SOUTHWEST RESEARCH INSTITUTE ®

SAN ANTONIO, TX  ● HOUSTON, TX  ● WASHINGTON, DC

EPACT/V2/E-89 FUEL BLENDING 

FINAL REPORT 

NREL Subcontract No. ACI-8-88612-01 

US EPA Contract EP-C-07-028, 

Work Assignments 0-01, 1-04, and 1-10 

SwRI® Project Nos. 03. 03.13363.01, 03.14175.04, 

03.14175.10, and 03.14295 

Prepared for: 

Dr. Douglas Lawson 

National Renewable Energy Laboratory 

1617 Cole Boulevard 

Golden, CO 80401 

and 

Dr. Rafal Sobotowski 

Environmental Protection Agency 

2000 Traverwood Drive 

Ann Arbor, Michigan 48105 

Prepared by: 

Kevin A. Whitney 

Manager, Light-Duty Vehicle Emissions 

Emissions R&D Department 

September 2010
EPACT/V2/E-89 FUEL BLENDING 

FINAL REPORT 

NREL Subcontract No. ACI-8-88612-01 

US EPA Contract EP-C-07-028, 

Work Assignments 0-01, 1-04, and 1-10 

SwRI® Project Nos. 03. 03.13363.01, 03.14175.04, 

03.14175.10, and 03.14295 

Prepared for: 

Dr. Douglas Lawson 

National Renewable Energy Laboratory 

1617 Cole Boulevard 

Golden, CO 80401 

and 

Dr. Rafal Sobotowski 

Environmental Protection Agency 

2000 Traverwood Drive 

Ann Arbor, Michigan 48105 

September 2010

Prepared by: Approved by: 

 

_________________________________ ________________________________ 

Kevin A Whitney, Manager Jeff J. White, Director 

EMISSIONS RESEARCH AND DEVELOPMENT DEPARTMENT 

ENGINE, EMISSIONS AND VEHICLE RESEARCH DIVISION 

This report shall not be reproduced, except in full, without the written approval of Southwest Research Institute®. 

Results and discussion given in this report relate only to the test items described in this report. 
REPORT 03.14295/03-51563E ii 

FOREWORD 

This report covers work the Southwest Research Institute (SwRI®) Office of Automotive 

Engineering has conducted for the National Renewable Energy Laboratory (NREL) and the U.S. 

Environmental Protection Agency (EPA) in support of the Energy Policy Act of 2005 (EPAct). 

Section 1506 of EPAct requires EPA to produce an updated fuel effects model representing the 

2007 light-duty gasoline fleet, including determination of the emissions impacts of increased 

renewable fuel use. 

This report covers the formulation, analysis, and procurement of test fuels for the EPAct 

Gasoline Light-Duty Exhaust Fuel Effects Test Program, also referred to as the EPAct/V2/E-89 

Program. It is expected that this report will be an attachment or chapter in the overall 

EPAct/V2/E-89 Program report prepared by EPA and NREL. Other EPAct/V2/E-89 reports are 

expected to cover room temperature and 50°F emissions testing of three fuels using nineteen Tier 

2 vehicles (known as Phase 1, Phase 2, and Interim FTP Testing); emissions testing of 28 fuels 

using sixteen Tier 2 vehicles (Phase 3); room temperature, 95°F, and 20°F testing of three fuels 

using six Tier 2 vehicles (Phase 4); and room temperature, 95°F, and 20°F testing of three fuels 

using three high-emitting vehicles (Phase 5). 

SwRI’s portion of this fuel blending effort was funded under NREL Subcontract No. 

ACI-8-88612-01 and EPA Contract No. EP-C-07-028, Work Assignments 0-01, 1-04, and 1-10. 

The project was based on SwRI Proposal Nos. 03-50782C, 03-53262A, 03-51563E and 03-

54753. 

The program was identified within SwRI under Project Nos. 03.13363.01, 03.14175.04, 

03.14175.10, and 03.14295. The program was monitored by Douglas Lawson of NREL and 

Rafal Sobotowski of EPA. The SwRI Project Manager was Kevin Whitney, and the Project 

Leader was Kevin Brunner. Fuel was blended and supplied by Haltermann Products based on 

formulations jointly developed by Haltermann and EPA. Dr. Sobotowski of EPA offered 

substantial assistance in the formulation and approval of test fuels. 

Fuel formulation and procurement occurred between March 2008 and May 2009. At the 

time this report was written, some fuels were still being utilized in testing under the EPAct/V2/E89 Program. Details of fuel handling and quality checks to confirm each fuel drum for ethanol 

content, aromatic content, and T90 are included in individual reports or chapters associated with 

the testing using specific fuels. 

 
REPORT 03.14295/03-51563E iii 

TABLE OF CONTENTS

Page

FOREWARD .................................................................................................................................. ii 

LIST OF FIGURES ....................................................................................................................... iv 

LIST OF TABLES ......................................................................................................................... iv 

ACKNOWLEDGEMENTS ............................................................................................................ V

ACRONYMS AND ABBREVIATIONS ...................................................................................... vI 

1.0 INTRODUCTION ...............................................................................................................1 

2.0 TECHNICAL APPROACH AND RESULTS .....................................................................2 

3.0 CLOSURE .........................................................................................................................12 

APPENDICES No. of Pages

A - DEATILED FUEL INSPECTION DATA ..........................................................................5 

B - FUEL ANALYSES SUMMARY ......................................................................................50 

C - DETAILED HYDROCARBON ANALYSIS RESULTS ...............................................600 

 
REPORT 03.14295/03-51563E iv 

LIST OF FIGURES 

Figure Page

 1 Constant-Temperature Storage of Unopened Fuel Drums .................................................11 

LIST OF TABLES 

Table Page

 1 EPACT/V2/E-89 Gasoline Light-Duty Exhaust Fuel Effects Test Program 

 Fuel Properties .....................................................................................................................3 

 2 Fuel Development Protocol .................................................................................................7

 
REPORT 03.14295/03-51563E v 

ACKNOWLEDGEMENTS 

SwRI acknowledges the following: 

• The Department of Energy Office of Biomass Programs and Office of Vehicle 

Technologies for their financial support provided through the National Renewable 

Energy Laboratory 

• The Environmental Protection Agency for their funding and extensive technical 

support in the development of these test fuels 

• The Coordinating Research Council for providing Fuel 29 

 
REPORT 03.14295/03-51563E vi 

ACRONYMS AND ABBREVIATIONS 

°F degrees Fahrenheit 

IBP initial boiling point 

API American Petroleum Institute 

ASTM American Society for Testing and Materials 

Btu British thermal unit 

CRC Coordinating Research Council 

DHA detailed hydrocarbon analysis 

DVPE dry vapor pressure equivalent 

EPA US Environmental Protection Agency 

EPAct 2007 Energy Policy Act 

E10 gasoline containing 10 percent volume denatured ethanol 

E15 gasoline containing 15 percent volume denatured ethanol 

E20 gasoline containing 20 percent volume denatured ethanol 

E85 gasoline containing 85 percent volume denatured ethanol 

FBP final boiling point 

FIA flame ionization analyzer 

g gram 

HP Haltermann products 

IBP initial boiling point 

Kg kilogram 

kPa kilopascal 

lb pound mass 

mg milligram 

MJ megajoule 

mL milliliter 

MON motor octane number 

NREL National Renewable Energy Laboratory 

psi pounds per square inch 

ppm parts per million 

RON research octane number 

RVP Reid vapor pressure 

SwRI Southwest Research Institute 

vol. volume 

WAM work assignment manager 
REPORT 03.03.14295/03-51563E 1 of 12 

1.0 INTRODUCTION

The National Renewable Energy Laboratory and the US Environmental Protection 

Agency (EPA), with support from the Coordinating Research Council (CRC), are conducting the 

EPAct Gasoline Light-Duty Exhaust Fuel Effects Test Program, also referred to as the 

EPAct/V2/E-89 Program. This emission test program includes multiple fuel properties, multiple 

ambient test temperatures, and different vehicle technologies. This report covers the 

formulation, analysis, and procurement of the thirty-one test fuels used in the EPAct/V2/E-89 

Program. This effort was funded under NREL Subcontract No. ACI-8-88612-01 and EPA 

Contract No. EP-C-07-028, Work Assignments 0-01, 1-04, and 1-10. One test fuel was provided 

by the Coordinating Research Council. 

 
REPORT 03.03.14295/03-51563E 2 of 12 

2.0 TECHNICAL APPROACH AND RESULTS 

Test fuels were procured from Haltermann Products. EPA provided SwRI with target 

fuel specifications. These test fuels were designed to cover a broad range of properties and were 

not representative of commercial fuels. Many of these fuels were extremely difficult to blend to 

meet all specification, and in some cases EPA and NREL approved fuel blends that did not meet 

all target specifications. To help the reader understand these differences, Table 1 contains target 

fuel specifications as well as SwRI inspection data of final approved fuels. 

Fuels 17, 18, and 19 were the first fuels blended, and were formulated by Haltermann 

based on EPA’s recommendation and NREL’s acceptance. However, based on the challenges of 

blending these fuels, a formalized fuel development protocol was created. Using this protocol, 

all other test fuels except Fuel 29 were formulated by Rafal Sobotowski of the EPA in 

conjunction with Haltermann, who provided EPA with data for all their blendstock components. 

The final fuel development protocol used for this program is given in Table 2. Fuel 29 was 

provided to the program by the Coordinating Research Council. 

Detailed fuel inspection results as determined by SwRI are provided in Appendix A. The 

format of Appendix A is the same as an EPA-coordinated EPAct/V2/E-89 Fuels Round Robin 

study, which is expected to be separately reported. All data provided in Appendix A are the 

same as those SwRI provided to EPA for the round robin data study. The inspection data in 

Appendix A are much more detailed than the information provided in Table 1, which includes 

only the fuel specifications and related inspection results. 

Over the course of fuel development, Haltermann Products used the following external 

laboratories for analyses: Dixie, Gage, Core, Inspectorate, Paragon, and Saybolt. Following 

every set of analyses, Haltermann compiled these inspection results in spreadsheets, which were 

forwarded to NREL, EPA, and SwRI. These detailed fuel inspection data are provided for 

reference in Appendix B. 

In addition to the provided inspection data, all fuels except Fuel 29 received detailed 

hydrocarbon analysis (DHA) using ASTM Method D6729. These results are given in Appendix 

C. DHA results show that Fuels 17 and 18 contained unusually high amounts of cyclohexane: 

approximately 18 and 13 volume percent respectively. Haltermann used cyclohexane as a one of 

the fuel blending components in an effort to meet EPA’s request to “match” the three fuels 

within a 20°F window across as much of the distillation curve as possible. 

The data in Appendices A, B, and C have also been provided in Excel format as part of 

the electronic submission of this report 
REPORT 03.14295/03-51563E 3 of 12 TABLE 1. EPACT/V2/E-89 GASOLINE LIGHT-DUTY EXHAUST FUEL EFFECTS TEST 

FUEL PROPERTIES 

a – inspection results from Haltermann 

 NOTE: Properties in bold were varied within the fuel matrix. All other properties were held constant. 

Test Fuel Specification

123456

Spec. SwRI Result Spec. SwRI Result Spec. SwRI Result Spec. SwRI Result Spec. SwRI Result Spec. 

Density, 60o

F g/cm3 D4052 NA Report 0.7214 Report 0.7224 Report 0.7360 Report 0.7350 Report 0.7578 Report 

API Gravity, 60o

F oAPI D4052 NA Report 64.5 Report 64.3 Report 60.7 Report 60.9 Report 55.2 Report 

Ethanol Content vol. % D5599

E0: < 0.1; 

E10: ± 0.5; E15: ± 0.5; 

E20: ±0.5; 

E85: ±2

10 10.1 0 <0.1 10 10.4 10 9.8 0 <0.2 10 

Total Content of Oxygenates Other than Ethanol vol. % D5599 - <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 T10 oF D86 - <158 117 <158 121 <158 142 <158 123 <158 143 <158 T50 oF D86 ± 4 150 149 240 236 220 218 220 219 240 236 190 T90 oF D86 ± 5 300 303 340 341 300 300 340 337 300 301 340 FBP oF D86 - <437 368 <437 375 <437 372 <437 371 <437 360 <437 DVPE psi D5191 ± 0.25 10.0 10.1 10.0 10.4 7.0 6.8 10.0 10.0 7.0 6.9 7.0 Aromatics vol. % D1319 ± 1.5 15.0 15.5 15.0 14.1 15.0 15.9 15.0 15.6 35.0 35.8 15.0 Olefins vol. % D1319 ± 1.5 7 7.5 7 7.2 7 7.3 7 6.9 7 7.0 7 Benzene vol. % D3606 ± 0.15 0.62 0.71 0.62 0.50 0.62 0.75 0.62 0.57 0.62 0.49 0.62 S mg/kg D5453 ± 5 25 30 25 23 25 26 25 21 25 25 25 (R + M)/2 - Calc. - ≥ 87.0 91 ≥ 87.0 92 ≥ 87.0 93 ≥ 87.0 93 ≥ 87.0 91 ≥ 87.0 

C mass % Calc. - Report 82.2 Report 85.4 Report 82.4 Report 82.2 Report 87.0 Report H mass % D4808 Method A - Report 13.6 Report 14.3 Report 14.0 Report 13.9 Report 13.0 Report 

O mass % D5599 - Report 3.9 Report <0.1 Report 3.9 Report 3.7 Report <0.1 Report Gross Heat of Combustion Btu/lb D4809 - Report 19,318 Report 20,216 Report 19,242 Report 19,312 Report 19,628 Report Water Contenta mg/kg E1064 - Report 0.1 Report <0.1 Report 0.1 Report <0.1 Report <0.1 Report 

Copper Strip Corrosion, 3h at 122o

Fa - D130 - <No. 1 1A <No. 1 1A <No. 1 1A <No. 1 1A <No. 1 1A <No. 1 

Solvent-Washed Gum Contenta mg/100 ml D381 - < 5 <0.5 < 5 <0.5 < 5 <0.5 < 5 1.5 < 5 <0.5 < 5 

Oxidation Stabilitya minute D525 - >240 >240 >240 >240 >240 >240 >240 >240 >240 >240 >240 

PROPERTY UNIT METHOD BLENDING TOLERANCE 

TEST FUELS

E0/E10 Fuels
REPORT 03.14295/03-51563E 4 of 12 TABLE 1 (CONT'D). EPACT/V2/E-89 GASOLINE LIGHT-DUTY EXHAUST FUEL EFFECTS 

FUEL PROPERTIES 

 a – inspection results from Haltermann NOTE: Properties in bold were varied within the fuel matrix. All other properties were held constant.

Test Fuel Specification

9 10 11 12 13 14 

Spec. SwRI Result Spec. SwRI Result Spec. SwRI Result Spec. SwRI Result Spec. SwRI Result Spec. S

R

Density, 60o

F g/cm3 D4052 NA Report 0.7453 Report 0.7663 Report 0.7601 Report 0.7521 Report 0.7544 Report 0

API Gravity, 60o

F oAPI D4052 NA Report 58.3 Report 53.1 Report 54.6 Report 56.6 Report 56.0 Report 

Ethanol Content vol. % D5599

E0: < 0.1; 

E10: ± 0.5; E15: ± 0.5; 

E20: ±0.5; 

E85: ±2

0 <0.1 10 9.9 10 10.2 10 9.9 0 <0.1 0 <

Total Content of Oxygenates Other than Ethanol vol. % D5599 - <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <T10 oF D86 - <158 113 <158 137 <158 125 <158 117 <158 137 <158 T50 oF D86 ± 4 190 191 220 218 190 196 150 153 220 222 190 T90 oF D86 ± 5 340 341 340 342 300 303 340 342 340 339 340 FBP oF D86 - <437 381 <437 372 <437 361 <437 380 <437 377 <437 DVPE psi D5191 ± 0.25 10.0 10.3 7.0 7.0 10.0 9.9 10.0 10.1 7.0 6.9 7.0 Aromatics vol. % D1319 ± 1.5 35.0 37.3 35.0 35.6 35.0 35.1 35.0 35.1 35.0 33.5 15.0 Olefins vol. % D1319 ± 1.5 7 6.2 7 6.0 7 6.3 7 6.0 7 5.1 7 Benzene vol. % D3606 ± 0.15 0.62 0.55 0.62 0.58 0.62 0.57 0.62 0.62 0.62 0.53 0.62 S mg/kg D5453 ± 5 25 23 25 25 25 22 25 19 25 22 25 (R + M)/2 - Calc. - ≥ 87.0 90 ≥ 87.0 93 ≥ 87.0 92 ≥ 87.0 94 ≥ 87.0 91 ≥ 87.0 

C mass % Calc. - Report 87.2 Report 83.5 Report 83.7 Report 83.8 Report 86.6 Report H mass % D4808 Method A - Report 12.8 Report 12.7 Report 12.5 Report 12.7 Report 13.6 Report 

O mass % D5599 - Report <0.1 Report 3.6 Report 3.7 Report 3.6 Report <0.1 Report <Gross Heat of Combustion Btu/lb D4809 - Report 19,757 Report 18,958 Report 18,817 Report 18,950 Report 19,729 Report 2Water Contenta mg/kg E1064 - Report <0.1 Report 0.1 Report 0.1 Report 0.1 Report <0.1 Report <

Copper Strip Corrosion, 3h at 122o

Fa - D130 - <No. 1 1A <No. 1 1A <No. 1 1A <No. 1 1A <No. 1 1A <No. 1 

Solvent-Washed Gum Contenta mg/100 ml D381 - < 5 <0.5 < 5 <0.5 < 5 0.5 < 5 <0.5 < 5 1.5 < 5 <

Oxidation Stabilitya minute D525 - >240 >240 >240 >240 >240 >240 >240 >240 >240 >240 >240 >

PROPERTY UNIT METHOD BLENDING TOLERANCE 

TEST FUELS

E0/E10 Fuels
REPORT 03.14295/03-51563E 5 of 12 TABLE 1 (CONT'D). EPACT/V2/E-89 GASOLINE LIGHT-DUTY EXHAUST FUEL EFFECTS 

FUEL PROPERTIES 

a – inspection results from Haltermann 

 NOTE: Properties in bold were varied within the fuel matrix. All other properties were held constant.

Test Fuel Specification

September 22, 2008

17 18 19 20 21 22 

Spec. SwRI Result Spec. SwRI Result Spec. SwRI Result Spec. SwRI Result Spec. SwRI Result Spec. S

R

Density, 60o

F g/cm3 D4052 NA Report 0.7581 Report 0.7537 Report 0.7498 Report 0.7429 Report 0.7764 Report 0

API Gravity, 60o

F oAPI D4052 NA Report 55.1 Report 56.1 Report 57.4 Report 58.9 Report 50.7 Report 

Ethanol Content vol. % D5599

E0: < 0.1; 

E10: ± 0.5; E15: ± 0.5; 

E20: ±0.5; 

E85: ±2

0 <0.1 9.5 9.4 14.5 14.1 20 19.8 20 20.0 20 

Total Content of Oxygenates Other than Ethanol vol. % D5599 - <0.1 <0.1 <0.1 <0.1 <0.15 <0.1 <0.2 <0.1 <0.2 <0.1 <0.2 T10 oF D86 - <158 130 <158 134 <158 128 <158 143 <158 142 <158 T50 oF D86 ± 4 215 215 202 211 195 181 165 162 165 168 165 T90 oF D86 ± 5 325 323 325 319 325 312 300 300 300 308 300 FBP oF D86 - <437 371 <437 345 <437 350 <437 377 <437 360 <437 DVPE psi D5191 ± 0.25 8.9 9.2 8.9 9.0 8.9 9.0 7.0 6.7 7.0 6.9 10.0 Aromatics vol. % D1319 ± 1.5 29.5 29.5 24.9 22.9 22.6 22.1 15.0 16.3 35.0 34.5 15.0 Olefins vol. % D1319 ± 1.5 7 6.3 7 5.7 7 6.2 7 7.3 7 7.1 7 Benzene vol. % D3606 ± 0.15 0.62 0.46 0.62 0.68 0.62 0.71 0.62 0.69 0.62 0.72 0.62 S mg/kg D5453 ± 5 25 23 25 22 25 21 25 23 25 20 25 (R + M)/2 - Calc. - ≥ 87.0 88 ≥ 87.0 89 ≥ 87.0 89 ≥ 87.0 96 ≥ 87.0 94 ≥ 87.0 

C mass % Calc. - Report 86.5 Report 82.9 Report 81.5 Report 78.0 Report 80.7 Report H mass % D4808 Method A - Report 13.5 Report 13.7 Report 13.5 Report 14.3 Report 12.2 Report 

O mass % D5599 - Report <0.1 Report 3.4 Report 5.1 Report 7.4 Report 7.1 Report Gross Heat of Combustion Btu/lb D4809 - Report 19,775 Report 19,117 Report 18,725 Report 18,473 Report 18,021 Report 1

Water Contenta mg/kg E1064 - Report <0.1 Report 0.1 Report 0.2 Report <0.1 Report <0.1 Report 

Copper Strip Corrosion, 3h at 122o

Fa - D130 - <No. 1 1A <No. 1 1A <No. 1 1A <No. 1 1A <No. 1 1A <No. 1 

Solvent-Washed Gum Contenta mg/100 ml D381 - < 5 <0.5 < 5 <0.5 < 5 0.5 < 5 <0.5 < 5 0.5 < 5 

Oxidation Stabilitya minute D525 - >240 >240 >240 >240 >240 >240 >240 >240 >240 >240 >240 >

E15/E20 

TEST FUELS

PROPERTY UNIT METHOD BLENDING TOLERANCE 

RFS2 Fuels
REPORT 03.14295/03-51563E 6 of 12 TABLE 1 (CONT'D). EPACT/V2/E-89 GASOLINE LIGHT-DUTY EXHAUST FUEL EFFECTS 

FUEL PROPERTIES 

 a – inspection results from Haltermann b – fuel provided by CRC c – inspection results from EPA Fuels Round Robin study 

 NOTE: Properties in bold were varied within the fuel matrix. All other properties were held constant.

Test Fuel Specification

25 26 27 28 29b 

Spec. SwRI Result Spec. SwRI Result Spec. SwRI Result Spec. SwRI Result Spec. 

R

Density, 60o

F g/cm3 D4052 NA Report 0.7714 Report 0.7624 Report 0.7448 Report 0.7724 Report 

API Gravity, 60o

F oAPI D4052 NA Report 51.8 Report 54.0 Report 58.4 Report 51.6 Report 

Ethanol Content vol. % D5599

E0: < 0.1; 

E10: ± 0.5; E15: ± 0.5; 

E20: ±0.5; 

E85: ±2

20 19.9 15 15.1 15 14.7 15 14.6 81 

Total Content of Oxygenates Other than Ethanol vol. % D5599 - <0.2 <0.1 <0.15 <0.1 <0.15 <0.1 <0.15 <0.1 <2.0 T10 oF D86 - <158 129 <158 119 <158 143 <158 144 Report T50 oF D86 ± 4 165 167 160 161 220 225 220 219 Report T90 oF D86 ± 5 340 344 340 344 340 342 300 303 Report FBP oF D86 - <437 377 <437 376 <437 372 <437 364 Report DVPE psi D5191 ± 0.25 10.0 10.1 10.0 10.0 7.0 6.9 7.0 6.8 6.9 Aromatics vol. % D1319 ± 1.5 35.0 37.9 35.0 36.9 15.0 16.2 35.0 36.5 Report Olefins vol. % D1319 ± 1.5 7 6.8 7 6.8 7 8.1 7 7.2 Report Benzene vol. % D3606 ± 0.15 0.62 0.75 0.62 0.67 0.62 0.66 0.62 0.69 Report S mg/kg D5453 ± 5 25 25 25 23 25 26 25 24 15 (R + M)/2 - Calc. - ≥ 87.0 95 ≥ 87.0 95 ≥ 87.0 95 ≥ 87.0 96 Report 

C mass % Calc. - Report 81.0 Report 82.1 Report 81.1 Report 82.1 Report H mass % D4808 Method A - Report 11.9 Report 12.2 Report 13.9 Report 12.5 Report O mass % D5599 - Report 7.1 Report 5.5 Report 5.5 Report 5.2 Report Gross Heat of Combustion Btu/lb D4809 - Report 17,309 Report 18,524 Report 18,972 Report 18,575 Report Water Contenta mg/kg E1064 - Report 0.1 Report 0.1 Report 0.1 Report 0.1 <10,000 

Copper Strip Corrosion, 3h at 122o

Fa - D130 - <No. 1 1A <No. 1 1A <No. 1 1A <No. 1 1A na 

Solvent-Washed Gum Contenta mg/100 ml D381 - < 5 <0.5 < 5 <0.5 < 5 0.5 < 5 <0.5 < 5 

Oxidation Stabilitya minute D525 - >240 >240 >240 >240 >240 >240 >240 >240 na 

PROPERTY UNIT METHOD BLENDING TOLERANCE 

TEST FUELS

E15/E20 Fuels E85 
REPORT 03.14295/03-51563E 7 of 12 

TABLE 2. FUEL DEVELOPMENT PROTOCOL 

Step 1: Based on the specification provided in Table 1, the EPA shall generate a recipe for each 

test fuel and forward it to Haltermann Products (HP)1

Step 2: HP shall prepare a hand blend and perform its analysis. The scope of this analysis shall 

include, at the minimum, D86 distillation, D1319 FIA and D5191 DVPE 

 • If the predicted S content of this blend is ≥ 27 ppm, then S by D5453 shall also be 

measured 

 • If the predicted benzene content of this blend ≥ 0.70, then benzene by D3606 shall 

also be measured 

 • If the predicted anti knock index ((R+M)/2) of this blend ≤ 88.0, D2699 research and 

D2700 motor octane numbers shall also be measured 

 Note: OptiDist distillation stills shall be used to generate D86 distillation data for all E10, 

E15, E20 and E85 fuels 

 Note: Distillation, FIA, and RVP shall be measured by HP and a contract laboratory of 

HP’s choice 

 Note: For a typical fuel, it is expected that Steps 1 and 2 may be repeated up to three 

more times; more iterations may be necessary for some fuels. 

Step 3: Once the blend meets the T10, T50, T90, FBP, DVPE, FIA aromatics, FIA olefins, 

benzene content, S content, ethanol content and anti knock index requirements of the 

specification provided in Table 1, its inspection data shall be presented to the EPA WAM for 

approval 

Step 4: Upon approval of the hand blend inspection data, the EPA WAM shall generate the final 

specification for the bulk blend of this fuel based on the following table: 

 

1

 Communications between EPA and HP will take place via SwRI 
REPORT 03.14295/03-51563E 8 of 12 

TABLE 2 (CONT'D). FUEL DEVELOPMENT PROTOCOL 
REPORT 03.14295/03-51563E 9 of 12 

TABLE 2 (CONT'D). FUEL DEVELOPMENT PROTOCOL 

Step 5: HP shall prepare the bulk blend of the fuel and adjust its properties until it meets the 

specification defined in Step 4 

 Note: OptiDist distillation stills shall be used to generate D86 distillation data for all E10, 

E15, E20 and E85 fuels 

 Note: Distillation, FIA, RVP, S content, benzene content and anti knock index shall be 

determined by HP 

 Note: The fuel shall be also analyzed by a contract laboratory of HP’s choice in two 

phases 

 Phase 1: Initially, the distillation, FIA, and RVP shall be determined 

 • S content, benzene content and anti knock index shall also be determined if the 

criteria listed for these parameters in Step 2 are met 

 Phase 2: The remaining fuel properties shall be determined only when the average values 

of distillation parameters, FIA, RVP, S content, benzene content and anti knock index 

determined by HP and the contract lab have been shown to meet the requirements of the 

specification defined in Step 4 (Phase 2). They must also be within the reproducibility 

limits of each test method. 

Step 6: Once the inspection data generated by HP and the contract laboratory indicate that the 

final blend meets the specification defined in Step 4, a sample shall be shipped to SWRI for 

confirmatory analysis 

Step 7: SWRI shall perform tests listed in WA 1-04, contract EP-C-07-028, except for H by 

D4808 which has been dropped from the EPAct fuel specification 

 Note: OptiDist distillation stills shall be used to generate D86 distillation data for all E10, 

E15, E20 and E85 fuels 

Step 8: If SwRI analytical results are outside of test reproducibility limits for any parameter, 

discussions will be necessary among EPA, SwRI, and Haltermann regarding the disposition of 

the fuel. Otherwise, following review of SwRI and Haltermann results, EPA will approve the 

bulk blend for shipment to SwRI. 

Blending sequence: E0 and E10 fuels will be blended first, followed by E20 fuels, E15 fuels and 

the E85 fuel 
REPORT 03.14295/03-51563E 10 of 12 

SwRI procured the following fuel amounts: 

Number of 55-Gallon Drums 

EPA funding NREL funding Provided by CRC

Shipped to 

SwRI Shipped to EPA Shipped to SwRI 

Fuel 1 10 

Fuel 2 10 

Fuel 3 10 

Fuel 4 10 

Fuel 5 10 

Fuel 6 10 

Fuel 7 10 

Fuel 8 10 

Fuel 9 10 

Fuel 10 10 

Fuel 11 10 

Fuel 12 10 

Fuel 13 10 

Fuel 14 10 

Fuel 15 10 

Fuel 16 10 

Fuel 17 20 4 2 

Fuel 18 20 4 2 

Fuel 19 20 4 2 

Fuel 20 10 

Fuel 21 10 

Fuel 22 10 

Fuel 23 10 

Fuel 24 10 

Fuel 25 10 

Fuel 26 10 

Fuel 27 10 

Fuel 28 10 

Fuel 29 4 

Fuel 30 10 

Fuel 31 10 

For contingency purposes, these amounts included approximately 20 percent more fuel 

than the anticipated need to complete the program. All fuels were maintained in sealed epoxylined 5B drums at a constant temperature of less than 75°F (Figure 1). The storage temperature 

for unopened drums was 70°F ± 5°F. Prior to opening a drum, it was conditioned to a 

temperature of less than 50°F. Once a drum of fuel was opened, it continued to be stored at 

45°F ± 5°F. In an effort to ensure correct drum labeling, during the conduct of the program each 

time a new drum was opened ethanol content, aromatic content, and T90 were determined using 
REPORT 03.14295/03-51563E 11 of 12 

a PetroSpec portable gasoline analyzer. PetroSpec analyses were performed as part of individual 

NREL and EPA contracts and work assignments, some of which are still ongoing. As such, 

PetroSpec results are not reported here and will be included in appropriate reports for Phases 1, 

2, 3, 4, & 5, and Interim FTP Testing. 

FIGURE 1. CONSTANT-TEMPERATURE STORAGE OF UNOPENED FUEL DRUMS 

 
REPORT 03.14295/03-51563E 12 of 12 

3.0 CLOSURE 

 All analytical results included in the report have also been submitted electronically to 

NREL and EPA. With the submission of this final report, all contracted items of work under the 

relevant proposals are complete. 
REPORT 03.14295/03-51563E 

APPENDIX A 

DETAILED FUEL INSPECTION DATA 
REPORT 03.14295/03-51563E A-1 

EPACT/V2/E-89 GASOLINE LIGHT-DUTY EXHAUST FUEL EFFECTS TEST 

PROGRAM – DETAILED FUEL INSPECTION DATA 

 

FUEL

123456

Density, 60o

F g/cm3 D4052 0.7214 0.7224 0.7360 0.7350 0.7578 0.7345

API Gravity, 60o

F oAPI D4052 64.5 64.3 60.7 60.9 55.2 61.1

Ethanol vol. % D5599 10.14 <0.1 10.42 9.83 <0.2 10.55

Total Content of Oxygenates 

Other Than Ethanol vol. % D5599 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1

Distillation IBP oF 94 83 109 94 94 109

5% evap oF 113 105 137 113 125 132

10% evap oF 117 121 142 123 143 137

20% evap oF 124 153 149 140 171 143

30% evap oF 131 190 155 151 198 149

40% evap oF 140 218 180 158 221 154

50% evap oF 149 236 218 219 236 196

60% evap oF 177 251 225 243 248 231

70% evap oF 226 272 245 267 260 274

80% evap oF 256 305 260 300 274 315

90% evap oF 303 341 300 337 301 344

95% evap oF 338 353 340 350 324 358

FBP oF 368 375 372 371 360 370

Recovery vol. % 98.4 96.8 98.2 97.6 97.3 97.1

Residue vol. % 1.1 0.9 1.0 0.8 1 1.1

Loss vol. % 0.5 2.3 0.8 1.6 1.7 1.8

DVPE psi D5191 10.05 10.38 6.78 10.00 6.86 7.19

Aromatics vol. % D1319 15.5 14.1 15.9 15.6 35.8 15.4

Olefins vol. % D1319 7.5 7.2 7.3 6.9 7.0 9.0

Benzene vol. % D3606 0.71 0.50 0.75 0.57 0.49 0.82

S mg/kg D5453 30 23 26 21 25 22

RON - D2699 94.9 96 98 97 96 96

MON - D2700 86.7 89 88 88 86 87

(R + M)/2 - Calc. 90.8 92 93 93 91 92

C mass % D5291 mod. 82.16 85.39 82.44 82.23 86.98 81.42

H mass % D5291 mod. 13.60 14.25 14.04 13.90 13.04 14.26

O mass % D5599 3.9 <0.1 3.9 3.7 <0.1 4.0

Gross Heat of Combustion Btu/lb D4809 19,318 20,216 19,242 19,312 19,628 19,191

Toluene vol. % D3606 4.66 3.95 4.46 4.13 11.93 3.94

Watera mass % E-1064 0.052 0.005 0.051 0.063 0.004 0.058

Leada g/l D3237 - <0.001 - - <0.003 -

Copper Strip Corrosiona - D130 1A 1A 1A 1A 1A 1A

Solvent Washed Gum Contenta mg/100ml D381 <0.5 <0.5 <0.5 1.5 <0.5 <0.5

Oxidation Stabilitya min. D525 >240 >240 >240 >240 >240 >240

a

 – inspection results from Haltermann

b

 – inspection results from EPA Fuels Round Robin study

TEST 

METHOD PROPERTY UNIT

D86 (OptiDist 

or equivalent for 

E10, E15 and 

E20 fuels)
REPORT 03.14295/03-51563E A-2 

EPACT/V2/E-89 GASOLINE LIGHT-DUTY EXHAUST FUEL EFFECTS TEST 

PROGRAM – DETAILED FUEL INSPECTION DATA (CONT’D) 

 

FUEL

7 8 9 10 11 12

Density, 60o

F g/cm3 D4052 0.7211 0.7203 0.7453 0.7663 0.7601 0.7521

API Gravity, 60o

F oAPI D4052 64.7 64.9 58.3 53.1 54.6 56.6

Ethanol vol. % D5599 <0.1 <0.1 <0.1 9.87 10.21 9.85

Total Content of Oxygenates 

Other Than Ethanol vol. % D5599 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1

Distillation IBP oF 100 84 84 106 92 92

5% evap oF 128 108 102 131 117 111

10% evap oF 137 124 113 137 125 117

20% evap oF 149 152 129 144 138 124

30% evap oF 161 182 146 151 148 134

40% evap oF 177 205 166 163 157 143

50% evap oF 193 222 191 218 196 153

60% evap oF 210 234 223 263 233 210

70% evap oF 229 248 260 289 253 280

80% evap oF 252 266 292 319 273 312

90% evap oF 297 304 341 342 303 342

95% evap oF 329 332 363 357 336 365

FBP oF 359 360 381 372 361 380

Recovery vol. % 97.9 96.9 97.2 98.0 97.9 97.5

Residue vol. % 0.8 1.1 0.5 1.0 1.0 1.1

Loss vol. % 1.3 2 2.3 1.0 1.1 1.4

DVPE psi D5191 7.32 9.93 10.32 7.02 9.87 10.14

Aromatics vol. % D1319 16.7 16.0 37.3 35.6 35.1 35.1

Olefins vol. % D1319 7.3 6.2 6.2 6.0 6.3 6.0

Benzene vol. % D3606 0.55 0.48 0.55 0.58 0.57 0.62

S mg/kg D5453 23 22 23 25 22 19

RON - D2699 92 96 94 98 98 100

MON - D2700 85 88 85 87 86 88

(R + M)/2 - Calc. 88 92 90 93 92 94

C mass % D5291 mod. 85.32 85.49 87.15 83.49 83.71 83.76

H mass % D5291 mod. 14.20 14.16 12.78 12.67 12.50 12.74

O mass % D5599 <0.1 0 <0.1 3.6 3.7 3.6

Gross Heat of Combustion Btu/lb D4809 20,125 20,209 19,757 18,958 18,817 18,950

Toluene vol. % D3606 5.07 4.31 14.16 8.5 12.77 8.58

Watera mass % E-1064 0.005 <0.1 0.007 0.058 0.055 0.053

Leada g/l D3237 <0.001 0.001 <0.001 <0.003 - <0.003

Copper Strip Corrosiona - D130 1A 1A 1A 1A 1A 1A

Solvent Washed Gum Contenta mg/100ml D381 <0.5 <0.5 <0.5 <0.5 0.5 <0.5

Oxidation Stabilitya min. D525 >240 >240 >240 >240 >240 >240

a

 – inspection results from Haltermann

b

 – inspection results from EPA Fuels Round Robin study

PROPERTY UNIT TEST 

METHOD

D86 (OptiDist 

or equivalent for 

E10, E15 and 

E20 fuels)
REPORT 03.14295/03-51563E A-3 

EPACT/V2/E-89 GASOLINE LIGHT-DUTY EXHAUST FUEL EFFECTS TEST 

PROGRAM – DETAILED FUEL INSPECTION DATA (CONT’D) 

 

FUEL

13 14 15 16 17 18 19

Density, 60o

F g/cm3 D4052 0.7544 0.7227 0.7431 0.7645 0.7583 0.7536 0.7495

API Gravity, 60o

F oAPI D4052 56.0 64.2 58.8 53.5 55.1 56.1 57.3

Ethanol vol. % D5599 <0.1 <0.1 <0.1 10.62 <0.1 9.39 13.94

Total Content of Oxygenates 

Other Than Ethanol vol. % D5599 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1

Distillation IBP oF 97 99 80 106 89 98 93

5% evap oF 123 124 106 134 116 123 117

10% evap oF 137 134 116 140 130 134 128

20% evap oF 157 146 131 148 158 148 137

30% evap oF 177 159 147 156 182 154 144

40% evap oF 198 174 166 175 199 170 156

50% evap oF 222 192 190 221 215 211 181

60% evap oF 245 210 216 238 235 233 246

70% evap oF 270 236 244 254 264 265 262

80% evap oF 303 277 267 271 296 297 287

90% evap oF 339 338 299 306 323 319 312

95% evap oF 355 354 328 342 339 330 327

FBP oF 377 369 365 370 371 345 350

Recovery vol. % 96.9 97.7 97.8 97.6 98.1 97.8 97.9

Residue vol. % 1 0.6 0.8 1.0 0.8 0.8 0.6

Loss vol. % 2.1 1.7 1.4 1.4 1.1 1.4 1.5

DVPE psi D5191 6.92 7.09 10.06 7.00 9.34 8.99 8.99

Aromatics vol. % D1319 33.5 16.6 36.7 36.7 29.5 22.9 22.06

Olefins vol. % D1319 5.1 7.7 7.2 6.7 6.3 5.7 6.18

Benzene vol. % D3606 0.53 0.52 0.53 0.65 0.46 0.68 0.71

S mg/kg D5453 22 24 23 22 23 22 21

RON - D2699 96 92 95 101 93 94 94

MON - D2700 86 85 85 88 83 85 85

(R + M)/2 - Calc. 91 88 90 95 88 89 89

C mass % D5291 mod. 86.63 85.42 87.06 83.32 86.50 82.92 81.47

H mass % D5291 mod. 13.60 14.24 12.91 12.64 13.50 13.66 13.45

O mass % D5599 <0.1 <0.1 <0.1 3.8 <0.1 3.42 5.08

Gross Heat of Combustion Btu/lb D4809 19,729 20,128 19,710 18,769 19,775 19,117 18,725

Toluene vol. % D3606 12.21 4.42 16.26 12.85 4.59 4.39 6.37

Watera mass % E-1064 <0.1 0.005 0.007 0.057 <0.1 <0.1 <0.1

Leada g/l D3237 <0.001 <0.001 <0.001 - - - -

Copper Strip Corrosiona - D130 1A 1A 1A 1A 1A 0 0

Solvent Washed Gum Contenta mg/100ml D381 1.5 <0.5 0.5 1 <0.5 0 0

Oxidation Stabilitya min. D525 >240 >240 >240 >240 >240 0 0

a

 – inspection results from Haltermann

b

 – inspection results from EPA Fuels Round Robin study

PROPERTY UNIT TEST 

METHOD

D86 (OptiDist 

or equivalent for 

E10, E15 and 

E20 fuels)
REPORT 03.14295/03-51563E A-4 

EPACT/V2/E-89 GASOLINE LIGHT-DUTY EXHAUST FUEL EFFECTS TEST 

PROGRAM – DETAILED FUEL INSPECTION DATA (CONT’D) 

 

FUEL

20 21 22 23 24 25

Density, 60o

F g/cm3 D4052 0.7429 0.7764 0.7375 0.7485 0.7428 0.7714

API Gravity, 60o

F oAPI D4052 58.9 50.7 60.3 57.5 58.9 51.8

Ethanol vol. % D5599 19.77 20.04 20.06 20.04 20.08 19.91

Total Content of Oxygenates 

Other Than Ethanol vol. % D5599 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1

Distillation IBP oF 107 109 93 110 91 92

5% evap oF 137 136 121 134 120 119

10% evap oF 143 142 130 139 129 129

20% evap oF 149 150 145 146 144 145

30% evap oF 155 157 154 152 154 155

40% evap oF 159 163 159 157 160 162

50% evap oF 162 168 163 162 165 167

60% evap oF 182 223 168 178 185 237

70% evap oF 234 255 234 272 270 289

80% evap oF 252 277 257 313 310 317

90% evap oF 300 308 303 338 341 344

95% evap oF 338 334 343 351 354 363

FBP oF 377 360 377 365 370 377

Recovery vol. % 98.8 98.2 97.8 98.6 97.6 97.1

Residue vol. % 1.0 1.0 1.0 1.0 1.1 1.1

Loss vol. % 0.2 0.8 1.2 0.4 1.3 1.8

DVPE psi D5191 6.70 6.94 10.22 6.64 10.19 10.10

Aromatics vol. % D1319 16.3 34.5 15.4 16.5 15.9 37.9

Olefins vol. % D1319 7.3 7.1 7.1 7.0 6.6 6.8

Benzene vol. % D3606 0.69 0.72 0.65 0.70 0.71 0.75

S mg/kg D5453 23 20 21 22 21 25

RON - D2699 102 100 101 98 101 101

MON - D2700 90 88 90 87 89 88

(R + M)/2 - Calc. 96 94 95 93 95 95

C mass % D5291 mod. 78.00 80.70 78.64 77.83 78.40 80.97

H mass % D5291 mod. 14.26 12.24 13.71 14.88 13.94 11.85

O mass % D5599 7.4 7.1 7.5 7.4 7.5 7.1

Gross Heat of Combustion Btu/lb D4809 18,473 18,021 18,470 18,434 18,447 17,309

Toluene vol. % D3606 4.15 12.81 4.10 4.06 4.08 8.78

Watera mass % E-1064 <0.1 <0.1 0.105 <0.1 0.103 0.113

Leada g/l D3237 <0.0003 0.009 0.004 <0.003 0.005 0.001

Copper Strip Corrosiona - D130 1A 1A 1A 1A 1A 1A

Solvent Washed Gum Contenta mg/100ml D381 <0.5 0.5 <0.5 0.5 0.5 <0.5

Oxidation Stabilitya min. D525 >240 >240 >240 >240 >240 >240

a

 – inspection results from Haltermann

b

 – inspection results from EPA Fuels Round Robin study

PROPERTY UNIT TEST 

METHOD

D86 (OptiDist 

or equivalent for 

E10, E15 and 

E20 fuels)
REPORT 03.14295/03-51563E A-5 

EPACT/V2/E-89 GASOLINE LIGHT-DUTY EXHAUST FUEL EFFECTS TEST 

PROGRAM – DETAILED FUEL INSPECTION DATA (CONT’D) 

FUEL

26 27 28 29b 30 31

Density, 60o

F g/cm3 D4052 0.7624 0.7448 0.7724 0.7797 0.7513 0.7748

API Gravity, 60o

F oAPI D4052 54.0 58.4 51.6 49.8 56.8 51.0

Ethanol vol. % D5599 15.13 14.71 14.59 77.15 9.91 20.08

Total Content of Oxygenates 

Other Than Ethanol vol. % D5599 <0.1 <0.1 <0.1 <0.01 <0.1 <0.1

Distillation IBP oF 93 111 107 99 92 106

5% evap oF 113 138 136 133 108 134

10% evap oF 119 143 144 154 115 140

20% evap oF 130 153 153 168 125 149

30% evap oF 140 159 159 170 134 156

40% evap oF 151 164 164 171 143 162

50% evap oF 161 225 219 172 152 167

60% evap oF 188 252 241 172 208 236

70% evap oF 280 276 254 173 270 274

80% evap oF 313 316 270 173 298 302

90% evap oF 344 342 303 174 329 330

95% evap oF 357 352 337 176 333 350

FBP oF 376 372 364 266 364 366

Recovery vol. % 97.4 97.5 98.2 na 97.2 97.6

Residue vol. % 1.1 1.0 1.0 na 1.0 1.0

Loss vol. % 1.5 1.5 0.8 na 1.8 1.4

DVPE psi D5191 9.96 6.92 6.80 8.92 10.04 6.88

Aromatics vol. % D1319 36.9 16.2 36.5 - 37.1 38.0

Olefins vol. % D1319 6.8 8.1 7.2 - 6.4 5.7

Benzene vol. % D3606 0.67 0.66 0.69 0.12 0.70 0.79

S mg/kg D5453 23 26 24 16 25 22

RON - D2699 101 100 102 - 100 101

MON - D2700 89 89 90 - 88 88

(R + M)/2 - Calc. 95 95 96 - 94 94

C mass % D5291 mod. 82.09 81.08 82.05 57.74 82.66 80.41

H mass % D5291 mod. 12.18 13.85 12.50 12.80 13.83 12.45

O mass % D5599 5.5 5.5 5.2 27.19 3.7 7.2

Gross Heat of Combustion Btu/lb D4809 18,524 18,972 18,575 12,925 18,963 18,021

Toluene vol. % D3606 8.65 3.91 12.38 - 9.69 9.67

Watera mass % E-1064 0.084 0.088 0.088 0.93 <0.1 <0.1

Leada g/l D3237 <0.003 <0.003 <0.003 - - <0.003

Copper Strip Corrosiona - D130 1A 1A 1A - 1A 1A

Solvent Washed Gum Contenta mg/100ml D381 <0.5 0.5 <0.5 1.9 <0.5 0.5

Oxidation Stabilitya min. D525 >240 >240 >240 - >240 >240

a

 – inspection results from Haltermann

b

 – inspection results from EPA Fuels Round Robin study

PROPERTY UNIT TEST 

METHOD

D86 (OptiDist 

or equivalent for 

E10, E15 and 

E20 fuels)
REPORT 03.14295/03-51563E

APPENDIX B 

FUEL ANALYSES SUMMARY 
REPORT 03.14295/03-51563E B-1 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 1 Batch No.: WL1821GP04 WL1821GP04 WL1821GP04 WL1821GP04 WL1821GP04 WL1821GP04 

PRODUCT CODE: HF078‐1 Analysis Date: 1/14/2009 1/12/2009 1/12/2009 1/9/2009 1/8/2009 1/7/2009 12/1

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RES

MIN TARGET MAX optidist optidist 

Distillation ‐ IBP ASTM D86 °F 93.0 93.0 95.5 

5% °F 111.6 111.9 111.6 10% °F 110 115 120 116.7 116.7 116.6 20% °F 120.0 123.4 123.1 30% °F 126 131 136 130.9 130.8 130.6 40% °F 139.5 139.5 138.9 50% °F 144 148 152 148.7 148.1 147.7 60% °F 170.5 171.8 164.5 70% °F 219 224 229 223.9 224.2 222.1 80% °F 252.8 254.5 248.9 90% °F 295 300 305 298.5 299.6 296.8 95% °F 333.6 334.1 329.7 Distillation ‐ EP °F 437 366.3 366.3 362.5 Recovery vol % Report 98.5 97.8 97.8 

Residue vol % Report 1.0 1.1 0.9 

Loss vol % Report 0.5 1.1 1.3 

Gravity ASTM D4052 °API Report 64.5 64.6 

Specific Gravity ASTM D4052  ‐ Report 0.7228 0.7215 

Reid Vapor Pressure ASTM D5191 psi 9.85 10.00 10.15 9.90 9.98/9.99 8.00 

Carbon ASTM D5291 wt fraction Report 81.5 Hydrogen ASTM D5291 wt fraction Report 14.5 Oxygen ASTM D5599 wt fraction Report 3.7 Oxygen, other then ETOH ASTM D5599 vol % 0.10 <0.01 Ethanol content ASTM D5599 vol % 9.50 10.50 9.59 Water content ASTM E1064 mg/kg Report 520 Sulfur ASTM D5453 ppm wt 20 30 34 32 24.6 

Composition, aromatics, corrected ASTM D1319 vol % 13.5 16.5 15.8 16.2 

Composition, olefins, corrected ASTM D1319 vol % 5.8 7.3 8.8 6.5 7.2 

Composition, saturates, corrected ASTM D1319 vol % Report 67.7 66.6 

Benzene ASTM D3606 vol % 0.47 0.77 0.59 0

Existent gum, washed ASTM D381 mg/100mls 5.0 <0.5

Research Octane Number ASTM D2699 Report 94.8

Motor Octane Number ASTM D2700 Report 87.3R+M D2699/2700 87.0 91.0

Corrosion, Copper ASTM D130 1 1A

Oxidation stability ASTM D525 minutes 240 >240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report 17991.0

ANALYST Paragon Core Dixie HP Inspectorate Gage D

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-2 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 1 Batch No.: 1C 1C 1B 1B 1A 1A 1A PRODUCT CODE: HF078‐1 Analysis Date: 11/26/2008 11/26/2008 11/11/2008 11/11/2008 11/3/2008 11/3/2008 11/3/2008 3/2

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RE

MIN TARGET MAX Optidist Optidist 2 Optidist 1 Distillation ‐ IBP ASTM D86 °F 91.3 97.0 95.2 93.5 

5% °F 109.0 113.1 112.6 111.6 110% °F 110 115 120 114.7 118.4 117.9 117.3 120% °F 121.9 125.5 125.1 124.6 130% °F 126 131 136 129.6 133.1 132.9 132.5 140% °F 138.1 142.4 142.1 141.8 150% °F 144 148 152 147.1 152.3 152.1 151.8 1

60% °F 166.1 176.6 172.9 170.1 170% °F 219 224 229 219.5 229.7 228.0 229.3 280% °F 252.8 257.3 256.0 255.0 290% °F 295 300 305 297.0 300.0 297.1 293.7 295% °F 332.8 335.1 333.8 331.7 3Distillation ‐ EP °F 437 366.9 369.6 361.7 364.3 3

Recovery vol % Report 97.2 98 97.9 97.6 

Residue vol % Report 1.1 1.0 1.0 1.0 Loss vol % Report 1.7 1.0 1.1 1.4 Gravity ASTM D4052 °API Report 64.2 64.1 64.0 Specific Gravity ASTM D4052  ‐ Report 0.7229 0.7235 0.7238 0

Reid Vapor Pressure ASTM D5191 psi 9.85 10.00 10.15 10.03 10.21 10.24 

Carbon ASTM D5291 wt fraction Report Hydrogen ASTM D5291 wt fraction Report Oxygen ASTM D5599 wt fraction Report Oxygen, other then ETOH ASTM D5599 vol % 0.10 Ethanol content ASTM D5599 vol % 9.50 10.50 1

Water content ASTM E1064 mg/kg ReportSulfur ASTM D5453 ppm wt 20 30 21

Composition, aromatics, corrected ASTM D1319 vol % 13.5 16.5 14.7 15.2 14.5 14.9 16.2 17.1 16.1 

Composition, olefins, corrected ASTM D1319 vol % 5.8 7.3 8.8 5.5 7.8 7.7 7.1 6.7 7.5 6.5 

Composition, saturates, corrected ASTM D1319 vol % Report 69.9 67.1 67.9 68.0 67.1 65.4 67.9 Benzene ASTM D3606 vol % 0.47 0.77 0.67

Existent gum, washed ASTM D381 mg/100mls 5.0

Research Octane Number ASTM D2699 Report 

Motor Octane Number ASTM D2700 Report 

R+M D2699/2700 87.0 

Corrosion, Copper ASTM D130 1Oxidation stability ASTM D525 minutes 240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report

ANALYST Dixie JB/INS JB JB Core Inspectorate JB 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-3 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 2 Batch No.: WK0521GP14 WK0521GP14 WK0521GP14 WK0521GP14 2E 2D 2C HB #9 HB #8 HB #7 HB #6 

PRODUCT CODE: HF0678‐2 Analysis Date: 11/26/2008 11/20/2008 11/18/2008 11/12/2008 10/24/2008 10/20/2008 10/13/2008 3/26/2008 3/26/2008 3/25/2008 3/

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS R

MIN TARGET MAX Distillation ‐ IBP ASTM D86 °F 79.3 87.0 82.0 90.5 82.8 85.6 92.1 82.0 82.0 95.0 

5% °F 99.2 107.8 97.0 93.2 103.4 104.7 112.7 102.7 102.7 113.2 10% °F 114 119 124 116.4 123.4 117.0 115.9 118.8 119.6 128.5 118.0 118.0 127.5 20% °F 150.9 157.0 152.0 148.1 151.0 150.9 158.2 149.6 149.6 163.6 30% °F 184 189 194 189.0 194.8 190.0 185.4 188.8 186.8 197.7 192.8 192.8 204.8 40% °F 217.8 223.3 218.0 216.1 218.2 218.0 225.4 224.0 224.0 230.1 50% °F 234 238 242 236.6 241.2 237.0 235.4 237.9 239.8 237.0 238.0 238.0 243.0 

60% °F 251.8 256.6 253.0 250.5 253.9 257.8 248.2 248.5 248.5 253.1 70% °F 268 273 278 271.0 275.4 271.0 269.4 272.7 280.1 258.2 260.9 260.9 266.9 80% °F 304.6 309.9 306.0 302.7 305.6 312.4 274.1 284.3 284.3 293.2 90% °F 335 340 345 337.5 344.5 342.0 323.1 339.4 338.0 325.9 344.2 344.2 349.6 95% °F 351.0 357.0 356.0 338.7 352.5 349.2 361.2 367.4 367.4 368.8 Distillation ‐ EP °F 437 375.2 381.4 373.0 375.3 371.9 368.4 388.8 392.3 392.3 390.4 Recovery vol % Report 97.3 97.3 97.0 95.1 97.2 97.2 96.9 97.5 97.5 96.8 Residue vol % Report 1.1 1.1 1.2 0.9 1.1 1.0 1.0 1.0 1.0 1.0 Loss vol % Report 1.6 1.6 1.8 4.0 1.7 1.8 2.1 1.5 1.5 2.2 Gravity ASTM D4052 °API Report 64.4 64.4 64.5 63.6 64.3 64.9 64.9 63.2 Specific Gravity ASTM D4052  ‐ Report 0.7227 0.7222 0.7221 0.7251 0.7227 0.7205 0.7205 0.7268 0Reid Vapor Pressure ASTM D5191 psi 9.90 10.05 10.20 9.98 10.15 10.20 10.05 10.3900 9.8100 9.24 11.20 11.20 9.60 

Carbon ASTM D5291 wt fraction Report 84.5 Hydrogen ASTM D5291 wt fraction Report 15.5 Oxygen ASTM D5599 wt fraction Report <0.1 Oxygen, other then ETOH ASTM D5599 wt fraction 0.10 <0.01 Ethanol content ASTM D5599 wt % 0.05 <0.01 Water content ASTM E1064 mg/kg Report 51 Sulfur ASTM D5453 ppm wt 20 30 25 18.28 23 22 Composition, aromatics ASTM D1319 vol % 13.5 15.0 16.5 14.2 14.1 15.0 14.2 14.6 

Composition, olefins ASTM D1319 vol % 5.5 7.0 8.5 6.3 5.7 6.5 7.4 5.5 

Composition, saturates ASTM D1319 vol % Report 79.5 80.2 78.5 78.4 79.9 

Benzene ASTM D3606 vol % 0.47 0.77 0.46 0.25 0.29 Existent gum, washed ASTM D381 mg/100mls 5.0 <0.5 Research Octane Number ASTM D2699 Report 96.1 96.3 95.6 91.6 

Motor Octane Number ASTM D2700 Report 88.4 88.9 88.4 85.1 

R+M D2699/2700 87.0 92.3 92.6 92.0 88.4 

Corrosion, Copper ASTM D130 1 1A Oxidation stability ASTM D525 minutes 240 >240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report 18745

ANALYST INS JB Dixie Gage JB JB JB HVD HVD HVD 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-4 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 3 Batch No.: XB0921GP01 XB0921GP01 XB0921GP01 XB0921GP01 XB0921GP01 XB0921GP01 XB0921GP01 XB0921GP01 3G 

PRODUCT CODE: HF0678‐3 Analysis Date: 2/26/2009 2/25/2009 2/23/2009 2/16/2009 2/16/2009 2/13/2009 2/16/2009 2/10/2009 2/2/2009 

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX Optidist 

Distillation ‐ IBP ASTM D86 °F 108.3 106.7 107.9 109 118.8 5% °F 136.1 135.6 137.0 135.9 137.5 10% °F 136 141 146 141.5 141.4 142.1 141.7 141.8 20% °F 148.5 148.7 149.1 145.4 149 

30% °F 149 154 159 154.5 154.7 155.3 154.5 155.5 

40% °F 175.5 174.8 182.6 182.5 182.7 50% °F 215 219 223 216.8 216.8 218.0 218.5 218.1 60% °F 229.8 231.1 231.8 232.7 231.8 70% °F 242 247 252 244.4 242.9 243.9 244.9 241.3 80% °F 258.5 247.7 258.1 259.5 259 

90% °F 295 300 305 297.1 293.7 294.5 296.1 293 

95% °F 333.2 332.7 328.8 334 329.9 Distillation ‐ EP °F 437 373.5 566.4 365.2 372.8 370.9 Recovery vol % Report 98.8 98.9 97.7 98.1 98.1 

Residue vol % Report 1.0 1.0 1.0 1.0 0.9 

Loss vol % Report 0.2 0.1 1.3 0.9 1 

Gravity ASTM D4052 °API Report 60.6 60.8 

Specific Gravity ASTM D4052  ‐ Report 0.736 

Reid Vapor Pressure ASTM D5191 psi 6.65 6.80 6.95 6.76 6.48 6.32 6.34 

Carbon ASTM D5291 wt fraction Report 81 Hydrogen ASTM D5291 wt fraction Report 14.4 Oxygen ASTM D5599 wt fraction Report 3.5 Oxygen, other then ETOH ASTM D5599 vol % 0.10 <0.01 Ethanol content ASTM D5599 vol % 9.50 10.0 10.50 10.15 9.40 Water content ASTM E1064 mg/kg Report 514.00 Sulfur ASTM D5453 ppm wt 20 25 30 23 17.71 

Composition, aromatics, corrected ASTM D1319 vol % 13.8 15.3 16.8 14.6 15.7 15.3 

Composition, olefins, corrected ASTM D1319 vol % 5.3 6.8 8.3 6.8 7.8 6.2 Composition, saturates, corrected ASTM D1319 vol % Report 68.7 66.5 68.5 

Benzene ASTM D3606 vol % 0.47 0.62 0.77 0.54 0.33

Existent gum, washed ASTM D381 mg/100mls 5.0 <0.5

Research Octane Number ASTM D2699 97.7

Motor Octane Number ASTM D2700 86.9

R+M D2699/2700 87.0 92.3

Corrosion, Copper ASTM D130 1 1A

Oxidation stability ASTM D525 minutes 240 >240Net Heat of Combustion ASTM D4809‐A BTU/lb Report 17567

ANALYST INS JAM Dixie Core Dixie INS JB Gage Core 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-5 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 3 Batch No.: 3F 3F 3F 3E 3E 3E 3E 3E 3E 3E 3D 

PRODUCT CODE: HF0678‐3 Analysis Date: 1/23/2009 1/23/2009 1/22/2009 12/30/2008 12/28/2008 12/26/2008 12/22/2008 12/22/2008 12/24/2008 12/22/2008 12/10/2008 12/

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RE

MIN TARGET MAX Optidist Optidist Optidist Optidist 

Distillation ‐ IBP ASTM D86 °F 110.1 109.6 113.2 111.9 108.5 109.4 

5% °F 136.8 136.4 137.8 138.4 137.3 137.1 10% °F 136 141 146 142 142.0 142.5 145.0 142.3 142.3 20% °F 148.8 148.9 149.7 150.1 149.2 149.4 30% °F 149 154 159 154.2 154.9 156.4 156.3 156.2 155.8 40% °F 181 180.7 190.6 196.4 193.8 186.0 50% °F 215 219 223 219.6 219.1 221.4 223.5 222.4 220.5 

60% °F 232.5 233.6 230.5 235.1 236.1 235.2 70% °F 242 247 252 245.1 245.1 241.5 243.6 243.0 247.2 80% °F 259.2 260.4 264.2 264.0 268.7 257.4 90% °F 295 300 305 295.3 294.7 305.1 310.8 313.2 301.0 

95% °F 331.5 332.3 341.1 347.8 350.6 337.8 Distillation ‐ EP °F 437 369.9 372.7 372.4 373.3 437.4 375.6 

Recovery vol % Report 97.6 98.6 98.4 97.5 97.7 98.8 

Residue vol % Report 1.0 1.0 1.0 1.1 1.1 1.1 Loss vol % Report 1.4 0.4 0.6 1.4 1.2 0.1 Gravity ASTM D4052 °API Report 60.2 60.4 60.4 60.1 

Specific Gravity ASTM D4052  ‐ Report 0.7380 0.7372 0.7384 

Reid Vapor Pressure ASTM D5191 psi 6.65 6.80 6.95 6.44 6.37 6.24 6.24 6.32 6.41 

Carbon ASTM D5291 wt fraction Report Hydrogen ASTM D5291 wt fraction Report Oxygen ASTM D5599 wt fraction Report Oxygen, other then ETOH ASTM D5599 vol % 0.10 Ethanol content ASTM D5599 vol % 9.50 10.0 10.50 9.9 Cal 9.9 Cal Water content ASTM E1064 mg/kg Report Sulfur ASTM D5453 ppm wt 20 25 30 25 Composition, aromatics, corrected ASTM D1319 vol % 13.8 15.3 16.8 16.0 15.0 15.0 15.8 

Composition, olefins, corrected ASTM D1319 vol % 5.3 6.8 8.3 7.7 6.1 6.1 7.2 

Composition, saturates, corrected ASTM D1319 vol % Report 66.2 69.0 69.0 67.1 

Benzene ASTM D3606 vol % 0.47 0.62 0.77 0.35 Existent gum, washed ASTM D381 mg/100mls 5.0 Research Octane Number ASTM D2699 Motor Octane Number ASTM D2700

R+M D2699/2700 87.0

Corrosion, Copper ASTM D130 1

Oxidation stability ASTM D525 minutes 240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report

ANALYST Dixie INS JB JB INS Core Core Dixie Inpectorate JB Dixie 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-6 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 3 Batch No.: 3B 3B 3A 3A 3A HB#5 HB#4 HB#3 

PRODUCT CODE: HF0678‐3 Analysis Date: 11/11/2008 11/11/2008 11/3/2008 11/3/2008 11/3/2008 4/1/2008 4/2/2008 4/1/2008 

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX Optidist 1 Distillation ‐ IBP ASTM D86 °F 108.2 109.6 108.2 105.5 105.3 

5% °F 135.9 134.0 132.4 132.9 131.4 10% °F 136 141 146 141.7 141.6 138.5 138.6 137.1 20% °F 150.1 150.1 146.5 146.5 145.4 30% °F 149 154 159 157.1 157.8 153.3 153.9 152.4 40% °F 175.2 177.1 178.4 179.7 173.2 50% °F 215 219 223 222.8 222.2 219.6 219.6 219.9 

60% °F 238.6 237.6 233.6 232.1 235.4 70% °F 242 247 252 249.1 249.8 246.3 244.9 249.5 80% °F 264.4 262.2 265.1 260.9 270.8 90% °F 295 300 305 301.6 288.4 299.0 292.5 311.1 95% °F 339.9 326.5 324.8 322.3 329.5 Distillation ‐ EP °F 437 378.2 367.7 355.5 355.5 356.7 

Recovery vol % Report 98.7 96.6 97.7 98.3 98.2 

Residue vol % Report 1.0 1.1 1.0 1.0 1.0 

Loss vol % Report 0.3 2.3 1.3 0.7 0.8 

Gravity ASTM D4052 °API Report 60.8 60.1 59.5 59.7 

Specific Gravity ASTM D4052  ‐ Report 0.736 0.7384 0.7409 0.7399 

Reid Vapor Pressure ASTM D5191 psi 6.65 6.80 6.95 6.78 6.68 6.77 6.88 

Carbon ASTM D5291 wt fraction Report Hydrogen ASTM D5291 wt fraction Report Oxygen ASTM D5599 wt fraction Report Oxygen, other then ETOH ASTM D5599 vol % 0.10 Ethanol content ASTM D5599 vol % 9.50 10.0 10.50 9.70 9.70 9.70 

Water content ASTM E1064 mg/kg Report Sulfur ASTM D5453 ppm wt 20 25 30 22 Composition, aromatics, corrected ASTM D1319 vol % 13.8 15.3 16.8 14.3 14.7 15.6 16.0 16.1 14.9 14.9 14.9 

Composition, olefins, corrected ASTM D1319 vol % 5.3 6.8 8.3 6.5 6.5 6.6 7.8 6.4 8.0 8.0 8.0 

Composition, saturates, corrected ASTM D1319 vol % Report 69.2 68.8 67.9 66.2 68.0 67.4 67.4 67.4 

Benzene ASTM D3606 vol % 0.47 0.62 0.77 0.34

Existent gum, washed ASTM D381 mg/100mls 5.0

Research Octane Number ASTM D2699 99.2 93.2 

Motor Octane Number ASTM D2700 88.7 84.8 

R+M D2699/2700 87.0 94.0 89.0 

Corrosion, Copper ASTM D130 1

Oxidation stability ASTM D525 minutes 240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report

ANALYST Dixie JB Core Inspectorate JB HVD HVD HVD 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-7 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 4 Batch No.: WL0121GP01 WL0121GP01 WL0121GP01 WL0121GP01 WL0121GP01 WL0121GP01 WL0121GP01 WL0121GP01 WL0121GP01 WL0121GP01 WL0121GP01 WL0

PRODUCT CODE: HF0678‐4 Analysis Date: 1/15/2009 12/26/2008 12/26/2008 12/20/2008 12/19/2008 12/12/2008 12/12/2008 12/12/2008 12/10/2008 12/10/2008 12/3/2008 11/

TEST METHOD UNITS SPECIFICATIONS Results Results Results Results Results Results Results Results Results Results Results R

MIN TARGET MAX optidist optidist optidist optidist optidist Optidist 

Distillation ‐ IBP ASTM D86 °F 90.7 88.7 88.0 92.4 86.1 88.6 92.0 

5% °F 112.8 116.9 116.3 113.7 113.1 112.4 110.0 10% °F 121 126 131 124.0 126.9 126.7 124.1 123.7 122.7 124.0 20% °F 139.0 141.4 141.6 139.6 139.0 138.6 140.0 30% °F 149 154 159 150.6 152.0 152.4 150.9 150.3 150.0 151.0 40% °F 157.8 164.2 165.5 161.0 157.8 158.7 158.0 50% °F 215 219 223 218.6 225.4 225.1 218.7 216.5 214.6 216.0 60% °F 239.2 242.7 247.7 243.9 240.0 237.1 247.0 70% °F 265 270 275 266.5 272.7 269.3 267.3 259.8 264.6 268.0 80% °F 301.8 308.1 309.9 302.4 296.6 294.9 302.0 90% °F 334 339 344 336.2 340.7 342.3 336.1 335.5 334.7 338.0 95% °F 350.4 356.4 358.7 350.1 350.0 350.1 355.0 Distillation ‐ EP °F 437 368.8 370.1 370.2 369.1 371.0 370.3 375.0 

Recovery vol % Report 97 97.1 97.3 97.3 97.5 97.2 97.3 

Residue vol % Report 1.1 1.1 1.1 1.1 1.1 1.1 1.1 

Loss vol % Report 1.9 1.8 1.6 1.6 1.4 1.7 1.6 

Gravity ASTM D4052 °API Report 60.7 61.4 61.4 

Specific Gravity ASTM D4052  ‐ Report 0.7361 0.7340 0.7340 0

Reid Vapor Pressure ASTM D5191 psi 9.95 10.10 10.25 9.95 9.93 10.00 10.01 10.10 

Carbon ASTM D5291 wt fraction Report 78.5 Hydrogen ASTM D5291 wt fraction Report 15.3 Oxygen ASTM D5599 wt fraction Report 3.6 Oxygen, other then ETOH ASTM D5599 wt fraction 0.10 <0.01 Ethanol content ASTM D5599 wt % 9.50 10.50 10.02 10.31 

Water content ASTM E1064 mg/kg Report 633 656 Sulfur ASTM D5453 ppm wt 20 25 30 30 23 

Composition, aromatics ASTM D1319 vol % 13.5 15.0 16.5 16.0 15.1 15.4 14.8 Composition, olefins ASTM D1319 vol % 4.6 6.1 7.6 6.1 6.1 6.6 6.0 Composition, saturates ASTM D1319 vol % Report 67.9 68.6 68.1 69.6 Benzene ASTM D3606 vol % 0.47 0.77 5.10 0.51 0.40 

Existent gum, washed ASTM D381 mg/100mls 5.0 1.5

Research Octane Number ASTM D2699 Report 97.2 

Motor Octane Number ASTM D2700 Report 87.5 

R+M D2699/2700 87.0 92.3 

Corrosion, Copper ASTM D130 1 1a

Oxidation stability ASTM D525 minutes 240 >240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report 17918

ANALYST Inspectorate JB INS INS JB Core Inspectorate Dixie Inspectorate JB Dixie 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-8 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 5 Batch No.: XB2321GP01 XB2321GP01 XB2321GP01 XB2321GP01 XB2321GP01 XB2321GP01 5 ReBl

PRODUCT CODE: HF0678‐5 Analysis Date: 3/3/2009 3/4/2009 3/2/2009 3/4/2009 2/27/2009 2/26/2009 1/7/2

Shipment Date: TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESU

MIN TARGET MAX 797 

Distillation ‐ IBP ASTM D86 °F 89.9 93.5 5% °F 125.3 126.7 10% °F 141 146 151 142.4 143.5 20% °F 170.4 170.3 30% °F 196 201 206 197.7 198.2 40% °F 220.3 221.2 50% °F 234 238 242 235.4 236.4 60% °F 247.2 247.2 70% °F 254 259 264 257.8 258 80% °F 271.8 272.3 90% °F 296 301 306 299.7 298.1 95% °F 322 323.1 Distillation ‐ EP °F 437 354.3 356.6 

Recovery vol % Report 98.5 98.1 

Residue vol % Report 1.0 1.0 

Loss vol % Report 0.5 0.9 

Gravity ASTM D4052 °API Report 55.0 

Specific Gravity ASTM D4052  ‐ Report 0.7585 

Reid Vapor Pressure ASTM D5191 psi 6.65 6.80 6.95 6.9200 6.76 6.85 6.34 6.8

Carbon ASTM D5291 wt fraction Report 86 Hydrogen ASTM D5291 wt fraction Report 13.6 Oxygen ASTM D5599 wt fraction Report <0.1 Oxygen, other then ETOH ASTM D5599 wt fraction 0.10 <0.01 Ethanol content ASTM D5599 wt % 0.05 <0.01

Water content ASTM E1064 mg/kg Report 43

Sulfur ASTM D5453 ppm wt 20 30 26

Composition, aromatics ASTM D1319 vol % 33.5 35.0 36.5 34 34.8 

Composition, olefins ASTM D1319 vol % 5.0 6.5 8.0 5.7 7.1 

Composition, saturates ASTM D1319 vol % Report 60.3 58.1 

Benzene ASTM D3606 vol % 0.47 0.77 0.48

Existent gum, washed ASTM D381 mg/100mls 5.0 <0.5

Research Octane Number ASTM D2699 Report 97.2

Motor Octane Number ASTM D2700 Report 86.1

R+M D2699/2700 87.0 91.7Corrosion, Copper ASTM D130 1 1A

Oxidation stability ASTM D525 minutes 240 >240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report 18346

ANALYST Core Dixie Inspectorate JB Gage Gage Dix

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-9 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 5 Batch No.: WC1121GP02 WC1121GP02 WC1121GP02 WC1121GP02 lab blend #6 LB 5 

PRODUCT CODE: HF0678‐5 Analysis Date: 5/23/2008 4/18/2008 4/9/2008 4/9/2008 2/28/2008 2/26/2008 

Shipment Date: TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX Distillation ‐ IBP ASTM D86 °F 95 95 99 99 99 100 

5% °F 125 125 131 128 131 136 10% °F 141 146 151 144 144 148 147 146 150 20% °F 172 172 175 174 170 173 30% °F 196 201 206 200 200 203 201 198 198 40% °F 227 227 228 226 225 220 50% °F 234 238 242 244 244 242 241 242 233 60% °F 254 254 252 253 253 243 70% °F 254 259 264 266 266 263 263 264 253 80% °F 278 278 277 277 278 267 90% °F 296 301 306 298 298 297 297 298 300 95% °F 316 316 315 316 319 323 Distillation ‐ EP °F 437 373 373 352 356 355 358 Recovery vol % Report 99 99 98.5 98.5 97.6 97.8 Residue vol % Report 0.8 0.8 0.9 0.9 1.0 1.0 Loss vol % Report 0.2 0.2 0.6 0.6 1.4 1.2 Gravity ASTM D4052 °API Report 53.0 53.9 53.8 Specific Gravity ASTM D4052  ‐ Report 0.7672 0.7633 0.7636 Reid Vapor Pressure ASTM D5191 psi 6.65 6.80 6.95 6.79 6.49 5.74 6.50 5.96 

Carbon ASTM D5291 wt fraction Report 86.9 Hydrogen ASTM D5291 wt fraction Report 12.7 Oxygen ASTM D5599 wt fraction Report <0.1

Oxygen, other then ETOH ASTM D5599 wt fraction 0.10 0.01

Ethanol content ASTM D5599 wt % 0.05 <0.01

Water content ASTM E1064 mg/kg Report 52

Sulfur ASTM D5453 ppm wt 20 30 23 23 21 

Composition, aromatics ASTM D1319 vol % 33.5 35.0 36.5 38.6 38.3 38.9 39.8 41.5 

Composition, olefins ASTM D1319 vol % 5.0 6.5 8.0 5.7 5.7 6.8 5.3 6.9 

Composition, saturates ASTM D1319 vol % Report 56.0 56.0 54.3 54.9 51.6 

Benzene ASTM D3606 vol % 0.47 0.77 0.54 0.54 0.44 

Existent gum, washed ASTM D381 mg/100mls 5.0 <0.5

Research Octane Number ASTM D2699 Report 94.0 92.5

Motor Octane Number ASTM D2700 Report 84.7 83.8

R+M D2699/2700 87.0 89.4 88.2

Corrosion, Copper ASTM D130 1 1a

Oxidation stability ASTM D525 minutes 240 >240 >240 >240 220.0

Net Heat of Combustion ASTM D4809‐A BTU/lb Report 18417 18417 18417

ANALYST Dixie Dixie Dixie Dixie JB JB 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendatio
REPORT 03.14295/03-51563E B-10 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 6 Batch No.: XA0821GP01 XA0821GP01 XA0821GP01 XA0821GP01 XA0821GP01 

PRODUCT CODE: HF0678‐6 Analysis Date: 3/11/2009 3/11/2009 3/11/2009 3/6/2009 3/6/2009 

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX Distillation ‐ IBP ASTM D86 °F 108.6 106.4 106.1 105.3 107.6 

5% °F 131.3 130.7 129.3 127 128.9 10% °F 131 136 141 136.3 135.7 135 133.9 134.7 20% °F 142.7 142.4 141.9 140.7 141.7 30% °F 142 147 152 148.5 147.9 147.5 147.7 147.4 40% °F 153.8 153 152.7 151.9 152.5 50% °F 187 191 195 191.7 189.4 185.6 180.3 185.5 60% °F 229.5 230.3 225.3 222.4 224.7 70% °F 264 269 274 269.6 270.7 264.8 261.9 264.6 80% °F 313.5 313.2 306.8 305.8 308.2 90% °F 336 341 346 342.4 342.2 338.7 338.2 339.4 95% °F 354.9 354.5 350.6 349.5 350.4 Distillation ‐ EP °F 369.7 370.1 367.4 366.1 368.4 Recovery vol % Report 97.9 97.6 98.3 97.4 98.0 Residue vol % Report 1.0 1.0 1.0 1.0 1.0 Loss vol % Report 1.1 1.4 0.7 1.6 1.0 Gravity ASTM D4052 °API Report Specific Gravity ASTM D4052  ‐ Report Reid Vapor Pressure ASTM D5191 psi 6.70 6.85 7.00 7.14 

Carbon ASTM D5291 wt fraction Report Hydrogen ASTM D5291 wt fraction Report

Oxygen ASTM D5599 wt fraction Report

Oxygen, other then ETOH ASTM D5599 vol % 0.10

Ethanol content ASTM D5599 vol % 9.50 10.50

Water content ASTM E1064 mg/kg Report

Sulfur ASTM D5453 ppm wt 20 30

Composition, aromatics, corrected ASTM D1319 vol % 13.5 15.0 16.5

Composition, olefins, corrected ASTM D1319 vol % 5.5 7.0 8.5

Composition, saturates, corrected ASTM D1319 vol % Report

Benzene ASTM D3606 vol % 0.47 0.62 0.77

Existent gum, washed ASTM D381 mg/100mls 5.0

Research Octane Number ASTM D2699 Report

Motor Octane Number ASTM D2700 Report

R+M D2699/2700 87.0Corrosion, Copper ASTM D130 1

Oxidation stability ASTM D525 minutes 240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report

ANALYST Saybolt Insp JAM Insp JB 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s re
REPORT 03.14295/03-51563E B-11 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 6 Batch No.: XA0821GP01 XA0821GP01 XA0821GP01 XA0821GP01 XA0821GP01 XA0821GP01 XA0821GP01 XA0

PRODUCT CODE: HF0678‐6 Analysis Date: 2/5/2009 2/3/2009 2/4/2009 1/21/2009 1/21/2009 1/22/2009 1/20/2009 1/

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS R

MIN TARGET MAX bz, rvp, etoh recheck optidist o

Distillation ‐ IBP ASTM D86 °F 102.3 114.3 109.4 

5% °F 125.7 136.2 132.6 10% °F 131 136 141 133 138.9 137.5 20% °F 140.3 144.7 143.4 30% °F 142 147 152 146.4 154.22 148.8 40% °F 151.2 170.6 153 50% °F 187 191 195 181.3 196.5 199 60% °F 221.1 233.2 235 70% °F 264 269 274 260 273.4 274.5 80% °F 305.5 315.1 315.1 90% °F 336 341 346 339.3 343 343.4 95% °F 350.5 355.6 356 Distillation ‐ EP °F 365.2 367.5 370.8 

Recovery vol % Report 96.9 97.2 97.5 

Residue vol % Report 1.1 1.0 1.0 

Loss vol % Report 2.0 1.8 1.5 

Gravity ASTM D4052 °API Report 61.1 Specific Gravity ASTM D4052  ‐ Report 0.735 Reid Vapor Pressure ASTM D5191 psi 6.70 6.85 7.00 7.22 7.14 6.66 

Carbon ASTM D5291 wt fraction Report 81.3 Hydrogen ASTM D5291 wt fraction Report 15.2 Oxygen ASTM D5599 wt fraction Report 3.4 Oxygen, other then ETOH ASTM D5599 vol % 0.10 0.01 Ethanol content ASTM D5599 vol % 9.50 10.50 9.97 9.13 Water content ASTM E1064 mg/kg Report 575.00 Sulfur ASTM D5453 ppm wt 20 30 22 

Composition, aromatics, corrected ASTM D1319 vol % 13.5 15.0 16.5 15.1 Composition, olefins, corrected ASTM D1319 vol % 5.5 7.0 8.5 8.1 Composition, saturates, corrected ASTM D1319 vol % Report 66.8 

Benzene ASTM D3606 vol % 0.47 0.62 0.77 0.61 0.19Existent gum, washed ASTM D381 mg/100mls 5.0 <0.5

Research Octane Number ASTM D2699 Report 95.8

Motor Octane Number ASTM D2700 Report 85.6

R+M D2699/2700 87.0 90.7

Corrosion, Copper ASTM D130 1 1A

Oxidation stability ASTM D525 minutes 240 >240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report 17950.0

ANALYST Insp Dixie Gage Core Dixie Inspectorate Inspectorate 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-12 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 6 Batch No.: 6D 6D 6D 6D 6C 6C 6C 6C 

PRODUCT CODE: HF0678‐6 Analysis Date: 12/22/2008 12/22/2008 12/24/2008 12/22/2008 12/15/2008 12/10/2008 12/10/2008 12/10/2008 

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX D86 re‐check Optidist Optidist 

Distillation ‐ IBP ASTM D86 °F 110.2 110.3 109.7 120.3 111.1 5% °F 129.8 131.0 131.5 133.6 130.4 10% °F 131 136 141 135.3 135.7 135.6 137.6 134.7 20% °F 141.2 142.1 140.7 142.8 140.4 30% °F 142 147 152 146.9 147.4 146 147.5 145.8 40% °F 152.1 151.6 151.5 151.3 150.8 50% °F 187 191 195 189.8 191.4 179.9 188.6 182 60% °F 228.3 229.8 220.2 225 221 70% °F 264 269 274 268.0 269.5 259.6 262.3 259 80% °F 308.3 312.0 302.8 304.2 303.8 90% °F 336 341 346 340.6 341.5 337.3 338 338.2 95% °F 351.3 353.4 349.4 349.2 351.1 Distillation ‐ EP °F 372.3 379.6 369.7 387.1 371.9 

Recovery vol % Report 97.2 98.3 98.1 98.8 98.1 

Residue vol % Report 1.0 1.0 1.0 0.1 1.1 Loss vol % Report 1.8 0.7 0.9 1.1 0.8 Gravity ASTM D4052 °API Report 60.7 61.22 

Specific Gravity ASTM D4052  ‐ Report 0.736 0.734 

Reid Vapor Pressure ASTM D5191 psi 6.70 6.85 7.00 6.66 6.76 6.82 6.75 6.96 6.68 

Carbon ASTM D5291 wt fraction Report Hydrogen ASTM D5291 wt fraction Report Oxygen ASTM D5599 wt fraction Report Oxygen, other then ETOH ASTM D5599 vol % 0.10 Ethanol content ASTM D5599 vol % 9.50 10.50 9.9 cal Water content ASTM E1064 mg/kg Report Sulfur ASTM D5453 ppm wt 20 30 

Composition, aromatics, corrected ASTM D1319 vol % 13.5 15.0 16.5 15.2 14.5 15 13.6 15.3 

Composition, olefins, corrected ASTM D1319 vol % 5.5 7.0 8.5 6.1 7.5 6.6 7.4 8.1 

Composition, saturates, corrected ASTM D1319 vol % Report 68.7 68.1 68.6 68.7 66.7 

Benzene ASTM D3606 vol % 0.47 0.62 0.77 

Existent gum, washed ASTM D381 mg/100mls 5.0

Research Octane Number ASTM D2699 Report

Motor Octane Number ASTM D2700 Report

R+M D2699/2700 87.0

Corrosion, Copper ASTM D130 1

Oxidation stability ASTM D525 minutes 240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report

ANALYST Core Dixie Inspectorate JB Inspectorate Core Inspectorate JB 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-13 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 7 Batch No.: WK0521GP13 WK0521GP13 WK0521GP13 WK0521GP13 W

PRODUCT CODE: HF0678‐7 Analysis Date: 12/12/2008 11/18/2008 11/26/2008 11/20/2008 

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX Distillation ‐ IBP ASTM D86 °F 100.0 97.5 105.0 

5% °F 128.0 124.3 132.0 10% °F 132 137 142 137.0 134.9 141.0 20% °F 149.0 147.8 153.0 30% °F 157 162 167 161.0 160.2 165.0 40% °F 177.0 175.6 180.0 50% °F 189 193 197 193.0 192.3 196.0 60% °F 210.0 209.9 214.0 70% °F 224 229 234 229.0 228.6 232.0 80% °F 252.0 250.8 255.0 90% °F 296 301 306 297.0 299.8 302.0 95% °F 329.0 328.7 333.0 Distillation ‐ EP °F 437 359.0 365.5 363.0 Recovery vol % Report 97.9 97.5 97.8 

Residue vol % Report 0.8 1.1 1.1 

Loss vol % Report 1.3 1.4 1.1 

Gravity ASTM D4052 °API Report 64.7 

Specific Gravity ASTM D4052 ‐ Report 0.721 

Reid Vapor Pressure ASTM D5191 psi 6.70 6.85 7.00 7.32 7.09 6.87 

Carbon ASTM D5291 wt fraction Report 85.04 

Hydrogen ASTM D5291 wt fraction Report 14.38 

Oxygen ASTM D5599 wt fraction Report <0.1 

Oxygen, other then ETOH ASTM D5599 wt fraction 0.10 <0.1 

Ethanol content ASTM D5599 wt % 0.05 <0.1 

Water content ASTM E1064 mg/kg Report 50 

Sulfur ASTM D5453 ppm wt 20 30 23 24 

Composition, aromatics ASTM D1319 vol % 14.0 16.5 18.0 16.7 17.6 

Composition, olefins ASTM D1319 vol % 6.3 7.8 9.3 7.3 7.1 

Composition, saturates ASTM D1319 vol % Report 76 75.3 

Benzene ASTM D3606 vol % 0.47 0.77 0.55 0.51 

Existent gum, washed ASTM D381 mg/100mls 5.0 

Research Octane Number ASTM D2699 Report 92.1 Motor Octane Number ASTM D2700 Report 84.7 

(R+M)/2 D2699/2700 87.0 88.4 Corrosion, Copper ASTM D130 1 

Oxidation stability ASTM D525 minutes 240 

Net Heat of Combustion ASTM D4809‐A BTU/lb Report 18813 

ANALYST SWRI Dixie INS JB 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis bas
REPORT 03.14295/03-51563E B-14 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 7 Batch No.: lab blend #11 lab blend #10 lab blend #9 lab blend #8 lab blend #7 lab blend #6 lab blend #5 lab 

PRODUCT CODE: HF0678‐7 Analysis Date: 3/26/2008 3/24/2008 3/20/2008 3/13/2008 3/12/2008 2/28/2008 2/28/2008 2/2

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RE

MIN TARGET MAX submit to SWRI Dist curve fix submit for re‐check Distillation ‐ IBP ASTM D86 °F 101 101 100 102 102 99 99 

5% °F 131 135 129 130 133 130 130 10% °F 132 137 142 143 145 140 141 143 140 140 20% °F 157 158 155 156 156 154 154 30% °F 157 162 167 171 171 169 170 170 167 167 40% °F 183 184 184 186 184 181 181 50% °F 189 193 197 196 197 197 200 196.1 194 194 160% °F 208 209 211 215 207 206 206 70% °F 224 229 234 223 224 228 236 220 219 219 80% °F 251 253 254 267 244 240 240 90% °F 296 301 306 300 305 304 311 314 296 296 95% °F 325 329 329 338 344 330 330 Distillation ‐ EP °F 437 368 370 370 380 384 372 372 Recovery vol % Report 96.7 97.9 96.6 97.2 98.1 97.5 97.5 Residue vol % Report 1.0 1.0 1.0 1.0 1.0 1.0 1.0 Loss vol % Report 2.3 1.1 2.4 1.8 0.9 1.5 1.5 Gravity ASTM D4052 °API Report 60.4 61.4 61.8 61.8 

Specific Gravity ASTM D4052  ‐ Report 0.738 0.733 0.732 0.732 0

Reid Vapor Pressure ASTM D5191 psi 6.70 6.85 7.00 6.50 6.50 6.83 6.80 7.04 

Carbon ASTM D5291 wt fraction Report Hydrogen ASTM D5291 wt fraction Report Oxygen ASTM D5599 wt fraction Report Oxygen, other then ETOH ASTM D5599 wt fraction 0.10 Ethanol content ASTM D5599 wt % 0.05 Water content ASTM E1064 mg/kg Report Sulfur ASTM D5453 ppm wt 20 30 

Composition, aromatics ASTM D1319 vol % 14.0 16.5 18.0 17.6 16.0 15.9 Composition, olefins ASTM D1319 vol % 6.3 7.8 9.3 6.0 7.4 7.1 Composition, saturates ASTM D1319 vol % Report 76.4 76.6 

Benzene ASTM D3606 vol % 0.47 0.77 0.50 

Existent gum, washed ASTM D381 mg/100mls 5.0

Research Octane Number ASTM D2699 Report 92.3 

Motor Octane Number ASTM D2700 Report 84.7 

(R+M)/2 D2699/2700 87.0 88.5 

Corrosion, Copper ASTM D130 1

Oxidation stability ASTM D525 minutes 240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report

ANALYST JB JB JB JB JB Dixie Svcs JB 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-15 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 8 Batch No.: WJ1521GP01 WJ1521GP01 WJ1521GP01 WJ1521GP01 WJ1521GP01 WJ1521GP01 8C 

PRODUCT CODE: HF0678‐8 Analysis Date: 10/24/2008 10/24/2008 10/22/2008 10/21/2008 10/21/2008 10/16/2008 10/6/2

8C 

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESU

MIN TARGET MAX Run 2 Run 1 Optid

Distillation ‐ IBP ASTM D86 °F 88.3 83.0 84.0 90.3 87.

5% °F 105.4 99.0 100.0 104.4 10810% °F 118 123 128 120.7 118.0 118.0 119.8 12320% °F 148.3 149.0 148.0 147.7 15030% °F 175 180 185 178.0 179.0 178.0 177.3 18040% °F 202.3 203.0 203.0 202.1 20450% °F 217 221 225 219.2 221.0 220.0 219.0 22160% °F 232.2 233.0 234.0 232.3 23470% °F 241 246 251 245.1 246.0 245.0 244.2 24680% °F 261.1 264.0 263.0 261.5 26390% °F 296 301 306 300.2 301.0 302.0 300.6 30195% °F 326.7 331.0 330.0 326.7 330Distillation ‐ EP °F 437 357.8 361.0 363.0 360.3 356Recovery vol % Report 96.2 96.1 96.7 96.4 97.

Residue vol % Report 1.0 1.2 1.1 1.0 1.0 Loss vol % Report 2.8 2.1 2.2 2.6 1.4 Gravity ASTM D4052 °API Report 65.1 65.2 65.2 65.

Specific Gravity ASTM D4052  ‐ Report 0.7196 0.7197 0.7193 0.72

Reid Vapor Pressure ASTM D5191 psi 10.00 10.15 10.30 10.28 10.22 10.17 10.1

Carbon ASTM D5291 wt fraction Report 85.2 84.9 Hydrogen ASTM D5291 wt fraction Report 14.8 14.6 Oxygen ASTM D5599 wt fraction Report <0.1 Oxygen, other then ETOH ASTM D5599 wt fraction 0.10 <0.01 Ethanol content ASTM D5599 wt % 0.05 <0.01

Sulfur ASTM D5453 ppm wt 20 25 30 26 19

Composition, aromatics ASTM D1319 vol % 14.4 15.9 17.4 15.9 15.3 15.8 15.

Composition, olefins ASTM D1319 vol % 5.8 7.3 8.8 6.5 5.1 5.5 7.3 

Composition, saturates ASTM D1319 vol % Report 77.6 79.6 78.7 76.

Benzene ASTM D3606 vol % 0.47 0.62 0.77 0.48 0.34 0.33Existent gum, washed ASTM D381 mg/100mls 5.0 <0.5Research Octane Number ASTM D2699 91.0 95.0 95.5Motor Octane Number ASTM D2700 83.0 87.0 87.6R+M D2699/2700 87.0 91.0 91.6Corrosion, Copper ASTM D130 1 1A

Oxidation stability ASTM D525 minutes 240 >240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report 18959.0

ANALYST Dixie Gage HP‐jam Dixie Dixie Gage JB 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-16 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 8 Batch No.: HB#8 HB#7 HB#6 HB#5 HB#4 

PRODUCT CODE: HF0678‐8 Analysis Date: 3/13/2008 3/12/2008 3/11/2008 3/5/2008 3/5/2008 

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX Distillation ‐ IBP ASTM D86 °F 91.8 89.7 89.8 91.8 89.3 

5% °F 106.0 108.6 110.5 111.2 109.2 10% °F 118 123 128 118.3 118.9 119.9 120.3 119.3 20% °F 138.1 136.2 136.5 138.0 137.4 30% °F 175 180 185 162.1 158.1 157.4 159.9 160.8 40% °F 190.3 186.1 184.5 188.7 191.6 50% °F 217 221 225 217.3 214.1 212.4 216.4 219.2 

60% °F 235.5 232.0 230.8 232.4 234.1 70% °F 241 246 251 248.5 243.9 243.9 244.4 245.6 80% °F 265.1 259.8 260.6 260.8 263.5 90% °F 296 301 306 300.3 299.2 302.1 303.1 307.5 95% °F 324.5 325.9 327.3 328.6 330.6 Distillation ‐ EP °F 437 364.3 363.0 365.4 366.1 366.1 Recovery vol % Report 96.3 97.5 97.7 97.9 97.6 

Residue vol % Report 1.0 1.0 1.0 1.0 1.0 Loss vol % Report 2.7 1.5 1.3 1.1 1.4 Gravity ASTM D4052 °API Report 67.4 67.1 67.9 67.6 

Specific Gravity ASTM D4052  ‐ Report 1.0760 0.7114 0.7125 0.7098 0.7107 Reid Vapor Pressure ASTM D5191 psi 10.00 10.15 10.30 10.20 10.50 9.90 10.05 9.86 

Carbon ASTM D5291 wt fraction Report Hydrogen ASTM D5291 wt fraction ReportOxygen ASTM D5599 wt fraction ReportOxygen, other then ETOH ASTM D5599 wt fraction 0.10

Ethanol content ASTM D5599 wt % 0.05

Sulfur ASTM D5453 ppm wt 20 25 30

Composition, aromatics ASTM D1319 vol % 14.4 15.9 17.4 14.5 14.5 13.6 13.7 

Composition, olefins ASTM D1319 vol % 5.8 7.3 8.8 7.3 7.3 6.4 5.5 

Composition, saturates ASTM D1319 vol % Report 78.2 78.2 80.0 80.8 

Benzene ASTM D3606 vol % 0.47 0.62 0.77 0.21Existent gum, washed ASTM D381 mg/100mls 5.0

Research Octane Number ASTM D2699 91.0 95.0 93.5 94.3 94.5 93.8 

Motor Octane Number ASTM D2700 83.0 87.0 86.2 86.9 87.8 87.7 

R+M D2699/2700 87.0 91.0 89.9 90.6 91.2 90.8 

Corrosion, Copper ASTM D130 1

Oxidation stability ASTM D525 minutes 240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report

ANALYST HVD HVD HVD HVD HVD 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s re
REPORT 03.14295/03-51563E B-17 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 9 Batch No.: WK0521GP05 WK0521GP05 9G lab blend 13 lab blend 13 lab blend 12 lab blend 12 lab 

PRODUCT CODE: HF0678‐9 Analysis Date: 11/20/2008 11/18/2008 10/27/2008 8/27/2008 8/27/2008 8/27/2008 8/27/2008 8/2

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RE

MIN TARGET MAX Distillation ‐ IBP ASTM D86 °F 83.9 85.0 83.1 86 90 86.9 90 

5% °F 104.8 103.0 105.3 106.7 113 98.6 113 10% °F 158 114.1 115.0 115.0 117.5 121 114.3 122 20% °F 130.0 131.0 130.8 135.5 137 133.3 138 130% °F 146.8 149.0 148.2 154.4 155 153.3 156 140% °F 167.7 169.0 168.5 175.1 175 174.9 176 150% °F 186 194 192.5 194.0 192.6 194.9 194.7 194.7 194.7 60% °F 225.0 227.0 223.2 214.7 214 214.3 213 270% °F 260.5 261.0 259.2 244.4 243 243 241 280% °F 293.0 290.0 292.7 289.4 289 284.7 285 290% °F 335 345 341.9 344.0 342.8 339.8 338 337.8 334.8 395% °F 362.8 365.0 364.9 364.1 361 362.7 358 3Distillation ‐ EP °F 379.8 387.0 379.2 395.6 383 379.9 383.4 3Recovery vol % Report 97.6 97.8 97.8 99.0 98.7 94.6 99.9 

Residue vol % Report 1.1 0.9 1.1 0.5 1.0 1.1 0.1 

Loss vol % Report 1.3 1.3 1.1 0.5 0.3 4.3 0.0 

Gravity ASTM D4052 °API Report 58.3 58.3 52.45 53.80 Specific Gravity ASTM D4052  ‐ Report 0.746 0.746 0.769 0.764 

Reid Vapor Pressure ASTM D5191 psi 9.85 10.15 10.02 10.32 10.02 9.88 9.94 

Carbon ASTM D5291 wt fraction Report 84 Hydrogen ASTM D5291 wt fraction Report 14 Oxygen ASTM D5599 wt fraction Report <0.1 Oxygen, other then ETOH ASTM D5599 wt fraction 0.10 <0.01 Ethanol content ASTM D5599 wt % 0.05 <0.01

Sulfur ASTM D5453 ppm wt 20 30 20 23

Composition, aromatics ASTM D1319 vol % 38.5 41.5 35.7 35.4 40.37 37.3 

Composition, olefins ASTM D1319 vol % 5.5 8.5 36.4 5.5 7.1 5.88 6.3 

Composition, saturates ASTM D1319 vol % Report 6.0 58.8 57.5 53.8 56.4 

Benzene ASTM D3606 vol % 0.47 0.77 57.6 0.37 0.42

Existent gum, washed ASTM D381 mg/100mls 5.0 <0.5

Research Octane Number ASTM D2699 91.0 95.0 94.6 94.0 96.7 96.7

Motor Octane Number ASTM D2700 83.0 87.0 85.3 84.7 84.3

R+M D2699/2700 87.0 91.0 90.0 89.4 90.5

Corrosion, Copper ASTM D130 1 1A

Oxidation stability ASTM D525 minutes 240 >240Net Heat of Combustion ASTM D4809‐A BTU/lb Report 18424.0

ANALYST Dixie JB Dixie JB JB JB 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-18 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 9 Batch No.: lab blend 9 lab blend 9 lab blend 9 lab blend 8 lab blend 7 lab blend 6 lab blend 5 lab 

PRODUCT CODE: HF0678‐9 Analysis Date: 8/22/2008 8/22/2008 8/22/2008 3/24/2008 3/20/2008 3/18/2008 3/3/2008 2/2

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS R

MIN TARGET MAX Distillation ‐ IBP ASTM D86 °F 86 84.9 87.7 86 90 89 83 

5% °F 99.5 101.7 105.7 107 108 108 105 10% °F 158 109.4 110.1 114 117 118 119 115 20% °F 123.8 124 126.5 133 134 135 132 30% °F 141.8 140.2 142.9 152 153 153 150 40% °F 165.2 164.7 166.9 172 173 173 172 50% °F 186 194 199.4 199.4 203 192 192 193 192 60% °F 243.5 243.9 245.8 211 211 213 212 70% °F 279.5 279 280.1 240 241 241 247 80% °F 304.7 303.4 304 287 287 285 306 90% °F 335 345 323.6 330.6 331.1 336 340 329 339 95% °F 351.5 350.8 350.9 359 363 350 351 Distillation ‐ EP °F 382.1 373.3 375.7 388 391 381 377 Recovery vol % Report 98.0 97.5 98.7 97.4 97.0 97.7 97.4 

Residue vol % Report 0.9 1.0 1.0 1.0 1.0 1.0 1.0 Loss vol % Report 1.1 1.5 0.3 1.6 2.0 1.3 1.6 Gravity ASTM D4052 °API Report 55.37 52.66 52.30 

Specific Gravity ASTM D4052  ‐ Report 0.7572 0.7684 0.769 

Reid Vapor Pressure ASTM D5191 psi 9.85 10.15 10.22 10.25 10.15 

Carbon ASTM D5291 wt fraction Report Hydrogen ASTM D5291 wt fraction Report Oxygen ASTM D5599 wt fraction Report Oxygen, other then ETOH ASTM D5599 wt fraction 0.10 Ethanol content ASTM D5599 wt % 0.05 Sulfur ASTM D5453 ppm wt 20 30 24 

Composition, aromatics ASTM D1319 vol % 38.5 41.5 43.6 40.5 

Composition, olefins ASTM D1319 vol % 5.5 8.5 5.3 5.7 

Composition, saturates ASTM D1319 vol % Report 51.1 Benzene ASTM D3606 vol % 0.47 0.77 0.48 

Existent gum, washed ASTM D381 mg/100mls 5.0Research Octane Number ASTM D2699 91.0 95.0 96.2 

Motor Octane Number ASTM D2700 83.0 87.0 83.7 

R+M D2699/2700 87.0 91.0 90.0 

Corrosion, Copper ASTM D130 1

Oxidation stability ASTM D525 minutes 240Net Heat of Combustion ASTM D4809‐A BTU/lb Report

ANALYST Dixie JB JB JB JB JB JB/Dixie 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-19 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 10 Batch No.: XC2521GP02 XC2521GP02 XC2521GP02 XC2521GP02 XC2521GP02 XC2521GP0

PRODUCT CODE: HF0678‐10 (TR1166) Analysis Date: 4/13/2009 4/11/2009 4/9/2009 4/8/2009 4/7/2009 4/7/2009 

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX 958 797 958 

Distillation ‐ IBP ASTM D86 °F 107.4 104.4 111.4 105.6 105.4 5% °F 129.1 130.5 128.1 129.4 128.7 10% °F 132 137 142 135.9 136.1 134.4 135.7 135.3 20% °F 144.1 144.1 142.9 143.8 143.8 30% °F 146 151 156 151.1 150.8 149.7 150.9 150.6 40% °F 162.5 160.1 156.7 161 160.8 50% °F 217 221 225 217.2 217.9 215.8 215.8 215.7 60% °F 261.3 261.9 260.2 261.5 261.5 70% °F 289 294 299 291.1 292.5 290.7 287.8 290.6 80% °F 317.2 317.7 317.1 315.5 316.7 90% °F 337 342 347 339.2 340.5 340 339.4 340.3 95% °F 355.3 353.8 352 351.9 354.1 Distillation ‐ EP °F 437 375.7 371.3 373.5 371.6 375.6 

Recovery vol % Report 97.9 98.5 97.9 98.7 97.9 

Residue vol % Report 1.0 1.0 0.9 1.0 1.1 

Loss vol % Report 1.1 0.5 1.2 0.3 1 

Gravity ASTM D4052 °API Report 

Specific Gravity ASTM D4052  ‐ Report 0.7655 Reid Vapor Pressure ASTM D5191 psi 6.65 6.80 6.95 7.06 6.87 

Carbon ASTM D5291 wt fraction Report Hydrogen ASTM D5291 wt fraction Report Oxygen ASTM D5599 wt fraction Report Oxygen, other then ETOH ASTM D5599 vol % 0.10

Ethanol content ASTM D5599 vol % 9.50 10.50 9.83

Sulfur ASTM D5453 ppm wt 20 30 25 

Composition, aromatics, corrected ASTM D1319 vol % 33.8 35.3 36.8 34.2

Composition, olefins, corrected ASTM D1319 vol % 4.9 6.4 7.9 6.6

Composition, saturates, corrected ASTM D1319 vol % Report 49.2

Benzene ASTM D3606 vol % 0.47 0.77 0.50

Existent gum, washed ASTM D381 mg/100mls 5.0Research Octane Number ASTM D2699Motor Octane Number ASTM D2700R+M D2699/2700 87.0Corrosion, Copper ASTM D130 1

Oxidation stability ASTM D525 minutes 240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report

Lead ASTM D3237 g/L Report

ANALYST HP Inpectorate Gage Dixie JB JB 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendatio
REPORT 03.14295/03-51563E B-20 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 10 Batch No.: XC2521GP02 XC2521GP02 XC2521GP02 XC2521GP02 XC2521GP02 XC2521GP02 10G 

PRODUCT CODE: HF0678‐10 (TR1166) Analysis Date: 3/31/2009 4/1/2009 3/31/2009 3/30/2009 3/30/2009 3/27/2009 3/13/2

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESUL

MIN TARGET MAX 797 958 

Distillation ‐ IBP ASTM D86 °F 109.2 111.6 111 115.5 

5% °F 133.3 133.5 132.6 133 10% °F 132 137 142 138.6 138.7 138 138 20% °F 146.6 145.8 145.7 145.4 30% °F 146 151 156 152.6 152.5 152.3 151.7 40% °F 168.2 165.6 164.6 157.8 50% °F 217 221 225 227.8 226.3 225.8 227.8 60% °F 270.8 268.1 267.8 267.8 70% °F 289 294 299 296.3 293.3 293.7 294.3 80% °F 321.1 318.7 319 319.1 90% °F 337 342 347 343.5 340.5 341 341.1 95% °F 358.2 353.8 354.2 354.9 Distillation ‐ EP °F 437 369.9 371.8 371.9 372 Recovery vol % Report 97.6 98.3 98 98.1 

Residue vol % Report 1.0 1.0 1.0 0.9 

Loss vol % Report 1.4 0.7 1 1 

Gravity ASTM D4052 °API Report 52.0 46.2 

Specific Gravity ASTM D4052  ‐ Report 0.7701 0.7711 0.7905 

Reid Vapor Pressure ASTM D5191 psi 6.65 6.80 6.95 6.18 6.07 6.15 Carbon ASTM D5291 wt fraction Report 82.6 Hydrogen ASTM D5291 wt fraction Report 14 Oxygen ASTM D5599 wt fraction Report 3.6 Oxygen, other then ETOH ASTM D5599 vol % 0.10 <0.01 Ethanol content ASTM D5599 vol % 9.50 10.50 10.30

Sulfur ASTM D5453 ppm wt 20 30 21 19.66 

Composition, aromatics, corrected ASTM D1319 vol % 33.8 35.3 36.8 36.0 36.0 34.7 

Composition, olefins, corrected ASTM D1319 vol % 4.9 6.4 7.9 5.1 6.9 6 

Composition, saturates, corrected ASTM D1319 vol % Report 48.9 47.1 49.2 

Benzene ASTM D3606 vol % 0.47 0.77 0.29

Existent gum, washed ASTM D381 mg/100mls 5.0 <0.5Research Octane Number ASTM D2699 99.7

Motor Octane Number ASTM D2700 86.7

R+M D2699/2700 87.0 93.2

Corrosion, Copper ASTM D130 1 1A

Oxidation stability ASTM D525 minutes 240 >240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report 17528.0Lead ASTM D3237 g/L Report <0.003

ANALYST Core Dixie Insp JB JB Gage Core 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-21 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 10 Batch No.: 10F 10F 10F 10F 10E 

PRODUCT CODE: HF0678‐10 (TR1166) Analysis Date: 3/2/2009 3/2/2009 2/27/2009 2/27/2009 1/30/2009 

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX 958 Distillation ‐ IBP ASTM D86 °F 105.4 111.8 

5% °F 129.6 131.1 10% °F 132 137 142 136.2 136.7 20% °F 144 144.1 30% °F 146 151 156 150 150.7 40% °F 156.2 161 50% °F 217 221 225 216.5 217.1 60% °F 262.9 263.9 70% °F 289 294 299 293.4 288 80% °F 318.6 318.4 90% °F 337 342 347 341.6 341.1 95% °F 354.7 354.7 Distillation ‐ EP °F 437 370 371.3 Recovery vol % Report 98.6 98 

Residue vol % Report 1.0 1.0 Loss vol % Report 0.4 1 Gravity ASTM D4052 °API Report 52.7 

Specific Gravity ASTM D4052  ‐ Report 0.7682 

Reid Vapor Pressure ASTM D5191 psi 6.65 6.80 6.95 6.48 6.28 

Carbon ASTM D5291 wt fraction Report Hydrogen ASTM D5291 wt fraction ReportOxygen ASTM D5599 wt fraction ReportOxygen, other then ETOH ASTM D5599 vol % 0.10

Ethanol content ASTM D5599 vol % 9.50 10.50

Sulfur ASTM D5453 ppm wt 20 30 23 

Composition, aromatics, corrected ASTM D1319 vol % 33.8 35.3 36.8 33.9 35.7 36 

Composition, olefins, corrected ASTM D1319 vol % 4.9 6.4 7.9 6.4 6.7 5.2 

Composition, saturates, corrected ASTM D1319 vol % Report 49.7 47.6 48.8 Benzene ASTM D3606 vol % 0.47 0.77

Existent gum, washed ASTM D381 mg/100mls 5.0

Research Octane Number ASTM D2699

Motor Octane Number ASTM D2700

R+M D2699/2700 87.0

Corrosion, Copper ASTM D130 1Oxidation stability ASTM D525 minutes 240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report

Lead ASTM D3237 g/L Report

ANALYST Core Dixie Insp JB Core 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s re
REPORT 03.14295/03-51563E B-22 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 10 Batch No.: 10D 10D 10D 10D 

PRODUCT CODE: HF0678‐10 (TR1166) Analysis Date: 12/26/2008 12/23/2008 12/22/2008 12/22/2008 

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX 

Distillation ‐ IBP ASTM D86 °F 108.9 101.8 

5% °F 130.8 134.6 10% °F 132 137 142 136.4 139.4 20% °F 143.9 146.1 30% °F 146 151 156 151.0 152.4 40% °F 158.4 167.2 50% °F 217 221 225 215.1 228.7 

60% °F 260.4 268.4 70% °F 289 294 299 291.0 296.4 80% °F 316.3 320.3 90% °F 337 342 347 339.7 341.7 95% °F 353.1 352.9 Distillation ‐ EP °F 437 370.1 406.5 Recovery vol % Report 98.6 98.0 Residue vol % Report 1.0 1.0 Loss vol % Report 0.4 1.0 Gravity ASTM D4052 °API Report 52.8 

Specific Gravity ASTM D4052  ‐ Report 0.7678 

Reid Vapor Pressure ASTM D5191 psi 6.65 6.80 6.95 6.60 6.54 6.65

Carbon ASTM D5291 wt fraction ReportHydrogen ASTM D5291 wt fraction ReportOxygen ASTM D5599 wt fraction ReportOxygen, other then ETOH ASTM D5599 vol % 0.10

Ethanol content ASTM D5599 vol % 9.50 10.50

Sulfur ASTM D5453 ppm wt 20 30

Composition, aromatics, corrected ASTM D1319 vol % 33.8 35.3 36.8 35.9 

Composition, olefins, corrected ASTM D1319 vol % 4.9 6.4 7.9 3.9 

Composition, saturates, corrected ASTM D1319 vol % Report 50.3 

Benzene ASTM D3606 vol % 0.47 0.77

Existent gum, washed ASTM D381 mg/100mls 5.0

Research Octane Number ASTM D2699

Motor Octane Number ASTM D2700

R+M D2699/2700 87.0

Corrosion, Copper ASTM D130 1

Oxidation stability ASTM D525 minutes 240Net Heat of Combustion ASTM D4809‐A BTU/lb Report

Lead ASTM D3237 g/L Report

ANALYST JB INS Core Dixie I

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis base
REPORT 03.14295/03-51563E B-23 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 10 Batch No.: 10C 10C 10C 10C 10B 10B 

PRODUCT CODE: HF0678‐10 (TR1166) Analysis Date: 12/16/2008 12/9/2008 12/9/2008 12/9/2008 11/26/2008 12/5/2008 

re‐blended TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX Optidist Optidist Optidist Optidist 

Distillation ‐ IBP ASTM D86 °F 104.7 101.9 107.4 107.6 5% °F 127.2 125.5 127.6 132.4 10% °F 132 137 142 133.3 132.5 133.8 137.6 20% °F 141.1 141.3 141.6 145.7 30% °F 146 151 156 149 148.3 149.2 152.5 40% °F 157.2 156 156.2 166.6 50% °F 217 221 225 207.6 205.8 206.9 217.3 60% °F 256.6 254.3 256.1 250.6 70% °F 289 294 299 288.3 287.1 288.1 278.3 80% °F 312.5 313.9 314.5 306.4 90% °F 337 342 347 335.9 337.8 338.6 336.6 95% °F 351.8 351.6 352.3 353.7 Distillation ‐ EP °F 437 369.1 368.8 370.9 378.9 

Recovery vol % Report 98 97.6 97.9 98.5 

Residue vol % Report 1.0 1.0 1.0 1.1 

Loss vol % Report 1 1.4 1.1 0.4 

Gravity ASTM D4052 °API Report 52.6 

Specific Gravity ASTM D4052  ‐ Report 0.7686 

Reid Vapor Pressure ASTM D5191 psi 6.65 6.80 6.95 7.01 7.14 6.83 

Carbon ASTM D5291 wt fraction Report Hydrogen ASTM D5291 wt fraction Report Oxygen ASTM D5599 wt fraction Report Oxygen, other then ETOH ASTM D5599 vol % 0.10

Ethanol content ASTM D5599 vol % 9.50 10.50

Sulfur ASTM D5453 ppm wt 20 30 

Composition, aromatics, corrected ASTM D1319 vol % 33.8 35.3 36.8 35.6 34.6 35.2 

Composition, olefins, corrected ASTM D1319 vol % 4.9 6.4 7.9 5.8 7.2 5.8 Composition, saturates, corrected ASTM D1319 vol % Report 48.7 48.3 49.1 

Benzene ASTM D3606 vol % 0.47 0.77 

Existent gum, washed ASTM D381 mg/100mls 5.0Research Octane Number ASTM D2699Motor Octane Number ASTM D2700R+M D2699/2700 87.0Corrosion, Copper ASTM D130 1

Oxidation stability ASTM D525 minutes 240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report

Lead ASTM D3237 g/L Report

ANALYST JB Core Inspectorate JB Dixie JB 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendatio
REPORT 03.14295/03-51563E B-24 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 11 Batch No.: XA0821GP02 XA0821GP02 XA0821GP02 XA0821GP02 XA0821GP02 XA0821GP02 XA0821GP02 XA0821GP02 XA0821GP02 XA0821GP

PRODUCT CODE: HF0678‐11 Analysis Date: 2/18/2009 2/18/2009 2/17/2009 2/16/2009 2/5/2009 2/5/2009 2/5/2009 1/20/2009 1/20/2009 1/29/200

TEST METHOD UNITS SPECIFICATIONS Results Results Results Results Results Results Results Results Results Results 

MIN TARGET MAX HTC1 HTC2 958 797 S‐958 S‐958 S‐797 recheck 

Distillation ‐ IBP ASTM D86 °F 92.7 91.2 94.2 90.8 87.5 85.6 85.2 92 86.5 

5% °F 113.7 113.2 114.6 115.4 113.9 112.9 112.6 110 116.3 10% °F 119 124 129 123.4 123.4 123.9 124.5 123.4 122.9 122.5 122 125.2 20% °F 137.1 136.8 137.6 138.0 136.8 135.7 136.6 137 138.2 30% °F 143 148 153 147.2 147.4 148.2 148.1 147.5 147.0 147.3 148 148.8 40% °F 155.1 155.3 157.0 156.8 155.8 155.1 156.1 156 156.3 50% °F 186 190 194 188.6 188.4 190.0 189.8 187.3 185.6 187.7 190 195.9 60% °F 230.0 229.5 231.0 230.9 228.8 230.1 228.4 231 233.9 70% °F 245 250 255 250.2 249.3 251.0 251.8 251.5 252.1 251.3 252 253.2 80% °F 269.4 268.9 269.1 270.3 268.9 269.9 269.3 271 273.1 90% °F 294 299 304 298.0 297.5 299.0 298.2 297.8 298.5 295.6 300 303.9 95% °F 323.4 323.1 325.5 324.7 323.4 325.1 323.8 329 337.4 Distillation ‐ EP °F 437 358.0 358.7 358.6 357.8 358.7 359.2 357.8 361 368.5 Recovery vol % Report 97.2 97.3 97.5 98.1 97.6 98.0 97.9 98 97.8 

Residue vol % Report 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 

Loss vol % Report 1.8 1.7 1.5 0.9 1.4 1.0 1.1 1 1.2 

Gravity ASTM D4052 °API Report 54.6 Specific Gravity ASTM D4052  ‐ Report 0.7608 Reid Vapor Pressure ASTM D5191 psi 9.85 10.15 9.92 

Carbon ASTM D5291 wt fraction Report 82.6 Hydrogen ASTM D5291 wt fraction Report 13.6 Oxygen ASTM D5599 wt fraction Report 3.5 Oxygen, other then ETOH ASTM D5599 vol % 0.10 <0.01 Ethanol content ASTM D5599 vol % 9.50 10.50 9.69 Water content ASTM E1064 mg/kg Report 551 Sulfur ASTM D5453 ppm wt 20 30 27 Composition, aromatics, corrected ASTM D1319 vol % 33.5 35.0 36.5 34.4 33.8 

Composition, olefins, corrected ASTM D1319 vol % 5.5 8.5 6.8 7.2 

Composition, saturates, corrected ASTM D1319 vol % Report 48.9 49.1 

Benzene ASTM D3606 vol % 0.47 0.77 0.50

Existent gum, washed ASTM D381 mg/100mls 5.0 0.5

Research Octane Number ASTM D2699 Report 97.4

Motor Octane Number ASTM D2700 Report 85.0

R+M D2699/2700 87.0 91.2

Corrosion, Copper ASTM D130 1 1A

Oxidation stability ASTM D525 minutes 240 >240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report 17614.0

ANALYST Insp Insp JB JB HP HP HP Core Dixie Insp 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-25 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 11 Batch No.: 11G 11G 11G 11G 11F 11F 11F 11E 11E 11D 11D 1

PRODUCT CODE: HF0678‐11 Analysis Date: 12/22/2008 12/22/2008 12/24/2008 12/22/2008 12/9/2008 12/9/2008 12/9/2008 11/26/2008 11/26/2008 11/11/2008 11/11/2008 11/3

TEST METHOD UNITS SPECIFICATIONS Results Results Results Results RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RES

MIN TARGET MAX Optidist Optidist Optidist Optidist Optidist Optidist 1 Distillation ‐ IBP ASTM D86 °F 91.2 92.1 89.3 93 88.6 96.5 

5% °F 113.2 114.9 113.7 113.6 111.1 116.4 10% °F 119 124 129 122.9 124.2 122.8 122.9 121.3 125.2 20% °F 136.7 137.7 137.1 137.3 135.7 138.2 30% °F 143 148 153 147.3 148.4 148.3 148.4 146.7 148.7 40% °F 156.0 156.4 155.9 157.7 155.3 157.2 50% °F 186 190 194 188.7 190.3 193.6 193.9 186.1 178.4 60% °F 229.9 229.6 231.8 232.9 227.4 226 70% °F 245 250 255 250.1 250.3 250.5 251.1 247.9 252 80% °F 269.0 269.8 269.6 269.3 267.7 273.4 90% °F 294 299 304 298.0 300.3 298 299.7 295.5 303.4 95% °F 326.1 327.8 325.9 328.1 322.1 331 Distillation ‐ EP °F 437 360.9 360.6 358.6 362.7 357.7 365.9 

Recovery vol % Report 97.4 97.8 97.3 97.6 97.2 97.9 

Residue vol % Report 1.0 1.0 1.0 1.0 1.0 1.0 

Loss vol % Report 1.6 1.2 1.7 1.4 1.8 1.1 

Gravity ASTM D4052 °API Report 54.4 54.3 54.3 54.5 

Specific Gravity ASTM D4052  ‐ Report 0.7612 0.7618 0.7618 0.7606 

Reid Vapor Pressure ASTM D5191 psi 9.85 10.15 9.65 9.74 10.04 10.12 9.75 9.82 9.97 

Carbon ASTM D5291 wt fraction Report Hydrogen ASTM D5291 wt fraction Report Oxygen ASTM D5599 wt fraction Report Oxygen, other then ETOH ASTM D5599 vol % 0.10 Ethanol content ASTM D5599 vol % 9.50 10.50 

Water content ASTM E1064 mg/kg Report Sulfur ASTM D5453 ppm wt 20 30 21 Composition, aromatics, corrected ASTM D1319 vol % 33.5 35.0 36.5 34.7 35.7 35.1 33.5 35.7 36.3 34.4 35.5 3

Composition, olefins, corrected ASTM D1319 vol % 5.5 8.5 5.5 5.8 6.3 6.9 5.9 6.5 5.5 6.7 

Composition, saturates, corrected ASTM D1319 vol % Report 49.9 48.6 48.7 49.6 48.5 47.3 50.1 47.8 4

Benzene ASTM D3606 vol % 0.47 0.77 0.57 Existent gum, washed ASTM D381 mg/100mls 5.0 Research Octane Number ASTM D2699 Report Motor Octane Number ASTM D2700 Report R+M D2699/2700 87.0

Corrosion, Copper ASTM D130 1

Oxidation stability ASTM D525 minutes 240Net Heat of Combustion ASTM D4809‐A BTU/lb Report

ANALYST Core Dixie Inspectorate JB Core Inspectorate JB Dixie JB/INS JB JB C

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-26 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 12 Batch No.: WL1821GP03 WL1821GP03 WL1821GP03 WL1821GP03 WL1821GP03 WL1821GP03 WL1821GP03 WL1821GP03 12C 12C 12C 12B 

PRODUCT CODE: HF078‐12 Analysis Date: 1/16/2009 1/16/2009 1/12/2009 1/13/2009 1/9/2009 1/9/2009 1/7/2009 1/7/2009 12/9/2008 12/9/2008 12/9/2008 12/3/2008 

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX recheck optidist optidist 

Distillation ‐ IBP ASTM D86 °F 92.1 92.9 95.9 88.2 93.6 

5% °F 110.8 111.9 111.6 104.7 109 10% °F 109 114 119 117.0 117.6 117.7 112.5 115.1 20% °F 123.8 125.5 126.0 122.2 123.8 30% °F 126 131 136 133.2 133.9 133.7 130.5 132.2 40% °F 142.3 143.0 140.7 139.4 141.3 50% °F 147 151 155 151.3 151.5 151.0 149.9 151.9 60% °F 200.1 200.8 200.8 182.3 186.4 70% °F 267 272 277 275.5 276.0 275.9 271.1 272.3 80% °F 307.7 308.0 307.4 305.2 305.7 90% °F 334 339 344 340.1 339.4 339.3 337.8 339.2 95% °F 357.5 357.0 357.1 357 357.3 Distillation ‐ EP °F 437 376.3 373.6 375.6 375.6 376.7 

Recovery vol % Report 97.8 97.4 98.0 97.2 97.6 

Residue vol % Report 1.1 1.1 0.8 1.1 1.1 

Loss vol % Report 1.1 1.5 1.2 1.7 1.3 

Gravity ASTM D4052 °API Report 56.7 56.3 56.4 56.5 

Specific Gravity ASTM D4052  ‐ Report 0.7520 0.7539 0.7529 0.7526 

Reid Vapor Pressure ASTM D5191 psi 9.85 10.00 10.15 10.10 9.99 9.54 9.57/9.56 8.70 10.33 10.31 10.04 

Carbon ASTM D5291 wt fraction Report 82.2 Hydrogen ASTM D5291 wt fraction Report 13.4 Oxygen ASTM D5599 wt fraction Report 3.4 Oxygen, other then ETOH ASTM D5599 wt fraction 0.10 <0.01 Ethanol content ASTM D5599 wt % 9.50 10.50 9.83 Water content ASTM E1064 mg/kg Report 523.00 Sulfur ASTM D5453 ppm wt 20 30 21 16.4 

Composition, aromatics ASTM D1319 vol % 33.5 35.0 36.5 34.6 37.3 36.7 35.3 33.3 36.4 32.8 

Composition, olefins ASTM D1319 vol % 4.7 6.2 7.7 6.4 5.9 5.5 5.7 6.8 5.6 6 

Composition, saturates ASTM D1319 vol % Report 49 46.8 47.8 49.1 49.9 48.1 51.3 

Benzene ASTM D3606 vol % 0.47 0.77 0.52 0.20 

Existent gum, washed ASTM D381 mg/100mls 5.0 <0.5 Research Octane Number ASTM D2699 Report 99.9 Motor Octane Number ASTM D2700 Report 88.5

R+M D2699/2700 87.0 94.2

Corrosion, Copper ASTM D130 1 1A

Oxidation stability ASTM D525 minutes 240 >240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report 17663.0

ANALYST Dixie Gage Core Dixie HP HP Inspectorate Gage Core Inspectorate JB Dixie 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-27 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 13 Batch No.: WJ1521GP02 WJ1521GP02 WJ1521GP02 WJ1521GP02 WJ1521GP02 WJ1521GP02 WJ152

PRODUCT CODE: HF0678‐13 Analysis Date: 11/26/2008 11/20/2008 11/13/2008 10/31/2008 10/30/2008 10/24/2008 10/22/

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESU

MIN TARGET MAX Optidist Optidist 

Distillation ‐ IBP ASTM D86 °F 93.8 93.2 99.0 97.0 99.9 

5% °F 123.8 125.6 123.0 120.0 125.2 10% °F 131 136 141 137.6 137.9 137.0 135.0 136.9 20% °F 157.2 156.8 157.0 156.0 155.1 30% °F 169 174 179 176.6 176.8 177.0 176.0 174.2 40% °F 198.4 198.9 199.0 197.0 196.5 50% °F 215 219 223 221.1 221.0 222.0 219.0 220.6 60% °F 244.0 244.5 245.0 246.0 245.7 70% °F 267 272 277 268.4 269.2 270.0 272.0 271.9 80% °F 301.7 302.5 305.0 307.0 306.1 90% °F 333 338 343 336.7 337.2 337.0 339.0 338.2 95% °F 353.1 353.7 356.0 355.0 353.5 Distillation ‐ EP °F 437 373.6 375.6 385.0 390.0 375.4 

Recovery vol % Report 97.5 97.7 98.5 98.4 97.5 Residue vol % Report 1.1 1.1 0.9 0.8 1.0 Loss vol % Report 1.4 1.2 0.6 0.8 1.5 Gravity ASTM D4052 °API Report 56.0 56.8 56.9 

Specific Gravity ASTM D4052  ‐ Report 0.855 0.752 0.751 Reid Vapor Pressure ASTM D5191 psi 6.71 6.86 7.01 6.64 6.83 7.060 7.060 6.950 Carbon ASTM D5291 wt fraction Report 86.4 Hydrogen ASTM D5291 wt fraction Report 13.6 Oxygen ASTM D5599 wt fraction Report <0.1 

Oxygen, other then ETOH ASTM D5599 wt fraction 0.10 <0.01 

Ethanol content ASTM D5599 wt % 0.05 <0.01 

Sulfur ASTM D5453 ppm wt 20 25 30 26 Lead ASTM D3237 g/l 0.01 <0.001 

Composition, aromatics ASTM D1319 vol % 32.6 34.1 35.6 34.7 33.9 34.1 31.0 33

Composition, olefins ASTM D1319 vol % 4.8 6.3 7.8 6.5 5.2 6.0 7.1 6.

Composition, saturates ASTM D1319 vol % Report 58.8 60.9 59.9 61.9 59

Benzene ASTM D3606 vol % 0.47 0.62 0.77 0.500 

Existent gum, washed ASTM D381 mg/100mls 5.0 1.500 

Research Octane Number ASTM D2699 91.0 95.0 95.800 

Motor Octane Number ASTM D2700 83.0 87.0 86.100 

R+M D2699/2700 87.0 91.0 90.950 Corrosion, Copper ASTM D130 1 1A 

Oxidation stability ASTM D525 minutes 240 >240 

Net Heat of Combustion ASTM D4809‐A BTU/lb Report 18566.0 

ANALYST INS JB Dixie Dixie Dixie Gage HP‐j

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-28 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 13 Batch No.: lab blend #9 lab blend #8 lab blend #7 lab blend #6a lab blend #6 lab blend #5 

PRODUCT CODE: HF0678‐13 Analysis Date: 10/6/2008 10/3/2008 10/2/2008 3/13/2008 3/12/2008 3/4/2008 2/29/2008 2/28/2008 2/26/2008 

13C 13B 13B TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX OptiDist OptiDist Dist. curve fix Distillation ‐ IBP ASTM D86 °F 97 94 106 103 98 98 91 

5% °F 125 121 131 132 132 127 120 10% °F 131 136 141 136 133 145 146 146 140 134 20% °F 155 153 167 166 167 162 159 30% °F 169 174 179 174 174 189 185 187 183 184 40% °F 195 197 210 202 204 202 205 50% °F 215 219 223 219 222 230 218 219 218 222 60% °F 245 244 254 235 237 234 241 70% °F 267 272 277 272 268 285 263 261 260 275 80% °F 305 298 312 325 308 309 324 90% °F 333 338 343 338 333 334 359 338 337 350 95% °F 354 352 349 372.8 352 350 364 Distillation ‐ EP °F 437 373 375 376 385 378 377 389 Recovery vol % Report 97.7 97.2 97.4 97.4 97.8 98.0 97.5 

Residue vol % Report 1.1 1.1 1.0 1.0 1.0 1.0 1.0 Loss vol % Report 1.2 1.2 1.6 1.6 1.2 1.0 1.5 Gravity ASTM D4052 °API Report 56.9 55.6 51.9 53.45 53.3 Specific Gravity ASTM D4052  ‐ Report 0.751 0.757 0.7715 0.7651 0.7659 

Reid Vapor Pressure ASTM D5191 psi 6.71 6.86 7.01 6.86 7.04 6.48 7.36 8.27 

Carbon ASTM D5291 wt fraction Report Hydrogen ASTM D5291 wt fraction Report Oxygen ASTM D5599 wt fraction Report Oxygen, other then ETOH ASTM D5599 wt fraction 0.10 Ethanol content ASTM D5599 wt % 0.05 Sulfur ASTM D5453 ppm wt 20 25 30 21 

Lead ASTM D3237 g/l 0.01 Composition, aromatics ASTM D1319 vol % 32.6 34.1 35.6 34.1 33.7 38.5 42.6 36.1 37.7 36.9 

Composition, olefins ASTM D1319 vol % 4.8 6.3 7.8 6.3 5.4 6.3 7.0 5.0 4.4 4.7 

Composition, saturates ASTM D1319 vol % Report 59.6 60.9 55.2 50.4 58.9 57.9 58.3 

Benzene ASTM D3606 vol % 0.47 0.62 0.77 0.48 

Existent gum, washed ASTM D381 mg/100mls 5.0

Research Octane Number ASTM D2699 91.0 95.0 93.6 

Motor Octane Number ASTM D2700 83.0 87.0 83.5 

R+M D2699/2700 87.0 91.0 88.6 

Corrosion, Copper ASTM D130 1

Oxidation stability ASTM D525 minutes 240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report

ANALYST JB Dixie JB JB JB JB Dixie JB JB 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-29 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 14 Batch No.: WK0521GP07 WK0521GP07 WK0521GP07 WK0521GP07 WK0521GP07 14D 14D(a) 14D 14C 14C 14C L

PRODUCT CODE: HF0678‐14 Analysis Date: 11/19/2008 11/26/2008 11/20/2008 11/19/2008 11/12/2008 10/29/2008 10/24/2008 10/20/2008 10/15/2008 10/15/2008 10/13/2008 

FIA re‐check Octane recheck TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RE

MIN TARGET MAX Distillation ‐ IBP ASTM D86 °F 97.4 105.0 101.0 103.1 102.5 103.1 100.8 100.6 

5% °F 122.7 131.0 123.0 126.3 128.8 123.8 128.5 121.4 10% °F 132 137 142 132.9 139.0 134.0 134.6 137.1 134.6 136.7 133.8 20% °F 145.7 150.0 146.0 146.3 147.8 147.2 148.6 146.7 30% °F 157 162 167 158.5 163.0 159.0 159.3 161.6 158.9 161.1 159.4 40% °F 174.0 178.0 174.0 174.0 176.7 174.2 175.6 173.8 50% °F 188 192 196 191.6 196.2 193.0 191.7 192.1 190.4 191.8 190.1 60% °F 210.9 216.0 212.0 210.9 211.9 208.4 210.2 208.9 70% °F 230 235 240 236.2 241.3 237.0 237.2 235.4 234.5 235.7 234.7 80% °F 279.5 283.0 281.0 279.1 278.0 280.4 278.4 276.9 90% °F 333 338 434 337.1 343.0 338.0 338.2 337.7 338.0 337.9 337.1 95% °F 354.0 359.0 355.0 354.0 354.8 356.0 254.8 354.1 Distillation ‐ EP °F 437 371.7 377.0 388.0 373.1 372.6 377.6 269.8 369.8 Recovery vol % Report 97.2 98.3 98.5 97.7 98.3 98.1 98.1 95.6 Residue vol % Report 1.1 1.1 0.9 1.0 1.1 1.1 1.1 1.1 Loss vol % Report 1.7 0.6 0.6 1.3 0.6 0.8 0.8 3.3 Gravity ASTM D4052 °API Report 64.3 64.3 64.2 64.1 Specific Gravity ASTM D4052  ‐ Report 0.723 0.723 0.723 0.723 

Reid Vapor Pressure ASTM D5191 psi 6.70 6.85 7.00 7.18 6.970 7.250 7.030 6.880 6.810 

Carbon ASTM D5291 wt fraction Report 84.7 Hydrogen ASTM D5291 wt fraction Report 15.3 Oxygen ASTM D5599 wt fraction Report <0.1 Oxygen, other then ETOH ASTM D5599 wt fraction 0.10 <0.01 Ethanol content ASTM D5599 wt % 0.05 <0.01 Water content ASTM E1064 mg/kg Report 50 tbd Sulfur ASTM D5453 ppm wt 20 30 25 21 19 23 22 Lead ASTM D3237 g/l 0.01 <0.001 Composition, aromatics ASTM D1319 vol % 15.0 16.5 18.0 16.5 17 16.9 16.1 16.4 

Composition, olefins ASTM D1319 vol % 6.4 7.9 9.4 8.4 7.6 7.1 8.7 7.4 

Composition, saturates ASTM D1319 vol % Report 75.1 75.4 76.0 75.3 76.2 

Benzene ASTM D3606 vol % 0.47 0.77 0.49 0.42 0.49 0.55 Existent gum, washed ASTM D381 mg/100mls 5.0 <0.5 Research Octane Number ASTM D2699 Report 91.5 91.1 90.0 89.5 

Motor Octane Number ASTM D2700 Report 85.1 84.6 84.0 83.6 R+M D2699/2700 87.0 88.3 87.9 87.0 86.6 

Corrosion, Copper ASTM D130 1 1A

Oxidation stability ASTM D525 minutes 240 >240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report 18388

ANALYST Dixie INS JB Dixie Gage JB Dixie JB Dixie JAM JB 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-30 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 15 Batch No.: WK0521GP06 WK0521GP06 WK0521GP06 WK0521GP06 WK0521GP06 15F 15F 15E 15D 15D 1

PRODUCT CODE: HF067‐15 Analysis Date: Report 12/12 11/14/2008 11/25/2008 11/20/2008 11/14/2008 11/12/2008 10/27/2008 10/20/2008 10/15/2008 10/15/2008 10/13

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RES

MIN TARGET MAX Distillation ‐ IBP ASTM D86 °F 80.0 84.0 82.0 88.6 84.0 91.6 83.9 84.3 88.7 83.2 8

5% °F 106.0 102.0 101.9 108.6 102.0 109.8 106.8 106.5 104.9 106.7 910% °F 112 117 122 116.0 114.0 112.9 118.4 114.0 117.7 116.9 116.6 115.7 116.9 1120% °F 131.0 130.0 128.9 133.3 130.0 131.4 132.5 132.3 131.0 132.1 1230% °F 144 149 154 147.0 146.0 145.4 149.7 146.0 147.4 148.9 148.8 147.2 148.6 1440% °F 166.0 167.0 165.1 169.2 167.0 166.8 168.7 168.3 167.0 167.9 1650% °F 189 191 195 190.0 190.0 188.3 192.6 190.0 189.9 190.9 190.8 189.5 190.2 1860% °F 216.0 217.0 215.1 219.3 217.0 216.3 217.0 216.2 218.3 216.4 2170% °F 238 243 248 244.0 242.0 242.1 246.0 242.0 243.1 242.8 243.1 242.6 244.1 2480% °F 267.0 265.0 264.4 269.7 265.0 265.6 266.0 266.8 286.7 268.7 2690% °F 295 300 305 299.0 300.0 298.1 303.0 300.0 299.1 300.4 301.4 302.0 301.2 3095% °F 328.0 330.0 327.1 333.0 330.0 330.4 329.5 330.4 332.6 328.0 32Distillation ‐ EP °F 437 365.0 366.0 361.4 368.0 366.0 361.6 361.0 361.9 360.5 363.2 35

Recovery vol % Report 97.8 98.0 96.9 97.8 98.0 98.1 98.3 98 98.1 98.1 9Residue vol % Report 0.8 0.9 1.0 1.0 0.9 1.0 1.0 1.0 1.0 1.0 1Loss vol % Report 1.4 1.0 2.1 1.2 1.0 0.9 0.7 1 0.8 0.8 3Gravity ASTM D4052 °API Report 58.8 58.9 58.9 58.9 58.7 59.3 5

Specific Gravity ASTM D4052  ‐ Report 0.7434 0.7437 0.7437 0.7433 0.7440 0.7416 0.7Reid Vapor Pressure ASTM D5191 psi 9.85 10.00 10.15 10.06 10.16 10.02 10.34 10.18 10.00 9.87 9Carbon ASTM D5291 wt fraction Report 86.4 86.5 86.5 Hydrogen ASTM D5291 wt fraction Report 12.59 13.5 13.5 Oxygen ASTM D5599 wt fraction Report <0.1 <0.1 <0.1 Oxygen, other then ETOH ASTM D5599 wt fraction 0.10 <0.01 <0.01 <0.01 Ethanol content ASTM D5599 wt % 0.05 <0.01 <0.01 <0.01 Water content ASTM E1064 mg/kg Report x 71 tbd Sulfur ASTM D5453 ppm wt 20 30 22.9 25 21 18.24 25 23 22 Lead ASTM D3237 g/l 0.01 x <0.001 <0.001 Composition, aromatics ASTM D1319 vol % 34.5 36.0 37.5 36.7 33.4 35.4 33.4 36.2 31.9 33.5 

Composition, olefins ASTM D1319 vol % 5.5 7.0 8.5 7.2 6.3 7 6.3 6.7 7 5.3 Composition, saturates ASTM D1319 vol % Report 60.3 60.3 57.6 60.3 57.1 61.1 61.2 Benzene ASTM D3606 vol % 0.47 0.77 0.49 0.49 0.49 0.6 0.58 0.65Existent gum, washed ASTM D381 mg/100mls 5.0 x 0.5 0.5

Research Octane Number ASTM D2699 Report 94.7 94.9 94.9 94.5 93.6 93.2 

Motor Octane Number ASTM D2700 Report 84.9 85.2 85.2 84.8 84.2 83.9 R+M D2699/2700 87.0 89.8 90.1 90.1 89.7 88.9 88.6 

Corrosion, Copper ASTM D130 1 x 1A 1A

Oxidation stability ASTM D525 minutes 240 x >240 >240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report 18562 18379 18379

ANALYST SwRI Dixie INS JB Dixie Gage JB JB Dixie JAM J

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-31 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 16 Batch No.: XA0821GP03 XA0821GP03 XA0821GP03 XA0821GP03 XA0821GP03 XA0821GP03 XA0821GP03 XA0821GP03 XA0821GP03 

PRODUCT CODE: HF0678‐16 Analysis Date: 2/27/2009 2/19/2009 2/3/2009 1/30/2009 1/23/2009 1/20/2009 1/16/2009 1/16/2009 1/16/2009 

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX etoh adj rvp adj rvp adj optidist optidist 

Distillation ‐ IBP ASTM D86 °F 104.7 107.2 

5% °F 134.8 134.0 10% °F 134 144 140.0 139.5 20% °F 148.5 147.6 30% °F 150 160 153.5 154.8 40% °F 180.0 177.2 50% °F 216 224 220.6 220.6 60% °F 238.6 238.0 70% °F 246 256 253.0 252.1 80% °F 269.8 268.1 90% °F 295 305 302.0 300.0 95% °F 333.3 329.0 Distillation ‐ EP °F 437 364.5 367.8 Recovery vol % Report 98.3 98.5 

Residue vol % Report 1.0 1.0 Loss vol % Report 0.7 0.5 Gravity ASTM D4052 °API Report 53.4 53.2 

Specific Gravity ASTM D4052  ‐ Report 0.7658 0.7659 

Reid Vapor Pressure ASTM D5191 psi 6.70 6.85 7.00 6.9500 6.8000 6.4700 6.2600 6.3400 

Carbon ASTM D5291 wt fraction Report 79.7 Hydrogen ASTM D5291 wt fraction Report 13.1 Oxygen ASTM D5599 wt fraction Report 3.7 3.4 Oxygen, other then ETOH ASTM D5599 vol % 0.10 <0.01 <0.01 Ethanol content ASTM D5599 vol % 9.50 10.50 10.69 10.16 9.98 9.27 9.34 Water content ASTM E1064 mg/kg Report 570.00 Sulfur ASTM D5453 ppm wt 20 30 26 Composition, aromatics, corrected ASTM D1319 vol % 33.5 35.0 36.5 34.6 35.6 36.2 

Composition, olefins, corrected ASTM D1319 vol % 5.5 8.5 6.6 5.9 5.5 

Composition, saturates, corrected ASTM D1319 vol % Report 49.4 48.5 48.3 

Benzene ASTM D3606 vol % 0.47 0.77 0.60 0.33

Existent gum, washed ASTM D381 mg/100mls 5.0 1.0

Research Octane Number ASTM D2699 Report 100.8

Motor Octane Number ASTM D2700 Report 88.1

R+M D2699/2700 87.0 94.4

Corrosion, Copper ASTM D130 1 1AOxidation stability ASTM D525 minutes 240 >240Net Heat of Combustion ASTM D4809‐A BTU/lb Report 17567.0

ANALYST Dixie Dixie Dixie Dixie Gage Dixie Core Insp JB 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-32 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 16 Batch No.: 16F 16F 16F 16E 16E 16E 16D 16D 16C 

PRODUCT CODE: HF0678‐16 Analysis Date: 12/9/2008 12/9/2008 12/9/2008 11/26/2008 11/26/2008 11/26/2008 11/11/2008 11/11/2008 11/3/2008 

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX Optidist Optidist Optidist Optidist Optidist 1 

Distillation ‐ IBP ASTM D86 °F 102.7 110.2 106.7 103.0 110.4 5% °F 131.5 131.8 130.9 131.1 135.1 10% °F 134 144 137.7 137.8 137.5 137.1 140.9 20% °F 146.4 146.6 145.1 145.2 149.3 30% °F 150 160 153.2 154.8 151.9 152.4 157.1 40% °F 171.2 171.8 163.4 160.6 172.4 50% °F 216 224 221.1 221.3 210.5 212.0 222.4 60% °F 238.1 238.8 232.7 233.3 241.8 70% °F 246 256 250.2 252 249.7 249.8 256.9 80% °F 267.8 268 264.9 266.1 273 90% °F 295 305 298.3 299.6 297 296.3 301.6 95% °F 326.3 329.6 324.9 323.6 328.6 Distillation ‐ EP °F 437 365.5 367.7 360.5 359.7 364.3 Recovery vol % Report 97.9 98.3 97.8 98.0 98.6 Residue vol % Report 1.0 1.0 1.0 1.0 1.0 Loss vol % Report 1.1 0.7 1.2 1.0 0.4 Gravity ASTM D4052 °API Report 53.1 53.4 52.5 Specific Gravity ASTM D4052  ‐ Report 0.7666 0.7654 0.7690 

Reid Vapor Pressure ASTM D5191 psi 6.70 6.85 7.00 6.8600 6.9600 6.7100 6.4700 6.7000 

Carbon ASTM D5291 wt fraction Report Hydrogen ASTM D5291 wt fraction Report Oxygen ASTM D5599 wt fraction Report Oxygen, other then ETOH ASTM D5599 vol % 0.10 Ethanol content ASTM D5599 vol % 9.50 10.50 Water content ASTM E1064 mg/kg Report Sulfur ASTM D5453 ppm wt 20 30 21 

Composition, aromatics, corrected ASTM D1319 vol % 33.5 35.0 36.5 34.5 33.5 35.8 34.0 35.6 33.9 35.4 34.8 

Composition, olefins, corrected ASTM D1319 vol % 5.5 8.5 6.1 7.9 6.3 6.7 7.4 6.0 6.3 6.2 

Composition, saturates, corrected ASTM D1319 vol % Report 49.5 48.7 48.0 49.5 47.1 50.0 48.3 49.0 

Benzene ASTM D3606 vol % 0.47 0.77 0.62 

Existent gum, washed ASTM D381 mg/100mls 5.0

Research Octane Number ASTM D2699 Report 

Motor Octane Number ASTM D2700 Report 

R+M D2699/2700 87.0 

Corrosion, Copper ASTM D130 1

Oxidation stability ASTM D525 minutes 240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report

ANALYST Core Inspectorate JB Dixie JB JB/INS Dixie JB Core 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-33 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 20 Batch No.: XA2121GP01 XA2121GP01 XA2121GP01 XA2121GP01 X

PRODUCT CODE: TR1181 Analysis Date: 2/13/2009 2/6/2009 2/8/2009 2/16/2009 

recheck TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX optidist 

Distillation ‐ IBP ASTM D86 °F 106.3 

5% °F 137.7 10% °F 137 142 147 142.7 20% °F 149.7 30% °F 150 155 160 155.3 40% °F 159.4 50% °F 148 162 166 162.7 60% °F 186.3 70% °F 232 237 242 234 80% °F 252 90% °F 296 301 306 300.9 95% °F 339.4 Distillation ‐ EP °F 437 368.1 Recovery vol % Report 98.5 

Residue vol % Report 1.0 

Loss vol % Report 0.5 

Gravity ASTM D4052 °API Report 59.00 Specific Gravity ASTM D4052  ‐ Report 0.7431 

Reid Vapor Pressure ASTM D5191 psi 6.65 6.80 6.95 6.66 

Carbon ASTM D5291 wt fraction Report 70.8Hydrogen ASTM D5291 wt fraction Report 12.7Oxygen ASTM D5599 wt fraction Report 7.1Oxygen, other then ETOH ASTM D5599 wt fraction 0.10 0.03

Ethanol content ASTM D5599 wt % 19.50 20.50 20.33

Sulfur ASTM D5453 ppm wt 20 30 22 

Lead ASTM D3237 g/l 0.01 <0.0003Composition, aromatics ASTM D1319 vol % 14.0 15.5 17.0 15.4 

Composition, olefins ASTM D1319 vol % 5.7 7.2 8.7 6 

Composition, saturates ASTM D1319 vol % Report 58.6 

Benzene ASTM D3606 vol % 0.47 0.77 0.57 0.30

Existent gum, washed ASTM D381 mg/100mls 5.0 <0.5Research Octane Number ASTM D2699 101.6

Motor Octane Number ASTM D2700 95.3R+M D2699/2700 87.0 89.0

Corrosion, Copper ASTM D130 1 1A

Oxidation stability ASTM D525 minutes 240 >240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report 17, 242

ANALYST Dixie Core Dixie Insp 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis base
REPORT 03.14295/03-51563E B-34 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 20 Batch No.: 20C 20C 20C 20C 20B 20B 20B 

PRODUCT CODE: TR1181 Analysis Date: 1/7/2009 1/7/2009 1/7/2009 1/7/2009 12/16/2008 12/16/2008 12/16/2008 12/

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RE

MIN TARGET MAX optidist optidist optidist o

Distillation ‐ IBP ASTM D86 °F 109.4 106.9 106.1 1

5% °F 137.3 135.9 135.5 110% °F 137 142 147 142.1 141.8 140.8 120% °F 149.3 149.2 148.5 130% °F 150 155 160 154.8 155 155.2 140% °F 158.8 159.5 159.6 150% °F 148 162 166 161.7 163.1 162.7 160% °F 173.6 173 169.3 170% °F 232 237 242 236.7 238 236.4 280% °F 256.6 257.1 258.1 290% °F 296 301 306 300.8 301 298.5 395% °F 335.6 337.8 337.1 3Distillation ‐ EP °F 437 369.8 371.7 375.3 

Recovery vol % Report 98.1 98.2 98.2 Residue vol % Report 1.1 1.1 1.0 Loss vol % Report 0.8 0.7 0.8 Gravity ASTM D4052 °API Report 58.5 

Specific Gravity ASTM D4052  ‐ Report 0.7449 0

Reid Vapor Pressure ASTM D5191 psi 6.65 6.80 6.95 6.6200 6.4500 6.8300 6.8500 6.7900 

Carbon ASTM D5291 wt fraction Report Hydrogen ASTM D5291 wt fraction Report Oxygen ASTM D5599 wt fraction Report Oxygen, other then ETOH ASTM D5599 wt fraction 0.10 Ethanol content ASTM D5599 wt % 19.50 20.50 Sulfur ASTM D5453 ppm wt 20 30 Lead ASTM D3237 g/l 0.01

Composition, aromatics ASTM D1319 vol % 14.0 15.5 17.0 15.9 15.1 15 15 14.2 

Composition, olefins ASTM D1319 vol % 5.7 7.2 8.7 6.48 7.9 5.8 6.2 8.2 

Composition, saturates ASTM D1319 vol % Report 57.6 57 59.1 58.7 57.7 

Benzene ASTM D3606 vol % 0.47 0.77

Existent gum, washed ASTM D381 mg/100mls 5.0Research Octane Number ASTM D2699

Motor Octane Number ASTM D2700R+M D2699/2700 87.0

Corrosion, Copper ASTM D130 1

Oxidation stability ASTM D525 minutes 240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report

ANALYST Core Dixie Inpectorate JB Core Dixie Inpectorate 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-35 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 21 Batch No.: XB2321GP02 XB2321GP02 XB2321GP02 XB2321GP02 XB2321GP02 XB2321GP02 XB2321GP02 

PRODUCT CODE: TR1182 Analysis Date: 3/3/2009 2/27/2009 2/25/2009 2/26/2009 2/24/2009 2/24/2009 2/23/2009 1/

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS R

MIN TARGET MAX 797 

Distillation ‐ IBP ASTM D86 °F 108.6 111.8 

5% °F 137.1 135.6 10% °F 136 141 146 142.6 141.8 20% °F 150.9 150.9 30% °F 152 157 162 157.6 157.5 40% °F 162.7 162.7 50% °F 163 167 171 167.7 168.1 60% °F 224.5 217.5 70% °F 250 255 260 256.5 253.4 80% °F 274.6 273.5 90% °F 298 303 308 305.6 303.7 95% °F 334.5 329.2 Distillation ‐ EP °F 437 361.9 359.4 

Recovery vol % Report 98.4 98.4 

Residue vol % Report 1.0 1.0 Loss vol % Report 0.6 0.6 Gravity ASTM D4052 °API Report 50.5 50.5 Specific Gravity ASTM D4052  ‐ Report 0.7780 0.7775 

Reid Vapor Pressure ASTM D5191 psi 6.65 6.80 6.95 6.85 6.80 6.42 6.16 6.37 

Carbon ASTM D5291 wt fraction Report 79.9 Hydrogen ASTM D5291 wt fraction Report 12.9 Oxygen ASTM D5599 wt fraction Report 7 Oxygen, other then ETOH ASTM D5599 wt fraction 0.10 <0.01 Ethanol content ASTM D5599 wt % 19.50 20.0 20.50 20.32 Sulfur ASTM D5453 ppm wt 20 30 27 16.8 Lead ASTM D3237 g/l 0.01 0.009

Composition, aromatics ASTM D1319 vol % 35.0 36.5 38.0 35.0 37.0 

Composition, olefins ASTM D1319 vol % 5.1 6.6 8.1 6.6 7.3 

Composition, saturates ASTM D1319 vol % Report 38.3 35.7 

Benzene ASTM D3606 vol % 0.47 0.77 0.52 0.41

Existent gum, washed ASTM D381 mg/100mls 5.0 0.5

Research Octane Number ASTM D2699 101.6

Motor Octane Number ASTM D2700 86.8

R+M D2699/2700 87.0 94.2

Corrosion, Copper ASTM D130 1 1A

Oxidation stability ASTM D525 minutes 240 >240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report 16845.0

ANALYST Dixie Gage Core Dixie Inspectorate JB Gage 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-36 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 22 Batch No.: WL2621GP02 WL2621GP02 WL2621GP02 WL2621GP02 

PRODUCT CODE: HF0678‐22 Analysis Date: 1/27/2009 1/23/2009 1/15/2009 1/14/2009 

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX rvp adj rvp adj 

Distillation ‐ IBP ASTM D86 °F 

5% °F 

10% °F 122 127 132 20% °F 30% °F 147 152 157 40% °F 50% °F 158 162 166 60% °F 70% °F 227 232 237 

80% °F 

90% °F 293 298 303 95% °F Distillation ‐ EP °F 437 Recovery vol % Report 

Residue vol % Report 

Loss vol % Report 

Gravity ASTM D4052 °API Report 60.1 

Specific Gravity ASTM D4052 ‐ Report 0.7390 

Reid Vapor Pressure ASTM D5191 psi 10.00 10.15 10.30 10.21 9.85 9.74 9.57 

Carbon ASTM D5291 wt fraction Report 77

Hydrogen ASTM D5291 wt fraction Report 15.3

Oxygen ASTM D5599 wt fraction Report 7.1

Oxygen, other then ETOH ASTM D5599 wt fraction 0.10 0.03

Ethanol content ASTM D5599 wt % 19.50 20.50 20.58

Water content ASTM E1064 mg/kg Report 1051

Sulfur ASTM D5453 ppm wt 20 30 21

Lead ASTM D3237 g/l 0.01 0.004

Composition, aromatics ASTM D1319 vol % 13.5 15.0 16.5 14.6 

Composition, olefins ASTM D1319 vol % 5.5 7.0 8.5 6.6 

Composition, saturates ASTM D1319 vol % Report 58.8 

Benzene ASTM D3606 vol % 0.47 0.77 0.56 0.29

Existent gum, washed ASTM D381 mg/100mls 5.0 <0.5

Research Octane Number ASTM D2699 Report 101.8

Motor Octane Number ASTM D2700 Report 89.8

R+M D2699/2700 87.0 95.8

Corrosion, Copper ASTM D130 1 1AOxidation stability ASTM D525 minutes 240 >240Net Heat of Combustion ASTM D4809‐A BTU/lb Report 17118

ANALYST Dixie Gage Dixie Core 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis bas
REPORT 03.14295/03-51563E B-37 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 22 Batch No.: 22B 22B 22B 22B 22A 22A 22A Blend #5 

PRODUCT CODE: HF0678‐22 Analysis Date: 12/16/2008 12/16/2008 12/16/2008 12/16/2008 12/5/2008 12/5/2008 12/5/2008 3/7/2008 

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX optidist optidist optidist optidist Distillation ‐ IBP ASTM D86 °F 90.1 91.1 91 88.5 111 

5% °F 115.2 116.2 109.9 110 130 10% °F 122 127 132 126.2 127.4 116.3 116.1 135 20% °F 141.7 142.7 124.4 124.1 141 30% °F 147 152 157 152 152.6 133.4 133.1 148 40% °F 158.1 158.6 143.2 143.5 155 50% °F 158 162 166 162.1 162.6 152.9 153.3 162 60% °F 165.2 166.4 160.3 160.9 168 70% °F 227 232 237 230.8 232.8 165 166 255 80% °F 251.9 253.9 243.9 245.5 276 90% °F 293 298 303 295.9 299.1 293.8 294.8 300 95% °F 332.3 337 332.4 332.6 314 Distillation ‐ EP °F 437 366.2 371 369.2 365.7 343 

Recovery vol % Report 97.3 97.6 98.1 98.1 98.4 Residue vol % Report 1.1 1.1 1.0 1.0 1.0 Loss vol % Report 1.6 1.3 0.9 0.9 0.6 Gravity ASTM D4052 °API Report 59.4 59.8 49.8 

Specific Gravity ASTM D4052  ‐ Report 0.7411 0.7397 0.7807 

Reid Vapor Pressure ASTM D5191 psi 10.00 10.15 10.30 9.94 9.98 9.85 10.07 10.21 10.03 6.74 

Carbon ASTM D5291 wt fraction Report Hydrogen ASTM D5291 wt fraction Report Oxygen ASTM D5599 wt fraction Report Oxygen, other then ETOH ASTM D5599 wt fraction 0.10 Ethanol content ASTM D5599 wt % 19.50 20.50 Water content ASTM E1064 mg/kg Report Sulfur ASTM D5453 ppm wt 20 30 Lead ASTM D3237 g/l 0.01 Composition, aromatics ASTM D1319 vol % 13.5 15.0 16.5 14 15.4 14.7 15 16.3 16.5 38.8 

Composition, olefins ASTM D1319 vol % 5.5 7.0 8.5 5.9 5.5 7.6 6.4 6.8 8.2 7.5 Composition, saturates ASTM D1319 vol % Report 60.1 59.1 57.9 58.6 56.9 55.3 32.7 Benzene ASTM D3606 vol % 0.47 0.77

Existent gum, washed ASTM D381 mg/100mls 5.0

Research Octane Number ASTM D2699 Report 

Motor Octane Number ASTM D2700 Report 

R+M D2699/2700 87.0

Corrosion, Copper ASTM D130 1

Oxidation stability ASTM D525 minutes 240Net Heat of Combustion ASTM D4809‐A BTU/lb Report

ANALYST Core Dixie Inspectorate JB Core Inspectorate JB JB 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-38 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 23 Batch No.: XA2121GP02 XA2121GP02 XA2121GP02 XA2121GP02 XA2121GP02 XA2121GP02 XA2121GP02 

PRODUCT CODE: TR1184 Analysis Date: 2/23/2009 2/16/2009 2/12/2009 2/12/2009 2/13/2009 2/13/2009 2/10/2009 1/

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RE

MIN TARGET MAX optidist Distillation ‐ IBP ASTM D86 °F 110.8 110.0 109.8 116.8 

5% °F 131.8 132.8 131.7 133.0 10% °F 133 138 143 138.0 138.6 138.0 138.7 20% °F 145.0 145.9 145.4 146.3 30% °F 147 152 157 151.8 151.9 151.8 152.6 40% °F 157.2 157.6 157.6 158.0 50% °F 158 162 166 161.2 162.5 162.4 163.0 60% °F 167.7 172.6 171.0 174.0 70% °F 265 270 275 270.1 269.5 271.8 272.5 80% °F 309.8 311.0 309.8 312.3 90% °F 333 338 343 337.6 338.1 337.6 338.4 95% °F 349.2 348.7 349.6 350.1 Distillation ‐ EP °F 437 366.0 365.2 365.6 368.4 Recovery vol % Report 97.0 98.4 97.6 97.6 

Residue vol % Report 1.0 1.0 1.0 1.0 

Loss vol % Report 2.0 0.6 1.4 1.4 

Gravity ASTM D4052 °API Report 57.5 57.6 

Specific Gravity ASTM D4052  ‐ Report 0.7489 0.7482 

Reid Vapor Pressure ASTM D5191 psi 6.65 6.80 6.95 6.68 6.58 6.60 

Carbon ASTM D5291 wt fraction Report 77.4 Hydrogen ASTM D5291 wt fraction Report 13.9 Oxygen ASTM D5599 wt fraction Report 7 Oxygen, other then ETOH ASTM D5599 wt fraction 0.20 <0.01 Ethanol content ASTM D5599 wt % 19.50 20.50 20.26 Sulfur ASTM D5453 ppm wt 20 30 22 17.3 Lead ASTM D3237 g/l 0.01 <0.003

Composition, aromatics ASTM D1319 vol % 14.0 15.5 17.0 15.5 16.6 Composition, olefins ASTM D1319 vol % 5.8 7.3 8.8 6.8 7.9 Composition, saturates ASTM D1319 vol % Report 57.7 55.5 Benzene ASTM D3606 vol % 0.47 0.77 0.68 0.35Existent gum, washed ASTM D381 mg/100mls 5.0 0.5

Research Octane Number ASTM D2699 Report 97.2

Motor Octane Number ASTM D2700 Report 86.4

R+M D2699/2700 87.0 91.8

Corrosion, Copper ASTM D130 1 1A

Oxidation stability ASTM D525 minutes 240 >240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report 17152

ANALYST Dixie Core Dixie Insp JB JB Gage 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-39 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 24 Batch No.: WL2621GP03 WL2621GP03 WL2621GP03 WL2621GP03 WL2621GP03 WL2621GP03 24

PRODUCT CODE: HF0678‐24 Analysis Date: 1/21/2009 1/19/2009 1/16/2009 1/14/2009 1/14/2009 1/14/2009 12/16/

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESU

MIN TARGET MAX optidist optidist 

Distillation ‐ IBP ASTM D86 °F 89.8 91.2 5% °F 114 112.3 10% °F 119 124 129 125.5 124.1 20% °F 141.7 141.4 30% °F 147 152 157 152.3 152.5 40% °F 159.7 159.3 50% °F 160 164 168 164.4 163.9 60% °F 174.2 169.7 70% °F 262 267 272 265.1 262.8 80% °F 303.6 302.6 90% °F 334 339 344 337.6 336.1 95% °F 349.8 349.1 Distillation ‐ EP °F 437 366 367.7 

Recovery vol % Report 97.2 96.4 

Residue vol % Report 1.1 1.1 Loss vol % Report 1.7 2.5 Gravity ASTM D4052 °API Report 58.90 58.79 

Specific Gravity ASTM D4052  ‐ Report 0.7436 0.7436 

Reid Vapor Pressure ASTM D5191 psi 10.00 10.15 10.30 10.1600 10.1400 9.9200 9.7700 9.6500 10.Carbon ASTM D5291 wt fraction Report 78 Hydrogen ASTM D5291 wt fraction Report 15.2 Oxygen ASTM D5599 wt fraction Report 7.1 Oxygen, other then ETOH ASTM D5599 wt fraction 0.10 0.03 Ethanol content ASTM D5599 wt % 19.50 20.50 20.44

Water content ASTM D1064 mg/kg Report 1031

Sulfur ASTM D5453 ppm wt 20 30 22

Lead ASTM D3237 g/l 0.01 0.005Composition, aromatics ASTM D1319 vol % 13.5 15.0 16.5 14.6 15.9 15 

Composition, olefins ASTM D1319 vol % 5.5 7.0 8.5 7.4 7 6.3 

Composition, saturates ASTM D1319 vol % Report 57.9 57.1 58.

