**~t~** R?•..,08 

### n:: 

## o?;!::vaa- ONn:**~~AL SftVICES~**  LLC WAftS I'ROl'XU st7MlU.ar Ver5iOD·Q6.04 • : TWZ-JJU26
. 

### ., JSlliESS: US l\DlY £MI:mEEll CEN'l'D 

### n:w, iPT ••••• : •• DXXECTOR. OF l"UBLI:C WORD**D~** 1.: -J..ll4 1ST 

### sr awe :2229" 

# .....**~:** AT%.'1' DPW £E BLDG ":2101· I.TY/ 

## 'f FORT LEONARD WOOD ORr:. 

### .' ,sn NAME: DECOJI WArD·TREATED VX**~** GB TO Dli.DO:IJrG WATER S'tANDAIWS .OC&SS**G~'HHG** HAS'l'E: DECON OF CHEHI:CAL WEAPONS RECOGN1T:r.ON' TRAXNXNG COM BIP. IIJI,KE: NON-REGULATED to..T!!:UAL DDL.· DJ'!:SC:


# ,._ IODlml H'fl)ltOXD!: >11-'t'Rl: .Cill:M:J:CALS Sl:Jl'Blt TROPICAL B:t.EACa 

## -0"""""' TltAC&$' OF VX ,_ND Gil AGJUI'l' ARB lJltUTRAL:I.ZED Wl:TR llLEACR AHD R.:r.NS'ED 1fl:T8 TSOUSANDS OF GALLON's OF WATU# 'l'KER COLLECTED FOR X!fCXRERA'X'l:ON.**~** HATER**X~** TESTED PJU:OR TO SH:rl'M£Wr TO ENSUR.E**.COMPL~C&** WXTR**DR~** WAT'Kil S'l'AliiDlt.aDS. VX AND G&**~;::a,A~~:N s.::~~Enl:I'XBD**  '1'0 BS BELOW 20 l'I'B**~** AltB tJSUALLY**N1lMIU!:~** •••••••• : 1.42-4.-44.1
. l'UONE ••••• : ••• : EXPI.RES ••••••• : 07/24/10 STA'IUS •• - ••..• :. APl'it FOR**S~V FEP£~**  EPA XD:**M0~213720979** STATE. EPA rD •• :**92900l.!r9~9** El'X' STATU"S •••• 1 tnni£TEIUIINUL SALES OFFICi: •• :**lU~K.**


# ""' 

# " 1 1 KAX tm:r.T**tiESCJti~:I.lm'** 100 \:.



# ' '
5 '

"· Hlri.'ALS ickel. as N.i 

### "rm,.il.ium lUll 

# " ToX/TC? PHYSJ:o.L**~STJ:CS** l'hysical. State..·.-!: Li.quid T1 Jtari.u. aa 

# ••

.:a..i.W. a$ Cd < b.J;ooaium tot Cr e&d ac 

### Pb •**'Sil~er** as Ag 

# :,.ntiaa

.. y

azuu:tium 1011.0 

# ""'' 1.0 

## .,n 

# '·' 

# ""'' s.o il&g/1**5.~** 

# ""''**F~ash** Point •••••• :**~-** 200 pli:

................ :.05.0**~** 09.0 Col.or •••..••..••• : V,f!Jtl:ES**Odo~~:** •••••••**~** •••••• lllOliE La.yers ••••••••••• < SLngle Layer Specific**G~avity.:** 0.,50- 1.1.50 Free Liqu.ida ••••• : 99

- 100 cyani.des ••••••••. : < 5 CL

PPH 

## ' -roru. 

# ....... -

:r::sen.ic 

# •• 

# .. 5.0 

# ·' ' 

# """ ""'' Su1:f.id.es •.••••••• : < PC&'J···;;
....... : K/A Ploehol.;lcs •••••••• • < . 3 .I':PM

. ·TOT.1U;o. ppra..**Regu.bt.~d** by. t;b**~** 71>1: .•• ercury 

# •• 

# •• :ll.er 

# J=**·Po~**

Odl.. el-1.UDt.**a.~** 

# .. ' < 1.0 L'br.oa:i.Wil· Hex 

### mg11 % "'l'a¥able •••••••• r Tz-eatmflnt Cod
.... : T0"1**~** 

### RPT OTr .••••• : EPA Permit ••••••• : Hazard Class .•.•• : Stat.e Codes •••.•• : 050002 Beiu:ene ..•...... : Pack.ing- Group •••. ' Process Codes ••.. : DI2 Cert:. of D•t.rct- ltq: Y 10 OOT UN/NA lfBlt:**Ma~eri.a.l** Cl.a.ss: EXP:

NESKAP•



### RANDuNG • N-DJi::x l:NNER. GLOVE rriu proshi,el.d 

### :r., l:I 

## '-

.. ·.1::HD'*iai.m;: NrTRl:L£ (.J:NNE:R**G~OV£1**

ll·KAU.Ji. 

### w'rJ:H**,OEC~KJ.>OSJ:hON PR.OD~~S** **~F** 

### riB{yx-:**~J:Vl;.** CA'TEGOltY: A (FOR ·sCHEi:itTLmG ONLY}··

raSte Type**··o~_Code** DOT "PaoPtii-iES Oral: 1 ·

· B219 

# ' Flallomabie:. 0 PPM •



# VES 003100

# < m (/) 

### 0 0 

# w**~** 

### 0**~** 

# ... 

# .


# .

## TWI Laboratory. Analysis Report Receiver 

## #: 3284'30 Sample·Required**#ofDru~:1** Oate: 

### 712/2008

·.?file#: 396926 

## ..nerator. US ARMY ENGINEER CENTER FLW



## . Oesaipt DECON WI.\TER,TREATED VX 

### & GB TO DRINKING WATER STANDARDS

Process Code(s): Dl2 ·



### · Sample Number 

### 284140 

# I 001069294FLE



### Drum Rep 

### I Comp BULK/0 Drum Storage Compatablrtty 

### ·Profiled DOT Hazard**Cl~_9** 

### __ P=Pass F=Fail 8A 

### 415



# -- 

# -- 

# --

Free liquid 

### (%) 100 

# I 

# tiUIIIIIIIIm· Protae Conform Date Initials 

### P.umpable YES 

# 284140

# ~ 

# "'" "" 

# """"' YesjNo 01/03/08 

# ..

· La¥ers/Phases**~%** Ea. 100 i 

# f0,. "'""""'" ""'

# ~"" Colo' colorless 

# i 

# 10-. ""'""' """ "" 10-.""-""

. Turbidfty .tr;;snaparent 

# ' 10-.""'-""'-"""""'""'" 10-.""'-""'-"

· Visco.sity**1~** 

# ' L 

# I ' i 

### .Physical .state: liquid i 

# 10-.""-"-""**~"** 

# '\:**10,.~'\; ~ater** **Misci~il'rty** Mise

# ~""'""~"**~ 10,.~"\** 

.**Ad.~· ~sc;rii?tion** 



### . WatOc Rl!i!Otillily No tutti

# ~""""""'~**~"~ Radia~on**  

### Screen -BKG =BKG X



### . Ram. POt Screen NEGATIVE 

### See Rashpoint X



### pH Screen 6 at 100 pent 

### 2-12.5 X 

## Oxidizer Screen POSITIVE As 0 

### Hg 0

# ~"~ · Paint Filter. 

## Test 

# .,. Be 0 

### K 0

# 10-.~

. Cyanide Screen NEGATIVE 

# c.:d 0 

### Na 0

# 10-.""-~

Sulfitte 

### Screen NEGATIVE 

### Cr 

### .o 

## Pb 0

# ~"~ lncide:ntal Odor
. ·No 

# 10-.""- ""'"""'""' ""'""'"**10-.~**

. . SpecifiC Grnvfty 1.02**0.~50-1.15\l**

# ~~"' 01/03/D_B 

# ...

BTUILb <500 

### 1 -5000

# ~""-""-'\ 01/03/.08 

### SL

### %~Jeride <0.5 

### 2 -0

# ~""'" 01{03/08 RIIH

.**R~Sh ~oint-**  

### Oeg 

### F >140

# 0:.."-~ 01/01/00 

### PCBs 

### By GC- mg/kg 

### <50ppm
. . r;n/03/0S**PCBs~screen-** 

### ppm <50ppm 01/01/0Q !·· 

### 2,4,5-

### Ttsil~ex: ppm I

# ~'""'""'""''"**~"""'"** 0!/0t/00



# .. pep· 

### screen ..., ppm 

# 10-. ""'" """""'"

# ~"""' Ol/Ol/00 pH byMett;:r 

# 10-. ""'"

# ~" ""'""'"

# ~"""'" 01/01/00 Additional Comments: MAY EXHIBiT 

### POSmVE OXID:IZER DUE TO BLEACH-GENERATOR DOES NOT WANT TO ADD 0003. 

### Profile Review for Appendix WAP-C Consitituents by: CAK ·


### , Date: 7/212008 1 

### ·Reactive 

## Category: A Add. Commenls: 01- WATER WITH DECOMPOSITION PRODUCT OF GB/VX



# VES 003102

# i1NI Laboratory Analysis 'Report Receiver#: 328431 Sample Required. ## Qf Drums: 1 

### '\;Jle: 7/212008

!>file 

### #: 396926
.

### -~US ARMY ENGINEER CENTE.R FLW

. 

### pesaipt: DECON WATER-lREATED VX & 

### GB TO DRINKING WATER STANDARDS

. Process Code{s): 012

Sample Number 

### 2941391 ·001069272n..& 

### Drum Rep I 

### Comp Drum Storape**c~Patabirrty** 

## Profiled DOT 

## Hazan! 

## a.Ss _9_.
_ P =Pass 

### F=Fail 

### ·sA

__ 

# us: __ 415
__

Free 

### Uq!Jid (%) BULK/0 · 

# 1•• I Profile Conform Dale 

### Initials Pumpable 

# 284139**~'\.'\.'\.'\.'\.'\.'\.~** YesjNo 07/03/08 KZ

# ~'\.~)_'\.~**~'\.'\.'\**

# ~""""'~"'-'\

# ~"""**LarersJPt~ases** 

# -%ea. 100 coloriless 

### Color 

## .. Turt)ldity transpaNnt

# ~"**~~** "'-.

"'-.



# "'-."**~** 

# "'-.



# "'-." Vtscosity 

### L 

# "I X**Ph~** 

### State liquid

# ~:..~"'-.'>--"**~**

# ~""" .

# ~"" 

# """ '\.

# ~**~'\.'\."\** ·**~ater** 

### Miscibility Mise



### . · Add. 

### DescriPtion- • Water Reaptivity No 1001

# ~**~** 

# '\."" ""0:**~"~** R.a9iation Screen =BKG X



### · Aam. Pol Screen NEGATIVE See Aashpoint X



### ·. pH Screen a at 100 pent 

### 2-12.5 X



### Oxidizer Screen POSITIVE 

## As 0 N/A 

### Be 0 

### Cyanide Screen NEGATIVE 

### Cd 0



### - Sulfide Screen 

## C< 0



### lncideiltal Odor No 

### Spec!Hc Gravil)' 1 .• o1
. 

### 0.950-1
.. 150



### . BTU/Lb <.soo 1 -SilOS



### -. %**Chi~;Jrid~** :<0.5 

### 2 -0



## FlaSh Point- Deg 

## F >140 

### PCBs BY GC
- mglkg


### . <50ppm O'U03/08**P~creen:-ppm** 

### :<:50ppm

. · Ol/01/00 

### ,2,4,5'-T/Si!Yex ·ppm I 

### PCP Screen- ppm 

### pH by Meter 

### Additional Comments: MAY EXHIBIT POSITIVE OXIDIZER DUE TO BLEACH-GENERATOR DOES NOT WANT TO ADD 0003. Profile Review for Appendix \fr/AP..C Consitituents 

### by: 

## cAK - · 1 

### Date: 712/2008 i 

### Reactive Category: A Add. Comments: 01- WATER WITH DECOMPOSffiON PRODUCT OF GB/VX



# VES 003103!pOrt;: lt1008 \.Tit: 07/'ll./08 Otmr:.'**~-** fi.K_Vl:CES, LLC WASTE P_ROFn.B SUHHAllY


### ms:um:ss. P.utXER 

### ABn 'i>P't' •• :: •• :**~J:?.~S** 1: :Zl20 PJU.NER AVE 'lDII.ES.$ 2 ;_ HI 4.9001

'UTE NAME:· ct'MnOE .SOLV'l'l:OiJ Ll:Q'trmS 

### Ri:nmu •••••**.-~- ~**  PROBE.: •••••**~·-•** EXP:nt'ES ••• - ••• : 07/02/U STATtJS ••••••••**~** APPil 

### lfOJl _s'E:II.V FEDERAL EPA XD: MXDOOSSl.SBSl STATE**EPA~--=** 92,0019'§' EPA STA'I'US •••• ; C:ID: R£S'I'Rl:CT SALES OFRCB •• : Dft

.. ')lbe!E.S$**aem:RAT~** IUSTE:**CL~** BATH Ll:QUIDS FROM ELEC't'llOPLATitHG OPERAXl:O**SliXP~--m.M£;** HAS'l'E COUOS:rv£.. LYQUms, ':I'OXIC, N.O.s

### 'K00L~ pRSC:
.

## ~~~"l'RX Criztto.i.s _; WATU{Ol:L •**~ ~YJi.lttDE**  

### Sot.UT:rovs. L:IQ.Ul:D**~ALS** EP TOX/TCLP**~i.zeU.i.e** as A$ S. 0 

### o:,..;a.i- as Cd l.. o r.e.ad as Pb 5.0 W.-nn.\il'y Al5 89 .l s•l.-tum. •• ·s. .., 1.11**~VAl** Rex lfic:ke.l.

.... lf.l '.rh&l.l.i-.xm 

### a:sr '!'l 

# ..,,, og/1 

# ""'' 

# """ ,..,, PRXS:iCAL CIIAR.ACl'£aiSTCS**Pbyai~al State~**  •.• Liquid 1!'l.as:h Point •.••.. ; 100

- 200 CL pll

...............**~ ~2.5**  - U.O Color •••••••••••• : ULLOW Odor- ••••••••••••• t NONB Layers ••••••••••• ; SlAgle Layer**spe~i£ie** GraYity.: 0.750- 1.158 Free Liquids ••.•. ; .,5

- 100 cyanideD ...•• · •••. :< 5 .Su1ficles ••.•.•••• : < 3 ·l'PH PPH PCB's •••••..•• : •• : ppm, Regul.abttd by 40 CFR**'tt01~**

Federal Code:;;; 0003 FOO' D002 POOl. PheDOlics ••••••.• : < \:. TaXallole. •••• - •• -:**~ataeUt.** Code• •• : 1'07 CRQ I!.P'l' Q.TX'

...... ; EPA .Permit •••..•• : Hazard Cl.ass ••••• • 8 Stat'e Codes.- ••••• : 09{)001**B...,:Z~ll;e** •• ·:··•··' Packing' Group •••.**~ I~** **rxo~e&~** Code$ ••••**~** SFl. C•rt of D•trot Rq:**~ lii-D~**  X:m:>er Glove NEO. GREY GLOVES SAA>NEX Tl'l'B C USP:tll CONS'l' FLOW IHbEX{BLU&: NXTR.ILB: UNNER GLOVE) .·SF

- CYAN:IDE SOt.tJTJ:Ofl'. PH :. 12.5**cotl'l'AY~S** Cli'MI':ID'£8"

- DO NOT MIX wi:m Pll < 6.

Waste Type**Fo~** Code Oarllllll; l DO'T PR.OPERTXES**Oral.":-~·**

9].1.9 1 10 PPH

Hateri.a1 c1a:u:. BXP:
Nl!!SIU\.P:



### ae..,i.tb.:. o



# VES 003104

# < m (/) 

### 0 

### 0 

# w**~** 

### 0 

### 01

### ~ -· 

# : : .,-., ·-·;.**~.** 

## ,, ., 

# .. _i,
:·.- .,.·**.:~,**

... 

# ::.**-.~ ·~**  

# '·'



# . :·:·, 

## ..
.- 

### '•:**~;** 

### ·-::· 'I. 

## ... ,•, .:,. 

# . -,._.**~.-** ,. ·.: 

# . 

# . ·**-~** 

# ,, ,I,



# ,.**.~-- ··-~-.;**  

## .. 

## ---·:



# I. '

-i: 

### -' 

# ::.-

. . 

# . . 

## -**-~**



## -·
__ 

### ._ ·.- ..



## ....... 

# . 

# .....

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# . ::'

. ·.:



## .-· .· CO!Of.

_ , 

# .**i>j,,~** JJA.l : 

## - .... - 

## .. , 

# ..**PeS:~ ~~uired**  Sample.Required ·



## ·. ::. 

# . · .. 

# . 

# . . .

·. · orum Storage-tornPabititiity.- 

# · :_**~rofir~~O.~~~:-~** 

# ·.:-> P.=PaSS ·:F7hil: 

## ._,.-. 

## .. .:· 

### :-.**~** . 

## -**BA~-** 

# ·_._.ne·. -' 

# ·"vs
.. · -.- -·---.- .. ,-

__ 

## ,

., 

# ....... Ptcime :

### :cOnt~nn Date_
. ·.·

### l~ls- · ..



## , •. : i•A. 

# :@**T~l** Opq 'NIA 'lP 11..· 

### 0 · .. 

# . ·. 0.. """'" """"" ""

# ~ '\'\.. '\ 

# 0...".'-.'>..'-.""-"-""-" &"'..'\..'\ :.

...... ;· _-; .· 

# ... _ 

## ...... 

# \ · · .· :water**R~ity** 

### I ' · ...... .

### ~; 

## · "Badfati(,n 'sCrf!Ein

. 

## "\J<l.No·RXN ()RXI!O:.. ·.

## ~'\.."-'.."'.""-""-..'\.~~"""'**'.'~** •.• ·

.**~** 

### ,;BKG" ( )>BKG"

. ,.- ' · . "=E!KEl

. 

## :)t: ·:.··: ; : . ·/

... ·:· fo3m:_po(sqOOn · . ·**_:~~-** 

## _, •( ) pos'·-( }BOC. · · · :·: 

## j:'· · : .::- "'·: s'ee AashpQint_ ,)q:· · .· ... . 

## "":"c-o.· pH So/een,_



# . ··.· : ;'· ,J. ,_,. ·.·.·-·:._:,· ' 

# .

. ->-;;. ··'. 

## -·. __ .. · 

### ·: _: 

# :- '• '.: 

### '_'.!)4"1DO% tiW'Io**>f-i~S** 

# · :.:;;: /: >.1>:.ey 

# 'l6 · ·_: :. .. 

# .-· '.l)tl'!'leg**_..·;()Po~.'·.-'"** 

### ··. _."'. 

## -"·JY,· -·"

. 0 

### ·:Hg·-
.. 

# 0.--"""-'\: {;. · ·•;

_("}PaSs. 

### ()Fail (J.V:-Fail.-\)!il'J/,1!..-**·-;a~_(.>:.·····** 

### K :_;.-·**~'\c"'-'\** 

# ':;•:>-**.c<~i'**

'· 

# .

. •' 

# .

. :·:. . .**~** ..**-~---** ... · 

## :

____ ,. 

## - 

## .. 

# .. ·•· . ·_· 

## ..**~** ... 

# .,_ ·:·-· 

## ....... :-. ·. 

## _,.'



# ... ".•



# VES 003106

# ~~:::~~~" . 

# -

# ---~-~--...:.----~ \ ffll tti&,a
... J 

# nn111ySIS

# Rep~--- 

# .•. .---- ··- PCB Analysis 

### Required 

### #of 

# Drums': 11 Date: 5/3012006**_,-·-·~Profile#:639242** 

### · 

### )eneratoc PARKER ABEX. Oescript CY}\.NIOE SOLUTION LIQUIDS 

### ·Process Code(s): SF1 · Sample 

### Required 

# /.
Drum Storage Compatability

## Profiled-DOTH~~**Cl~_8__** ;;

Sample _Number 

### Drum Rop I Comp Free Uquid (%) Pump;;tble

### LayerslP~es -% 

### Ea. Color

. · Turbidit)'

VIScosity



### . · ?_hySical State

Water Miscibility



### ... Add: Description



### .. ) Water R<!llt!Mty · ·

.**RadiatiOnS~** 

### . 

### Aant.Pot. 

### Screen pH Screen**Ox-idizer_S~** 

### . 

### "Paint Riter Test**~yanide** 

### Screen Sulfide 

## Screen IOcidental 

### Odor.


# · · {:s')ecific Gravity 

## 283310 

# I 00011"7974vES 

# gNo

N/A TnsP-

### ~Opq 

# NJApt. .H.

### -~_Part Aoats Sinl<s Emls

## ~No RXN (");RXN: ·

## ~=BKG (_) >BKG:

. 

# • %
NIA lP 

### 1\. 0 NIALMH· Uq 

### sOl S1g.Ss t.tPFSE



### MNeg ( ) Pos ( ) 

# edc.

\ll100% ( )W% 

# /-J"2,**~.** 

## )<) Neg ( ) 

### Pos ( ) Pass ( ) FaU ( ) V-FaU }Q.N(A ' { ) Neg

### ~os 

# ( ) N/A 

### /_/"\11 _()QNeg ( 

### )Pos ( )N/A 

# 1'f No 

### (.)Yes: 3 %·
.NfA TP Tl 0 NIAL.M H 

# P =Pass 

# ii:Pil
81{ 

### 8 

### 415
__


### Profile eonfQnn Date

# ~



# "'-""" 

# "'-

"'-

"'-



# "'-"'"'**~** 

# "'"'"' l 

## )q Uq ·Soi·Sig Ss MPFSE

.



### ---· .=BKG 

## 1--,o
.. int 

# ia >12.5 

# ·.·I As 

### Ee Cd 

### Na 

### Cr lriitials



### . BTU/lb 

## .. ., ;:;!)0

. 

# 1 -1oooo ·**~** 

# "'-**~ f{;-j~;,L**  

# m. 111**%Chlori<!~.** 

### t 

### -5**10-.'x~** 

# __,_. >t4b



# . wruvw mstiluble**aceton~exane** "<50ppm


# : PtP Screen- .ppm·**-~--** . 

# . .. 

# . ' . 

### ()Kit ( 

## YGC 1 

## J 1oo% 

# r J tO"/. :PG;B. analysis to be xletermined upon 

### visual jr..spes;tion of waste
. 

### Ad9filbnai
.. Corilments: SF- CYANIDE SOLUTION, PH > 

### 12.5. If (irum is mostly oll. expect BTU's to be greater 

### tHan 10,000. 

### Profile Reviev.r for

### ~ppendix WAP-'C Consitituents 

### by: CLF

### ~ 

# I
"Date: 

### 712/20{17
. · . 

# I I"{

.

# o:-•'-00~~-.,. 

# . 

# J**'~4i IX~.~,:;·;~.:,**  

# ,: ... ·. .. '

.
VES 003107

### Sample f.!umber 

## 28l310 

# I 000117972VES Drum Rep 

### I Comp 

### T-8/T-2,4-$,8 

## TWI laboratory Analysis Report PCB Analysis 

### Required Sample Required ·

Drum Storage CompatabDity. 

## Profiled DOT 

### Hazard Class 

# _a __ P=Pass 

### F=Fail 

### 8A

# ~4/5



# -- --

Free liquid(%) · 

# (iii 

# I 

# ·111111\ltl Profile 

### Conform 

### D 

### ate lnitiats**Pum~bJe** 

# {fey No 

## 282310 

# 10."' '"' "'-

"'-"'

# ""'~ Y-es[ No 

# <:l:rdm ..IL. Layers/Phases-% 

### Ea. 1· 

# '-1 % 2_l.___%. 3 

### %

.

# ~"' "'-"" 

# """" 

# ""'**~ ~~~**  . .



### Color· 

# f<.(;l)--:-

.**~tt..L6).)**

# ~ 

# "'"'"'"" ""'"'**~ ~"'~** **Tu~idfty** 

### <j{A

### ~T""- 0pq 

### I@TP TL 0 N/A lP 1l 0

# ~ '\,_



# "'"" """**"'~ ~'"'~**  VISCOSity 

# .. N/A(t,MH @L M 

# H NIALMH 

### l 

# f\ Physical Slate 

## !{i9)Sor>d Sludge

........

### l,fq~Ss Uq 

### sor S1!J Ss

# ~ """'"""""" ""0:**~""~** · Water M*tSCJbllity j(.r._fil)Part Floats 

### Sinks Emls 

# M/YF&e. MPFSE 

# 10-. '\..

'\..

'\..

'\..

'\..

'\..

'\..**~**

# ~"""'**~"'d.** DI!Scription

# ~ ..

# -~; nl' 

# t

# B~ f.AtJMZ. 

# ,.

. ];, Reactivity

. 

# lijNoRXN 

# ( ) RXJ:l: 

# /

# ~'~"'-~10-.'\..~ Radlation Sa-een 

# KtJ=BKG ( )>BKG: =BKG 

# lie -, / 

### Ram. Pot Screen MN!'Q 

### ( )Pos ( )BOC 

# ./**~e** 

### Aashpoint 

# l\c .' 

### pH Screen- 

### · )6100% ( po% 

## .>i?...S / 

### >12.5 

# It

· OxKiizer Screen · 

### U)Neg 

### ( )Pos As }ig 

# 10-'\.. '\.."' Paint Riter Test 

## r'(}Pass ( )

## F~~ ( ) '1(-FaB"''liWA 

### Be K

# ~"""' Cyanide Screen


### . .()Neg 

### · bf;Pos ./fJNIA Cd. 

### Na

# ~""'"' : Sulfide Screen· 

### VJ·Neg () Pos ( )NJA Cr 

### Pb

# ~'"'~

Incidental odor· 

### 04:'No ()Yes:

# ~~

# ~'\.."'-~

# ~'""~ . Specifit-Gravity 

# -- 0.750-1.150 

# 10-..""'-"""'
. -"--

BTU/lb.

### -~,._ 

# .L!S:OO 

# ..---- .1 -10000 

# 10-.'\.. '\.."**~..:M3** 

# v-N % Ctd.olide 

# .. fi:;..( 

# .'_.s-- 1/ 

### 1 

### -5

.

# ~"'""~ _j__

# ~- .Rash ·.POint-**Des~** 

### F 

## " >140

# ~""'-"'-~ 'PCI!s By G.C- 

### mglkg · 

# · wnii:n,- 

# - .<50ppm 

## PCBs-Screim- ppin 0 

### <SOppm**~.4~5-oTJSilvex.-** 

### ppm· 

### ' 

# .

# ~"""" 

# """" '-

'\.."" '\**~"-"0:** .. .pCP screea.:... ppm - 

# ( !'Kit (.J 

# GC

# ~"" '\"" '\.."'-._

# ""~ 10-.. "'"'

# ~ · pH 

### u;:::ijoter (')100"k( )10%. 

# 10."'""""""""""" "'"' 

# l0-"'"'"' ·-PCB--analysis to be determined Upon-visual ifl!'iPection 

### of waste 

### r

### Ad~fional**Com~tS:** SF-- CYANIDE

### SOLU'fiON..._~H > 

### 12.5-. If drum is mostly .ojl, eXpect 

### BTU's 

## to be greater 

### than 10,000 .



### . Profile Review f9( 

### Awendlx WAP-C 

### Coositituents uy: CLF

. - '

_ · . . - 

# t·**·~:** 

### 712/2007'
. . .

.

