Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

1200067 Cleary

Flood 8 No.6 Fuel Oil (residual or bunker C)Fuel Type 2 Fuel Type 3 Other Fuel Description

No.2 Fuel Oil (distillate) Note 1: separate samples were taken for No. 6 and No. 2 oil each day of testing Note 2: No. 2 Oil was about 7-10% of the total (combined No. 6 and No. 2) oil flow rateNote 1: separate samples were taken for No. 6 and No. 2 oil each day of testing Note 2: No. 2 Oil was about 7-10% of the total (combined No. 6 and No. 2) oil flow rateEIA

Facility Code Facility Name Boiler ID Basis An alyte 1200067 Cleary Flood 8 As Received Higher Heating Value 1200067 Cleary Flood 8 As Received % Moisture 1200067 Cleary Flood 8 As Received % Ash 1200067 Cleary Flood 8 As Received % Sulfur 1200067 Cleary Flood 8 Dry basis Higher Heating Value 1200067 Cleary Flood 8 Dry basis % Ash 1200067 Cleary Flood 8 Dry basis % Sulfur 1200067 Cleary Flood 8 Dry basis Antim ony 1200067 Cleary Flood 8 Dry basis Arsenic 1200067 Cleary Flood 8 Dry basis Beryllium 1200067 Cleary Flood 8 Dry basis Cadmium 1200067 Cleary Flood 8 Dry basis Chlorine 1200067 Cleary Flood 8 Dry basis Chromium 1200067 Cleary Flood 8 Dry basis Cobalt 1200067 Cleary Flood 8 Dry basis Fluorine 1200067 Cleary Flood 8 Dry basis Lead 1200067 Cleary Flood 8 Dry basis Manganese 1200067 Cleary Flood 8 Dry basis Mercury 1200067 Cleary Flood 8 Dry basis Nickel 1200067 Cleary Flood 8 Dry basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) D240

D482 D1552

SW6010B SW6010B SW6010B SW6010B E776/9253 SW6010B SW6010B D3761 SW6010B SW6010B SW7470 SW6010B SW6010BEIA Facility Code Facility

Name Boiler ID 1200067 Cleary Flood 8

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) R10090070-01 [2 Oil] 9/20/2010 9/20/2010 19240.00 R10090070-02 [6 Oil] 9/20/2010 9/20/2010 18270.00 R10090070-03 [2 Oil] 9/21/2010 9/21/2010 19200.00 R10090070-04 [6 Oil] 9/21/2010 9/21/2010 18350.00 R10090070-05 [2 Oil] 9/22/2010 9/22/2010 19430.00 R10090070-06 [6 Oil] 9/22/2010 9/22/2010 18310.00 R10090070-07 [2 Oil] 9/23/2010 9/23/2010 19380.00 R10090070-08 [6 Oil] 9/23/2010 9/23/2010 18450.00 Fuel Testing ResultsHAPs Test Group

Mercury and non-mercury metalic HAPs

HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) Btu/lb 0.1 Btu/lb 0.14 Btu/lb 0.12 Btu/lb 0.16 Btu/lb 0.11 Btu/lb 0.17 Btu/lb 0.08 Btu/lb 0.29HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units 0.01 % BRL mg/Kg 0.02 % BRL mg/Kg 0.07 % BRL mg/Kg 0.01 % BRL mg/Kg 0.02 % BRL mg/Kg 0.02 % BRL mg/Kg 0.03 % BRL mg/Kg 0.01 % BRLAn timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL mg/Kg 0.567 BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL BRL mg/Kg BRL mg/Kg BRL mg/Kg BRL mg/Kg BRLChromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units mg/Kg BRL mg/Kg 0.582 mg/Kg BRL mg/Kg BRL mg/Kg mg/Kg BRL mg/Kg 0.62 mg/Kg 2.51 mg/Kg BRL mg/Kg mg/Kg BRL mg/Kg 0.592 mg/Kg BRL mg/Kg BRL mg/Kg mg/Kg 0.824 mg/Kg 0.706 mg/Kg 1.5 mg/Kg BRL mg/Kg mg/Kg BRL mg/Kg 0.558 mg/Kg BRL mg/Kg BRL mg/Kg mg/Kg BRL mg/Kg 0.672 mg/Kg 2.22 mg/Kg BRL mg/Kg mg/Kg BRL mg/Kg 0.55 mg/Kg 1.81 mg/Kg BRL mg/Kg mg/Kg BRL mg/Kg 0.641 mg/Kg 2.2 mg/Kg BRL mg/KgNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Fluorine (Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h Fixed Carbon BRL mg/Kg BRL mg/Kg BRL mg/Kg 0.126 mg/Kg BRL mg/Kg 0.182 mg/Kg 0.152 mg/Kg 0.166 mg/Kg Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen

86.3 12.9 0.01 0.25 0.45 87.6 10.9 0.45 0.91 0.01 86.3 13.2 0.03 0.23 0.12 87.5 10.8 0.41 0.93 0.2 86.2 13.2 0.02 0.24 0.2 87.9 10.8 0.44 0.85 0.01 86.7 13.2 0.03 0.25 0.01 87.6 10.9 0.43 0.95 0.01 Ultimate Analy

ses, % by

wtEIA Facility Code Facility Name Boiler ID 1200067 Cleary Flood 8

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) R10090070-03 [2 Oil] 9/21/2010 9/21/2010 19200.00 R10090070-04 [6 Oil] 9/21/2010 9/21/2010 18350.00 R10090070-05 [2 Oil] 9/22/2010 9/22/2010 19430.00 R10090070-06 [6 Oil] 9/22/2010 9/22/2010 18310.00 R10090070-07 [2 Oil] 9/23/2010 9/23/2010 19380.00 R10090070-08 [6 Oil] 9/23/2010 9/23/2010 18450.00 Fuel Testing ResultsHAPs Test Group

Dioxin/furan HAPs

HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) Btu/lb 0.12 0.23 Btu/lb 0.16 0.93 Btu/lb 0.11 0.24 Btu/lb 0.17 0.85 Btu/lb 0.08 0.25 Btu/lb 0.29 0.95HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units 0.07 % 0.01 % 0.02 % 0.02 % 0.03 % 0.01 %An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis)Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

UnitsNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Fluorine (Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h Fixed Carbon Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen 86.3 13.2 0.03 0.23 0.12 87.5 10.8 0.41 0.93 0.2 86.2 13.2 0.02 0.24 0.2 87.9 10.8 0.44 0.85 0.01 86.7 13.2 0.03 0.25 0.01 87.6 10.9 0.43 0.95 0.01

Ultimate Analy

ses, % by

wtEIA Facility Code Facility Name Boiler ID 1200067 Cleary Flood 8

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) R10090070-01 [2 Oil] 9/20/2010 9/20/2010 19240.00 R10090070-02 [6 Oil] 9/20/2010 9/20/2010 18270.00 R10090070-03 [2 Oil] 9/21/2010 9/21/2010 19200.00 R10090070-04 [6 Oil] 9/21/2010 9/21/2010 18350.00 R10090070-05 [2 Oil] 9/22/2010 9/22/2010 19430.00 R10090070-06 [6 Oil] 9/22/2010 9/22/2010 18310.00 R10090070-09 [2 Oil] 9/24/2010 9/24/2010 19340.00 R10090070-10 [6 Oil] 9/24/2010 9/24/2010 18340.00 Fuel Testing ResultsHAPs Test Group

Non-dioxin/furan organic HAPs

HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) Btu/lb 0.1 Btu/lb 0.14 Btu/lb 0.12 Btu/lb 0.16 Btu/lb 0.11 Btu/lb 0.17 Btu/lb 0.01 Btu/lb 0.05HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

UnitsAn timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis)Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

UnitsNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Fluorine (Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h Fixed Carbon Carbon 86.3 87.6 86.3 87.5 86.2 87.9 86.3 87.3 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Hydrogen Nitrogen Total Sulfur Oxygen 12.9 0.01 0.25 0.45 10.9 0.45 0.91 0.01 13.2 0.03 0.23 0.12 10.8 0.41 0.93 0.2 13.2 0.02 0.24 0.2 10.8 0.44 0.85 0.01 13.3 0.01 0.25 0.1 10.8 0.41 0.92 0.5 Ultimate Analy

ses, % by

wtEIA Facility Code Facility Name Boiler ID 1200067 Cleary Flood 8

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) R10090070-01 [2 Oil] 9/20/2010 9/20/2010 19240.00 R10090070-02 [6 Oil] 9/20/2010 9/20/2010 18270.00 R10090070-03 [2 Oil] 9/21/2010 9/21/2010 19200.00 R10090070-04 [6 Oil] 9/21/2010 9/21/2010 18350.00 R10090070-05 [2 Oil] 9/22/2010 9/22/2010 19430.00 R10090070-06 [6 Oil] 9/22/2010 9/22/2010 18310.00 Fuel Testing ResultsHAPs Test Group

Acid gas HAPs

HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) Btu/lb 0.1 0.25 Btu/lb 0.14 0.91 Btu/lb 0.12 0.23 Btu/lb 0.16 0.93 Btu/lb 0.11 0.24 Btu/lb 0.17 0.85HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units 0.01 % 0.02 % 0.07 % 0.01 % 0.02 % 0.02 %An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis)Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

UnitsNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Fluorine (Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h Fixed Carbon 11 ppm 10 ppm 15 ppm 16 ppm 9 ppm 11 ppm Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen 86.3 12.9 0.01 0.25 0.45 87.6 10.9 0.45 0.91 0.01 86.3 13.2 0.03 0.23 0.12 87.5 10.8 0.41 0.93 0.2 86.2 13.2 0.02 0.24 0.2 87.9 10.8 0.44 0.85 0.01

Ultimate Analy

ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm