# Filename: **C:\PROGRA~2\Documentum\CTS\docbases\ProDocbase\config\temp_sessions\829904501995469794\[EPA-HQ-OAR-2013-0290-DRAFT-0039.xls]Wet Scrubber #2 D-F Data** Date: 12/1/14

Plant name: Dal Italia LLC Location: FACID: Test date: 5/10-5/16/10 UNITID: Equipment: Roller Kilns #3,4 Control device: Wet Scrubber #2 Gas Volum. Emission Process

Run Test O2

# conc.,volume, flow rate, Mass, Concentration, rate, rate, Emission factor, Pollutant No. Method % DSCF DSCFM g BDL MW gr/dscf ppm vd @7%O2 

# lb/hr ton/hr lb/ton lb/lb HCl 1 M320 36.5 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 36.5 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! 3 36.5 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! HF 1 M320 36.5 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 36.5 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! 3 36.5 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! @7%O2 

# PM 1 M5 #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! 3 #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Muskogee, OK

1 of 3

# Gas Volum. Emission Process Run Test O2

# conc.,volume, flow rate, Mass, Concentration, rate, rate, Emission factor, Pollutant No. Method % DSCF DSCFM g BDL MW gr/dscf ppm vd @7%O2 

# lb/hr ton/hr lb/ton lb/lb

ug gr/dscf mg/dscm @7%O2 

# Antimony 1 M29 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! 3 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Arsenic 1 M29 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! 3 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Beryllium 1 M29 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! 3 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Cadmium 1 M29 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! 3 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Chromium 1 M29 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! 3 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Cobalt 1 M29 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! 3 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Lead 1 M29 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! 3 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Manganese 1 M29 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! 3 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Mercury 1 M29 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! 3 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Nickel 1 M29 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 of 3

# Gas Volum. Emission Process Run Test O2

# conc.,volume, flow rate, Mass, Concentration, rate, rate, Emission factor, Pollutant No. Method % DSCF DSCFM g BDL MW gr/dscf ppm vd @7%O2 

# lb/hr ton/hr lb/ton lb/lb 3 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Selenium 1 M29 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! 3 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!
ng gr/dscf ng/dscm @7%O2 

# g/hr g/ton g/lb CDD/CDF 1 M23 18.6 146.7 50,239 71.8 7.55E-09 17.28 104.41.47E-03 #REF! #REF!

2 19.0 161.7 51,264 61.6 5.88E-09 13.46 98.41.17E-03 #REF! #REF! 3 18.8 162.9 51,356 88.6 8.39E-09 19.19 127.01.67E-03 #REF! #REF! Average 18.8 50,953 7.27E-09 16.64 110.01.44E-03 #REF! #REF! TEQ 1 M23 18.6 146.7 50,239 1.70 1.79E-10 0.408 2.473.49E-05 #REF! #REF!

2 19.0 161.7 51,264 1.72 1.64E-10 0.376 2.753.27E-05 #REF! #REF! 3 18.8 162.9 51,356 2.29 2.17E-10 0.497 3.294.34E-05 #REF! #REF! Average 18.8 50,953 1.87E-10 0.427 2.843.70E-05 #REF! #REF! Notes:

3 of 3DIOXIN-FURAN PARTICLE CATCH **Wet Scrubber #2** Measured wt, ng Measured wt, pg Measured wt, pg Congener Run 1 Run 2 Run 3 Congener Run 1 Run 2 Run 3 Congener Flag Run 1 Flag Run 2 Flag Run 3 Total TCDD 6.57 6.51 11.2 Total TCDD 6570 6510 11200 Total TCDD 6570 6510 11200 Total PeCDD 6.56 6.62 9.71 Total PeCDD 6560 6620 9710 Total PeCDD 6560 6620 9710 Total HxCDD 9.08 7.76 10.7 Total HxCDD 9080 7760 10700 Total HxCDD 9080 7760 10700 Total HpCDD 10.2 8.22 13.4 Total HpCDD 10200 8220 13400 Total HpCDD 10200 8220 13400 Total OCDD 39.3 32.4 43.4 Total OCDD 39300 32400 43400 Total OCDD 39300 32400 43400

Total dioxins 71.71 61.51 88.41 Total TCDF 0.0504 0.0738 0.0966 Total TCDF 50.4 73.8 96.6 Total TCDF 50.4 73.8 96.6 Total PeCDF 0.00557 0.0456 0.0351 Total PeCDF 5.57 45.6 35.1 Total PeCDF 5.57 45.6 35.1 Total HxCDF 0.0136 0.0052 0.00366 Total HxCDF 13.6 5.2 3.66 Total HxCDF 13.6 5.2 3.66 Total HpCDF 0.000770.00076 0.00066 Total HpCDF 0.77 0.76 0.66 Total HpCDF < 0.77< 0.76< 0.66 Total OCDF 0.0078 0.0038 0.0061 Total OCDF 7.8 3.8 6.1 Total OCDF < R 7.8< R 3.8<R 6.1

Total furans0.07814 0.12916 0.14212 TOTAL CDD/CDF 71.7881 61.6392 88.5521

Measured wt, ng TEQ, ng Measured wt, pg Measured wt, pg Congener Run 1 Run 2 Run 3 Run 1 Run 2 Run 3 TEF Congener Run 1 Run 2 Run 3 Congener Flag Run 1 Flag Run 2 Flag Run 3 2,3,7,8 TCDD 0.768 0.744 1.09 0.768 0.744 1.09 1 2,3,7,8-TCDD 768 744 1090 2,3,7,8-TCDD 768 744 1090 1,2,3,7,8 PeCDD 0.705 0.78 0.941 0.705 0.78 0.941 1 1,2,3,7,8-PeCDD 705 780 941 1,2,3,7,8-PeCDD 705 780 941 1,2,3,4,7,8 HxCDD 0.345 0.271 0.35 0.0345 0.0271 0.035 0.1 1,2,3,4,7,8-HxCDD 345 271 350 1,2,3,4,7,8-HxCDD 345 271 350 1,2,3,6,7,8 HxCDD 0.414 0.377 0.473 0.0414 0.0377 0.0473 0.1 1,2,3,6,7,8-HxCDD 414 377 473 1,2,3,6,7,8-HxCDD 414 377 473 1,2,3,7,8,9 HxCDD 0.908 0.834 1.05 0.0908 0.0834 0.105 0.1 1,2,3,7,8,9-HxCDD 908 834 1050 1,2,3,7,8,9-HxCDD 908 834 1050 1,2,3,4,6,7,8 HpCDD 4.15 3.36 5.87 0.0415 0.0336 0.0587 0.01 1,2,3,4,6,7,8-HpCDD 4150 3360 5870 1,2,3,4,6,7,8-HpCDD 4150 3360 5870 Total OCDD 39.3 32.4 43.4 0.011790.00972 0.01302 0.0003 OCDD 39300 32400 43400 OCDD 39300 32400 43400 Total CDD congeners 46.59 38.766 53.174 1.69299 1.715522.29002 Measured wt, ng TEQ, ng 2,3,7,8 TCDF 0.0138 0.0076 0.01230.001380.00076 0.00123 0.1 2,3,7,8-TCDF 13.8 7.6 12.3 2,3,7,8-TCDF 13.8 < R 7.6 12.3 1,2,3,7,8 PeCDF 0.00470.00752 0.00460.00014 0.000230.00014 0.03 1,2,3,7,8-PeCDF 4.7 7.52 4.6 1,2,3,7,8-PeCDF < R 4.7 7.52< R 4.6 2,3,4,7,8 PeCDF 0.0051 0.00726 0.00842 0.001530.002180.00253 0.3 2,3,4,7,8-PeCDF 5.1 7.26 8.42 2,3,4,7,8-PeCDF < R 5.1 7.26 8.42 1,2,3,4,7,8 HxCDF 0.0027 0.0025 0.00170.000270.000250.00017 0.1 1,2,3,4,7,8-HxCDF 2.7 2.5 1.7 1,2,3,4,7,8-HxCDF < R 2.7 < R 2.5< R 1.7 1,2,3,6,7,8 HxCDF 0.0046 0.0055 0.0041 0.00046 0.000550.00041 0.1 1,2,3,6,7,8-HxCDF 4.6 5.5 4.1 1,2,3,6,7,8-HxCDF < R 4.6 < R 5.5< R 4.1 2,3,4,6,7,8 HxCDF 0.002 0.00267 0.0021 0.0002 0.000270.00021 0.1 2,3,4,6,7,8-HxCDF 2.0 2.67 2.1 2,3,4,6,7,8-HxCDF < R 2.0 2.67< R 2.1 1,2,3,7,8,9 HxCDF 0.0014 0.002270.000990.00014 0.00023 9.9E-05 0.1 1,2,3,7,8,9-HxCDF 1.4 2.27 0.99 1,2,3,7,8,9-HxCDF < 1.4 2.27< 0.99 1,2,3,4,6,7,8 HpCDF 0.0057 0.0059 0.0045 5.7E-05 5.9E-05 4.5E-05 0.01 1,2,3,4,6,7,8-HpCDF 5.7 5.9 4.5 1,2,3,4,6,7,8-HpCDF< R 5.7 < R 5.9< R 4.5 1,2,3,4,7,8,9 HpCDF 0.0019 0.002 0.00066 1.9E-050.00002 6.6E-06 0.01 1,2,3,4,7,8,9-HpCDF 1.9 2.0 0.66 1,2,3,4,7,8,9-HpCDF< R 1.9 < R 2.0< 0.66 Total OCDF 0.0078 0.0038 0.0061 2.3E-06 1.1E-06 1.8E-06 0.0003 OCDF 7.8 3.8 6.1 OCDF < R 7.8 < R 3.8< R 6.1 Total CDF congeners 0.04970.04702 0.04547 0.0042 0.00454 0.00484 **TOTA L CDD/CDF (TEQ)**  46.6397 38.81353.2195 1.69719 1.720062.29486 √ 7/17/12 √ 7/17/12 √ 7/17/12

R indicates that the ion abundance ratio for this compound did not meet the acceptance criterion.

EPA-HQ-OAR-2013-0290-DRAFT-0039 Wet Scrubber #2 D-F Data 12/1/2014R indicates that the ion abundance ratio for this compound did not meet the acceptance criterion.

EPA-HQ-OAR-2013-0290-DRAFT-0039 Wet Scrubber #2 D-F Data 12/1/2014

# Filename: **C:\PROGRA~2\Documentum\CTS\docbases\ProDocbase\config\temp_sessions\829904501995469794\[EPA-HQ-OAR-2013-0290-DRAFT-0039.xls]Wet Scrubber #2 D-F Data** Date: 12/1/14

Plant name: Dal Italia LLC Location: FACID: Test date: 5/10-5/16/10 UNITID: Equipment: Spray Dryer Control device: Fabric Filter Gas Volum. Emission Process

Run Test O2

# conc.,volume, flow rate, Mass, Concentration, rate, rate, Emission factor, Pollutant No. Method % DSCF DSCFM ng BDL MW gr/dscf ng/dscm @7%O2 

# g/hr ton/hr g/ton g/lb CDD/CDF 1 M23 18.0 147.2 49,226 8.96 9.39E-10 2.15 10.301.80E-04 #REF! #REF!

2 18.5 146.4 49,677 8.04 8.47E-10 1.94 11.23 1.64E-04 #REF! #REF! 3 18.0 143.5 51,422 11.48 1.23E-09 2.82 13.52.47E-04 #REF! #REF! Average 18.2 50,108 1.01E-09 2.30 11.691.97E-04 #REF! #REF! TEQ 1 M23 18.0 147.2 49,226 0.114 1.19E-11 0.0273 0.1312.29E-06 #REF! #REF!

2 18.5 146.4 49,677 0.143 1.51E-11 0.0346 0.2002.92E-06 #REF! #REF! 3 18.0 143.5 51,422 0.1035 1.11E-11 0.0255 0.1222.23E-06 #REF! #REF! Average 18.2 50,108 1.27E-11 0.0291 0.1512.48E-06 #REF! #REF! Notes: Muskogee, OK

1 of 1DIOXIN-FURAN PARTICLE CATCH **Spray Dryer** Measured wt, ng Measured wt, pg Measured wt, pg Congener Run 1 Run 2 Run 3 Congener Run 1 Run 2 Run 3 Congener Flag Run 1 Flag Run 2 Flag Run 3 Total TCDD 0.354 0.335 0.222 Total TCDD 354 335 222 Total TCDD 354 335 222 Total PeCDD 0.368 0.186 0.251 Total PeCDD 368 186 251 Total PeCDD 368 186 251 Total Hx CDD 0.28 0.339 0.391 Total Hx CDD 280 339 391 Total Hx CDD 280 339 391 Total HpCDD 0.685 0.629 0.696 Total HpCDD 685 629 696 Total HpCDD 685 629 696 Total OCDD 7.26 6.54 9.91 Total OCDD 7260 6540 9910 Total OCDD 7260 6540 9910

Total dioxins 8.947 8.029 11.47 Total TCDF 0.0024 0.0019 0.0014 Total TCDF 2.4 1.9 1.4 Total TCDF < 2.4< 1.9< 1.4 Total PeCDF 0.00130.000990.00056 Total PeCDF 1.3 0.99 0.56 Total PeCDF < 1.3< 0.99< 0.56 Total Hx CDF 0.0011 0.001 0.00052 Total Hx CDF 1.1 1.0 0.52 Total Hx CDF < 1.1< 1.0< 0.52 Total HpCDF 0.0018 0.0017 0.001 Total HpCDF 1.8 1.7 1.0 Total HpCDF < 1.8< 1.7< 1.0 Total OCDF 0.004 0.0023 0.0026 Total OCDF 4.0 2.3 2.6 Total OCDF < R 4.0< R 2.3<R 2.6

Total furans 0.01060.007890.00608 TOTAL CDD/CDF 8.95768.03689 11.4761

Measured wt, ng TEQ, ng Measured wt, pg Measured wt, pg Congener Run 1 Run 2 Run 3 Run 1 Run 2 Run 3 TEF Congener Run 1 Run 2 Run 3 Congener Flag Run 1 Flag Run 2 Flag Run 3 2,3,7,8 TCDD 0.0593 0.0729 0.051 0.0593 0.0729 0.051 1 2,3,7,8-TCDD 59.3 72.9 51.0 2,3,7,8-TCDD 59.3 72.9 51.0 1,2,3,7,8 PeCDD 0.0384 0.0529 0.037 0.0384 0.0529 0.037 1 1,2,3,7,8-PeCDD 38.4 52.9 37.0 1,2,3,7,8-PeCDD 38.4 52.9 37.0 1,2,3,4,7,8 Hx

CDD 0.0089 0.0091 0.0120.000890.00091 0.0012 0.1 1,2,3,4,7,8-Hx CDD 8.9 9.1 12.0 1,2,3,4,7,8-Hx CDD < R 8.9 < R 9.1 12.0 1,2,3,6,7,8 Hx

CDD 0.015 0.0254 0.013 0.00150.00254 0.0013 0.1 1,2,3,6,7,8-Hx CDD 15 25.4 13.0 1,2,3,6,7,8-Hx CDD < R 15 25.4< R 13.0 1,2,3,7,8,9 Hx

CDD 0.0769 0.0845 0.06530.007690.008450.00653 0.1 1,2,3,7,8,9-Hx CDD 76.9 84.5 65.3 1,2,3,7,8,9-Hx CDD 76.9 84.5 65.3 1,2,3,4,6,7,8 HpCDD 0.285 0.261 0.2990.002850.00261 0.00299 0.01 1,2,3,4,6,7,8-HpCDD 285 261 299 1,2,3,4,6,7,8-HpCDD 285 261 299 Total OCDD 7.26 6.54 9.91 0.002180.001960.00297 0.0003 OCDD 7260 6540 9910 OCDD 7260 6540 9910 Total CDD congeners 7.7435 7.0458 10.38730.11281 0.142270.10299 Measured wt, ng TEQ, ng 2,3,7,8 TCDF 0.0024 0.0019 0.00140.000240.000190.00014 0.1 2,3,7,8-TCDF 2.4 1.9 1.4 2,3,7,8-TCDF < 2.4< 1.9< 1.4 1,2,3,7,8 PeCDF 0.00130.000990.00056 3.9E-05 3E-05 1.7E-05 0.03 1,2,3,7,8-PeCDF 1.3 0.99 0.56 1,2,3,7,8-PeCDF < 1.3< 0.99< 0.56 2,3,4,7,8 PeCDF 0.00150.000940.000540.000450.000280.00016 0.3 2,3,4,7,8-PeCDF 1.5 0.94 0.54 2,3,4,7,8-PeCDF < R 1.5< 0.94< 0.54 1,2,3,4,7,8 Hx

CDF 0.000950.00088 0.0007 9.5E-05 8.8E-050.00007 0.1 1,2,3,4,7,8-Hx CDF 0.95 0.88 0.70 1,2,3,4,7,8-Hx CDF < 0.95< 0.88<R 0.70 1,2,3,6,7,8 Hx

CDF 0.000860.000790.00041 8.6E-05 7.9E-05 4.1E-05 0.1 1,2,3,6,7,8-Hx CDF 0.86 0.79 0.41 1,2,3,6,7,8-Hx CDF < 0.86< 0.79< 0.41 2,3,4,6,7,8 Hx

CDF 0.00092 0.00230.00044 9.2E-050.00023 4.4E-05 0.1 2,3,4,6,7,8-Hx CDF 0.92 2.3 0.44 2,3,4,6,7,8-Hx CDF < 0.92< R 2.3< 0.44 1,2,3,7,8,9 Hx

CDF 0.0011 0.001 0.000520.00011 0.0001 5.2E-05 0.1 1,2,3,7,8,9-Hx CDF 1.1 1.0 0.52 1,2,3,7,8,9-Hx CDF < 1.1< 1.0< 0.52 1,2,3,4,6,7,8 HpCDF 0.0021 0.00130.00076 2.1E-05 1.3E-05 7.6E-06 0.01 1,2,3,4,6,7,8-HpCDF 2.1 1.3 0.76 1,2,3,4,6,7,8-HpCDF< R 2.1< 1.3< 0.76 1,2,3,4,7,8,9 HpCDF 0.0018 0.0017 0.001 1.8E-05 1.7E-050.00001 0.01 1,2,3,4,7,8,9-HpCDF 1.8 1.7 1.0 1,2,3,4,7,8,9-HpCDF< 1.8< 1.7< 1.0 Total OCDF 0.004 0.0023 0.0026 1.2E-06 6.9E-07 7.8E-07 0.0003 OCDF 4.0 2.3 2.6 OCDF < R 4.0< R 2.3<R 2.6 Total CDF congeners 0.01693 0.0141 0.008930.001150.001030.00054 **TOTA L CDD/CDF (TEQ)**  7.76043 7.0599 10.39620.11396 0.14330.10354 √ 7/17/12 √ 7/17/12 √ 7/17/12

R indicates that the ion abundance ratio for this compound did not meet the acceptance criterion.

EPA-HQ-OAR-2013-0290-DRAFT-0039 Spray Dryer D-F Data 12/1/2014

# Filename: **C:\PROGRA~2\Documentum\CTS\docbases\ProDocbase\config\temp_sessions\829904501995469794\[EPA-HQ-OAR-2013-0290-DRAFT-0039.xls]Wet Scrubber #2 D-F Data** Date: 12/1/14

Plant name: Dal Italia LLC Location: FACID: Test date: 5/10-5/16/10 UNITID: Equipment: Tile Dryer Control device: None Gas Volum. Emission Process

Run Test O2

# conc.,volume, flow rate, Mass, Concentration, rate, rate, Emission factor, Pollutant No. Method % DSCF DSCFM ng BDL MW gr/dscf ng/dscm @7%O2 

# g/hr ton/hr g/ton g/lb CDD/CDF 1 M23 18.9 150.4 3,581 2.38 2.45E-10 0.560 3.893.41E-06 #REF! #REF!

2 18.8 147.9 3,516 1.113 1.16E-10 0.266 1.761.59E-06 #REF! #REF! 3 18.3 147.1 3,561 1.999 2.10E-10 0.480 2.572.90E-06 #REF! #REF! Average 18.7 3,553 1.90E-10 0.435 2.742.63E-06 #REF! #REF! TEQ 1 M23 18.9 150.4 3,581 0.0461 4.74E-12 0.01084 0.07536.59E-08 #REF! #REF!

2 18.8 147.9 3,516 0.0370 3.86E-12 0.00884 0.05855.28E-08 #REF! #REF! 3 18.3 147.1 3,561 0.0937 9.83E-12 0.0225 0.1201.36E-07 #REF! #REF! Average 18.7 3,553 6.14E-12 0.0141 0.08478.50E-08 #REF! #REF! Notes: Muskogee, OK

1 of 1DIOXIN-FURAN PARTICLE CATCH **Tile Dryer** Measured wt, ng Measured wt, pg Measured wt, pg Congener Run 1 Run 2 Run 3 Congener Run 1 Run 2 Run 3 Congener Flag Run 1 Flag Run 2 Flag Run 3 Total TCDD 0.169 0.137 0.647 Total TCDD 169 137 647 Total TCDD 169 137 647 Total PeCDD 0.0852 0.0331 0.241 Total PeCDD 85.2 33.1 241 Total PeCDD 85.2 33.1 241 Total HxCDD 0.111 0.00413 0.0559 Total HxCDD 111 4.13 55.9 Total HxCDD 111 4.13 55.9 Total HpCDD 0.223 0.0924 0.149 Total HpCDD 223 92.4 149 Total HpCDD 223 92.4 149 Total OCDD 1.75 0.842 0.899 Total OCDD 1750 842 899 Total OCDD 1750 842 899

Total dioxins 2.3382 1.10863 1.9919 Total TCDF 0.00079 0.00083 0.001 Total TCDF 0.79 0.83 1.0 Total TCDF < 0.79< 0.83< 1.0 Total PeCDF 0.00193 0.00074 0.0013 Total PeCDF 1.93 0.74 1.3 Total PeCDF 1.93< 0.74< 1.3 Total HxCDF 0.00132 0.00071 0.00078 Total HxCDF 1.32 0.71 0.78 Total HxCDF 1.32< 0.71< 0.78 Total HpCDF 0.00089 0.00092 0.0016 Total HpCDF 0.89 0.92 1.6 Total HpCDF < 0.89< 0.92< 1.6 Total OCDF 0.0416 0.00134 0.0028 Total OCDF 41.6 1.34 2.8 Total OCDF 41.6 1.34< 2.8

Total furans0.04653 0.00454 0.00748 TOTAL CDD/CDF 2.38473 1.11317 1.99938

Measured wt, ng TEQ, ng Measured wt, pg Measured wt, pg Congener Run 1 Run 2 Run 3 Run 1 Run 2 Run 3 TEF Congener Run 1 Run 2 Run 3 Congener Flag Run 1 Flag Run 2 Flag Run 3 2,3,7,8 TCDD 0.028 0.026 0.0699 0.028 0.026 0.0699 1 2,3,7,8-TCDD 28 26 69.9 2,3,7,8-TCDD <R 28<R 26 69.9 1,2,3,7,8 PeCDD 0.0117 0.00914 0.0211 0.0117 0.00914 0.0211 1 1,2,3,7,8-PeCDD 11.7 9.14 21.1 1,2,3,7,8-PeCDD 11.7 9.14 21.1 1,2,3,4,7,8 HxCDD 0.00556 0.001 0.0051 0.00056 0.0001 0.00051 0.1 1,2,3,4,7,8-HxCDD 5.56 1.0 5.1 1,2,3,4,7,8-HxCDD 5.56<R 1.0<R 5.1 1,2,3,6,7,8 HxCDD 0.00522 0.002 0.003 0.00052 0.0002 0.0003 0.1 1,2,3,6,7,8-HxCDD 5.22 2.0 3.0 1,2,3,6,7,8-HxCDD 5.22<R 2.0<R 3.0 1,2,3,7,8,9 HxCDD 0.0185 0 0 0.00185 0 0 0.1 1,2,3,7,8,9-HxCDD 18.5 6.9 12 1,2,3,7,8,9-HxCDD 18.5<R 6.9<R 12 1,2,3,4,6,7,8 HpCDD 0.1 0.0399 0.0594 0.001 0.0004 0.00059 0.01 1,2,3,4,6,7,8-HpCDD 100 39.9 59.4 1,2,3,4,6,7,8-HpCDD 100 39.9 59.4 Total OCDD 1.75 0.842 0.899 0.00053 0.00025 0.00027 0.0003 OCDD 1750 842 899 OCDD 1750 842 899 Total CDD congeners 1.91898 0.92004 1.0575 0.04415 0.03609 0.09267 Measured wt, ng TEQ, ng 2,3,7,8 TCDF 0.00079 0.00083 0.001 7.9E-05 8.3E-05 0.0001 0.1 2,3,7,8-TCDF 0.79 0.83 1.0 2,3,7,8-TCDF < 0.79< 0.83< 1.0 1,2,3,7,8 PeCDF 0.0041 0.00074 0.0013 0.00012 2.2E-05 3.9E-05 0.03 1,2,3,7,8-PeCDF 4.1 0.74 1.3 1,2,3,7,8-PeCDF <R 4.1< 0.74< 1.3 2,3,4,7,8 PeCDF 0.0018 0.0019 0.002 0.00054 0.00057 0.0006 0.3 2,3,4,7,8-PeCDF 1.8 1.9 2.0 2,3,4,7,8-PeCDF <R 1.8<R 1.9<R 2.0 1,2,3,4,7,8 HxCDF 0.0068 0.00062 0.00069 0.00068 6.2E-05 6.9E-05 0.1 1,2,3,4,7,8-HxCDF 6.8 0.62 0.69 1,2,3,4,7,8-HxCDF <R 6.8< 0.62< 0.69 1,2,3,6,7,8 HxCDF 0.0025 0.00056 0.00062 0.00025 5.6E-05 6.2E-05 0.1 1,2,3,6,7,8-HxCDF 2.5 0.56 0.62 1,2,3,6,7,8-HxCDF <R 2.5< 0.56< 0.62 2,3,4,6,7,8 HxCDF 0.00082 0.0006 0.00066 8.2E-05 0.00006 6.6E-05 0.1 2,3,4,6,7,8-HxCDF 0.82 0.6 0.66 2,3,4,6,7,8-HxCDF <R 0.82< 0.6< 0.66 1,2,3,7,8,9 HxCDF 0.00042 0.00071 0.00078 4.2E-05 7.1E-05 7.8E-05 0.1 1,2,3,7,8,9-HxCDF 0.42 0.71 0.78 1,2,3,7,8,9-HxCDF < 0.42< 0.71< 0.78 1,2,3,4,6,7,8 HpCDF 0.016 0.0016 0.0012 0.00016 1.6E-05 1.2E-05 0.01 1,2,3,4,6,7,8-HpCDF 16 1.6 1.2 1,2,3,4,6,7,8-HpCDF <R 16<R 1.6< 1.2 1,2,3,4,7,8,9 HpCDF 0.0026 0.00092 0.0016 2.6E-05 9.2E-06 1.6E-05 0.01 1,2,3,4,7,8,9-HpCDF 2.6 0.92 1.6 1,2,3,4,7,8,9-HpCDF <R 2.6< 0.92< 1.6 Total OCDF 0.0416 0.00134 0.0028 1.2E-05 4E-07 8.4E-07 0.0003 OCDF 41.6 1.34 2.8 OCDF 41.6 1.34< 2.8 Total CDF congeners 0.07743 0.00982 0.01265 0.00199 0.00095 0.00104 **TOTAL CDD/CDF (TEQ)** 1.99641 0.92986 1.07015 0.04615 0.03704 0.09372 √ 7/17/12 √ 7/17/12 √ 7/17/12

R indicates that the ion abundance ratio for this compound did not meet the acceptance criterion.

EPA-HQ-OAR-2013-0290-DRAFT-0039 Tile Dryer D-F Data 12/1/2014

# Filename: **C:\PROGRA~2\Documentum\CTS\docbases\ProDocbase\config\temp_sessions\829904501995469794\[EPA-HQ-OAR-2013-0290-DRAFT-0039.xls]Wet Scrubber #2 D-F Data** Date: 12/1/14

Plant name: Dal Italia LLC Location: FACID: Test date: 5/10-5/16/10 UNITID: Equipment: Glaze Lines Control device: Fabric Filter Gas Volum. Emission Process

Run Test O2

# conc.,volume, flow rate, Mass, Concentration, rate, rate, Emission factor, Pollutant No. Method % DSCF DSCFM g BDL MW gr/dscf mg/dscm @7%O2 

# lb/hr ton/hr lb/ton lb/lb PM 1 M5 #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! 3 #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Muskogee, OK

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# Gas Volum. Emission Process Run Test O2

# conc.,volume, flow rate, Mass, Concentration, rate, rate, Emission factor, Pollutant No. Method % DSCF DSCFM g BDL MW gr/dscf mg/dscm @7%O2 

# lb/hr ton/hr lb/ton lb/lb

ug Antimony 1 M29 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! 3 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Arsenic 1 M29 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! 3 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Beryllium 1 M29 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! 3 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Cadmium 1 M29 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! 3 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Chromium 1 M29 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! 3 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Cobalt 1 M29 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! 3 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Lead 1 M29 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! 3 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Manganese 1 M29 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! 3 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Mercury 1 M29 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! 3 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Nickel 1 M29 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! 3 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

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# Gas Volum. Emission Process Run Test O2

# conc.,volume, flow rate, Mass, Concentration, rate, rate, Emission factor, Pollutant No. Method % DSCF DSCFM g BDL MW gr/dscf mg/dscm @7%O2 

# lb/hr ton/hr lb/ton lb/lb Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Selenium 1 M29 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0!

2 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! 3 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Average#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #REF! #DIV/0! Notes:

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