# itai~Cja;,fdes-DONOTmixwithpH-<6 - 

# #:
_ _._.·:_ .. · ·**~** 

# ..,.., :- .· '.'f ·C,
. 

# (p '{

. ' . '

- . ' .

### -~ . -

### ~ 

# . .- . 

### ..**:~. ~** **~-** 

# .

. ' 

# - 

# •tr

.·.-.


# VES 003108

## Receiver#: TK002 1/.ofOrums: 1 

### Date: 6/2912001 Profile#:=

.**~erator.** 

### TRADE WASTE INCINERATION 

## ici;pt

, .-6cess COde(s):

Sample Number 

### 2851.74j ILOOOOOOOl 

### Drum Rep I Comp 1/ Free Uquld 

### (%) 

# I Pumpable NO Layers/Phases-% 

### Ea. Color Turtiidity 

### Viscosity Physical State 

### Water Misability 

### Add. ·oesaiption 

### • -(ater Reactivity .• -adiation Screen 

### Flam. Pot Screen pH Screen at 100 pent Oxidizer Screen Paint Riter Test 

### Cyanide Screen Sulfide Screen

. 

### Incidental Odor Specific Gravity 

### BTU/lb 

### %Chloride Rash· Point - Deg F PCBs 

### By GC
- mg!kg 

### PCBs-screen
- ppm 2,4,5-T/Silvex- 

### ppm I PCP Screen • ppm pH byMe"ter Profile Review for Appendix WAP-c Consitituents by: 

## Date: 

## lWI Laboratol}' Analyois 

## Report \fiswa11Rspceti81 k; 

### Sieve Box 'l:';;lleJ Feede:

Drum Storage**~QlpatabiUty** 

### Profiled DOT Hazard Class _9_._ 

### P =Pass F= 

### Fail 8A

__ 

## as __ 4/s

__ 

# 1111 Profile 

### COnfonn Date 

### Initials 

# 285174 

# i0.."'"' '"'"'"'**~** Yes 

## No 08/01/08 liJ 

# i0..

"'"' "'"'"'"'

# ~ 10.."'-'-0: 

# i0.."'"' '"'"'"'

# ~ 10.."'-"'-'\

# ~"'"""'"""'\**~"'~** l 

# I X

# ~"'" ""'"' "''-0:

# ~"'~

# ~""" "'"'" '-0:

# ~"""**~"""'""~** 

# &"-" =BKG X 

### See Aashpoint X 

### 2-12.5 X 

### As 

## -<>-;vtD Hg 

## -<>-**o.o.;~** 

# 10-.""""" Be 

# +-o."'- K 0 

# 10-."""'" Cd 

# ._ q,s Na 0 

# 10..."-."-." Cr 

# -t'i Pb 

# .._ t. :> 

# 10..'-.'-0:**A~** 

# :: .:?.**35"~** 

# f.

# ~"" ""'"" '-0: 10.."'-'-0: 10..'-."'-" 08/01108 Poi] 

# 10.."'-'-0: 08/0l/08 

# "" 10.."'-"'-" 06/01/08 JF

# ~~" 01/01/00 <50ppm 08/01/08 <50ppm 01/0l/00

# ~""""**~"** 

# """""**\\\."-.~** 01/0l/00 

# li0.."'-"'-"""""0:**10.."'-~** 01/01/00

# ~"" """ "'-0: 

# i0.. '-.'-0: 01/01/00

Add. Comments: 

### The data in the sample information section(6/2912001)is date**profi~** 

### ZZZ2ZZ was 

## created.



# VES 003109**~~>"** ll"IOOS yB·} O"l/31/08 

### otrn ElN.[R.OJQIBl(TAL SEllVI:C:U. LLC JfASTIC PI!.OY.ILE SUMRA11:
J:I'SSS; ll T VANDERBILT COMPANY :otC 

# · ... -.;. IDRE.- '-;: mRI 

### j

t/'1:..

- ': L'AC'l'--= •• VANDERBXL'!' CE£MXCAL-HtmllAT



# ....... JOE CURTIS**~E** )OdiE: Dut.lt M:CX£0**l;ll~S"n:** LIQUIDS lOOCESS GE;N£llATING WI\STE: WASTE ALCOHOLS. SPENT**SCRUBB~** SOLUTIONS, stnn"WAT&
.

p_ NAME: MAST£ ALCOHOLS, N.O.S**~-** 

### D&SC• Verriou 0' .n4 '**Tta~3818S'Z** $ELLD1G li.EGl:OH 

### ta MJU. NDM8E2 •••••••. : 105-0-61,**l'BOHE----·~···"** 2"i0/753-U2f> EXP:IltES •••••.• : 03/l.!/10 S1'1\.T\TS •••••••• : APPR FOR .SEJi(V FEDEIQ.l. EPA 'XD: :cni05llSOZ2!1 

### snn EPA 

### m .. =. 921001UU EPX s:rATdS •• • •• : "CB1t.Jt£STIUC'r SALES OFFJ:CE •• : 'nf:I

MD< - 1Wt UNXT**D'E;S~OH** 

# =· )"lUH Rl:DROA:rriE 

### sdD:rUM .CARBONATE «oN-T1l:t**CS~CAL.S** •J\l.D?ROLS IISOPROPAHOL, £THYL BEXA»>L, ETC) AMDf&S (D:tBUTtL·. OXMETBYL-, D:tAM:n.-, ETC) IoVE:N£DU¥DI'E 

### CJ..UON- oxs'tl'f,FXDE 50 

# • • 0 

# • " 

# • " ' 

# "' so 

# '

2 

# ' 5 

# ' 2 

# •

METALS • EP**~ll'inie** as· AS -;.l.dmi:u• as Cd bead""" t>b H10rcU:ry as. Hq TOX/TCLP 

# '·' JJJog'!l. PII.TS:ICAL**~S'r:ICS** PbyricAl. Stata.**·~:** Liquid < 1'.0 

# ""'''**Fl.~** l"oi.nt ••••.• : < '70 • 13!1 CL 5.0 mg/'}-

.2 ag/1 

### pa ............... : 

## u.s- 14.0 Col. or •••••••••••• : VH.:IES Odor
............. : HOME e!lf!.D.i.1lll\ as Se b.ro•S.um H•'<:**¥l.eke~** &,s N.i .:rhal.l.i.ua as Tl. 1.0 

# '""" La.yers ••••• : • • - •• ; Single Lay!"'t' Spoe.ifie**Cra~ty.: o.~o**  - 1.150 

# )

Fedeial Cod6s:

·11£0. GllE:Y GLOVES _.C.f!Y)**F~ee** Ltquids •• : •• :. !IS- 100 Cyanides ••••••••• : Sul.t:i.de.s ••••••••• : < pca•s ............. : Ph&oo1.ics ••••• - .• : <**%'~i-e** .••••..• : Tx;eaJ:B.e.Dt COdes.·. : T07 '· CRQ .RP't QTY· ••••••. : 1.00 EPA "l'u:Jilit ••••••• :- • Hazard _Cl.as.s ••••• :. 3 St.te COdes .•.•.••**~** Q!IODDl**_B~:zene** .•••••.•• ,; Packing Group .•.• : IX:t Process Codes •••• : BLH Cert of**D~trct** Rq:

DOOl. D002 D.£i U221 VO.!I2 ·DD08

EAlroLJ:IIIC li-DEX J:NHElt Gi.oVB..

- 'l""I'PE C It:tSP.:tR COHST · JtLOW
. 

# -----**-~~~-SuSPECT** AGENT: Lu.fi
. . : CHECk;· COKP)..'l'" CU.EFULLY 

### -to.r CON'l'AniJ

## ~**~** 15\: NadB"

## ~- 

# ma xta)ms

### ;1~-~.':rp R.M!IGE_S :IN CREH COMP. BTU AKP. J>E MAY.-VAU J;REA'rLY·**De:or.a.l.~.** ) 

### .nor PB.OPnhEs Oril1:. 2 5 

### > _ppm.**~a.ted** by 40 CFIL "IU.: l.O

- PPM DOT Ull/JO. NBR:. t!Nl.9B"l Material Class: EU,;

NESHAP:

_'Health: o**~.:**



# VES003110

## .• veTaioti 06.04 'l'H:I.-3811522 >Ort.'. ;RfO'O! rE: 0.,/31:/08

NESS;' BAYER CROP sc:Ui;NC£ ONYX ENVIJU)lOlEdTAL SERVl:CES: • LLC WASTE l:'l!.OFIL£ SIJMH).AY SEt.l.IRG JtEGXOH £AB - 'IO.L JWMBE1L ••**·~----:** 103,·9-594

M'I 4.9445**~ACT··' PilON£---------~**  D_;PntES ••••••• : 01./0S/10 • STATtJS ••••••••**~** APP1t FOil SE&V

FEDElt1oL 

### EPa. XD: J:5:I:D080358351 ·srA'l'E £f/'A ,xn •• t**~260019,9** EPA ftA"l'D'S •••• ;: CBX lt.ES'rlUC'r SALES OFFJ:CE: •• : 'nU: .s:rE JOIH&: MO'l'll£li LXQ001l. RESIDOE l()CftSS GENEIU'.'l'ING_**~ASTE:** PROCESS WJ\STE FROH MANUFACTURlliG OF



# p: :lVoM&•· BAZABJ>OUS to.ST£, Ll:QOID,. 

### a.O.s 

# x.: '..u.ts4: (tm':[KAllOL. GLUFOSJ:NA'l'E AHIIOB:rmll



# .**-~**

### 1-~l: 

### ciiHxO.i:.s**~·t)$INATE:** AMM.oNXUK**~CRLOUDE**

### ~ 

# .. .,.,_, .

ii:::;ntX 'c'lqUll:CALS**~** 

## ·· orftn**ULA~** COMPOUNDS



# .**~.** 

### :**:~·-ALB** 

### SP Teix/Tct.P**-,~As** 5.0 

# '·' s,o



# -• '·' ... 

# ,, "!"911. 

# .. ,, •g/l 

# ..,,, 

# ...... """ """' 

# ' 

# " ' ' ?;D 

# ' 

# ' 5.0 

# ' 

# •• 70'



# • 

# • 

# • t>BYSICAL " OUJIAct'Eltl:ST:ICS Phy:d
.. ca.l State. ••• : Liqni.d Flash Point ••.••• : 1.00

- 200 CL 

### pD---------·····-= o4.o- o&.o Col.or •••••••••••• : 811.0_WN/VltltX'B.S**Od~"¥="·············•** ¥OliE

_ Layf!.X"s •• · .•••••••• ; H\ll.ti Laye.X: Spe.e.i.f:ic: Gra..ri.ty.: 0.,50 -·1.1S0 :Free Liqu.i.CI.s ••.• :·.: U 100 ey.nid.ea· •••.•**~** . .'.: < s DSSCIUl'TXDlf

.·.: 

## - Sul.fidl!!.s.· •••••••• : < l PCB"6 •••••••••• ;.:**l"helu>~ics** ••.••••. : < 't**Taxah~e** •••..•..**~** 10 PP"'•**:Reg:u.1ate~** by 40 CFR 761.:- PPM

·::**~----** .• 

### ;_,,,-.

# ~~---< ,f;:,


# .. . 

# . . . -

FOb).

o.Or-ma1: 2 

# . 

# '**"rt:"ea.~t** Cot;t'es •• : To7**CRQ,~** QTY..., ••••• : Ei'A Parllli.t • ." ••**~** •• : /Ba:z;U4**Cla5~s** ••••• : 9

state Codes •••••• :**09000~** Benz:eue ••••••••• ·: PacldD,g Group •••• : 

### :r:n: 'rocess Codes ..•• : BLL CeJ:"t of pstrct**Rq~**

.

### D~**·pa~~:O:ri£S** 

## _'' 0-.:al: 2' 

# .:n, ;,.**--"-----~** 

# .**....:.,..~"'-'"'>--~·~~~~....,__c** DOT tni/NA NBlh NAJOB2. HateJ:"ial.-' Cl.ass: Ul":
.



## ..**~-**

' 

# .

. -. . . 

# . -·. Beale;:; 0 

# .,

VES 003111

# )



# UNIT 2 WASTE FEED PROFILE ' ·WEEK OF SEPTEMBER 8, 2008 TESTING

.. 

## )

/



# VES 003112... 

### , . 

## _.- ...... _ 

# ')



# ) ... '·

. . 

# . ··-

. 

# ' : 

## - 

# .. ·--· ·'·".;: 

# . ·.- 

## ..**-~** . 

### "· 

# . . . 

# ·- .·

.. ; :-. 

### ·;



## - . 

## -. 

# .· ;; 

## .. - . ·;--. 

## ---·:.· 

# UNIT? TEST CQNDITlONS ._ . : . 

# September; 

# 2008

ciiloririe -- lbS!hr

. - · .. -. · Hexachloroethane (6.4lbstbag in sands)

. 

# Prufu Solids -lbsthr 

# . ·- ..



# .**Ll~ad** 

# N.itrate (2.6 lbslbag) ·

. 

# . . ' 

# High Btu Uquids 

# {i ank 

# 2)
- lbS/hr-

.

. _

Chromic Acid 

# (250 lbslhr) Low Btu

# Uqu.id~ (01)

# -~ lbslhr

. .

# Sp~cialty Liquids

# '-l~sfhr ... '

_ 

### _..



# Solids.:.. Zexel Carlieout Area +Sand (ash) Specialty Feeder- Patker Abex .. .-· :



## ..**~** 

## .--. 

# 200 •250**~** 

# ..



# · 9oo -95o 1d3 i24 ibstcha'rotH



# 500-700
. 

# 9oo 11o(L: ·.

Low Btu Liquids- PQ

. . . . High Btu Liquids- Bayer CropSeience, Cambrex Char1es City, Veolia ES
· Technical Solutions, · Metal Feeds (Spike +Waste Feeds) Lead - 661bslhr ·Chromium
- 

# 45 lbslhr
One Condition, Three .Runs Only

VES 

# 003113**~te"port ~**  R."f 008**)A'rE~** 01/0lFOI 

# ....**Eawn~~i~=s~~P. --~**  \fASTE l'B.bn:t.&

### ~'''"--.: ·.: . V'e.rsi.cn 0'. 04

- •• 

### <Jwr-nuU 

# ""> !3tJS:is£ss : i£X£L CARVEOtJT AB.EA • tELL:mG ll.EGXON" Ll\11**~** NUHIJER. •••••••• : l.f.J:-1-66,**~lt£SS** 1, 212.1 

### s :niBoo£11 CotntT U:.Oftr-""1 2' 

### cx-r···· cON. riECA'rUR R_DNALD W. ELDI>lt 

### wi.sT£: W.HE: SOLJ:DXf"lf!l) St.IJOOE PROH£.· •••••.••• : 3lo('/ti82-l.St0.

XL '"2521..**~PrRES** ••• ; ••• : 02/a_l_/10. STAriJS •••••••• ; APl'll. FOR s£a.v FEDERAL EPA DO:**XLRaoo~~03S'** STAT£**~PA** ID •• : l.lSOl.S$433 EPA STA"t'U"s.: •• : cu:.R:esTa:rcT P&OCESS GENERATING WAST£: SXTE REMEDtATIOII SALES OFPXCE •• : TWX SKrP. NAME:: Hli.ZAilDiluS WAST£. SOLm_ ll(.o.s ADOL. DESc":**(TRXC~It.OETHXLENE,** TE'f'ltACHLoltOnKEHE.-**CXS.-l.-.2-0iciu.oRO~**
.C'IS-1, 2 -DXCHLOROETHENE STYllENE

. TE:Tll.A.Caz.Oao-ETBAN&**~CBLOROETHEN£** 

# ··=- SO:!:L. NoJ,\--nz CR£MlCALS !=00 COB o\BSOltii.Nn""**-~** JU-s'eai.e. aS.ASI Cad-.l.wa .as Cd Lead a:s Pb" Ke.t:'eury as Hg Se.lcm.i...un &s Se Chroold....... Htox Ni.,kd a.s Hi**Th~ll.l.W11** as Tl.



### ····'. EP TOX/TCLP 

## ;;:0. i.o 

# '·' _, LO

. 

# ·-·

DOH 0040 

# ... ,, "'!!ll. 

# ""'" -..g/1. m9/l 

# • 

# "



# .. """· u.ocioo 3100000 

### tJ:Ni:T D"cti.r-1'"1X0N
. 

# .. , 

# .. li'G/tr::G U.lOOO UC/m 

### l1S0oo UGlkG. •• 

### l.o 1i 

# ... "' BllYSXCAL • CKARACTEii.IftJ:cs

### ~i;ica·l**sta~** ..• : Solid. Flash" Poi.-.:r.t.• ••• .._.;;.B./A Ct. pU ••••••• : .••••.•• : 05.0

- 09.0.
· Ccl.cr ••••..••••.• ;; IIR.OWN Ockn;: ••••••••••••• : lfOHE**~yers** ........ .-. -- :, Sl.ngle Layer Specl."tio;;: Cra?tr:**~** o. ooo trae. Llqu.Ld..s ••••• • 0 • lO • Cyio.nid.es: •• ___ •. ,.: < Sul.f:i.c;!.es ••..••••• ; => PCJl•z·-· ••...•.... ;**P~oli-cs** .....•.•. :. < S PPM T<n'AL l 'i>PK t'eTAL

ppm. 1\e<JUl'l-ted by .tO·**C~R** 1·,1;

. 10 

# .....

. "'**"T~a.b1e.** •.**·~-** •••• =**T~e.ut** ·ecdeS •. = T07

CltQ.RPT QTr
.. : ••• : DOT UH/tiA NB.R.; Kl\.3077
EPA- rerai.1.t ••••••• =**~zaxd** 

### Cla.s ••..**~~, Sta~e**  CodU ••••.• " &9oo"oi. 8ea.-i-e
........ 

### -= ·Pack1ng**G~oup** •••• : x:rr**P~ocess Code~**  .•.• : BSH c-c.rt ot:**n"s~rct** aq: He.teri.al Cla.,s' 

# """'

li"ESHAP:.



# s"""""'
. TYPE C: llESPIR COUST FLOW

.



## ,**.:r~~i~..;n..---2.** 

## :·' •.'.- oeroo.,.l: ·2 · DO"l.' PltOPEI'frl:ES oO:a.L: 

### :z

. stnOO.:a.Y 

## .asu 1



# VES 003114

# < m 

# en 0 

### 0 

# w**~ ~**  ()1 

## '.· 

# ,. '•.



# . , 

# .. :· 

# .. ··',·



### ·.·.·, 

# .·::-. :·'. ; 

# .. '.·.



# . . . ..-':·:.



## . :1'·. 

# ...... ,, ;·. :,.: 

# ..

.. :·?



### ..•... · 

# .....

'•·.



## ., ..•.

. 

## ... :-.._ 

# . .. ·

. ,•" 

## :P.B:J20S

# ~o:h.~i~~**_8·Y~~~~.f\ci~i~'.** '**~** 

### ·::;. '!

## As~:·f3s,ss



# · 

# .. , ,.'.



# ....

,• 

## :;
.

## '·Receiver#: 329006 #of Drums: 1 Dale:71:1712008 

### ·t'<r- 

### ·<F. 032206
· G 

## \x: ZEXEL CAmiEOUT AREA 

# V&._.,t SOUDIAED st.!JDGE 

## Process Code(s); BSH



### Sample Number 

### 2846381 000231228VES



### . QrumRepJComp 

### ·Btrr...K/0 - 

## 1WI Lab.;>ratory Analysis RepOrt · Sample Required

.



### _Orum**siorag~** 

### Compatabillty 

## Proilied DOT Hazard'l:las&_·s

__ 

### P=Pass F=Fafl



# -- -·- 

# -- BA 

### 68



# .. Free 

### Uquld (%) 

# • I

. 

# .**~111!~,** 

# I
Profile 

### Confaqn 

### Date Initials· • Pumpable NO

# ~""" """""""""

# """~ !Yes\ No 07/17/08 

### ..._,.,Phasas -% 

### Ea 

# '"

.

# ~""""""""" """""""""

# ~**~""'0** Color boo"!fl -**da~k**

# ~"" ""'""""""''\**~"""~** Tumidity 

# "" 

# 0-""-"'" '"" 0..'-..'-..'-.: .• VISCOSity**~7A** 

## .. NIA 

# I X

· Physical Stale**~lid** 

# 10-"0.."""

# ""'~ 10..'-..'-.." : Water Miscibility Part Floats SiQks

# ~""'""" """"""""""""

# ~**~""'0** :**~-** Description- sludge 

# }r _Reactivity Oo RXN 

# 0..'\..'\..'-..'-..'\..'-..'-..""' 0..'-..'-..'-.:

· t'UK&ia:tion Sa"een 

# .. ,., ·=BKG X



### · Ram. Pol Screen**~IOOATIVE:** 

### See Aashpoiot X



### pl:f 

## ·sC!'een 6 at 1.0 pent 

### 2-12.5. X**~i.Zer** 

### Screen NEGA't:rVB As 

# ,_. Hg -H6- 

### \.0"3

# ~"""""'" P.aintfi!tef Test N/A 

### Be •. 1

# ~""'0 Cyanide Screen NBGA'rEW CYAN'l'E:Sl'IO • 

### Cd 

# '" Na 

# ..**~"""~** Sulfide.S?"een**PO~I'!IVE** 

# ex 1193 ·Pb 

# -.;toy

# ~"""""" Incidental Odor No· 

### A</1 3HA

# ~"" """" """""""" "\:

# ~"""""' Spr!:Cific Gravity 

### 0_.000

- 0.000

# ~""-.'-:-: 01/01/00 

# eruJp> 23-tO 

# zooci -1 

# OQOo 

# .. 0..'\..'\..'\ in/l"l/08 . . % 

### ChloRGe <:0.5 

## 1**-~** 

# .

.

# ~""""" "\ 07/'17ioa

. Aash·Point- Oeg F 

### NIA

# ~""~ 01/01./00



### PCBs-By<iC.: mglkg 

### <50ppm 071.17/08**P~s-Screen** 

### -ppm <SOppm 

## ttoitoo



# . . .



### Z.4.5-TISilveX.- 

# ppm I 

# ffi"'""""**"""'\.~**

# ~""'" 01/01./00



### · PCP 

## screen -ppm

# ~""""" 

# """" "-..""""""

# ~""""**61/01/~0** 

### pH**byM~ter**

# ~**"0.~** 

# "-""'0**~"-.."""** 01{01./00 Addiliorlat Comments: 12 samples 

## were Pl.!lled from 4 rollotf boxes, and the average number was used for metals. 

### P-:ofile Review for Appendix WAP..C Consitituents by: KMEREDITH Date: 2111/2008 · · 

# ..,.

ott TD 

# -

VES 003116

## ___ _... ......**#•~·-~·** 

## ···- .. 

# .**~eceiver** 

## #: 329047 l 

### of Drums: 1 · Uai.Q".]/17}2008 

### · PI
. 

# "!: 032206
.**~** 

### )or: 

## ZEXEt.. CARVEOOT /4REA**·J~** 

### SOUDIRED SLUDGE

. =>rocess COde(s): BSH



## - . 

### Sainpfe 

### Number · 284637 

# f**.00023123~VES** Drum 

### Rep I Camp BULK/0 

# lW( LaboratorY Analysis 

# Report Sample Required



### .Drum**S~e~atabtftty** 

# Profited ooT:.iazard**Clas~** 

# _9
__ .

. P=PasS F=Fail



# --.- _. ___ 4



# -- 8A 

### SB /5



# . Free Uquid 

### (-%} 0 

# I 

# Ullllllill
Profile Coofoon 

### Oat<! lniHals 

### Pumpable NO 

## 284637

.

# ~"'""'"'"'-"'-~ YesjNo 01/1.7/08 

### t.:ayers/Phases -% 

### Ea. 100

# ~ 

# "'-

"'-

"'-

"'-



# "'-

"'-**~ ~"'-."0:**  Colo< bJ;OWQ.

- dart

# ~ 

# """"" "'-

"'-

"'-**"'-~ ~**  

# "'-

"'-

"'\ TUibidlly . N/A 

# 10-. "-

"-

"-

"-

"-

"-

"-

"'\**i0..'-.'.~ V~lly**  

### 'a/A NlA X

.. P!lySicai State

. s61id

# ~ 

# "'-

"'-

"'-



# "'-

"'-



# "'-**~** 

# 10.. "'-

"0: ' Water Miscibility**~art F1oats-~1nks** 

# ~ 

# ""'"**~ '\.~** **~"'-~** .4r.l_d... Oescrip601l II"IU¢-li"ke 

# J!" Reactivity 

# """"" i0..":--,.**~~** 

# "-

"'\: 

# 10.. "-

"-

"'\:**R~ation** Screen 

# .. .., .,eKG X 

### Aam. Pot. Screen NEGATIVE 

### See Rashpolnt X



### . pHSq-een £ a.t. 10 pent: 

### 2-12.5 X



### · Olddizer Screen

. NEGA"l'IVR As 

# ' 

# .. _Hg 

# -··0::>**~** 

# "'-

"'-

"'\ Paint FHter Test N/A 

## Be 0.1

# ~"'-"'-"'\

. Cyaoide screen NEGATIVE Cl7.NT8SMO 

### Cd 198 

## Na 0

# ~"-"-"'

. Sulfide Screen 

### rosrnvE C< 119'3 

### Pb 

# ..... .z..oiO 

# 10-. "'-

"'-

"'\: Incidental Odor" No P.SIJ**u..~R**

# ~ 

# "'-

"'-



# "'-

"'-



# "'-

"'-**~** 

# 10-. "'-

"0:

· Specific !3ravity 

### 0.000

- 

# o.ooo

# ~"'-"'-~ 01.{01/00
.



### BTUA.f? 21.10 

## 2ooo

- toooo·

# ~"'-."'-"'\ O"l/1."1/08**%€hlorid~** <0.5 

## t -5 

# 10-. '\."0: 07/l:rto8 

### Rash Point-**D~;F** 

### >II 

## A

# ~'\."'-.'-' n/01/00



### .**PCB~.** 

### By·GC
- 

### mgfkg 

### <SOppm_ 07/1.7/08 

### : PCBS..Screen 

# -ppm <50ppm 01/0lloo



### 2,4,5-TISilvex- 

### ppm I

# ~" 

# "-.'\."" '\."'-. 

# "'-

"'\**~'-,'-."'\** 01tinjoo
. 

### PCP Screen- 

### ppm

# ~ 

# "'-

"'-

"'-

"'-

"'-

"'-

"'-

"'\:**~"'-~** Ol/01/DO 

### pH by Meter

..

## ~"'-"-"'-"-'\.**"'-."0:~"-'0** 01/01/00 

### AddibOnal Comments: 

### 12 samples were pulled from 4**ro~o~** 

### boxes. and 

### the average nUmber was used for metals. 

### Profile Review for Appendix WAP-C Consltituents by: KMEREDITH · 

### Date: 2/11/2008



## ; 

# ...,



# ""

- 

# ""

VES003117**~-~--.o.....;·** 

### ... ,# •••• ···--·--.--··- ,. •••**----~------** ........ 

# '

. . Receiver#: .329110 tofOtums: 

### 1 late: 7/1712000 

### Per
...... _,.. 1 

### 032206 Gt 

## )t ZEXEL CARVEOUT AREA "J.SUop\: SOUDIFIED SLUDGE 

### 'ro<:ess 

### CodO{s): BSH



# .. ·. ·.·

Sample 

### N1.a11ber 284642 

# t 000231230wS

.. Drum 

### Rep I 

### Comp 

### BULK/0 

## TWI Laboratory Analysis Report Sample Required



### Drum storage**Compata~Jnty** Profiled 

### DOT Hazard 

### C1iJss _9
__ P=Pass F=Fai7. 

### 8A

____ 8B

____ 4ffi

__ __



### o 

# I Pumpable 

# llliiUIIIIUI .284642 Profile Confunn Oatil · 

## ln!fials**~"'"'** "'-.

"'-.

""'-

""'-

""'-

"-': Yesj No 07/1B/oo ""

. l.aye(s/Phases -% Ea**~.oo**



### TUrbidity

. _ Voscosily



## · Physic8t State



### . vilaf.e£**Mis~lity**



### .**~-Cescription** 

# J

ReacliVity
. 

## Ftadiation Saeen 

## F.tam. Pol Screen jlHScreen 

### Oxidi:z;ef Saeen

· Paint Filler Test

: Sulfide 

### Saeeo

Incidental Odor 

### SpeCific Gravity



### , BTU{\.b

%Chloride 

### I'QBs**~y.** 

### GC

- mglkg



### PCP 

## screen- ppm



### . pHbyMetor H/A

soli.d Part Plo_at:s Sinks 

## dirt. plastic. ppe. cl.ot:hi.ng •. 

### and !&.ape**No~·** 

# ..... BOC. 6 at 10 pcut

H/A NBGATIVE L>OSITIVE

. 

## Sno

c; 0.5 

### N/A 

# I "

.

.. 

# 10,."' """""""""""""""' '""'

# ~"~ =BKG 

# • See 

### Acishpolnt X 

### 2-12..5 X As 3.< 

## Be 0.1 

### Cd 198 

### Cc 11.93 

# ... . 7UA" 

### 0.000 • 0.000 

### 2000--10000

. 

### 1 -5

### ~ 

# ""'"0: 07/10/08



### · NIA <SOp!Mn**~ppm 01/0~/.00** 

### ·A:ddi~onal Comments: 12 sa!f1ples

### ~ere polled from 4 rolloff boxes, and the average number was used for met31s. ·Profile 

### Review for**~dix** 

### WAP..f.; Consitituents 

### by: KMERED!rn · 

### Date: 211112008 

# . 

# .,

VES 003118

## 'Receiver#:

# 329~4 #Of Drums: 1 

### 0- 7117/2008**Pre~** 

### -<.f: 032206 

### Gt 

## )x: ZEXEL CARVEDUT AREA D.es....,>t SOUOIFJEO !>LUOGE Process Code(s): BSH.

Sample Number 

### 284643 

# r ••• ,.J.232Vj!S Drum 

### Rep I Comp .BOLK/0 Free Uquid 

### (%) 

### o 

# I Pumpable 110


### _· Layers/Phases-% 

### Ea.. 100



### Color**b~** Tufl>ldity 

# .,.

.**vtseOsl~** N/A

### Physi~t~tat~ solid



### _ Water·M!sabtlity Part Floats SiPks



### Ar,td.**Oesaip~on** !Rld-li.ke**\orR~** 

# ''""'" f<adialion SCreen 

# .. ,., Aam. Pol Screen NEGATIVE**pH~creen** 1 at 10 pent 

### Oxidizer Screen NEGA'l'rv£ Paint Filter Test M/A 

### Cyanide Screen Nl!GATIW**~~tid~** 

### Screen POSITIVB 

### lncidehtal Odor NO**S~Gr.avity** 

## iWI 

## Laboratory Anaiysis Report Sample Required



# . Ull\lltlltl
284543

As 

# '·' Be 0.1 

### Cd 196 

# «r 1193 

# "'" 

# .. : 

# .. OrtJm**st~ge** 

### Compatttbifrty Prollled 

### DOT Hazard Class _9
__ P=Pass 

### F=Fail 

### SA

__ 

## as __ 415
__

PrDme CQnform Date ln16als \\_"""""""" """"""

# ~ Yes 

# I No 07/U/08 >3



### N/A 

# I. X



### =BKG X 

### See Aashpoint X 

### 2-12.5 X



### 0.000-0.000

## ~""**~** 01/01/00 

## BTUil.b 2110 

### 2000 -10000**10..~ 07/18/0~**  

### ... %Chloride. <: 

### 0.5



### -**~-h** 

### POint- 

### Deg F

PGBs**~y** 

### GC
- mglkg- 

### <SOppm tn/1&/o&.**P~E}~~screen** 

### -ppm 

## <SGpp.n- 01/0l/06 2,4.5,-TISilvex- ppm. 

### /. 

### PCP Screen -·ppm 

## PH by Meter Additional Comments: 12 samples were 

### pulled from ·4 roUoff boxes, 

### and the average number was 

### used for metals. Pr6file Review far Appendix WAP-C ConSitittients by: KMEREDtTH 

### Date: 2111/2008



# VES 003119WASTE I'JlOFZL£ SUMMARY '11U-85'16l.7**~** ... TE: '"0.8/20/08

# (~·)· SELLiliG 

## itGxalit: 

## u.a - lW. SINE.SS: PQ COII.P OUT ••••• :**~DR5SS·** 1:**~700·KANSAS** AVE • "lDRESS 2.:

r:TY/ST •• : KANSAS CrrY •NTAt;T•. < D U105-11JB

n5 ;'u>; MONOXSOBVTYLMU:N£**~ Ia~**  lUX mn«BER.
.......... ltl-,-4t4 PllOVE ••••••••• : EXPDlES ••••••• : 03/07/U STATUS •••••••• : APPR POI SERV "l'EDEII.AL 

### El'i ID: KSD00020371l.**STA~** EPA XD •. :**920001~~59** EPA STA"IUS •••• : em:: RBSrR.l:C'l' SALES OFFrCE: •• : P"l'A**lOCt.-~** .GitNERA'TJ:NG NAS"l'£: FLJt.SB COliDbSATZ "I'KOM ZEOLITE AANOI"ACTWINQ iii'·. Nl\Mt: WAST£**~LE** Ll.QtriDS. COJ!.ROSZ\l'E, R •. O.S •• .>DL. DESC: ICONTAXJI'S KONOISOB"UT:ILAMXNE)

1\TD.. NON-iR.l: CHnti:CAt.S HONOXSOBOTYLAMZNE """llXETHYL.AK:INI: CBEMJ:CAL Coiwos:tTX.OR**~** TCA OR. TOTAL Ni.c:kel. a.s Hi. 2.5 Thalli.Ullll as 

### Ti 10

ari.UIII 

# •• 

# •• 2.5

# ·-~ •• Cd 2.5 .hJ:O!I"iwa t"?t; Cr 2.S L•ad. 

# •• 

# •• 2.5 :;:ilve?: 

# •• Ag 2.S .ntboony 2.5 

# """ 

# ... 

# . .. 

# ·- ... HXN

- llAx fn:n"l' DESCHXPTION 60 70 \: 0 0 

# ... 40 • Pllt"Sl"CAL CHUtACTElUST:ICS Pb.pS.c•l State ••• : Li.quid. Fl....,.b Po.i.ut. •.•••**~** 100-- 140 pa

••••••.•..••.•• :. l.2..5- 14.0**~ol.or** ••••••••••.**~.** = VAlUES**OO.o~:** ••••••••••••• : AKXIIE-- .L:IU Layers ••.••.•..•. : sbigl• 

### r. ..**y.~** Spec1fic**G?:aV~ty.:** 0.800 • 1.200 Free Liquid$ ••••• :**·~9** - 100 CL

"anadi.u. 2.5 

# . ... 

# .... 

# ... ... PP.· 

# . ... 

# .... PJ1" 

# .... ey-ides
......... : < S P.PN· TO%AL .-rsen:l.c 

# •• 

# •• 2.0 Merc:ury 

# •• Hg 0.05 lleryll..i.um 2.S •otll.s#:i"IUI 12.5 lodi-u. 

## s.o Selen.i.um aa 

# •• 2.S Z.ino: 2.S \.luaiuum 20.0 

# )**Fede~:al** Codes: DOOI. tl002.

.dEO. GR:&Y GLOVES Pv:c: YELLOW OVR BOOT COVER rNP&X/BLDE NITRILE**$I~ER** GLOVES)**~l:-~UST7C"** LXQUID; FR >10 

# ... ...
....

CPF3**Der~~U~.l.:** l**Wast:~·** Type Foqo CodeCRAAGE Con£:
.. CORL PE VNTl:L**)··31~0!1** SUJ.f.ides •.**~** .•••.• -:: < PCB"s •••••• :.: ••• : N/A Pbenol.ics •••••••• ; None "'· Taxable. ••.••••• :**Tr~t•ent** Codep •. : T07 CAQ RPT QTr ...••• : EPA Permi.·t
..**Ha~ard. cla~s**  ..... : 3 State codes •••••• : 090001 Benz4Zioe ••••••••• :**Pa~.ig Group~**  ••• : Xl: Pll;"oce5s Code$ •.••• : DX1.**Cer~** 

### of**ti•t~:ct** ltq:

:oOT. :PBriPER.'rtl!:S" O>:ra1:**~ Fl~l.ei**  o

Bi19·**"~**

### ~y**co~g.·** 

### "REVl'IOOciJ 

## -. . 

# :

. 

# : _._: . . 

# :**Fo~:MA~~~-** Po.**~~oan** 

### for a/15/oa ·· 3**p~ -~**  ppm.. Re5JUla.t.ed.**~y** 4.0 CFlt 16"1.:

Materi.al Class: EXP:

··.·, 

# .. .·.· . -"."



## -:-,. ::



# VES 003120

# < m (j) 

### 0 

### 0 

# w**~** 

# "'**~** '·"'--'

# ~~~ 

# ;\vasie**T~acki.ig** 

# S%tefri•••· !'·.··

.. ·.·•.··•···
._,_,_,_,.,__ 

# ... ·.··-'--•;-.,-.--·.··--··- -' '.-··-· ,._, __ 

## .. '**~lle** 

### Inventory Print Approvals Chemist Receiving Labor&tory**T~nkFarm** 

### Process Planning 

## Window Billing Help 

# i>rotne Approvals · .-.-, -. "

. 

# . .. ' . "'-" ·. " 

### ,., .. 

### Profile.. 

# ·_f_lric.om
..

# i~l._g**.~n.** al.ty_s.i9. 

# Req. uire. 

# d.
. . '
. ·. . 

# I 

# r**S~ple ~hara~;feJi.~S$.:·.··.':~.'**  ;··::. ·-:..::: : . :

# ;·~·**.·;_.~_--,~~'~** Number
. rf'rocess.Code(•l
. . 

# I DOTH dCI

## rVrscoort~. . ·. 

# '"·'•r-"c. '·I'·• ······-··: J857617 [ID11 

# iJl OiJ 

# J iJ

. ja azar ass ,..,. '**~· •··~·u<.-.**  

# •. ,,,,... .. ...... Aetriei•e 

# j r PCB

# Ana~oi,**Ae,!l"o~d** •. . • .. .**-~-....1** 

### ·· 

# ·r .La!J;.Aun-metals.as**$Pe~ifi~~·below.** 

# r**Dlci~<i~:Pre9ur$Qf An~lyiis** **·R~qUir"ed** 

# r 'Ed1H1'iic:FJ**~** 

# .• ,. .............**~** 

### Update 

## Cancel

# ~I J 

# iJ Visuai_IJ:lS'PSctlon Onl_y 

# r**Visu~llnspection: ~love**  

### BoM 

### I Hooded Feeder 

# .r InSpect Outer 

## Drum Onl,y ·Do 

## Not-Open· Comments 

## Below 

# r**A~ceiving:** 

## Verify 0(iginal Consumer 

## Label and Write Label 

## Info on PDW 

# ·r Decant Sample Required 

# P Sample 

### Requi.red**Anal~tical** 

### COmments**Referen~e** 

## Trocking #I Sample# for**ana~,;~** 

# r "Oio!(iri Precursor analjiSis:·r.es:Uits b.er.ow**s~e** 

## action 

## levels

# r**Nb-!ddl~iot:~~r ~~al9si!**  

## required 

# . r**Rurl.~n e~qh**  

## load 

# ' 'r**A~~IY.tis ,SI..!P.Pii~:d** **b,Y'~ener~tor** 

### ·:See Tech. 

## Manager File

. c••t Updated

# B~: 

# J 

# l r ·**~pe_- i!lri.a~is** **~~ ~8** **detemll.ne~** Upon visual inspection. of

# w.a~te d 'th
. Addrbonal Comments: · mere 1 • · ·



# ---**------~· --~7---------------------~**  Pro 

# rae and H and!ing 

# Comments:;;::· -;:;,·**=:·;::::~·;:;.;;;;;;::-::~:;;;;;;;:--·-------l** 

## Profile A evie"' for AppendiH**W~P·C** 

## Con•tituents**~J':** 

## jKMEREDITH on J311 

## 0/2005 

# r Water 

## A.eactive •**ov~id con.ta~t**  

## with:fnoislute 

# r Contains 

## Cyanids. DO NOT mix·with 

# PI-:!-< 6 

# I - .:::.1**8.t;~nz~.;~ne** 

## NESHAP**~Oritrol$** 

## reguired 

# r Pois-on Inhalation 

## Hazllrd 

# ·r**Cont~im** 

## Acrylonitrile 

# r Contains**Hydrofl~uric** 

## Acid 

# I 3 Reactive

# ~teQOI.Y Additionol Comments:

# .';:;ID~I-~CI\~US~T;!;IC=u"'g""u"'ro'":""P'"'H"7>-.:c1 0;:--------....:.---- 'K 'f12.5 

## NA 

# fs PB·'f2.5 

## 'ASN·j4.48

(**~--~-**

## Receiver#: 329352 #of Drums: 1 Date: 7/2312008 

## J'"'lile II: 857617 ·


# . ""tor. PQ CORP · · 

### .>ipt MONOISOOUTYlAMINE & 

### WATER MIX
· Process COde(s): 011

Sampte Number 

### 2848491 00139n94FLE 

### Drum 

### Rep 

### I Comp 

### BULK/1 TWl Labomory Analysis 

### Report Sample Required

Dnun St{trage Compatability Profiled DOT Hazard Cfass _8
__ P=Pass F=FaH



# -- -- s __ BA 

### 88 41 

# .

Free liquid (%) 100 

# l 

# 11m Prome Confonn 

### D•fs 

### InitialS Pumpable YES· 

## .284849 Laye<i;!Phases -% 

### Ee. 

## ioo
. Color yellolo! 

### Turbidity translucent 

### VIScosity**l~** 

### Physical State liquid 

### Water Miscibility Mise 

### Add. Description**·~er** 

### Reactivity No RXN 

### Radiation screen •BKG 

### Ram. Pol Screen POsrrtvE 

### pH Screen >12.5 at 100 pent 

### Oxidizer Screen NEGA'I'lV£ • 

### Paint Filter Test N/1'. 

### Cyanide Screen NEGATIVE 

### Sulfide Screen NBGATIVE 

### Incidental Odor No Specific Gravity . 0.98 

### BlU/Lb 

# ,..

· %Chloride <0.5



### Rash Point- Oeg 

### F PCBs 

### By GC
- mg/k:g 

### PC8s-5creen- ppm**2,4,5-T/Silvex~ppm** I 

### PCP 

## screen - ppm pH by 

### Meter 100 Pent 12-26 

### Profile Review for Appendix WAP-C Consitituents by; 

### KMEREDITH 

# oate: 3/10/2oo8 Ad.d. Comments: 01-CAUSTIC LIQlltO; PH >10 As 2 

### Be 2.5 

### Cd 2.5 

### Ct 2.5 

# 0-."" """ """"""""" YesjNo 01/24/08 

# .., 0-.

"""""""""" """"" 0-."""""" 0-."""""""""""" """ 0-."" """ 0-."""" """"""""""" 0-."""""" l.. 

# , ...... f0-."""" """"" ""'"""

# ~"" 

# """" f0-.

"''\.."" """ """"

# ~"""""" f0-."""" """""""" """

# ~""""" =BKG 

# - See Flashpoint 

### -""" >12.5 

# < Pb 2.5

# ~""'-~ Hg 0.05

# ~""'-~ Na .JJJ-0. 

# s**~""'-""'-~** K 

### -+- 

## CJ.S 

# 0-."" "-."": 0-.

"""""" """"" "" 0-. """""" 0.800-1.200 

# 0-. """""" 01/24./08 AJ 

### 1 -5000

# ~ 

# ""'-



# ""'-

'\ 01/U/08 MT 

### 1 -5

# ~ 

# ""'-""'- \ 07/24/08 

# """ <73 <140

# ~""'-""'-~ 01/{11/00 

### <SOwm 07/24/08 

### <SOppm 01/01/00


# ::-....



# ""'-

""'-

""'-"" 

# """""""" ::-.... 

# ""'-

""'-"" 01/01/00

# ~ 

# ""'-



# ""'-



# ""'-' '""'- ""'-

'\ 0.. ""'-

""'-**~** Ol./01/00 

# 0..

""'-

""'-

""'-

""'-

""'-

""'-

""'-

\ 0.. ""'-

""'-**~** 07/24{08 AJ



# VES 003122;,pOrt: ll7008 \.'1"£: Q7 /31./08 

### ·**owrx·'EIND~-** !=Eli.VXCES. Lt.C lU.S'1'I'**~Fn.E** stJlQOJI.Y Ven-Lm. 0' .0
..

## ("'fi[--s.na~ 

## · ·**SUJ;~iotll** w.B - 

## Hat.. ;)E:n' •• -.· •• : 

### i:IDa'E:st 1: 222G P.JI..(.l(£R._ AvE 

## tiDRiss 2:. \.::rT" .•**~** CQl ). : HJ: '!1.'001 

### Bi:nmn ••••• ::..**~** 1.4.3.:1--tU l'&ONE: ••••• 

## :··= EXPXRES ••••••• : 07/02/0' tt.&.'I.'US: •••••••• :**APP~ ~lit.**  

### _snv FEi:ID.AL EPA m: MIDOOSSU853 S1:ATE El'A 

### ;p.**~=** S2,00UI'§' EPA S"l"AWS •••• i CU. R.KSTJUCT Sl\LES OFF·XClt •• : DE'l" · AS1'E

### lfAM£~ 

### · CYNnnE

### SOt.oT'IO~ LtQ'amS**~** CENERATU!l WASTE: CLEAHnfG BATH i:rounts FlilOB:. ELEC"rB.OPLATDtG OPEBATJ:O**SEIP~;NAME:** WASTE CORB.OSrv£.**t.t:nli:p~s.** WXJ:C. H.0.s RE 

### crAM:o.>ES u.E. 

### usim**~Dr.~** D'£SC:

## -~:.-n.x**f:::l~EM"ta.Ls,.;** • MA.'rU/O:tL

·: cYJUrtn& 

### Sot.trnOllS.

_**~** EP TO.X/TCLP .l:>:ad:U.c: as ll.s S. G**~-as** Cd 1..0 .ead as Ph S.O te.:euky .a5 Kg**J•le~~.i~** ... 

# s. ·Chroaiua R•M:

. Hiek.el. as Hi.

:b.al.l.ium ali" t"l < < 

# -• LD ""/L mg/L og/L ag/1 ../L PHtSiCAL**-·~n:rcs** Physical State ••• :**il~id** l!'l.a&lh l'Di.ll'C. ••••.: 100

- 200 CL pll •• _ ••••••••••••• : :J.:2.5- 1\1.0 Col.or •••.•••••••• : %ELLOR Odor ••••••••••• ··' MONS**Laye~s** ••••••••••• : Singl• Layer Specific**Gra~ty.: 0.~50**  - 1.1.59 Frea**Li.~ids** ••••• :**~5--** l.Oa CyaA!.d- ..• - .· •• -- 

### =. < 5 _:sd£:ides ••••••••• :_ < 3 ·1'1'1( PPM 

# .-

PCB•$" ••••••••• : •• : ppa. llegul.3.ted by 40 CFR**~lil.:**

_ Federal. Codes: 0003 FOO' 0002 DOOl.

.l·De.K Xnner G1ove**~Yl'E** C R.ESi.>IR CONST FLOW**Olb~/Bt.UE** NITRXt.E IJ:NNER GLOVEJ SF

-**CY~.NrDE SOLUTXOM~**  l'H ;. 12.S Phenol.ics •.•••••• : <**~ T~Le**  •••••••• : 't'r;-eatm.eRt Code• •• ; 'tO., .CR.Q U't' (trY •••••• ; EPJI. -Per:mit .•••••• :
· K&za.rd.: Class ••••• : 1 St:.it.t:e. Codes.· •••••. : 090001 Benx!-D:e- 

## ······4··= l'acklng" Gi':-oU.p ...• : :rt.·**P~c.s~** CodeS •••• : SFL Cert of DstrCt 

### aq:

SARANEX

COKTAll!S**CY~t.OES** - DO NOT Mil Wi:Til I'-ll <:: 6.

lrihal.illtion.:· :.

\'faste Type f"or:m Code -Der.rnal: 3 DOT l'llOl'Ea.Tl:ES Ora.b ·3·**~** 

### iau 

# ' 1.0**PI'~** DOT ON/W.. 011.; OH2 9:Z2 Ma.teri.:o-1 Clas:s:: S:Xl':

Hea.ith::. 0



# VES 003123

# < m (/) 

### 0 0 

# w**~** 

# "' .j>. 

## Number 

# q>>92A.0
?.etrlt!<-'e-

_ . .J_:, 

# /I-**(f;~fQ:;¥0.:~~**

i· 

# '**_U;..d~t~~** 

# Ji·

Cancel .... 

## ·.·J:



# -EJsfr .. La•I.Updoled·ij)< 

# .. fortin



# I 

# :::r :; 

# :· .,. 

# .... __ 

### ,. 

# ·:·· <·;I,

.. - ......**~-,~~:.**

·.; 

# · .... 

### "'· ._;

### ···~. 

## ·._., 

# ... ; 

# . ··: " 

# ..

, 

# .......... "" 

## ··.·:· ,•,.



# . :·.' 

### :·-...,. 

# ·•···· .: 

### ·.:



# r**·Cot'itain~:k:YdtO'ti?~¥~-~~:i:~**

<o:. •' ,'-''\· •.: 

# .. 

# ·'

,., ,·



### -.:



## •• .'·· '· 

# . 

# . ' 

# ·:1. ;,M


# .. 

# -.

. ..**·~---** 

## ·•· 

# ...

# ·.

·,_-

•. 

## ·-··

·.-. .--'
• ·.!'.



# . .-.:



# ...... • ,. '! • ::'· - ·-:

·.:_{



### .... 

### ,_ 

# .. ··'--:. UQUIDS

. 

## -,-;

..,, __ . 

# ·· . 

# ··- .. = ::



### ':-· 

# -- 

# . ·•

# P~:~~~red S3mple.Re<juired



# ..

- 

# .



# . '



# . ·: 

## .. ::.



## --·--**·.·-~-:-** 

# .. .. 

# / / 

# ..

· ·- · orum Sto;...ge

# .ComP8~ity. -- · -.



# .**~;.~90~~~;1~·--~-** 

# :·-:···:< P 

### .= PaSS ·:F 

## =::·J?a.ff.' .• - · .

- 

# . ·::_**:-~** 

### -

# 8A~8~-**~ -~** **./~~~:** ,-,.

# ~:·' . ."


## ., 

# •·.

· 

## ..**~-** . 

## ·'



# ...... -

. 

# -·- .**-,~_-·_** --; 

## ·-.·. _ 

# . .,.,


# VES 003125

# ·r:·**-~\11,1** II 

# .·**3.-~:** 

# .... i.cf :M1 . .. ; . ''"'
.



# .**-~~** . 

# .
1 I I 

## Receive.-#: 32671 S · # 

## ororurni: 11 · 

### Dale: 5/3012008

.**~_(e_"(rolilet~:539242** 

### · I

# ~~--...~~-~~--~~ 

# \ TVVII**li~** 

# .• """',**..U~rySili Rep.;rt-~--~,---~~**  

# -- PCB 

### Analysis Required 

### Sample 

### Required**·::;·~-}"eoerator:** 

### PARKERABEX.

.. 1:lescripl:**CV~IDE** 

### SOLIJTIOI! liQUIDS



## "Process Code(s)'SF1
I 

# / ·{)rum**~?ge** 

### Compatabitity. 

### Profiled. odT Hazard ·aas's 8



# . 

# ---

I< 

### ' 

## .. Sampte _Number 

### Drum 

## R10P /Comp Roe Uquid (%) 

## 283310 

# I 00011ni74vES 

# lnd**~No** % 2 

## 2633ffi 3 %. 

### P=Pass 

# @1!" : "" 8 :415
__
Prqtile ConfQrm 

### Date 

# :0.,"-,"'-."'-."'-."'-."'-."-,'\ YesjNo lt.J, L

# ~"""**"'""'""''~ ~"""'"'.**  Color 

## An• · 

# tJ6 E
: Turbid"Jtv.**~AWTI.O** WATP1l0



### V!Scosity**WAt;)M~H~** NIALUH' N/At:MH 

### L 

# _)'1 PhySical State Uq Sol Slg.Ss. Uq'Sd·Sig Ss



### ·· Water Miscibi(ity MPFS'E**MP~SE Add:D~cription-** 

# ~NoRXN ():RJ\N:

# 0s."-~**""""""'\,~~""'** \)t=BKG (_)'>BKG;. ,..._. .. ,•BKG. ')!-· 

### Flant.Pol Screen _M'Neg (.)Pas ( ) BdC_ / 

### !>Point 

### 'fl pHScmen

### ~100% ()tO% 

# /J2;:=. (**>12~s·-]** 

# f)O O><ldizeciScreeri

. 

### )()Neg ( ) Pas As 

### "Hg

## ~"""**~** kiitials

# .-f-1'-ai_nl_FU_t_er_T_es_l_~l-'-( '-)

# Pass:---:(;_;);,_F_aH~(.;,);_V_-F_a_ii_<.~.,:,-.,.N/'-_A __ •

# -+-:lle--i---+'-"-f----:--1~~~~~~~~1--J--f-+-i**~anide** Screen 

# < J Neg 

# )>ll,Pos

- < 

## J N/A 

# {ml Cd Na

## ~"""~ Sulf<de 

## Scre<n.

.**~** Neg ( ) Pos ( ) NIA 

### C< Pb

### ~ "'-.""'

# ti.cid~ntll Odot I 

## )'i No ()Yes: 

# 10,"""""" '-.**"""~""' ~**  

# "'-.**~** 

# .. :S)ecmc Gra>ily

## -~ .

## 0~750**~** 1:150

## ~""-""' ,

.. ( BTIJibb -·. .. 

# < 5J)fJ ' l • 10000. ·.**~"'~** 

### .. : : . 

# c,.;..,- .. 1 -5

## ~"""~**·~~~.**

.· -: r>ce;tay.Gc·- oiylkg 

### :·,**~~~~---ppm.-** ()Kit()'GC 

### ( )100%(") 10%



# VES 003126

## TWilaboratory Analysis 

## Report PCB Analysis 

### Required Sample ReqUired ·

## O~m**.Sto~ge** Compatability. Profited OOTHazaid 

# aass_s __ P=Pa:ss F=Fail 

### Sample'**~umber** 

### 1-8/1-2,4-S,B 282310 

# L 000117ilnVES 

# qljl 

# ·llttlllllmtm OtumRep/Comp 

### Free Liquid 

### (%) · 

## 282310 8A
__

# ~415 __


### Profile 

### Conform Date 

### Initials

. Layers/Phases-% 

### Ea.. 1· 

# ?1 %



### Color· 

### t@TP lL 0 N/A TP 1L 0 

### Voscosi1y •. 

## NI"C;) M. H 

# @ _L " H NIALMH 

### L 

# _tj

· Physical Stale 

# 143Jl;oll' s.- 

# s......., l,lq**~** Ss Uq Sol" Slg Ss



### · watetMiscibility

### ~~Part Aoab S1nb Emls

### Ut)_F~E. -uP 

### F 

## s E



### '·•.DOscription

## ~-~U1L6**B~** I.Pr<HR 

## 'i



# .ArROactivity· 

# :1k\NoRXN ( )RXN:· ·

. Radiation Screen 

# I 

# itJ =BK-G ( ) >BKG: 

### /
. ;!IKG 

# }o

Ram. PoL Scre<o 

### MN<>Q ( ) Pos ( ) 

### BOC
.**~** 

### Aastipoint · \;::_ 

### pH Screen- ·. 

# p6 ioo% ( ).10% 

# ->12
.. 

# 5 >12.5 -"'


### · Oxidizer Screen · 

# ¥J -Neg ( ) Pos As



### Paint Filter Test (**~Pass** 

### ( )**F~A** 

### ( ) \(-Fail 

### (}{.b!IA Be Cyanide Screen

. .( ) Neg l)l:Pos _,/( ) NIA 

### Cd 

### : Sl>Uide Screen· \,t)·Neg ( ) Pos ( ) NIA



### tncidental odQr ·

### ~No ( ) Yes:

. Specffit!-Gravitv



### BTUJlb
.. %Chlwide 

# v

_ Jl"CBs By 

### G.C- mglkg · 

### _PC8s--Sc:reeA- ppm 

### :PCP Sereea:- ppm · 

## ( j"Ki! (_) 

## GC**-·pHby~** 

### (")100% ( ) 10%
.

· --PCS·analysis to be determined Upon-visual**in~Pedion** 

### of waste
. . l

### Ad~tional**Com~tS:** SF-- CYANIDE SOLU"fiON,_ PH 

### > 12.S. If drum 

### is. 

### rqostly 

### ojl, 

## eipeq 8Tl:J"s to 

### be greater 

### than 10",000.

# PrQi:e!~;~~**~dix WA~-c**  .Consitiluents by: ClF

. · '

. . . . .. . · . .· · 

# l

..

.. <la•n•

# C~amdes- 00 NO,- 

### m1x

# ~th pH<6 ·

# ~,_.!· l ; '•

# ~l<{**~~**

VES 003127

## Receiver#: l'K002 #of 

## Drums: 1 Date: 

### 6/2912001 

### "'>file 

## #: ZZZZZZ.

. perator. TRADE WAST£ INCINERATION 

## _.;script
. Process Code(s):

Sample Number 

### 286331/ ILOOOOOOOl 

## Drum**~ep** 

## I Comp 

### 1/ - 

### 'dbuallaspectiet&. Glove Box 1 

### llooded Fcedu

. Drum**S~** 

### Compatability

Profiled DDT Hazard 

### Class _9
__ . 

### P 

# = Pi!ss P 

### == Fail 8A



# -- 8B 

# -- 415



# --

Free Liquid(%) 

# I 

# II II Profile 

## Conlonn Date**I~·** 

### Pumpable NO

### 2863~1

## 0,.'\.,.'\.,.'\.,.'\.,.'\.,.'\.,.'\.,.~ YeS No 09/08/08 JS 

### layers/Phases-% Ea.

## 0,.'\.,.'\.,.'\.,.'\.,.'\.,.'\.,.'\.,.~

## 0,.'\.,.~ Color

## 0,.'\.,.'\.,.'\.,.'\.,.'\.,.'\.,.~

# ~"~ Tulbidity 

# t0.. '\,."'\.."**"~ ~**  

# t0.."-"-" Viscosity 

### L 

# j_ X 

### Physical Slate

# ~" '\.,."""" '0 -0-.'\.,.'\.,.'\ Water Miscibili1y

# ~" 

# """"**"~** 0,.'\.,.'\.,.'\ Ad<l Description 

# 11.-i.1:. ,.-, S.....Jc " 

## 2.6 (, Z:7 I 

# /N•<er Reactivity

## 0,.'\.,.'\.,.'\.,.'\.,.'\.,.'\.,.'\.,.~ 

# 0,.'\.,.'\.,.'\

··. Radiation Screen -BKG X



### Aam. Pol Screen See Aashpoint X**pHScr~** 5 at 

# JoT. 2-12.5 X 

### Oxidizer Screen 

### As 15.129 

### Pb 14.165

## ~'\.,.'\.,."\ Paint Rter 

### Test 

## Be 1.865 Hg , CL002

## ~'\.,.'\.,."\ Cyanide Screen Cd 3.51.1 

### Na 0

## ~'\.,.'\.,."\. Sulfide Screen Cr 6. !143 

### K 0

## ~'\.,.'\.,."\ Incidental Odor 

### lhd· 'l.fX>'f 

# 0-..'\:

# ~"""" 0,.'\.,.'\.,.'\ Specific 

### GmYity 0.95

## ~'\.,.'\.,."\ 09/08/08 JS 

### BTU/lb

. 5Zl0 

# f0,.'\.,.'\.,.'\ 09/08/08 JS 

### %Chloride 1.02

# -~~**09{08/~B** JS 

### Rash Point- 

## 0eg F

# ~""" 01/01/00 

### PCBs By 

### GC -. mg/kg 

### <SOppm**09108/0~** 

### PCBs-Screen- ppm <50ppm 01/01/00 

### 2,4,5-**T/S~vex-** 

### ppm J 

# f0.. '\.,." '\.,.""" "\**~""'-"'-"\** 01/01/00 

### PCP Screen- ppm 

# E0-.'\.,."-. "'-"""

# ~**~"\:\."-;** 01/01/00· pH by Meter

# ~ 

# "" "'-" '-"**~ ~""'-"'-"\**  01/01/00


### Date: 

# -,.;.tw_ Profile Review for 

### Appendix WAP-C 

### Consitiluents by:
. 

# ·:fi**~**

. 1 

### Add. Comments: The data in 

### the sample information sectlon(6129/2001

# ~s date profile 

### ZZZZZZ. was

# crea~ 

# ;u.i

VES 003128'l'Wt-388955 Cheaical. Naste Manage.eot., :me. -st;e l'rofile**s~** Sell.ing- lleg"i.aa. Lab - lOU. BAYER. 

### caoPscmNi:::Es

- .ATDI 1ULLXE TATOM 84.00 KAWl'HOIWE ltD 

### ro eor 4!113 

# """"""= MO 64.120-00l.l
WaSte NUM!: LSlB W1ISTB OMANICS/MEH (SBNCOR/FOS/JAU)
· Brocess Generating Wa.stoe : RESlDUE FROM VARIOUS PltOC&SSES Ship. Na:llle: WASTB FL11HHABL£ Ll:QOl.DS, 'l'OXtC, N.O.S Jlddl. De.:>C: {MBTH!L :r50BIJTYL lCE'I.'OliE, MEtHYL**HYDRAZ~DI"'DIIOM.'B)** NON-TR.I OIEMICALS •DIAOOLONE Ch...teal Callpo:d.tiou
PllfACOLONB RBSrotJE (A VARIETY OF HIGII BOILING OBGAN.IC {E.G. 

### an:mt mATBD AND oxtGDUcr'ED HnlllOCAitBOK) OJMPQONDS) TOL1JD1E NON-TRI CIIEKICALS FOE/TOLUENE RESIDOS (TOLUENE FREEl (RESIDUE CONTAl:NS MOS'n.Y B:ISSULFtDE 10:TH SMALL Q011NT1TIES OF FOE TKODIICAL) HDTC/TOt.UERE RESIDUE {TOLUSRB FREEl {ll.ESlDOB CONTAINS >90\ BtsiJLF mEl HYDRAZIHE ...,....,.. MBTHYL tsOBtlT!L
. n:TONE 

# ·- ·- -ires Sta<us Federal EPA to State BPA l:D EPASt&tua Sa1es**.Office~** 1033436" OOODOOOOOO 1/5/2010 Appr for serv "I«)D056389828 U!tOOU!HI9 CHlt RESTIUCT 'EWI

0 1 pet; 0 '' pet 0 70 pet 0 30 pet 0 70 pet 0 0.5 pct. 0 45 pet + Ket..la 1:CA or T.ot&l l'll.ytlical cba.n.etfn:iaties .All.SEMIC .AS AS < 5 • 0 ODM:rtl( .AS CD < 1. 0 LE1U> AS PB < 5.0 MBRCORT AS. HG .2 SBLENIUM .AS SE 1. 0 CHROMtOM HEJ: lfl:CKEL AS Nr 'l'KALLXUM 1\.S TL aawHitiM TOT 

### ca. .>"' S • 0 mg/L

Federal COdes: Handling N-DEX :INNER GLOVE Physical Stat& Fluh POint pH COlor odor Layers Specific Gravity Free Liquids Cyanide• Sulfides PC8'5' Phenolic: a t Taxable Treatment COdes CRO RPT QT'l "EPA Permit Ha.:zard Class St.a.te Codes 

# .......**~** Liq>UO < 70

- 139 CL**4.~0** - 9.0 

# """""'**No~** SntGLE LAYER 0.950

- l..l.Sb 98 "... 100 < 5 < 3 N/A <10 ppm, 1\egul.ated. by 40 em 761, DOT UN/NA NBR.: UNl992 T07 10D l./l./1900 3 090001 Mat:erial Class: EXP: 1/l./1900
HBSHJU'o Packing Gnrup 

### :rr Process Co4es BLH Cert of Dstrct Rq: No

NBO • -GREY GLOVES NOMEX TYPE C RESPIR. CONST FLOW INDEX/BLUE NITlULE (INNER GLOVE) Inha.la.ticm:
Form Cocie waste ·Type
OIAR.GE COPE:- NS 

### Dot 11'rcperti.es Dema.b 3
1 B2U**~rof~le ~andling**  ltBVJ:BWED" 1'0it ·lO.CI' METALS ORE JUNE 1, 200-t, OM.Y TO CLEAR. tqED .WEIGHT I2E UNTtL -4-28-0' Clral• 3**Fl~le:** 0**a.dOtheE:"~ts:** CHARGE CODE: NS RKVIEWED FOR IQ.C'r MET.I'LS NEED WEIGHT PB tJNTl:L 12-31-08
. CL ,(7/05 5.8 NO SC_9/8(05 Health: 0

7.1 NO SC +



# VES 003129Cbeaiea.l Waste Manage.ent, 

### :me:. 'I'W7-388,SS_

- Wute. Profile**~** Adden&u. Cbemical Coa!poaitiou: Md1tioaal. Comltituea.ta Not in.elu4ed Oil**Wa:~~te- P~f:il.e**  su-.ry Jieport -·--.. Cb.ellieal COPI{>Oeit!.on 

# - 

# -- Usdt "Dueripti.oa 

### f'DU OIEKICALS 

### I MIBX/SENCOR RESIDUE {MIBJ: FRlm) (RES=!=DilE CONl'AUfS MOSTLY E.OTn.THI
· ON, SENCOR., AliD N-MBTH!L ISCHER.)

MDX/HDTC RESn>tJE (MIBK Fli.BB) (RBSIDt:Jiil COUTAINS :>,0\" OF 'l'HE MIBK IJ!TAZDIE) K£Tl<ANOL .SULFIDE SEE TECH J«;R F'Ot.VER FOR AVEUGB AMOUNTS OF THE ABOVE COMl'OONDSCHLORlNI!

## ~= IGl POLDEJI. FOR AVBIJ.Jii;£ AMoUNTS OF '1'HB ABOVE COMPOUNDS. SEE TECH M3R. F()[,l)Sl!. FOR AVBRJIGB AMOtJN'1'S OF THE ABOVE C!OMI?Qtl'NDS. 

# """""""" $BB TECH MGa FOLDEB. 5'0R**A~** AMOUNTS OF THE ABOVE COMPOONDS. pro£ile BaAdl:lag' IUl.d other ec-.enta 0 es pet 0 

## ss pet 0 

# ,, pet 0 

# ' pet 0 

### s pet 

# , • pc<

Cit S/7/05 5.8 'INVOICE; DOES OP SURCKM.GES Not il>elu.cled aa. Wa•te**P~fil.e s~**  llepcn::t HO SC S/8/05 7.1 )11) SC Bl:LLING: 2'\" D:lSCOUNT ON DISP & TRANS"; SHOif 01'1 Qal HOT APPLY TO FBE:S & SOR.CHARGES CSJh SEE BAYER. LOAD SHEET FOR. CL, BTtr & PH H:lSTOR"f 2008 PO 260240352



# )

VES 003130

# ?j:sl

THI-CG6944 Chelllica1 Waste**Mana~t.**

.... !:."' l'x:ofile. s-ry CAMBRD: CBA2LE5 q:TY llfC Inc. Selling Regi011 Lab

- MaL llusi.neSS· 

### Dept

........ 1

### ~~~~2 

# •ce > 1205 U'l'H S'I' A CAMBRU CO CHARLES· 

### ciTY SARAH VANCE :lA 506"16-34.66" 

# - ...,.. 

# _ ..... Statwo Federal. Bl'A ID State EPA ID EPA Status S;Lles Office 1051142 "641257D37 11/11/2008 App:r .fOr Serv IAD984S91B91 91500199951 

### au< lU!STRICT 

# ..... Waste Bame; PILOT PLANT SOLVERTS ProcesS Generating Haste: ll & tl AcrnriT'l IN PHARMACEtn'ICAI. :PILOT Ship. Name: WASTE FLl\MI'lABt.E LIQDXDS. N.O.S .Addl. De.e>c: (METHANOL, ETHANOL)
ISOPROPYL ACETATE Btn:ANOL ETIOOIOL MB"l1WIQL ISOPROPANOL 

# ........... Btn:ANOL £TIWIOL B£TIWIOL l:SOPIIOPl\RlL TOLUENE Btn:ANOL Ket:.a.l.• T'C& or Total. ARSEHIC AS AS < 5.0 CMJMI0M M CD < l. 0 LEAD .AS PB < 5.0 MERCURY AS MG < .2 SEJ..ENIUM AS SEt l. 0 amoMIOM HEX IIICXEL AS NI**~ItlM** AS "TL



## ) Chem.i.cal. COmpos.f.ti.on



# .. ,.

..

/L 

# .. ,. mg/L og/L

Federal Codest DOIJl FOOl FOOS Handling Physical sta.te Fluh Poitl.t. 

# .. COl.or Odor Layers Specific Gravity Pne Liquids Cyanides Sulfides 

### l'CB'• Phenolics**"tT~le** 'fl:eatment COdes CRQ RPT QT"{ BPA Permit Hazard Class State Codes**...,.~ ~**  

### -**~** 

### Uoit**Deacr.f.pti~** 0 100 pet

0 100**pc~**

0 

### uo pet +**Phfa~cal** Cb&racter.f.atics Liquid < 73 CL 4.0

- 9.0 CLEAA**y~** SINGLE LAYER 0.700- 0.950**~5** - 100 < 

### s < 3 ppm, Regulate.d by 40 CFR 761: :. < 10 DOT UN/NA NBR: mU9'3



# .,.,, 100 1/l./1900 3 0,0001 Material 

### Class , EXP: 1/1/1,00 

# -· Packing" Group :U: l'rocess COdes DLF BF cert of Dstrct Rq: Yes

ti-DEX INNER GLOVE TYP£ 

### c R£SPIR CONST FLOW NBll. GREEN GLOVES FULLFACE RESPIRATOR CPF <
INDEX/BLUE NITRILE (INNER GLOVE)
Inhail.a.tion: 2 Form code · Waste Type Dot Properti.e4 Dermal: 2
1 B203 Flaaunable: 0**Health~** o

l':eofile K&nd1ing anc1 Othe:e Coalenta NO PRICE CHANGES FOR THE YEAR 19!151 GOOD TO 1.231.9' CHARGE CODE: NS PE RENEWED EXPIRES 12-31-08 JlBVIJnf£0 FOll KACt' METALS WITN INCREASE 1-l.-08 00 NOT BILL. TRANS IF TRANSPORTER. IS ROBBIE WOOD ONE 'I'IHE ONLY.**O~Y** TO SHIP U15f.. NO TRANS ON TT LOAD FOR 7•11 OR**7•14~0'** WT 2008 UPDATED AND LSSli.IES UJ?DA1'ED



# VES 003131

## ,.



# -. • ETHANOL ) MmfANOL

ISOI?ROPANOL OC1'JiliB BtlTANOL E'l'I!ANOL MBmANOL ISOPROPANOL ORGANXCS SOl'ANOL E'l'I!ANOL 

### ....,.,.,L ISOPROPJINOL O!UlliN%CS Cheaical. Waste Ma.J:I.ageDent, 

### :me. 1t.Ute l'E:ofil.e 

### s-ry Addell4u. Cb.eadc:::al.**-~itiOil=** Mditic:md. Cootlti.tue:a.t:J Not ia.elv.ded OQ wa.ste. l'J:Ofil.e s-cy :a.eport Chem:ica.l. COalp0$1tiozt

MErHTL**~** U'I'ON£ ACETONE METHYL ISOBOTYt. CETONE ORIM>IICS 

# ""'""' OBGANIC SETTLED SOLIDS FROM SlNTHESIS OF Btrn'L ACETATE :tNTERMEDI.ATE mARMACEUl"ICAL PRODDC'l'S 

# """"""PYL>IMIIOl> .ORGANICS 

## mm. ACErA1'B ORGAHIC SEt"l'LED SOLIDS FROM S1NTHESIS OF IIUT'lL ACE'I'A"m ZN'l"ERMED.tA'l'B PIIARHAC£t1I'ICAL PRDDOCTS TB'r!Wm>ROPURAN PR.Opyt, ACB'rATE TBRT-Bf:TrYI. tam1YL E'l'KER ORGANIC SE'rl'LED SOLIDS FROM SYNTHESIS OF E'IHYL """"' nrt'ERHBDIATB PKARMACEtrriCAL PROOOC'l'S TB'l'RAHY!>RO""""" ORG>\NICS TERT·BUTYL MlnllYJ,. ETHER ORGANIC SETTLED SOLIDS FROM SYN'l'HESIS OF 

### ..,.Y!. ETHER INTERMEDIATE PHARMACEUTICAL PR.ODOCrS TETRAHYDRO

...... 

### """"TS • ORGAJUC SBTTL£0 SOLIDS FROM snrTHESIS OF

. ") INTERMED:tAT£ PHARMACEUTICAL PII.ODDCI'S ACB'l"'NNTRILE TWI-CG6,44 

# ""' 

# -- 'Oidt Deacrlption 

# • 100 

# "'"

50 100 pet 

# • 50 pet
0 

### so pet 0 2 pet
0 

### so pet 

# • 2 pet 

# • 100 pet 0 2 pet
0 

### so pet 0 2 pet

0 2 pet 0 100 pet



# VES 003132

# 35""/07/
"Oew.ica.l. -Waste Management. 

# =· "IWI-351071 11i1Late P:cofile s-:cy VEOLU ES TECBII:ICAL Sot.unONS Se_ll!Dg B>egi.oll. Lab

- HBL
•• AnW $OSMf SCH!aCIDEIL 4 79. Wl2-IIC4Sl. BOtJNDARY RD HENOMJNEE FALLS
. WI 53051-1603 

### Waste Name: 

### BULZED**L~~D H~GH**  

### BTU >3000 

# ......, 

# ..... Expires Status Federal EPA ID: State Ei'A II> BPA Status Sales Office · ll!JU32 0000000000 9/19/2009 Appr far 

## .serv- N/A 9550019!199 CHK RBSTIUCl" DEH Process Generating WUte: J..CCtlMOLA't:rON OF RASTE FROM SOL'VBYT R£O:Mm.Y l?ROCESS Ship. Name: RQ, HAZARDOUS WA$TB, LIQUID, N.O.S Add]..**Des~:** ('l"B'CHNI_CIU. DESCRIPTIONS, RQS VALUES ILL VARY) OIL NON-HALOGEHATBO SOLVENTS ACEroNE MBTimo E"!HYL """""' XYLENE
. II'1'IWICL lSOPR.OPA!lOL GLYC>L fuL'OENE' 

# ...... ..,..,.,L .MS'IHYl. ISOBUTYL lCETONS llet.ab• 'rCA o:c Total .ARSBHIC AS AS >• 5.0 1l1iR%tJM AS BA >• "100.0 CADM7tH AS CD >• 1.0 CHROHnJM TOT Cll 5 • 0 LBIU>AS E'B ,_,. 5.0 MERCURY AS HG • 2 SELENI.DM AS SE 1. 0 SILVER AS AG >- 5.0 MICI!:EL AS HI THALLIUM AS TL CIDI.OMIDK HEJ: 

# ) Cheai.c&.l. Coapositi.oo



### ...

/L og/L 

### ""/L "'if/L "'i!/L "'if/L og/L "<J/L 

### Pby.tca.l state Plash. Point pK
. Co1o< Odo< Layeis Specific Gn.vity Free Liquids Cyanides SUlfides 

### PCS'• PbeDOlics**'t~le** "Treatment Codes CRQ RPT QTY EPA"Permit lllu:ard Class State Codes**Benz~** Packing- Group Process Cades Cert af Dstrct Rq Kin - Max m:d.t »eserlt>tiou. 0 60 pet 40 60 pet

+ i'bysie&l Cb&r&cteriatiea Liquid 

## _;o .- 200 

## a. -G,O

- 12.5 VBIES, BRONN

## ·~ SrNGLB LAYER

- 1.1.00
. 

### roo
ppm. RegulAted by 40 CFR "Jfil: 0.800 !IS '- <50 < 3 N/A <10 DOT UN/NA NBR: NiJ082 

# ., 0 1/1/HOO 

# ' 090001 < 1000 III 

### BtoH Yeo Mat:erial. Class: EXP: l./1/1900
NESHAP: Not**Ben~** NESKAP

Feder&l**C~s:** 0001 0002 0003 0004 0005 0006 DG07 0008 DQO'J 0010 DOll 0012 DOLl 0014 DOLS DOlE+llandl.ingNBR GREEN GLOVES Cl>F -4 • N-DEX INNER GLOVE POLI.FACE RESPIRATOR 'n'J.>B C Rl"!S!'IR CONST FLOW INDEX/BLUE: NITRILE (INNER GLOVE) CANCER SUSJ?"ECT AGENTS: CADMIUM. LEAD, BENZENE, VINYL CHLORIDE, FORMALDEIJYDE, ARS'ENJ:C + Inba.la.tion: 3 .Foru cede Waste Type Dot Propertle8 Dermal: l 

# ' 8201. Oral: 3

Profile H&Ddl.i.n!J and Other MAY BE SHJ:PPED .AS HAZ OR NON RAZ Fla.maable, o



### c-.nts P/B IN PLACE. BXPIRES 12/31./05 Health: 0

REVJ::l'M£D FOR. MllCr METALS.
. ON CHLORINE CONTENT. SEB PE FOR BILLING. REPOR.T CHLORINE CONTENT 'FOil. BILLING. PB HODIJ!'U:O '1'0 UI"CLODE Vldll:OOS l'RICDIG DEPDDDlG EFFECTXV 11•17-05 CHLORJ:NE t.'ON'l'ENT ON RECEIPT MUST BE ON INVOICE. !'E EXP 1:2-31.-08 RENEW W INCREASE 1-1-08 WT UPDATED +



# VES 003133

### ;.



## , Emit. ACErA'l'E

## )-~~'l'B

GioYCOL ETHER**~c::al.** Waste Management, rnc. waste ProfU.e**s~ ~**  Che.icd eo.poaiuon: Ad.dit:.ioaal. COnsti.tuents Hot**~l~** em 1f-te Profile**Swaaa~** lteport C'he:lt.le&l.**COiapoa:L~o:a.** .



# .. 

# - hALOGENATED 50LV'Ji:NTS MB"l'HYLENB cm.otu:DB CIILOROFOIIII CIUlBOK 'l'B'l'RACRLoR.XDB**l,l,l~TIU.CBLOROETHANE** · 

# ''""""""""""""' ·Tti'RAO!LOR:o&'l'HYLENE 1,1,2-TRICRLOR0-1,2,2-TRIFLOOROETHANE 

### TIUCiii.C>l!OETilY IIIERTS Dl:R.T, SLODGE MAY ALSO INCLUDE SUR.FAC'l"ANS, S'UINS, AND VA!U1ISHEs
. 'l'RAT WILL BE COMPA'I'£0 PIUOR TO ADDITI:OIJ. COMMEioTs TOTAL SODJDf ANO POTASSIIJH 

# .....,_..., Hot inelwfed on Wulte. Profile SUIIIIII&J:T Report YELLOW OVER, BOOT COVBJt ltrofile Ean411Dg and Ot:h.r Cocm.emt• Not ineludecl o.n. WB.ste PrOfile**SW~~a~ary** Report PE ON FILE 12-ll.-07 RENEWBD '



# ) TWJ:-'351071

0 6'0 pet 0 12 pet

0 

## s pet
1000 10000 pPm



# VES 003134