing Results


HAPs Test Group

Non-dioxin/furan organic HAPs

HHV Units

% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis)

Btu/lb 0.1

Btu/lb 0.14

Btu/lb 0.12

Btu/lb 0.16

Btu/lb 0.11

Btu/lb 0.17

Btu/lb 0.01

Btu/lb 0.05


HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis)

Mercury

Units


Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)


Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units


Note the Proximate/Ultimate data below should be reco

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon Carbon

86.3

87.6

86.3

87.5

86.2

87.9

86.3

87.3

Proximate Analyses, % by wt


a below should be recorded on a dry basis (including ash).

Hydrogen Nitrogen Total Sulfur Oxygen

12.9 0.01 0.25 0.45

10.9 0.45 0.91 0.01

13.2 0.03 0.23 0.12

10.8 0.41 0.93 0.2

13.2 0.02 0.24 0.2

10.8 0.44 0.85 0.01

13.3 0.01 0.25 0.1

10.8 0.41 0.92 0.5

Ultimate Analyses, % by wt


EIA Facility Code Facility Name Boiler ID

1200067 Cleary Flood 8

Sample Number (minimum 

of 3 composite samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received)

R10090070-01 [2 Oil] 9/20/2010 9/20/2010 19240.00

R10090070-02 [6 Oil] 9/20/2010 9/20/2010 18270.00

R10090070-03 [2 Oil] 9/21/2010 9/21/2010 19200.00

R10090070-04 [6 Oil] 9/21/2010 9/21/2010 18350.00

R10090070-05 [2 Oil] 9/22/2010 9/22/2010 19430.00

R10090070-06 [6 Oil] 9/22/2010 9/22/2010 18310.00

 Fuel Testing Results


HAPs Test Group

Acid gas HAPs

HHV Units

% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis)

Btu/lb 0.1 0.25

Btu/lb 0.14 0.91

Btu/lb 0.12 0.23

Btu/lb 0.16 0.93

Btu/lb 0.11 0.24

Btu/lb 0.17 0.85


HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis)

Mercury

Units

0.01 %

0.02 %

0.07 %

0.01 %

0.02 %

0.02 %


Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)


Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units


Note the Proximate/Ultimate data below should be record

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon

11 ppm

10 ppm

15 ppm

16 ppm

9 ppm

11 ppm

Proximate Analyses, % by wt


data below should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen

86.3 12.9 0.01 0.25 0.45

87.6 10.9 0.45 0.91 0.01

86.3 13.2 0.03 0.23 0.12

87.5 10.8 0.41 0.93 0.2

86.2 13.2 0.02 0.24 0.2

87.9 10.8 0.44 0.85 0.01

Ultimate Analyses, % by wt


Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the 

Fuel Units of Measure - HHV

anthracite Btu/lb

bituminous Btu/gallon

subbituminous

lignite

coal refuse (culm or gob)

No.2 Fuel Oil (distillate)

No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals

synfuel mg/g

petroleum coke μg/g

other mg/Kg

nit of measure to the orange hightlighted cell, if necessary.

Units of Measure - Cl, Fl

%

ppm