Benzene ASTM D3606 vol % 0.47 0.77 0.56 0.32

Existent gum, washed ASTM D381 mg/100mls 5.0 0.5

Research Octane Number ASTM D2699 Report 100.9

Motor Octane Number ASTM D2700 Report 89.6

R+M D2699/2700 87.0 95.2

Corrosion, Copper ASTM D130 1 1A

Oxidation stability ASTM D525 minutes 240 >240Net Heat of Combustion ASTM D4809‐A BTU/lb Report

ANALYST Dixie Gage Dixie Core JB Insp Cor

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-40 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 24 Batch No.: 24A 24A 24A LB #7 LB #6 LB #5 LB 

PRODUCT CODE: HF0678‐24 Analysis Date: 12/5/2008 12/5/2008 12/5/2008 3/7/2008 3/5/2008 3/3/2

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESU

MIN TARGET MAX optidist optidist Distillation ‐ IBP ASTM D86 °F 90.8 87.3 93 93 91 9

5% °F 114.8 113.3 112 112 109 1110% °F 119 124 129 126.2 125.4 118 118 116 1120% °F 143.1 142.9 127 127 127 1330% °F 147 152 157 154.2 154 137 137 138 1440% °F 160.2 160.6 149 149 150 1550% °F 160 164 168 164.4 164.6 160 160 161 1660% °F 170.5 172.5 167 167 168 1670% °F 262 267 272 255.9 254 223 223 226 2480% °F 288.7 288 278 278 280 2890% °F 334 339 344 331.2 331.5 340 340 342 3495% °F 348.5 348.9 356 356 358 36Distillation ‐ EP °F 437 370.4 368.8 381 381 383 39Recovery vol % Report 97.2 97.3 97.8 97.7 97Residue vol % Report 1.1 1.1 1.0 1.0 1.Loss vol % Report 1.7 1.6 1 1.5 1.Gravity ASTM D4052 °API Report 57.98 51.9 52.0 51

Specific Gravity ASTM D4052  ‐ Report 0.7468 0.7716 0.7724 0.77

Reid Vapor Pressure ASTM D5191 psi 10.00 10.15 10.30 10.01 10.15 10.05 9.76 10.68 10.

Carbon ASTM D5291 wt fraction Report Hydrogen ASTM D5291 wt fraction Report Oxygen ASTM D5599 wt fraction Report Oxygen, other then ETOH ASTM D5599 wt fraction 0.10 Ethanol content ASTM D5599 wt % 19.50 20.50

Water content ASTM D1064 mg/kg Report

Sulfur ASTM D5453 ppm wt 20 30 

Lead ASTM D3237 g/l 0.01Composition, aromatics ASTM D1319 vol % 13.5 15.0 16.5 14.9 14.8 38.4 38.9 37

Composition, olefins ASTM D1319 vol % 5.5 7.0 8.5 6.2 8.1 9.1 7.8 8.

Composition, saturates ASTM D1319 vol % Report 59 57.1 31.5 33.3 32

Benzene ASTM D3606 vol % 0.47 0.77 

Existent gum, washed ASTM D381 mg/100mls 5.0

Research Octane Number ASTM D2699 Report 104

Motor Octane Number ASTM D2700 Report 88R+M D2699/2700 87.0Corrosion, Copper ASTM D130 1

Oxidation stability ASTM D525 minutes 240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report

ANALYST Core Inspectorate JB JB JB JB JB 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-41 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 25 Batch No.: XC1021GP03 XC1021GP03 XC1021GP03 XC1021GP03 XC1021GP03 XC1021GP03 XC1021GP03 XC1021GP03 

PRODUCT CODE: TR1186 Analysis Date: 3/31/2009 3/26/2009 3/27/2009 3/25/2009 3/20/2009 3/20/2009 3/17/2009 3/17/2009 

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX Optidist re check Distillation ‐ IBP ASTM D86 °F 92.7 88.3 

5% °F 117.5 115.2 10% °F 123 128 133 128 126.3 20% °F 143.7 143.1 30% °F 148 153 158 154.3 154 40% °F 161.5 161.1 50% °F 163 167 171 167.3 167.5 60% °F 214 226.8 70% °F 278 283 288 285.8 284.7 80% °F 312.4 314.2 90% °F 335 340 345 340.8 342.1 95% °F 357.5 359.8 Distillation ‐ EP °F 437 372.2 369.7 Recovery vol % Report 98 97.1 Residue vol % Report 1.1 1.1 Loss vol % Report 0.9 1.8 Gravity ASTM D4052 °API Report 

Specific Gravity ASTM D4052  ‐ Report Reid Vapor Pressure ASTM D5191 psi 10.00 10.15 10.30 10.21 

Carbon ASTM D5291 wt fraction Report 79 Hydrogen ASTM D5291 wt fraction Report 13.7 Oxygen ASTM D5599 wt fraction Report 7 Oxygen, other then ETOH ASTM D5599 wt fraction 0.20 <0.01 Ethanol content ASTM D5599 wt % 19.50 20.0 20.50 20.23 Sulfur ASTM D5453 ppm wt 20 25 30 27 22 21.6 21 21 

Lead ASTM D3237 g/l 0.01 0.001 Composition, aromatics ASTM D1319 vol % 34.0 35.5 37.0 35.4 

Composition, olefins ASTM D1319 vol % 5.5 7.0 8.5 5.44 Composition, saturates ASTM D1319 vol % Report 39.1 Benzene ASTM D3606 vol % 0.47 0.62 0.77 0.59 0.19Existent gum, washed ASTM D381 mg/100mls 5.0 <0.5

Research Octane Number ASTM D2699 102.6

Motor Octane Number ASTM D2700 88.2R+M D2699/2700 87.0 95.4Corrosion, Copper ASTM D130 1 1A

Oxidation stability ASTM D525 minutes 240 >240Net Heat of Combustion ASTM D4809‐A BTU/lb Report 16918.0

Water content ASTM E1064 mg/kg Report 1131

ANALYST Dixie Saybolt Paragon Gage Dixie Insp Core Dixie 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-42 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 25 Batch No.: 25C 25C 25C 25C 25B 25B 25B 25B 

PRODUCT CODE: TR1186 Analysis Date: 3/2/2009 3/2/2009 2/27/2009 2/27/2009 1/23/2009 1/23/2009 1/23/2009 1/22/2009 TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX optidist optidist 

Distillation ‐ IBP ASTM D86 °F 90.9 96.6 89.8 89.2 

5% °F 118 116.2 113.4 111.1 10% °F 123 128 133 128.3 126.7 125.6 123.9 20% °F 143.2 142.1 143.2 142.2 30% °F 148 153 158 153.3 152.8 154.2 153.7 40% °F 160.7 160.4 161.2 161.4 50% °F 163 167 171 166.8 166.9 167.4 167.3 60% °F 189.5 182.8 196 193.7 70% °F 278 283 288 284.4 282.5 285.1 284.2 80% °F 313 307.4 310.6 309.3 90% °F 335 340 345 340.9 339.1 338.2 336.1 95% °F 357.8 356.4 353.7 352.9 Distillation ‐ EP °F 437 373.1 374 373.6 371 Recovery vol % Report 98 97.3 97.6 97.1 Residue vol % Report 1.1 1.1 1.0 1.1 Loss vol % Report 0.9 1.6 1.4 1.8 Gravity ASTM D4052 °API Report 51.8 51.4 Specific Gravity ASTM D4052  ‐ Report 0.7722 0.7736 

Reid Vapor Pressure ASTM D5191 psi 10.00 10.15 10.30 9.68 9.36 10.07 9.94 

Carbon ASTM D5291 wt fraction Report Hydrogen ASTM D5291 wt fraction Report Oxygen ASTM D5599 wt fraction Report Oxygen, other then ETOH ASTM D5599 wt fraction 0.20 Ethanol content ASTM D5599 wt % 19.50 20.0 20.50 Sulfur ASTM D5453 ppm wt 20 25 30 22 Lead ASTM D3237 g/l 0.01 Composition, aromatics ASTM D1319 vol % 34.0 35.5 37.0 35.1 36 36 37.7 

Composition, olefins ASTM D1319 vol % 5.5 7.0 8.5 5.7 5.6 6.1 6.2 

Composition, saturates ASTM D1319 vol % Report 39.2 38.4 37.9 36.2 

Benzene ASTM D3606 vol % 0.47 0.62 0.77

Existent gum, washed ASTM D381 mg/100mls 5.0

Research Octane Number ASTM D2699

Motor Octane Number ASTM D2700

R+M D2699/2700 87.0

Corrosion, Copper ASTM D130 1

Oxidation stability ASTM D525 minutes 240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report

Water content ASTM E1064 mg/kg Report

ANALYST Dixie Core Insp JB Dixie Core Insp JB 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-43 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 26 Batch No.: XC1621GP01 XC1621GP01 XC1621GP01 XC1621GP01 XC1621GP01 XC1621GP01 XC1621GP01 XC1621GP01 26B 26B 26B 

PRODUCT CODE: HF0678‐26 Analysis Date: 4/8/2009 3/30/2009 3/20/2009 3/19/2009 3/25/2009 3/23/2009 3/23/2009 3/18/2009 1/23/2009 1/23/2009 1/23/2009 1/2

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RE

MIN TARGET MAX 797 958 optidist op

Distillation ‐ IBP ASTM D86 °F 85.7 91.1 91.8 95.5 90.5 9

5% °F 107.4 109.3 107.4 110.3 109.2 110% °F 112 117 122 115.6 116.7 115.5 117 117.1 120% °F 126.6 127.5 126.5 126.9 127.6 130% °F 133 138 143 137.6 137.9 137.5 137.7 138.2 140% °F 149.2 149.2 149 148.5 149.2 150% °F 156 160 164 159.7 160 160.3 159.3 159.8 160% °F 172.4 175.6 173.7 166.3 172.8 70% °F 272 277 282 275.7 277.6 276.8 275.7 278.1 80% °F 304.5 307.6 305.1 303.6 306.5 390% °F 334 339 344 338.1 338.1 337.9 335.1 339.6 395% °F 354.9 357.1 356.3 355.1 357.3 3Distillation ‐ EP °F 437 373.5 379.6 377.3 379 376.7 3

Recovery vol % Report 98 98.1 96.8 97.4 97.4 9Residue vol % Report 1.1 1.1 1.1 0.9 1.1 

Loss vol % Report 0.9 0.8 2.1 1.7 1.5 

Gravity ASTM D4052 °API Report 54.7 54.8 5

Specific Gravity ASTM D4052  ‐ Report 0.7599 0.7595 0.

Reid Vapor Pressure ASTM D5191 psi 10.00 10.15 10.30 10.1800 10.0400 10.0500 10.0300 9.

Carbon ASTM D5291 wt fraction Report 80.6 Hydrogen ASTM D5291 wt fraction Report 13.8 Oxygen ASTM D5599 wt fraction Report 5.2 Oxygen, other then ETOH ASTM D5599 wt fraction 0.15 <0.01 Ethanol content ASTM D5599 wt % 14.50 15.50 15.05 Sulfur ASTM D5453 ppm wt 20 25 30 24 22 21 Lead ASTM D3237 g/l 0.01 <0.003 Composition, aromatics ASTM D1319 vol % 35.3 36.8 38.3 35.4 37.3 35.9 3

Composition, olefins ASTM D1319 vol % 4.4 5.9 7.4 5.6 5.7 6.4 

Composition, saturates ASTM D1319 vol % Report 43.9 42 42.8 4

Benzene ASTM D3606 vol % 0.47 0.62 0.77 0.56 0.20 Existent gum, washed ASTM D381 mg/100mls 5.0 <0.5 Research Octane Number ASTM D2699 101.6 Motor Octane Number ASTM D2700 88.0 R+M D2699/2700 87.0 94.8

Corrosion, Copper ASTM D130 1 1A

Oxidation stability ASTM D525 minutes 240 >240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report 17249.0

Water Content EN1064 mg/kg 838

ANALYST Saybolt Dixie Core Dixie Insp JB JB Gage Core Dixie Insp 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-44 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 27 Batch No.: XC2521GP03 XC2521GP03 XC2521GP03 XC2521GP03 XC2521GP03 XC2521GP03 XC2521GP03 27C 

PRODUCT CODE: HF0678‐27 (TR1188) Analysis Date: 4/8/2009 4/6/2009 4/2/2009 4/1/2009 3/31/2009 4/1/2009 3/27/2009 3/13/2009 

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX 958 

Distillation ‐ IBP ASTM D86 °F 101.5 104.7 110.5 

5% °F 134.5 132.3 133.5 10% °F 138 143 148 141.7 141.2 140.9 20% °F 151.5 151.4 151.5 30% °F 153 158 163 155 158.2 158.4 40% °F 163 163.3 163.4 50% °F 217 221 225 223.6 218.1 224.1 60% °F 250.5 251.1 250.5 70% °F 274 279 284 276.6 274.2 274.6 80% °F 312.5 309.6 311 90% °F 338 343 348 341.4 339.3 340.3 95% °F 354.4 351 352.2 Distillation ‐ EP °F 436 368 373.7 373.5 Recovery vol % Report 97.7 97.6 97.8 Residue vol % Report 1.0 1.0 1.2 Loss vol % Report 1.3 1.4 1 Gravity ASTM D4052 °API Report 58.6 58.7 

Specific Gravity ASTM D4052  ‐ Report 0.7441 0.7442 0.7440 

Reid Vapor Pressure ASTM D5191 psi 6.65 6.80 6.95 6.91 6.77 6.95 6.84 

Carbon ASTM D5291 wt fraction Report 79.3 Hydrogen ASTM D5291 wt fraction Report 15.9 Oxygen ASTM D5599 wt fraction Report 5.3 Oxygen, other then ETOH ASTM D5599 wt fraction 0.15 <0.01 Ethanol content ASTM D5599 wt % 14.50 15.0 16.50 15.15 Sulfur ASTM D5453 ppm wt 20 25 30 26 25.4 20 25.2 24 Lead ASTM D3237 g/l 0.01 <0.003 Composition, aromatics ASTM D1319 vol % 13.5 15.0 16.5 14.1 14.6 21.25 

Composition, olefins ASTM D1319 vol % 5.1 6.6 8.1 6 7.7 3.06 

Composition, saturates ASTM D1319 vol % Report 64.9 62.7 60.69 

Benzene ASTM D3606 vol % 0.47 0.62 0.77 0.53 0.19Existent gum, washed ASTM D381 mg/100mls 5.0 0.5Research Octane Number ASTM D2699 100.7

Motor Octane Number ASTM D2700 89.1

R+M D2699/2700 87.0 91.0 94.9

Corrosion, Copper ASTM D130 1 1AOxidation stability ASTM D525 minutes 240 >240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report 17554.0Water E1064 mg/kg Report 882

ANALYST Dixie Gage Core Dixie Insp JB Gage Dixie 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-45 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 27 Batch No.: 27B 27B 27B 27B 27B 27B 27B 27B 

PRODUCT CODE: HF0678‐27 (TR1188) Analysis Date: 3/4/2009 3/4/2009 2/27/2009 2/26/2009 1/23/2009 1/23/2009 1/23/2009 1/22/2009 

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX 797 Distillation ‐ IBP ASTM D86 °F 108.4 110 100.9 107.3 105.4 104.8 

5% °F 136.5 137.2 134.4 134 135.7 133.1 10% °F 138 143 148 142.9 143.4 142.2 141.6 142.7 141.6 20% °F 152 152.9 152.1 151.4 152.1 151.7 30% °F 153 158 163 158.8 159.4 158.4 158.4 158.5 158.5 40% °F 164.1 164.2 162.7 162.6 163 163.9 50% °F 217 221 225 226.3 228.5 225 219.5 227.1 220.8 60% °F 254 255.8 250.5 248.5 253 256.4 70% °F 274 279 284 282.4 282.9 280.6 277.3 279.7 281.1 80% °F 319.7 320 316.9 315.2 316.6 316.8 90% °F 338 343 348 344.8 345.4 343.8 342.4 342.9 343.3 95% °F 357.3 357.9 354.9 353.4 353.5 354.3 Distillation ‐ EP °F 436 372.6 373.8 369.5 375.1 372.7 372.2 Recovery vol % Report 97.9 97.8 98.2 97.9 97.6 97.4 Residue vol % Report 1.1 1.1 1.0 1.0 1.0 1.1 Loss vol % Report 1 1.1 0.8 1.1 1.4 1.5 Gravity ASTM D4052 °API Report 58.0 

Specific Gravity ASTM D4052  ‐ Report 0.7467 

Reid Vapor Pressure ASTM D5191 psi 6.65 6.80 6.95 6.75 6.68 

Carbon ASTM D5291 wt fraction Report Hydrogen ASTM D5291 wt fraction Report Oxygen ASTM D5599 wt fraction Report Oxygen, other then ETOH ASTM D5599 wt fraction 0.15 Ethanol content ASTM D5599 wt % 14.50 15.0 16.50 Sulfur ASTM D5453 ppm wt 20 25 30 Lead ASTM D3237 g/l 0.01 Composition, aromatics ASTM D1319 vol % 13.5 15.0 16.5 14.7 16.2 

Composition, olefins ASTM D1319 vol % 5.1 6.6 8.1 6.6 7.2 

Composition, saturates ASTM D1319 vol % Report 63.7 61.6 

Benzene ASTM D3606 vol % 0.47 0.62 0.77

Existent gum, washed ASTM D381 mg/100mls 5.0

Research Octane Number ASTM D2699

Motor Octane Number ASTM D2700

R+M D2699/2700 87.0 91.0

Corrosion, Copper ASTM D130 1

Oxidation stability ASTM D525 minutes 240Net Heat of Combustion ASTM D4809‐A BTU/lb Report

Water E1064 mg/kg Report

ANALYST Saybolt Saybolt Insp JB Dixie Core Insp JB 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-46 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 28 Batch No.: XC2521GP04 XC2521GP04 XC2521GP04 XC2521GP04 XC2521GP04 XC2521GP04 28D 28D 

PRODUCT CODE: HF0678‐28 (TR1189) Analysis Date: 4/8/2009 4/2/2009 4/2/2009 4/1/2009 4/1/2009 3/30/2009 3/2/2009 3/2/2009 

Shipment Date: 

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX 797 

Distillation ‐ IBP ASTM D86 °F 100.6 105.6 112.5 

5% °F 135.4 133.8 133.5 10% °F 141 146 151 143.5 142.9 142.7 20% °F 153.7 153.3 153.5 30% °F 155 160 165 159.2 160 160.2 40% °F 162.6 166.5 166.3 50% °F 215 219 223 216.9 215.9 215.8 60% °F 237.8 240.1 240.4 70% °F 246 254 259 247.3 253.2 251.4 80% °F 267.7 268 266.9 90% °F 296 301 306 298.4 298.6 297.7 95% °F 326 327.5 325.2 Distillation ‐ EP °F 437 362.4 362.8 363.2 

Recovery vol % Report 98.5 97.7 97.8 

Residue vol % Report 1.0 1.0 0.8 

Loss vol % Report 0.5 1.3 1.4 

Gravity ASTM D4052 °API Report 52.12 52.1 52.2 

Specific Gravity ASTM D4052  ‐ Report 0.7706 0.7709 0.7701 

Reid Vapor Pressure ASTM D5191 psi 6.65 6.80 6.95 6.81 6.64 6.77 6.2800 

Carbon ASTM D5291 wt fraction Report 80.3 Hydrogen ASTM D5291 wt fraction Report 14.1 Oxygen ASTM D5599 wt fraction Report 5.2 Oxygen, other then ETOH ASTM D5599 wt fraction 0.15 <0.01 Ethanol content ASTM D5599 wt % 14.50 15.0 15.50 14.96 Sulfur ASTM D5453 ppm wt 20 30 24 21 21 20 Lead ASTM D3237 g/l <0.003 Composition, aromatics ASTM D1319 vol % 33.5 35.0 36.5 33.7 34.6 32.4 33.8 

Composition, olefins ASTM D1319 vol % 5.4 6.9 8.4 5.4 6.9 6.4 6.2 

Composition, saturates ASTM D1319 vol % Report 46 43.5 46.2 45 

Benzene ASTM D3606 vol % 0.47 0.62 0.77 0.54 0.19

Existent gum, washed ASTM D381 mg/100mls 5.0 <0.5

Research Octane Number ASTM D2699 102.8

Motor Octane Number ASTM D2700 88.9

R+M D2699/2700 87.0 95.8

Corrosion, Copper ASTM D130 1 1A

Oxidation stability ASTM D525 minutes 240 >240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report 17274.0Water E1064 mg/kg Report 881

ANALYST Dixie Core Dixie Insp JB Gage Dixie Core 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-47 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 28 Batch No.: 28C 28C 28C 28C 28B 28B 28B 28B 28A 28A 

PRODUCT CODE: HF0678‐28 (TR1189) Analysis Date: 1/30/2009 2/2/2009 1/30/2009 1/29/2009 1/23/2009 1.23/09 1/23/2009 1/22/2009 1/7/2009 1/12/200

Shipment Date: TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX optidist optidist re check Distillation ‐ IBP ASTM D86 °F 103.4 105.4 109.9 108.8 

5% °F 134.3 136.8 136.8 135.9 10% °F 141 146 151 143.8 145.2 142.5 142.3 20% °F 154.4 155.4 151 150.4 30% °F 155 160 165 160.1 162.1 156.7 157.2 40% °F 166.3 169.7 163.2 163 50% °F 215 219 223 224.7 228.1 186.3 185.5 60% °F 245 244.8 235.2 234.5 70% °F 246 254 259 253.6 253.2 250.3 250.1 80% °F 269.4 270.2 265.8 266.6 90% °F 296 301 306 299.4 301.6 298.9 297.7 95% °F 327.7 328.6 327 327.1 Distillation ‐ EP °F 437 361.8 360.9 371.8 370.7 

Recovery vol % Report 97.4 98.2 98.3 98.1 Residue vol % Report 1.0 1.0 1.0 1.0 Loss vol % Report 1.6 0.8 0.7 0.9 Gravity ASTM D4052 °API Report 51.4 52.2 

Specific Gravity ASTM D4052  ‐ Report 0.7737 0.7703 

Reid Vapor Pressure ASTM D5191 psi 6.65 6.80 6.95 6.6300 6.5500 6.3200 6.2500 6.5900 

Carbon ASTM D5291 wt fraction Report Hydrogen ASTM D5291 wt fraction Report Oxygen ASTM D5599 wt fraction Report Oxygen, other then ETOH ASTM D5599 wt fraction 0.15 Ethanol content ASTM D5599 wt % 14.50 15.0 15.50 Sulfur ASTM D5453 ppm wt 20 30 20 Lead ASTM D3237 g/l Composition, aromatics ASTM D1319 vol % 33.5 35.0 36.5 34.2 35.1 34.9 37.4 35.9 

Composition, olefins ASTM D1319 vol % 5.4 6.9 8.4 5.7 6.7 6.2 6 5.2 

Composition, saturates ASTM D1319 vol % Report 45.1 43.2 43.9 41.6 43.9 

Benzene ASTM D3606 vol % 0.47 0.62 0.77 Existent gum, washed ASTM D381 mg/100mls 5.0

Research Octane Number ASTM D2699

Motor Octane Number ASTM D2700

R+M D2699/2700 87.0

Corrosion, Copper ASTM D130 1Oxidation stability ASTM D525 minutes 240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report

Water E1064 mg/kg Report

ANALYST Dixie Core Insp JB Dixie Core Insp JB Dixie Core 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-48 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 30 Batch No.: XA2121GP03 XA2121GP03 XA2121GP03 XA2121GP03 XA2121GP03 XA2121GP03 XA2121GP03 XA2121GP03 XA2121GP03 XA2121GP

PRODUCT CODE: HF0678‐30 Analysis Date: 2/18/2009 2/18/2009 2/23/2009 2/17/2009 2/16/2009 2/10/2009 2/6/2009 2/8/2009 2/8/2009 2/4/2009 

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX HTC1 HTC2 958 958 optidist (797) optidist ( 958 ) Distillation ‐ IBP ASTM D86 °F 89.2 90.3 92.4 89.7 90.6 90.6 92.7 

5% °F 110.3 110.8 109.8 108.5 108.2 107.4 109.4 10% °F 111 116 121 116.4 116.6 116.1 115.1 115.0 114.0 115.5 20% °F 125.4 125.4 124.7 124.2 123.8 123.0 123.6 30% °F 128 133 138 134.2 134.1 133.2 133.3 132.8 131.9 132.4 40% °F 142.9 142.9 142.6 142.7 142.1 141.9 141.8 50% °F 148 152 156 151.3 151.7 152.8 152.9 152.0 152.2 151.2 60% °F 199.9 200.7 196.4 195.4 191.5 190.6 194.5 70% °F 262 267 272 268.3 268.3 267.9 266.8 266.3 266.5 266.9 80% °F 294.3 294.4 294.1 294.3 292.8 292.3 294.8 90% °F 321 326 331 323.8 324.1 323.9 323.3 323.0 323.8 324.1 95% °F 341.2 341.6 341.4 341.2 340.5 341.7 341.8 Distillation ‐ EP °F 437 363.7 363.6 366.4 363.2 366.5 366.0 364.1 Recovery vol % Report 98.2 97.9 98.1 97.7 97.8 97.2 97.7 

Residue vol % Report 1.0 1.0 1.0 1.0 1.0 1.0 1.0 

Loss vol % Report 0.8 1.1 0.9 1.3 1.2 1.8 1.3 

Gravity ASTM D4052 °API Report 56.7 56.9 

Specific Gravity ASTM D4052  ‐ Report 0.7519 0.7510 

Reid Vapor Pressure ASTM D5191 psi 9.90 10.05 10.20 10.27 10.1500 10.15 Carbon ASTM D5291 wt fraction Report 83 Hydrogen ASTM D5291 wt fraction Report 13.6 Oxygen ASTM D5599 wt fraction Report 3.4 Oxygen, other then ETOH ASTM D5599 wt fraction 0.10 <0.01 Ethanol content ASTM D5599 wt % 9.5 10 10.50 9.74 Sulfur ASTM D5453 ppm wt 20 30 24 19 16.53 Composition, aromatics ASTM D1319 vol % 34.3 35.8 37.3 34.1 36.6 35.4 

Composition, olefins ASTM D1319 vol % 4.7 6.2 7.7 5.7 6.1 6.2 Composition, saturates ASTM D1319 vol % Report 50.2 47.3 48.4 Benzene ASTM D3606 vol % 0.47 0.62 0.77 0.53 0.19 Existent gum, washed ASTM D381 mg/100mls 5.0 <0.5 Research Octane Number ASTM D2699 Report 100.5

Motor Octane Number ASTM D2700 Report 94.0

R+M D2699/2700 87.0 87.6Corrosion, Copper ASTM D130 1 1A

Oxidation stability ASTM D525 minutes 240 >240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report 17, 653

ANALYST Insp Insp Dixie JB JB Dixie Core JB JB Gage 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E B-49 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 31 Batch No.: XC0221GP01 XC0221GP01 XC0221GP01 XC0221GP01 XC0221GP01 

PRODUCT CODE: TR1263 Analysis Date: 3/20/2009 3/13/2009 3/11/2009 3/6/2009 3/9/2009 

TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS 

MIN TARGET MAX 

Distillation ‐ IBP ASTM D86 °F 5% °F 10% °F 133 138 143 20% °F 30% °F 149 154 159 40% °F 50% °F 163 167 171 60% °F 70% °F 268 273 278 80% °F 90% °F 322 327 332 95% °F Distillation ‐ EP °F 436 

Recovery vol % Report 

Residue vol % Report Loss vol % Report Gravity ASTM D4052 °API Report Specific Gravity ASTM D4052  ‐ Report Reid Vapor Pressure ASTM D5191 psi 6.65 6.80 6.95 6.85 6.86 6.48 

Carbon ASTM D5291 wt fraction Report 79.5 Hydrogen ASTM D5291 wt fraction Report 13

Oxygen ASTM D5599 wt fraction Report 7

Oxygen, other then ETOH ASTM D5599 wt fraction 0.20 <0.01

Ethanol content ASTM D5599 wt % 19.50 20.0 20.50 20.19

Sulfur ASTM D5453 ppm wt 20 25 30 27 21 

Lead ASTM D3237 g/l <0.003

Composition, aromatics ASTM D1319 vol % 34.3 35.8 37.3 35.4 Composition, olefins ASTM D1319 vol % 4.8 6.3 7.8 5.8 Composition, saturates ASTM D1319 vol % Report 38.8 Benzene ASTM D3606 vol % 0.47 0.62 0.77 0.60 0.30Existent gum, washed ASTM D381 mg/100mls 5.0 0.5

Research Octane Number ASTM D2699 101.9

Motor Octane Number ASTM D2700 88.0

R+M D2699/2700 87.0 95.0

Corrosion, Copper ASTM D130 1 1AOxidation stability ASTM D525 minutes 240 >240Net Heat of Combustion ASTM D4809‐A BTU/lb Report 16855.0

ANALYST Dixie Dixie Gage Core Dixie 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s re
REPORT 03.14295/03-51563E B-50 EPACT FUEL ANALYSIS SUMMARY PRODUCT: EPA Matrix Fuel 31 Batch No.: 31B 31B 31B 31B 31B 31B 31A 

PRODUCT CODE: TR1263 Analysis Date: 2/24/2009 2/23/2009 1/30/2009 2/2/2009 2/1/2009 1/29/2009 1/20/2009 1/

re‐blended re‐blended TEST METHOD UNITS SPECIFICATIONS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RESULTS RE

MIN TARGET MAX 797 optidist optidist recheck Distillation ‐ IBP ASTM D86 °F 107 107.4 111.6 108.6 

5% °F 133.3 128.7 132.3 131.7 10% °F 133 138 143 138.7 137 137.4 137.9 20% °F 147.6 146 144.5 147.0 30% °F 149 154 159 154.8 153.9 151.2 154.7 40% °F 161.1 160.8 160.9 161.5 50% °F 163 167 171 166.5 166.6 215.7 167.3 60% °F 223.9 210.1 253.6 214.5 70% °F 268 273 278 273.3 272.9 280.0 274.0 80% °F 298.6 297.7 308.1 298.9 90% °F 322 327 332 327.4 326.1 337.8 326.9 95% °F 345.7 343.3 353.8 343.2 Distillation ‐ EP °F 436 366.5 365 372.3 365.6 Recovery vol % Report 98.6 96.8 97.3 98.0 Residue vol % Report 1.0 1.0 1.1 1.0 Loss vol % Report 0.4 2.2 1.6 1.0 Gravity ASTM D4052 °API Report 50.7 

Specific Gravity ASTM D4052  ‐ Report 0.7766 

Reid Vapor Pressure ASTM D5191 psi 6.65 6.80 6.95 6.5900 6.5700 6

Carbon ASTM D5291 wt fraction Report Hydrogen ASTM D5291 wt fraction Report Oxygen ASTM D5599 wt fraction Report Oxygen, other then ETOH ASTM D5599 wt fraction 0.20 Ethanol content ASTM D5599 wt % 19.50 20.0 20.50 Sulfur ASTM D5453 ppm wt 20 25 30 22 Lead ASTM D3237 g/l

Composition, aromatics ASTM D1319 vol % 34.3 35.8 37.3 36 35.5 36.7 

Composition, olefins ASTM D1319 vol % 4.8 6.3 7.8 6.2 6.4 5.4 

Composition, saturates ASTM D1319 vol % Report 37.8 38.1 37.8 

Benzene ASTM D3606 vol % 0.47 0.62 0.77Existent gum, washed ASTM D381 mg/100mls 5.0

Research Octane Number ASTM D2699

Motor Octane Number ASTM D2700

R+M D2699/2700 87.0

Corrosion, Copper ASTM D130 1

Oxidation stability ASTM D525 minutes 240

Net Heat of Combustion ASTM D4809‐A BTU/lb Report

ANALYST Insp JB Dixie Core Insp JB Core 

NOTE: Highlighted cells are near or out of specification. In some cases, the fuel was approved with select properties out of specification. These approvals were made on a case‐by‐case basis based on EPA’s recommendation.
REPORT 03.14295/03-51563E

APPENDIX C 

DETAILED HYDROCARBON ANALYSIS RESULTS 
Hydrocarbon Expert V4.7 Wed Aug 25 16:51:12 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91308 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91308

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 10.907 12.118 11.272

I-Paraffins 41.057 44.544 38.393

Aromatics 21.495 17.700 16.790

Mono-Aromatics 20.516 16.957 16.130

Naphthalenes 0.077 0.054 0.049

Naphtheno/Olefino-Benzs 0.159 0.128 0.100

Indenes 0.743 0.561 0.511

Naphthenes 7.436 7.020 7.009

Mono-Naphthenes 7.436 7.020 7.009

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 7.679 8.170 8.360

n-Olefins 3.263 3.548 3.648

Iso-Olefins 3.747 4.001 3.984

Naphtheno-Olefins 0.642 0.592 0.696

Di-Olefins 0.027 0.028 0.033

Oxygenates 9.308 8.480 16.828

Unidentified 2.117 1.968 1.348

Plus 0.000 0.000 0.000

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Hydrocarbon Expert V4.7 Wed Aug 25 16:51:12 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91308 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91308

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C2 9.196 8.379 16.672

C3 0.115 0.105 0.162

C4 0.548 0.669 0.797

C5 25.438 29.118 29.598

C6 18.536 19.229 18.217

C7 12.806 11.855 11.170

C8 17.326 16.410 12.988

C9 8.500 7.611 5.765

C10 4.219 3.565 2.632

C11 1.086 0.999 0.592

C12 0.113 0.093 0.058

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Hydrocarbon Expert V4.7 Wed Aug 25 16:51:12 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91308 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91308

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C3 0.003 0.005 0.006

C4 0.308 0.383 0.443

C5 4.874 5.596 5.643

C6 3.981 4.340 3.858

C7 0.905 0.952 0.755

C8 0.425 0.435 0.311

C9 0.294 0.295 0.192

C10 0.064 0.063 0.038

C11 0.051 0.049 0.027

I-Paraffins C4 0.040 0.052 0.058

C5 16.263 18.873 18.826

C6 6.876 7.516 6.664

C7 2.656 2.806 2.214

C8 10.720 10.794 7.838

C9 2.975 3.012 1.937

C10 0.834 0.823 0.486

C11 0.680 0.657 0.363

C12 0.013 0.012 0.006

Mono-Aromatics C6 0.831 0.680 0.889

C7 6.056 5.021 5.489

C8 5.652 4.689 4.447

C9 5.090 4.198 3.537

C10 2.486 2.043 1.547

C11 0.300 0.244 0.169

C12 0.101 0.081 0.052

Naphthalenes C10 0.061 0.043 0.040

C11 0.016 0.011 0.009

Naphtheno/Olefino-Benzs C10 0.159 0.128 0.100

Indenes C9 0.124 0.092 0.088

C10 0.614 0.464 0.421

C11 0.005 0.004 0.003

Mono-Naphthenes C5 0.449 0.433 0.535

C6 4.135 3.906 4.104

C7 2.343 2.208 1.993

C8 0.493 0.458 0.367

C9 0.017 0.014 0.011

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Hydrocarbon Expert V4.7 Wed Aug 25 16:51:12 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91308 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91308

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Mono-Naphthenes

n-Olefins C4 0.199 0.235 0.297

C5 1.709 1.894 2.036

C6 1.211 1.274 1.202

C7 0.110 0.112 0.093

C11 0.034 0.033 0.020

Iso-Olefins C5 1.909 2.101 2.273

C6 1.065 1.113 1.057

C7 0.737 0.754 0.627

C8 0.036 0.033 0.026

Naphtheno-Olefins C5 0.206 0.192 0.253

C6 0.436 0.400 0.443

Di-Olefins C5 0.027 0.028 0.033

Oxygenates C2 9.196 8.379 16.672

C3 0.112 0.101 0.156

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File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91308 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91308

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 35.78 31.61

5% 79.59 79.45

10% 80.59 80.31

15% 81.59 81.17

20% 94.75 82.03

25% 100.83 95.95

30% 139.74 120.87

35% 154.13 140.43

40% 157.48 154.33

45% 172.52 157.78

50% 173.11 172.58

55% 187.75 173.22

60% 210.19 193.48

65% 230.81 212.27

70% 233.98 230.91

75% 237.97 236.08

80% 255.30 243.75

85% 281.77 277.11

90% 322.42 318.26

95% 352.22 347.32

FBP 388.19 387.31

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Hydrocarbon Expert V4.7 Wed Aug 25 16:51:12 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91308 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91308

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 7.390 74-98-6 P3 Propane 0.003 0.005 0.006 0.788

2 8.612 75-28-5 I4 i-Butane 0.040 0.052 0.058 9.925

3 9.404 115-11-7 K4 Isobutene 0.016 0.019 0.024 4.054

4 9.444 106-98-9 K4 Butene-1 0.019 0.023 0.029 4.953

5 9.793 106-97-8 P4 n-Butane 0.308 0.383 0.443 76.175

6 10.267 624-64-6 K4 t-Butene-2 0.075 0.089 0.112 19.229

7 10.389 463-82-1 I5 2,2-Dimethylpropane 0.057 0.069 0.065 14.063

8 10.987 590-18-1 K4 c-Butene-2 0.089 0.103 0.132 22.743

9 12.745 64-17-5 X2 Ethanol 9.196 8.379 16.672 1011.630

10 13.128 563-45-1 C5 3-Methylbutene-1 0.300 0.344 0.357 76.734

11 14.727 78-78-4 I5 i-Pentane 16.207 18.804 18.761 4032.715

12 16.338 109-67-1 K5 Pentene-1 0.346 0.388 0.412 88.469

13 17.172 563-46-2 C5 2-Methylbutene-1 0.525 0.581 0.626 134.460

14 17.700 109-66-0 P5 n-Pentane 4.874 5.596 5.643 1212.875

15 18.209 78-79-5 E5 2-Methyl-1,3-Butadiene 0.011 0.011 0.013 2.829

16 18.797 646-04-8 K5 t-Pentene-2 0.881 0.977 1.049 225.410

17 19.821 627-20-3 K5 c-Pentene-2 0.483 0.530 0.575 123.614

18 20.491 513-35-9 C5 2-Methylbutene-2 1.084 1.177 1.291 277.414

19 20.823 2004-70-8 E5 1t,3-Pentadiene 0.016 0.017 0.020 4.233

20 22.064 ? Unidentified 0.006 0.006 0.008 1.883

21 22.608 75-83-2 I6 2,2-Dimethylbutane 0.310 0.343 0.300 77.375

22 25.250 142-29-0 B5 Cyclopentene 0.206 0.192 0.253 54.331

23 26.426 ? Unidentified 0.044 0.039 0.061 13.657

24 26.498 71-23-8 X3 n-Propanol 0.112 0.101 0.156 20.102

25 27.092 287-92-3 M5 Cyclopentane 0.449 0.433 0.535 114.905

26 27.833 79-29-8 I6 2,3-Dimethylbutane 0.785 0.853 0.761 196.149

27 28.233 ? Unidentified 0.054 0.052 0.051 16.789

28 28.695 691-38-3 C6 4-Methyl-c-pentene-2 0.047 0.050 0.047 12.061

29 28.918 107-83-5 I6 2-Methylpentane 3.405 3.748 3.300 850.670

30 29.349 674-76-0 C6 4-Methyl-t-pentene-2 0.138 0.148 0.137 35.376

31 31.558 96-14-0 I6 3-Methylpentane 2.376 2.571 2.303 593.542

32 32.722 763-29-1 C6 2-Methylpentene-1 0.237 0.249 0.235 60.619

33 32.943 592-41-6 K6 Hexene-1 0.170 0.180 0.168 43.445

34 35.305 110-54-3 P6 n-Hexane 3.981 4.340 3.858 994.579

35 35.93613269-52-8 K6 t-Hexene-3 0.279 0.294 0.277 71.401

36 36.414 4050-45-7 K6 t-Hexene-2 0.535 0.563 0.531 136.913

37 36.906 625-27-4 C6 2-Methylpentene-2 0.363 0.377 0.360 92.848

38 37.321 922-62-3 C6 3-Methyl-c-pentene-2 0.281 0.289 0.278 71.798

39 38.254 7688-21-3 K6 c-Hexene-2 0.228 0.237 0.226 58.285

40 39.590 3404-73-7 C7 3,3-Dimethylpentene-1 0.332 0.340 0.283 85.027

41 40.168 96-37-7 M6 Methylcyclopentane 2.373 2.279 2.355 607.301

42 41.741 108-08-7 I7 2,4-Dimethylpentane 0.424 0.453 0.353 106.370

43 42.039 594-56-9 C7 2,3,3-Trimethylbutene-1 0.015 0.015 0.013 3.775

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C-6
Hydrocarbon Expert V4.7 Wed Aug 25 16:51:12 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91308 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91308

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 42.277 464-06-2 I7 2,2,3-Trimethylbutane 0.053 0.055 0.044 13.318

45 44.938 ? Unidentified 0.012 0.012 0.013 3.894

46 45.140 71-42-3 Q6 Benzene 0.831 0.680 0.889 229.079

47 45.347 693-89-0 B6 1-Methylcyclopentene 0.388 0.358 0.395 101.725

48 46.162 3404-61-3 C7 3-Methylhexene-1 0.017 0.017 0.014 4.257

49 46.749 3524-73-0 C7 5-Methylhexene-1 0.084 0.087 0.071 21.467

50 47.063 110-82-7 M6 Cyclohexane 1.762 1.628 1.749 451.067

51 47.602 ? Unidentified 0.036 0.037 0.031 11.379

52 48.80615840-60-5 C7 2-Methyl-c-hexene-3 0.043 0.045 0.037 11.006

53 49.152 3769-23-1 C7 4-Methylhexene-1 0.011 0.011 0.009 2.847

54 49.805 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.054 0.055 0.046 13.838

55 50.197 591-76-4 I7 2-Methylhexane 1.372 1.453 1.143 344.059

56 50.675 110-83-8 B6 Cyclohexene 0.047 0.042 0.048 12.145

57 52.034 589-34-4 I7 3-Methylhexane 0.807 0.844 0.673 202.424

58 52.885 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.242 0.232 0.206 61.894

59 53.471 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.195 0.188 0.166 49.809

60 54.098 822-50-4 M7 1t,2-Dimethylcyclopentane 0.293 0.280 0.249 74.973

61 54.402 C7 C7 - Iso-Olefin - 2 0.024 0.024 0.020 6.018

62 54.689 540-84-1 I8 2,2,4-Trimethylpentane 1.160 1.205 0.848 291.532

63 55.027 592-76-7 K7 Heptene-1 0.031 0.032 0.027 8.050

64 56.365 4914-89-0 C7 3-Methyl-c-hexene-3 0.015 0.015 0.013 3.865

65 56.88314686-14-7 K7 t-Heptene-3 0.035 0.036 0.030 8.889

66 57.246 6094-02-6 C7 2-Methylhexene-1 0.062 0.064 0.053 15.916

67 57.624 142-82-5 P7 n-Heptane 0.905 0.952 0.755 227.081

68 57.839 7642-10-6 K7 c-Heptene-3 0.026 0.027 0.022 6.690

69 58.118 2738-19-4 C7 2-Methyl-2-hexene 0.028 0.029 0.024 7.239

70 58.363 3899-36-3 C7 3-Methyl-t-hexene-3 0.022 0.022 0.018 5.522

71 58.74814686-13-6 K7 t-Heptene-2 0.017 0.018 0.015 4.402

72 59.20516491-15-9 M7 Cyclopentene, 1,5-dimethyl- 0.020 0.019 0.017 5.062

73 59.64920710-38-8 C7 3-Methyl-t-hexene-2 0.016 0.016 0.014 4.157

74 60.434 4914-91-4 C7 2-Pentene, 3,4-dimethyl-, (Z)- 0.014 0.014 0.012 3.666

75 61.070 108-87-2 M7 Methylcyclohexane 1.542 1.440 1.311 394.560

76 62.018 4516-69-2 M8 1,1,3-Trimethylcyclopentane 0.038 0.036 0.028 9.687

77 62.423 590-73-8 I8 2,2-Dimethylhexane 0.030 0.031 0.022 7.476

78 63.860 1640-89-7 M7 Ethylcyclopentane 0.052 0.049 0.044 13.312

79 64.512 564-02-3 I8 2,2,3-Trimethylpentane 0.303 0.304 0.221 76.117

80 64.754 592-13-2 I8 2,5-Dimethylhexane 0.645 0.669 0.472 162.099

81 65.092 589-43-5 I8 2,4-Dimethylhexane 0.581 0.597 0.425 146.037

82 65.930 4850-28-6 M8 1c,2t,4-Trimethylcyclopentane 0.035 0.033 0.026 8.961

83 66.333 563-16-6 I8 3,3-Dimethylhexane 0.021 0.022 0.016 5.354

84 67.46015890-40-1 M8 1t,2c,3-Trimethylcyclopentane 0.030 0.028 0.022 7.567

85 68.098 565-75-3 I8 2,3,4-Trimethylpentane 2.844 2.844 2.080 714.827

86 68.631 108-88-3 Q7 Toluene 6.056 5.021 5.489 1650.972

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C-7
Hydrocarbon Expert V4.7 Wed Aug 25 16:51:12 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91308 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91308

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 68.778 560-21-4 I8 2,3,3-Trimethylpentane 3.583 3.547 2.619 900.391

88 70.131 C8 C8 - Diolefin - 1 0.012 0.011 0.009 3.017

89 70.432 584-94-1 I8 2,3-Dimethylhexane 0.829 0.837 0.606 208.377

90 71.702 592-27-8 I8 2-Methylheptane 0.242 0.249 0.177 60.786

91 71.961 589-53-7 I8 4-Methylheptane 0.168 0.171 0.123 42.188

92 72.096 ? Unidentified 0.073 0.073 0.054 23.034

93 72.865 M8 1,3-dimethyl-t-cyclohexane 0.173 0.162 0.129 44.347

94 73.024 589-81-1 I8 3-Methylheptane 0.206 0.210 0.150 51.711

95 73.209 619-99-8 I8 3-Ethylhexane 0.109 0.109 0.079 27.295

96 74.105 ? Unidentified 0.027 0.025 0.020 8.494

97 74.936 3522-94-9 I9 2,2,5-Trimethylhexane 2.094 2.129 1.364 527.376

98 75.273 M8 3c-Ethylmethylcyclopentane 0.009 0.009 0.007 2.399

99 75.493 M8 3t-Ethylmethylcyclopentane 0.013 0.012 0.010 3.375

100 75.910 ? Unidentified 0.014 0.014 0.009 4.366

101 76.196 2207-03-6 M8 1t,3-Dimethylcyclohexane 0.074 0.069 0.055 19.011

102 77.567 111-65-9 P8 n-Octane 0.425 0.435 0.311 106.791

103 78.511 ? Unidentified 0.051 0.050 0.034 16.140

104 80.059 1069-53-0 I9 2,3,5-Trimethylhexane 0.346 0.344 0.225 87.074

105 80.619 C8 C9 - IsoOlefin - 1 0.013 0.012 0.010 3.335

106 81.057 2207-01-4 M8 1c,2-Dimethylcyclohexane 0.013 0.012 0.009 3.262

107 81.235 1071-26-7 I9 2,4-Dimethylheptane 0.062 0.063 0.040 15.565

108 81.870 1678-91-7 M8 Ethylcyclohexane 0.107 0.098 0.080 27.459

109 82.197 1072-05-5 I9 2,6-Dimethylheptane 0.096 0.097 0.062 24.096

110 82.676 ? Unidentified 0.020 0.021 0.013 6.335

111 83.130 I9 2,5-Dimethylheptane 0.201 0.202 0.131 50.507

112 83.304 926-82-9 I9 3,5-Dimethylheptane 0.021 0.021 0.014 5.324

113 84.441 100-41-4 Q8 Ethylbenzene 1.020 0.846 0.802 275.975

114 84.621 ? Unidentified 0.026 0.025 0.017 8.075

115 84.862 ? Unidentified 0.031 0.029 0.021 9.743

116 85.671 108-38-3 Q8 m-Xylene 2.565 2.134 2.018 694.152

117 85.820 106-42-3 Q8 p-Xylene 1.157 0.966 0.911 313.155

118 85.966 ? Unidentified 0.060 0.060 0.039 18.870

119 86.221 C8 C9-IsoOlefin-3 0.011 0.010 0.007 2.846

120 86.329 ? Unidentified 0.011 0.011 0.007 3.430

121 87.017 2216-34-4 I9 4-Methyloctane 0.040 0.040 0.026 10.037

122 87.149 3221-61-2 I9 2-Methyloctane 0.055 0.055 0.036 13.832

123 88.015 2216-33-3 I9 3-Methyloctane 0.061 0.061 0.040 15.443

124 88.481 ? Unidentified 0.118 0.125 0.078 37.130

125 88.653 95-47-6 Q8 o-Xylene 0.910 0.743 0.716 246.110

126 89.070 I10 C10 - IsoParaffin - 1 0.400 0.395 0.235 100.835

127 89.643 M9 trans-1,3-Diethylcyclopentane 0.017 0.014 0.011 4.560

128 89.91614720-74-2 I10 2,2,4-trimethylheptane 0.280 0.277 0.164 70.641

129 91.485 111-84-2 P9 n-Nonane 0.294 0.295 0.192 74.085

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C-8
Hydrocarbon Expert V4.7 Wed Aug 25 16:51:12 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91308 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91308

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 92.840 98-82-8 Q9 i-Propylbenzene 0.035 0.029 0.025 9.479

131 93.600 ? Unidentified 0.044 0.043 0.026 13.696

132 93.82415869-87-1 I10 2,2-Dimethyloctane 0.017 0.017 0.010 4.327

133 94.63015869-89-3 I10 2,5-Dimethyloctane 0.010 0.010 0.006 2.510

134 94.816 I10 C10 - IsoParaffin - 2 0.010 0.010 0.006 2.647

135 95.266 2051-30-1 I10 2,4-Dimethyloctane 0.012 0.012 0.007 2.976

136 95.661 I10 2,6-Dimethyloctane 0.010 0.009 0.006 2.418

137 96.307 103-65-1 Q9 n-Propylbenzene 0.255 0.213 0.177 68.654

138 97.155 620-14-4 Q9 1-Methyl-3-ethylbenzene 0.997 0.829 0.693 268.029

139 97.389 622-96-8 Q9 1-Methyl-4-ethylbenzene 0.475 0.396 0.330 127.589

140 98.015 108-67-8 Q9 1,3,5-Trimethylbenzene 0.634 0.527 0.441 170.506

141 98.68417301-94-8 I10 4-Methylnonane 0.012 0.011 0.007 2.938

142 98.885 ? Unidentified 0.235 0.233 0.138 73.669

143 99.100 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.388 0.317 0.270 104.326

144 99.663 5911-04-6 I10 3-Methylnonane 0.017 0.016 0.010 4.176

145 100.129 ? Unidentified 0.020 0.014 0.011 6.177

146 100.254 ? Unidentified 0.059 0.057 0.031 18.380

147 100.478 I11 C11-Isoparaffin-2 0.030 0.029 0.016 7.687

148 100.737 95-63-6 Q9 1,2,4-Trimethylbenzene 1.953 1.603 1.357 525.082

149 100.942 ? Unidentified 0.041 0.042 0.025 12.941

150 101.065 ? Unidentified 0.022 0.022 0.013 7.033

151 102.10917302-01-1 I10 3-Ethyl-3-methylheptane 0.068 0.065 0.036 17.109

152 102.390 538-93-2 Q10 i-Butylbenzene 0.094 0.079 0.058 25.039

153 102.657 124-18-5 P10 n-Decane 0.064 0.063 0.038 16.253

154 102.976 ? Unidentified 0.018 0.017 0.010 5.618

155 103.612 526-73-8 Q9 1,2,3-Trimethylbenzene 0.352 0.283 0.245 94.713

156 104.005 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.014 0.012 0.009 3.714

157 104.194 I11 C11 Isoparaffin-4 0.011 0.010 0.006 2.690

158 104.395 ? Unidentified 0.066 0.055 0.041 20.702

159 104.803 J9 Indan 0.124 0.092 0.088 33.876

160 105.431 J10 Indene 0.435 0.325 0.308 118.912

161 106.148 I11 C11-Isoparaffin-7 0.194 0.187 0.104 48.994

162 106.334 141-93-5 Q10 1,3-Diethylbenzene 0.044 0.037 0.028 11.844

163 106.625 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 0.649 0.542 0.404 173.548

164 106.918 105-05-5 Q10 1,4-Diethylbenzene 0.214 0.178 0.133 57.206

165 107.176 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.116 0.095 0.072 30.996

166 107.428 135-01-3 Q10 1,2-Diethylbenzene 0.045 0.037 0.028 11.949

167 107.888 ? Unidentified 0.050 0.048 0.027 15.627

168 108.026 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.045 0.037 0.028 11.916

169 108.163 ? Unidentified 0.058 0.057 0.032 18.289

170 108.245 ? Unidentified 0.051 0.049 0.027 15.925

171 108.367 I11 C11- Isoparaffin-11 0.445 0.430 0.238 112.411

172 108.549 ? Unidentified 0.145 0.140 0.077 45.338

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C-9
Hydrocarbon Expert V4.7 Wed Aug 25 16:51:12 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91308 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91308

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 108.880 1758-88-9 Q10 1,4,Dimethyl-2-ethylbenzene 0.081 0.067 0.051 21.759

174 108.982 ? Unidentified 0.454 0.372 0.283 142.345

175 109.206 J10 2-Methylindan 0.076 0.057 0.048 20.864

176 109.544 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.256 0.210 0.159 68.453

177 110.101 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.405 0.327 0.252 108.326

178 110.529 ? Unidentified 0.014 0.012 0.007 4.250

179 110.731 693-61-8 K11 2-Undecene, (E)- 0.034 0.033 0.020 8.523

180 110.858 ? Unidentified 0.082 0.080 0.049 25.775

181 111.133 ? Unidentified 0.068 0.057 0.038 21.219

182 111.219 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.064 0.051 0.040 17.039

183 111.532 1120-21-4 P11 n-Undecane 0.051 0.049 0.027 12.912

184 111.688 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.058 0.047 0.033 15.364

185 111.799 ? Unidentified 0.038 0.031 0.021 11.848

186 112.164 Q10 1,2,4,5-Tetramethylbenzene 0.195 0.158 0.122 52.220

187 112.430 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.265 0.214 0.165 70.824

188 112.786 ? Unidentified 0.016 0.013 0.010 4.914

189 112.967 I12 C12 - IsoParaffin - 1 0.013 0.012 0.006 3.168

190 113.294 ? Unidentified 0.022 0.022 0.011 6.961

191 113.585 Q11 C11 - Aromatic - 3 0.045 0.036 0.025 11.872

192 113.763 874-35-1 H10 5-Methylindan 0.077 0.062 0.049 20.644

193 113.903 Q12 1,2-Di-i-propylbenzene 0.032 0.026 0.017 8.578

194 114.118 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.046 0.037 0.026 12.203

195 114.281 Q11 C11 - Aromatic - 4 0.025 0.020 0.014 6.628

196 114.515 824-22-6 J10 4-Methylindan 0.102 0.083 0.065 27.392

197 114.682 ? Unidentified 0.023 0.019 0.013 7.181

198 114.766 824-63-5 H10 2-Methylindan 0.082 0.066 0.052 21.813

199 114.979 ? Unidentified 0.008 0.007 0.005 2.641

200 115.092 538-68-1 Q11 n-Pentylbenzene 0.011 0.009 0.006 2.876

201 115.321 Q11 tert-Pentylbenzene 0.045 0.036 0.025 11.966

202 115.634 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.019 0.016 0.011 5.161

203 115.745 Q11 C11 - Aromatic - 7 0.026 0.022 0.015 6.925

204 116.206 100-18-5 Q12 1,4-Di-i-propylbenzene 0.035 0.028 0.018 9.335

205 116.633 91-20-3 G10 Naphthalene 0.061 0.043 0.040 17.146

206 117.081 J11 1,1-Dimethyl Indane 0.005 0.004 0.003 1.451

207 117.432 7364-19-4 Q12 1t-Butyl-4-ethylbenzene 0.004 0.003 0.002 1.144

208 117.737 Q12 1,3-Di-n-propylbenzene 0.029 0.023 0.015 7.625

209 117.847 Q11 C11 - Aromatic - 11 0.016 0.014 0.009 4.307

210 118.403 Q11 C11 - Aromatic - 12 0.010 0.008 0.006 2.639

211 123.283 91-57-6 G11 2-Methylnaphthalene 0.010 0.007 0.006 2.778

212 124.150 90-12-0 G11 1-Methylnaphthalene 0.006 0.004 0.003 1.542

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C-10
Hydrocarbon Expert V4.7 Wed Aug 25 16:51:12 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91308 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91308

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 7.390 74-98-6 Propane 0.003 0.005 0.006 0.788

9.793 106-97-8 n-Butane 0.308 0.383 0.443 76.175

17.700 109-66-0 n-Pentane 4.874 5.596 5.643 1212.875

35.305 110-54-3 n-Hexane 3.981 4.340 3.858 994.579

57.624 142-82-5 n-Heptane 0.905 0.952 0.755 227.081

77.567 111-65-9 n-Octane 0.425 0.435 0.311 106.791

91.485 111-84-2 n-Nonane 0.294 0.295 0.192 74.085

102.657 124-18-5 n-Decane 0.064 0.063 0.038 16.253

111.532 1120-21-4 n-Undecane 0.051 0.049 0.027 12.912

I-Paraffins 8.612 75-28-5 i-Butane 0.040 0.052 0.058 9.925

10.389 463-82-1 2,2-Dimethylpropane 0.057 0.069 0.065 14.063

14.727 78-78-4 i-Pentane 16.207 18.804 18.761 4032.715

22.608 75-83-2 2,2-Dimethylbutane 0.310 0.343 0.300 77.375

27.833 79-29-8 2,3-Dimethylbutane 0.785 0.853 0.761 196.149

28.918 107-83-5 2-Methylpentane 3.405 3.748 3.300 850.670

31.558 96-14-0 3-Methylpentane 2.376 2.571 2.303 593.542

41.741 108-08-7 2,4-Dimethylpentane 0.424 0.453 0.353 106.370

42.277 464-06-2 2,2,3-Trimethylbutane 0.053 0.055 0.044 13.318

50.197 591-76-4 2-Methylhexane 1.372 1.453 1.143 344.059

52.034 589-34-4 3-Methylhexane 0.807 0.844 0.673 202.424

54.689 540-84-1 2,2,4-Trimethylpentane 1.160 1.205 0.848 291.532

62.423 590-73-8 2,2-Dimethylhexane 0.030 0.031 0.022 7.476

64.512 564-02-3 2,2,3-Trimethylpentane 0.303 0.304 0.221 76.117

64.754 592-13-2 2,5-Dimethylhexane 0.645 0.669 0.472 162.099

65.092 589-43-5 2,4-Dimethylhexane 0.581 0.597 0.425 146.037

66.333 563-16-6 3,3-Dimethylhexane 0.021 0.022 0.016 5.354

68.098 565-75-3 2,3,4-Trimethylpentane 2.844 2.844 2.080 714.827

68.778 560-21-4 2,3,3-Trimethylpentane 3.583 3.547 2.619 900.391

70.432 584-94-1 2,3-Dimethylhexane 0.829 0.837 0.606 208.377

71.702 592-27-8 2-Methylheptane 0.242 0.249 0.177 60.786

71.961 589-53-7 4-Methylheptane 0.168 0.171 0.123 42.188

73.024 589-81-1 3-Methylheptane 0.206 0.210 0.150 51.711

73.209 619-99-8 3-Ethylhexane 0.109 0.109 0.079 27.295

74.936 3522-94-9 2,2,5-Trimethylhexane 2.094 2.129 1.364 527.376

80.059 1069-53-0 2,3,5-Trimethylhexane 0.346 0.344 0.225 87.074

81.235 1071-26-7 2,4-Dimethylheptane 0.062 0.063 0.040 15.565

82.197 1072-05-5 2,6-Dimethylheptane 0.096 0.097 0.062 24.096

83.130 2,5-Dimethylheptane 0.201 0.202 0.131 50.507

83.304 926-82-9 3,5-Dimethylheptane 0.021 0.021 0.014 5.324

87.017 2216-34-4 4-Methyloctane 0.040 0.040 0.026 10.037

87.149 3221-61-2 2-Methyloctane 0.055 0.055 0.036 13.832

88.015 2216-33-3 3-Methyloctane 0.061 0.061 0.040 15.443

89.070 C10 - IsoParaffin - 1 0.400 0.395 0.235 100.835

89.91614720-74-2 2,2,4-trimethylheptane 0.280 0.277 0.164 70.641

93.82415869-87-1 2,2-Dimethyloctane 0.017 0.017 0.010 4.327

94.63015869-89-3 2,5-Dimethyloctane 0.010 0.010 0.006 2.510

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C-11
Hydrocarbon Expert V4.7 Wed Aug 25 16:51:12 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91308 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91308

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

I-Paraffins 94.816 C10 - IsoParaffin - 2 0.010 0.010 0.006 2.647

95.266 2051-30-1 2,4-Dimethyloctane 0.012 0.012 0.007 2.976

95.661 2,6-Dimethyloctane 0.010 0.009 0.006 2.418

98.68417301-94-8 4-Methylnonane 0.012 0.011 0.007 2.938

99.663 5911-04-6 3-Methylnonane 0.017 0.016 0.010 4.176

100.478 C11-Isoparaffin-2 0.030 0.029 0.016 7.687

102.10917302-01-1 3-Ethyl-3-methylheptane 0.068 0.065 0.036 17.109

104.194 C11 Isoparaffin-4 0.011 0.010 0.006 2.690

106.148 C11-Isoparaffin-7 0.194 0.187 0.104 48.994

108.367 C11- Isoparaffin-11 0.445 0.430 0.238 112.411

112.967 C12 - IsoParaffin - 1 0.013 0.012 0.006 3.168

Aromatics

Mono-Aromatics 45.140 71-42-3 Benzene 0.831 0.680 0.889 229.079

68.631 108-88-3 Toluene 6.056 5.021 5.489 1650.972

84.441 100-41-4 Ethylbenzene 1.020 0.846 0.802 275.975

85.671 108-38-3 m-Xylene 2.565 2.134 2.018 694.152

85.820 106-42-3 p-Xylene 1.157 0.966 0.911 313.155

88.653 95-47-6 o-Xylene 0.910 0.743 0.716 246.110

92.840 98-82-8 i-Propylbenzene 0.035 0.029 0.025 9.479

96.307 103-65-1 n-Propylbenzene 0.255 0.213 0.177 68.654

97.155 620-14-4 1-Methyl-3-ethylbenzene 0.997 0.829 0.693 268.029

97.389 622-96-8 1-Methyl-4-ethylbenzene 0.475 0.396 0.330 127.589

98.015 108-67-8 1,3,5-Trimethylbenzene 0.634 0.527 0.441 170.506

99.100 611-14-3 1-Methyl-2-ethylbenzene 0.388 0.317 0.270 104.326

100.737 95-63-6 1,2,4-Trimethylbenzene 1.953 1.603 1.357 525.082

102.390 538-93-2 i-Butylbenzene 0.094 0.079 0.058 25.039

103.612 526-73-8 1,2,3-Trimethylbenzene 0.352 0.283 0.245 94.713

104.005 535-77-3 1-Methyl-3-i-propylbenzene 0.014 0.012 0.009 3.714

106.334 141-93-5 1,3-Diethylbenzene 0.044 0.037 0.028 11.844

106.625 1074-43-7 1-Methyl-3-n-propylbenzene 0.649 0.542 0.404 173.548

106.918 105-05-5 1,4-Diethylbenzene 0.214 0.178 0.133 57.206

107.176 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.116 0.095 0.072 30.996

107.428 135-01-3 1,2-Diethylbenzene 0.045 0.037 0.028 11.949

108.026 1074-17-5 1-Methyl-2-n-propylbenzene 0.045 0.037 0.028 11.916

108.880 1758-88-9 1,4,Dimethyl-2-ethylbenzene 0.081 0.067 0.051 21.759

109.544 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.256 0.210 0.159 68.453

110.101 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.405 0.327 0.252 108.326

111.219 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.064 0.051 0.040 17.039

111.688 4218-48-8 1-Ethyl-4-i-propylbenzene 0.058 0.047 0.033 15.364

112.164 1,2,4,5-Tetramethylbenzene 0.195 0.158 0.122 52.220

112.430 527-53-7 1,2,3,5-Tetramethylbenzene 0.265 0.214 0.165 70.824

113.585 C11 - Aromatic - 3 0.045 0.036 0.025 11.872

113.903 1,2-Di-i-propylbenzene 0.032 0.026 0.017 8.578

114.118 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.046 0.037 0.026 12.203

114.281 C11 - Aromatic - 4 0.025 0.020 0.014 6.628

115.092 538-68-1 n-Pentylbenzene 0.011 0.009 0.006 2.876

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C-12
Hydrocarbon Expert V4.7 Wed Aug 25 16:51:12 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91308 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91308

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 115.321 tert-Pentylbenzene 0.045 0.036 0.025 11.966

115.634 577-55-9 1-Methyl-2-n-butylbenzene 0.019 0.016 0.011 5.161

115.745 C11 - Aromatic - 7 0.026 0.022 0.015 6.925

116.206 100-18-5 1,4-Di-i-propylbenzene 0.035 0.028 0.018 9.335

117.432 7364-19-4 1t-Butyl-4-ethylbenzene 0.004 0.003 0.002 1.144

117.737 1,3-Di-n-propylbenzene 0.029 0.023 0.015 7.625

117.847 C11 - Aromatic - 11 0.016 0.014 0.009 4.307

118.403 C11 - Aromatic - 12 0.010 0.008 0.006 2.639

Naphthalenes 116.633 91-20-3 Naphthalene 0.061 0.043 0.040 17.146

123.283 91-57-6 2-Methylnaphthalene 0.010 0.007 0.006 2.778

124.150 90-12-0 1-Methylnaphthalene 0.006 0.004 0.003 1.542

Naphtheno/Olefino-Benzs 113.763 874-35-1 5-Methylindan 0.077 0.062 0.049 20.644

114.766 824-63-5 2-Methylindan 0.082 0.066 0.052 21.813

Indenes 104.803 Indan 0.124 0.092 0.088 33.876

105.431 Indene 0.435 0.325 0.308 118.912

109.206 2-Methylindan 0.076 0.057 0.048 20.864

114.515 824-22-6 4-Methylindan 0.102 0.083 0.065 27.392

117.081 1,1-Dimethyl Indane 0.005 0.004 0.003 1.451

Naphthenes

Mono-Naphthenes 27.092 287-92-3 Cyclopentane 0.449 0.433 0.535 114.905

40.168 96-37-7 Methylcyclopentane 2.373 2.279 2.355 607.301

47.063 110-82-7 Cyclohexane 1.762 1.628 1.749 451.067

52.885 1759-58-6 1t,3-Dimethylcyclopentane 0.242 0.232 0.206 61.894

53.471 2532-58-3 1c,3-Dimethylcyclopentane 0.195 0.188 0.166 49.809

54.098 822-50-4 1t,2-Dimethylcyclopentane 0.293 0.280 0.249 74.973

59.20516491-15-9 Cyclopentene, 1,5-dimethyl- 0.020 0.019 0.017 5.062

61.070 108-87-2 Methylcyclohexane 1.542 1.440 1.311 394.560

62.018 4516-69-2 1,1,3-Trimethylcyclopentane 0.038 0.036 0.028 9.687

63.860 1640-89-7 Ethylcyclopentane 0.052 0.049 0.044 13.312

65.930 4850-28-6 1c,2t,4-Trimethylcyclopentane 0.035 0.033 0.026 8.961

67.46015890-40-1 1t,2c,3-Trimethylcyclopentane 0.030 0.028 0.022 7.567

72.865 1,3-dimethyl-t-cyclohexane 0.173 0.162 0.129 44.347

75.273 3c-Ethylmethylcyclopentane 0.009 0.009 0.007 2.399

75.493 3t-Ethylmethylcyclopentane 0.013 0.012 0.010 3.375

76.196 2207-03-6 1t,3-Dimethylcyclohexane 0.074 0.069 0.055 19.011

81.057 2207-01-4 1c,2-Dimethylcyclohexane 0.013 0.012 0.009 3.262

81.870 1678-91-7 Ethylcyclohexane 0.107 0.098 0.080 27.459

89.643 trans-1,3-Diethylcyclopentane 0.017 0.014 0.011 4.560

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.404 115-11-7 Isobutene 0.016 0.019 0.024 4.054

9.444 106-98-9 Butene-1 0.019 0.023 0.029 4.953

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C-13
Hydrocarbon Expert V4.7 Wed Aug 25 16:51:12 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91308 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91308

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

n-Olefins 10.267 624-64-6 t-Butene-2 0.075 0.089 0.112 19.229

10.987 590-18-1 c-Butene-2 0.089 0.103 0.132 22.743

16.338 109-67-1 Pentene-1 0.346 0.388 0.412 88.469

18.797 646-04-8 t-Pentene-2 0.881 0.977 1.049 225.410

19.821 627-20-3 c-Pentene-2 0.483 0.530 0.575 123.614

32.943 592-41-6 Hexene-1 0.170 0.180 0.168 43.445

35.93613269-52-8 t-Hexene-3 0.279 0.294 0.277 71.401

36.414 4050-45-7 t-Hexene-2 0.535 0.563 0.531 136.913

38.254 7688-21-3 c-Hexene-2 0.228 0.237 0.226 58.285

55.027 592-76-7 Heptene-1 0.031 0.032 0.027 8.050

56.88314686-14-7 t-Heptene-3 0.035 0.036 0.030 8.889

57.839 7642-10-6 c-Heptene-3 0.026 0.027 0.022 6.690

58.74814686-13-6 t-Heptene-2 0.017 0.018 0.015 4.402

110.731 693-61-8 2-Undecene, (E)- 0.034 0.033 0.020 8.523

Iso-Olefins 13.128 563-45-1 3-Methylbutene-1 0.300 0.344 0.357 76.734

17.172 563-46-2 2-Methylbutene-1 0.525 0.581 0.626 134.460

20.491 513-35-9 2-Methylbutene-2 1.084 1.177 1.291 277.414

28.695 691-38-3 4-Methyl-c-pentene-2 0.047 0.050 0.047 12.061

29.349 674-76-0 4-Methyl-t-pentene-2 0.138 0.148 0.137 35.376

32.722 763-29-1 2-Methylpentene-1 0.237 0.249 0.235 60.619

36.906 625-27-4 2-Methylpentene-2 0.363 0.377 0.360 92.848

37.321 922-62-3 3-Methyl-c-pentene-2 0.281 0.289 0.278 71.798

39.590 3404-73-7 3,3-Dimethylpentene-1 0.332 0.340 0.283 85.027

42.039 594-56-9 2,3,3-Trimethylbutene-1 0.015 0.015 0.013 3.775

46.162 3404-61-3 3-Methylhexene-1 0.017 0.017 0.014 4.257

46.749 3524-73-0 5-Methylhexene-1 0.084 0.087 0.071 21.467

48.80615840-60-5 2-Methyl-c-hexene-3 0.043 0.045 0.037 11.006

49.152 3769-23-1 4-Methylhexene-1 0.011 0.011 0.009 2.847

49.805 3404-55-5 4-Methyl-t/c-hexene-2 0.054 0.055 0.046 13.838

54.402 C7 - Iso-Olefin - 2 0.024 0.024 0.020 6.018

56.365 4914-89-0 3-Methyl-c-hexene-3 0.015 0.015 0.013 3.865

57.246 6094-02-6 2-Methylhexene-1 0.062 0.064 0.053 15.916

58.118 2738-19-4 2-Methyl-2-hexene 0.028 0.029 0.024 7.239

58.363 3899-36-3 3-Methyl-t-hexene-3 0.022 0.022 0.018 5.522

59.64920710-38-8 3-Methyl-t-hexene-2 0.016 0.016 0.014 4.157

60.434 4914-91-4 2-Pentene, 3,4-dimethyl-, (Z)- 0.014 0.014 0.012 3.666

70.131 C8 - Diolefin - 1 0.012 0.011 0.009 3.017

80.619 C9 - IsoOlefin - 1 0.013 0.012 0.010 3.335

86.221 C9-IsoOlefin-3 0.011 0.010 0.007 2.846

Naphtheno-Olefins 25.250 142-29-0 Cyclopentene 0.206 0.192 0.253 54.331

45.347 693-89-0 1-Methylcyclopentene 0.388 0.358 0.395 101.725

50.675 110-83-8 Cyclohexene 0.047 0.042 0.048 12.145

Di-Olefins 18.209 78-79-5 2-Methyl-1,3-Butadiene 0.011 0.011 0.013 2.829

20.823 2004-70-8 1t,3-Pentadiene 0.016 0.017 0.020 4.233

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C-14
Hydrocarbon Expert V4.7 Wed Aug 25 16:51:12 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91308 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91308

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Di-Olefins

Oxygenates 12.745 64-17-5 Ethanol 9.196 8.379 16.672 1011.630

26.498 71-23-8 n-Propanol 0.112 0.101 0.156 20.102

Unidentified 22.064 Unidentified 0.006 0.006 0.008 1.883

26.426 Unidentified 0.044 0.039 0.061 13.657

28.233 Unidentified 0.054 0.052 0.051 16.789

44.938 Unidentified 0.012 0.012 0.013 3.894

47.602 Unidentified 0.036 0.037 0.031 11.379

72.096 Unidentified 0.073 0.073 0.054 23.034

74.105 Unidentified 0.027 0.025 0.020 8.494

75.910 Unidentified 0.014 0.014 0.009 4.366

78.511 Unidentified 0.051 0.050 0.034 16.140

82.676 Unidentified 0.020 0.021 0.013 6.335

84.621 Unidentified 0.026 0.025 0.017 8.075

84.862 Unidentified 0.031 0.029 0.021 9.743

85.966 Unidentified 0.060 0.060 0.039 18.870

86.329 Unidentified 0.011 0.011 0.007 3.430

88.481 Unidentified 0.118 0.125 0.078 37.130

93.600 Unidentified 0.044 0.043 0.026 13.696

98.885 Unidentified 0.235 0.233 0.138 73.669

100.129 Unidentified 0.020 0.014 0.011 6.177

100.254 Unidentified 0.059 0.057 0.031 18.380

100.942 Unidentified 0.041 0.042 0.025 12.941

101.065 Unidentified 0.022 0.022 0.013 7.033

102.976 Unidentified 0.018 0.017 0.010 5.618

104.395 Unidentified 0.066 0.055 0.041 20.702

107.888 Unidentified 0.050 0.048 0.027 15.627

108.163 Unidentified 0.058 0.057 0.032 18.289

108.245 Unidentified 0.051 0.049 0.027 15.925

108.549 Unidentified 0.145 0.140 0.077 45.338

108.982 Unidentified 0.454 0.372 0.283 142.345

110.529 Unidentified 0.014 0.012 0.007 4.250

110.858 Unidentified 0.082 0.080 0.049 25.775

111.133 Unidentified 0.068 0.057 0.038 21.219

111.799 Unidentified 0.038 0.031 0.021 11.848

112.786 Unidentified 0.016 0.013 0.010 4.914

113.294 Unidentified 0.022 0.022 0.011 6.961

114.682 Unidentified 0.023 0.019 0.013 7.181

114.979 Unidentified 0.008 0.007 0.005 2.641

Plus

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C-15
Hydrocarbon Expert V4.7 Wed Aug 25 16:51:12 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91308 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91308

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF

20.0 15.0 10.0 5.0 0.0

Propane

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

Ethanol

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

Unidentified

2,2-Dimethylbutane

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C-16
Hydrocarbon Expert V4.7 Wed Aug 25 16:51:12 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91308 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91308

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

Unidentified n-Propanol

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

n-Hexane

t-Hexene-3

t-Hexene-2

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane 2,3,3-Trimethylbutene-1 2,2,3-Trimethylbutane

Unidentified Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1 Cyclohexane

Unidentified

2-Methyl-c-hexene-3

4-Methylhexene-1

4-Methyl-t/c-hexene-2

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C-17
Hydrocarbon Expert V4.7 Wed Aug 25 16:51:12 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91308 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91308

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF

70.0 65.0 60.0 55.0 50.0

2-Methylhexane

Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane C7 - Iso-Olefin - 2 2,2,4-Trimethylpentane

Heptene-1

3-Methyl-c-hexene-3

t-Heptene-3

2-Methylhexene-1

n-Heptane c-Heptene-3 2-Methyl-2-hexene 3-Methyl-t-hexene-3

t-Heptene-2

Cyclopentene, 1,5-dimethyl3-Methyl-t-hexene-2

2-Pentene, 3,4-dimethyl-, (Z)-

Methylcyclohexane

1,1,3-Trimethylcyclopentane

2,2-Dimethylhexane

Ethylcyclopentane

2,2,3-Trimethylpentane 2,5-Dimethylhexane

2,4-Dimethylhexane

1c,2t,4-Trimethylcyclopentane

3,3-Dimethylhexane

1t,2c,3-Trimethylcyclopentane

2,3,4-Trimethylpentane

Toluene 2,3,3-Trimethylpentane

C8 - Diolefin - 1 2,3-Dimethylhexane

2-Methylheptane

Unidentified 4-Methylheptane

1,3-dimethyl-t-cyclohexane 3-Methylheptane 3-Ethylhexane

Unidentified

2,2,5-Trimethylhexane

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C-18
Hydrocarbon Expert V4.7 Wed Aug 25 16:51:12 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91308 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91308

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF

95.0 90.0 85.0 80.0 75.0

3c-Ethylmethylcyclopentane 3t-Ethylmethylcyclopentane

Unidentified 1t,3-Dimethylcyclohexane

n-Octane

Unidentified

2,3,5-Trimethylhexane

C9 - IsoOlefin - 1

1c,2-Dimethylcyclohexane 2,4-Dimethylheptane

Ethylcyclohexane

2,6-Dimethylheptane

Unidentified

2,5-Dimethylheptane 3,5-Dimethylheptane

Ethylbenzene Unidentified

m-Xylene Unidentified p-Xylene

C9-IsoOlefin-3 Unidentified

4-Methyloctane 2-Methyloctane

3-Methyloctane

Unidentified o-Xylene

C10 - IsoParaffin - 1

trans-1,3-Diethylcyclopentane 2,2,4-trimethylheptane

n-Nonane

i-Propylbenzene

Unidentified 2,2-Dimethyloctane

2,5-Dimethyloctane C10 - IsoParaffin - 2

2,4-Dimethyloctane

2,6-Dimethyloctane

n-Propylbenzene

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

4-Methylnonane Unidentified 1-Methyl-2-ethylbenzene

3-Methylnonane

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C-19
Hydrocarbon Expert V4.7 Wed Aug 25 16:51:12 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91308 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91308

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified

C11-Isoparaffin-2 1,2,4-Trimethylbenzene Unidentified

3-Ethyl-3-methylheptane i-Butylbenzene n-Decane

Unidentified

1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene C11 Isoparaffin-4 Unidentified

Indan

Indene

C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene 1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

Unidentified 1-Methyl-2-n-propylbenzene Unidentified C11- Isoparaffin-11 Unidentified

1,4,Dimethyl-2-ethylbenzene Unidentified 2-Methylindan

1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

Unidentified 2-Undecene, (E)- Unidentified Unidentified 1,2-Dimethyl-3-ethylbenzene n-Undecane Unidentified 1-Ethyl-4-i-propylbenzene

1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene

Unidentified C12 - IsoParaffin - 1

Unidentified C11 - Aromatic - 3 5-Methylindan 1,2-Di-i-propylbenzene 1-methyl-4-(1-methylpropyl)be C11 - Aromatic - 4 4-Methylindan Unidentified 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene 1-Methyl-2-n-butylbenzene C11 - Aromatic - 7

1,4-Di-i-propylbenzene

Naphthalene

1,1-Dimethyl Indane

1t-Butyl-4-ethylbenzene

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

C11 - Aromatic - 12

2-Methylnaphthalene

1-Methylnaphthalene

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C-20
Hydrocarbon Expert V4.7 Wed Aug 25 16:51:12 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91308 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91308

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000004.D\SIG1000004_FID1_A.CDF

145.0 140.0 135.0 130.0 125.0

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C-21
Hydrocarbon Expert V4.7 Wed Aug 25 17:08:36 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91309 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91309

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 9.494 11.579 14.880

I-Paraffins 52.502 54.556 46.950

Aromatics 23.810 19.614 20.918

Mono-Aromatics 21.324 17.732 18.928

Naphthalenes 0.126 0.089 0.094

Naphtheno/Olefino-Benzs 0.216 0.175 0.159

Indenes 2.145 1.618 1.737

Naphthenes 1.287 1.235 1.441

Mono-Naphthenes 1.287 1.235 1.441

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 7.508 8.052 9.629

n-Olefins 3.380 3.707 4.450

Iso-Olefins 3.513 3.770 4.394

Naphtheno-Olefins 0.591 0.549 0.751

Di-Olefins 0.024 0.026 0.034

Oxygenates 0.198 0.179 0.321

Unidentified 5.201 4.786 5.860

Plus 0.000 0.000 0.000

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C-22
Hydrocarbon Expert V4.7 Wed Aug 25 17:08:36 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91309 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91309

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C3 0.199 0.181 0.324

C4 7.925 9.888 13.300

C5 9.788 11.132 13.380

C6 9.084 9.500 10.459

C7 8.451 7.786 8.669

C8 34.173 33.913 29.491

C9 9.859 9.042 7.757

C10 12.601 11.229 9.050

C11 2.511 2.369 1.586

C12 0.208 0.176 0.124

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C-23
Hydrocarbon Expert V4.7 Wed Aug 25 17:08:36 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91309 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91309

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C3 0.001 0.001 0.002

C4 7.610 9.509 12.756

C5 0.877 1.014 1.185

C6 0.455 0.499 0.514

C7 0.092 0.097 0.090

C8 0.028 0.029 0.024

C9 0.274 0.276 0.208

C10 0.062 0.061 0.042

C11 0.095 0.093 0.059

I-Paraffins C4 0.045 0.059 0.076

C5 4.969 5.801 6.710

C6 4.277 4.698 4.835

C7 2.530 2.702 2.460

C8 28.765 29.389 24.534

C9 4.363 4.447 3.314

C10 5.610 5.571 3.811

C11 1.899 1.846 1.183

C12 0.045 0.043 0.026

Mono-Aromatics C6 0.663 0.545 0.827

C7 5.145 4.293 5.441

C8 5.332 4.450 4.893

C9 4.977 4.129 4.034

C10 4.660 3.866 3.383

C11 0.389 0.319 0.256

C12 0.158 0.128 0.095

Naphthalenes C10 0.104 0.073 0.079

C11 0.022 0.016 0.015

Naphtheno/Olefino-Benzs C10 0.216 0.175 0.159

Indenes C9 0.214 0.161 0.176

C10 1.891 1.427 1.534

C11 0.035 0.026 0.023

C12 0.005 0.004 0.004

Mono-Naphthenes C5 0.109 0.105 0.151

C6 0.892 0.859 1.033

C7 0.170 0.164 0.169

C8 0.032 0.030 0.028

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C-24
Hydrocarbon Expert V4.7 Wed Aug 25 17:08:36 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91309 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91309

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Mono-Naphthenes C9 0.032 0.028 0.024

C10 0.053 0.048 0.037

n-Olefins C4 0.270 0.320 0.468

C5 1.800 2.007 2.501

C6 1.222 1.292 1.414

C7 0.017 0.018 0.017

C11 0.071 0.069 0.049

Iso-Olefins C5 1.807 1.990 2.511

C6 1.187 1.246 1.374

C7 0.496 0.511 0.492

C8 0.017 0.016 0.013

C10 0.007 0.007 0.005

Naphtheno-Olefins C5 0.202 0.189 0.289

C6 0.390 0.360 0.462

Di-Olefins C5 0.024 0.026 0.034

Oxygenates C3 0.198 0.179 0.321

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C-25
Hydrocarbon Expert V4.7 Wed Aug 25 17:08:36 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91309 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91309

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 21.21 21.07

5% 27.39 26.01

10% 79.94 61.95

15% 96.88 81.49

20% 138.32 100.41

25% 155.78 140.92

30% 197.12 164.98

35% 209.78 209.22

40% 210.50 209.91

45% 230.00 215.65

50% 231.59 230.20

55% 235.89 232.78

60% 237.84 236.60

65% 247.22 238.31

70% 277.14 250.85

75% 296.60 281.40

80% 331.74 320.72

85% 335.68 332.38

90% 358.47 352.22

95% 363.20 363.20

FBP 404.36 399.20

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C-26
Hydrocarbon Expert V4.7 Wed Aug 25 17:08:36 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91309 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91309

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 7.391 74-98-6 P3 Propane 0.001 0.001 0.002 0.238

2 8.614 75-28-5 I4 i-Butane 0.045 0.059 0.076 10.860

3 9.406 115-11-7 K4 Isobutene 0.024 0.029 0.041 5.882

4 9.445 106-98-9 K4 Butene-1 0.028 0.034 0.049 6.958

5 9.794 106-97-8 P4 n-Butane 7.610 9.509 12.756 1825.633

6 10.269 624-64-6 K4 t-Butene-2 0.103 0.123 0.178 25.477

7 10.392 463-82-1 I5 2,2-Dimethylpropane 0.016 0.020 0.022 3.924

8 10.990 590-18-1 K4 c-Butene-2 0.115 0.134 0.201 28.695

9 13.132 563-45-1 C5 3-Methylbutene-1 0.079 0.091 0.109 19.531

10 14.711 78-78-4 I5 i-Pentane 4.953 5.781 6.688 1196.406

11 16.335 109-67-1 K5 Pentene-1 0.361 0.408 0.501 89.699

12 17.174 563-46-2 C5 2-Methylbutene-1 0.565 0.628 0.785 140.345

13 17.694 109-66-0 P5 n-Pentane 0.877 1.014 1.185 211.976

14 18.213 78-79-5 E5 2-Methyl-1,3-Butadiene 0.010 0.010 0.014 2.525

15 18.805 646-04-8 K5 t-Pentene-2 0.930 1.038 1.292 231.167

16 19.439 ? Unidentified 0.006 0.007 0.009 1.943

17 19.822 627-20-3 K5 c-Pentene-2 0.509 0.561 0.707 126.428

18 20.493 513-35-9 C5 2-Methylbutene-2 1.164 1.271 1.617 289.185

19 20.830 2004-70-8 E5 1t,3-Pentadiene 0.014 0.015 0.020 3.628

20 22.645 75-83-2 I6 2,2-Dimethylbutane 0.034 0.038 0.039 8.285

21 25.253 142-29-0 B5 Cyclopentene 0.202 0.189 0.289 51.612

22 26.495 71-23-8 X3 n-Propanol 0.198 0.179 0.321 34.490

23 27.103 287-92-3 M5 Cyclopentane 0.109 0.105 0.151 26.962

24 27.841 79-29-8 I6 2,3-Dimethylbutane 1.239 1.355 1.401 300.613

25 28.236 ? Unidentified 0.056 0.055 0.062 17.185

26 28.696 691-38-3 C6 4-Methyl-c-pentene-2 0.049 0.053 0.057 12.274

27 28.909 107-83-5 I6 2-Methylpentane 1.873 2.074 2.117 454.233

28 29.342 674-76-0 C6 4-Methyl-t-pentene-2 0.146 0.157 0.169 36.318

29 31.558 96-14-0 I6 3-Methylpentane 1.130 1.231 1.278 274.132

30 32.719 763-29-1 C6 2-Methylpentene-1 0.248 0.262 0.287 61.701

31 32.942 592-41-6 K6 Hexene-1 0.170 0.181 0.196 42.151

32 35.133 760-21-4 C6 2-Ethylbutene-1 0.076 0.079 0.088 18.784

33 35.289 110-54-3 P6 n-Hexane 0.455 0.499 0.514 110.296

34 35.93613269-52-8 K6 t-Hexene-3 0.284 0.302 0.329 70.681

35 36.412 4050-45-7 K6 t-Hexene-2 0.539 0.571 0.624 133.884

36 36.904 625-27-4 C6 2-Methylpentene-2 0.378 0.396 0.438 94.017

37 37.312 922-62-3 C6 3-Methyl-c-pentene-2 0.289 0.299 0.335 71.804

38 38.242 7688-21-3 K6 c-Hexene-2 0.229 0.239 0.265 56.822

39 39.582 3404-73-7 C7 3,3-Dimethylpentene-1 0.343 0.354 0.340 85.254

40 40.153 96-37-7 M6 Methylcyclopentane 0.816 0.788 0.944 202.724

41 41.734 108-08-7 I7 2,4-Dimethylpentane 1.061 1.140 1.031 258.258

42 42.041 594-56-9 C7 2,3,3-Trimethylbutene-1 0.012 0.012 0.012 2.989

43 42.281 464-06-2 I7 2,2,3-Trimethylbutane 0.054 0.057 0.053 13.225

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C-27
Hydrocarbon Expert V4.7 Wed Aug 25 17:08:36 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91309 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91309

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 44.929 ? Unidentified 0.011 0.011 0.013 3.443

45 45.137 71-42-3 Q6 Benzene 0.663 0.545 0.827 177.372

46 45.337 693-89-0 B6 1-Methylcyclopentene 0.352 0.327 0.418 89.681

47 46.159 3404-61-3 C7 3-Methylhexene-1 0.013 0.014 0.013 3.327

48 46.743 3524-73-0 C7 5-Methylhexene-1 0.022 0.023 0.022 5.581

49 47.051 110-82-7 M6 Cyclohexane 0.076 0.071 0.088 18.902

50 47.587 ? Unidentified 0.030 0.031 0.030 9.268

51 48.80615840-60-5 C7 2-Methyl-c-hexene-3 0.033 0.035 0.033 8.287

52 49.798 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.039 0.040 0.038 9.604

53 50.202 591-76-4 I7 2-Methylhexane 1.135 1.210 1.103 276.336

54 50.670 110-83-8 B6 Cyclohexene 0.037 0.033 0.044 9.213

55 52.028 589-34-4 I7 3-Methylhexane 0.281 0.295 0.273 68.305

56 52.885 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.067 0.065 0.066 16.641

57 53.472 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.043 0.042 0.043 10.746

58 54.101 822-50-4 M7 1t,2-Dimethylcyclopentane 0.033 0.031 0.032 8.102

59 54.750 540-84-1 I8 2,2,4-Trimethylpentane 9.991 10.444 8.522 2437.780

60 56.88314686-14-7 K7 t-Heptene-3 0.017 0.018 0.017 4.325

61 57.235 6094-02-6 C7 2-Methylhexene-1 0.027 0.028 0.027 6.823

62 57.614 142-82-5 P7 n-Heptane 0.092 0.097 0.090 22.433

63 58.114 2738-19-4 C7 2-Methyl-2-hexene 0.005 0.005 0.005 1.315

64 61.052 108-87-2 M7 Methylcyclohexane 0.028 0.026 0.027 6.859

65 64.513 564-02-3 I8 2,2,3-Trimethylpentane 0.713 0.720 0.608 173.975

66 64.762 592-13-2 I8 2,5-Dimethylhexane 1.590 1.658 1.356 387.889

67 65.100 589-43-5 I8 2,4-Dimethylhexane 1.521 1.571 1.297 371.133

68 68.121 565-75-3 I8 2,3,4-Trimethylpentane 6.067 6.103 5.175 1480.332

69 68.628 108-88-3 Q7 Toluene 5.145 4.293 5.441 1361.918

70 68.800 560-21-4 I8 2,3,3-Trimethylpentane 6.862 6.835 5.853 1674.338

71 70.438 584-94-1 I8 2,3-Dimethylhexane 1.675 1.701 1.428 408.602

72 71.699 592-27-8 I8 2-Methylheptane 0.086 0.089 0.073 21.022

73 71.965 589-53-7 I8 4-Methylheptane 0.184 0.189 0.157 44.962

74 72.096 ? Unidentified 0.138 0.138 0.117 41.908

75 73.022 589-81-1 I8 3-Methylheptane 0.075 0.077 0.064 18.404

76 74.944 3522-94-9 I9 2,2,5-Trimethylhexane 3.375 3.451 2.563 825.027

77 75.910 3875-51-2 M8 i-Propylcyclopentane 0.032 0.030 0.028 7.902

78 77.564 111-65-9 P8 n-Octane 0.028 0.029 0.024 6.759

79 78.507 ? Unidentified 0.078 0.076 0.059 23.702

80 80.057 1069-53-0 I9 2,3,5-Trimethylhexane 0.534 0.535 0.405 130.490

81 81.233 1071-26-7 I9 2,4-Dimethylheptane 0.077 0.078 0.058 18.744

82 82.195 1072-05-5 I9 2,6-Dimethylheptane 0.097 0.099 0.073 23.610

83 83.129 I9 2,5-Dimethylheptane 0.255 0.257 0.193 62.228

84 84.439 100-41-4 Q8 Ethylbenzene 1.009 0.842 0.926 265.092

85 84.617 ? Unidentified 0.035 0.035 0.028 10.715

86 84.858 ? Unidentified 0.029 0.027 0.022 8.815

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C-28
Hydrocarbon Expert V4.7 Wed Aug 25 17:08:36 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91309 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91309

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 85.666 108-38-3 Q8 m-Xylene 2.374 1.987 2.178 623.536

88 85.815 106-42-3 Q8 p-Xylene 1.112 0.934 1.021 292.195

89 85.963 ? Unidentified 0.081 0.081 0.062 24.719

90 86.220 C8 C9-IsoOlefin-3 0.017 0.016 0.013 4.207

91 86.328 ? Unidentified 0.014 0.014 0.011 4.378

92 87.147 3221-61-2 I9 2-Methyloctane 0.017 0.017 0.013 4.036

93 88.012 2216-33-3 I9 3-Methyloctane 0.010 0.010 0.008 2.537

94 88.480 ? Unidentified 0.162 0.171 0.125 49.219

95 88.650 95-47-6 Q8 o-Xylene 0.836 0.687 0.768 219.714

96 89.068 I10 C10 - IsoParaffin - 1 0.562 0.559 0.385 137.798

97 89.91414720-74-2 I10 2,2,4-trimethylheptane 0.387 0.385 0.265 94.884

98 91.459 111-84-2 P9 n-Nonane 0.274 0.276 0.208 66.938

99 92.087 4926-90-3 M9 1,1-Methylethylcyclohexane 0.025 0.022 0.019 6.224

100 92.837 98-82-8 Q9 i-Propylbenzene 0.033 0.028 0.027 8.711

101 93.027 ? Unidentified 0.017 0.016 0.013 5.298

102 93.027 ? Unidentified 0.017 0.018 0.012 5.298

103 93.027 ? Unidentified 0.017 0.013 0.012 5.298

104 93.135 696-29-7 M9 1-Methyl-2-propyl-cyclopentan 0.007 0.006 0.005 1.660

105 93.135 C10 C10-IsoOlefin-4 0.007 0.007 0.005 1.660

106 93.135 I10 C10-isoparaffin-x 0.000 0.000 0.000 1.660

107 93.602 ? Unidentified 0.213 0.212 0.146 64.761

108 93.82515869-87-1 I10 2,2-Dimethyloctane 0.073 0.073 0.050 17.793

109 94.267 ? Unidentified 0.023 0.017 2.266 7.078

110 94.267 ? Unidentified 0.023 0.024 0.016 7.078

111 94.62315869-89-3 I10 2,5-Dimethyloctane 0.112 0.111 0.076 27.337

112 95.101 2040-95-1 I10 2,7-Dimethyloctane 0.054 0.053 0.037 13.127

113 95.266 2051-30-1 I10 2,4-Dimethyloctane 0.242 0.241 0.166 59.312

114 95.660 I10 2,6-Dimethyloctane 0.071 0.070 0.048 17.322

115 96.304 103-65-1 Q9 n-Propylbenzene 0.268 0.225 0.217 69.964

116 97.153 620-14-4 Q9 1-Methyl-3-ethylbenzene 0.940 0.787 0.762 245.384

117 97.387 622-96-8 Q9 1-Methyl-4-ethylbenzene 0.442 0.371 0.358 115.423

118 98.013 108-67-8 Q9 1,3,5-Trimethylbenzene 0.652 0.545 0.528 170.112

119 98.902 I10 2,2,6-Trimethyloctane 3.607 3.591 2.470 883.576

120 99.099 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.359 0.295 0.291 93.606

121 99.472 ? Unidentified 0.011 0.011 0.008 3.397

122 99.663 5911-04-6 I10 3-Methylnonane 0.016 0.015 0.011 3.801

123 99.839 ? Unidentified 0.011 0.011 0.007 3.261

124 100.129 ? Unidentified 0.214 0.155 0.134 65.229

125 100.256 ? Unidentified 0.571 0.555 0.356 173.820

126 100.481 I11 C11-Isoparaffin-2 0.306 0.298 0.191 75.057

127 100.737 95-63-6 Q9 1,2,4-Trimethylbenzene 1.933 1.597 1.567 504.588

128 100.945 ? Unidentified 0.352 0.363 0.244 107.019

129 101.066 ? Unidentified 0.208 0.206 0.143 63.457

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C-29
Hydrocarbon Expert V4.7 Wed Aug 25 17:08:36 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91309 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91309

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 101.323 1678-98-4 M10 i-Butylcyclohexane 0.051 0.046 0.035 12.644

131 101.966 ? Unidentified 0.020 0.018 0.014 6.013

132 102.11117302-01-1 I10 3-Ethyl-3-methylheptane 0.487 0.474 0.304 119.460

133 102.324 ? Unidentified 0.139 0.118 0.101 42.320

134 102.465 538-93-2 Q10 i-Butylbenzene 0.341 0.289 0.248 88.576

135 102.662 124-18-5 P10 n-Decane 0.062 0.061 0.042 15.142

136 102.976 ? Unidentified 0.131 0.128 0.082 39.935

137 103.468 ? Unidentified 0.016 0.013 0.013 4.772

138 103.614 526-73-8 Q9 1,2,3-Trimethylbenzene 0.349 0.282 0.283 91.056

139 103.978 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.040 0.033 0.029 10.293

140 104.192 I11 C11 Isoparaffin-4 0.057 0.056 0.036 14.100

141 104.397 ? Unidentified 0.280 0.236 0.203 85.224

142 104.803 J9 Indan 0.214 0.161 0.176 56.785

143 105.059 I11 C11-Isoparaffin-5 0.028 0.027 0.017 6.878

144 105.440 J10 Indene 1.607 1.206 1.325 426.325

145 105.857 M10 n-ButylCyclohexane 0.002 0.002 0.001 0.534

146 105.994 ? Unidentified 0.013 0.012 0.009 3.965

147 106.154 I11 C11-Isoparaffin-7 0.582 0.566 0.363 142.769

148 106.335 141-93-5 Q10 1,3-Diethylbenzene 0.049 0.041 0.036 12.828

149 106.634 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 1.607 1.350 1.167 417.204

150 106.905 105-05-5 Q10 1,4-Diethylbenzene 0.459 0.385 0.333 119.254

151 107.176 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.136 0.112 0.099 35.293

152 107.423 135-01-3 Q10 1,2-Diethylbenzene 0.128 0.105 0.093 33.253

153 107.889 ? Unidentified 0.133 0.130 0.083 40.617

154 108.026 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.056 0.046 0.041 14.536

155 108.164 ? Unidentified 0.132 0.129 0.083 40.238

156 108.245 ? Unidentified 0.123 0.120 0.077 37.475

157 108.369 I11 C11- Isoparaffin-11 0.925 0.899 0.576 226.780

158 108.552 ? Unidentified 0.302 0.293 0.188 91.811

159 108.984 ? Unidentified 0.905 0.746 0.657 275.522

160 109.205 J10 2-Methylindan 0.146 0.110 0.108 38.783

161 109.544 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.368 0.304 0.267 95.474

162 109.703 ? Unidentified 0.063 0.047 0.046 19.169

163 110.102 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.781 0.634 0.567 202.650

164 110.528 ? Unidentified 0.031 0.028 0.020 9.567

165 110.729 693-61-8 K11 2-Undecene, (E)- 0.071 0.069 0.049 17.406

166 110.859 ? Unidentified 0.148 0.145 0.103 45.088

167 111.132 ? Unidentified 0.130 0.110 0.085 39.466

168 111.215 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.083 0.067 0.060 21.476

169 111.532 1120-21-4 P11 n-Undecane 0.095 0.093 0.059 23.348

170 111.688 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.106 0.086 0.070 27.365

171 111.798 ? Unidentified 0.074 0.060 0.048 22.449

172 112.163 Q10 1,2,4,5-Tetramethylbenzene 0.264 0.215 0.192 68.534

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C-30
Hydrocarbon Expert V4.7 Wed Aug 25 17:08:36 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91309 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91309

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 112.429 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.348 0.283 0.253 90.340

174 112.653 ? Unidentified 0.013 0.011 0.009 4.083

175 112.784 ? Unidentified 0.022 0.018 0.016 6.611

176 112.965 I12 C12 - IsoParaffin - 1 0.028 0.028 0.016 6.984

177 113.296 ? Unidentified 0.036 0.036 0.022 11.096

178 113.447 ? Unidentified 0.014 0.014 0.008 4.326

179 113.654 ? Unidentified 0.071 0.058 0.047 21.743

180 113.760 874-35-1 H10 5-Methylindan 0.108 0.087 0.079 27.938

181 113.901 Q12 1,2-Di-i-propylbenzene 0.048 0.039 0.029 12.271

182 114.117 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.064 0.052 0.042 16.605

183 114.290 Q11 C11 - Aromatic - 4 0.040 0.033 0.027 10.448

184 114.513 824-22-6 J10 4-Methylindan 0.137 0.111 0.101 35.591

185 114.683 ? Unidentified 0.031 0.025 0.020 9.474

186 114.765 824-63-5 H10 2-Methylindan 0.108 0.088 0.080 28.076

187 114.978 ? Unidentified 0.014 0.011 0.009 4.236

188 115.090 538-68-1 Q11 n-Pentylbenzene 0.016 0.013 0.011 4.160

189 115.320 Q11 tert-Pentylbenzene 0.059 0.048 0.039 15.326

190 115.632 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.029 0.024 0.019 7.604

191 115.744 Q11 C11 - Aromatic - 7 0.040 0.034 0.026 10.364

192 116.093 I12 C12 - IsoParaffin - 4 0.016 0.016 0.009 4.203

193 116.205 100-18-5 Q12 1,4-Di-i-propylbenzene 0.054 0.044 0.032 13.846

194 116.636 91-20-3 G10 Naphthalene 0.104 0.073 0.079 28.146

195 116.796 J11 4,7-Dimethyl Indane 0.022 0.017 0.015 5.944

196 116.972 ? Unidentified 0.007 0.006 0.004 2.091

197 117.079 J11 1,1-Dimethyl Indane 0.013 0.009 0.008 3.327

198 117.248 J12 Dimethyl Indane - 1 0.005 0.004 0.004 1.448

199 117.431 7364-19-4 Q12 1t-Butyl-4-ethylbenzene 0.010 0.008 0.006 2.680

200 117.734 Q12 1,3-Di-n-propylbenzene 0.038 0.031 0.023 9.758

201 117.847 Q11 C11 - Aromatic - 11 0.019 0.017 0.013 5.024

202 118.402 Q11 C11 - Aromatic - 12 0.014 0.012 0.009 3.732

203 122.541 877-44-1 Q12 1,2,4-Triethylbenzene 0.008 0.007 0.005 2.176

204 123.280 91-57-6 G11 2-Methylnaphthalene 0.015 0.011 0.010 4.101

205 124.146 90-12-0 G11 1-Methylnaphthalene 0.007 0.005 0.005 1.903

206 126.171 ? Unidentified 0.009 0.008 0.006 2.827

207 126.171 ? Unidentified 0.009 0.008 0.005 2.827

208 126.171 ? Unidentified 0.009 0.009 0.005 2.827

209 127.135 ? Unidentified 0.003 0.003 0.001 0.914

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C-31
Hydrocarbon Expert V4.7 Wed Aug 25 17:08:36 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91309 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91309

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 7.391 74-98-6 Propane 0.001 0.001 0.002 0.238

9.794 106-97-8 n-Butane 7.610 9.509 12.756 1825.633

17.694 109-66-0 n-Pentane 0.877 1.014 1.185 211.976

35.289 110-54-3 n-Hexane 0.455 0.499 0.514 110.296

57.614 142-82-5 n-Heptane 0.092 0.097 0.090 22.433

77.564 111-65-9 n-Octane 0.028 0.029 0.024 6.759

91.459 111-84-2 n-Nonane 0.274 0.276 0.208 66.938

102.662 124-18-5 n-Decane 0.062 0.061 0.042 15.142

111.532 1120-21-4 n-Undecane 0.095 0.093 0.059 23.348

I-Paraffins 8.614 75-28-5 i-Butane 0.045 0.059 0.076 10.860

10.392 463-82-1 2,2-Dimethylpropane 0.016 0.020 0.022 3.924

14.711 78-78-4 i-Pentane 4.953 5.781 6.688 1196.406

22.645 75-83-2 2,2-Dimethylbutane 0.034 0.038 0.039 8.285

27.841 79-29-8 2,3-Dimethylbutane 1.239 1.355 1.401 300.613

28.909 107-83-5 2-Methylpentane 1.873 2.074 2.117 454.233

31.558 96-14-0 3-Methylpentane 1.130 1.231 1.278 274.132

41.734 108-08-7 2,4-Dimethylpentane 1.061 1.140 1.031 258.258

42.281 464-06-2 2,2,3-Trimethylbutane 0.054 0.057 0.053 13.225

50.202 591-76-4 2-Methylhexane 1.135 1.210 1.103 276.336

52.028 589-34-4 3-Methylhexane 0.281 0.295 0.273 68.305

54.750 540-84-1 2,2,4-Trimethylpentane 9.991 10.444 8.522 2437.780

64.513 564-02-3 2,2,3-Trimethylpentane 0.713 0.720 0.608 173.975

64.762 592-13-2 2,5-Dimethylhexane 1.590 1.658 1.356 387.889

65.100 589-43-5 2,4-Dimethylhexane 1.521 1.571 1.297 371.133

68.121 565-75-3 2,3,4-Trimethylpentane 6.067 6.103 5.175 1480.332

68.800 560-21-4 2,3,3-Trimethylpentane 6.862 6.835 5.853 1674.338

70.438 584-94-1 2,3-Dimethylhexane 1.675 1.701 1.428 408.602

71.699 592-27-8 2-Methylheptane 0.086 0.089 0.073 21.022

71.965 589-53-7 4-Methylheptane 0.184 0.189 0.157 44.962

73.022 589-81-1 3-Methylheptane 0.075 0.077 0.064 18.404

74.944 3522-94-9 2,2,5-Trimethylhexane 3.375 3.451 2.563 825.027

80.057 1069-53-0 2,3,5-Trimethylhexane 0.534 0.535 0.405 130.490

81.233 1071-26-7 2,4-Dimethylheptane 0.077 0.078 0.058 18.744

82.195 1072-05-5 2,6-Dimethylheptane 0.097 0.099 0.073 23.610

83.129 2,5-Dimethylheptane 0.255 0.257 0.193 62.228

87.147 3221-61-2 2-Methyloctane 0.017 0.017 0.013 4.036

88.012 2216-33-3 3-Methyloctane 0.010 0.010 0.008 2.537

89.068 C10 - IsoParaffin - 1 0.562 0.559 0.385 137.798

89.91414720-74-2 2,2,4-trimethylheptane 0.387 0.385 0.265 94.884

93.135 C10-isoparaffin-x 0.000 0.000 0.000 1.660

93.82515869-87-1 2,2-Dimethyloctane 0.073 0.073 0.050 17.793

94.62315869-89-3 2,5-Dimethyloctane 0.112 0.111 0.076 27.337

95.101 2040-95-1 2,7-Dimethyloctane 0.054 0.053 0.037 13.127

95.266 2051-30-1 2,4-Dimethyloctane 0.242 0.241 0.166 59.312

95.660 2,6-Dimethyloctane 0.071 0.070 0.048 17.322

98.902 2,2,6-Trimethyloctane 3.607 3.591 2.470 883.576

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C-32
Hydrocarbon Expert V4.7 Wed Aug 25 17:08:36 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91309 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91309

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

I-Paraffins 99.663 5911-04-6 3-Methylnonane 0.016 0.015 0.011 3.801

100.481 C11-Isoparaffin-2 0.306 0.298 0.191 75.057

102.11117302-01-1 3-Ethyl-3-methylheptane 0.487 0.474 0.304 119.460

104.192 C11 Isoparaffin-4 0.057 0.056 0.036 14.100

105.059 C11-Isoparaffin-5 0.028 0.027 0.017 6.878

106.154 C11-Isoparaffin-7 0.582 0.566 0.363 142.769

108.369 C11- Isoparaffin-11 0.925 0.899 0.576 226.780

112.965 C12 - IsoParaffin - 1 0.028 0.028 0.016 6.984

116.093 C12 - IsoParaffin - 4 0.016 0.016 0.009 4.203

Aromatics

Mono-Aromatics 45.137 71-42-3 Benzene 0.663 0.545 0.827 177.372

68.628 108-88-3 Toluene 5.145 4.293 5.441 1361.918

84.439 100-41-4 Ethylbenzene 1.009 0.842 0.926 265.092

85.666 108-38-3 m-Xylene 2.374 1.987 2.178 623.536

85.815 106-42-3 p-Xylene 1.112 0.934 1.021 292.195

88.650 95-47-6 o-Xylene 0.836 0.687 0.768 219.714

92.837 98-82-8 i-Propylbenzene 0.033 0.028 0.027 8.711

96.304 103-65-1 n-Propylbenzene 0.268 0.225 0.217 69.964

97.153 620-14-4 1-Methyl-3-ethylbenzene 0.940 0.787 0.762 245.384

97.387 622-96-8 1-Methyl-4-ethylbenzene 0.442 0.371 0.358 115.423

98.013 108-67-8 1,3,5-Trimethylbenzene 0.652 0.545 0.528 170.112

99.099 611-14-3 1-Methyl-2-ethylbenzene 0.359 0.295 0.291 93.606

100.737 95-63-6 1,2,4-Trimethylbenzene 1.933 1.597 1.567 504.588

102.465 538-93-2 i-Butylbenzene 0.341 0.289 0.248 88.576

103.614 526-73-8 1,2,3-Trimethylbenzene 0.349 0.282 0.283 91.056

103.978 535-77-3 1-Methyl-3-i-propylbenzene 0.040 0.033 0.029 10.293

106.335 141-93-5 1,3-Diethylbenzene 0.049 0.041 0.036 12.828

106.634 1074-43-7 1-Methyl-3-n-propylbenzene 1.607 1.350 1.167 417.204

106.905 105-05-5 1,4-Diethylbenzene 0.459 0.385 0.333 119.254

107.176 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.136 0.112 0.099 35.293

107.423 135-01-3 1,2-Diethylbenzene 0.128 0.105 0.093 33.253

108.026 1074-17-5 1-Methyl-2-n-propylbenzene 0.056 0.046 0.041 14.536

109.544 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.368 0.304 0.267 95.474

110.102 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.781 0.634 0.567 202.650

111.215 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.083 0.067 0.060 21.476

111.688 4218-48-8 1-Ethyl-4-i-propylbenzene 0.106 0.086 0.070 27.365

112.163 1,2,4,5-Tetramethylbenzene 0.264 0.215 0.192 68.534

112.429 527-53-7 1,2,3,5-Tetramethylbenzene 0.348 0.283 0.253 90.340

113.901 1,2-Di-i-propylbenzene 0.048 0.039 0.029 12.271

114.117 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.064 0.052 0.042 16.605

114.290 C11 - Aromatic - 4 0.040 0.033 0.027 10.448

115.090 538-68-1 n-Pentylbenzene 0.016 0.013 0.011 4.160

115.320 tert-Pentylbenzene 0.059 0.048 0.039 15.326

115.632 577-55-9 1-Methyl-2-n-butylbenzene 0.029 0.024 0.019 7.604

115.744 C11 - Aromatic - 7 0.040 0.034 0.026 10.364

116.205 100-18-5 1,4-Di-i-propylbenzene 0.054 0.044 0.032 13.846

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C-33
Hydrocarbon Expert V4.7 Wed Aug 25 17:08:36 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91309 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91309

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 117.431 7364-19-4 1t-Butyl-4-ethylbenzene 0.010 0.008 0.006 2.680

117.734 1,3-Di-n-propylbenzene 0.038 0.031 0.023 9.758

117.847 C11 - Aromatic - 11 0.019 0.017 0.013 5.024

118.402 C11 - Aromatic - 12 0.014 0.012 0.009 3.732

122.541 877-44-1 1,2,4-Triethylbenzene 0.008 0.007 0.005 2.176

Naphthalenes 116.636 91-20-3 Naphthalene 0.104 0.073 0.079 28.146

123.280 91-57-6 2-Methylnaphthalene 0.015 0.011 0.010 4.101

124.146 90-12-0 1-Methylnaphthalene 0.007 0.005 0.005 1.903

Naphtheno/Olefino-Benzs 113.760 874-35-1 5-Methylindan 0.108 0.087 0.079 27.938

114.765 824-63-5 2-Methylindan 0.108 0.088 0.080 28.076

Indenes 104.803 Indan 0.214 0.161 0.176 56.785

105.440 Indene 1.607 1.206 1.325 426.325

109.205 2-Methylindan 0.146 0.110 0.108 38.783

114.513 824-22-6 4-Methylindan 0.137 0.111 0.101 35.591

116.796 4,7-Dimethyl Indane 0.022 0.017 0.015 5.944

117.079 1,1-Dimethyl Indane 0.013 0.009 0.008 3.327

117.248 Dimethyl Indane - 1 0.005 0.004 0.004 1.448

Naphthenes

Mono-Naphthenes 27.103 287-92-3 Cyclopentane 0.109 0.105 0.151 26.962

40.153 96-37-7 Methylcyclopentane 0.816 0.788 0.944 202.724

47.051 110-82-7 Cyclohexane 0.076 0.071 0.088 18.902

52.885 1759-58-6 1t,3-Dimethylcyclopentane 0.067 0.065 0.066 16.641

53.472 2532-58-3 1c,3-Dimethylcyclopentane 0.043 0.042 0.043 10.746

54.101 822-50-4 1t,2-Dimethylcyclopentane 0.033 0.031 0.032 8.102

61.052 108-87-2 Methylcyclohexane 0.028 0.026 0.027 6.859

75.910 3875-51-2 i-Propylcyclopentane 0.032 0.030 0.028 7.902

92.087 4926-90-3 1,1-Methylethylcyclohexane 0.025 0.022 0.019 6.224

93.135 696-29-7 1-Methyl-2-propyl-cyclopentan 0.007 0.006 0.005 1.660

101.323 1678-98-4 i-Butylcyclohexane 0.051 0.046 0.035 12.644

105.857 n-ButylCyclohexane 0.002 0.002 0.001 0.534

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.406 115-11-7 Isobutene 0.024 0.029 0.041 5.882

9.445 106-98-9 Butene-1 0.028 0.034 0.049 6.958

10.269 624-64-6 t-Butene-2 0.103 0.123 0.178 25.477

10.990 590-18-1 c-Butene-2 0.115 0.134 0.201 28.695

16.335 109-67-1 Pentene-1 0.361 0.408 0.501 89.699

18.805 646-04-8 t-Pentene-2 0.930 1.038 1.292 231.167

19.822 627-20-3 c-Pentene-2 0.509 0.561 0.707 126.428

32.942 592-41-6 Hexene-1 0.170 0.181 0.196 42.151

35.93613269-52-8 t-Hexene-3 0.284 0.302 0.329 70.681

36.412 4050-45-7 t-Hexene-2 0.539 0.571 0.624 133.884

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C-34
Hydrocarbon Expert V4.7 Wed Aug 25 17:08:36 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91309 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91309

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

n-Olefins 38.242 7688-21-3 c-Hexene-2 0.229 0.239 0.265 56.822

56.88314686-14-7 t-Heptene-3 0.017 0.018 0.017 4.325

110.729 693-61-8 2-Undecene, (E)- 0.071 0.069 0.049 17.406

Iso-Olefins 13.132 563-45-1 3-Methylbutene-1 0.079 0.091 0.109 19.531

17.174 563-46-2 2-Methylbutene-1 0.565 0.628 0.785 140.345

20.493 513-35-9 2-Methylbutene-2 1.164 1.271 1.617 289.185

28.696 691-38-3 4-Methyl-c-pentene-2 0.049 0.053 0.057 12.274

29.342 674-76-0 4-Methyl-t-pentene-2 0.146 0.157 0.169 36.318

32.719 763-29-1 2-Methylpentene-1 0.248 0.262 0.287 61.701

35.133 760-21-4 2-Ethylbutene-1 0.076 0.079 0.088 18.784

36.904 625-27-4 2-Methylpentene-2 0.378 0.396 0.438 94.017

37.312 922-62-3 3-Methyl-c-pentene-2 0.289 0.299 0.335 71.804

39.582 3404-73-7 3,3-Dimethylpentene-1 0.343 0.354 0.340 85.254

42.041 594-56-9 2,3,3-Trimethylbutene-1 0.012 0.012 0.012 2.989

46.159 3404-61-3 3-Methylhexene-1 0.013 0.014 0.013 3.327

46.743 3524-73-0 5-Methylhexene-1 0.022 0.023 0.022 5.581

48.80615840-60-5 2-Methyl-c-hexene-3 0.033 0.035 0.033 8.287

49.798 3404-55-5 4-Methyl-t/c-hexene-2 0.039 0.040 0.038 9.604

57.235 6094-02-6 2-Methylhexene-1 0.027 0.028 0.027 6.823

58.114 2738-19-4 2-Methyl-2-hexene 0.005 0.005 0.005 1.315

86.220 C9-IsoOlefin-3 0.017 0.016 0.013 4.207

93.135 C10-IsoOlefin-4 0.007 0.007 0.005 1.660

Naphtheno-Olefins 25.253 142-29-0 Cyclopentene 0.202 0.189 0.289 51.612

45.337 693-89-0 1-Methylcyclopentene 0.352 0.327 0.418 89.681

50.670 110-83-8 Cyclohexene 0.037 0.033 0.044 9.213

Di-Olefins 18.213 78-79-5 2-Methyl-1,3-Butadiene 0.010 0.010 0.014 2.525

20.830 2004-70-8 1t,3-Pentadiene 0.014 0.015 0.020 3.628

Oxygenates 26.495 71-23-8 n-Propanol 0.198 0.179 0.321 34.490

Unidentified 19.439 Unidentified 0.006 0.007 0.009 1.943

28.236 Unidentified 0.056 0.055 0.062 17.185

44.929 Unidentified 0.011 0.011 0.013 3.443

47.587 Unidentified 0.030 0.031 0.030 9.268

72.096 Unidentified 0.138 0.138 0.117 41.908

78.507 Unidentified 0.078 0.076 0.059 23.702

84.617 Unidentified 0.035 0.035 0.028 10.715

84.858 Unidentified 0.029 0.027 0.022 8.815

85.963 Unidentified 0.081 0.081 0.062 24.719

86.328 Unidentified 0.014 0.014 0.011 4.378

88.480 Unidentified 0.162 0.171 0.125 49.219

93.027 Unidentified 0.017 0.016 0.013 5.298

93.027 Unidentified 0.017 0.018 0.012 5.298

93.027 Unidentified 0.017 0.013 0.012 5.298

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C-35
Hydrocarbon Expert V4.7 Wed Aug 25 17:08:36 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91309 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91309

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Unidentified 93.602 Unidentified 0.213 0.212 0.146 64.761

94.267 Unidentified 0.023 0.017 2.266 7.078

94.267 Unidentified 0.023 0.024 0.016 7.078

99.472 Unidentified 0.011 0.011 0.008 3.397

99.839 Unidentified 0.011 0.011 0.007 3.261

100.129 Unidentified 0.214 0.155 0.134 65.229

100.256 Unidentified 0.571 0.555 0.356 173.820

100.945 Unidentified 0.352 0.363 0.244 107.019

101.066 Unidentified 0.208 0.206 0.143 63.457

101.966 Unidentified 0.020 0.018 0.014 6.013

102.324 Unidentified 0.139 0.118 0.101 42.320

102.976 Unidentified 0.131 0.128 0.082 39.935

103.468 Unidentified 0.016 0.013 0.013 4.772

104.397 Unidentified 0.280 0.236 0.203 85.224

105.994 Unidentified 0.013 0.012 0.009 3.965

107.889 Unidentified 0.133 0.130 0.083 40.617

108.164 Unidentified 0.132 0.129 0.083 40.238

108.245 Unidentified 0.123 0.120 0.077 37.475

108.552 Unidentified 0.302 0.293 0.188 91.811

108.984 Unidentified 0.905 0.746 0.657 275.522

109.703 Unidentified 0.063 0.047 0.046 19.169

110.528 Unidentified 0.031 0.028 0.020 9.567

110.859 Unidentified 0.148 0.145 0.103 45.088

111.132 Unidentified 0.130 0.110 0.085 39.466

111.798 Unidentified 0.074 0.060 0.048 22.449

112.653 Unidentified 0.013 0.011 0.009 4.083

112.784 Unidentified 0.022 0.018 0.016 6.611

113.296 Unidentified 0.036 0.036 0.022 11.096

113.447 Unidentified 0.014 0.014 0.008 4.326

113.654 Unidentified 0.071 0.058 0.047 21.743

114.683 Unidentified 0.031 0.025 0.020 9.474

114.978 Unidentified 0.014 0.011 0.009 4.236

116.972 Unidentified 0.007 0.006 0.004 2.091

126.171 Unidentified 0.009 0.008 0.006 2.827

126.171 Unidentified 0.009 0.008 0.005 2.827

126.171 Unidentified 0.009 0.009 0.005 2.827

127.135 Unidentified 0.003 0.003 0.001 0.914

Plus

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C-36
Hydrocarbon Expert V4.7 Wed Aug 25 17:08:36 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91309 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91309

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF

20.0 15.0 10.0 5.0 0.0

Propane

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

Unidentified

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

2,2-Dimethylbutane

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C-37
Hydrocarbon Expert V4.7 Wed Aug 25 17:08:36 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91309 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91309

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

n-Propanol

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

2-Ethylbutene-1 n-Hexane

t-Hexene-3

t-Hexene-2

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane 2,3,3-Trimethylbutene-1 2,2,3-Trimethylbutane

Unidentified Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1 Cyclohexane

Unidentified

2-Methyl-c-hexene-3

4-Methyl-t/c-hexene-2

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C-38
Hydrocarbon Expert V4.7 Wed Aug 25 17:08:36 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91309 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91309

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF

70.0 65.0 60.0 55.0 50.0

2-Methylhexane

Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane

2,2,4-Trimethylpentane

t-Heptene-3

2-Methylhexene-1

n-Heptane

2-Methyl-2-hexene

Methylcyclohexane

2,2,3-Trimethylpentane 2,5-Dimethylhexane

2,4-Dimethylhexane

2,3,4-Trimethylpentane

Toluene 2,3,3-Trimethylpentane

2,3-Dimethylhexane

2-Methylheptane

Unidentified 4-Methylheptane

3-Methylheptane

2,2,5-Trimethylhexane

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C-39
Hydrocarbon Expert V4.7 Wed Aug 25 17:08:36 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91309 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91309

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF

95.0 90.0 85.0 80.0 75.0

i-Propylcyclopentane

n-Octane

Unidentified

2,3,5-Trimethylhexane

2,4-Dimethylheptane

2,6-Dimethylheptane

2,5-Dimethylheptane

Ethylbenzene Unidentified

m-Xylene Unidentified p-Xylene

C9-IsoOlefin-3 Unidentified

2-Methyloctane

3-Methyloctane

Unidentified o-Xylene

C10 - IsoParaffin - 1

2,2,4-trimethylheptane

n-Nonane

1,1-Methylethylcyclohexane

i-Propylbenzene 1-Methyl-2-propyl-cyclopentan/C10-IsoOlefin-4/C10-isoparaffin-x Unidentified

Unidentified 2,2-Dimethyloctane

Unidentified

2,5-Dimethyloctane

2,7-Dimethyloctane 2,4-Dimethyloctane

2,6-Dimethyloctane

n-Propylbenzene

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

2,2,6-Trimethyloctane 1-Methyl-2-ethylbenzene

Unidentified 3-Methylnonane Unidentified

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C-40
Hydrocarbon Expert V4.7 Wed Aug 25 17:08:36 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91309 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91309

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified Unidentified C11-Isoparaffin-2 1,2,4-Trimethylbenzene

Unidentified Unidentified

i-Butylcyclohexane

Unidentified 3-Ethyl-3-methylheptane Unidentified i-Butylbenzene n-Decane Unidentified

Unidentified 1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene C11 Isoparaffin-4 Unidentified

Indan C11-Isoparaffin-5

Indene

n-ButylCyclohexane Unidentified C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene 1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

Unidentified 1-Methyl-2-n-propylbenzene Unidentified C11- Isoparaffin-11 Unidentified

Unidentified 2-Methylindan

1,2-Dimethyl-4-ethylbenzene Unidentified

1,3-Dimethyl-2-ethylbenzene

Unidentified 2-Undecene, (E)- Unidentified

1,2-Dimethyl-3-ethylbenzene Unidentified

n-Undecane Unidentified 1-Ethyl-4-i-propylbenzene

1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene Unidentified C12 - IsoParaffin - 1

Unidentified

5-Methylindan 1,2-Di-i-propylbenzene 1-methyl-4-(1-methylpropyl)be C11 - Aromatic - 4 4-Methylindan Unidentified 2-Methylindan

n-Pentylbenzene Unidentified

tert-Pentylbenzene 1-Methyl-2-n-butylbenzene C11 - Aromatic - 7

C12 - IsoParaffin - 4 1,4-Di-i-propylbenzene

Naphthalene 4,7-Dimethyl Indane Unidentified 1,1-Dimethyl Indane Dimethyl Indane - 1 1t-Butyl-4-ethylbenzene

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

C11 - Aromatic - 12

1,2,4-Triethylbenzene

2-Methylnaphthalene

1-Methylnaphthalene

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C-41
Hydrocarbon Expert V4.7 Wed Aug 25 17:08:36 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91309 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91309

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000005.D\SIG1000005_FID1_A.CDF

145.0 140.0 135.0 130.0 125.0

Unidentified

Unidentified

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C-42
Hydrocarbon Expert V4.7 Thu Aug 26 08:04:00 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91310 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91310

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 6.743 7.618 7.467

I-Paraffins 49.355 52.034 42.026

Aromatics 19.783 16.589 16.677

Mono-Aromatics 18.793 15.822 15.960

Naphthalenes 0.134 0.096 0.093

Naphtheno/Olefino-Benzs 0.206 0.170 0.141

Indenes 0.651 0.501 0.482

Naphthenes 4.785 4.592 4.780

Mono-Naphthenes 4.785 4.592 4.780

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 7.333 7.945 8.650

n-Olefins 3.109 3.443 3.769

Iso-Olefins 3.589 3.901 4.131

Naphtheno-Olefins 0.609 0.572 0.716

Di-Olefins 0.026 0.028 0.034

Oxygenates 9.533 8.844 18.680

Unidentified 2.468 2.378 1.721

Plus 0.000 0.000 0.000

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C-43
Hydrocarbon Expert V4.7 Thu Aug 26 08:04:00 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91310 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91310

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C2 9.432 8.752 18.528

C3 0.107 0.102 0.165

C4 1.351 1.699 2.113

C5 9.206 10.589 11.695

C6 13.831 14.626 14.743

C7 11.550 11.013 10.889

C8 36.105 36.126 28.945

C9 10.410 9.818 7.570

C10 4.474 3.918 3.004

C11 0.924 0.858 0.547

C12 0.143 0.120 0.080

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C-44
Hydrocarbon Expert V4.7 Thu Aug 26 08:04:00 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91310 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91310

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C3 0.006 0.009 0.013

C4 1.108 1.402 1.725

C5 1.166 1.364 1.463

C6 2.728 3.029 2.865

C7 0.689 0.738 0.623

C8 0.546 0.569 0.433

C9 0.427 0.435 0.301

C10 0.040 0.040 0.025

C11 0.032 0.032 0.019

I-Paraffins C4 0.053 0.070 0.083

C5 4.200 4.964 5.268

C6 5.287 5.878 5.552

C7 3.274 3.532 2.957

C8 29.426 30.317 23.314

C9 5.226 5.388 3.688

C10 1.322 1.328 0.837

C11 0.550 0.542 0.319

C12 0.016 0.015 0.008

Mono-Aromatics C6 0.735 0.612 0.852

C7 5.234 4.420 5.141

C8 5.547 4.686 4.728

C9 4.640 3.902 3.494

C10 2.229 1.863 1.503

C11 0.285 0.237 0.174

C12 0.123 0.101 0.069

Naphthalenes C10 0.116 0.083 0.082

C11 0.017 0.012 0.011

Naphtheno/Olefino-Benzs C10 0.206 0.170 0.141

Indenes C9 0.076 0.058 0.058

C10 0.559 0.432 0.414

C11 0.011 0.008 0.007

C12 0.004 0.003 0.003

Mono-Naphthenes C5 0.144 0.141 0.185

C6 2.508 2.414 2.697

C7 1.562 1.500 1.440

C8 0.531 0.502 0.429

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C-45
Hydrocarbon Expert V4.7 Thu Aug 26 08:04:00 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91310 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91310

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Mono-Naphthenes C9 0.041 0.035 0.029

n-Olefins C4 0.189 0.227 0.305

C5 1.637 1.847 2.112

C6 1.150 1.231 1.236

C7 0.105 0.110 0.097

C11 0.028 0.028 0.018

Iso-Olefins C5 1.837 2.059 2.370

C6 1.010 1.074 1.086

C7 0.685 0.714 0.632

C8 0.054 0.051 0.042

C10 0.002 0.003 0.002

Naphtheno-Olefins C5 0.197 0.187 0.262

C6 0.412 0.386 0.454

Di-Olefins C5 0.026 0.028 0.034

Oxygenates C2 9.432 8.752 18.528

C3 0.101 0.092 0.152

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C-46
Hydrocarbon Expert V4.7 Thu Aug 26 08:04:00 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91310 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91310

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 24.50 23.49

5% 81.26 80.63

10% 100.96 97.18

15% 144.13 138.61

20% 155.27 153.92

25% 172.43 160.63

30% 173.01 172.73

35% 177.16 175.13

40% 209.25 197.28

45% 210.21 209.76

50% 228.59 212.40

55% 230.95 230.77

60% 234.81 234.05

65% 236.63 235.98

70% 238.01 237.44

75% 243.86 239.11

80% 258.64 254.81

85% 281.77 279.29

90% 320.83 317.38

95% 352.12 336.85

FBP 402.72 389.41

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C-47
Hydrocarbon Expert V4.7 Thu Aug 26 08:04:00 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91310 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91310

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 7.391 74-98-6 P3 Propane 0.006 0.009 0.013 1.698

2 8.613 75-28-5 I4 i-Butane 0.053 0.070 0.083 14.393

3 9.405 115-11-7 K4 Isobutene 0.015 0.019 0.024 4.238

4 9.444 106-98-9 K4 Butene-1 0.018 0.022 0.029 5.067

5 9.793 106-97-8 P4 n-Butane 1.108 1.402 1.725 299.818

6 10.267 624-64-6 K4 t-Butene-2 0.071 0.087 0.115 20.025

7 10.390 463-82-1 I5 2,2-Dimethylpropane 0.013 0.016 0.016 3.416

8 10.989 590-18-1 K4 c-Butene-2 0.085 0.100 0.136 23.705

9 12.753 64-17-5 X2 Ethanol 9.432 8.752 18.528 1136.062

10 13.128 563-45-1 C5 3-Methylbutene-1 0.297 0.346 0.383 83.131

11 14.713 78-78-4 I5 i-Pentane 4.188 4.948 5.253 1140.912

12 16.337 109-67-1 K5 Pentene-1 0.331 0.379 0.428 92.873

13 17.165 563-46-2 C5 2-Methylbutene-1 0.503 0.567 0.650 141.068

14 17.696 109-66-0 P5 n-Pentane 1.166 1.364 1.463 317.807

15 18.208 78-79-5 E5 2-Methyl-1,3-Butadiene 0.010 0.011 0.014 2.994

16 18.798 646-04-8 K5 t-Pentene-2 0.843 0.952 1.088 236.251

17 19.439 ? Unidentified 0.006 0.006 0.007 1.936

18 19.822 627-20-3 K5 c-Pentene-2 0.462 0.516 0.597 129.552

19 20.490 513-35-9 C5 2-Methylbutene-2 1.037 1.146 1.338 290.485

20 20.818 2004-70-8 E5 1t,3-Pentadiene 0.015 0.016 0.020 4.373

21 22.071 ? Unidentified 0.006 0.006 0.008 2.041

22 22.623 75-83-2 I6 2,2-Dimethylbutane 0.077 0.087 0.081 20.997

23 25.249 142-29-0 B5 Cyclopentene 0.197 0.187 0.262 56.828

24 26.430 ? Unidentified 0.045 0.041 0.068 15.395

25 26.504 71-23-8 X3 n-Propanol 0.101 0.092 0.152 19.798

26 27.099 287-92-3 M5 Cyclopentane 0.144 0.141 0.185 40.242

27 27.833 79-29-8 I6 2,3-Dimethylbutane 1.138 1.259 1.195 311.211

28 28.228 ? Unidentified 0.051 0.050 0.052 17.407

29 28.696 691-38-3 C6 4-Methyl-c-pentene-2 0.045 0.048 0.048 12.494

30 28.904 107-83-5 I6 2-Methylpentane 2.321 2.602 2.438 635.007

31 29.339 674-76-0 C6 4-Methyl-t-pentene-2 0.131 0.142 0.141 36.738

32 31.547 96-14-0 I6 3-Methylpentane 1.751 1.930 1.839 478.997

33 32.718 763-29-1 C6 2-Methylpentene-1 0.225 0.240 0.242 63.033

34 32.942 592-41-6 K6 Hexene-1 0.161 0.174 0.174 45.242

35 35.303 110-54-3 P6 n-Hexane 2.728 3.029 2.865 746.276

36 35.94213269-52-8 K6 t-Hexene-3 0.265 0.284 0.285 74.235

37 36.410 4050-45-7 K6 t-Hexene-2 0.508 0.545 0.546 142.292

38 36.900 625-27-4 C6 2-Methylpentene-2 0.344 0.364 0.370 96.344

39 37.313 922-62-3 C6 3-Methyl-c-pentene-2 0.266 0.279 0.286 74.498

40 38.237 7688-21-3 K6 c-Hexene-2 0.216 0.228 0.232 60.446

41 39.588 3404-73-7 C7 3,3-Dimethylpentene-1 0.315 0.329 0.291 88.376

42 40.162 96-37-7 M6 Methylcyclopentane 1.490 1.457 1.602 417.419

43 41.732 108-08-7 I7 2,4-Dimethylpentane 0.971 1.056 0.877 266.530

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C-48
Hydrocarbon Expert V4.7 Thu Aug 26 08:04:00 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91310 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91310

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 42.034 594-56-9 C7 2,3,3-Trimethylbutene-1 0.014 0.015 0.013 3.988

45 42.276 464-06-2 I7 2,2,3-Trimethylbutane 0.076 0.080 0.068 20.786

46 44.931 ? Unidentified 0.012 0.011 0.013 4.044

47 45.137 71-42-3 Q6 Benzene 0.735 0.612 0.852 221.834

48 45.336 693-89-0 B6 1-Methylcyclopentene 0.367 0.345 0.405 105.417

49 46.159 3404-61-3 C7 3-Methylhexene-1 0.016 0.016 0.014 4.391

50 46.742 3524-73-0 C7 5-Methylhexene-1 0.065 0.068 0.060 18.261

51 47.057 110-82-7 M6 Cyclohexane 1.018 0.958 1.095 285.348

52 47.596 ? Unidentified 0.035 0.036 0.032 11.890

53 48.80515840-60-5 C7 2-Methyl-c-hexene-3 0.041 0.044 0.038 11.564

54 49.146 3769-23-1 C7 4-Methylhexene-1 0.010 0.011 0.009 2.855

55 49.797 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.051 0.053 0.047 14.405

56 50.197 591-76-4 I7 2-Methylhexane 1.566 1.690 1.414 430.088

57 50.669 110-83-8 B6 Cyclohexene 0.045 0.041 0.050 12.602

58 52.028 589-34-4 I7 3-Methylhexane 0.662 0.706 0.598 181.839

59 52.882 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.170 0.166 0.156 47.503

60 53.470 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.131 0.129 0.121 36.786

61 54.094 822-50-4 M7 1t,2-Dimethylcyclopentane 0.187 0.183 0.173 52.531

62 54.429 C7 C7 - Iso-Olefin - 2 0.022 0.022 0.020 6.183

63 54.738 540-84-1 I8 2,2,4-Trimethylpentane 7.470 7.905 5.918 2055.609

64 55.028 592-76-7 K7 Heptene-1 0.030 0.031 0.028 8.377

65 56.359 4914-89-0 C7 3-Methyl-c-hexene-3 0.014 0.015 0.013 4.021

66 56.88014686-14-7 K7 t-Heptene-3 0.033 0.035 0.031 9.287

67 57.242 6094-02-6 C7 2-Methylhexene-1 0.059 0.062 0.054 16.551

68 57.617 142-82-5 P7 n-Heptane 0.689 0.738 0.623 189.290

69 57.834 7642-10-6 K7 c-Heptene-3 0.025 0.026 0.023 7.035

70 58.113 2738-19-4 C7 2-Methyl-2-hexene 0.027 0.028 0.025 7.601

71 58.359 3899-36-3 C7 3-Methyl-t-hexene-3 0.021 0.022 0.019 5.773

72 58.74214686-13-6 K7 t-Heptene-2 0.017 0.018 0.016 4.727

73 59.20216491-15-9 M7 Cyclopentene, 1,5-dimethyl- 0.018 0.018 0.017 5.174

74 59.64420710-38-8 C7 3-Methyl-t-hexene-2 0.015 0.016 0.014 4.294

75 60.429 4914-91-4 C7 2-Pentene, 3,4-dimethyl-, (Z)- 0.014 0.014 0.013 3.812

76 61.062 108-87-2 M7 Methylcyclohexane 1.017 0.968 0.937 284.936

77 62.012 4516-69-2 M8 1,1,3-Trimethylcyclopentane 0.030 0.030 0.025 8.543

78 62.418 590-73-8 I8 2,2-Dimethylhexane 0.030 0.031 0.023 8.132

79 63.857 1640-89-7 M7 Ethylcyclopentane 0.038 0.037 0.035 10.744

80 64.513 564-02-3 I8 2,2,3-Trimethylpentane 0.749 0.766 0.593 206.023

81 64.760 592-13-2 I8 2,5-Dimethylhexane 1.519 1.604 1.204 418.070

82 65.100 589-43-5 I8 2,4-Dimethylhexane 1.433 1.498 1.135 394.285

83 65.930 4850-28-6 M8 1c,2t,4-Trimethylcyclopentane 0.031 0.030 0.025 8.692

84 66.331 563-16-6 I8 3,3-Dimethylhexane 0.021 0.022 0.017 5.883

85 67.46115890-40-1 M8 1t,2c,3-Trimethylcyclopentane 0.028 0.026 0.022 7.727

86 68.135 565-75-3 I8 2,3,4-Trimethylpentane 6.895 7.022 5.463 1897.493

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C-49
Hydrocarbon Expert V4.7 Thu Aug 26 08:04:00 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91310 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91310

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 68.637 108-88-3 Q7 Toluene 5.234 4.420 5.141 1562.352

88 68.821 560-21-4 I8 2,3,3-Trimethylpentane 8.453 8.522 6.697 2326.163

89 70.134 C8 C8 - Diolefin - 1 0.012 0.011 0.010 3.324

90 70.441 584-94-1 I8 2,3-Dimethylhexane 1.889 1.942 1.497 519.797

91 71.701 592-27-8 I8 2-Methylheptane 0.303 0.318 0.240 83.514

92 71.961 589-53-7 I8 4-Methylheptane 0.284 0.295 0.225 78.043

93 72.096 ? Unidentified 0.158 0.161 0.126 54.383

94 72.864 M8 1,3-dimethyl-t-cyclohexane 0.181 0.172 0.146 50.735

95 73.023 589-81-1 I8 3-Methylheptane 0.263 0.273 0.208 72.292

96 73.207 619-99-8 I8 3-Ethylhexane 0.117 0.120 0.093 32.285

97 74.103 ? Unidentified 0.030 0.028 0.024 10.196

98 74.950 3522-94-9 I9 2,2,5-Trimethylhexane 3.735 3.866 2.635 1029.771

99 75.272 M8 3c-Ethylmethylcyclopentane 0.011 0.010 0.009 3.060

100 75.495 M8 3t-Ethylmethylcyclopentane 0.015 0.014 0.012 4.182

101 75.910 ? Unidentified 0.029 0.027 0.023 9.886

102 76.198 2207-03-6 M8 1t,3-Dimethylcyclohexane 0.084 0.079 0.068 23.559

103 77.567 111-65-9 P8 n-Octane 0.546 0.569 0.433 150.328

104 78.509 ? Unidentified 0.094 0.093 0.066 32.143

105 80.057 1069-53-0 I9 2,3,5-Trimethylhexane 0.619 0.628 0.437 170.654

106 80.618 C8 C9 - IsoOlefin - 1 0.019 0.018 0.015 5.247

107 81.055 2207-01-4 M8 1c,2-Dimethylcyclohexane 0.016 0.015 0.013 4.451

108 81.233 1071-26-7 I9 2,4-Dimethylheptane 0.113 0.117 0.080 31.196

109 81.869 1678-91-7 M8 Ethylcyclohexane 0.126 0.118 0.101 35.261

110 82.195 1072-05-5 I9 2,6-Dimethylheptane 0.163 0.168 0.115 44.810

111 82.674 ? Unidentified 0.030 0.032 0.021 10.181

112 83.130 I9 2,5-Dimethylheptane 0.340 0.348 0.240 93.846

113 83.300 926-82-9 I9 3,5-Dimethylheptane 0.034 0.034 0.024 9.290

114 84.440 100-41-4 Q8 Ethylbenzene 0.964 0.814 0.821 285.467

115 84.620 ? Unidentified 0.048 0.048 0.035 16.327

116 84.859 ? Unidentified 0.049 0.046 0.035 16.930

117 85.671 108-38-3 Q8 m-Xylene 2.568 2.175 2.189 760.710

118 85.818 106-42-3 Q8 p-Xylene 1.135 0.965 0.967 336.205

119 85.965 ? Unidentified 0.127 0.128 0.089 43.485

120 86.221 C8 C9-IsoOlefin-3 0.024 0.022 0.017 6.657

121 86.328 ? Unidentified 0.022 0.023 0.016 7.717

122 86.618 1067-20-5 I9 3,3-Diethylpentane 0.004 0.004 0.003 1.197

123 87.015 2216-34-4 I9 4-Methyloctane 0.057 0.058 0.040 15.625

124 87.148 3221-61-2 I9 2-Methyloctane 0.076 0.078 0.054 21.082

125 87.85015869-80-4 I9 Heptane, 3-ethyl- 0.010 0.010 0.007 2.791

126 88.013 2216-33-3 I9 3-Methyloctane 0.075 0.076 0.053 20.696

127 88.480 ? Unidentified 0.205 0.220 0.147 70.483

128 88.652 95-47-6 Q8 o-Xylene 0.880 0.732 0.750 260.821

129 89.068 I10 C10 - IsoParaffin - 1 0.665 0.669 0.423 183.644

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C-50
Hydrocarbon Expert V4.7 Thu Aug 26 08:04:00 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91310 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91310

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 89.488 3728-57-2 M8 Cyclopentane, 1-methyl-2-propyl- 0.009 0.008 0.008 2.811

131 89.643 M9 trans-1,3-Diethylcyclopentane 0.022 0.018 0.016 6.570

132 89.91514720-74-2 I10 2,2,4-trimethylheptane 0.469 0.472 0.298 129.541

133 91.476 111-84-2 P9 n-Nonane 0.427 0.435 0.301 117.650

134 92.053 4926-90-3 M9 1,1-Methylethylcyclohexane 0.016 0.015 0.012 4.528

135 92.837 98-82-8 Q9 i-Propylbenzene 0.032 0.027 0.024 9.385

136 93.028 ? Unidentified 0.008 0.008 0.006 2.747

137 93.028 ? Unidentified 0.008 0.008 0.005 2.747

138 93.028 ? Unidentified 0.008 0.006 0.005 2.747

139 93.139 696-29-7 M9 1-Methyl-2-propyl-cyclopentan 0.002 0.002 0.002 0.683

140 93.139 C10 C10-IsoOlefin-4 0.002 0.003 0.002 0.683

141 93.139 I10 C10-isoparaffin-x 0.000 0.000 0.000 0.683

142 93.600 ? Unidentified 0.085 0.086 0.054 29.069

143 93.82415869-87-1 I10 2,2-Dimethyloctane 0.030 0.030 0.019 8.266

144 94.63015869-89-3 I10 2,5-Dimethyloctane 0.017 0.017 0.011 4.671

145 94.814 I10 C10 - IsoParaffin - 2 0.010 0.010 0.006 2.692

146 95.265 2051-30-1 I10 2,4-Dimethyloctane 0.025 0.026 0.016 7.002

147 95.660 I10 2,6-Dimethyloctane 0.013 0.013 0.008 3.658

148 96.305 103-65-1 Q9 n-Propylbenzene 0.275 0.233 0.207 80.905

149 97.155 620-14-4 Q9 1-Methyl-3-ethylbenzene 1.034 0.876 0.779 304.465

150 97.387 622-96-8 Q9 1-Methyl-4-ethylbenzene 0.479 0.408 0.361 141.098

151 98.015 108-67-8 Q9 1,3,5-Trimethylbenzene 0.606 0.513 0.456 178.294

152 98.68217301-94-8 I10 4-Methylnonane 0.012 0.012 0.007 3.195

153 98.883 ? Unidentified 0.302 0.304 0.192 103.678

154 99.099 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.354 0.294 0.267 104.266

155 99.661 5911-04-6 I10 3-Methylnonane 0.016 0.016 0.010 4.292

156 100.127 ? Unidentified 0.024 0.018 0.014 8.302

157 100.251 ? Unidentified 0.065 0.064 0.038 22.337

158 100.476 I11 C11-Isoparaffin-2 0.036 0.036 0.021 9.990

159 100.733 95-63-6 Q9 1,2,4-Trimethylbenzene 1.654 1.383 1.246 486.978

160 100.941 ? Unidentified 0.046 0.048 0.029 15.652

161 101.062 ? Unidentified 0.028 0.028 0.018 9.462

162 101.320 98-06-6 Q10 t-Butylbenzene 0.007 0.006 0.005 2.012

163 102.10817302-01-1 I10 3-Ethyl-3-methylheptane 0.066 0.065 0.038 18.229

164 102.456 538-93-2 Q10 i-Butylbenzene 0.080 0.068 0.054 23.371

165 102.595 124-18-5 P10 n-Decane 0.040 0.040 0.025 10.930

166 102.974 ? Unidentified 0.018 0.018 0.011 6.344

167 103.609 526-73-8 Q9 1,2,3-Trimethylbenzene 0.206 0.168 0.155 60.511

168 103.991 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.009 0.008 0.006 2.681

169 104.190 I11 C11 Isoparaffin-4 0.009 0.009 0.005 2.609

170 104.394 ? Unidentified 0.056 0.048 0.038 19.166

171 104.801 J9 Indan 0.076 0.058 0.058 22.715

172 105.429 J10 Indene 0.386 0.293 0.296 115.521

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C-51
Hydrocarbon Expert V4.7 Thu Aug 26 08:04:00 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91310 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91310

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 106.147 I11 C11-Isoparaffin-7 0.160 0.157 0.092 44.169

174 106.332 141-93-5 Q10 1,3-Diethylbenzene 0.024 0.020 0.016 6.917

175 106.621 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 0.499 0.424 0.336 146.108

176 106.922 105-05-5 Q10 1,4-Diethylbenzene 0.186 0.158 0.125 54.488

177 107.173 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.109 0.091 0.074 31.943

178 107.428 135-01-3 Q10 1,2-Diethylbenzene 0.039 0.033 0.026 11.502

179 107.886 ? Unidentified 0.040 0.039 0.023 13.584

180 108.025 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.044 0.037 0.029 12.780

181 108.161 ? Unidentified 0.046 0.046 0.027 15.918

182 108.244 ? Unidentified 0.042 0.041 0.024 14.362

183 108.365 I11 C11- Isoparaffin-11 0.345 0.340 0.200 95.418

184 108.550 ? Unidentified 0.111 0.109 0.064 38.149

185 108.877 1758-88-9 Q10 1,4,Dimethyl-2-ethylbenzene 0.091 0.076 0.061 26.507

186 108.981 ? Unidentified 0.386 0.322 0.260 132.391

187 109.203 J10 2-Methylindan 0.059 0.044 0.040 17.525

188 109.543 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.258 0.216 0.174 75.621

189 110.101 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.336 0.276 0.227 98.408

190 110.528 ? Unidentified 0.011 0.010 0.007 3.900

191 110.729 693-61-8 K11 2-Undecene, (E)- 0.028 0.028 0.018 7.782

192 110.857 ? Unidentified 0.065 0.064 0.042 22.346

193 111.132 ? Unidentified 0.055 0.047 0.033 18.831

194 111.219 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.063 0.052 0.042 18.375

195 111.531 1120-21-4 P11 n-Undecane 0.032 0.032 0.019 8.875

196 111.687 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.043 0.035 0.026 12.478

197 111.798 ? Unidentified 0.026 0.021 0.016 8.785

198 112.162 Q10 1,2,4,5-Tetramethylbenzene 0.204 0.168 0.137 59.668

199 112.430 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.281 0.231 0.189 82.148

200 112.785 ? Unidentified 0.006 0.005 0.004 2.187

201 112.966 I12 C12 - IsoParaffin - 1 0.010 0.010 0.005 2.763

202 113.293 ? Unidentified 0.019 0.019 0.010 6.538

203 113.445 ? Unidentified 0.007 0.007 0.004 2.291

204 113.584 Q11 C11 - Aromatic - 3 0.025 0.021 0.015 7.283

205 113.652 ? Unidentified 0.021 0.017 0.013 7.134

206 113.762 874-35-1 H10 5-Methylindan 0.091 0.075 0.062 26.545

207 113.902 Q12 1,2-Di-i-propylbenzene 0.034 0.028 0.019 9.786

208 114.117 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.045 0.037 0.028 13.171

209 114.286 Q11 C11 - Aromatic - 4 0.029 0.024 0.018 8.592

210 114.513 824-22-6 J10 4-Methylindan 0.115 0.094 0.078 33.536

211 114.765 824-63-5 H10 2-Methylindan 0.115 0.095 0.079 33.795

212 114.978 ? Unidentified 0.009 0.009 0.005 3.121

213 115.091 538-68-1 Q11 n-Pentylbenzene 0.011 0.009 0.006 3.099

214 115.319 Q11 tert-Pentylbenzene 0.044 0.036 0.027 12.909

215 115.633 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.021 0.017 0.013 6.160

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C-52
Hydrocarbon Expert V4.7 Thu Aug 26 08:04:00 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91310 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91310

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

216 115.744 Q11 C11 - Aromatic - 7 0.033 0.029 0.020 9.747

217 116.092 I12 C12 - IsoParaffin - 4 0.006 0.005 0.003 1.644

218 116.205 100-18-5 Q12 1,4-Di-i-propylbenzene 0.041 0.033 0.023 11.816

219 116.634 91-20-3 G10 Naphthalene 0.116 0.083 0.082 35.678

220 116.798 ? Unidentified 0.015 0.015 0.008 5.186

221 116.972 ? Unidentified 0.005 0.004 0.003 1.645

222 117.087 J11 1,1-Dimethyl Indane 0.011 0.008 0.007 3.263

223 117.248 J12 Dimethyl Indane - 1 0.004 0.003 0.003 1.334

224 117.432 7364-19-4 Q12 1t-Butyl-4-ethylbenzene 0.007 0.006 0.004 2.153

225 117.736 Q12 1,3-Di-n-propylbenzene 0.035 0.029 0.020 10.262

226 117.846 Q11 C11 - Aromatic - 11 0.018 0.016 0.011 5.308

227 118.402 Q11 C11 - Aromatic - 12 0.015 0.013 0.009 4.321

228 122.542 877-44-1 Q12 1,2,4-Triethylbenzene 0.006 0.005 0.004 1.826

229 123.281 91-57-6 G11 2-Methylnaphthalene 0.012 0.008 0.007 3.566

230 124.144 90-12-0 G11 1-Methylnaphthalene 0.006 0.004 0.004 1.706

231 126.172 ? Unidentified 0.008 0.007 0.004 2.619

232 127.137 ? Unidentified 0.002 0.001 0.001 0.586

233 129.864 ? Unidentified 0.003 0.002 0.002 1.129

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C-53
Hydrocarbon Expert V4.7 Thu Aug 26 08:04:00 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91310 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91310

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 7.391 74-98-6 Propane 0.006 0.009 0.013 1.698

9.793 106-97-8 n-Butane 1.108 1.402 1.725 299.818

17.696 109-66-0 n-Pentane 1.166 1.364 1.463 317.807

35.303 110-54-3 n-Hexane 2.728 3.029 2.865 746.276

57.617 142-82-5 n-Heptane 0.689 0.738 0.623 189.290

77.567 111-65-9 n-Octane 0.546 0.569 0.433 150.328

91.476 111-84-2 n-Nonane 0.427 0.435 0.301 117.650

102.595 124-18-5 n-Decane 0.040 0.040 0.025 10.930

111.531 1120-21-4 n-Undecane 0.032 0.032 0.019 8.875

I-Paraffins 8.613 75-28-5 i-Butane 0.053 0.070 0.083 14.393

10.390 463-82-1 2,2-Dimethylpropane 0.013 0.016 0.016 3.416

14.713 78-78-4 i-Pentane 4.188 4.948 5.253 1140.912

22.623 75-83-2 2,2-Dimethylbutane 0.077 0.087 0.081 20.997

27.833 79-29-8 2,3-Dimethylbutane 1.138 1.259 1.195 311.211

28.904 107-83-5 2-Methylpentane 2.321 2.602 2.438 635.007

31.547 96-14-0 3-Methylpentane 1.751 1.930 1.839 478.997

41.732 108-08-7 2,4-Dimethylpentane 0.971 1.056 0.877 266.530

42.276 464-06-2 2,2,3-Trimethylbutane 0.076 0.080 0.068 20.786

50.197 591-76-4 2-Methylhexane 1.566 1.690 1.414 430.088

52.028 589-34-4 3-Methylhexane 0.662 0.706 0.598 181.839

54.738 540-84-1 2,2,4-Trimethylpentane 7.470 7.905 5.918 2055.609

62.418 590-73-8 2,2-Dimethylhexane 0.030 0.031 0.023 8.132

64.513 564-02-3 2,2,3-Trimethylpentane 0.749 0.766 0.593 206.023

64.760 592-13-2 2,5-Dimethylhexane 1.519 1.604 1.204 418.070

65.100 589-43-5 2,4-Dimethylhexane 1.433 1.498 1.135 394.285

66.331 563-16-6 3,3-Dimethylhexane 0.021 0.022 0.017 5.883

68.135 565-75-3 2,3,4-Trimethylpentane 6.895 7.022 5.463 1897.493

68.821 560-21-4 2,3,3-Trimethylpentane 8.453 8.522 6.697 2326.163

70.441 584-94-1 2,3-Dimethylhexane 1.889 1.942 1.497 519.797

71.701 592-27-8 2-Methylheptane 0.303 0.318 0.240 83.514

71.961 589-53-7 4-Methylheptane 0.284 0.295 0.225 78.043

73.023 589-81-1 3-Methylheptane 0.263 0.273 0.208 72.292

73.207 619-99-8 3-Ethylhexane 0.117 0.120 0.093 32.285

74.950 3522-94-9 2,2,5-Trimethylhexane 3.735 3.866 2.635 1029.771

80.057 1069-53-0 2,3,5-Trimethylhexane 0.619 0.628 0.437 170.654

81.233 1071-26-7 2,4-Dimethylheptane 0.113 0.117 0.080 31.196

82.195 1072-05-5 2,6-Dimethylheptane 0.163 0.168 0.115 44.810

83.130 2,5-Dimethylheptane 0.340 0.348 0.240 93.846

83.300 926-82-9 3,5-Dimethylheptane 0.034 0.034 0.024 9.290

86.618 1067-20-5 3,3-Diethylpentane 0.004 0.004 0.003 1.197

87.015 2216-34-4 4-Methyloctane 0.057 0.058 0.040 15.625

87.148 3221-61-2 2-Methyloctane 0.076 0.078 0.054 21.082

87.85015869-80-4 Heptane, 3-ethyl- 0.010 0.010 0.007 2.791

88.013 2216-33-3 3-Methyloctane 0.075 0.076 0.053 20.696

89.068 C10 - IsoParaffin - 1 0.665 0.669 0.423 183.644

89.91514720-74-2 2,2,4-trimethylheptane 0.469 0.472 0.298 129.541

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C-54
Hydrocarbon Expert V4.7 Thu Aug 26 08:04:00 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91310 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91310

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

I-Paraffins 93.139 C10-isoparaffin-x 0.000 0.000 0.000 0.683

93.82415869-87-1 2,2-Dimethyloctane 0.030 0.030 0.019 8.266

94.63015869-89-3 2,5-Dimethyloctane 0.017 0.017 0.011 4.671

94.814 C10 - IsoParaffin - 2 0.010 0.010 0.006 2.692

95.265 2051-30-1 2,4-Dimethyloctane 0.025 0.026 0.016 7.002

95.660 2,6-Dimethyloctane 0.013 0.013 0.008 3.658

98.68217301-94-8 4-Methylnonane 0.012 0.012 0.007 3.195

99.661 5911-04-6 3-Methylnonane 0.016 0.016 0.010 4.292

100.476 C11-Isoparaffin-2 0.036 0.036 0.021 9.990

102.10817302-01-1 3-Ethyl-3-methylheptane 0.066 0.065 0.038 18.229

104.190 C11 Isoparaffin-4 0.009 0.009 0.005 2.609

106.147 C11-Isoparaffin-7 0.160 0.157 0.092 44.169

108.365 C11- Isoparaffin-11 0.345 0.340 0.200 95.418

112.966 C12 - IsoParaffin - 1 0.010 0.010 0.005 2.763

116.092 C12 - IsoParaffin - 4 0.006 0.005 0.003 1.644

Aromatics

Mono-Aromatics 45.137 71-42-3 Benzene 0.735 0.612 0.852 221.834

68.637 108-88-3 Toluene 5.234 4.420 5.141 1562.352

84.440 100-41-4 Ethylbenzene 0.964 0.814 0.821 285.467

85.671 108-38-3 m-Xylene 2.568 2.175 2.189 760.710

85.818 106-42-3 p-Xylene 1.135 0.965 0.967 336.205

88.652 95-47-6 o-Xylene 0.880 0.732 0.750 260.821

92.837 98-82-8 i-Propylbenzene 0.032 0.027 0.024 9.385

96.305 103-65-1 n-Propylbenzene 0.275 0.233 0.207 80.905

97.155 620-14-4 1-Methyl-3-ethylbenzene 1.034 0.876 0.779 304.465

97.387 622-96-8 1-Methyl-4-ethylbenzene 0.479 0.408 0.361 141.098

98.015 108-67-8 1,3,5-Trimethylbenzene 0.606 0.513 0.456 178.294

99.099 611-14-3 1-Methyl-2-ethylbenzene 0.354 0.294 0.267 104.266

100.733 95-63-6 1,2,4-Trimethylbenzene 1.654 1.383 1.246 486.978

101.320 98-06-6 t-Butylbenzene 0.007 0.006 0.005 2.012

102.456 538-93-2 i-Butylbenzene 0.080 0.068 0.054 23.371

103.609 526-73-8 1,2,3-Trimethylbenzene 0.206 0.168 0.155 60.511

103.991 535-77-3 1-Methyl-3-i-propylbenzene 0.009 0.008 0.006 2.681

106.332 141-93-5 1,3-Diethylbenzene 0.024 0.020 0.016 6.917

106.621 1074-43-7 1-Methyl-3-n-propylbenzene 0.499 0.424 0.336 146.108

106.922 105-05-5 1,4-Diethylbenzene 0.186 0.158 0.125 54.488

107.173 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.109 0.091 0.074 31.943

107.428 135-01-3 1,2-Diethylbenzene 0.039 0.033 0.026 11.502

108.025 1074-17-5 1-Methyl-2-n-propylbenzene 0.044 0.037 0.029 12.780

108.877 1758-88-9 1,4,Dimethyl-2-ethylbenzene 0.091 0.076 0.061 26.507

109.543 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.258 0.216 0.174 75.621

110.101 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.336 0.276 0.227 98.408

111.219 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.063 0.052 0.042 18.375

111.687 4218-48-8 1-Ethyl-4-i-propylbenzene 0.043 0.035 0.026 12.478

112.162 1,2,4,5-Tetramethylbenzene 0.204 0.168 0.137 59.668

112.430 527-53-7 1,2,3,5-Tetramethylbenzene 0.281 0.231 0.189 82.148

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C-55
Hydrocarbon Expert V4.7 Thu Aug 26 08:04:00 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91310 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91310

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 113.584 C11 - Aromatic - 3 0.025 0.021 0.015 7.283

113.902 1,2-Di-i-propylbenzene 0.034 0.028 0.019 9.786

114.117 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.045 0.037 0.028 13.171

114.286 C11 - Aromatic - 4 0.029 0.024 0.018 8.592

115.091 538-68-1 n-Pentylbenzene 0.011 0.009 0.006 3.099

115.319 tert-Pentylbenzene 0.044 0.036 0.027 12.909

115.633 577-55-9 1-Methyl-2-n-butylbenzene 0.021 0.017 0.013 6.160

115.744 C11 - Aromatic - 7 0.033 0.029 0.020 9.747

116.205 100-18-5 1,4-Di-i-propylbenzene 0.041 0.033 0.023 11.816

117.432 7364-19-4 1t-Butyl-4-ethylbenzene 0.007 0.006 0.004 2.153

117.736 1,3-Di-n-propylbenzene 0.035 0.029 0.020 10.262

117.846 C11 - Aromatic - 11 0.018 0.016 0.011 5.308

118.402 C11 - Aromatic - 12 0.015 0.013 0.009 4.321

122.542 877-44-1 1,2,4-Triethylbenzene 0.006 0.005 0.004 1.826

Naphthalenes 116.634 91-20-3 Naphthalene 0.116 0.083 0.082 35.678

123.281 91-57-6 2-Methylnaphthalene 0.012 0.008 0.007 3.566

124.144 90-12-0 1-Methylnaphthalene 0.006 0.004 0.004 1.706

Naphtheno/Olefino-Benzs 113.762 874-35-1 5-Methylindan 0.091 0.075 0.062 26.545

114.765 824-63-5 2-Methylindan 0.115 0.095 0.079 33.795

Indenes 104.801 Indan 0.076 0.058 0.058 22.715

105.429 Indene 0.386 0.293 0.296 115.521

109.203 2-Methylindan 0.059 0.044 0.040 17.525

114.513 824-22-6 4-Methylindan 0.115 0.094 0.078 33.536

117.087 1,1-Dimethyl Indane 0.011 0.008 0.007 3.263

117.248 Dimethyl Indane - 1 0.004 0.003 0.003 1.334

Naphthenes

Mono-Naphthenes 27.099 287-92-3 Cyclopentane 0.144 0.141 0.185 40.242

40.162 96-37-7 Methylcyclopentane 1.490 1.457 1.602 417.419

47.057 110-82-7 Cyclohexane 1.018 0.958 1.095 285.348

52.882 1759-58-6 1t,3-Dimethylcyclopentane 0.170 0.166 0.156 47.503

53.470 2532-58-3 1c,3-Dimethylcyclopentane 0.131 0.129 0.121 36.786

54.094 822-50-4 1t,2-Dimethylcyclopentane 0.187 0.183 0.173 52.531

59.20216491-15-9 Cyclopentene, 1,5-dimethyl- 0.018 0.018 0.017 5.174

61.062 108-87-2 Methylcyclohexane 1.017 0.968 0.937 284.936

62.012 4516-69-2 1,1,3-Trimethylcyclopentane 0.030 0.030 0.025 8.543

63.857 1640-89-7 Ethylcyclopentane 0.038 0.037 0.035 10.744

65.930 4850-28-6 1c,2t,4-Trimethylcyclopentane 0.031 0.030 0.025 8.692

67.46115890-40-1 1t,2c,3-Trimethylcyclopentane 0.028 0.026 0.022 7.727

72.864 1,3-dimethyl-t-cyclohexane 0.181 0.172 0.146 50.735

75.272 3c-Ethylmethylcyclopentane 0.011 0.010 0.009 3.060

75.495 3t-Ethylmethylcyclopentane 0.015 0.014 0.012 4.182

76.198 2207-03-6 1t,3-Dimethylcyclohexane 0.084 0.079 0.068 23.559

81.055 2207-01-4 1c,2-Dimethylcyclohexane 0.016 0.015 0.013 4.451

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C-56
Hydrocarbon Expert V4.7 Thu Aug 26 08:04:00 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91310 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91310

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Naphthenes 81.869 1678-91-7 Ethylcyclohexane 0.126 0.118 0.101 35.261

89.488 3728-57-2 Cyclopentane, 1-methyl-2-propyl- 0.009 0.008 0.008 2.811

89.643 trans-1,3-Diethylcyclopentane 0.022 0.018 0.016 6.570

92.053 4926-90-3 1,1-Methylethylcyclohexane 0.016 0.015 0.012 4.528

93.139 696-29-7 1-Methyl-2-propyl-cyclopentan 0.002 0.002 0.002 0.683

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.405 115-11-7 Isobutene 0.015 0.019 0.024 4.238

9.444 106-98-9 Butene-1 0.018 0.022 0.029 5.067

10.267 624-64-6 t-Butene-2 0.071 0.087 0.115 20.025

10.989 590-18-1 c-Butene-2 0.085 0.100 0.136 23.705

16.337 109-67-1 Pentene-1 0.331 0.379 0.428 92.873

18.798 646-04-8 t-Pentene-2 0.843 0.952 1.088 236.251

19.822 627-20-3 c-Pentene-2 0.462 0.516 0.597 129.552

32.942 592-41-6 Hexene-1 0.161 0.174 0.174 45.242

35.94213269-52-8 t-Hexene-3 0.265 0.284 0.285 74.235

36.410 4050-45-7 t-Hexene-2 0.508 0.545 0.546 142.292

38.237 7688-21-3 c-Hexene-2 0.216 0.228 0.232 60.446

55.028 592-76-7 Heptene-1 0.030 0.031 0.028 8.377

56.88014686-14-7 t-Heptene-3 0.033 0.035 0.031 9.287

57.834 7642-10-6 c-Heptene-3 0.025 0.026 0.023 7.035

58.74214686-13-6 t-Heptene-2 0.017 0.018 0.016 4.727

110.729 693-61-8 2-Undecene, (E)- 0.028 0.028 0.018 7.782

Iso-Olefins 13.128 563-45-1 3-Methylbutene-1 0.297 0.346 0.383 83.131

17.165 563-46-2 2-Methylbutene-1 0.503 0.567 0.650 141.068

20.490 513-35-9 2-Methylbutene-2 1.037 1.146 1.338 290.485

28.696 691-38-3 4-Methyl-c-pentene-2 0.045 0.048 0.048 12.494

29.339 674-76-0 4-Methyl-t-pentene-2 0.131 0.142 0.141 36.738

32.718 763-29-1 2-Methylpentene-1 0.225 0.240 0.242 63.033

36.900 625-27-4 2-Methylpentene-2 0.344 0.364 0.370 96.344

37.313 922-62-3 3-Methyl-c-pentene-2 0.266 0.279 0.286 74.498

39.588 3404-73-7 3,3-Dimethylpentene-1 0.315 0.329 0.291 88.376

42.034 594-56-9 2,3,3-Trimethylbutene-1 0.014 0.015 0.013 3.988

46.159 3404-61-3 3-Methylhexene-1 0.016 0.016 0.014 4.391

46.742 3524-73-0 5-Methylhexene-1 0.065 0.068 0.060 18.261

48.80515840-60-5 2-Methyl-c-hexene-3 0.041 0.044 0.038 11.564

49.146 3769-23-1 4-Methylhexene-1 0.010 0.011 0.009 2.855

49.797 3404-55-5 4-Methyl-t/c-hexene-2 0.051 0.053 0.047 14.405

54.429 C7 - Iso-Olefin - 2 0.022 0.022 0.020 6.183

56.359 4914-89-0 3-Methyl-c-hexene-3 0.014 0.015 0.013 4.021

57.242 6094-02-6 2-Methylhexene-1 0.059 0.062 0.054 16.551

58.113 2738-19-4 2-Methyl-2-hexene 0.027 0.028 0.025 7.601

58.359 3899-36-3 3-Methyl-t-hexene-3 0.021 0.022 0.019 5.773

59.64420710-38-8 3-Methyl-t-hexene-2 0.015 0.016 0.014 4.294

60.429 4914-91-4 2-Pentene, 3,4-dimethyl-, (Z)- 0.014 0.014 0.013 3.812

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C-57
Hydrocarbon Expert V4.7 Thu Aug 26 08:04:00 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91310 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91310

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Iso-Olefins 70.134 C8 - Diolefin - 1 0.012 0.011 0.010 3.324

80.618 C9 - IsoOlefin - 1 0.019 0.018 0.015 5.247

86.221 C9-IsoOlefin-3 0.024 0.022 0.017 6.657

93.139 C10-IsoOlefin-4 0.002 0.003 0.002 0.683

Naphtheno-Olefins 25.249 142-29-0 Cyclopentene 0.197 0.187 0.262 56.828

45.336 693-89-0 1-Methylcyclopentene 0.367 0.345 0.405 105.417

50.669 110-83-8 Cyclohexene 0.045 0.041 0.050 12.602

Di-Olefins 18.208 78-79-5 2-Methyl-1,3-Butadiene 0.010 0.011 0.014 2.994

20.818 2004-70-8 1t,3-Pentadiene 0.015 0.016 0.020 4.373

Oxygenates 12.753 64-17-5 Ethanol 9.432 8.752 18.528 1136.062

26.504 71-23-8 n-Propanol 0.101 0.092 0.152 19.798

Unidentified 19.439 Unidentified 0.006 0.006 0.007 1.936

22.071 Unidentified 0.006 0.006 0.008 2.041

26.430 Unidentified 0.045 0.041 0.068 15.395

28.228 Unidentified 0.051 0.050 0.052 17.407

44.931 Unidentified 0.012 0.011 0.013 4.044

47.596 Unidentified 0.035 0.036 0.032 11.890

72.096 Unidentified 0.158 0.161 0.126 54.383

74.103 Unidentified 0.030 0.028 0.024 10.196

75.910 Unidentified 0.029 0.027 0.023 9.886

78.509 Unidentified 0.094 0.093 0.066 32.143

82.674 Unidentified 0.030 0.032 0.021 10.181

84.620 Unidentified 0.048 0.048 0.035 16.327

84.859 Unidentified 0.049 0.046 0.035 16.930

85.965 Unidentified 0.127 0.128 0.089 43.485

86.328 Unidentified 0.022 0.023 0.016 7.717

88.480 Unidentified 0.205 0.220 0.147 70.483

93.028 Unidentified 0.008 0.008 0.006 2.747

93.028 Unidentified 0.008 0.008 0.005 2.747

93.028 Unidentified 0.008 0.006 0.005 2.747

93.600 Unidentified 0.085 0.086 0.054 29.069

98.883 Unidentified 0.302 0.304 0.192 103.678

100.127 Unidentified 0.024 0.018 0.014 8.302

100.251 Unidentified 0.065 0.064 0.038 22.337

100.941 Unidentified 0.046 0.048 0.029 15.652

101.062 Unidentified 0.028 0.028 0.018 9.462

102.974 Unidentified 0.018 0.018 0.011 6.344

104.394 Unidentified 0.056 0.048 0.038 19.166

107.886 Unidentified 0.040 0.039 0.023 13.584

108.161 Unidentified 0.046 0.046 0.027 15.918

108.244 Unidentified 0.042 0.041 0.024 14.362

108.550 Unidentified 0.111 0.109 0.064 38.149

108.981 Unidentified 0.386 0.322 0.260 132.391

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C-58
Hydrocarbon Expert V4.7 Thu Aug 26 08:04:00 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91310 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91310

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Unidentified 110.528 Unidentified 0.011 0.010 0.007 3.900

110.857 Unidentified 0.065 0.064 0.042 22.346

111.132 Unidentified 0.055 0.047 0.033 18.831

111.798 Unidentified 0.026 0.021 0.016 8.785

112.785 Unidentified 0.006 0.005 0.004 2.187

113.293 Unidentified 0.019 0.019 0.010 6.538

113.445 Unidentified 0.007 0.007 0.004 2.291

113.652 Unidentified 0.021 0.017 0.013 7.134

114.978 Unidentified 0.009 0.009 0.005 3.121

116.798 Unidentified 0.015 0.015 0.008 5.186

116.972 Unidentified 0.005 0.004 0.003 1.645

126.172 Unidentified 0.008 0.007 0.004 2.619

127.137 Unidentified 0.002 0.001 0.001 0.586

129.864 Unidentified 0.003 0.002 0.002 1.129

Plus

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C-59
Hydrocarbon Expert V4.7 Thu Aug 26 08:04:00 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91310 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91310

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF

20.0 15.0 10.0 5.0 0.0

Propane

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

Ethanol

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

Unidentified

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

Unidentified

2,2-Dimethylbutane

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C-60
Hydrocarbon Expert V4.7 Thu Aug 26 08:04:00 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91310 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91310

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

Unidentified n-Propanol

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

n-Hexane

t-Hexene-3

t-Hexene-2

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane 2,3,3-Trimethylbutene-1 2,2,3-Trimethylbutane

Unidentified Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1Cyclohexane

Unidentified

2-Methyl-c-hexene-3

4-Methylhexene-1

4-Methyl-t/c-hexene-2

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C-61
Hydrocarbon Expert V4.7 Thu Aug 26 08:04:00 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91310 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91310

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF

70.0 65.0 60.0 55.0 50.0

2-Methylhexane

Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane

C7 - Iso-Olefin - 2 2,2,4-Trimethylpentane Heptene-1

3-Methyl-c-hexene-3

t-Heptene-3

2-Methylhexene-1

n-Heptane c-Heptene-3 2-Methyl-2-hexene 3-Methyl-t-hexene-3

t-Heptene-2

Cyclopentene, 1,5-dimethyl3-Methyl-t-hexene-2

2-Pentene, 3,4-dimethyl-, (Z)-

Methylcyclohexane

1,1,3-Trimethylcyclopentane

2,2-Dimethylhexane

Ethylcyclopentane

2,2,3-Trimethylpentane 2,5-Dimethylhexane

2,4-Dimethylhexane

1c,2t,4-Trimethylcyclopentane

3,3-Dimethylhexane

1t,2c,3-Trimethylcyclopentane

2,3,4-Trimethylpentane

Toluene 2,3,3-Trimethylpentane

C8 - Diolefin - 1 2,3-Dimethylhexane

2-Methylheptane

Unidentified 4-Methylheptane

1,3-dimethyl-t-cyclohexane 3-Methylheptane 3-Ethylhexane

Unidentified

2,2,5-Trimethylhexane

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C-62
Hydrocarbon Expert V4.7 Thu Aug 26 08:04:00 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91310 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91310

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF

95.0 90.0 85.0 80.0 75.0

3c-Ethylmethylcyclopentane 3t-Ethylmethylcyclopentane

Unidentified 1t,3-Dimethylcyclohexane

n-Octane

Unidentified

2,3,5-Trimethylhexane

C9 - IsoOlefin - 1

1c,2-Dimethylcyclohexane 2,4-Dimethylheptane

Ethylcyclohexane

2,6-Dimethylheptane

Unidentified

2,5-Dimethylheptane 3,5-Dimethylheptane

Ethylbenzene Unidentified

m-Xylene Unidentified p-Xylene

C9-IsoOlefin-3 Unidentified 3,3-Diethylpentane

4-Methyloctane 2-Methyloctane

Heptane, 3-ethyl- 3-Methyloctane

Unidentified o-Xylene

C10 - IsoParaffin - 1

Cyclopentane, 1-methyl-2-propyl- trans-1,3-Diethylcyclopentane 2,2,4-trimethylheptane

n-Nonane

1,1-Methylethylcyclohexane

i-Propylbenzene 1-Methyl-2-propyl-cyclopentan/C10-IsoOlefin-4/C10-isoparaffin-x Unidentified

Unidentified 2,2-Dimethyloctane

2,5-Dimethyloctane C10 - IsoParaffin - 2

2,4-Dimethyloctane

2,6-Dimethyloctane

n-Propylbenzene

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

4-Methylnonane Unidentified 1-Methyl-2-ethylbenzene

3-Methylnonane

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C-63
Hydrocarbon Expert V4.7 Thu Aug 26 08:04:00 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91310 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91310

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified

C11-Isoparaffin-2 1,2,4-Trimethylbenzene Unidentified

t-Butylbenzene

3-Ethyl-3-methylheptane

i-Butylbenzene n-Decane

Unidentified

1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene C11 Isoparaffin-4 Unidentified

Indan

Indene

C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene 1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

Unidentified 1-Methyl-2-n-propylbenzene Unidentified C11- Isoparaffin-11 Unidentified

1,4,Dimethyl-2-ethylbenzene Unidentified 2-Methylindan

1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

Unidentified 2-Undecene, (E)- Unidentified Unidentified 1,2-Dimethyl-3-ethylbenzene n-Undecane Unidentified 1-Ethyl-4-i-propylbenzene

1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene

Unidentified C12 - IsoParaffin - 1

Unidentified C11 - Aromatic - 3 5-Methylindan 1,2-Di-i-propylbenzene 1-methyl-4-(1-methylpropyl)be C11 - Aromatic - 4 4-Methylindan 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene 1-Methyl-2-n-butylbenzene C11 - Aromatic - 7

C12 - IsoParaffin - 4 1,4-Di-i-propylbenzene

Naphthalene Unidentified 1,1-Dimethyl Indane Dimethyl Indane - 1 1t-Butyl-4-ethylbenzene

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

C11 - Aromatic - 12

1,2,4-Triethylbenzene

2-Methylnaphthalene

1-Methylnaphthalene

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C-64
Hydrocarbon Expert V4.7 Thu Aug 26 08:04:00 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91310 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91310

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000006.D\SIG1000006_FID1_A.CDF

145.0 140.0 135.0 130.0 125.0

Unidentified

Unidentified

Unidentified

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C-65
Hydrocarbon Expert V4.7 Thu Aug 26 10:00:23 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91311 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91311

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 9.854 11.721 12.377

I-Paraffins 38.721 41.264 32.458

Aromatics 25.136 21.112 20.180

Mono-Aromatics 22.924 19.407 18.567

Naphthalenes 0.105 0.076 0.071

Naphtheno/Olefino-Benzs 0.193 0.160 0.129

Indenes 1.914 1.470 1.413

Naphthenes 4.846 4.672 4.675

Mono-Naphthenes 4.846 4.672 4.675

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 7.429 8.119 8.663

n-Olefins 3.237 3.613 3.872

Iso-Olefins 3.602 3.945 4.106

Naphtheno-Olefins 0.567 0.536 0.655

Di-Olefins 0.023 0.025 0.030

Oxygenates 8.958 8.358 17.155

Unidentified 5.056 4.753 4.493

Plus 0.000 0.000 0.000

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C-66
Hydrocarbon Expert V4.7 Thu Aug 26 10:00:23 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91311 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91311

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C2 8.768 8.183 16.875

C3 0.195 0.182 0.290

C4 5.051 6.413 7.719

C5 11.049 12.809 13.729

C6 11.305 11.968 11.831

C7 11.105 10.482 10.304

C8 23.761 23.570 18.782

C9 10.111 9.257 7.281

C10 11.008 9.907 7.214

C11 2.415 2.326 1.388

C12 0.175 0.149 0.095

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C-67
Hydrocarbon Expert V4.7 Thu Aug 26 10:00:23 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91311 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91311

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C3 0.005 0.008 0.010

C4 4.744 6.035 7.236

C5 1.905 2.240 2.340

C6 1.171 1.307 1.204

C7 0.760 0.818 0.672

C8 0.638 0.669 0.495

C9 0.442 0.454 0.306

C10 0.089 0.090 0.055

C11 0.101 0.100 0.058

I-Paraffins C4 0.056 0.074 0.085

C5 5.085 6.044 6.248

C6 4.654 5.209 4.788

C7 2.411 2.614 2.133

C8 16.842 17.497 13.072

C9 3.393 3.516 2.346

C10 4.411 4.459 2.726

C11 1.841 1.822 1.044

C12 0.029 0.029 0.015

Mono-Aromatics C6 0.687 0.576 0.780

C7 5.623 4.776 5.411

C8 5.611 4.768 4.686

C9 5.995 5.065 4.422

C10 4.492 3.794 2.967

C11 0.370 0.309 0.221

C12 0.146 0.120 0.080

Naphthalenes C10 0.085 0.061 0.059

C11 0.020 0.014 0.012

Naphtheno/Olefino-Benzs C10 0.193 0.160 0.129

Indenes C9 0.213 0.163 0.160

C10 1.689 1.298 1.245

C11 0.011 0.009 0.007

Mono-Naphthenes C5 0.209 0.206 0.264

C6 2.115 2.051 2.228

C7 1.791 1.726 1.617

C8 0.619 0.588 0.490

C9 0.067 0.059 0.047

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C-68
Hydrocarbon Expert V4.7 Thu Aug 26 10:00:23 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91311 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91311

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Mono-Naphthenes C10 0.044 0.041 0.028

n-Olefins C4 0.252 0.304 0.398

C5 1.719 1.951 2.173

C6 1.178 1.269 1.241

C7 0.017 0.017 0.015

C11 0.072 0.071 0.045

Iso-Olefins C5 1.916 2.158 2.422

C6 1.127 1.205 1.187

C7 0.504 0.529 0.455

C8 0.051 0.048 0.039

C10 0.005 0.006 0.003

Naphtheno-Olefins C5 0.193 0.184 0.251

C6 0.374 0.352 0.404

Di-Olefins C5 0.023 0.025 0.030

Oxygenates C2 8.768 8.183 16.875

C3 0.190 0.175 0.280

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C-69
Hydrocarbon Expert V4.7 Thu Aug 26 10:00:23 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91311 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91311

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 21.52 21.28

5% 34.82 29.07

10% 81.64 80.44

15% 100.27 95.01

20% 142.42 134.41

25% 157.91 145.71

30% 172.65 165.52

35% 173.26 172.82

40% 205.78 176.93

45% 210.40 209.37

50% 230.77 212.26

55% 233.70 230.87

60% 237.08 235.12

65% 245.27 238.10

70% 277.00 254.85

75% 291.73 281.32

80% 324.57 319.97

85% 334.95 332.28

90% 355.84 352.22

95% 363.20 363.20

FBP 402.00 389.03

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C-70
Hydrocarbon Expert V4.7 Thu Aug 26 10:00:23 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91311 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91311

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 7.391 74-98-6 P3 Propane 0.005 0.008 0.010 1.346

2 8.613 75-28-5 I4 i-Butane 0.056 0.074 0.085 14.694

3 9.406 115-11-7 K4 Isobutene 0.022 0.027 0.035 6.070

4 9.445 106-98-9 K4 Butene-1 0.026 0.032 0.041 7.066

5 9.794 106-97-8 P4 n-Butane 4.744 6.035 7.236 1251.766

6 10.268 624-64-6 K4 t-Butene-2 0.095 0.116 0.151 26.095

7 10.390 463-82-1 I5 2,2-Dimethylpropane 0.021 0.027 0.026 5.672

8 10.988 590-18-1 K4 c-Butene-2 0.108 0.128 0.171 29.537

9 12.745 64-17-5 X2 Ethanol 8.768 8.183 16.875 1029.989

10 13.130 563-45-1 C5 3-Methylbutene-1 0.268 0.314 0.338 73.137

11 14.713 78-78-4 I5 i-Pentane 5.063 6.018 6.222 1345.320

12 16.335 109-67-1 K5 Pentene-1 0.345 0.396 0.436 94.186

13 17.175 563-46-2 C5 2-Methylbutene-1 0.538 0.609 0.680 146.981

14 17.700 109-66-0 P5 n-Pentane 1.905 2.240 2.340 506.058

15 18.213 78-79-5 E5 2-Methyl-1,3-Butadiene 0.009 0.010 0.012 2.617

16 18.804 646-04-8 K5 t-Pentene-2 0.888 1.009 1.123 242.815

17 19.447 ? Unidentified 0.006 0.007 0.008 2.076

18 19.824 627-20-3 K5 c-Pentene-2 0.486 0.546 0.614 132.821

19 20.489 513-35-9 C5 2-Methylbutene-2 1.110 1.235 1.404 303.484

20 20.818 2004-70-8 E5 1t,3-Pentadiene 0.014 0.015 0.018 3.910

21 22.067 ? Unidentified 0.005 0.005 0.007 1.634

22 22.614 75-83-2 I6 2,2-Dimethylbutane 0.133 0.151 0.137 35.394

23 25.253 142-29-0 B5 Cyclopentene 0.193 0.184 0.251 54.271

24 26.487 71-23-8 X3 n-Propanol 0.190 0.175 0.280 36.331

25 27.103 287-92-3 M5 Cyclopentane 0.209 0.206 0.264 57.120

26 27.831 79-29-8 I6 2,3-Dimethylbutane 0.899 1.000 0.925 239.759

27 28.238 ? Unidentified 0.055 0.054 0.055 18.264

28 28.695 691-38-3 C6 4-Methyl-c-pentene-2 0.047 0.051 0.050 12.848

29 28.908 107-83-5 I6 2-Methylpentane 2.257 2.544 2.322 601.975

30 29.345 674-76-0 C6 4-Methyl-t-pentene-2 0.140 0.153 0.147 38.214

31 31.551 96-14-0 I6 3-Methylpentane 1.366 1.514 1.405 364.340

32 32.718 763-29-1 C6 2-Methylpentene-1 0.238 0.256 0.251 65.016

33 32.940 592-41-6 K6 Hexene-1 0.170 0.185 0.179 46.445

34 35.140 760-21-4 C6 2-Ethylbutene-1 0.065 0.069 0.068 17.712

35 35.291 110-54-3 P6 n-Hexane 1.171 1.307 1.204 312.270

36 35.93813269-52-8 K6 t-Hexene-3 0.272 0.294 0.287 74.454

37 36.409 4050-45-7 K6 t-Hexene-2 0.516 0.556 0.543 140.949

38 36.902 625-27-4 C6 2-Methylpentene-2 0.361 0.385 0.380 98.710

39 37.312 922-62-3 C6 3-Methyl-c-pentene-2 0.276 0.291 0.291 75.389

40 38.243 7688-21-3 K6 c-Hexene-2 0.219 0.234 0.231 59.980

41 39.588 3404-73-7 C7 3,3-Dimethylpentene-1 0.329 0.345 0.297 89.806

42 40.157 96-37-7 M6 Methylcyclopentane 1.337 1.315 1.409 365.410

43 41.731 108-08-7 I7 2,4-Dimethylpentane 0.654 0.716 0.579 175.234

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C-71
Hydrocarbon Expert V4.7 Thu Aug 26 10:00:23 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91311 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91311

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 42.037 594-56-9 C7 2,3,3-Trimethylbutene-1 0.011 0.012 0.010 3.132

45 42.276 464-06-2 I7 2,2,3-Trimethylbutane 0.046 0.050 0.041 12.446

46 44.935 ? Unidentified 0.011 0.011 0.012 3.586

47 45.136 71-42-3 Q6 Benzene 0.687 0.576 0.780 202.176

48 45.339 693-89-0 B6 1-Methylcyclopentene 0.338 0.319 0.365 94.630

49 46.162 3404-61-3 C7 3-Methylhexene-1 0.013 0.014 0.012 3.496

50 46.743 3524-73-0 C7 5-Methylhexene-1 0.051 0.054 0.046 13.935

51 47.054 110-82-7 M6 Cyclohexane 0.778 0.736 0.820 212.680

52 47.596 ? Unidentified 0.029 0.031 0.027 9.827

53 48.80515840-60-5 C7 2-Methyl-c-hexene-3 0.032 0.034 0.029 8.671

54 49.801 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.037 0.039 0.033 10.097

55 50.197 591-76-4 I7 2-Methylhexane 1.172 1.272 1.037 314.015

56 50.667 110-83-8 B6 Cyclohexene 0.036 0.033 0.039 9.790

57 52.029 589-34-4 I7 3-Methylhexane 0.538 0.576 0.476 144.014

58 52.883 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.152 0.150 0.137 41.597

59 53.470 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.123 0.122 0.111 33.728

60 54.092 822-50-4 M7 1t,2-Dimethylcyclopentane 0.175 0.171 0.158 47.766

61 54.718 540-84-1 I8 2,2,4-Trimethylpentane 4.891 5.206 3.796 1312.640

62 56.88214686-14-7 K7 t-Heptene-3 0.017 0.017 0.015 4.552

63 57.236 6094-02-6 C7 2-Methylhexene-1 0.026 0.027 0.023 7.021

64 57.617 142-82-5 P7 n-Heptane 0.760 0.818 0.672 203.464

65 58.116 2738-19-4 C7 2-Methyl-2-hexene 0.006 0.006 0.005 1.526

66 61.064 108-87-2 M7 Methylcyclohexane 1.295 1.239 1.169 353.928

67 62.014 4516-69-2 M8 1,1,3-Trimethylcyclopentane 0.035 0.034 0.028 9.553

68 62.418 590-73-8 I8 2,2-Dimethylhexane 0.036 0.038 0.028 9.606

69 63.856 1640-89-7 M7 Ethylcyclopentane 0.046 0.044 0.041 12.458

70 64.509 ? Unidentified 0.342 0.351 0.265 114.352

71 64.754 592-13-2 I8 2,5-Dimethylhexane 0.972 1.032 0.754 260.745

72 65.093 589-43-5 I8 2,4-Dimethylhexane 0.929 0.977 0.721 249.300

73 65.927 4850-28-6 M8 1c,2t,4-Trimethylcyclopentane 0.035 0.034 0.028 9.573

74 66.330 563-16-6 I8 3,3-Dimethylhexane 0.026 0.027 0.020 7.040

75 67.45815890-40-1 M8 1t,2c,3-Trimethylcyclopentane 0.031 0.030 0.025 8.500

76 68.105 565-75-3 I8 2,3,4-Trimethylpentane 3.717 3.807 2.885 997.618

77 68.630 108-88-3 Q7 Toluene 5.623 4.776 5.411 1637.091

78 68.784 560-21-4 I8 2,3,3-Trimethylpentane 4.272 4.332 3.316 1146.564

79 70.129 C8 C8 - Diolefin - 1 0.013 0.013 0.011 3.664

80 70.433 584-94-1 I8 2,3-Dimethylhexane 1.073 1.110 0.833 288.011

81 71.700 592-27-8 I8 2-Methylheptane 0.311 0.328 0.241 83.489

82 71.958 589-53-7 I8 4-Methylheptane 0.211 0.220 0.163 56.522

83 72.096 ? Unidentified 0.089 0.091 0.069 29.749

84 72.863 M8 1,3-dimethyl-t-cyclohexane 0.214 0.205 0.169 58.547

85 73.022 589-81-1 I8 3-Methylheptane 0.268 0.280 0.208 71.971

86 73.207 619-99-8 I8 3-Ethylhexane 0.136 0.140 0.105 36.402

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C-72
Hydrocarbon Expert V4.7 Thu Aug 26 10:00:23 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91311 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91311

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 74.103 ? Unidentified 0.035 0.033 0.028 11.764

88 74.937 3522-94-9 I9 2,2,5-Trimethylhexane 2.255 2.348 1.559 606.420

89 75.271 M8 3c-Ethylmethylcyclopentane 0.013 0.013 0.010 3.614

90 75.492 M8 3t-Ethylmethylcyclopentane 0.017 0.016 0.013 4.643

91 75.909 ? Unidentified 0.016 0.016 0.011 5.465

92 76.194 2207-03-6 M8 1t,3-Dimethylcyclohexane 0.098 0.093 0.078 26.881

93 77.567 111-65-9 P8 n-Octane 0.638 0.669 0.495 171.241

94 78.510 ? Unidentified 0.055 0.055 0.038 18.377

95 80.056 1069-53-0 I9 2,3,5-Trimethylhexane 0.363 0.370 0.251 97.612

96 80.617 C8 C9 - IsoOlefin - 1 0.022 0.021 0.017 6.013

97 81.052 2207-01-4 M8 1c,2-Dimethylcyclohexane 0.018 0.017 0.014 4.961

98 81.233 1071-26-7 I9 2,4-Dimethylheptane 0.079 0.082 0.055 21.296

99 81.868 1678-91-7 M8 Ethylcyclohexane 0.147 0.138 0.116 40.204

100 82.194 1072-05-5 I9 2,6-Dimethylheptane 0.130 0.135 0.090 34.825

101 82.673 ? Unidentified 0.031 0.034 0.022 10.468

102 83.127 I9 2,5-Dimethylheptane 0.239 0.246 0.165 64.315

103 83.307 926-82-9 I9 3,5-Dimethylheptane 0.031 0.031 0.021 8.270

104 84.440 100-41-4 Q8 Ethylbenzene 1.019 0.866 0.851 294.532

105 84.619 ? Unidentified 0.031 0.031 0.022 10.355

106 84.860 ? Unidentified 0.040 0.038 0.028 13.495

107 85.670 108-38-3 Q8 m-Xylene 2.559 2.180 2.137 739.243

108 85.817 106-42-3 Q8 p-Xylene 1.136 0.972 0.949 328.278

109 85.964 ? Unidentified 0.080 0.081 0.055 26.710

110 86.220 C8 C9-IsoOlefin-3 0.015 0.015 0.011 4.218

111 86.328 ? Unidentified 0.014 0.015 0.010 4.796

112 86.459 I9 3,5-Dimethylheptane 0.012 0.012 0.008 3.133

113 86.618 1067-20-5 I9 3,3-Diethylpentane 0.010 0.010 0.007 2.796

114 87.015 2216-34-4 I9 4-Methyloctane 0.070 0.072 0.048 18.808

115 87.148 3221-61-2 I9 2-Methyloctane 0.096 0.099 0.066 25.681

116 87.85015869-80-4 I9 Heptane, 3-ethyl- 0.013 0.013 0.009 3.572

117 88.013 2216-33-3 I9 3-Methyloctane 0.096 0.098 0.066 25.793

118 88.480 ? Unidentified 0.113 0.121 0.079 37.683

119 88.651 95-47-6 Q8 o-Xylene 0.896 0.750 0.749 258.967

120 89.067 I10 C10 - IsoParaffin - 1 0.394 0.399 0.246 106.186

121 89.488 3728-57-2 M8 Cyclopentane, 1-methyl-2-propyl- 0.010 0.008 0.008 2.921

122 89.642 M9 trans-1,3-Diethylcyclopentane 0.032 0.027 0.023 9.326

123 89.91414720-74-2 I10 2,2,4-trimethylheptane 0.295 0.298 0.184 79.366

124 91.493 111-84-2 P9 n-Nonane 0.442 0.454 0.306 118.845

125 92.061 4926-90-3 M9 1,1-Methylethylcyclohexane 0.030 0.027 0.021 8.171

126 92.838 98-82-8 Q9 i-Propylbenzene 0.040 0.034 0.029 11.459

127 93.029 ? Unidentified 0.012 0.011 0.008 4.049

128 93.029 ? Unidentified 0.012 0.013 0.008 4.049

129 93.029 ? Unidentified 0.012 0.009 0.008 4.049

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C-73
Hydrocarbon Expert V4.7 Thu Aug 26 10:00:23 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91311 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91311

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 93.140 696-29-7 M9 1-Methyl-2-propyl-cyclopentan 0.005 0.005 0.004 1.444

131 93.140 C10 C10-IsoOlefin-4 0.005 0.006 0.003 1.444

132 93.140 I10 C10-isoparaffin-x 0.000 0.000 0.000 1.444

133 93.601 ? Unidentified 0.162 0.165 0.101 54.403

134 93.82415869-87-1 I10 2,2-Dimethyloctane 0.058 0.059 0.036 15.626

135 94.269 ? Unidentified 0.014 0.010 1.245 4.701

136 94.269 ? Unidentified 0.014 0.015 0.009 4.701

137 94.62515869-89-3 I10 2,5-Dimethyloctane 0.085 0.086 0.053 22.890

138 94.812 I10 C10 - IsoParaffin - 2 0.020 0.021 0.013 5.502

139 95.103 2040-95-1 I10 2,7-Dimethyloctane 0.043 0.044 0.027 11.709

140 95.267 2051-30-1 I10 2,4-Dimethyloctane 0.184 0.186 0.115 49.587

141 95.661 I10 2,6-Dimethyloctane 0.064 0.064 0.040 17.222

142 95.821 ? Unidentified 0.004 0.004 0.003 1.448

143 96.306 103-65-1 Q9 n-Propylbenzene 0.311 0.266 0.230 89.331

144 96.516 I10 3-Methyl-5-ethylheptane 0.009 0.009 0.006 2.421

145 97.156 620-14-4 Q9 1-Methyl-3-ethylbenzene 1.147 0.977 0.846 329.185

146 97.389 622-96-8 Q9 1-Methyl-4-ethylbenzene 0.543 0.464 0.401 155.889

147 98.016 108-67-8 Q9 1,3,5-Trimethylbenzene 0.789 0.672 0.582 226.584

148 98.49915869-85-9 I10 5-Methylnonane 0.009 0.009 0.006 2.467

149 98.68817301-94-8 I10 4-Methylnonane 0.022 0.022 0.014 5.870

150 98.900 I10 2,2,6-Trimethyloctane 2.806 2.845 1.749 756.161

151 99.100 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.438 0.366 0.323 125.598

152 99.472 ? Unidentified 0.008 0.008 0.005 2.614

153 99.664 5911-04-6 I10 3-Methylnonane 0.024 0.024 0.015 6.488

154 99.839 ? Unidentified 0.009 0.010 0.006 3.124

155 100.130 ? Unidentified 0.167 0.123 0.095 55.868

156 100.257 ? Unidentified 0.452 0.448 0.257 151.398

157 100.480 I11 C11-Isoparaffin-2 0.240 0.238 0.136 64.734

158 100.742 95-63-6 Q9 1,2,4-Trimethylbenzene 2.319 1.950 1.711 665.683

159 100.946 ? Unidentified 0.280 0.294 0.177 93.692

160 101.066 ? Unidentified 0.166 0.166 0.103 55.483

161 101.322 1678-98-4 M10 i-Butylcyclohexane 0.041 0.038 0.026 11.340

162 101.966 ? Unidentified 0.016 0.014 0.010 5.257

163 102.11217302-01-1 I10 3-Ethyl-3-methylheptane 0.397 0.393 0.225 107.049

164 102.326 ? Unidentified 0.112 0.096 0.074 37.372

165 102.466 538-93-2 Q10 i-Butylbenzene 0.288 0.249 0.190 82.288

166 102.657 124-18-5 P10 n-Decane 0.089 0.090 0.055 23.965

167 102.975 ? Unidentified 0.104 0.103 0.059 34.809

168 103.468 ? Unidentified 0.012 0.010 0.009 4.150

169 103.614 526-73-8 Q9 1,2,3-Trimethylbenzene 0.408 0.336 0.301 117.257

170 103.981 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.035 0.030 0.023 10.133

171 104.193 I11 C11 Isoparaffin-4 0.048 0.047 0.027 12.916

172 104.395 ? Unidentified 0.247 0.212 0.163 82.822

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C-74
Hydrocarbon Expert V4.7 Thu Aug 26 10:00:23 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91311 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91311

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 104.803 J9 Indan 0.213 0.163 0.160 62.286

174 105.058 I11 C11-Isoparaffin-5 0.026 0.026 0.015 7.047

175 105.439 J10 Indene 1.415 1.081 1.062 412.963

176 105.852 M10 n-ButylCyclohexane 0.002 0.002 0.001 0.648

177 105.994 ? Unidentified 0.012 0.011 0.007 3.888

178 106.154 I11 C11-Isoparaffin-7 0.541 0.535 0.307 145.841

179 106.333 141-93-5 Q10 1,3-Diethylbenzene 0.054 0.046 0.036 15.373

180 106.634 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 1.591 1.361 1.051 454.260

181 106.906 105-05-5 Q10 1,4-Diethylbenzene 0.436 0.372 0.288 124.455

182 107.175 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.132 0.111 0.088 37.824

183 107.422 135-01-3 Q10 1,2-Diethylbenzene 0.120 0.100 0.079 34.250

184 107.889 ? Unidentified 0.130 0.128 0.074 43.447

185 108.027 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.053 0.045 0.035 15.261

186 108.164 ? Unidentified 0.132 0.132 0.076 44.311

187 108.245 ? Unidentified 0.119 0.118 0.068 39.904

188 108.369 I11 C11- Isoparaffin-11 0.986 0.976 0.559 265.970

189 108.552 ? Unidentified 0.314 0.311 0.178 105.123

190 108.983 ? Unidentified 0.913 0.766 0.603 305.601

191 109.206 J10 2-Methylindan 0.151 0.115 0.101 43.973

192 109.543 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.345 0.291 0.228 98.647

193 109.703 ? Unidentified 0.064 0.049 0.043 21.367

194 110.102 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.807 0.667 0.533 230.373

195 110.527 ? Unidentified 0.033 0.030 0.019 11.146

196 110.729 693-61-8 K11 2-Undecene, (E)- 0.072 0.071 0.045 19.459

197 110.857 ? Unidentified 0.156 0.155 0.099 52.275

198 111.131 ? Unidentified 0.136 0.118 0.081 45.609

199 111.212 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.072 0.059 0.048 20.555

200 111.530 1120-21-4 P11 n-Undecane 0.101 0.100 0.058 27.357

201 111.687 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.111 0.091 0.066 31.440

202 111.799 ? Unidentified 0.077 0.063 0.046 25.634

203 112.163 Q10 1,2,4,5-Tetramethylbenzene 0.241 0.200 0.159 68.841

204 112.429 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.317 0.262 0.209 90.442

205 112.653 ? Unidentified 0.014 0.012 0.009 4.778

206 112.784 ? Unidentified 0.021 0.017 0.014 7.016

207 112.965 I12 C12 - IsoParaffin - 1 0.029 0.029 0.015 7.834

208 113.293 ? Unidentified 0.034 0.035 0.019 11.521

209 113.447 ? Unidentified 0.013 0.013 0.007 4.355

210 113.653 ? Unidentified 0.062 0.051 0.037 20.761

211 113.760 874-35-1 H10 5-Methylindan 0.096 0.080 0.065 27.500

212 113.901 Q12 1,2-Di-i-propylbenzene 0.042 0.035 0.023 11.963

213 114.117 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.058 0.048 0.035 16.420

214 114.287 Q11 C11 - Aromatic - 4 0.036 0.029 0.021 10.117

215 114.513 824-22-6 J10 4-Methylindan 0.123 0.102 0.082 35.082

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C-75
Hydrocarbon Expert V4.7 Thu Aug 26 10:00:23 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91311 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91311

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

216 114.681 ? Unidentified 0.028 0.023 0.017 9.459

217 114.764 824-63-5 H10 2-Methylindan 0.097 0.080 0.065 27.579

218 114.977 ? Unidentified 0.012 0.010 0.007 4.058

219 115.090 538-68-1 Q11 n-Pentylbenzene 0.014 0.012 0.009 4.079

220 115.320 Q11 tert-Pentylbenzene 0.054 0.045 0.032 15.323

221 115.631 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.026 0.022 0.016 7.514

222 115.743 Q11 C11 - Aromatic - 7 0.040 0.035 0.024 11.474

223 116.205 100-18-5 Q12 1,4-Di-i-propylbenzene 0.054 0.045 0.030 15.365

224 116.633 91-20-3 G10 Naphthalene 0.085 0.061 0.059 25.418

225 116.797 ? Unidentified 0.012 0.009 0.007 3.973

226 116.973 ? Unidentified 0.005 0.004 0.003 1.612

227 117.078 J11 1,1-Dimethyl Indane 0.011 0.009 0.007 3.339

228 117.430 7364-19-4 Q12 1t-Butyl-4-ethylbenzene 0.015 0.012 0.008 4.243

229 117.734 Q12 1,3-Di-n-propylbenzene 0.034 0.028 0.019 9.672

230 117.846 Q11 C11 - Aromatic - 11 0.019 0.016 0.011 5.275

231 118.401 Q11 C11 - Aromatic - 12 0.012 0.011 0.007 3.481

232 123.280 91-57-6 G11 2-Methylnaphthalene 0.013 0.010 0.008 3.963

233 124.146 90-12-0 G11 1-Methylnaphthalene 0.007 0.005 0.004 1.992

234 126.170 ? Unidentified 0.005 0.004 0.002 1.621

235 126.170 ? Unidentified 0.005 0.005 0.002 1.621

236 129.861 ? Unidentified 0.003 0.002 0.002 1.025

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C-76
Hydrocarbon Expert V4.7 Thu Aug 26 10:00:23 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91311 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91311

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 7.391 74-98-6 Propane 0.005 0.008 0.010 1.346

9.794 106-97-8 n-Butane 4.744 6.035 7.236 1251.766

17.700 109-66-0 n-Pentane 1.905 2.240 2.340 506.058

35.291 110-54-3 n-Hexane 1.171 1.307 1.204 312.270

57.617 142-82-5 n-Heptane 0.760 0.818 0.672 203.464

77.567 111-65-9 n-Octane 0.638 0.669 0.495 171.241

91.493 111-84-2 n-Nonane 0.442 0.454 0.306 118.845

102.657 124-18-5 n-Decane 0.089 0.090 0.055 23.965

111.530 1120-21-4 n-Undecane 0.101 0.100 0.058 27.357

I-Paraffins 8.613 75-28-5 i-Butane 0.056 0.074 0.085 14.694

10.390 463-82-1 2,2-Dimethylpropane 0.021 0.027 0.026 5.672

14.713 78-78-4 i-Pentane 5.063 6.018 6.222 1345.320

22.614 75-83-2 2,2-Dimethylbutane 0.133 0.151 0.137 35.394

27.831 79-29-8 2,3-Dimethylbutane 0.899 1.000 0.925 239.759

28.908 107-83-5 2-Methylpentane 2.257 2.544 2.322 601.975

31.551 96-14-0 3-Methylpentane 1.366 1.514 1.405 364.340

41.731 108-08-7 2,4-Dimethylpentane 0.654 0.716 0.579 175.234

42.276 464-06-2 2,2,3-Trimethylbutane 0.046 0.050 0.041 12.446

50.197 591-76-4 2-Methylhexane 1.172 1.272 1.037 314.015

52.029 589-34-4 3-Methylhexane 0.538 0.576 0.476 144.014

54.718 540-84-1 2,2,4-Trimethylpentane 4.891 5.206 3.796 1312.640

62.418 590-73-8 2,2-Dimethylhexane 0.036 0.038 0.028 9.606

64.754 592-13-2 2,5-Dimethylhexane 0.972 1.032 0.754 260.745

65.093 589-43-5 2,4-Dimethylhexane 0.929 0.977 0.721 249.300

66.330 563-16-6 3,3-Dimethylhexane 0.026 0.027 0.020 7.040

68.105 565-75-3 2,3,4-Trimethylpentane 3.717 3.807 2.885 997.618

68.784 560-21-4 2,3,3-Trimethylpentane 4.272 4.332 3.316 1146.564

70.433 584-94-1 2,3-Dimethylhexane 1.073 1.110 0.833 288.011

71.700 592-27-8 2-Methylheptane 0.311 0.328 0.241 83.489

71.958 589-53-7 4-Methylheptane 0.211 0.220 0.163 56.522

73.022 589-81-1 3-Methylheptane 0.268 0.280 0.208 71.971

73.207 619-99-8 3-Ethylhexane 0.136 0.140 0.105 36.402

74.937 3522-94-9 2,2,5-Trimethylhexane 2.255 2.348 1.559 606.420

80.056 1069-53-0 2,3,5-Trimethylhexane 0.363 0.370 0.251 97.612

81.233 1071-26-7 2,4-Dimethylheptane 0.079 0.082 0.055 21.296

82.194 1072-05-5 2,6-Dimethylheptane 0.130 0.135 0.090 34.825

83.127 2,5-Dimethylheptane 0.239 0.246 0.165 64.315

83.307 926-82-9 3,5-Dimethylheptane 0.031 0.031 0.021 8.270

86.459 3,5-Dimethylheptane 0.012 0.012 0.008 3.133

86.618 1067-20-5 3,3-Diethylpentane 0.010 0.010 0.007 2.796

87.015 2216-34-4 4-Methyloctane 0.070 0.072 0.048 18.808

87.148 3221-61-2 2-Methyloctane 0.096 0.099 0.066 25.681

87.85015869-80-4 Heptane, 3-ethyl- 0.013 0.013 0.009 3.572

88.013 2216-33-3 3-Methyloctane 0.096 0.098 0.066 25.793

89.067 C10 - IsoParaffin - 1 0.394 0.399 0.246 106.186

89.91414720-74-2 2,2,4-trimethylheptane 0.295 0.298 0.184 79.366

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C-77
Hydrocarbon Expert V4.7 Thu Aug 26 10:00:23 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91311 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91311

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

I-Paraffins 93.140 C10-isoparaffin-x 0.000 0.000 0.000 1.444

93.82415869-87-1 2,2-Dimethyloctane 0.058 0.059 0.036 15.626

94.62515869-89-3 2,5-Dimethyloctane 0.085 0.086 0.053 22.890

94.812 C10 - IsoParaffin - 2 0.020 0.021 0.013 5.502

95.103 2040-95-1 2,7-Dimethyloctane 0.043 0.044 0.027 11.709

95.267 2051-30-1 2,4-Dimethyloctane 0.184 0.186 0.115 49.587

95.661 2,6-Dimethyloctane 0.064 0.064 0.040 17.222

96.516 3-Methyl-5-ethylheptane 0.009 0.009 0.006 2.421

98.49915869-85-9 5-Methylnonane 0.009 0.009 0.006 2.467

98.68817301-94-8 4-Methylnonane 0.022 0.022 0.014 5.870

98.900 2,2,6-Trimethyloctane 2.806 2.845 1.749 756.161

99.664 5911-04-6 3-Methylnonane 0.024 0.024 0.015 6.488

100.480 C11-Isoparaffin-2 0.240 0.238 0.136 64.734

102.11217302-01-1 3-Ethyl-3-methylheptane 0.397 0.393 0.225 107.049

104.193 C11 Isoparaffin-4 0.048 0.047 0.027 12.916

105.058 C11-Isoparaffin-5 0.026 0.026 0.015 7.047

106.154 C11-Isoparaffin-7 0.541 0.535 0.307 145.841

108.369 C11- Isoparaffin-11 0.986 0.976 0.559 265.970

112.965 C12 - IsoParaffin - 1 0.029 0.029 0.015 7.834

Aromatics

Mono-Aromatics 45.136 71-42-3 Benzene 0.687 0.576 0.780 202.176

68.630 108-88-3 Toluene 5.623 4.776 5.411 1637.091

84.440 100-41-4 Ethylbenzene 1.019 0.866 0.851 294.532

85.670 108-38-3 m-Xylene 2.559 2.180 2.137 739.243

85.817 106-42-3 p-Xylene 1.136 0.972 0.949 328.278

88.651 95-47-6 o-Xylene 0.896 0.750 0.749 258.967

92.838 98-82-8 i-Propylbenzene 0.040 0.034 0.029 11.459

96.306 103-65-1 n-Propylbenzene 0.311 0.266 0.230 89.331

97.156 620-14-4 1-Methyl-3-ethylbenzene 1.147 0.977 0.846 329.185

97.389 622-96-8 1-Methyl-4-ethylbenzene 0.543 0.464 0.401 155.889

98.016 108-67-8 1,3,5-Trimethylbenzene 0.789 0.672 0.582 226.584

99.100 611-14-3 1-Methyl-2-ethylbenzene 0.438 0.366 0.323 125.598

100.742 95-63-6 1,2,4-Trimethylbenzene 2.319 1.950 1.711 665.683

102.466 538-93-2 i-Butylbenzene 0.288 0.249 0.190 82.288

103.614 526-73-8 1,2,3-Trimethylbenzene 0.408 0.336 0.301 117.257

103.981 535-77-3 1-Methyl-3-i-propylbenzene 0.035 0.030 0.023 10.133

106.333 141-93-5 1,3-Diethylbenzene 0.054 0.046 0.036 15.373

106.634 1074-43-7 1-Methyl-3-n-propylbenzene 1.591 1.361 1.051 454.260

106.906 105-05-5 1,4-Diethylbenzene 0.436 0.372 0.288 124.455

107.175 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.132 0.111 0.088 37.824

107.422 135-01-3 1,2-Diethylbenzene 0.120 0.100 0.079 34.250

108.027 1074-17-5 1-Methyl-2-n-propylbenzene 0.053 0.045 0.035 15.261

109.543 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.345 0.291 0.228 98.647

110.102 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.807 0.667 0.533 230.373

111.212 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.072 0.059 0.048 20.555

111.687 4218-48-8 1-Ethyl-4-i-propylbenzene 0.111 0.091 0.066 31.440

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C-78
Hydrocarbon Expert V4.7 Thu Aug 26 10:00:23 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91311 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91311

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 112.163 1,2,4,5-Tetramethylbenzene 0.241 0.200 0.159 68.841

112.429 527-53-7 1,2,3,5-Tetramethylbenzene 0.317 0.262 0.209 90.442

113.901 1,2-Di-i-propylbenzene 0.042 0.035 0.023 11.963

114.117 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.058 0.048 0.035 16.420

114.287 C11 - Aromatic - 4 0.036 0.029 0.021 10.117

115.090 538-68-1 n-Pentylbenzene 0.014 0.012 0.009 4.079

115.320 tert-Pentylbenzene 0.054 0.045 0.032 15.323

115.631 577-55-9 1-Methyl-2-n-butylbenzene 0.026 0.022 0.016 7.514

115.743 C11 - Aromatic - 7 0.040 0.035 0.024 11.474

116.205 100-18-5 1,4-Di-i-propylbenzene 0.054 0.045 0.030 15.365

117.430 7364-19-4 1t-Butyl-4-ethylbenzene 0.015 0.012 0.008 4.243

117.734 1,3-Di-n-propylbenzene 0.034 0.028 0.019 9.672

117.846 C11 - Aromatic - 11 0.019 0.016 0.011 5.275

118.401 C11 - Aromatic - 12 0.012 0.011 0.007 3.481

Naphthalenes 116.633 91-20-3 Naphthalene 0.085 0.061 0.059 25.418

123.280 91-57-6 2-Methylnaphthalene 0.013 0.010 0.008 3.963

124.146 90-12-0 1-Methylnaphthalene 0.007 0.005 0.004 1.992

Naphtheno/Olefino-Benzs 113.760 874-35-1 5-Methylindan 0.096 0.080 0.065 27.500

114.764 824-63-5 2-Methylindan 0.097 0.080 0.065 27.579

Indenes 104.803 Indan 0.213 0.163 0.160 62.286

105.439 Indene 1.415 1.081 1.062 412.963

109.206 2-Methylindan 0.151 0.115 0.101 43.973

114.513 824-22-6 4-Methylindan 0.123 0.102 0.082 35.082

117.078 1,1-Dimethyl Indane 0.011 0.009 0.007 3.339

Naphthenes

Mono-Naphthenes 27.103 287-92-3 Cyclopentane 0.209 0.206 0.264 57.120

40.157 96-37-7 Methylcyclopentane 1.337 1.315 1.409 365.410

47.054 110-82-7 Cyclohexane 0.778 0.736 0.820 212.680

52.883 1759-58-6 1t,3-Dimethylcyclopentane 0.152 0.150 0.137 41.597

53.470 2532-58-3 1c,3-Dimethylcyclopentane 0.123 0.122 0.111 33.728

54.092 822-50-4 1t,2-Dimethylcyclopentane 0.175 0.171 0.158 47.766

61.064 108-87-2 Methylcyclohexane 1.295 1.239 1.169 353.928

62.014 4516-69-2 1,1,3-Trimethylcyclopentane 0.035 0.034 0.028 9.553

63.856 1640-89-7 Ethylcyclopentane 0.046 0.044 0.041 12.458

65.927 4850-28-6 1c,2t,4-Trimethylcyclopentane 0.035 0.034 0.028 9.573

67.45815890-40-1 1t,2c,3-Trimethylcyclopentane 0.031 0.030 0.025 8.500

72.863 1,3-dimethyl-t-cyclohexane 0.214 0.205 0.169 58.547

75.271 3c-Ethylmethylcyclopentane 0.013 0.013 0.010 3.614

75.492 3t-Ethylmethylcyclopentane 0.017 0.016 0.013 4.643

76.194 2207-03-6 1t,3-Dimethylcyclohexane 0.098 0.093 0.078 26.881

81.052 2207-01-4 1c,2-Dimethylcyclohexane 0.018 0.017 0.014 4.961

81.868 1678-91-7 Ethylcyclohexane 0.147 0.138 0.116 40.204

89.488 3728-57-2 Cyclopentane, 1-methyl-2-propyl- 0.010 0.008 0.008 2.921

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C-79
Hydrocarbon Expert V4.7 Thu Aug 26 10:00:23 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91311 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91311

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Naphthenes 89.642 trans-1,3-Diethylcyclopentane 0.032 0.027 0.023 9.326

92.061 4926-90-3 1,1-Methylethylcyclohexane 0.030 0.027 0.021 8.171

93.140 696-29-7 1-Methyl-2-propyl-cyclopentan 0.005 0.005 0.004 1.444

101.322 1678-98-4 i-Butylcyclohexane 0.041 0.038 0.026 11.340

105.852 n-ButylCyclohexane 0.002 0.002 0.001 0.648

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.406 115-11-7 Isobutene 0.022 0.027 0.035 6.070

9.445 106-98-9 Butene-1 0.026 0.032 0.041 7.066

10.268 624-64-6 t-Butene-2 0.095 0.116 0.151 26.095

10.988 590-18-1 c-Butene-2 0.108 0.128 0.171 29.537

16.335 109-67-1 Pentene-1 0.345 0.396 0.436 94.186

18.804 646-04-8 t-Pentene-2 0.888 1.009 1.123 242.815

19.824 627-20-3 c-Pentene-2 0.486 0.546 0.614 132.821

32.940 592-41-6 Hexene-1 0.170 0.185 0.179 46.445

35.93813269-52-8 t-Hexene-3 0.272 0.294 0.287 74.454

36.409 4050-45-7 t-Hexene-2 0.516 0.556 0.543 140.949

38.243 7688-21-3 c-Hexene-2 0.219 0.234 0.231 59.980

56.88214686-14-7 t-Heptene-3 0.017 0.017 0.015 4.552

110.729 693-61-8 2-Undecene, (E)- 0.072 0.071 0.045 19.459

Iso-Olefins 13.130 563-45-1 3-Methylbutene-1 0.268 0.314 0.338 73.137

17.175 563-46-2 2-Methylbutene-1 0.538 0.609 0.680 146.981

20.489 513-35-9 2-Methylbutene-2 1.110 1.235 1.404 303.484

28.695 691-38-3 4-Methyl-c-pentene-2 0.047 0.051 0.050 12.848

29.345 674-76-0 4-Methyl-t-pentene-2 0.140 0.153 0.147 38.214

32.718 763-29-1 2-Methylpentene-1 0.238 0.256 0.251 65.016

35.140 760-21-4 2-Ethylbutene-1 0.065 0.069 0.068 17.712

36.902 625-27-4 2-Methylpentene-2 0.361 0.385 0.380 98.710

37.312 922-62-3 3-Methyl-c-pentene-2 0.276 0.291 0.291 75.389

39.588 3404-73-7 3,3-Dimethylpentene-1 0.329 0.345 0.297 89.806

42.037 594-56-9 2,3,3-Trimethylbutene-1 0.011 0.012 0.010 3.132

46.162 3404-61-3 3-Methylhexene-1 0.013 0.014 0.012 3.496

46.743 3524-73-0 5-Methylhexene-1 0.051 0.054 0.046 13.935

48.80515840-60-5 2-Methyl-c-hexene-3 0.032 0.034 0.029 8.671

49.801 3404-55-5 4-Methyl-t/c-hexene-2 0.037 0.039 0.033 10.097

57.236 6094-02-6 2-Methylhexene-1 0.026 0.027 0.023 7.021

58.116 2738-19-4 2-Methyl-2-hexene 0.006 0.006 0.005 1.526

70.129 C8 - Diolefin - 1 0.013 0.013 0.011 3.664

80.617 C9 - IsoOlefin - 1 0.022 0.021 0.017 6.013

86.220 C9-IsoOlefin-3 0.015 0.015 0.011 4.218

93.140 C10-IsoOlefin-4 0.005 0.006 0.003 1.444

Naphtheno-Olefins 25.253 142-29-0 Cyclopentene 0.193 0.184 0.251 54.271

45.339 693-89-0 1-Methylcyclopentene 0.338 0.319 0.365 94.630

50.667 110-83-8 Cyclohexene 0.036 0.033 0.039 9.790

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C-80
Hydrocarbon Expert V4.7 Thu Aug 26 10:00:23 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91311 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91311

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Naphtheno-Olefins

Di-Olefins 18.213 78-79-5 2-Methyl-1,3-Butadiene 0.009 0.010 0.012 2.617

20.818 2004-70-8 1t,3-Pentadiene 0.014 0.015 0.018 3.910

Oxygenates 12.745 64-17-5 Ethanol 8.768 8.183 16.875 1029.989

26.487 71-23-8 n-Propanol 0.190 0.175 0.280 36.331

Unidentified 19.447 Unidentified 0.006 0.007 0.008 2.076

22.067 Unidentified 0.005 0.005 0.007 1.634

28.238 Unidentified 0.055 0.054 0.055 18.264

44.935 Unidentified 0.011 0.011 0.012 3.586

47.596 Unidentified 0.029 0.031 0.027 9.827

64.509 Unidentified 0.342 0.351 0.265 114.352

72.096 Unidentified 0.089 0.091 0.069 29.749

74.103 Unidentified 0.035 0.033 0.028 11.764

75.909 Unidentified 0.016 0.016 0.011 5.465

78.510 Unidentified 0.055 0.055 0.038 18.377

82.673 Unidentified 0.031 0.034 0.022 10.468

84.619 Unidentified 0.031 0.031 0.022 10.355

84.860 Unidentified 0.040 0.038 0.028 13.495

85.964 Unidentified 0.080 0.081 0.055 26.710

86.328 Unidentified 0.014 0.015 0.010 4.796

88.480 Unidentified 0.113 0.121 0.079 37.683

93.029 Unidentified 0.012 0.011 0.008 4.049

93.029 Unidentified 0.012 0.013 0.008 4.049

93.029 Unidentified 0.012 0.009 0.008 4.049

93.601 Unidentified 0.162 0.165 0.101 54.403

94.269 Unidentified 0.014 0.010 1.245 4.701

94.269 Unidentified 0.014 0.015 0.009 4.701

95.821 Unidentified 0.004 0.004 0.003 1.448

99.472 Unidentified 0.008 0.008 0.005 2.614

99.839 Unidentified 0.009 0.010 0.006 3.124

100.130 Unidentified 0.167 0.123 0.095 55.868

100.257 Unidentified 0.452 0.448 0.257 151.398

100.946 Unidentified 0.280 0.294 0.177 93.692

101.066 Unidentified 0.166 0.166 0.103 55.483

101.966 Unidentified 0.016 0.014 0.010 5.257

102.326 Unidentified 0.112 0.096 0.074 37.372

102.975 Unidentified 0.104 0.103 0.059 34.809

103.468 Unidentified 0.012 0.010 0.009 4.150

104.395 Unidentified 0.247 0.212 0.163 82.822

105.994 Unidentified 0.012 0.011 0.007 3.888

107.889 Unidentified 0.130 0.128 0.074 43.447

108.164 Unidentified 0.132 0.132 0.076 44.311

108.245 Unidentified 0.119 0.118 0.068 39.904

108.552 Unidentified 0.314 0.311 0.178 105.123

108.983 Unidentified 0.913 0.766 0.603 305.601

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C-81
Hydrocarbon Expert V4.7 Thu Aug 26 10:00:23 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91311 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91311

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Unidentified 109.703 Unidentified 0.064 0.049 0.043 21.367

110.527 Unidentified 0.033 0.030 0.019 11.146

110.857 Unidentified 0.156 0.155 0.099 52.275

111.131 Unidentified 0.136 0.118 0.081 45.609

111.799 Unidentified 0.077 0.063 0.046 25.634

112.653 Unidentified 0.014 0.012 0.009 4.778

112.784 Unidentified 0.021 0.017 0.014 7.016

113.293 Unidentified 0.034 0.035 0.019 11.521

113.447 Unidentified 0.013 0.013 0.007 4.355

113.653 Unidentified 0.062 0.051 0.037 20.761

114.681 Unidentified 0.028 0.023 0.017 9.459

114.977 Unidentified 0.012 0.010 0.007 4.058

116.797 Unidentified 0.012 0.009 0.007 3.973

116.973 Unidentified 0.005 0.004 0.003 1.612

126.170 Unidentified 0.005 0.004 0.002 1.621

126.170 Unidentified 0.005 0.005 0.002 1.621

129.861 Unidentified 0.003 0.002 0.002 1.025

Plus

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C-82
Hydrocarbon Expert V4.7 Thu Aug 26 10:00:23 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91311 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91311

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF

20.0 15.0 10.0 5.0 0.0

Propane

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

Ethanol

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

Unidentified

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

Unidentified

2,2-Dimethylbutane

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C-83
Hydrocarbon Expert V4.7 Thu Aug 26 10:00:23 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91311 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91311

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

n-Propanol

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

2-Ethylbutene-1 n-Hexane

t-Hexene-3

t-Hexene-2

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane 2,3,3-Trimethylbutene-1 2,2,3-Trimethylbutane

Unidentified Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1 Cyclohexane

Unidentified

2-Methyl-c-hexene-3

4-Methyl-t/c-hexene-2

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C-84
Hydrocarbon Expert V4.7 Thu Aug 26 10:00:23 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91311 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91311

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF

70.0 65.0 60.0 55.0 50.0

2-Methylhexane

Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane

2,2,4-Trimethylpentane

t-Heptene-3

2-Methylhexene-1

n-Heptane

2-Methyl-2-hexene

Methylcyclohexane

1,1,3-Trimethylcyclopentane

2,2-Dimethylhexane

Ethylcyclopentane

Unidentified 2,5-Dimethylhexane

2,4-Dimethylhexane

1c,2t,4-Trimethylcyclopentane

3,3-Dimethylhexane

1t,2c,3-Trimethylcyclopentane

2,3,4-Trimethylpentane

Toluene 2,3,3-Trimethylpentane

C8 - Diolefin - 1 2,3-Dimethylhexane

2-Methylheptane

Unidentified 4-Methylheptane

1,3-dimethyl-t-cyclohexane 3-Methylheptane 3-Ethylhexane

Unidentified

2,2,5-Trimethylhexane

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C-85
Hydrocarbon Expert V4.7 Thu Aug 26 10:00:23 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91311 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91311

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF

95.0 90.0 85.0 80.0 75.0

3c-Ethylmethylcyclopentane 3t-Ethylmethylcyclopentane

Unidentified 1t,3-Dimethylcyclohexane

n-Octane

Unidentified

2,3,5-Trimethylhexane

C9 - IsoOlefin - 1

1c,2-Dimethylcyclohexane 2,4-Dimethylheptane

Ethylcyclohexane

2,6-Dimethylheptane

Unidentified

2,5-Dimethylheptane 3,5-Dimethylheptane

Ethylbenzene Unidentified

m-Xylene Unidentified p-Xylene

C9-IsoOlefin-3 Unidentified 3,5-Dimethylheptane 3,3-Diethylpentane

4-Methyloctane 2-Methyloctane

Heptane, 3-ethyl- 3-Methyloctane

Unidentifiedo-Xylene

C10 - IsoParaffin - 1

Cyclopentane, 1-methyl-2-propyl- trans-1,3-Diethylcyclopentane 2,2,4-trimethylheptane

n-Nonane

1,1-Methylethylcyclohexane

i-Propylbenzene Unidentified 1-Methyl-2-propyl-cyclopentan/C10-IsoOlefin-4/C10-isoparaffin-x

Unidentified 2,2-Dimethyloctane

Unidentified

2,5-Dimethyloctane C10 - IsoParaffin - 2 2,7-Dimethyloctane 2,4-Dimethyloctane

2,6-Dimethyloctane Unidentified

n-Propylbenzene 3-Methyl-5-ethylheptane

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

5-Methylnonane 4-Methylnonane 2,2,6-Trimethyloctane 1-Methyl-2-ethylbenzene

Unidentified 3-Methylnonane Unidentified

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C-86
Hydrocarbon Expert V4.7 Thu Aug 26 10:00:23 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91311 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91311

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified Unidentified C11-Isoparaffin-2 1,2,4-Trimethylbenzene

Unidentified Unidentified

i-Butylcyclohexane

Unidentified 3-Ethyl-3-methylheptane Unidentified i-Butylbenzene n-Decane

Unidentified

Unidentified 1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene C11 Isoparaffin-4 Unidentified

Indan C11-Isoparaffin-5

Indene

n-ButylCyclohexane Unidentified C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene 1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

Unidentified 1-Methyl-2-n-propylbenzene UnidentifiedC11- Isoparaffin-11 Unidentified

Unidentified 2-Methylindan

1,2-Dimethyl-4-ethylbenzene Unidentified

1,3-Dimethyl-2-ethylbenzene

Unidentified 2-Undecene, (E)- Unidentified

1,2-Dimethyl-3-ethylbenzene Unidentified

n-Undecane Unidentified 1-Ethyl-4-i-propylbenzene

1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene Unidentified C12 - IsoParaffin - 1

Unidentified

5-Methylindan 1,2-Di-i-propylbenzene 1-methyl-4-(1-methylpropyl)be C11 - Aromatic - 4 4-Methylindan Unidentified 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene 1-Methyl-2-n-butylbenzene C11 - Aromatic - 7

1,4-Di-i-propylbenzene

Naphthalene Unidentified 1,1-Dimethyl Indane

1t-Butyl-4-ethylbenzene

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

C11 - Aromatic - 12

2-Methylnaphthalene

1-Methylnaphthalene

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C-87
Hydrocarbon Expert V4.7 Thu Aug 26 10:00:23 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91311 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91311

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000007.D\SIG1000007_FID1_A.CDF

145.0 140.0 135.0 130.0 125.0

Unidentified

Unidentified

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C-88
Hydrocarbon Expert V4.7 Fri Aug 27 15:39:02 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91312 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91312

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 8.729 10.455 11.199

I-Paraffins 33.099 36.336 31.006

Aromatics 43.990 38.260 41.128

Mono-Aromatics 42.927 37.407 40.310

Naphthalenes 0.132 0.097 0.098

Naphtheno/Olefino-Benzs 0.250 0.212 0.182

Indenes 0.681 0.544 0.538

Naphthenes 5.522 5.473 5.806

Mono-Naphthenes 5.522 5.473 5.806

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 6.928 7.736 8.677

n-Olefins 3.019 3.458 3.906

Iso-Olefins 3.285 3.670 3.988

Naphtheno-Olefins 0.599 0.582 0.748

Di-Olefins 0.025 0.027 0.035

Oxygenates 0.112 0.106 0.179

Unidentified 1.621 1.634 2.005

Plus 0.000 0.000 0.000

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C-89
Hydrocarbon Expert V4.7 Fri Aug 27 15:39:02 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91312 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91312

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C3 0.119 0.116 0.194

C4 2.824 3.680 4.683

C5 11.839 14.117 15.927

C6 11.198 12.147 12.709

C7 22.973 21.095 23.557

C8 31.822 30.516 27.856

C9 10.326 9.865 8.026

C10 6.387 6.004 4.486

C11 0.744 0.701 0.469

C12 0.146 0.124 0.086

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C-90
Hydrocarbon Expert V4.7 Fri Aug 27 15:39:02 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91312 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91312

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C3 0.007 0.011 0.016

C4 2.583 3.375 4.273

C5 2.607 3.148 3.474

C6 1.508 1.729 1.682

C7 0.876 0.969 0.840

C8 0.638 0.687 0.537

C9 0.443 0.467 0.332

C10 0.057 0.059 0.038

C11 0.011 0.011 0.007

I-Paraffins C4 0.054 0.074 0.090

C5 5.567 6.796 7.419

C6 4.142 4.765 4.621

C7 1.860 2.066 1.785

C8 13.873 14.639 11.678

C9 4.209 4.480 3.155

C10 3.000 3.116 2.016

C11 0.394 0.400 0.242

Mono-Aromatics C6 0.624 0.537 0.768

C7 17.346 15.130 18.100

C8 16.602 14.498 15.035

C9 5.502 4.776 4.401

C10 2.395 2.072 1.716

C11 0.313 0.270 0.203

C12 0.146 0.124 0.086

Naphthalenes C10 0.118 0.087 0.088

C11 0.014 0.011 0.010

Naphtheno/Olefino-Benzs C10 0.250 0.212 0.182

Indenes C9 0.122 0.096 0.099

C10 0.547 0.438 0.431

C11 0.012 0.009 0.008

Mono-Naphthenes C5 0.264 0.268 0.362

C6 2.399 2.387 2.741

C7 2.135 2.116 2.091

C8 0.653 0.637 0.560

C9 0.050 0.045 0.038

C10 0.021 0.020 0.014

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C-91
Hydrocarbon Expert V4.7 Fri Aug 27 15:39:02 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91312 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91312

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Mono-Naphthenes

n-Olefins C4 0.187 0.232 0.320

C5 1.604 1.869 2.198

C6 1.129 1.249 1.289

C7 0.100 0.108 0.098

Iso-Olefins C5 1.581 1.819 2.167

C6 0.991 1.089 1.132

C7 0.656 0.707 0.643

C8 0.057 0.055 0.047

Naphtheno-Olefins C5 0.193 0.189 0.272

C6 0.406 0.393 0.476

Di-Olefins C5 0.025 0.027 0.035

Oxygenates C3 0.112 0.106 0.179

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C-92
Hydrocarbon Expert V4.7 Fri Aug 27 15:39:02 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91312 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91312

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 22.30 21.82

5% 79.91 79.30

10% 94.11 81.69

15% 121.32 97.04

20% 152.92 138.74

25% 173.34 154.30

30% 208.90 176.97

35% 230.74 210.59

40% 230.84 230.75

45% 230.95 230.87

50% 231.05 230.99

55% 235.77 234.29

60% 238.24 236.99

65% 254.66 241.30

70% 276.24 256.22

75% 280.98 279.06

80% 281.89 281.55

85% 291.84 291.59

90% 324.07 321.56

95% 347.21 336.34

FBP 404.50 401.19

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C-93
Hydrocarbon Expert V4.7 Fri Aug 27 15:39:02 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91312 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91312

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 7.390 74-98-6 P3 Propane 0.007 0.011 0.016 1.931

2 8.612 75-28-5 I4 i-Butane 0.054 0.074 0.090 14.889

3 9.405 115-11-7 K4 Isobutene 0.015 0.019 0.025 4.205

4 9.444 106-98-9 K4 Butene-1 0.018 0.023 0.031 5.095

5 9.793 106-97-8 P4 n-Butane 2.583 3.375 4.273 706.418

6 10.268 624-64-6 K4 t-Butene-2 0.071 0.088 0.121 19.989

7 10.390 463-82-1 I5 2,2-Dimethylpropane 0.020 0.026 0.027 5.496

8 10.988 590-18-1 K4 c-Butene-2 0.083 0.102 0.143 23.628

9 13.131 563-45-1 C5 3-Methylbutene-1 0.067 0.081 0.092 19.045

10 14.714 78-78-4 I5 i-Pentane 5.547 6.771 7.392 1527.638

11 16.337 109-67-1 K5 Pentene-1 0.325 0.384 0.446 92.164

12 17.169 563-46-2 C5 2-Methylbutene-1 0.495 0.576 0.679 140.224

13 17.696 109-66-0 P5 n-Pentane 2.607 3.148 3.474 717.875

14 18.207 78-79-5 E5 2-Methyl-1,3-Butadiene 0.010 0.011 0.014 2.901

15 18.804 646-04-8 K5 t-Pentene-2 0.826 0.964 1.133 234.031

16 19.444 ? Unidentified 0.006 0.007 0.008 1.945

17 19.828 627-20-3 K5 c-Pentene-2 0.452 0.521 0.620 128.015

18 20.489 513-35-9 C5 2-Methylbutene-2 1.018 1.163 1.396 288.432

19 20.825 2004-70-8 E5 1t,3-Pentadiene 0.015 0.016 0.021 4.266

20 22.077 ? Unidentified 0.006 0.006 0.008 1.965

21 22.618 75-83-2 I6 2,2-Dimethylbutane 0.173 0.202 0.193 47.941

22 25.252 142-29-0 B5 Cyclopentene 0.193 0.189 0.272 56.283

23 26.420 ? Unidentified 0.037 0.035 0.059 12.823

24 26.492 71-23-8 X3 n-Propanol 0.112 0.106 0.179 22.154

25 27.105 287-92-3 M5 Cyclopentane 0.264 0.268 0.362 74.721

26 27.837 79-29-8 I6 2,3-Dimethylbutane 0.464 0.530 0.517 128.182

27 28.231 ? Unidentified 0.051 0.052 0.055 17.571

28 28.690 691-38-3 C6 4-Methyl-c-pentene-2 0.043 0.048 0.049 12.156

29 28.909 107-83-5 I6 2-Methylpentane 2.182 2.527 2.435 603.375

30 29.343 674-76-0 C6 4-Methyl-t-pentene-2 0.129 0.145 0.147 36.488

31 31.551 96-14-0 I6 3-Methylpentane 1.323 1.506 1.476 365.693

32 32.728 763-29-1 C6 2-Methylpentene-1 0.222 0.245 0.253 62.795

33 32.942 592-41-6 K6 Hexene-1 0.159 0.178 0.182 45.116

34 35.297 110-54-3 P6 n-Hexane 1.508 1.729 1.682 416.829

35 35.94013269-52-8 K6 t-Hexene-3 0.260 0.288 0.297 73.558

36 36.412 4050-45-7 K6 t-Hexene-2 0.498 0.551 0.569 141.009

37 36.908 625-27-4 C6 2-Methylpentene-2 0.337 0.369 0.385 95.505

38 37.313 922-62-3 C6 3-Methyl-c-pentene-2 0.260 0.282 0.297 73.741

39 38.244 7688-21-3 K6 c-Hexene-2 0.212 0.232 0.242 60.014

40 39.591 3404-73-7 C7 3,3-Dimethylpentene-1 0.309 0.333 0.303 87.618

41 40.161 96-37-7 M6 Methylcyclopentane 1.457 1.472 1.664 412.630

42 41.741 108-08-7 I7 2,4-Dimethylpentane 0.224 0.252 0.215 62.201

43 42.042 594-56-9 C7 2,3,3-Trimethylbutene-1 0.014 0.015 0.014 3.992

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C-94
Hydrocarbon Expert V4.7 Fri Aug 27 15:39:02 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91312 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91312

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 42.279 464-06-2 I7 2,2,3-Trimethylbutane 0.025 0.027 0.024 6.945

45 44.937 ? Unidentified 0.012 0.012 0.014 4.097

46 45.140 71-42-3 Q6 Benzene 0.624 0.537 0.768 190.375

47 45.344 693-89-0 B6 1-Methylcyclopentene 0.362 0.351 0.424 105.055

48 46.164 3404-61-3 C7 3-Methylhexene-1 0.016 0.017 0.015 4.435

49 46.748 3524-73-0 C7 5-Methylhexene-1 0.057 0.062 0.056 16.240

50 47.060 110-82-7 M6 Cyclohexane 0.942 0.915 1.076 266.886

51 47.596 ? Unidentified 0.034 0.037 0.034 11.948

52 48.80615840-60-5 C7 2-Methyl-c-hexene-3 0.040 0.044 0.039 11.419

53 49.800 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.051 0.055 0.050 14.377

54 50.196 591-76-4 I7 2-Methylhexane 0.978 1.089 0.938 271.379

55 50.674 110-83-8 B6 Cyclohexene 0.044 0.041 0.052 12.514

56 52.032 589-34-4 I7 3-Methylhexane 0.633 0.697 0.608 175.756

57 52.885 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.203 0.205 0.199 57.537

58 53.474 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.163 0.165 0.159 46.110

59 54.094 822-50-4 M7 1t,2-Dimethylcyclopentane 0.241 0.243 0.236 68.257

60 54.398 C7 C7 - Iso-Olefin - 2 0.022 0.023 0.022 6.324

61 54.684 540-84-1 I8 2,2,4-Trimethylpentane 0.250 0.273 0.211 69.577

62 55.028 592-76-7 K7 Heptene-1 0.030 0.032 0.029 8.363

63 56.362 4914-89-0 C7 3-Methyl-c-hexene-3 0.014 0.015 0.014 4.003

64 56.88414686-14-7 K7 t-Heptene-3 0.032 0.035 0.032 9.165

65 57.246 6094-02-6 C7 2-Methylhexene-1 0.058 0.063 0.056 16.332

66 57.622 142-82-5 P7 n-Heptane 0.876 0.969 0.840 243.113

67 57.837 7642-10-6 K7 c-Heptene-3 0.024 0.026 0.023 6.742

68 58.117 2738-19-4 C7 2-Methyl-2-hexene 0.026 0.028 0.026 7.433

69 58.361 3899-36-3 C7 3-Methyl-t-hexene-3 0.020 0.022 0.019 5.618

70 58.74514686-13-6 K7 t-Heptene-2 0.015 0.016 0.014 4.121

71 59.20616491-15-9 M7 Cyclopentene, 1,5-dimethyl- 0.018 0.018 0.018 5.091

72 59.64820710-38-8 C7 3-Methyl-t-hexene-2 0.015 0.016 0.015 4.321

73 60.432 4914-91-4 C7 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.014 0.013 3.802

74 61.069 108-87-2 M7 Methylcyclohexane 1.455 1.430 1.425 412.203

75 62.015 4516-69-2 M8 1,1,3-Trimethylcyclopentane 0.041 0.041 0.035 11.584

76 62.423 590-73-8 I8 2,2-Dimethylhexane 0.033 0.036 0.028 9.183

77 63.861 1640-89-7 M7 Ethylcyclopentane 0.055 0.055 0.054 15.678

78 64.513 564-02-3 I8 2,2,3-Trimethylpentane 0.422 0.446 0.355 117.429

79 64.757 592-13-2 I8 2,5-Dimethylhexane 0.781 0.852 0.657 217.244

80 65.096 589-43-5 I8 2,4-Dimethylhexane 0.702 0.758 0.591 195.293

81 65.930 4850-28-6 M8 1c,2t,4-Trimethylcyclopentane 0.040 0.040 0.034 11.390

82 66.335 563-16-6 I8 3,3-Dimethylhexane 0.025 0.027 0.021 7.092

83 67.46415890-40-1 M8 1t,2c,3-Trimethylcyclopentane 0.035 0.035 0.030 9.996

84 68.129 565-75-3 I8 2,3,4-Trimethylpentane 4.456 4.687 3.751 1239.462

85 68.718 108-88-3 Q7 Toluene 17.346 15.130 18.100 5233.747

86 68.837 560-21-4 I8 2,3,3-Trimethylpentane 4.966 5.172 4.180 1381.299

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C-95
Hydrocarbon Expert V4.7 Fri Aug 27 15:39:02 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91312 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91312

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 70.138 C8 C8 - Diolefin - 1 0.015 0.015 0.013 4.307

88 70.439 584-94-1 I8 2,3-Dimethylhexane 1.244 1.321 1.047 346.086

89 71.704 592-27-8 I8 2-Methylheptane 0.330 0.357 0.277 91.676

90 71.963 589-53-7 I8 4-Methylheptane 0.240 0.258 0.202 66.823

91 72.099 ? Unidentified 0.110 0.115 0.092 38.113

92 72.867 M8 1,3-dimethyl-t-cyclohexane 0.225 0.221 0.193 63.858

93 73.025 589-81-1 I8 3-Methylheptane 0.282 0.302 0.237 78.425

94 73.210 619-99-8 I8 3-Ethylhexane 0.141 0.150 0.119 39.352

95 74.105 ? Unidentified 0.036 0.035 0.031 12.411

96 74.944 3522-94-9 I9 2,2,5-Trimethylhexane 2.875 3.075 2.155 801.339

97 75.274 M8 3c-Ethylmethylcyclopentane 0.013 0.013 0.011 3.696

98 75.495 M8 3t-Ethylmethylcyclopentane 0.018 0.018 0.015 5.120

99 75.911 ? Unidentified 0.021 0.021 0.018 7.347

100 76.197 2207-03-6 M8 1t,3-Dimethylcyclohexane 0.103 0.100 0.088 29.111

101 77.569 111-65-9 P8 n-Octane 0.638 0.687 0.537 177.379

102 78.511 ? Unidentified 0.079 0.077 0.068 27.364

103 80.059 1069-53-0 I9 2,3,5-Trimethylhexane 0.512 0.536 0.384 142.627

104 80.618 C8 C9 - IsoOlefin - 1 0.021 0.021 0.018 6.075

105 81.057 2207-01-4 M8 1c,2-Dimethylcyclohexane 0.019 0.018 0.016 5.270

106 81.235 1071-26-7 I9 2,4-Dimethylheptane 0.096 0.102 0.072 26.839

107 81.870 1678-91-7 M8 Ethylcyclohexane 0.148 0.143 0.127 41.964

108 82.197 1072-05-5 I9 2,6-Dimethylheptane 0.152 0.162 0.114 42.338

109 82.675 ? Unidentified 0.032 0.031 0.027 11.121

110 83.135 I9 2,5-Dimethylheptane 0.303 0.320 0.227 84.432

111 83.309 926-82-9 I9 3,5-Dimethylheptane 0.032 0.034 0.024 8.993

112 84.459 100-41-4 Q8 Ethylbenzene 2.932 2.558 2.656 878.098

113 84.623 ? Unidentified 0.039 0.040 0.030 13.534

114 84.866 ? Unidentified 0.049 0.047 0.037 16.845

115 85.717 108-38-3 Q8 m-Xylene 7.862 6.880 7.121 2354.451

116 85.858 106-42-3 Q8 p-Xylene 3.682 3.234 3.334 1102.488

117 86.224 C8 C9-IsoOlefin-3 0.020 0.020 0.015 5.719

118 86.330 ? Unidentified 0.019 0.019 0.015 6.658

119 87.020 2216-34-4 I9 4-Methyloctane 0.062 0.065 0.046 17.238

120 87.152 3221-61-2 I9 2-Methyloctane 0.084 0.089 0.063 23.458

121 88.016 2216-33-3 I9 3-Methyloctane 0.092 0.097 0.069 25.706

122 88.484 ? Unidentified 0.198 0.219 0.151 68.672

123 88.667 95-47-6 Q8 o-Xylene 2.125 1.826 1.925 636.409

124 89.069 I10 C10 - IsoParaffin - 1 0.626 0.650 0.423 174.741

125 89.490 3728-57-2 M8 Cyclopentane, 1-methyl-2-propyl- 0.010 0.009 0.009 3.090

126 89.644 M9 trans-1,3-Diethylcyclopentane 0.026 0.022 0.020 7.669

127 89.91614720-74-2 I10 2,2,4-trimethylheptane 0.439 0.457 0.297 122.677

128 91.480 111-84-2 P9 n-Nonane 0.443 0.467 0.332 123.591

129 92.067 4926-90-3 M9 1,1-Methylethylcyclohexane 0.025 0.023 0.019 7.022

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C-96
Hydrocarbon Expert V4.7 Fri Aug 27 15:39:02 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91312 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91312

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 92.838 98-82-8 Q9 i-Propylbenzene 0.038 0.033 0.030 11.256

131 93.029 ? Unidentified 0.022 0.021 0.017 7.692

132 93.029 ? Unidentified 0.022 0.024 0.015 7.692

133 93.029 ? Unidentified 0.022 0.017 0.015 7.692

134 93.601 ? Unidentified 0.128 0.134 0.087 44.490

135 93.82415869-87-1 I10 2,2-Dimethyloctane 0.045 0.047 0.030 12.529

136 94.269 ? Unidentified 0.008 0.006 0.778 2.807

137 94.269 ? Unidentified 0.008 0.009 0.006 2.807

138 94.62515869-89-3 I10 2,5-Dimethyloctane 0.068 0.070 0.046 18.921

139 95.101 2040-95-1 I10 2,7-Dimethyloctane 0.025 0.026 0.017 7.109

140 95.266 2051-30-1 I10 2,4-Dimethyloctane 0.103 0.108 0.070 28.899

141 95.661 I10 2,6-Dimethyloctane 0.038 0.039 0.026 10.618

142 96.305 103-65-1 Q9 n-Propylbenzene 0.307 0.269 0.246 91.310

143 97.156 620-14-4 Q9 1-Methyl-3-ethylbenzene 1.153 1.008 0.922 342.957

144 97.389 622-96-8 Q9 1-Methyl-4-ethylbenzene 0.535 0.470 0.428 159.175

145 98.015 108-67-8 Q9 1,3,5-Trimethylbenzene 0.722 0.631 0.578 214.872

146 98.68517301-94-8 I10 4-Methylnonane 0.014 0.015 0.010 4.015

147 98.891 I10 2,2,6-Trimethyloctane 1.445 1.504 0.976 403.485

148 99.099 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.398 0.342 0.319 118.476

149 99.662 5911-04-6 I10 3-Methylnonane 0.018 0.019 0.012 5.094

150 100.128 ? Unidentified 0.079 0.060 0.049 27.488

151 100.254 ? Unidentified 0.216 0.220 0.133 75.093

152 100.478 I11 C11-Isoparaffin-2 0.115 0.117 0.071 32.107

153 100.739 95-63-6 Q9 1,2,4-Trimethylbenzene 2.029 1.752 1.623 603.617

154 100.942 ? Unidentified 0.128 0.138 0.088 44.457

155 101.063 ? Unidentified 0.076 0.078 0.051 26.411

156 101.320 1678-98-4 M10 i-Butylcyclohexane 0.021 0.020 0.014 5.975

157 102.10817302-01-1 I10 3-Ethyl-3-methylheptane 0.178 0.181 0.109 49.656

158 102.461 538-93-2 Q10 i-Butylbenzene 0.183 0.162 0.131 54.023

159 102.652 124-18-5 P10 n-Decane 0.057 0.059 0.038 15.850

160 102.975 ? Unidentified 0.040 0.041 0.025 13.917

161 103.611 526-73-8 Q9 1,2,3-Trimethylbenzene 0.320 0.271 0.256 95.211

162 103.986 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.023 0.020 0.017 6.854

163 104.192 I11 C11 Isoparaffin-4 0.018 0.018 0.011 4.995

164 104.396 ? Unidentified 0.079 0.069 0.056 27.282

165 104.802 J9 Indan 0.122 0.096 0.099 36.951

166 105.430 J10 Indene 0.384 0.301 0.312 116.086

167 106.146 I11 C11-Isoparaffin-7 0.116 0.118 0.071 32.444

168 106.332 141-93-5 Q10 1,3-Diethylbenzene 0.041 0.036 0.029 12.074

169 106.617 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 0.432 0.379 0.309 127.788

170 106.948 105-05-5 Q10 1,4-Diethylbenzene 0.171 0.150 0.122 50.580

171 107.174 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.149 0.128 0.107 44.095

172 107.439 135-01-3 Q10 1,2-Diethylbenzene 0.025 0.021 0.018 7.329

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C-97
Hydrocarbon Expert V4.7 Fri Aug 27 15:39:02 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91312 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91312

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 107.886 ? Unidentified 0.017 0.017 0.010 5.741

174 108.025 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.053 0.046 0.038 15.777

175 108.364 I11 C11- Isoparaffin-11 0.145 0.147 0.089 40.533

176 108.549 ? Unidentified 0.030 0.030 0.018 10.360

177 108.876 1758-88-9 Q10 1,4,Dimethyl-2-ethylbenzene 0.128 0.110 0.092 37.874

178 109.038 874-41-9 Q10 1,3-Dimethyl-4-ethylbenzene 0.184 0.158 0.132 54.362

179 109.196 J10 2-Methylindan 0.018 0.014 0.013 5.371

180 109.544 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.296 0.256 0.212 87.465

181 110.097 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.034 0.029 0.024 9.934

182 111.012 Q11 1-Methyl-4-t-butylbenzene 0.018 0.016 0.012 5.316

183 111.222 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.082 0.069 0.059 24.230

184 111.527 1120-21-4 P11 n-Undecane 0.011 0.011 0.007 2.979

185 112.163 Q10 1,2,4,5-Tetramethylbenzene 0.247 0.211 0.177 73.163

186 112.429 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.349 0.297 0.250 103.312

187 113.288 ? Unidentified 0.008 0.008 0.005 2.737

188 113.581 Q11 C11 - Aromatic - 3 0.034 0.029 0.022 10.028

189 113.763 874-35-1 H10 5-Methylindan 0.107 0.091 0.077 31.523

190 113.903 Q12 1,2-Di-i-propylbenzene 0.039 0.034 0.023 11.589

191 114.117 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.058 0.049 0.038 17.138

192 114.274 Q11 C11 - Aromatic - 4 0.030 0.026 0.020 8.867

193 114.514 824-22-6 J10 4-Methylindan 0.145 0.123 0.106 42.951

194 114.765 824-63-5 H10 2-Methylindan 0.143 0.122 0.104 42.465

195 114.978 ? Unidentified 0.010 0.008 0.006 3.345

196 115.091 538-68-1 Q11 n-Pentylbenzene 0.013 0.011 0.009 3.937

197 115.320 Q11 tert-Pentylbenzene 0.059 0.050 0.038 17.315

198 115.633 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.026 0.022 0.017 7.799

199 115.743 Q11 C11 - Aromatic - 7 0.033 0.029 0.021 9.683

200 116.205 100-18-5 Q12 1,4-Di-i-propylbenzene 0.049 0.042 0.029 14.472

201 116.632 91-20-3 G10 Naphthalene 0.118 0.087 0.088 36.509

202 117.090 J11 1,1-Dimethyl Indane 0.012 0.009 0.008 3.651

203 117.431 7364-19-4 Q12 1t-Butyl-4-ethylbenzene 0.013 0.011 0.008 3.857

204 117.737 Q12 1,3-Di-n-propylbenzene 0.044 0.037 0.026 12.870

205 117.847 Q11 C11 - Aromatic - 11 0.025 0.022 0.016 7.224

206 118.40217851-27-2 Q11 1-ethyl-2,4,5-trimethylbenzen 0.017 0.015 0.011 4.960

207 123.282 91-57-6 G11 2-Methylnaphthalene 0.009 0.007 0.006 2.848

208 124.149 90-12-0 G11 1-Methylnaphthalene 0.005 0.004 0.003 1.530

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C-98
Hydrocarbon Expert V4.7 Fri Aug 27 15:39:02 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91312 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91312

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 7.390 74-98-6 Propane 0.007 0.011 0.016 1.931

9.793 106-97-8 n-Butane 2.583 3.375 4.273 706.418

17.696 109-66-0 n-Pentane 2.607 3.148 3.474 717.875

35.297 110-54-3 n-Hexane 1.508 1.729 1.682 416.829

57.622 142-82-5 n-Heptane 0.876 0.969 0.840 243.113

77.569 111-65-9 n-Octane 0.638 0.687 0.537 177.379

91.480 111-84-2 n-Nonane 0.443 0.467 0.332 123.591

102.652 124-18-5 n-Decane 0.057 0.059 0.038 15.850

111.527 1120-21-4 n-Undecane 0.011 0.011 0.007 2.979

I-Paraffins 8.612 75-28-5 i-Butane 0.054 0.074 0.090 14.889

10.390 463-82-1 2,2-Dimethylpropane 0.020 0.026 0.027 5.496

14.714 78-78-4 i-Pentane 5.547 6.771 7.392 1527.638

22.618 75-83-2 2,2-Dimethylbutane 0.173 0.202 0.193 47.941

27.837 79-29-8 2,3-Dimethylbutane 0.464 0.530 0.517 128.182

28.909 107-83-5 2-Methylpentane 2.182 2.527 2.435 603.375

31.551 96-14-0 3-Methylpentane 1.323 1.506 1.476 365.693

41.741 108-08-7 2,4-Dimethylpentane 0.224 0.252 0.215 62.201

42.279 464-06-2 2,2,3-Trimethylbutane 0.025 0.027 0.024 6.945

50.196 591-76-4 2-Methylhexane 0.978 1.089 0.938 271.379

52.032 589-34-4 3-Methylhexane 0.633 0.697 0.608 175.756

54.684 540-84-1 2,2,4-Trimethylpentane 0.250 0.273 0.211 69.577

62.423 590-73-8 2,2-Dimethylhexane 0.033 0.036 0.028 9.183

64.513 564-02-3 2,2,3-Trimethylpentane 0.422 0.446 0.355 117.429

64.757 592-13-2 2,5-Dimethylhexane 0.781 0.852 0.657 217.244

65.096 589-43-5 2,4-Dimethylhexane 0.702 0.758 0.591 195.293

66.335 563-16-6 3,3-Dimethylhexane 0.025 0.027 0.021 7.092

68.129 565-75-3 2,3,4-Trimethylpentane 4.456 4.687 3.751 1239.462

68.837 560-21-4 2,3,3-Trimethylpentane 4.966 5.172 4.180 1381.299

70.439 584-94-1 2,3-Dimethylhexane 1.244 1.321 1.047 346.086

71.704 592-27-8 2-Methylheptane 0.330 0.357 0.277 91.676

71.963 589-53-7 4-Methylheptane 0.240 0.258 0.202 66.823

73.025 589-81-1 3-Methylheptane 0.282 0.302 0.237 78.425

73.210 619-99-8 3-Ethylhexane 0.141 0.150 0.119 39.352

74.944 3522-94-9 2,2,5-Trimethylhexane 2.875 3.075 2.155 801.339

80.059 1069-53-0 2,3,5-Trimethylhexane 0.512 0.536 0.384 142.627

81.235 1071-26-7 2,4-Dimethylheptane 0.096 0.102 0.072 26.839

82.197 1072-05-5 2,6-Dimethylheptane 0.152 0.162 0.114 42.338

83.135 2,5-Dimethylheptane 0.303 0.320 0.227 84.432

83.309 926-82-9 3,5-Dimethylheptane 0.032 0.034 0.024 8.993

87.020 2216-34-4 4-Methyloctane 0.062 0.065 0.046 17.238

87.152 3221-61-2 2-Methyloctane 0.084 0.089 0.063 23.458

88.016 2216-33-3 3-Methyloctane 0.092 0.097 0.069 25.706

89.069 C10 - IsoParaffin - 1 0.626 0.650 0.423 174.741

89.91614720-74-2 2,2,4-trimethylheptane 0.439 0.457 0.297 122.677

93.82415869-87-1 2,2-Dimethyloctane 0.045 0.047 0.030 12.529

94.62515869-89-3 2,5-Dimethyloctane 0.068 0.070 0.046 18.921

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C-99
Hydrocarbon Expert V4.7 Fri Aug 27 15:39:02 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91312 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91312

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

I-Paraffins 95.101 2040-95-1 2,7-Dimethyloctane 0.025 0.026 0.017 7.109

95.266 2051-30-1 2,4-Dimethyloctane 0.103 0.108 0.070 28.899

95.661 2,6-Dimethyloctane 0.038 0.039 0.026 10.618

98.68517301-94-8 4-Methylnonane 0.014 0.015 0.010 4.015

98.891 2,2,6-Trimethyloctane 1.445 1.504 0.976 403.485

99.662 5911-04-6 3-Methylnonane 0.018 0.019 0.012 5.094

100.478 C11-Isoparaffin-2 0.115 0.117 0.071 32.107

102.10817302-01-1 3-Ethyl-3-methylheptane 0.178 0.181 0.109 49.656

104.192 C11 Isoparaffin-4 0.018 0.018 0.011 4.995

106.146 C11-Isoparaffin-7 0.116 0.118 0.071 32.444

108.364 C11- Isoparaffin-11 0.145 0.147 0.089 40.533

Aromatics

Mono-Aromatics 45.140 71-42-3 Benzene 0.624 0.537 0.768 190.375

68.718 108-88-3 Toluene 17.346 15.130 18.100 5233.747

84.459 100-41-4 Ethylbenzene 2.932 2.558 2.656 878.098

85.717 108-38-3 m-Xylene 7.862 6.880 7.121 2354.451

85.858 106-42-3 p-Xylene 3.682 3.234 3.334 1102.488

88.667 95-47-6 o-Xylene 2.125 1.826 1.925 636.409

92.838 98-82-8 i-Propylbenzene 0.038 0.033 0.030 11.256

96.305 103-65-1 n-Propylbenzene 0.307 0.269 0.246 91.310

97.156 620-14-4 1-Methyl-3-ethylbenzene 1.153 1.008 0.922 342.957

97.389 622-96-8 1-Methyl-4-ethylbenzene 0.535 0.470 0.428 159.175

98.015 108-67-8 1,3,5-Trimethylbenzene 0.722 0.631 0.578 214.872

99.099 611-14-3 1-Methyl-2-ethylbenzene 0.398 0.342 0.319 118.476

100.739 95-63-6 1,2,4-Trimethylbenzene 2.029 1.752 1.623 603.617

102.461 538-93-2 i-Butylbenzene 0.183 0.162 0.131 54.023

103.611 526-73-8 1,2,3-Trimethylbenzene 0.320 0.271 0.256 95.211

103.986 535-77-3 1-Methyl-3-i-propylbenzene 0.023 0.020 0.017 6.854

106.332 141-93-5 1,3-Diethylbenzene 0.041 0.036 0.029 12.074

106.617 1074-43-7 1-Methyl-3-n-propylbenzene 0.432 0.379 0.309 127.788

106.948 105-05-5 1,4-Diethylbenzene 0.171 0.150 0.122 50.580

107.174 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.149 0.128 0.107 44.095

107.439 135-01-3 1,2-Diethylbenzene 0.025 0.021 0.018 7.329

108.025 1074-17-5 1-Methyl-2-n-propylbenzene 0.053 0.046 0.038 15.777

108.876 1758-88-9 1,4,Dimethyl-2-ethylbenzene 0.128 0.110 0.092 37.874

109.038 874-41-9 1,3-Dimethyl-4-ethylbenzene 0.184 0.158 0.132 54.362

109.544 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.296 0.256 0.212 87.465

110.097 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.034 0.029 0.024 9.934

111.012 1-Methyl-4-t-butylbenzene 0.018 0.016 0.012 5.316

111.222 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.082 0.069 0.059 24.230

112.163 1,2,4,5-Tetramethylbenzene 0.247 0.211 0.177 73.163

112.429 527-53-7 1,2,3,5-Tetramethylbenzene 0.349 0.297 0.250 103.312

113.581 C11 - Aromatic - 3 0.034 0.029 0.022 10.028

113.903 1,2-Di-i-propylbenzene 0.039 0.034 0.023 11.589

114.117 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.058 0.049 0.038 17.138

114.274 C11 - Aromatic - 4 0.030 0.026 0.020 8.867

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C-100
Hydrocarbon Expert V4.7 Fri Aug 27 15:39:02 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91312 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91312

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 115.091 538-68-1 n-Pentylbenzene 0.013 0.011 0.009 3.937

115.320 tert-Pentylbenzene 0.059 0.050 0.038 17.315

115.633 577-55-9 1-Methyl-2-n-butylbenzene 0.026 0.022 0.017 7.799

115.743 C11 - Aromatic - 7 0.033 0.029 0.021 9.683

116.205 100-18-5 1,4-Di-i-propylbenzene 0.049 0.042 0.029 14.472

117.431 7364-19-4 1t-Butyl-4-ethylbenzene 0.013 0.011 0.008 3.857

117.737 1,3-Di-n-propylbenzene 0.044 0.037 0.026 12.870

117.847 C11 - Aromatic - 11 0.025 0.022 0.016 7.224

118.40217851-27-2 1-ethyl-2,4,5-trimethylbenzen 0.017 0.015 0.011 4.960

Naphthalenes 116.632 91-20-3 Naphthalene 0.118 0.087 0.088 36.509

123.282 91-57-6 2-Methylnaphthalene 0.009 0.007 0.006 2.848

124.149 90-12-0 1-Methylnaphthalene 0.005 0.004 0.003 1.530

Naphtheno/Olefino-Benzs 113.763 874-35-1 5-Methylindan 0.107 0.091 0.077 31.523

114.765 824-63-5 2-Methylindan 0.143 0.122 0.104 42.465

Indenes 104.802 Indan 0.122 0.096 0.099 36.951

105.430 Indene 0.384 0.301 0.312 116.086

109.196 2-Methylindan 0.018 0.014 0.013 5.371

114.514 824-22-6 4-Methylindan 0.145 0.123 0.106 42.951

117.090 1,1-Dimethyl Indane 0.012 0.009 0.008 3.651

Naphthenes

Mono-Naphthenes 27.105 287-92-3 Cyclopentane 0.264 0.268 0.362 74.721

40.161 96-37-7 Methylcyclopentane 1.457 1.472 1.664 412.630

47.060 110-82-7 Cyclohexane 0.942 0.915 1.076 266.886

52.885 1759-58-6 1t,3-Dimethylcyclopentane 0.203 0.205 0.199 57.537

53.474 2532-58-3 1c,3-Dimethylcyclopentane 0.163 0.165 0.159 46.110

54.094 822-50-4 1t,2-Dimethylcyclopentane 0.241 0.243 0.236 68.257

59.20616491-15-9 Cyclopentene, 1,5-dimethyl- 0.018 0.018 0.018 5.091

61.069 108-87-2 Methylcyclohexane 1.455 1.430 1.425 412.203

62.015 4516-69-2 1,1,3-Trimethylcyclopentane 0.041 0.041 0.035 11.584

63.861 1640-89-7 Ethylcyclopentane 0.055 0.055 0.054 15.678

65.930 4850-28-6 1c,2t,4-Trimethylcyclopentane 0.040 0.040 0.034 11.390

67.46415890-40-1 1t,2c,3-Trimethylcyclopentane 0.035 0.035 0.030 9.996

72.867 1,3-dimethyl-t-cyclohexane 0.225 0.221 0.193 63.858

75.274 3c-Ethylmethylcyclopentane 0.013 0.013 0.011 3.696

75.495 3t-Ethylmethylcyclopentane 0.018 0.018 0.015 5.120

76.197 2207-03-6 1t,3-Dimethylcyclohexane 0.103 0.100 0.088 29.111

81.057 2207-01-4 1c,2-Dimethylcyclohexane 0.019 0.018 0.016 5.270

81.870 1678-91-7 Ethylcyclohexane 0.148 0.143 0.127 41.964

89.490 3728-57-2 Cyclopentane, 1-methyl-2-propyl- 0.010 0.009 0.009 3.090

89.644 trans-1,3-Diethylcyclopentane 0.026 0.022 0.020 7.669

92.067 4926-90-3 1,1-Methylethylcyclohexane 0.025 0.023 0.019 7.022

101.320 1678-98-4 i-Butylcyclohexane 0.021 0.020 0.014 5.975

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.405 115-11-7 Isobutene 0.015 0.019 0.025 4.205

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C-101
Hydrocarbon Expert V4.7 Fri Aug 27 15:39:02 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91312 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91312

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

n-Olefins 9.444 106-98-9 Butene-1 0.018 0.023 0.031 5.095

10.268 624-64-6 t-Butene-2 0.071 0.088 0.121 19.989

10.988 590-18-1 c-Butene-2 0.083 0.102 0.143 23.628

16.337 109-67-1 Pentene-1 0.325 0.384 0.446 92.164

18.804 646-04-8 t-Pentene-2 0.826 0.964 1.133 234.031

19.828 627-20-3 c-Pentene-2 0.452 0.521 0.620 128.015

32.942 592-41-6 Hexene-1 0.159 0.178 0.182 45.116

35.94013269-52-8 t-Hexene-3 0.260 0.288 0.297 73.558

36.412 4050-45-7 t-Hexene-2 0.498 0.551 0.569 141.009

38.244 7688-21-3 c-Hexene-2 0.212 0.232 0.242 60.014

55.028 592-76-7 Heptene-1 0.030 0.032 0.029 8.363

56.88414686-14-7 t-Heptene-3 0.032 0.035 0.032 9.165

57.837 7642-10-6 c-Heptene-3 0.024 0.026 0.023 6.742

58.74514686-13-6 t-Heptene-2 0.015 0.016 0.014 4.121

Iso-Olefins 13.131 563-45-1 3-Methylbutene-1 0.067 0.081 0.092 19.045

17.169 563-46-2 2-Methylbutene-1 0.495 0.576 0.679 140.224

20.489 513-35-9 2-Methylbutene-2 1.018 1.163 1.396 288.432

28.690 691-38-3 4-Methyl-c-pentene-2 0.043 0.048 0.049 12.156

29.343 674-76-0 4-Methyl-t-pentene-2 0.129 0.145 0.147 36.488

32.728 763-29-1 2-Methylpentene-1 0.222 0.245 0.253 62.795

36.908 625-27-4 2-Methylpentene-2 0.337 0.369 0.385 95.505

37.313 922-62-3 3-Methyl-c-pentene-2 0.260 0.282 0.297 73.741

39.591 3404-73-7 3,3-Dimethylpentene-1 0.309 0.333 0.303 87.618

42.042 594-56-9 2,3,3-Trimethylbutene-1 0.014 0.015 0.014 3.992

46.164 3404-61-3 3-Methylhexene-1 0.016 0.017 0.015 4.435

46.748 3524-73-0 5-Methylhexene-1 0.057 0.062 0.056 16.240

48.80615840-60-5 2-Methyl-c-hexene-3 0.040 0.044 0.039 11.419

49.800 3404-55-5 4-Methyl-t/c-hexene-2 0.051 0.055 0.050 14.377

54.398 C7 - Iso-Olefin - 2 0.022 0.023 0.022 6.324

56.362 4914-89-0 3-Methyl-c-hexene-3 0.014 0.015 0.014 4.003

57.246 6094-02-6 2-Methylhexene-1 0.058 0.063 0.056 16.332

58.117 2738-19-4 2-Methyl-2-hexene 0.026 0.028 0.026 7.433

58.361 3899-36-3 3-Methyl-t-hexene-3 0.020 0.022 0.019 5.618

59.64820710-38-8 3-Methyl-t-hexene-2 0.015 0.016 0.015 4.321

60.432 4914-91-4 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.014 0.013 3.802

70.138 C8 - Diolefin - 1 0.015 0.015 0.013 4.307

80.618 C9 - IsoOlefin - 1 0.021 0.021 0.018 6.075

86.224 C9-IsoOlefin-3 0.020 0.020 0.015 5.719

Naphtheno-Olefins 25.252 142-29-0 Cyclopentene 0.193 0.189 0.272 56.283

45.344 693-89-0 1-Methylcyclopentene 0.362 0.351 0.424 105.055

50.674 110-83-8 Cyclohexene 0.044 0.041 0.052 12.514

Di-Olefins 18.207 78-79-5 2-Methyl-1,3-Butadiene 0.010 0.011 0.014 2.901

20.825 2004-70-8 1t,3-Pentadiene 0.015 0.016 0.021 4.266

Oxygenates 26.492 71-23-8 n-Propanol 0.112 0.106 0.179 22.154

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C-102
Hydrocarbon Expert V4.7 Fri Aug 27 15:39:02 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91312 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91312

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Oxygenates

Unidentified 19.444 Unidentified 0.006 0.007 0.008 1.945

22.077 Unidentified 0.006 0.006 0.008 1.965

26.420 Unidentified 0.037 0.035 0.059 12.823

28.231 Unidentified 0.051 0.052 0.055 17.571

44.937 Unidentified 0.012 0.012 0.014 4.097

47.596 Unidentified 0.034 0.037 0.034 11.948

72.099 Unidentified 0.110 0.115 0.092 38.113

74.105 Unidentified 0.036 0.035 0.031 12.411

75.911 Unidentified 0.021 0.021 0.018 7.347

78.511 Unidentified 0.079 0.077 0.068 27.364

82.675 Unidentified 0.032 0.031 0.027 11.121

84.623 Unidentified 0.039 0.040 0.030 13.534

84.866 Unidentified 0.049 0.047 0.037 16.845

86.330 Unidentified 0.019 0.019 0.015 6.658

88.484 Unidentified 0.198 0.219 0.151 68.672

93.029 Unidentified 0.022 0.021 0.017 7.692

93.029 Unidentified 0.022 0.024 0.015 7.692

93.029 Unidentified 0.022 0.017 0.015 7.692

93.601 Unidentified 0.128 0.134 0.087 44.490

94.269 Unidentified 0.008 0.006 0.778 2.807

94.269 Unidentified 0.008 0.009 0.006 2.807

100.128 Unidentified 0.079 0.060 0.049 27.488

100.254 Unidentified 0.216 0.220 0.133 75.093

100.942 Unidentified 0.128 0.138 0.088 44.457

101.063 Unidentified 0.076 0.078 0.051 26.411

102.975 Unidentified 0.040 0.041 0.025 13.917

104.396 Unidentified 0.079 0.069 0.056 27.282

107.886 Unidentified 0.017 0.017 0.010 5.741

108.549 Unidentified 0.030 0.030 0.018 10.360

113.288 Unidentified 0.008 0.008 0.005 2.737

114.978 Unidentified 0.010 0.008 0.006 3.345

Plus

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C-103
Hydrocarbon Expert V4.7 Fri Aug 27 15:39:02 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91312 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91312

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF

20.0 15.0 10.0 5.0 0.0

Propane

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

Unidentified

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

Unidentified

2,2-Dimethylbutane

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C-104
Hydrocarbon Expert V4.7 Fri Aug 27 15:39:02 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91312 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91312

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

Unidentified n-Propanol

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

n-Hexane

t-Hexene-3

t-Hexene-2

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane 2,3,3-Trimethylbutene-1 2,2,3-Trimethylbutane

Unidentified Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1 Cyclohexane

Unidentified

2-Methyl-c-hexene-3

4-Methyl-t/c-hexene-2

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C-105
Hydrocarbon Expert V4.7 Fri Aug 27 15:39:02 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91312 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91312

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF

70.0 65.0 60.0 55.0 50.0

2-Methylhexane

Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane C7 - Iso-Olefin - 2 2,2,4-Trimethylpentane

Heptene-1

3-Methyl-c-hexene-3

t-Heptene-3

2-Methylhexene-1

n-Heptane c-Heptene-3 2-Methyl-2-hexene 3-Methyl-t-hexene-3

t-Heptene-2

Cyclopentene, 1,5-dimethyl3-Methyl-t-hexene-2

2-Pentene, 3,4-dimethyl-, (Z)-

Methylcyclohexane

1,1,3-Trimethylcyclopentane

2,2-Dimethylhexane

Ethylcyclopentane

2,2,3-Trimethylpentane 2,5-Dimethylhexane

2,4-Dimethylhexane

1c,2t,4-Trimethylcyclopentane

3,3-Dimethylhexane

1t,2c,3-Trimethylcyclopentane

2,3,4-Trimethylpentane

2,3,3-Trimethylpentane Toluene

C8 - Diolefin - 1 2,3-Dimethylhexane

2-Methylheptane

Unidentified 4-Methylheptane

1,3-dimethyl-t-cyclohexane 3-Methylheptane 3-Ethylhexane

Unidentified

2,2,5-Trimethylhexane

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C-106
Hydrocarbon Expert V4.7 Fri Aug 27 15:39:02 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91312 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91312

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF

95.0 90.0 85.0 80.0 75.0

3c-Ethylmethylcyclopentane 3t-Ethylmethylcyclopentane

Unidentified 1t,3-Dimethylcyclohexane

n-Octane

Unidentified

2,3,5-Trimethylhexane

C9 - IsoOlefin - 1

1c,2-Dimethylcyclohexane 2,4-Dimethylheptane

Ethylcyclohexane

2,6-Dimethylheptane

Unidentified

2,5-Dimethylheptane 3,5-Dimethylheptane

Ethylbenzene Unidentified

m-Xylene p-Xylene

C9-IsoOlefin-3 Unidentified

4-Methyloctane 2-Methyloctane

3-Methyloctane

Unidentified o-Xylene

C10 - IsoParaffin - 1

Cyclopentane, 1-methyl-2-propyl- trans-1,3-Diethylcyclopentane 2,2,4-trimethylheptane

n-Nonane

1,1-Methylethylcyclohexane

i-Propylbenzene Unidentified

Unidentified 2,2-Dimethyloctane

Unidentified

2,5-Dimethyloctane

2,7-Dimethyloctane 2,4-Dimethyloctane

2,6-Dimethyloctane

n-Propylbenzene

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

4-Methylnonane 2,2,6-Trimethyloctane 1-Methyl-2-ethylbenzene

3-Methylnonane

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C-107
Hydrocarbon Expert V4.7 Fri Aug 27 15:39:02 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91312 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91312

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified Unidentified C11-Isoparaffin-2 1,2,4-Trimethylbenzene Unidentified

i-Butylcyclohexane

3-Ethyl-3-methylheptane

i-Butylbenzene n-Decane

Unidentified

1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene C11 Isoparaffin-4 Unidentified

Indan

Indene

C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene

1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

Unidentified 1-Methyl-2-n-propylbenzene

C11- Isoparaffin-11 Unidentified

1,4,Dimethyl-2-ethylbenzene 1,3-Dimethyl-4-ethylbenzene 2-Methylindan

1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

1-Methyl-4-t-butylbenzene 1,2-Dimethyl-3-ethylbenzene n-Undecane

1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene

Unidentified C11 - Aromatic - 3 5-Methylindan 1,2-Di-i-propylbenzene

C11 - Aromatic - 4 1-methyl-4-(1-methylpropyl)be

4-Methylindan 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene 1-Methyl-2-n-butylbenzene C11 - Aromatic - 7

1,4-Di-i-propylbenzene

Naphthalene

1,1-Dimethyl Indane

1t-Butyl-4-ethylbenzene

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

1-ethyl-2,4,5-trimethylbenzen

2-Methylnaphthalene

1-Methylnaphthalene

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C-108
Hydrocarbon Expert V4.7 Fri Aug 27 15:39:02 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91312 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91312

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000017.D\SIG1000017_FID1_A.CDF

145.0 140.0 135.0 130.0 125.0

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C-109
Hydrocarbon Expert V4.7 Thu Aug 26 10:08:56 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91313 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91313

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 6.856 7.845 7.555

I-Paraffins 41.626 44.836 35.885

Aromatics 24.375 20.489 19.484

Mono-Aromatics 21.929 18.602 17.708

Naphthalenes 0.104 0.075 0.070

Naphtheno/Olefino-Benzs 0.194 0.161 0.129

Indenes 2.148 1.652 1.577

Naphthenes 3.309 3.216 3.407

Mono-Naphthenes 3.309 3.216 3.407

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 8.753 9.551 9.904

n-Olefins 4.609 5.098 5.225

Iso-Olefins 3.506 3.844 3.944

Naphtheno-Olefins 0.613 0.580 0.702

Di-Olefins 0.026 0.028 0.033

Oxygenates 9.688 9.057 18.459

Unidentified 5.393 5.006 5.305

Plus 0.000 0.000 0.000

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C-110
Hydrocarbon Expert V4.7 Thu Aug 26 10:08:56 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91313 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91313

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C2 9.506 8.889 18.193

C3 0.182 0.168 0.267

C4 1.266 1.602 1.931

C5 8.230 9.515 10.198

C6 24.737 26.860 25.571

C7 9.511 9.020 8.796

C8 19.219 19.034 15.155

C9 7.222 6.401 5.228

C10 11.881 10.772 7.732

C11 2.677 2.581 1.529

C12 0.178 0.153 0.096

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C-111
Hydrocarbon Expert V4.7 Thu Aug 26 10:08:56 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91313 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91313

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C4 1.053 1.342 1.597

C5 0.830 0.978 1.014

C6 4.467 4.998 4.571

C7 0.210 0.226 0.184

C8 0.025 0.026 0.019

C9 0.107 0.110 0.073

C10 0.060 0.060 0.037

C11 0.105 0.104 0.059

I-Paraffins C4 0.021 0.028 0.032

C5 3.608 4.296 4.409

C6 12.698 14.234 12.992

C7 2.835 3.081 2.494

C8 13.722 14.348 10.591

C9 1.439 1.496 0.989

C10 5.219 5.287 3.205

C11 2.046 2.029 1.154

C12 0.038 0.037 0.019

Mono-Aromatics C6 0.830 0.697 0.937

C7 5.273 4.487 5.046

C8 5.472 4.660 4.545

C9 5.488 4.651 4.026

C10 4.320 3.652 2.838

C11 0.405 0.339 0.241

C12 0.140 0.116 0.076

Naphthalenes C10 0.086 0.062 0.059

C11 0.018 0.013 0.011

Naphtheno/Olefino-Benzs C10 0.194 0.161 0.129

Indenes C9 0.184 0.141 0.137

C10 1.936 1.489 1.423

C11 0.028 0.021 0.017

Mono-Naphthenes C5 0.134 0.133 0.168

C6 2.711 2.632 2.840

C7 0.399 0.390 0.358

C9 0.004 0.004 0.003

C10 0.061 0.057 0.039

n-Olefins C4 0.192 0.232 0.302

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C-112
Hydrocarbon Expert V4.7 Thu Aug 26 10:08:56 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91313 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91313

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

n-Olefins C5 1.637 1.862 2.058

C6 2.601 2.820 2.725

C7 0.104 0.110 0.094

C11 0.075 0.074 0.047

Iso-Olefins C5 1.798 2.030 2.261

C6 1.013 1.085 1.061

C7 0.690 0.725 0.620

C10 0.004 0.004 0.003

Naphtheno-Olefins C5 0.197 0.188 0.255

C6 0.416 0.392 0.447

Di-Olefins C5 0.026 0.028 0.033

Oxygenates C2 9.506 8.889 18.193

C3 0.182 0.168 0.267

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C-113
Hydrocarbon Expert V4.7 Thu Aug 26 10:08:56 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91313 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91313

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 25.07 24.01

5% 81.73 80.99

10% 133.69 100.24

15% 139.15 138.19

20% 144.63 140.31

25% 153.05 145.52

30% 155.55 154.43

35% 172.46 157.59

40% 173.02 172.60

45% 177.21 173.21

50% 209.56 193.46

55% 228.46 209.90

60% 230.79 229.87

65% 237.35 232.45

70% 277.56 239.32

75% 303.39 281.69

80% 331.87 322.74

85% 336.04 332.54

90% 358.69 352.22

95% 363.20 363.20

FBP 402.18 393.64

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C-114
Hydrocarbon Expert V4.7 Thu Aug 26 10:08:56 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91313 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91313

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 8.611 75-28-5 I4 i-Butane 0.021 0.028 0.032 5.507

2 9.404 115-11-7 K4 Isobutene 0.015 0.019 0.024 4.181

3 9.442 106-98-9 K4 Butene-1 0.019 0.023 0.029 5.037

4 9.791 106-97-8 P4 n-Butane 1.053 1.342 1.597 275.365

5 10.265 624-64-6 K4 t-Butene-2 0.073 0.089 0.114 19.651

6 10.387 463-82-1 I5 2,2-Dimethylpropane 0.008 0.010 0.010 2.212

7 10.986 590-18-1 K4 c-Butene-2 0.086 0.102 0.135 23.193

8 12.745 64-17-5 X2 Ethanol 9.506 8.889 18.193 1107.028

9 13.121 563-45-1 C5 3-Methylbutene-1 0.258 0.303 0.324 69.877

10 14.703 78-78-4 I5 i-Pentane 3.599 4.286 4.398 948.107

11 16.329 109-67-1 K5 Pentene-1 0.332 0.382 0.417 89.856

12 17.170 563-46-2 C5 2-Methylbutene-1 0.504 0.571 0.633 136.420

13 17.690 109-66-0 P5 n-Pentane 0.830 0.978 1.014 218.613

14 18.200 78-79-5 E5 2-Methyl-1,3-Butadiene 0.010 0.011 0.014 2.910

15 18.796 646-04-8 K5 t-Pentene-2 0.843 0.959 1.059 228.284

16 19.820 627-20-3 K5 c-Pentene-2 0.463 0.521 0.581 125.316

17 20.489 513-35-9 C5 2-Methylbutene-2 1.037 1.155 1.304 280.960

18 20.818 2004-70-8 E5 1t,3-Pentadiene 0.015 0.017 0.020 4.247

19 22.065 ? Unidentified 0.006 0.006 0.008 1.914

20 22.615 75-83-2 I6 2,2-Dimethylbutane 0.101 0.115 0.103 26.713

21 25.246 142-29-0 B5 Cyclopentene 0.197 0.188 0.255 54.978

22 26.486 71-23-8 X3 n-Propanol 0.182 0.168 0.267 34.488

23 27.097 287-92-3 M5 Cyclopentane 0.134 0.133 0.168 36.306

24 27.829 79-29-8 I6 2,3-Dimethylbutane 1.479 1.649 1.513 391.141

25 28.236 ? Unidentified 0.050 0.050 0.050 16.756

26 28.688 691-38-3 C6 4-Methyl-c-pentene-2 0.043 0.047 0.045 11.722

27 28.927 107-83-5 I6 2-Methylpentane 6.385 7.213 6.533 1688.583

28 29.333 674-76-0 C6 4-Methyl-t-pentene-2 0.131 0.144 0.137 35.501

29 31.568 96-14-0 I6 3-Methylpentane 4.733 5.257 4.843 1251.770

30 32.719 763-29-1 C6 2-Methylpentene-1 0.224 0.241 0.235 60.708

31 32.943 592-41-6 K6 Hexene-1 1.605 1.747 1.682 434.942

32 35.306 110-54-3 P6 n-Hexane 4.467 4.998 4.571 1181.419

33 35.93413269-52-8 K6 t-Hexene-3 0.269 0.291 0.282 72.948

34 36.403 4050-45-7 K6 t-Hexene-2 0.510 0.551 0.534 138.223

35 36.896 625-27-4 C6 2-Methylpentene-2 0.345 0.368 0.361 93.457

36 37.312 922-62-3 C6 3-Methyl-c-pentene-2 0.269 0.285 0.282 72.981

37 38.230 7688-21-3 K6 c-Hexene-2 0.216 0.231 0.227 58.623

38 39.580 3404-73-7 C7 3,3-Dimethylpentene-1 0.318 0.334 0.286 86.204

39 40.153 96-37-7 M6 Methylcyclopentane 1.672 1.648 1.751 452.929

40 41.731 108-08-7 I7 2,4-Dimethylpentane 0.857 0.940 0.754 227.620

41 42.032 594-56-9 C7 2,3,3-Trimethylbutene-1 0.014 0.014 0.012 3.663

42 42.272 464-06-2 I7 2,2,3-Trimethylbutane 0.072 0.077 0.063 19.045

43 44.929 ? Unidentified 0.012 0.012 0.013 3.921

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C-115
Hydrocarbon Expert V4.7 Thu Aug 26 10:08:56 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91313 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91313

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 45.131 71-42-3 Q6 Benzene 0.830 0.697 0.937 242.286

45 45.334 693-89-0 B6 1-Methylcyclopentene 0.370 0.350 0.397 102.706

46 46.159 3404-61-3 C7 3-Methylhexene-1 0.016 0.017 0.014 4.268

47 46.742 3524-73-0 C7 5-Methylhexene-1 0.063 0.067 0.057 17.127

48 47.050 110-82-7 M6 Cyclohexane 1.039 0.985 1.088 281.457

49 47.593 ? Unidentified 0.035 0.037 0.032 11.652

50 48.80015840-60-5 C7 2-Methyl-c-hexene-3 0.041 0.044 0.037 11.222

51 49.146 3769-23-1 C7 4-Methylhexene-1 0.011 0.011 0.010 2.927

52 49.791 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.053 0.055 0.047 14.243

53 50.196 591-76-4 I7 2-Methylhexane 1.344 1.461 1.182 356.780

54 50.669 110-83-8 B6 Cyclohexene 0.046 0.042 0.049 12.422

55 52.025 589-34-4 I7 3-Methylhexane 0.562 0.603 0.494 149.213

56 52.879 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.116 0.115 0.104 31.489

57 53.466 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.080 0.080 0.072 21.787

58 54.096 822-50-4 M7 1t,2-Dimethylcyclopentane 0.094 0.093 0.085 25.565

59 54.418 C7 C7 - Iso-Olefin - 2 0.023 0.024 0.021 6.216

60 54.725 540-84-1 I8 2,2,4-Trimethylpentane 5.835 6.222 4.504 1552.483

61 55.019 592-76-7 K7 Heptene-1 0.030 0.032 0.027 8.231

62 56.355 4914-89-0 C7 3-Methyl-c-hexene-3 0.014 0.015 0.013 3.864

63 56.87814686-14-7 K7 t-Heptene-3 0.033 0.034 0.029 8.876

64 57.239 6094-02-6 C7 2-Methylhexene-1 0.058 0.062 0.052 15.835

65 57.611 142-82-5 P7 n-Heptane 0.210 0.226 0.184 55.631

66 57.831 7642-10-6 K7 c-Heptene-3 0.025 0.026 0.023 6.797

67 58.110 2738-19-4 C7 2-Methyl-2-hexene 0.026 0.027 0.024 7.119

68 58.355 3899-36-3 C7 3-Methyl-t-hexene-3 0.020 0.021 0.018 5.432

69 58.74014686-13-6 K7 t-Heptene-2 0.016 0.017 0.014 4.353

70 59.20016491-15-9 M7 Cyclopentene, 1,5-dimethyl- 0.019 0.018 0.017 5.035

71 59.64120710-38-8 C7 3-Methyl-t-hexene-2 0.016 0.016 0.014 4.306

72 60.425 4914-91-4 C7 2-Pentene, 3,4-dimethyl-, (Z)- 0.017 0.017 0.015 4.615

73 61.051 108-87-2 M7 Methylcyclohexane 0.089 0.085 0.080 24.121

74 63.108 ? Unidentified 0.019 0.020 0.015 6.363

75 64.507 564-02-3 I8 2,2,3-Trimethylpentane 0.324 0.334 0.250 86.182

76 64.750 592-13-2 I8 2,5-Dimethylhexane 0.740 0.787 0.571 196.892

77 65.089 589-43-5 I8 2,4-Dimethylhexane 0.711 0.749 0.549 189.097

78 68.091 565-75-3 I8 2,3,4-Trimethylpentane 2.613 2.681 2.017 695.175

79 68.621 108-88-3 Q7 Toluene 5.273 4.487 5.046 1521.901

80 68.764 560-21-4 I8 2,3,3-Trimethylpentane 2.646 2.689 2.042 704.029

81 70.428 584-94-1 I8 2,3-Dimethylhexane 0.691 0.716 0.533 183.818

82 71.695 592-27-8 I8 2-Methylheptane 0.043 0.045 0.033 11.357

83 71.961 589-53-7 I8 4-Methylheptane 0.077 0.081 0.060 20.531

84 72.092 ? Unidentified 0.054 0.055 0.041 17.834

85 73.020 589-81-1 I8 3-Methylheptane 0.042 0.044 0.032 11.085

86 74.926 3522-94-9 I9 2,2,5-Trimethylhexane 1.122 1.170 0.771 299.057

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C-116
Hydrocarbon Expert V4.7 Thu Aug 26 10:08:56 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91313 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91313

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 75.907 ? Unidentified 0.009 0.008 0.006 2.826

88 77.563 111-65-9 P8 n-Octane 0.025 0.026 0.019 6.608

89 78.506 ? Unidentified 0.026 0.026 0.018 8.529

90 80.054 1069-53-0 I9 2,3,5-Trimethylhexane 0.176 0.180 0.121 46.915

91 81.233 1071-26-7 I9 2,4-Dimethylheptane 0.027 0.028 0.019 7.264

92 82.194 1072-05-5 I9 2,6-Dimethylheptane 0.030 0.031 0.020 7.894

93 83.128 I9 2,5-Dimethylheptane 0.077 0.080 0.053 20.613

94 84.440 100-41-4 Q8 Ethylbenzene 0.982 0.835 0.815 281.186

95 84.617 ? Unidentified 0.012 0.012 0.008 3.921

96 84.859 ? Unidentified 0.010 0.009 0.007 3.248

97 85.669 108-38-3 Q8 m-Xylene 2.519 2.151 2.092 721.507

98 85.817 106-42-3 Q8 p-Xylene 1.160 0.994 0.963 332.176

99 85.963 ? Unidentified 0.026 0.026 0.018 8.624

100 88.011 2216-33-3 I9 3-Methyloctane 0.007 0.007 0.005 1.752

101 88.479 ? Unidentified 0.048 0.052 0.034 15.974

102 88.652 95-47-6 Q8 o-Xylene 0.812 0.681 0.674 232.555

103 89.067 I10 C10 - IsoParaffin - 1 0.172 0.174 0.107 45.911

104 89.91314720-74-2 I10 2,2,4-trimethylheptane 0.122 0.123 0.075 32.507

105 91.460 111-84-2 P9 n-Nonane 0.107 0.110 0.073 28.498

106 92.085 ? Unidentified 0.011 0.010 0.007 3.546

107 92.838 98-82-8 Q9 i-Propylbenzene 0.030 0.026 0.022 8.569

108 93.028 ? Unidentified 0.011 0.010 0.008 3.580

109 93.028 ? Unidentified 0.011 0.011 0.007 3.580

110 93.028 ? Unidentified 0.011 0.008 0.007 3.580

111 93.138 696-29-7 M9 1-Methyl-2-propyl-cyclopentan 0.004 0.004 0.003 1.142

112 93.138 C10 C10-IsoOlefin-4 0.004 0.004 0.003 1.142

113 93.138 I10 C10-isoparaffin-x 0.000 0.000 0.000 1.142

114 93.602 ? Unidentified 0.159 0.162 0.099 52.853

115 93.82515869-87-1 I10 2,2-Dimethyloctane 0.055 0.056 0.034 14.762

116 94.267 ? Unidentified 0.022 0.016 1.949 7.338

117 94.267 ? Unidentified 0.022 0.023 0.014 7.338

118 94.487 ? Unidentified 0.021 0.019 0.015 6.923

119 94.62515869-89-3 I10 2,5-Dimethyloctane 0.092 0.092 0.057 24.444

120 95.019 ? Unidentified 0.021 0.021 0.013 6.923

121 95.104 2040-95-1 I10 2,7-Dimethyloctane 0.026 0.026 0.016 6.899

122 95.268 2051-30-1 I10 2,4-Dimethyloctane 0.243 0.246 0.151 64.889

123 95.661 I10 2,6-Dimethyloctane 0.069 0.070 0.043 18.544

124 96.306 103-65-1 Q9 n-Propylbenzene 0.331 0.284 0.243 94.310

125 97.155 620-14-4 Q9 1-Methyl-3-ethylbenzene 1.193 1.018 0.875 339.465

126 97.389 622-96-8 Q9 1-Methyl-4-ethylbenzene 0.543 0.465 0.399 154.616

127 98.015 108-67-8 Q9 1,3,5-Trimethylbenzene 0.758 0.646 0.556 215.659

128 98.69017301-94-8 I10 4-Methylnonane 0.013 0.013 0.008 3.465

129 98.907 I10 2,2,6-Trimethyloctane 3.876 3.937 2.402 1035.316

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C-117
Hydrocarbon Expert V4.7 Thu Aug 26 10:08:56 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91313 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91313

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 99.100 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.395 0.331 0.290 112.335

131 99.475 ? Unidentified 0.012 0.012 0.007 3.902

132 99.665 5911-04-6 I10 3-Methylnonane 0.019 0.019 0.012 5.104

133 99.841 ? Unidentified 0.011 0.011 0.007 3.552

134 100.131 ? Unidentified 0.222 0.164 0.125 73.829

135 100.258 ? Unidentified 0.622 0.617 0.351 206.582

136 100.481 I11 C11-Isoparaffin-2 0.329 0.326 0.185 87.844

137 100.740 95-63-6 Q9 1,2,4-Trimethylbenzene 2.000 1.685 1.467 569.076

138 100.946 ? Unidentified 0.372 0.391 0.234 123.449

139 101.068 ? Unidentified 0.220 0.222 0.137 73.129

140 101.324 1678-98-4 M10 i-Butylcyclohexane 0.059 0.055 0.037 16.027

141 101.969 ? Unidentified 0.025 0.023 0.016 8.214

142 102.11217302-01-1 I10 3-Ethyl-3-methylheptane 0.533 0.529 0.301 142.528

143 102.323 ? Unidentified 0.140 0.121 0.092 46.622

144 102.465 ? Unidentified 0.331 0.286 0.217 109.800

145 102.660 124-18-5 P10 n-Decane 0.060 0.060 0.037 15.982

146 102.976 ? Unidentified 0.146 0.145 0.082 48.425

147 103.468 ? Unidentified 0.017 0.014 0.013 5.658

148 103.614 526-73-8 Q9 1,2,3-Trimethylbenzene 0.238 0.196 0.174 67.684

149 103.977 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.039 0.033 0.025 10.974

150 104.193 I11 C11 Isoparaffin-4 0.062 0.061 0.035 16.566

151 104.398 ? Unidentified 0.325 0.280 0.213 107.836

152 104.808 J9 Indan 0.184 0.141 0.137 53.261

153 105.061 I11 C11-Isoparaffin-5 0.027 0.027 0.015 7.346

154 105.442 J10 Indene 1.660 1.270 1.238 480.056

155 105.856 M10 n-ButylCyclohexane 0.002 0.002 0.001 0.589

156 105.995 ? Unidentified 0.013 0.012 0.008 4.456

157 106.156 I11 C11-Isoparaffin-7 0.601 0.596 0.339 160.585

158 106.336 141-93-5 Q10 1,3-Diethylbenzene 0.025 0.022 0.017 7.189

159 106.638 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 1.731 1.484 1.137 490.089

160 106.904 105-05-5 Q10 1,4-Diethylbenzene 0.439 0.376 0.288 124.232

161 107.177 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.102 0.085 0.067 28.836

162 107.423 135-01-3 Q10 1,2-Diethylbenzene 0.128 0.107 0.084 36.211

163 107.890 ? Unidentified 0.140 0.139 0.079 46.418

164 108.027 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.046 0.039 0.031 13.154

165 108.164 ? Unidentified 0.138 0.137 0.079 45.652

166 108.245 ? Unidentified 0.126 0.125 0.071 41.797

167 108.370 I11 C11- Isoparaffin-11 1.028 1.019 0.580 274.780

168 108.550 ? Unidentified 0.328 0.326 0.185 109.027

169 108.983 ? Unidentified 0.928 0.781 0.610 308.045

170 109.206 J10 2-Methylindan 0.153 0.117 0.102 44.354

171 109.544 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.345 0.291 0.227 97.622

172 109.703 ? Unidentified 0.066 0.050 0.044 21.863

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C-118
Hydrocarbon Expert V4.7 Thu Aug 26 10:08:56 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91313 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91313

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 110.102 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.834 0.691 0.548 236.002

174 110.528 ? Unidentified 0.034 0.031 0.019 11.232

175 110.730 693-61-8 K11 2-Undecene, (E)- 0.075 0.074 0.047 19.997

176 110.858 ? Unidentified 0.161 0.160 0.101 53.348

177 111.131 ? Unidentified 0.143 0.124 0.085 47.335

178 111.214 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.070 0.058 0.046 19.869

179 111.531 1120-21-4 P11 n-Undecane 0.105 0.104 0.059 28.170

180 111.687 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.114 0.095 0.068 32.259

181 111.798 ? Unidentified 0.080 0.066 0.048 26.517

182 112.164 Q10 1,2,4,5-Tetramethylbenzene 0.242 0.201 0.159 68.488

183 112.430 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.319 0.264 0.209 90.269

184 112.654 ? Unidentified 0.015 0.012 0.009 4.881

185 112.784 ? Unidentified 0.022 0.018 0.015 7.391

186 112.966 I12 C12 - IsoParaffin - 1 0.030 0.030 0.016 8.132

187 113.294 ? Unidentified 0.036 0.036 0.019 11.991

188 113.448 ? Unidentified 0.014 0.014 0.007 4.649

189 113.585 Q11 C11 - Aromatic - 3 0.029 0.024 0.017 8.230

190 113.654 ? Unidentified 0.040 0.033 0.024 13.292

191 113.761 874-35-1 H10 5-Methylindan 0.097 0.080 0.065 27.430

192 113.901 Q12 1,2-Di-i-propylbenzene 0.043 0.036 0.023 12.053

193 114.117 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.058 0.048 0.034 16.342

194 114.293 Q11 C11 - Aromatic - 4 0.037 0.030 0.022 10.358

195 114.514 824-22-6 J10 4-Methylindan 0.123 0.102 0.082 34.770

196 114.682 ? Unidentified 0.028 0.023 0.017 9.294

197 114.765 824-63-5 H10 2-Methylindan 0.097 0.081 0.065 27.522

198 114.978 ? Unidentified 0.012 0.010 0.007 4.092

199 115.090 538-68-1 Q11 n-Pentylbenzene 0.014 0.012 0.009 4.060

200 115.320 Q11 tert-Pentylbenzene 0.053 0.044 0.032 15.033

201 115.633 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.027 0.022 0.016 7.536

202 115.744 Q11 C11 - Aromatic - 7 0.042 0.036 0.025 11.771

203 116.093 I12 C12 - IsoParaffin - 4 0.007 0.007 0.004 2.022

204 116.206 100-18-5 Q12 1,4-Di-i-propylbenzene 0.048 0.040 0.026 13.409

205 116.635 91-20-3 G10 Naphthalene 0.086 0.062 0.059 25.500

206 116.797 J11 4,7-Dimethyl Indane 0.016 0.013 0.010 4.756

207 116.972 ? Unidentified 0.006 0.005 0.003 1.841

208 117.080 J11 1,1-Dimethyl Indane 0.011 0.009 0.007 3.301

209 117.432 7364-19-4 Q12 1t-Butyl-4-ethylbenzene 0.015 0.013 0.008 4.263

210 117.735 Q12 1,3-Di-n-propylbenzene 0.034 0.028 0.019 9.625

211 117.847 Q11 C11 - Aromatic - 11 0.018 0.016 0.011 5.154

212 118.402 Q11 C11 - Aromatic - 12 0.012 0.011 0.007 3.456

213 123.281 91-57-6 G11 2-Methylnaphthalene 0.012 0.009 0.007 3.554

214 124.145 90-12-0 G11 1-Methylnaphthalene 0.005 0.004 0.003 1.616

215 125.444 ? Unidentified 0.003 0.003 0.002 1.118

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C-119
Hydrocarbon Expert V4.7 Thu Aug 26 10:08:56 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91313 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91313

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

216 126.172 ? Unidentified 0.006 0.005 0.003 2.120

217 126.172 ? Unidentified 0.006 0.005 0.003 2.120

218 126.172 ? Unidentified 0.006 0.006 0.003 2.120

219 129.864 ? Unidentified 0.003 0.003 0.002 1.106

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C-120
Hydrocarbon Expert V4.7 Thu Aug 26 10:08:56 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91313 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91313

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 9.791 106-97-8 n-Butane 1.053 1.342 1.597 275.365

17.690 109-66-0 n-Pentane 0.830 0.978 1.014 218.613

35.306 110-54-3 n-Hexane 4.467 4.998 4.571 1181.419

57.611 142-82-5 n-Heptane 0.210 0.226 0.184 55.631

77.563 111-65-9 n-Octane 0.025 0.026 0.019 6.608

91.460 111-84-2 n-Nonane 0.107 0.110 0.073 28.498

102.660 124-18-5 n-Decane 0.060 0.060 0.037 15.982

111.531 1120-21-4 n-Undecane 0.105 0.104 0.059 28.170

I-Paraffins 8.611 75-28-5 i-Butane 0.021 0.028 0.032 5.507

10.387 463-82-1 2,2-Dimethylpropane 0.008 0.010 0.010 2.212

14.703 78-78-4 i-Pentane 3.599 4.286 4.398 948.107

22.615 75-83-2 2,2-Dimethylbutane 0.101 0.115 0.103 26.713

27.829 79-29-8 2,3-Dimethylbutane 1.479 1.649 1.513 391.141

28.927 107-83-5 2-Methylpentane 6.385 7.213 6.533 1688.583

31.568 96-14-0 3-Methylpentane 4.733 5.257 4.843 1251.770

41.731 108-08-7 2,4-Dimethylpentane 0.857 0.940 0.754 227.620

42.272 464-06-2 2,2,3-Trimethylbutane 0.072 0.077 0.063 19.045

50.196 591-76-4 2-Methylhexane 1.344 1.461 1.182 356.780

52.025 589-34-4 3-Methylhexane 0.562 0.603 0.494 149.213

54.725 540-84-1 2,2,4-Trimethylpentane 5.835 6.222 4.504 1552.483

64.507 564-02-3 2,2,3-Trimethylpentane 0.324 0.334 0.250 86.182

64.750 592-13-2 2,5-Dimethylhexane 0.740 0.787 0.571 196.892

65.089 589-43-5 2,4-Dimethylhexane 0.711 0.749 0.549 189.097

68.091 565-75-3 2,3,4-Trimethylpentane 2.613 2.681 2.017 695.175

68.764 560-21-4 2,3,3-Trimethylpentane 2.646 2.689 2.042 704.029

70.428 584-94-1 2,3-Dimethylhexane 0.691 0.716 0.533 183.818

71.695 592-27-8 2-Methylheptane 0.043 0.045 0.033 11.357

71.961 589-53-7 4-Methylheptane 0.077 0.081 0.060 20.531

73.020 589-81-1 3-Methylheptane 0.042 0.044 0.032 11.085

74.926 3522-94-9 2,2,5-Trimethylhexane 1.122 1.170 0.771 299.057

80.054 1069-53-0 2,3,5-Trimethylhexane 0.176 0.180 0.121 46.915

81.233 1071-26-7 2,4-Dimethylheptane 0.027 0.028 0.019 7.264

82.194 1072-05-5 2,6-Dimethylheptane 0.030 0.031 0.020 7.894

83.128 2,5-Dimethylheptane 0.077 0.080 0.053 20.613

88.011 2216-33-3 3-Methyloctane 0.007 0.007 0.005 1.752

89.067 C10 - IsoParaffin - 1 0.172 0.174 0.107 45.911

89.91314720-74-2 2,2,4-trimethylheptane 0.122 0.123 0.075 32.507

93.138 C10-isoparaffin-x 0.000 0.000 0.000 1.142

93.82515869-87-1 2,2-Dimethyloctane 0.055 0.056 0.034 14.762

94.62515869-89-3 2,5-Dimethyloctane 0.092 0.092 0.057 24.444

95.104 2040-95-1 2,7-Dimethyloctane 0.026 0.026 0.016 6.899

95.268 2051-30-1 2,4-Dimethyloctane 0.243 0.246 0.151 64.889

95.661 2,6-Dimethyloctane 0.069 0.070 0.043 18.544

98.69017301-94-8 4-Methylnonane 0.013 0.013 0.008 3.465

98.907 2,2,6-Trimethyloctane 3.876 3.937 2.402 1035.316

99.665 5911-04-6 3-Methylnonane 0.019 0.019 0.012 5.104

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C-121
Hydrocarbon Expert V4.7 Thu Aug 26 10:08:56 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91313 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91313

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

I-Paraffins 100.481 C11-Isoparaffin-2 0.329 0.326 0.185 87.844

102.11217302-01-1 3-Ethyl-3-methylheptane 0.533 0.529 0.301 142.528

104.193 C11 Isoparaffin-4 0.062 0.061 0.035 16.566

105.061 C11-Isoparaffin-5 0.027 0.027 0.015 7.346

106.156 C11-Isoparaffin-7 0.601 0.596 0.339 160.585

108.370 C11- Isoparaffin-11 1.028 1.019 0.580 274.780

112.966 C12 - IsoParaffin - 1 0.030 0.030 0.016 8.132

116.093 C12 - IsoParaffin - 4 0.007 0.007 0.004 2.022

Aromatics

Mono-Aromatics 45.131 71-42-3 Benzene 0.830 0.697 0.937 242.286

68.621 108-88-3 Toluene 5.273 4.487 5.046 1521.901

84.440 100-41-4 Ethylbenzene 0.982 0.835 0.815 281.186

85.669 108-38-3 m-Xylene 2.519 2.151 2.092 721.507

85.817 106-42-3 p-Xylene 1.160 0.994 0.963 332.176

88.652 95-47-6 o-Xylene 0.812 0.681 0.674 232.555

92.838 98-82-8 i-Propylbenzene 0.030 0.026 0.022 8.569

96.306 103-65-1 n-Propylbenzene 0.331 0.284 0.243 94.310

97.155 620-14-4 1-Methyl-3-ethylbenzene 1.193 1.018 0.875 339.465

97.389 622-96-8 1-Methyl-4-ethylbenzene 0.543 0.465 0.399 154.616

98.015 108-67-8 1,3,5-Trimethylbenzene 0.758 0.646 0.556 215.659

99.100 611-14-3 1-Methyl-2-ethylbenzene 0.395 0.331 0.290 112.335

100.740 95-63-6 1,2,4-Trimethylbenzene 2.000 1.685 1.467 569.076

103.614 526-73-8 1,2,3-Trimethylbenzene 0.238 0.196 0.174 67.684

103.977 535-77-3 1-Methyl-3-i-propylbenzene 0.039 0.033 0.025 10.974

106.336 141-93-5 1,3-Diethylbenzene 0.025 0.022 0.017 7.189

106.638 1074-43-7 1-Methyl-3-n-propylbenzene 1.731 1.484 1.137 490.089

106.904 105-05-5 1,4-Diethylbenzene 0.439 0.376 0.288 124.232

107.177 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.102 0.085 0.067 28.836

107.423 135-01-3 1,2-Diethylbenzene 0.128 0.107 0.084 36.211

108.027 1074-17-5 1-Methyl-2-n-propylbenzene 0.046 0.039 0.031 13.154

109.544 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.345 0.291 0.227 97.622

110.102 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.834 0.691 0.548 236.002

111.214 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.070 0.058 0.046 19.869

111.687 4218-48-8 1-Ethyl-4-i-propylbenzene 0.114 0.095 0.068 32.259

112.164 1,2,4,5-Tetramethylbenzene 0.242 0.201 0.159 68.488

112.430 527-53-7 1,2,3,5-Tetramethylbenzene 0.319 0.264 0.209 90.269

113.585 C11 - Aromatic - 3 0.029 0.024 0.017 8.230

113.901 1,2-Di-i-propylbenzene 0.043 0.036 0.023 12.053

114.117 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.058 0.048 0.034 16.342

114.293 C11 - Aromatic - 4 0.037 0.030 0.022 10.358

115.090 538-68-1 n-Pentylbenzene 0.014 0.012 0.009 4.060

115.320 tert-Pentylbenzene 0.053 0.044 0.032 15.033

115.633 577-55-9 1-Methyl-2-n-butylbenzene 0.027 0.022 0.016 7.536

115.744 C11 - Aromatic - 7 0.042 0.036 0.025 11.771

116.206 100-18-5 1,4-Di-i-propylbenzene 0.048 0.040 0.026 13.409

117.432 7364-19-4 1t-Butyl-4-ethylbenzene 0.015 0.013 0.008 4.263

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C-122
Hydrocarbon Expert V4.7 Thu Aug 26 10:08:56 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91313 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91313

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 117.735 1,3-Di-n-propylbenzene 0.034 0.028 0.019 9.625

117.847 C11 - Aromatic - 11 0.018 0.016 0.011 5.154

118.402 C11 - Aromatic - 12 0.012 0.011 0.007 3.456

Naphthalenes 116.635 91-20-3 Naphthalene 0.086 0.062 0.059 25.500

123.281 91-57-6 2-Methylnaphthalene 0.012 0.009 0.007 3.554

124.145 90-12-0 1-Methylnaphthalene 0.005 0.004 0.003 1.616

Naphtheno/Olefino-Benzs 113.761 874-35-1 5-Methylindan 0.097 0.080 0.065 27.430

114.765 824-63-5 2-Methylindan 0.097 0.081 0.065 27.522

Indenes 104.808 Indan 0.184 0.141 0.137 53.261

105.442 Indene 1.660 1.270 1.238 480.056

109.206 2-Methylindan 0.153 0.117 0.102 44.354

114.514 824-22-6 4-Methylindan 0.123 0.102 0.082 34.770

116.797 4,7-Dimethyl Indane 0.016 0.013 0.010 4.756

117.080 1,1-Dimethyl Indane 0.011 0.009 0.007 3.301

Naphthenes

Mono-Naphthenes 27.097 287-92-3 Cyclopentane 0.134 0.133 0.168 36.306

40.153 96-37-7 Methylcyclopentane 1.672 1.648 1.751 452.929

47.050 110-82-7 Cyclohexane 1.039 0.985 1.088 281.457

52.879 1759-58-6 1t,3-Dimethylcyclopentane 0.116 0.115 0.104 31.489

53.466 2532-58-3 1c,3-Dimethylcyclopentane 0.080 0.080 0.072 21.787

54.096 822-50-4 1t,2-Dimethylcyclopentane 0.094 0.093 0.085 25.565

59.20016491-15-9 Cyclopentene, 1,5-dimethyl- 0.019 0.018 0.017 5.035

61.051 108-87-2 Methylcyclohexane 0.089 0.085 0.080 24.121

93.138 696-29-7 1-Methyl-2-propyl-cyclopentan 0.004 0.004 0.003 1.142

101.324 1678-98-4 i-Butylcyclohexane 0.059 0.055 0.037 16.027

105.856 n-ButylCyclohexane 0.002 0.002 0.001 0.589

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.404 115-11-7 Isobutene 0.015 0.019 0.024 4.181

9.442 106-98-9 Butene-1 0.019 0.023 0.029 5.037

10.265 624-64-6 t-Butene-2 0.073 0.089 0.114 19.651

10.986 590-18-1 c-Butene-2 0.086 0.102 0.135 23.193

16.329 109-67-1 Pentene-1 0.332 0.382 0.417 89.856

18.796 646-04-8 t-Pentene-2 0.843 0.959 1.059 228.284

19.820 627-20-3 c-Pentene-2 0.463 0.521 0.581 125.316

32.943 592-41-6 Hexene-1 1.605 1.747 1.682 434.942

35.93413269-52-8 t-Hexene-3 0.269 0.291 0.282 72.948

36.403 4050-45-7 t-Hexene-2 0.510 0.551 0.534 138.223

38.230 7688-21-3 c-Hexene-2 0.216 0.231 0.227 58.623

55.019 592-76-7 Heptene-1 0.030 0.032 0.027 8.231

56.87814686-14-7 t-Heptene-3 0.033 0.034 0.029 8.876

57.831 7642-10-6 c-Heptene-3 0.025 0.026 0.023 6.797

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C-123
Hydrocarbon Expert V4.7 Thu Aug 26 10:08:56 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91313 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91313

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

n-Olefins 58.74014686-13-6 t-Heptene-2 0.016 0.017 0.014 4.353

110.730 693-61-8 2-Undecene, (E)- 0.075 0.074 0.047 19.997

Iso-Olefins 13.121 563-45-1 3-Methylbutene-1 0.258 0.303 0.324 69.877

17.170 563-46-2 2-Methylbutene-1 0.504 0.571 0.633 136.420

20.489 513-35-9 2-Methylbutene-2 1.037 1.155 1.304 280.960

28.688 691-38-3 4-Methyl-c-pentene-2 0.043 0.047 0.045 11.722

29.333 674-76-0 4-Methyl-t-pentene-2 0.131 0.144 0.137 35.501

32.719 763-29-1 2-Methylpentene-1 0.224 0.241 0.235 60.708

36.896 625-27-4 2-Methylpentene-2 0.345 0.368 0.361 93.457

37.312 922-62-3 3-Methyl-c-pentene-2 0.269 0.285 0.282 72.981

39.580 3404-73-7 3,3-Dimethylpentene-1 0.318 0.334 0.286 86.204

42.032 594-56-9 2,3,3-Trimethylbutene-1 0.014 0.014 0.012 3.663

46.159 3404-61-3 3-Methylhexene-1 0.016 0.017 0.014 4.268

46.742 3524-73-0 5-Methylhexene-1 0.063 0.067 0.057 17.127

48.80015840-60-5 2-Methyl-c-hexene-3 0.041 0.044 0.037 11.222

49.146 3769-23-1 4-Methylhexene-1 0.011 0.011 0.010 2.927

49.791 3404-55-5 4-Methyl-t/c-hexene-2 0.053 0.055 0.047 14.243

54.418 C7 - Iso-Olefin - 2 0.023 0.024 0.021 6.216

56.355 4914-89-0 3-Methyl-c-hexene-3 0.014 0.015 0.013 3.864

57.239 6094-02-6 2-Methylhexene-1 0.058 0.062 0.052 15.835

58.110 2738-19-4 2-Methyl-2-hexene 0.026 0.027 0.024 7.119

58.355 3899-36-3 3-Methyl-t-hexene-3 0.020 0.021 0.018 5.432

59.64120710-38-8 3-Methyl-t-hexene-2 0.016 0.016 0.014 4.306

60.425 4914-91-4 2-Pentene, 3,4-dimethyl-, (Z)- 0.017 0.017 0.015 4.615

93.138 C10-IsoOlefin-4 0.004 0.004 0.003 1.142

Naphtheno-Olefins 25.246 142-29-0 Cyclopentene 0.197 0.188 0.255 54.978

45.334 693-89-0 1-Methylcyclopentene 0.370 0.350 0.397 102.706

50.669 110-83-8 Cyclohexene 0.046 0.042 0.049 12.422

Di-Olefins 18.200 78-79-5 2-Methyl-1,3-Butadiene 0.010 0.011 0.014 2.910

20.818 2004-70-8 1t,3-Pentadiene 0.015 0.017 0.020 4.247

Oxygenates 12.745 64-17-5 Ethanol 9.506 8.889 18.193 1107.028

26.486 71-23-8 n-Propanol 0.182 0.168 0.267 34.488

Unidentified 22.065 Unidentified 0.006 0.006 0.008 1.914

28.236 Unidentified 0.050 0.050 0.050 16.756

44.929 Unidentified 0.012 0.012 0.013 3.921

47.593 Unidentified 0.035 0.037 0.032 11.652

63.108 Unidentified 0.019 0.020 0.015 6.363

72.092 Unidentified 0.054 0.055 0.041 17.834

75.907 Unidentified 0.009 0.008 0.006 2.826

78.506 Unidentified 0.026 0.026 0.018 8.529

84.617 Unidentified 0.012 0.012 0.008 3.921

84.859 Unidentified 0.010 0.009 0.007 3.248

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C-124
Hydrocarbon Expert V4.7 Thu Aug 26 10:08:56 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91313 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91313

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Unidentified 85.963 Unidentified 0.026 0.026 0.018 8.624

88.479 Unidentified 0.048 0.052 0.034 15.974

92.085 Unidentified 0.011 0.010 0.007 3.546

93.028 Unidentified 0.011 0.010 0.008 3.580

93.028 Unidentified 0.011 0.011 0.007 3.580

93.028 Unidentified 0.011 0.008 0.007 3.580

93.602 Unidentified 0.159 0.162 0.099 52.853

94.267 Unidentified 0.022 0.016 1.949 7.338

94.267 Unidentified 0.022 0.023 0.014 7.338

94.487 Unidentified 0.021 0.019 0.015 6.923

95.019 Unidentified 0.021 0.021 0.013 6.923

99.475 Unidentified 0.012 0.012 0.007 3.902

99.841 Unidentified 0.011 0.011 0.007 3.552

100.131 Unidentified 0.222 0.164 0.125 73.829

100.258 Unidentified 0.622 0.617 0.351 206.582

100.946 Unidentified 0.372 0.391 0.234 123.449

101.068 Unidentified 0.220 0.222 0.137 73.129

101.969 Unidentified 0.025 0.023 0.016 8.214

102.323 Unidentified 0.140 0.121 0.092 46.622

102.465 Unidentified 0.331 0.286 0.217 109.800

102.976 Unidentified 0.146 0.145 0.082 48.425

103.468 Unidentified 0.017 0.014 0.013 5.658

104.398 Unidentified 0.325 0.280 0.213 107.836

105.995 Unidentified 0.013 0.012 0.008 4.456

107.890 Unidentified 0.140 0.139 0.079 46.418

108.164 Unidentified 0.138 0.137 0.079 45.652

108.245 Unidentified 0.126 0.125 0.071 41.797

108.550 Unidentified 0.328 0.326 0.185 109.027

108.983 Unidentified 0.928 0.781 0.610 308.045

109.703 Unidentified 0.066 0.050 0.044 21.863

110.528 Unidentified 0.034 0.031 0.019 11.232

110.858 Unidentified 0.161 0.160 0.101 53.348

111.131 Unidentified 0.143 0.124 0.085 47.335

111.798 Unidentified 0.080 0.066 0.048 26.517

112.654 Unidentified 0.015 0.012 0.009 4.881

112.784 Unidentified 0.022 0.018 0.015 7.391

113.294 Unidentified 0.036 0.036 0.019 11.991

113.448 Unidentified 0.014 0.014 0.007 4.649

113.654 Unidentified 0.040 0.033 0.024 13.292

114.682 Unidentified 0.028 0.023 0.017 9.294

114.978 Unidentified 0.012 0.010 0.007 4.092

116.972 Unidentified 0.006 0.005 0.003 1.841

125.444 Unidentified 0.003 0.003 0.002 1.118

126.172 Unidentified 0.006 0.005 0.003 2.120

126.172 Unidentified 0.006 0.005 0.003 2.120

126.172 Unidentified 0.006 0.006 0.003 2.120

129.864 Unidentified 0.003 0.003 0.002 1.106

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C-125
Hydrocarbon Expert V4.7 Thu Aug 26 10:08:56 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91313 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91313

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Unidentified

Plus

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C-126
Hydrocarbon Expert V4.7 Thu Aug 26 10:08:56 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91313 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91313

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF

20.0 15.0 10.0 5.0 0.0

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

Ethanol

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

Unidentified

2,2-Dimethylbutane

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C-127
Hydrocarbon Expert V4.7 Thu Aug 26 10:08:56 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91313 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91313

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

n-Propanol

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

n-Hexane

t-Hexene-3

t-Hexene-2

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane 2,3,3-Trimethylbutene-1 2,2,3-Trimethylbutane

Unidentified Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1 Cyclohexane

Unidentified

2-Methyl-c-hexene-3

4-Methylhexene-1

4-Methyl-t/c-hexene-2

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C-128
Hydrocarbon Expert V4.7 Thu Aug 26 10:08:56 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91313 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91313

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF

70.0 65.0 60.0 55.0 50.0

2-Methylhexane

Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane

C7 - Iso-Olefin - 2 2,2,4-Trimethylpentane Heptene-1

3-Methyl-c-hexene-3

t-Heptene-3

2-Methylhexene-1

n-Heptane c-Heptene-3 2-Methyl-2-hexene 3-Methyl-t-hexene-3

t-Heptene-2

Cyclopentene, 1,5-dimethyl3-Methyl-t-hexene-2

2-Pentene, 3,4-dimethyl-, (Z)-

Methylcyclohexane

Unidentified

2,2,3-Trimethylpentane 2,5-Dimethylhexane

2,4-Dimethylhexane

2,3,4-Trimethylpentane

Toluene 2,3,3-Trimethylpentane

2,3-Dimethylhexane

2-Methylheptane

Unidentified 4-Methylheptane

3-Methylheptane

2,2,5-Trimethylhexane

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C-129
Hydrocarbon Expert V4.7 Thu Aug 26 10:08:56 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91313 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91313

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF

95.0 90.0 85.0 80.0 75.0

Unidentified

n-Octane

Unidentified

2,3,5-Trimethylhexane

2,4-Dimethylheptane

2,6-Dimethylheptane

2,5-Dimethylheptane

Ethylbenzene Unidentified

m-Xylene Unidentified p-Xylene

3-Methyloctane

Unidentified o-Xylene

C10 - IsoParaffin - 1

2,2,4-trimethylheptane

n-Nonane

Unidentified

i-Propylbenzene 1-Methyl-2-propyl-cyclopentan/C10-IsoOlefin-4/C10-isoparaffin-x Unidentified

Unidentified 2,2-Dimethyloctane

Unidentified

2,5-Dimethyloctane

Unidentified 2,7-Dimethyloctane 2,4-Dimethyloctane

2,6-Dimethyloctane

n-Propylbenzene

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

4-Methylnonane 2,2,6-Trimethyloctane 1-Methyl-2-ethylbenzene

Unidentified 3-Methylnonane Unidentified

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C-130
Hydrocarbon Expert V4.7 Thu Aug 26 10:08:56 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91313 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91313

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified Unidentified C11-Isoparaffin-2 1,2,4-Trimethylbenzene

Unidentified Unidentified

i-Butylcyclohexane

Unidentified3-Ethyl-3-methylheptane Unidentified Unidentified n-Decane Unidentified

Unidentified 1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene C11 Isoparaffin-4 Unidentified

Indan C11-Isoparaffin-5

Indene

n-ButylCyclohexane Unidentified C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene 1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

Unidentified 1-Methyl-2-n-propylbenzene Unidentified C11- Isoparaffin-11 Unidentified

Unidentified 2-Methylindan

1,2-Dimethyl-4-ethylbenzene Unidentified

1,3-Dimethyl-2-ethylbenzene

Unidentified 2-Undecene, (E)- Unidentified

1,2-Dimethyl-3-ethylbenzene Unidentified

n-Undecane Unidentified 1-Ethyl-4-i-propylbenzene

1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene Unidentified C12 - IsoParaffin - 1

Unidentified C11 - Aromatic - 3 5-Methylindan 1,2-Di-i-propylbenzene 1-methyl-4-(1-methylpropyl)be C11 - Aromatic - 4 4-Methylindan Unidentified 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene 1-Methyl-2-n-butylbenzene C11 - Aromatic - 7

C12 - IsoParaffin - 4 1,4-Di-i-propylbenzene

Naphthalene 4,7-Dimethyl Indane Unidentified 1,1-Dimethyl Indane

1t-Butyl-4-ethylbenzene

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

C11 - Aromatic - 12

2-Methylnaphthalene

1-Methylnaphthalene

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C-131
Hydrocarbon Expert V4.7 Thu Aug 26 10:08:56 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91313 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91313

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000009.D\SIG1000009_FID1_A.CDF

145.0 140.0 135.0 130.0 125.0

Unidentified

Unidentified

Unidentified

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C-132
Hydrocarbon Expert V4.7 Thu Aug 26 10:21:23 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91314 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91314

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 11.444 12.660 13.176

I-Paraffins 47.226 50.315 45.963

Aromatics 23.314 19.187 20.473

Mono-Aromatics 22.309 18.420 19.717

Naphthalenes 0.099 0.069 0.071

Naphtheno/Olefino-Benzs 0.240 0.193 0.170

Indenes 0.666 0.504 0.514

Naphthenes 9.372 8.840 10.478

Mono-Naphthenes 9.372 8.840 10.478

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 6.522 6.949 8.098

n-Olefins 2.912 3.177 3.731

Iso-Olefins 3.065 3.267 3.697

Naphtheno-Olefins 0.523 0.482 0.640

Di-Olefins 0.021 0.022 0.029

Oxygenates 0.174 0.156 0.272

Unidentified 1.947 1.893 1.540

Plus 0.000 0.000 0.000

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C-133
Hydrocarbon Expert V4.7 Thu Aug 26 10:21:23 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91314 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91314

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C3 0.175 0.158 0.275

C4 0.719 0.879 1.175

C5 18.645 21.048 24.460

C6 24.413 25.345 26.918

C7 12.717 11.707 12.509

C8 27.374 26.719 22.917

C9 7.744 6.749 5.953

C10 5.363 4.708 3.701

C11 0.775 0.690 0.478

C12 0.128 0.103 0.074

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C-134
Hydrocarbon Expert V4.7 Thu Aug 26 10:21:23 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91314 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91314

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C3 0.001 0.001 0.002

C4 0.455 0.564 0.735

C5 3.315 3.800 4.315

C6 6.645 7.234 7.242

C7 0.582 0.611 0.546

C8 0.173 0.177 0.142

C9 0.192 0.192 0.141

C10 0.066 0.065 0.043

C11 0.016 0.015 0.010

I-Paraffins C4 0.032 0.041 0.052

C5 10.489 12.156 13.655

C6 8.513 9.287 9.278

C7 3.404 3.596 3.191

C8 20.493 20.961 16.850

C9 1.859 1.880 1.361

C10 2.046 2.017 1.342

C11 0.391 0.377 0.235

Mono-Aromatics C6 0.683 0.558 0.822

C7 6.716 5.561 6.846

C8 6.490 5.378 5.741

C9 5.555 4.575 4.341

C10 2.401 1.971 1.680

C11 0.335 0.274 0.212

C12 0.128 0.103 0.074

Naphthalenes C10 0.081 0.056 0.059

C11 0.018 0.013 0.012

Naphtheno/Olefino-Benzs C10 0.240 0.193 0.170

Indenes C9 0.138 0.103 0.110

C10 0.513 0.390 0.394

C11 0.015 0.011 0.010

Mono-Naphthenes C5 1.465 1.411 1.962

C6 6.166 5.792 6.882

C7 1.506 1.418 1.440

C8 0.218 0.203 0.183

C10 0.017 0.015 0.011

n-Olefins C4 0.232 0.274 0.389

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C-135
Hydrocarbon Expert V4.7 Thu Aug 26 10:21:23 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91314 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91314

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

n-Olefins C5 1.585 1.754 2.123

C6 1.079 1.133 1.204

C7 0.016 0.016 0.015

Iso-Olefins C5 1.591 1.739 2.131

C6 0.981 1.023 1.095

C7 0.493 0.505 0.472

Naphtheno-Olefins C5 0.177 0.165 0.245

C6 0.346 0.317 0.396

Di-Olefins C5 0.021 0.022 0.029

Oxygenates C3 0.174 0.156 0.272

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C-136
Hydrocarbon Expert V4.7 Thu Aug 26 10:21:23 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91314 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91314

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 30.37 28.15

5% 80.03 79.82

10% 81.59 81.16

15% 96.32 94.14

20% 121.26 100.81

25% 140.51 138.19

30% 154.23 144.81

35% 155.31 154.54

40% 167.48 155.54

45% 177.35 176.43

50% 209.18 191.39

55% 209.80 209.34

60% 210.42 209.93

65% 230.75 210.53

70% 231.02 230.81

75% 237.03 232.66

80% 261.17 238.72

85% 281.92 279.02

90% 323.28 320.50

95% 345.33 335.88

FBP 403.15 390.91

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C-137
Hydrocarbon Expert V4.7 Thu Aug 26 10:21:23 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91314 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91314

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 7.390 74-98-6 P3 Propane 0.001 0.001 0.002 0.261

2 8.611 75-28-5 I4 i-Butane 0.032 0.041 0.052 8.316

3 9.404 115-11-7 K4 Isobutene 0.020 0.024 0.034 5.483

4 9.443 106-98-9 K4 Butene-1 0.024 0.029 0.040 6.413

5 9.792 106-97-8 P4 n-Butane 0.455 0.564 0.735 118.589

6 10.266 624-64-6 K4 t-Butene-2 0.088 0.105 0.148 23.854

7 10.388 463-82-1 I5 2,2-Dimethylpropane 0.045 0.055 0.059 11.868

8 10.987 590-18-1 K4 c-Butene-2 0.100 0.116 0.168 27.050

9 13.128 563-45-1 C5 3-Methylbutene-1 0.069 0.079 0.092 18.571

10 14.719 78-78-4 I5 i-Pentane 10.444 12.101 13.596 2743.138

11 16.335 109-67-1 K5 Pentene-1 0.317 0.356 0.425 85.773

12 17.168 563-46-2 C5 2-Methylbutene-1 0.497 0.549 0.666 134.306

13 17.701 109-66-0 P5 n-Pentane 3.315 3.800 4.315 870.648

14 18.206 78-79-5 E5 2-Methyl-1,3-Butadiene 0.009 0.009 0.012 2.388

15 18.801 646-04-8 K5 t-Pentene-2 0.820 0.908 1.098 221.406

16 19.824 627-20-3 K5 c-Pentene-2 0.448 0.491 0.600 121.087

17 20.489 513-35-9 C5 2-Methylbutene-2 1.025 1.111 1.373 276.986

18 20.825 2004-70-8 E5 1t,3-Pentadiene 0.012 0.013 0.017 3.464

19 22.615 75-83-2 I6 2,2-Dimethylbutane 0.615 0.680 0.670 162.169

20 25.243 142-29-0 B5 Cyclopentene 0.177 0.165 0.245 49.352

21 26.491 71-23-8 X3 n-Propanol 0.174 0.156 0.272 32.976

22 27.108 287-92-3 M5 Cyclopentane 1.465 1.411 1.962 395.865

23 27.829 79-29-8 I6 2,3-Dimethylbutane 0.972 1.055 1.060 256.443

24 28.230 ? Unidentified 0.050 0.049 0.053 16.558

25 28.689 691-38-3 C6 4-Methyl-c-pentene-2 0.043 0.045 0.048 11.528

26 28.913 107-83-5 I6 2-Methylpentane 3.670 4.034 4.000 967.867

27 29.337 674-76-0 C6 4-Methyl-t-pentene-2 0.129 0.137 0.144 34.767

28 31.556 96-14-0 I6 3-Methylpentane 3.255 3.517 3.547 858.234

29 32.715 763-29-1 C6 2-Methylpentene-1 0.220 0.230 0.245 59.344

30 32.937 592-41-6 K6 Hexene-1 0.149 0.158 0.167 40.364

31 35.323 110-54-3 P6 n-Hexane 6.645 7.234 7.242 1752.162

32 35.93613269-52-8 K6 t-Hexene-3 0.251 0.265 0.281 67.927

33 36.408 4050-45-7 K6 t-Hexene-2 0.476 0.501 0.531 128.613

34 36.897 625-27-4 C6 2-Methylpentene-2 0.334 0.347 0.373 90.341

35 37.313 922-62-3 C6 3-Methyl-c-pentene-2 0.256 0.263 0.285 69.049

36 38.233 7688-21-3 K6 c-Hexene-2 0.202 0.210 0.226 54.614

37 39.584 3404-73-7 C7 3,3-Dimethylpentene-1 0.304 0.311 0.291 82.063

38 40.165 96-37-7 M6 Methylcyclopentane 2.886 2.768 3.221 779.767

39 41.733 108-08-7 I7 2,4-Dimethylpentane 0.700 0.746 0.656 185.196

40 42.273 464-06-2 I7 2,2,3-Trimethylbutane 0.088 0.092 0.083 23.332

41 45.136 71-42-3 Q6 Benzene 0.683 0.558 0.822 198.819

42 45.334 693-89-0 B6 1-Methylcyclopentene 0.313 0.288 0.358 86.500

43 46.164 3404-61-3 C7 3-Methylhexene-1 0.012 0.012 0.011 3.214

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C-138
Hydrocarbon Expert V4.7 Thu Aug 26 10:21:23 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91314 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91314

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 46.752 3524-73-0 C7 5-Methylhexene-1 0.088 0.091 0.084 23.815

45 47.067 110-82-7 M6 Cyclohexane 3.280 3.024 3.660 886.034

46 47.590 ? Unidentified 0.027 0.028 0.026 8.919

47 48.80715840-60-5 C7 2-Methyl-c-hexene-3 0.030 0.031 0.029 8.066

48 49.797 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.035 0.036 0.033 9.433

49 50.199 591-76-4 I7 2-Methylhexane 1.862 1.969 1.745 492.861

50 50.670 110-83-8 B6 Cyclohexene 0.033 0.029 0.038 8.993

51 52.032 589-34-4 I7 3-Methylhexane 0.755 0.789 0.708 199.861

52 52.883 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.161 0.155 0.154 43.594

53 53.470 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.130 0.126 0.125 35.193

54 54.097 822-50-4 M7 1t,2-Dimethylcyclopentane 0.203 0.194 0.195 54.936

55 54.766 540-84-1 I8 2,2,4-Trimethylpentane 11.643 12.080 9.574 3088.711

56 56.88414686-14-7 K7 t-Heptene-3 0.016 0.016 0.015 4.191

57 57.240 6094-02-6 C7 2-Methylhexene-1 0.024 0.025 0.023 6.589

58 57.617 142-82-5 P7 n-Heptane 0.582 0.611 0.546 154.096

59 59.432 ? Unidentified 0.459 0.458 0.439 151.754

60 61.062 108-87-2 M7 Methylcyclohexane 0.977 0.912 0.935 264.025

61 62.013 4516-69-2 M8 1,1,3-Trimethylcyclopentane 0.021 0.020 0.017 5.577

62 62.420 590-73-8 I8 2,2-Dimethylhexane 0.018 0.019 0.015 4.870

63 63.642 ? Unidentified 0.123 0.118 0.105 40.622

64 63.857 1640-89-7 M7 Ethylcyclopentane 0.033 0.031 0.032 8.981

65 64.510 ? Unidentified 0.321 0.322 0.264 106.239

66 64.754 592-13-2 I8 2,5-Dimethylhexane 0.971 1.005 0.798 257.600

67 65.092 589-43-5 I8 2,4-Dimethylhexane 0.846 0.868 0.696 224.550

68 65.926 4850-28-6 M8 1c,2t,4-Trimethylcyclopentane 0.019 0.017 0.015 5.002

69 67.45615890-40-1 M8 1t,2c,3-Trimethylcyclopentane 0.015 0.014 0.012 3.928

70 68.096 565-75-3 I8 2,3,4-Trimethylpentane 2.888 2.883 2.375 766.099

71 68.634 108-88-3 Q7 Toluene 6.716 5.561 6.846 1932.795

72 68.773 560-21-4 I8 2,3,3-Trimethylpentane 2.982 2.948 2.452 791.102

73 70.428 584-94-1 I8 2,3-Dimethylhexane 0.740 0.746 0.609 196.347

74 71.695 592-27-8 I8 2-Methylheptane 0.123 0.127 0.101 32.635

75 71.958 589-53-7 I8 4-Methylheptane 0.113 0.115 0.093 29.883

76 72.091 ? Unidentified 0.059 0.059 0.048 19.489

77 72.860 M8 1,3-dimethyl-t-cyclohexane 0.086 0.080 0.072 23.209

78 73.019 589-81-1 I8 3-Methylheptane 0.112 0.113 0.092 29.592

79 73.203 619-99-8 I8 3-Ethylhexane 0.056 0.057 0.046 14.916

80 74.102 ? Unidentified 0.013 0.012 0.011 4.428

81 74.927 3522-94-9 I9 2,2,5-Trimethylhexane 1.370 1.391 1.004 364.251

82 75.904 ? Unidentified 0.010 0.010 0.007 3.365

83 76.189 2207-03-6 M8 1t,3-Dimethylcyclohexane 0.035 0.032 0.029 9.362

84 77.562 111-65-9 P8 n-Octane 0.173 0.177 0.142 45.940

85 78.506 ? Unidentified 0.035 0.033 0.030 11.721

86 80.054 1069-53-0 I9 2,3,5-Trimethylhexane 0.233 0.232 0.171 61.917

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C-139
Hydrocarbon Expert V4.7 Thu Aug 26 10:21:23 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91314 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91314

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 81.232 1071-26-7 I9 2,4-Dimethylheptane 0.037 0.038 0.027 9.960

88 81.867 1678-91-7 M8 Ethylcyclohexane 0.044 0.040 0.037 11.911

89 82.193 1072-05-5 I9 2,6-Dimethylheptane 0.051 0.052 0.038 13.683

90 82.672 ? Unidentified 0.008 0.007 0.007 2.581

91 83.127 I9 2,5-Dimethylheptane 0.114 0.114 0.083 30.182

92 84.439 100-41-4 Q8 Ethylbenzene 1.230 1.018 1.088 351.186

93 84.858 ? Unidentified 0.018 0.017 0.013 5.985

94 85.671 108-38-3 Q8 m-Xylene 2.930 2.434 2.592 836.731

95 85.819 106-42-3 Q8 p-Xylene 1.400 1.167 1.238 399.740

96 86.326 ? Unidentified 0.015 0.015 0.011 4.852

97 87.013 2216-34-4 I9 4-Methyloctane 0.014 0.014 0.010 3.801

98 87.146 3221-61-2 I9 2-Methyloctane 0.019 0.019 0.014 5.133

99 88.011 2216-33-3 I9 3-Methyloctane 0.020 0.019 0.014 5.192

100 88.478 ? Unidentified 0.082 0.086 0.061 27.065

101 88.651 95-47-6 Q8 o-Xylene 0.931 0.759 0.823 265.782

102 89.065 I10 C10 - IsoParaffin - 1 0.274 0.271 0.181 73.080

103 89.91214720-74-2 I10 2,2,4-trimethylheptane 0.197 0.194 0.130 52.342

104 91.465 111-84-2 P9 n-Nonane 0.192 0.192 0.141 51.004

105 92.836 98-82-8 Q9 i-Propylbenzene 0.031 0.026 0.024 8.887

106 93.028 ? Unidentified 0.014 0.013 0.010 4.670

107 93.028 ? Unidentified 0.014 0.014 0.009 4.670

108 93.028 ? Unidentified 0.014 0.010 0.009 4.670

109 93.600 ? Unidentified 0.099 0.098 0.065 32.754

110 93.82315869-87-1 I10 2,2-Dimethyloctane 0.033 0.033 0.022 8.823

111 94.62315869-89-3 I10 2,5-Dimethyloctane 0.032 0.031 0.021 8.489

112 95.099 2040-95-1 I10 2,7-Dimethyloctane 0.019 0.018 0.012 4.952

113 95.265 2051-30-1 I10 2,4-Dimethyloctane 0.087 0.086 0.057 23.138

114 95.659 I10 2,6-Dimethyloctane 0.029 0.029 0.019 7.772

115 96.304 103-65-1 Q9 n-Propylbenzene 0.276 0.230 0.216 78.426

116 97.153 620-14-4 Q9 1-Methyl-3-ethylbenzene 1.074 0.892 0.840 304.872

117 97.387 622-96-8 Q9 1-Methyl-4-ethylbenzene 0.513 0.428 0.401 145.593

118 98.014 108-67-8 Q9 1,3,5-Trimethylbenzene 0.709 0.589 0.554 201.264

119 98.68417301-94-8 I10 4-Methylnonane 0.011 0.011 0.007 2.958

120 98.887 I10 2,2,6-Trimethyloctane 1.203 1.188 0.794 320.293

121 99.098 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.417 0.340 0.325 118.194

122 99.660 5911-04-6 I10 3-Methylnonane 0.015 0.015 0.010 4.023

123 100.127 ? Unidentified 0.063 0.045 0.038 20.795

124 100.252 ? Unidentified 0.177 0.171 0.107 58.693

125 100.476 I11 C11-Isoparaffin-2 0.092 0.089 0.056 24.662

126 100.737 95-63-6 Q9 1,2,4-Trimethylbenzene 2.152 1.764 1.681 610.516

127 100.941 ? Unidentified 0.103 0.105 0.069 34.022

128 101.062 ? Unidentified 0.061 0.060 0.040 20.207

129 101.319 1678-98-4 M10 i-Butylcyclohexane 0.017 0.015 0.011 4.544

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C-140
Hydrocarbon Expert V4.7 Thu Aug 26 10:21:23 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91314 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91314

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 102.10717302-01-1 I10 3-Ethyl-3-methylheptane 0.147 0.142 0.088 39.105

131 102.454 538-93-2 Q10 i-Butylbenzene 0.162 0.136 0.113 45.695

132 102.656 124-18-5 P10 n-Decane 0.066 0.065 0.043 17.520

133 102.974 ? Unidentified 0.032 0.031 0.019 10.714

134 103.610 526-73-8 Q9 1,2,3-Trimethylbenzene 0.382 0.307 0.299 108.469

135 103.997 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.017 0.014 0.012 4.874

136 104.190 I11 C11 Isoparaffin-4 0.015 0.014 0.009 3.998

137 104.393 ? Unidentified 0.069 0.058 0.048 22.878

138 104.800 J9 Indan 0.138 0.103 0.110 39.897

139 105.428 J10 Indene 0.358 0.266 0.284 103.114

140 106.145 I11 C11-Isoparaffin-7 0.111 0.107 0.067 29.611

141 106.330 141-93-5 Q10 1,3-Diethylbenzene 0.052 0.043 0.037 14.730

142 106.614 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 0.436 0.364 0.305 123.082

143 106.947 105-05-5 Q10 1,4-Diethylbenzene 0.174 0.145 0.122 49.151

144 107.172 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.143 0.116 0.100 40.294

145 107.440 135-01-3 Q10 1,2-Diethylbenzene 0.027 0.022 0.019 7.499

146 107.884 ? Unidentified 0.017 0.017 0.010 5.756

147 108.023 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.054 0.044 0.038 15.164

148 108.362 I11 C11- Isoparaffin-11 0.172 0.166 0.103 45.876

149 108.548 ? Unidentified 0.036 0.035 0.022 11.972

150 108.875 1758-88-9 Q10 1,4,Dimethyl-2-ethylbenzene 0.120 0.098 0.084 33.898

151 109.032 874-41-9 Q10 1,3-Dimethyl-4-ethylbenzene 0.208 0.171 0.146 58.813

152 109.197 J10 2-Methylindan 0.019 0.014 0.014 5.522

153 109.542 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.275 0.226 0.192 77.546

154 110.097 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.075 0.061 0.053 21.236

155 111.009 Q11 1-Methyl-4-t-butylbenzene 0.020 0.017 0.013 5.753

156 111.219 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.098 0.079 0.068 27.607

157 111.525 1120-21-4 P11 n-Undecane 0.016 0.015 0.010 4.243

158 111.689 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.012 0.010 0.008 3.383

159 112.160 Q10 1,2,4,5-Tetramethylbenzene 0.232 0.188 0.162 65.445

160 112.427 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.329 0.265 0.230 92.747

161 113.289 ? Unidentified 0.009 0.009 0.005 3.017

162 113.581 Q11 C11 - Aromatic - 3 0.042 0.034 0.027 11.936

163 113.761 874-35-1 H10 5-Methylindan 0.098 0.079 0.069 27.578

164 113.901 Q12 1,2-Di-i-propylbenzene 0.042 0.034 0.024 11.683

165 114.115 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.060 0.048 0.038 16.861

166 114.275 Q11 C11 - Aromatic - 4 0.030 0.024 0.019 8.505

167 114.512 824-22-6 J10 4-Methylindan 0.136 0.110 0.097 38.420

168 114.763 824-63-5 H10 2-Methylindan 0.142 0.115 0.101 40.068

169 114.977 ? Unidentified 0.011 0.009 0.007 3.521

170 115.089 538-68-1 Q11 n-Pentylbenzene 0.015 0.012 0.009 4.099

171 115.321 Q11 tert-Pentylbenzene 0.060 0.049 0.038 16.961

172 115.631 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.026 0.021 0.016 7.304

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C-141
Hydrocarbon Expert V4.7 Thu Aug 26 10:21:23 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91314 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91314

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 115.741 Q11 C11 - Aromatic - 7 0.034 0.029 0.022 9.625

174 116.204 100-18-5 Q12 1,4-Di-i-propylbenzene 0.048 0.038 0.028 13.326

175 116.631 91-20-3 G10 Naphthalene 0.081 0.056 0.059 23.838

176 116.801 ? Unidentified 0.008 0.006 0.005 2.530

177 117.080 J11 1,1-Dimethyl Indane 0.015 0.011 0.010 4.275

178 117.734 Q12 1,3-Di-n-propylbenzene 0.039 0.031 0.023 10.934

179 117.845 Q11 C11 - Aromatic - 11 0.021 0.018 0.014 6.036

180 118.400 Q11 C11 - Aromatic - 12 0.013 0.011 0.008 3.740

181 123.280 91-57-6 G11 2-Methylnaphthalene 0.012 0.009 0.008 3.622

182 124.145 90-12-0 G11 1-Methylnaphthalene 0.006 0.004 0.004 1.781

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C-142
Hydrocarbon Expert V4.7 Thu Aug 26 10:21:23 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91314 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91314

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 7.390 74-98-6 Propane 0.001 0.001 0.002 0.261

9.792 106-97-8 n-Butane 0.455 0.564 0.735 118.589

17.701 109-66-0 n-Pentane 3.315 3.800 4.315 870.648

35.323 110-54-3 n-Hexane 6.645 7.234 7.242 1752.162

57.617 142-82-5 n-Heptane 0.582 0.611 0.546 154.096

77.562 111-65-9 n-Octane 0.173 0.177 0.142 45.940

91.465 111-84-2 n-Nonane 0.192 0.192 0.141 51.004

102.656 124-18-5 n-Decane 0.066 0.065 0.043 17.520

111.525 1120-21-4 n-Undecane 0.016 0.015 0.010 4.243

I-Paraffins 8.611 75-28-5 i-Butane 0.032 0.041 0.052 8.316

10.388 463-82-1 2,2-Dimethylpropane 0.045 0.055 0.059 11.868

14.719 78-78-4 i-Pentane 10.444 12.101 13.596 2743.138

22.615 75-83-2 2,2-Dimethylbutane 0.615 0.680 0.670 162.169

27.829 79-29-8 2,3-Dimethylbutane 0.972 1.055 1.060 256.443

28.913 107-83-5 2-Methylpentane 3.670 4.034 4.000 967.867

31.556 96-14-0 3-Methylpentane 3.255 3.517 3.547 858.234

41.733 108-08-7 2,4-Dimethylpentane 0.700 0.746 0.656 185.196

42.273 464-06-2 2,2,3-Trimethylbutane 0.088 0.092 0.083 23.332

50.199 591-76-4 2-Methylhexane 1.862 1.969 1.745 492.861

52.032 589-34-4 3-Methylhexane 0.755 0.789 0.708 199.861

54.766 540-84-1 2,2,4-Trimethylpentane 11.643 12.080 9.574 3088.711

62.420 590-73-8 2,2-Dimethylhexane 0.018 0.019 0.015 4.870

64.754 592-13-2 2,5-Dimethylhexane 0.971 1.005 0.798 257.600

65.092 589-43-5 2,4-Dimethylhexane 0.846 0.868 0.696 224.550

68.096 565-75-3 2,3,4-Trimethylpentane 2.888 2.883 2.375 766.099

68.773 560-21-4 2,3,3-Trimethylpentane 2.982 2.948 2.452 791.102

70.428 584-94-1 2,3-Dimethylhexane 0.740 0.746 0.609 196.347

71.695 592-27-8 2-Methylheptane 0.123 0.127 0.101 32.635

71.958 589-53-7 4-Methylheptane 0.113 0.115 0.093 29.883

73.019 589-81-1 3-Methylheptane 0.112 0.113 0.092 29.592

73.203 619-99-8 3-Ethylhexane 0.056 0.057 0.046 14.916

74.927 3522-94-9 2,2,5-Trimethylhexane 1.370 1.391 1.004 364.251

80.054 1069-53-0 2,3,5-Trimethylhexane 0.233 0.232 0.171 61.917

81.232 1071-26-7 2,4-Dimethylheptane 0.037 0.038 0.027 9.960

82.193 1072-05-5 2,6-Dimethylheptane 0.051 0.052 0.038 13.683

83.127 2,5-Dimethylheptane 0.114 0.114 0.083 30.182

87.013 2216-34-4 4-Methyloctane 0.014 0.014 0.010 3.801

87.146 3221-61-2 2-Methyloctane 0.019 0.019 0.014 5.133

88.011 2216-33-3 3-Methyloctane 0.020 0.019 0.014 5.192

89.065 C10 - IsoParaffin - 1 0.274 0.271 0.181 73.080

89.91214720-74-2 2,2,4-trimethylheptane 0.197 0.194 0.130 52.342

93.82315869-87-1 2,2-Dimethyloctane 0.033 0.033 0.022 8.823

94.62315869-89-3 2,5-Dimethyloctane 0.032 0.031 0.021 8.489

95.099 2040-95-1 2,7-Dimethyloctane 0.019 0.018 0.012 4.952

95.265 2051-30-1 2,4-Dimethyloctane 0.087 0.086 0.057 23.138

95.659 2,6-Dimethyloctane 0.029 0.029 0.019 7.772

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C-143
Hydrocarbon Expert V4.7 Thu Aug 26 10:21:23 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91314 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91314

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

I-Paraffins 98.68417301-94-8 4-Methylnonane 0.011 0.011 0.007 2.958

98.887 2,2,6-Trimethyloctane 1.203 1.188 0.794 320.293

99.660 5911-04-6 3-Methylnonane 0.015 0.015 0.010 4.023

100.476 C11-Isoparaffin-2 0.092 0.089 0.056 24.662

102.10717302-01-1 3-Ethyl-3-methylheptane 0.147 0.142 0.088 39.105

104.190 C11 Isoparaffin-4 0.015 0.014 0.009 3.998

106.145 C11-Isoparaffin-7 0.111 0.107 0.067 29.611

108.362 C11- Isoparaffin-11 0.172 0.166 0.103 45.876

Aromatics

Mono-Aromatics 45.136 71-42-3 Benzene 0.683 0.558 0.822 198.819

68.634 108-88-3 Toluene 6.716 5.561 6.846 1932.795

84.439 100-41-4 Ethylbenzene 1.230 1.018 1.088 351.186

85.671 108-38-3 m-Xylene 2.930 2.434 2.592 836.731

85.819 106-42-3 p-Xylene 1.400 1.167 1.238 399.740

88.651 95-47-6 o-Xylene 0.931 0.759 0.823 265.782

92.836 98-82-8 i-Propylbenzene 0.031 0.026 0.024 8.887

96.304 103-65-1 n-Propylbenzene 0.276 0.230 0.216 78.426

97.153 620-14-4 1-Methyl-3-ethylbenzene 1.074 0.892 0.840 304.872

97.387 622-96-8 1-Methyl-4-ethylbenzene 0.513 0.428 0.401 145.593

98.014 108-67-8 1,3,5-Trimethylbenzene 0.709 0.589 0.554 201.264

99.098 611-14-3 1-Methyl-2-ethylbenzene 0.417 0.340 0.325 118.194

100.737 95-63-6 1,2,4-Trimethylbenzene 2.152 1.764 1.681 610.516

102.454 538-93-2 i-Butylbenzene 0.162 0.136 0.113 45.695

103.610 526-73-8 1,2,3-Trimethylbenzene 0.382 0.307 0.299 108.469

103.997 535-77-3 1-Methyl-3-i-propylbenzene 0.017 0.014 0.012 4.874

106.330 141-93-5 1,3-Diethylbenzene 0.052 0.043 0.037 14.730

106.614 1074-43-7 1-Methyl-3-n-propylbenzene 0.436 0.364 0.305 123.082

106.947 105-05-5 1,4-Diethylbenzene 0.174 0.145 0.122 49.151

107.172 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.143 0.116 0.100 40.294

107.440 135-01-3 1,2-Diethylbenzene 0.027 0.022 0.019 7.499

108.023 1074-17-5 1-Methyl-2-n-propylbenzene 0.054 0.044 0.038 15.164

108.875 1758-88-9 1,4,Dimethyl-2-ethylbenzene 0.120 0.098 0.084 33.898

109.032 874-41-9 1,3-Dimethyl-4-ethylbenzene 0.208 0.171 0.146 58.813

109.542 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.275 0.226 0.192 77.546

110.097 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.075 0.061 0.053 21.236

111.009 1-Methyl-4-t-butylbenzene 0.020 0.017 0.013 5.753

111.219 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.098 0.079 0.068 27.607

111.689 4218-48-8 1-Ethyl-4-i-propylbenzene 0.012 0.010 0.008 3.383

112.160 1,2,4,5-Tetramethylbenzene 0.232 0.188 0.162 65.445

112.427 527-53-7 1,2,3,5-Tetramethylbenzene 0.329 0.265 0.230 92.747

113.581 C11 - Aromatic - 3 0.042 0.034 0.027 11.936

113.901 1,2-Di-i-propylbenzene 0.042 0.034 0.024 11.683

114.115 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.060 0.048 0.038 16.861

114.275 C11 - Aromatic - 4 0.030 0.024 0.019 8.505

115.089 538-68-1 n-Pentylbenzene 0.015 0.012 0.009 4.099

115.321 tert-Pentylbenzene 0.060 0.049 0.038 16.961

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C-144
Hydrocarbon Expert V4.7 Thu Aug 26 10:21:23 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91314 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91314

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 115.631 577-55-9 1-Methyl-2-n-butylbenzene 0.026 0.021 0.016 7.304

115.741 C11 - Aromatic - 7 0.034 0.029 0.022 9.625

116.204 100-18-5 1,4-Di-i-propylbenzene 0.048 0.038 0.028 13.326

117.734 1,3-Di-n-propylbenzene 0.039 0.031 0.023 10.934

117.845 C11 - Aromatic - 11 0.021 0.018 0.014 6.036

118.400 C11 - Aromatic - 12 0.013 0.011 0.008 3.740

Naphthalenes 116.631 91-20-3 Naphthalene 0.081 0.056 0.059 23.838

123.280 91-57-6 2-Methylnaphthalene 0.012 0.009 0.008 3.622

124.145 90-12-0 1-Methylnaphthalene 0.006 0.004 0.004 1.781

Naphtheno/Olefino-Benzs 113.761 874-35-1 5-Methylindan 0.098 0.079 0.069 27.578

114.763 824-63-5 2-Methylindan 0.142 0.115 0.101 40.068

Indenes 104.800 Indan 0.138 0.103 0.110 39.897

105.428 Indene 0.358 0.266 0.284 103.114

109.197 2-Methylindan 0.019 0.014 0.014 5.522

114.512 824-22-6 4-Methylindan 0.136 0.110 0.097 38.420

117.080 1,1-Dimethyl Indane 0.015 0.011 0.010 4.275

Naphthenes

Mono-Naphthenes 27.108 287-92-3 Cyclopentane 1.465 1.411 1.962 395.865

40.165 96-37-7 Methylcyclopentane 2.886 2.768 3.221 779.767

47.067 110-82-7 Cyclohexane 3.280 3.024 3.660 886.034

52.883 1759-58-6 1t,3-Dimethylcyclopentane 0.161 0.155 0.154 43.594

53.470 2532-58-3 1c,3-Dimethylcyclopentane 0.130 0.126 0.125 35.193

54.097 822-50-4 1t,2-Dimethylcyclopentane 0.203 0.194 0.195 54.936

61.062 108-87-2 Methylcyclohexane 0.977 0.912 0.935 264.025

62.013 4516-69-2 1,1,3-Trimethylcyclopentane 0.021 0.020 0.017 5.577

63.857 1640-89-7 Ethylcyclopentane 0.033 0.031 0.032 8.981

65.926 4850-28-6 1c,2t,4-Trimethylcyclopentane 0.019 0.017 0.015 5.002

67.45615890-40-1 1t,2c,3-Trimethylcyclopentane 0.015 0.014 0.012 3.928

72.860 1,3-dimethyl-t-cyclohexane 0.086 0.080 0.072 23.209

76.189 2207-03-6 1t,3-Dimethylcyclohexane 0.035 0.032 0.029 9.362

81.867 1678-91-7 Ethylcyclohexane 0.044 0.040 0.037 11.911

101.319 1678-98-4 i-Butylcyclohexane 0.017 0.015 0.011 4.544

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.404 115-11-7 Isobutene 0.020 0.024 0.034 5.483

9.443 106-98-9 Butene-1 0.024 0.029 0.040 6.413

10.266 624-64-6 t-Butene-2 0.088 0.105 0.148 23.854

10.987 590-18-1 c-Butene-2 0.100 0.116 0.168 27.050

16.335 109-67-1 Pentene-1 0.317 0.356 0.425 85.773

18.801 646-04-8 t-Pentene-2 0.820 0.908 1.098 221.406

19.824 627-20-3 c-Pentene-2 0.448 0.491 0.600 121.087

32.937 592-41-6 Hexene-1 0.149 0.158 0.167 40.364

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C-145
Hydrocarbon Expert V4.7 Thu Aug 26 10:21:23 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91314 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91314

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

n-Olefins 35.93613269-52-8 t-Hexene-3 0.251 0.265 0.281 67.927

36.408 4050-45-7 t-Hexene-2 0.476 0.501 0.531 128.613

38.233 7688-21-3 c-Hexene-2 0.202 0.210 0.226 54.614

56.88414686-14-7 t-Heptene-3 0.016 0.016 0.015 4.191

Iso-Olefins 13.128 563-45-1 3-Methylbutene-1 0.069 0.079 0.092 18.571

17.168 563-46-2 2-Methylbutene-1 0.497 0.549 0.666 134.306

20.489 513-35-9 2-Methylbutene-2 1.025 1.111 1.373 276.986

28.689 691-38-3 4-Methyl-c-pentene-2 0.043 0.045 0.048 11.528

29.337 674-76-0 4-Methyl-t-pentene-2 0.129 0.137 0.144 34.767

32.715 763-29-1 2-Methylpentene-1 0.220 0.230 0.245 59.344

36.897 625-27-4 2-Methylpentene-2 0.334 0.347 0.373 90.341

37.313 922-62-3 3-Methyl-c-pentene-2 0.256 0.263 0.285 69.049

39.584 3404-73-7 3,3-Dimethylpentene-1 0.304 0.311 0.291 82.063

46.164 3404-61-3 3-Methylhexene-1 0.012 0.012 0.011 3.214

46.752 3524-73-0 5-Methylhexene-1 0.088 0.091 0.084 23.815

48.80715840-60-5 2-Methyl-c-hexene-3 0.030 0.031 0.029 8.066

49.797 3404-55-5 4-Methyl-t/c-hexene-2 0.035 0.036 0.033 9.433

57.240 6094-02-6 2-Methylhexene-1 0.024 0.025 0.023 6.589

Naphtheno-Olefins 25.243 142-29-0 Cyclopentene 0.177 0.165 0.245 49.352

45.334 693-89-0 1-Methylcyclopentene 0.313 0.288 0.358 86.500

50.670 110-83-8 Cyclohexene 0.033 0.029 0.038 8.993

Di-Olefins 18.206 78-79-5 2-Methyl-1,3-Butadiene 0.009 0.009 0.012 2.388

20.825 2004-70-8 1t,3-Pentadiene 0.012 0.013 0.017 3.464

Oxygenates 26.491 71-23-8 n-Propanol 0.174 0.156 0.272 32.976

Unidentified 28.230 Unidentified 0.050 0.049 0.053 16.558

47.590 Unidentified 0.027 0.028 0.026 8.919

59.432 Unidentified 0.459 0.458 0.439 151.754

63.642 Unidentified 0.123 0.118 0.105 40.622

64.510 Unidentified 0.321 0.322 0.264 106.239

72.091 Unidentified 0.059 0.059 0.048 19.489

74.102 Unidentified 0.013 0.012 0.011 4.428

75.904 Unidentified 0.010 0.010 0.007 3.365

78.506 Unidentified 0.035 0.033 0.030 11.721

82.672 Unidentified 0.008 0.007 0.007 2.581

84.858 Unidentified 0.018 0.017 0.013 5.985

86.326 Unidentified 0.015 0.015 0.011 4.852

88.478 Unidentified 0.082 0.086 0.061 27.065

93.028 Unidentified 0.014 0.013 0.010 4.670

93.028 Unidentified 0.014 0.014 0.009 4.670

93.028 Unidentified 0.014 0.010 0.009 4.670

93.600 Unidentified 0.099 0.098 0.065 32.754

100.127 Unidentified 0.063 0.045 0.038 20.795

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C-146
Hydrocarbon Expert V4.7 Thu Aug 26 10:21:23 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91314 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91314

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Unidentified 100.252 Unidentified 0.177 0.171 0.107 58.693

100.941 Unidentified 0.103 0.105 0.069 34.022

101.062 Unidentified 0.061 0.060 0.040 20.207

102.974 Unidentified 0.032 0.031 0.019 10.714

104.393 Unidentified 0.069 0.058 0.048 22.878

107.884 Unidentified 0.017 0.017 0.010 5.756

108.548 Unidentified 0.036 0.035 0.022 11.972

113.289 Unidentified 0.009 0.009 0.005 3.017

114.977 Unidentified 0.011 0.009 0.007 3.521

116.801 Unidentified 0.008 0.006 0.005 2.530

Plus

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C-147
Hydrocarbon Expert V4.7 Thu Aug 26 10:21:23 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91314 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91314

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF

20.0 15.0 10.0 5.0 0.0

Propane

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

2,2-Dimethylbutane

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C-148
Hydrocarbon Expert V4.7 Thu Aug 26 10:21:23 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91314 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91314

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

n-Propanol

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

n-Hexane

t-Hexene-3

t-Hexene-2

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane

2,2,3-Trimethylbutane

Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1 Cyclohexane

Unidentified

2-Methyl-c-hexene-3

4-Methyl-t/c-hexene-2

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C-149
Hydrocarbon Expert V4.7 Thu Aug 26 10:21:23 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91314 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91314

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF

70.0 65.0 60.0 55.0 50.0

2-Methylhexane

Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane

2,2,4-Trimethylpentane

t-Heptene-3

2-Methylhexene-1

n-Heptane

Unidentified

Methylcyclohexane

1,1,3-Trimethylcyclopentane

2,2-Dimethylhexane

Unidentified Ethylcyclopentane

Unidentified 2,5-Dimethylhexane

2,4-Dimethylhexane

1c,2t,4-Trimethylcyclopentane

1t,2c,3-Trimethylcyclopentane

2,3,4-Trimethylpentane

Toluene 2,3,3-Trimethylpentane

2,3-Dimethylhexane

2-Methylheptane

Unidentified 4-Methylheptane

1,3-dimethyl-t-cyclohexane 3-Methylheptane 3-Ethylhexane

Unidentified

2,2,5-Trimethylhexane

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C-150
Hydrocarbon Expert V4.7 Thu Aug 26 10:21:23 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91314 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91314

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF

95.0 90.0 85.0 80.0 75.0

Unidentified 1t,3-Dimethylcyclohexane

n-Octane

Unidentified

2,3,5-Trimethylhexane

2,4-Dimethylheptane

Ethylcyclohexane

2,6-Dimethylheptane

Unidentified

2,5-Dimethylheptane

Ethylbenzene

Unidentified

m-Xylene p-Xylene

Unidentified

4-Methyloctane 2-Methyloctane

3-Methyloctane

Unidentified o-Xylene

C10 - IsoParaffin - 1

2,2,4-trimethylheptane

n-Nonane

i-Propylbenzene Unidentified

Unidentified 2,2-Dimethyloctane

2,5-Dimethyloctane

2,7-Dimethyloctane 2,4-Dimethyloctane

2,6-Dimethyloctane

n-Propylbenzene

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

4-Methylnonane 2,2,6-Trimethyloctane 1-Methyl-2-ethylbenzene

3-Methylnonane

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C-151
Hydrocarbon Expert V4.7 Thu Aug 26 10:21:23 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91314 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91314

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified Unidentified C11-Isoparaffin-2 1,2,4-Trimethylbenzene Unidentified

i-Butylcyclohexane

3-Ethyl-3-methylheptane

i-Butylbenzene n-Decane

Unidentified

1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene C11 Isoparaffin-4 Unidentified

Indan

Indene

C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene

1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

Unidentified 1-Methyl-2-n-propylbenzene

C11- Isoparaffin-11 Unidentified

1,4,Dimethyl-2-ethylbenzene 1,3-Dimethyl-4-ethylbenzene 2-Methylindan

1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

1-Methyl-4-t-butylbenzene 1,2-Dimethyl-3-ethylbenzene n-Undecane 1-Ethyl-4-i-propylbenzene

1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene

Unidentified C11 - Aromatic - 3 5-Methylindan 1,2-Di-i-propylbenzene 1-methyl-4-(1-methylpropyl)be C11 - Aromatic - 4 4-Methylindan 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene 1-Methyl-2-n-butylbenzene C11 - Aromatic - 7

1,4-Di-i-propylbenzene

Naphthalene Unidentified 1,1-Dimethyl Indane

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

C11 - Aromatic - 12

2-Methylnaphthalene

1-Methylnaphthalene

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C-152
Hydrocarbon Expert V4.7 Thu Aug 26 10:21:23 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91314 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91314

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000010.D\SIG1000010_FID1_A.CDF

145.0 140.0 135.0 130.0 125.0

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C-153
Hydrocarbon Expert V4.7 Thu Aug 26 10:26:55 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91315 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91315

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 12.781 15.058 18.346

I-Paraffins 51.591 53.212 46.296

Aromatics 22.030 18.057 19.486

Mono-Aromatics 20.939 17.229 18.645

Naphthalenes 0.074 0.052 0.054

Naphtheno/Olefino-Benzs 0.209 0.168 0.151

Indenes 0.807 0.608 0.635

Naphthenes 3.670 3.454 4.023

Mono-Naphthenes 3.670 3.454 4.023

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 6.545 6.950 8.255

n-Olefins 2.929 3.185 3.814

Iso-Olefins 3.070 3.260 3.760

Naphtheno-Olefins 0.525 0.482 0.653

Di-Olefins 0.021 0.022 0.029

Oxygenates 0.176 0.157 0.279

Unidentified 3.207 3.112 3.315

Plus 0.000 0.000 0.000

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C-154
Hydrocarbon Expert V4.7 Thu Aug 26 10:26:55 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91315 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91315

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C3 0.177 0.159 0.282

C4 7.792 9.620 12.807

C5 10.224 11.514 13.667

C6 13.177 13.634 14.805

C7 10.004 9.109 10.034

C8 38.591 37.840 32.623

C9 10.411 9.427 8.028

C10 5.492 4.766 3.866

C11 0.820 0.734 0.513

C12 0.104 0.083 0.061

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C-155
Hydrocarbon Expert V4.7 Thu Aug 26 10:26:55 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91315 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91315

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C3 0.001 0.002 0.003

C4 7.517 9.293 12.342

C5 1.907 2.179 2.523

C6 2.529 2.745 2.801

C7 0.297 0.311 0.283

C8 0.089 0.090 0.074

C9 0.363 0.362 0.270

C10 0.062 0.061 0.042

C11 0.014 0.014 0.009

I-Paraffins C4 0.040 0.051 0.065

C5 4.713 5.445 6.234

C6 5.116 5.562 5.665

C7 2.617 2.758 2.493

C8 32.337 32.648 27.014

C9 4.428 4.463 3.295

C10 1.881 1.845 1.250

C11 0.459 0.441 0.280

Mono-Aromatics C6 0.646 0.526 0.790

C7 5.772 4.764 5.978

C8 6.051 4.996 5.439

C9 5.434 4.459 4.314

C10 2.617 2.143 1.861

C11 0.315 0.256 0.203

C12 0.104 0.083 0.061

Naphthalenes C10 0.055 0.038 0.041

C11 0.019 0.013 0.013

Naphtheno/Olefino-Benzs C10 0.209 0.168 0.151

Indenes C9 0.156 0.116 0.126

C10 0.638 0.483 0.501

C11 0.013 0.009 0.008

Mono-Naphthenes C5 0.207 0.199 0.282

C6 2.472 2.328 2.803

C7 0.843 0.792 0.819

C8 0.094 0.087 0.080

C9 0.031 0.027 0.023

C10 0.023 0.020 0.015

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C-156
Hydrocarbon Expert V4.7 Thu Aug 26 10:26:55 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91315 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91315

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Mono-Naphthenes

n-Olefins C4 0.235 0.276 0.400

C5 1.595 1.760 2.170

C6 1.083 1.133 1.228

C7 0.016 0.016 0.015

Iso-Olefins C5 1.601 1.744 2.178

C6 0.984 1.023 1.116

C7 0.458 0.468 0.445

C8 0.020 0.018 0.015

C10 0.006 0.007 0.004

Naphtheno-Olefins C5 0.179 0.166 0.250

C6 0.346 0.317 0.402

Di-Olefins C5 0.021 0.022 0.029

Oxygenates C3 0.176 0.157 0.279

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C-157
Hydrocarbon Expert V4.7 Thu Aug 26 10:26:55 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91315 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91315

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 21.24 21.10

5% 27.49 26.16

10% 80.12 78.85

15% 96.00 81.85

20% 138.22 100.24

25% 154.03 140.27

30% 169.90 154.81

35% 206.70 176.86

40% 209.73 209.26

45% 210.36 209.87

50% 229.51 210.48

55% 230.86 229.99

60% 234.11 231.76

65% 236.86 235.56

70% 238.19 237.39

75% 254.49 238.95

80% 278.11 255.26

85% 292.29 281.91

90% 327.44 321.10

95% 350.87 336.69

FBP 400.85 388.14

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C-158
Hydrocarbon Expert V4.7 Thu Aug 26 10:26:55 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91315 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91315

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 7.391 74-98-6 P3 Propane 0.001 0.002 0.003 0.304

2 8.612 75-28-5 I4 i-Butane 0.040 0.051 0.065 9.521

3 9.403 115-11-7 K4 Isobutene 0.020 0.025 0.035 5.059

4 9.442 106-98-9 K4 Butene-1 0.024 0.029 0.041 5.955

5 9.791 106-97-8 P4 n-Butane 7.517 9.293 12.342 1799.592

6 10.265 624-64-6 K4 t-Butene-2 0.089 0.106 0.152 22.150

7 10.388 463-82-1 I5 2,2-Dimethylpropane 0.029 0.035 0.038 6.970

8 10.986 590-18-1 K4 c-Butene-2 0.101 0.117 0.172 25.142

9 13.127 563-45-1 C5 3-Methylbutene-1 0.070 0.079 0.095 17.274

10 14.706 78-78-4 I5 i-Pentane 4.684 5.410 6.195 1129.155

11 16.330 109-67-1 K5 Pentene-1 0.320 0.357 0.435 79.317

12 17.166 563-46-2 C5 2-Methylbutene-1 0.500 0.550 0.681 124.010

13 17.689 109-66-0 P5 n-Pentane 1.907 2.179 2.523 459.763

14 18.203 78-79-5 E5 2-Methyl-1,3-Butadiene 0.008 0.009 0.012 2.169

15 18.795 646-04-8 K5 t-Pentene-2 0.825 0.910 1.122 204.461

16 19.817 627-20-3 K5 c-Pentene-2 0.451 0.492 0.613 111.729

17 20.485 513-35-9 C5 2-Methylbutene-2 1.031 1.114 1.403 255.675

18 20.826 2004-70-8 E5 1t,3-Pentadiene 0.012 0.013 0.017 3.165

19 22.613 75-83-2 I6 2,2-Dimethylbutane 0.124 0.137 0.138 30.126

20 25.243 142-29-0 B5 Cyclopentene 0.179 0.166 0.250 45.591

21 26.486 71-23-8 X3 n-Propanol 0.176 0.157 0.279 30.550

22 27.094 287-92-3 M5 Cyclopentane 0.207 0.199 0.282 51.438

23 27.828 79-29-8 I6 2,3-Dimethylbutane 0.856 0.925 0.948 207.098

24 28.222 ? Unidentified 0.050 0.048 0.054 15.201

25 28.684 691-38-3 C6 4-Methyl-c-pentene-2 0.043 0.046 0.049 10.769

26 28.899 107-83-5 I6 2-Methylpentane 2.394 2.623 2.651 579.326

27 29.332 674-76-0 C6 4-Methyl-t-pentene-2 0.129 0.137 0.147 32.078

28 31.543 96-14-0 I6 3-Methylpentane 1.742 1.877 1.929 421.632

29 32.710 763-29-1 C6 2-Methylpentene-1 0.220 0.230 0.250 54.576

30 32.933 592-41-6 K6 Hexene-1 0.151 0.159 0.171 37.317

31 35.291 110-54-3 P6 n-Hexane 2.529 2.745 2.801 612.125

32 35.92913269-52-8 K6 t-Hexene-3 0.252 0.264 0.286 62.455

33 36.401 4050-45-7 K6 t-Hexene-2 0.477 0.500 0.541 118.380

34 36.894 625-27-4 C6 2-Methylpentene-2 0.335 0.347 0.380 83.155

35 37.306 922-62-3 C6 3-Methyl-c-pentene-2 0.256 0.263 0.290 63.497

36 38.233 7688-21-3 K6 c-Hexene-2 0.203 0.210 0.230 50.351

37 39.581 3404-73-7 C7 3,3-Dimethylpentene-1 0.305 0.311 0.296 75.555

38 40.153 96-37-7 M6 Methylcyclopentane 1.533 1.465 1.738 380.015

39 41.726 108-08-7 I7 2,4-Dimethylpentane 0.585 0.623 0.557 142.210

40 42.271 464-06-2 I7 2,2,3-Trimethylbutane 0.049 0.051 0.047 11.987

41 45.132 71-42-3 Q6 Benzene 0.646 0.526 0.790 172.575

42 45.337 693-89-0 B6 1-Methylcyclopentene 0.313 0.287 0.364 79.482

43 46.157 3404-61-3 C7 3-Methylhexene-1 0.012 0.012 0.012 3.005

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C-159
Hydrocarbon Expert V4.7 Thu Aug 26 10:26:55 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91315 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91315

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 46.738 3524-73-0 C7 5-Methylhexene-1 0.054 0.055 0.052 13.343

45 47.047 110-82-7 M6 Cyclohexane 0.939 0.863 1.065 232.871

46 48.80115840-60-5 C7 2-Methyl-c-hexene-3 0.030 0.031 0.029 7.336

47 49.800 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.033 0.034 0.032 8.173

48 50.197 591-76-4 I7 2-Methylhexane 1.472 1.552 1.402 357.716

49 50.669 110-83-8 B6 Cyclohexene 0.033 0.029 0.039 8.245

50 52.028 589-34-4 I7 3-Methylhexane 0.510 0.532 0.486 124.039

51 52.880 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.112 0.107 0.109 27.833

52 53.473 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.086 0.083 0.084 21.353

53 54.096 822-50-4 M7 1t,2-Dimethylcyclopentane 0.111 0.106 0.108 27.642

54 54.761 540-84-1 I8 2,2,4-Trimethylpentane 11.461 11.852 9.574 2790.355

55 56.88414686-14-7 K7 t-Heptene-3 0.016 0.016 0.015 3.950

56 57.238 6094-02-6 C7 2-Methylhexene-1 0.025 0.026 0.024 6.224

57 57.615 142-82-5 P7 n-Heptane 0.297 0.311 0.283 72.223

58 61.059 108-87-2 M7 Methylcyclohexane 0.513 0.477 0.499 127.214

59 63.856 1640-89-7 M7 Ethylcyclopentane 0.020 0.019 0.019 4.952

60 64.510 564-02-3 I8 2,2,3-Trimethylpentane 0.663 0.663 0.554 161.495

61 64.758 592-13-2 I8 2,5-Dimethylhexane 1.330 1.373 1.111 323.907

62 65.096 589-43-5 I8 2,4-Dimethylhexane 1.092 1.116 0.912 265.925

63 68.126 565-75-3 I8 2,3,4-Trimethylpentane 6.897 6.863 5.761 1679.101

64 68.633 108-88-3 Q7 Toluene 5.772 4.764 5.978 1524.479

65 68.814 560-21-4 I8 2,3,3-Trimethylpentane 8.803 8.674 7.354 2143.232

66 70.436 584-94-1 I8 2,3-Dimethylhexane 1.645 1.653 1.375 400.609

67 71.698 592-27-8 I8 2-Methylheptane 0.108 0.110 0.090 26.218

68 71.963 589-53-7 I8 4-Methylheptane 0.200 0.203 0.167 48.673

69 72.093 ? Unidentified 0.141 0.141 0.118 42.947

70 72.863 M8 1,3-dimethyl-t-cyclohexane 0.048 0.044 0.040 11.803

71 73.021 589-81-1 I8 3-Methylheptane 0.102 0.104 0.086 24.949

72 73.202 619-99-8 I8 3-Ethylhexane 0.036 0.036 0.030 8.672

73 74.942 3522-94-9 I9 2,2,5-Trimethylhexane 3.275 3.314 2.437 798.940

74 75.909 ? Unidentified 0.025 0.024 0.019 7.558

75 76.194 2207-03-6 M8 1t,3-Dimethylcyclohexane 0.020 0.018 0.017 4.919

76 77.563 111-65-9 P8 n-Octane 0.089 0.090 0.074 21.621

77 78.507 ? Unidentified 0.084 0.081 0.062 25.461

78 80.058 1069-53-0 I9 2,3,5-Trimethylhexane 0.635 0.630 0.473 154.964

79 81.232 1071-26-7 I9 2,4-Dimethylheptane 0.074 0.075 0.055 18.127

80 81.867 1678-91-7 M8 Ethylcyclohexane 0.026 0.024 0.022 6.552

81 82.194 1072-05-5 I9 2,6-Dimethylheptane 0.109 0.110 0.081 26.617

82 82.674 ? Unidentified 0.008 0.009 0.006 2.483

83 83.128 I9 2,5-Dimethylheptane 0.291 0.291 0.217 71.006

84 84.439 100-41-4 Q8 Ethylbenzene 1.019 0.841 0.916 267.051

85 84.617 ? Unidentified 0.046 0.045 0.035 13.925

86 84.857 ? Unidentified 0.038 0.035 0.029 11.560

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C-160
Hydrocarbon Expert V4.7 Thu Aug 26 10:26:55 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91315 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91315

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 85.669 108-38-3 Q8 m-Xylene 2.759 2.284 2.480 723.115

88 85.817 106-42-3 Q8 p-Xylene 1.267 1.053 1.139 332.164

89 85.963 ? Unidentified 0.095 0.093 0.070 28.711

90 86.219 C8 C9-IsoOlefin-3 0.020 0.018 0.015 4.986

91 86.327 ? Unidentified 0.017 0.017 0.013 5.245

92 87.014 2216-34-4 I9 4-Methyloctane 0.011 0.011 0.008 2.743

93 87.146 3221-61-2 I9 2-Methyloctane 0.016 0.016 0.012 3.945

94 88.011 2216-33-3 I9 3-Methyloctane 0.016 0.016 0.012 3.948

95 88.480 ? Unidentified 0.276 0.289 0.208 83.729

96 88.650 95-47-6 Q8 o-Xylene 1.007 0.818 0.905 263.837

97 89.068 I10 C10 - IsoParaffin - 1 0.808 0.794 0.542 197.423

98 89.91414720-74-2 I10 2,2,4-trimethylheptane 0.556 0.547 0.373 136.024

99 91.461 111-84-2 P9 n-Nonane 0.363 0.362 0.270 88.528

100 92.083 4926-90-3 M9 1,1-Methylethylcyclohexane 0.024 0.022 0.018 6.022

101 92.837 98-82-8 Q9 i-Propylbenzene 0.033 0.027 0.026 8.478

102 93.028 ? Unidentified 0.017 0.016 0.013 5.221

103 93.028 ? Unidentified 0.017 0.018 0.012 5.221

104 93.028 ? Unidentified 0.017 0.012 0.012 5.221

105 93.133 696-29-7 M9 1-Methyl-2-propyl-cyclopentan 0.006 0.006 0.005 1.603

106 93.133 C10 C10-IsoOlefin-4 0.006 0.007 0.004 1.603

107 93.133 I10 C10-isoparaffin-x 0.000 0.000 0.000 1.603

108 93.602 ? Unidentified 0.193 0.191 0.129 58.622

109 93.82415869-87-1 I10 2,2-Dimethyloctane 0.063 0.062 0.042 15.285

110 94.269 ? Unidentified 0.012 0.008 1.105 3.517

111 94.269 ? Unidentified 0.012 0.012 0.008 3.517

112 94.62515869-89-3 I10 2,5-Dimethyloctane 0.062 0.061 0.042 15.240

113 95.101 2040-95-1 I10 2,7-Dimethyloctane 0.026 0.025 0.017 6.357

114 95.265 2051-30-1 I10 2,4-Dimethyloctane 0.114 0.112 0.076 27.766

115 95.660 I10 2,6-Dimethyloctane 0.037 0.036 0.025 9.036

116 96.303 103-65-1 Q9 n-Propylbenzene 0.262 0.218 0.208 68.313

117 97.152 620-14-4 Q9 1-Methyl-3-ethylbenzene 1.018 0.843 0.808 265.192

118 97.386 622-96-8 Q9 1-Methyl-4-ethylbenzene 0.488 0.406 0.388 127.206

119 98.014 108-67-8 Q9 1,3,5-Trimethylbenzene 0.694 0.574 0.551 180.862

120 98.68417301-94-8 I10 4-Methylnonane 0.010 0.010 0.007 2.454

121 98.889 ? Unidentified 1.284 1.265 0.861 390.019

122 99.097 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.404 0.329 0.321 105.308

123 99.467 ? Unidentified 0.004 0.004 0.003 1.244

124 99.661 5911-04-6 I10 3-Methylnonane 0.014 0.014 0.009 3.450

125 100.127 ? Unidentified 0.089 0.064 0.054 27.013

126 100.253 ? Unidentified 0.239 0.230 0.146 72.642

127 100.478 I11 C11-Isoparaffin-2 0.128 0.123 0.078 31.380

128 100.736 95-63-6 Q9 1,2,4-Trimethylbenzene 2.134 1.743 1.694 555.657

129 100.941 ? Unidentified 0.143 0.146 0.098 43.555

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C-161
Hydrocarbon Expert V4.7 Thu Aug 26 10:26:55 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91315 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91315

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 101.063 ? Unidentified 0.086 0.084 0.057 25.995

131 101.320 1678-98-4 M10 i-Butylcyclohexane 0.023 0.020 0.015 5.616

132 101.964 ? Unidentified 0.008 0.007 0.005 2.437

133 102.10717302-01-1 I10 3-Ethyl-3-methylheptane 0.191 0.184 0.117 46.826

134 102.460 538-93-2 Q10 i-Butylbenzene 0.213 0.179 0.151 55.175

135 102.660 124-18-5 P10 n-Decane 0.062 0.061 0.042 15.250

136 102.974 ? Unidentified 0.045 0.043 0.028 13.737

137 103.611 526-73-8 Q9 1,2,3-Trimethylbenzene 0.400 0.320 0.317 104.112

138 103.992 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.021 0.017 0.015 5.372

139 104.190 I11 C11 Isoparaffin-4 0.021 0.020 0.013 5.086

140 104.395 ? Unidentified 0.093 0.077 0.066 28.152

141 104.800 J9 Indan 0.156 0.116 0.126 41.272

142 105.428 J10 Indene 0.471 0.350 0.381 124.780

143 106.145 I11 C11-Isoparaffin-7 0.147 0.142 0.090 36.015

144 106.331 141-93-5 Q10 1,3-Diethylbenzene 0.055 0.046 0.039 14.329

145 106.617 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 0.528 0.439 0.376 136.898

146 106.944 105-05-5 Q10 1,4-Diethylbenzene 0.191 0.159 0.136 49.561

147 107.173 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.145 0.118 0.103 37.440

148 107.434 135-01-3 Q10 1,2-Diethylbenzene 0.032 0.026 0.023 8.355

149 107.885 ? Unidentified 0.024 0.023 0.014 7.161

150 108.024 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.051 0.041 0.036 13.086

151 108.160 ? Unidentified 0.024 0.023 0.015 7.141

152 108.242 ? Unidentified 0.021 0.020 0.013 6.319

153 108.362 I11 C11- Isoparaffin-11 0.163 0.156 0.099 39.817

154 108.550 ? Unidentified 0.047 0.045 0.029 14.197

155 108.874 1758-88-9 Q10 1,4,Dimethyl-2-ethylbenzene 0.114 0.093 0.081 29.579

156 109.028 874-41-9 Q10 1,3-Dimethyl-4-ethylbenzene 0.229 0.187 0.163 59.253

157 109.199 J10 2-Methylindan 0.022 0.017 0.016 5.949

158 109.542 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.272 0.223 0.193 70.444

159 110.097 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.090 0.072 0.064 23.357

160 111.009 Q11 1-Methyl-4-t-butylbenzene 0.026 0.022 0.017 6.733

161 111.221 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.099 0.080 0.071 25.729

162 111.528 1120-21-4 P11 n-Undecane 0.014 0.014 0.009 3.507

163 111.689 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.015 0.012 0.010 3.853

164 112.161 Q10 1,2,4,5-Tetramethylbenzene 0.237 0.191 0.169 61.470

165 112.428 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.339 0.273 0.241 87.889

166 113.581 Q11 C11 - Aromatic - 3 0.049 0.040 0.032 12.740

167 113.761 874-35-1 H10 5-Methylindan 0.105 0.084 0.076 27.119

168 113.901 Q12 1,2-Di-i-propylbenzene 0.041 0.033 0.024 10.657

169 114.116 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.058 0.047 0.037 15.015

170 114.278 Q11 C11 - Aromatic - 4 0.027 0.022 0.018 7.015

171 114.512 824-22-6 J10 4-Methylindan 0.145 0.116 0.104 37.454

172 114.680 ? Unidentified 0.026 0.021 0.017 8.049

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C-162
Hydrocarbon Expert V4.7 Thu Aug 26 10:26:55 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91315 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91315

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 114.764 824-63-5 H10 2-Methylindan 0.104 0.084 0.075 27.061

174 114.977 ? Unidentified 0.010 0.008 0.007 3.113

175 115.089 538-68-1 Q11 n-Pentylbenzene 0.012 0.010 0.008 3.052

176 115.317 Q11 tert-Pentylbenzene 0.056 0.045 0.036 14.562

177 115.632 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.022 0.018 0.014 5.778

178 115.742 Q11 C11 - Aromatic - 7 0.029 0.024 0.019 7.454

179 116.204 100-18-5 Q12 1,4-Di-i-propylbenzene 0.038 0.030 0.022 9.646

180 116.633 91-20-3 G10 Naphthalene 0.055 0.038 0.041 14.950

181 116.797 J11 4,7-Dimethyl Indane 0.008 0.006 0.005 2.148

182 117.080 J11 1,1-Dimethyl Indane 0.005 0.003 0.003 1.223

183 117.735 Q12 1,3-Di-n-propylbenzene 0.025 0.020 0.015 6.398

184 117.846 Q11 C11 - Aromatic - 11 0.012 0.010 0.008 3.082

185 118.401 Q11 C11 - Aromatic - 12 0.008 0.006 0.005 1.973

186 123.280 91-57-6 G11 2-Methylnaphthalene 0.013 0.009 0.009 3.444

187 124.145 90-12-0 G11 1-Methylnaphthalene 0.006 0.004 0.004 1.708

188 126.171 ? Unidentified 0.004 0.004 0.003 1.353

189 126.171 ? Unidentified 0.004 0.004 0.002 1.353

190 126.171 ? Unidentified 0.004 0.004 0.002 1.353

191 129.863 ? Unidentified 0.004 0.003 0.002 1.077

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C-163
Hydrocarbon Expert V4.7 Thu Aug 26 10:26:55 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91315 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91315

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 7.391 74-98-6 Propane 0.001 0.002 0.003 0.304

9.791 106-97-8 n-Butane 7.517 9.293 12.342 1799.592

17.689 109-66-0 n-Pentane 1.907 2.179 2.523 459.763

35.291 110-54-3 n-Hexane 2.529 2.745 2.801 612.125

57.615 142-82-5 n-Heptane 0.297 0.311 0.283 72.223

77.563 111-65-9 n-Octane 0.089 0.090 0.074 21.621

91.461 111-84-2 n-Nonane 0.363 0.362 0.270 88.528

102.660 124-18-5 n-Decane 0.062 0.061 0.042 15.250

111.528 1120-21-4 n-Undecane 0.014 0.014 0.009 3.507

I-Paraffins 8.612 75-28-5 i-Butane 0.040 0.051 0.065 9.521

10.388 463-82-1 2,2-Dimethylpropane 0.029 0.035 0.038 6.970

14.706 78-78-4 i-Pentane 4.684 5.410 6.195 1129.155

22.613 75-83-2 2,2-Dimethylbutane 0.124 0.137 0.138 30.126

27.828 79-29-8 2,3-Dimethylbutane 0.856 0.925 0.948 207.098

28.899 107-83-5 2-Methylpentane 2.394 2.623 2.651 579.326

31.543 96-14-0 3-Methylpentane 1.742 1.877 1.929 421.632

41.726 108-08-7 2,4-Dimethylpentane 0.585 0.623 0.557 142.210

42.271 464-06-2 2,2,3-Trimethylbutane 0.049 0.051 0.047 11.987

50.197 591-76-4 2-Methylhexane 1.472 1.552 1.402 357.716

52.028 589-34-4 3-Methylhexane 0.510 0.532 0.486 124.039

54.761 540-84-1 2,2,4-Trimethylpentane 11.461 11.852 9.574 2790.355

64.510 564-02-3 2,2,3-Trimethylpentane 0.663 0.663 0.554 161.495

64.758 592-13-2 2,5-Dimethylhexane 1.330 1.373 1.111 323.907

65.096 589-43-5 2,4-Dimethylhexane 1.092 1.116 0.912 265.925

68.126 565-75-3 2,3,4-Trimethylpentane 6.897 6.863 5.761 1679.101

68.814 560-21-4 2,3,3-Trimethylpentane 8.803 8.674 7.354 2143.232

70.436 584-94-1 2,3-Dimethylhexane 1.645 1.653 1.375 400.609

71.698 592-27-8 2-Methylheptane 0.108 0.110 0.090 26.218

71.963 589-53-7 4-Methylheptane 0.200 0.203 0.167 48.673

73.021 589-81-1 3-Methylheptane 0.102 0.104 0.086 24.949

73.202 619-99-8 3-Ethylhexane 0.036 0.036 0.030 8.672

74.942 3522-94-9 2,2,5-Trimethylhexane 3.275 3.314 2.437 798.940

80.058 1069-53-0 2,3,5-Trimethylhexane 0.635 0.630 0.473 154.964

81.232 1071-26-7 2,4-Dimethylheptane 0.074 0.075 0.055 18.127

82.194 1072-05-5 2,6-Dimethylheptane 0.109 0.110 0.081 26.617

83.128 2,5-Dimethylheptane 0.291 0.291 0.217 71.006

87.014 2216-34-4 4-Methyloctane 0.011 0.011 0.008 2.743

87.146 3221-61-2 2-Methyloctane 0.016 0.016 0.012 3.945

88.011 2216-33-3 3-Methyloctane 0.016 0.016 0.012 3.948

89.068 C10 - IsoParaffin - 1 0.808 0.794 0.542 197.423

89.91414720-74-2 2,2,4-trimethylheptane 0.556 0.547 0.373 136.024

93.133 C10-isoparaffin-x 0.000 0.000 0.000 1.603

93.82415869-87-1 2,2-Dimethyloctane 0.063 0.062 0.042 15.285

94.62515869-89-3 2,5-Dimethyloctane 0.062 0.061 0.042 15.240

95.101 2040-95-1 2,7-Dimethyloctane 0.026 0.025 0.017 6.357

95.265 2051-30-1 2,4-Dimethyloctane 0.114 0.112 0.076 27.766

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C-164
Hydrocarbon Expert V4.7 Thu Aug 26 10:26:55 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91315 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91315

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

I-Paraffins 95.660 2,6-Dimethyloctane 0.037 0.036 0.025 9.036

98.68417301-94-8 4-Methylnonane 0.010 0.010 0.007 2.454

99.661 5911-04-6 3-Methylnonane 0.014 0.014 0.009 3.450

100.478 C11-Isoparaffin-2 0.128 0.123 0.078 31.380

102.10717302-01-1 3-Ethyl-3-methylheptane 0.191 0.184 0.117 46.826

104.190 C11 Isoparaffin-4 0.021 0.020 0.013 5.086

106.145 C11-Isoparaffin-7 0.147 0.142 0.090 36.015

108.362 C11- Isoparaffin-11 0.163 0.156 0.099 39.817

Aromatics

Mono-Aromatics 45.132 71-42-3 Benzene 0.646 0.526 0.790 172.575

68.633 108-88-3 Toluene 5.772 4.764 5.978 1524.479

84.439 100-41-4 Ethylbenzene 1.019 0.841 0.916 267.051

85.669 108-38-3 m-Xylene 2.759 2.284 2.480 723.115

85.817 106-42-3 p-Xylene 1.267 1.053 1.139 332.164

88.650 95-47-6 o-Xylene 1.007 0.818 0.905 263.837

92.837 98-82-8 i-Propylbenzene 0.033 0.027 0.026 8.478

96.303 103-65-1 n-Propylbenzene 0.262 0.218 0.208 68.313

97.152 620-14-4 1-Methyl-3-ethylbenzene 1.018 0.843 0.808 265.192

97.386 622-96-8 1-Methyl-4-ethylbenzene 0.488 0.406 0.388 127.206

98.014 108-67-8 1,3,5-Trimethylbenzene 0.694 0.574 0.551 180.862

99.097 611-14-3 1-Methyl-2-ethylbenzene 0.404 0.329 0.321 105.308

100.736 95-63-6 1,2,4-Trimethylbenzene 2.134 1.743 1.694 555.657

102.460 538-93-2 i-Butylbenzene 0.213 0.179 0.151 55.175

103.611 526-73-8 1,2,3-Trimethylbenzene 0.400 0.320 0.317 104.112

103.992 535-77-3 1-Methyl-3-i-propylbenzene 0.021 0.017 0.015 5.372

106.331 141-93-5 1,3-Diethylbenzene 0.055 0.046 0.039 14.329

106.617 1074-43-7 1-Methyl-3-n-propylbenzene 0.528 0.439 0.376 136.898

106.944 105-05-5 1,4-Diethylbenzene 0.191 0.159 0.136 49.561

107.173 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.145 0.118 0.103 37.440

107.434 135-01-3 1,2-Diethylbenzene 0.032 0.026 0.023 8.355

108.024 1074-17-5 1-Methyl-2-n-propylbenzene 0.051 0.041 0.036 13.086

108.874 1758-88-9 1,4,Dimethyl-2-ethylbenzene 0.114 0.093 0.081 29.579

109.028 874-41-9 1,3-Dimethyl-4-ethylbenzene 0.229 0.187 0.163 59.253

109.542 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.272 0.223 0.193 70.444

110.097 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.090 0.072 0.064 23.357

111.009 1-Methyl-4-t-butylbenzene 0.026 0.022 0.017 6.733

111.221 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.099 0.080 0.071 25.729

111.689 4218-48-8 1-Ethyl-4-i-propylbenzene 0.015 0.012 0.010 3.853

112.161 1,2,4,5-Tetramethylbenzene 0.237 0.191 0.169 61.470

112.428 527-53-7 1,2,3,5-Tetramethylbenzene 0.339 0.273 0.241 87.889

113.581 C11 - Aromatic - 3 0.049 0.040 0.032 12.740

113.901 1,2-Di-i-propylbenzene 0.041 0.033 0.024 10.657

114.116 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.058 0.047 0.037 15.015

114.278 C11 - Aromatic - 4 0.027 0.022 0.018 7.015

115.089 538-68-1 n-Pentylbenzene 0.012 0.010 0.008 3.052

115.317 tert-Pentylbenzene 0.056 0.045 0.036 14.562

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C-165
Hydrocarbon Expert V4.7 Thu Aug 26 10:26:55 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91315 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91315

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 115.632 577-55-9 1-Methyl-2-n-butylbenzene 0.022 0.018 0.014 5.778

115.742 C11 - Aromatic - 7 0.029 0.024 0.019 7.454

116.204 100-18-5 1,4-Di-i-propylbenzene 0.038 0.030 0.022 9.646

117.735 1,3-Di-n-propylbenzene 0.025 0.020 0.015 6.398

117.846 C11 - Aromatic - 11 0.012 0.010 0.008 3.082

118.401 C11 - Aromatic - 12 0.008 0.006 0.005 1.973

Naphthalenes 116.633 91-20-3 Naphthalene 0.055 0.038 0.041 14.950

123.280 91-57-6 2-Methylnaphthalene 0.013 0.009 0.009 3.444

124.145 90-12-0 1-Methylnaphthalene 0.006 0.004 0.004 1.708

Naphtheno/Olefino-Benzs 113.761 874-35-1 5-Methylindan 0.105 0.084 0.076 27.119

114.764 824-63-5 2-Methylindan 0.104 0.084 0.075 27.061

Indenes 104.800 Indan 0.156 0.116 0.126 41.272

105.428 Indene 0.471 0.350 0.381 124.780

109.199 2-Methylindan 0.022 0.017 0.016 5.949

114.512 824-22-6 4-Methylindan 0.145 0.116 0.104 37.454

116.797 4,7-Dimethyl Indane 0.008 0.006 0.005 2.148

117.080 1,1-Dimethyl Indane 0.005 0.003 0.003 1.223

Naphthenes

Mono-Naphthenes 27.094 287-92-3 Cyclopentane 0.207 0.199 0.282 51.438

40.153 96-37-7 Methylcyclopentane 1.533 1.465 1.738 380.015

47.047 110-82-7 Cyclohexane 0.939 0.863 1.065 232.871

52.880 1759-58-6 1t,3-Dimethylcyclopentane 0.112 0.107 0.109 27.833

53.473 2532-58-3 1c,3-Dimethylcyclopentane 0.086 0.083 0.084 21.353

54.096 822-50-4 1t,2-Dimethylcyclopentane 0.111 0.106 0.108 27.642

61.059 108-87-2 Methylcyclohexane 0.513 0.477 0.499 127.214

63.856 1640-89-7 Ethylcyclopentane 0.020 0.019 0.019 4.952

72.863 1,3-dimethyl-t-cyclohexane 0.048 0.044 0.040 11.803

76.194 2207-03-6 1t,3-Dimethylcyclohexane 0.020 0.018 0.017 4.919

81.867 1678-91-7 Ethylcyclohexane 0.026 0.024 0.022 6.552

92.083 4926-90-3 1,1-Methylethylcyclohexane 0.024 0.022 0.018 6.022

93.133 696-29-7 1-Methyl-2-propyl-cyclopentan 0.006 0.006 0.005 1.603

101.320 1678-98-4 i-Butylcyclohexane 0.023 0.020 0.015 5.616

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.403 115-11-7 Isobutene 0.020 0.025 0.035 5.059

9.442 106-98-9 Butene-1 0.024 0.029 0.041 5.955

10.265 624-64-6 t-Butene-2 0.089 0.106 0.152 22.150

10.986 590-18-1 c-Butene-2 0.101 0.117 0.172 25.142

16.330 109-67-1 Pentene-1 0.320 0.357 0.435 79.317

18.795 646-04-8 t-Pentene-2 0.825 0.910 1.122 204.461

19.817 627-20-3 c-Pentene-2 0.451 0.492 0.613 111.729

32.933 592-41-6 Hexene-1 0.151 0.159 0.171 37.317

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C-166
Hydrocarbon Expert V4.7 Thu Aug 26 10:26:55 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91315 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91315

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

n-Olefins 35.92913269-52-8 t-Hexene-3 0.252 0.264 0.286 62.455

36.401 4050-45-7 t-Hexene-2 0.477 0.500 0.541 118.380

38.233 7688-21-3 c-Hexene-2 0.203 0.210 0.230 50.351

56.88414686-14-7 t-Heptene-3 0.016 0.016 0.015 3.950

Iso-Olefins 13.127 563-45-1 3-Methylbutene-1 0.070 0.079 0.095 17.274

17.166 563-46-2 2-Methylbutene-1 0.500 0.550 0.681 124.010

20.485 513-35-9 2-Methylbutene-2 1.031 1.114 1.403 255.675

28.684 691-38-3 4-Methyl-c-pentene-2 0.043 0.046 0.049 10.769

29.332 674-76-0 4-Methyl-t-pentene-2 0.129 0.137 0.147 32.078

32.710 763-29-1 2-Methylpentene-1 0.220 0.230 0.250 54.576

36.894 625-27-4 2-Methylpentene-2 0.335 0.347 0.380 83.155

37.306 922-62-3 3-Methyl-c-pentene-2 0.256 0.263 0.290 63.497

39.581 3404-73-7 3,3-Dimethylpentene-1 0.305 0.311 0.296 75.555

46.157 3404-61-3 3-Methylhexene-1 0.012 0.012 0.012 3.005

46.738 3524-73-0 5-Methylhexene-1 0.054 0.055 0.052 13.343

48.80115840-60-5 2-Methyl-c-hexene-3 0.030 0.031 0.029 7.336

49.800 3404-55-5 4-Methyl-t/c-hexene-2 0.033 0.034 0.032 8.173

57.238 6094-02-6 2-Methylhexene-1 0.025 0.026 0.024 6.224

86.219 C9-IsoOlefin-3 0.020 0.018 0.015 4.986

93.133 C10-IsoOlefin-4 0.006 0.007 0.004 1.603

Naphtheno-Olefins 25.243 142-29-0 Cyclopentene 0.179 0.166 0.250 45.591

45.337 693-89-0 1-Methylcyclopentene 0.313 0.287 0.364 79.482

50.669 110-83-8 Cyclohexene 0.033 0.029 0.039 8.245

Di-Olefins 18.203 78-79-5 2-Methyl-1,3-Butadiene 0.008 0.009 0.012 2.169

20.826 2004-70-8 1t,3-Pentadiene 0.012 0.013 0.017 3.165

Oxygenates 26.486 71-23-8 n-Propanol 0.176 0.157 0.279 30.550

Unidentified 28.222 Unidentified 0.050 0.048 0.054 15.201

72.093 Unidentified 0.141 0.141 0.118 42.947

75.909 Unidentified 0.025 0.024 0.019 7.558

78.507 Unidentified 0.084 0.081 0.062 25.461

82.674 Unidentified 0.008 0.009 0.006 2.483

84.617 Unidentified 0.046 0.045 0.035 13.925

84.857 Unidentified 0.038 0.035 0.029 11.560

85.963 Unidentified 0.095 0.093 0.070 28.711

86.327 Unidentified 0.017 0.017 0.013 5.245

88.480 Unidentified 0.276 0.289 0.208 83.729

93.028 Unidentified 0.017 0.016 0.013 5.221

93.028 Unidentified 0.017 0.018 0.012 5.221

93.028 Unidentified 0.017 0.012 0.012 5.221

93.602 Unidentified 0.193 0.191 0.129 58.622

94.269 Unidentified 0.012 0.008 1.105 3.517

94.269 Unidentified 0.012 0.012 0.008 3.517

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C-167
Hydrocarbon Expert V4.7 Thu Aug 26 10:26:55 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91315 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91315

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Unidentified 98.889 Unidentified 1.284 1.265 0.861 390.019

99.467 Unidentified 0.004 0.004 0.003 1.244

100.127 Unidentified 0.089 0.064 0.054 27.013

100.253 Unidentified 0.239 0.230 0.146 72.642

100.941 Unidentified 0.143 0.146 0.098 43.555

101.063 Unidentified 0.086 0.084 0.057 25.995

101.964 Unidentified 0.008 0.007 0.005 2.437

102.974 Unidentified 0.045 0.043 0.028 13.737

104.395 Unidentified 0.093 0.077 0.066 28.152

107.885 Unidentified 0.024 0.023 0.014 7.161

108.160 Unidentified 0.024 0.023 0.015 7.141

108.242 Unidentified 0.021 0.020 0.013 6.319

108.550 Unidentified 0.047 0.045 0.029 14.197

114.680 Unidentified 0.026 0.021 0.017 8.049

114.977 Unidentified 0.010 0.008 0.007 3.113

126.171 Unidentified 0.004 0.004 0.003 1.353

126.171 Unidentified 0.004 0.004 0.002 1.353

126.171 Unidentified 0.004 0.004 0.002 1.353

129.863 Unidentified 0.004 0.003 0.002 1.077

Plus

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C-168
Hydrocarbon Expert V4.7 Thu Aug 26 10:26:55 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91315 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91315

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF

20.0 15.0 10.0 5.0 0.0

Propane

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

2,2-Dimethylbutane

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C-169
Hydrocarbon Expert V4.7 Thu Aug 26 10:26:55 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91315 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91315

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

n-Propanol

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

n-Hexane

t-Hexene-3

t-Hexene-2

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane

2,2,3-Trimethylbutane

Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1 Cyclohexane

2-Methyl-c-hexene-3

4-Methyl-t/c-hexene-2

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C-170
Hydrocarbon Expert V4.7 Thu Aug 26 10:26:55 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91315 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91315

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF

70.0 65.0 60.0 55.0 50.0

2-Methylhexane

Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane

2,2,4-Trimethylpentane

t-Heptene-3

2-Methylhexene-1

n-Heptane

Methylcyclohexane

Ethylcyclopentane

2,2,3-Trimethylpentane 2,5-Dimethylhexane

2,4-Dimethylhexane

2,3,4-Trimethylpentane

Toluene 2,3,3-Trimethylpentane

2,3-Dimethylhexane

2-Methylheptane

Unidentified 4-Methylheptane

1,3-dimethyl-t-cyclohexane 3-Methylheptane 3-Ethylhexane

2,2,5-Trimethylhexane

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C-171
Hydrocarbon Expert V4.7 Thu Aug 26 10:26:55 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91315 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91315

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF

95.0 90.0 85.0 80.0 75.0

Unidentified 1t,3-Dimethylcyclohexane

n-Octane

Unidentified

2,3,5-Trimethylhexane

2,4-Dimethylheptane

Ethylcyclohexane

2,6-Dimethylheptane

Unidentified

2,5-Dimethylheptane

Ethylbenzene Unidentified

m-Xylene Unidentifiedp-Xylene

C9-IsoOlefin-3 Unidentified

4-Methyloctane 2-Methyloctane

3-Methyloctane

Unidentified o-Xylene

C10 - IsoParaffin - 1

2,2,4-trimethylheptane

n-Nonane

1,1-Methylethylcyclohexane

i-Propylbenzene 1-Methyl-2-propyl-cyclopentan/C10-IsoOlefin-4/C10-isoparaffin-x Unidentified

Unidentified 2,2-Dimethyloctane

Unidentified

2,5-Dimethyloctane

2,7-Dimethyloctane 2,4-Dimethyloctane

2,6-Dimethyloctane

n-Propylbenzene

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

4-Methylnonane Unidentified 1-Methyl-2-ethylbenzene

Unidentified 3-Methylnonane

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C-172
Hydrocarbon Expert V4.7 Thu Aug 26 10:26:55 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91315 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91315

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified Unidentified C11-Isoparaffin-21,2,4-Trimethylbenzene Unidentified

i-Butylcyclohexane

Unidentified 3-Ethyl-3-methylheptane

i-Butylbenzene n-Decane Unidentified

1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene C11 Isoparaffin-4 Unidentified

Indan

Indene

C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene

1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

Unidentified 1-Methyl-2-n-propylbenzene

C11- Isoparaffin-11 Unidentified

1,4,Dimethyl-2-ethylbenzene 1,3-Dimethyl-4-ethylbenzene 2-Methylindan

1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

1-Methyl-4-t-butylbenzene 1,2-Dimethyl-3-ethylbenzene n-Undecane 1-Ethyl-4-i-propylbenzene

1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene

C11 - Aromatic - 3 5-Methylindan 1,2-Di-i-propylbenzene 1-methyl-4-(1-methylpropyl)be C11 - Aromatic - 4 4-Methylindan Unidentified 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene 1-Methyl-2-n-butylbenzene C11 - Aromatic - 7

1,4-Di-i-propylbenzene

Naphthalene 4,7-Dimethyl Indane 1,1-Dimethyl Indane

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

C11 - Aromatic - 12

2-Methylnaphthalene

1-Methylnaphthalene

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C-173
Hydrocarbon Expert V4.7 Thu Aug 26 10:26:55 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91315 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91315

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000011.D\SIG1000011_FID1_A.CDF

145.0 140.0 135.0 130.0 125.0

Unidentified

Unidentified

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C-174
Hydrocarbon Expert V4.7 Thu Aug 26 13:36:06 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91316 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91316

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 13.967 16.585 17.183

I-Paraffins 23.619 27.367 26.260

Aromatics 47.067 40.259 40.242

Mono-Aromatics 44.465 38.173 38.390

Naphthalenes 0.252 0.184 0.177

Naphtheno/Olefino-Benzs 0.756 0.634 0.519

Indenes 1.594 1.268 1.156

Naphthenes 5.847 5.746 6.153

Mono-Naphthenes 5.847 5.746 6.153

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 6.969 7.721 8.350

n-Olefins 3.107 3.525 3.842

Iso-Olefins 3.277 3.632 3.813

Naphtheno-Olefins 0.563 0.539 0.665

Di-Olefins 0.023 0.025 0.030

Oxygenates 0.188 0.175 0.283

Unidentified 2.344 2.148 1.529

Plus 0.000 0.000 0.000

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C-175
Hydrocarbon Expert V4.7 Thu Aug 26 13:36:06 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91316 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91316

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C3 0.189 0.177 0.285

C4 4.561 5.869 7.131

C5 18.430 21.880 23.317

C6 21.530 23.383 22.919

C7 22.174 19.947 21.525

C8 13.659 11.870 11.640

C9 3.834 3.286 2.891

C10 10.043 8.526 6.847

C11 2.646 2.415 1.584

C12 0.590 0.499 0.331

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C-176
Hydrocarbon Expert V4.7 Thu Aug 26 13:36:06 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91316 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91316

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C3 0.001 0.002 0.002

C4 4.275 5.515 6.671

C5 2.361 2.815 2.968

C6 6.582 7.454 6.928

C7 0.454 0.495 0.411

C8 0.122 0.129 0.097

C9 0.031 0.032 0.022

C10 0.043 0.044 0.028

C11 0.099 0.099 0.057

I-Paraffins C4 0.038 0.052 0.060

C5 12.244 14.758 15.393

C6 7.298 8.275 7.681

C7 2.133 2.341 1.930

C8 0.286 0.304 0.227

C9 0.048 0.051 0.034

C10 0.505 0.517 0.316

C11 1.033 1.037 0.599

C12 0.034 0.034 0.018

Mono-Aromatics C6 0.657 0.558 0.763

C7 17.964 15.471 17.684

C8 13.134 11.324 11.221

C9 3.617 3.097 2.730

C10 7.134 6.064 4.821

C11 1.427 1.212 0.873

C12 0.532 0.446 0.297

Naphthalenes C10 0.234 0.170 0.165

C11 0.019 0.014 0.012

Naphtheno/Olefino-Benzs C10 0.756 0.634 0.519

Indenes C9 0.138 0.107 0.106

C10 1.363 1.089 0.993

C11 0.068 0.053 0.042

C12 0.025 0.019 0.015

Mono-Naphthenes C5 0.242 0.242 0.313

C6 4.406 4.330 4.749

C7 1.073 1.052 0.991

C8 0.117 0.114 0.095

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C-177
Hydrocarbon Expert V4.7 Thu Aug 26 13:36:06 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91316 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91316

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Mono-Naphthenes C10 0.008 0.008 0.005

n-Olefins C4 0.247 0.303 0.400

C5 1.682 1.936 2.175

C6 1.161 1.268 1.251

C7 0.017 0.018 0.015

Iso-Olefins C5 1.689 1.920 2.184

C6 1.053 1.143 1.135

C7 0.535 0.570 0.494

Naphtheno-Olefins C5 0.190 0.184 0.253

C6 0.373 0.356 0.412

Di-Olefins C5 0.023 0.025 0.030

Oxygenates C3 0.188 0.175 0.283

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C-178
Hydrocarbon Expert V4.7 Thu Aug 26 13:36:06 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91316 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91316

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 21.67 21.39

5% 78.84 29.91

10% 80.16 79.64

15% 81.49 80.74

20% 96.52 81.84

25% 138.22 97.08

30% 145.29 138.23

35% 154.76 144.89

40% 157.30 154.52

45% 177.16 155.49

50% 229.03 175.61

55% 229.63 207.32

60% 230.23 229.48

65% 230.83 230.18

70% 277.09 230.88

75% 281.55 278.54

80% 291.76 281.93

85% 347.64 329.27

90% 363.20 362.78

95% 381.20 377.97

FBP 408.42 404.60

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C-179
Hydrocarbon Expert V4.7 Thu Aug 26 13:36:06 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91316 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91316

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 7.389 74-98-6 P3 Propane 0.001 0.002 0.002 0.273

2 8.609 75-28-5 I4 i-Butane 0.038 0.052 0.060 9.972

3 9.400 115-11-7 K4 Isobutene 0.022 0.027 0.035 5.822

4 9.439 106-98-9 K4 Butene-1 0.025 0.032 0.041 6.821

5 9.789 106-97-8 P4 n-Butane 4.275 5.515 6.671 1107.495

6 10.262 624-64-6 K4 t-Butene-2 0.094 0.116 0.152 25.244

7 10.385 463-82-1 I5 2,2-Dimethylpropane 0.044 0.055 0.055 11.450

8 10.983 590-18-1 K4 c-Butene-2 0.106 0.128 0.172 28.488

9 13.123 563-45-1 C5 3-Methylbutene-1 0.073 0.087 0.094 19.585

10 14.712 78-78-4 I5 i-Pentane 12.200 14.703 15.338 3182.770

11 16.328 109-67-1 K5 Pentene-1 0.336 0.392 0.435 90.275

12 17.164 563-46-2 C5 2-Methylbutene-1 0.527 0.605 0.681 141.339

13 17.687 109-66-0 P5 n-Pentane 2.361 2.815 2.968 615.837

14 18.201 78-79-5 E5 2-Methyl-1,3-Butadiene 0.009 0.010 0.012 2.543

15 18.790 646-04-8 K5 t-Pentene-2 0.870 1.002 1.125 233.318

16 19.431 ? Unidentified 0.006 0.007 0.008 2.094

17 19.814 627-20-3 K5 c-Pentene-2 0.476 0.542 0.616 127.733

18 20.484 513-35-9 C5 2-Methylbutene-2 1.089 1.228 1.409 292.249

19 20.815 2004-70-8 E5 1t,3-Pentadiene 0.014 0.015 0.018 3.762

20 22.607 75-83-2 I6 2,2-Dimethylbutane 0.153 0.175 0.161 39.957

21 25.241 142-29-0 B5 Cyclopentene 0.190 0.184 0.253 52.437

22 26.483 71-23-8 X3 n-Propanol 0.188 0.175 0.283 35.238

23 27.089 287-92-3 M5 Cyclopentane 0.242 0.242 0.313 64.950

24 27.820 79-29-8 I6 2,3-Dimethylbutane 0.607 0.686 0.639 159.095

25 28.223 ? Unidentified 0.054 0.054 0.055 17.624

26 28.680 691-38-3 C6 4-Methyl-c-pentene-2 0.046 0.051 0.049 12.318

27 28.904 107-83-5 I6 2-Methylpentane 3.380 3.864 3.558 885.263

28 29.330 674-76-0 C6 4-Methyl-t-pentene-2 0.138 0.153 0.149 36.992

29 31.550 96-14-0 I6 3-Methylpentane 3.158 3.550 3.324 827.082

30 32.709 763-29-1 C6 2-Methylpentene-1 0.236 0.257 0.254 63.324

31 32.933 592-41-6 K6 Hexene-1 0.161 0.177 0.174 43.204

32 35.316 110-54-3 P6 n-Hexane 6.582 7.454 6.928 1723.994

33 35.93013269-52-8 K6 t-Hexene-3 0.270 0.296 0.291 72.486

34 36.401 4050-45-7 K6 t-Hexene-2 0.512 0.560 0.552 137.416

35 36.894 625-27-4 C6 2-Methylpentene-2 0.359 0.388 0.387 96.358

36 37.305 922-62-3 C6 3-Methyl-c-pentene-2 0.275 0.294 0.296 73.686

37 38.232 7688-21-3 K6 c-Hexene-2 0.217 0.235 0.234 58.349

38 39.579 3404-73-7 C7 3,3-Dimethylpentene-1 0.326 0.347 0.302 87.579

39 40.158 96-37-7 M6 Methylcyclopentane 2.720 2.713 2.931 729.812

40 41.728 108-08-7 I7 2,4-Dimethylpentane 0.393 0.436 0.356 103.315

41 42.033 594-56-9 C7 2,3,3-Trimethylbutene-1 0.012 0.013 0.011 3.217

42 42.268 464-06-2 I7 2,2,3-Trimethylbutane 0.057 0.062 0.052 15.032

43 44.924 ? Unidentified 0.011 0.011 0.012 3.559

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C-180
Hydrocarbon Expert V4.7 Thu Aug 26 13:36:06 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91316 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91316

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 45.129 71-42-3 Q6 Benzene 0.657 0.558 0.763 189.866

45 45.332 693-89-0 B6 1-Methylcyclopentene 0.337 0.323 0.372 92.688

46 46.153 3404-61-3 C7 3-Methylhexene-1 0.013 0.014 0.012 3.391

47 46.738 3524-73-0 C7 5-Methylhexene-1 0.083 0.089 0.077 22.306

48 47.053 110-82-7 M6 Cyclohexane 1.686 1.617 1.817 452.441

49 47.587 ? Unidentified 0.029 0.031 0.027 9.598

50 48.79815840-60-5 C7 2-Methyl-c-hexene-3 0.032 0.034 0.029 8.532

51 49.792 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.037 0.040 0.035 10.022

52 50.186 591-76-4 I7 2-Methylhexane 1.062 1.168 0.961 279.191

53 50.663 110-83-8 B6 Cyclohexene 0.036 0.033 0.039 9.536

54 52.025 589-34-4 I7 3-Methylhexane 0.621 0.675 0.562 163.233

55 52.878 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.136 0.136 0.126 36.581

56 53.463 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.106 0.106 0.098 28.491

57 54.092 822-50-4 M7 1t,2-Dimethylcyclopentane 0.147 0.146 0.136 39.552

58 54.687 540-84-1 I8 2,2,4-Trimethylpentane 0.016 0.017 0.013 4.154

59 56.88014686-14-7 K7 t-Heptene-3 0.017 0.018 0.015 4.489

60 57.233 6094-02-6 C7 2-Methylhexene-1 0.026 0.028 0.024 6.915

61 57.612 142-82-5 P7 n-Heptane 0.454 0.495 0.411 119.286

62 58.111 2738-19-4 C7 2-Methyl-2-hexene 0.005 0.006 0.005 1.462

63 61.058 108-87-2 M7 Methylcyclohexane 0.660 0.641 0.610 177.137

64 62.011 4516-69-2 M8 1,1,3-Trimethylcyclopentane 0.013 0.013 0.011 3.587

65 63.855 1640-89-7 M7 Ethylcyclopentane 0.023 0.022 0.021 6.158

66 64.744 592-13-2 I8 2,5-Dimethylhexane 0.019 0.021 0.015 5.133

67 65.083 589-43-5 I8 2,4-Dimethylhexane 0.026 0.028 0.021 6.837

68 68.705 108-88-3 Q7 Toluene 17.964 15.471 17.684 5134.580

69 70.427 584-94-1 I8 2,3-Dimethylhexane 0.016 0.017 0.013 4.176

70 71.695 592-27-8 I8 2-Methylheptane 0.072 0.077 0.057 18.891

71 71.947 589-53-7 I8 4-Methylheptane 0.031 0.033 0.025 8.180

72 72.859 M8 1,3-dimethyl-t-cyclohexane 0.056 0.054 0.045 14.932

73 73.019 589-81-1 I8 3-Methylheptane 0.068 0.072 0.054 17.960

74 73.201 619-99-8 I8 3-Ethylhexane 0.038 0.040 0.030 9.984

75 74.100 ? Unidentified 0.008 0.008 0.007 2.767

76 76.187 2207-03-6 M8 1t,3-Dimethylcyclohexane 0.022 0.022 0.018 6.012

77 77.561 111-65-9 P8 n-Octane 0.122 0.129 0.097 32.043

78 81.867 1678-91-7 M8 Ethylcyclohexane 0.026 0.025 0.021 6.986

79 82.193 1072-05-5 I9 2,6-Dimethylheptane 0.007 0.007 0.005 1.855

80 83.130 I9 2,5-Dimethylheptane 0.007 0.008 0.005 1.931

81 84.452 100-41-4 Q8 Ethylbenzene 2.515 2.166 2.148 713.310

82 85.699 108-38-3 Q8 m-Xylene 6.074 5.248 5.189 1722.882

83 85.842 106-42-3 Q8 p-Xylene 2.846 2.468 2.432 807.379

84 87.016 2216-34-4 I9 4-Methyloctane 0.009 0.010 0.007 2.434

85 87.148 3221-61-2 I9 2-Methyloctane 0.012 0.013 0.009 3.191

86 88.012 2216-33-3 I9 3-Methyloctane 0.013 0.013 0.009 3.389

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C-181
Hydrocarbon Expert V4.7 Thu Aug 26 13:36:06 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91316 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91316

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 88.660 95-47-6 Q8 o-Xylene 1.700 1.442 1.452 482.170

88 91.506 111-84-2 P9 n-Nonane 0.031 0.032 0.022 8.054

89 92.837 98-82-8 Q9 i-Propylbenzene 0.035 0.031 0.027 9.922

90 95.264 2051-30-1 I10 2,4-Dimethyloctane 0.010 0.010 0.006 2.570

91 96.303 103-65-1 Q9 n-Propylbenzene 0.188 0.163 0.142 52.919

92 97.149 620-14-4 Q9 1-Methyl-3-ethylbenzene 0.686 0.592 0.518 193.320

93 97.384 622-96-8 Q9 1-Methyl-4-ethylbenzene 0.325 0.282 0.246 91.710

94 98.011 108-67-8 Q9 1,3,5-Trimethylbenzene 0.420 0.362 0.317 118.327

95 98.68017301-94-8 I10 4-Methylnonane 0.006 0.006 0.004 1.635

96 98.881 I10 2,2,6-Trimethyloctane 0.378 0.388 0.241 99.894

97 99.096 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.272 0.230 0.205 76.615

98 99.659 5911-04-6 I10 3-Methylnonane 0.009 0.009 0.006 2.374

99 100.126 ? Unidentified 0.028 0.021 0.016 9.328

100 100.251 ? Unidentified 0.085 0.086 0.050 28.048

101 100.476 I11 C11-Isoparaffin-2 0.046 0.046 0.026 12.073

102 100.730 95-63-6 Q9 1,2,4-Trimethylbenzene 1.375 1.172 1.038 387.549

103 100.940 ? Unidentified 0.065 0.069 0.042 21.235

104 101.061 ? Unidentified 0.037 0.037 0.023 12.035

105 101.319 1678-98-4 M10 i-Butylcyclohexane 0.008 0.008 0.005 2.164

106 102.10617302-01-1 I10 3-Ethyl-3-methylheptane 0.103 0.103 0.060 27.186

107 102.464 538-93-2 Q10 i-Butylbenzene 0.127 0.111 0.086 35.470

108 102.658 124-18-5 P10 n-Decane 0.043 0.044 0.028 11.467

109 102.974 ? Unidentified 0.028 0.028 0.016 9.148

110 103.609 526-73-8 Q9 1,2,3-Trimethylbenzene 0.316 0.264 0.239 89.141

111 103.996 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.018 0.015 0.012 4.966

112 104.191 I11 C11 Isoparaffin-4 0.016 0.016 0.009 4.231

113 104.393 ? Unidentified 0.101 0.088 0.068 33.104

114 104.800 J9 Indan 0.138 0.107 0.106 39.478

115 105.432 J10 Indene 0.703 0.545 0.540 201.463

116 106.150 I11 C11-Isoparaffin-7 0.311 0.312 0.181 82.415

117 106.333 141-93-5 Q10 1,3-Diethylbenzene 0.080 0.069 0.054 22.408

118 106.623 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 1.065 0.924 0.720 298.653

119 106.949 105-05-5 Q10 1,4-Diethylbenzene 0.490 0.425 0.331 137.395

120 107.177 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.384 0.326 0.259 107.630

121 107.437 135-01-3 Q10 1,2-Diethylbenzene 0.085 0.072 0.057 23.801

122 107.889 ? Unidentified 0.081 0.081 0.047 26.540

123 108.027 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.158 0.135 0.107 44.207

124 108.164 ? Unidentified 0.091 0.092 0.054 29.965

125 108.246 ? Unidentified 0.086 0.086 0.050 28.119

126 108.368 I11 C11- Isoparaffin-11 0.660 0.662 0.383 174.791

127 108.551 ? Unidentified 0.225 0.226 0.131 74.011

128 108.881 1758-88-9 Q10 1,4,Dimethyl-2-ethylbenzene 0.384 0.327 0.260 107.763

129 108.988 ? Unidentified 0.967 0.823 0.654 317.913

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C-182
Hydrocarbon Expert V4.7 Thu Aug 26 13:36:06 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91316 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91316

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 109.204 J10 2-Methylindan 0.144 0.111 0.099 41.208

131 109.550 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 1.078 0.921 0.729 302.324

132 110.102 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.681 0.571 0.460 190.938

133 110.529 ? Unidentified 0.019 0.018 0.011 6.391

134 110.731 ? Unidentified 0.045 0.045 0.029 14.765

135 110.860 ? Unidentified 0.068 0.069 0.044 22.412

136 111.008 Q11 1-Methyl-4-t-butylbenzene 0.122 0.107 0.074 33.957

137 111.223 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.435 0.364 0.294 122.052

138 111.533 1120-21-4 P11 n-Undecane 0.099 0.099 0.057 26.223

139 111.690 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.109 0.091 0.066 30.315

140 111.800 ? Unidentified 0.053 0.045 0.033 17.543

141 111.905 Q11 C11 - Aromatic - 1 0.027 0.023 0.017 7.629

142 112.170 Q10 1,2,4,5-Tetramethylbenzene 0.902 0.759 0.610 252.910

143 112.439 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 1.247 1.046 0.842 349.483

144 112.636 ? Unidentified 0.016 0.013 0.010 5.132

145 112.791 ? Unidentified 0.020 0.015 0.012 6.457

146 112.968 I12 C12 - IsoParaffin - 1 0.025 0.026 0.014 6.743

147 113.292 ? Unidentified 0.046 0.047 0.026 15.206

148 113.450 ? Unidentified 0.009 0.009 0.005 2.913

149 113.583 Q11 C11 - Aromatic - 3 0.169 0.142 0.104 47.309

150 113.765 874-35-1 H10 5-Methylindan 0.372 0.312 0.255 104.301

151 113.905 Q12 1,2-Di-i-propylbenzene 0.162 0.136 0.091 45.078

152 114.119 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.230 0.193 0.141 64.194

153 114.278 Q11 C11 - Aromatic - 4 0.114 0.096 0.070 31.873

154 114.518 824-22-6 J10 4-Methylindan 0.516 0.433 0.354 144.733

155 114.680 ? Unidentified 0.121 0.101 0.074 39.611

156 114.768 824-63-5 H10 2-Methylindan 0.384 0.322 0.263 107.582

157 114.979 ? Unidentified 0.041 0.034 0.025 13.462

158 115.091 538-68-1 Q11 n-Pentylbenzene 0.057 0.048 0.035 15.895

159 115.322 Q11 tert-Pentylbenzene 0.235 0.197 0.144 65.468

160 115.633 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.104 0.088 0.064 29.161

161 115.743 Q11 C11 - Aromatic - 7 0.133 0.117 0.081 37.116

162 116.074 I12 C12 - IsoParaffin - 4 0.008 0.008 0.004 2.262

163 116.206 100-18-5 Q12 1,4-Di-i-propylbenzene 0.196 0.164 0.109 54.436

164 116.633 91-20-3 G10 Naphthalene 0.234 0.170 0.165 68.549

165 116.842 J11 4,7-Dimethyl Indane 0.014 0.011 0.008 3.888

166 117.081 J11 1,1-Dimethyl Indane 0.055 0.042 0.034 15.707

167 117.250 J12 Dimethyl Indane - 1 0.019 0.015 0.012 5.461

168 117.431 7364-19-4 Q12 1t-Butyl-4-ethylbenzene 0.027 0.023 0.015 7.636

169 117.565 J12 Dimethyl Indane - 2 0.006 0.004 0.004 1.643

170 117.736 Q12 1,3-Di-n-propylbenzene 0.141 0.118 0.079 39.207

171 117.847 Q11 C11 - Aromatic - 11 0.078 0.068 0.047 21.663

172 118.401 Q11 C11 - Aromatic - 12 0.043 0.038 0.026 12.064

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C-183
Hydrocarbon Expert V4.7 Thu Aug 26 13:36:06 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91316 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91316

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 119.031 Q11 C11 - Aromatic - 13 0.006 0.005 0.004 1.658

174 119.341 102-25-0 Q12 1,3,5-Triethylbenzene 0.006 0.005 0.003 1.628

175 123.282 91-57-6 G11 2-Methylnaphthalene 0.012 0.009 0.008 3.511

176 124.148 90-12-0 G11 1-Methylnaphthalene 0.007 0.005 0.004 1.909

177 129.863 ? Unidentified 0.004 0.003 0.002 1.349

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C-184
Hydrocarbon Expert V4.7 Thu Aug 26 13:36:06 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91316 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91316

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 7.389 74-98-6 Propane 0.001 0.002 0.002 0.273

9.789 106-97-8 n-Butane 4.275 5.515 6.671 1107.495

17.687 109-66-0 n-Pentane 2.361 2.815 2.968 615.837

35.316 110-54-3 n-Hexane 6.582 7.454 6.928 1723.994

57.612 142-82-5 n-Heptane 0.454 0.495 0.411 119.286

77.561 111-65-9 n-Octane 0.122 0.129 0.097 32.043

91.506 111-84-2 n-Nonane 0.031 0.032 0.022 8.054

102.658 124-18-5 n-Decane 0.043 0.044 0.028 11.467

111.533 1120-21-4 n-Undecane 0.099 0.099 0.057 26.223

I-Paraffins 8.609 75-28-5 i-Butane 0.038 0.052 0.060 9.972

10.385 463-82-1 2,2-Dimethylpropane 0.044 0.055 0.055 11.450

14.712 78-78-4 i-Pentane 12.200 14.703 15.338 3182.770

22.607 75-83-2 2,2-Dimethylbutane 0.153 0.175 0.161 39.957

27.820 79-29-8 2,3-Dimethylbutane 0.607 0.686 0.639 159.095

28.904 107-83-5 2-Methylpentane 3.380 3.864 3.558 885.263

31.550 96-14-0 3-Methylpentane 3.158 3.550 3.324 827.082

41.728 108-08-7 2,4-Dimethylpentane 0.393 0.436 0.356 103.315

42.268 464-06-2 2,2,3-Trimethylbutane 0.057 0.062 0.052 15.032

50.186 591-76-4 2-Methylhexane 1.062 1.168 0.961 279.191

52.025 589-34-4 3-Methylhexane 0.621 0.675 0.562 163.233

54.687 540-84-1 2,2,4-Trimethylpentane 0.016 0.017 0.013 4.154

64.744 592-13-2 2,5-Dimethylhexane 0.019 0.021 0.015 5.133

65.083 589-43-5 2,4-Dimethylhexane 0.026 0.028 0.021 6.837

70.427 584-94-1 2,3-Dimethylhexane 0.016 0.017 0.013 4.176

71.695 592-27-8 2-Methylheptane 0.072 0.077 0.057 18.891

71.947 589-53-7 4-Methylheptane 0.031 0.033 0.025 8.180

73.019 589-81-1 3-Methylheptane 0.068 0.072 0.054 17.960

73.201 619-99-8 3-Ethylhexane 0.038 0.040 0.030 9.984

82.193 1072-05-5 2,6-Dimethylheptane 0.007 0.007 0.005 1.855

83.130 2,5-Dimethylheptane 0.007 0.008 0.005 1.931

87.016 2216-34-4 4-Methyloctane 0.009 0.010 0.007 2.434

87.148 3221-61-2 2-Methyloctane 0.012 0.013 0.009 3.191

88.012 2216-33-3 3-Methyloctane 0.013 0.013 0.009 3.389

95.264 2051-30-1 2,4-Dimethyloctane 0.010 0.010 0.006 2.570

98.68017301-94-8 4-Methylnonane 0.006 0.006 0.004 1.635

98.881 2,2,6-Trimethyloctane 0.378 0.388 0.241 99.894

99.659 5911-04-6 3-Methylnonane 0.009 0.009 0.006 2.374

100.476 C11-Isoparaffin-2 0.046 0.046 0.026 12.073

102.10617302-01-1 3-Ethyl-3-methylheptane 0.103 0.103 0.060 27.186

104.191 C11 Isoparaffin-4 0.016 0.016 0.009 4.231

106.150 C11-Isoparaffin-7 0.311 0.312 0.181 82.415

108.368 C11- Isoparaffin-11 0.660 0.662 0.383 174.791

112.968 C12 - IsoParaffin - 1 0.025 0.026 0.014 6.743

116.074 C12 - IsoParaffin - 4 0.008 0.008 0.004 2.262

Aromatics

Mono-Aromatics 45.129 71-42-3 Benzene 0.657 0.558 0.763 189.866

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C-185
Hydrocarbon Expert V4.7 Thu Aug 26 13:36:06 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91316 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91316

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 68.705 108-88-3 Toluene 17.964 15.471 17.684 5134.580

84.452 100-41-4 Ethylbenzene 2.515 2.166 2.148 713.310

85.699 108-38-3 m-Xylene 6.074 5.248 5.189 1722.882

85.842 106-42-3 p-Xylene 2.846 2.468 2.432 807.379

88.660 95-47-6 o-Xylene 1.700 1.442 1.452 482.170

92.837 98-82-8 i-Propylbenzene 0.035 0.031 0.027 9.922

96.303 103-65-1 n-Propylbenzene 0.188 0.163 0.142 52.919

97.149 620-14-4 1-Methyl-3-ethylbenzene 0.686 0.592 0.518 193.320

97.384 622-96-8 1-Methyl-4-ethylbenzene 0.325 0.282 0.246 91.710

98.011 108-67-8 1,3,5-Trimethylbenzene 0.420 0.362 0.317 118.327

99.096 611-14-3 1-Methyl-2-ethylbenzene 0.272 0.230 0.205 76.615

100.730 95-63-6 1,2,4-Trimethylbenzene 1.375 1.172 1.038 387.549

102.464 538-93-2 i-Butylbenzene 0.127 0.111 0.086 35.470

103.609 526-73-8 1,2,3-Trimethylbenzene 0.316 0.264 0.239 89.141

103.996 535-77-3 1-Methyl-3-i-propylbenzene 0.018 0.015 0.012 4.966

106.333 141-93-5 1,3-Diethylbenzene 0.080 0.069 0.054 22.408

106.623 1074-43-7 1-Methyl-3-n-propylbenzene 1.065 0.924 0.720 298.653

106.949 105-05-5 1,4-Diethylbenzene 0.490 0.425 0.331 137.395

107.177 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.384 0.326 0.259 107.630

107.437 135-01-3 1,2-Diethylbenzene 0.085 0.072 0.057 23.801

108.027 1074-17-5 1-Methyl-2-n-propylbenzene 0.158 0.135 0.107 44.207

108.881 1758-88-9 1,4,Dimethyl-2-ethylbenzene 0.384 0.327 0.260 107.763

109.550 934-80-5 1,2-Dimethyl-4-ethylbenzene 1.078 0.921 0.729 302.324

110.102 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.681 0.571 0.460 190.938

111.008 1-Methyl-4-t-butylbenzene 0.122 0.107 0.074 33.957

111.223 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.435 0.364 0.294 122.052

111.690 4218-48-8 1-Ethyl-4-i-propylbenzene 0.109 0.091 0.066 30.315

111.905 C11 - Aromatic - 1 0.027 0.023 0.017 7.629

112.170 1,2,4,5-Tetramethylbenzene 0.902 0.759 0.610 252.910

112.439 527-53-7 1,2,3,5-Tetramethylbenzene 1.247 1.046 0.842 349.483

113.583 C11 - Aromatic - 3 0.169 0.142 0.104 47.309

113.905 1,2-Di-i-propylbenzene 0.162 0.136 0.091 45.078

114.119 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.230 0.193 0.141 64.194

114.278 C11 - Aromatic - 4 0.114 0.096 0.070 31.873

115.091 538-68-1 n-Pentylbenzene 0.057 0.048 0.035 15.895

115.322 tert-Pentylbenzene 0.235 0.197 0.144 65.468

115.633 577-55-9 1-Methyl-2-n-butylbenzene 0.104 0.088 0.064 29.161

115.743 C11 - Aromatic - 7 0.133 0.117 0.081 37.116

116.206 100-18-5 1,4-Di-i-propylbenzene 0.196 0.164 0.109 54.436

117.431 7364-19-4 1t-Butyl-4-ethylbenzene 0.027 0.023 0.015 7.636

117.736 1,3-Di-n-propylbenzene 0.141 0.118 0.079 39.207

117.847 C11 - Aromatic - 11 0.078 0.068 0.047 21.663

118.401 C11 - Aromatic - 12 0.043 0.038 0.026 12.064

119.031 C11 - Aromatic - 13 0.006 0.005 0.004 1.658

119.341 102-25-0 1,3,5-Triethylbenzene 0.006 0.005 0.003 1.628

Naphthalenes 116.633 91-20-3 Naphthalene 0.234 0.170 0.165 68.549

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C-186
Hydrocarbon Expert V4.7 Thu Aug 26 13:36:06 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91316 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91316

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Naphthalenes 123.282 91-57-6 2-Methylnaphthalene 0.012 0.009 0.008 3.511

124.148 90-12-0 1-Methylnaphthalene 0.007 0.005 0.004 1.909

Naphtheno/Olefino-Benzs 113.765 874-35-1 5-Methylindan 0.372 0.312 0.255 104.301

114.768 824-63-5 2-Methylindan 0.384 0.322 0.263 107.582

Indenes 104.800 Indan 0.138 0.107 0.106 39.478

105.432 Indene 0.703 0.545 0.540 201.463

109.204 2-Methylindan 0.144 0.111 0.099 41.208

114.518 824-22-6 4-Methylindan 0.516 0.433 0.354 144.733

116.842 4,7-Dimethyl Indane 0.014 0.011 0.008 3.888

117.081 1,1-Dimethyl Indane 0.055 0.042 0.034 15.707

117.250 Dimethyl Indane - 1 0.019 0.015 0.012 5.461

117.565 Dimethyl Indane - 2 0.006 0.004 0.004 1.643

Naphthenes

Mono-Naphthenes 27.089 287-92-3 Cyclopentane 0.242 0.242 0.313 64.950

40.158 96-37-7 Methylcyclopentane 2.720 2.713 2.931 729.812

47.053 110-82-7 Cyclohexane 1.686 1.617 1.817 452.441

52.878 1759-58-6 1t,3-Dimethylcyclopentane 0.136 0.136 0.126 36.581

53.463 2532-58-3 1c,3-Dimethylcyclopentane 0.106 0.106 0.098 28.491

54.092 822-50-4 1t,2-Dimethylcyclopentane 0.147 0.146 0.136 39.552

61.058 108-87-2 Methylcyclohexane 0.660 0.641 0.610 177.137

62.011 4516-69-2 1,1,3-Trimethylcyclopentane 0.013 0.013 0.011 3.587

63.855 1640-89-7 Ethylcyclopentane 0.023 0.022 0.021 6.158

72.859 1,3-dimethyl-t-cyclohexane 0.056 0.054 0.045 14.932

76.187 2207-03-6 1t,3-Dimethylcyclohexane 0.022 0.022 0.018 6.012

81.867 1678-91-7 Ethylcyclohexane 0.026 0.025 0.021 6.986

101.319 1678-98-4 i-Butylcyclohexane 0.008 0.008 0.005 2.164

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.400 115-11-7 Isobutene 0.022 0.027 0.035 5.822

9.439 106-98-9 Butene-1 0.025 0.032 0.041 6.821

10.262 624-64-6 t-Butene-2 0.094 0.116 0.152 25.244

10.983 590-18-1 c-Butene-2 0.106 0.128 0.172 28.488

16.328 109-67-1 Pentene-1 0.336 0.392 0.435 90.275

18.790 646-04-8 t-Pentene-2 0.870 1.002 1.125 233.318

19.814 627-20-3 c-Pentene-2 0.476 0.542 0.616 127.733

32.933 592-41-6 Hexene-1 0.161 0.177 0.174 43.204

35.93013269-52-8 t-Hexene-3 0.270 0.296 0.291 72.486

36.401 4050-45-7 t-Hexene-2 0.512 0.560 0.552 137.416

38.232 7688-21-3 c-Hexene-2 0.217 0.235 0.234 58.349

56.88014686-14-7 t-Heptene-3 0.017 0.018 0.015 4.489

Iso-Olefins 13.123 563-45-1 3-Methylbutene-1 0.073 0.087 0.094 19.585

17.164 563-46-2 2-Methylbutene-1 0.527 0.605 0.681 141.339

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C-187
Hydrocarbon Expert V4.7 Thu Aug 26 13:36:06 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91316 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91316

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Iso-Olefins 20.484 513-35-9 2-Methylbutene-2 1.089 1.228 1.409 292.249

28.680 691-38-3 4-Methyl-c-pentene-2 0.046 0.051 0.049 12.318

29.330 674-76-0 4-Methyl-t-pentene-2 0.138 0.153 0.149 36.992

32.709 763-29-1 2-Methylpentene-1 0.236 0.257 0.254 63.324

36.894 625-27-4 2-Methylpentene-2 0.359 0.388 0.387 96.358

37.305 922-62-3 3-Methyl-c-pentene-2 0.275 0.294 0.296 73.686

39.579 3404-73-7 3,3-Dimethylpentene-1 0.326 0.347 0.302 87.579

42.033 594-56-9 2,3,3-Trimethylbutene-1 0.012 0.013 0.011 3.217

46.153 3404-61-3 3-Methylhexene-1 0.013 0.014 0.012 3.391

46.738 3524-73-0 5-Methylhexene-1 0.083 0.089 0.077 22.306

48.79815840-60-5 2-Methyl-c-hexene-3 0.032 0.034 0.029 8.532

49.792 3404-55-5 4-Methyl-t/c-hexene-2 0.037 0.040 0.035 10.022

57.233 6094-02-6 2-Methylhexene-1 0.026 0.028 0.024 6.915

58.111 2738-19-4 2-Methyl-2-hexene 0.005 0.006 0.005 1.462

Naphtheno-Olefins 25.241 142-29-0 Cyclopentene 0.190 0.184 0.253 52.437

45.332 693-89-0 1-Methylcyclopentene 0.337 0.323 0.372 92.688

50.663 110-83-8 Cyclohexene 0.036 0.033 0.039 9.536

Di-Olefins 18.201 78-79-5 2-Methyl-1,3-Butadiene 0.009 0.010 0.012 2.543

20.815 2004-70-8 1t,3-Pentadiene 0.014 0.015 0.018 3.762

Oxygenates 26.483 71-23-8 n-Propanol 0.188 0.175 0.283 35.238

Unidentified 19.431 Unidentified 0.006 0.007 0.008 2.094

28.223 Unidentified 0.054 0.054 0.055 17.624

44.924 Unidentified 0.011 0.011 0.012 3.559

47.587 Unidentified 0.029 0.031 0.027 9.598

74.100 Unidentified 0.008 0.008 0.007 2.767

100.126 Unidentified 0.028 0.021 0.016 9.328

100.251 Unidentified 0.085 0.086 0.050 28.048

100.940 Unidentified 0.065 0.069 0.042 21.235

101.061 Unidentified 0.037 0.037 0.023 12.035

102.974 Unidentified 0.028 0.028 0.016 9.148

104.393 Unidentified 0.101 0.088 0.068 33.104

107.889 Unidentified 0.081 0.081 0.047 26.540

108.164 Unidentified 0.091 0.092 0.054 29.965

108.246 Unidentified 0.086 0.086 0.050 28.119

108.551 Unidentified 0.225 0.226 0.131 74.011

108.988 Unidentified 0.967 0.823 0.654 317.913

110.529 Unidentified 0.019 0.018 0.011 6.391

110.731 Unidentified 0.045 0.045 0.029 14.765

110.860 Unidentified 0.068 0.069 0.044 22.412

111.800 Unidentified 0.053 0.045 0.033 17.543

112.636 Unidentified 0.016 0.013 0.010 5.132

112.791 Unidentified 0.020 0.015 0.012 6.457

113.292 Unidentified 0.046 0.047 0.026 15.206

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C-188
Hydrocarbon Expert V4.7 Thu Aug 26 13:36:06 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91316 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91316

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Unidentified 113.450 Unidentified 0.009 0.009 0.005 2.913

114.680 Unidentified 0.121 0.101 0.074 39.611

114.979 Unidentified 0.041 0.034 0.025 13.462

129.863 Unidentified 0.004 0.003 0.002 1.349

Plus

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C-189
Hydrocarbon Expert V4.7 Thu Aug 26 13:36:06 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91316 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91316

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF

20.0 15.0 10.0 5.0 0.0

Propane

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

Unidentified

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

2,2-Dimethylbutane

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C-190
Hydrocarbon Expert V4.7 Thu Aug 26 13:36:06 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91316 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91316

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

n-Propanol

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

n-Hexane

t-Hexene-3

t-Hexene-2

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane 2,3,3-Trimethylbutene-1 2,2,3-Trimethylbutane

Unidentified Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1 Cyclohexane

Unidentified

2-Methyl-c-hexene-3

4-Methyl-t/c-hexene-2

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C-191
Hydrocarbon Expert V4.7 Thu Aug 26 13:36:06 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91316 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91316

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF

70.0 65.0 60.0 55.0 50.0

2-Methylhexane

Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane

2,2,4-Trimethylpentane

t-Heptene-3

2-Methylhexene-1

n-Heptane

2-Methyl-2-hexene

Methylcyclohexane

1,1,3-Trimethylcyclopentane

Ethylcyclopentane

2,5-Dimethylhexane

2,4-Dimethylhexane

Toluene

2,3-Dimethylhexane

2-Methylheptane 4-Methylheptane

1,3-dimethyl-t-cyclohexane 3-Methylheptane 3-Ethylhexane

Unidentified

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C-192
Hydrocarbon Expert V4.7 Thu Aug 26 13:36:06 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91316 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91316

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF

95.0 90.0 85.0 80.0 75.0

1t,3-Dimethylcyclohexane

n-Octane

Ethylcyclohexane

2,6-Dimethylheptane

2,5-Dimethylheptane

Ethylbenzene

m-Xylene p-Xylene

4-Methyloctane 2-Methyloctane

3-Methyloctane

o-Xylene

n-Nonane

i-Propylbenzene

2,4-Dimethyloctane

n-Propylbenzene

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

4-Methylnonane 2,2,6-Trimethyloctane 1-Methyl-2-ethylbenzene

3-Methylnonane

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C-193
Hydrocarbon Expert V4.7 Thu Aug 26 13:36:06 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91316 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91316

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified

C11-Isoparaffin-2 1,2,4-Trimethylbenzene Unidentified

i-Butylcyclohexane

3-Ethyl-3-methylheptane

i-Butylbenzene n-Decane

Unidentified

1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene C11 Isoparaffin-4 Unidentified

Indan

Indene

C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene

1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

Unidentified Unidentified 1-Methyl-2-n-propylbenzene

C11- Isoparaffin-11 Unidentified

1,4,Dimethyl-2-ethylbenzene Unidentified 2-Methylindan

1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

Unidentified

1-Methyl-4-t-butylbenzene 1,2-Dimethyl-3-ethylbenzene n-Undecane Unidentified 1-Ethyl-4-i-propylbenzene C11 - Aromatic - 1 1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene Unidentified

C12 - IsoParaffin - 1

Unidentified C11 - Aromatic - 3 5-Methylindan 1,2-Di-i-propylbenzene 1-methyl-4-(1-methylpropyl)be C11 - Aromatic - 4 4-Methylindan Unidentified 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene 1-Methyl-2-n-butylbenzene C11 - Aromatic - 7

C12 - IsoParaffin - 4 1,4-Di-i-propylbenzene

Naphthalene 4,7-Dimethyl Indane 1,1-Dimethyl Indane Dimethyl Indane - 1

Dimethyl Indane - 2 1t-Butyl-4-ethylbenzene

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

C11 - Aromatic - 12

C11 - Aromatic - 13

1,3,5-Triethylbenzene

2-Methylnaphthalene

1-Methylnaphthalene

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C-194
Hydrocarbon Expert V4.7 Thu Aug 26 13:36:06 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91316 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91316

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000012.D\SIG1000012_FID1_A.CDF

145.0 140.0 135.0 130.0 125.0

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C-195
Hydrocarbon Expert V4.7 Thu Aug 26 13:41:34 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91317 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91317

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 7.718 9.218 8.649

I-Paraffins 23.428 26.796 21.984

Aromatics 45.586 40.064 37.081

Mono-Aromatics 42.844 37.837 35.128

Naphthalenes 0.254 0.191 0.175

Naphtheno/Olefino-Benzs 0.547 0.472 0.367

Indenes 1.940 1.565 1.411

Naphthenes 4.162 4.207 4.320

Mono-Naphthenes 4.162 4.207 4.320

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 6.986 7.948 8.103

n-Olefins 2.929 3.406 3.495

Iso-Olefins 3.450 3.941 3.905

Naphtheno-Olefins 0.582 0.573 0.670

Di-Olefins 0.025 0.028 0.032

Oxygenates 8.722 8.486 16.720

Unidentified 3.398 3.280 3.143

Plus 0.000 0.000 0.000

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C-196
Hydrocarbon Expert V4.7 Thu Aug 26 13:41:34 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91317 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91317

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C2 8.550 8.321 16.466

C3 0.173 0.166 0.255

C4 1.272 1.676 1.951

C5 8.985 10.805 11.192

C6 21.874 24.679 22.737

C7 15.823 14.791 14.981

C8 13.542 12.311 11.224

C9 11.871 10.586 8.731

C10 11.539 10.538 7.609

C11 2.566 2.492 1.487

C12 0.408 0.355 0.224

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C-197
Hydrocarbon Expert V4.7 Thu Aug 26 13:41:34 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91317 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91317

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C3 0.001 0.001 0.001

C4 1.079 1.431 1.646

C5 1.652 2.025 2.031

C6 4.380 5.100 4.509

C7 0.285 0.320 0.252

C8 0.053 0.058 0.041

C9 0.069 0.074 0.048

C10 0.102 0.108 0.064

C11 0.097 0.101 0.055

I-Paraffins C4 0.015 0.021 0.023

C5 3.492 4.329 4.295

C6 11.292 13.190 11.626

C7 1.869 2.110 1.655

C8 1.493 1.612 1.160

C9 0.695 0.752 0.481

C10 3.040 3.204 1.877

C11 1.505 1.554 0.854

C12 0.026 0.027 0.013

Mono-Aromatics C6 0.645 0.564 0.733

C7 12.177 10.785 11.726

C8 11.951 10.597 9.987

C9 10.810 9.524 7.980

C10 6.002 5.270 3.968

C11 0.897 0.785 0.537

C12 0.361 0.312 0.198

Naphthalenes C10 0.246 0.184 0.170

C11 0.009 0.007 0.005

Naphtheno/Olefino-Benzs C10 0.547 0.472 0.367

Indenes C9 0.296 0.236 0.222

C10 1.566 1.267 1.141

C11 0.057 0.046 0.035

C12 0.021 0.017 0.013

Mono-Naphthenes C5 0.296 0.305 0.375

C6 3.100 3.128 3.268

C7 0.687 0.695 0.620

C8 0.045 0.044 0.035

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C-198
Hydrocarbon Expert V4.7 Thu Aug 26 13:41:34 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91317 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91317

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Mono-Naphthenes C10 0.035 0.034 0.022

n-Olefins C4 0.178 0.224 0.282

C5 1.554 1.840 1.966

C6 1.099 1.234 1.159

C7 0.098 0.107 0.088

Iso-Olefins C5 1.778 2.092 2.249

C6 0.964 1.076 1.017

C7 0.708 0.774 0.640

Naphtheno-Olefins C5 0.188 0.187 0.244

C6 0.394 0.387 0.426

Di-Olefins C5 0.025 0.028 0.032

Oxygenates C2 8.550 8.321 16.466

C3 0.172 0.165 0.254

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C-199
Hydrocarbon Expert V4.7 Thu Aug 26 13:41:34 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91317 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91317

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 25.05 23.86

5% 81.79 80.86

10% 111.42 97.15

15% 138.92 137.68

20% 144.65 139.76

25% 154.67 145.26

30% 161.16 154.79

35% 172.76 160.79

40% 176.42 172.76

45% 229.82 176.69

50% 230.34 228.56

55% 230.86 230.39

60% 276.01 230.97

65% 281.34 277.06

70% 291.64 281.77

75% 322.60 320.72

80% 332.52 329.36

85% 341.97 335.97

90% 362.56 359.10

95% 372.56 368.14

FBP 404.60 404.60

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C-200
Hydrocarbon Expert V4.7 Thu Aug 26 13:41:34 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91317 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91317

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 7.386 74-98-6 P3 Propane 0.001 0.001 0.001 0.159

2 8.607 75-28-5 I4 i-Butane 0.015 0.021 0.023 4.223

3 9.399 115-11-7 K4 Isobutene 0.014 0.018 0.022 4.074

4 9.438 106-98-9 K4 Butene-1 0.017 0.022 0.027 4.884

5 9.787 106-97-8 P4 n-Butane 1.079 1.431 1.646 300.047

6 10.261 624-64-6 K4 t-Butene-2 0.067 0.086 0.107 19.405

7 10.383 463-82-1 I5 2,2-Dimethylpropane 0.009 0.012 0.011 2.575

8 10.981 590-18-1 K4 c-Butene-2 0.080 0.099 0.126 22.975

9 12.739 64-17-5 X2 Ethanol 8.550 8.321 16.466 1058.804

10 13.119 563-45-1 C5 3-Methylbutene-1 0.315 0.386 0.399 90.871

11 14.701 78-78-4 I5 i-Pentane 3.483 4.317 4.283 975.682

12 16.325 109-67-1 K5 Pentene-1 0.315 0.377 0.398 90.649

13 17.162 563-46-2 C5 2-Methylbutene-1 0.478 0.564 0.604 137.656

14 17.687 109-66-0 P5 n-Pentane 1.652 2.025 2.031 462.691

15 18.199 78-79-5 E5 2-Methyl-1,3-Butadiene 0.010 0.011 0.013 2.927

16 18.792 646-04-8 K5 t-Pentene-2 0.801 0.949 1.013 230.692

17 19.812 627-20-3 K5 c-Pentene-2 0.439 0.514 0.556 126.522

18 20.482 513-35-9 C5 2-Methylbutene-2 0.985 1.141 1.245 283.664

19 20.812 2004-70-8 E5 1t,3-Pentadiene 0.015 0.017 0.019 4.358

20 22.061 ? Unidentified 0.006 0.006 0.007 1.971

21 22.606 75-83-2 I6 2,2-Dimethylbutane 0.294 0.348 0.303 82.714

22 25.241 142-29-0 B5 Cyclopentene 0.188 0.187 0.244 55.667

23 26.486 71-23-8 X3 n-Propanol 0.172 0.165 0.254 34.733

24 27.094 287-92-3 M5 Cyclopentane 0.296 0.305 0.375 85.306

25 27.826 79-29-8 I6 2,3-Dimethylbutane 1.092 1.268 1.124 307.138

26 28.226 ? Unidentified 0.048 0.050 0.049 17.082

27 28.687 691-38-3 C6 4-Methyl-c-pentene-2 0.041 0.046 0.043 11.671

28 28.926 107-83-5 I6 2-Methylpentane 6.264 7.365 6.449 1761.717

29 29.334 674-76-0 C6 4-Methyl-t-pentene-2 0.126 0.143 0.133 36.232

30 31.558 96-14-0 I6 3-Methylpentane 3.641 4.209 3.749 1024.040

31 32.713 763-29-1 C6 2-Methylpentene-1 0.215 0.241 0.226 61.837

32 32.937 592-41-6 K6 Hexene-1 0.154 0.175 0.163 44.483

33 35.310 110-54-3 P6 n-Hexane 4.380 5.100 4.509 1231.787

34 35.93213269-52-8 K6 t-Hexene-3 0.253 0.285 0.267 72.835

35 36.406 4050-45-7 K6 t-Hexene-2 0.486 0.547 0.513 140.069

36 36.898 625-27-4 C6 2-Methylpentene-2 0.329 0.365 0.347 94.769

37 37.310 922-62-3 C6 3-Methyl-c-pentene-2 0.255 0.280 0.268 73.371

38 38.235 7688-21-3 K6 c-Hexene-2 0.206 0.228 0.217 59.259

39 39.585 3404-73-7 C7 3,3-Dimethylpentene-1 0.303 0.331 0.274 87.250

40 40.158 96-37-7 M6 Methylcyclopentane 1.799 1.845 1.896 518.281

41 41.732 108-08-7 I7 2,4-Dimethylpentane 0.331 0.377 0.293 93.328

42 42.035 594-56-9 C7 2,3,3-Trimethylbutene-1 0.014 0.015 0.012 3.936

43 42.272 464-06-2 I7 2,2,3-Trimethylbutane 0.047 0.053 0.042 13.359

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C-201
Hydrocarbon Expert V4.7 Thu Aug 26 13:41:34 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91317 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91317

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 44.931 ? Unidentified 0.012 0.012 0.013 4.090

45 45.132 71-42-3 Q6 Benzene 0.645 0.564 0.733 200.223

46 45.337 693-89-0 B6 1-Methylcyclopentene 0.351 0.346 0.379 103.600

47 46.157 3404-61-3 C7 3-Methylhexene-1 0.016 0.017 0.014 4.490

48 46.743 3524-73-0 C7 5-Methylhexene-1 0.071 0.078 0.064 20.387

49 47.057 110-82-7 M6 Cyclohexane 1.301 1.283 1.371 374.784

50 47.594 3404-72-6 C7 1-Pentene, 2,3-dimethyl- 0.041 0.045 0.037 11.767

51 48.80415840-60-5 C7 2-Methyl-c-hexene-3 0.039 0.043 0.035 11.187

52 49.148 3769-23-1 C7 4-Methylhexene-1 0.011 0.012 0.010 3.218

53 49.793 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.050 0.054 0.045 14.264

54 50.191 591-76-4 I7 2-Methylhexane 0.946 1.070 0.837 266.976

55 50.668 110-83-8 B6 Cyclohexene 0.043 0.041 0.047 12.431

56 52.029 589-34-4 I7 3-Methylhexane 0.546 0.610 0.484 154.186

57 52.880 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.132 0.135 0.119 37.906

58 53.467 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.096 0.099 0.087 27.606

59 54.091 822-50-4 M7 1t,2-Dimethylcyclopentane 0.122 0.124 0.110 35.025

60 54.391 C7 C7 - Iso-Olefin - 2 0.022 0.024 0.020 6.338

61 54.684 540-84-1 I8 2,2,4-Trimethylpentane 0.048 0.053 0.037 13.557

62 55.023 592-76-7 K7 Heptene-1 0.028 0.031 0.026 8.132

63 56.358 4914-89-0 C7 3-Methyl-c-hexene-3 0.013 0.014 0.012 3.869

64 56.87914686-14-7 K7 t-Heptene-3 0.031 0.034 0.028 9.019

65 57.241 6094-02-6 C7 2-Methylhexene-1 0.056 0.062 0.051 16.117

66 57.612 142-82-5 P7 n-Heptane 0.285 0.320 0.252 80.332

67 57.832 7642-10-6 K7 c-Heptene-3 0.024 0.026 0.022 6.946

68 58.111 2738-19-4 C7 2-Methyl-2-hexene 0.026 0.028 0.023 7.410

69 58.355 3899-36-3 C7 3-Methyl-t-hexene-3 0.020 0.022 0.018 5.647

70 58.74114686-13-6 K7 t-Heptene-2 0.014 0.015 0.013 4.010

71 59.19916491-15-9 M7 Cyclopentene, 1,5-dimethyl- 0.018 0.018 0.016 5.067

72 59.64120710-38-8 C7 3-Methyl-t-hexene-2 0.015 0.016 0.014 4.308

73 60.425 4914-91-4 C7 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.014 0.012 3.765

74 61.054 108-87-2 M7 Methylcyclohexane 0.308 0.307 0.278 88.705

75 63.099 ? Unidentified 0.021 0.022 0.017 7.297

76 63.854 1640-89-7 M7 Ethylcyclopentane 0.012 0.012 0.011 3.490

77 64.504 ? Unidentified 0.059 0.064 0.046 20.937

78 64.742 592-13-2 I8 2,5-Dimethylhexane 0.135 0.150 0.105 38.210

79 65.081 589-43-5 I8 2,4-Dimethylhexane 0.126 0.138 0.098 35.610

80 68.080 565-75-3 I8 2,3,4-Trimethylpentane 0.806 0.861 0.626 228.114

81 68.666 108-88-3 Q7 Toluene 12.177 10.785 11.726 3737.342

82 70.423 584-94-1 I8 2,3-Dimethylhexane 0.224 0.241 0.174 63.268

83 71.693 592-27-8 I8 2-Methylheptane 0.048 0.052 0.037 13.473

84 71.954 589-53-7 I8 4-Methylheptane 0.043 0.047 0.033 12.104

85 72.088 ? Unidentified 0.021 0.022 0.016 7.318

86 72.858 M8 1,3-dimethyl-t-cyclohexane 0.022 0.022 0.017 6.349

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C-202
Hydrocarbon Expert V4.7 Thu Aug 26 13:41:34 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91317 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91317

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 73.017 589-81-1 I8 3-Methylheptane 0.046 0.050 0.036 13.078

88 73.196 619-99-8 I8 3-Ethylhexane 0.018 0.019 0.014 5.079

89 74.919 3522-94-9 I9 2,2,5-Trimethylhexane 0.520 0.565 0.360 147.522

90 76.186 2207-03-6 M8 1t,3-Dimethylcyclohexane 0.009 0.009 0.007 2.691

91 77.560 111-65-9 P8 n-Octane 0.053 0.058 0.041 15.111

92 78.505 ? Unidentified 0.014 0.014 0.011 4.905

93 80.053 1069-53-0 I9 2,3,5-Trimethylhexane 0.090 0.096 0.062 25.466

94 81.231 1071-26-7 I9 2,4-Dimethylheptane 0.014 0.015 0.009 3.862

95 81.865 1678-91-7 M8 Ethylcyclohexane 0.013 0.013 0.011 3.837

96 82.193 1072-05-5 I9 2,6-Dimethylheptane 0.020 0.022 0.014 5.736

97 83.129 I9 2,5-Dimethylheptane 0.043 0.046 0.030 12.123

98 84.449 100-41-4 Q8 Ethylbenzene 2.212 1.959 1.849 673.769

99 85.698 108-38-3 Q8 m-Xylene 5.682 5.049 4.749 1730.792

100 85.840 106-42-3 Q8 p-Xylene 2.586 2.306 2.161 787.582

101 88.011 2216-33-3 I9 3-Methyloctane 0.008 0.009 0.006 2.369

102 88.479 ? Unidentified 0.031 0.035 0.022 11.052

103 88.657 95-47-6 Q8 o-Xylene 1.471 1.283 1.229 447.970

104 89.064 I10 C10 - IsoParaffin - 1 0.108 0.114 0.068 30.799

105 89.91014720-74-2 I10 2,2,4-trimethylheptane 0.076 0.080 0.047 21.586

106 91.463 111-84-2 P9 n-Nonane 0.069 0.074 0.048 19.654

107 92.836 98-82-8 Q9 i-Propylbenzene 0.032 0.029 0.024 9.820

108 93.600 ? Unidentified 0.078 0.083 0.049 27.637

109 93.82315869-87-1 I10 2,2-Dimethyloctane 0.028 0.029 0.017 7.829

110 94.265 ? Unidentified 0.011 0.009 1.002 3.987

111 94.265 ? Unidentified 0.011 0.012 0.007 3.987

112 94.62115869-89-3 I10 2,5-Dimethyloctane 0.064 0.067 0.040 18.208

113 95.101 2040-95-1 I10 2,7-Dimethyloctane 0.028 0.029 0.017 7.876

114 95.266 2051-30-1 I10 2,4-Dimethyloctane 0.126 0.133 0.078 35.702

115 95.663 I10 2,6-Dimethyloctane 0.038 0.040 0.023 10.683

116 96.307 103-65-1 Q9 n-Propylbenzene 0.540 0.481 0.399 163.527

117 97.165 620-14-4 Q9 1-Methyl-3-ethylbenzene 2.178 1.935 1.608 659.245

118 97.395 622-96-8 Q9 1-Methyl-4-ethylbenzene 1.026 0.915 0.757 310.465

119 98.021 108-67-8 Q9 1,3,5-Trimethylbenzene 1.362 1.209 1.006 412.315

120 98.49915869-85-9 I10 5-Methylnonane 0.010 0.010 0.006 2.777

121 98.69017301-94-8 I10 4-Methylnonane 0.023 0.024 0.014 6.550

122 98.896 I10 2,2,6-Trimethyloctane 2.172 2.296 1.354 616.965

123 99.103 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.807 0.703 0.595 244.090

124 99.470 ? Unidentified 0.005 0.005 0.003 1.784

125 99.664 5911-04-6 I10 3-Methylnonane 0.033 0.035 0.021 9.423

126 99.843 ? Unidentified 0.006 0.006 0.004 2.067

127 100.130 ? Unidentified 0.127 0.098 0.072 44.950

128 100.258 ? Unidentified 0.361 0.372 0.205 127.351

129 100.480 I11 C11-Isoparaffin-2 0.192 0.198 0.109 54.676

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C-203
Hydrocarbon Expert V4.7 Thu Aug 26 13:41:34 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91317 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91317

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 100.758 95-63-6 Q9 1,2,4-Trimethylbenzene 4.131 3.622 3.049 1250.078

131 100.944 ? Unidentified 0.220 0.241 0.139 77.618

132 101.065 ? Unidentified 0.131 0.137 0.082 46.234

133 101.321 1678-98-4 M10 i-Butylcyclohexane 0.035 0.034 0.022 10.205

134 102.11017302-01-1 I10 3-Ethyl-3-methylheptane 0.335 0.346 0.190 95.287

135 102.460 538-93-2 Q10 i-Butylbenzene 0.370 0.333 0.245 111.470

136 102.661 124-18-5 P10 n-Decane 0.102 0.108 0.064 29.086

137 102.975 ? Unidentified 0.085 0.087 0.048 29.901

138 103.616 526-73-8 Q9 1,2,3-Trimethylbenzene 0.734 0.630 0.542 222.095

139 103.990 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.036 0.032 0.024 10.803

140 104.191 I11 C11 Isoparaffin-4 0.038 0.040 0.022 10.895

141 104.394 ? Unidentified 0.211 0.189 0.140 74.544

142 104.802 J9 Indan 0.296 0.236 0.222 90.988

143 105.058 I11 C11-Isoparaffin-5 0.020 0.021 0.011 5.758

144 105.437 J10 Indene 1.131 0.901 0.849 347.983

145 106.153 I11 C11-Isoparaffin-7 0.437 0.451 0.248 124.343

146 106.333 141-93-5 Q10 1,3-Diethylbenzene 0.095 0.085 0.063 28.625

147 106.629 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 1.477 1.318 0.976 444.653

148 106.940 105-05-5 Q10 1,4-Diethylbenzene 0.493 0.439 0.326 148.512

149 107.176 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.298 0.260 0.197 89.714

150 107.430 135-01-3 Q10 1,2-Diethylbenzene 0.099 0.087 0.066 29.908

151 107.889 ? Unidentified 0.100 0.103 0.057 35.174

152 108.026 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.116 0.102 0.077 34.861

153 108.166 ? Unidentified 0.107 0.111 0.062 37.912

154 108.245 ? Unidentified 0.091 0.094 0.052 32.152

155 108.369 I11 C11- Isoparaffin-11 0.817 0.843 0.464 232.339

156 108.551 ? Unidentified 0.260 0.269 0.148 91.943

157 108.986 ? Unidentified 1.060 0.928 0.700 373.988

158 109.204 J10 2-Methylindan 0.144 0.115 0.097 44.389

159 109.547 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.763 0.670 0.504 229.534

160 110.101 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.683 0.589 0.452 205.632

161 110.528 ? Unidentified 0.028 0.026 0.016 9.800

162 110.729 ? Unidentified 0.048 0.050 0.030 16.947

163 110.859 ? Unidentified 0.075 0.077 0.047 26.330

164 111.000 Q11 1-Methyl-4-t-butylbenzene 0.091 0.082 0.055 27.344

165 111.221 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.312 0.269 0.206 93.946

166 111.531 1120-21-4 P11 n-Undecane 0.097 0.101 0.055 27.701

167 111.689 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.099 0.086 0.060 29.800

168 111.798 ? Unidentified 0.064 0.055 0.038 22.505

169 112.166 Q10 1,2,4,5-Tetramethylbenzene 0.547 0.473 0.361 164.526

170 112.433 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.713 0.615 0.471 214.572

171 112.641 ? Unidentified 0.015 0.013 0.009 5.301

172 112.785 ? Unidentified 0.017 0.014 0.010 6.092

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C-204
Hydrocarbon Expert V4.7 Thu Aug 26 13:41:34 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91317 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91317

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 112.965 I12 C12 - IsoParaffin - 1 0.026 0.027 0.013 7.357

174 113.291 ? Unidentified 0.052 0.055 0.028 18.438

175 113.583 Q11 C11 - Aromatic - 3 0.094 0.081 0.056 28.237

176 113.763 874-35-1 H10 5-Methylindan 0.235 0.203 0.158 70.839

177 113.903 Q12 1,2-Di-i-propylbenzene 0.085 0.073 0.046 25.263

178 114.118 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.123 0.107 0.074 37.010

179 114.275 Q11 C11 - Aromatic - 4 0.071 0.061 0.042 21.163

180 114.514 824-22-6 J10 4-Methylindan 0.291 0.251 0.195 87.481

181 114.766 824-63-5 H10 2-Methylindan 0.311 0.269 0.209 93.740

182 114.979 ? Unidentified 0.023 0.020 0.014 8.140

183 115.089 538-68-1 Q11 n-Pentylbenzene 0.038 0.033 0.023 11.495

184 115.320 Q11 tert-Pentylbenzene 0.130 0.112 0.078 38.972

185 115.632 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.060 0.052 0.036 18.055

186 115.743 Q11 C11 - Aromatic - 7 0.080 0.072 0.048 23.836

187 116.205 100-18-5 Q12 1,4-Di-i-propylbenzene 0.123 0.106 0.067 36.682

188 116.632 91-20-3 G10 Naphthalene 0.246 0.184 0.170 77.392

189 116.841 J11 4,7-Dimethyl Indane 0.014 0.011 0.008 4.183

190 117.091 J11 1,1-Dimethyl Indane 0.044 0.035 0.026 13.403

191 117.249 J12 Dimethyl Indane - 1 0.021 0.017 0.013 6.512

192 117.430 7364-19-4 Q12 1t-Butyl-4-ethylbenzene 0.028 0.024 0.015 8.268

193 117.737 Q12 1,3-Di-n-propylbenzene 0.107 0.093 0.059 32.110

194 117.845 Q11 C11 - Aromatic - 11 0.060 0.054 0.036 17.968

195 118.401 Q11 C11 - Aromatic - 12 0.043 0.039 0.026 12.929

196 119.028 Q11 C11 - Aromatic - 13 0.007 0.006 0.004 2.108

197 119.340 102-25-0 Q12 1,3,5-Triethylbenzene 0.012 0.011 0.007 3.721

198 119.990 Q12 C12 - Aromatic - 1 0.006 0.005 0.003 1.898

199 123.281 91-57-6 G11 2-Methylnaphthalene 0.009 0.007 0.005 2.733

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C-205
Hydrocarbon Expert V4.7 Thu Aug 26 13:41:34 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91317 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91317

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 7.386 74-98-6 Propane 0.001 0.001 0.001 0.159

9.787 106-97-8 n-Butane 1.079 1.431 1.646 300.047

17.687 109-66-0 n-Pentane 1.652 2.025 2.031 462.691

35.310 110-54-3 n-Hexane 4.380 5.100 4.509 1231.787

57.612 142-82-5 n-Heptane 0.285 0.320 0.252 80.332

77.560 111-65-9 n-Octane 0.053 0.058 0.041 15.111

91.463 111-84-2 n-Nonane 0.069 0.074 0.048 19.654

102.661 124-18-5 n-Decane 0.102 0.108 0.064 29.086

111.531 1120-21-4 n-Undecane 0.097 0.101 0.055 27.701

I-Paraffins 8.607 75-28-5 i-Butane 0.015 0.021 0.023 4.223

10.383 463-82-1 2,2-Dimethylpropane 0.009 0.012 0.011 2.575

14.701 78-78-4 i-Pentane 3.483 4.317 4.283 975.682

22.606 75-83-2 2,2-Dimethylbutane 0.294 0.348 0.303 82.714

27.826 79-29-8 2,3-Dimethylbutane 1.092 1.268 1.124 307.138

28.926 107-83-5 2-Methylpentane 6.264 7.365 6.449 1761.717

31.558 96-14-0 3-Methylpentane 3.641 4.209 3.749 1024.040

41.732 108-08-7 2,4-Dimethylpentane 0.331 0.377 0.293 93.328

42.272 464-06-2 2,2,3-Trimethylbutane 0.047 0.053 0.042 13.359

50.191 591-76-4 2-Methylhexane 0.946 1.070 0.837 266.976

52.029 589-34-4 3-Methylhexane 0.546 0.610 0.484 154.186

54.684 540-84-1 2,2,4-Trimethylpentane 0.048 0.053 0.037 13.557

64.742 592-13-2 2,5-Dimethylhexane 0.135 0.150 0.105 38.210

65.081 589-43-5 2,4-Dimethylhexane 0.126 0.138 0.098 35.610

68.080 565-75-3 2,3,4-Trimethylpentane 0.806 0.861 0.626 228.114

70.423 584-94-1 2,3-Dimethylhexane 0.224 0.241 0.174 63.268

71.693 592-27-8 2-Methylheptane 0.048 0.052 0.037 13.473

71.954 589-53-7 4-Methylheptane 0.043 0.047 0.033 12.104

73.017 589-81-1 3-Methylheptane 0.046 0.050 0.036 13.078

73.196 619-99-8 3-Ethylhexane 0.018 0.019 0.014 5.079

74.919 3522-94-9 2,2,5-Trimethylhexane 0.520 0.565 0.360 147.522

80.053 1069-53-0 2,3,5-Trimethylhexane 0.090 0.096 0.062 25.466

81.231 1071-26-7 2,4-Dimethylheptane 0.014 0.015 0.009 3.862

82.193 1072-05-5 2,6-Dimethylheptane 0.020 0.022 0.014 5.736

83.129 2,5-Dimethylheptane 0.043 0.046 0.030 12.123

88.011 2216-33-3 3-Methyloctane 0.008 0.009 0.006 2.369

89.064 C10 - IsoParaffin - 1 0.108 0.114 0.068 30.799

89.91014720-74-2 2,2,4-trimethylheptane 0.076 0.080 0.047 21.586

93.82315869-87-1 2,2-Dimethyloctane 0.028 0.029 0.017 7.829

94.62115869-89-3 2,5-Dimethyloctane 0.064 0.067 0.040 18.208

95.101 2040-95-1 2,7-Dimethyloctane 0.028 0.029 0.017 7.876

95.266 2051-30-1 2,4-Dimethyloctane 0.126 0.133 0.078 35.702

95.663 2,6-Dimethyloctane 0.038 0.040 0.023 10.683

98.49915869-85-9 5-Methylnonane 0.010 0.010 0.006 2.777

98.69017301-94-8 4-Methylnonane 0.023 0.024 0.014 6.550

98.896 2,2,6-Trimethyloctane 2.172 2.296 1.354 616.965

99.664 5911-04-6 3-Methylnonane 0.033 0.035 0.021 9.423

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C-206
Hydrocarbon Expert V4.7 Thu Aug 26 13:41:34 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91317 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91317

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

I-Paraffins 100.480 C11-Isoparaffin-2 0.192 0.198 0.109 54.676

102.11017302-01-1 3-Ethyl-3-methylheptane 0.335 0.346 0.190 95.287

104.191 C11 Isoparaffin-4 0.038 0.040 0.022 10.895

105.058 C11-Isoparaffin-5 0.020 0.021 0.011 5.758

106.153 C11-Isoparaffin-7 0.437 0.451 0.248 124.343

108.369 C11- Isoparaffin-11 0.817 0.843 0.464 232.339

112.965 C12 - IsoParaffin - 1 0.026 0.027 0.013 7.357

Aromatics

Mono-Aromatics 45.132 71-42-3 Benzene 0.645 0.564 0.733 200.223

68.666 108-88-3 Toluene 12.177 10.785 11.726 3737.342

84.449 100-41-4 Ethylbenzene 2.212 1.959 1.849 673.769

85.698 108-38-3 m-Xylene 5.682 5.049 4.749 1730.792

85.840 106-42-3 p-Xylene 2.586 2.306 2.161 787.582

88.657 95-47-6 o-Xylene 1.471 1.283 1.229 447.970

92.836 98-82-8 i-Propylbenzene 0.032 0.029 0.024 9.820

96.307 103-65-1 n-Propylbenzene 0.540 0.481 0.399 163.527

97.165 620-14-4 1-Methyl-3-ethylbenzene 2.178 1.935 1.608 659.245

97.395 622-96-8 1-Methyl-4-ethylbenzene 1.026 0.915 0.757 310.465

98.021 108-67-8 1,3,5-Trimethylbenzene 1.362 1.209 1.006 412.315

99.103 611-14-3 1-Methyl-2-ethylbenzene 0.807 0.703 0.595 244.090

100.758 95-63-6 1,2,4-Trimethylbenzene 4.131 3.622 3.049 1250.078

102.460 538-93-2 i-Butylbenzene 0.370 0.333 0.245 111.470

103.616 526-73-8 1,2,3-Trimethylbenzene 0.734 0.630 0.542 222.095

103.990 535-77-3 1-Methyl-3-i-propylbenzene 0.036 0.032 0.024 10.803

106.333 141-93-5 1,3-Diethylbenzene 0.095 0.085 0.063 28.625

106.629 1074-43-7 1-Methyl-3-n-propylbenzene 1.477 1.318 0.976 444.653

106.940 105-05-5 1,4-Diethylbenzene 0.493 0.439 0.326 148.512

107.176 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.298 0.260 0.197 89.714

107.430 135-01-3 1,2-Diethylbenzene 0.099 0.087 0.066 29.908

108.026 1074-17-5 1-Methyl-2-n-propylbenzene 0.116 0.102 0.077 34.861

109.547 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.763 0.670 0.504 229.534

110.101 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.683 0.589 0.452 205.632

111.000 1-Methyl-4-t-butylbenzene 0.091 0.082 0.055 27.344

111.221 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.312 0.269 0.206 93.946

111.689 4218-48-8 1-Ethyl-4-i-propylbenzene 0.099 0.086 0.060 29.800

112.166 1,2,4,5-Tetramethylbenzene 0.547 0.473 0.361 164.526

112.433 527-53-7 1,2,3,5-Tetramethylbenzene 0.713 0.615 0.471 214.572

113.583 C11 - Aromatic - 3 0.094 0.081 0.056 28.237

113.903 1,2-Di-i-propylbenzene 0.085 0.073 0.046 25.263

114.118 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.123 0.107 0.074 37.010

114.275 C11 - Aromatic - 4 0.071 0.061 0.042 21.163

115.089 538-68-1 n-Pentylbenzene 0.038 0.033 0.023 11.495

115.320 tert-Pentylbenzene 0.130 0.112 0.078 38.972

115.632 577-55-9 1-Methyl-2-n-butylbenzene 0.060 0.052 0.036 18.055

115.743 C11 - Aromatic - 7 0.080 0.072 0.048 23.836

116.205 100-18-5 1,4-Di-i-propylbenzene 0.123 0.106 0.067 36.682

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C-207
Hydrocarbon Expert V4.7 Thu Aug 26 13:41:34 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91317 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91317

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 117.430 7364-19-4 1t-Butyl-4-ethylbenzene 0.028 0.024 0.015 8.268

117.737 1,3-Di-n-propylbenzene 0.107 0.093 0.059 32.110

117.845 C11 - Aromatic - 11 0.060 0.054 0.036 17.968

118.401 C11 - Aromatic - 12 0.043 0.039 0.026 12.929

119.028 C11 - Aromatic - 13 0.007 0.006 0.004 2.108

119.340 102-25-0 1,3,5-Triethylbenzene 0.012 0.011 0.007 3.721

119.990 C12 - Aromatic - 1 0.006 0.005 0.003 1.898

Naphthalenes 116.632 91-20-3 Naphthalene 0.246 0.184 0.170 77.392

123.281 91-57-6 2-Methylnaphthalene 0.009 0.007 0.005 2.733

Naphtheno/Olefino-Benzs 113.763 874-35-1 5-Methylindan 0.235 0.203 0.158 70.839

114.766 824-63-5 2-Methylindan 0.311 0.269 0.209 93.740

Indenes 104.802 Indan 0.296 0.236 0.222 90.988

105.437 Indene 1.131 0.901 0.849 347.983

109.204 2-Methylindan 0.144 0.115 0.097 44.389

114.514 824-22-6 4-Methylindan 0.291 0.251 0.195 87.481

116.841 4,7-Dimethyl Indane 0.014 0.011 0.008 4.183

117.091 1,1-Dimethyl Indane 0.044 0.035 0.026 13.403

117.249 Dimethyl Indane - 1 0.021 0.017 0.013 6.512

Naphthenes

Mono-Naphthenes 27.094 287-92-3 Cyclopentane 0.296 0.305 0.375 85.306

40.158 96-37-7 Methylcyclopentane 1.799 1.845 1.896 518.281

47.057 110-82-7 Cyclohexane 1.301 1.283 1.371 374.784

52.880 1759-58-6 1t,3-Dimethylcyclopentane 0.132 0.135 0.119 37.906

53.467 2532-58-3 1c,3-Dimethylcyclopentane 0.096 0.099 0.087 27.606

54.091 822-50-4 1t,2-Dimethylcyclopentane 0.122 0.124 0.110 35.025

59.19916491-15-9 Cyclopentene, 1,5-dimethyl- 0.018 0.018 0.016 5.067

61.054 108-87-2 Methylcyclohexane 0.308 0.307 0.278 88.705

63.854 1640-89-7 Ethylcyclopentane 0.012 0.012 0.011 3.490

72.858 1,3-dimethyl-t-cyclohexane 0.022 0.022 0.017 6.349

76.186 2207-03-6 1t,3-Dimethylcyclohexane 0.009 0.009 0.007 2.691

81.865 1678-91-7 Ethylcyclohexane 0.013 0.013 0.011 3.837

101.321 1678-98-4 i-Butylcyclohexane 0.035 0.034 0.022 10.205

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.399 115-11-7 Isobutene 0.014 0.018 0.022 4.074

9.438 106-98-9 Butene-1 0.017 0.022 0.027 4.884

10.261 624-64-6 t-Butene-2 0.067 0.086 0.107 19.405

10.981 590-18-1 c-Butene-2 0.080 0.099 0.126 22.975

16.325 109-67-1 Pentene-1 0.315 0.377 0.398 90.649

18.792 646-04-8 t-Pentene-2 0.801 0.949 1.013 230.692

19.812 627-20-3 c-Pentene-2 0.439 0.514 0.556 126.522

32.937 592-41-6 Hexene-1 0.154 0.175 0.163 44.483

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C-208
Hydrocarbon Expert V4.7 Thu Aug 26 13:41:34 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91317 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91317

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

n-Olefins 35.93213269-52-8 t-Hexene-3 0.253 0.285 0.267 72.835

36.406 4050-45-7 t-Hexene-2 0.486 0.547 0.513 140.069

38.235 7688-21-3 c-Hexene-2 0.206 0.228 0.217 59.259

55.023 592-76-7 Heptene-1 0.028 0.031 0.026 8.132

56.87914686-14-7 t-Heptene-3 0.031 0.034 0.028 9.019

57.832 7642-10-6 c-Heptene-3 0.024 0.026 0.022 6.946

58.74114686-13-6 t-Heptene-2 0.014 0.015 0.013 4.010

Iso-Olefins 13.119 563-45-1 3-Methylbutene-1 0.315 0.386 0.399 90.871

17.162 563-46-2 2-Methylbutene-1 0.478 0.564 0.604 137.656

20.482 513-35-9 2-Methylbutene-2 0.985 1.141 1.245 283.664

28.687 691-38-3 4-Methyl-c-pentene-2 0.041 0.046 0.043 11.671

29.334 674-76-0 4-Methyl-t-pentene-2 0.126 0.143 0.133 36.232

32.713 763-29-1 2-Methylpentene-1 0.215 0.241 0.226 61.837

36.898 625-27-4 2-Methylpentene-2 0.329 0.365 0.347 94.769

37.310 922-62-3 3-Methyl-c-pentene-2 0.255 0.280 0.268 73.371

39.585 3404-73-7 3,3-Dimethylpentene-1 0.303 0.331 0.274 87.250

42.035 594-56-9 2,3,3-Trimethylbutene-1 0.014 0.015 0.012 3.936

46.157 3404-61-3 3-Methylhexene-1 0.016 0.017 0.014 4.490

46.743 3524-73-0 5-Methylhexene-1 0.071 0.078 0.064 20.387

47.594 3404-72-6 1-Pentene, 2,3-dimethyl- 0.041 0.045 0.037 11.767

48.80415840-60-5 2-Methyl-c-hexene-3 0.039 0.043 0.035 11.187

49.148 3769-23-1 4-Methylhexene-1 0.011 0.012 0.010 3.218

49.793 3404-55-5 4-Methyl-t/c-hexene-2 0.050 0.054 0.045 14.264

54.391 C7 - Iso-Olefin - 2 0.022 0.024 0.020 6.338

56.358 4914-89-0 3-Methyl-c-hexene-3 0.013 0.014 0.012 3.869

57.241 6094-02-6 2-Methylhexene-1 0.056 0.062 0.051 16.117

58.111 2738-19-4 2-Methyl-2-hexene 0.026 0.028 0.023 7.410

58.355 3899-36-3 3-Methyl-t-hexene-3 0.020 0.022 0.018 5.647

59.64120710-38-8 3-Methyl-t-hexene-2 0.015 0.016 0.014 4.308

60.425 4914-91-4 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.014 0.012 3.765

Naphtheno-Olefins 25.241 142-29-0 Cyclopentene 0.188 0.187 0.244 55.667

45.337 693-89-0 1-Methylcyclopentene 0.351 0.346 0.379 103.600

50.668 110-83-8 Cyclohexene 0.043 0.041 0.047 12.431

Di-Olefins 18.199 78-79-5 2-Methyl-1,3-Butadiene 0.010 0.011 0.013 2.927

20.812 2004-70-8 1t,3-Pentadiene 0.015 0.017 0.019 4.358

Oxygenates 12.739 64-17-5 Ethanol 8.550 8.321 16.466 1058.804

26.486 71-23-8 n-Propanol 0.172 0.165 0.254 34.733

Unidentified 22.061 Unidentified 0.006 0.006 0.007 1.971

28.226 Unidentified 0.048 0.050 0.049 17.082

44.931 Unidentified 0.012 0.012 0.013 4.090

63.099 Unidentified 0.021 0.022 0.017 7.297

64.504 Unidentified 0.059 0.064 0.046 20.937

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C-209
Hydrocarbon Expert V4.7 Thu Aug 26 13:41:34 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91317 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91317

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Unidentified 72.088 Unidentified 0.021 0.022 0.016 7.318

78.505 Unidentified 0.014 0.014 0.011 4.905

88.479 Unidentified 0.031 0.035 0.022 11.052

93.600 Unidentified 0.078 0.083 0.049 27.637

94.265 Unidentified 0.011 0.009 1.002 3.987

94.265 Unidentified 0.011 0.012 0.007 3.987

99.470 Unidentified 0.005 0.005 0.003 1.784

99.843 Unidentified 0.006 0.006 0.004 2.067

100.130 Unidentified 0.127 0.098 0.072 44.950

100.258 Unidentified 0.361 0.372 0.205 127.351

100.944 Unidentified 0.220 0.241 0.139 77.618

101.065 Unidentified 0.131 0.137 0.082 46.234

102.975 Unidentified 0.085 0.087 0.048 29.901

104.394 Unidentified 0.211 0.189 0.140 74.544

107.889 Unidentified 0.100 0.103 0.057 35.174

108.166 Unidentified 0.107 0.111 0.062 37.912

108.245 Unidentified 0.091 0.094 0.052 32.152

108.551 Unidentified 0.260 0.269 0.148 91.943

108.986 Unidentified 1.060 0.928 0.700 373.988

110.528 Unidentified 0.028 0.026 0.016 9.800

110.729 Unidentified 0.048 0.050 0.030 16.947

110.859 Unidentified 0.075 0.077 0.047 26.330

111.798 Unidentified 0.064 0.055 0.038 22.505

112.641 Unidentified 0.015 0.013 0.009 5.301

112.785 Unidentified 0.017 0.014 0.010 6.092

113.291 Unidentified 0.052 0.055 0.028 18.438

114.979 Unidentified 0.023 0.020 0.014 8.140

Plus

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C-210
Hydrocarbon Expert V4.7 Thu Aug 26 13:41:34 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91317 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91317

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF

20.0 15.0 10.0 5.0 0.0

Propane

i-Butane

Isobutene Butene-1

n-Butane

2,2-Dimethylpropane t-Butene-2

c-Butene-2

Ethanol

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

Unidentified

2,2-Dimethylbutane

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C-211
Hydrocarbon Expert V4.7 Thu Aug 26 13:41:34 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91317 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91317

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

n-Propanol

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

n-Hexane

t-Hexene-3

t-Hexene-2

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane 2,3,3-Trimethylbutene-1 2,2,3-Trimethylbutane

Unidentified Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1 Cyclohexane

1-Pentene, 2,3-dimethyl2-Methyl-c-hexene-3

4-Methylhexene-1

4-Methyl-t/c-hexene-2

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C-212
Hydrocarbon Expert V4.7 Thu Aug 26 13:41:34 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91317 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91317

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF

70.0 65.0 60.0 55.0 50.0

2-Methylhexane

Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane C7 - Iso-Olefin - 2 2,2,4-Trimethylpentane

Heptene-1

3-Methyl-c-hexene-3

t-Heptene-3

2-Methylhexene-1

n-Heptane c-Heptene-3 2-Methyl-2-hexene 3-Methyl-t-hexene-3

t-Heptene-2

Cyclopentene, 1,5-dimethyl3-Methyl-t-hexene-2

2-Pentene, 3,4-dimethyl-, (Z)-

Methylcyclohexane

Unidentified

Ethylcyclopentane

Unidentified 2,5-Dimethylhexane

2,4-Dimethylhexane

2,3,4-Trimethylpentane

Toluene

2,3-Dimethylhexane

2-Methylheptane

Unidentified 4-Methylheptane

1,3-dimethyl-t-cyclohexane 3-Methylheptane 3-Ethylhexane

2,2,5-Trimethylhexane

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C-213
Hydrocarbon Expert V4.7 Thu Aug 26 13:41:34 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91317 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91317

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF

95.0 90.0 85.0 80.0 75.0

1t,3-Dimethylcyclohexane

n-Octane

Unidentified

2,3,5-Trimethylhexane

2,4-Dimethylheptane

Ethylcyclohexane

2,6-Dimethylheptane

2,5-Dimethylheptane

Ethylbenzene

m-Xylene p-Xylene

3-Methyloctane

Unidentified o-Xylene

C10 - IsoParaffin - 1

2,2,4-trimethylheptane

n-Nonane

i-Propylbenzene

Unidentified 2,2-Dimethyloctane

Unidentified

2,5-Dimethyloctane

2,7-Dimethyloctane 2,4-Dimethyloctane

2,6-Dimethyloctane

n-Propylbenzene

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

5-Methylnonane 4-Methylnonane 2,2,6-Trimethyloctane 1-Methyl-2-ethylbenzene

Unidentified 3-Methylnonane Unidentified

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C-214
Hydrocarbon Expert V4.7 Thu Aug 26 13:41:34 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91317 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91317

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified Unidentified C11-Isoparaffin-2 1,2,4-Trimethylbenzene

Unidentified Unidentified

i-Butylcyclohexane

3-Ethyl-3-methylheptane

i-Butylbenzene n-Decane Unidentified

1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene C11 Isoparaffin-4 Unidentified

Indan C11-Isoparaffin-5

Indene

C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene 1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

Unidentified 1-Methyl-2-n-propylbenzene UnidentifiedC11- Isoparaffin-11 Unidentified

Unidentified 2-Methylindan

1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

Unidentified

1-Methyl-4-t-butylbenzene 1,2-Dimethyl-3-ethylbenzene n-Undecane Unidentified 1-Ethyl-4-i-propylbenzene

1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene Unidentified

C12 - IsoParaffin - 1

Unidentified C11 - Aromatic - 3 5-Methylindan 1,2-Di-i-propylbenzene

C11 - Aromatic - 4 1-methyl-4-(1-methylpropyl)be

4-Methylindan 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene 1-Methyl-2-n-butylbenzene C11 - Aromatic - 7

1,4-Di-i-propylbenzene

Naphthalene 4,7-Dimethyl Indane 1,1-Dimethyl Indane Dimethyl Indane - 1 1t-Butyl-4-ethylbenzene

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

C11 - Aromatic - 12

C11 - Aromatic - 13

1,3,5-Triethylbenzene

C12 - Aromatic - 1

2-Methylnaphthalene

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C-215
Hydrocarbon Expert V4.7 Thu Aug 26 13:41:34 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91317 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91317

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000013.D\SIG1000013_FID1_A.CDF

145.0 140.0 135.0 130.0 125.0

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C-216
Hydrocarbon Expert V4.7 Thu Aug 26 13:53:12 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91318 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91318

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 13.004 15.663 14.829

I-Paraffins 17.787 20.361 16.768

Aromatics 44.642 38.930 36.630

Mono-Aromatics 43.740 38.197 36.029

Naphthalenes 0.095 0.070 0.061

Naphtheno/Olefino-Benzs 0.272 0.232 0.174

Indenes 0.536 0.431 0.366

Naphthenes 7.088 7.041 6.622

Mono-Naphthenes 7.088 7.041 6.622

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 7.367 8.272 8.138

n-Olefins 3.095 3.554 3.520

Iso-Olefins 3.632 4.092 3.912

Naphtheno-Olefins 0.614 0.597 0.673

Di-Olefins 0.026 0.029 0.032

Oxygenates 8.901 8.549 16.245

Unidentified 1.211 1.183 0.768

Plus 0.000 0.000 0.000

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C-217
Hydrocarbon Expert V4.7 Thu Aug 26 13:53:12 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91318 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91318

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C2 8.719 8.377 15.990

C3 0.189 0.184 0.270

C4 4.445 5.813 6.472

C5 11.832 14.125 13.999

C6 16.432 17.990 16.331

C7 23.846 22.104 21.435

C8 21.370 19.463 16.779

C9 7.528 6.857 5.219

C10 3.692 3.251 2.329

C11 0.583 0.523 0.328

C12 0.152 0.129 0.079

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C-218
Hydrocarbon Expert V4.7 Thu Aug 26 13:53:12 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91318 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91318

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C3 0.008 0.012 0.015

C4 4.179 5.473 6.075

C5 2.838 3.435 3.323

C6 3.854 4.431 3.779

C7 0.983 1.090 0.829

C8 0.785 0.847 0.581

C9 0.276 0.291 0.182

C10 0.055 0.057 0.033

C11 0.025 0.026 0.014

I-Paraffins C4 0.072 0.099 0.105

C5 4.963 6.074 5.812

C6 5.724 6.594 5.611

C7 2.425 2.700 2.044

C8 2.630 2.814 1.945

C9 1.340 1.424 0.882

C10 0.512 0.533 0.302

C11 0.122 0.124 0.066

Mono-Aromatics C6 0.653 0.563 0.706

C7 17.283 15.111 15.847

C8 17.130 14.993 13.632

C9 5.784 5.036 4.065

C10 2.329 2.011 1.466

C11 0.411 0.354 0.234

C12 0.152 0.129 0.079

Naphthalenes C10 0.080 0.059 0.053

C11 0.015 0.011 0.009

Naphtheno/Olefino-Benzs C10 0.272 0.232 0.174

Indenes C9 0.081 0.064 0.058

C10 0.444 0.359 0.302

C11 0.010 0.008 0.006

Mono-Naphthenes C5 0.284 0.289 0.342

C6 3.615 3.600 3.629

C7 2.361 2.345 2.032

C8 0.781 0.765 0.588

C9 0.047 0.042 0.032

n-Olefins C4 0.194 0.241 0.292

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C-219
Hydrocarbon Expert V4.7 Thu Aug 26 13:53:12 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91318 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91318

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

n-Olefins C5 1.646 1.924 1.983

C6 1.155 1.280 1.159

C7 0.101 0.109 0.087

Iso-Olefins C5 1.877 2.180 2.261

C6 1.016 1.119 1.020

C7 0.694 0.749 0.597

C8 0.045 0.044 0.034

Naphtheno-Olefins C5 0.198 0.195 0.246

C6 0.416 0.403 0.428

Di-Olefins C5 0.026 0.029 0.032

Oxygenates C2 8.719 8.377 15.990

C3 0.182 0.172 0.255

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C-220
Hydrocarbon Expert V4.7 Thu Aug 26 13:53:12 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91318 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91318

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 21.62 21.32

5% 78.81 29.90

10% 82.90 80.72

15% 100.10 94.99

20% 140.24 116.45

25% 154.52 143.98

30% 160.39 154.56

35% 172.71 159.50

40% 174.38 172.68

45% 197.39 174.38

50% 230.74 197.31

55% 230.85 230.74

60% 230.95 230.86

65% 231.05 230.97

70% 257.58 235.35

75% 279.25 276.89

80% 281.48 280.86

85% 282.26 281.96

90% 321.38 300.27

95% 345.48 336.13

FBP 404.50 401.94

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C-221
Hydrocarbon Expert V4.7 Thu Aug 26 13:53:12 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91318 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91318

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 7.389 74-98-6 P3 Propane 0.008 0.012 0.015 1.988

2 8.610 75-28-5 I4 i-Butane 0.072 0.099 0.105 18.561

3 9.403 115-11-7 K4 Isobutene 0.015 0.020 0.023 4.088

4 9.443 106-98-9 K4 Butene-1 0.019 0.024 0.028 4.985

5 9.791 106-97-8 P4 n-Butane 4.179 5.473 6.075 1071.032

6 10.265 624-64-6 K4 t-Butene-2 0.073 0.092 0.110 19.366

7 10.387 463-82-1 I5 2,2-Dimethylpropane 0.021 0.027 0.025 5.505

8 10.986 590-18-1 K4 c-Butene-2 0.087 0.106 0.130 22.981

9 12.742 64-17-5 X2 Ethanol 8.719 8.377 15.990 994.782

10 13.125 563-45-1 C5 3-Methylbutene-1 0.329 0.398 0.397 87.383

11 14.710 78-78-4 I5 i-Pentane 4.942 6.046 5.787 1275.307

12 16.334 109-67-1 K5 Pentene-1 0.334 0.395 0.402 88.578

13 17.172 563-46-2 C5 2-Methylbutene-1 0.507 0.591 0.610 134.487

14 17.700 109-66-0 P5 n-Pentane 2.838 3.435 3.323 732.268

15 18.208 78-79-5 E5 2-Methyl-1,3-Butadiene 0.010 0.012 0.013 2.859

16 18.803 646-04-8 K5 t-Pentene-2 0.847 0.991 1.021 224.950

17 19.442 ? Unidentified 0.006 0.007 0.007 1.857

18 19.825 627-20-3 K5 c-Pentene-2 0.465 0.538 0.560 123.392

19 20.494 513-35-9 C5 2-Methylbutene-2 1.041 1.192 1.255 276.421

20 20.825 2004-70-8 E5 1t,3-Pentadiene 0.016 0.017 0.019 4.254

21 22.078 ? Unidentified 0.006 0.006 0.008 1.924

22 22.622 75-83-2 I6 2,2-Dimethylbutane 0.187 0.218 0.183 48.371

23 25.256 142-29-0 B5 Cyclopentene 0.198 0.195 0.246 54.138

24 26.501 71-23-8 X3 n-Propanol 0.182 0.172 0.255 33.724

25 27.110 287-92-3 M5 Cyclopentane 0.284 0.289 0.342 75.365

26 27.840 79-29-8 I6 2,3-Dimethylbutane 0.550 0.630 0.539 142.540

27 28.242 ? Unidentified 0.051 0.052 0.049 16.633

28 28.701 691-38-3 C6 4-Methyl-c-pentene-2 0.045 0.050 0.045 11.856

29 28.922 107-83-5 I6 2-Methylpentane 2.834 3.289 2.778 734.135

30 29.350 674-76-0 C6 4-Methyl-t-pentene-2 0.132 0.149 0.133 35.035

31 31.564 96-14-0 I6 3-Methylpentane 2.153 2.457 2.111 557.837

32 32.730 763-29-1 C6 2-Methylpentene-1 0.226 0.250 0.227 59.949

33 32.953 592-41-6 K6 Hexene-1 0.162 0.181 0.163 43.077

34 35.320 110-54-3 P6 n-Hexane 3.854 4.431 3.779 998.635

35 35.94713269-52-8 K6 t-Hexene-3 0.266 0.295 0.267 70.539

36 36.422 4050-45-7 K6 t-Hexene-2 0.511 0.567 0.512 135.510

37 36.913 625-27-4 C6 2-Methylpentene-2 0.346 0.379 0.347 91.750

38 37.324 922-62-3 C6 3-Methyl-c-pentene-2 0.268 0.291 0.269 71.051

39 38.250 7688-21-3 K6 c-Hexene-2 0.216 0.237 0.217 57.376

40 39.598 3404-73-7 C7 3,3-Dimethylpentene-1 0.317 0.342 0.273 84.077

41 40.172 96-37-7 M6 Methylcyclopentane 2.055 2.081 2.063 545.518

42 41.744 108-08-7 I7 2,4-Dimethylpentane 0.320 0.361 0.270 83.311

43 42.044 594-56-9 C7 2,3,3-Trimethylbutene-1 0.014 0.015 0.012 3.834

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C-222
Hydrocarbon Expert V4.7 Thu Aug 26 13:53:12 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91318 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91318

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 42.283 464-06-2 I7 2,2,3-Trimethylbutane 0.046 0.051 0.039 11.990

45 44.940 ? Unidentified 0.012 0.012 0.012 3.942

46 45.142 71-42-3 Q6 Benzene 0.653 0.563 0.706 186.666

47 45.346 693-89-0 B6 1-Methylcyclopentene 0.370 0.360 0.381 100.625

48 46.168 3404-61-3 C7 3-Methylhexene-1 0.016 0.018 0.014 4.337

49 46.750 3524-73-0 C7 5-Methylhexene-1 0.082 0.089 0.070 21.674

50 47.066 110-82-7 M6 Cyclohexane 1.559 1.519 1.565 413.927

51 47.602 ? Unidentified 0.035 0.038 0.030 11.476

52 48.80915840-60-5 C7 2-Methyl-c-hexene-3 0.041 0.045 0.036 10.972

53 49.804 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.052 0.056 0.045 13.774

54 50.197 591-76-4 I7 2-Methylhexane 1.265 1.413 1.067 329.111

55 50.673 110-83-8 B6 Cyclohexene 0.045 0.043 0.047 12.073

56 52.032 589-34-4 I7 3-Methylhexane 0.793 0.875 0.669 206.268

57 52.883 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.223 0.225 0.191 59.064

58 53.470 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.179 0.183 0.154 47.601

59 54.096 822-50-4 M7 1t,2-Dimethylcyclopentane 0.273 0.276 0.235 72.579

60 54.393 C7 C7 - Iso-Olefin - 2 0.023 0.024 0.019 5.981

61 54.687 540-84-1 I8 2,2,4-Trimethylpentane 0.065 0.071 0.048 16.966

62 55.027 592-76-7 K7 Heptene-1 0.030 0.032 0.026 7.899

63 56.359 4914-89-0 C7 3-Methyl-c-hexene-3 0.014 0.015 0.012 3.823

64 56.88014686-14-7 K7 t-Heptene-3 0.033 0.036 0.028 8.752

65 57.241 6094-02-6 C7 2-Methylhexene-1 0.058 0.064 0.050 15.505

66 57.617 142-82-5 P7 n-Heptane 0.983 1.090 0.829 255.710

67 57.834 7642-10-6 K7 c-Heptene-3 0.024 0.026 0.021 6.362

68 58.112 2738-19-4 C7 2-Methyl-2-hexene 0.027 0.028 0.023 7.104

69 58.354 3899-36-3 C7 3-Methyl-t-hexene-3 0.020 0.022 0.018 5.441

70 58.74214686-13-6 K7 t-Heptene-2 0.014 0.015 0.012 3.722

71 59.19916491-15-9 M7 Cyclopentene, 1,5-dimethyl- 0.019 0.019 0.016 4.931

72 59.64320710-38-8 C7 3-Methyl-t-hexene-2 0.016 0.017 0.014 4.182

73 60.425 4914-91-4 C7 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.014 0.012 3.576

74 61.063 108-87-2 M7 Methylcyclohexane 1.610 1.586 1.385 427.242

75 62.010 4516-69-2 M8 1,1,3-Trimethylcyclopentane 0.045 0.045 0.034 11.895

76 62.414 590-73-8 I8 2,2-Dimethylhexane 0.036 0.039 0.026 9.292

77 63.852 1640-89-7 M7 Ethylcyclopentane 0.058 0.057 0.050 15.280

78 64.502 564-02-3 I8 2,2,3-Trimethylpentane 0.079 0.084 0.059 20.632

79 64.741 592-13-2 I8 2,5-Dimethylhexane 0.197 0.215 0.146 51.360

80 65.079 589-43-5 I8 2,4-Dimethylhexane 0.192 0.208 0.142 50.169

81 65.919 4850-28-6 M8 1c,2t,4-Trimethylcyclopentane 0.045 0.045 0.034 11.970

82 66.322 563-16-6 I8 3,3-Dimethylhexane 0.029 0.031 0.021 7.459

83 67.45015890-40-1 M8 1t,2c,3-Trimethylcyclopentane 0.040 0.039 0.030 10.560

84 68.081 565-75-3 I8 2,3,4-Trimethylpentane 0.815 0.859 0.602 212.324

85 68.691 108-88-3 Q7 Toluene 17.283 15.111 15.847 4886.507

86 70.125 C8 C8 - Diolefin - 1 0.017 0.017 0.013 4.553

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C-223
Hydrocarbon Expert V4.7 Thu Aug 26 13:53:12 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91318 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91318

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 70.421 584-94-1 I8 2,3-Dimethylhexane 0.270 0.287 0.200 70.337

88 71.693 592-27-8 I8 2-Methylheptane 0.332 0.361 0.246 86.538

89 71.947 589-53-7 I8 4-Methylheptane 0.171 0.184 0.126 44.481

90 72.857 M8 1,3-dimethyl-t-cyclohexane 0.269 0.265 0.202 71.384

91 73.016 589-81-1 I8 3-Methylheptane 0.281 0.302 0.208 73.278

92 73.201 619-99-8 I8 3-Ethylhexane 0.163 0.174 0.121 42.581

93 74.097 ? Unidentified 0.043 0.042 0.032 13.913

94 74.917 3522-94-9 I9 2,2,5-Trimethylhexane 0.545 0.584 0.359 142.398

95 75.264 M8 3c-Ethylmethylcyclopentane 0.015 0.015 0.012 4.111

96 75.483 M8 3t-Ethylmethylcyclopentane 0.022 0.022 0.016 5.793

97 76.184 2207-03-6 M8 1t,3-Dimethylcyclohexane 0.124 0.121 0.093 32.920

98 77.562 111-65-9 P8 n-Octane 0.785 0.847 0.581 204.704

99 78.506 ? Unidentified 0.018 0.018 0.014 5.922

100 80.050 1069-53-0 I9 2,3,5-Trimethylhexane 0.103 0.108 0.068 26.782

101 80.613 C8 C9 - IsoOlefin - 1 0.027 0.027 0.021 7.296

102 81.048 2207-01-4 M8 1c,2-Dimethylcyclohexane 0.023 0.022 0.018 6.223

103 81.230 1071-26-7 I9 2,4-Dimethylheptane 0.051 0.055 0.034 13.351

104 81.864 1678-91-7 M8 Ethylcyclohexane 0.197 0.191 0.149 52.401

105 82.191 1072-05-5 I9 2,6-Dimethylheptane 0.097 0.104 0.064 25.415

106 82.669 ? Unidentified 0.041 0.040 0.031 13.439

107 83.128 I9 2,5-Dimethylheptane 0.144 0.152 0.095 37.561

108 83.318 926-82-9 I9 3,5-Dimethylheptane 0.028 0.030 0.019 7.398

109 84.454 100-41-4 Q8 Ethylbenzene 3.147 2.751 2.504 882.957

110 84.863 ? Unidentified 0.028 0.027 0.019 9.026

111 85.710 108-38-3 Q8 m-Xylene 7.983 7.002 6.353 2240.073

112 85.852 106-42-3 Q8 p-Xylene 3.714 3.270 2.956 1042.294

113 86.326 ? Unidentified 0.019 0.018 0.012 6.062

114 86.466 I9 3,5-Dimethylheptane 0.017 0.018 0.011 4.511

115 86.617 1067-20-5 I9 3,3-Diethylpentane 0.014 0.014 0.009 3.578

116 87.016 2216-34-4 I9 4-Methyloctane 0.088 0.093 0.058 23.092

117 87.149 3221-61-2 I9 2-Methyloctane 0.119 0.126 0.078 31.018

118 87.84815869-80-4 I9 Heptane, 3-ethyl- 0.017 0.018 0.011 4.392

119 88.011 2216-33-3 I9 3-Methyloctane 0.116 0.122 0.077 30.351

120 88.481 ? Unidentified 0.035 0.039 0.023 11.275

121 88.664 95-47-6 Q8 o-Xylene 2.286 1.969 1.819 641.414

122 89.064 I10 C10 - IsoParaffin - 1 0.118 0.123 0.070 30.833

123 89.640 M9 trans-1,3-Diethylcyclopentane 0.031 0.027 0.021 8.749

124 89.91414720-74-2 I10 2,2,4-trimethylheptane 0.103 0.107 0.061 26.851

125 91.501 111-84-2 P9 n-Nonane 0.276 0.291 0.182 72.003

126 92.026 4926-90-3 M9 1,1-Methylethylcyclohexane 0.016 0.015 0.011 4.243

127 92.836 98-82-8 Q9 i-Propylbenzene 0.040 0.035 0.028 11.076

128 93.591 ? Unidentified 0.017 0.018 0.010 5.603

129 93.81715869-87-1 I10 2,2-Dimethyloctane 0.011 0.011 0.006 2.807

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C-224
Hydrocarbon Expert V4.7 Thu Aug 26 13:53:12 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91318 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91318

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 94.62715869-89-3 I10 2,5-Dimethyloctane 0.009 0.009 0.005 2.341

131 94.812 I10 C10 - IsoParaffin - 2 0.015 0.015 0.009 3.863

132 95.657 I10 2,6-Dimethyloctane 0.011 0.011 0.007 2.892

133 96.303 103-65-1 Q9 n-Propylbenzene 0.331 0.291 0.232 92.212

134 97.154 620-14-4 Q9 1-Methyl-3-ethylbenzene 1.283 1.125 0.902 357.818

135 97.386 622-96-8 Q9 1-Methyl-4-ethylbenzene 0.597 0.525 0.420 166.416

136 98.013 108-67-8 Q9 1,3,5-Trimethylbenzene 0.762 0.667 0.535 212.349

137 98.49015869-85-9 I10 5-Methylnonane 0.007 0.007 0.004 1.884

138 98.68017301-94-8 I10 4-Methylnonane 0.018 0.018 0.011 4.644

139 98.881 I10 2,2,6-Trimethyloctane 0.162 0.169 0.096 42.483

140 99.097 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.440 0.379 0.309 122.667

141 99.659 5911-04-6 I10 3-Methylnonane 0.023 0.024 0.014 6.009

142 100.250 ? Unidentified 0.041 0.042 0.022 13.256

143 100.473 I11 C11-Isoparaffin-2 0.016 0.017 0.009 4.264

144 100.735 95-63-6 Q9 1,2,4-Trimethylbenzene 2.073 1.794 1.457 577.860

145 100.937 ? Unidentified 0.023 0.024 0.014 7.368

146 101.060 ? Unidentified 0.011 0.012 0.007 3.680

147 102.10517302-01-1 I10 3-Ethyl-3-methylheptane 0.036 0.037 0.020 9.473

148 102.384 538-93-2 Q10 i-Butylbenzene 0.054 0.048 0.034 14.909

149 102.592 124-18-5 P10 n-Decane 0.055 0.057 0.033 14.422

150 102.972 ? Unidentified 0.009 0.010 0.005 3.040

151 103.608 526-73-8 Q9 1,2,3-Trimethylbenzene 0.259 0.219 0.182 72.104

152 104.391 ? Unidentified 0.035 0.035 0.019 11.324

153 104.799 J9 Indan 0.081 0.064 0.058 23.076

154 105.426 J10 Indene 0.241 0.190 0.172 68.367

155 106.145 I11 C11-Isoparaffin-7 0.106 0.108 0.057 27.667

156 106.330 141-93-5 Q10 1,3-Diethylbenzene 0.030 0.026 0.019 8.247

157 106.616 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 0.397 0.350 0.250 110.209

158 106.942 105-05-5 Q10 1,4-Diethylbenzene 0.169 0.149 0.107 46.976

159 107.172 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.131 0.113 0.082 36.330

160 107.433 135-01-3 Q10 1,2-Diethylbenzene 0.030 0.026 0.019 8.401

161 107.885 ? Unidentified 0.027 0.028 0.015 8.893

162 108.023 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.055 0.048 0.035 15.209

163 108.160 ? Unidentified 0.032 0.033 0.017 10.388

164 108.242 ? Unidentified 0.027 0.028 0.015 8.911

165 108.363 ? Unidentified 0.202 0.206 0.109 65.743

166 108.547 ? Unidentified 0.080 0.082 0.043 26.148

167 108.876 1758-88-9 Q10 1,4,Dimethyl-2-ethylbenzene 0.123 0.106 0.077 34.029

168 108.984 ? Unidentified 0.329 0.284 0.207 106.864

169 109.201 J10 2-Methylindan 0.048 0.037 0.030 13.509

170 109.542 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.327 0.283 0.206 90.659

171 110.097 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.231 0.197 0.145 64.083

172 110.526 ? Unidentified 0.007 0.006 0.004 2.163

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C-225
Hydrocarbon Expert V4.7 Thu Aug 26 13:53:12 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91318 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91318

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 110.727 ? Unidentified 0.014 0.014 0.008 4.513

174 110.857 ? Unidentified 0.023 0.024 0.014 7.518

175 111.003 Q11 1-Methyl-4-t-butylbenzene 0.036 0.032 0.021 9.986

176 111.218 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.134 0.114 0.084 37.125

177 111.529 1120-21-4 P11 n-Undecane 0.025 0.026 0.014 6.667

178 111.687 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.031 0.027 0.018 8.663

179 111.796 ? Unidentified 0.015 0.013 0.009 5.035

180 112.162 Q10 1,2,4,5-Tetramethylbenzene 0.268 0.229 0.169 74.447

181 112.428 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.379 0.323 0.239 105.147

182 113.289 ? Unidentified 0.013 0.013 0.006 4.107

183 113.581 Q11 C11 - Aromatic - 3 0.049 0.041 0.028 13.434

184 113.761 874-35-1 H10 5-Methylindan 0.112 0.095 0.071 30.969

185 113.901 Q12 1,2-Di-i-propylbenzene 0.047 0.040 0.024 12.929

186 114.115 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.067 0.057 0.038 18.623

187 114.275 Q11 C11 - Aromatic - 4 0.033 0.028 0.019 9.094

188 114.512 824-22-6 J10 4-Methylindan 0.155 0.132 0.099 42.969

189 114.764 824-63-5 H10 2-Methylindan 0.161 0.137 0.103 44.520

190 114.977 ? Unidentified 0.012 0.012 0.006 3.857

191 115.089 538-68-1 Q11 n-Pentylbenzene 0.017 0.014 0.009 4.567

192 115.321 Q11 tert-Pentylbenzene 0.069 0.059 0.040 19.185

193 115.631 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.031 0.026 0.017 8.461

194 115.741 Q11 C11 - Aromatic - 7 0.040 0.035 0.023 10.964

195 116.204 100-18-5 Q12 1,4-Di-i-propylbenzene 0.055 0.047 0.029 15.267

196 116.630 91-20-3 G10 Naphthalene 0.080 0.059 0.053 23.163

197 117.080 J11 1,1-Dimethyl Indane 0.010 0.008 0.006 2.894

198 117.429 7364-19-4 Q12 1t-Butyl-4-ethylbenzene 0.006 0.005 0.003 1.664

199 117.735 Q12 1,3-Di-n-propylbenzene 0.043 0.037 0.022 11.851

200 117.845 Q11 C11 - Aromatic - 11 0.024 0.021 0.014 6.605

201 118.40017851-27-2 Q11 1-ethyl-2,4,5-trimethylbenzen 0.014 0.012 0.008 3.807

202 123.281 91-57-6 G11 2-Methylnaphthalene 0.010 0.007 0.006 2.742

203 124.147 90-12-0 G11 1-Methylnaphthalene 0.005 0.004 0.003 1.501

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C-226
Hydrocarbon Expert V4.7 Thu Aug 26 13:53:12 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91318 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91318

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 7.389 74-98-6 Propane 0.008 0.012 0.015 1.988

9.791 106-97-8 n-Butane 4.179 5.473 6.075 1071.032

17.700 109-66-0 n-Pentane 2.838 3.435 3.323 732.268

35.320 110-54-3 n-Hexane 3.854 4.431 3.779 998.635

57.617 142-82-5 n-Heptane 0.983 1.090 0.829 255.710

77.562 111-65-9 n-Octane 0.785 0.847 0.581 204.704

91.501 111-84-2 n-Nonane 0.276 0.291 0.182 72.003

102.592 124-18-5 n-Decane 0.055 0.057 0.033 14.422

111.529 1120-21-4 n-Undecane 0.025 0.026 0.014 6.667

I-Paraffins 8.610 75-28-5 i-Butane 0.072 0.099 0.105 18.561

10.387 463-82-1 2,2-Dimethylpropane 0.021 0.027 0.025 5.505

14.710 78-78-4 i-Pentane 4.942 6.046 5.787 1275.307

22.622 75-83-2 2,2-Dimethylbutane 0.187 0.218 0.183 48.371

27.840 79-29-8 2,3-Dimethylbutane 0.550 0.630 0.539 142.540

28.922 107-83-5 2-Methylpentane 2.834 3.289 2.778 734.135

31.564 96-14-0 3-Methylpentane 2.153 2.457 2.111 557.837

41.744 108-08-7 2,4-Dimethylpentane 0.320 0.361 0.270 83.311

42.283 464-06-2 2,2,3-Trimethylbutane 0.046 0.051 0.039 11.990

50.197 591-76-4 2-Methylhexane 1.265 1.413 1.067 329.111

52.032 589-34-4 3-Methylhexane 0.793 0.875 0.669 206.268

54.687 540-84-1 2,2,4-Trimethylpentane 0.065 0.071 0.048 16.966

62.414 590-73-8 2,2-Dimethylhexane 0.036 0.039 0.026 9.292

64.502 564-02-3 2,2,3-Trimethylpentane 0.079 0.084 0.059 20.632

64.741 592-13-2 2,5-Dimethylhexane 0.197 0.215 0.146 51.360

65.079 589-43-5 2,4-Dimethylhexane 0.192 0.208 0.142 50.169

66.322 563-16-6 3,3-Dimethylhexane 0.029 0.031 0.021 7.459

68.081 565-75-3 2,3,4-Trimethylpentane 0.815 0.859 0.602 212.324

70.421 584-94-1 2,3-Dimethylhexane 0.270 0.287 0.200 70.337

71.693 592-27-8 2-Methylheptane 0.332 0.361 0.246 86.538

71.947 589-53-7 4-Methylheptane 0.171 0.184 0.126 44.481

73.016 589-81-1 3-Methylheptane 0.281 0.302 0.208 73.278

73.201 619-99-8 3-Ethylhexane 0.163 0.174 0.121 42.581

74.917 3522-94-9 2,2,5-Trimethylhexane 0.545 0.584 0.359 142.398

80.050 1069-53-0 2,3,5-Trimethylhexane 0.103 0.108 0.068 26.782

81.230 1071-26-7 2,4-Dimethylheptane 0.051 0.055 0.034 13.351

82.191 1072-05-5 2,6-Dimethylheptane 0.097 0.104 0.064 25.415

83.128 2,5-Dimethylheptane 0.144 0.152 0.095 37.561

83.318 926-82-9 3,5-Dimethylheptane 0.028 0.030 0.019 7.398

86.466 3,5-Dimethylheptane 0.017 0.018 0.011 4.511

86.617 1067-20-5 3,3-Diethylpentane 0.014 0.014 0.009 3.578

87.016 2216-34-4 4-Methyloctane 0.088 0.093 0.058 23.092

87.149 3221-61-2 2-Methyloctane 0.119 0.126 0.078 31.018

87.84815869-80-4 Heptane, 3-ethyl- 0.017 0.018 0.011 4.392

88.011 2216-33-3 3-Methyloctane 0.116 0.122 0.077 30.351

89.064 C10 - IsoParaffin - 1 0.118 0.123 0.070 30.833

89.91414720-74-2 2,2,4-trimethylheptane 0.103 0.107 0.061 26.851

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C-227
Hydrocarbon Expert V4.7 Thu Aug 26 13:53:12 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91318 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91318

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

I-Paraffins 93.81715869-87-1 2,2-Dimethyloctane 0.011 0.011 0.006 2.807

94.62715869-89-3 2,5-Dimethyloctane 0.009 0.009 0.005 2.341

94.812 C10 - IsoParaffin - 2 0.015 0.015 0.009 3.863

95.657 2,6-Dimethyloctane 0.011 0.011 0.007 2.892

98.49015869-85-9 5-Methylnonane 0.007 0.007 0.004 1.884

98.68017301-94-8 4-Methylnonane 0.018 0.018 0.011 4.644

98.881 2,2,6-Trimethyloctane 0.162 0.169 0.096 42.483

99.659 5911-04-6 3-Methylnonane 0.023 0.024 0.014 6.009

100.473 C11-Isoparaffin-2 0.016 0.017 0.009 4.264

102.10517302-01-1 3-Ethyl-3-methylheptane 0.036 0.037 0.020 9.473

106.145 C11-Isoparaffin-7 0.106 0.108 0.057 27.667

Aromatics

Mono-Aromatics 45.142 71-42-3 Benzene 0.653 0.563 0.706 186.666

68.691 108-88-3 Toluene 17.283 15.111 15.847 4886.507

84.454 100-41-4 Ethylbenzene 3.147 2.751 2.504 882.957

85.710 108-38-3 m-Xylene 7.983 7.002 6.353 2240.073

85.852 106-42-3 p-Xylene 3.714 3.270 2.956 1042.294

88.664 95-47-6 o-Xylene 2.286 1.969 1.819 641.414

92.836 98-82-8 i-Propylbenzene 0.040 0.035 0.028 11.076

96.303 103-65-1 n-Propylbenzene 0.331 0.291 0.232 92.212

97.154 620-14-4 1-Methyl-3-ethylbenzene 1.283 1.125 0.902 357.818

97.386 622-96-8 1-Methyl-4-ethylbenzene 0.597 0.525 0.420 166.416

98.013 108-67-8 1,3,5-Trimethylbenzene 0.762 0.667 0.535 212.349

99.097 611-14-3 1-Methyl-2-ethylbenzene 0.440 0.379 0.309 122.667

100.735 95-63-6 1,2,4-Trimethylbenzene 2.073 1.794 1.457 577.860

102.384 538-93-2 i-Butylbenzene 0.054 0.048 0.034 14.909

103.608 526-73-8 1,2,3-Trimethylbenzene 0.259 0.219 0.182 72.104

106.330 141-93-5 1,3-Diethylbenzene 0.030 0.026 0.019 8.247

106.616 1074-43-7 1-Methyl-3-n-propylbenzene 0.397 0.350 0.250 110.209

106.942 105-05-5 1,4-Diethylbenzene 0.169 0.149 0.107 46.976

107.172 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.131 0.113 0.082 36.330

107.433 135-01-3 1,2-Diethylbenzene 0.030 0.026 0.019 8.401

108.023 1074-17-5 1-Methyl-2-n-propylbenzene 0.055 0.048 0.035 15.209

108.876 1758-88-9 1,4,Dimethyl-2-ethylbenzene 0.123 0.106 0.077 34.029

109.542 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.327 0.283 0.206 90.659

110.097 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.231 0.197 0.145 64.083

111.003 1-Methyl-4-t-butylbenzene 0.036 0.032 0.021 9.986

111.218 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.134 0.114 0.084 37.125

111.687 4218-48-8 1-Ethyl-4-i-propylbenzene 0.031 0.027 0.018 8.663

112.162 1,2,4,5-Tetramethylbenzene 0.268 0.229 0.169 74.447

112.428 527-53-7 1,2,3,5-Tetramethylbenzene 0.379 0.323 0.239 105.147

113.581 C11 - Aromatic - 3 0.049 0.041 0.028 13.434

113.901 1,2-Di-i-propylbenzene 0.047 0.040 0.024 12.929

114.115 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.067 0.057 0.038 18.623

114.275 C11 - Aromatic - 4 0.033 0.028 0.019 9.094

115.089 538-68-1 n-Pentylbenzene 0.017 0.014 0.009 4.567

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C-228
Hydrocarbon Expert V4.7 Thu Aug 26 13:53:12 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91318 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91318

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 115.321 tert-Pentylbenzene 0.069 0.059 0.040 19.185

115.631 577-55-9 1-Methyl-2-n-butylbenzene 0.031 0.026 0.017 8.461

115.741 C11 - Aromatic - 7 0.040 0.035 0.023 10.964

116.204 100-18-5 1,4-Di-i-propylbenzene 0.055 0.047 0.029 15.267

117.429 7364-19-4 1t-Butyl-4-ethylbenzene 0.006 0.005 0.003 1.664

117.735 1,3-Di-n-propylbenzene 0.043 0.037 0.022 11.851

117.845 C11 - Aromatic - 11 0.024 0.021 0.014 6.605

118.40017851-27-2 1-ethyl-2,4,5-trimethylbenzen 0.014 0.012 0.008 3.807

Naphthalenes 116.630 91-20-3 Naphthalene 0.080 0.059 0.053 23.163

123.281 91-57-6 2-Methylnaphthalene 0.010 0.007 0.006 2.742

124.147 90-12-0 1-Methylnaphthalene 0.005 0.004 0.003 1.501

Naphtheno/Olefino-Benzs 113.761 874-35-1 5-Methylindan 0.112 0.095 0.071 30.969

114.764 824-63-5 2-Methylindan 0.161 0.137 0.103 44.520

Indenes 104.799 Indan 0.081 0.064 0.058 23.076

105.426 Indene 0.241 0.190 0.172 68.367

109.201 2-Methylindan 0.048 0.037 0.030 13.509

114.512 824-22-6 4-Methylindan 0.155 0.132 0.099 42.969

117.080 1,1-Dimethyl Indane 0.010 0.008 0.006 2.894

Naphthenes

Mono-Naphthenes 27.110 287-92-3 Cyclopentane 0.284 0.289 0.342 75.365

40.172 96-37-7 Methylcyclopentane 2.055 2.081 2.063 545.518

47.066 110-82-7 Cyclohexane 1.559 1.519 1.565 413.927

52.883 1759-58-6 1t,3-Dimethylcyclopentane 0.223 0.225 0.191 59.064

53.470 2532-58-3 1c,3-Dimethylcyclopentane 0.179 0.183 0.154 47.601

54.096 822-50-4 1t,2-Dimethylcyclopentane 0.273 0.276 0.235 72.579

59.19916491-15-9 Cyclopentene, 1,5-dimethyl- 0.019 0.019 0.016 4.931

61.063 108-87-2 Methylcyclohexane 1.610 1.586 1.385 427.242

62.010 4516-69-2 1,1,3-Trimethylcyclopentane 0.045 0.045 0.034 11.895

63.852 1640-89-7 Ethylcyclopentane 0.058 0.057 0.050 15.280

65.919 4850-28-6 1c,2t,4-Trimethylcyclopentane 0.045 0.045 0.034 11.970

67.45015890-40-1 1t,2c,3-Trimethylcyclopentane 0.040 0.039 0.030 10.560

72.857 1,3-dimethyl-t-cyclohexane 0.269 0.265 0.202 71.384

75.264 3c-Ethylmethylcyclopentane 0.015 0.015 0.012 4.111

75.483 3t-Ethylmethylcyclopentane 0.022 0.022 0.016 5.793

76.184 2207-03-6 1t,3-Dimethylcyclohexane 0.124 0.121 0.093 32.920

81.048 2207-01-4 1c,2-Dimethylcyclohexane 0.023 0.022 0.018 6.223

81.864 1678-91-7 Ethylcyclohexane 0.197 0.191 0.149 52.401

89.640 trans-1,3-Diethylcyclopentane 0.031 0.027 0.021 8.749

92.026 4926-90-3 1,1-Methylethylcyclohexane 0.016 0.015 0.011 4.243

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.403 115-11-7 Isobutene 0.015 0.020 0.023 4.088

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C-229
Hydrocarbon Expert V4.7 Thu Aug 26 13:53:12 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91318 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91318

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

n-Olefins 9.443 106-98-9 Butene-1 0.019 0.024 0.028 4.985

10.265 624-64-6 t-Butene-2 0.073 0.092 0.110 19.366

10.986 590-18-1 c-Butene-2 0.087 0.106 0.130 22.981

16.334 109-67-1 Pentene-1 0.334 0.395 0.402 88.578

18.803 646-04-8 t-Pentene-2 0.847 0.991 1.021 224.950

19.825 627-20-3 c-Pentene-2 0.465 0.538 0.560 123.392

32.953 592-41-6 Hexene-1 0.162 0.181 0.163 43.077

35.94713269-52-8 t-Hexene-3 0.266 0.295 0.267 70.539

36.422 4050-45-7 t-Hexene-2 0.511 0.567 0.512 135.510

38.250 7688-21-3 c-Hexene-2 0.216 0.237 0.217 57.376

55.027 592-76-7 Heptene-1 0.030 0.032 0.026 7.899

56.88014686-14-7 t-Heptene-3 0.033 0.036 0.028 8.752

57.834 7642-10-6 c-Heptene-3 0.024 0.026 0.021 6.362

58.74214686-13-6 t-Heptene-2 0.014 0.015 0.012 3.722

Iso-Olefins 13.125 563-45-1 3-Methylbutene-1 0.329 0.398 0.397 87.383

17.172 563-46-2 2-Methylbutene-1 0.507 0.591 0.610 134.487

20.494 513-35-9 2-Methylbutene-2 1.041 1.192 1.255 276.421

28.701 691-38-3 4-Methyl-c-pentene-2 0.045 0.050 0.045 11.856

29.350 674-76-0 4-Methyl-t-pentene-2 0.132 0.149 0.133 35.035

32.730 763-29-1 2-Methylpentene-1 0.226 0.250 0.227 59.949

36.913 625-27-4 2-Methylpentene-2 0.346 0.379 0.347 91.750

37.324 922-62-3 3-Methyl-c-pentene-2 0.268 0.291 0.269 71.051

39.598 3404-73-7 3,3-Dimethylpentene-1 0.317 0.342 0.273 84.077

42.044 594-56-9 2,3,3-Trimethylbutene-1 0.014 0.015 0.012 3.834

46.168 3404-61-3 3-Methylhexene-1 0.016 0.018 0.014 4.337

46.750 3524-73-0 5-Methylhexene-1 0.082 0.089 0.070 21.674

48.80915840-60-5 2-Methyl-c-hexene-3 0.041 0.045 0.036 10.972

49.804 3404-55-5 4-Methyl-t/c-hexene-2 0.052 0.056 0.045 13.774

54.393 C7 - Iso-Olefin - 2 0.023 0.024 0.019 5.981

56.359 4914-89-0 3-Methyl-c-hexene-3 0.014 0.015 0.012 3.823

57.241 6094-02-6 2-Methylhexene-1 0.058 0.064 0.050 15.505

58.112 2738-19-4 2-Methyl-2-hexene 0.027 0.028 0.023 7.104

58.354 3899-36-3 3-Methyl-t-hexene-3 0.020 0.022 0.018 5.441

59.64320710-38-8 3-Methyl-t-hexene-2 0.016 0.017 0.014 4.182

60.425 4914-91-4 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.014 0.012 3.576

70.125 C8 - Diolefin - 1 0.017 0.017 0.013 4.553

80.613 C9 - IsoOlefin - 1 0.027 0.027 0.021 7.296

Naphtheno-Olefins 25.256 142-29-0 Cyclopentene 0.198 0.195 0.246 54.138

45.346 693-89-0 1-Methylcyclopentene 0.370 0.360 0.381 100.625

50.673 110-83-8 Cyclohexene 0.045 0.043 0.047 12.073

Di-Olefins 18.208 78-79-5 2-Methyl-1,3-Butadiene 0.010 0.012 0.013 2.859

20.825 2004-70-8 1t,3-Pentadiene 0.016 0.017 0.019 4.254

Oxygenates 12.742 64-17-5 Ethanol 8.719 8.377 15.990 994.782

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C-230
Hydrocarbon Expert V4.7 Thu Aug 26 13:53:12 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91318 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91318

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Oxygenates 26.501 71-23-8 n-Propanol 0.182 0.172 0.255 33.724

Unidentified 19.442 Unidentified 0.006 0.007 0.007 1.857

22.078 Unidentified 0.006 0.006 0.008 1.924

28.242 Unidentified 0.051 0.052 0.049 16.633

44.940 Unidentified 0.012 0.012 0.012 3.942

47.602 Unidentified 0.035 0.038 0.030 11.476

74.097 Unidentified 0.043 0.042 0.032 13.913

78.506 Unidentified 0.018 0.018 0.014 5.922

82.669 Unidentified 0.041 0.040 0.031 13.439

84.863 Unidentified 0.028 0.027 0.019 9.026

86.326 Unidentified 0.019 0.018 0.012 6.062

88.481 Unidentified 0.035 0.039 0.023 11.275

93.591 Unidentified 0.017 0.018 0.010 5.603

100.250 Unidentified 0.041 0.042 0.022 13.256

100.937 Unidentified 0.023 0.024 0.014 7.368

101.060 Unidentified 0.011 0.012 0.007 3.680

102.972 Unidentified 0.009 0.010 0.005 3.040

104.391 Unidentified 0.035 0.035 0.019 11.324

107.885 Unidentified 0.027 0.028 0.015 8.893

108.160 Unidentified 0.032 0.033 0.017 10.388

108.242 Unidentified 0.027 0.028 0.015 8.911

108.363 Unidentified 0.202 0.206 0.109 65.743

108.547 Unidentified 0.080 0.082 0.043 26.148

108.984 Unidentified 0.329 0.284 0.207 106.864

110.526 Unidentified 0.007 0.006 0.004 2.163

110.727 Unidentified 0.014 0.014 0.008 4.513

110.857 Unidentified 0.023 0.024 0.014 7.518

111.796 Unidentified 0.015 0.013 0.009 5.035

113.289 Unidentified 0.013 0.013 0.006 4.107

114.977 Unidentified 0.012 0.012 0.006 3.857

Plus

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C-231
Hydrocarbon Expert V4.7 Thu Aug 26 13:53:12 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91318 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91318

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF

20.0 15.0 10.0 5.0 0.0

Propane

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

Ethanol

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

Unidentified

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

Unidentified

2,2-Dimethylbutane

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C-232
Hydrocarbon Expert V4.7 Thu Aug 26 13:53:12 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91318 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91318

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

n-Propanol

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

n-Hexane

t-Hexene-3

t-Hexene-2

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane 2,3,3-Trimethylbutene-1 2,2,3-Trimethylbutane

Unidentified Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1 Cyclohexane

Unidentified

2-Methyl-c-hexene-3

4-Methyl-t/c-hexene-2

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C-233
Hydrocarbon Expert V4.7 Thu Aug 26 13:53:12 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91318 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91318

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF

70.0 65.0 60.0 55.0 50.0

2-Methylhexane

Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane C7 - Iso-Olefin - 2 2,2,4-Trimethylpentane

Heptene-1

3-Methyl-c-hexene-3

t-Heptene-3

2-Methylhexene-1

n-Heptane c-Heptene-3 2-Methyl-2-hexene 3-Methyl-t-hexene-3

t-Heptene-2

Cyclopentene, 1,5-dimethyl3-Methyl-t-hexene-2

2-Pentene, 3,4-dimethyl-, (Z)-

Methylcyclohexane

1,1,3-Trimethylcyclopentane

2,2-Dimethylhexane

Ethylcyclopentane

2,2,3-Trimethylpentane 2,5-Dimethylhexane

2,4-Dimethylhexane

1c,2t,4-Trimethylcyclopentane

3,3-Dimethylhexane

1t,2c,3-Trimethylcyclopentane

2,3,4-Trimethylpentane

Toluene

C8 - Diolefin - 1 2,3-Dimethylhexane

2-Methylheptane 4-Methylheptane

1,3-dimethyl-t-cyclohexane 3-Methylheptane 3-Ethylhexane

Unidentified

2,2,5-Trimethylhexane

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C-234
Hydrocarbon Expert V4.7 Thu Aug 26 13:53:12 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91318 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91318

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF

95.0 90.0 85.0 80.0 75.0

3c-Ethylmethylcyclopentane 3t-Ethylmethylcyclopentane

1t,3-Dimethylcyclohexane

n-Octane

Unidentified

2,3,5-Trimethylhexane

C9 - IsoOlefin - 1

1c,2-Dimethylcyclohexane 2,4-Dimethylheptane

Ethylcyclohexane

2,6-Dimethylheptane

Unidentified

2,5-Dimethylheptane 3,5-Dimethylheptane

Ethylbenzene

Unidentified

m-Xylene p-Xylene

Unidentified 3,5-Dimethylheptane 3,3-Diethylpentane

4-Methyloctane 2-Methyloctane

Heptane, 3-ethyl- 3-Methyloctane

Unidentified o-Xylene

C10 - IsoParaffin - 1

trans-1,3-Diethylcyclopentane 2,2,4-trimethylheptane

n-Nonane

1,1-Methylethylcyclohexane

i-Propylbenzene

Unidentified 2,2-Dimethyloctane

2,5-Dimethyloctane C10 - IsoParaffin - 2

2,6-Dimethyloctane

n-Propylbenzene

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

5-Methylnonane 4-Methylnonane 2,2,6-Trimethyloctane 1-Methyl-2-ethylbenzene

3-Methylnonane

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C-235
Hydrocarbon Expert V4.7 Thu Aug 26 13:53:12 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91318 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91318

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified C11-Isoparaffin-2 1,2,4-Trimethylbenzene Unidentified

3-Ethyl-3-methylheptane i-Butylbenzene n-Decane

Unidentified

1,2,3-Trimethylbenzene

Unidentified

Indan

Indene

C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene

1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

Unidentified 1-Methyl-2-n-propylbenzene

Unidentified Unidentified

1,4,Dimethyl-2-ethylbenzene Unidentified 2-Methylindan

1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

Unidentified

1-Methyl-4-t-butylbenzene 1,2-Dimethyl-3-ethylbenzene

n-Undecane Unidentified 1-Ethyl-4-i-propylbenzene

1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene

Unidentified C11 - Aromatic - 3 5-Methylindan 1,2-Di-i-propylbenzene 1-methyl-4-(1-methylpropyl)be C11 - Aromatic - 4 4-Methylindan 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene 1-Methyl-2-n-butylbenzene C11 - Aromatic - 7

1,4-Di-i-propylbenzene

Naphthalene

1,1-Dimethyl Indane

1t-Butyl-4-ethylbenzene

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

1-ethyl-2,4,5-trimethylbenzen

2-Methylnaphthalene

1-Methylnaphthalene

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C-236
Hydrocarbon Expert V4.7 Thu Aug 26 13:53:12 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91318 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91318

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000014.D\SIG1000014_FID1_A.CDF

145.0 140.0 135.0 130.0 125.0

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C-237
Hydrocarbon Expert V4.7 Thu Aug 26 13:59:05 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91319 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91319

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 3.414 4.204 4.355

I-Paraffins 32.566 37.842 34.129

Aromatics 45.272 38.847 34.931

Mono-Aromatics 42.987 37.004 33.407

Naphthalenes 0.232 0.170 0.154

Naphtheno/Olefino-Benzs 0.716 0.603 0.462

Indenes 1.336 1.071 0.908

Naphthenes 1.386 1.385 1.418

Mono-Naphthenes 1.386 1.385 1.418

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 7.518 8.347 8.389

n-Olefins 3.187 3.614 3.642

Iso-Olefins 3.676 4.100 4.018

Naphtheno-Olefins 0.628 0.604 0.696

Di-Olefins 0.026 0.029 0.033

Oxygenates 8.732 8.292 16.092

Unidentified 1.112 1.083 0.684

Plus 0.000 0.000 0.000

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C-238
Hydrocarbon Expert V4.7 Thu Aug 26 13:59:05 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91319 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91319

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C2 8.547 8.118 15.829

C3 0.186 0.174 0.264

C4 2.115 2.727 3.115

C5 17.135 20.403 20.410

C6 23.265 26.011 23.201

C7 12.808 11.495 11.727

C8 11.687 10.125 9.388

C9 11.137 9.554 7.909

C10 9.362 7.949 5.994

C11 2.102 1.901 1.191

C12 0.546 0.462 0.288

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C-239
Hydrocarbon Expert V4.7 Thu Aug 26 13:59:05 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91319 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91319

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C4 1.890 2.448 2.775

C5 0.819 0.981 0.969

C6 0.426 0.484 0.422

C7 0.095 0.104 0.081

C8 0.018 0.019 0.013

C10 0.099 0.102 0.060

C11 0.066 0.066 0.036

I-Paraffins C4 0.029 0.039 0.043

C5 12.234 14.800 14.467

C6 18.582 21.182 18.398

C7 0.882 0.972 0.751

C8 0.047 0.050 0.035

C10 0.129 0.131 0.074

C11 0.644 0.649 0.351

C12 0.019 0.019 0.010

Mono-Aromatics C6 0.707 0.603 0.773

C7 10.784 9.322 9.986

C8 11.622 10.056 9.340

C9 10.885 9.357 7.727

C10 7.203 6.147 4.579

C11 1.283 1.094 0.738

C12 0.504 0.424 0.265

Naphthalenes C10 0.218 0.159 0.145

C11 0.014 0.011 0.009

Naphtheno/Olefino-Benzs C10 0.716 0.603 0.462

Indenes C9 0.252 0.196 0.182

C10 0.997 0.807 0.675

C11 0.064 0.050 0.037

C12 0.023 0.018 0.014

Mono-Naphthenes C5 0.270 0.272 0.329

C6 0.829 0.827 0.840

C7 0.287 0.286 0.249

n-Olefins C4 0.195 0.240 0.297

C5 1.675 1.935 2.037

C6 1.184 1.298 1.200

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C-240
Hydrocarbon Expert V4.7 Thu Aug 26 13:59:05 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91319 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91319

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

n-Olefins C7 0.102 0.109 0.089

C11 0.032 0.032 0.019

Iso-Olefins C5 1.908 2.190 2.321

C6 1.110 1.208 1.126

C7 0.658 0.702 0.572

Naphtheno-Olefins C5 0.202 0.196 0.253

C6 0.426 0.408 0.442

Di-Olefins C5 0.026 0.029 0.033

Oxygenates C2 8.547 8.118 15.829

C3 0.186 0.174 0.264

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C-241
Hydrocarbon Expert V4.7 Thu Aug 26 13:59:05 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91319 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91319

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 23.07 22.44

5% 79.42 79.17

10% 80.75 80.26

15% 83.61 81.36

20% 133.76 96.69

25% 138.48 135.45

30% 139.95 138.57

35% 144.73 139.85

40% 154.11 144.40

45% 172.56 145.94

50% 173.20 172.35

55% 216.24 173.01

60% 224.33 214.14

65% 264.63 223.50

70% 281.36 266.81

75% 286.57 281.60

80% 325.06 320.98

85% 336.00 334.33

90% 362.58 355.82

95% 380.31 374.05

FBP 407.09 404.60

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C-242
Hydrocarbon Expert V4.7 Thu Aug 26 13:59:05 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91319 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91319

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 8.618 75-28-5 I4 i-Butane 0.029 0.039 0.043 7.802

2 9.412 115-11-7 K4 Isobutene 0.016 0.020 0.024 4.346

3 9.452 106-98-9 K4 Butene-1 0.019 0.024 0.029 5.219

4 9.801 106-97-8 P4 n-Butane 1.890 2.448 2.775 506.033

5 10.277 624-64-6 K4 t-Butene-2 0.074 0.091 0.112 20.424

6 10.399 463-82-1 I5 2,2-Dimethylpropane 0.029 0.036 0.034 7.749

7 11.000 590-18-1 K4 c-Butene-2 0.087 0.105 0.133 24.178

8 12.764 64-17-5 X2 Ethanol 8.547 8.118 15.829 1018.567

9 13.145 563-45-1 C5 3-Methylbutene-1 0.331 0.396 0.403 91.846

10 14.745 78-78-4 I5 i-Pentane 12.205 14.763 14.433 3290.084

11 16.360 109-67-1 K5 Pentene-1 0.339 0.397 0.412 93.993

12 17.198 563-46-2 C5 2-Methylbutene-1 0.515 0.593 0.627 142.805

13 17.722 109-66-0 P5 n-Pentane 0.819 0.981 0.969 220.865

14 18.234 78-79-5 E5 2-Methyl-1,3-Butadiene 0.011 0.012 0.013 3.049

15 18.830 646-04-8 K5 t-Pentene-2 0.862 0.997 1.049 239.110

16 19.469 ? Unidentified 0.006 0.007 0.007 1.974

17 19.852 627-20-3 K5 c-Pentene-2 0.473 0.541 0.576 131.228

18 20.523 513-35-9 C5 2-Methylbutene-2 1.061 1.201 1.291 294.302

19 20.853 2004-70-8 E5 1t,3-Pentadiene 0.016 0.018 0.020 4.514

20 22.104 ? Unidentified 0.006 0.006 0.008 2.024

21 22.649 75-83-2 I6 2,2-Dimethylbutane 0.322 0.371 0.318 87.037

22 25.284 142-29-0 B5 Cyclopentene 0.202 0.196 0.253 57.731

23 26.530 71-23-8 X3 n-Propanol 0.186 0.174 0.264 36.052

24 27.137 287-92-3 M5 Cyclopentane 0.270 0.272 0.329 74.922

25 27.871 79-29-8 I6 2,3-Dimethylbutane 1.591 1.803 1.575 430.647

26 28.273 ? Unidentified 0.053 0.053 0.051 17.943

27 28.738 691-38-3 C6 4-Methyl-c-pentene-2 0.043 0.048 0.044 12.008

28 28.992 107-83-5 I6 2-Methylpentane 10.430 11.969 10.327 2822.785

29 29.383 674-76-0 C6 4-Methyl-t-pentene-2 0.136 0.151 0.137 37.578

30 31.616 96-14-0 I6 3-Methylpentane 6.239 7.039 6.177 1688.612

31 32.755 763-29-1 C6 2-Methylpentene-1 0.232 0.254 0.235 64.237

32 32.979 592-41-6 K6 Hexene-1 0.166 0.184 0.168 46.069

33 35.165 760-21-4 C6 2-Ethylbutene-1 0.071 0.077 0.072 19.694

34 35.323 110-54-3 P6 n-Hexane 0.426 0.484 0.422 115.358

35 35.96713269-52-8 K6 t-Hexene-3 0.273 0.300 0.276 75.589

36 36.441 4050-45-7 K6 t-Hexene-2 0.523 0.574 0.530 145.033

37 36.933 625-27-4 C6 2-Methylpentene-2 0.354 0.384 0.359 98.249

38 37.344 922-62-3 C6 3-Methyl-c-pentene-2 0.274 0.295 0.278 76.109

39 38.268 7688-21-3 K6 c-Hexene-2 0.222 0.240 0.225 61.522

40 39.613 3404-73-7 C7 3,3-Dimethylpentene-1 0.325 0.348 0.283 90.243

41 40.181 96-37-7 M6 Methylcyclopentane 0.763 0.764 0.774 211.574

42 41.768 108-08-7 I7 2,4-Dimethylpentane 0.152 0.169 0.129 41.289

43 42.062 594-56-9 C7 2,3,3-Trimethylbutene-1 0.011 0.011 0.009 2.930

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C-243
Hydrocarbon Expert V4.7 Thu Aug 26 13:59:05 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91319 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91319

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 44.952 ? Unidentified 0.012 0.012 0.013 4.227

45 45.154 71-42-3 Q6 Benzene 0.707 0.603 0.773 211.249

46 45.357 693-89-0 B6 1-Methylcyclopentene 0.379 0.365 0.394 107.702

47 46.176 3404-61-3 C7 3-Methylhexene-1 0.017 0.018 0.014 4.587

48 46.760 3524-73-0 C7 5-Methylhexene-1 0.023 0.025 0.020 6.502

49 47.068 110-82-7 M6 Cyclohexane 0.066 0.063 0.067 18.243

50 47.610 ? Unidentified 0.036 0.038 0.031 12.157

51 48.81515840-60-5 C7 2-Methyl-c-hexene-3 0.042 0.045 0.037 11.660

52 49.160 3769-23-1 C7 4-Methylhexene-1 0.012 0.013 0.011 3.352

53 49.807 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.053 0.056 0.046 14.686

54 50.198 591-76-4 I7 2-Methylhexane 0.444 0.491 0.378 120.723

55 50.676 110-83-8 B6 Cyclohexene 0.046 0.043 0.048 12.859

56 52.032 589-34-4 I7 3-Methylhexane 0.286 0.312 0.243 77.645

57 52.884 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.100 0.100 0.087 27.704

58 53.472 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.067 0.067 0.058 18.498

59 54.098 822-50-4 M7 1t,2-Dimethylcyclopentane 0.059 0.059 0.052 16.442

60 54.396 C7 C7 - Iso-Olefin - 2 0.023 0.024 0.020 6.406

61 55.024 592-76-7 K7 Heptene-1 0.028 0.030 0.024 7.779

62 56.358 4914-89-0 C7 3-Methyl-c-hexene-3 0.014 0.015 0.013 4.011

63 56.87914686-14-7 K7 t-Heptene-3 0.034 0.036 0.029 9.321

64 57.237 6094-02-6 C7 2-Methylhexene-1 0.060 0.064 0.052 16.594

65 57.610 142-82-5 P7 n-Heptane 0.095 0.104 0.081 25.819

66 57.830 7642-10-6 K7 c-Heptene-3 0.027 0.029 0.023 7.450

67 58.109 2738-19-4 C7 2-Methyl-2-hexene 0.027 0.028 0.024 7.502

68 58.353 3899-36-3 C7 3-Methyl-t-hexene-3 0.021 0.022 0.018 5.726

69 58.73714686-13-6 K7 t-Heptene-2 0.014 0.014 0.012 3.753

70 59.19616491-15-9 M7 Cyclopentene, 1,5-dimethyl- 0.019 0.019 0.016 5.253

71 59.63720710-38-8 C7 3-Methyl-t-hexene-2 0.016 0.017 0.014 4.475

72 60.423 4914-91-4 C7 2-Pentene, 3,4-dimethyl-, (Z)- 0.014 0.014 0.012 3.778

73 61.035 108-87-2 M7 Methylcyclohexane 0.042 0.041 0.037 11.658

74 68.651 108-88-3 Q7 Toluene 10.784 9.322 9.986 3184.956

75 71.685 592-27-8 I8 2-Methylheptane 0.017 0.018 0.013 4.680

76 71.938 589-53-7 I8 4-Methylheptane 0.010 0.010 0.007 2.625

77 73.011 589-81-1 I8 3-Methylheptane 0.020 0.021 0.015 5.419

78 77.555 111-65-9 P8 n-Octane 0.018 0.019 0.013 4.885

79 84.445 100-41-4 Q8 Ethylbenzene 2.185 1.889 1.756 640.555

80 85.692 108-38-3 Q8 m-Xylene 5.346 4.637 4.297 1567.149

81 85.836 106-42-3 Q8 p-Xylene 2.512 2.187 2.019 736.435

82 88.657 95-47-6 Q8 o-Xylene 1.578 1.343 1.268 462.494

83 92.836 98-82-8 Q9 i-Propylbenzene 0.039 0.034 0.028 11.462

84 95.265 2051-30-1 I10 2,4-Dimethyloctane 0.008 0.008 0.005 2.089

85 96.305 103-65-1 Q9 n-Propylbenzene 0.490 0.426 0.348 142.603

86 97.164 620-14-4 Q9 1-Methyl-3-ethylbenzene 2.108 1.827 1.496 613.883

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C-244
Hydrocarbon Expert V4.7 Thu Aug 26 13:59:05 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91319 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91319

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 97.394 622-96-8 Q9 1-Methyl-4-ethylbenzene 1.013 0.882 0.719 295.144

88 98.022 108-67-8 Q9 1,3,5-Trimethylbenzene 1.391 1.205 0.988 405.233

89 98.49615869-85-9 I10 5-Methylnonane 0.007 0.007 0.004 1.941

90 98.68517301-94-8 I10 4-Methylnonane 0.018 0.018 0.011 4.889

91 98.885 ? Unidentified 0.212 0.219 0.127 72.155

92 99.102 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.819 0.697 0.582 238.610

93 99.663 5911-04-6 I10 3-Methylnonane 0.035 0.036 0.021 9.549

94 100.128 ? Unidentified 0.018 0.013 0.010 5.995

95 100.255 ? Unidentified 0.053 0.053 0.029 17.901

96 100.476 I11 C11-Isoparaffin-2 0.029 0.029 0.016 8.000

97 100.757 95-63-6 Q9 1,2,4-Trimethylbenzene 4.265 3.650 3.028 1242.251

98 100.941 ? Unidentified 0.038 0.041 0.023 12.875

99 101.062 ? Unidentified 0.021 0.022 0.013 7.243

100 102.10717302-01-1 I10 3-Ethyl-3-methylheptane 0.062 0.062 0.034 16.838

101 102.384 538-93-2 Q10 i-Butylbenzene 0.119 0.105 0.076 34.516

102 102.662 124-18-5 P10 n-Decane 0.099 0.102 0.060 27.135

103 102.973 ? Unidentified 0.016 0.017 0.010 5.594

104 103.614 526-73-8 Q9 1,2,3-Trimethylbenzene 0.758 0.635 0.538 220.858

105 104.011 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.022 0.019 0.014 6.377

106 104.192 I11 C11 Isoparaffin-4 0.011 0.011 0.006 2.959

107 104.393 ? Unidentified 0.062 0.054 0.039 20.934

108 104.802 J9 Indan 0.252 0.196 0.182 74.684

109 105.430 J10 Indene 0.411 0.319 0.297 121.557

110 106.149 I11 C11-Isoparaffin-7 0.184 0.185 0.100 50.221

111 106.333 141-93-5 Q10 1,3-Diethylbenzene 0.121 0.105 0.077 35.120

112 106.612 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 0.847 0.737 0.538 245.270

113 106.952 105-05-5 Q10 1,4-Diethylbenzene 0.352 0.306 0.224 101.935

114 107.049 104-51-8 Q10 n-Butylbenzene 0.077 0.067 0.049 22.398

115 107.176 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.417 0.355 0.265 120.839

116 107.449 135-01-3 Q10 1,2-Diethylbenzene 0.059 0.050 0.037 17.075

117 107.888 ? Unidentified 0.046 0.046 0.025 15.665

118 108.025 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.156 0.134 0.099 45.234

119 108.163 ? Unidentified 0.054 0.055 0.030 18.347

120 108.244 ? Unidentified 0.048 0.048 0.026 16.228

121 108.366 I11 C11- Isoparaffin-11 0.420 0.423 0.229 114.992

122 108.551 ? Unidentified 0.136 0.137 0.074 46.154

123 108.880 1758-88-9 Q10 1,4,Dimethyl-2-ethylbenzene 0.385 0.329 0.245 111.500

124 109.036 874-41-9 Q10 1,3-Dimethyl-4-ethylbenzene 0.830 0.709 0.528 240.423

125 109.201 J10 2-Methylindan 0.093 0.072 0.060 27.469

126 109.549 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.975 0.836 0.620 282.584

127 110.099 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.412 0.347 0.262 119.420

128 110.528 ? Unidentified 0.011 0.010 0.006 3.669

129 110.729 693-61-8 K11 2-Undecene, (E)- 0.032 0.032 0.019 8.655

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C-245
Hydrocarbon Expert V4.7 Thu Aug 26 13:59:05 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91319 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91319

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 110.859 ? Unidentified 0.039 0.039 0.024 13.207

131 111.010 Q11 1-Methyl-4-t-butylbenzene 0.099 0.088 0.057 28.659

132 111.223 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.370 0.311 0.235 107.190

133 111.533 1120-21-4 P11 n-Undecane 0.066 0.066 0.036 17.952

134 111.691 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.070 0.059 0.041 20.330

135 111.799 ? Unidentified 0.029 0.025 0.017 9.917

136 111.904 Q11 C11 - Aromatic - 1 0.016 0.014 0.009 4.647

137 112.169 Q10 1,2,4,5-Tetramethylbenzene 0.867 0.732 0.551 251.079

138 112.438 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 1.193 1.004 0.758 345.596

139 112.624 ? Unidentified 0.010 0.008 0.006 3.329

140 112.796 ? Unidentified 0.011 0.009 0.007 3.813

141 112.967 I12 C12 - IsoParaffin - 1 0.012 0.012 0.006 3.388

142 113.291 ? Unidentified 0.031 0.032 0.016 10.619

143 113.583 Q11 C11 - Aromatic - 3 0.153 0.129 0.088 44.075

144 113.766 874-35-1 H10 5-Methylindan 0.350 0.295 0.226 101.485

145 113.904 Q12 1,2-Di-i-propylbenzene 0.152 0.128 0.080 43.793

146 114.119 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.217 0.183 0.125 62.662

147 114.278 Q11 C11 - Aromatic - 4 0.105 0.088 0.060 30.286

148 114.517 824-22-6 J10 4-Methylindan 0.493 0.415 0.318 142.830

149 114.680 ? Unidentified 0.115 0.097 0.066 38.983

150 114.768 824-63-5 H10 2-Methylindan 0.366 0.308 0.236 106.043

151 114.979 ? Unidentified 0.038 0.032 0.022 12.859

152 115.091 538-68-1 Q11 n-Pentylbenzene 0.053 0.045 0.031 15.365

153 115.322 Q11 tert-Pentylbenzene 0.224 0.188 0.129 64.488

154 115.634 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.099 0.083 0.057 28.520

155 115.743 Q11 C11 - Aromatic - 7 0.125 0.110 0.072 36.010

156 116.073 I12 C12 - IsoParaffin - 4 0.007 0.007 0.003 1.960

157 116.206 100-18-5 Q12 1,4-Di-i-propylbenzene 0.185 0.156 0.097 53.144

158 116.633 91-20-3 G10 Naphthalene 0.218 0.159 0.145 66.044

159 116.843 J11 4,7-Dimethyl Indane 0.012 0.009 0.007 3.597

160 117.081 J11 1,1-Dimethyl Indane 0.052 0.040 0.030 15.309

161 117.250 J12 Dimethyl Indane - 1 0.018 0.014 0.011 5.350

162 117.431 7364-19-4 Q12 1t-Butyl-4-ethylbenzene 0.026 0.022 0.014 7.479

163 117.565 J12 Dimethyl Indane - 2 0.005 0.004 0.003 1.557

164 117.735 Q12 1,3-Di-n-propylbenzene 0.135 0.113 0.071 38.715

165 117.847 Q11 C11 - Aromatic - 11 0.074 0.065 0.043 21.340

166 118.402 Q11 C11 - Aromatic - 12 0.042 0.037 0.024 12.031

167 119.030 Q11 C11 - Aromatic - 13 0.006 0.005 0.003 1.606

168 119.340 102-25-0 Q12 1,3,5-Triethylbenzene 0.006 0.005 0.003 1.696

169 123.282 91-57-6 G11 2-Methylnaphthalene 0.009 0.007 0.006 2.828

170 124.147 90-12-0 G11 1-Methylnaphthalene 0.005 0.004 0.003 1.515

171 125.443 ? Unidentified 0.004 0.003 0.002 1.502

172 129.864 ? Unidentified 0.003 0.002 0.002 1.017

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C-246
Hydrocarbon Expert V4.7 Thu Aug 26 13:59:05 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91319 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91319

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 132.811 ? Unidentified 0.004 0.004 0.001 1.250

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C-247
Hydrocarbon Expert V4.7 Thu Aug 26 13:59:05 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91319 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91319

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 9.801 106-97-8 n-Butane 1.890 2.448 2.775 506.033

17.722 109-66-0 n-Pentane 0.819 0.981 0.969 220.865

35.323 110-54-3 n-Hexane 0.426 0.484 0.422 115.358

57.610 142-82-5 n-Heptane 0.095 0.104 0.081 25.819

77.555 111-65-9 n-Octane 0.018 0.019 0.013 4.885

102.662 124-18-5 n-Decane 0.099 0.102 0.060 27.135

111.533 1120-21-4 n-Undecane 0.066 0.066 0.036 17.952

I-Paraffins 8.618 75-28-5 i-Butane 0.029 0.039 0.043 7.802

10.399 463-82-1 2,2-Dimethylpropane 0.029 0.036 0.034 7.749

14.745 78-78-4 i-Pentane 12.205 14.763 14.433 3290.084

22.649 75-83-2 2,2-Dimethylbutane 0.322 0.371 0.318 87.037

27.871 79-29-8 2,3-Dimethylbutane 1.591 1.803 1.575 430.647

28.992 107-83-5 2-Methylpentane 10.430 11.969 10.327 2822.785

31.616 96-14-0 3-Methylpentane 6.239 7.039 6.177 1688.612

41.768 108-08-7 2,4-Dimethylpentane 0.152 0.169 0.129 41.289

50.198 591-76-4 2-Methylhexane 0.444 0.491 0.378 120.723

52.032 589-34-4 3-Methylhexane 0.286 0.312 0.243 77.645

71.685 592-27-8 2-Methylheptane 0.017 0.018 0.013 4.680

71.938 589-53-7 4-Methylheptane 0.010 0.010 0.007 2.625

73.011 589-81-1 3-Methylheptane 0.020 0.021 0.015 5.419

95.265 2051-30-1 2,4-Dimethyloctane 0.008 0.008 0.005 2.089

98.49615869-85-9 5-Methylnonane 0.007 0.007 0.004 1.941

98.68517301-94-8 4-Methylnonane 0.018 0.018 0.011 4.889

99.663 5911-04-6 3-Methylnonane 0.035 0.036 0.021 9.549

100.476 C11-Isoparaffin-2 0.029 0.029 0.016 8.000

102.10717302-01-1 3-Ethyl-3-methylheptane 0.062 0.062 0.034 16.838

104.192 C11 Isoparaffin-4 0.011 0.011 0.006 2.959

106.149 C11-Isoparaffin-7 0.184 0.185 0.100 50.221

108.366 C11- Isoparaffin-11 0.420 0.423 0.229 114.992

112.967 C12 - IsoParaffin - 1 0.012 0.012 0.006 3.388

116.073 C12 - IsoParaffin - 4 0.007 0.007 0.003 1.960

Aromatics

Mono-Aromatics 45.154 71-42-3 Benzene 0.707 0.603 0.773 211.249

68.651 108-88-3 Toluene 10.784 9.322 9.986 3184.956

84.445 100-41-4 Ethylbenzene 2.185 1.889 1.756 640.555

85.692 108-38-3 m-Xylene 5.346 4.637 4.297 1567.149

85.836 106-42-3 p-Xylene 2.512 2.187 2.019 736.435

88.657 95-47-6 o-Xylene 1.578 1.343 1.268 462.494

92.836 98-82-8 i-Propylbenzene 0.039 0.034 0.028 11.462

96.305 103-65-1 n-Propylbenzene 0.490 0.426 0.348 142.603

97.164 620-14-4 1-Methyl-3-ethylbenzene 2.108 1.827 1.496 613.883

97.394 622-96-8 1-Methyl-4-ethylbenzene 1.013 0.882 0.719 295.144

98.022 108-67-8 1,3,5-Trimethylbenzene 1.391 1.205 0.988 405.233

99.102 611-14-3 1-Methyl-2-ethylbenzene 0.819 0.697 0.582 238.610

100.757 95-63-6 1,2,4-Trimethylbenzene 4.265 3.650 3.028 1242.251

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C-248
Hydrocarbon Expert V4.7 Thu Aug 26 13:59:05 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91319 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91319

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 102.384 538-93-2 i-Butylbenzene 0.119 0.105 0.076 34.516

103.614 526-73-8 1,2,3-Trimethylbenzene 0.758 0.635 0.538 220.858

104.011 535-77-3 1-Methyl-3-i-propylbenzene 0.022 0.019 0.014 6.377

106.333 141-93-5 1,3-Diethylbenzene 0.121 0.105 0.077 35.120

106.612 1074-43-7 1-Methyl-3-n-propylbenzene 0.847 0.737 0.538 245.270

106.952 105-05-5 1,4-Diethylbenzene 0.352 0.306 0.224 101.935

107.049 104-51-8 n-Butylbenzene 0.077 0.067 0.049 22.398

107.176 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.417 0.355 0.265 120.839

107.449 135-01-3 1,2-Diethylbenzene 0.059 0.050 0.037 17.075

108.025 1074-17-5 1-Methyl-2-n-propylbenzene 0.156 0.134 0.099 45.234

108.880 1758-88-9 1,4,Dimethyl-2-ethylbenzene 0.385 0.329 0.245 111.500

109.036 874-41-9 1,3-Dimethyl-4-ethylbenzene 0.830 0.709 0.528 240.423

109.549 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.975 0.836 0.620 282.584

110.099 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.412 0.347 0.262 119.420

111.010 1-Methyl-4-t-butylbenzene 0.099 0.088 0.057 28.659

111.223 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.370 0.311 0.235 107.190

111.691 4218-48-8 1-Ethyl-4-i-propylbenzene 0.070 0.059 0.041 20.330

111.904 C11 - Aromatic - 1 0.016 0.014 0.009 4.647

112.169 1,2,4,5-Tetramethylbenzene 0.867 0.732 0.551 251.079

112.438 527-53-7 1,2,3,5-Tetramethylbenzene 1.193 1.004 0.758 345.596

113.583 C11 - Aromatic - 3 0.153 0.129 0.088 44.075

113.904 1,2-Di-i-propylbenzene 0.152 0.128 0.080 43.793

114.119 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.217 0.183 0.125 62.662

114.278 C11 - Aromatic - 4 0.105 0.088 0.060 30.286

115.091 538-68-1 n-Pentylbenzene 0.053 0.045 0.031 15.365

115.322 tert-Pentylbenzene 0.224 0.188 0.129 64.488

115.634 577-55-9 1-Methyl-2-n-butylbenzene 0.099 0.083 0.057 28.520

115.743 C11 - Aromatic - 7 0.125 0.110 0.072 36.010

116.206 100-18-5 1,4-Di-i-propylbenzene 0.185 0.156 0.097 53.144

117.431 7364-19-4 1t-Butyl-4-ethylbenzene 0.026 0.022 0.014 7.479

117.735 1,3-Di-n-propylbenzene 0.135 0.113 0.071 38.715

117.847 C11 - Aromatic - 11 0.074 0.065 0.043 21.340

118.402 C11 - Aromatic - 12 0.042 0.037 0.024 12.031

119.030 C11 - Aromatic - 13 0.006 0.005 0.003 1.606

119.340 102-25-0 1,3,5-Triethylbenzene 0.006 0.005 0.003 1.696

Naphthalenes 116.633 91-20-3 Naphthalene 0.218 0.159 0.145 66.044

123.282 91-57-6 2-Methylnaphthalene 0.009 0.007 0.006 2.828

124.147 90-12-0 1-Methylnaphthalene 0.005 0.004 0.003 1.515

Naphtheno/Olefino-Benzs 113.766 874-35-1 5-Methylindan 0.350 0.295 0.226 101.485

114.768 824-63-5 2-Methylindan 0.366 0.308 0.236 106.043

Indenes 104.802 Indan 0.252 0.196 0.182 74.684

105.430 Indene 0.411 0.319 0.297 121.557

109.201 2-Methylindan 0.093 0.072 0.060 27.469

114.517 824-22-6 4-Methylindan 0.493 0.415 0.318 142.830

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C-249
Hydrocarbon Expert V4.7 Thu Aug 26 13:59:05 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91319 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91319

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Indenes 116.843 4,7-Dimethyl Indane 0.012 0.009 0.007 3.597

117.081 1,1-Dimethyl Indane 0.052 0.040 0.030 15.309

117.250 Dimethyl Indane - 1 0.018 0.014 0.011 5.350

117.565 Dimethyl Indane - 2 0.005 0.004 0.003 1.557

Naphthenes

Mono-Naphthenes 27.137 287-92-3 Cyclopentane 0.270 0.272 0.329 74.922

40.181 96-37-7 Methylcyclopentane 0.763 0.764 0.774 211.574

47.068 110-82-7 Cyclohexane 0.066 0.063 0.067 18.243

52.884 1759-58-6 1t,3-Dimethylcyclopentane 0.100 0.100 0.087 27.704

53.472 2532-58-3 1c,3-Dimethylcyclopentane 0.067 0.067 0.058 18.498

54.098 822-50-4 1t,2-Dimethylcyclopentane 0.059 0.059 0.052 16.442

59.19616491-15-9 Cyclopentene, 1,5-dimethyl- 0.019 0.019 0.016 5.253

61.035 108-87-2 Methylcyclohexane 0.042 0.041 0.037 11.658

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.412 115-11-7 Isobutene 0.016 0.020 0.024 4.346

9.452 106-98-9 Butene-1 0.019 0.024 0.029 5.219

10.277 624-64-6 t-Butene-2 0.074 0.091 0.112 20.424

11.000 590-18-1 c-Butene-2 0.087 0.105 0.133 24.178

16.360 109-67-1 Pentene-1 0.339 0.397 0.412 93.993

18.830 646-04-8 t-Pentene-2 0.862 0.997 1.049 239.110

19.852 627-20-3 c-Pentene-2 0.473 0.541 0.576 131.228

32.979 592-41-6 Hexene-1 0.166 0.184 0.168 46.069

35.96713269-52-8 t-Hexene-3 0.273 0.300 0.276 75.589

36.441 4050-45-7 t-Hexene-2 0.523 0.574 0.530 145.033

38.268 7688-21-3 c-Hexene-2 0.222 0.240 0.225 61.522

55.024 592-76-7 Heptene-1 0.028 0.030 0.024 7.779

56.87914686-14-7 t-Heptene-3 0.034 0.036 0.029 9.321

57.830 7642-10-6 c-Heptene-3 0.027 0.029 0.023 7.450

58.73714686-13-6 t-Heptene-2 0.014 0.014 0.012 3.753

110.729 693-61-8 2-Undecene, (E)- 0.032 0.032 0.019 8.655

Iso-Olefins 13.145 563-45-1 3-Methylbutene-1 0.331 0.396 0.403 91.846

17.198 563-46-2 2-Methylbutene-1 0.515 0.593 0.627 142.805

20.523 513-35-9 2-Methylbutene-2 1.061 1.201 1.291 294.302

28.738 691-38-3 4-Methyl-c-pentene-2 0.043 0.048 0.044 12.008

29.383 674-76-0 4-Methyl-t-pentene-2 0.136 0.151 0.137 37.578

32.755 763-29-1 2-Methylpentene-1 0.232 0.254 0.235 64.237

35.165 760-21-4 2-Ethylbutene-1 0.071 0.077 0.072 19.694

36.933 625-27-4 2-Methylpentene-2 0.354 0.384 0.359 98.249

37.344 922-62-3 3-Methyl-c-pentene-2 0.274 0.295 0.278 76.109

39.613 3404-73-7 3,3-Dimethylpentene-1 0.325 0.348 0.283 90.243

42.062 594-56-9 2,3,3-Trimethylbutene-1 0.011 0.011 0.009 2.930

46.176 3404-61-3 3-Methylhexene-1 0.017 0.018 0.014 4.587

46.760 3524-73-0 5-Methylhexene-1 0.023 0.025 0.020 6.502

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C-250
Hydrocarbon Expert V4.7 Thu Aug 26 13:59:05 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91319 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91319

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Iso-Olefins 48.81515840-60-5 2-Methyl-c-hexene-3 0.042 0.045 0.037 11.660

49.160 3769-23-1 4-Methylhexene-1 0.012 0.013 0.011 3.352

49.807 3404-55-5 4-Methyl-t/c-hexene-2 0.053 0.056 0.046 14.686

54.396 C7 - Iso-Olefin - 2 0.023 0.024 0.020 6.406

56.358 4914-89-0 3-Methyl-c-hexene-3 0.014 0.015 0.013 4.011

57.237 6094-02-6 2-Methylhexene-1 0.060 0.064 0.052 16.594

58.109 2738-19-4 2-Methyl-2-hexene 0.027 0.028 0.024 7.502

58.353 3899-36-3 3-Methyl-t-hexene-3 0.021 0.022 0.018 5.726

59.63720710-38-8 3-Methyl-t-hexene-2 0.016 0.017 0.014 4.475

60.423 4914-91-4 2-Pentene, 3,4-dimethyl-, (Z)- 0.014 0.014 0.012 3.778

Naphtheno-Olefins 25.284 142-29-0 Cyclopentene 0.202 0.196 0.253 57.731

45.357 693-89-0 1-Methylcyclopentene 0.379 0.365 0.394 107.702

50.676 110-83-8 Cyclohexene 0.046 0.043 0.048 12.859

Di-Olefins 18.234 78-79-5 2-Methyl-1,3-Butadiene 0.011 0.012 0.013 3.049

20.853 2004-70-8 1t,3-Pentadiene 0.016 0.018 0.020 4.514

Oxygenates 12.764 64-17-5 Ethanol 8.547 8.118 15.829 1018.567

26.530 71-23-8 n-Propanol 0.186 0.174 0.264 36.052

Unidentified 19.469 Unidentified 0.006 0.007 0.007 1.974

22.104 Unidentified 0.006 0.006 0.008 2.024

28.273 Unidentified 0.053 0.053 0.051 17.943

44.952 Unidentified 0.012 0.012 0.013 4.227

47.610 Unidentified 0.036 0.038 0.031 12.157

98.885 Unidentified 0.212 0.219 0.127 72.155

100.128 Unidentified 0.018 0.013 0.010 5.995

100.255 Unidentified 0.053 0.053 0.029 17.901

100.941 Unidentified 0.038 0.041 0.023 12.875

101.062 Unidentified 0.021 0.022 0.013 7.243

102.973 Unidentified 0.016 0.017 0.010 5.594

104.393 Unidentified 0.062 0.054 0.039 20.934

107.888 Unidentified 0.046 0.046 0.025 15.665

108.163 Unidentified 0.054 0.055 0.030 18.347

108.244 Unidentified 0.048 0.048 0.026 16.228

108.551 Unidentified 0.136 0.137 0.074 46.154

110.528 Unidentified 0.011 0.010 0.006 3.669

110.859 Unidentified 0.039 0.039 0.024 13.207

111.799 Unidentified 0.029 0.025 0.017 9.917

112.624 Unidentified 0.010 0.008 0.006 3.329

112.796 Unidentified 0.011 0.009 0.007 3.813

113.291 Unidentified 0.031 0.032 0.016 10.619

114.680 Unidentified 0.115 0.097 0.066 38.983

114.979 Unidentified 0.038 0.032 0.022 12.859

125.443 Unidentified 0.004 0.003 0.002 1.502

129.864 Unidentified 0.003 0.002 0.002 1.017

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C-251
Hydrocarbon Expert V4.7 Thu Aug 26 13:59:05 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91319 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91319

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Unidentified 132.811 Unidentified 0.004 0.004 0.001 1.250

Plus

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C-252
Hydrocarbon Expert V4.7 Thu Aug 26 13:59:05 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91319 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91319

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF

20.0 15.0 10.0 5.0 0.0

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

Ethanol

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

Unidentified

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

Unidentified

2,2-Dimethylbutane

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C-253
Hydrocarbon Expert V4.7 Thu Aug 26 13:59:05 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91319 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91319

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

n-Propanol

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

2-Ethylbutene-1 n-Hexane

t-Hexene-3

t-Hexene-2

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane 2,3,3-Trimethylbutene-1

Unidentified Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1 Cyclohexane

Unidentified

2-Methyl-c-hexene-3

4-Methylhexene-1

4-Methyl-t/c-hexene-2

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C-254
Hydrocarbon Expert V4.7 Thu Aug 26 13:59:05 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91319 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91319

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF

70.0 65.0 60.0 55.0 50.0

2-Methylhexane

Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane C7 - Iso-Olefin - 2

Heptene-1

3-Methyl-c-hexene-3

t-Heptene-3

2-Methylhexene-1

n-Heptane c-Heptene-3 2-Methyl-2-hexene 3-Methyl-t-hexene-3

t-Heptene-2

Cyclopentene, 1,5-dimethyl3-Methyl-t-hexene-2

2-Pentene, 3,4-dimethyl-, (Z)-

Methylcyclohexane

Toluene

2-Methylheptane 4-Methylheptane

3-Methylheptane

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C-255
Hydrocarbon Expert V4.7 Thu Aug 26 13:59:05 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91319 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91319

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF

95.0 90.0 85.0 80.0 75.0

n-Octane

Ethylbenzene

m-Xylene p-Xylene

o-Xylene

i-Propylbenzene

2,4-Dimethyloctane

n-Propylbenzene

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

5-Methylnonane 4-Methylnonane Unidentified 1-Methyl-2-ethylbenzene

3-Methylnonane

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C-256
Hydrocarbon Expert V4.7 Thu Aug 26 13:59:05 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91319 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91319

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified

C11-Isoparaffin-2 1,2,4-Trimethylbenzene Unidentified

3-Ethyl-3-methylheptane i-Butylbenzene n-Decane Unidentified

1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene C11 Isoparaffin-4 Unidentified

Indan

Indene

C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene

n-Butylbenzene 1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

Unidentified Unidentified 1-Methyl-2-n-propylbenzene

C11- Isoparaffin-11 Unidentified

1,4,Dimethyl-2-ethylbenzene 1,3-Dimethyl-4-ethylbenzene 2-Methylindan

1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

Unidentified 2-Undecene, (E)- Unidentified 1-Methyl-4-t-butylbenzene 1,2-Dimethyl-3-ethylbenzene n-Undecane Unidentified 1-Ethyl-4-i-propylbenzene C11 - Aromatic - 1 1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene Unidentified

C12 - IsoParaffin - 1

Unidentified C11 - Aromatic - 3 5-Methylindan 1,2-Di-i-propylbenzene 1-methyl-4-(1-methylpropyl)be C11 - Aromatic - 4 4-Methylindan Unidentified 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene 1-Methyl-2-n-butylbenzene C11 - Aromatic - 7

C12 - IsoParaffin - 4 1,4-Di-i-propylbenzene

Naphthalene 4,7-Dimethyl Indane 1,1-Dimethyl Indane Dimethyl Indane - 1

Dimethyl Indane - 2 1t-Butyl-4-ethylbenzene

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

C11 - Aromatic - 12

C11 - Aromatic - 13

1,3,5-Triethylbenzene

2-Methylnaphthalene

1-Methylnaphthalene

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C-257
Hydrocarbon Expert V4.7 Thu Aug 26 13:59:05 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91319 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91319

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000015.D\SIG1000015_FID1_A.CDF

145.0 140.0 135.0 130.0 125.0

Unidentified

Unidentified

Unidentified

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C-258
Hydrocarbon Expert V4.7 Fri Aug 27 15:55:27 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91320 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91320

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 9.210 10.918 11.430

I-Paraffins 28.756 32.600 29.644

Aromatics 47.072 40.840 42.347

Mono-Aromatics 44.838 39.031 40.637

Naphthalenes 0.123 0.091 0.090

Naphtheno/Olefino-Benzs 0.578 0.492 0.420

Indenes 1.533 1.227 1.198

Naphthenes 5.419 5.392 5.997

Mono-Naphthenes 5.419 5.392 5.997

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 6.741 7.568 8.511

n-Olefins 3.069 3.521 3.963

Iso-Olefins 3.117 3.504 3.850

Naphtheno-Olefins 0.534 0.519 0.668

Di-Olefins 0.022 0.024 0.031

Oxygenates 0.111 0.105 0.178

Unidentified 2.692 2.578 1.894

Plus 0.000 0.000 0.000

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C-259
Hydrocarbon Expert V4.7 Fri Aug 27 15:55:27 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91320 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91320

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C3 0.112 0.107 0.180

C4 1.807 2.349 3.002

C5 13.617 16.303 18.294

C6 17.895 19.659 20.208

C7 21.903 20.227 22.445

C8 19.824 19.193 17.370

C9 11.545 10.253 9.175

C10 8.125 7.009 5.879

C11 2.165 2.048 1.369

C12 0.315 0.273 0.186

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C-260
Hydrocarbon Expert V4.7 Fri Aug 27 15:55:27 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91320 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91320

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C3 0.001 0.002 0.002

C4 1.534 2.006 2.536

C5 2.607 3.152 3.473

C6 4.196 4.818 4.681

C7 0.431 0.478 0.414

C8 0.152 0.164 0.128

C9 0.086 0.090 0.064

C10 0.106 0.110 0.072

C11 0.096 0.098 0.059

I-Paraffins C4 0.037 0.051 0.062

C5 7.294 8.915 9.718

C6 6.924 7.962 7.724

C7 3.071 3.424 2.946

C8 8.807 9.516 7.412

C9 1.139 1.215 0.854

C10 0.401 0.414 0.264

C11 1.056 1.075 0.650

C12 0.027 0.028 0.015

Mono-Aromatics C6 0.610 0.526 0.751

C7 16.637 14.528 17.357

C8 10.697 9.348 9.686

C9 10.024 8.704 8.017

C10 5.705 4.926 4.086

C11 0.877 0.754 0.569

C12 0.288 0.245 0.171

Naphthalenes C10 0.102 0.075 0.076

C11 0.021 0.016 0.014

Naphtheno/Olefino-Benzs C10 0.578 0.492 0.420

Indenes C9 0.261 0.205 0.213

C10 1.223 0.983 0.954

C11 0.049 0.038 0.032

Mono-Naphthenes C5 0.279 0.283 0.383

C6 3.710 3.690 4.237

C7 1.252 1.243 1.226

C8 0.168 0.165 0.144

C10 0.010 0.009 0.007

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C-261
Hydrocarbon Expert V4.7 Fri Aug 27 15:55:27 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91320 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91320

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Mono-Naphthenes

n-Olefins C4 0.236 0.293 0.404

C5 1.614 1.884 2.212

C6 1.102 1.221 1.259

C7 0.016 0.018 0.016

C9 0.035 0.039 0.027

C11 0.065 0.067 0.045

Iso-Olefins C5 1.621 1.868 2.222

C6 1.000 1.100 1.142

C7 0.496 0.536 0.486

Naphtheno-Olefins C5 0.181 0.177 0.255

C6 0.353 0.342 0.413

Di-Olefins C5 0.022 0.024 0.031

Oxygenates C3 0.111 0.105 0.178

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C-262
Hydrocarbon Expert V4.7 Fri Aug 27 15:55:27 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91320 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91320

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 23.50 22.69

5% 80.11 79.67

10% 87.52 81.50

15% 101.34 96.27

20% 140.23 135.33

25% 154.41 144.17

30% 158.84 154.55

35% 187.04 158.56

40% 209.76 182.15

45% 229.83 209.58

50% 230.21 228.41

55% 230.58 230.18

60% 230.96 230.61

65% 254.84 231.04

70% 281.15 275.47

75% 291.57 281.55

80% 323.22 318.96

85% 335.58 334.04

90% 358.77 352.22

95% 372.94 368.42

FBP 404.60 404.60

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C-263
Hydrocarbon Expert V4.7 Fri Aug 27 15:55:27 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91320 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91320

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 7.389 74-98-6 P3 Propane 0.001 0.002 0.002 0.267

2 8.610 75-28-5 I4 i-Butane 0.037 0.051 0.062 9.903

3 9.402 115-11-7 K4 Isobutene 0.020 0.026 0.035 5.622

4 9.441 106-98-9 K4 Butene-1 0.024 0.031 0.042 6.677

5 9.790 106-97-8 P4 n-Butane 1.534 2.006 2.536 406.830

6 10.264 624-64-6 K4 t-Butene-2 0.089 0.112 0.153 24.556

7 10.386 463-82-1 I5 2,2-Dimethylpropane 0.034 0.044 0.046 9.189

8 10.984 590-18-1 K4 c-Butene-2 0.102 0.124 0.174 27.905

9 13.124 563-45-1 C5 3-Methylbutene-1 0.070 0.085 0.096 19.337

10 14.709 78-78-4 I5 i-Pentane 7.259 8.871 9.673 1939.149

11 16.326 109-67-1 K5 Pentene-1 0.323 0.382 0.443 88.811

12 17.162 563-46-2 C5 2-Methylbutene-1 0.507 0.590 0.694 139.210

13 17.690 109-66-0 P5 n-Pentane 2.607 3.152 3.473 696.284

14 18.203 78-79-5 E5 2-Methyl-1,3-Butadiene 0.009 0.010 0.012 2.473

15 18.796 646-04-8 K5 t-Pentene-2 0.835 0.975 1.144 229.307

16 19.815 627-20-3 K5 c-Pentene-2 0.456 0.527 0.625 125.356

17 20.488 513-35-9 C5 2-Methylbutene-2 1.044 1.193 1.431 286.849

18 20.820 2004-70-8 E5 1t,3-Pentadiene 0.013 0.014 0.018 3.642

19 22.069 ? Unidentified 0.005 0.005 0.007 1.531

20 22.613 75-83-2 I6 2,2-Dimethylbutane 0.183 0.213 0.204 49.009

21 25.240 142-29-0 B5 Cyclopentene 0.181 0.177 0.255 51.071

22 26.411 ? Unidentified 0.038 0.036 0.061 12.774

23 26.477 71-23-8 X3 n-Propanol 0.111 0.105 0.178 21.352

24 27.089 287-92-3 M5 Cyclopentane 0.279 0.283 0.383 76.677

25 27.824 79-29-8 I6 2,3-Dimethylbutane 1.230 1.407 1.372 329.850

26 28.224 ? Unidentified 0.051 0.052 0.056 17.235

27 28.682 691-38-3 C6 4-Methyl-c-pentene-2 0.044 0.049 0.050 12.103

28 28.903 107-83-5 I6 2-Methylpentane 3.098 3.591 3.455 830.722

29 29.336 674-76-0 C6 4-Methyl-t-pentene-2 0.132 0.148 0.150 36.167

30 31.543 96-14-0 I6 3-Methylpentane 2.414 2.751 2.692 647.278

31 32.710 763-29-1 C6 2-Methylpentene-1 0.224 0.248 0.256 61.558

32 32.936 592-41-6 K6 Hexene-1 0.155 0.173 0.177 42.683

33 35.302 110-54-3 P6 n-Hexane 4.196 4.818 4.681 1125.424

34 35.92813269-52-8 K6 t-Hexene-3 0.256 0.284 0.292 70.339

35 36.399 4050-45-7 K6 t-Hexene-2 0.484 0.537 0.553 133.118

36 36.895 625-27-4 C6 2-Methylpentene-2 0.340 0.373 0.388 93.437

37 37.305 922-62-3 C6 3-Methyl-c-pentene-2 0.260 0.282 0.297 71.432

38 38.233 7688-21-3 K6 c-Hexene-2 0.207 0.226 0.236 56.757

39 39.578 3404-73-7 C7 3,3-Dimethylpentene-1 0.311 0.335 0.304 85.343

40 40.155 96-37-7 M6 Methylcyclopentane 2.129 2.153 2.431 584.826

41 41.729 108-08-7 I7 2,4-Dimethylpentane 0.897 1.009 0.860 241.393

42 42.269 464-06-2 I7 2,2,3-Trimethylbutane 0.099 0.109 0.095 26.755

43 44.927 ? Unidentified 0.010 0.010 0.012 3.400

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C-264
Hydrocarbon Expert V4.7 Fri Aug 27 15:55:27 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91320 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91320

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 45.128 71-42-3 Q6 Benzene 0.610 0.526 0.751 180.590

45 45.336 693-89-0 B6 1-Methylcyclopentene 0.319 0.310 0.373 89.771

46 46.154 3404-61-3 C7 3-Methylhexene-1 0.011 0.012 0.011 3.112

47 46.741 3524-73-0 C7 5-Methylhexene-1 0.080 0.087 0.078 21.944

48 47.056 110-82-7 M6 Cyclohexane 1.581 1.538 1.806 434.417

49 47.589 ? Unidentified 0.028 0.030 0.027 9.343

50 48.80015840-60-5 C7 2-Methyl-c-hexene-3 0.030 0.033 0.029 8.239

51 49.793 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.034 0.037 0.033 9.400

52 50.192 591-76-4 I7 2-Methylhexane 1.456 1.625 1.397 392.129

53 50.665 110-83-8 B6 Cyclohexene 0.034 0.032 0.040 9.367

54 52.027 589-34-4 I7 3-Methylhexane 0.619 0.682 0.593 166.545

55 52.878 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.146 0.148 0.143 40.200

56 53.467 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.116 0.117 0.113 31.756

57 54.093 822-50-4 M7 1t,2-Dimethylcyclopentane 0.158 0.159 0.155 43.438

58 54.711 540-84-1 I8 2,2,4-Trimethylpentane 4.501 4.926 3.788 1214.468

59 56.87914686-14-7 K7 t-Heptene-3 0.016 0.018 0.016 4.478

60 57.232 6094-02-6 C7 2-Methylhexene-1 0.025 0.027 0.025 6.952

61 57.613 142-82-5 P7 n-Heptane 0.431 0.478 0.414 116.130

62 58.113 2738-19-4 C7 2-Methyl-2-hexene 0.005 0.005 0.005 1.277

63 61.060 108-87-2 M7 Methylcyclohexane 0.802 0.789 0.785 220.262

64 62.012 4516-69-2 M8 1,1,3-Trimethylcyclopentane 0.017 0.017 0.014 4.630

65 62.419 590-73-8 I8 2,2-Dimethylhexane 0.020 0.022 0.017 5.419

66 63.856 1640-89-7 M7 Ethylcyclopentane 0.030 0.030 0.030 8.309

67 64.508 564-02-3 I8 2,2,3-Trimethylpentane 0.296 0.313 0.249 79.766

68 64.750 592-13-2 I8 2,5-Dimethylhexane 0.684 0.747 0.576 184.579

69 65.089 589-43-5 I8 2,4-Dimethylhexane 0.570 0.616 0.479 153.656

70 65.926 4850-28-6 M8 1c,2t,4-Trimethylcyclopentane 0.016 0.016 0.014 4.377

71 68.097 565-75-3 I8 2,3,4-Trimethylpentane 1.925 2.027 1.620 519.307

72 68.693 108-88-3 Q7 Toluene 16.637 14.528 17.357 4869.130

73 70.428 584-94-1 I8 2,3-Dimethylhexane 0.490 0.521 0.412 132.194

74 71.697 592-27-8 I8 2-Methylheptane 0.101 0.109 0.085 27.231

75 71.957 589-53-7 I8 4-Methylheptane 0.081 0.087 0.068 21.896

76 72.092 ? Unidentified 0.037 0.039 0.032 12.619

77 72.862 M8 1,3-dimethyl-t-cyclohexane 0.071 0.070 0.061 19.490

78 73.021 589-81-1 I8 3-Methylheptane 0.092 0.099 0.077 24.815

79 73.204 619-99-8 I8 3-Ethylhexane 0.047 0.050 0.040 12.715

80 74.103 ? Unidentified 0.011 0.010 0.009 3.639

81 74.925 3522-94-9 I9 2,2,5-Trimethylhexane 0.862 0.923 0.646 232.996

82 76.189 2207-03-6 M8 1t,3-Dimethylcyclohexane 0.028 0.027 0.024 7.713

83 77.563 111-65-9 P8 n-Octane 0.152 0.164 0.128 41.057

84 78.507 ? Unidentified 0.017 0.017 0.015 5.779

85 80.054 1069-53-0 I9 2,3,5-Trimethylhexane 0.123 0.129 0.092 33.233

86 81.232 1071-26-7 I9 2,4-Dimethylheptane 0.019 0.020 0.014 5.151

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C-265
Hydrocarbon Expert V4.7 Fri Aug 27 15:55:27 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91320 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91320

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 81.867 1678-91-7 M8 Ethylcyclohexane 0.037 0.035 0.031 10.074

88 82.194 1072-05-5 I9 2,6-Dimethylheptane 0.032 0.034 0.024 8.706

89 83.130 I9 2,5-Dimethylheptane 0.061 0.065 0.046 16.484

90 84.446 100-41-4 Q8 Ethylbenzene 1.798 1.570 1.628 522.199

91 84.861 ? Unidentified 0.008 0.007 0.006 2.531

92 85.692 108-38-3 Q8 m-Xylene 4.994 4.376 4.523 1450.718

93 85.835 106-42-3 Q8 p-Xylene 2.297 2.020 2.080 667.297

94 87.016 2216-34-4 I9 4-Methyloctane 0.011 0.012 0.008 3.053

95 87.149 3221-61-2 I9 2-Methyloctane 0.015 0.016 0.011 4.036

96 88.012 2216-33-3 I9 3-Methyloctane 0.016 0.016 0.012 4.198

97 88.481 K9 C9-isoolefin 0.035 0.039 0.027 9.721

98 88.659 95-47-6 Q8 o-Xylene 1.607 1.382 1.455 466.792

99 89.067 I10 C10 - IsoParaffin - 1 0.115 0.120 0.078 31.233

100 89.91314720-74-2 I10 2,2,4-trimethylheptane 0.081 0.085 0.055 22.023

101 91.477 111-84-2 P9 n-Nonane 0.086 0.090 0.064 23.168

102 92.837 98-82-8 Q9 i-Propylbenzene 0.038 0.034 0.031 11.070

103 93.600 ? Unidentified 0.028 0.029 0.019 9.494

104 93.82215869-87-1 I10 2,2-Dimethyloctane 0.010 0.010 0.007 2.698

105 95.266 2051-30-1 I10 2,4-Dimethyloctane 0.022 0.023 0.015 5.950

106 95.662 I10 2,6-Dimethyloctane 0.010 0.010 0.007 2.644

107 96.307 103-65-1 Q9 n-Propylbenzene 0.431 0.379 0.345 124.442

108 97.163 620-14-4 Q9 1-Methyl-3-ethylbenzene 1.886 1.651 1.508 544.214

109 97.393 622-96-8 Q9 1-Methyl-4-ethylbenzene 0.916 0.805 0.733 264.365

110 98.022 108-67-8 Q9 1,3,5-Trimethylbenzene 1.278 1.118 1.022 368.823

111 98.68717301-94-8 I10 4-Methylnonane 0.017 0.017 0.011 4.512

112 98.887 ? Unidentified 0.426 0.444 0.288 143.526

113 99.103 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.755 0.649 0.604 217.809

114 99.664 5911-04-6 I10 3-Methylnonane 0.029 0.030 0.020 7.929

115 100.130 ? Unidentified 0.036 0.027 0.022 12.175

116 100.256 ? Unidentified 0.104 0.106 0.064 35.042

117 100.478 I11 C11-Isoparaffin-2 0.059 0.060 0.036 16.005

118 100.755 95-63-6 Q9 1,2,4-Trimethylbenzene 3.994 3.452 3.194 1152.541

119 100.943 ? Unidentified 0.078 0.084 0.053 26.125

120 101.064 ? Unidentified 0.045 0.046 0.030 15.025

121 101.322 1678-98-4 M10 i-Butylcyclohexane 0.010 0.009 0.007 2.651

122 102.10917302-01-1 I10 3-Ethyl-3-methylheptane 0.117 0.119 0.072 31.663

123 102.388 538-93-2 Q10 i-Butylbenzene 0.176 0.156 0.126 50.492

124 102.662 124-18-5 P10 n-Decane 0.106 0.110 0.072 28.825

125 102.976 ? Unidentified 0.033 0.034 0.020 11.176

126 103.615 526-73-8 Q9 1,2,3-Trimethylbenzene 0.726 0.615 0.581 209.610

127 104.006 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.026 0.023 0.019 7.534

128 104.193 I11 C11 Isoparaffin-4 0.019 0.019 0.011 5.039

129 104.396 ? Unidentified 0.105 0.093 0.075 35.312

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C-266
Hydrocarbon Expert V4.7 Fri Aug 27 15:55:27 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91320 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91320

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 104.804 J9 Indan 0.261 0.205 0.213 76.622

131 105.434 J10 Indene 0.745 0.585 0.606 218.479

132 106.151 I11 C11-Isoparaffin-7 0.321 0.327 0.198 87.090

133 106.334 141-93-5 Q10 1,3-Diethylbenzene 0.107 0.094 0.077 30.811

134 106.623 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 1.079 0.949 0.773 309.837

135 106.943 105-05-5 Q10 1,4-Diethylbenzene 0.424 0.373 0.304 121.822

136 107.177 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.299 0.257 0.214 85.906

137 107.434 135-01-3 Q10 1,2-Diethylbenzene 0.085 0.073 0.061 24.410

138 107.889 ? Unidentified 0.083 0.084 0.051 27.896

139 108.027 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.104 0.090 0.074 29.713

140 108.165 ? Unidentified 0.095 0.097 0.059 31.866

141 108.246 ? Unidentified 0.085 0.087 0.052 28.648

142 108.369 I11 C11- Isoparaffin-11 0.658 0.669 0.404 178.339

143 108.552 ? Unidentified 0.225 0.229 0.138 75.739

144 108.882 1758-88-9 Q10 1,4,Dimethyl-2-ethylbenzene 0.222 0.192 0.159 63.736

145 108.987 ? Unidentified 0.837 0.722 0.600 281.737

146 109.206 J10 2-Methylindan 0.132 0.104 0.096 38.666

147 109.547 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.740 0.640 0.530 212.344

148 110.102 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.710 0.604 0.509 203.833

149 110.529 ? Unidentified 0.029 0.027 0.018 9.678

150 110.730 693-61-8 K11 2-Undecene, (E)- 0.065 0.067 0.045 17.715

151 110.861 ? Unidentified 0.077 0.078 0.052 25.772

152 111.000 Q11 1-Methyl-4-t-butylbenzene 0.090 0.080 0.058 25.705

153 111.222 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.331 0.281 0.237 95.136

154 111.533 1120-21-4 P11 n-Undecane 0.096 0.098 0.059 26.131

155 111.691 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.105 0.090 0.068 30.145

156 111.799 ? Unidentified 0.073 0.062 0.047 24.589

157 112.167 Q10 1,2,4,5-Tetramethylbenzene 0.587 0.501 0.420 168.482

158 112.435 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.814 0.692 0.583 233.637

159 112.649 ? Unidentified 0.014 0.012 0.009 4.800

160 112.788 ? Unidentified 0.022 0.018 0.016 7.298

161 112.967 I12 C12 - IsoParaffin - 1 0.027 0.028 0.015 7.328

162 113.295 ? Unidentified 0.040 0.041 0.023 13.337

163 113.449 ? Unidentified 0.012 0.012 0.007 4.069

164 113.585 Q11 C11 - Aromatic - 3 0.119 0.102 0.077 34.127

165 113.765 874-35-1 H10 5-Methylindan 0.261 0.222 0.190 74.824

166 113.904 Q12 1,2-Di-i-propylbenzene 0.105 0.089 0.062 29.918

167 114.119 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.145 0.123 0.094 41.447

168 114.282 Q11 C11 - Aromatic - 4 0.071 0.060 0.046 20.327

169 114.516 824-22-6 J10 4-Methylindan 0.346 0.295 0.252 99.408

170 114.768 824-63-5 H10 2-Methylindan 0.317 0.270 0.231 91.139

171 114.980 ? Unidentified 0.027 0.023 0.018 9.117

172 115.092 538-68-1 Q11 n-Pentylbenzene 0.030 0.026 0.020 8.691

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C-267
Hydrocarbon Expert V4.7 Fri Aug 27 15:55:27 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91320 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91320

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 115.323 Q11 tert-Pentylbenzene 0.138 0.118 0.090 39.540

174 115.634 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.058 0.049 0.038 16.606

175 115.744 Q11 C11 - Aromatic - 7 0.079 0.070 0.051 22.475

176 116.207 100-18-5 Q12 1,4-Di-i-propylbenzene 0.110 0.094 0.065 31.401

177 116.636 91-20-3 G10 Naphthalene 0.102 0.075 0.076 30.582

178 116.800 J11 4,7-Dimethyl Indane 0.021 0.016 0.014 6.122

179 117.083 J11 1,1-Dimethyl Indane 0.028 0.022 0.018 8.232

180 117.433 7364-19-4 Q12 1t-Butyl-4-ethylbenzene 0.022 0.019 0.013 6.377

181 117.736 Q12 1,3-Di-n-propylbenzene 0.051 0.043 0.030 14.398

182 117.847 Q11 C11 - Aromatic - 11 0.026 0.024 0.017 7.558

183 118.403 Q11 C11 - Aromatic - 12 0.014 0.013 0.009 4.018

184 123.282 91-57-6 G11 2-Methylnaphthalene 0.015 0.011 0.010 4.326

185 124.147 90-12-0 G11 1-Methylnaphthalene 0.007 0.005 0.004 1.945

186 126.173 ? Unidentified 0.007 0.006 0.004 2.416

187 126.173 ? Unidentified 0.007 0.007 0.003 2.416

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C-268
Hydrocarbon Expert V4.7 Fri Aug 27 15:55:27 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91320 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91320

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 7.389 74-98-6 Propane 0.001 0.002 0.002 0.267

9.790 106-97-8 n-Butane 1.534 2.006 2.536 406.830

17.690 109-66-0 n-Pentane 2.607 3.152 3.473 696.284

35.302 110-54-3 n-Hexane 4.196 4.818 4.681 1125.424

57.613 142-82-5 n-Heptane 0.431 0.478 0.414 116.130

77.563 111-65-9 n-Octane 0.152 0.164 0.128 41.057

91.477 111-84-2 n-Nonane 0.086 0.090 0.064 23.168

102.662 124-18-5 n-Decane 0.106 0.110 0.072 28.825

111.533 1120-21-4 n-Undecane 0.096 0.098 0.059 26.131

I-Paraffins 8.610 75-28-5 i-Butane 0.037 0.051 0.062 9.903

10.386 463-82-1 2,2-Dimethylpropane 0.034 0.044 0.046 9.189

14.709 78-78-4 i-Pentane 7.259 8.871 9.673 1939.149

22.613 75-83-2 2,2-Dimethylbutane 0.183 0.213 0.204 49.009

27.824 79-29-8 2,3-Dimethylbutane 1.230 1.407 1.372 329.850

28.903 107-83-5 2-Methylpentane 3.098 3.591 3.455 830.722

31.543 96-14-0 3-Methylpentane 2.414 2.751 2.692 647.278

41.729 108-08-7 2,4-Dimethylpentane 0.897 1.009 0.860 241.393

42.269 464-06-2 2,2,3-Trimethylbutane 0.099 0.109 0.095 26.755

50.192 591-76-4 2-Methylhexane 1.456 1.625 1.397 392.129

52.027 589-34-4 3-Methylhexane 0.619 0.682 0.593 166.545

54.711 540-84-1 2,2,4-Trimethylpentane 4.501 4.926 3.788 1214.468

62.419 590-73-8 2,2-Dimethylhexane 0.020 0.022 0.017 5.419

64.508 564-02-3 2,2,3-Trimethylpentane 0.296 0.313 0.249 79.766

64.750 592-13-2 2,5-Dimethylhexane 0.684 0.747 0.576 184.579

65.089 589-43-5 2,4-Dimethylhexane 0.570 0.616 0.479 153.656

68.097 565-75-3 2,3,4-Trimethylpentane 1.925 2.027 1.620 519.307

70.428 584-94-1 2,3-Dimethylhexane 0.490 0.521 0.412 132.194

71.697 592-27-8 2-Methylheptane 0.101 0.109 0.085 27.231

71.957 589-53-7 4-Methylheptane 0.081 0.087 0.068 21.896

73.021 589-81-1 3-Methylheptane 0.092 0.099 0.077 24.815

73.204 619-99-8 3-Ethylhexane 0.047 0.050 0.040 12.715

74.925 3522-94-9 2,2,5-Trimethylhexane 0.862 0.923 0.646 232.996

80.054 1069-53-0 2,3,5-Trimethylhexane 0.123 0.129 0.092 33.233

81.232 1071-26-7 2,4-Dimethylheptane 0.019 0.020 0.014 5.151

82.194 1072-05-5 2,6-Dimethylheptane 0.032 0.034 0.024 8.706

83.130 2,5-Dimethylheptane 0.061 0.065 0.046 16.484

87.016 2216-34-4 4-Methyloctane 0.011 0.012 0.008 3.053

87.149 3221-61-2 2-Methyloctane 0.015 0.016 0.011 4.036

88.012 2216-33-3 3-Methyloctane 0.016 0.016 0.012 4.198

89.067 C10 - IsoParaffin - 1 0.115 0.120 0.078 31.233

89.91314720-74-2 2,2,4-trimethylheptane 0.081 0.085 0.055 22.023

93.82215869-87-1 2,2-Dimethyloctane 0.010 0.010 0.007 2.698

95.266 2051-30-1 2,4-Dimethyloctane 0.022 0.023 0.015 5.950

95.662 2,6-Dimethyloctane 0.010 0.010 0.007 2.644

98.68717301-94-8 4-Methylnonane 0.017 0.017 0.011 4.512

99.664 5911-04-6 3-Methylnonane 0.029 0.030 0.020 7.929

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C-269
Hydrocarbon Expert V4.7 Fri Aug 27 15:55:27 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91320 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91320

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

I-Paraffins 100.478 C11-Isoparaffin-2 0.059 0.060 0.036 16.005

102.10917302-01-1 3-Ethyl-3-methylheptane 0.117 0.119 0.072 31.663

104.193 C11 Isoparaffin-4 0.019 0.019 0.011 5.039

106.151 C11-Isoparaffin-7 0.321 0.327 0.198 87.090

108.369 C11- Isoparaffin-11 0.658 0.669 0.404 178.339

112.967 C12 - IsoParaffin - 1 0.027 0.028 0.015 7.328

Aromatics

Mono-Aromatics 45.128 71-42-3 Benzene 0.610 0.526 0.751 180.590

68.693 108-88-3 Toluene 16.637 14.528 17.357 4869.130

84.446 100-41-4 Ethylbenzene 1.798 1.570 1.628 522.199

85.692 108-38-3 m-Xylene 4.994 4.376 4.523 1450.718

85.835 106-42-3 p-Xylene 2.297 2.020 2.080 667.297

88.659 95-47-6 o-Xylene 1.607 1.382 1.455 466.792

92.837 98-82-8 i-Propylbenzene 0.038 0.034 0.031 11.070

96.307 103-65-1 n-Propylbenzene 0.431 0.379 0.345 124.442

97.163 620-14-4 1-Methyl-3-ethylbenzene 1.886 1.651 1.508 544.214

97.393 622-96-8 1-Methyl-4-ethylbenzene 0.916 0.805 0.733 264.365

98.022 108-67-8 1,3,5-Trimethylbenzene 1.278 1.118 1.022 368.823

99.103 611-14-3 1-Methyl-2-ethylbenzene 0.755 0.649 0.604 217.809

100.755 95-63-6 1,2,4-Trimethylbenzene 3.994 3.452 3.194 1152.541

102.388 538-93-2 i-Butylbenzene 0.176 0.156 0.126 50.492

103.615 526-73-8 1,2,3-Trimethylbenzene 0.726 0.615 0.581 209.610

104.006 535-77-3 1-Methyl-3-i-propylbenzene 0.026 0.023 0.019 7.534

106.334 141-93-5 1,3-Diethylbenzene 0.107 0.094 0.077 30.811

106.623 1074-43-7 1-Methyl-3-n-propylbenzene 1.079 0.949 0.773 309.837

106.943 105-05-5 1,4-Diethylbenzene 0.424 0.373 0.304 121.822

107.177 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.299 0.257 0.214 85.906

107.434 135-01-3 1,2-Diethylbenzene 0.085 0.073 0.061 24.410

108.027 1074-17-5 1-Methyl-2-n-propylbenzene 0.104 0.090 0.074 29.713

108.882 1758-88-9 1,4,Dimethyl-2-ethylbenzene 0.222 0.192 0.159 63.736

109.547 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.740 0.640 0.530 212.344

110.102 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.710 0.604 0.509 203.833

111.000 1-Methyl-4-t-butylbenzene 0.090 0.080 0.058 25.705

111.222 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.331 0.281 0.237 95.136

111.691 4218-48-8 1-Ethyl-4-i-propylbenzene 0.105 0.090 0.068 30.145

112.167 1,2,4,5-Tetramethylbenzene 0.587 0.501 0.420 168.482

112.435 527-53-7 1,2,3,5-Tetramethylbenzene 0.814 0.692 0.583 233.637

113.585 C11 - Aromatic - 3 0.119 0.102 0.077 34.127

113.904 1,2-Di-i-propylbenzene 0.105 0.089 0.062 29.918

114.119 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.145 0.123 0.094 41.447

114.282 C11 - Aromatic - 4 0.071 0.060 0.046 20.327

115.092 538-68-1 n-Pentylbenzene 0.030 0.026 0.020 8.691

115.323 tert-Pentylbenzene 0.138 0.118 0.090 39.540

115.634 577-55-9 1-Methyl-2-n-butylbenzene 0.058 0.049 0.038 16.606

115.744 C11 - Aromatic - 7 0.079 0.070 0.051 22.475

116.207 100-18-5 1,4-Di-i-propylbenzene 0.110 0.094 0.065 31.401

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C-270
Hydrocarbon Expert V4.7 Fri Aug 27 15:55:27 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91320 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91320

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 117.433 7364-19-4 1t-Butyl-4-ethylbenzene 0.022 0.019 0.013 6.377

117.736 1,3-Di-n-propylbenzene 0.051 0.043 0.030 14.398

117.847 C11 - Aromatic - 11 0.026 0.024 0.017 7.558

118.403 C11 - Aromatic - 12 0.014 0.013 0.009 4.018

Naphthalenes 116.636 91-20-3 Naphthalene 0.102 0.075 0.076 30.582

123.282 91-57-6 2-Methylnaphthalene 0.015 0.011 0.010 4.326

124.147 90-12-0 1-Methylnaphthalene 0.007 0.005 0.004 1.945

Naphtheno/Olefino-Benzs 113.765 874-35-1 5-Methylindan 0.261 0.222 0.190 74.824

114.768 824-63-5 2-Methylindan 0.317 0.270 0.231 91.139

Indenes 104.804 Indan 0.261 0.205 0.213 76.622

105.434 Indene 0.745 0.585 0.606 218.479

109.206 2-Methylindan 0.132 0.104 0.096 38.666

114.516 824-22-6 4-Methylindan 0.346 0.295 0.252 99.408

116.800 4,7-Dimethyl Indane 0.021 0.016 0.014 6.122

117.083 1,1-Dimethyl Indane 0.028 0.022 0.018 8.232

Naphthenes

Mono-Naphthenes 27.089 287-92-3 Cyclopentane 0.279 0.283 0.383 76.677

40.155 96-37-7 Methylcyclopentane 2.129 2.153 2.431 584.826

47.056 110-82-7 Cyclohexane 1.581 1.538 1.806 434.417

52.878 1759-58-6 1t,3-Dimethylcyclopentane 0.146 0.148 0.143 40.200

53.467 2532-58-3 1c,3-Dimethylcyclopentane 0.116 0.117 0.113 31.756

54.093 822-50-4 1t,2-Dimethylcyclopentane 0.158 0.159 0.155 43.438

61.060 108-87-2 Methylcyclohexane 0.802 0.789 0.785 220.262

62.012 4516-69-2 1,1,3-Trimethylcyclopentane 0.017 0.017 0.014 4.630

63.856 1640-89-7 Ethylcyclopentane 0.030 0.030 0.030 8.309

65.926 4850-28-6 1c,2t,4-Trimethylcyclopentane 0.016 0.016 0.014 4.377

72.862 1,3-dimethyl-t-cyclohexane 0.071 0.070 0.061 19.490

76.189 2207-03-6 1t,3-Dimethylcyclohexane 0.028 0.027 0.024 7.713

81.867 1678-91-7 Ethylcyclohexane 0.037 0.035 0.031 10.074

101.322 1678-98-4 i-Butylcyclohexane 0.010 0.009 0.007 2.651

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.402 115-11-7 Isobutene 0.020 0.026 0.035 5.622

9.441 106-98-9 Butene-1 0.024 0.031 0.042 6.677

10.264 624-64-6 t-Butene-2 0.089 0.112 0.153 24.556

10.984 590-18-1 c-Butene-2 0.102 0.124 0.174 27.905

16.326 109-67-1 Pentene-1 0.323 0.382 0.443 88.811

18.796 646-04-8 t-Pentene-2 0.835 0.975 1.144 229.307

19.815 627-20-3 c-Pentene-2 0.456 0.527 0.625 125.356

32.936 592-41-6 Hexene-1 0.155 0.173 0.177 42.683

35.92813269-52-8 t-Hexene-3 0.256 0.284 0.292 70.339

36.399 4050-45-7 t-Hexene-2 0.484 0.537 0.553 133.118

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C-271
Hydrocarbon Expert V4.7 Fri Aug 27 15:55:27 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91320 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91320

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

n-Olefins 38.233 7688-21-3 c-Hexene-2 0.207 0.226 0.236 56.757

56.87914686-14-7 t-Heptene-3 0.016 0.018 0.016 4.478

88.481 C9-isoolefin 0.035 0.039 0.027 9.721

110.730 693-61-8 2-Undecene, (E)- 0.065 0.067 0.045 17.715

Iso-Olefins 13.124 563-45-1 3-Methylbutene-1 0.070 0.085 0.096 19.337

17.162 563-46-2 2-Methylbutene-1 0.507 0.590 0.694 139.210

20.488 513-35-9 2-Methylbutene-2 1.044 1.193 1.431 286.849

28.682 691-38-3 4-Methyl-c-pentene-2 0.044 0.049 0.050 12.103

29.336 674-76-0 4-Methyl-t-pentene-2 0.132 0.148 0.150 36.167

32.710 763-29-1 2-Methylpentene-1 0.224 0.248 0.256 61.558

36.895 625-27-4 2-Methylpentene-2 0.340 0.373 0.388 93.437

37.305 922-62-3 3-Methyl-c-pentene-2 0.260 0.282 0.297 71.432

39.578 3404-73-7 3,3-Dimethylpentene-1 0.311 0.335 0.304 85.343

46.154 3404-61-3 3-Methylhexene-1 0.011 0.012 0.011 3.112

46.741 3524-73-0 5-Methylhexene-1 0.080 0.087 0.078 21.944

48.80015840-60-5 2-Methyl-c-hexene-3 0.030 0.033 0.029 8.239

49.793 3404-55-5 4-Methyl-t/c-hexene-2 0.034 0.037 0.033 9.400

57.232 6094-02-6 2-Methylhexene-1 0.025 0.027 0.025 6.952

58.113 2738-19-4 2-Methyl-2-hexene 0.005 0.005 0.005 1.277

Naphtheno-Olefins 25.240 142-29-0 Cyclopentene 0.181 0.177 0.255 51.071

45.336 693-89-0 1-Methylcyclopentene 0.319 0.310 0.373 89.771

50.665 110-83-8 Cyclohexene 0.034 0.032 0.040 9.367

Di-Olefins 18.203 78-79-5 2-Methyl-1,3-Butadiene 0.009 0.010 0.012 2.473

20.820 2004-70-8 1t,3-Pentadiene 0.013 0.014 0.018 3.642

Oxygenates 26.477 71-23-8 n-Propanol 0.111 0.105 0.178 21.352

Unidentified 22.069 Unidentified 0.005 0.005 0.007 1.531

26.411 Unidentified 0.038 0.036 0.061 12.774

28.224 Unidentified 0.051 0.052 0.056 17.235

44.927 Unidentified 0.010 0.010 0.012 3.400

47.589 Unidentified 0.028 0.030 0.027 9.343

72.092 Unidentified 0.037 0.039 0.032 12.619

74.103 Unidentified 0.011 0.010 0.009 3.639

78.507 Unidentified 0.017 0.017 0.015 5.779

84.861 Unidentified 0.008 0.007 0.006 2.531

93.600 Unidentified 0.028 0.029 0.019 9.494

98.887 Unidentified 0.426 0.444 0.288 143.526

100.130 Unidentified 0.036 0.027 0.022 12.175

100.256 Unidentified 0.104 0.106 0.064 35.042

100.943 Unidentified 0.078 0.084 0.053 26.125

101.064 Unidentified 0.045 0.046 0.030 15.025

102.976 Unidentified 0.033 0.034 0.020 11.176

104.396 Unidentified 0.105 0.093 0.075 35.312

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C-272
Hydrocarbon Expert V4.7 Fri Aug 27 15:55:27 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91320 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91320

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Unidentified 107.889 Unidentified 0.083 0.084 0.051 27.896

108.165 Unidentified 0.095 0.097 0.059 31.866

108.246 Unidentified 0.085 0.087 0.052 28.648

108.552 Unidentified 0.225 0.229 0.138 75.739

108.987 Unidentified 0.837 0.722 0.600 281.737

110.529 Unidentified 0.029 0.027 0.018 9.678

110.861 Unidentified 0.077 0.078 0.052 25.772

111.799 Unidentified 0.073 0.062 0.047 24.589

112.649 Unidentified 0.014 0.012 0.009 4.800

112.788 Unidentified 0.022 0.018 0.016 7.298

113.295 Unidentified 0.040 0.041 0.023 13.337

113.449 Unidentified 0.012 0.012 0.007 4.069

114.980 Unidentified 0.027 0.023 0.018 9.117

126.173 Unidentified 0.007 0.006 0.004 2.416

126.173 Unidentified 0.007 0.007 0.003 2.416

Plus

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C-273
Hydrocarbon Expert V4.7 Fri Aug 27 15:55:27 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91320 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91320

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF

20.0 15.0 10.0 5.0 0.0

Propane

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

Unidentified

2,2-Dimethylbutane

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C-274
Hydrocarbon Expert V4.7 Fri Aug 27 15:55:27 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91320 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91320

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

Unidentified n-Propanol

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

n-Hexane

t-Hexene-3

t-Hexene-2

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane

2,2,3-Trimethylbutane

Unidentified Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1 Cyclohexane

Unidentified

2-Methyl-c-hexene-3

4-Methyl-t/c-hexene-2

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C-275
Hydrocarbon Expert V4.7 Fri Aug 27 15:55:27 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91320 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91320

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF

70.0 65.0 60.0 55.0 50.0

2-Methylhexane

Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane

2,2,4-Trimethylpentane

t-Heptene-3

2-Methylhexene-1

n-Heptane

2-Methyl-2-hexene

Methylcyclohexane

1,1,3-Trimethylcyclopentane

2,2-Dimethylhexane

Ethylcyclopentane

2,2,3-Trimethylpentane 2,5-Dimethylhexane

2,4-Dimethylhexane

1c,2t,4-Trimethylcyclopentane

2,3,4-Trimethylpentane

Toluene

2,3-Dimethylhexane

2-Methylheptane

Unidentified 4-Methylheptane

1,3-dimethyl-t-cyclohexane 3-Methylheptane 3-Ethylhexane

Unidentified

2,2,5-Trimethylhexane

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C-276
Hydrocarbon Expert V4.7 Fri Aug 27 15:55:27 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91320 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91320

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF

95.0 90.0 85.0 80.0 75.0

1t,3-Dimethylcyclohexane

n-Octane

Unidentified

2,3,5-Trimethylhexane

2,4-Dimethylheptane

Ethylcyclohexane

2,6-Dimethylheptane

2,5-Dimethylheptane

Ethylbenzene

Unidentified

m-Xylene p-Xylene

4-Methyloctane 2-Methyloctane

3-Methyloctane

C9-isoolefin o-Xylene

C10 - IsoParaffin - 1

2,2,4-trimethylheptane

n-Nonane

i-Propylbenzene

Unidentified 2,2-Dimethyloctane

2,4-Dimethyloctane

2,6-Dimethyloctane

n-Propylbenzene

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

4-Methylnonane Unidentified 1-Methyl-2-ethylbenzene

3-Methylnonane

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C-277
Hydrocarbon Expert V4.7 Fri Aug 27 15:55:27 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91320 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91320

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified

C11-Isoparaffin-2 1,2,4-Trimethylbenzene Unidentified

i-Butylcyclohexane

3-Ethyl-3-methylheptane i-Butylbenzene n-Decane Unidentified

1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene C11 Isoparaffin-4 Unidentified

Indan

Indene

C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene

1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

Unidentified 1-Methyl-2-n-propylbenzene Unidentified C11- Isoparaffin-11 Unidentified

1,4,Dimethyl-2-ethylbenzene Unidentified 2-Methylindan

1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

Unidentified 2-Undecene, (E)- Unidentified 1-Methyl-4-t-butylbenzene 1,2-Dimethyl-3-ethylbenzene n-Undecane Unidentified 1-Ethyl-4-i-propylbenzene

1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene Unidentified C12 - IsoParaffin - 1

Unidentified C11 - Aromatic - 3 5-Methylindan 1,2-Di-i-propylbenzene 1-methyl-4-(1-methylpropyl)be C11 - Aromatic - 4 4-Methylindan 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene 1-Methyl-2-n-butylbenzene C11 - Aromatic - 7

1,4-Di-i-propylbenzene

Naphthalene 4,7-Dimethyl Indane 1,1-Dimethyl Indane

1t-Butyl-4-ethylbenzene

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

C11 - Aromatic - 12

2-Methylnaphthalene

1-Methylnaphthalene

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C-278
Hydrocarbon Expert V4.7 Fri Aug 27 15:55:27 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91320 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91320

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG1000018.D\SIG1000018_FID1_A.CDF

145.0 140.0 135.0 130.0 125.0

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C-279
Hydrocarbon Expert V4.7 Thu Aug 26 16:41:24 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF 24-Aug-10, 17:46:58

Sample: ODDB-91321 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91321

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 10.491 11.676 12.131

I-Paraffins 43.167 46.627 43.041

Aromatics 25.125 20.714 21.444

Mono-Aromatics 23.036 19.123 19.847

Naphthalenes 0.129 0.091 0.093

Naphtheno/Olefino-Benzs 0.306 0.248 0.218

Indenes 1.654 1.252 1.285

Naphthenes 8.794 8.354 9.942

Mono-Naphthenes 8.794 8.354 9.942

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 7.782 8.327 9.682

n-Olefins 3.409 3.739 4.367

Iso-Olefins 3.609 3.872 4.379

Naphtheno-Olefins 0.724 0.675 0.883

Di-Olefins 0.040 0.042 0.052

Oxygenates 0.132 0.119 0.192

Unidentified 4.509 4.182 3.567

Plus 0.000 0.000 0.000

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C-280
Hydrocarbon Expert V4.7 Thu Aug 26 16:41:24 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF 24-Aug-10, 17:46:58

Sample: ODDB-91321 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91321

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C3 0.082 0.074 0.129

C4 0.744 0.896 1.207

C5 19.256 21.845 25.413

C6 23.872 24.945 26.466

C7 11.566 10.774 11.420

C8 24.611 24.311 20.711

C9 5.555 4.684 4.341

C10 7.232 5.939 5.168

C11 2.325 2.144 1.433

C12 0.249 0.207 0.144

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C-281
Hydrocarbon Expert V4.7 Thu Aug 26 16:41:24 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF 24-Aug-10, 17:46:58

Sample: ODDB-91321 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91321

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C3 0.001 0.001 0.002

C4 0.379 0.473 0.616

C5 2.987 3.446 3.908

C6 6.286 6.888 6.887

C7 0.502 0.530 0.473

C8 0.144 0.148 0.119

C9 0.062 0.063 0.046

C10 0.042 0.042 0.028

C11 0.088 0.086 0.053

I-Paraffins C4 0.035 0.045 0.056

C5 10.747 12.534 14.062

C6 8.301 9.115 9.093

C7 3.307 3.516 3.116

C8 18.410 19.094 15.215

C9 0.436 0.443 0.321

C10 0.448 0.440 0.284

C11 1.451 1.409 0.877

C12 0.032 0.031 0.018

Mono-Aromatics C6 0.652 0.536 0.788

C7 5.884 4.903 6.029

C8 5.884 4.907 5.232

C9 4.884 4.048 3.836

C10 4.859 4.017 3.418

C11 0.664 0.543 0.423

C12 0.208 0.169 0.121

Naphthalenes C10 0.109 0.077 0.080

C11 0.020 0.014 0.013

Naphtheno/Olefino-Benzs C10 0.306 0.248 0.218

Indenes C9 0.167 0.125 0.134

C10 1.447 1.097 1.126

C11 0.030 0.023 0.020

C12 0.009 0.006 0.006

Mono-Naphthenes C5 1.519 1.472 2.044

C6 5.809 5.496 6.516

C7 1.268 1.202 1.219

C8 0.173 0.162 0.145

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C-282
Hydrocarbon Expert V4.7 Thu Aug 26 16:41:24 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF 24-Aug-10, 17:46:58

Sample: ODDB-91321 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91321

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Mono-Naphthenes C9 0.005 0.004 0.004

C10 0.020 0.018 0.014

n-Olefins C4 0.280 0.331 0.470

C5 1.879 2.092 2.529

C6 1.162 1.228 1.303

C7 0.018 0.018 0.017

C11 0.071 0.069 0.048

Iso-Olefins C5 1.883 2.071 2.535

C6 1.154 1.212 1.295

C7 0.572 0.589 0.550

Naphtheno-Olefins C5 0.216 0.203 0.299

C6 0.508 0.472 0.584

Di-Olefins C5 0.025 0.027 0.035

C7 0.015 0.015 0.017

Oxygenates C3 0.081 0.073 0.127

C4 0.051 0.046 0.065

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C-283
Hydrocarbon Expert V4.7 Thu Aug 26 16:41:24 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF 24-Aug-10, 17:46:58

Sample: ODDB-91321 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91321

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 32.41 29.23

5% 80.02 79.81

10% 81.54 81.11

15% 96.23 93.70

20% 120.18 100.22

25% 140.09 137.63

30% 153.23 144.34

35% 155.20 154.35

40% 161.11 155.40

45% 177.26 172.56

50% 209.20 190.14

55% 209.71 209.29

60% 210.23 209.78

65% 228.48 210.28

70% 230.98 228.77

75% 257.41 231.05

80% 282.29 277.93

85% 332.39 321.66

90% 352.22 348.98

95% 365.79 363.20

FBP 404.60 404.08

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C-284
Hydrocarbon Expert V4.7 Thu Aug 26 16:41:24 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF 24-Aug-10, 17:46:58

Sample: ODDB-91321 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91321

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 7.553 74-98-6 P3 Propane 0.001 0.001 0.002 0.235

2 8.810 75-28-5 I4 i-Butane 0.035 0.045 0.056 9.068

3 9.623 115-11-7 K4 Isobutene 0.026 0.031 0.043 7.006

4 9.664 106-98-9 K4 Butene-1 0.028 0.034 0.047 7.552

5 10.024 106-97-8 P4 n-Butane 0.379 0.473 0.616 99.231

6 10.510 624-64-6 K4 t-Butene-2 0.106 0.127 0.179 28.830

7 10.637 463-82-1 I5 2,2-Dimethylpropane 0.040 0.048 0.052 10.455

8 11.252 590-18-1 K4 c-Butene-2 0.119 0.139 0.201 32.379

9 13.455 563-45-1 C5 3-Methylbutene-1 0.081 0.094 0.110 22.084

10 15.090 78-78-4 I5 i-Pentane 10.707 12.485 14.010 2821.802

11 16.729 109-67-1 K5 Pentene-1 0.377 0.426 0.508 102.255

12 17.582 563-46-2 C5 2-Methylbutene-1 0.589 0.654 0.792 159.588

13 18.121 109-66-0 P5 n-Pentane 2.987 3.446 3.908 787.160

14 18.628 78-79-5 E5 2-Methyl-1,3-Butadiene 0.010 0.011 0.014 2.801

15 19.239 646-04-8 K5 t-Pentene-2 0.971 1.082 1.307 263.114

16 19.883 ? Unidentified 0.007 0.008 0.009 2.310

17 20.272 627-20-3 K5 c-Pentene-2 0.531 0.585 0.715 143.898

18 20.947 513-35-9 C5 2-Methylbutene-2 1.213 1.323 1.633 328.791

19 21.277 2004-70-8 E5 1t,3-Pentadiene 0.015 0.016 0.021 4.277

20 22.539 1574-41-0 B5 1,3-Cyclopentadiene 0.006 0.007 0.009 1.746

21 23.096 75-83-2 I6 2,2-Dimethylbutane 0.612 0.681 0.671 161.972

22 25.742 142-29-0 B5 Cyclopentene 0.210 0.196 0.290 58.464

23 26.912 71-23-8 X3 n-Propanol 0.081 0.073 0.127 15.363

24 26.992 ? Unidentified 0.071 0.077 0.080 23.617

25 27.612 287-92-3 M5 Cyclopentane 1.519 1.472 2.044 411.671

26 28.339 79-29-8 I6 2,3-Dimethylbutane 0.857 0.936 0.938 226.672

27 28.738 ? Unidentified 0.065 0.064 0.070 21.715

28 29.205 691-38-3 C6 4-Methyl-c-pentene-2 0.053 0.057 0.059 14.376

29 29.427 107-83-5 I6 2-Methylpentane 3.627 4.012 3.973 959.623

30 29.847 674-76-0 C6 4-Methyl-t-pentene-2 0.152 0.163 0.171 41.215

31 32.083 96-14-0 I6 3-Methylpentane 3.205 3.486 3.511 847.965

32 33.234 763-29-1 C6 2-Methylpentene-1 0.259 0.273 0.290 70.189

33 33.459 592-41-6 K6 Hexene-1 0.176 0.187 0.197 47.682

34 35.847 110-54-3 P6 n-Hexane 6.286 6.888 6.887 1663.319

35 36.44513269-52-8 K6 t-Hexene-3 0.295 0.313 0.331 80.091

36 36.921 4050-45-7 K6 t-Hexene-2 0.452 0.479 0.508 122.651

37 37.045 1120-62-3 B6 3-Methylcyclopentene 0.107 0.101 0.123 28.971

38 37.412 625-27-4 C6 2-Methylpentene-2 0.392 0.410 0.440 106.242

39 37.828 922-62-3 C6 3-Methyl-c-pentene-2 0.298 0.309 0.335 80.887

40 38.749 7688-21-3 K6 c-Hexene-2 0.238 0.248 0.267 64.468

41 40.098 3404-73-7 C7 3,3-Dimethylpentene-1 0.353 0.364 0.340 95.773

42 40.687 96-37-7 M6 Methylcyclopentane 2.831 2.732 3.175 767.258

43 42.240 108-08-7 I7 2,4-Dimethylpentane 0.582 0.625 0.548 154.532

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C-285
Hydrocarbon Expert V4.7 Thu Aug 26 16:41:24 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF 24-Aug-10, 17:46:58

Sample: ODDB-91321 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91321

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 42.538 594-56-9 C7 2,3,3-Trimethylbutene-1 0.013 0.013 0.012 3.408

45 42.784 464-06-2 I7 2,2,3-Trimethylbutane 0.064 0.067 0.060 17.052

46 45.435 1528-30-9 E7 C6-Diolefin-1 0.015 0.015 0.017 4.082

47 45.641 71-42-3 Q6 Benzene 0.652 0.536 0.788 190.432

48 45.840 693-89-0 B6 1-Methylcyclopentene 0.362 0.336 0.417 100.617

49 46.649 3404-61-3 C7 3-Methylhexene-1 0.013 0.014 0.013 3.607

50 47.245 3524-73-0 C7 5-Methylhexene-1 0.082 0.085 0.078 22.121

51 47.577 110-82-7 M6 Cyclohexane 2.978 2.764 3.341 807.279

52 48.063 71-36-3 X4 n-Butanol 0.051 0.046 0.065 10.479

53 49.27815840-60-5 C7 2-Methyl-c-hexene-3 0.035 0.036 0.033 9.363

54 50.273 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.041 0.042 0.039 11.053

55 50.679 591-76-4 I7 2-Methylhexane 1.937 2.062 1.825 514.592

56 51.161 110-83-8 B6 Cyclohexene 0.039 0.035 0.045 10.544

57 52.502 589-34-4 I7 3-Methylhexane 0.724 0.762 0.682 192.398

58 53.360 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.150 0.145 0.144 40.687

59 53.947 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.118 0.115 0.114 32.108

60 54.572 822-50-4 M7 1t,2-Dimethylcyclopentane 0.177 0.170 0.170 47.914

61 55.260 540-84-1 I8 2,2,4-Trimethylpentane 13.971 14.589 11.546 3718.827

62 57.34014686-14-7 K7 t-Heptene-3 0.018 0.018 0.017 4.826

63 57.685 6094-02-6 C7 2-Methylhexene-1 0.028 0.029 0.027 7.647

64 58.062 142-82-5 P7 n-Heptane 0.502 0.530 0.473 133.309

65 58.555 2738-19-4 C7 2-Methyl-2-hexene 0.007 0.007 0.007 1.965

66 59.882 ? Unidentified 0.278 0.280 0.267 92.350

67 61.523 108-87-2 M7 Methylcyclohexane 0.795 0.746 0.764 215.396

68 62.463 4516-69-2 M8 1,1,3-Trimethylcyclopentane 0.016 0.016 0.014 4.465

69 62.852 590-73-8 I8 2,2-Dimethylhexane 0.016 0.016 0.013 4.183

70 64.072 ? Unidentified 0.075 0.073 0.064 24.985

71 64.305 1640-89-7 M7 Ethylcyclopentane 0.028 0.026 0.027 7.559

72 64.953 564-02-3 I8 2,2,3-Trimethylpentane 0.277 0.279 0.229 73.640

73 65.180 592-13-2 I8 2,5-Dimethylhexane 0.748 0.780 0.619 199.218

74 65.518 589-43-5 I8 2,4-Dimethylhexane 0.620 0.640 0.513 165.139

75 66.352 4850-28-6 M8 1c,2t,4-Trimethylcyclopentane 0.015 0.014 0.013 4.144

76 66.745 563-16-6 I8 3,3-Dimethylhexane 0.011 0.011 0.009 2.828

77 67.86415890-40-1 M8 1t,2c,3-Trimethylcyclopentane 0.012 0.011 0.010 3.129

78 68.484 565-75-3 I8 2,3,4-Trimethylpentane 1.267 1.273 1.047 337.123

79 69.030 108-88-3 Q7 Toluene 5.884 4.903 6.029 1699.030

80 69.156 560-21-4 I8 2,3,3-Trimethylpentane 0.944 0.939 0.780 251.324

81 70.796 584-94-1 I8 2,3-Dimethylhexane 0.277 0.281 0.229 73.630

82 72.048 592-27-8 I8 2-Methylheptane 0.092 0.095 0.076 24.474

83 72.309 589-53-7 I8 4-Methylheptane 0.056 0.057 0.046 14.917

84 72.451 ? Unidentified 0.018 0.018 0.015 6.056

85 73.227 M8 1,3-dimethyl-t-cyclohexane 0.068 0.064 0.057 18.470

86 73.364 589-81-1 I8 3-Methylheptane 0.086 0.088 0.071 22.762

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C-286
Hydrocarbon Expert V4.7 Thu Aug 26 16:41:24 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF 24-Aug-10, 17:46:58

Sample: ODDB-91321 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91321

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 73.563 619-99-8 I8 3-Ethylhexane 0.046 0.047 0.038 12.239

88 74.463 ? Unidentified 0.011 0.010 0.009 3.534

89 75.251 3522-94-9 I9 2,2,5-Trimethylhexane 0.294 0.300 0.216 78.349

90 76.533 2207-03-6 M8 1t,3-Dimethylcyclohexane 0.027 0.025 0.022 7.184

91 77.871 111-65-9 P8 n-Octane 0.144 0.148 0.119 38.212

92 78.825 ? Unidentified 0.007 0.007 0.006 2.319

93 80.355 1069-53-0 I9 2,3,5-Trimethylhexane 0.043 0.043 0.032 11.415

94 81.522 1071-26-7 I9 2,4-Dimethylheptane 0.012 0.013 0.009 3.281

95 82.177 1678-91-7 M8 Ethylcyclohexane 0.035 0.032 0.029 9.472

96 82.478 1072-05-5 I9 2,6-Dimethylheptane 0.018 0.018 0.013 4.765

97 83.408 I9 2,5-Dimethylheptane 0.028 0.029 0.021 7.530

98 84.734 100-41-4 Q8 Ethylbenzene 1.104 0.920 0.982 316.388

99 85.151 ? Unidentified 0.005 0.005 0.004 1.742

100 85.959 108-38-3 Q8 m-Xylene 2.669 2.231 2.373 764.768

101 86.105 106-42-3 Q8 p-Xylene 1.242 1.042 1.105 355.958

102 87.276 2216-34-4 I9 4-Methyloctane 0.011 0.011 0.008 2.940

103 87.407 3221-61-2 I9 2-Methyloctane 0.014 0.015 0.011 3.853

104 88.272 2216-33-3 I9 3-Methyloctane 0.015 0.015 0.011 4.114

105 88.746 ? Unidentified 0.009 0.009 0.006 2.830

106 88.930 95-47-6 Q8 o-Xylene 0.869 0.714 0.773 249.125

107 89.324 I10 C10 - IsoParaffin - 1 0.035 0.035 0.024 9.468

108 89.913 M9 trans-1,3-Diethylcyclopentane 0.005 0.004 0.004 1.560

109 90.16814720-74-2 I10 2,2,4-trimethylheptane 0.031 0.030 0.020 8.169

110 91.737 111-84-2 P9 n-Nonane 0.062 0.063 0.046 16.584

111 93.096 98-82-8 Q9 i-Propylbenzene 0.032 0.026 0.025 8.984

112 93.843 ? Unidentified 0.043 0.043 0.029 14.413

113 94.06615869-87-1 I10 2,2-Dimethyloctane 0.016 0.016 0.011 4.374

114 94.527 ? Unidentified 0.004 0.003 0.411 1.444

115 94.527 ? Unidentified 0.004 0.004 0.003 1.444

116 94.86215869-89-3 I10 2,5-Dimethyloctane 0.019 0.019 0.013 5.116

117 95.327 2040-95-1 I10 2,7-Dimethyloctane 0.015 0.015 0.010 3.998

118 95.508 2051-30-1 I10 2,4-Dimethyloctane 0.068 0.068 0.045 18.171

119 95.895 I10 2,6-Dimethyloctane 0.020 0.020 0.013 5.383

120 96.555 103-65-1 Q9 n-Propylbenzene 0.249 0.209 0.196 70.985

121 97.401 620-14-4 Q9 1-Methyl-3-ethylbenzene 0.939 0.785 0.738 267.484

122 97.635 622-96-8 Q9 1-Methyl-4-ethylbenzene 0.446 0.374 0.350 126.991

123 98.261 108-67-8 Q9 1,3,5-Trimethylbenzene 0.608 0.507 0.477 173.016

124 98.91117301-94-8 I10 4-Methylnonane 0.010 0.010 0.007 2.667

125 99.122 ? Unidentified 0.998 0.993 0.662 331.444

126 99.347 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.366 0.300 0.288 104.234

127 99.704 ? Unidentified 0.003 0.003 0.002 1.104

128 99.889 5911-04-6 I10 3-Methylnonane 0.014 0.013 0.009 3.649

129 100.354 ? Unidentified 0.079 0.057 0.048 26.357

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C-287
Hydrocarbon Expert V4.7 Thu Aug 26 16:41:24 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF 24-Aug-10, 17:46:58

Sample: ODDB-91321 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91321

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 100.486 ? Unidentified 0.219 0.213 0.133 72.879

131 100.703 I11 C11-Isoparaffin-2 0.117 0.113 0.070 31.207

132 100.980 95-63-6 Q9 1,2,4-Trimethylbenzene 1.887 1.557 1.482 537.379

133 101.167 ? Unidentified 0.148 0.152 0.099 49.063

134 101.289 ? Unidentified 0.085 0.084 0.057 28.354

135 101.553 1678-98-4 M10 i-Butylcyclohexane 0.020 0.018 0.014 5.475

136 102.195 ? Unidentified 0.008 0.008 0.006 2.786

137 102.33917302-01-1 I10 3-Ethyl-3-methylheptane 0.220 0.213 0.133 58.813

138 102.548 ? Unidentified 0.059 0.057 0.036 19.569

139 102.686 538-93-2 Q10 i-Butylbenzene 0.195 0.165 0.137 55.333

140 102.899 124-18-5 P10 n-Decane 0.042 0.042 0.028 11.236

141 103.201 ? Unidentified 0.058 0.057 0.039 19.391

142 103.689 ? Unidentified 0.008 0.007 0.007 2.795

143 103.854 526-73-8 Q9 1,2,3-Trimethylbenzene 0.357 0.288 0.280 101.644

144 104.204 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.025 0.021 0.018 7.074

145 104.412 I11 C11 Isoparaffin-4 0.030 0.029 0.018 7.968

146 104.619 99-87-6 Q10 1-Methyl-4-i-propylbenzene 0.194 0.164 0.137 55.009

147 105.048 J9 Indan 0.167 0.125 0.134 48.420

148 105.648 J10 Indene 1.086 0.814 0.868 314.254

149 106.205 ? Unidentified 0.008 0.007 0.005 2.588

150 106.362 I11 C11-Isoparaffin-7 0.445 0.432 0.269 118.933

151 106.551 141-93-5 Q10 1,3-Diethylbenzene 0.057 0.048 0.040 16.096

152 106.843 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 1.291 1.084 0.908 365.741

153 107.109 105-05-5 Q10 1,4-Diethylbenzene 0.425 0.356 0.299 120.424

154 107.386 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.182 0.149 0.128 51.507

155 107.623 135-01-3 Q10 1,2-Diethylbenzene 0.106 0.087 0.075 30.062

156 108.086 ? Unidentified 0.111 0.107 0.067 36.719

157 108.237 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.073 0.060 0.051 20.594

158 108.361 ? Unidentified 0.123 0.099 0.096 40.729

159 108.440 ? Unidentified 0.117 0.113 0.070 38.722

160 108.569 I11 C11- Isoparaffin-11 0.860 0.836 0.520 230.181

161 108.749 ? Unidentified 0.291 0.283 0.176 96.728

162 109.173 ? Unidentified 1.032 0.850 0.726 342.565

163 109.398 J10 2-Methylindan 0.158 0.118 0.113 45.732

164 109.745 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.489 0.404 0.344 138.531

165 109.872 ? Unidentified 0.039 0.032 0.027 12.898

166 109.968 ? Unidentified 0.030 0.022 0.021 9.926

167 110.290 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.846 0.686 0.595 239.497

168 110.713 ? Unidentified 0.028 0.025 0.017 9.282

169 110.908 693-61-8 K11 2-Undecene, (E)- 0.071 0.069 0.048 19.099

170 111.042 ? Unidentified 0.161 0.157 0.108 53.412

171 111.313 ? Unidentified 0.138 0.112 0.088 45.861

172 111.414 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.114 0.092 0.080 32.246

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C-288
Hydrocarbon Expert V4.7 Thu Aug 26 16:41:24 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF 24-Aug-10, 17:46:58

Sample: ODDB-91321 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91321

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 111.714 1120-21-4 P11 n-Undecane 0.088 0.086 0.053 23.597

174 111.864 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.110 0.089 0.070 31.016

175 111.975 ? Unidentified 0.064 0.052 0.041 21.126

176 112.352 Q10 1,2,4,5-Tetramethylbenzene 0.364 0.296 0.256 102.987

177 112.618 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.498 0.404 0.350 141.055

178 112.825 ? Unidentified 0.012 0.010 0.008 4.127

179 112.958 ? Unidentified 0.017 0.014 0.012 5.787

180 113.132 I12 C12 - IsoParaffin - 1 0.027 0.027 0.015 7.355

181 113.481 ? Unidentified 0.039 0.038 0.021 12.854

182 113.614 ? Unidentified 0.012 0.012 0.007 4.006

183 113.761 Q11 C11 - Aromatic - 3 0.098 0.080 0.063 27.733

184 113.948 874-35-1 H10 5-Methylindan 0.153 0.124 0.109 43.398

185 114.072 Q12 1,2-Di-i-propylbenzene 0.066 0.053 0.038 18.466

186 114.287 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.092 0.074 0.058 25.870

187 114.449 Q11 C11 - Aromatic - 4 0.053 0.043 0.034 14.853

188 114.697 824-22-6 J10 4-Methylindan 0.203 0.165 0.145 57.573

189 114.849 5161-04-6 Q11 Benzene, 1-methyl-4-(2-methylpropyl)-0.058 0.047 0.037 16.408

190 114.944 824-63-5 H10 2-Methylindan 0.153 0.124 0.109 43.236

191 115.147 ? Unidentified 0.018 0.015 0.012 6.016

192 115.259 538-68-1 Q11 n-Pentylbenzene 0.023 0.018 0.014 6.387

193 115.488 Q11 tert-Pentylbenzene 0.091 0.074 0.058 25.596

194 115.800 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.038 0.031 0.024 10.842

195 115.910 Q11 C11 - Aromatic - 7 0.051 0.043 0.032 14.356

196 116.245 I12 C12 - IsoParaffin - 4 0.005 0.004 0.003 1.312

197 116.370 100-18-5 Q12 1,4-Di-i-propylbenzene 0.073 0.059 0.043 20.562

198 116.812 91-20-3 G10 Naphthalene 0.109 0.077 0.080 32.240

199 116.948 J11 4,7-Dimethyl Indane 0.008 0.006 0.005 2.403

200 117.242 J11 1,1-Dimethyl Indane 0.022 0.017 0.014 6.416

201 117.414 J12 Dimethyl Indane - 1 0.009 0.006 0.006 2.471

202 117.594 7364-19-4 Q12 1t-Butyl-4-ethylbenzene 0.013 0.011 0.008 3.785

203 117.894 Q12 1,3-Di-n-propylbenzene 0.056 0.045 0.033 15.718

204 118.006 Q11 C11 - Aromatic - 11 0.031 0.027 0.020 8.794

205 118.559 Q11 C11 - Aromatic - 12 0.019 0.016 0.012 5.268

206 123.439 91-57-6 G11 2-Methylnaphthalene 0.013 0.009 0.009 3.794

207 124.306 90-12-0 G11 1-Methylnaphthalene 0.007 0.005 0.005 2.049

208 130.002 ? Unidentified 0.004 0.003 0.002 1.337

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C-289
Hydrocarbon Expert V4.7 Thu Aug 26 16:41:24 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF 24-Aug-10, 17:46:58

Sample: ODDB-91321 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91321

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 7.553 74-98-6 Propane 0.001 0.001 0.002 0.235

10.024 106-97-8 n-Butane 0.379 0.473 0.616 99.231

18.121 109-66-0 n-Pentane 2.987 3.446 3.908 787.160

35.847 110-54-3 n-Hexane 6.286 6.888 6.887 1663.319

58.062 142-82-5 n-Heptane 0.502 0.530 0.473 133.309

77.871 111-65-9 n-Octane 0.144 0.148 0.119 38.212

91.737 111-84-2 n-Nonane 0.062 0.063 0.046 16.584

102.899 124-18-5 n-Decane 0.042 0.042 0.028 11.236

111.714 1120-21-4 n-Undecane 0.088 0.086 0.053 23.597

I-Paraffins 8.810 75-28-5 i-Butane 0.035 0.045 0.056 9.068

10.637 463-82-1 2,2-Dimethylpropane 0.040 0.048 0.052 10.455

15.090 78-78-4 i-Pentane 10.707 12.485 14.010 2821.802

23.096 75-83-2 2,2-Dimethylbutane 0.612 0.681 0.671 161.972

28.339 79-29-8 2,3-Dimethylbutane 0.857 0.936 0.938 226.672

29.427 107-83-5 2-Methylpentane 3.627 4.012 3.973 959.623

32.083 96-14-0 3-Methylpentane 3.205 3.486 3.511 847.965

42.240 108-08-7 2,4-Dimethylpentane 0.582 0.625 0.548 154.532

42.784 464-06-2 2,2,3-Trimethylbutane 0.064 0.067 0.060 17.052

50.679 591-76-4 2-Methylhexane 1.937 2.062 1.825 514.592

52.502 589-34-4 3-Methylhexane 0.724 0.762 0.682 192.398

55.260 540-84-1 2,2,4-Trimethylpentane 13.971 14.589 11.546 3718.827

62.852 590-73-8 2,2-Dimethylhexane 0.016 0.016 0.013 4.183

64.953 564-02-3 2,2,3-Trimethylpentane 0.277 0.279 0.229 73.640

65.180 592-13-2 2,5-Dimethylhexane 0.748 0.780 0.619 199.218

65.518 589-43-5 2,4-Dimethylhexane 0.620 0.640 0.513 165.139

66.745 563-16-6 3,3-Dimethylhexane 0.011 0.011 0.009 2.828

68.484 565-75-3 2,3,4-Trimethylpentane 1.267 1.273 1.047 337.123

69.156 560-21-4 2,3,3-Trimethylpentane 0.944 0.939 0.780 251.324

70.796 584-94-1 2,3-Dimethylhexane 0.277 0.281 0.229 73.630

72.048 592-27-8 2-Methylheptane 0.092 0.095 0.076 24.474

72.309 589-53-7 4-Methylheptane 0.056 0.057 0.046 14.917

73.364 589-81-1 3-Methylheptane 0.086 0.088 0.071 22.762

73.563 619-99-8 3-Ethylhexane 0.046 0.047 0.038 12.239

75.251 3522-94-9 2,2,5-Trimethylhexane 0.294 0.300 0.216 78.349

80.355 1069-53-0 2,3,5-Trimethylhexane 0.043 0.043 0.032 11.415

81.522 1071-26-7 2,4-Dimethylheptane 0.012 0.013 0.009 3.281

82.478 1072-05-5 2,6-Dimethylheptane 0.018 0.018 0.013 4.765

83.408 2,5-Dimethylheptane 0.028 0.029 0.021 7.530

87.276 2216-34-4 4-Methyloctane 0.011 0.011 0.008 2.940

87.407 3221-61-2 2-Methyloctane 0.014 0.015 0.011 3.853

88.272 2216-33-3 3-Methyloctane 0.015 0.015 0.011 4.114

89.324 C10 - IsoParaffin - 1 0.035 0.035 0.024 9.468

90.16814720-74-2 2,2,4-trimethylheptane 0.031 0.030 0.020 8.169

94.06615869-87-1 2,2-Dimethyloctane 0.016 0.016 0.011 4.374

94.86215869-89-3 2,5-Dimethyloctane 0.019 0.019 0.013 5.116

95.327 2040-95-1 2,7-Dimethyloctane 0.015 0.015 0.010 3.998

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C-290
Hydrocarbon Expert V4.7 Thu Aug 26 16:41:24 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF 24-Aug-10, 17:46:58

Sample: ODDB-91321 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91321

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

I-Paraffins 95.508 2051-30-1 2,4-Dimethyloctane 0.068 0.068 0.045 18.171

95.895 2,6-Dimethyloctane 0.020 0.020 0.013 5.383

98.91117301-94-8 4-Methylnonane 0.010 0.010 0.007 2.667

99.889 5911-04-6 3-Methylnonane 0.014 0.013 0.009 3.649

100.703 C11-Isoparaffin-2 0.117 0.113 0.070 31.207

102.33917302-01-1 3-Ethyl-3-methylheptane 0.220 0.213 0.133 58.813

104.412 C11 Isoparaffin-4 0.030 0.029 0.018 7.968

106.362 C11-Isoparaffin-7 0.445 0.432 0.269 118.933

108.569 C11- Isoparaffin-11 0.860 0.836 0.520 230.181

113.132 C12 - IsoParaffin - 1 0.027 0.027 0.015 7.355

116.245 C12 - IsoParaffin - 4 0.005 0.004 0.003 1.312

Aromatics

Mono-Aromatics 45.641 71-42-3 Benzene 0.652 0.536 0.788 190.432

69.030 108-88-3 Toluene 5.884 4.903 6.029 1699.030

84.734 100-41-4 Ethylbenzene 1.104 0.920 0.982 316.388

85.959 108-38-3 m-Xylene 2.669 2.231 2.373 764.768

86.105 106-42-3 p-Xylene 1.242 1.042 1.105 355.958

88.930 95-47-6 o-Xylene 0.869 0.714 0.773 249.125

93.096 98-82-8 i-Propylbenzene 0.032 0.026 0.025 8.984

96.555 103-65-1 n-Propylbenzene 0.249 0.209 0.196 70.985

97.401 620-14-4 1-Methyl-3-ethylbenzene 0.939 0.785 0.738 267.484

97.635 622-96-8 1-Methyl-4-ethylbenzene 0.446 0.374 0.350 126.991

98.261 108-67-8 1,3,5-Trimethylbenzene 0.608 0.507 0.477 173.016

99.347 611-14-3 1-Methyl-2-ethylbenzene 0.366 0.300 0.288 104.234

100.980 95-63-6 1,2,4-Trimethylbenzene 1.887 1.557 1.482 537.379

102.686 538-93-2 i-Butylbenzene 0.195 0.165 0.137 55.333

103.854 526-73-8 1,2,3-Trimethylbenzene 0.357 0.288 0.280 101.644

104.204 535-77-3 1-Methyl-3-i-propylbenzene 0.025 0.021 0.018 7.074

104.619 99-87-6 1-Methyl-4-i-propylbenzene 0.194 0.164 0.137 55.009

106.551 141-93-5 1,3-Diethylbenzene 0.057 0.048 0.040 16.096

106.843 1074-43-7 1-Methyl-3-n-propylbenzene 1.291 1.084 0.908 365.741

107.109 105-05-5 1,4-Diethylbenzene 0.425 0.356 0.299 120.424

107.386 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.182 0.149 0.128 51.507

107.623 135-01-3 1,2-Diethylbenzene 0.106 0.087 0.075 30.062

108.237 1074-17-5 1-Methyl-2-n-propylbenzene 0.073 0.060 0.051 20.594

109.745 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.489 0.404 0.344 138.531

110.290 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.846 0.686 0.595 239.497

111.414 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.114 0.092 0.080 32.246

111.864 4218-48-8 1-Ethyl-4-i-propylbenzene 0.110 0.089 0.070 31.016

112.352 1,2,4,5-Tetramethylbenzene 0.364 0.296 0.256 102.987

112.618 527-53-7 1,2,3,5-Tetramethylbenzene 0.498 0.404 0.350 141.055

113.761 C11 - Aromatic - 3 0.098 0.080 0.063 27.733

114.072 1,2-Di-i-propylbenzene 0.066 0.053 0.038 18.466

114.287 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.092 0.074 0.058 25.870

114.449 C11 - Aromatic - 4 0.053 0.043 0.034 14.853

114.849 5161-04-6 Benzene, 1-methyl-4-(2-methylpropyl)-0.058 0.047 0.037 16.408

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C-291
Hydrocarbon Expert V4.7 Thu Aug 26 16:41:24 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF 24-Aug-10, 17:46:58

Sample: ODDB-91321 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91321

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 115.259 538-68-1 n-Pentylbenzene 0.023 0.018 0.014 6.387

115.488 tert-Pentylbenzene 0.091 0.074 0.058 25.596

115.800 577-55-9 1-Methyl-2-n-butylbenzene 0.038 0.031 0.024 10.842

115.910 C11 - Aromatic - 7 0.051 0.043 0.032 14.356

116.370 100-18-5 1,4-Di-i-propylbenzene 0.073 0.059 0.043 20.562

117.594 7364-19-4 1t-Butyl-4-ethylbenzene 0.013 0.011 0.008 3.785

117.894 1,3-Di-n-propylbenzene 0.056 0.045 0.033 15.718

118.006 C11 - Aromatic - 11 0.031 0.027 0.020 8.794

118.559 C11 - Aromatic - 12 0.019 0.016 0.012 5.268

Naphthalenes 116.812 91-20-3 Naphthalene 0.109 0.077 0.080 32.240

123.439 91-57-6 2-Methylnaphthalene 0.013 0.009 0.009 3.794

124.306 90-12-0 1-Methylnaphthalene 0.007 0.005 0.005 2.049

Naphtheno/Olefino-Benzs 113.948 874-35-1 5-Methylindan 0.153 0.124 0.109 43.398

114.944 824-63-5 2-Methylindan 0.153 0.124 0.109 43.236

Indenes 105.048 Indan 0.167 0.125 0.134 48.420

105.648 Indene 1.086 0.814 0.868 314.254

109.398 2-Methylindan 0.158 0.118 0.113 45.732

114.697 824-22-6 4-Methylindan 0.203 0.165 0.145 57.573

116.948 4,7-Dimethyl Indane 0.008 0.006 0.005 2.403

117.242 1,1-Dimethyl Indane 0.022 0.017 0.014 6.416

117.414 Dimethyl Indane - 1 0.009 0.006 0.006 2.471

Naphthenes

Mono-Naphthenes 27.612 287-92-3 Cyclopentane 1.519 1.472 2.044 411.671

40.687 96-37-7 Methylcyclopentane 2.831 2.732 3.175 767.258

47.577 110-82-7 Cyclohexane 2.978 2.764 3.341 807.279

53.360 1759-58-6 1t,3-Dimethylcyclopentane 0.150 0.145 0.144 40.687

53.947 2532-58-3 1c,3-Dimethylcyclopentane 0.118 0.115 0.114 32.108

54.572 822-50-4 1t,2-Dimethylcyclopentane 0.177 0.170 0.170 47.914

61.523 108-87-2 Methylcyclohexane 0.795 0.746 0.764 215.396

62.463 4516-69-2 1,1,3-Trimethylcyclopentane 0.016 0.016 0.014 4.465

64.305 1640-89-7 Ethylcyclopentane 0.028 0.026 0.027 7.559

66.352 4850-28-6 1c,2t,4-Trimethylcyclopentane 0.015 0.014 0.013 4.144

67.86415890-40-1 1t,2c,3-Trimethylcyclopentane 0.012 0.011 0.010 3.129

73.227 1,3-dimethyl-t-cyclohexane 0.068 0.064 0.057 18.470

76.533 2207-03-6 1t,3-Dimethylcyclohexane 0.027 0.025 0.022 7.184

82.177 1678-91-7 Ethylcyclohexane 0.035 0.032 0.029 9.472

89.913 trans-1,3-Diethylcyclopentane 0.005 0.004 0.004 1.560

101.553 1678-98-4 i-Butylcyclohexane 0.020 0.018 0.014 5.475

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.623 115-11-7 Isobutene 0.026 0.031 0.043 7.006

9.664 106-98-9 Butene-1 0.028 0.034 0.047 7.552

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C-292
Hydrocarbon Expert V4.7 Thu Aug 26 16:41:24 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF 24-Aug-10, 17:46:58

Sample: ODDB-91321 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91321

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

n-Olefins 10.510 624-64-6 t-Butene-2 0.106 0.127 0.179 28.830

11.252 590-18-1 c-Butene-2 0.119 0.139 0.201 32.379

16.729 109-67-1 Pentene-1 0.377 0.426 0.508 102.255

19.239 646-04-8 t-Pentene-2 0.971 1.082 1.307 263.114

20.272 627-20-3 c-Pentene-2 0.531 0.585 0.715 143.898

33.459 592-41-6 Hexene-1 0.176 0.187 0.197 47.682

36.44513269-52-8 t-Hexene-3 0.295 0.313 0.331 80.091

36.921 4050-45-7 t-Hexene-2 0.452 0.479 0.508 122.651

38.749 7688-21-3 c-Hexene-2 0.238 0.248 0.267 64.468

57.34014686-14-7 t-Heptene-3 0.018 0.018 0.017 4.826

110.908 693-61-8 2-Undecene, (E)- 0.071 0.069 0.048 19.099

Iso-Olefins 13.455 563-45-1 3-Methylbutene-1 0.081 0.094 0.110 22.084

17.582 563-46-2 2-Methylbutene-1 0.589 0.654 0.792 159.588

20.947 513-35-9 2-Methylbutene-2 1.213 1.323 1.633 328.791

29.205 691-38-3 4-Methyl-c-pentene-2 0.053 0.057 0.059 14.376

29.847 674-76-0 4-Methyl-t-pentene-2 0.152 0.163 0.171 41.215

33.234 763-29-1 2-Methylpentene-1 0.259 0.273 0.290 70.189

37.412 625-27-4 2-Methylpentene-2 0.392 0.410 0.440 106.242

37.828 922-62-3 3-Methyl-c-pentene-2 0.298 0.309 0.335 80.887

40.098 3404-73-7 3,3-Dimethylpentene-1 0.353 0.364 0.340 95.773

42.538 594-56-9 2,3,3-Trimethylbutene-1 0.013 0.013 0.012 3.408

46.649 3404-61-3 3-Methylhexene-1 0.013 0.014 0.013 3.607

47.245 3524-73-0 5-Methylhexene-1 0.082 0.085 0.078 22.121

49.27815840-60-5 2-Methyl-c-hexene-3 0.035 0.036 0.033 9.363

50.273 3404-55-5 4-Methyl-t/c-hexene-2 0.041 0.042 0.039 11.053

57.685 6094-02-6 2-Methylhexene-1 0.028 0.029 0.027 7.647

58.555 2738-19-4 2-Methyl-2-hexene 0.007 0.007 0.007 1.965

Naphtheno-Olefins 22.539 1574-41-0 1,3-Cyclopentadiene 0.006 0.007 0.009 1.746

25.742 142-29-0 Cyclopentene 0.210 0.196 0.290 58.464

37.045 1120-62-3 3-Methylcyclopentene 0.107 0.101 0.123 28.971

45.840 693-89-0 1-Methylcyclopentene 0.362 0.336 0.417 100.617

51.161 110-83-8 Cyclohexene 0.039 0.035 0.045 10.544

Di-Olefins 18.628 78-79-5 2-Methyl-1,3-Butadiene 0.010 0.011 0.014 2.801

21.277 2004-70-8 1t,3-Pentadiene 0.015 0.016 0.021 4.277

45.435 1528-30-9 C6-Diolefin-1 0.015 0.015 0.017 4.082

Oxygenates 26.912 71-23-8 n-Propanol 0.081 0.073 0.127 15.363

48.063 71-36-3 n-Butanol 0.051 0.046 0.065 10.479

Unidentified 19.883 Unidentified 0.007 0.008 0.009 2.310

26.992 Unidentified 0.071 0.077 0.080 23.617

28.738 Unidentified 0.065 0.064 0.070 21.715

59.882 Unidentified 0.278 0.280 0.267 92.350

64.072 Unidentified 0.075 0.073 0.064 24.985

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C-293
Hydrocarbon Expert V4.7 Thu Aug 26 16:41:24 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF 24-Aug-10, 17:46:58

Sample: ODDB-91321 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91321

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Unidentified 72.451 Unidentified 0.018 0.018 0.015 6.056

74.463 Unidentified 0.011 0.010 0.009 3.534

78.825 Unidentified 0.007 0.007 0.006 2.319

85.151 Unidentified 0.005 0.005 0.004 1.742

88.746 Unidentified 0.009 0.009 0.006 2.830

93.843 Unidentified 0.043 0.043 0.029 14.413

94.527 Unidentified 0.004 0.003 0.411 1.444

94.527 Unidentified 0.004 0.004 0.003 1.444

99.122 Unidentified 0.998 0.993 0.662 331.444

99.704 Unidentified 0.003 0.003 0.002 1.104

100.354 Unidentified 0.079 0.057 0.048 26.357

100.486 Unidentified 0.219 0.213 0.133 72.879

101.167 Unidentified 0.148 0.152 0.099 49.063

101.289 Unidentified 0.085 0.084 0.057 28.354

102.195 Unidentified 0.008 0.008 0.006 2.786

102.548 Unidentified 0.059 0.057 0.036 19.569

103.201 Unidentified 0.058 0.057 0.039 19.391

103.689 Unidentified 0.008 0.007 0.007 2.795

106.205 Unidentified 0.008 0.007 0.005 2.588

108.086 Unidentified 0.111 0.107 0.067 36.719

108.361 Unidentified 0.123 0.099 0.096 40.729

108.440 Unidentified 0.117 0.113 0.070 38.722

108.749 Unidentified 0.291 0.283 0.176 96.728

109.173 Unidentified 1.032 0.850 0.726 342.565

109.872 Unidentified 0.039 0.032 0.027 12.898

109.968 Unidentified 0.030 0.022 0.021 9.926

110.713 Unidentified 0.028 0.025 0.017 9.282

111.042 Unidentified 0.161 0.157 0.108 53.412

111.313 Unidentified 0.138 0.112 0.088 45.861

111.975 Unidentified 0.064 0.052 0.041 21.126

112.825 Unidentified 0.012 0.010 0.008 4.127

112.958 Unidentified 0.017 0.014 0.012 5.787

113.481 Unidentified 0.039 0.038 0.021 12.854

113.614 Unidentified 0.012 0.012 0.007 4.006

115.147 Unidentified 0.018 0.015 0.012 6.016

130.002 Unidentified 0.004 0.003 0.002 1.337

Plus

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C-294
Hydrocarbon Expert V4.7 Thu Aug 26 16:41:24 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF 24-Aug-10, 17:46:58

Sample: ODDB-91321 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91321

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF

20.0 15.0 10.0 5.0 0.0

Propane

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

Unidentified

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

1,3-Cyclopentadiene

2,2-Dimethylbutane

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C-295
Hydrocarbon Expert V4.7 Thu Aug 26 16:41:24 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF 24-Aug-10, 17:46:58

Sample: ODDB-91321 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91321

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

n-Propanol Unidentified

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

n-Hexane

t-Hexene-3

t-Hexene-2 3-Methylcyclopentene

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane 2,3,3-Trimethylbutene-1 2,2,3-Trimethylbutane

C6-Diolefin-1 Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1

Cyclohexane

n-Butanol

2-Methyl-c-hexene-3

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C-296
Hydrocarbon Expert V4.7 Thu Aug 26 16:41:24 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF 24-Aug-10, 17:46:58

Sample: ODDB-91321 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91321

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF

70.0 65.0 60.0 55.0 50.0

4-Methyl-t/c-hexene-2

2-Methylhexane

Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane

2,2,4-Trimethylpentane

t-Heptene-3

2-Methylhexene-1

n-Heptane

2-Methyl-2-hexene

Unidentified

Methylcyclohexane

1,1,3-Trimethylcyclopentane

2,2-Dimethylhexane

Unidentified Ethylcyclopentane

2,2,3-Trimethylpentane 2,5-Dimethylhexane

2,4-Dimethylhexane

1c,2t,4-Trimethylcyclopentane

3,3-Dimethylhexane

1t,2c,3-Trimethylcyclopentane

2,3,4-Trimethylpentane

Toluene 2,3,3-Trimethylpentane

2,3-Dimethylhexane

2-Methylheptane

Unidentified 4-Methylheptane

1,3-dimethyl-t-cyclohexane 3-Methylheptane 3-Ethylhexane

Unidentified

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C-297
Hydrocarbon Expert V4.7 Thu Aug 26 16:41:24 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF 24-Aug-10, 17:46:58

Sample: ODDB-91321 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91321

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF

95.0 90.0 85.0 80.0 75.0

2,2,5-Trimethylhexane

1t,3-Dimethylcyclohexane

n-Octane

Unidentified

2,3,5-Trimethylhexane

2,4-Dimethylheptane

Ethylcyclohexane 2,6-Dimethylheptane

2,5-Dimethylheptane

Ethylbenzene

Unidentified

m-Xylene p-Xylene

4-Methyloctane 2-Methyloctane

3-Methyloctane

Unidentified o-Xylene

C10 - IsoParaffin - 1

trans-1,3-Diethylcyclopentane 2,2,4-trimethylheptane

n-Nonane

i-Propylbenzene

Unidentified 2,2-Dimethyloctane

Unidentified

2,5-Dimethyloctane

2,7-Dimethyloctane 2,4-Dimethyloctane

2,6-Dimethyloctane

n-Propylbenzene

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

4-Methylnonane Unidentified 1-Methyl-2-ethylbenzene

Unidentified 3-Methylnonane

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C-298
Hydrocarbon Expert V4.7 Thu Aug 26 16:41:24 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF 24-Aug-10, 17:46:58

Sample: ODDB-91321 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91321

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified Unidentified C11-Isoparaffin-2 1,2,4-Trimethylbenzene Unidentified

i-Butylcyclohexane

Unidentified 3-Ethyl-3-methylheptane Unidentified i-Butylbenzene n-Decane Unidentified

Unidentified 1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene C11 Isoparaffin-4 1-Methyl-4-i-propylbenzene

Indan

Indene

Unidentified C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene 1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

Unidentified 1-Methyl-2-n-propylbenzene Unidentified C11- Isoparaffin-11 Unidentified

Unidentified 2-Methylindan

Unidentified 1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

Unidentified 2-Undecene, (E)- Unidentified

1,2-Dimethyl-3-ethylbenzene Unidentified

n-Undecane Unidentified 1-Ethyl-4-i-propylbenzene

1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene Unidentified C12 - IsoParaffin - 1

Unidentified C11 - Aromatic - 3 5-Methylindan 1,2-Di-i-propylbenzene 1-methyl-4-(1-methylpropyl)be C11 - Aromatic - 4 4-Methylindan Benzene, 1-methyl-4-(2-methylpropyl)- 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene 1-Methyl-2-n-butylbenzene C11 - Aromatic - 7

C12 - IsoParaffin - 4 1,4-Di-i-propylbenzene

Naphthalene 4,7-Dimethyl Indane 1,1-Dimethyl Indane Dimethyl Indane - 1 1t-Butyl-4-ethylbenzene

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

C11 - Aromatic - 12

2-Methylnaphthalene

1-Methylnaphthalene

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C-299
Hydrocarbon Expert V4.7 Thu Aug 26 16:41:24 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF 24-Aug-10, 17:46:58

Sample: ODDB-91321 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91321

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000003.D\SIG2000003_FID2_B.CDF

145.0 140.0 135.0 130.0 125.0

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C-300
Hydrocarbon Expert V4.7 Thu Aug 26 16:53:07 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91322 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91322

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 15.166 17.813 18.361

I-Paraffins 26.340 30.029 28.307

Aromatics 43.085 36.374 36.975

Mono-Aromatics 42.174 35.661 36.340

Naphthalenes 0.096 0.069 0.064

Naphtheno/Olefino-Benzs 0.224 0.185 0.149

Indenes 0.591 0.460 0.422

Naphthenes 6.544 6.325 6.605

Mono-Naphthenes 6.544 6.325 6.605

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 7.575 8.247 8.786

n-Olefins 3.303 3.690 3.961

Iso-Olefins 3.530 3.851 3.982

Naphtheno-Olefins 0.702 0.665 0.796

Di-Olefins 0.039 0.041 0.047

Oxygenates 0.125 0.115 0.169

Unidentified 1.165 1.097 0.797

Plus 0.000 0.000 0.000

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C-301
Hydrocarbon Expert V4.7 Thu Aug 26 16:53:07 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91322 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91322

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C3 0.079 0.073 0.116

C4 5.216 6.583 7.854

C5 21.676 25.287 26.455

C6 21.269 22.686 21.854

C7 24.293 21.482 22.749

C8 16.388 14.374 13.367

C9 5.486 4.668 3.982

C10 3.365 2.800 2.218

C11 0.902 0.815 0.521

C12 0.164 0.136 0.088

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C-302
Hydrocarbon Expert V4.7 Thu Aug 26 16:53:07 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91322 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91322

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C3 0.002 0.002 0.003

C4 4.842 6.142 7.292

C5 3.777 4.428 4.582

C6 5.710 6.357 5.799

C7 0.558 0.599 0.487

C8 0.174 0.182 0.133

C9 0.049 0.050 0.033

C10 0.026 0.026 0.016

C11 0.027 0.027 0.015

I-Paraffins C4 0.043 0.057 0.065

C5 13.536 16.041 16.419

C6 7.755 8.650 7.876

C7 2.129 2.299 1.860

C8 2.138 2.241 1.638

C9 0.254 0.262 0.174

C10 0.100 0.100 0.059

C11 0.376 0.371 0.210

C12 0.008 0.008 0.004

Mono-Aromatics C6 0.637 0.532 0.713

C7 19.510 16.520 18.532

C8 13.890 11.774 11.450

C9 5.058 4.260 3.683

C10 2.462 2.062 1.605

C11 0.462 0.385 0.273

C12 0.156 0.128 0.084

Naphthalenes C10 0.079 0.056 0.054

C11 0.017 0.013 0.011

Naphtheno/Olefino-Benzs C10 0.224 0.185 0.149

Indenes C9 0.117 0.089 0.087

C10 0.473 0.370 0.335

Mono-Naphthenes C5 0.367 0.362 0.458

C6 4.460 4.313 4.638

C7 1.524 1.467 1.359

C8 0.186 0.177 0.145

C9 0.007 0.006 0.005

n-Olefins C4 0.282 0.340 0.440

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C-303
Hydrocarbon Expert V4.7 Thu Aug 26 16:53:07 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91322 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91322

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

n-Olefins C5 1.877 2.125 2.343

C6 1.107 1.188 1.151

C7 0.017 0.018 0.015

C11 0.020 0.019 0.012

Iso-Olefins C5 1.880 2.101 2.346

C6 1.111 1.185 1.155

C7 0.539 0.565 0.481

Naphtheno-Olefins C5 0.213 0.204 0.275

C6 0.489 0.462 0.521

Di-Olefins C5 0.025 0.027 0.032

C7 0.014 0.014 0.015

Oxygenates C3 0.077 0.071 0.113

C4 0.047 0.044 0.056

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C-304
Hydrocarbon Expert V4.7 Thu Aug 26 16:53:07 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91322 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91322

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 21.53 21.30

5% 32.49 28.95

10% 79.90 79.44

15% 81.10 80.46

20% 93.48 81.47

25% 99.16 94.27

30% 138.85 99.90

35% 145.72 138.61

40% 154.99 145.16

45% 160.31 154.68

50% 190.98 158.41

55% 230.73 177.10

60% 230.82 210.94

65% 230.91 230.80

70% 231.00 230.91

75% 245.77 231.02

80% 279.56 276.00

85% 281.87 281.34

90% 320.98 291.67

95% 350.02 336.40

FBP 403.28 398.03

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C-305
Hydrocarbon Expert V4.7 Thu Aug 26 16:53:07 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91322 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91322

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 7.553 74-98-6 P3 Propane 0.002 0.002 0.003 0.390

2 8.809 75-28-5 I4 i-Butane 0.043 0.057 0.065 10.908

3 9.622 115-11-7 K4 Isobutene 0.026 0.032 0.040 6.684

4 9.664 106-98-9 K4 Butene-1 0.028 0.034 0.043 7.220

5 10.023 106-97-8 P4 n-Butane 4.842 6.142 7.292 1214.581

6 10.509 624-64-6 K4 t-Butene-2 0.107 0.130 0.167 27.870

7 10.637 463-82-1 I5 2,2-Dimethylpropane 0.060 0.074 0.073 15.132

8 11.251 590-18-1 K4 c-Butene-2 0.121 0.144 0.189 31.554

9 13.453 563-45-1 C5 3-Methylbutene-1 0.083 0.097 0.103 21.504

10 15.091 78-78-4 I5 i-Pentane 13.476 15.966 16.347 3403.446

11 16.727 109-67-1 K5 Pentene-1 0.378 0.433 0.471 98.111

12 17.581 563-46-2 C5 2-Methylbutene-1 0.590 0.666 0.737 153.394

13 18.121 109-66-0 P5 n-Pentane 3.777 4.428 4.582 953.910

14 18.628 78-79-5 E5 2-Methyl-1,3-Butadiene 0.010 0.011 0.013 2.693

15 19.234 646-04-8 K5 t-Pentene-2 0.970 1.098 1.210 251.892

16 19.878 ? Unidentified 0.007 0.008 0.009 2.217

17 20.265 627-20-3 K5 c-Pentene-2 0.530 0.593 0.661 137.684

18 20.949 513-35-9 C5 2-Methylbutene-2 1.207 1.338 1.506 313.560

19 21.271 2004-70-8 E5 1t,3-Pentadiene 0.015 0.016 0.019 3.977

20 22.541 1574-41-0 B5 1,3-Cyclopentadiene 0.006 0.007 0.008 1.675

21 23.086 75-83-2 I6 2,2-Dimethylbutane 0.251 0.283 0.254 63.532

22 25.750 142-29-0 B5 Cyclopentene 0.207 0.197 0.266 55.409

23 26.904 71-23-8 X3 n-Propanol 0.077 0.071 0.113 14.067

24 26.992 ? Unidentified 0.070 0.077 0.073 22.337

25 27.607 287-92-3 M5 Cyclopentane 0.367 0.362 0.458 95.385

26 28.341 79-29-8 I6 2,3-Dimethylbutane 0.804 0.892 0.817 203.889

27 28.735 ? Unidentified 0.063 0.062 0.062 19.922

28 29.196 691-38-3 C6 4-Methyl-c-pentene-2 0.052 0.056 0.054 13.440

29 29.430 107-83-5 I6 2-Methylpentane 3.651 4.104 3.708 925.860

30 29.838 674-76-0 C6 4-Methyl-t-pentene-2 0.147 0.160 0.153 38.256

31 32.081 96-14-0 I6 3-Methylpentane 3.049 3.370 3.097 773.214

32 33.235 763-29-1 C6 2-Methylpentene-1 0.250 0.268 0.260 64.935

33 33.459 592-41-6 K6 Hexene-1 0.169 0.183 0.176 43.925

34 35.835 110-54-3 P6 n-Hexane 5.710 6.357 5.799 1447.834

35 36.43713269-52-8 K6 t-Hexene-3 0.283 0.305 0.294 73.510

36 36.916 4050-45-7 K6 t-Hexene-2 0.428 0.460 0.445 111.062

37 37.052 1120-62-3 B6 3-Methylcyclopentene 0.109 0.105 0.116 28.297

38 37.411 625-27-4 C6 2-Methylpentene-2 0.376 0.399 0.391 97.588

39 37.821 922-62-3 C6 3-Methyl-c-pentene-2 0.286 0.301 0.297 74.313

40 38.749 7688-21-3 K6 c-Hexene-2 0.227 0.241 0.236 59.038

41 40.087 3404-73-7 C7 3,3-Dimethylpentene-1 0.338 0.353 0.301 87.687

42 40.684 96-37-7 M6 Methylcyclopentane 2.852 2.796 2.965 740.776

43 42.234 108-08-7 I7 2,4-Dimethylpentane 0.456 0.497 0.398 115.963

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C-306
Hydrocarbon Expert V4.7 Thu Aug 26 16:53:07 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91322 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91322

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 42.536 594-56-9 C7 2,3,3-Trimethylbutene-1 0.010 0.010 0.009 2.522

45 42.782 464-06-2 I7 2,2,3-Trimethylbutane 0.053 0.057 0.047 13.584

46 45.426 1528-30-9 E7 C6-Diolefin-1 0.014 0.014 0.015 3.691

47 45.637 71-42-3 Q6 Benzene 0.637 0.532 0.713 178.108

48 45.836 693-89-0 B6 1-Methylcyclopentene 0.344 0.324 0.366 91.415

49 46.642 3404-61-3 C7 3-Methylhexene-1 0.012 0.013 0.011 3.208

50 47.234 3524-73-0 C7 5-Methylhexene-1 0.076 0.081 0.068 19.858

51 47.560 110-82-7 M6 Cyclohexane 1.609 1.517 1.673 417.909

52 48.060 71-36-3 X4 n-Butanol 0.047 0.044 0.056 9.334

53 49.27215840-60-5 C7 2-Methyl-c-hexene-3 0.033 0.034 0.029 8.463

54 50.266 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.038 0.040 0.034 9.955

55 50.663 591-76-4 I7 2-Methylhexane 1.013 1.096 0.885 257.982

56 50.840 ? Unidentified 0.065 0.069 0.059 20.803

57 51.155 110-83-8 B6 Cyclohexene 0.036 0.033 0.039 9.472

58 52.493 589-34-4 I7 3-Methylhexane 0.607 0.649 0.530 154.584

59 53.354 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.163 0.160 0.145 42.386

60 53.940 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.132 0.130 0.118 34.376

61 54.562 822-50-4 M7 1t,2-Dimethylcyclopentane 0.187 0.182 0.166 48.511

62 55.147 540-84-1 I8 2,2,4-Trimethylpentane 1.008 1.069 0.772 257.064

63 57.33214686-14-7 K7 t-Heptene-3 0.017 0.018 0.015 4.363

64 57.681 6094-02-6 C7 2-Methylhexene-1 0.027 0.028 0.024 6.925

65 58.057 142-82-5 P7 n-Heptane 0.558 0.599 0.487 142.091

66 58.548 2738-19-4 C7 2-Methyl-2-hexene 0.006 0.006 0.005 1.512

67 61.520 108-87-2 M7 Methylcyclohexane 1.007 0.961 0.898 261.594

68 62.459 4516-69-2 M8 1,1,3-Trimethylcyclopentane 0.021 0.021 0.016 5.446

69 62.848 590-73-8 I8 2,2-Dimethylhexane 0.017 0.018 0.013 4.369

70 64.301 1640-89-7 M7 Ethylcyclopentane 0.035 0.034 0.031 9.101

71 64.946 564-02-3 I8 2,2,3-Trimethylpentane 0.047 0.048 0.036 11.955

72 65.169 592-13-2 I8 2,5-Dimethylhexane 0.136 0.144 0.104 34.691

73 65.507 589-43-5 I8 2,4-Dimethylhexane 0.143 0.150 0.110 36.524

74 66.347 4850-28-6 M8 1c,2t,4-Trimethylcyclopentane 0.019 0.019 0.015 4.998

75 66.743 563-16-6 I8 3,3-Dimethylhexane 0.012 0.013 0.009 3.092

76 67.86415890-40-1 M8 1t,2c,3-Trimethylcyclopentane 0.015 0.014 0.012 3.904

77 68.483 565-75-3 I8 2,3,4-Trimethylpentane 0.352 0.359 0.270 89.806

78 69.119 108-88-3 Q7 Toluene 19.510 16.520 18.532 5398.904

79 70.795 584-94-1 I8 2,3-Dimethylhexane 0.110 0.113 0.084 28.064

80 72.048 592-27-8 I8 2-Methylheptane 0.103 0.109 0.079 26.387

81 72.303 589-53-7 I8 4-Methylheptane 0.060 0.062 0.046 15.241

82 73.225 M8 1,3-dimethyl-t-cyclohexane 0.087 0.083 0.068 22.674

83 73.361 589-81-1 I8 3-Methylheptane 0.094 0.098 0.072 24.015

84 73.563 619-99-8 I8 3-Ethylhexane 0.056 0.057 0.043 14.257

85 74.459 ? Unidentified 0.013 0.012 0.010 4.134

86 75.247 3522-94-9 I9 2,2,5-Trimethylhexane 0.143 0.148 0.097 36.462

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C-307
Hydrocarbon Expert V4.7 Thu Aug 26 16:53:07 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91322 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91322

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 76.530 ? Unidentified 0.028 0.026 0.022 8.891

88 77.869 111-65-9 P8 n-Octane 0.174 0.182 0.133 44.393

89 80.353 1069-53-0 I9 2,3,5-Trimethylhexane 0.021 0.021 0.014 5.275

90 81.522 1071-26-7 I9 2,4-Dimethylheptane 0.009 0.010 0.006 2.354

91 82.174 1678-91-7 M8 Ethylcyclohexane 0.043 0.040 0.034 11.217

92 82.476 1072-05-5 I9 2,6-Dimethylheptane 0.015 0.016 0.010 3.844

93 82.976 ? Unidentified 0.006 0.006 0.005 1.855

94 83.409 I9 2,5-Dimethylheptane 0.020 0.021 0.014 5.170

95 84.745 100-41-4 Q8 Ethylbenzene 2.658 2.251 2.191 729.994

96 85.989 108-38-3 Q8 m-Xylene 6.429 5.461 5.300 1765.617

97 86.130 106-42-3 Q8 p-Xylene 3.031 2.584 2.499 832.419

98 87.277 2216-34-4 I9 4-Methyloctane 0.013 0.013 0.009 3.221

99 87.408 3221-61-2 I9 2-Methyloctane 0.017 0.017 0.011 4.258

100 88.271 2216-33-3 I9 3-Methyloctane 0.017 0.018 0.012 4.407

101 88.938 95-47-6 Q8 o-Xylene 1.771 1.477 1.460 486.459

102 89.322 I10 C10 - IsoParaffin - 1 0.015 0.015 0.009 3.722

103 89.911 M9 trans-1,3-Diethylcyclopentane 0.007 0.006 0.005 1.877

104 90.17114720-74-2 I10 2,2,4-trimethylheptane 0.016 0.016 0.010 4.036

105 91.746 111-84-2 P9 n-Nonane 0.049 0.050 0.033 12.527

106 93.095 98-82-8 Q9 i-Propylbenzene 0.035 0.030 0.025 9.521

107 95.505 2051-30-1 I10 2,4-Dimethyloctane 0.006 0.006 0.004 1.633

108 96.554 103-65-1 Q9 n-Propylbenzene 0.249 0.212 0.181 67.984

109 97.400 620-14-4 Q9 1-Methyl-3-ethylbenzene 0.988 0.839 0.719 269.512

110 97.634 622-96-8 Q9 1-Methyl-4-ethylbenzene 0.472 0.402 0.343 128.663

111 98.260 108-67-8 Q9 1,3,5-Trimethylbenzene 0.626 0.531 0.456 170.850

112 98.90717301-94-8 I10 4-Methylnonane 0.009 0.009 0.006 2.307

113 99.114 ? Unidentified 0.135 0.136 0.083 42.887

114 99.345 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.384 0.320 0.280 104.820

115 99.886 5911-04-6 I10 3-Methylnonane 0.015 0.015 0.009 3.896

116 100.352 ? Unidentified 0.012 0.009 0.007 3.889

117 100.483 ? Unidentified 0.034 0.034 0.019 10.877

118 100.697 I11 C11-Isoparaffin-2 0.019 0.019 0.011 4.922

119 100.977 95-63-6 Q9 1,2,4-Trimethylbenzene 1.950 1.634 1.420 532.008

120 101.163 ? Unidentified 0.026 0.028 0.016 8.382

121 101.286 ? Unidentified 0.014 0.014 0.009 4.511

122 102.33517302-01-1 I10 3-Ethyl-3-methylheptane 0.039 0.039 0.022 10.039

123 102.625 538-93-2 Q10 i-Butylbenzene 0.065 0.056 0.042 17.548

124 102.804 124-18-5 P10 n-Decane 0.026 0.026 0.016 6.699

125 102.900 ? Unidentified 0.027 0.023 0.018 8.576

126 103.198 ? Unidentified 0.011 0.011 0.006 3.587

127 103.851 526-73-8 Q9 1,2,3-Trimethylbenzene 0.355 0.291 0.259 96.871

128 104.242 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.009 0.008 0.006 2.572

129 104.617 99-87-6 Q10 1-Methyl-4-i-propylbenzene 0.042 0.036 0.028 11.524

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C-308
Hydrocarbon Expert V4.7 Thu Aug 26 16:53:07 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91322 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91322

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 105.044 J9 Indan 0.117 0.089 0.087 32.576

131 105.638 J10 Indene 0.271 0.206 0.201 75.147

132 106.354 I11 C11-Isoparaffin-7 0.115 0.113 0.064 29.383

133 106.547 141-93-5 Q10 1,3-Diethylbenzene 0.051 0.043 0.033 13.806

134 106.825 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 0.433 0.369 0.282 117.435

135 107.163 105-05-5 Q10 1,4-Diethylbenzene 0.164 0.139 0.107 44.426

136 107.261 104-51-8 Q10 n-Butylbenzene 0.030 0.025 0.019 8.061

137 107.382 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.150 0.125 0.098 40.765

138 107.628 135-01-3 Q10 1,2-Diethylbenzene 0.032 0.027 0.021 8.819

139 108.080 ? Unidentified 0.030 0.029 0.017 9.489

140 108.233 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.058 0.049 0.038 15.841

141 108.354 ? Unidentified 0.034 0.034 0.020 10.972

142 108.435 ? Unidentified 0.032 0.032 0.018 10.312

143 108.562 I11 C11- Isoparaffin-11 0.242 0.239 0.136 62.077

144 108.745 ? Unidentified 0.083 0.082 0.046 26.352

145 109.079 1758-88-9 Q10 1,4,Dimethyl-2-ethylbenzene 0.119 0.100 0.078 32.365

146 109.168 ? Unidentified 0.344 0.288 0.225 109.572

147 109.395 J10 2-Methylindan 0.051 0.039 0.034 14.229

148 109.741 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.330 0.277 0.215 89.447

149 110.286 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.252 0.208 0.165 68.481

150 110.710 ? Unidentified 0.007 0.006 0.004 2.286

151 110.905 693-61-8 K11 2-Undecene, (E)- 0.020 0.019 0.012 5.034

152 111.039 ? Unidentified 0.025 0.025 0.016 7.993

153 111.195 Q11 1-Methyl-4-t-butylbenzene 0.038 0.032 0.022 10.136

154 111.314 ? Unidentified 0.039 0.032 0.023 12.538

155 111.413 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.095 0.078 0.062 25.748

156 111.710 1120-21-4 P11 n-Undecane 0.027 0.027 0.015 7.046

157 111.864 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.034 0.028 0.020 9.070

158 111.973 ? Unidentified 0.016 0.013 0.010 5.202

159 112.349 Q10 1,2,4,5-Tetramethylbenzene 0.265 0.219 0.173 71.832

160 112.614 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.367 0.302 0.239 99.520

161 113.132 I12 C12 - IsoParaffin - 1 0.008 0.008 0.004 2.058

162 113.482 ? Unidentified 0.016 0.016 0.008 4.955

163 113.755 Q11 C11 - Aromatic - 3 0.053 0.044 0.031 14.402

164 113.946 874-35-1 H10 5-Methylindan 0.109 0.090 0.072 29.604

165 114.071 Q12 1,2-Di-i-propylbenzene 0.047 0.038 0.025 12.530

166 114.285 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.066 0.055 0.039 17.931

167 114.444 Q11 C11 - Aromatic - 4 0.035 0.029 0.021 9.434

168 114.695 824-22-6 J10 4-Methylindan 0.151 0.125 0.100 41.010

169 114.847 5161-04-6 Q11 Benzene, 1-methyl-4-(2-methylpropyl)-0.043 0.035 0.025 11.552

170 114.942 824-63-5 H10 2-Methylindan 0.115 0.095 0.076 31.306

171 115.146 ? Unidentified 0.012 0.012 0.006 3.874

172 115.258 538-68-1 Q11 n-Pentylbenzene 0.017 0.014 0.010 4.471

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C-309
Hydrocarbon Expert V4.7 Thu Aug 26 16:53:07 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91322 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91322

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 115.487 Q11 tert-Pentylbenzene 0.069 0.057 0.041 18.737

174 115.799 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.030 0.025 0.018 8.150

175 115.908 Q11 C11 - Aromatic - 6 0.039 0.034 0.023 10.674

176 116.368 100-18-5 Q12 1,4-Di-i-propylbenzene 0.054 0.044 0.029 14.492

177 116.811 91-20-3 G10 Naphthalene 0.079 0.056 0.054 22.369

178 117.241 ? Unidentified 0.010 0.008 0.005 3.091

179 117.593 7364-19-4 Q12 1t-Butyl-4-ethylbenzene 0.013 0.011 0.007 3.552

180 117.894 Q12 1,3-Di-n-propylbenzene 0.042 0.035 0.023 11.349

181 118.005 Q11 C11 - Aromatic - 11 0.024 0.020 0.014 6.397

182 118.559 Q11 C11 - Aromatic - 12 0.014 0.012 0.008 3.792

183 123.439 91-57-6 G11 2-Methylnaphthalene 0.011 0.008 0.007 3.197

184 124.306 90-12-0 G11 1-Methylnaphthalene 0.006 0.004 0.004 1.712

185 130.003 ? Unidentified 0.003 0.003 0.002 1.090

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C-310
Hydrocarbon Expert V4.7 Thu Aug 26 16:53:07 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91322 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91322

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 7.553 74-98-6 Propane 0.002 0.002 0.003 0.390

10.023 106-97-8 n-Butane 4.842 6.142 7.292 1214.581

18.121 109-66-0 n-Pentane 3.777 4.428 4.582 953.910

35.835 110-54-3 n-Hexane 5.710 6.357 5.799 1447.834

58.057 142-82-5 n-Heptane 0.558 0.599 0.487 142.091

77.869 111-65-9 n-Octane 0.174 0.182 0.133 44.393

91.746 111-84-2 n-Nonane 0.049 0.050 0.033 12.527

102.804 124-18-5 n-Decane 0.026 0.026 0.016 6.699

111.710 1120-21-4 n-Undecane 0.027 0.027 0.015 7.046

I-Paraffins 8.809 75-28-5 i-Butane 0.043 0.057 0.065 10.908

10.637 463-82-1 2,2-Dimethylpropane 0.060 0.074 0.073 15.132

15.091 78-78-4 i-Pentane 13.476 15.966 16.347 3403.446

23.086 75-83-2 2,2-Dimethylbutane 0.251 0.283 0.254 63.532

28.341 79-29-8 2,3-Dimethylbutane 0.804 0.892 0.817 203.889

29.430 107-83-5 2-Methylpentane 3.651 4.104 3.708 925.860

32.081 96-14-0 3-Methylpentane 3.049 3.370 3.097 773.214

42.234 108-08-7 2,4-Dimethylpentane 0.456 0.497 0.398 115.963

42.782 464-06-2 2,2,3-Trimethylbutane 0.053 0.057 0.047 13.584

50.663 591-76-4 2-Methylhexane 1.013 1.096 0.885 257.982

52.493 589-34-4 3-Methylhexane 0.607 0.649 0.530 154.584

55.147 540-84-1 2,2,4-Trimethylpentane 1.008 1.069 0.772 257.064

62.848 590-73-8 2,2-Dimethylhexane 0.017 0.018 0.013 4.369

64.946 564-02-3 2,2,3-Trimethylpentane 0.047 0.048 0.036 11.955

65.169 592-13-2 2,5-Dimethylhexane 0.136 0.144 0.104 34.691

65.507 589-43-5 2,4-Dimethylhexane 0.143 0.150 0.110 36.524

66.743 563-16-6 3,3-Dimethylhexane 0.012 0.013 0.009 3.092

68.483 565-75-3 2,3,4-Trimethylpentane 0.352 0.359 0.270 89.806

70.795 584-94-1 2,3-Dimethylhexane 0.110 0.113 0.084 28.064

72.048 592-27-8 2-Methylheptane 0.103 0.109 0.079 26.387

72.303 589-53-7 4-Methylheptane 0.060 0.062 0.046 15.241

73.361 589-81-1 3-Methylheptane 0.094 0.098 0.072 24.015

73.563 619-99-8 3-Ethylhexane 0.056 0.057 0.043 14.257

75.247 3522-94-9 2,2,5-Trimethylhexane 0.143 0.148 0.097 36.462

80.353 1069-53-0 2,3,5-Trimethylhexane 0.021 0.021 0.014 5.275

81.522 1071-26-7 2,4-Dimethylheptane 0.009 0.010 0.006 2.354

82.476 1072-05-5 2,6-Dimethylheptane 0.015 0.016 0.010 3.844

83.409 2,5-Dimethylheptane 0.020 0.021 0.014 5.170

87.277 2216-34-4 4-Methyloctane 0.013 0.013 0.009 3.221

87.408 3221-61-2 2-Methyloctane 0.017 0.017 0.011 4.258

88.271 2216-33-3 3-Methyloctane 0.017 0.018 0.012 4.407

89.322 C10 - IsoParaffin - 1 0.015 0.015 0.009 3.722

90.17114720-74-2 2,2,4-trimethylheptane 0.016 0.016 0.010 4.036

95.505 2051-30-1 2,4-Dimethyloctane 0.006 0.006 0.004 1.633

98.90717301-94-8 4-Methylnonane 0.009 0.009 0.006 2.307

99.886 5911-04-6 3-Methylnonane 0.015 0.015 0.009 3.896

100.697 C11-Isoparaffin-2 0.019 0.019 0.011 4.922

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C-311
Hydrocarbon Expert V4.7 Thu Aug 26 16:53:07 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91322 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91322

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

I-Paraffins 102.33517302-01-1 3-Ethyl-3-methylheptane 0.039 0.039 0.022 10.039

106.354 C11-Isoparaffin-7 0.115 0.113 0.064 29.383

108.562 C11- Isoparaffin-11 0.242 0.239 0.136 62.077

113.132 C12 - IsoParaffin - 1 0.008 0.008 0.004 2.058

Aromatics

Mono-Aromatics 45.637 71-42-3 Benzene 0.637 0.532 0.713 178.108

69.119 108-88-3 Toluene 19.510 16.520 18.532 5398.904

84.745 100-41-4 Ethylbenzene 2.658 2.251 2.191 729.994

85.989 108-38-3 m-Xylene 6.429 5.461 5.300 1765.617

86.130 106-42-3 p-Xylene 3.031 2.584 2.499 832.419

88.938 95-47-6 o-Xylene 1.771 1.477 1.460 486.459

93.095 98-82-8 i-Propylbenzene 0.035 0.030 0.025 9.521

96.554 103-65-1 n-Propylbenzene 0.249 0.212 0.181 67.984

97.400 620-14-4 1-Methyl-3-ethylbenzene 0.988 0.839 0.719 269.512

97.634 622-96-8 1-Methyl-4-ethylbenzene 0.472 0.402 0.343 128.663

98.260 108-67-8 1,3,5-Trimethylbenzene 0.626 0.531 0.456 170.850

99.345 611-14-3 1-Methyl-2-ethylbenzene 0.384 0.320 0.280 104.820

100.977 95-63-6 1,2,4-Trimethylbenzene 1.950 1.634 1.420 532.008

102.625 538-93-2 i-Butylbenzene 0.065 0.056 0.042 17.548

103.851 526-73-8 1,2,3-Trimethylbenzene 0.355 0.291 0.259 96.871

104.242 535-77-3 1-Methyl-3-i-propylbenzene 0.009 0.008 0.006 2.572

104.617 99-87-6 1-Methyl-4-i-propylbenzene 0.042 0.036 0.028 11.524

106.547 141-93-5 1,3-Diethylbenzene 0.051 0.043 0.033 13.806

106.825 1074-43-7 1-Methyl-3-n-propylbenzene 0.433 0.369 0.282 117.435

107.163 105-05-5 1,4-Diethylbenzene 0.164 0.139 0.107 44.426

107.261 104-51-8 n-Butylbenzene 0.030 0.025 0.019 8.061

107.382 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.150 0.125 0.098 40.765

107.628 135-01-3 1,2-Diethylbenzene 0.032 0.027 0.021 8.819

108.233 1074-17-5 1-Methyl-2-n-propylbenzene 0.058 0.049 0.038 15.841

109.079 1758-88-9 1,4,Dimethyl-2-ethylbenzene 0.119 0.100 0.078 32.365

109.741 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.330 0.277 0.215 89.447

110.286 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.252 0.208 0.165 68.481

111.195 1-Methyl-4-t-butylbenzene 0.038 0.032 0.022 10.136

111.413 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.095 0.078 0.062 25.748

111.864 4218-48-8 1-Ethyl-4-i-propylbenzene 0.034 0.028 0.020 9.070

112.349 1,2,4,5-Tetramethylbenzene 0.265 0.219 0.173 71.832

112.614 527-53-7 1,2,3,5-Tetramethylbenzene 0.367 0.302 0.239 99.520

113.755 C11 - Aromatic - 3 0.053 0.044 0.031 14.402

114.071 1,2-Di-i-propylbenzene 0.047 0.038 0.025 12.530

114.285 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.066 0.055 0.039 17.931

114.444 C11 - Aromatic - 4 0.035 0.029 0.021 9.434

114.847 5161-04-6 Benzene, 1-methyl-4-(2-methylpropyl)-0.043 0.035 0.025 11.552

115.258 538-68-1 n-Pentylbenzene 0.017 0.014 0.010 4.471

115.487 tert-Pentylbenzene 0.069 0.057 0.041 18.737

115.799 577-55-9 1-Methyl-2-n-butylbenzene 0.030 0.025 0.018 8.150

115.908 C11 - Aromatic - 6 0.039 0.034 0.023 10.674

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C-312
Hydrocarbon Expert V4.7 Thu Aug 26 16:53:07 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91322 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91322

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 116.368 100-18-5 1,4-Di-i-propylbenzene 0.054 0.044 0.029 14.492

117.593 7364-19-4 1t-Butyl-4-ethylbenzene 0.013 0.011 0.007 3.552

117.894 1,3-Di-n-propylbenzene 0.042 0.035 0.023 11.349

118.005 C11 - Aromatic - 11 0.024 0.020 0.014 6.397

118.559 C11 - Aromatic - 12 0.014 0.012 0.008 3.792

Naphthalenes 116.811 91-20-3 Naphthalene 0.079 0.056 0.054 22.369

123.439 91-57-6 2-Methylnaphthalene 0.011 0.008 0.007 3.197

124.306 90-12-0 1-Methylnaphthalene 0.006 0.004 0.004 1.712

Naphtheno/Olefino-Benzs 113.946 874-35-1 5-Methylindan 0.109 0.090 0.072 29.604

114.942 824-63-5 2-Methylindan 0.115 0.095 0.076 31.306

Indenes 105.044 Indan 0.117 0.089 0.087 32.576

105.638 Indene 0.271 0.206 0.201 75.147

109.395 2-Methylindan 0.051 0.039 0.034 14.229

114.695 824-22-6 4-Methylindan 0.151 0.125 0.100 41.010

Naphthenes

Mono-Naphthenes 27.607 287-92-3 Cyclopentane 0.367 0.362 0.458 95.385

40.684 96-37-7 Methylcyclopentane 2.852 2.796 2.965 740.776

47.560 110-82-7 Cyclohexane 1.609 1.517 1.673 417.909

53.354 1759-58-6 1t,3-Dimethylcyclopentane 0.163 0.160 0.145 42.386

53.940 2532-58-3 1c,3-Dimethylcyclopentane 0.132 0.130 0.118 34.376

54.562 822-50-4 1t,2-Dimethylcyclopentane 0.187 0.182 0.166 48.511

61.520 108-87-2 Methylcyclohexane 1.007 0.961 0.898 261.594

62.459 4516-69-2 1,1,3-Trimethylcyclopentane 0.021 0.021 0.016 5.446

64.301 1640-89-7 Ethylcyclopentane 0.035 0.034 0.031 9.101

66.347 4850-28-6 1c,2t,4-Trimethylcyclopentane 0.019 0.019 0.015 4.998

67.86415890-40-1 1t,2c,3-Trimethylcyclopentane 0.015 0.014 0.012 3.904

73.225 1,3-dimethyl-t-cyclohexane 0.087 0.083 0.068 22.674

82.174 1678-91-7 Ethylcyclohexane 0.043 0.040 0.034 11.217

89.911 trans-1,3-Diethylcyclopentane 0.007 0.006 0.005 1.877

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.622 115-11-7 Isobutene 0.026 0.032 0.040 6.684

9.664 106-98-9 Butene-1 0.028 0.034 0.043 7.220

10.509 624-64-6 t-Butene-2 0.107 0.130 0.167 27.870

11.251 590-18-1 c-Butene-2 0.121 0.144 0.189 31.554

16.727 109-67-1 Pentene-1 0.378 0.433 0.471 98.111

19.234 646-04-8 t-Pentene-2 0.970 1.098 1.210 251.892

20.265 627-20-3 c-Pentene-2 0.530 0.593 0.661 137.684

33.459 592-41-6 Hexene-1 0.169 0.183 0.176 43.925

36.43713269-52-8 t-Hexene-3 0.283 0.305 0.294 73.510

36.916 4050-45-7 t-Hexene-2 0.428 0.460 0.445 111.062

38.749 7688-21-3 c-Hexene-2 0.227 0.241 0.236 59.038

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C-313
Hydrocarbon Expert V4.7 Thu Aug 26 16:53:07 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91322 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91322

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

n-Olefins 57.33214686-14-7 t-Heptene-3 0.017 0.018 0.015 4.363

110.905 693-61-8 2-Undecene, (E)- 0.020 0.019 0.012 5.034

Iso-Olefins 13.453 563-45-1 3-Methylbutene-1 0.083 0.097 0.103 21.504

17.581 563-46-2 2-Methylbutene-1 0.590 0.666 0.737 153.394

20.949 513-35-9 2-Methylbutene-2 1.207 1.338 1.506 313.560

29.196 691-38-3 4-Methyl-c-pentene-2 0.052 0.056 0.054 13.440

29.838 674-76-0 4-Methyl-t-pentene-2 0.147 0.160 0.153 38.256

33.235 763-29-1 2-Methylpentene-1 0.250 0.268 0.260 64.935

37.411 625-27-4 2-Methylpentene-2 0.376 0.399 0.391 97.588

37.821 922-62-3 3-Methyl-c-pentene-2 0.286 0.301 0.297 74.313

40.087 3404-73-7 3,3-Dimethylpentene-1 0.338 0.353 0.301 87.687

42.536 594-56-9 2,3,3-Trimethylbutene-1 0.010 0.010 0.009 2.522

46.642 3404-61-3 3-Methylhexene-1 0.012 0.013 0.011 3.208

47.234 3524-73-0 5-Methylhexene-1 0.076 0.081 0.068 19.858

49.27215840-60-5 2-Methyl-c-hexene-3 0.033 0.034 0.029 8.463

50.266 3404-55-5 4-Methyl-t/c-hexene-2 0.038 0.040 0.034 9.955

57.681 6094-02-6 2-Methylhexene-1 0.027 0.028 0.024 6.925

58.548 2738-19-4 2-Methyl-2-hexene 0.006 0.006 0.005 1.512

Naphtheno-Olefins 22.541 1574-41-0 1,3-Cyclopentadiene 0.006 0.007 0.008 1.675

25.750 142-29-0 Cyclopentene 0.207 0.197 0.266 55.409

37.052 1120-62-3 3-Methylcyclopentene 0.109 0.105 0.116 28.297

45.836 693-89-0 1-Methylcyclopentene 0.344 0.324 0.366 91.415

51.155 110-83-8 Cyclohexene 0.036 0.033 0.039 9.472

Di-Olefins 18.628 78-79-5 2-Methyl-1,3-Butadiene 0.010 0.011 0.013 2.693

21.271 2004-70-8 1t,3-Pentadiene 0.015 0.016 0.019 3.977

45.426 1528-30-9 C6-Diolefin-1 0.014 0.014 0.015 3.691

Oxygenates 26.904 71-23-8 n-Propanol 0.077 0.071 0.113 14.067

48.060 71-36-3 n-Butanol 0.047 0.044 0.056 9.334

Unidentified 19.878 Unidentified 0.007 0.008 0.009 2.217

26.992 Unidentified 0.070 0.077 0.073 22.337

28.735 Unidentified 0.063 0.062 0.062 19.922

50.840 Unidentified 0.065 0.069 0.059 20.803

74.459 Unidentified 0.013 0.012 0.010 4.134

76.530 Unidentified 0.028 0.026 0.022 8.891

82.976 Unidentified 0.006 0.006 0.005 1.855

99.114 Unidentified 0.135 0.136 0.083 42.887

100.352 Unidentified 0.012 0.009 0.007 3.889

100.483 Unidentified 0.034 0.034 0.019 10.877

101.163 Unidentified 0.026 0.028 0.016 8.382

101.286 Unidentified 0.014 0.014 0.009 4.511

102.900 Unidentified 0.027 0.023 0.018 8.576

103.198 Unidentified 0.011 0.011 0.006 3.587

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C-314
Hydrocarbon Expert V4.7 Thu Aug 26 16:53:07 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91322 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91322

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Unidentified 108.080 Unidentified 0.030 0.029 0.017 9.489

108.354 Unidentified 0.034 0.034 0.020 10.972

108.435 Unidentified 0.032 0.032 0.018 10.312

108.745 Unidentified 0.083 0.082 0.046 26.352

109.168 Unidentified 0.344 0.288 0.225 109.572

110.710 Unidentified 0.007 0.006 0.004 2.286

111.039 Unidentified 0.025 0.025 0.016 7.993

111.314 Unidentified 0.039 0.032 0.023 12.538

111.973 Unidentified 0.016 0.013 0.010 5.202

113.482 Unidentified 0.016 0.016 0.008 4.955

115.146 Unidentified 0.012 0.012 0.006 3.874

117.241 Unidentified 0.010 0.008 0.005 3.091

130.003 Unidentified 0.003 0.003 0.002 1.090

Plus

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C-315
Hydrocarbon Expert V4.7 Thu Aug 26 16:53:07 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91322 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91322

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF

20.0 15.0 10.0 5.0 0.0

Propane

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

Unidentified

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

1,3-Cyclopentadiene

2,2-Dimethylbutane

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C-316
Hydrocarbon Expert V4.7 Thu Aug 26 16:53:07 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91322 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91322

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

n-Propanol Unidentified

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

n-Hexane

t-Hexene-3

t-Hexene-2 3-Methylcyclopentene

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane 2,3,3-Trimethylbutene-1 2,2,3-Trimethylbutane

C6-Diolefin-1 Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1

Cyclohexane

n-Butanol

2-Methyl-c-hexene-3

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C-317
Hydrocarbon Expert V4.7 Thu Aug 26 16:53:07 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91322 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91322

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF

70.0 65.0 60.0 55.0 50.0

4-Methyl-t/c-hexene-2

2-Methylhexane Unidentified Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane

2,2,4-Trimethylpentane

t-Heptene-3

2-Methylhexene-1

n-Heptane

2-Methyl-2-hexene

Methylcyclohexane

1,1,3-Trimethylcyclopentane

2,2-Dimethylhexane

Ethylcyclopentane

2,2,3-Trimethylpentane 2,5-Dimethylhexane

2,4-Dimethylhexane

1c,2t,4-Trimethylcyclopentane

3,3-Dimethylhexane

1t,2c,3-Trimethylcyclopentane

2,3,4-Trimethylpentane

Toluene

2,3-Dimethylhexane

2-Methylheptane 4-Methylheptane

1,3-dimethyl-t-cyclohexane 3-Methylheptane 3-Ethylhexane

Unidentified

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C-318
Hydrocarbon Expert V4.7 Thu Aug 26 16:53:07 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91322 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91322

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF

95.0 90.0 85.0 80.0 75.0

2,2,5-Trimethylhexane

Unidentified

n-Octane

2,3,5-Trimethylhexane

2,4-Dimethylheptane

Ethylcyclohexane 2,6-Dimethylheptane

Unidentified

2,5-Dimethylheptane

Ethylbenzene

m-Xylene p-Xylene

4-Methyloctane 2-Methyloctane

3-Methyloctane

o-Xylene

C10 - IsoParaffin - 1

trans-1,3-Diethylcyclopentane 2,2,4-trimethylheptane

n-Nonane

i-Propylbenzene

2,4-Dimethyloctane

n-Propylbenzene

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

4-Methylnonane Unidentified 1-Methyl-2-ethylbenzene

3-Methylnonane

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C-319
Hydrocarbon Expert V4.7 Thu Aug 26 16:53:07 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91322 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91322

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified

C11-Isoparaffin-21,2,4-Trimethylbenzene Unidentified

3-Ethyl-3-methylheptane i-Butylbenzene n-Decane Unidentified Unidentified

1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene

1-Methyl-4-i-propylbenzene

Indan

Indene

C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene

n-Butylbenzene 1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

Unidentified 1-Methyl-2-n-propylbenzene

C11- Isoparaffin-11 Unidentified

1,4,Dimethyl-2-ethylbenzene Unidentified 2-Methylindan

1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

Unidentified 2-Undecene, (E)- Unidentified 1-Methyl-4-t-butylbenzene 1,2-Dimethyl-3-ethylbenzene n-Undecane Unidentified 1-Ethyl-4-i-propylbenzene

1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene

C12 - IsoParaffin - 1

Unidentified C11 - Aromatic - 3 5-Methylindan 1,2-Di-i-propylbenzene 1-methyl-4-(1-methylpropyl)be C11 - Aromatic - 4 4-Methylindan Benzene, 1-methyl-4-(2-methylpropyl)- 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene 1-Methyl-2-n-butylbenzene C11 - Aromatic - 6

1,4-Di-i-propylbenzene

Naphthalene

Unidentified

1t-Butyl-4-ethylbenzene

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

C11 - Aromatic - 12

2-Methylnaphthalene

1-Methylnaphthalene

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C-320
Hydrocarbon Expert V4.7 Thu Aug 26 16:53:07 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF 24-Aug-10, 20:15:02

Sample: ODDB-91322 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91322

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000004.D\SIG2000004_FID2_B.CDF

145.0 140.0 135.0 130.0 125.0

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C-321
Hydrocarbon Expert V4.7 Thu Aug 26 16:57:37 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91323 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91323

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 6.906 8.243 7.693

I-Paraffins 28.366 31.684 24.604

Aromatics 41.804 36.628 34.990

Mono-Aromatics 40.963 35.943 34.418

Naphthalenes 0.100 0.074 0.066

Naphtheno/Olefino-Benzs 0.226 0.193 0.147

Indenes 0.516 0.418 0.360

Naphthenes 3.699 3.711 3.664

Mono-Naphthenes 3.699 3.711 3.664

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 7.039 7.921 7.918

n-Olefins 2.948 3.404 3.421

Iso-Olefins 3.351 3.787 3.674

Naphtheno-Olefins 0.699 0.686 0.776

Di-Olefins 0.040 0.044 0.048

Oxygenates 10.889 10.511 20.262

Unidentified 1.297 1.302 0.868

Plus 0.000 0.000 0.000

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C-322
Hydrocarbon Expert V4.7 Thu Aug 26 16:57:37 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91323 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91323

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C2 10.756 10.385 20.087

C3 0.079 0.076 0.113

C4 1.304 1.685 1.923

C5 10.808 12.963 13.025

C6 13.960 15.359 14.147

C7 20.559 18.912 18.923

C8 28.531 27.577 22.379

C9 7.887 7.411 5.528

C10 3.784 3.378 2.424

C11 0.854 0.798 0.485

C12 0.181 0.155 0.096

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C-323
Hydrocarbon Expert V4.7 Thu Aug 26 16:57:37 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91323 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91323

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C3 0.001 0.001 0.002

C4 1.038 1.366 1.537

C5 2.215 2.694 2.641

C6 3.053 3.527 3.048

C7 0.327 0.365 0.281

C8 0.074 0.080 0.056

C9 0.156 0.166 0.105

C10 0.017 0.018 0.010

C11 0.024 0.025 0.013

I-Paraffins C4 0.020 0.028 0.030

C5 4.839 5.950 5.770

C6 5.137 5.945 5.128

C7 2.103 2.358 1.805

C8 12.748 13.664 9.601

C9 2.460 2.640 1.650

C10 0.716 0.749 0.431

C11 0.341 0.350 0.188

C12 0.001 0.001 0.001

Mono-Aromatics C6 0.762 0.660 0.839

C7 16.516 14.511 15.421

C8 15.555 13.681 12.605

C9 5.195 4.545 3.718

C10 2.306 2.002 1.478

C11 0.456 0.395 0.265

C12 0.174 0.150 0.092

Naphthalenes C10 0.085 0.063 0.057

C11 0.015 0.011 0.009

Naphtheno/Olefino-Benzs C10 0.226 0.193 0.147

Indenes C9 0.076 0.060 0.055

C10 0.434 0.353 0.301

C12 0.005 0.004 0.003

Mono-Naphthenes C5 0.211 0.216 0.259

C6 2.497 2.504 2.553

C7 0.847 0.849 0.742

C8 0.144 0.142 0.111

n-Olefins C4 0.191 0.238 0.293

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C-324
Hydrocarbon Expert V4.7 Thu Aug 26 16:57:37 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91323 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91323

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

n-Olefins C5 1.620 1.902 1.987

C6 1.022 1.139 1.045

C7 0.098 0.107 0.086

C11 0.017 0.017 0.010

Iso-Olefins C5 1.697 1.973 2.082

C6 0.990 1.096 1.012

C7 0.653 0.708 0.572

C8 0.011 0.010 0.007

Naphtheno-Olefins C5 0.201 0.199 0.254

C6 0.498 0.488 0.522

Di-Olefins C5 0.026 0.029 0.032

C7 0.015 0.015 0.015

Oxygenates C2 10.756 10.385 20.087

C3 0.078 0.074 0.112

C4 0.055 0.052 0.064

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C-325
Hydrocarbon Expert V4.7 Thu Aug 26 16:57:37 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91323 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91323

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 25.14 23.93

5% 81.10 80.44

10% 97.22 94.84

15% 139.57 131.76

20% 154.53 144.68

25% 172.23 155.08

30% 172.73 172.33

35% 173.24 172.85

40% 197.42 176.07

45% 228.41 209.29

50% 230.13 228.91

55% 230.51 230.22

60% 230.89 230.65

65% 234.98 231.22

70% 239.92 237.34

75% 276.50 255.09

80% 281.21 278.79

85% 282.09 281.76

90% 320.72 292.60

95% 339.72 335.93

FBP 403.56 399.20

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C-326
Hydrocarbon Expert V4.7 Thu Aug 26 16:57:37 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91323 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91323

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 7.554 74-98-6 P3 Propane 0.001 0.001 0.002 0.237

2 8.810 75-28-5 I4 i-Butane 0.020 0.028 0.030 5.687

3 9.623 115-11-7 K4 Isobutene 0.016 0.020 0.024 4.578

4 9.665 106-98-9 K4 Butene-1 0.018 0.023 0.027 5.141

5 10.023 106-97-8 P4 n-Butane 1.038 1.366 1.537 289.748

6 10.510 624-64-6 K4 t-Butene-2 0.072 0.091 0.111 20.857

7 10.637 463-82-1 I5 2,2-Dimethylpropane 0.016 0.021 0.020 4.627

8 11.251 590-18-1 K4 c-Butene-2 0.085 0.104 0.131 24.611

9 13.062 64-17-5 X2 Ethanol 10.756 10.385 20.087 1280.145

10 13.450 563-45-1 C5 3-Methylbutene-1 0.173 0.210 0.213 50.077

11 15.082 78-78-4 I5 i-Pentane 4.822 5.929 5.750 1355.113

12 16.730 109-67-1 K5 Pentene-1 0.328 0.391 0.403 94.912

13 17.580 563-46-2 C5 2-Methylbutene-1 0.499 0.584 0.612 144.229

14 18.114 109-66-0 P5 n-Pentane 2.215 2.694 2.641 622.394

15 18.626 78-79-5 E5 2-Methyl-1,3-Butadiene 0.010 0.011 0.013 3.050

16 19.233 646-04-8 K5 t-Pentene-2 0.834 0.980 1.023 241.073

17 19.880 ? Unidentified 0.006 0.007 0.007 2.020

18 20.262 627-20-3 K5 c-Pentene-2 0.457 0.531 0.561 132.177

19 20.944 513-35-9 C5 2-Methylbutene-2 1.025 1.179 1.257 296.164

20 21.268 2004-70-8 E5 1t,3-Pentadiene 0.015 0.017 0.019 4.549

21 22.531 1574-41-0 B5 1,3-Cyclopentadiene 0.007 0.008 0.009 2.052

22 23.095 75-83-2 I6 2,2-Dimethylbutane 0.121 0.142 0.121 34.238

23 25.744 142-29-0 B5 Cyclopentene 0.194 0.191 0.245 57.679

24 26.900 71-23-8 X3 n-Propanol 0.078 0.074 0.112 15.799

25 26.989 ? Unidentified 0.056 0.064 0.058 19.922

26 27.606 287-92-3 M5 Cyclopentane 0.211 0.216 0.259 61.042

27 28.333 79-29-8 I6 2,3-Dimethylbutane 0.750 0.863 0.748 211.474

28 28.732 ? Unidentified 0.052 0.053 0.051 18.373

29 29.193 691-38-3 C6 4-Methyl-c-pentene-2 0.045 0.051 0.046 13.117

30 29.418 107-83-5 I6 2-Methylpentane 2.416 2.818 2.412 681.717

31 29.841 674-76-0 C6 4-Methyl-t-pentene-2 0.129 0.146 0.132 37.315

32 32.067 96-14-0 I6 3-Methylpentane 1.850 2.121 1.846 521.798

33 33.229 763-29-1 C6 2-Methylpentene-1 0.221 0.245 0.226 63.771

34 33.450 592-41-6 K6 Hexene-1 0.157 0.177 0.161 45.517

35 35.821 110-54-3 P6 n-Hexane 3.053 3.527 3.048 861.460

36 36.44013269-52-8 K6 t-Hexene-3 0.259 0.289 0.265 74.877

37 36.916 4050-45-7 K6 t-Hexene-2 0.395 0.441 0.404 114.209

38 37.036 1120-62-3 B6 3-Methylcyclopentene 0.101 0.101 0.106 29.186

39 37.407 625-27-4 C6 2-Methylpentene-2 0.336 0.370 0.343 97.066

40 37.818 922-62-3 C6 3-Methyl-c-pentene-2 0.259 0.283 0.265 74.916

41 38.740 7688-21-3 K6 c-Hexene-2 0.211 0.232 0.215 60.847

42 40.089 3404-73-7 C7 3,3-Dimethylpentene-1 0.305 0.331 0.267 88.098

43 40.675 96-37-7 M6 Methylcyclopentane 1.565 1.592 1.599 452.199

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C-327
Hydrocarbon Expert V4.7 Thu Aug 26 16:57:37 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91323 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91323

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 42.230 108-08-7 I7 2,4-Dimethylpentane 0.538 0.609 0.462 152.407

45 42.534 594-56-9 C7 2,3,3-Trimethylbutene-1 0.013 0.014 0.011 3.763

46 42.781 464-06-2 I7 2,2,3-Trimethylbutane 0.047 0.051 0.040 13.209

47 45.426 1528-30-9 E7 C6-Diolefin-1 0.015 0.015 0.015 4.249

48 45.634 71-42-3 Q6 Benzene 0.762 0.660 0.839 237.175

49 45.833 693-89-0 B6 1-Methylcyclopentene 0.353 0.345 0.370 104.623

50 46.638 3404-61-3 C7 3-Methylhexene-1 0.015 0.016 0.013 4.354

51 47.231 3524-73-0 C7 5-Methylhexene-1 0.054 0.059 0.048 15.678

52 47.553 110-82-7 M6 Cyclohexane 0.932 0.912 0.953 269.515

53 48.056 71-36-3 X4 n-Butanol 0.055 0.052 0.064 11.986

54 49.27115840-60-5 C7 2-Methyl-c-hexene-3 0.040 0.044 0.035 11.538

55 49.619 3769-23-1 C7 4-Methylhexene-1 0.012 0.013 0.010 3.337

56 50.261 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.050 0.054 0.044 14.467

57 50.664 591-76-4 I7 2-Methylhexane 1.003 1.126 0.861 284.040

58 50.836 ? Unidentified 0.039 0.043 0.035 13.977

59 51.151 110-83-8 B6 Cyclohexene 0.044 0.041 0.046 12.672

60 52.490 589-34-4 I7 3-Methylhexane 0.515 0.571 0.442 145.972

61 53.351 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.139 0.142 0.122 40.249

62 53.937 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.103 0.105 0.090 29.742

63 54.562 822-50-4 M7 1t,2-Dimethylcyclopentane 0.133 0.135 0.116 38.375

64 54.855 C7 C7 - Iso-Olefin - 2 0.022 0.023 0.019 6.381

65 55.166 540-84-1 I8 2,2,4-Trimethylpentane 3.105 3.418 2.338 881.243

66 55.468 592-76-7 K7 Heptene-1 0.029 0.031 0.025 8.271

67 56.801 4914-89-0 C7 3-Methyl-c-hexene-3 0.014 0.015 0.012 3.977

68 57.32814686-14-7 K7 t-Heptene-3 0.031 0.034 0.028 9.103

69 57.683 6094-02-6 C7 2-Methylhexene-1 0.056 0.062 0.049 16.277

70 58.053 142-82-5 P7 n-Heptane 0.327 0.365 0.281 92.763

71 58.271 7642-10-6 K7 c-Heptene-3 0.025 0.027 0.022 7.113

72 58.547 2738-19-4 C7 2-Methyl-2-hexene 0.026 0.027 0.022 7.371

73 58.79010574-36-4 C7 3-Methyl-c-hexene-2 0.019 0.021 0.017 5.576

74 59.17214686-13-6 K7 t-Heptene-2 0.014 0.015 0.012 3.949

75 59.64916491-15-9 M7 Cyclopentene, 1,5-dimethyl- 0.018 0.018 0.016 5.236

76 60.07420710-38-8 C7 3-Methyl-t-hexene-2 0.015 0.016 0.013 4.351

77 60.859 4914-91-4 C7 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.013 0.011 3.672

78 61.513 108-87-2 M7 Methylcyclohexane 0.430 0.425 0.376 124.148

79 63.384 ? Unidentified 0.027 0.029 0.021 9.577

80 64.295 1640-89-7 M7 Ethylcyclopentane 0.024 0.024 0.021 6.964

81 64.948 564-02-3 I8 2,2,3-Trimethylpentane 0.358 0.381 0.270 101.573

82 65.177 592-13-2 I8 2,5-Dimethylhexane 0.729 0.801 0.549 207.023

83 65.514 589-43-5 I8 2,4-Dimethylhexane 0.670 0.728 0.504 190.076

84 68.513 565-75-3 I8 2,3,4-Trimethylpentane 3.335 3.533 2.511 946.399

85 69.118 108-88-3 Q7 Toluene 16.516 14.511 15.421 5084.878

86 69.224 560-21-4 I8 2,3,3-Trimethylpentane 3.366 3.531 2.535 955.458

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C-328
Hydrocarbon Expert V4.7 Thu Aug 26 16:57:37 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91323 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91323

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 70.801 584-94-1 I8 2,3-Dimethylhexane 0.888 0.950 0.669 252.112

88 72.047 592-27-8 I8 2-Methylheptane 0.080 0.088 0.060 22.779

89 72.316 589-53-7 I8 4-Methylheptane 0.114 0.124 0.086 32.426

90 72.449 ? Unidentified 0.075 0.080 0.057 26.628

91 73.225 M8 1,3-dimethyl-t-cyclohexane 0.033 0.033 0.025 9.569

92 73.361 589-81-1 I8 3-Methylheptane 0.076 0.082 0.057 21.485

93 73.555 619-99-8 I8 3-Ethylhexane 0.026 0.028 0.020 7.458

94 75.260 3522-94-9 I9 2,2,5-Trimethylhexane 1.861 2.004 1.248 529.196

95 76.235 3875-51-2 M8 i-Propylcyclopentane 0.018 0.017 0.013 5.059

96 76.534 2207-03-6 M8 1t,3-Dimethylcyclohexane 0.014 0.014 0.011 4.150

97 77.867 111-65-9 P8 n-Octane 0.074 0.080 0.056 21.014

98 78.820 M8 C8 - MonoNaph - 3 0.058 0.058 0.045 16.896

99 80.353 1069-53-0 I9 2,3,5-Trimethylhexane 0.323 0.340 0.216 91.736

100 81.519 1071-26-7 I9 2,4-Dimethylheptane 0.045 0.048 0.030 12.839

101 82.171 1678-91-7 M8 Ethylcyclohexane 0.021 0.020 0.016 5.986

102 82.476 1072-05-5 I9 2,6-Dimethylheptane 0.058 0.063 0.039 16.547

103 83.411 I9 2,5-Dimethylheptane 0.145 0.155 0.098 41.337

104 84.749 100-41-4 Q8 Ethylbenzene 2.921 2.566 2.367 892.510

105 84.900 ? Unidentified 0.020 0.021 0.014 7.125

106 85.148 ? Unidentified 0.020 0.019 0.013 6.955

107 86.000 108-38-3 Q8 m-Xylene 7.170 6.320 5.810 2190.845

108 86.140 106-42-3 Q8 p-Xylene 3.429 3.034 2.779 1047.780

109 86.490 C8 C9-IsoOlefin-3 0.011 0.010 0.007 3.096

110 86.597 ? Unidentified 0.009 0.009 0.006 3.115

111 87.277 2216-34-4 I9 4-Methyloctane 0.007 0.008 0.005 2.113

112 87.409 3221-61-2 I9 2-Methyloctane 0.010 0.011 0.007 2.976

113 88.270 2216-33-3 I9 3-Methyloctane 0.010 0.011 0.007 2.970

114 88.747 ? Unidentified 0.119 0.133 0.081 42.266

115 88.942 95-47-6 Q8 o-Xylene 2.035 1.761 1.649 621.671

116 89.323 I10 C10 - IsoParaffin - 1 0.371 0.388 0.224 105.583

117 90.16514720-74-2 I10 2,2,4-trimethylheptane 0.250 0.262 0.151 71.304

118 91.711 111-84-2 P9 n-Nonane 0.156 0.166 0.105 44.343

119 93.094 98-82-8 Q9 i-Propylbenzene 0.032 0.029 0.023 9.854

120 93.840 ? Unidentified 0.043 0.045 0.026 15.189

121 94.06415869-87-1 I10 2,2-Dimethyloctane 0.014 0.015 0.008 3.989

122 94.86515869-89-3 I10 2,5-Dimethyloctane 0.005 0.005 0.003 1.487

123 95.505 2051-30-1 I10 2,4-Dimethyloctane 0.011 0.012 0.007 3.199

124 96.553 103-65-1 Q9 n-Propylbenzene 0.297 0.262 0.212 90.093

125 97.401 620-14-4 Q9 1-Methyl-3-ethylbenzene 1.153 1.016 0.825 349.962

126 97.635 622-96-8 Q9 1-Methyl-4-ethylbenzene 0.536 0.474 0.383 162.579

127 98.259 108-67-8 Q9 1,3,5-Trimethylbenzene 0.678 0.597 0.485 205.829

128 98.90617301-94-8 I10 4-Methylnonane 0.010 0.011 0.006 2.956

129 99.113 ? Unidentified 0.166 0.174 0.100 58.751

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C-329
Hydrocarbon Expert V4.7 Thu Aug 26 16:57:37 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91323 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91323

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 99.344 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.394 0.341 0.282 119.695

131 99.884 5911-04-6 I10 3-Methylnonane 0.016 0.017 0.010 4.631

132 100.351 ? Unidentified 0.013 0.010 0.007 4.764

133 100.481 ? Unidentified 0.037 0.037 0.020 12.966

134 100.697 I11 C11-Isoparaffin-2 0.020 0.021 0.011 5.847

135 100.977 95-63-6 Q9 1,2,4-Trimethylbenzene 1.871 1.627 1.339 568.018

136 101.163 ? Unidentified 0.026 0.028 0.016 9.046

137 101.284 ? Unidentified 0.015 0.015 0.009 5.207

138 102.33417302-01-1 I10 3-Ethyl-3-methylheptane 0.038 0.039 0.021 10.942

139 102.627 538-93-2 Q10 i-Butylbenzene 0.054 0.048 0.034 16.250

140 102.801 124-18-5 P10 n-Decane 0.017 0.018 0.010 4.852

141 102.899 ? Unidentified 0.017 0.015 0.011 6.081

142 103.197 ? Unidentified 0.011 0.011 0.006 3.792

143 103.849 526-73-8 Q9 1,2,3-Trimethylbenzene 0.234 0.199 0.167 71.027

144 104.614 99-87-6 Q10 1-Methyl-4-i-propylbenzene 0.039 0.035 0.025 11.844

145 105.043 J9 Indan 0.076 0.060 0.055 23.343

146 105.637 J10 Indene 0.239 0.189 0.174 73.690

147 106.352 I11 C11-Isoparaffin-7 0.099 0.101 0.054 28.124

148 106.546 141-93-5 Q10 1,3-Diethylbenzene 0.028 0.025 0.018 8.585

149 106.826 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 0.365 0.323 0.234 110.217

150 107.162 105-05-5 Q10 1,4-Diethylbenzene 0.140 0.123 0.090 42.193

151 107.260 104-51-8 Q10 n-Butylbenzene 0.024 0.021 0.015 7.124

152 107.381 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.128 0.111 0.082 38.708

153 107.627 135-01-3 Q10 1,2-Diethylbenzene 0.028 0.024 0.018 8.497

154 108.079 ? Unidentified 0.025 0.026 0.014 8.864

155 108.232 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.054 0.047 0.034 16.172

156 108.354 ? Unidentified 0.029 0.030 0.016 10.424

157 108.435 ? Unidentified 0.027 0.028 0.015 9.667

158 108.561 I11 C11- Isoparaffin-11 0.222 0.228 0.122 63.417

159 108.743 ? Unidentified 0.072 0.073 0.039 25.407

160 109.078 1758-88-9 Q10 1,4,Dimethyl-2-ethylbenzene 0.120 0.104 0.077 36.272

161 109.167 ? Unidentified 0.311 0.270 0.199 110.054

162 109.394 J10 2-Methylindan 0.042 0.033 0.028 13.032

163 109.741 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.328 0.285 0.210 98.972

164 110.286 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.219 0.188 0.141 66.200

165 110.709 ? Unidentified 0.006 0.006 0.004 2.242

166 110.903 693-61-8 K11 2-Undecene, (E)- 0.017 0.017 0.010 4.845

167 111.038 ? Unidentified 0.022 0.023 0.014 7.882

168 111.195 Q11 1-Methyl-4-t-butylbenzene 0.034 0.030 0.020 10.192

169 111.413 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.133 0.113 0.085 40.093

170 111.711 1120-21-4 P11 n-Undecane 0.024 0.025 0.013 6.966

171 111.865 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.030 0.026 0.018 9.085

172 111.972 ? Unidentified 0.015 0.013 0.009 5.198

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C-330
Hydrocarbon Expert V4.7 Thu Aug 26 16:57:37 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91323 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91323

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 112.348 Q10 1,2,4,5-Tetramethylbenzene 0.269 0.231 0.172 81.212

174 112.614 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.377 0.323 0.242 113.923

175 113.131 I12 C12 - IsoParaffin - 1 0.001 0.001 0.001 0.286

176 113.484 ? Unidentified 0.013 0.014 0.007 4.765

177 113.754 Q11 C11 - Aromatic - 3 0.053 0.045 0.031 15.844

178 113.945 874-35-1 H10 5-Methylindan 0.109 0.094 0.071 33.009

179 114.071 Q12 1,2-Di-i-propylbenzene 0.046 0.040 0.025 13.902

180 114.285 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.066 0.057 0.038 19.852

181 114.445 Q11 C11 - Aromatic - 4 0.035 0.030 0.020 10.503

182 114.694 824-22-6 J10 4-Methylindan 0.153 0.131 0.100 46.330

183 114.846 5161-04-6 Q11 Benzene, 1-methyl-4-(2-methylpropyl)-0.043 0.037 0.025 13.009

184 114.942 824-63-5 H10 2-Methylindan 0.116 0.099 0.076 35.088

185 115.145 ? Unidentified 0.012 0.013 0.006 4.426

186 115.258 538-68-1 Q11 n-Pentylbenzene 0.017 0.015 0.010 5.102

187 115.487 Q11 tert-Pentylbenzene 0.070 0.060 0.040 20.966

188 115.798 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.030 0.026 0.017 9.011

189 115.908 Q11 C11 - Aromatic - 6 0.040 0.036 0.023 11.982

190 116.368 100-18-5 Q12 1,4-Di-i-propylbenzene 0.058 0.050 0.031 17.460

191 116.810 91-20-3 G10 Naphthalene 0.085 0.063 0.057 26.861

192 116.945 ? Unidentified 0.007 0.008 0.004 2.642

193 117.241 Q12 C12-Aromatic-1 0.017 0.016 0.009 5.222

194 117.413 J12 Dimethyl Indane - 1 0.005 0.004 0.003 1.693

195 117.593 7364-19-4 Q12 1t-Butyl-4-ethylbenzene 0.009 0.008 0.005 2.825

196 117.893 Q12 1,3-Di-n-propylbenzene 0.043 0.037 0.023 12.830

197 118.005 Q11 C11 - Aromatic - 11 0.024 0.021 0.014 7.124

198 118.558 Q11 C11 - Aromatic - 12 0.015 0.013 0.009 4.427

199 123.439 91-57-6 G11 2-Methylnaphthalene 0.010 0.007 0.006 3.084

200 124.305 90-12-0 G11 1-Methylnaphthalene 0.005 0.004 0.003 1.565

201 126.297 ? Unidentified 0.003 0.003 0.001 1.031

202 130.003 ? Unidentified 0.003 0.002 0.002 1.044

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C-331
Hydrocarbon Expert V4.7 Thu Aug 26 16:57:37 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91323 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91323

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 7.554 74-98-6 Propane 0.001 0.001 0.002 0.237

10.023 106-97-8 n-Butane 1.038 1.366 1.537 289.748

18.114 109-66-0 n-Pentane 2.215 2.694 2.641 622.394

35.821 110-54-3 n-Hexane 3.053 3.527 3.048 861.460

58.053 142-82-5 n-Heptane 0.327 0.365 0.281 92.763

77.867 111-65-9 n-Octane 0.074 0.080 0.056 21.014

91.711 111-84-2 n-Nonane 0.156 0.166 0.105 44.343

102.801 124-18-5 n-Decane 0.017 0.018 0.010 4.852

111.711 1120-21-4 n-Undecane 0.024 0.025 0.013 6.966

I-Paraffins 8.810 75-28-5 i-Butane 0.020 0.028 0.030 5.687

10.637 463-82-1 2,2-Dimethylpropane 0.016 0.021 0.020 4.627

15.082 78-78-4 i-Pentane 4.822 5.929 5.750 1355.113

23.095 75-83-2 2,2-Dimethylbutane 0.121 0.142 0.121 34.238

28.333 79-29-8 2,3-Dimethylbutane 0.750 0.863 0.748 211.474

29.418 107-83-5 2-Methylpentane 2.416 2.818 2.412 681.717

32.067 96-14-0 3-Methylpentane 1.850 2.121 1.846 521.798

42.230 108-08-7 2,4-Dimethylpentane 0.538 0.609 0.462 152.407

42.781 464-06-2 2,2,3-Trimethylbutane 0.047 0.051 0.040 13.209

50.664 591-76-4 2-Methylhexane 1.003 1.126 0.861 284.040

52.490 589-34-4 3-Methylhexane 0.515 0.571 0.442 145.972

55.166 540-84-1 2,2,4-Trimethylpentane 3.105 3.418 2.338 881.243

64.948 564-02-3 2,2,3-Trimethylpentane 0.358 0.381 0.270 101.573

65.177 592-13-2 2,5-Dimethylhexane 0.729 0.801 0.549 207.023

65.514 589-43-5 2,4-Dimethylhexane 0.670 0.728 0.504 190.076

68.513 565-75-3 2,3,4-Trimethylpentane 3.335 3.533 2.511 946.399

69.224 560-21-4 2,3,3-Trimethylpentane 3.366 3.531 2.535 955.458

70.801 584-94-1 2,3-Dimethylhexane 0.888 0.950 0.669 252.112

72.047 592-27-8 2-Methylheptane 0.080 0.088 0.060 22.779

72.316 589-53-7 4-Methylheptane 0.114 0.124 0.086 32.426

73.361 589-81-1 3-Methylheptane 0.076 0.082 0.057 21.485

73.555 619-99-8 3-Ethylhexane 0.026 0.028 0.020 7.458

75.260 3522-94-9 2,2,5-Trimethylhexane 1.861 2.004 1.248 529.196

80.353 1069-53-0 2,3,5-Trimethylhexane 0.323 0.340 0.216 91.736

81.519 1071-26-7 2,4-Dimethylheptane 0.045 0.048 0.030 12.839

82.476 1072-05-5 2,6-Dimethylheptane 0.058 0.063 0.039 16.547

83.411 2,5-Dimethylheptane 0.145 0.155 0.098 41.337

87.277 2216-34-4 4-Methyloctane 0.007 0.008 0.005 2.113

87.409 3221-61-2 2-Methyloctane 0.010 0.011 0.007 2.976

88.270 2216-33-3 3-Methyloctane 0.010 0.011 0.007 2.970

89.323 C10 - IsoParaffin - 1 0.371 0.388 0.224 105.583

90.16514720-74-2 2,2,4-trimethylheptane 0.250 0.262 0.151 71.304

94.06415869-87-1 2,2-Dimethyloctane 0.014 0.015 0.008 3.989

94.86515869-89-3 2,5-Dimethyloctane 0.005 0.005 0.003 1.487

95.505 2051-30-1 2,4-Dimethyloctane 0.011 0.012 0.007 3.199

98.90617301-94-8 4-Methylnonane 0.010 0.011 0.006 2.956

99.884 5911-04-6 3-Methylnonane 0.016 0.017 0.010 4.631

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C-332
Hydrocarbon Expert V4.7 Thu Aug 26 16:57:37 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91323 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91323

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

I-Paraffins 100.697 C11-Isoparaffin-2 0.020 0.021 0.011 5.847

102.33417302-01-1 3-Ethyl-3-methylheptane 0.038 0.039 0.021 10.942

106.352 C11-Isoparaffin-7 0.099 0.101 0.054 28.124

108.561 C11- Isoparaffin-11 0.222 0.228 0.122 63.417

113.131 C12 - IsoParaffin - 1 0.001 0.001 0.001 0.286

Aromatics

Mono-Aromatics 45.634 71-42-3 Benzene 0.762 0.660 0.839 237.175

69.118 108-88-3 Toluene 16.516 14.511 15.421 5084.878

84.749 100-41-4 Ethylbenzene 2.921 2.566 2.367 892.510

86.000 108-38-3 m-Xylene 7.170 6.320 5.810 2190.845

86.140 106-42-3 p-Xylene 3.429 3.034 2.779 1047.780

88.942 95-47-6 o-Xylene 2.035 1.761 1.649 621.671

93.094 98-82-8 i-Propylbenzene 0.032 0.029 0.023 9.854

96.553 103-65-1 n-Propylbenzene 0.297 0.262 0.212 90.093

97.401 620-14-4 1-Methyl-3-ethylbenzene 1.153 1.016 0.825 349.962

97.635 622-96-8 1-Methyl-4-ethylbenzene 0.536 0.474 0.383 162.579

98.259 108-67-8 1,3,5-Trimethylbenzene 0.678 0.597 0.485 205.829

99.344 611-14-3 1-Methyl-2-ethylbenzene 0.394 0.341 0.282 119.695

100.977 95-63-6 1,2,4-Trimethylbenzene 1.871 1.627 1.339 568.018

102.627 538-93-2 i-Butylbenzene 0.054 0.048 0.034 16.250

103.849 526-73-8 1,2,3-Trimethylbenzene 0.234 0.199 0.167 71.027

104.614 99-87-6 1-Methyl-4-i-propylbenzene 0.039 0.035 0.025 11.844

106.546 141-93-5 1,3-Diethylbenzene 0.028 0.025 0.018 8.585

106.826 1074-43-7 1-Methyl-3-n-propylbenzene 0.365 0.323 0.234 110.217

107.162 105-05-5 1,4-Diethylbenzene 0.140 0.123 0.090 42.193

107.260 104-51-8 n-Butylbenzene 0.024 0.021 0.015 7.124

107.381 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.128 0.111 0.082 38.708

107.627 135-01-3 1,2-Diethylbenzene 0.028 0.024 0.018 8.497

108.232 1074-17-5 1-Methyl-2-n-propylbenzene 0.054 0.047 0.034 16.172

109.078 1758-88-9 1,4,Dimethyl-2-ethylbenzene 0.120 0.104 0.077 36.272

109.741 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.328 0.285 0.210 98.972

110.286 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.219 0.188 0.141 66.200

111.195 1-Methyl-4-t-butylbenzene 0.034 0.030 0.020 10.192

111.413 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.133 0.113 0.085 40.093

111.865 4218-48-8 1-Ethyl-4-i-propylbenzene 0.030 0.026 0.018 9.085

112.348 1,2,4,5-Tetramethylbenzene 0.269 0.231 0.172 81.212

112.614 527-53-7 1,2,3,5-Tetramethylbenzene 0.377 0.323 0.242 113.923

113.754 C11 - Aromatic - 3 0.053 0.045 0.031 15.844

114.071 1,2-Di-i-propylbenzene 0.046 0.040 0.025 13.902

114.285 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.066 0.057 0.038 19.852

114.445 C11 - Aromatic - 4 0.035 0.030 0.020 10.503

114.846 5161-04-6 Benzene, 1-methyl-4-(2-methylpropyl)-0.043 0.037 0.025 13.009

115.258 538-68-1 n-Pentylbenzene 0.017 0.015 0.010 5.102

115.487 tert-Pentylbenzene 0.070 0.060 0.040 20.966

115.798 577-55-9 1-Methyl-2-n-butylbenzene 0.030 0.026 0.017 9.011

115.908 C11 - Aromatic - 6 0.040 0.036 0.023 11.982

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C-333
Hydrocarbon Expert V4.7 Thu Aug 26 16:57:37 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91323 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91323

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 116.368 100-18-5 1,4-Di-i-propylbenzene 0.058 0.050 0.031 17.460

117.241 C12-Aromatic-1 0.017 0.016 0.009 5.222

117.593 7364-19-4 1t-Butyl-4-ethylbenzene 0.009 0.008 0.005 2.825

117.893 1,3-Di-n-propylbenzene 0.043 0.037 0.023 12.830

118.005 C11 - Aromatic - 11 0.024 0.021 0.014 7.124

118.558 C11 - Aromatic - 12 0.015 0.013 0.009 4.427

Naphthalenes 116.810 91-20-3 Naphthalene 0.085 0.063 0.057 26.861

123.439 91-57-6 2-Methylnaphthalene 0.010 0.007 0.006 3.084

124.305 90-12-0 1-Methylnaphthalene 0.005 0.004 0.003 1.565

Naphtheno/Olefino-Benzs 113.945 874-35-1 5-Methylindan 0.109 0.094 0.071 33.009

114.942 824-63-5 2-Methylindan 0.116 0.099 0.076 35.088

Indenes 105.043 Indan 0.076 0.060 0.055 23.343

105.637 Indene 0.239 0.189 0.174 73.690

109.394 2-Methylindan 0.042 0.033 0.028 13.032

114.694 824-22-6 4-Methylindan 0.153 0.131 0.100 46.330

117.413 Dimethyl Indane - 1 0.005 0.004 0.003 1.693

Naphthenes

Mono-Naphthenes 27.606 287-92-3 Cyclopentane 0.211 0.216 0.259 61.042

40.675 96-37-7 Methylcyclopentane 1.565 1.592 1.599 452.199

47.553 110-82-7 Cyclohexane 0.932 0.912 0.953 269.515

53.351 1759-58-6 1t,3-Dimethylcyclopentane 0.139 0.142 0.122 40.249

53.937 2532-58-3 1c,3-Dimethylcyclopentane 0.103 0.105 0.090 29.742

54.562 822-50-4 1t,2-Dimethylcyclopentane 0.133 0.135 0.116 38.375

59.64916491-15-9 Cyclopentene, 1,5-dimethyl- 0.018 0.018 0.016 5.236

61.513 108-87-2 Methylcyclohexane 0.430 0.425 0.376 124.148

64.295 1640-89-7 Ethylcyclopentane 0.024 0.024 0.021 6.964

73.225 1,3-dimethyl-t-cyclohexane 0.033 0.033 0.025 9.569

76.235 3875-51-2 i-Propylcyclopentane 0.018 0.017 0.013 5.059

76.534 2207-03-6 1t,3-Dimethylcyclohexane 0.014 0.014 0.011 4.150

78.820 C8 - MonoNaph - 3 0.058 0.058 0.045 16.896

82.171 1678-91-7 Ethylcyclohexane 0.021 0.020 0.016 5.986

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.623 115-11-7 Isobutene 0.016 0.020 0.024 4.578

9.665 106-98-9 Butene-1 0.018 0.023 0.027 5.141

10.510 624-64-6 t-Butene-2 0.072 0.091 0.111 20.857

11.251 590-18-1 c-Butene-2 0.085 0.104 0.131 24.611

16.730 109-67-1 Pentene-1 0.328 0.391 0.403 94.912

19.233 646-04-8 t-Pentene-2 0.834 0.980 1.023 241.073

20.262 627-20-3 c-Pentene-2 0.457 0.531 0.561 132.177

33.450 592-41-6 Hexene-1 0.157 0.177 0.161 45.517

36.44013269-52-8 t-Hexene-3 0.259 0.289 0.265 74.877

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C-334
Hydrocarbon Expert V4.7 Thu Aug 26 16:57:37 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91323 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91323

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

n-Olefins 36.916 4050-45-7 t-Hexene-2 0.395 0.441 0.404 114.209

38.740 7688-21-3 c-Hexene-2 0.211 0.232 0.215 60.847

55.468 592-76-7 Heptene-1 0.029 0.031 0.025 8.271

57.32814686-14-7 t-Heptene-3 0.031 0.034 0.028 9.103

58.271 7642-10-6 c-Heptene-3 0.025 0.027 0.022 7.113

59.17214686-13-6 t-Heptene-2 0.014 0.015 0.012 3.949

110.903 693-61-8 2-Undecene, (E)- 0.017 0.017 0.010 4.845

Iso-Olefins 13.450 563-45-1 3-Methylbutene-1 0.173 0.210 0.213 50.077

17.580 563-46-2 2-Methylbutene-1 0.499 0.584 0.612 144.229

20.944 513-35-9 2-Methylbutene-2 1.025 1.179 1.257 296.164

29.193 691-38-3 4-Methyl-c-pentene-2 0.045 0.051 0.046 13.117

29.841 674-76-0 4-Methyl-t-pentene-2 0.129 0.146 0.132 37.315

33.229 763-29-1 2-Methylpentene-1 0.221 0.245 0.226 63.771

37.407 625-27-4 2-Methylpentene-2 0.336 0.370 0.343 97.066

37.818 922-62-3 3-Methyl-c-pentene-2 0.259 0.283 0.265 74.916

40.089 3404-73-7 3,3-Dimethylpentene-1 0.305 0.331 0.267 88.098

42.534 594-56-9 2,3,3-Trimethylbutene-1 0.013 0.014 0.011 3.763

46.638 3404-61-3 3-Methylhexene-1 0.015 0.016 0.013 4.354

47.231 3524-73-0 5-Methylhexene-1 0.054 0.059 0.048 15.678

49.27115840-60-5 2-Methyl-c-hexene-3 0.040 0.044 0.035 11.538

49.619 3769-23-1 4-Methylhexene-1 0.012 0.013 0.010 3.337

50.261 3404-55-5 4-Methyl-t/c-hexene-2 0.050 0.054 0.044 14.467

54.855 C7 - Iso-Olefin - 2 0.022 0.023 0.019 6.381

56.801 4914-89-0 3-Methyl-c-hexene-3 0.014 0.015 0.012 3.977

57.683 6094-02-6 2-Methylhexene-1 0.056 0.062 0.049 16.277

58.547 2738-19-4 2-Methyl-2-hexene 0.026 0.027 0.022 7.371

58.79010574-36-4 3-Methyl-c-hexene-2 0.019 0.021 0.017 5.576

60.07420710-38-8 3-Methyl-t-hexene-2 0.015 0.016 0.013 4.351

60.859 4914-91-4 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.013 0.011 3.672

86.490 C9-IsoOlefin-3 0.011 0.010 0.007 3.096

Naphtheno-Olefins 22.531 1574-41-0 1,3-Cyclopentadiene 0.007 0.008 0.009 2.052

25.744 142-29-0 Cyclopentene 0.194 0.191 0.245 57.679

37.036 1120-62-3 3-Methylcyclopentene 0.101 0.101 0.106 29.186

45.833 693-89-0 1-Methylcyclopentene 0.353 0.345 0.370 104.623

51.151 110-83-8 Cyclohexene 0.044 0.041 0.046 12.672

Di-Olefins 18.626 78-79-5 2-Methyl-1,3-Butadiene 0.010 0.011 0.013 3.050

21.268 2004-70-8 1t,3-Pentadiene 0.015 0.017 0.019 4.549

45.426 1528-30-9 C6-Diolefin-1 0.015 0.015 0.015 4.249

Oxygenates 13.062 64-17-5 Ethanol 10.756 10.385 20.087 1280.145

26.900 71-23-8 n-Propanol 0.078 0.074 0.112 15.799

48.056 71-36-3 n-Butanol 0.055 0.052 0.064 11.986

Unidentified 19.880 Unidentified 0.006 0.007 0.007 2.020

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C-335
Hydrocarbon Expert V4.7 Thu Aug 26 16:57:37 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91323 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91323

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Unidentified 26.989 Unidentified 0.056 0.064 0.058 19.922

28.732 Unidentified 0.052 0.053 0.051 18.373

50.836 Unidentified 0.039 0.043 0.035 13.977

63.384 Unidentified 0.027 0.029 0.021 9.577

72.449 Unidentified 0.075 0.080 0.057 26.628

84.900 Unidentified 0.020 0.021 0.014 7.125

85.148 Unidentified 0.020 0.019 0.013 6.955

86.597 Unidentified 0.009 0.009 0.006 3.115

88.747 Unidentified 0.119 0.133 0.081 42.266

93.840 Unidentified 0.043 0.045 0.026 15.189

99.113 Unidentified 0.166 0.174 0.100 58.751

100.351 Unidentified 0.013 0.010 0.007 4.764

100.481 Unidentified 0.037 0.037 0.020 12.966

101.163 Unidentified 0.026 0.028 0.016 9.046

101.284 Unidentified 0.015 0.015 0.009 5.207

102.899 Unidentified 0.017 0.015 0.011 6.081

103.197 Unidentified 0.011 0.011 0.006 3.792

108.079 Unidentified 0.025 0.026 0.014 8.864

108.354 Unidentified 0.029 0.030 0.016 10.424

108.435 Unidentified 0.027 0.028 0.015 9.667

108.743 Unidentified 0.072 0.073 0.039 25.407

109.167 Unidentified 0.311 0.270 0.199 110.054

110.709 Unidentified 0.006 0.006 0.004 2.242

111.038 Unidentified 0.022 0.023 0.014 7.882

111.972 Unidentified 0.015 0.013 0.009 5.198

113.484 Unidentified 0.013 0.014 0.007 4.765

115.145 Unidentified 0.012 0.013 0.006 4.426

116.945 Unidentified 0.007 0.008 0.004 2.642

126.297 Unidentified 0.003 0.003 0.001 1.031

130.003 Unidentified 0.003 0.002 0.002 1.044

Plus

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C-336
Hydrocarbon Expert V4.7 Thu Aug 26 16:57:37 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91323 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91323

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF

20.0 15.0 10.0 5.0 0.0

Propane

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

Ethanol

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

Unidentified

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

1,3-Cyclopentadiene

2,2-Dimethylbutane

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C-337
Hydrocarbon Expert V4.7 Thu Aug 26 16:57:37 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91323 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91323

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

n-Propanol Unidentified

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

n-Hexane

t-Hexene-3

t-Hexene-2 3-Methylcyclopentene

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane 2,3,3-Trimethylbutene-1 2,2,3-Trimethylbutane

C6-Diolefin-1 Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1

Cyclohexane

n-Butanol

2-Methyl-c-hexene-3

4-Methylhexene-1

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C-338
Hydrocarbon Expert V4.7 Thu Aug 26 16:57:37 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91323 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91323

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF

70.0 65.0 60.0 55.0 50.0

4-Methyl-t/c-hexene-2

2-Methylhexane Unidentified Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane C7 - Iso-Olefin - 2

2,2,4-Trimethylpentane Heptene-1

3-Methyl-c-hexene-3

t-Heptene-3

2-Methylhexene-1

n-Heptane c-Heptene-3 2-Methyl-2-hexene 3-Methyl-c-hexene-2

t-Heptene-2

Cyclopentene, 1,5-dimethyl3-Methyl-t-hexene-2

2-Pentene, 3,4-dimethyl-, (Z)-

Methylcyclohexane

Unidentified

Ethylcyclopentane

2,2,3-Trimethylpentane 2,5-Dimethylhexane

2,4-Dimethylhexane

2,3,4-Trimethylpentane

2,3,3-Trimethylpentane Toluene

2,3-Dimethylhexane

2-Methylheptane

Unidentified 4-Methylheptane

1,3-dimethyl-t-cyclohexane 3-Methylheptane 3-Ethylhexane

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C-339
Hydrocarbon Expert V4.7 Thu Aug 26 16:57:37 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91323 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91323

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF

95.0 90.0 85.0 80.0 75.0

2,2,5-Trimethylhexane

i-Propylcyclopentane 1t,3-Dimethylcyclohexane

n-Octane

C8 - MonoNaph - 3

2,3,5-Trimethylhexane

2,4-Dimethylheptane

Ethylcyclohexane 2,6-Dimethylheptane

2,5-Dimethylheptane

Unidentified Ethylbenzene

m-Xylene p-Xylene

C9-IsoOlefin-3 Unidentified

4-Methyloctane 2-Methyloctane

3-Methyloctane

Unidentified o-Xylene

C10 - IsoParaffin - 1

2,2,4-trimethylheptane

n-Nonane

i-Propylbenzene

Unidentified 2,2-Dimethyloctane

2,5-Dimethyloctane

2,4-Dimethyloctane

n-Propylbenzene

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

4-Methylnonane Unidentified 1-Methyl-2-ethylbenzene

3-Methylnonane

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C-340
Hydrocarbon Expert V4.7 Thu Aug 26 16:57:37 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91323 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91323

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified

C11-Isoparaffin-2 1,2,4-Trimethylbenzene Unidentified

3-Ethyl-3-methylheptane i-Butylbenzene n-Decane Unidentified Unidentified

1,2,3-Trimethylbenzene

1-Methyl-4-i-propylbenzene

Indan

Indene

C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene

n-Butylbenzene 1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

Unidentified 1-Methyl-2-n-propylbenzene

C11- Isoparaffin-11 Unidentified

1,4,Dimethyl-2-ethylbenzene Unidentified 2-Methylindan

1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

Unidentified 2-Undecene, (E)- Unidentified 1-Methyl-4-t-butylbenzene 1,2-Dimethyl-3-ethylbenzene n-Undecane Unidentified 1-Ethyl-4-i-propylbenzene

1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene

C12 - IsoParaffin - 1

Unidentified C11 - Aromatic - 3 5-Methylindan 1,2-Di-i-propylbenzene 1-methyl-4-(1-methylpropyl)be C11 - Aromatic - 4 4-Methylindan Benzene, 1-methyl-4-(2-methylpropyl)- 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene 1-Methyl-2-n-butylbenzene C11 - Aromatic - 6

1,4-Di-i-propylbenzene

Unidentified Naphthalene

C12-Aromatic-1 Dimethyl Indane - 1 1t-Butyl-4-ethylbenzene

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

C11 - Aromatic - 12

2-Methylnaphthalene

1-Methylnaphthalene

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C-341
Hydrocarbon Expert V4.7 Thu Aug 26 16:57:37 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF 24-Aug-10, 22:43:27

Sample: ODDB-91323 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91323

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000005.D\SIG2000005_FID2_B.CDF

145.0 140.0 135.0 130.0 125.0

Unidentified

Unidentified

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C-342
Hydrocarbon Expert V4.0 Fri Apr 11 11:06:22 2008 Page 1

File: C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF 10-Apr-08, 17:29:10

Sample: ODDB-69590 Operator: AAD

Parameter: C:\HPCHEM\HCE40\ODDB-69590

ODDB-69590

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 7.234 8.810 9.515

I-Paraffins 22.271 24.875 21.153

Aromatics 37.108 32.516 33.093

Mono-Aromatics 36.003 31.605 32.266

Naphthalenes 0.165 0.127 0.121

Naphtheno/Olefino-Benz 0.497 0.427 0.366

Indenes 0.336 0.267 0.277

Naphthenes 21.259 20.874 23.909

Mono-Naphthenes 20.986 20.612 23.717

Di/Bicyclo-Naphthenes 0.083 0.079 0.052

Olefins 7.129 8.023 8.698

n-Olefins 2.777 3.193 3.564

Iso-Olefins 3.420 3.858 4.130

Naphtheno-Olefins 0.267 0.260 0.362

Di-Olefins 0.227 0.242 0.259

Oxygenates 0.116 0.120 0.128

Plus 0.000 0.000 0.000

C-343
Hydrocarbon Expert V4.0 Fri Apr 11 11:06:22 2008 Page 1

File: C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF 10-Apr-08, 17:29:10

Sample: ODDB-69590 Operator: AAD

Parameter: C:\HPCHEM\HCE40\ODDB-69590

ODDB-69590

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C4 3.876 5.106 6.498

C5 7.910 9.450 10.785

C6 26.058 26.494 30.087

C7 11.034 10.318 11.449

C8 20.377 19.845 18.095

C9 16.174 14.853 12.909

C10 7.142 6.810 5.063

C11 1.997 1.851 1.287

C12 0.513 0.456 0.305

C13 0.034 0.034 0.018

C-344
Hydrocarbon Expert V4.0 Fri Apr 11 11:06:22 2008 Page 1

File: C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF 10-Apr-08, 17:29:10

Sample: ODDB-69590 Operator: AAD

Parameter: C:\HPCHEM\HCE40\ODDB-69590

ODDB-69590

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C4 3.709 4.895 6.211

C5 0.862 1.051 1.162

C6 0.555 0.643 0.627

C7 0.088 0.098 0.085

C8 0.102 0.111 0.087

C9 0.699 0.744 0.530

C10 0.933 0.976 0.638

C11 0.236 0.242 0.147

C12 0.036 0.037 0.021

C13 0.014 0.014 0.007

I-Paraffins C4 0.030 0.041 0.050

C5 3.458 4.266 4.663

C6 3.513 4.076 3.967

C7 1.536 1.730 1.492

C8 8.775 9.559 7.475

C9 2.009 2.136 1.524

C10 2.381 2.480 1.628

C11 0.548 0.566 0.341

C13 0.020 0.020 0.011

Aromatics C12 0.106 0.091 0.063

Mono-Aromatics C6 0.710 0.617 0.885

C7 8.300 7.312 8.766

C8 11.138 9.812 10.210

C9 12.056 10.565 9.761

C10 2.395 2.095 1.736

C11 1.128 0.968 0.743

C12 0.275 0.236 0.165

Naphthalenes C10 0.132 0.103 0.098

C11 0.033 0.025 0.022

Naphtheno/Olefino-BenzsC10 0.497 0.427 0.366

Indenes C10 0.336 0.267 0.277

Naphthenes C8 0.011 0.011 0.010

C9 0.115 0.112 0.089

C10 0.011 0.010 0.007

C11 0.052 0.050 0.033

Mono-Naphthenes C5 0.104 0.106 0.144

C-345
Hydrocarbon Expert V4.0 Fri Apr 11 11:06:22 2008 Page 2

File: C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF 10-Apr-08, 17:29:10

Sample: ODDB-69590 Operator: AAD

Parameter: C:\HPCHEM\HCE40\ODDB-69590

ODDB-69590

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Mono-Naphthenes C6 19.262 18.921 22.272

C7 0.289 0.293 0.286

C8 0.222 0.219 0.193

C9 0.826 0.804 0.637

C10 0.187 0.175 0.130

C12 0.096 0.092 0.056

Di/Bicyclo-Naphthenes C10 0.083 0.079 0.052

Olefins C4 0.000 0.000 0.000

C6 0.058 0.064 0.067

C7 0.048 0.053 0.048

C8 0.016 0.017 0.016

C9 0.317 0.337 0.252

n-Olefins C4 0.137 0.170 0.237

C5 1.492 1.756 2.070

C6 0.903 1.009 1.044

C7 0.090 0.098 0.090

C8 0.036 0.038 0.031

C9 0.119 0.121 0.092

Iso-Olefins C5 1.626 1.891 2.257

C6 0.961 1.070 1.111

C7 0.614 0.663 0.608

C9 0.032 0.035 0.025

C10 0.187 0.198 0.130

Naphtheno-Olefins C5 0.191 0.189 0.273

C6 0.076 0.071 0.090

Di-Olefins C5 0.062 0.071 0.089

C6 0.020 0.022 0.024

C7 0.068 0.070 0.073

C8 0.076 0.078 0.073

Oxygenates C5 0.116 0.120 0.128

C-346
Hydrocarbon Expert V4.0 Fri Apr 11 11:06:22 2008 Page 1

File: C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF 10-Apr-08, 17:29:10

Sample: ODDB-69590 Operator: AAD

Parameter: C:\HPCHEM\HCE40\ODDB-69590

ODDB-69590

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol

1 8.665 75-28-5 I4 i-Butane 0.030 0.041 0.050

2 9.390 115-11-7 O4 isobutene 0.000 0.000 0.000

3 9.430 106-98-9 K4 Butene-1 0.013 0.017 0.023

4 9.737 106-97-8 P4 n-Butane 3.709 4.895 6.211

5 10.183 624-64-6 K4 t-Butene-2 0.038 0.048 0.065

6 10.265 463-82-1 I5 2,2-Dimethylpropane 0.064 0.083 0.087

7 10.825 590-18-1 K4 c-Butene-2 0.086 0.106 0.149

8 12.802 563-45-1 C5 3-Methylbutene-1 0.078 0.095 0.108

9 14.153 78-78-4 I5 i-Pentane 3.393 4.183 4.576

10 15.639 109-67-1 K5 Pentene-1 0.294 0.351 0.408

11 16.404 563-46-2 C5 2-Methylbutene-1 0.497 0.584 0.690

12 16.870 109-66-0 P5 n-Pentane 0.862 1.051 1.162

13 17.412 78-79-5 E5 2-Methyl-1,3-Butadiene 0.018 0.020 0.026

14 17.907 646-04-8 K5 t-Pentene-2 0.757 0.892 1.050

15 18.484 598-25-4 E5 3-Methylbutadiene-1,2 0.031 0.037 0.044

16 18.852 627-20-3 K5 c-Pentene-2 0.441 0.513 0.611

17 19.472 513-35-9 C5 2-Methylbutene-2 1.051 1.212 1.459

20 21.064 1574-41-0 E5 1c,3-Pentadiene 0.013 0.014 0.019

21 21.415 75-83-2 I6 2,2-Dimethylbutane 0.081 0.095 0.092

22 23.926 142-29-0 B5 Cyclopentene 0.191 0.189 0.273

24 25.084 691-37-2 C6 4-Methylpentene-1 0.085 0.097 0.098

25 25.643 287-92-3 M5 Cyclopentane 0.104 0.106 0.144

26 26.327 79-29-8 I6 2,3-Dimethylbutane 0.885 1.021 0.999

27 26.739 1634-04-4 X5 Methyl-t-butylether 0.116 0.120 0.128

28 27.175 691-38-3 C6 4-Methyl-c-pentene-2 0.046 0.052 0.053

29 27.366 107-83-5 I6 2-Methylpentane 1.568 1.834 1.771

30 27.797 674-76-0 C6 4-Methyl-t-pentene-2 0.146 0.166 0.169

31 29.878 96-14-0 I6 3-Methylpentane 0.979 1.126 1.106

32 31.033 763-29-1 C6 2-Methylpentene-1 0.182 0.203 0.211

33 31.253 592-41-6 K6 Hexene-1 0.140 0.158 0.162

35 33.480 110-54-3 P6 n-Hexane 0.555 0.643 0.627

36 34.14913269-52-8 K6 t-Hexene-3 0.203 0.227 0.235

37 34.609 4050-45-7 K6 t-Hexene-2 0.380 0.426 0.440

38 35.080 625-27-4 C6 2-Methylpentene-2 0.277 0.306 0.320

39 35.333 O6 O13 0.058 0.064 0.067

40 35.465 922-62-3 C6 3-Methyl-c-pentene-2 0.225 0.246 0.260

41 36.378 7688-21-3 K6 c-Hexene-2 0.179 0.198 0.207

43 37.682 3404-73-7 C7 3,3-Dimethylpentene-1 0.234 0.255 0.232

45 38.162 96-37-7 M6 Methylcyclopentane 0.616 0.628 0.712

46 38.970 563-79-1 E7 2,3-Dimethyl-2-Butene 0.017 0.018 0.020

48 39.715 108-08-7 I7 2,4-Dimethylpentane 0.605 0.687 0.587

49 40.217 464-06-2 I7 2,2,3-Trimethylbutane 0.063 0.069 0.061

52 41.934 762-63-0 C7 4,4-Dimethyl-c-pentene-2 0.018 0.019 0.018

53 42.875 E6 Diolefin 0.020 0.022 0.024

C-347
Hydrocarbon Expert V4.0 Fri Apr 11 11:06:22 2008 Page 2

File: C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF 10-Apr-08, 17:29:10

Sample: ODDB-69590 Operator: AAD

Parameter: C:\HPCHEM\HCE40\ODDB-69590

ODDB-69590

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol

54 43.156 71-42-3 Q6 Benzene 0.710 0.617 0.885

55 44.152 C7 2-Methyl-c-hexene-3 0.042 0.046 0.042

56 45.167 110-82-7 M6 Cyclohexane 18.646 18.293 21.560

58 45.604 692-24-0 C7 2-Methyl-t-hexene-3 0.033 0.037 0.033

62 46.682 7357-93-9 C7 2-Ethyl-3-methylbutene-1 0.038 0.041 0.038

63 47.002 3769-23-1 C7 4-Methylhexene-1 0.022 0.024 0.022

66 47.632 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.034 0.037 0.034

67 47.983 591-76-4 I7 2-Methylhexane 0.594 0.668 0.577

69 48.455 110-83-8 B6 Cyclohexene 0.076 0.071 0.090

74 49.779 589-34-4 I7 3-Methylhexane 0.275 0.306 0.267

75 50.579 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.095 0.097 0.094

76 51.157 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.069 0.070 0.068

78 51.768 822-50-4 M7 1t,2-Dimethylcyclopentane 0.037 0.038 0.037

80 52.461 540-84-1 I8 2,2,4-Trimethylpentane 4.369 4.823 3.722

81 52.940 1541-23-7 E7 1,5-Heptadiene 0.051 0.052 0.054

83 54.104 4914-89-0 C7 3-Methyl-c-hexene-3 0.032 0.034 0.032

84 54.58214686-14-7 K7 t-Heptene-3 0.037 0.041 0.037

85 54.904 O7 C7-Olefin2 0.038 0.042 0.038

86 55.289 142-82-5 P7 n-Heptane 0.088 0.098 0.085

87 55.533 7642-10-6 K7 c-Heptene-3 0.032 0.035 0.032

88 55.856 2738-19-4 C7 2-Methyl-2-hexene 0.027 0.029 0.027

89 56.07510574-36-4 C7 3-Methyl-c-hexene-2 0.044 0.047 0.043

90 56.611 816-79-5 C7 3-Ethylpentene-2 0.020 0.022 0.020

91 56.835 C7 1,5-DM-Cyclopentene 0.040 0.042 0.040

92 57.36520710-38-8 C7 3-Methyl-t-hexene-2 0.028 0.030 0.028

94 58.099 6443-92-1 K7 c-Heptene-2 0.021 0.023 0.021

95 58.576 108-87-2 M7 Methylcyclohexane 0.058 0.057 0.057

96 58.978 1192-18-3 M7 1c,2-Dimethylcyclopentane 0.013 0.014 0.013

98 59.535 4516-69-2 M8 1,1,3-Trimethylcyclopentane 0.014 0.014 0.012

105 61.384 1640-89-7 M7 Ethylcyclopentane 0.017 0.017 0.017

106 62.004 564-02-3 I8 2,2,3-Trimethylpentane 0.282 0.301 0.240

107 62.305 592-13-2 I8 2,5-Dimethylhexane 0.592 0.652 0.504

108 62.628 589-43-5 I8 2,4-Dimethylhexane 0.547 0.597 0.466

109 63.418 4850-28-6 M8 1c,2t,4-Trimethylcyclopentane 0.014 0.014 0.012

111 63.852 563-16-6 I8 3,3-Dimethylhexane 0.017 0.019 0.015

112 64.156 O7 O38 0.010 0.010 0.010

115 64.995 O8 C8-Olefin2 0.016 0.017 0.016

116 65.708 565-75-3 I8 2,3,4-Trimethylpentane 1.855 1.970 1.580

117 66.486 108-88-3 Q7 Toluene 8.300 7.312 8.766

118 67.750 E8 C8-Diolefin3 0.054 0.056 0.054

119 68.152 584-94-1 I8 2,3-Dimethylhexane 0.779 0.836 0.664

120 69.499 592-27-8 I8 2-Methylheptane 0.083 0.090 0.070

121 69.733 589-53-7 I8 4-Methylheptane 0.082 0.089 0.070

124 70.866 589-81-1 I8 3-Methylheptane 0.169 0.183 0.144

C-348
Hydrocarbon Expert V4.0 Fri Apr 11 11:06:22 2008 Page 3

File: C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF 10-Apr-08, 17:29:10

Sample: ODDB-69590 Operator: AAD

Parameter: C:\HPCHEM\HCE40\ODDB-69590

ODDB-69590

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol

125 71.864 1002-33-1 E8 1,3-Octadiene 0.022 0.022 0.020

128 72.818 3522-94-9 I9 2,2,5-Trimethylhexane 0.772 0.834 0.586

129 73.097 M8 3c-Ethylmethylcyclopentane 0.021 0.021 0.018

130 73.348 M8 3t-Ethylmethylcyclopentane 0.021 0.021 0.019

131 73.604 111-66-0 M8 2t-Ethylmethylcyclopentane 0.017 0.017 0.015

132 73.78314850-23-8 K8 t-Octene-4 0.028 0.030 0.025

133 74.03116747-50-5 M8 1,1-Methylethylcyclopentane 0.038 0.037 0.033

135 74.34116747-26-5 I9 2,2,4-Trimethylhexane 0.018 0.019 0.014

137 74.776 2207-03-6 M8 1t,3-Dimethylcyclohexane 0.012 0.012 0.010

139 75.13019549-89-4 C9 3,3-Dimethylheptene-1 0.015 0.015 0.011

140 75.316 M8 1c,2c,3-Trimethylcyclopentane 0.030 0.029 0.026

141 75.601 111-65-9 P8 n-Octane 0.102 0.111 0.087

142 76.451 O9 C9-Olefin1 0.072 0.077 0.063

143 77.055 O9 C9-Olefin2 0.019 0.020 0.015

146 77.622 7642-04-8 K8 c-Octene-2 0.008 0.008 0.007

148 78.070 921-47-1 I9 2,3,4-Trimethylhexane 0.146 0.151 0.111

152 79.304 2207-01-4 M8 1c,2-Dimethylcyclohexane 0.037 0.035 0.032

154 79.868 1071-26-7 I9 2,2-Dimethylheptane 0.071 0.077 0.054

155 80.13519550-75-6 C9 t-2,2-Dimethylheptene-3 0.017 0.019 0.013

156 80.29616747-25-4 I9 2,2,3-Trimethylhexane 0.075 0.080 0.057

157 80.677 1068-19-5 I9 4,4-Dimethylheptane 0.049 0.052 0.037

158 81.028 1678-91-7 M8 Ethylcyclohexane 0.020 0.019 0.017

159 81.245 1795-27-3 M9 1c,3c,5-Trimethylcyclohexane 0.089 0.088 0.068

160 81.418 4032-86-4 I9 3,3-Dimethylheptane 0.032 0.034 0.024

162 81.926 3074-75-7 I9 2-Methyl-4-ethylhexane 0.026 0.027 0.020

164 82.409 N8 N8 0.011 0.011 0.010

165 82.776 100-41-4 Q8 Ethylbenzene 9.943 8.759 9.114

166 82.993 7667-60-9 M9 1c,2t,4t-Trimethylcyclohexane 0.396 0.388 0.306

168 83.880 108-38-3 Q8 m-Xylene 0.377 0.334 0.346

169 84.052 106-42-3 Q8 p-Xylene 0.476 0.422 0.436

171 84.793 1067-20-5 I9 3,3-Diethylpentane 0.133 0.135 0.101

172 85.212 2216-34-4 I9 4-Methyloctane 0.117 0.124 0.089

173 85.350 3221-61-2 I9 2-Methyloctane 0.188 0.202 0.143

175 86.046 M9 1c,2t,4c-Trimethylcyclohexane 0.066 0.065 0.050

176 86.228 2216-33-3 I9 3-Methyloctane 0.198 0.210 0.150

178 86.897 95-47-6 Q8 o-Xylene 0.341 0.296 0.313

179 87.278 O9 C9-Olefin4 0.226 0.240 0.174

180 87.636 N9 N18 0.045 0.044 0.035

182 88.113 I9 C9-Isoparaffin1 0.184 0.192 0.140

185 89.35620237-46-0 K9 c-Nonene-3 0.036 0.040 0.028

187 89.785 111-84-2 P9 n-Nonane 0.699 0.744 0.530

188 90.189 4926-90-3 M9 1,1-Methylethylcyclohexane 0.130 0.123 0.100

189 90.546 4984-01-4 C10 3,7-Dimethyloctene-1 0.095 0.104 0.066

190 91.144 98-82-8 Q9 i-Propylbenzene 0.100 0.089 0.081

C-349
Hydrocarbon Expert V4.0 Fri Apr 11 11:06:22 2008 Page 4

File: C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF 10-Apr-08, 17:29:10

Sample: ODDB-69590 Operator: AAD

Parameter: C:\HPCHEM\HCE40\ODDB-69590

ODDB-69590

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol

191 91.440 6434-77-1 K9 c-Nonene-2 0.083 0.081 0.064

192 91.741 N9 N26 0.044 0.042 0.034

193 91.854 696-29-7 M9 i-Propylcyclohexane 0.066 0.063 0.051

194 92.08815869-87-1 I10 2,2-Dimethyloctane 0.116 0.122 0.079

195 92.267 N9 N28 0.026 0.025 0.020

196 92.360 4032-94-4 I10 2,4-Dimethyloctane 0.059 0.062 0.040

197 92.777 2051-30-1 I10 2,6-Dimethyloctane 0.065 0.069 0.045

198 92.92215869-89-3 I10 2,5-Dimethyloctane 0.088 0.092 0.060

201 93.403 I10 I12 0.071 0.074 0.048

202 93.526 2040-95-1 M9 n-Butylcyclopentane 0.079 0.077 0.061

203 93.774 N10 N30 0.011 0.010 0.007

204 93.958 4110-44-5 I10 3,3-Dimethyloctane 0.182 0.188 0.125

205 94.091 I10 I14 0.056 0.059 0.039

207 94.625 103-65-1 Q9 n-Propylbenzene 0.586 0.519 0.474

208 94.80752896-90-9 I10 3-Methyl-5-ethylheptane 0.166 0.174 0.113

212 95.517 620-14-4 Q9 1-Methyl-3-ethylbenzene 2.398 2.118 1.941

213 95.733 622-96-8 Q9 1-Methyl-4-ethylbenzene 1.381 1.225 1.118

215 96.365 108-67-8 Q9 1,3,5-Trimethylbenzene 1.504 1.327 1.217

217 96.82515869-85-9 I10 5-Methylnonane 0.172 0.180 0.118

218 97.01617301-94-8 I10 4-Methylnonane 0.268 0.279 0.183

219 97.167 871-83-0 I10 2-Methylnonane 0.199 0.209 0.136

221 97.421 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.893 0.775 0.723

222 97.666 5881-17-4 I10 3-Ethyloctane 0.156 0.161 0.107

223 98.002 5911-04-6 I10 3-Methylnonane 0.355 0.370 0.243

226 98.558 I10 C10-Isoparaffin1 0.071 0.073 0.048

227 98.797 I10 I19 0.084 0.086 0.057

228 99.127 95-63-6 Q9 1,2,4-Trimethylbenzene 4.188 3.652 3.391

229 99.484 I10 I21 0.174 0.180 0.119

230 99.713 I10 C10-Isoparaffin2 0.099 0.103 0.068

232 100.38819781-18-0 C10 2,3-Dimethyloctene-2 0.092 0.095 0.064

234 100.721 135-98-8 Q10 sec-Butylbenzene 0.093 0.082 0.067

235 100.943 124-18-5 P10 n-Decane 0.933 0.976 0.638

236 101.260 I11 I26 0.063 0.066 0.040

237 101.406 I11 C11-Isoparaffin1 0.061 0.063 0.038

238 101.646 N11 N39 0.052 0.050 0.033

240 101.929 526-73-8 Q9 1,2,3-Trimethylbenzene 1.006 0.859 0.815

241 102.363 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.076 0.067 0.055

245 102.734 99-87-6 Q10 1-Methyl-4-i-propylbenzene 0.055 0.049 0.040

247 103.104 496-11-7 J10 2,3-Dihydroindene 0.336 0.267 0.277

248 103.375 7058-01-7 M10 sec-Butylcyclohexane 0.187 0.175 0.130

249 103.744 527-84-4 Q10 1-Methyl-2-i-propylbenzene 0.161 0.141 0.117

250 103.87017362-11-3 I11 3-Ethylnonane 0.062 0.063 0.038

255 104.726 141-93-5 Q10 1,3-Diethylbenzene 0.130 0.115 0.094

256 104.963 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 0.418 0.371 0.303

C-350
Hydrocarbon Expert V4.0 Fri Apr 11 11:06:22 2008 Page 5

File: C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF 10-Apr-08, 17:29:10

Sample: ODDB-69590 Operator: AAD

Parameter: C:\HPCHEM\HCE40\ODDB-69590

ODDB-69590

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol

258 105.376 105-05-5 Q10 1,4-Diethylbenzene 0.147 0.130 0.106

259 105.600 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.325 0.282 0.236

260 105.859 135-01-3 Q10 1,2-Diethylbenzene 0.088 0.076 0.064

262 106.338 493-02-7 D10 t-Decahydronaphthalene 0.083 0.079 0.052

263 106.626 I11 C11-Isoparaffin3 0.183 0.189 0.114

265 106.934 I11 C11-Isoparaffin4 0.094 0.097 0.058

267 107.263 I11 C11-Isoparaffin5 0.085 0.088 0.053

269 107.626 874-41-9 Q10 1,3-Dimethyl-4-ethylbenzene 0.181 0.157 0.131

272 108.189 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.342 0.299 0.248

274 108.761 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.202 0.173 0.146

276 109.533 Q11 4M-1tC4Benz 0.040 0.034 0.029

279 109.939 Q11 1-Methyl-4-t-butylbenzene 0.066 0.059 0.043

280 110.112 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.116 0.099 0.084

281 110.462 1120-21-4 P11 n-Undecane 0.236 0.242 0.147

282 110.643 95-93-2 Q10 1,2,4,5-Tetramethylbenzene 0.062 0.054 0.045

285 111.188 Q11 1-Methyl-1-n-butylbenzene 0.266 0.228 0.175

286 111.499 1074-92-6 Q11 1-t-Butyl-2-methylbenzene 0.374 0.321 0.245

294 112.992 Q11 C11-Aromatic1 0.067 0.058 0.044

295 113.130 874-35-1 H10 5-Methylindan 0.121 0.104 0.089

296 113.327 Q11 C11-Aromatic2 0.092 0.079 0.061

297 113.607 Q11 C11-Aromatic3 0.157 0.135 0.103

298 114.011 824-22-6 H10 4-Methylindan 0.191 0.164 0.141

299 114.347 824-63-5 H10 2-Methylindan 0.185 0.159 0.136

302 115.130 M12 1t-M-2-(4-MP)cyclopentane 0.096 0.092 0.056

305 115.513 Q11 1-Methyl-2-n-butylbenzene 0.038 0.033 0.025

306 115.652 100-18-5 Q12 1,4-Di-i-propylbenzene 0.105 0.090 0.063

308 116.284 119-64-2 G10 1,2,3,4-Tetrahydronaphthalene 0.096 0.076 0.071

310 116.785 91-20-3 G10 Naphthalene 0.036 0.027 0.027

313 117.363 Q12 1t-Butyl-4-ethylbenzene 0.046 0.039 0.027

317 118.243 Q12 1,3-Di-n-propylbenzene 0.053 0.046 0.032

318 118.374 A12 A5 0.106 0.091 0.063

319 119.065 112-40-3 P12 n-Dodecane 0.036 0.037 0.021

325 120.531 102-25-0 Q12 1,3,5-Triethylbenzene 0.011 0.010 0.007

329 121.198 877-44-1 Q12 1,2,4-Triethylbenzene 0.027 0.023 0.016

336 122.541 Q12 1-Methyl-4-n-pentylbenzene 0.021 0.018 0.013

342 123.524 1077-16-3 Q12 n-Hexylbenzene 0.012 0.010 0.007

343 123.748 I13 I49 0.020 0.020 0.011

350 124.932 700-12-9 Q11 Pentamethylbenzene 0.028 0.021 0.018

354 125.810 91-57-6 G11 2-Methylnaphthalene 0.020 0.015 0.013

357 126.386 90-12-0 G11 1-Methylnaphthalene 0.013 0.010 0.009

360 126.764 629-50-5 P13 n-Tridecane 0.014 0.014 0.007

C-351
Hydrocarbon Expert V4.0 Fri Apr 11 11:06:22 2008 Page 1

File: C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF 10-Apr-08, 17:29:10

Sample: ODDB-69590 Operator: AAD

Parameter: C:\HPCHEM\HCE40\ODDB-69590

ODDB-69590

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol

Paraffin 9.737 106-97-8 n-Butane 3.709 4.895 6.211

16.870 109-66-0 n-Pentane 0.862 1.051 1.162

33.480 110-54-3 n-Hexane 0.555 0.643 0.627

55.289 142-82-5 n-Heptane 0.088 0.098 0.085

75.601 111-65-9 n-Octane 0.102 0.111 0.087

89.785 111-84-2 n-Nonane 0.699 0.744 0.530

100.943 124-18-5 n-Decane 0.933 0.976 0.638

110.462 1120-21-4 n-Undecane 0.236 0.242 0.147

119.065 112-40-3 n-Dodecane 0.036 0.037 0.021

126.764 629-50-5 n-Tridecane 0.014 0.014 0.007

I-Paraffins 8.665 75-28-5 i-Butane 0.030 0.041 0.050

10.265 463-82-1 2,2-Dimethylpropane 0.064 0.083 0.087

14.153 78-78-4 i-Pentane 3.393 4.183 4.576

21.415 75-83-2 2,2-Dimethylbutane 0.081 0.095 0.092

26.327 79-29-8 2,3-Dimethylbutane 0.885 1.021 0.999

27.366 107-83-5 2-Methylpentane 1.568 1.834 1.771

29.878 96-14-0 3-Methylpentane 0.979 1.126 1.106

39.715 108-08-7 2,4-Dimethylpentane 0.605 0.687 0.587

40.217 464-06-2 2,2,3-Trimethylbutane 0.063 0.069 0.061

47.983 591-76-4 2-Methylhexane 0.594 0.668 0.577

49.779 589-34-4 3-Methylhexane 0.275 0.306 0.267

52.461 540-84-1 2,2,4-Trimethylpentane 4.369 4.823 3.722

62.004 564-02-3 2,2,3-Trimethylpentane 0.282 0.301 0.240

62.305 592-13-2 2,5-Dimethylhexane 0.592 0.652 0.504

62.628 589-43-5 2,4-Dimethylhexane 0.547 0.597 0.466

63.852 563-16-6 3,3-Dimethylhexane 0.017 0.019 0.015

65.708 565-75-3 2,3,4-Trimethylpentane 1.855 1.970 1.580

68.152 584-94-1 2,3-Dimethylhexane 0.779 0.836 0.664

69.499 592-27-8 2-Methylheptane 0.083 0.090 0.070

69.733 589-53-7 4-Methylheptane 0.082 0.089 0.070

70.866 589-81-1 3-Methylheptane 0.169 0.183 0.144

72.818 3522-94-9 2,2,5-Trimethylhexane 0.772 0.834 0.586

74.34116747-26-5 2,2,4-Trimethylhexane 0.018 0.019 0.014

78.070 921-47-1 2,3,4-Trimethylhexane 0.146 0.151 0.111

79.868 1071-26-7 2,2-Dimethylheptane 0.071 0.077 0.054

80.29616747-25-4 2,2,3-Trimethylhexane 0.075 0.080 0.057

80.677 1068-19-5 4,4-Dimethylheptane 0.049 0.052 0.037

81.418 4032-86-4 3,3-Dimethylheptane 0.032 0.034 0.024

81.926 3074-75-7 2-Methyl-4-ethylhexane 0.026 0.027 0.020

84.793 1067-20-5 3,3-Diethylpentane 0.133 0.135 0.101

85.212 2216-34-4 4-Methyloctane 0.117 0.124 0.089

85.350 3221-61-2 2-Methyloctane 0.188 0.202 0.143

86.228 2216-33-3 3-Methyloctane 0.198 0.210 0.150

88.113 C9-Isoparaffin1 0.184 0.192 0.140

92.08815869-87-1 2,2-Dimethyloctane 0.116 0.122 0.079

92.360 4032-94-4 2,4-Dimethyloctane 0.059 0.062 0.040

92.777 2051-30-1 2,6-Dimethyloctane 0.065 0.069 0.045

C-352
Hydrocarbon Expert V4.0 Fri Apr 11 11:06:22 2008 Page 2

File: C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF 10-Apr-08, 17:29:10

Sample: ODDB-69590 Operator: AAD

Parameter: C:\HPCHEM\HCE40\ODDB-69590

ODDB-69590

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol

I-Paraffins 92.92215869-89-3 2,5-Dimethyloctane 0.088 0.092 0.060

93.403 I12 0.071 0.074 0.048

93.958 4110-44-5 3,3-Dimethyloctane 0.182 0.188 0.125

94.091 I14 0.056 0.059 0.039

94.80752896-90-9 3-Methyl-5-ethylheptane 0.166 0.174 0.113

96.82515869-85-9 5-Methylnonane 0.172 0.180 0.118

97.01617301-94-8 4-Methylnonane 0.268 0.279 0.183

97.167 871-83-0 2-Methylnonane 0.199 0.209 0.136

97.666 5881-17-4 3-Ethyloctane 0.156 0.161 0.107

98.002 5911-04-6 3-Methylnonane 0.355 0.370 0.243

98.558 C10-Isoparaffin1 0.071 0.073 0.048

98.797 I19 0.084 0.086 0.057

99.484 I21 0.174 0.180 0.119

99.713 C10-Isoparaffin2 0.099 0.103 0.068

101.260 I26 0.063 0.066 0.040

101.406 C11-Isoparaffin1 0.061 0.063 0.038

103.87017362-11-3 3-Ethylnonane 0.062 0.063 0.038

106.626 C11-Isoparaffin3 0.183 0.189 0.114

106.934 C11-Isoparaffin4 0.094 0.097 0.058

107.263 C11-Isoparaffin5 0.085 0.088 0.053

123.748 I49 0.020 0.020 0.011

Aromatics 118.374 A5 0.106 0.091 0.063

Mono-Aromatics 43.156 71-42-3 Benzene 0.710 0.617 0.885

66.486 108-88-3 Toluene 8.300 7.312 8.766

82.776 100-41-4 Ethylbenzene 9.943 8.759 9.114

83.880 108-38-3 m-Xylene 0.377 0.334 0.346

84.052 106-42-3 p-Xylene 0.476 0.422 0.436

86.897 95-47-6 o-Xylene 0.341 0.296 0.313

91.144 98-82-8 i-Propylbenzene 0.100 0.089 0.081

94.625 103-65-1 n-Propylbenzene 0.586 0.519 0.474

95.517 620-14-4 1-Methyl-3-ethylbenzene 2.398 2.118 1.941

95.733 622-96-8 1-Methyl-4-ethylbenzene 1.381 1.225 1.118

96.365 108-67-8 1,3,5-Trimethylbenzene 1.504 1.327 1.217

97.421 611-14-3 1-Methyl-2-ethylbenzene 0.893 0.775 0.723

99.127 95-63-6 1,2,4-Trimethylbenzene 4.188 3.652 3.391

100.721 135-98-8 sec-Butylbenzene 0.093 0.082 0.067

101.929 526-73-8 1,2,3-Trimethylbenzene 1.006 0.859 0.815

102.363 535-77-3 1-Methyl-3-i-propylbenzene 0.076 0.067 0.055

102.734 99-87-6 1-Methyl-4-i-propylbenzene 0.055 0.049 0.040

103.744 527-84-4 1-Methyl-2-i-propylbenzene 0.161 0.141 0.117

104.726 141-93-5 1,3-Diethylbenzene 0.130 0.115 0.094

104.963 1074-43-7 1-Methyl-3-n-propylbenzene 0.418 0.371 0.303

105.376 105-05-5 1,4-Diethylbenzene 0.147 0.130 0.106

105.600 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.325 0.282 0.236

105.859 135-01-3 1,2-Diethylbenzene 0.088 0.076 0.064

107.626 874-41-9 1,3-Dimethyl-4-ethylbenzene 0.181 0.157 0.131

C-353
Hydrocarbon Expert V4.0 Fri Apr 11 11:06:22 2008 Page 3

File: C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF 10-Apr-08, 17:29:10

Sample: ODDB-69590 Operator: AAD

Parameter: C:\HPCHEM\HCE40\ODDB-69590

ODDB-69590

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol

Mono-Aromatics 108.189 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.342 0.299 0.248

108.761 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.202 0.173 0.146

109.533 4M-1tC4Benz 0.040 0.034 0.029

109.939 1-Methyl-4-t-butylbenzene 0.066 0.059 0.043

110.112 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.116 0.099 0.084

110.643 95-93-2 1,2,4,5-Tetramethylbenzene 0.062 0.054 0.045

111.188 1-Methyl-1-n-butylbenzene 0.266 0.228 0.175

111.499 1074-92-6 1-t-Butyl-2-methylbenzene 0.374 0.321 0.245

112.992 C11-Aromatic1 0.067 0.058 0.044

113.327 C11-Aromatic2 0.092 0.079 0.061

113.607 C11-Aromatic3 0.157 0.135 0.103

115.513 1-Methyl-2-n-butylbenzene 0.038 0.033 0.025

115.652 100-18-5 1,4-Di-i-propylbenzene 0.105 0.090 0.063

117.363 1t-Butyl-4-ethylbenzene 0.046 0.039 0.027

118.243 1,3-Di-n-propylbenzene 0.053 0.046 0.032

120.531 102-25-0 1,3,5-Triethylbenzene 0.011 0.010 0.007

121.198 877-44-1 1,2,4-Triethylbenzene 0.027 0.023 0.016

122.541 1-Methyl-4-n-pentylbenzene 0.021 0.018 0.013

123.524 1077-16-3 n-Hexylbenzene 0.012 0.010 0.007

124.932 700-12-9 Pentamethylbenzene 0.028 0.021 0.018

Naphthalenes 116.284 119-64-2 1,2,3,4-Tetrahydronaphthalene 0.096 0.076 0.071

116.785 91-20-3 Naphthalene 0.036 0.027 0.027

125.810 91-57-6 2-Methylnaphthalene 0.020 0.015 0.013

126.386 90-12-0 1-Methylnaphthalene 0.013 0.010 0.009

Naphtheno/Olefin 113.130 874-35-1 5-Methylindan 0.121 0.104 0.089

114.011 824-22-6 4-Methylindan 0.191 0.164 0.141

114.347 824-63-5 2-Methylindan 0.185 0.159 0.136

Indenes 103.104 496-11-7 2,3-Dihydroindene 0.336 0.267 0.277

Naphthenes 82.409 N8 0.011 0.011 0.010

87.636 N18 0.045 0.044 0.035

91.741 N26 0.044 0.042 0.034

92.267 N28 0.026 0.025 0.020

93.774 N30 0.011 0.010 0.007

101.646 N39 0.052 0.050 0.033

Mono-Naphthene 25.643 287-92-3 Cyclopentane 0.104 0.106 0.144

38.162 96-37-7 Methylcyclopentane 0.616 0.628 0.712

45.167 110-82-7 Cyclohexane 18.646 18.293 21.560

50.579 2532-58-3 1c,3-Dimethylcyclopentane 0.095 0.097 0.094

51.157 1759-58-6 1t,3-Dimethylcyclopentane 0.069 0.070 0.068

51.768 822-50-4 1t,2-Dimethylcyclopentane 0.037 0.038 0.037

58.576 108-87-2 Methylcyclohexane 0.058 0.057 0.057

58.978 1192-18-3 1c,2-Dimethylcyclopentane 0.013 0.014 0.013

59.535 4516-69-2 1,1,3-Trimethylcyclopentane 0.014 0.014 0.012

C-354
Hydrocarbon Expert V4.0 Fri Apr 11 11:06:22 2008 Page 4

File: C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF 10-Apr-08, 17:29:10

Sample: ODDB-69590 Operator: AAD

Parameter: C:\HPCHEM\HCE40\ODDB-69590

ODDB-69590

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol

Mono-Naphthene 61.384 1640-89-7 Ethylcyclopentane 0.017 0.017 0.017

63.418 4850-28-6 1c,2t,4-Trimethylcyclopentane 0.014 0.014 0.012

73.097 3c-Ethylmethylcyclopentane 0.021 0.021 0.018

73.348 3t-Ethylmethylcyclopentane 0.021 0.021 0.019

73.604 111-66-0 2t-Ethylmethylcyclopentane 0.017 0.017 0.015

74.03116747-50-5 1,1-Methylethylcyclopentane 0.038 0.037 0.033

74.776 2207-03-6 1t,3-Dimethylcyclohexane 0.012 0.012 0.010

75.316 1c,2c,3-Trimethylcyclopentane 0.030 0.029 0.026

79.304 2207-01-4 1c,2-Dimethylcyclohexane 0.037 0.035 0.032

81.028 1678-91-7 Ethylcyclohexane 0.020 0.019 0.017

81.245 1795-27-3 1c,3c,5-Trimethylcyclohexane 0.089 0.088 0.068

82.993 7667-60-9 1c,2t,4t-Trimethylcyclohexane 0.396 0.388 0.306

86.046 1c,2t,4c-Trimethylcyclohexane 0.066 0.065 0.050

90.189 4926-90-3 1,1-Methylethylcyclohexane 0.130 0.123 0.100

91.854 696-29-7 i-Propylcyclohexane 0.066 0.063 0.051

93.526 2040-95-1 n-Butylcyclopentane 0.079 0.077 0.061

103.375 7058-01-7 sec-Butylcyclohexane 0.187 0.175 0.130

115.130 1t-M-2-(4-MP)cyclopentane 0.096 0.092 0.056

Di/Bicyclo-Naphth106.338 493-02-7 t-Decahydronaphthalene 0.083 0.079 0.052

Olefins 9.390 115-11-7 isobutene 0.000 0.000 0.000

35.333 O13 0.058 0.064 0.067

54.904 C7-Olefin2 0.038 0.042 0.038

64.156 O38 0.010 0.010 0.010

64.995 C8-Olefin2 0.016 0.017 0.016

76.451 C9-Olefin1 0.072 0.077 0.063

77.055 C9-Olefin2 0.019 0.020 0.015

87.278 C9-Olefin4 0.226 0.240 0.174

n-Olefins 9.430 106-98-9 Butene-1 0.013 0.017 0.023

10.183 624-64-6 t-Butene-2 0.038 0.048 0.065

10.825 590-18-1 c-Butene-2 0.086 0.106 0.149

15.639 109-67-1 Pentene-1 0.294 0.351 0.408

17.907 646-04-8 t-Pentene-2 0.757 0.892 1.050

18.852 627-20-3 c-Pentene-2 0.441 0.513 0.611

31.253 592-41-6 Hexene-1 0.140 0.158 0.162

34.14913269-52-8 t-Hexene-3 0.203 0.227 0.235

34.609 4050-45-7 t-Hexene-2 0.380 0.426 0.440

36.378 7688-21-3 c-Hexene-2 0.179 0.198 0.207

54.58214686-14-7 t-Heptene-3 0.037 0.041 0.037

55.533 7642-10-6 c-Heptene-3 0.032 0.035 0.032

58.099 6443-92-1 c-Heptene-2 0.021 0.023 0.021

73.78314850-23-8 t-Octene-4 0.028 0.030 0.025

77.622 7642-04-8 c-Octene-2 0.008 0.008 0.007

89.35620237-46-0 c-Nonene-3 0.036 0.040 0.028

91.440 6434-77-1 c-Nonene-2 0.083 0.081 0.064

Iso-Olefins 12.802 563-45-1 3-Methylbutene-1 0.078 0.095 0.108

C-355
Hydrocarbon Expert V4.0 Fri Apr 11 11:06:22 2008 Page 5

File: C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF 10-Apr-08, 17:29:10

Sample: ODDB-69590 Operator: AAD

Parameter: C:\HPCHEM\HCE40\ODDB-69590

ODDB-69590

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol

Iso-Olefins 16.404 563-46-2 2-Methylbutene-1 0.497 0.584 0.690

19.472 513-35-9 2-Methylbutene-2 1.051 1.212 1.459

25.084 691-37-2 4-Methylpentene-1 0.085 0.097 0.098

27.175 691-38-3 4-Methyl-c-pentene-2 0.046 0.052 0.053

27.797 674-76-0 4-Methyl-t-pentene-2 0.146 0.166 0.169

31.033 763-29-1 2-Methylpentene-1 0.182 0.203 0.211

35.080 625-27-4 2-Methylpentene-2 0.277 0.306 0.320

35.465 922-62-3 3-Methyl-c-pentene-2 0.225 0.246 0.260

37.682 3404-73-7 3,3-Dimethylpentene-1 0.234 0.255 0.232

41.934 762-63-0 4,4-Dimethyl-c-pentene-2 0.018 0.019 0.018

44.152 2-Methyl-c-hexene-3 0.042 0.046 0.042

45.604 692-24-0 2-Methyl-t-hexene-3 0.033 0.037 0.033

46.682 7357-93-9 2-Ethyl-3-methylbutene-1 0.038 0.041 0.038

47.002 3769-23-1 4-Methylhexene-1 0.022 0.024 0.022

47.632 3404-55-5 4-Methyl-t/c-hexene-2 0.034 0.037 0.034

54.104 4914-89-0 3-Methyl-c-hexene-3 0.032 0.034 0.032

55.856 2738-19-4 2-Methyl-2-hexene 0.027 0.029 0.027

56.07510574-36-4 3-Methyl-c-hexene-2 0.044 0.047 0.043

56.611 816-79-5 3-Ethylpentene-2 0.020 0.022 0.020

56.835 1,5-DM-Cyclopentene 0.040 0.042 0.040

57.36520710-38-8 3-Methyl-t-hexene-2 0.028 0.030 0.028

75.13019549-89-4 3,3-Dimethylheptene-1 0.015 0.015 0.011

80.13519550-75-6 t-2,2-Dimethylheptene-3 0.017 0.019 0.013

90.546 4984-01-4 3,7-Dimethyloctene-1 0.095 0.104 0.066

100.38819781-18-0 2,3-Dimethyloctene-2 0.092 0.095 0.064

Naphtheno-Olefin 23.926 142-29-0 Cyclopentene 0.191 0.189 0.273

48.455 110-83-8 Cyclohexene 0.076 0.071 0.090

Di-Olefins 17.412 78-79-5 2-Methyl-1,3-Butadiene 0.018 0.020 0.026

18.484 598-25-4 3-Methylbutadiene-1,2 0.031 0.037 0.044

21.064 1574-41-0 1c,3-Pentadiene 0.013 0.014 0.019

38.970 563-79-1 2,3-Dimethyl-2-Butene 0.017 0.018 0.020

42.875 Diolefin 0.020 0.022 0.024

52.940 1541-23-7 1,5-Heptadiene 0.051 0.052 0.054

67.750 C8-Diolefin3 0.054 0.056 0.054

71.864 1002-33-1 1,3-Octadiene 0.022 0.022 0.020

Oxygenates 26.739 1634-04-4 Methyl-t-butylether 0.116 0.120 0.128

Plus

C-356
Hydrocarbon Expert V4.0 Fri Apr 11 11:06:22 2008 Page 1

File: C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF 10-Apr-08, 17:29:10

Sample: ODDB-69590 Operator: AAD

Parameter: C:\HPCHEM\HCE40\ODDB-69590

ODDB-69590

Sample Chromatogram

C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF

2 22.50 20.00 17.50 15.00 12.50 10.00 7.50 5.00 2.50

i-Butane

Butene-1 isobutene

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

3-Methylbutadiene-1,2 c-Pentene-2

2-Methylbutene-2

1c,3-Pentadiene

2,2-Dimethylbutane

Cyclopentene

4-Methylpentene-1

C-357
Hydrocarbon Expert V4.0 Fri Apr 11 11:06:22 2008 Page 2

File: C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF 10-Apr-08, 17:29:10

Sample: ODDB-69590 Operator: AAD

Parameter: C:\HPCHEM\HCE40\ODDB-69590

ODDB-69590

Sample Chromatogram

C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF

5 47.50 45.00 42.50 40.00 37.50 35.00 32.50 30.00 27.50

Cyclopentane

2,3-Dimethylbutane

Methyl-t-butylether

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

n-Hexane

t-Hexene-3

t-Hexene-2

2-Methylpentene-2 O133-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,3-Dimethyl-2-Butene

2,4-Dimethylpentane

2,2,3-Trimethylbutane

4,4-Dimethyl-c-pentene-2

DiolefinBenzene

2-Methyl-c-hexene-3

Cyclohexane

2-Methyl-t-hexene-3

2-Ethyl-3-methylbutene-1

4-Methylhexene-1

4-Methyl-t/c-hexene-2 2-Methylhexane

Cyclohexene

3-Methylhexane

C-358
Hydrocarbon Expert V4.0 Fri Apr 11 11:06:22 2008 Page 3

File: C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF 10-Apr-08, 17:29:10

Sample: ODDB-69590 Operator: AAD

Parameter: C:\HPCHEM\HCE40\ODDB-69590

ODDB-69590

Sample Chromatogram

C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF

7 72.50 70.00 67.50 65.00 62.50 60.00 57.50 55.00 52.50

1c,3-Dimethylcyclopentane

1t,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane

2,2,4-Trimethylpentane

1,5-Heptadiene

3-Methyl-c-hexene-3

t-Heptene-3

C7-Olefin2

n-Heptane c-Heptene-3

2-Methyl-2-hexene 3-Methyl-c-hexene-2

3-Ethylpentene-2 1,5-DM-Cyclopentene

3-Methyl-t-hexene-2

c-Heptene-2

Methylcyclohexane

1c,2-Dimethylcyclopentane

1,1,3-Trimethylcyclopentane

Ethylcyclopentane

2,2,3-Trimethylpentane 2,5-Dimethylhexane

2,4-Dimethylhexane

1c,2t,4-Trimethylcyclopentane

3,3-Dimethylhexane O38

C8-Olefin2

2,3,4-Trimethylpentane

Toluene

C8-Diolefin3

2,3-Dimethylhexane

2-Methylheptane 4-Methylheptane

3-Methylheptane

1,3-Octadiene

2,2,5-Trimethylhexane 3c-Ethylmethylcyclopentane 3t-Ethylmethylcyclopentane 2t-Ethylmethylcyclopentane t-Octene-4 1,1-Methylethylcyclopentane

2,2,4-Trimethylhexane

1t,3-Dimethylcyclohexane

C-359
Hydrocarbon Expert V4.0 Fri Apr 11 11:06:22 2008 Page 4

File: C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF 10-Apr-08, 17:29:10

Sample: ODDB-69590 Operator: AAD

Parameter: C:\HPCHEM\HCE40\ODDB-69590

ODDB-69590

Sample Chromatogram

C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF

1 97.50 95.00 92.50 90.00 87.50 85.00 82.50 80.00 77.50

3,3-Dimethylheptene-1 1c,2c,3-Trimethylcyclopentane n-Octane

C9-Olefin1

C9-Olefin2

c-Octene-2

2,3,4-Trimethylhexane

1c,2-Dimethylcyclohexane

2,2-Dimethylheptane t-2,2-Dimethylheptene-3 2,2,3-Trimethylhexane

4,4-Dimethylheptane

Ethylcyclohexane 1c,3c,5-Trimethylcyclohexane 3,3-Dimethylheptane

2-Methyl-4-ethylhexane

N8

Ethylbenzene 1c,2t,4t-Trimethylcyclohexane

m-Xylene p-Xylene

3,3-Diethylpentane

4-Methyloctane 2-Methyloctane

1c,2t,4c-Trimethylcyclohexane 3-Methyloctane

o-Xylene

C9-Olefin4

N18

C9-Isoparaffin1

c-Nonene-3

n-Nonane

1,1-Methylethylcyclohexane

3,7-Dimethyloctene-1

i-Propylbenzene c-Nonene-2 N26 i-Propylcyclohexane 2,2-Dimethyloctane N28 2,4-Dimethyloctane

2,6-Dimethyloctane 2,5-Dimethyloctane

I12 n-Butylcyclopentane N303,3-Dimethyloctane I14

n-Propylbenzene 3-Methyl-5-ethylheptane

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

5-Methylnonane 4-Methylnonane 2-Methylnonane 1-Methyl-2-ethylbenzene 3-Ethyloctane 3-Methylnonane

C10-Isoparaffin1 I19

1,2,4-Trimethylbenzene I21 C10-Isoparaffin2

C-360
Hydrocarbon Expert V4.0 Fri Apr 11 11:06:22 2008 Page 5

File: C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF 10-Apr-08, 17:29:10

Sample: ODDB-69590 Operator: AAD

Parameter: C:\HPCHEM\HCE40\ODDB-69590

ODDB-69590

Sample Chromatogram

C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF

1 122.50 120.00 117.50 115.00 112.50 110.00 107.50 105.00 102.50

2,3-Dimethyloctene-2 sec-Butylbenzene n-Decane

C11-Isoparaffin1 I26

N39 1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene

1-Methyl-4-i-propylbenzene 2,3-Dihydroindene sec-Butylcyclohexane 1-Methyl-2-i-propylbenzene 3-Ethylnonane

1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene

1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

t-Decahydronaphthalene C11-Isoparaffin3 C11-Isoparaffin4

C11-Isoparaffin5 1,3-Dimethyl-4-ethylbenzene

1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

4M-1tC4Benz

1-Methyl-4-t-butylbenzene 1,2-Dimethyl-3-ethylbenzene n-Undecane 1,2,4,5-Tetramethylbenzene

1-Methyl-1-n-butylbenzene 1-t-Butyl-2-methylbenzene

C11-Aromatic1 5-Methylindan C11-Aromatic2 C11-Aromatic3

4-Methylindan 2-Methylindan

1t-M-2-(4-MP)cyclopentane 1-Methyl-2-n-butylbenzene 1,4-Di-i-propylbenzene

1,2,3,4-Tetrahydronaphthalene

Naphthalene

1t-Butyl-4-ethylbenzene

A51,3-Di-n-propylbenzene

n-Dodecane

1,3,5-Triethylbenzene

1,2,4-Triethylbenzene

1-Methyl-4-n-pentylbenzene

n-Hexylbenzene I49

Pentamethylbenzene

C-361
Hydrocarbon Expert V4.0 Fri Apr 11 11:06:22 2008 Page 6

File: C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF 10-Apr-08, 17:29:10

Sample: ODDB-69590 Operator: AAD

Parameter: C:\HPCHEM\HCE40\ODDB-69590

ODDB-69590

Sample Chromatogram

C:\HPCHEM\2\DATA\4-10-08\004F0401.D\004F0401_ADC1_B.CDF

1 147.50 145.00 142.50 140.00 137.50 135.00 132.50 130.00 127.50

2-Methylnaphthalene

1-Methylnaphthalene

n-Tridecane

C-362
Hydrocarbon Expert V4.0 Tue Jul 01 17:21:08 2008 Page 1

File: C:\HPCHEM\2\DATA\6-29-08\002F0201.D\002F0201_ADC1_B.CDF 29-Jun-08, 15:09:16

Sample: ODDB-71719 Operator: RAS

Parameter: C:\HPCHEM\HCE40\ODDB-71719

ODDB-71719 R.

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 10.240 12.177 11.986

I-Paraffins 20.915 22.900 17.480

Aromatics 31.538 27.621 26.882

Mono-Aromatics 31.231 27.379 26.646

Naphthalenes 0.015 0.011 0.010

Naphtheno/Olefino-Benz 0.009 0.008 0.006

Indenes 0.283 0.223 0.219

Naphthenes 17.329 16.922 17.717

Mono-Naphthenes 17.222 16.820 17.650

Di/Bicyclo-Naphthenes 0.078 0.075 0.047

Olefins 5.647 6.250 5.779

n-Olefins 4.777 5.347 5.155

Iso-Olefins 0.594 0.616 0.401

Naphtheno-Olefins 0.000 0.000 0.000

Di-Olefins 0.097 0.099 0.085

Oxygenates 7.659 7.383 15.209

Plus 0.000 0.000 0.000

C-363
Hydrocarbon Expert V4.0 Tue Jul 01 17:21:08 2008 Page 1

File: C:\HPCHEM\2\DATA\6-29-08\002F0201.D\002F0201_ADC1_B.CDF 29-Jun-08, 15:09:16

Sample: ODDB-71719 Operator: RAS

Parameter: C:\HPCHEM\HCE40\ODDB-71719

ODDB-71719 R.

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C2 7.659 7.383 15.209

C4 2.846 3.741 4.479

C5 1.207 1.467 1.532

C6 28.262 29.900 30.538

C7 13.297 12.911 12.764

C8 16.110 15.267 13.559

C9 13.687 12.450 10.262

C10 9.738 9.629 6.402

C11 0.511 0.494 0.302

C12 0.006 0.006 0.003

C13 0.005 0.005 0.002

C-364
Hydrocarbon Expert V4.0 Tue Jul 01 17:21:08 2008 Page 1

File: C:\HPCHEM\2\DATA\6-29-08\002F0201.D\002F0201_ADC1_B.CDF 29-Jun-08, 15:09:16

Sample: ODDB-71719 Operator: RAS

Parameter: C:\HPCHEM\HCE40\ODDB-71719

ODDB-71719 R.

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C4 2.807 3.688 4.418

C5 0.410 0.498 0.520

C6 5.403 6.232 5.735

C7 0.597 0.664 0.545

C8 0.607 0.657 0.486

C9 0.238 0.253 0.170

C10 0.152 0.158 0.098

C11 0.016 0.016 0.009

C12 0.006 0.006 0.003

C13 0.005 0.005 0.002

I-Paraffins C4 0.039 0.053 0.061

C5 0.749 0.920 0.950

C6 4.172 4.814 4.429

C7 3.836 4.308 3.502

C8 4.269 4.632 3.419

C9 1.389 1.472 0.991

C10 5.977 6.233 3.843

C11 0.485 0.470 0.287

Mono-Aromatics C6 0.722 0.625 0.846

C7 7.495 6.575 7.441

C8 10.457 9.206 9.011

C9 9.937 8.670 7.563

C10 2.614 2.298 1.781

C11 0.006 0.005 0.003

Naphthalenes C10 0.011 0.008 0.008

C11 0.004 0.003 0.003

Naphtheno/Olefino-BenzsC10 0.009 0.008 0.006

Indenes C10 0.283 0.223 0.219

Naphthenes C9 0.028 0.028 0.021

Mono-Naphthenes C5 0.048 0.048 0.062

C6 13.284 12.978 14.440

C7 1.346 1.339 1.254

C8 0.615 0.607 0.501

C9 1.850 1.772 1.341

C10 0.079 0.075 0.052

Di/Bicyclo-Naphthenes C10 0.078 0.075 0.047

C-365
Hydrocarbon Expert V4.0 Tue Jul 01 17:21:08 2008 Page 2

File: C:\HPCHEM\2\DATA\6-29-08\002F0201.D\002F0201_ADC1_B.CDF 29-Jun-08, 15:09:16

Sample: ODDB-71719 Operator: RAS

Parameter: C:\HPCHEM\HCE40\ODDB-71719

ODDB-71719 R.

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Di/Bicyclo-Naphthenes

Olefins C8 0.054 0.056 0.048

C9 0.125 0.132 0.090

n-Olefins C6 4.669 5.238 5.075

C7 0.004 0.005 0.004

C8 0.011 0.012 0.009

C9 0.082 0.082 0.060

C10 0.010 0.011 0.007

Iso-Olefins C6 0.012 0.013 0.013

C7 0.019 0.021 0.018

C9 0.037 0.042 0.027

C10 0.525 0.541 0.343

Di-Olefins C8 0.097 0.099 0.085

Oxygenates C2 7.659 7.383 15.209

C-366
Hydrocarbon Expert V4.0 Tue Jul 01 17:21:08 2008 Page 1

File: C:\HPCHEM\2\DATA\6-29-08\002F0201.D\002F0201_ADC1_B.CDF 29-Jun-08, 15:09:16

Sample: ODDB-71719 Operator: RAS

Parameter: C:\HPCHEM\HCE40\ODDB-71719

ODDB-71719 R.

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol

1 8.732 75-28-5 I4 i-Butane 0.039 0.053 0.061

2 9.790 106-97-8 P4 n-Butane 2.807 3.688 4.418

3 10.322 463-82-1 I5 2,2-Dimethylpropane 0.011 0.014 0.014

4 12.696 64-17-5 X2 Ethanol 7.659 7.383 15.209

5 14.142 78-78-4 I5 i-Pentane 0.738 0.906 0.936

6 16.834 109-66-0 P5 n-Pentane 0.410 0.498 0.520

7 21.364 75-83-2 I6 2,2-Dimethylbutane 0.056 0.065 0.059

8 25.538 287-92-3 M5 Cyclopentane 0.048 0.048 0.062

9 26.218 79-29-8 I6 2,3-Dimethylbutane 0.457 0.526 0.485

10 27.257 107-83-5 I6 2-Methylpentane 1.720 2.003 1.826

11 29.772 96-14-0 I6 3-Methylpentane 1.939 2.220 2.058

12 31.175 592-41-6 K6 Hexene-1 4.669 5.238 5.075

13 33.440 110-54-3 P6 n-Hexane 5.403 6.232 5.735

15 35.315 922-62-3 C6 3-Methyl-c-pentene-2 0.012 0.013 0.013

16 37.505 3404-73-7 C7 3,3-Dimethylpentene-1 0.008 0.009 0.008

17 38.004 590-35-2 I7 2,2-Dimethylpentane 1.608 1.816 1.468

18 39.553 108-08-7 I7 2,4-Dimethylpentane 0.495 0.559 0.452

19 40.073 464-06-2 I7 2,2,3-Trimethylbutane 0.083 0.092 0.076

20 42.853 71-42-3 Q6 Benzene 0.722 0.625 0.846

21 44.937 110-82-7 M6 Cyclohexane 13.284 12.978 14.440

22 45.344 692-24-0 C7 2-Methyl-t-hexene-3 0.006 0.007 0.006

23 47.828 591-76-4 I7 2-Methylhexane 1.120 1.256 1.023

24 49.613 589-34-4 I7 3-Methylhexane 0.529 0.585 0.483

25 50.414 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.099 0.101 0.092

26 50.987 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.088 0.090 0.082

27 51.592 822-50-4 M7 1t,2-Dimethylcyclopentane 0.130 0.131 0.121

29 52.217 540-84-1 I8 2,2,4-Trimethylpentane 1.830 2.012 1.466

30 55.114 142-82-5 P7 n-Heptane 0.597 0.664 0.545

31 55.80410574-36-4 C7 3-Methyl-c-hexene-2 0.005 0.005 0.004

34 57.895 6443-92-1 K7 c-Heptene-2 0.004 0.005 0.004

35 58.417 108-87-2 M7 Methylcyclohexane 1.022 1.010 0.952

36 58.815 1192-18-3 M7 1c,2-Dimethylcyclopentane 0.007 0.007 0.006

37 59.374 4516-69-2 M8 1,1,3-Trimethylcyclopentane 0.037 0.038 0.030

38 59.822 590-73-8 I8 2,2-Dimethylhexane 0.033 0.036 0.026

41 61.834 564-02-3 I8 2,2,3-Trimethylpentane 0.115 0.122 0.092

42 62.121 592-13-2 I8 2,5-Dimethylhexane 0.283 0.311 0.227

43 62.444 589-43-5 I8 2,4-Dimethylhexane 0.254 0.276 0.203

45 63.238 4850-28-6 M8 1c,2t,4-Trimethylcyclopentane 0.037 0.037 0.030

46 63.677 563-16-6 I8 3,3-Dimethylhexane 0.025 0.026 0.020

47 64.820 O8 C8-Olefin2 0.031 0.033 0.029

48 65.504 565-75-3 I8 2,3,4-Trimethylpentane 0.717 0.758 0.574

49 66.212 108-88-3 Q7 Toluene 7.495 6.575 7.441

50 67.285 E8 C8-Diolefin3 0.015 0.016 0.014

51 67.614 E8 C8-Diolefin4 0.030 0.031 0.028

C-367
Hydrocarbon Expert V4.0 Tue Jul 01 17:21:08 2008 Page 2

File: C:\HPCHEM\2\DATA\6-29-08\002F0201.D\002F0201_ADC1_B.CDF 29-Jun-08, 15:09:16

Sample: ODDB-71719 Operator: RAS

Parameter: C:\HPCHEM\HCE40\ODDB-71719

ODDB-71719 R.

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol

52 67.976 609-26-7 I8 2-Methyl-3-ethylpentane 0.239 0.255 0.191

53 68.289 4259-00-1 M8 1,1,2-Trimethylcyclopentane 0.010 0.010 0.008

54 68.507 O8 C8-Olefin3 0.023 0.024 0.018

55 69.334 592-27-8 I8 2-Methylheptane 0.281 0.306 0.225

56 69.581 589-53-7 I8 4-Methylheptane 0.116 0.125 0.093

58 69.935 583-48-2 I8 3,4-Dimethylhexane 0.012 0.013 0.010

59 70.438 2207-04-7 M8 1t,4-Dimethylcyclohexane 0.224 0.224 0.183

60 70.693 589-81-1 I8 3-Methylheptane 0.227 0.245 0.182

61 70.807 619-99-8 I8 3-Ethylhexane 0.137 0.146 0.110

62 71.709 1002-33-1 E8 1,3-Octadiene 0.052 0.051 0.043

65 72.652 3522-94-9 I9 2,2,5-Trimethylhexane 0.303 0.326 0.216

66 72.950 M8 3c-Ethylmethylcyclopentane 0.018 0.018 0.015

67 73.175 M8 3t-Ethylmethylcyclopentane 0.023 0.023 0.019

68 73.439 111-66-0 M8 2t-Ethylmethylcyclopentane 0.009 0.009 0.007

69 73.62914850-23-8 K8 t-Octene-4 0.006 0.006 0.005

70 73.86216747-50-5 M8 1,1-Methylethylcyclopentane 0.107 0.104 0.087

71 74.10016747-26-5 I9 2,2,4-Trimethylhexane 0.005 0.006 0.004

72 74.85914919-01-8 K8 t-Octene-3 0.005 0.005 0.004

73 75.159 M8 1c,2c,3-Trimethylcyclopentane 0.070 0.068 0.057

74 75.419 111-65-9 P8 n-Octane 0.607 0.657 0.486

76 76.425 3875-51-2 M8 i-Propylcyclopentane 0.005 0.005 0.004

78 77.927 921-47-1 I9 2,3,4-Trimethylhexane 0.053 0.054 0.038

81 79.158 2207-01-4 M8 1c,2-Dimethylcyclohexane 0.045 0.043 0.036

83 79.713 1071-26-7 I9 2,2-Dimethylheptane 0.181 0.194 0.129

84 79.97219550-75-6 C9 t-2,2-Dimethylheptene-3 0.019 0.021 0.014

85 80.15816747-25-4 I9 2,2,3-Trimethylhexane 0.123 0.131 0.088

86 80.535 1068-19-5 I9 4,4-Dimethylheptane 0.091 0.097 0.065

87 80.889 1678-91-7 M8 Ethylcyclohexane 0.031 0.030 0.025

88 81.110 1795-27-3 M9 1c,3c,5-Trimethylcyclohexane 0.112 0.111 0.081

89 81.286 4032-86-4 I9 3,3-Dimethylheptane 0.042 0.044 0.030

91 81.784 3074-75-7 I9 2-Methyl-4-ethylhexane 0.017 0.018 0.012

93 82.441 100-41-4 Q8 Ethylbenzene 1.981 1.738 1.707

95 82.790 7667-60-9 M9 1c,2t,4t-Trimethylcyclohexane 0.061 0.059 0.044

96 83.043 4588-18-5 C9 2-Methyloctene-1 0.014 0.015 0.010

99 83.797 108-38-3 Q8 m-Xylene 5.953 5.239 5.130

100 83.928 106-42-3 Q8 p-Xylene 2.523 2.229 2.174

101 84.247 3074-71-3 I9 2,3-Dimethylheptane 0.032 0.034 0.023

103 84.672 1067-20-5 I9 3,3-Diethylpentane 0.062 0.062 0.044

104 85.094 2216-34-4 I9 4-Methyloctane 0.110 0.116 0.078

105 85.235 3221-61-2 I9 2-Methyloctane 0.142 0.151 0.101

106 85.547 O9 C9-Olefin3 0.038 0.040 0.027

107 85.924 M9 1c,2t,4c-Trimethylcyclohexane 0.040 0.040 0.029

108 86.101 2216-33-3 I9 3-Methyloctane 0.139 0.146 0.099

111 86.698 7094-26-0 M9 1,1,2-Trimethylcyclohexane 1.013 0.963 0.734

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Hydrocarbon Expert V4.0 Tue Jul 01 17:21:08 2008 Page 3

File: C:\HPCHEM\2\DATA\6-29-08\002F0201.D\002F0201_ADC1_B.CDF 29-Jun-08, 15:09:16

Sample: ODDB-71719 Operator: RAS

Parameter: C:\HPCHEM\HCE40\ODDB-71719

ODDB-71719 R.

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol

113 87.163 O9 C9-Olefin4 0.087 0.092 0.063

114 87.516 N9 N18 0.021 0.020 0.015

116 87.997 I9 C9-Isoparaffin1 0.089 0.092 0.063

118 88.495 3788-32-7 M9 i-Butylcyclopentane 0.012 0.011 0.008

120 88.98320063-92-8 C9 t-7-Methyloctene-3 0.005 0.005 0.003

121 89.23020237-46-0 K9 c-Nonene-3 0.015 0.016 0.011

124 89.654 111-84-2 P9 n-Nonane 0.238 0.253 0.170

125 90.103 6434-78-2 K9 t-Nonene-2 0.048 0.047 0.035

126 90.402 4984-01-4 C10 3,7-Dimethyloctene-1 0.012 0.013 0.008

128 90.925 98-82-8 Q9 i-Propylbenzene 0.050 0.044 0.038

130 91.256 6434-77-1 K9 c-Nonene-2 0.020 0.019 0.014

132 91.743 696-29-7 M9 i-Propylcyclohexane 0.263 0.249 0.191

133 91.96315869-87-1 I10 2,2-Dimethyloctane 0.083 0.088 0.054

134 92.125 N9 N28 0.007 0.007 0.005

135 92.309 4032-94-4 I10 2,4-Dimethyloctane 0.046 0.048 0.029

136 92.637 2051-30-1 I10 2,6-Dimethyloctane 0.064 0.067 0.041

137 92.81015869-89-3 I10 2,5-Dimethyloctane 0.097 0.101 0.063

139 93.402 2040-95-1 M9 n-Butylcyclopentane 0.350 0.339 0.253

140 93.851 4110-44-5 I10 3,3-Dimethyloctane 0.121 0.125 0.078

142 94.431 103-65-1 Q9 n-Propylbenzene 0.480 0.423 0.365

143 94.70352896-90-9 I10 3-Methyl-5-ethylheptane 0.014 0.014 0.009

146 95.347 620-14-4 Q9 1-Methyl-3-ethylbenzene 1.983 1.745 1.509

147 95.564 622-96-8 Q9 1-Methyl-4-ethylbenzene 0.972 0.859 0.740

150 96.203 108-67-8 Q9 1,3,5-Trimethylbenzene 1.271 1.117 0.967

154 97.160 871-83-0 I10 2-Methylnonane 4.358 4.563 2.802

155 97.254 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.637 0.550 0.485

157 97.902 5911-04-6 I10 3-Methylnonane 0.046 0.047 0.029

161 98.477 I10 C10-Isoparaffin1 0.786 0.808 0.506

162 98.712 I10 I19 0.361 0.371 0.232

163 98.990 95-63-6 Q9 1,2,4-Trimethylbenzene 3.751 3.257 2.855

168 99.833 872-05-9 K10 Decene-1 0.010 0.011 0.007

169 100.156 M10 1t-Methyl-2-n-propylcyclohexanR 0.040 0.038 0.026

170 100.29619781-18-0 C10 2,3-Dimethyloctene-2 0.513 0.528 0.335

171 100.526 135-98-8 Q10 sec-Butylbenzene 0.226 0.199 0.154

173 100.823 124-18-5 P10 n-Decane 0.152 0.158 0.098

175 101.284 I11 C11-Isoparaffin1 0.047 0.049 0.028

177 101.771 526-73-8 Q9 1,2,3-Trimethylbenzene 0.793 0.675 0.604

179 102.177 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.070 0.062 0.048

181 102.560 99-87-6 Q10 1-Methyl-4-i-propylbenzene 0.312 0.276 0.212

182 102.915 496-11-7 J10 2,3-Dihydroindene 0.283 0.223 0.219

184 103.275 7058-01-7 M10 sec-Butylcyclohexane 0.039 0.036 0.025

190 104.390 I11 C11-Isoparaffin2 0.370 0.352 0.220

191 104.537 141-93-5 Q10 1,3-Diethylbenzene 0.095 0.083 0.065

192 104.866 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 1.097 0.969 0.747

C-369
Hydrocarbon Expert V4.0 Tue Jul 01 17:21:08 2008 Page 4

File: C:\HPCHEM\2\DATA\6-29-08\002F0201.D\002F0201_ADC1_B.CDF 29-Jun-08, 15:09:16

Sample: ODDB-71719 Operator: RAS

Parameter: C:\HPCHEM\HCE40\ODDB-71719

ODDB-71719 R.

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol

194 105.161 105-05-5 Q10 1,4-Diethylbenzene 0.261 0.230 0.178

195 105.441 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.114 0.098 0.078

196 105.719 135-01-3 Q10 1,2-Diethylbenzene 0.078 0.068 0.053

198 106.219 493-02-7 D10 t-Decahydronaphthalene 0.078 0.075 0.047

199 106.316 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.018 0.015 0.012

200 106.508 I11 C11-Isoparaffin3 0.067 0.069 0.039

204 107.264 1758-88-9 Q10 1,4,Dimethyl-2-ethylbenzene 0.018 0.016 0.013

205 107.419 874-41-9 Q10 1,3-Dimethyl-4-ethylbenzene 0.177 0.153 0.120

207 107.987 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.029 0.025 0.020

209 108.652 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.098 0.083 0.067

213 109.649 Q11 1-Methyl-4-t-butylbenzene 0.006 0.005 0.003

214 109.835 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.014 0.012 0.010

215 110.337 1120-21-4 P11 n-Undecane 0.016 0.016 0.009

216 110.486 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.007 0.006 0.005

219 112.903 874-35-1 H10 5-Methylindan 0.009 0.008 0.006

221 116.685 91-20-3 G10 Naphthalene 0.011 0.008 0.008

223 118.896 112-40-3 P12 n-Dodecane 0.006 0.006 0.003

224 126.247 90-12-0 G11 1-Methylnaphthalene 0.004 0.003 0.003

225 126.686 629-50-5 P13 n-Tridecane 0.005 0.005 0.002

C-370
Hydrocarbon Expert V4.0 Tue Jul 01 17:21:08 2008 Page 1

File: C:\HPCHEM\2\DATA\6-29-08\002F0201.D\002F0201_ADC1_B.CDF 29-Jun-08, 15:09:16

Sample: ODDB-71719 Operator: RAS

Parameter: C:\HPCHEM\HCE40\ODDB-71719

ODDB-71719 R.

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol

Paraffin 9.790 106-97-8 n-Butane 2.807 3.688 4.418

16.834 109-66-0 n-Pentane 0.410 0.498 0.520

33.440 110-54-3 n-Hexane 5.403 6.232 5.735

55.114 142-82-5 n-Heptane 0.597 0.664 0.545

75.419 111-65-9 n-Octane 0.607 0.657 0.486

89.654 111-84-2 n-Nonane 0.238 0.253 0.170

100.823 124-18-5 n-Decane 0.152 0.158 0.098

110.337 1120-21-4 n-Undecane 0.016 0.016 0.009

118.896 112-40-3 n-Dodecane 0.006 0.006 0.003

126.686 629-50-5 n-Tridecane 0.005 0.005 0.002

I-Paraffins 8.732 75-28-5 i-Butane 0.039 0.053 0.061

10.322 463-82-1 2,2-Dimethylpropane 0.011 0.014 0.014

14.142 78-78-4 i-Pentane 0.738 0.906 0.936

21.364 75-83-2 2,2-Dimethylbutane 0.056 0.065 0.059

26.218 79-29-8 2,3-Dimethylbutane 0.457 0.526 0.485

27.257 107-83-5 2-Methylpentane 1.720 2.003 1.826

29.772 96-14-0 3-Methylpentane 1.939 2.220 2.058

38.004 590-35-2 2,2-Dimethylpentane 1.608 1.816 1.468

39.553 108-08-7 2,4-Dimethylpentane 0.495 0.559 0.452

40.073 464-06-2 2,2,3-Trimethylbutane 0.083 0.092 0.076

47.828 591-76-4 2-Methylhexane 1.120 1.256 1.023

49.613 589-34-4 3-Methylhexane 0.529 0.585 0.483

52.217 540-84-1 2,2,4-Trimethylpentane 1.830 2.012 1.466

59.822 590-73-8 2,2-Dimethylhexane 0.033 0.036 0.026

61.834 564-02-3 2,2,3-Trimethylpentane 0.115 0.122 0.092

62.121 592-13-2 2,5-Dimethylhexane 0.283 0.311 0.227

62.444 589-43-5 2,4-Dimethylhexane 0.254 0.276 0.203

63.677 563-16-6 3,3-Dimethylhexane 0.025 0.026 0.020

65.504 565-75-3 2,3,4-Trimethylpentane 0.717 0.758 0.574

67.976 609-26-7 2-Methyl-3-ethylpentane 0.239 0.255 0.191

69.334 592-27-8 2-Methylheptane 0.281 0.306 0.225

69.581 589-53-7 4-Methylheptane 0.116 0.125 0.093

69.935 583-48-2 3,4-Dimethylhexane 0.012 0.013 0.010

70.693 589-81-1 3-Methylheptane 0.227 0.245 0.182

70.807 619-99-8 3-Ethylhexane 0.137 0.146 0.110

72.652 3522-94-9 2,2,5-Trimethylhexane 0.303 0.326 0.216

74.10016747-26-5 2,2,4-Trimethylhexane 0.005 0.006 0.004

77.927 921-47-1 2,3,4-Trimethylhexane 0.053 0.054 0.038

79.713 1071-26-7 2,2-Dimethylheptane 0.181 0.194 0.129

80.15816747-25-4 2,2,3-Trimethylhexane 0.123 0.131 0.088

80.535 1068-19-5 4,4-Dimethylheptane 0.091 0.097 0.065

81.286 4032-86-4 3,3-Dimethylheptane 0.042 0.044 0.030

81.784 3074-75-7 2-Methyl-4-ethylhexane 0.017 0.018 0.012

84.247 3074-71-3 2,3-Dimethylheptane 0.032 0.034 0.023

84.672 1067-20-5 3,3-Diethylpentane 0.062 0.062 0.044

85.094 2216-34-4 4-Methyloctane 0.110 0.116 0.078

85.235 3221-61-2 2-Methyloctane 0.142 0.151 0.101

C-371
Hydrocarbon Expert V4.0 Tue Jul 01 17:21:08 2008 Page 2

File: C:\HPCHEM\2\DATA\6-29-08\002F0201.D\002F0201_ADC1_B.CDF 29-Jun-08, 15:09:16

Sample: ODDB-71719 Operator: RAS

Parameter: C:\HPCHEM\HCE40\ODDB-71719

ODDB-71719 R.

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol

I-Paraffins 86.101 2216-33-3 3-Methyloctane 0.139 0.146 0.099

87.997 C9-Isoparaffin1 0.089 0.092 0.063

91.96315869-87-1 2,2-Dimethyloctane 0.083 0.088 0.054

92.309 4032-94-4 2,4-Dimethyloctane 0.046 0.048 0.029

92.637 2051-30-1 2,6-Dimethyloctane 0.064 0.067 0.041

92.81015869-89-3 2,5-Dimethyloctane 0.097 0.101 0.063

93.851 4110-44-5 3,3-Dimethyloctane 0.121 0.125 0.078

94.70352896-90-9 3-Methyl-5-ethylheptane 0.014 0.014 0.009

97.160 871-83-0 2-Methylnonane 4.358 4.563 2.802

97.902 5911-04-6 3-Methylnonane 0.046 0.047 0.029

98.477 C10-Isoparaffin1 0.786 0.808 0.506

98.712 I19 0.361 0.371 0.232

101.284 C11-Isoparaffin1 0.047 0.049 0.028

104.390 C11-Isoparaffin2 0.370 0.352 0.220

106.508 C11-Isoparaffin3 0.067 0.069 0.039

Aromatics

Mono-Aromatics 42.853 71-42-3 Benzene 0.722 0.625 0.846

66.212 108-88-3 Toluene 7.495 6.575 7.441

82.441 100-41-4 Ethylbenzene 1.981 1.738 1.707

83.797 108-38-3 m-Xylene 5.953 5.239 5.130

83.928 106-42-3 p-Xylene 2.523 2.229 2.174

90.925 98-82-8 i-Propylbenzene 0.050 0.044 0.038

94.431 103-65-1 n-Propylbenzene 0.480 0.423 0.365

95.347 620-14-4 1-Methyl-3-ethylbenzene 1.983 1.745 1.509

95.564 622-96-8 1-Methyl-4-ethylbenzene 0.972 0.859 0.740

96.203 108-67-8 1,3,5-Trimethylbenzene 1.271 1.117 0.967

97.254 611-14-3 1-Methyl-2-ethylbenzene 0.637 0.550 0.485

98.990 95-63-6 1,2,4-Trimethylbenzene 3.751 3.257 2.855

100.526 135-98-8 sec-Butylbenzene 0.226 0.199 0.154

101.771 526-73-8 1,2,3-Trimethylbenzene 0.793 0.675 0.604

102.177 535-77-3 1-Methyl-3-i-propylbenzene 0.070 0.062 0.048

102.560 99-87-6 1-Methyl-4-i-propylbenzene 0.312 0.276 0.212

104.537 141-93-5 1,3-Diethylbenzene 0.095 0.083 0.065

104.866 1074-43-7 1-Methyl-3-n-propylbenzene 1.097 0.969 0.747

105.161 105-05-5 1,4-Diethylbenzene 0.261 0.230 0.178

105.441 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.114 0.098 0.078

105.719 135-01-3 1,2-Diethylbenzene 0.078 0.068 0.053

106.316 1074-17-5 1-Methyl-2-n-propylbenzene 0.018 0.015 0.012

107.264 1758-88-9 1,4,Dimethyl-2-ethylbenzene 0.018 0.016 0.013

107.419 874-41-9 1,3-Dimethyl-4-ethylbenzene 0.177 0.153 0.120

107.987 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.029 0.025 0.020

108.652 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.098 0.083 0.067

109.649 1-Methyl-4-t-butylbenzene 0.006 0.005 0.003

109.835 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.014 0.012 0.010

110.486 527-53-7 1,2,3,5-Tetramethylbenzene 0.007 0.006 0.005

Naphthalenes 116.685 91-20-3 Naphthalene 0.011 0.008 0.008

C-372
Hydrocarbon Expert V4.0 Tue Jul 01 17:21:08 2008 Page 3

File: C:\HPCHEM\2\DATA\6-29-08\002F0201.D\002F0201_ADC1_B.CDF 29-Jun-08, 15:09:16

Sample: ODDB-71719 Operator: RAS

Parameter: C:\HPCHEM\HCE40\ODDB-71719

ODDB-71719 R.

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol

Naphthalenes 126.247 90-12-0 1-Methylnaphthalene 0.004 0.003 0.003

Naphtheno/Olefin 112.903 874-35-1 5-Methylindan 0.009 0.008 0.006

Indenes 102.915 496-11-7 2,3-Dihydroindene 0.283 0.223 0.219

Naphthenes 87.516 N18 0.021 0.020 0.015

92.125 N28 0.007 0.007 0.005

Mono-Naphthene 25.538 287-92-3 Cyclopentane 0.048 0.048 0.062

44.937 110-82-7 Cyclohexane 13.284 12.978 14.440

50.414 2532-58-3 1c,3-Dimethylcyclopentane 0.099 0.101 0.092

50.987 1759-58-6 1t,3-Dimethylcyclopentane 0.088 0.090 0.082

51.592 822-50-4 1t,2-Dimethylcyclopentane 0.130 0.131 0.121

58.417 108-87-2 Methylcyclohexane 1.022 1.010 0.952

58.815 1192-18-3 1c,2-Dimethylcyclopentane 0.007 0.007 0.006

59.374 4516-69-2 1,1,3-Trimethylcyclopentane 0.037 0.038 0.030

63.238 4850-28-6 1c,2t,4-Trimethylcyclopentane 0.037 0.037 0.030

68.289 4259-00-1 1,1,2-Trimethylcyclopentane 0.010 0.010 0.008

70.438 2207-04-7 1t,4-Dimethylcyclohexane 0.224 0.224 0.183

72.950 3c-Ethylmethylcyclopentane 0.018 0.018 0.015

73.175 3t-Ethylmethylcyclopentane 0.023 0.023 0.019

73.439 111-66-0 2t-Ethylmethylcyclopentane 0.009 0.009 0.007

73.86216747-50-5 1,1-Methylethylcyclopentane 0.107 0.104 0.087

75.159 1c,2c,3-Trimethylcyclopentane 0.070 0.068 0.057

76.425 3875-51-2 i-Propylcyclopentane 0.005 0.005 0.004

79.158 2207-01-4 1c,2-Dimethylcyclohexane 0.045 0.043 0.036

80.889 1678-91-7 Ethylcyclohexane 0.031 0.030 0.025

81.110 1795-27-3 1c,3c,5-Trimethylcyclohexane 0.112 0.111 0.081

82.790 7667-60-9 1c,2t,4t-Trimethylcyclohexane 0.061 0.059 0.044

85.924 1c,2t,4c-Trimethylcyclohexane 0.040 0.040 0.029

86.698 7094-26-0 1,1,2-Trimethylcyclohexane 1.013 0.963 0.734

88.495 3788-32-7 i-Butylcyclopentane 0.012 0.011 0.008

91.743 696-29-7 i-Propylcyclohexane 0.263 0.249 0.191

93.402 2040-95-1 n-Butylcyclopentane 0.350 0.339 0.253

100.156 1t-Methyl-2-n-propylcyclohexanR 0.040 0.038 0.026

103.275 7058-01-7 sec-Butylcyclohexane 0.039 0.036 0.025

Di/Bicyclo-Naphth106.219 493-02-7 t-Decahydronaphthalene 0.078 0.075 0.047

Olefins 64.820 C8-Olefin2 0.031 0.033 0.029

68.507 C8-Olefin3 0.023 0.024 0.018

85.547 C9-Olefin3 0.038 0.040 0.027

87.163 C9-Olefin4 0.087 0.092 0.063

n-Olefins 31.175 592-41-6 Hexene-1 4.669 5.238 5.075

57.895 6443-92-1 c-Heptene-2 0.004 0.005 0.004

73.62914850-23-8 t-Octene-4 0.006 0.006 0.005

C-373
Hydrocarbon Expert V4.0 Tue Jul 01 17:21:08 2008 Page 4

File: C:\HPCHEM\2\DATA\6-29-08\002F0201.D\002F0201_ADC1_B.CDF 29-Jun-08, 15:09:16

Sample: ODDB-71719 Operator: RAS

Parameter: C:\HPCHEM\HCE40\ODDB-71719

ODDB-71719 R.

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol

n-Olefins 74.85914919-01-8 t-Octene-3 0.005 0.005 0.004

89.23020237-46-0 c-Nonene-3 0.015 0.016 0.011

90.103 6434-78-2 t-Nonene-2 0.048 0.047 0.035

91.256 6434-77-1 c-Nonene-2 0.020 0.019 0.014

99.833 872-05-9 Decene-1 0.010 0.011 0.007

Iso-Olefins 35.315 922-62-3 3-Methyl-c-pentene-2 0.012 0.013 0.013

37.505 3404-73-7 3,3-Dimethylpentene-1 0.008 0.009 0.008

45.344 692-24-0 2-Methyl-t-hexene-3 0.006 0.007 0.006

55.80410574-36-4 3-Methyl-c-hexene-2 0.005 0.005 0.004

79.97219550-75-6 t-2,2-Dimethylheptene-3 0.019 0.021 0.014

83.043 4588-18-5 2-Methyloctene-1 0.014 0.015 0.010

88.98320063-92-8 t-7-Methyloctene-3 0.005 0.005 0.003

90.402 4984-01-4 3,7-Dimethyloctene-1 0.012 0.013 0.008

100.29619781-18-0 2,3-Dimethyloctene-2 0.513 0.528 0.335

Naphtheno-Olefin

Di-Olefins 67.285 C8-Diolefin3 0.015 0.016 0.014

67.614 C8-Diolefin4 0.030 0.031 0.028

71.709 1002-33-1 1,3-Octadiene 0.052 0.051 0.043

Oxygenates 12.696 64-17-5 Ethanol 7.659 7.383 15.209

Plus

C-374
Hydrocarbon Expert V4.0 Tue Jul 01 17:21:08 2008 Page 1

File: C:\HPCHEM\2\DATA\6-29-08\002F0201.D\002F0201_ADC1_B.CDF 29-Jun-08, 15:09:16

Sample: ODDB-71719 Operator: RAS

Parameter: C:\HPCHEM\HCE40\ODDB-71719

ODDB-71719 R.

Sample Chromatogram

C:\HPCHEM\2\DATA\6-29-08\002F0201.D\002F0201_ADC1_B.CDF

2 22.50 20.00 17.50 15.00 12.50 10.00 7.50 5.00 2.50

i-Butane

n-Butane

2,2-Dimethylpropane

Ethanol

i-Pentane

n-Pentane

2,2-Dimethylbutane

C-375
Hydrocarbon Expert V4.0 Tue Jul 01 17:21:08 2008 Page 2

File: C:\HPCHEM\2\DATA\6-29-08\002F0201.D\002F0201_ADC1_B.CDF 29-Jun-08, 15:09:16

Sample: ODDB-71719 Operator: RAS

Parameter: C:\HPCHEM\HCE40\ODDB-71719

ODDB-71719 R.

Sample Chromatogram

C:\HPCHEM\2\DATA\6-29-08\002F0201.D\002F0201_ADC1_B.CDF

5 47.50 45.00 42.50 40.00 37.50 35.00 32.50 30.00 27.50

Cyclopentane

2,3-Dimethylbutane

2-Methylpentane

3-Methylpentane

Hexene-1

n-Hexane

3-Methyl-c-pentene-2

3,3-Dimethylpentene-1

2,2-Dimethylpentane

2,4-Dimethylpentane

2,2,3-Trimethylbutane

Benzene

Cyclohexane

2-Methyl-t-hexene-3

2-Methylhexane

3-Methylhexane

C-376
Hydrocarbon Expert V4.0 Tue Jul 01 17:21:08 2008 Page 3

File: C:\HPCHEM\2\DATA\6-29-08\002F0201.D\002F0201_ADC1_B.CDF 29-Jun-08, 15:09:16

Sample: ODDB-71719 Operator: RAS

Parameter: C:\HPCHEM\HCE40\ODDB-71719

ODDB-71719 R.

Sample Chromatogram

C:\HPCHEM\2\DATA\6-29-08\002F0201.D\002F0201_ADC1_B.CDF

7 72.50 70.00 67.50 65.00 62.50 60.00 57.50 55.00 52.50

1c,3-Dimethylcyclopentane

1t,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane

2,2,4-Trimethylpentane

n-Heptane

3-Methyl-c-hexene-2

c-Heptene-2

Methylcyclohexane

1c,2-Dimethylcyclopentane

1,1,3-Trimethylcyclopentane

2,2-Dimethylhexane

2,2,3-Trimethylpentane 2,5-Dimethylhexane

2,4-Dimethylhexane

1c,2t,4-Trimethylcyclopentane

3,3-Dimethylhexane

C8-Olefin2

2,3,4-Trimethylpentane

Toluene

C8-Diolefin3

C8-Diolefin4

2-Methyl-3-ethylpentane 1,1,2-Trimethylcyclopentane C8-Olefin3

2-Methylheptane 4-Methylheptane 3,4-Dimethylhexane

1t,4-Dimethylcyclohexane 3-Ethylhexane 3-Methylheptane

1,3-Octadiene

2,2,5-Trimethylhexane 3c-Ethylmethylcyclopentane 3t-Ethylmethylcyclopentane 2t-Ethylmethylcyclopentane t-Octene-4 1,1-Methylethylcyclopentane 2,2,4-Trimethylhexane

t-Octene-3

C-377
Hydrocarbon Expert V4.0 Tue Jul 01 17:21:08 2008 Page 4

File: C:\HPCHEM\2\DATA\6-29-08\002F0201.D\002F0201_ADC1_B.CDF 29-Jun-08, 15:09:16

Sample: ODDB-71719 Operator: RAS

Parameter: C:\HPCHEM\HCE40\ODDB-71719

ODDB-71719 R.

Sample Chromatogram

C:\HPCHEM\2\DATA\6-29-08\002F0201.D\002F0201_ADC1_B.CDF

1 97.50 95.00 92.50 90.00 87.50 85.00 82.50 80.00 77.50

1c,2c,3-Trimethylcyclopentane n-Octane

i-Propylcyclopentane

2,3,4-Trimethylhexane

1c,2-Dimethylcyclohexane

2,2-Dimethylheptane t-2,2-Dimethylheptene-3 2,2,3-Trimethylhexane

4,4-Dimethylheptane

Ethylcyclohexane 1c,3c,5-Trimethylcyclohexane 3,3-Dimethylheptane

2-Methyl-4-ethylhexane

Ethylbenzene 1c,2t,4t-Trimethylcyclohexane 2-Methyloctene-1

m-Xylene p-Xylene 2,3-Dimethylheptane

3,3-Diethylpentane

4-Methyloctane 2-Methyloctane C9-Olefin3

1c,2t,4c-Trimethylcyclohexane 3-Methyloctane

1,1,2-Trimethylcyclohexane

C9-Olefin4

N18

C9-Isoparaffin1

i-Butylcyclopentane

t-7-Methyloctene-3 c-Nonene-3

n-Nonane

t-Nonene-2 3,7-Dimethyloctene-1

i-Propylbenzene

c-Nonene-2

i-Propylcyclohexane 2,2-Dimethyloctane N28 2,4-Dimethyloctane

2,6-Dimethyloctane 2,5-Dimethyloctane

n-Butylcyclopentane

3,3-Dimethyloctane

n-Propylbenzene 3-Methyl-5-ethylheptane

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

1-Methyl-2-ethylbenzene 2-Methylnonane

3-Methylnonane

C10-Isoparaffin1 I19 1,2,4-Trimethylbenzene

Decene-1

C-378
Hydrocarbon Expert V4.0 Tue Jul 01 17:21:08 2008 Page 5

File: C:\HPCHEM\2\DATA\6-29-08\002F0201.D\002F0201_ADC1_B.CDF 29-Jun-08, 15:09:16

Sample: ODDB-71719 Operator: RAS

Parameter: C:\HPCHEM\HCE40\ODDB-71719

ODDB-71719 R.

Sample Chromatogram

C:\HPCHEM\2\DATA\6-29-08\002F0201.D\002F0201_ADC1_B.CDF

1 122.50 120.00 117.50 115.00 112.50 110.00 107.50 105.00 102.50

1t-Methyl-2-n-propylcyclohexanR 2,3-Dimethyloctene-2 sec-Butylbenzene n-Decane

C11-Isoparaffin1

1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene 1-Methyl-4-i-propylbenzene 2,3-Dihydroindene sec-Butylcyclohexane

C11-Isoparaffin2 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene 1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

1-Methyl-2-n-propylbenzene t-Decahydronaphthalene C11-Isoparaffin3

1,4,Dimethyl-2-ethylbenzene 1,3-Dimethyl-4-ethylbenzene

1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

1-Methyl-4-t-butylbenzene 1,2-Dimethyl-3-ethylbenzene

n-Undecane 1,2,3,5-Tetramethylbenzene

5-Methylindan

Naphthalene

n-Dodecane

C-379
Hydrocarbon Expert V4.0 Tue Jul 01 17:21:08 2008 Page 6

File: C:\HPCHEM\2\DATA\6-29-08\002F0201.D\002F0201_ADC1_B.CDF 29-Jun-08, 15:09:16

Sample: ODDB-71719 Operator: RAS

Parameter: C:\HPCHEM\HCE40\ODDB-71719

ODDB-71719 R.

Sample Chromatogram

C:\HPCHEM\2\DATA\6-29-08\002F0201.D\002F0201_ADC1_B.CDF

1 147.50 145.00 142.50 140.00 137.50 135.00 132.50 130.00 127.50

1-Methylnaphthalene

n-Tridecane

C-380
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 1

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 10.977 12.565 11.015

I-Paraffins 26.015 28.917 23.032

Aromatics 31.773 27.542 26.225

Mono-Aromatics 31.210 27.099 25.816

Naphthalenes 0.064 0.049 0.042

Naphtheno/Olefino-Benz 0.043 0.036 0.029

Indenes 0.445 0.348 0.332

Naphthenes 8.725 8.554 7.671

Mono-Naphthenes 8.396 8.239 7.456

Di/Bicyclo-Naphthenes 0.067 0.063 0.038

Olefins 4.083 4.450 3.905

n-Olefins 3.101 3.420 3.145

Iso-Olefins 0.459 0.494 0.332

Naphtheno-Olefins 0.007 0.007 0.009

Di-Olefins 0.214 0.215 0.182

Oxygenates 12.087 11.560 23.113

Unidentified 6.341 6.413 5.040

Plus 0.000 0.000 0.000

C-381
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 1

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C2 12.079 11.551 23.104

C4 2.693 3.513 4.082

C5 7.949 9.638 9.715

C6 8.971 9.665 9.360

C7 16.083 15.338 14.872

C8 20.364 19.816 16.301

C9 17.077 15.882 12.245

C10 7.022 6.779 4.479

C11 1.293 1.283 0.734

C12 0.120 0.112 0.063

C13 0.010 0.010 0.005

C-382
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 1

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C4 2.633 3.433 3.992

C5 0.981 1.182 1.199

C6 1.306 1.495 1.336

C7 1.606 1.772 1.412

C8 1.672 1.796 1.290

C9 1.267 1.332 0.870

C10 1.202 1.243 0.745

C11 0.260 0.263 0.146

C12 0.042 0.042 0.022

C13 0.007 0.007 0.003

I-Paraffins C4 0.057 0.077 0.086

C5 6.771 8.247 8.270

C6 2.167 2.486 2.216

C7 2.375 2.634 2.089

C8 7.343 7.898 5.664

C9 3.493 3.674 2.400

C10 2.887 2.977 1.788

C11 0.892 0.897 0.504

C12 0.026 0.026 0.013

C13 0.003 0.003 0.001

Aromatics C12 0.011 0.009 0.006

Mono-Aromatics C6 0.656 0.563 0.740

C7 8.665 7.541 8.287

C8 9.279 8.082 7.702

C9 10.671 9.233 7.824

C10 1.821 1.580 1.196

C11 0.079 0.068 0.047

C12 0.037 0.032 0.020

Naphthalenes C10 0.051 0.039 0.035

C11 0.013 0.009 0.008

Naphtheno/Olefino-BenzsC10 0.043 0.036 0.029

Indenes C10 0.445 0.348 0.332

Naphthenes C8 0.005 0.004 0.004

C9 0.202 0.195 0.141

C10 0.006 0.006 0.004

C11 0.049 0.046 0.028

Mono-Naphthenes C5 0.122 0.123 0.153

C-383
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 2

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Mono-Naphthenes C6 2.081 2.050 2.179

C7 3.390 3.342 3.042

C8 1.677 1.641 1.317

C9 0.825 0.800 0.576

C10 0.298 0.279 0.187

C12 0.003 0.003 0.002

Di/Bicyclo-Naphthenes C10 0.067 0.063 0.038

Olefins C6 0.001 0.001 0.001

C7 0.011 0.012 0.010

C8 0.131 0.135 0.113

C9 0.159 0.166 0.114

n-Olefins C4 0.001 0.001 0.002

C5 0.035 0.040 0.044

C6 2.732 3.041 2.861

C7 0.009 0.010 0.008

C8 0.055 0.057 0.043

C9 0.260 0.260 0.181

C10 0.010 0.010 0.006

Iso-Olefins C5 0.022 0.025 0.027

C6 0.022 0.024 0.023

C7 0.025 0.027 0.023

C9 0.200 0.221 0.140

C10 0.190 0.197 0.120

Naphtheno-Olefins C5 0.004 0.004 0.005

C6 0.003 0.003 0.003

Di-Olefins C5 0.009 0.010 0.012

C6 0.001 0.001 0.001

C7 0.001 0.001 0.001

C8 0.203 0.203 0.169

Oxygenates C2 12.079 11.551 23.104

C4 0.002 0.002 0.002

C5 0.005 0.005 0.005

C6 0.001 0.001 0.001

C-384
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 1

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol

1 7.612 ? Unidentified 0.002 0.003 0.004

2 8.696 75-28-5 I4 i-Butane 0.057 0.077 0.086

3 9.740 106-97-8 P4 n-Butane 2.633 3.433 3.992

4 10.159 624-64-6 K4 t-Butene-2 0.001 0.001 0.001

5 10.276 463-82-1 I5 2,2-Dimethylpropane 0.015 0.020 0.019

6 10.798 590-18-1 K4 c-Butene-2 0.001 0.001 0.001

7 12.708 64-17-5 X2 Ethanol 12.079 11.551 23.104

8 14.140 78-78-4 I5 i-Pentane 6.756 8.227 8.251

9 14.734 ? Unidentified 0.004 0.005 0.007

10 14.814 ? Unidentified 0.002 0.002 0.003

11 14.853 ? Unidentified 0.003 0.004 0.004

12 14.910 ? Unidentified 0.016 0.019 0.020

13 15.238 ? Unidentified 0.001 0.001 0.001

14 15.258 ? Unidentified 0.001 0.002 0.002

15 15.286 ? Unidentified 0.007 0.009 0.009

16 15.546 109-67-1 K5 Pentene-1 0.019 0.022 0.024

17 15.818 ? Unidentified 0.002 0.002 0.003

18 15.878 ? Unidentified 0.004 0.004 0.006

19 15.989 ? Unidentified 0.001 0.001 0.001

20 16.008 ? Unidentified 0.004 0.003 0.005

21 16.115 ? Unidentified 0.001 0.001 0.002

22 16.144 ? Unidentified 0.001 0.001 0.002

23 16.185 ? Unidentified 0.001 0.001 0.001

24 16.301 563-46-2 C5 2-Methylbutene-1 0.012 0.014 0.015

25 16.482 ? Unidentified 0.001 0.002 0.002

26 16.524 ? Unidentified 0.004 0.004 0.005

27 16.754 109-66-0 P5 n-Pentane 0.981 1.182 1.199

28 17.219 78-79-5 E5 2-Methyl-1,3-Butadiene 0.004 0.005 0.005

29 17.318 ? Unidentified 0.001 0.001 0.001

30 17.351 ? Unidentified 0.002 0.002 0.003

31 17.452 ? Unidentified 0.002 0.002 0.002

32 17.503 ? Unidentified 0.001 0.001 0.001

33 17.537 ? Unidentified 0.000 0.001 0.001

34 17.562 ? Unidentified 0.001 0.001 0.001

35 17.589 ? Unidentified 0.001 0.002 0.002

36 17.635 ? Unidentified 0.001 0.001 0.001

37 17.768 646-04-8 K5 t-Pentene-2 0.009 0.010 0.011

38 17.907 ? Unidentified 0.001 0.002 0.002

39 17.968 ? Unidentified 0.002 0.002 0.002

40 18.037 ? Unidentified 0.001 0.001 0.001

41 18.064 ? Unidentified 0.002 0.002 0.003

42 18.190 ? Unidentified 0.002 0.002 0.002

43 18.235 ? Unidentified 0.001 0.001 0.001

44 18.257 ? Unidentified 0.001 0.001 0.001

C-385
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 2

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol

45 18.313 ? Unidentified 0.001 0.001 0.001

46 18.333 ? Unidentified 0.001 0.001 0.001

47 18.397 598-25-4 E5 3-Methylbutadiene-1,2 0.002 0.002 0.002

48 18.463 ? Unidentified 0.001 0.001 0.002

49 18.494 ? Unidentified 0.001 0.001 0.001

50 18.538 ? Unidentified 0.001 0.001 0.001

51 18.578 ? Unidentified 0.001 0.001 0.001

52 18.703 627-20-3 K5 c-Pentene-2 0.007 0.008 0.009

53 18.850 ? Unidentified 0.001 0.001 0.001

54 18.950 ? Unidentified 0.004 0.003 0.004

55 19.063 ? Unidentified 0.001 0.001 0.001

56 19.102 ? Unidentified 0.001 0.001 0.001

57 19.147 75-65-0 X4 t-Butanol 0.001 0.001 0.001

58 19.186 ? Unidentified 0.001 0.001 0.001

59 19.312 513-35-9 C5 2-Methylbutene-2 0.010 0.011 0.012

60 19.480 ? Unidentified 0.001 0.002 0.002

61 19.561 ? Unidentified 0.001 0.001 0.001

62 19.630 2004-70-8 E5 1t,3-Pentadiene 0.002 0.003 0.003

63 19.685 ? Unidentified 0.001 0.001 0.001

64 19.743 ? Unidentified 0.002 0.002 0.002

65 19.795 ? Unidentified 0.001 0.001 0.001

66 19.830 ? Unidentified 0.000 0.000 0.001

67 19.893 ? Unidentified 0.001 0.001 0.002

68 19.939 ? Unidentified 0.001 0.001 0.001

69 19.975 ? Unidentified 0.001 0.001 0.001

70 20.078 ? Unidentified 0.003 0.003 0.003

71 20.161 ? Unidentified 0.001 0.001 0.001

72 20.230 ? Unidentified 0.001 0.001 0.001

73 20.283 ? Unidentified 0.001 0.001 0.001

74 20.307 ? Unidentified 0.000 0.001 0.001

75 20.341 ? Unidentified 0.001 0.001 0.001

76 20.398 ? Unidentified 0.001 0.001 0.001

77 20.564 ? Unidentified 0.003 0.004 0.004

78 20.647 ? Unidentified 0.001 0.001 0.001

79 20.756 ? Unidentified 0.003 0.003 0.004

80 20.855 1574-41-0 E5 1c,3-Pentadiene 0.001 0.001 0.001

81 20.922 ? Unidentified 0.001 0.001 0.001

82 20.947 ? Unidentified 0.000 0.001 0.001

83 21.020 ? Unidentified 0.001 0.001 0.001

84 21.062 ? Unidentified 0.001 0.001 0.001

85 21.092 ? Unidentified 0.001 0.001 0.001

86 21.256 75-83-2 I6 2,2-Dimethylbutane 0.130 0.152 0.133

87 21.447 ? Unidentified 0.002 0.002 0.002

88 21.559 ? Unidentified 0.002 0.002 0.002

C-386
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 3

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol

89 21.694 ? Unidentified 0.001 0.001 0.001

90 21.722 ? Unidentified 0.000 0.001 0.000

91 21.750 ? Unidentified 0.001 0.001 0.001

92 21.837 ? Unidentified 0.001 0.001 0.001

93 21.867 ? Unidentified 0.001 0.001 0.001

94 21.981 ? Unidentified 0.001 0.002 0.002

95 22.004 ? Unidentified 0.001 0.001 0.001

96 22.082 ? Unidentified 0.001 0.001 0.001

97 22.122 ? Unidentified 0.000 0.000 0.000

98 22.186 ? Unidentified 0.002 0.002 0.002

99 22.281 ? Unidentified 0.001 0.001 0.001

100 22.330 ? Unidentified 0.001 0.001 0.001

101 22.440 ? Unidentified 0.001 0.001 0.001

102 22.541 ? Unidentified 0.001 0.001 0.002

103 22.592 ? Unidentified 0.001 0.001 0.001

104 22.664 ? Unidentified 0.001 0.001 0.002

105 22.698 ? Unidentified 0.000 0.000 0.001

106 22.784 ? Unidentified 0.001 0.001 0.002

107 22.825 ? Unidentified 0.000 0.000 0.001

108 22.866 ? Unidentified 0.000 0.000 0.001

109 22.931 ? Unidentified 0.001 0.001 0.002

110 23.035 ? Unidentified 0.001 0.001 0.001

111 23.107 ? Unidentified 0.000 0.000 0.001

112 23.160 ? Unidentified 0.001 0.001 0.001

113 23.203 ? Unidentified 0.001 0.001 0.001

114 23.304 ? Unidentified 0.002 0.002 0.002

115 23.412 ? Unidentified 0.000 0.000 0.001

116 23.468 ? Unidentified 0.002 0.002 0.002

117 23.566 ? Unidentified 0.001 0.001 0.001

118 23.704 142-29-0 B5 Cyclopentene 0.004 0.004 0.005

119 23.871 ? Unidentified 0.002 0.002 0.002

120 24.010 ? Unidentified 0.001 0.001 0.001

121 24.040 ? Unidentified 0.001 0.001 0.001

122 24.118 ? Unidentified 0.001 0.001 0.001

123 24.165 ? Unidentified 0.001 0.001 0.001

124 24.205 ? Unidentified 0.001 0.001 0.001

125 24.299 ? Unidentified 0.001 0.001 0.001

126 24.327 ? Unidentified 0.001 0.001 0.001

127 24.428 ? Unidentified 0.001 0.001 0.001

128 24.509 ? Unidentified 0.000 0.001 0.001

129 24.577 ? Unidentified 0.001 0.001 0.001

130 24.608 ? Unidentified 0.001 0.001 0.001

131 24.794 ? Unidentified 0.001 0.002 0.002

132 24.896 691-37-2 C6 4-Methylpentene-1 0.004 0.005 0.004

C-387
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 4

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol

133 25.015 ? Unidentified 0.001 0.001 0.001

134 25.133 ? Unidentified 0.001 0.001 0.002

135 25.161 ? Unidentified 0.001 0.001 0.001

136 25.193 ? Unidentified 0.000 0.000 0.001

137 25.244 ? Unidentified 0.001 0.001 0.001

138 25.419 287-92-3 M5 Cyclopentane 0.122 0.123 0.153

139 25.626 ? Unidentified 0.001 0.001 0.001

140 25.696 ? Unidentified 0.001 0.001 0.001

141 25.728 ? Unidentified 0.001 0.001 0.001

142 25.782 ? Unidentified 0.001 0.001 0.001

143 25.853 ? Unidentified 0.000 0.001 0.000

144 26.106 79-29-8 I6 2,3-Dimethylbutane 0.483 0.550 0.494

145 26.351 ? Unidentified 0.002 0.002 0.002

146 26.524 1634-04-4 X5 Methyl-t-butylether 0.005 0.005 0.005

147 26.653 ? Unidentified 0.001 0.001 0.001

148 26.735 ? Unidentified 0.001 0.001 0.001

149 26.798 ? Unidentified 0.001 0.001 0.001

150 26.819 ? Unidentified 0.001 0.001 0.001

151 26.870 691-38-3 C6 4-Methyl-c-pentene-2 0.001 0.001 0.001

152 27.126 107-83-5 I6 2-Methylpentane 0.960 1.110 0.982

153 27.558 674-76-0 C6 4-Methyl-t-pentene-2 0.004 0.004 0.004

154 27.702 ? Unidentified 0.000 0.000 0.000

155 27.727 ? Unidentified 0.000 0.000 0.000

156 27.753 ? Unidentified 0.000 0.000 0.000

157 27.839 ? Unidentified 0.001 0.001 0.001

158 27.908 ? Unidentified 0.001 0.001 0.001

159 28.007 ? Unidentified 0.000 0.000 0.000

160 28.062 ? Unidentified 0.001 0.001 0.001

161 28.141 ? Unidentified 0.000 0.001 0.000

162 28.229 ? Unidentified 0.000 0.001 0.000

163 28.332 ? Unidentified 0.000 0.000 0.000

164 28.358 ? Unidentified 0.001 0.001 0.001

165 28.502 ? Unidentified 0.001 0.002 0.001

166 28.558 ? Unidentified 0.000 0.001 0.000

167 28.619 ? Unidentified 0.000 0.000 0.000

168 28.652 ? Unidentified 0.001 0.001 0.001

169 28.729 ? Unidentified 0.000 0.001 0.000

170 28.784 ? Unidentified 0.000 0.001 0.000

171 28.812 ? Unidentified 0.000 0.000 0.000

172 28.896 ? Unidentified 0.001 0.002 0.001

173 29.124 ? Unidentified 0.001 0.001 0.001

174 29.155 ? Unidentified 0.000 0.001 0.000

175 29.252 ? Unidentified 0.000 0.000 0.000

176 29.307 ? Unidentified 0.001 0.001 0.001

C-388
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 5

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol

177 29.371 ? Unidentified 0.001 0.001 0.001

178 29.626 96-14-0 I6 3-Methylpentane 0.594 0.675 0.607

179 29.945 ? Unidentified 0.000 0.001 0.000

180 30.037 ? Unidentified 0.000 0.000 0.000

181 30.064 ? Unidentified 0.000 0.000 0.000

182 30.127 ? Unidentified 0.001 0.001 0.001

183 30.207 ? Unidentified 0.001 0.001 0.001

184 30.389 ? Unidentified 0.001 0.001 0.001

185 30.594 ? Unidentified 0.000 0.000 0.000

186 31.005 592-41-6 K6 Hexene-1 2.717 3.024 2.845

187 31.678 ? Unidentified 0.001 0.001 0.001

188 31.721 ? Unidentified 0.001 0.001 0.001

189 31.795 ? Unidentified 0.002 0.002 0.002

190 31.939 ? Unidentified 0.001 0.001 0.001

191 32.053 ? Unidentified 0.001 0.001 0.001

192 32.072 ? Unidentified 0.000 0.000 0.001

193 32.174 ? Unidentified 0.001 0.001 0.001

194 32.211 ? Unidentified 0.001 0.001 0.001

195 32.321 ? Unidentified 0.000 0.000 0.001

196 32.349 ? Unidentified 0.001 0.001 0.001

197 32.463 ? Unidentified 0.000 0.000 0.001

198 32.544 ? Unidentified 0.000 0.000 0.001

199 32.601 ? Unidentified 0.001 0.000 0.001

200 32.693 ? Unidentified 0.000 0.000 0.000

201 32.747 ? Unidentified 0.001 0.001 0.001

202 32.832 ? Unidentified 0.001 0.001 0.001

203 32.880 ? Unidentified 0.000 0.001 0.000

204 32.921 ? Unidentified 0.000 0.000 0.000

205 33.228 110-54-3 P6 n-Hexane 1.306 1.495 1.336

206 33.634 ? Unidentified 0.001 0.002 0.001

207 33.85613269-52-8 K6 t-Hexene-3 0.005 0.006 0.005

208 34.045 ? Unidentified 0.000 0.000 0.000

209 34.072 ? Unidentified 0.000 0.001 0.000

210 34.121 ? Unidentified 0.000 0.000 0.000

211 34.319 4050-45-7 K6 t-Hexene-2 0.007 0.007 0.007

212 34.523 ? Unidentified 0.001 0.001 0.001

213 34.792 625-27-4 C6 2-Methylpentene-2 0.004 0.004 0.004

214 34.935 ? Unidentified 0.001 0.001 0.001

215 35.183 922-62-3 C6 3-Methyl-c-pentene-2 0.010 0.011 0.010

216 35.395 ? Unidentified 0.000 0.000 0.000

217 35.441 ? Unidentified 0.001 0.001 0.001

218 35.554 ? Unidentified 0.001 0.001 0.001

219 35.605 ? Unidentified 0.000 0.001 0.001

220 35.759 O6 O14 0.001 0.001 0.001

C-389
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 6

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol

221 35.881 ? Unidentified 0.000 0.000 0.000

222 36.080 7688-21-3 K6 c-Hexene-2 0.004 0.004 0.004

223 36.248 ? Unidentified 0.001 0.001 0.001

224 36.512 ? Unidentified 0.000 0.000 0.000

225 36.589 ? Unidentified 0.001 0.001 0.001

226 36.677 ? Unidentified 0.001 0.001 0.001

227 36.811 ? Unidentified 0.000 0.000 0.000

228 37.098 ? Unidentified 0.001 0.001 0.001

229 37.130 ? Unidentified 0.000 0.001 0.000

230 37.188 ? Unidentified 0.000 0.000 0.000

231 37.372 3404-73-7 C7 3,3-Dimethylpentene-1 0.007 0.007 0.006

232 37.861 96-37-7 M6 Methylcyclopentane 0.869 0.875 0.909

233 38.223 ? Unidentified 0.000 0.000 0.001

234 38.383 ? Unidentified 0.001 0.001 0.001

235 38.580 ? Unidentified 0.001 0.001 0.001

236 38.633 ? Unidentified 0.000 0.001 0.001

237 38.685 563-79-1 E7 2,3-Dimethyl-2-Butene 0.001 0.001 0.001

238 38.812 ? Unidentified 0.000 0.000 0.000

239 38.871 ? Unidentified 0.000 0.000 0.000

240 39.033 ? Unidentified 0.001 0.001 0.001

241 39.091 ? Unidentified 0.001 0.001 0.001

242 39.171 ? Unidentified 0.001 0.001 0.001

243 39.411 108-08-7 I7 2,4-Dimethylpentane 0.399 0.448 0.351

244 39.680 594-56-9 C7 2,3,3-Trimethylbutene-1 0.001 0.001 0.001

245 39.932 464-06-2 I7 2,2,3-Trimethylbutane 0.052 0.057 0.046

246 40.226 ? Unidentified 0.001 0.001 0.001

247 40.416 ? Unidentified 0.000 0.000 0.000

248 40.569 ? Unidentified 0.001 0.001 0.001

249 40.640 7385-78-6 C7 3,4-Dimethylpentene-1 0.001 0.001 0.000

250 40.708 ? Unidentified 0.000 0.000 0.000

251 40.824 ? Unidentified 0.000 0.001 0.000

252 40.860 ? Unidentified 0.000 0.000 0.000

253 41.012 ? Unidentified 0.001 0.001 0.001

254 41.068 ? Unidentified 0.001 0.002 0.001

255 41.384 ? Unidentified 0.001 0.001 0.001

256 41.476 ? Unidentified 0.001 0.001 0.000

257 41.586 762-63-0 C7 4,4-Dimethyl-c-pentene-2 0.001 0.001 0.001

258 41.710 ? Unidentified 0.001 0.001 0.001

259 41.895 ? Unidentified 0.001 0.001 0.000

260 41.985 ? Unidentified 0.001 0.001 0.001

261 42.090 ? Unidentified 0.001 0.001 0.000

262 42.251 ? Unidentified 0.001 0.001 0.001

263 42.502 E6 Diolefin 0.001 0.001 0.001

264 42.702 71-42-3 Q6 Benzene 0.656 0.563 0.740

C-390
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 7

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol

265 43.291 ? Unidentified 0.001 0.001 0.001

266 43.380 ? Unidentified 0.001 0.001 0.000

267 43.481 ? Unidentified 0.001 0.001 0.001

268 43.693 ? Unidentified 0.000 0.000 0.000

269 43.765 C7 2-Methyl-c-hexene-3 0.001 0.001 0.001

270 43.848 ? Unidentified 0.001 0.001 0.000

271 44.271 562-49-2 I7 3,3-Dimethylpentane 0.064 0.069 0.056

272 44.537 110-82-7 M6 Cyclohexane 1.212 1.175 1.269

273 45.121 692-24-0 C7 2-Methyl-t-hexene-3 0.003 0.003 0.002

274 45.278 ? Unidentified 0.001 0.001 0.001

275 45.410 ? Unidentified 0.000 0.000 0.000

276 45.599 71-36-3 X4 n-Butanol 0.001 0.001 0.001

277 45.814 ? Unidentified 0.001 0.001 0.001

278 45.950 ? Unidentified 0.000 0.000 0.001

279 46.054 ? Unidentified 0.001 0.001 0.001

280 46.305 7357-93-9 C7 2-Ethyl-3-methylbutene-1 0.001 0.001 0.001

281 46.670 3769-23-1 C7 4-Methylhexene-1 0.001 0.001 0.001

282 46.824 ? Unidentified 0.001 0.001 0.001

283 47.295 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.002 0.002 0.001

284 47.659 591-76-4 I7 2-Methylhexane 1.191 1.325 1.048

285 48.071 110-83-8 B6 Cyclohexene 0.003 0.003 0.003

286 48.278 ? Unidentified 0.000 0.000 0.001

287 48.344 ? Unidentified 0.001 0.001 0.001

288 48.517 994-05-8 X6 TAME 0.001 0.001 0.001

289 48.799 ? Unidentified 0.001 0.001 0.001

290 48.889 ? Unidentified 0.000 0.000 0.000

291 49.024 ? Unidentified 0.001 0.001 0.001

292 49.135 ? Unidentified 0.001 0.001 0.000

293 49.450 589-34-4 I7 3-Methylhexane 0.669 0.734 0.588

294 49.925 ? Unidentified 0.001 0.001 0.001

295 50.241 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.180 0.183 0.162

296 50.596 ? Unidentified 0.001 0.001 0.001

297 50.810 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.168 0.170 0.151

298 51.100 C7 2-Ethylpentene-1 0.001 0.001 0.001

299 51.163 ? Unidentified 0.001 0.001 0.001

300 51.414 822-50-4 M7 1t,2-Dimethylcyclopentane 0.270 0.271 0.242

301 51.611 ? Unidentified 0.041 0.041 0.037

302 52.072 540-84-1 I8 2,2,4-Trimethylpentane 2.604 2.840 2.009

303 53.029 ? Unidentified 0.001 0.001 0.001

304 53.088 ? Unidentified 0.001 0.001 0.001

305 53.164 ? Unidentified 0.001 0.001 0.000

306 53.234 ? Unidentified 0.001 0.001 0.001

307 53.348 ? Unidentified 0.000 0.001 0.000

308 53.394 ? Unidentified 0.001 0.001 0.001

C-391
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 8

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol

309 53.596 ? Unidentified 0.000 0.000 0.000

310 53.725 4914-89-0 C7 3-Methyl-c-hexene-3 0.002 0.002 0.002

311 53.959 ? Unidentified 0.001 0.001 0.001

312 54.189 ? Unidentified 0.002 0.002 0.002

313 54.22414686-14-7 K7 t-Heptene-3 0.001 0.001 0.001

314 54.359 ? Unidentified 0.001 0.001 0.001

315 54.527 ? Unidentified 0.002 0.002 0.002

316 54.627 O7 C7-Olefin2 0.002 0.003 0.002

317 54.975 142-82-5 P7 n-Heptane 1.606 1.772 1.412

318 55.412 ? Unidentified 0.001 0.001 0.001

319 55.475 2738-19-4 C7 2-Methyl-2-hexene 0.004 0.005 0.004

320 55.618 ? Unidentified 0.005 0.005 0.004

321 55.974 ? Unidentified 0.001 0.001 0.001

322 56.031 ? Unidentified 0.001 0.001 0.000

323 56.09814686-13-6 K7 t-Heptene-2 0.003 0.003 0.002

324 56.242 816-79-5 C7 3-Ethylpentene-2 0.002 0.002 0.001

325 56.743 ? Unidentified 2.386 2.504 2.141

326 57.363 ? Unidentified 0.007 0.007 0.006

327 57.595 ? Unidentified 0.001 0.001 0.000

328 57.729 6443-92-1 K7 c-Heptene-2 0.006 0.006 0.005

329 58.291 108-87-2 M7 Methylcyclohexane 2.757 2.704 2.474

330 58.636 1192-18-3 M7 1c,2-Dimethylcyclopentane 0.015 0.015 0.013

331 59.192 4516-69-2 M8 1,1,3-Trimethylcyclopentane 0.093 0.094 0.073

332 59.647 590-73-8 I8 2,2-Dimethylhexane 0.082 0.089 0.063

333 59.889 ? Unidentified 0.001 0.001 0.001

334 60.031 ? Unidentified 0.005 0.004 0.003

335 60.174 ? Unidentified 0.001 0.001 0.001

336 60.239 ? Unidentified 0.001 0.002 0.001

337 60.317 ? Unidentified 0.001 0.002 0.001

338 60.387 O7 O35 0.002 0.002 0.002

339 60.521 ? Unidentified 0.003 0.003 0.002

340 60.867 ? Unidentified 0.747 0.769 0.670

341 61.657 564-02-3 I8 2,2,3-Trimethylpentane 0.164 0.173 0.126

342 61.953 592-13-2 I8 2,5-Dimethylhexane 0.445 0.484 0.343

343 62.274 589-43-5 I8 2,4-Dimethylhexane 0.437 0.471 0.337

344 62.520 ? Unidentified 0.010 0.010 0.009

345 63.059 4850-28-6 M8 1c,2t,4-Trimethylcyclopentane 0.099 0.098 0.078

346 63.492 563-16-6 I8 3,3-Dimethylhexane 0.070 0.074 0.054

347 63.811 O7 O38 0.007 0.007 0.006

348 63.980 ? Unidentified 0.002 0.002 0.002

349 64.208 ? Unidentified 0.004 0.004 0.003

350 64.362 ? Unidentified 0.004 0.004 0.003

351 64.635 O8 C8-Olefin2 0.090 0.093 0.081

352 65.327 565-75-3 I8 2,3,4-Trimethylpentane 1.019 1.070 0.786

C-392
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 9

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol

353 66.046 108-88-3 Q7 Toluene 8.665 7.541 8.287

354 67.115 ? Unidentified 0.019 0.019 0.017

355 67.435 E8 C8-Diolefin4 0.067 0.069 0.060

356 67.812 584-94-1 I8 2,3-Dimethylhexane 0.419 0.443 0.323

357 68.350 O8 C8-Olefin3 0.041 0.042 0.032

358 69.195 592-27-8 I8 2-Methylheptane 0.749 0.810 0.578

359 69.436 589-53-7 I8 4-Methylheptane 0.347 0.371 0.268

360 69.769 583-48-2 I8 3,4-Dimethylhexane 0.027 0.028 0.021

361 70.289 638-04-0 M8 1c,3-Dimethylcyclohexane 0.610 0.604 0.479

362 70.549 589-81-1 I8 3-Methylheptane 0.635 0.679 0.490

363 70.655 619-99-8 I8 3-Ethylhexane 0.346 0.366 0.267

364 71.233 M8 1c,2t,3-Trimethylcyclopentane 0.005 0.005 0.004

365 71.547 1002-33-1 E8 1,3-Octadiene 0.136 0.134 0.108

366 71.724 ? Unidentified 0.016 0.016 0.013

367 71.988 ? Unidentified 0.007 0.007 0.005

368 72.504 3522-94-9 I9 2,2,5-Trimethylhexane 0.437 0.467 0.301

369 72.795 M8 3c-Ethylmethylcyclopentane 0.047 0.046 0.037

370 73.020 M8 3t-Ethylmethylcyclopentane 0.061 0.060 0.048

371 73.285 111-66-0 M8 2t-Ethylmethylcyclopentane 0.022 0.022 0.017

372 73.47614850-23-8 K8 t-Octene-4 0.012 0.013 0.010

373 73.70916747-50-5 M8 1,1-Methylethylcyclopentane 0.311 0.300 0.244

374 74.360 2207-03-6 M8 1t,3-Dimethylcyclohexane 0.005 0.005 0.004

375 74.70614919-01-8 K8 t-Octene-3 0.015 0.016 0.012

376 75.004 M8 1c,2c,3-Trimethylcyclopentane 0.196 0.190 0.154

377 75.307 111-65-9 P8 n-Octane 1.672 1.796 1.290

378 75.91213389-42-9 K8 t-Octene-2 0.005 0.005 0.004

379 76.160 O9 C9-Olefin1 0.032 0.033 0.025

380 76.279 ? Unidentified 0.014 0.015 0.010

381 76.552 O9 C9-Olefin2 0.012 0.012 0.008

382 76.884 ? Unidentified 0.009 0.010 0.006

383 77.222 7642-04-8 K8 c-Octene-2 0.023 0.024 0.018

384 77.482 ? Unidentified 0.003 0.003 0.002

385 77.581 ? Unidentified 0.003 0.003 0.002

386 77.787 C9 2,3,3-Trimethylhexene-1 0.092 0.102 0.065

387 78.115 N8 N3 0.005 0.004 0.004

388 78.392 ? Unidentified 0.070 0.073 0.048

389 78.713 ? Unidentified 0.060 0.062 0.041

390 79.022 2207-01-4 M8 1c,2-Dimethylcyclohexane 0.132 0.125 0.103

391 79.221 ? Unidentified 0.018 0.018 0.015

392 79.575 1071-26-7 I9 2,2-Dimethylheptane 0.532 0.565 0.365

393 79.83519550-75-6 C9 t-2,2-Dimethylheptene-3 0.062 0.069 0.044

394 80.02316747-25-4 I9 2,2,3-Trimethylhexane 0.354 0.374 0.243

395 80.393 1068-19-5 I9 4,4-Dimethylheptane 0.289 0.304 0.198

396 80.745 1678-91-7 M8 Ethylcyclohexane 0.096 0.092 0.075

C-393
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 10

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol

397 80.975 1795-27-3 M9 1c,3c,5-Trimethylcyclohexane 0.317 0.311 0.222

398 81.148 4032-86-4 I9 3,3-Dimethylheptane 0.132 0.137 0.091

399 81.408 ? Unidentified 0.046 0.051 0.032

400 81.647 3074-75-7 I9 2-Methyl-4-ethylhexane 0.062 0.065 0.043

401 81.990 ? Unidentified 0.014 0.013 0.010

402 82.282 100-41-4 Q8 Ethylbenzene 1.440 1.253 1.195

403 82.435 ? Unidentified 0.038 0.036 0.026

404 82.644 7667-60-9 M9 1c,2t,4t-Trimethylcyclohexane 0.188 0.182 0.131

405 82.897 4588-18-5 C9 2-Methyloctene-1 0.032 0.036 0.022

406 83.210 ? Unidentified 0.054 0.060 0.038

407 83.617 108-38-3 Q8 m-Xylene 4.534 3.958 3.763

408 83.749 106-42-3 Q8 p-Xylene 1.903 1.668 1.580

409 83.862 ? Unidentified 0.173 0.151 0.143

410 84.110 3074-71-3 I9 2,3-Dimethylheptane 0.059 0.062 0.041

411 84.230 ? Unidentified 0.099 0.103 0.068

412 84.538 1067-20-5 I9 3,3-Diethylpentane 0.132 0.132 0.091

413 84.971 2216-34-4 I9 4-Methyloctane 0.354 0.371 0.243

414 85.115 3221-61-2 I9 2-Methyloctane 0.467 0.494 0.321

415 85.395 N9 N15 0.075 0.073 0.053

416 85.791 M9 1c,2t,4c-Trimethylcyclohexane 0.124 0.121 0.087

417 85.981 2216-33-3 I9 3-Methyloctane 0.485 0.508 0.333

418 86.194 ? Unidentified 0.011 0.012 0.008

419 86.388 ? Unidentified 0.072 0.074 0.049

420 86.573 95-47-6 Q8 o-Xylene 1.403 1.202 1.164

421 86.779 ? Unidentified 0.040 0.038 0.028

422 87.033 O9 C9-Olefin4 0.115 0.121 0.081

423 87.385 N9 N18 0.054 0.052 0.038

424 87.527 ? Unidentified 0.161 0.156 0.112

425 87.831 I9 C9-Isoparaffin1 0.189 0.196 0.130

426 88.174 124-11-8 K9 Nonene-1 0.022 0.024 0.015

427 88.361 ? Unidentified 0.024 0.024 0.017

428 88.536 ? Unidentified 0.018 0.018 0.013

429 88.85820063-92-8 C9 t-7-Methyloctene-3 0.013 0.015 0.009

430 89.09220237-46-0 K9 c-Nonene-3 0.041 0.046 0.029

431 89.269 ? Unidentified 0.007 0.007 0.005

432 89.557 111-84-2 P9 n-Nonane 1.267 1.332 0.870

433 89.923 6434-78-2 K9 t-Nonene-2 0.120 0.116 0.084

434 90.280 4984-01-4 C10 3,7-Dimethyloctene-1 0.059 0.064 0.037

435 90.479 ? Unidentified 0.013 0.012 0.009

436 90.797 98-82-8 Q9 i-Propylbenzene 0.176 0.154 0.129

437 91.015 ? Unidentified 0.014 0.013 0.009

438 91.213 6434-77-1 K9 c-Nonene-2 0.077 0.074 0.054

439 91.481 N9 N26 0.047 0.044 0.032

440 91.610 696-29-7 M9 i-Propylcyclohexane 0.085 0.080 0.059

C-394
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 11

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol

441 91.84215869-87-1 I10 2,2-Dimethyloctane 0.137 0.143 0.085

442 92.008 N9 N28 0.026 0.025 0.018

443 92.117 4032-94-4 I10 2,4-Dimethyloctane 0.037 0.039 0.023

444 92.276 ? Unidentified 0.009 0.009 0.006

445 92.522 2051-30-1 I10 2,6-Dimethyloctane 0.076 0.078 0.047

446 92.69115869-89-3 I10 2,5-Dimethyloctane 0.108 0.112 0.067

447 92.758 ? Unidentified 0.139 0.144 0.086

448 92.925 ? Unidentified 0.024 0.025 0.015

449 93.173 I10 I12 0.088 0.091 0.054

450 93.275 2040-95-1 M9 n-Butylcyclopentane 0.110 0.106 0.077

451 93.528 N10 N30 0.006 0.006 0.004

452 93.728 4110-44-5 I10 3,3-Dimethyloctane 0.233 0.238 0.144

453 93.854 I10 I14 0.055 0.057 0.034

454 94.069 ? Unidentified 0.051 0.052 0.031

455 94.303 103-65-1 Q9 n-Propylbenzene 0.681 0.596 0.499

456 94.57652896-90-9 I10 3-Methyl-5-ethylheptane 0.065 0.068 0.040

457 94.744 ? Unidentified 0.009 0.009 0.005

458 94.874 ? Unidentified 0.013 0.012 0.008

459 94.995 ? Unidentified 0.017 0.016 0.011

460 95.216 620-14-4 Q9 1-Methyl-3-ethylbenzene 2.163 1.888 1.586

461 95.437 622-96-8 Q9 1-Methyl-4-ethylbenzene 1.256 1.101 0.921

462 95.653 ? Unidentified 0.013 0.012 0.010

463 95.782 ? Unidentified 0.005 0.005 0.003

464 96.066 108-67-8 Q9 1,3,5-Trimethylbenzene 1.277 1.113 0.936

465 96.285 ? Unidentified 0.022 0.023 0.014

466 96.422 ? Unidentified 0.031 0.032 0.019

467 96.59115869-85-9 I10 5-Methylnonane 0.166 0.171 0.103

468 96.78717301-94-8 I10 4-Methylnonane 0.297 0.306 0.184

469 96.948 871-83-0 I10 2-Methylnonane 0.751 0.780 0.465

470 97.111 611-14-3 Q9 1-Methyl-2-ethylbenzene 1.137 0.974 0.834

471 97.431 5881-17-4 I10 3-Ethyloctane 0.084 0.086 0.052

472 97.764 5911-04-6 I10 3-Methylnonane 0.394 0.405 0.244

473 97.981 ? Unidentified 0.023 0.022 0.014

474 98.206 ? Unidentified 0.080 0.087 0.051

475 98.314 I10 C10-Isoparaffin1 0.163 0.167 0.101

476 98.569 I10 I19 0.116 0.118 0.072

477 98.815 95-63-6 Q9 1,2,4-Trimethylbenzene 2.674 2.304 1.961

478 98.921 ? Unidentified 0.079 0.081 0.049

479 99.036 1678-98-4 M10 i-Butylcyclohexane 0.127 0.120 0.080

480 99.143 ? Unidentified 0.058 0.059 0.036

481 99.232 I10 I21 0.090 0.092 0.056

482 99.363 ? Unidentified 0.016 0.016 0.010

483 99.464 I10 C10-Isoparaffin2 0.026 0.026 0.016

484 99.560 ? Unidentified 0.017 0.017 0.010

C-395
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 12

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol

485 99.692 ? Unidentified 0.020 0.020 0.012

486 99.828 872-05-9 K10 Decene-1 0.010 0.010 0.006

487 99.904 ? Unidentified 0.007 0.007 0.004

488 100.014 M10 1t-Methyl-2-n-propylcyclohexanR 0.011 0.010 0.007

489 100.14819781-18-0 C10 2,3-Dimethyloctene-2 0.131 0.134 0.082

490 100.386 ? Unidentified 0.098 0.100 0.060

491 100.502 135-98-8 Q10 sec-Butylbenzene 0.064 0.056 0.042

492 100.726 124-18-5 P10 n-Decane 1.202 1.243 0.745

493 101.039 I11 I26 0.278 0.283 0.157

494 101.415 N11 N39 0.049 0.046 0.028

495 101.647 526-73-8 Q9 1,2,3-Trimethylbenzene 1.307 1.102 0.958

496 101.867 ? Unidentified 0.032 0.033 0.018

497 102.054 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.069 0.060 0.045

498 102.262 ? Unidentified 0.049 0.050 0.027

499 102.338 ? Unidentified 0.041 0.036 0.027

500 102.427 ? Unidentified 0.044 0.038 0.029

501 102.500 99-87-6 Q10 1-Methyl-4-i-propylbenzene 0.057 0.050 0.038

502 102.779 496-11-7 J10 2,3-Dihydroindene 0.445 0.348 0.332

503 103.149 7058-01-7 M10 sec-Butylcyclohexane 0.161 0.149 0.101

504 103.377 ? Unidentified 0.019 0.017 0.013

505 103.525 ? Unidentified 0.222 0.191 0.145

506 103.64517362-11-3 I11 3-Ethylnonane 0.072 0.073 0.041

507 103.731 ? Unidentified 0.021 0.020 0.012

508 103.854 ? Unidentified 0.058 0.054 0.033

509 104.061 ? Unidentified 0.012 0.011 0.007

510 104.246 I11 C11-Isoparaffin2 0.169 0.159 0.096

511 104.404 141-93-5 Q10 1,3-Diethylbenzene 0.135 0.118 0.089

512 104.691 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 0.473 0.414 0.310

513 104.888 ? Unidentified 0.011 0.011 0.006

514 105.045 105-05-5 Q10 1,4-Diethylbenzene 0.193 0.169 0.127

515 105.308 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.221 0.189 0.145

516 105.495 ? Unidentified 0.016 0.015 0.009

517 105.601 135-01-3 Q10 1,2-Diethylbenzene 0.043 0.037 0.028

518 105.906 ? Unidentified 0.039 0.037 0.022

519 106.097 493-02-7 D10 t-Decahydronaphthalene 0.067 0.063 0.038

520 106.180 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.046 0.040 0.030

521 106.397 I11 C11-Isoparaffin3 0.119 0.122 0.067

522 106.566 ? Unidentified 0.088 0.090 0.050

523 106.694 I11 C11-Isoparaffin4 0.104 0.106 0.059

524 106.830 I11 I38 0.021 0.022 0.012

525 107.027 I11 C11-Isoparaffin5 0.101 0.103 0.057

526 107.132 1758-88-9 Q10 1,4,Dimethyl-2-ethylbenzene 0.100 0.086 0.066

527 107.298 874-41-9 Q10 1,3-Dimethyl-4-ethylbenzene 0.150 0.129 0.098

528 107.629 ? Unidentified 0.084 0.086 0.048

C-396
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 13

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol

529 107.872 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.129 0.111 0.085

530 108.121 I11 I41 0.014 0.014 0.008

531 108.264 I11 I42 0.015 0.015 0.008

532 108.522 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.095 0.080 0.062

533 108.964 ? Unidentified 0.020 0.017 0.013

534 109.160 Q11 4M-1tC4Benz 0.004 0.003 0.002

535 109.320 ? Unidentified 0.021 0.018 0.014

536 109.519 Q11 1-Methyl-4-t-butylbenzene 0.014 0.013 0.008

537 109.715 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.027 0.023 0.018

538 109.899 ? Unidentified 0.007 0.006 0.004

539 110.227 1120-21-4 P11 n-Undecane 0.260 0.263 0.146

540 110.402 95-93-2 Q10 1,2,4,5-Tetramethylbenzene 0.019 0.016 0.013

541 110.572 ? Unidentified 0.017 0.014 0.011

542 110.745 ? Unidentified 0.002 0.002 0.001

543 110.884 Q11 1-Methyl-1-n-butylbenzene 0.015 0.012 0.009

544 111.038 ? Unidentified 0.006 0.005 0.003

545 111.184 1074-92-6 Q11 1-t-Butyl-2-methylbenzene 0.014 0.012 0.008

546 111.350 ? Unidentified 0.006 0.005 0.004

547 111.524 ? Unidentified 0.014 0.012 0.008

548 111.688 ? Unidentified 0.008 0.007 0.005

549 111.859 ? Unidentified 0.011 0.010 0.007

550 111.951 ? Unidentified 0.013 0.011 0.007

551 112.082 ? Unidentified 0.005 0.004 0.003

552 112.247 ? Unidentified 0.006 0.005 0.003

553 112.453 ? Unidentified 0.015 0.013 0.008

554 112.794 874-35-1 H10 5-Methylindan 0.026 0.022 0.017

555 113.018 Q11 C11-Aromatic2 0.011 0.010 0.007

556 113.272 ? Unidentified 0.007 0.006 0.004

557 113.377 Q11 C11-Aromatic3 0.006 0.005 0.003

558 113.458 ? Unidentified 0.014 0.012 0.007

559 113.682 824-22-6 H10 4-Methylindan 0.009 0.008 0.006

560 113.828 ? Unidentified 0.001 0.001 0.001

561 113.948 ? Unidentified 0.005 0.004 0.003

562 114.041 824-63-5 H10 2-Methylindan 0.008 0.007 0.005

563 114.239 ? Unidentified 0.010 0.008 0.005

564 114.442 ? Unidentified 0.007 0.006 0.004

565 114.684 ? Unidentified 0.008 0.008 0.004

566 114.783 M12 1t-M-2-(4-MP)cyclopentane 0.003 0.003 0.002

567 114.887 ? Unidentified 0.006 0.006 0.003

568 115.052 I12 I46 0.011 0.011 0.006

569 115.158 Q11 1-Methyl-2-n-butylbenzene 0.014 0.012 0.008

570 115.347 100-18-5 Q12 1,4-Di-i-propylbenzene 0.006 0.005 0.003

571 115.489 I12 I48 0.015 0.015 0.008

572 115.644 ? Unidentified 0.067 0.068 0.035

C-397
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 14

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol

573 115.845 119-64-2 G10 1,2,3,4-Tetrahydronaphthalene 0.035 0.027 0.023

574 116.035 ? Unidentified 0.011 0.008 0.007

575 116.300 A12 A6 0.011 0.009 0.006

576 116.421 91-20-3 G10 Naphthalene 0.017 0.012 0.011

577 116.558 ? Unidentified 0.012 0.009 0.008

578 116.758 ? Unidentified 0.010 0.007 0.007

579 116.919 ? Unidentified 0.005 0.005 0.003

580 117.019 ? Unidentified 0.003 0.003 0.002

581 117.129 Q12 1t-Butyl-4-ethylbenzene 0.002 0.001 0.001

582 117.205 ? Unidentified 0.002 0.002 0.001

583 117.366 ? Unidentified 0.005 0.004 0.003

584 117.487 ? Unidentified 0.002 0.002 0.001

585 117.655 ? Unidentified 0.006 0.005 0.003

586 117.913 Q12 1,3-Di-n-propylbenzene 0.012 0.010 0.007

587 118.343 ? Unidentified 0.006 0.005 0.003

588 118.529 ? Unidentified 0.003 0.003 0.001

589 118.769 112-40-3 P12 n-Dodecane 0.042 0.042 0.022

590 118.897 ? Unidentified 0.003 0.003 0.001

591 119.046 ? Unidentified 0.003 0.003 0.001

592 119.292 ? Unidentified 0.002 0.002 0.001

593 119.400 ? Unidentified 0.001 0.001 0.001

594 119.480 ? Unidentified 0.001 0.001 0.000

595 119.628 ? Unidentified 0.002 0.002 0.001

596 119.723 ? Unidentified 0.003 0.002 0.002

597 119.831 ? Unidentified 0.003 0.003 0.002

598 120.066 102-25-0 Q12 1,3,5-Triethylbenzene 0.010 0.008 0.005

599 120.357 ? Unidentified 0.006 0.005 0.003

600 120.564 ? Unidentified 0.002 0.001 0.001

601 120.702 ? Unidentified 0.004 0.003 0.002

602 120.846 877-44-1 Q12 1,2,4-Triethylbenzene 0.003 0.003 0.002

603 120.973 ? Unidentified 0.002 0.002 0.001

604 121.243 ? Unidentified 0.004 0.003 0.002

605 121.372 ? Unidentified 0.001 0.001 0.001

606 121.479 ? Unidentified 0.001 0.001 0.000

607 121.632 ? Unidentified 0.001 0.001 0.001

608 121.827 ? Unidentified 0.001 0.001 0.001

609 121.988 ? Unidentified 0.001 0.000 0.000

610 122.119 Q12 1-Methyl-4-n-pentylbenzene 0.003 0.003 0.002

611 122.317 ? Unidentified 0.001 0.001 0.001

612 122.649 ? Unidentified 0.001 0.001 0.000

613 122.911 ? Unidentified 0.002 0.002 0.001

614 123.060 1077-16-3 Q12 n-Hexylbenzene 0.002 0.002 0.001

615 123.157 ? Unidentified 0.001 0.001 0.001

616 123.399 I13 I49 0.003 0.003 0.001

C-398
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 15

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol

617 123.724 ? Unidentified 0.002 0.002 0.001

618 123.928 ? Unidentified 0.001 0.001 0.001

619 124.126 ? Unidentified 0.001 0.001 0.001

620 124.213 ? Unidentified 0.001 0.001 0.001

621 124.420 700-12-9 Q11 Pentamethylbenzene 0.001 0.001 0.001

622 124.525 ? Unidentified 0.003 0.002 0.002

623 125.179 91-57-6 G11 2-Methylnaphthalene 0.009 0.006 0.005

624 125.363 ? Unidentified 0.003 0.002 0.002

625 125.614 ? Unidentified 0.001 0.001 0.001

626 125.970 90-12-0 G11 1-Methylnaphthalene 0.004 0.003 0.002

627 126.135 629-50-5 P13 n-Tridecane 0.007 0.007 0.003

628 126.291 ? Unidentified 0.002 0.002 0.001

C-399
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 1

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol

Paraffin 9.740 106-97-8 n-Butane 2.633 3.433 3.992

16.754 109-66-0 n-Pentane 0.981 1.182 1.199

33.228 110-54-3 n-Hexane 1.306 1.495 1.336

54.975 142-82-5 n-Heptane 1.606 1.772 1.412

75.307 111-65-9 n-Octane 1.672 1.796 1.290

89.557 111-84-2 n-Nonane 1.267 1.332 0.870

100.726 124-18-5 n-Decane 1.202 1.243 0.745

110.227 1120-21-4 n-Undecane 0.260 0.263 0.146

118.769 112-40-3 n-Dodecane 0.042 0.042 0.022

126.135 629-50-5 n-Tridecane 0.007 0.007 0.003

I-Paraffins 8.696 75-28-5 i-Butane 0.057 0.077 0.086

10.276 463-82-1 2,2-Dimethylpropane 0.015 0.020 0.019

14.140 78-78-4 i-Pentane 6.756 8.227 8.251

21.256 75-83-2 2,2-Dimethylbutane 0.130 0.152 0.133

26.106 79-29-8 2,3-Dimethylbutane 0.483 0.550 0.494

27.126 107-83-5 2-Methylpentane 0.960 1.110 0.982

29.626 96-14-0 3-Methylpentane 0.594 0.675 0.607

39.411 108-08-7 2,4-Dimethylpentane 0.399 0.448 0.351

39.932 464-06-2 2,2,3-Trimethylbutane 0.052 0.057 0.046

44.271 562-49-2 3,3-Dimethylpentane 0.064 0.069 0.056

47.659 591-76-4 2-Methylhexane 1.191 1.325 1.048

49.450 589-34-4 3-Methylhexane 0.669 0.734 0.588

52.072 540-84-1 2,2,4-Trimethylpentane 2.604 2.840 2.009

59.647 590-73-8 2,2-Dimethylhexane 0.082 0.089 0.063

61.657 564-02-3 2,2,3-Trimethylpentane 0.164 0.173 0.126

61.953 592-13-2 2,5-Dimethylhexane 0.445 0.484 0.343

62.274 589-43-5 2,4-Dimethylhexane 0.437 0.471 0.337

63.492 563-16-6 3,3-Dimethylhexane 0.070 0.074 0.054

65.327 565-75-3 2,3,4-Trimethylpentane 1.019 1.070 0.786

67.812 584-94-1 2,3-Dimethylhexane 0.419 0.443 0.323

69.195 592-27-8 2-Methylheptane 0.749 0.810 0.578

69.436 589-53-7 4-Methylheptane 0.347 0.371 0.268

69.769 583-48-2 3,4-Dimethylhexane 0.027 0.028 0.021

70.549 589-81-1 3-Methylheptane 0.635 0.679 0.490

70.655 619-99-8 3-Ethylhexane 0.346 0.366 0.267

72.504 3522-94-9 2,2,5-Trimethylhexane 0.437 0.467 0.301

79.575 1071-26-7 2,2-Dimethylheptane 0.532 0.565 0.365

80.02316747-25-4 2,2,3-Trimethylhexane 0.354 0.374 0.243

80.393 1068-19-5 4,4-Dimethylheptane 0.289 0.304 0.198

81.148 4032-86-4 3,3-Dimethylheptane 0.132 0.137 0.091

81.647 3074-75-7 2-Methyl-4-ethylhexane 0.062 0.065 0.043

84.110 3074-71-3 2,3-Dimethylheptane 0.059 0.062 0.041

84.538 1067-20-5 3,3-Diethylpentane 0.132 0.132 0.091

84.971 2216-34-4 4-Methyloctane 0.354 0.371 0.243

85.115 3221-61-2 2-Methyloctane 0.467 0.494 0.321

85.981 2216-33-3 3-Methyloctane 0.485 0.508 0.333

87.831 C9-Isoparaffin1 0.189 0.196 0.130

C-400
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 2

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol

I-Paraffins 91.84215869-87-1 2,2-Dimethyloctane 0.137 0.143 0.085

92.117 4032-94-4 2,4-Dimethyloctane 0.037 0.039 0.023

92.522 2051-30-1 2,6-Dimethyloctane 0.076 0.078 0.047

92.69115869-89-3 2,5-Dimethyloctane 0.108 0.112 0.067

93.173 I12 0.088 0.091 0.054

93.728 4110-44-5 3,3-Dimethyloctane 0.233 0.238 0.144

93.854 I14 0.055 0.057 0.034

94.57652896-90-9 3-Methyl-5-ethylheptane 0.065 0.068 0.040

96.59115869-85-9 5-Methylnonane 0.166 0.171 0.103

96.78717301-94-8 4-Methylnonane 0.297 0.306 0.184

96.948 871-83-0 2-Methylnonane 0.751 0.780 0.465

97.431 5881-17-4 3-Ethyloctane 0.084 0.086 0.052

97.764 5911-04-6 3-Methylnonane 0.394 0.405 0.244

98.314 C10-Isoparaffin1 0.163 0.167 0.101

98.569 I19 0.116 0.118 0.072

99.232 I21 0.090 0.092 0.056

99.464 C10-Isoparaffin2 0.026 0.026 0.016

101.039 I26 0.278 0.283 0.157

103.64517362-11-3 3-Ethylnonane 0.072 0.073 0.041

104.246 C11-Isoparaffin2 0.169 0.159 0.096

106.397 C11-Isoparaffin3 0.119 0.122 0.067

106.694 C11-Isoparaffin4 0.104 0.106 0.059

106.830 I38 0.021 0.022 0.012

107.027 C11-Isoparaffin5 0.101 0.103 0.057

108.121 I41 0.014 0.014 0.008

108.264 I42 0.015 0.015 0.008

115.052 I46 0.011 0.011 0.006

115.489 I48 0.015 0.015 0.008

123.399 I49 0.003 0.003 0.001

Aromatics 116.300 A6 0.011 0.009 0.006

Mono-Aromatics 42.702 71-42-3 Benzene 0.656 0.563 0.740

66.046 108-88-3 Toluene 8.665 7.541 8.287

82.282 100-41-4 Ethylbenzene 1.440 1.253 1.195

83.617 108-38-3 m-Xylene 4.534 3.958 3.763

83.749 106-42-3 p-Xylene 1.903 1.668 1.580

86.573 95-47-6 o-Xylene 1.403 1.202 1.164

90.797 98-82-8 i-Propylbenzene 0.176 0.154 0.129

94.303 103-65-1 n-Propylbenzene 0.681 0.596 0.499

95.216 620-14-4 1-Methyl-3-ethylbenzene 2.163 1.888 1.586

95.437 622-96-8 1-Methyl-4-ethylbenzene 1.256 1.101 0.921

96.066 108-67-8 1,3,5-Trimethylbenzene 1.277 1.113 0.936

97.111 611-14-3 1-Methyl-2-ethylbenzene 1.137 0.974 0.834

98.815 95-63-6 1,2,4-Trimethylbenzene 2.674 2.304 1.961

100.502 135-98-8 sec-Butylbenzene 0.064 0.056 0.042

101.647 526-73-8 1,2,3-Trimethylbenzene 1.307 1.102 0.958

102.054 535-77-3 1-Methyl-3-i-propylbenzene 0.069 0.060 0.045

C-401
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 3

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol

Mono-Aromatics 102.500 99-87-6 1-Methyl-4-i-propylbenzene 0.057 0.050 0.038

104.404 141-93-5 1,3-Diethylbenzene 0.135 0.118 0.089

104.691 1074-43-7 1-Methyl-3-n-propylbenzene 0.473 0.414 0.310

105.045 105-05-5 1,4-Diethylbenzene 0.193 0.169 0.127

105.308 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.221 0.189 0.145

105.601 135-01-3 1,2-Diethylbenzene 0.043 0.037 0.028

106.180 1074-17-5 1-Methyl-2-n-propylbenzene 0.046 0.040 0.030

107.132 1758-88-9 1,4,Dimethyl-2-ethylbenzene 0.100 0.086 0.066

107.298 874-41-9 1,3-Dimethyl-4-ethylbenzene 0.150 0.129 0.098

107.872 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.129 0.111 0.085

108.522 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.095 0.080 0.062

109.160 4M-1tC4Benz 0.004 0.003 0.002

109.519 1-Methyl-4-t-butylbenzene 0.014 0.013 0.008

109.715 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.027 0.023 0.018

110.402 95-93-2 1,2,4,5-Tetramethylbenzene 0.019 0.016 0.013

110.884 1-Methyl-1-n-butylbenzene 0.015 0.012 0.009

111.184 1074-92-6 1-t-Butyl-2-methylbenzene 0.014 0.012 0.008

113.018 C11-Aromatic2 0.011 0.010 0.007

113.377 C11-Aromatic3 0.006 0.005 0.003

115.158 1-Methyl-2-n-butylbenzene 0.014 0.012 0.008

115.347 100-18-5 1,4-Di-i-propylbenzene 0.006 0.005 0.003

117.129 1t-Butyl-4-ethylbenzene 0.002 0.001 0.001

117.913 1,3-Di-n-propylbenzene 0.012 0.010 0.007

120.066 102-25-0 1,3,5-Triethylbenzene 0.010 0.008 0.005

120.846 877-44-1 1,2,4-Triethylbenzene 0.003 0.003 0.002

122.119 1-Methyl-4-n-pentylbenzene 0.003 0.003 0.002

123.060 1077-16-3 n-Hexylbenzene 0.002 0.002 0.001

124.420 700-12-9 Pentamethylbenzene 0.001 0.001 0.001

Naphthalenes 115.845 119-64-2 1,2,3,4-Tetrahydronaphthalene 0.035 0.027 0.023

116.421 91-20-3 Naphthalene 0.017 0.012 0.011

125.179 91-57-6 2-Methylnaphthalene 0.009 0.006 0.005

125.970 90-12-0 1-Methylnaphthalene 0.004 0.003 0.002

Naphtheno/Olefin 112.794 874-35-1 5-Methylindan 0.026 0.022 0.017

113.682 824-22-6 4-Methylindan 0.009 0.008 0.006

114.041 824-63-5 2-Methylindan 0.008 0.007 0.005

Indenes 102.779 496-11-7 2,3-Dihydroindene 0.445 0.348 0.332

Naphthenes 78.115 N3 0.005 0.004 0.004

85.395 N15 0.075 0.073 0.053

87.385 N18 0.054 0.052 0.038

91.481 N26 0.047 0.044 0.032

92.008 N28 0.026 0.025 0.018

93.528 N30 0.006 0.006 0.004

101.415 N39 0.049 0.046 0.028

Mono-Naphthene 25.419 287-92-3 Cyclopentane 0.122 0.123 0.153

C-402
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 4

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol

Mono-Naphthene 37.861 96-37-7 Methylcyclopentane 0.869 0.875 0.909

44.537 110-82-7 Cyclohexane 1.212 1.175 1.269

50.241 2532-58-3 1c,3-Dimethylcyclopentane 0.180 0.183 0.162

50.810 1759-58-6 1t,3-Dimethylcyclopentane 0.168 0.170 0.151

51.414 822-50-4 1t,2-Dimethylcyclopentane 0.270 0.271 0.242

58.291 108-87-2 Methylcyclohexane 2.757 2.704 2.474

58.636 1192-18-3 1c,2-Dimethylcyclopentane 0.015 0.015 0.013

59.192 4516-69-2 1,1,3-Trimethylcyclopentane 0.093 0.094 0.073

63.059 4850-28-6 1c,2t,4-Trimethylcyclopentane 0.099 0.098 0.078

70.289 638-04-0 1c,3-Dimethylcyclohexane 0.610 0.604 0.479

71.233 1c,2t,3-Trimethylcyclopentane 0.005 0.005 0.004

72.795 3c-Ethylmethylcyclopentane 0.047 0.046 0.037

73.020 3t-Ethylmethylcyclopentane 0.061 0.060 0.048

73.285 111-66-0 2t-Ethylmethylcyclopentane 0.022 0.022 0.017

73.70916747-50-5 1,1-Methylethylcyclopentane 0.311 0.300 0.244

74.360 2207-03-6 1t,3-Dimethylcyclohexane 0.005 0.005 0.004

75.004 1c,2c,3-Trimethylcyclopentane 0.196 0.190 0.154

79.022 2207-01-4 1c,2-Dimethylcyclohexane 0.132 0.125 0.103

80.745 1678-91-7 Ethylcyclohexane 0.096 0.092 0.075

80.975 1795-27-3 1c,3c,5-Trimethylcyclohexane 0.317 0.311 0.222

82.644 7667-60-9 1c,2t,4t-Trimethylcyclohexane 0.188 0.182 0.131

85.791 1c,2t,4c-Trimethylcyclohexane 0.124 0.121 0.087

91.610 696-29-7 i-Propylcyclohexane 0.085 0.080 0.059

93.275 2040-95-1 n-Butylcyclopentane 0.110 0.106 0.077

99.036 1678-98-4 i-Butylcyclohexane 0.127 0.120 0.080

100.014 1t-Methyl-2-n-propylcyclohexanR 0.011 0.010 0.007

103.149 7058-01-7 sec-Butylcyclohexane 0.161 0.149 0.101

114.783 1t-M-2-(4-MP)cyclopentane 0.003 0.003 0.002

Di/Bicyclo-Naphth106.097 493-02-7 t-Decahydronaphthalene 0.067 0.063 0.038

Olefins 35.759 O14 0.001 0.001 0.001

54.627 C7-Olefin2 0.002 0.003 0.002

60.387 O35 0.002 0.002 0.002

63.811 O38 0.007 0.007 0.006

64.635 C8-Olefin2 0.090 0.093 0.081

68.350 C8-Olefin3 0.041 0.042 0.032

76.160 C9-Olefin1 0.032 0.033 0.025

76.552 C9-Olefin2 0.012 0.012 0.008

87.033 C9-Olefin4 0.115 0.121 0.081

n-Olefins 10.159 624-64-6 t-Butene-2 0.001 0.001 0.001

10.798 590-18-1 c-Butene-2 0.001 0.001 0.001

15.546 109-67-1 Pentene-1 0.019 0.022 0.024

17.768 646-04-8 t-Pentene-2 0.009 0.010 0.011

18.703 627-20-3 c-Pentene-2 0.007 0.008 0.009

31.005 592-41-6 Hexene-1 2.717 3.024 2.845

33.85613269-52-8 t-Hexene-3 0.005 0.006 0.005

C-403
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 5

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol

n-Olefins 34.319 4050-45-7 t-Hexene-2 0.007 0.007 0.007

36.080 7688-21-3 c-Hexene-2 0.004 0.004 0.004

54.22414686-14-7 t-Heptene-3 0.001 0.001 0.001

56.09814686-13-6 t-Heptene-2 0.003 0.003 0.002

57.729 6443-92-1 c-Heptene-2 0.006 0.006 0.005

73.47614850-23-8 t-Octene-4 0.012 0.013 0.010

74.70614919-01-8 t-Octene-3 0.015 0.016 0.012

75.91213389-42-9 t-Octene-2 0.005 0.005 0.004

77.222 7642-04-8 c-Octene-2 0.023 0.024 0.018

88.174 124-11-8 Nonene-1 0.022 0.024 0.015

89.09220237-46-0 c-Nonene-3 0.041 0.046 0.029

89.923 6434-78-2 t-Nonene-2 0.120 0.116 0.084

91.213 6434-77-1 c-Nonene-2 0.077 0.074 0.054

99.828 872-05-9 Decene-1 0.010 0.010 0.006

Iso-Olefins 16.301 563-46-2 2-Methylbutene-1 0.012 0.014 0.015

19.312 513-35-9 2-Methylbutene-2 0.010 0.011 0.012

24.896 691-37-2 4-Methylpentene-1 0.004 0.005 0.004

26.870 691-38-3 4-Methyl-c-pentene-2 0.001 0.001 0.001

27.558 674-76-0 4-Methyl-t-pentene-2 0.004 0.004 0.004

34.792 625-27-4 2-Methylpentene-2 0.004 0.004 0.004

35.183 922-62-3 3-Methyl-c-pentene-2 0.010 0.011 0.010

37.372 3404-73-7 3,3-Dimethylpentene-1 0.007 0.007 0.006

39.680 594-56-9 2,3,3-Trimethylbutene-1 0.001 0.001 0.001

40.640 7385-78-6 3,4-Dimethylpentene-1 0.001 0.001 0.000

41.586 762-63-0 4,4-Dimethyl-c-pentene-2 0.001 0.001 0.001

43.765 2-Methyl-c-hexene-3 0.001 0.001 0.001

45.121 692-24-0 2-Methyl-t-hexene-3 0.003 0.003 0.002

46.305 7357-93-9 2-Ethyl-3-methylbutene-1 0.001 0.001 0.001

46.670 3769-23-1 4-Methylhexene-1 0.001 0.001 0.001

47.295 3404-55-5 4-Methyl-t/c-hexene-2 0.002 0.002 0.001

51.100 2-Ethylpentene-1 0.001 0.001 0.001

53.725 4914-89-0 3-Methyl-c-hexene-3 0.002 0.002 0.002

55.475 2738-19-4 2-Methyl-2-hexene 0.004 0.005 0.004

56.242 816-79-5 3-Ethylpentene-2 0.002 0.002 0.001

77.787 2,3,3-Trimethylhexene-1 0.092 0.102 0.065

79.83519550-75-6 t-2,2-Dimethylheptene-3 0.062 0.069 0.044

82.897 4588-18-5 2-Methyloctene-1 0.032 0.036 0.022

88.85820063-92-8 t-7-Methyloctene-3 0.013 0.015 0.009

90.280 4984-01-4 3,7-Dimethyloctene-1 0.059 0.064 0.037

100.14819781-18-0 2,3-Dimethyloctene-2 0.131 0.134 0.082

Naphtheno-Olefin 23.704 142-29-0 Cyclopentene 0.004 0.004 0.005

48.071 110-83-8 Cyclohexene 0.003 0.003 0.003

Di-Olefins 17.219 78-79-5 2-Methyl-1,3-Butadiene 0.004 0.005 0.005

18.397 598-25-4 3-Methylbutadiene-1,2 0.002 0.002 0.002

19.630 2004-70-8 1t,3-Pentadiene 0.002 0.003 0.003

C-404
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 6

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol

Di-Olefins 20.855 1574-41-0 1c,3-Pentadiene 0.001 0.001 0.001

38.685 563-79-1 2,3-Dimethyl-2-Butene 0.001 0.001 0.001

42.502 Diolefin 0.001 0.001 0.001

67.435 C8-Diolefin4 0.067 0.069 0.060

71.547 1002-33-1 1,3-Octadiene 0.136 0.134 0.108

Oxygenates 12.708 64-17-5 Ethanol 12.079 11.551 23.104

19.147 75-65-0 t-Butanol 0.001 0.001 0.001

26.524 1634-04-4 Methyl-t-butylether 0.005 0.005 0.005

45.599 71-36-3 n-Butanol 0.001 0.001 0.001

48.517 994-05-8 TAME 0.001 0.001 0.001

Unidentified 7.612 Unidentified 0.002 0.003 0.004

14.734 Unidentified 0.004 0.005 0.007

14.814 Unidentified 0.002 0.002 0.003

14.853 Unidentified 0.003 0.004 0.004

14.910 Unidentified 0.016 0.019 0.020

15.238 Unidentified 0.001 0.001 0.001

15.258 Unidentified 0.001 0.002 0.002

15.286 Unidentified 0.007 0.009 0.009

15.818 Unidentified 0.002 0.002 0.003

15.878 Unidentified 0.004 0.004 0.006

15.989 Unidentified 0.001 0.001 0.001

16.008 Unidentified 0.004 0.003 0.005

16.115 Unidentified 0.001 0.001 0.002

16.144 Unidentified 0.001 0.001 0.002

16.185 Unidentified 0.001 0.001 0.001

16.482 Unidentified 0.001 0.002 0.002

16.524 Unidentified 0.004 0.004 0.005

17.318 Unidentified 0.001 0.001 0.001

17.351 Unidentified 0.002 0.002 0.003

17.452 Unidentified 0.002 0.002 0.002

17.503 Unidentified 0.001 0.001 0.001

17.537 Unidentified 0.000 0.001 0.001

17.562 Unidentified 0.001 0.001 0.001

17.589 Unidentified 0.001 0.002 0.002

17.635 Unidentified 0.001 0.001 0.001

17.907 Unidentified 0.001 0.002 0.002

17.968 Unidentified 0.002 0.002 0.002

18.037 Unidentified 0.001 0.001 0.001

18.064 Unidentified 0.002 0.002 0.003

18.190 Unidentified 0.002 0.002 0.002

18.235 Unidentified 0.001 0.001 0.001

18.257 Unidentified 0.001 0.001 0.001

18.313 Unidentified 0.001 0.001 0.001

18.333 Unidentified 0.001 0.001 0.001

18.463 Unidentified 0.001 0.001 0.002

18.494 Unidentified 0.001 0.001 0.001

C-405
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 7

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol

Unidentified 18.538 Unidentified 0.001 0.001 0.001

18.578 Unidentified 0.001 0.001 0.001

18.850 Unidentified 0.001 0.001 0.001

18.950 Unidentified 0.004 0.003 0.004

19.063 Unidentified 0.001 0.001 0.001

19.102 Unidentified 0.001 0.001 0.001

19.186 Unidentified 0.001 0.001 0.001

19.480 Unidentified 0.001 0.002 0.002

19.561 Unidentified 0.001 0.001 0.001

19.685 Unidentified 0.001 0.001 0.001

19.743 Unidentified 0.002 0.002 0.002

19.795 Unidentified 0.001 0.001 0.001

19.830 Unidentified 0.000 0.000 0.001

19.893 Unidentified 0.001 0.001 0.002

19.939 Unidentified 0.001 0.001 0.001

19.975 Unidentified 0.001 0.001 0.001

20.078 Unidentified 0.003 0.003 0.003

20.161 Unidentified 0.001 0.001 0.001

20.230 Unidentified 0.001 0.001 0.001

20.283 Unidentified 0.001 0.001 0.001

20.307 Unidentified 0.000 0.001 0.001

20.341 Unidentified 0.001 0.001 0.001

20.398 Unidentified 0.001 0.001 0.001

20.564 Unidentified 0.003 0.004 0.004

20.647 Unidentified 0.001 0.001 0.001

20.756 Unidentified 0.003 0.003 0.004

20.922 Unidentified 0.001 0.001 0.001

20.947 Unidentified 0.000 0.001 0.001

21.020 Unidentified 0.001 0.001 0.001

21.062 Unidentified 0.001 0.001 0.001

21.092 Unidentified 0.001 0.001 0.001

21.447 Unidentified 0.002 0.002 0.002

21.559 Unidentified 0.002 0.002 0.002

21.694 Unidentified 0.001 0.001 0.001

21.722 Unidentified 0.000 0.001 0.000

21.750 Unidentified 0.001 0.001 0.001

21.837 Unidentified 0.001 0.001 0.001

21.867 Unidentified 0.001 0.001 0.001

21.981 Unidentified 0.001 0.002 0.002

22.004 Unidentified 0.001 0.001 0.001

22.082 Unidentified 0.001 0.001 0.001

22.122 Unidentified 0.000 0.000 0.000

22.186 Unidentified 0.002 0.002 0.002

22.281 Unidentified 0.001 0.001 0.001

22.330 Unidentified 0.001 0.001 0.001

22.440 Unidentified 0.001 0.001 0.001

22.541 Unidentified 0.001 0.001 0.002

22.592 Unidentified 0.001 0.001 0.001

C-406
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 8

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol

Unidentified 22.664 Unidentified 0.001 0.001 0.002

22.698 Unidentified 0.000 0.000 0.001

22.784 Unidentified 0.001 0.001 0.002

22.825 Unidentified 0.000 0.000 0.001

22.866 Unidentified 0.000 0.000 0.001

22.931 Unidentified 0.001 0.001 0.002

23.035 Unidentified 0.001 0.001 0.001

23.107 Unidentified 0.000 0.000 0.001

23.160 Unidentified 0.001 0.001 0.001

23.203 Unidentified 0.001 0.001 0.001

23.304 Unidentified 0.002 0.002 0.002

23.412 Unidentified 0.000 0.000 0.001

23.468 Unidentified 0.002 0.002 0.002

23.566 Unidentified 0.001 0.001 0.001

23.871 Unidentified 0.002 0.002 0.002

24.010 Unidentified 0.001 0.001 0.001

24.040 Unidentified 0.001 0.001 0.001

24.118 Unidentified 0.001 0.001 0.001

24.165 Unidentified 0.001 0.001 0.001

24.205 Unidentified 0.001 0.001 0.001

24.299 Unidentified 0.001 0.001 0.001

24.327 Unidentified 0.001 0.001 0.001

24.428 Unidentified 0.001 0.001 0.001

24.509 Unidentified 0.000 0.001 0.001

24.577 Unidentified 0.001 0.001 0.001

24.608 Unidentified 0.001 0.001 0.001

24.794 Unidentified 0.001 0.002 0.002

25.015 Unidentified 0.001 0.001 0.001

25.133 Unidentified 0.001 0.001 0.002

25.161 Unidentified 0.001 0.001 0.001

25.193 Unidentified 0.000 0.000 0.001

25.244 Unidentified 0.001 0.001 0.001

25.626 Unidentified 0.001 0.001 0.001

25.696 Unidentified 0.001 0.001 0.001

25.728 Unidentified 0.001 0.001 0.001

25.782 Unidentified 0.001 0.001 0.001

25.853 Unidentified 0.000 0.001 0.000

26.351 Unidentified 0.002 0.002 0.002

26.653 Unidentified 0.001 0.001 0.001

26.735 Unidentified 0.001 0.001 0.001

26.798 Unidentified 0.001 0.001 0.001

26.819 Unidentified 0.001 0.001 0.001

27.702 Unidentified 0.000 0.000 0.000

27.727 Unidentified 0.000 0.000 0.000

27.753 Unidentified 0.000 0.000 0.000

27.839 Unidentified 0.001 0.001 0.001

27.908 Unidentified 0.001 0.001 0.001

28.007 Unidentified 0.000 0.000 0.000

C-407
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 9

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol

Unidentified 28.062 Unidentified 0.001 0.001 0.001

28.141 Unidentified 0.000 0.001 0.000

28.229 Unidentified 0.000 0.001 0.000

28.332 Unidentified 0.000 0.000 0.000

28.358 Unidentified 0.001 0.001 0.001

28.502 Unidentified 0.001 0.002 0.001

28.558 Unidentified 0.000 0.001 0.000

28.619 Unidentified 0.000 0.000 0.000

28.652 Unidentified 0.001 0.001 0.001

28.729 Unidentified 0.000 0.001 0.000

28.784 Unidentified 0.000 0.001 0.000

28.812 Unidentified 0.000 0.000 0.000

28.896 Unidentified 0.001 0.002 0.001

29.124 Unidentified 0.001 0.001 0.001

29.155 Unidentified 0.000 0.001 0.000

29.252 Unidentified 0.000 0.000 0.000

29.307 Unidentified 0.001 0.001 0.001

29.371 Unidentified 0.001 0.001 0.001

29.945 Unidentified 0.000 0.001 0.000

30.037 Unidentified 0.000 0.000 0.000

30.064 Unidentified 0.000 0.000 0.000

30.127 Unidentified 0.001 0.001 0.001

30.207 Unidentified 0.001 0.001 0.001

30.389 Unidentified 0.001 0.001 0.001

30.594 Unidentified 0.000 0.000 0.000

31.678 Unidentified 0.001 0.001 0.001

31.721 Unidentified 0.001 0.001 0.001

31.795 Unidentified 0.002 0.002 0.002

31.939 Unidentified 0.001 0.001 0.001

32.053 Unidentified 0.001 0.001 0.001

32.072 Unidentified 0.000 0.000 0.001

32.174 Unidentified 0.001 0.001 0.001

32.211 Unidentified 0.001 0.001 0.001

32.321 Unidentified 0.000 0.000 0.001

32.349 Unidentified 0.001 0.001 0.001

32.463 Unidentified 0.000 0.000 0.001

32.544 Unidentified 0.000 0.000 0.001

32.601 Unidentified 0.001 0.000 0.001

32.693 Unidentified 0.000 0.000 0.000

32.747 Unidentified 0.001 0.001 0.001

32.832 Unidentified 0.001 0.001 0.001

32.880 Unidentified 0.000 0.001 0.000

32.921 Unidentified 0.000 0.000 0.000

33.634 Unidentified 0.001 0.002 0.001

34.045 Unidentified 0.000 0.000 0.000

34.072 Unidentified 0.000 0.001 0.000

34.121 Unidentified 0.000 0.000 0.000

34.523 Unidentified 0.001 0.001 0.001

C-408
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 10

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol

Unidentified 34.935 Unidentified 0.001 0.001 0.001

35.395 Unidentified 0.000 0.000 0.000

35.441 Unidentified 0.001 0.001 0.001

35.554 Unidentified 0.001 0.001 0.001

35.605 Unidentified 0.000 0.001 0.001

35.881 Unidentified 0.000 0.000 0.000

36.248 Unidentified 0.001 0.001 0.001

36.512 Unidentified 0.000 0.000 0.000

36.589 Unidentified 0.001 0.001 0.001

36.677 Unidentified 0.001 0.001 0.001

36.811 Unidentified 0.000 0.000 0.000

37.098 Unidentified 0.001 0.001 0.001

37.130 Unidentified 0.000 0.001 0.000

37.188 Unidentified 0.000 0.000 0.000

38.223 Unidentified 0.000 0.000 0.001

38.383 Unidentified 0.001 0.001 0.001

38.580 Unidentified 0.001 0.001 0.001

38.633 Unidentified 0.000 0.001 0.001

38.812 Unidentified 0.000 0.000 0.000

38.871 Unidentified 0.000 0.000 0.000

39.033 Unidentified 0.001 0.001 0.001

39.091 Unidentified 0.001 0.001 0.001

39.171 Unidentified 0.001 0.001 0.001

40.226 Unidentified 0.001 0.001 0.001

40.416 Unidentified 0.000 0.000 0.000

40.569 Unidentified 0.001 0.001 0.001

40.708 Unidentified 0.000 0.000 0.000

40.824 Unidentified 0.000 0.001 0.000

40.860 Unidentified 0.000 0.000 0.000

41.012 Unidentified 0.001 0.001 0.001

41.068 Unidentified 0.001 0.002 0.001

41.384 Unidentified 0.001 0.001 0.001

41.476 Unidentified 0.001 0.001 0.000

41.710 Unidentified 0.001 0.001 0.001

41.895 Unidentified 0.001 0.001 0.000

41.985 Unidentified 0.001 0.001 0.001

42.090 Unidentified 0.001 0.001 0.000

42.251 Unidentified 0.001 0.001 0.001

43.291 Unidentified 0.001 0.001 0.001

43.380 Unidentified 0.001 0.001 0.000

43.481 Unidentified 0.001 0.001 0.001

43.693 Unidentified 0.000 0.000 0.000

43.848 Unidentified 0.001 0.001 0.000

45.278 Unidentified 0.001 0.001 0.001

45.410 Unidentified 0.000 0.000 0.000

45.814 Unidentified 0.001 0.001 0.001

45.950 Unidentified 0.000 0.000 0.001

46.054 Unidentified 0.001 0.001 0.001

C-409
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 11

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol

Unidentified 46.824 Unidentified 0.001 0.001 0.001

48.278 Unidentified 0.000 0.000 0.001

48.344 Unidentified 0.001 0.001 0.001

48.799 Unidentified 0.001 0.001 0.001

48.889 Unidentified 0.000 0.000 0.000

49.024 Unidentified 0.001 0.001 0.001

49.135 Unidentified 0.001 0.001 0.000

49.925 Unidentified 0.001 0.001 0.001

50.596 Unidentified 0.001 0.001 0.001

51.163 Unidentified 0.001 0.001 0.001

51.611 Unidentified 0.041 0.041 0.037

53.029 Unidentified 0.001 0.001 0.001

53.088 Unidentified 0.001 0.001 0.001

53.164 Unidentified 0.001 0.001 0.000

53.234 Unidentified 0.001 0.001 0.001

53.348 Unidentified 0.000 0.001 0.000

53.394 Unidentified 0.001 0.001 0.001

53.596 Unidentified 0.000 0.000 0.000

53.959 Unidentified 0.001 0.001 0.001

54.189 Unidentified 0.002 0.002 0.002

54.359 Unidentified 0.001 0.001 0.001

54.527 Unidentified 0.002 0.002 0.002

55.412 Unidentified 0.001 0.001 0.001

55.618 Unidentified 0.005 0.005 0.004

55.974 Unidentified 0.001 0.001 0.001

56.031 Unidentified 0.001 0.001 0.000

56.743 Unidentified 2.386 2.504 2.141

57.363 Unidentified 0.007 0.007 0.006

57.595 Unidentified 0.001 0.001 0.000

59.889 Unidentified 0.001 0.001 0.001

60.031 Unidentified 0.005 0.004 0.003

60.174 Unidentified 0.001 0.001 0.001

60.239 Unidentified 0.001 0.002 0.001

60.317 Unidentified 0.001 0.002 0.001

60.521 Unidentified 0.003 0.003 0.002

60.867 Unidentified 0.747 0.769 0.670

62.520 Unidentified 0.010 0.010 0.009

63.980 Unidentified 0.002 0.002 0.002

64.208 Unidentified 0.004 0.004 0.003

64.362 Unidentified 0.004 0.004 0.003

67.115 Unidentified 0.019 0.019 0.017

71.724 Unidentified 0.016 0.016 0.013

71.988 Unidentified 0.007 0.007 0.005

76.279 Unidentified 0.014 0.015 0.010

76.884 Unidentified 0.009 0.010 0.006

77.482 Unidentified 0.003 0.003 0.002

77.581 Unidentified 0.003 0.003 0.002

78.392 Unidentified 0.070 0.073 0.048

C-410
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 12

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol

Unidentified 78.713 Unidentified 0.060 0.062 0.041

79.221 Unidentified 0.018 0.018 0.015

81.408 Unidentified 0.046 0.051 0.032

81.990 Unidentified 0.014 0.013 0.010

82.435 Unidentified 0.038 0.036 0.026

83.210 Unidentified 0.054 0.060 0.038

83.862 Unidentified 0.173 0.151 0.143

84.230 Unidentified 0.099 0.103 0.068

86.194 Unidentified 0.011 0.012 0.008

86.388 Unidentified 0.072 0.074 0.049

86.779 Unidentified 0.040 0.038 0.028

87.527 Unidentified 0.161 0.156 0.112

88.361 Unidentified 0.024 0.024 0.017

88.536 Unidentified 0.018 0.018 0.013

89.269 Unidentified 0.007 0.007 0.005

90.479 Unidentified 0.013 0.012 0.009

91.015 Unidentified 0.014 0.013 0.009

92.276 Unidentified 0.009 0.009 0.006

92.758 Unidentified 0.139 0.144 0.086

92.925 Unidentified 0.024 0.025 0.015

94.069 Unidentified 0.051 0.052 0.031

94.744 Unidentified 0.009 0.009 0.005

94.874 Unidentified 0.013 0.012 0.008

94.995 Unidentified 0.017 0.016 0.011

95.653 Unidentified 0.013 0.012 0.010

95.782 Unidentified 0.005 0.005 0.003

96.285 Unidentified 0.022 0.023 0.014

96.422 Unidentified 0.031 0.032 0.019

97.981 Unidentified 0.023 0.022 0.014

98.206 Unidentified 0.080 0.087 0.051

98.921 Unidentified 0.079 0.081 0.049

99.143 Unidentified 0.058 0.059 0.036

99.363 Unidentified 0.016 0.016 0.010

99.560 Unidentified 0.017 0.017 0.010

99.692 Unidentified 0.020 0.020 0.012

99.904 Unidentified 0.007 0.007 0.004

100.386 Unidentified 0.098 0.100 0.060

101.867 Unidentified 0.032 0.033 0.018

102.262 Unidentified 0.049 0.050 0.027

102.338 Unidentified 0.041 0.036 0.027

102.427 Unidentified 0.044 0.038 0.029

103.377 Unidentified 0.019 0.017 0.013

103.525 Unidentified 0.222 0.191 0.145

103.731 Unidentified 0.021 0.020 0.012

103.854 Unidentified 0.058 0.054 0.033

104.061 Unidentified 0.012 0.011 0.007

104.888 Unidentified 0.011 0.011 0.006

105.495 Unidentified 0.016 0.015 0.009

C-411
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 13

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol

Unidentified 105.906 Unidentified 0.039 0.037 0.022

106.566 Unidentified 0.088 0.090 0.050

107.629 Unidentified 0.084 0.086 0.048

108.964 Unidentified 0.020 0.017 0.013

109.320 Unidentified 0.021 0.018 0.014

109.899 Unidentified 0.007 0.006 0.004

110.572 Unidentified 0.017 0.014 0.011

110.745 Unidentified 0.002 0.002 0.001

111.038 Unidentified 0.006 0.005 0.003

111.350 Unidentified 0.006 0.005 0.004

111.524 Unidentified 0.014 0.012 0.008

111.688 Unidentified 0.008 0.007 0.005

111.859 Unidentified 0.011 0.010 0.007

111.951 Unidentified 0.013 0.011 0.007

112.082 Unidentified 0.005 0.004 0.003

112.247 Unidentified 0.006 0.005 0.003

112.453 Unidentified 0.015 0.013 0.008

113.272 Unidentified 0.007 0.006 0.004

113.458 Unidentified 0.014 0.012 0.007

113.828 Unidentified 0.001 0.001 0.001

113.948 Unidentified 0.005 0.004 0.003

114.239 Unidentified 0.010 0.008 0.005

114.442 Unidentified 0.007 0.006 0.004

114.684 Unidentified 0.008 0.008 0.004

114.887 Unidentified 0.006 0.006 0.003

115.644 Unidentified 0.067 0.068 0.035

116.035 Unidentified 0.011 0.008 0.007

116.558 Unidentified 0.012 0.009 0.008

116.758 Unidentified 0.010 0.007 0.007

116.919 Unidentified 0.005 0.005 0.003

117.019 Unidentified 0.003 0.003 0.002

117.205 Unidentified 0.002 0.002 0.001

117.366 Unidentified 0.005 0.004 0.003

117.487 Unidentified 0.002 0.002 0.001

117.655 Unidentified 0.006 0.005 0.003

118.343 Unidentified 0.006 0.005 0.003

118.529 Unidentified 0.003 0.003 0.001

118.897 Unidentified 0.003 0.003 0.001

119.046 Unidentified 0.003 0.003 0.001

119.292 Unidentified 0.002 0.002 0.001

119.400 Unidentified 0.001 0.001 0.001

119.480 Unidentified 0.001 0.001 0.000

119.628 Unidentified 0.002 0.002 0.001

119.723 Unidentified 0.003 0.002 0.002

119.831 Unidentified 0.003 0.003 0.002

120.357 Unidentified 0.006 0.005 0.003

120.564 Unidentified 0.002 0.001 0.001

120.702 Unidentified 0.004 0.003 0.002

C-412
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 14

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol

Unidentified 120.973 Unidentified 0.002 0.002 0.001

121.243 Unidentified 0.004 0.003 0.002

121.372 Unidentified 0.001 0.001 0.001

121.479 Unidentified 0.001 0.001 0.000

121.632 Unidentified 0.001 0.001 0.001

121.827 Unidentified 0.001 0.001 0.001

121.988 Unidentified 0.001 0.000 0.000

122.317 Unidentified 0.001 0.001 0.001

122.649 Unidentified 0.001 0.001 0.000

122.911 Unidentified 0.002 0.002 0.001

123.157 Unidentified 0.001 0.001 0.001

123.724 Unidentified 0.002 0.002 0.001

123.928 Unidentified 0.001 0.001 0.001

124.126 Unidentified 0.001 0.001 0.001

124.213 Unidentified 0.001 0.001 0.001

124.525 Unidentified 0.003 0.002 0.002

125.363 Unidentified 0.003 0.002 0.002

125.614 Unidentified 0.001 0.001 0.001

126.291 Unidentified 0.002 0.002 0.001

Plus

C-413
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 1

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Sample Chromatogram

C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF

2 22.50 20.00 17.50 15.00 12.50 10.00 7.50 5.00 2.50

Unidentified

i-Butane

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

Ethanol

i-Pentane

Unidentified

Unidentified

Pentene-1 Unidentified

2-Methylbutene-1 Unidentified n-Pentane

2-Methyl-1,3-Butadiene Unidentified

Unidentified t-Pentene-2

3-Methylbutadiene-1,2

Unidentified c-Pentene-2

t-Butanol 2-Methylbutene-2 Unidentified 1t,3-Pentadiene

1c,3-Pentadiene

2,2-Dimethylbutane Unidentified

Cyclopentene Unidentified

Unidentified 4-Methylpentene-1

C-414
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 2

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Sample Chromatogram

C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF

5 47.50 45.00 42.50 40.00 37.50 35.00 32.50 30.00 27.50

UUnidentified Unnididenentifi tifieedd Cyclopentane Unidentified

2,3-Dimethylbutane

Unidentified Unidentified Methyl-t-butylether

4-Methyl-c-pentene-2 2-Methylpentane

Unidentified 4-Methyl-t-pentene-2

3-Methylpentane Unidentified

Hexene-1

Unidentified

n-Hexane

Unidentified t-Hexene-3 Unidentified t-Hexene-2 Unidentified

Unidentified 2-Methylpentene-2

3-Methyl-c-pentene-2 Unidentified

O14 Unidentified c-Hexene-2 Unidentified

Unidentified 3,3-Dimethylpentene-1

Methylcyclopentane Unidentified

2,3-Dimethyl-2-Butene

2,4-Dimethylpentane 2,3,3-Trimethylbutene-1 2,2,3-Trimethylbutane Unidentified

3,4-Dimethylpentene-1

Unidentified 4,4-Dimethyl-c-pentene-2

Diolefin Benzene

Unidentified

2-Methyl-c-hexene-3

3,3-Dimethylpentane Cyclohexane

2-Methyl-t-hexene-3 Unidentified

n-Butanol Unidentified

2-Ethyl-3-methylbutene-1

4-Methylhexene-1 Unidentified

4-Methyl-t/c-hexene-2 2-Methylhexane

Cyclohexene Unidentified TAME Unidentified

3-Methylhexane

Unidentified

C-415
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 3

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Sample Chromatogram

C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF

7 72.50 70.00 67.50 65.00 62.50 60.00 57.50 55.00 52.50

1c,3-Dimethylcyclopentane

Unidentified 1t,3-Dimethylcyclopentane 2-Ethylpentene-1 Unidentified 1t,2-Dimethylcyclopentane Unidentified

2,2,4-Trimethylpentane

Unidentified

3-Methyl-c-hexene-3 Unidentified t-Heptene-3

C7-Olefin2

n-Heptane

Unidentified 2-Methyl-2-hexene

Unidentified t-Heptene-2 3-Ethylpentene-2

Unidentified

Unidentified

c-Heptene-2

Methylcyclohexane 1c,2-Dimethylcyclopentane

1,1,3-Trimethylcyclopentane

2,2-Dimethylhexane Unidentified

O35

Unidentified

2,2,3-Trimethylpentane 2,5-Dimethylhexane

2,4-Dimethylhexane Unidentified

1c,2t,4-Trimethylcyclopentane

3,3-Dimethylhexane

O38 Unidentified

C8-Olefin2

2,3,4-Trimethylpentane

Toluene

Unidentified

C8-Diolefin4

2,3-Dimethylhexane

C8-Olefin3

2-Methylheptane 4-Methylheptane 3,4-Dimethylhexane

1c,3-Dimethylcyclohexane 3-Ethylhexane 3-Methylheptane

1c,2t,3-Trimethylcyclopentane 1,3-Octadiene Unidentified Unidentified

2,2,5-Trimethylhexane 3c-Ethylmethylcyclopentane 3t-Ethylmethylcyclopentane 2t-Ethylmethylcyclopentane t-Octene-41,1-Methylethylcyclopentane

1t,3-Dimethylcyclohexane

t-Octene-3 1c 2c 3-Trimethylcyclopentane

C-416
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 4

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Sample Chromatogram

C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF

1 97.50 95.00 92.50 90.00 87.50 85.00 82.50 80.00 77.50

n-Octane

t-Octene-2

Unidentified C9-Olefin1

C9-Olefin2

Unidentified

c-Octene-2 Unidentified 2,3,3-Trimethylhexene-1 N3Unidentified

Unidentified

1c,2-Dimethylcyclohexane Unidentified

2,2-Dimethylheptane t-2,2-Dimethylheptene-3 2,2,3-Trimethylhexane 4,4-Dimethylheptane Ethylcyclohexane 1c,3c,5-Trimethylcyclohexane 3,3-Dimethylheptane Unidentified 2-Methyl-4-ethylhexane

Unidentified Ethylbenzene Unidentified 1c,2t,4t-Trimethylcyclohexane 2-Methyloctene-1

Unidentified

m-Xylene Unidentified p-Xylene 2,3-Dimethylheptane Unidentified

3,3-Diethylpentane

4-Methyloctane 2-Methyloctane N15

1c,2t,4c-Trimethylcyclohexane 3-Methyloctane Unidentified Unidentified o-Xylene Unidentified C9-Olefin4

N18 Unidentified C9-Isoparaffin1 Nonene-1 Unidentified Unidentified

t-7-Methyloctene-3 c-Nonene-3 Unidentified n-Nonane

t-Nonene-2

3,7-Dimethyloctene-1 Unidentified

i-Propylbenzene Unidentified c-Nonene-2 N26 i-Propylcyclohexane 2,2-Dimethyloctane N28 2,4-Dimethyloctane Unidentified 2,6-Dimethyloctane 2,5-Dimethyloctane Unidentified Unidentified

n-Butylcyclopentane I12

N30 3,3-Dimethyloctane I14 Unidentified n-Propylbenzene 3-Methyl-5-ethylheptane Unidentified Unidentified Unidentified 1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene Unidentified Unidentified

1,3,5-Trimethylbenzene Unidentified Unidentified 5-Methylnonane 4-Methylnonane 2-Methylnonane 1-Methyl-2-ethylbenzene 3-Ethyloctane3-Methylnonane Unidentified Unidentified C10-Isoparaffin1 I19

Unidentified 1,2,4-Trimethylbenzene Unidentified i-Butylcyclohexane Unidentified I21 C10-Isoparaffin2

Decene-1 Unidentified 1t-Methyl-2-n-propylcyclohexanR

C-417
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 5

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Sample Chromatogram

C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF

1 122.50 120.00 117.50 115.00 112.50 110.00 107.50 105.00 102.50

2,3-Dimethyloctene-2

sec-Butylbenzene Unidentified

n-Decane

I26

N39 1,2,3-Trimethylbenzene Unidentified 1-Methyl-3-i-propylbenzene Unidentified Unidentified 1-Methyl-4-i-propylbenzene 2,3-Dihydroindene sec-Butylcyclohexane Unidentified Unidentified Unidentified 3-Ethylnonane Unidentified UnidentifiedC11-Isoparaffin2 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene Unidentified 1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene Unidentified 1,2-Diethylbenzene Unidentified 1-Methyl-2-n-propylbenzene t-Decahydronaphthalene C11-Isoparaffin3 C11-Isoparaffin4 Unidentified I38 C11-Isoparaffin5 1,4,Dimethyl-2-ethylbenzene 1,3-Dimethyl-4-ethylbenzene Unidentified 1,2-Dimethyl-4-ethylbenzene I41 I42 1,3-Dimethyl-2-ethylbenzene

Unidentified 4M-1tC4Benz Unidentified 1-Methyl-4-t-butylbenzene 1,2-Dimethyl-3-ethylbenzene Unidentified

n-Undecane 1,2,4,5-Tetramethylbenzene Unidentified Unidentified 1-Methyl-1-n-butylbenzene Unidentified 1-t-Butyl-2-methylbenzene Unidentified Unidentified Unidentified

Unidentified Unidentified Unidentified

Unidentified

5-Methylindan C11-Aromatic2 Unidentified C11-Aromatic3 Unidentified

Unidentified 4-Methylindan Unidentified 2-Methylindan Unidentified Unidentified

1t-M-2-(4-MP)cyclopentane Unidentified

I461-Methyl-2-n-butylbenzene 1,4-Di-i-propylbenzene I48 Unidentified 1,2,3,4-Tetrahydronaphthalene Unidentified A6Unidentified Naphthalene

Unidentified Unidentified Unidentified Unidentified 1t-Butyl-4-ethylbenzene

1,3-Di-n-propylbenzene

Unidentified

Unidentified n-Dodecane

Unidentified

1,3,5-Triethylbenzene Unidentified

Unidentified 1,2,4-Triethylbenzene

Unidentified

1-Methyl-4-n-pentylbenzene Unidentified

Unidentified

n-Hexylbenzene

I49

Unidentified

Pentamethylbenzene Unidentified

C-418
Hydrocarbon Expert V4.7 Tue Jul 22 17:54:59 2008 Page 6

File: C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF 21-Jul-08, 23:56:15

Sample: ODDB-72366 Operator: AAD

Parameter: C:\HPCHEM\SeparationSystems\HCE4\ODDB-72366

ODDB-72366

Sample Chromatogram

C:\HPCHEM\2\DATA\07-21-08\004F0401.D\004F0401_ADC1_B.CDF

1 147.50 145.00 142.50 140.00 137.50 135.00 132.50 130.00 127.50

2-Methylnaphthalene Unidentified Unidentified

1-Methylnaphthalene n-Tridecane Unidentified

C-419
Hydrocarbon Expert V4.7 Thu Aug 26 17:04:50 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91324 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91324

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 3.891 4.430 3.716

I-Paraffins 42.144 45.328 31.970

Aromatics 18.679 15.841 13.777

Mono-Aromatics 17.762 15.124 13.196

Naphthalenes 0.129 0.093 0.078

Naphtheno/Olefino-Benzs 0.178 0.148 0.106

Indenes 0.611 0.477 0.396

Naphthenes 3.473 3.377 3.000

Mono-Naphthenes 3.473 3.377 3.000

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 7.304 7.991 7.554

n-Olefins 2.999 3.367 3.205

Iso-Olefins 3.554 3.903 3.580

Naphtheno-Olefins 0.710 0.678 0.725

Di-Olefins 0.041 0.043 0.045

Oxygenates 22.675 21.279 38.864

Unidentified 1.833 1.754 1.119

Plus 0.000 0.000 0.000

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C-420
Hydrocarbon Expert V4.7 Thu Aug 26 17:04:50 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91324 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91324

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C2 22.540 21.154 38.700

C3 0.087 0.084 0.117

C4 0.783 0.972 1.059

C5 9.218 10.718 10.234

C6 11.237 12.025 10.486

C7 10.695 10.274 8.824

C8 30.880 31.392 21.656

C9 7.573 7.045 4.851

C10 4.092 3.602 2.407

C11 0.933 0.871 0.484

C12 0.129 0.109 0.063

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C-421
Hydrocarbon Expert V4.7 Thu Aug 26 17:04:50 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91324 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91324

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C3 0.006 0.009 0.011

C4 0.479 0.613 0.652

C5 1.183 1.399 1.297

C6 0.839 0.942 0.770

C7 0.584 0.632 0.461

C8 0.472 0.497 0.327

C9 0.278 0.286 0.171

C10 0.020 0.020 0.011

C11 0.030 0.030 0.015

I-Paraffins C4 0.052 0.069 0.071

C5 4.195 5.014 4.599

C6 5.533 6.226 5.079

C7 2.943 3.210 2.323

C8 24.875 26.123 17.224

C9 2.918 3.041 1.800

C10 1.093 1.111 0.604

C11 0.522 0.520 0.264

C12 0.013 0.013 0.006

Mono-Aromatics C6 0.743 0.626 0.752

C7 5.029 4.295 4.317

C8 5.117 4.373 3.812

C9 4.277 3.638 2.815

C10 2.146 1.816 1.265

C11 0.338 0.284 0.180

C12 0.112 0.094 0.055

Naphthalenes C10 0.112 0.081 0.069

C11 0.017 0.012 0.009

Naphtheno/Olefino-Benzs C10 0.178 0.148 0.106

Indenes C9 0.070 0.054 0.047

C10 0.537 0.420 0.347

C12 0.004 0.003 0.002

Mono-Naphthenes C5 0.150 0.149 0.169

C6 1.501 1.467 1.411

C7 1.409 1.368 1.132

C8 0.376 0.360 0.265

C9 0.030 0.026 0.019

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C-422
Hydrocarbon Expert V4.7 Thu Aug 26 17:04:50 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91324 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91324

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Mono-Naphthenes C10 0.007 0.006 0.004

n-Olefins C4 0.197 0.239 0.278

C5 1.666 1.902 1.879

C6 1.040 1.127 0.978

C7 0.069 0.073 0.056

C11 0.026 0.026 0.015

Iso-Olefins C5 1.791 2.027 2.020

C6 1.077 1.158 1.012

C7 0.646 0.680 0.520

C8 0.040 0.038 0.027

Naphtheno-Olefins C5 0.206 0.198 0.239

C6 0.504 0.479 0.485

Di-Olefins C5 0.026 0.029 0.030

C7 0.015 0.015 0.014

Oxygenates C2 22.540 21.154 38.700

C3 0.081 0.075 0.106

C4 0.055 0.051 0.058

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C-423
Hydrocarbon Expert V4.7 Thu Aug 26 17:04:50 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91324 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91324

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 29.52 27.10

5% 81.81 81.17

10% 114.58 98.81

15% 144.41 139.00

20% 164.42 153.99

25% 172.44 172.31

30% 172.67 172.57

35% 172.91 172.82

40% 173.15 173.08

45% 177.19 176.24

50% 209.29 208.97

55% 209.94 209.71

60% 211.55 210.32

65% 230.81 228.71

70% 234.39 231.05

75% 237.47 236.74

80% 245.89 239.09

85% 279.99 268.46

90% 319.83 291.80

95% 348.60 336.10

FBP 400.46 388.16

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C-424
Hydrocarbon Expert V4.7 Thu Aug 26 17:04:50 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91324 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91324

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 7.554 74-98-6 P3 Propane 0.006 0.009 0.011 1.666

2 8.810 75-28-5 I4 i-Butane 0.052 0.069 0.071 13.823

3 9.624 115-11-7 K4 Isobutene 0.017 0.021 0.023 4.570

4 9.665 106-98-9 K4 Butene-1 0.018 0.023 0.026 5.010

5 10.023 106-97-8 P4 n-Butane 0.479 0.613 0.652 127.567

6 10.510 624-64-6 K4 t-Butene-2 0.074 0.091 0.105 20.522

7 10.638 463-82-1 I5 2,2-Dimethylpropane 0.012 0.015 0.013 3.130

8 11.252 590-18-1 K4 c-Butene-2 0.088 0.105 0.124 24.230

9 13.126 64-17-5 X2 Ethanol 22.540 21.154 38.700 2558.100

10 13.453 563-45-1 C5 3-Methylbutene-1 0.225 0.265 0.254 61.956

11 15.078 78-78-4 I5 i-Pentane 4.183 5.000 4.586 1121.004

12 16.732 109-67-1 K5 Pentene-1 0.338 0.391 0.381 93.178

13 17.583 563-46-2 C5 2-Methylbutene-1 0.514 0.585 0.579 141.572

14 18.116 109-66-0 P5 n-Pentane 1.183 1.399 1.297 317.000

15 18.625 78-79-5 E5 2-Methyl-1,3-Butadiene 0.011 0.012 0.012 3.013

16 19.234 646-04-8 K5 t-Pentene-2 0.858 0.980 0.968 236.495

17 19.877 ? Unidentified 0.006 0.007 0.007 1.976

18 20.269 627-20-3 K5 c-Pentene-2 0.470 0.531 0.530 129.585

19 20.945 513-35-9 C5 2-Methylbutene-2 1.053 1.177 1.187 290.107

20 21.270 2004-70-8 E5 1t,3-Pentadiene 0.016 0.017 0.018 4.430

21 22.537 1574-41-0 B5 1,3-Cyclopentadiene 0.007 0.007 0.008 1.979

22 23.096 75-83-2 I6 2,2-Dimethylbutane 0.094 0.107 0.086 25.259

23 25.742 142-29-0 B5 Cyclopentene 0.199 0.191 0.231 56.449

24 26.896 71-23-8 X3 n-Propanol 0.081 0.075 0.106 15.535

25 27.000 ? Unidentified 0.057 0.063 0.054 19.256

26 27.605 287-92-3 M5 Cyclopentane 0.150 0.149 0.169 41.421

27 28.340 79-29-8 I6 2,3-Dimethylbutane 1.146 1.283 1.052 308.342

28 28.736 ? Unidentified 0.053 0.053 0.048 17.997

29 29.203 691-38-3 C6 4-Methyl-c-pentene-2 0.046 0.051 0.044 12.794

30 29.421 107-83-5 I6 2-Methylpentane 2.676 3.034 2.456 719.907

31 29.842 674-76-0 C6 4-Methyl-t-pentene-2 0.132 0.145 0.124 36.274

32 32.069 96-14-0 I6 3-Methylpentane 1.617 1.803 1.484 435.084

33 33.225 763-29-1 C6 2-Methylpentene-1 0.224 0.243 0.211 61.862

34 33.446 592-41-6 K6 Hexene-1 0.160 0.175 0.151 44.141

35 35.641 760-21-4 C6 2-Ethylbutene-1 0.069 0.074 0.065 19.089

36 35.800 110-54-3 P6 n-Hexane 0.839 0.942 0.770 225.643

37 36.43713269-52-8 K6 t-Hexene-3 0.263 0.285 0.247 72.471

38 36.915 4050-45-7 K6 t-Hexene-2 0.403 0.438 0.379 111.187

39 37.041 1120-62-3 B6 3-Methylcyclopentene 0.101 0.098 0.097 27.771

40 37.410 625-27-4 C6 2-Methylpentene-2 0.341 0.366 0.321 94.058

41 37.823 922-62-3 C6 3-Methyl-c-pentene-2 0.264 0.280 0.248 72.747

42 38.740 7688-21-3 K6 c-Hexene-2 0.214 0.229 0.201 58.924

43 40.084 3404-73-7 C7 3,3-Dimethylpentene-1 0.308 0.325 0.248 85.004

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C-425
Hydrocarbon Expert V4.7 Thu Aug 26 17:04:50 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91324 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91324

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 40.669 96-37-7 M6 Methylcyclopentane 1.028 1.017 0.966 283.247

45 42.237 108-08-7 I7 2,4-Dimethylpentane 0.820 0.903 0.647 221.463

46 42.535 594-56-9 C7 2,3,3-Trimethylbutene-1 0.013 0.014 0.011 3.669

47 42.781 464-06-2 I7 2,2,3-Trimethylbutane 0.052 0.056 0.041 14.023

48 45.427 1528-30-9 E7 C6-Diolefin-1 0.015 0.015 0.014 4.112

49 45.635 71-42-3 Q6 Benzene 0.743 0.626 0.752 220.396

50 45.833 693-89-0 B6 1-Methylcyclopentene 0.359 0.341 0.346 101.275

51 46.640 3404-61-3 C7 3-Methylhexene-1 0.015 0.016 0.012 4.234

52 47.228 3524-73-0 C7 5-Methylhexene-1 0.042 0.044 0.034 11.469

53 47.552 110-82-7 M6 Cyclohexane 0.474 0.450 0.445 130.535

54 48.058 71-36-3 X4 n-Butanol 0.055 0.051 0.058 11.385

55 49.27115840-60-5 C7 2-Methyl-c-hexene-3 0.040 0.043 0.032 11.089

56 49.619 3769-23-1 C7 4-Methylhexene-1 0.011 0.011 0.009 3.003

57 50.265 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.051 0.053 0.041 13.947

58 50.672 591-76-4 I7 2-Methylhexane 1.518 1.657 1.198 410.084

59 51.153 110-83-8 B6 Cyclohexene 0.044 0.040 0.043 12.219

60 52.492 589-34-4 I7 3-Methylhexane 0.552 0.595 0.436 149.226

61 53.353 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.152 0.150 0.122 41.855

62 53.940 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.117 0.116 0.094 32.205

63 54.566 822-50-4 M7 1t,2-Dimethylcyclopentane 0.160 0.158 0.129 44.160

64 54.899 C7 C7 - Iso-Olefin - 2 0.021 0.022 0.017 5.859

65 55.232 540-84-1 I8 2,2,4-Trimethylpentane 11.022 11.796 7.632 2983.199

66 55.611 M7 C7 - MonoNaph - 1 0.028 0.027 0.020 7.645

67 56.802 4914-89-0 C7 3-Methyl-c-hexene-3 0.014 0.014 0.011 3.772

68 57.33114686-14-7 K7 t-Heptene-3 0.032 0.033 0.025 8.702

69 57.684 6094-02-6 C7 2-Methylhexene-1 0.057 0.060 0.046 15.641

70 58.056 142-82-5 P7 n-Heptane 0.584 0.632 0.461 157.722

71 58.273 7642-10-6 K7 c-Heptene-3 0.024 0.026 0.020 6.752

72 58.547 2738-19-4 C7 2-Methyl-2-hexene 0.026 0.027 0.021 7.167

73 58.79110574-36-4 C7 3-Methyl-c-hexene-2 0.020 0.021 0.016 5.445

74 59.17214686-13-6 K7 t-Heptene-2 0.013 0.014 0.011 3.658

75 59.64816491-15-9 M7 Cyclopentene, 1,5-dimethyl- 0.018 0.018 0.015 4.962

76 60.07520710-38-8 C7 3-Methyl-t-hexene-2 0.015 0.015 0.012 4.089

77 60.858 4914-91-4 C7 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.014 0.011 3.669

78 61.518 108-87-2 M7 Methylcyclohexane 0.886 0.852 0.714 244.129

79 62.457 4516-69-2 M8 1,1,3-Trimethylcyclopentane 0.027 0.026 0.019 7.338

80 62.847 590-73-8 I8 2,2-Dimethylhexane 0.027 0.028 0.018 7.211

81 63.360 ? Unidentified 0.052 0.054 0.038 17.660

82 64.294 1640-89-7 M7 Ethylcyclopentane 0.049 0.047 0.039 13.470

83 64.950 564-02-3 I8 2,2,3-Trimethylpentane 0.546 0.565 0.378 147.830

84 65.182 592-13-2 I8 2,5-Dimethylhexane 1.242 1.326 0.860 336.147

85 65.519 589-43-5 I8 2,4-Dimethylhexane 1.139 1.204 0.789 308.287

86 66.349 4850-28-6 M8 1c,2t,4-Trimethylcyclopentane 0.027 0.026 0.019 7.392

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C-426
Hydrocarbon Expert V4.7 Thu Aug 26 17:04:50 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91324 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91324

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 66.741 563-16-6 I8 3,3-Dimethylhexane 0.019 0.020 0.013 5.067

88 67.86215890-40-1 M8 1t,2c,3-Trimethylcyclopentane 0.024 0.023 0.017 6.647

89 68.509 565-75-3 I8 2,3,4-Trimethylpentane 4.276 4.403 2.961 1157.167

90 69.028 108-88-3 Q7 Toluene 5.029 4.295 4.317 1476.457

91 69.188 560-21-4 I8 2,3,3-Trimethylpentane 4.740 4.833 3.282 1282.747

92 70.514 C8 C8 - Diolefin - 1 0.010 0.010 0.007 2.769

93 70.799 584-94-1 I8 2,3-Dimethylhexane 1.127 1.172 0.780 304.957

94 72.048 592-27-8 I8 2-Methylheptane 0.243 0.258 0.168 65.714

95 72.310 589-53-7 I8 4-Methylheptane 0.185 0.194 0.128 50.063

96 72.448 ? Unidentified 0.089 0.092 0.062 30.210

97 73.224 M8 1,3-dimethyl-t-cyclohexane 0.155 0.149 0.109 42.805

98 73.360 589-81-1 I8 3-Methylheptane 0.210 0.220 0.145 56.789

99 73.561 619-99-8 I8 3-Ethylhexane 0.100 0.104 0.069 27.147

100 74.457 ? Unidentified 0.025 0.024 0.018 8.607

101 75.260 3522-94-9 I9 2,2,5-Trimethylhexane 1.994 2.088 1.230 540.830

102 75.609 M8 3c-Ethylmethylcyclopentane 0.009 0.009 0.006 2.528

103 75.826 M8 3t-Ethylmethylcyclopentane 0.013 0.012 0.009 3.495

104 76.233 ? Unidentified 0.015 0.014 0.010 4.926

105 76.532 ? Unidentified 0.059 0.056 0.041 19.802

106 77.869 111-65-9 P8 n-Octane 0.472 0.497 0.327 127.728

107 78.820 ? Unidentified 0.050 0.048 0.035 16.755

108 80.353 1069-53-0 I9 2,3,5-Trimethylhexane 0.330 0.338 0.203 89.373

109 80.905 C8 C9 - IsoOlefin - 1 0.016 0.015 0.011 4.377

110 81.367 2207-01-4 M8 1c,2-Dimethylcyclohexane 0.013 0.012 0.009 3.629

111 81.518 1071-26-7 I9 2,4-Dimethylheptane 0.069 0.072 0.043 18.763

112 82.173 1678-91-7 M8 Ethylcyclohexane 0.108 0.102 0.076 29.739

113 82.473 1072-05-5 I9 2,6-Dimethylheptane 0.105 0.109 0.065 28.373

114 82.974 ? Unidentified 0.024 0.023 0.017 8.014

115 83.404 I9 2,5-Dimethylheptane 0.201 0.208 0.124 54.408

116 83.580 926-82-9 I9 3,5-Dimethylheptane 0.024 0.025 0.015 6.558

117 84.728 100-41-4 Q8 Ethylbenzene 0.894 0.764 0.666 260.567

118 84.901 ? Unidentified 0.028 0.028 0.018 9.343

119 85.145 ? Unidentified 0.031 0.030 0.020 10.555

120 85.952 108-38-3 Q8 m-Xylene 2.374 2.034 1.769 691.839

121 86.098 106-42-3 Q8 p-Xylene 1.058 0.910 0.789 308.408

122 86.230 ? Unidentified 0.067 0.068 0.041 22.611

123 86.487 C8 C9-IsoOlefin-3 0.014 0.014 0.009 3.924

124 86.594 ? Unidentified 0.013 0.013 0.008 4.223

125 86.751 I9 3,5-Dimethylheptane 0.009 0.009 0.005 2.310

126 86.879 1067-20-5 I9 3,3-Diethylpentane 0.008 0.007 0.005 2.038

127 87.272 2216-34-4 I9 4-Methyloctane 0.047 0.048 0.029 12.776

128 87.404 3221-61-2 I9 2-Methyloctane 0.063 0.065 0.039 17.010

129 88.10615869-80-4 I9 Heptane, 3-ethyl- 0.008 0.009 0.005 2.293

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C-427
Hydrocarbon Expert V4.7 Thu Aug 26 17:04:50 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91324 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91324

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 88.267 2216-33-3 I9 3-Methyloctane 0.062 0.063 0.038 16.679

131 88.743 ? Unidentified 0.107 0.116 0.067 36.142

132 88.926 95-47-6 Q8 o-Xylene 0.790 0.665 0.589 230.183

133 89.321 I10 C10 - IsoParaffin - 1 0.344 0.350 0.191 93.372

134 89.909 M9 trans-1,3-Diethylcyclopentane 0.017 0.015 0.011 5.039

135 90.16414720-74-2 I10 2,2,4-trimethylheptane 0.247 0.251 0.137 67.095

136 91.729 111-84-2 P9 n-Nonane 0.278 0.286 0.171 75.261

137 92.301 4926-90-3 M9 1,1-Methylethylcyclohexane 0.012 0.011 0.008 3.438

138 93.093 98-82-8 Q9 i-Propylbenzene 0.030 0.025 0.019 8.543

139 93.271 ? Unidentified 0.007 0.007 0.005 2.442

140 93.271 ? Unidentified 0.007 0.008 0.004 2.442

141 93.271 ? Unidentified 0.007 0.005 0.004 2.442

142 93.839 ? Unidentified 0.050 0.051 0.028 16.961

143 94.06115869-87-1 I10 2,2-Dimethyloctane 0.019 0.019 0.010 5.100

144 94.86315869-89-3 I10 2,5-Dimethyloctane 0.012 0.013 0.007 3.388

145 95.066 I10 C10 - IsoParaffin - 2 0.007 0.007 0.004 1.960

146 95.504 2051-30-1 I10 2,4-Dimethyloctane 0.022 0.022 0.012 6.003

147 95.891 I10 2,6-Dimethyloctane 0.010 0.010 0.006 2.798

148 96.552 103-65-1 Q9 n-Propylbenzene 0.253 0.217 0.166 73.177

149 97.398 620-14-4 Q9 1-Methyl-3-ethylbenzene 0.954 0.817 0.628 276.302

150 97.631 622-96-8 Q9 1-Methyl-4-ethylbenzene 0.442 0.380 0.291 127.883

151 98.257 108-67-8 Q9 1,3,5-Trimethylbenzene 0.557 0.477 0.366 161.221

152 98.90517301-94-8 I10 4-Methylnonane 0.011 0.011 0.006 3.045

153 99.112 I10 2,2,6-Trimethyloctane 0.344 0.351 0.191 93.565

154 99.342 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.325 0.273 0.214 94.131

155 99.884 5911-04-6 I10 3-Methylnonane 0.015 0.015 0.008 3.948

156 100.349 ? Unidentified 0.023 0.017 0.011 7.617

157 100.480 ? Unidentified 0.060 0.060 0.030 20.252

158 100.696 I11 C11-Isoparaffin-2 0.033 0.033 0.017 9.019

159 100.972 95-63-6 Q9 1,2,4-Trimethylbenzene 1.526 1.290 1.004 441.812

160 101.162 ? Unidentified 0.042 0.045 0.024 14.311

161 101.283 ? Unidentified 0.025 0.026 0.014 8.583

162 101.548 1678-98-4 M10 i-Butylcyclohexane 0.007 0.006 0.004 1.869

163 102.33317302-01-1 I10 3-Ethyl-3-methylheptane 0.061 0.061 0.031 16.694

164 102.647 538-93-2 Q10 i-Butylbenzene 0.073 0.063 0.043 21.031

165 102.799 124-18-5 P10 n-Decane 0.020 0.020 0.011 5.489

166 102.896 ? Unidentified 0.014 0.012 0.008 4.698

167 103.196 ? Unidentified 0.017 0.017 0.009 5.905

168 103.847 526-73-8 Q9 1,2,3-Trimethylbenzene 0.190 0.158 0.125 55.090

169 104.212 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.008 0.007 0.005 2.444

170 104.406 I11 C11 Isoparaffin-4 0.009 0.009 0.005 2.434

171 104.614 99-87-6 Q10 1-Methyl-4-i-propylbenzene 0.062 0.053 0.036 17.809

172 105.043 J9 Indan 0.070 0.054 0.047 20.739

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C-428
Hydrocarbon Expert V4.7 Thu Aug 26 17:04:50 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91324 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91324

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 105.637 J10 Indene 0.365 0.281 0.245 107.521

174 106.352 I11 C11-Isoparaffin-7 0.152 0.152 0.077 41.437

175 106.545 141-93-5 Q10 1,3-Diethylbenzene 0.023 0.020 0.014 6.684

176 106.830 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 0.479 0.412 0.282 137.958

177 107.157 105-05-5 Q10 1,4-Diethylbenzene 0.180 0.155 0.106 51.889

178 107.380 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.108 0.091 0.064 31.187

179 107.620 135-01-3 Q10 1,2-Diethylbenzene 0.039 0.033 0.023 11.236

180 108.079 ? Unidentified 0.038 0.038 0.019 12.775

181 108.232 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.043 0.036 0.025 12.367

182 108.353 ? Unidentified 0.045 0.045 0.023 15.040

183 108.435 ? Unidentified 0.041 0.041 0.021 13.925

184 108.561 I11 C11- Isoparaffin-11 0.328 0.326 0.166 89.233

185 108.743 ? Unidentified 0.106 0.106 0.054 35.927

186 109.166 ? Unidentified 0.448 0.378 0.264 151.280

187 109.393 J10 2-Methylindan 0.056 0.043 0.034 16.550

188 109.739 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.268 0.227 0.158 77.278

189 110.285 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.318 0.265 0.187 91.604

190 110.709 ? Unidentified 0.011 0.010 0.006 3.688

191 110.903 693-61-8 K11 2-Undecene, (E)- 0.026 0.026 0.015 7.039

192 111.037 ? Unidentified 0.062 0.062 0.035 20.808

193 111.309 ? Unidentified 0.054 0.047 0.029 18.125

194 111.411 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.060 0.050 0.035 17.256

195 111.709 1120-21-4 P11 n-Undecane 0.030 0.030 0.015 8.135

196 111.861 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.041 0.034 0.022 11.745

197 111.972 ? Unidentified 0.024 0.020 0.013 8.189

198 112.346 Q10 1,2,4,5-Tetramethylbenzene 0.204 0.170 0.120 58.779

199 112.613 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.280 0.233 0.165 80.518

200 112.955 ? Unidentified 0.005 0.004 0.003 1.804

201 113.130 I12 C12 - IsoParaffin - 1 0.008 0.008 0.004 2.293

202 113.484 ? Unidentified 0.019 0.019 0.009 6.391

203 113.609 ? Unidentified 0.006 0.006 0.003 2.050

204 113.760 Q11 C11 - Aromatic - 3 0.050 0.041 0.027 14.268

205 113.944 874-35-1 H10 5-Methylindan 0.090 0.075 0.054 25.798

206 114.069 Q12 1,2-Di-i-propylbenzene 0.033 0.028 0.016 9.526

207 114.284 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.045 0.037 0.024 12.876

208 114.448 Q11 C11 - Aromatic - 4 0.031 0.026 0.016 8.790

209 114.693 824-22-6 J10 4-Methylindan 0.115 0.096 0.069 33.114

210 114.847 5161-04-6 Q11 Benzene, 1-methyl-4-(2-methylpropyl)-0.028 0.023 0.015 7.980

211 114.941 824-63-5 H10 2-Methylindan 0.088 0.073 0.053 25.317

212 115.143 ? Unidentified 0.010 0.010 0.005 3.289

213 115.257 538-68-1 Q11 n-Pentylbenzene 0.011 0.009 0.006 3.227

214 115.484 Q11 tert-Pentylbenzene 0.046 0.039 0.025 13.291

215 115.798 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.020 0.017 0.011 5.802

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C-429
Hydrocarbon Expert V4.7 Thu Aug 26 17:04:50 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91324 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91324

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

216 115.908 Q11 C11 - Aromatic - 6 0.032 0.028 0.017 9.217

217 116.248 I12 C12 - IsoParaffin - 4 0.004 0.004 0.002 1.205

218 116.367 100-18-5 Q12 1,4-Di-i-propylbenzene 0.038 0.032 0.019 10.926

219 116.809 91-20-3 G10 Naphthalene 0.112 0.081 0.069 33.752

220 116.942 ? Unidentified 0.013 0.013 0.006 4.352

221 117.125 ? Unidentified 0.004 0.003 0.002 1.303

222 117.246 ? Unidentified 0.009 0.008 0.004 3.053

223 117.409 J12 Dimethyl Indane - 1 0.004 0.003 0.002 1.189

224 117.594 7364-19-4 Q12 1t-Butyl-4-ethylbenzene 0.006 0.005 0.003 1.719

225 117.893 Q12 1,3-Di-n-propylbenzene 0.035 0.029 0.017 9.966

226 118.004 Q11 C11 - Aromatic - 11 0.019 0.016 0.010 5.362

227 118.557 Q11 C11 - Aromatic - 12 0.015 0.013 0.008 4.314

228 123.440 91-57-6 G11 2-Methylnaphthalene 0.011 0.008 0.006 3.391

229 124.305 90-12-0 G11 1-Methylnaphthalene 0.005 0.004 0.003 1.596

230 126.296 ? Unidentified 0.007 0.006 0.003 2.243

231 130.001 ? Unidentified 0.003 0.002 0.002 0.999

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C-430
Hydrocarbon Expert V4.7 Thu Aug 26 17:04:50 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91324 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91324

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 7.554 74-98-6 Propane 0.006 0.009 0.011 1.666

10.023 106-97-8 n-Butane 0.479 0.613 0.652 127.567

18.116 109-66-0 n-Pentane 1.183 1.399 1.297 317.000

35.800 110-54-3 n-Hexane 0.839 0.942 0.770 225.643

58.056 142-82-5 n-Heptane 0.584 0.632 0.461 157.722

77.869 111-65-9 n-Octane 0.472 0.497 0.327 127.728

91.729 111-84-2 n-Nonane 0.278 0.286 0.171 75.261

102.799 124-18-5 n-Decane 0.020 0.020 0.011 5.489

111.709 1120-21-4 n-Undecane 0.030 0.030 0.015 8.135

I-Paraffins 8.810 75-28-5 i-Butane 0.052 0.069 0.071 13.823

10.638 463-82-1 2,2-Dimethylpropane 0.012 0.015 0.013 3.130

15.078 78-78-4 i-Pentane 4.183 5.000 4.586 1121.004

23.096 75-83-2 2,2-Dimethylbutane 0.094 0.107 0.086 25.259

28.340 79-29-8 2,3-Dimethylbutane 1.146 1.283 1.052 308.342

29.421 107-83-5 2-Methylpentane 2.676 3.034 2.456 719.907

32.069 96-14-0 3-Methylpentane 1.617 1.803 1.484 435.084

42.237 108-08-7 2,4-Dimethylpentane 0.820 0.903 0.647 221.463

42.781 464-06-2 2,2,3-Trimethylbutane 0.052 0.056 0.041 14.023

50.672 591-76-4 2-Methylhexane 1.518 1.657 1.198 410.084

52.492 589-34-4 3-Methylhexane 0.552 0.595 0.436 149.226

55.232 540-84-1 2,2,4-Trimethylpentane 11.022 11.796 7.632 2983.199

62.847 590-73-8 2,2-Dimethylhexane 0.027 0.028 0.018 7.211

64.950 564-02-3 2,2,3-Trimethylpentane 0.546 0.565 0.378 147.830

65.182 592-13-2 2,5-Dimethylhexane 1.242 1.326 0.860 336.147

65.519 589-43-5 2,4-Dimethylhexane 1.139 1.204 0.789 308.287

66.741 563-16-6 3,3-Dimethylhexane 0.019 0.020 0.013 5.067

68.509 565-75-3 2,3,4-Trimethylpentane 4.276 4.403 2.961 1157.167

69.188 560-21-4 2,3,3-Trimethylpentane 4.740 4.833 3.282 1282.747

70.799 584-94-1 2,3-Dimethylhexane 1.127 1.172 0.780 304.957

72.048 592-27-8 2-Methylheptane 0.243 0.258 0.168 65.714

72.310 589-53-7 4-Methylheptane 0.185 0.194 0.128 50.063

73.360 589-81-1 3-Methylheptane 0.210 0.220 0.145 56.789

73.561 619-99-8 3-Ethylhexane 0.100 0.104 0.069 27.147

75.260 3522-94-9 2,2,5-Trimethylhexane 1.994 2.088 1.230 540.830

80.353 1069-53-0 2,3,5-Trimethylhexane 0.330 0.338 0.203 89.373

81.518 1071-26-7 2,4-Dimethylheptane 0.069 0.072 0.043 18.763

82.473 1072-05-5 2,6-Dimethylheptane 0.105 0.109 0.065 28.373

83.404 2,5-Dimethylheptane 0.201 0.208 0.124 54.408

83.580 926-82-9 3,5-Dimethylheptane 0.024 0.025 0.015 6.558

86.751 3,5-Dimethylheptane 0.009 0.009 0.005 2.310

86.879 1067-20-5 3,3-Diethylpentane 0.008 0.007 0.005 2.038

87.272 2216-34-4 4-Methyloctane 0.047 0.048 0.029 12.776

87.404 3221-61-2 2-Methyloctane 0.063 0.065 0.039 17.010

88.10615869-80-4 Heptane, 3-ethyl- 0.008 0.009 0.005 2.293

88.267 2216-33-3 3-Methyloctane 0.062 0.063 0.038 16.679

89.321 C10 - IsoParaffin - 1 0.344 0.350 0.191 93.372

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C-431
Hydrocarbon Expert V4.7 Thu Aug 26 17:04:50 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91324 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91324

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

I-Paraffins 90.16414720-74-2 2,2,4-trimethylheptane 0.247 0.251 0.137 67.095

94.06115869-87-1 2,2-Dimethyloctane 0.019 0.019 0.010 5.100

94.86315869-89-3 2,5-Dimethyloctane 0.012 0.013 0.007 3.388

95.066 C10 - IsoParaffin - 2 0.007 0.007 0.004 1.960

95.504 2051-30-1 2,4-Dimethyloctane 0.022 0.022 0.012 6.003

95.891 2,6-Dimethyloctane 0.010 0.010 0.006 2.798

98.90517301-94-8 4-Methylnonane 0.011 0.011 0.006 3.045

99.112 2,2,6-Trimethyloctane 0.344 0.351 0.191 93.565

99.884 5911-04-6 3-Methylnonane 0.015 0.015 0.008 3.948

100.696 C11-Isoparaffin-2 0.033 0.033 0.017 9.019

102.33317302-01-1 3-Ethyl-3-methylheptane 0.061 0.061 0.031 16.694

104.406 C11 Isoparaffin-4 0.009 0.009 0.005 2.434

106.352 C11-Isoparaffin-7 0.152 0.152 0.077 41.437

108.561 C11- Isoparaffin-11 0.328 0.326 0.166 89.233

113.130 C12 - IsoParaffin - 1 0.008 0.008 0.004 2.293

116.248 C12 - IsoParaffin - 4 0.004 0.004 0.002 1.205

Aromatics

Mono-Aromatics 45.635 71-42-3 Benzene 0.743 0.626 0.752 220.396

69.028 108-88-3 Toluene 5.029 4.295 4.317 1476.457

84.728 100-41-4 Ethylbenzene 0.894 0.764 0.666 260.567

85.952 108-38-3 m-Xylene 2.374 2.034 1.769 691.839

86.098 106-42-3 p-Xylene 1.058 0.910 0.789 308.408

88.926 95-47-6 o-Xylene 0.790 0.665 0.589 230.183

93.093 98-82-8 i-Propylbenzene 0.030 0.025 0.019 8.543

96.552 103-65-1 n-Propylbenzene 0.253 0.217 0.166 73.177

97.398 620-14-4 1-Methyl-3-ethylbenzene 0.954 0.817 0.628 276.302

97.631 622-96-8 1-Methyl-4-ethylbenzene 0.442 0.380 0.291 127.883

98.257 108-67-8 1,3,5-Trimethylbenzene 0.557 0.477 0.366 161.221

99.342 611-14-3 1-Methyl-2-ethylbenzene 0.325 0.273 0.214 94.131

100.972 95-63-6 1,2,4-Trimethylbenzene 1.526 1.290 1.004 441.812

102.647 538-93-2 i-Butylbenzene 0.073 0.063 0.043 21.031

103.847 526-73-8 1,2,3-Trimethylbenzene 0.190 0.158 0.125 55.090

104.212 535-77-3 1-Methyl-3-i-propylbenzene 0.008 0.007 0.005 2.444

104.614 99-87-6 1-Methyl-4-i-propylbenzene 0.062 0.053 0.036 17.809

106.545 141-93-5 1,3-Diethylbenzene 0.023 0.020 0.014 6.684

106.830 1074-43-7 1-Methyl-3-n-propylbenzene 0.479 0.412 0.282 137.958

107.157 105-05-5 1,4-Diethylbenzene 0.180 0.155 0.106 51.889

107.380 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.108 0.091 0.064 31.187

107.620 135-01-3 1,2-Diethylbenzene 0.039 0.033 0.023 11.236

108.232 1074-17-5 1-Methyl-2-n-propylbenzene 0.043 0.036 0.025 12.367

109.739 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.268 0.227 0.158 77.278

110.285 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.318 0.265 0.187 91.604

111.411 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.060 0.050 0.035 17.256

111.861 4218-48-8 1-Ethyl-4-i-propylbenzene 0.041 0.034 0.022 11.745

112.346 1,2,4,5-Tetramethylbenzene 0.204 0.170 0.120 58.779

112.613 527-53-7 1,2,3,5-Tetramethylbenzene 0.280 0.233 0.165 80.518

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C-432
Hydrocarbon Expert V4.7 Thu Aug 26 17:04:50 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91324 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91324

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 113.760 C11 - Aromatic - 3 0.050 0.041 0.027 14.268

114.069 1,2-Di-i-propylbenzene 0.033 0.028 0.016 9.526

114.284 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.045 0.037 0.024 12.876

114.448 C11 - Aromatic - 4 0.031 0.026 0.016 8.790

114.847 5161-04-6 Benzene, 1-methyl-4-(2-methylpropyl)-0.028 0.023 0.015 7.980

115.257 538-68-1 n-Pentylbenzene 0.011 0.009 0.006 3.227

115.484 tert-Pentylbenzene 0.046 0.039 0.025 13.291

115.798 577-55-9 1-Methyl-2-n-butylbenzene 0.020 0.017 0.011 5.802

115.908 C11 - Aromatic - 6 0.032 0.028 0.017 9.217

116.367 100-18-5 1,4-Di-i-propylbenzene 0.038 0.032 0.019 10.926

117.594 7364-19-4 1t-Butyl-4-ethylbenzene 0.006 0.005 0.003 1.719

117.893 1,3-Di-n-propylbenzene 0.035 0.029 0.017 9.966

118.004 C11 - Aromatic - 11 0.019 0.016 0.010 5.362

118.557 C11 - Aromatic - 12 0.015 0.013 0.008 4.314

Naphthalenes 116.809 91-20-3 Naphthalene 0.112 0.081 0.069 33.752

123.440 91-57-6 2-Methylnaphthalene 0.011 0.008 0.006 3.391

124.305 90-12-0 1-Methylnaphthalene 0.005 0.004 0.003 1.596

Naphtheno/Olefino-Benzs 113.944 874-35-1 5-Methylindan 0.090 0.075 0.054 25.798

114.941 824-63-5 2-Methylindan 0.088 0.073 0.053 25.317

Indenes 105.043 Indan 0.070 0.054 0.047 20.739

105.637 Indene 0.365 0.281 0.245 107.521

109.393 2-Methylindan 0.056 0.043 0.034 16.550

114.693 824-22-6 4-Methylindan 0.115 0.096 0.069 33.114

117.409 Dimethyl Indane - 1 0.004 0.003 0.002 1.189

Naphthenes

Mono-Naphthenes 27.605 287-92-3 Cyclopentane 0.150 0.149 0.169 41.421

40.669 96-37-7 Methylcyclopentane 1.028 1.017 0.966 283.247

47.552 110-82-7 Cyclohexane 0.474 0.450 0.445 130.535

53.353 1759-58-6 1t,3-Dimethylcyclopentane 0.152 0.150 0.122 41.855

53.940 2532-58-3 1c,3-Dimethylcyclopentane 0.117 0.116 0.094 32.205

54.566 822-50-4 1t,2-Dimethylcyclopentane 0.160 0.158 0.129 44.160

55.611 C7 - MonoNaph - 1 0.028 0.027 0.020 7.645

59.64816491-15-9 Cyclopentene, 1,5-dimethyl- 0.018 0.018 0.015 4.962

61.518 108-87-2 Methylcyclohexane 0.886 0.852 0.714 244.129

62.457 4516-69-2 1,1,3-Trimethylcyclopentane 0.027 0.026 0.019 7.338

64.294 1640-89-7 Ethylcyclopentane 0.049 0.047 0.039 13.470

66.349 4850-28-6 1c,2t,4-Trimethylcyclopentane 0.027 0.026 0.019 7.392

67.86215890-40-1 1t,2c,3-Trimethylcyclopentane 0.024 0.023 0.017 6.647

73.224 1,3-dimethyl-t-cyclohexane 0.155 0.149 0.109 42.805

75.609 3c-Ethylmethylcyclopentane 0.009 0.009 0.006 2.528

75.826 3t-Ethylmethylcyclopentane 0.013 0.012 0.009 3.495

81.367 2207-01-4 1c,2-Dimethylcyclohexane 0.013 0.012 0.009 3.629

82.173 1678-91-7 Ethylcyclohexane 0.108 0.102 0.076 29.739

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C-433
Hydrocarbon Expert V4.7 Thu Aug 26 17:04:50 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91324 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91324

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Naphthenes 89.909 trans-1,3-Diethylcyclopentane 0.017 0.015 0.011 5.039

92.301 4926-90-3 1,1-Methylethylcyclohexane 0.012 0.011 0.008 3.438

101.548 1678-98-4 i-Butylcyclohexane 0.007 0.006 0.004 1.869

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.624 115-11-7 Isobutene 0.017 0.021 0.023 4.570

9.665 106-98-9 Butene-1 0.018 0.023 0.026 5.010

10.510 624-64-6 t-Butene-2 0.074 0.091 0.105 20.522

11.252 590-18-1 c-Butene-2 0.088 0.105 0.124 24.230

16.732 109-67-1 Pentene-1 0.338 0.391 0.381 93.178

19.234 646-04-8 t-Pentene-2 0.858 0.980 0.968 236.495

20.269 627-20-3 c-Pentene-2 0.470 0.531 0.530 129.585

33.446 592-41-6 Hexene-1 0.160 0.175 0.151 44.141

36.43713269-52-8 t-Hexene-3 0.263 0.285 0.247 72.471

36.915 4050-45-7 t-Hexene-2 0.403 0.438 0.379 111.187

38.740 7688-21-3 c-Hexene-2 0.214 0.229 0.201 58.924

57.33114686-14-7 t-Heptene-3 0.032 0.033 0.025 8.702

58.273 7642-10-6 c-Heptene-3 0.024 0.026 0.020 6.752

59.17214686-13-6 t-Heptene-2 0.013 0.014 0.011 3.658

110.903 693-61-8 2-Undecene, (E)- 0.026 0.026 0.015 7.039

Iso-Olefins 13.453 563-45-1 3-Methylbutene-1 0.225 0.265 0.254 61.956

17.583 563-46-2 2-Methylbutene-1 0.514 0.585 0.579 141.572

20.945 513-35-9 2-Methylbutene-2 1.053 1.177 1.187 290.107

29.203 691-38-3 4-Methyl-c-pentene-2 0.046 0.051 0.044 12.794

29.842 674-76-0 4-Methyl-t-pentene-2 0.132 0.145 0.124 36.274

33.225 763-29-1 2-Methylpentene-1 0.224 0.243 0.211 61.862

35.641 760-21-4 2-Ethylbutene-1 0.069 0.074 0.065 19.089

37.410 625-27-4 2-Methylpentene-2 0.341 0.366 0.321 94.058

37.823 922-62-3 3-Methyl-c-pentene-2 0.264 0.280 0.248 72.747

40.084 3404-73-7 3,3-Dimethylpentene-1 0.308 0.325 0.248 85.004

42.535 594-56-9 2,3,3-Trimethylbutene-1 0.013 0.014 0.011 3.669

46.640 3404-61-3 3-Methylhexene-1 0.015 0.016 0.012 4.234

47.228 3524-73-0 5-Methylhexene-1 0.042 0.044 0.034 11.469

49.27115840-60-5 2-Methyl-c-hexene-3 0.040 0.043 0.032 11.089

49.619 3769-23-1 4-Methylhexene-1 0.011 0.011 0.009 3.003

50.265 3404-55-5 4-Methyl-t/c-hexene-2 0.051 0.053 0.041 13.947

54.899 C7 - Iso-Olefin - 2 0.021 0.022 0.017 5.859

56.802 4914-89-0 3-Methyl-c-hexene-3 0.014 0.014 0.011 3.772

57.684 6094-02-6 2-Methylhexene-1 0.057 0.060 0.046 15.641

58.547 2738-19-4 2-Methyl-2-hexene 0.026 0.027 0.021 7.167

58.79110574-36-4 3-Methyl-c-hexene-2 0.020 0.021 0.016 5.445

60.07520710-38-8 3-Methyl-t-hexene-2 0.015 0.015 0.012 4.089

60.858 4914-91-4 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.014 0.011 3.669

70.514 C8 - Diolefin - 1 0.010 0.010 0.007 2.769

80.905 C9 - IsoOlefin - 1 0.016 0.015 0.011 4.377

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C-434
Hydrocarbon Expert V4.7 Thu Aug 26 17:04:50 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91324 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91324

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Iso-Olefins 86.487 C9-IsoOlefin-3 0.014 0.014 0.009 3.924

Naphtheno-Olefins 22.537 1574-41-0 1,3-Cyclopentadiene 0.007 0.007 0.008 1.979

25.742 142-29-0 Cyclopentene 0.199 0.191 0.231 56.449

37.041 1120-62-3 3-Methylcyclopentene 0.101 0.098 0.097 27.771

45.833 693-89-0 1-Methylcyclopentene 0.359 0.341 0.346 101.275

51.153 110-83-8 Cyclohexene 0.044 0.040 0.043 12.219

Di-Olefins 18.625 78-79-5 2-Methyl-1,3-Butadiene 0.011 0.012 0.012 3.013

21.270 2004-70-8 1t,3-Pentadiene 0.016 0.017 0.018 4.430

45.427 1528-30-9 C6-Diolefin-1 0.015 0.015 0.014 4.112

Oxygenates 13.126 64-17-5 Ethanol 22.540 21.154 38.700 2558.100

26.896 71-23-8 n-Propanol 0.081 0.075 0.106 15.535

48.058 71-36-3 n-Butanol 0.055 0.051 0.058 11.385

Unidentified 19.877 Unidentified 0.006 0.007 0.007 1.976

27.000 Unidentified 0.057 0.063 0.054 19.256

28.736 Unidentified 0.053 0.053 0.048 17.997

63.360 Unidentified 0.052 0.054 0.038 17.660

72.448 Unidentified 0.089 0.092 0.062 30.210

74.457 Unidentified 0.025 0.024 0.018 8.607

76.233 Unidentified 0.015 0.014 0.010 4.926

76.532 Unidentified 0.059 0.056 0.041 19.802

78.820 Unidentified 0.050 0.048 0.035 16.755

82.974 Unidentified 0.024 0.023 0.017 8.014

84.901 Unidentified 0.028 0.028 0.018 9.343

85.145 Unidentified 0.031 0.030 0.020 10.555

86.230 Unidentified 0.067 0.068 0.041 22.611

86.594 Unidentified 0.013 0.013 0.008 4.223

88.743 Unidentified 0.107 0.116 0.067 36.142

93.271 Unidentified 0.007 0.007 0.005 2.442

93.271 Unidentified 0.007 0.008 0.004 2.442

93.271 Unidentified 0.007 0.005 0.004 2.442

93.839 Unidentified 0.050 0.051 0.028 16.961

100.349 Unidentified 0.023 0.017 0.011 7.617

100.480 Unidentified 0.060 0.060 0.030 20.252

101.162 Unidentified 0.042 0.045 0.024 14.311

101.283 Unidentified 0.025 0.026 0.014 8.583

102.896 Unidentified 0.014 0.012 0.008 4.698

103.196 Unidentified 0.017 0.017 0.009 5.905

108.079 Unidentified 0.038 0.038 0.019 12.775

108.353 Unidentified 0.045 0.045 0.023 15.040

108.435 Unidentified 0.041 0.041 0.021 13.925

108.743 Unidentified 0.106 0.106 0.054 35.927

109.166 Unidentified 0.448 0.378 0.264 151.280

110.709 Unidentified 0.011 0.010 0.006 3.688

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C-435
Hydrocarbon Expert V4.7 Thu Aug 26 17:04:50 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91324 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91324

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Unidentified 111.037 Unidentified 0.062 0.062 0.035 20.808

111.309 Unidentified 0.054 0.047 0.029 18.125

111.972 Unidentified 0.024 0.020 0.013 8.189

112.955 Unidentified 0.005 0.004 0.003 1.804

113.484 Unidentified 0.019 0.019 0.009 6.391

113.609 Unidentified 0.006 0.006 0.003 2.050

115.143 Unidentified 0.010 0.010 0.005 3.289

116.942 Unidentified 0.013 0.013 0.006 4.352

117.125 Unidentified 0.004 0.003 0.002 1.303

117.246 Unidentified 0.009 0.008 0.004 3.053

126.296 Unidentified 0.007 0.006 0.003 2.243

130.001 Unidentified 0.003 0.002 0.002 0.999

Plus

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C-436
Hydrocarbon Expert V4.7 Thu Aug 26 17:04:50 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91324 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91324

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF

20.0 15.0 10.0 5.0 0.0

Propane

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

Ethanol

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

Unidentified

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

1,3-Cyclopentadiene

2,2-Dimethylbutane

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C-437
Hydrocarbon Expert V4.7 Thu Aug 26 17:04:50 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91324 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91324

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

n-Propanol Unidentified

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

2-Ethylbutene-1 n-Hexane

t-Hexene-3

t-Hexene-2 3-Methylcyclopentene

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane 2,3,3-Trimethylbutene-1 2,2,3-Trimethylbutane

C6-Diolefin-1Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1

Cyclohexane

n-Butanol

2-Methyl-c-hexene-3

4-Methylhexene-1

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C-438
Hydrocarbon Expert V4.7 Thu Aug 26 17:04:50 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91324 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91324

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF

70.0 65.0 60.0 55.0 50.0

4-Methyl-t/c-hexene-2

2-Methylhexane

Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane

C7 - Iso-Olefin - 2

2,2,4-Trimethylpentane

C7 - MonoNaph - 1

3-Methyl-c-hexene-3

t-Heptene-3

2-Methylhexene-1

n-Heptane c-Heptene-3 2-Methyl-2-hexene 3-Methyl-c-hexene-2

t-Heptene-2

Cyclopentene, 1,5-dimethyl3-Methyl-t-hexene-2

2-Pentene, 3,4-dimethyl-, (Z)-

Methylcyclohexane

1,1,3-Trimethylcyclopentane

2,2-Dimethylhexane

Unidentified

Ethylcyclopentane

2,2,3-Trimethylpentane 2,5-Dimethylhexane

2,4-Dimethylhexane

1c,2t,4-Trimethylcyclopentane

3,3-Dimethylhexane

1t,2c,3-Trimethylcyclopentane

2,3,4-Trimethylpentane

Toluene 2,3,3-Trimethylpentane

C8 - Diolefin - 1 2,3-Dimethylhexane

2-Methylheptane

Unidentified 4-Methylheptane

1,3-dimethyl-t-cyclohexane 3-Methylheptane 3-Ethylhexane

Unidentified

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C-439
Hydrocarbon Expert V4.7 Thu Aug 26 17:04:50 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91324 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91324

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF

95.0 90.0 85.0 80.0 75.0

2,2,5-Trimethylhexane

3c-Ethylmethylcyclopentane 3t-Ethylmethylcyclopentane

Unidentified Unidentified

n-Octane

Unidentified

2,3,5-Trimethylhexane

C9 - IsoOlefin - 1

1c,2-Dimethylcyclohexane 2,4-Dimethylheptane

Ethylcyclohexane 2,6-Dimethylheptane

Unidentified

2,5-Dimethylheptane 3,5-Dimethylheptane

Ethylbenzene Unidentified

m-Xylene Unidentified p-Xylene

C9-IsoOlefin-3 Unidentified 3,5-Dimethylheptane 3,3-Diethylpentane

4-Methyloctane 2-Methyloctane

Heptane, 3-ethyl- 3-Methyloctane

Unidentified o-Xylene

C10 - IsoParaffin - 1

trans-1,3-Diethylcyclopentane 2,2,4-trimethylheptane

n-Nonane

1,1-Methylethylcyclohexane

i-Propylbenzene Unidentified

Unidentified 2,2-Dimethyloctane

2,5-Dimethyloctane C10 - IsoParaffin - 2

2,4-Dimethyloctane

2,6-Dimethyloctane

n-Propylbenzene

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

4-Methylnonane 2,2,6-Trimethyloctane 1-Methyl-2-ethylbenzene

3-Methylnonane

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C-440
Hydrocarbon Expert V4.7 Thu Aug 26 17:04:50 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91324 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91324

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified

C11-Isoparaffin-2 1,2,4-Trimethylbenzene Unidentified

i-Butylcyclohexane

3-Ethyl-3-methylheptane i-Butylbenzene Unidentified n-Decane

Unidentified

1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene C11 Isoparaffin-4 1-Methyl-4-i-propylbenzene

Indan

Indene

C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene

1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

Unidentified 1-Methyl-2-n-propylbenzene Unidentified C11- Isoparaffin-11 Unidentified

Unidentified 2-Methylindan

1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

Unidentified 2-Undecene, (E)- Unidentified Unidentified 1,2-Dimethyl-3-ethylbenzene n-Undecane Unidentified 1-Ethyl-4-i-propylbenzene

1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene

Unidentified C12 - IsoParaffin - 1

Unidentified C11 - Aromatic - 3 5-Methylindan 1,2-Di-i-propylbenzene 1-methyl-4-(1-methylpropyl)be C11 - Aromatic - 4 4-Methylindan Benzene, 1-methyl-4-(2-methylpropyl)- 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene

1-Methyl-2-n-butylbenzene C11 - Aromatic - 6

C12 - IsoParaffin - 4 1,4-Di-i-propylbenzene

Unidentified Naphthalene

Dimethyl Indane - 1 1t-Butyl-4-ethylbenzene

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

C11 - Aromatic - 12

2-Methylnaphthalene

1-Methylnaphthalene

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C-441
Hydrocarbon Expert V4.7 Thu Aug 26 17:04:50 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF 25-Aug-10, 01:11:34

Sample: ODDB-91324 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91324

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000006.D\SIG2000006_FID2_B.CDF

145.0 140.0 135.0 130.0 125.0

Unidentified

Unidentified

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C-442
Hydrocarbon Expert V4.7 Fri Aug 27 10:14:49 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91325 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91325

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 7.251 8.696 6.920

I-Paraffins 15.239 17.679 12.652

Aromatics 41.806 37.213 31.116

Mono-Aromatics 40.748 36.345 30.468

Naphthalenes 0.132 0.100 0.078

Naphtheno/Olefino-Benzs 0.220 0.191 0.128

Indenes 0.706 0.577 0.442

Naphthenes 5.215 5.296 4.455

Mono-Naphthenes 5.215 5.296 4.455

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 7.049 8.064 7.070

n-Olefins 2.900 3.403 3.005

Iso-Olefins 3.426 3.935 3.346

Naphtheno-Olefins 0.683 0.681 0.676

Di-Olefins 0.040 0.044 0.042

Oxygenates 22.006 21.592 36.603

Unidentified 1.433 1.459 1.183

Plus 0.000 0.000 0.000

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C-443
Hydrocarbon Expert V4.7 Fri Aug 27 10:14:49 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91325 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91325

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C2 21.878 21.468 36.452

C3 0.082 0.083 0.108

C4 1.214 1.593 1.596

C5 9.521 11.575 10.251

C6 13.490 15.037 12.201

C7 21.417 20.135 17.540

C8 18.508 17.133 13.227

C9 6.610 6.102 4.173

C10 5.022 4.653 2.854

C11 0.671 0.628 0.342

C12 0.153 0.133 0.073

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C-444
Hydrocarbon Expert V4.7 Fri Aug 27 10:14:49 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91325 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91325

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C3 0.007 0.010 0.011

C4 0.926 1.238 1.223

C5 1.956 2.418 2.081

C6 2.865 3.364 2.552

C7 0.733 0.830 0.561

C8 0.518 0.571 0.348

C9 0.199 0.215 0.119

C10 0.029 0.030 0.015

C11 0.018 0.019 0.009

I-Paraffins C4 0.047 0.066 0.062

C5 3.824 4.778 4.068

C6 4.638 5.457 4.131

C7 1.899 2.159 1.455

C8 2.166 2.365 1.455

C9 1.003 1.090 0.600

C10 1.441 1.531 0.771

C11 0.222 0.231 0.109

Mono-Aromatics C6 0.663 0.584 0.652

C7 16.289 14.546 13.570

C8 15.366 13.738 11.110

C9 5.257 4.672 3.357

C10 2.642 2.339 1.511

C11 0.384 0.339 0.199

C12 0.147 0.128 0.069

Naphthalenes C10 0.118 0.089 0.071

C11 0.014 0.011 0.007

Naphtheno/Olefino-Benzs C10 0.220 0.191 0.128

Indenes C9 0.119 0.095 0.077

C10 0.560 0.460 0.351

C11 0.021 0.017 0.011

C12 0.007 0.005 0.004

Mono-Naphthenes C5 0.203 0.210 0.222

C6 2.805 2.854 2.558

C7 1.734 1.760 1.355

C8 0.429 0.430 0.294

C9 0.032 0.029 0.020

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C-445
Hydrocarbon Expert V4.7 Fri Aug 27 10:14:49 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91325 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91325

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Mono-Naphthenes C10 0.013 0.012 0.007

n-Olefins C4 0.187 0.238 0.256

C5 1.599 1.908 1.750

C6 1.006 1.140 0.918

C7 0.096 0.106 0.075

C11 0.012 0.012 0.006

Iso-Olefins C5 1.716 2.031 1.879

C6 1.028 1.156 0.938

C7 0.653 0.719 0.510

C8 0.029 0.029 0.020

Naphtheno-Olefins C5 0.198 0.199 0.223

C6 0.485 0.482 0.453

Di-Olefins C5 0.025 0.029 0.029

C7 0.014 0.015 0.014

Oxygenates C2 21.878 21.468 36.452

C3 0.076 0.073 0.096

C4 0.053 0.051 0.055

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C-446
Hydrocarbon Expert V4.7 Fri Aug 27 10:14:49 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91325 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91325

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 25.32 23.88

5% 81.75 80.87

10% 100.89 96.79

15% 144.75 138.31

20% 155.48 152.87

25% 172.32 158.64

30% 172.57 172.37

35% 172.82 172.62

40% 173.06 172.87

45% 174.18 173.12

50% 208.82 177.08

55% 230.78 212.13

60% 230.89 230.81

65% 231.01 230.94

70% 243.86 231.06

75% 278.85 276.87

80% 281.46 281.08

85% 282.32 282.07

90% 323.02 321.27

95% 350.79 340.83

FBP 403.88 399.78

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C-447
Hydrocarbon Expert V4.7 Fri Aug 27 10:14:49 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91325 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91325

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 7.554 74-98-6 P3 Propane 0.007 0.010 0.011 1.866

2 8.810 75-28-5 I4 i-Butane 0.047 0.066 0.062 13.628

3 9.624 115-11-7 K4 Isobutene 0.015 0.020 0.021 4.617

4 9.665 106-98-9 K4 Butene-1 0.017 0.023 0.024 5.177

5 10.024 106-97-8 P4 n-Butane 0.926 1.238 1.223 266.821

6 10.510 624-64-6 K4 t-Butene-2 0.071 0.091 0.097 21.138

7 10.637 463-82-1 I5 2,2-Dimethylpropane 0.011 0.015 0.012 3.299

8 11.250 590-18-1 K4 c-Butene-2 0.084 0.104 0.115 24.994

9 13.136 64-17-5 X2 Ethanol 21.878 21.468 36.452 2688.961

10 13.454 563-45-1 C5 3-Methylbutene-1 0.214 0.264 0.234 63.815

11 15.076 78-78-4 I5 i-Pentane 3.812 4.764 4.056 1106.312

12 16.728 109-67-1 K5 Pentene-1 0.324 0.392 0.355 96.787

13 17.579 563-46-2 C5 2-Methylbutene-1 0.492 0.586 0.539 146.973

14 18.114 109-66-0 P5 n-Pentane 1.956 2.418 2.081 567.543

15 18.629 78-79-5 E5 2-Methyl-1,3-Butadiene 0.010 0.012 0.011 3.130

16 19.235 646-04-8 K5 t-Pentene-2 0.823 0.983 0.901 245.725

17 19.876 ? Unidentified 0.006 0.007 0.006 2.085

18 20.264 627-20-3 K5 c-Pentene-2 0.451 0.533 0.494 134.738

19 20.946 513-35-9 C5 2-Methylbutene-2 1.010 1.181 1.106 301.538

20 21.271 2004-70-8 E5 1t,3-Pentadiene 0.015 0.018 0.017 4.700

21 22.541 1574-41-0 B5 1,3-Cyclopentadiene 0.007 0.008 0.008 2.088

22 23.095 75-83-2 I6 2,2-Dimethylbutane 0.126 0.150 0.112 36.741

23 25.745 142-29-0 B5 Cyclopentene 0.191 0.192 0.215 58.746

24 26.897 71-23-8 X3 n-Propanol 0.076 0.073 0.096 15.782

25 26.999 ? Unidentified 0.056 0.065 0.051 20.474

26 27.606 287-92-3 M5 Cyclopentane 0.203 0.210 0.222 60.480

27 28.335 79-29-8 I6 2,3-Dimethylbutane 0.449 0.525 0.400 130.697

28 28.734 ? Unidentified 0.054 0.056 0.047 19.662

29 29.190 691-38-3 C6 4-Methyl-c-pentene-2 0.045 0.051 0.041 13.314

30 29.422 107-83-5 I6 2-Methylpentane 2.318 2.748 2.065 675.380

31 29.836 674-76-0 C6 4-Methyl-t-pentene-2 0.127 0.146 0.116 37.802

32 32.063 96-14-0 I6 3-Methylpentane 1.745 2.034 1.554 508.409

33 33.224 763-29-1 C6 2-Methylpentene-1 0.216 0.245 0.197 64.584

34 33.448 592-41-6 K6 Hexene-1 0.155 0.177 0.141 46.181

35 35.649 760-21-4 C6 2-Ethylbutene-1 0.057 0.063 0.052 16.939

36 35.812 110-54-3 P6 n-Hexane 2.865 3.364 2.552 834.756

37 36.44413269-52-8 K6 t-Hexene-3 0.254 0.288 0.232 75.829

38 36.913 4050-45-7 K6 t-Hexene-2 0.391 0.443 0.356 116.663

39 37.040 1120-62-3 B6 3-Methylcyclopentene 0.096 0.097 0.089 28.535

40 37.405 625-27-4 C6 2-Methylpentene-2 0.329 0.369 0.300 98.243

41 37.819 922-62-3 C6 3-Methyl-c-pentene-2 0.255 0.282 0.232 75.981

42 38.740 7688-21-3 K6 c-Hexene-2 0.207 0.231 0.189 61.700

43 40.086 3404-73-7 C7 3,3-Dimethylpentene-1 0.297 0.328 0.232 88.758

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C-448
Hydrocarbon Expert V4.7 Fri Aug 27 10:14:49 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91325 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91325

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 40.671 96-37-7 M6 Methylcyclopentane 1.630 1.686 1.487 486.537

45 42.230 108-08-7 I7 2,4-Dimethylpentane 0.278 0.320 0.213 81.360

46 42.529 594-56-9 C7 2,3,3-Trimethylbutene-1 0.013 0.014 0.010 3.926

47 42.776 464-06-2 I7 2,2,3-Trimethylbutane 0.037 0.042 0.029 10.886

48 45.422 1528-30-9 E7 C6-Diolefin-1 0.014 0.015 0.014 4.320

49 45.633 71-42-3 Q6 Benzene 0.663 0.584 0.652 213.261

50 45.832 693-89-0 B6 1-Methylcyclopentene 0.346 0.344 0.324 105.906

51 46.635 3404-61-3 C7 3-Methylhexene-1 0.015 0.017 0.012 4.448

52 47.233 3524-73-0 C7 5-Methylhexene-1 0.068 0.075 0.053 20.179

53 47.555 110-82-7 M6 Cyclohexane 1.175 1.168 1.071 350.637

54 48.053 71-36-3 X4 n-Butanol 0.053 0.051 0.055 11.979

55 49.27015840-60-5 C7 2-Methyl-c-hexene-3 0.039 0.043 0.030 11.625

56 49.617 3769-23-1 C7 4-Methylhexene-1 0.010 0.011 0.008 3.058

57 50.265 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.049 0.054 0.038 14.576

58 50.659 591-76-4 I7 2-Methylhexane 0.946 1.080 0.725 276.837

59 50.838 ? Unidentified 0.063 0.071 0.051 23.206

60 51.151 110-83-8 B6 Cyclohexene 0.043 0.041 0.040 12.780

61 52.491 589-34-4 I7 3-Methylhexane 0.637 0.718 0.488 186.352

62 53.351 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.179 0.185 0.140 53.382

63 53.936 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.141 0.146 0.110 42.044

64 54.559 822-50-4 M7 1t,2-Dimethylcyclopentane 0.206 0.213 0.161 61.581

65 54.839 C7 C7 - Iso-Olefin - 2 0.021 0.023 0.017 6.409

66 55.142 540-84-1 I8 2,2,4-Trimethylpentane 0.058 0.065 0.039 16.961

67 55.466 592-76-7 K7 Heptene-1 0.028 0.031 0.022 8.311

68 56.799 4914-89-0 C7 3-Methyl-c-hexene-3 0.013 0.014 0.011 4.010

69 57.32914686-14-7 K7 t-Heptene-3 0.031 0.034 0.024 9.204

70 57.681 6094-02-6 C7 2-Methylhexene-1 0.055 0.061 0.043 16.479

71 58.055 142-82-5 P7 n-Heptane 0.733 0.830 0.561 214.390

72 58.272 7642-10-6 K7 c-Heptene-3 0.024 0.026 0.019 7.071

73 58.546 2738-19-4 C7 2-Methyl-2-hexene 0.025 0.027 0.020 7.518

74 58.79010574-36-4 C7 3-Methyl-c-hexene-2 0.019 0.021 0.015 5.684

75 59.17114686-13-6 K7 t-Heptene-2 0.013 0.015 0.010 3.986

76 59.64716491-15-9 M7 Cyclopentene, 1,5-dimethyl- 0.018 0.018 0.014 5.299

77 60.07520710-38-8 C7 3-Methyl-t-hexene-2 0.015 0.016 0.012 4.412

78 60.858 4914-91-4 C7 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.013 0.010 3.732

79 61.519 108-87-2 M7 Methylcyclohexane 1.134 1.141 0.887 338.516

80 62.457 4516-69-2 M8 1,1,3-Trimethylcyclopentane 0.032 0.033 0.022 9.620

81 62.846 590-73-8 I8 2,2-Dimethylhexane 0.027 0.030 0.018 8.017

82 63.357 ? Unidentified 0.051 0.055 0.035 18.600

83 64.294 1640-89-7 M7 Ethylcyclopentane 0.056 0.056 0.044 16.693

84 64.943 564-02-3 I8 2,2,3-Trimethylpentane 0.074 0.080 0.050 21.734

85 65.167 592-13-2 I8 2,5-Dimethylhexane 0.169 0.189 0.113 49.503

86 65.504 589-43-5 I8 2,4-Dimethylhexane 0.163 0.180 0.110 47.824

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C-449
Hydrocarbon Expert V4.7 Fri Aug 27 10:14:49 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91325 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91325

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 66.343 4850-28-6 M8 1c,2t,4-Trimethylcyclopentane 0.032 0.032 0.022 9.483

88 66.738 563-16-6 I8 3,3-Dimethylhexane 0.021 0.023 0.014 6.121

89 67.85915890-40-1 M8 1t,2c,3-Trimethylcyclopentane 0.028 0.028 0.019 8.316

90 68.482 565-75-3 I8 2,3,4-Trimethylpentane 0.757 0.815 0.509 221.852

91 69.109 108-88-3 Q7 Toluene 16.289 14.546 13.570 5179.291

92 70.516 C8 C8 - Diolefin - 1 0.012 0.012 0.008 3.613

93 70.793 584-94-1 I8 2,3-Dimethylhexane 0.241 0.261 0.162 70.493

94 72.046 592-27-8 I8 2-Methylheptane 0.237 0.263 0.159 69.534

95 72.301 589-53-7 I8 4-Methylheptane 0.106 0.117 0.071 31.095

96 72.449 ? Unidentified 0.022 0.023 0.015 7.948

97 73.223 M8 1,3-dimethyl-t-cyclohexane 0.178 0.179 0.122 53.236

98 73.360 589-81-1 I8 3-Methylheptane 0.202 0.221 0.135 59.078

99 73.561 619-99-8 I8 3-Ethylhexane 0.111 0.121 0.075 32.604

100 74.456 ? Unidentified 0.029 0.028 0.020 10.431

101 75.247 3522-94-9 I9 2,2,5-Trimethylhexane 0.495 0.542 0.296 145.426

102 75.607 M8 3c-Ethylmethylcyclopentane 0.010 0.010 0.007 3.089

103 75.823 M8 3t-Ethylmethylcyclopentane 0.015 0.015 0.010 4.405

104 76.528 ? Unidentified 0.065 0.065 0.044 23.653

105 77.869 111-65-9 P8 n-Octane 0.518 0.571 0.348 151.827

106 78.822 ? Unidentified 0.015 0.015 0.010 5.428

107 80.350 1069-53-0 I9 2,3,5-Trimethylhexane 0.089 0.095 0.053 26.029

108 80.905 C8 C9 - IsoOlefin - 1 0.017 0.017 0.012 5.132

109 81.364 2207-01-4 M8 1c,2-Dimethylcyclohexane 0.015 0.014 0.010 4.332

110 81.519 1071-26-7 I9 2,4-Dimethylheptane 0.036 0.039 0.022 10.576

111 82.172 1678-91-7 M8 Ethylcyclohexane 0.119 0.118 0.082 35.624

112 82.474 1072-05-5 I9 2,6-Dimethylheptane 0.063 0.069 0.038 18.495

113 82.973 ? Unidentified 0.023 0.023 0.016 8.474

114 83.408 I9 2,5-Dimethylheptane 0.099 0.107 0.059 28.974

115 83.599 926-82-9 I9 3,5-Dimethylheptane 0.018 0.019 0.011 5.227

116 84.747 100-41-4 Q8 Ethylbenzene 2.730 2.437 1.973 861.317

117 85.154 ? Unidentified 0.017 0.017 0.010 6.281

118 86.002 108-38-3 Q8 m-Xylene 7.325 6.562 5.296 2311.502

119 86.140 106-42-3 Q8 p-Xylene 3.381 3.040 2.444 1066.798

120 86.596 ? Unidentified 0.012 0.012 0.007 4.383

121 86.762 I9 3,5-Dimethylheptane 0.010 0.010 0.006 2.838

122 86.881 1067-20-5 I9 3,3-Diethylpentane 0.008 0.008 0.005 2.329

123 87.276 2216-34-4 I9 4-Methyloctane 0.049 0.052 0.029 14.291

124 87.407 3221-61-2 I9 2-Methyloctane 0.064 0.070 0.039 18.913

125 88.10715869-80-4 I9 Heptane, 3-ethyl- 0.009 0.010 0.006 2.721

126 88.269 2216-33-3 I9 3-Methyloctane 0.064 0.069 0.038 18.740

127 88.745 ? Unidentified 0.033 0.037 0.020 11.959

128 88.941 95-47-6 Q8 o-Xylene 1.930 1.698 1.396 609.177

129 89.320 I10 C10 - IsoParaffin - 1 0.106 0.113 0.057 31.178

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C-450
Hydrocarbon Expert V4.7 Fri Aug 27 10:14:49 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91325 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91325

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 89.910 M9 trans-1,3-Diethylcyclopentane 0.019 0.017 0.012 6.149

131 90.16514720-74-2 I10 2,2,4-trimethylheptane 0.088 0.093 0.047 25.752

132 91.741 111-84-2 P9 n-Nonane 0.199 0.215 0.119 58.575

133 92.299 4926-90-3 M9 1,1-Methylethylcyclohexane 0.013 0.012 0.008 3.841

134 93.093 98-82-8 Q9 i-Propylbenzene 0.032 0.028 0.020 9.888

135 93.838 ? Unidentified 0.048 0.052 0.026 17.710

136 94.06115869-87-1 I10 2,2-Dimethyloctane 0.020 0.021 0.011 5.885

137 94.524 ? Unidentified 0.004 0.003 0.337 1.604

138 94.524 ? Unidentified 0.004 0.005 0.002 1.604

139 94.86115869-89-3 I10 2,5-Dimethyloctane 0.031 0.033 0.017 9.035

140 95.066 I10 C10 - IsoParaffin - 2 0.011 0.011 0.006 3.153

141 95.326 2040-95-1 I10 2,7-Dimethyloctane 0.015 0.016 0.008 4.522

142 95.504 2051-30-1 I10 2,4-Dimethyloctane 0.061 0.065 0.033 17.847

143 95.892 I10 2,6-Dimethyloctane 0.021 0.022 0.011 6.175

144 96.552 103-65-1 Q9 n-Propylbenzene 0.287 0.258 0.183 90.070

145 97.400 620-14-4 Q9 1-Methyl-3-ethylbenzene 1.108 0.992 0.708 347.428

146 97.634 622-96-8 Q9 1-Methyl-4-ethylbenzene 0.514 0.462 0.328 161.116

147 98.259 108-67-8 Q9 1,3,5-Trimethylbenzene 0.684 0.612 0.437 214.426

148 98.71715869-85-9 I10 5-Methylnonane 0.006 0.007 0.003 1.877

149 98.90617301-94-8 I10 4-Methylnonane 0.015 0.016 0.008 4.450

150 99.117 I10 2,2,6-Trimethyloctane 0.922 0.983 0.498 271.438

151 99.343 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.383 0.337 0.245 120.200

152 99.885 5911-04-6 I10 3-Methylnonane 0.018 0.019 0.010 5.214

153 100.350 ? Unidentified 0.052 0.040 0.026 19.071

154 100.482 ? Unidentified 0.143 0.149 0.070 52.277

155 100.697 I11 C11-Isoparaffin-2 0.076 0.079 0.037 22.299

156 100.979 95-63-6 Q9 1,2,4-Trimethylbenzene 1.943 1.718 1.241 609.157

157 101.163 ? Unidentified 0.086 0.095 0.047 31.626

158 101.284 ? Unidentified 0.051 0.054 0.028 18.710

159 101.548 1678-98-4 M10 i-Butylcyclohexane 0.013 0.012 0.007 3.746

160 102.33417302-01-1 I10 3-Ethyl-3-methylheptane 0.128 0.133 0.063 37.565

161 102.669 538-93-2 Q10 i-Butylbenzene 0.160 0.145 0.092 49.942

162 102.896 124-18-5 P10 n-Decane 0.029 0.030 0.015 8.448

163 103.196 ? Unidentified 0.029 0.030 0.016 10.658

164 103.849 526-73-8 Q9 1,2,3-Trimethylbenzene 0.306 0.265 0.195 95.835

165 104.209 ? Unidentified 0.010 0.009 0.006 3.688

166 104.408 I11 C11 Isoparaffin-4 0.013 0.014 0.007 3.972

167 104.614 99-87-6 Q10 1-Methyl-4-i-propylbenzene 0.083 0.075 0.047 25.874

168 105.042 J9 Indan 0.119 0.095 0.077 37.792

169 105.638 J10 Indene 0.374 0.300 0.243 119.045

170 106.352 I11 C11-Isoparaffin-7 0.133 0.138 0.065 39.196

171 106.546 141-93-5 Q10 1,3-Diethylbenzene 0.040 0.036 0.023 12.407

172 106.827 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 0.491 0.442 0.281 153.197

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C-451
Hydrocarbon Expert V4.7 Fri Aug 27 10:14:49 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91325 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91325

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 107.162 105-05-5 Q10 1,4-Diethylbenzene 0.188 0.168 0.107 58.495

174 107.380 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.147 0.130 0.084 45.929

175 107.624 135-01-3 Q10 1,2-Diethylbenzene 0.030 0.027 0.017 9.484

176 108.078 ? Unidentified 0.028 0.029 0.014 10.060

177 108.231 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.053 0.047 0.031 16.653

178 108.353 ? Unidentified 0.029 0.025 0.019 10.719

179 108.434 ? Unidentified 0.027 0.028 0.013 9.784

180 108.560 ? Unidentified 0.180 0.187 0.088 65.669

181 108.742 ? Unidentified 0.069 0.072 0.034 25.298

182 109.076 1758-88-9 Q10 1,4,Dimethyl-2-ethylbenzene 0.119 0.105 0.068 37.101

183 109.165 ? Unidentified 0.170 0.150 0.097 62.321

184 109.235 874-41-9 Q10 1,3-Dimethyl-4-ethylbenzene 0.127 0.112 0.073 39.538

185 109.393 J10 2-Methylindan 0.040 0.032 0.023 12.672

186 109.740 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.318 0.281 0.182 99.069

187 110.284 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.172 0.149 0.098 53.519

188 110.708 ? Unidentified 0.004 0.004 0.002 1.621

189 110.903 693-61-8 K11 2-Undecene, (E)- 0.012 0.012 0.006 3.442

190 111.037 ? Unidentified 0.016 0.017 0.009 5.995

191 111.193 Q11 1-Methyl-4-t-butylbenzene 0.026 0.023 0.013 7.982

192 111.413 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.107 0.093 0.061 33.341

193 111.708 1120-21-4 P11 n-Undecane 0.018 0.019 0.009 5.443

194 111.863 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.022 0.019 0.011 6.819

195 111.971 ? Unidentified 0.010 0.009 0.005 3.782

196 112.347 Q10 1,2,4,5-Tetramethylbenzene 0.254 0.222 0.145 79.201

197 112.613 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.353 0.307 0.202 110.152

198 113.481 ? Unidentified 0.013 0.013 0.006 4.607

199 113.753 Q11 C11 - Aromatic - 3 0.040 0.035 0.021 12.375

200 113.944 874-35-1 H10 5-Methylindan 0.109 0.095 0.063 34.083

201 114.069 Q12 1,2-Di-i-propylbenzene 0.039 0.034 0.019 12.169

202 114.284 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.057 0.049 0.029 17.602

203 114.440 Q11 C11 - Aromatic - 4 0.031 0.027 0.016 9.692

204 114.693 824-22-6 J10 4-Methylindan 0.147 0.128 0.085 45.715

205 114.845 5161-04-6 Q11 Benzene, 1-methyl-4-(2-methylpropyl)-0.034 0.030 0.018 10.541

206 114.941 824-63-5 H10 2-Methylindan 0.111 0.096 0.064 34.543

207 115.144 ? Unidentified 0.010 0.010 0.005 3.652

208 115.257 538-68-1 Q11 n-Pentylbenzene 0.013 0.012 0.007 4.185

209 115.484 Q11 tert-Pentylbenzene 0.060 0.052 0.031 18.533

210 115.797 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.027 0.023 0.014 8.262

211 115.906 Q11 C11 - Aromatic - 6 0.033 0.030 0.017 10.235

212 116.367 100-18-5 Q12 1,4-Di-i-propylbenzene 0.050 0.043 0.023 15.327

213 116.810 91-20-3 G10 Naphthalene 0.118 0.089 0.071 38.577

214 117.006 J11 4,7-Dimethyl Indane 0.005 0.004 0.003 1.713

215 117.250 J11 1,1-Dimethyl Indane 0.015 0.012 0.008 4.934

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C-452
Hydrocarbon Expert V4.7 Fri Aug 27 10:14:49 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91325 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91325

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

216 117.412 J12 Dimethyl Indane - 1 0.007 0.005 0.004 2.140

217 117.591 7364-19-4 Q12 1t-Butyl-4-ethylbenzene 0.009 0.008 0.004 2.898

218 117.893 Q12 1,3-Di-n-propylbenzene 0.044 0.038 0.021 13.687

219 118.004 Q11 C11 - Aromatic - 11 0.025 0.023 0.013 7.830

220 118.557 Q11 C11 - Aromatic - 12 0.017 0.016 0.009 5.315

221 119.485 102-25-0 Q12 1,3,5-Triethylbenzene 0.004 0.004 0.002 1.355

222 123.438 91-57-6 G11 2-Methylnaphthalene 0.009 0.007 0.005 2.903

223 124.304 90-12-0 G11 1-Methylnaphthalene 0.005 0.004 0.003 1.589

224 130.001 ? Unidentified 0.003 0.002 0.001 1.023

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C-453
Hydrocarbon Expert V4.7 Fri Aug 27 10:14:49 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91325 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91325

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 7.554 74-98-6 Propane 0.007 0.010 0.011 1.866

10.024 106-97-8 n-Butane 0.926 1.238 1.223 266.821

18.114 109-66-0 n-Pentane 1.956 2.418 2.081 567.543

35.812 110-54-3 n-Hexane 2.865 3.364 2.552 834.756

58.055 142-82-5 n-Heptane 0.733 0.830 0.561 214.390

77.869 111-65-9 n-Octane 0.518 0.571 0.348 151.827

91.741 111-84-2 n-Nonane 0.199 0.215 0.119 58.575

102.896 124-18-5 n-Decane 0.029 0.030 0.015 8.448

111.708 1120-21-4 n-Undecane 0.018 0.019 0.009 5.443

I-Paraffins 8.810 75-28-5 i-Butane 0.047 0.066 0.062 13.628

10.637 463-82-1 2,2-Dimethylpropane 0.011 0.015 0.012 3.299

15.076 78-78-4 i-Pentane 3.812 4.764 4.056 1106.312

23.095 75-83-2 2,2-Dimethylbutane 0.126 0.150 0.112 36.741

28.335 79-29-8 2,3-Dimethylbutane 0.449 0.525 0.400 130.697

29.422 107-83-5 2-Methylpentane 2.318 2.748 2.065 675.380

32.063 96-14-0 3-Methylpentane 1.745 2.034 1.554 508.409

42.230 108-08-7 2,4-Dimethylpentane 0.278 0.320 0.213 81.360

42.776 464-06-2 2,2,3-Trimethylbutane 0.037 0.042 0.029 10.886

50.659 591-76-4 2-Methylhexane 0.946 1.080 0.725 276.837

52.491 589-34-4 3-Methylhexane 0.637 0.718 0.488 186.352

55.142 540-84-1 2,2,4-Trimethylpentane 0.058 0.065 0.039 16.961

62.846 590-73-8 2,2-Dimethylhexane 0.027 0.030 0.018 8.017

64.943 564-02-3 2,2,3-Trimethylpentane 0.074 0.080 0.050 21.734

65.167 592-13-2 2,5-Dimethylhexane 0.169 0.189 0.113 49.503

65.504 589-43-5 2,4-Dimethylhexane 0.163 0.180 0.110 47.824

66.738 563-16-6 3,3-Dimethylhexane 0.021 0.023 0.014 6.121

68.482 565-75-3 2,3,4-Trimethylpentane 0.757 0.815 0.509 221.852

70.793 584-94-1 2,3-Dimethylhexane 0.241 0.261 0.162 70.493

72.046 592-27-8 2-Methylheptane 0.237 0.263 0.159 69.534

72.301 589-53-7 4-Methylheptane 0.106 0.117 0.071 31.095

73.360 589-81-1 3-Methylheptane 0.202 0.221 0.135 59.078

73.561 619-99-8 3-Ethylhexane 0.111 0.121 0.075 32.604

75.247 3522-94-9 2,2,5-Trimethylhexane 0.495 0.542 0.296 145.426

80.350 1069-53-0 2,3,5-Trimethylhexane 0.089 0.095 0.053 26.029

81.519 1071-26-7 2,4-Dimethylheptane 0.036 0.039 0.022 10.576

82.474 1072-05-5 2,6-Dimethylheptane 0.063 0.069 0.038 18.495

83.408 2,5-Dimethylheptane 0.099 0.107 0.059 28.974

83.599 926-82-9 3,5-Dimethylheptane 0.018 0.019 0.011 5.227

86.762 3,5-Dimethylheptane 0.010 0.010 0.006 2.838

86.881 1067-20-5 3,3-Diethylpentane 0.008 0.008 0.005 2.329

87.276 2216-34-4 4-Methyloctane 0.049 0.052 0.029 14.291

87.407 3221-61-2 2-Methyloctane 0.064 0.070 0.039 18.913

88.10715869-80-4 Heptane, 3-ethyl- 0.009 0.010 0.006 2.721

88.269 2216-33-3 3-Methyloctane 0.064 0.069 0.038 18.740

89.320 C10 - IsoParaffin - 1 0.106 0.113 0.057 31.178

90.16514720-74-2 2,2,4-trimethylheptane 0.088 0.093 0.047 25.752

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C-454
Hydrocarbon Expert V4.7 Fri Aug 27 10:14:49 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91325 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91325

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

I-Paraffins 94.06115869-87-1 2,2-Dimethyloctane 0.020 0.021 0.011 5.885

94.86115869-89-3 2,5-Dimethyloctane 0.031 0.033 0.017 9.035

95.066 C10 - IsoParaffin - 2 0.011 0.011 0.006 3.153

95.326 2040-95-1 2,7-Dimethyloctane 0.015 0.016 0.008 4.522

95.504 2051-30-1 2,4-Dimethyloctane 0.061 0.065 0.033 17.847

95.892 2,6-Dimethyloctane 0.021 0.022 0.011 6.175

98.71715869-85-9 5-Methylnonane 0.006 0.007 0.003 1.877

98.90617301-94-8 4-Methylnonane 0.015 0.016 0.008 4.450

99.117 2,2,6-Trimethyloctane 0.922 0.983 0.498 271.438

99.885 5911-04-6 3-Methylnonane 0.018 0.019 0.010 5.214

100.697 C11-Isoparaffin-2 0.076 0.079 0.037 22.299

102.33417302-01-1 3-Ethyl-3-methylheptane 0.128 0.133 0.063 37.565

104.408 C11 Isoparaffin-4 0.013 0.014 0.007 3.972

106.352 C11-Isoparaffin-7 0.133 0.138 0.065 39.196

Aromatics

Mono-Aromatics 45.633 71-42-3 Benzene 0.663 0.584 0.652 213.261

69.109 108-88-3 Toluene 16.289 14.546 13.570 5179.291

84.747 100-41-4 Ethylbenzene 2.730 2.437 1.973 861.317

86.002 108-38-3 m-Xylene 7.325 6.562 5.296 2311.502

86.140 106-42-3 p-Xylene 3.381 3.040 2.444 1066.798

88.941 95-47-6 o-Xylene 1.930 1.698 1.396 609.177

93.093 98-82-8 i-Propylbenzene 0.032 0.028 0.020 9.888

96.552 103-65-1 n-Propylbenzene 0.287 0.258 0.183 90.070

97.400 620-14-4 1-Methyl-3-ethylbenzene 1.108 0.992 0.708 347.428

97.634 622-96-8 1-Methyl-4-ethylbenzene 0.514 0.462 0.328 161.116

98.259 108-67-8 1,3,5-Trimethylbenzene 0.684 0.612 0.437 214.426

99.343 611-14-3 1-Methyl-2-ethylbenzene 0.383 0.337 0.245 120.200

100.979 95-63-6 1,2,4-Trimethylbenzene 1.943 1.718 1.241 609.157

102.669 538-93-2 i-Butylbenzene 0.160 0.145 0.092 49.942

103.849 526-73-8 1,2,3-Trimethylbenzene 0.306 0.265 0.195 95.835

104.614 99-87-6 1-Methyl-4-i-propylbenzene 0.083 0.075 0.047 25.874

106.546 141-93-5 1,3-Diethylbenzene 0.040 0.036 0.023 12.407

106.827 1074-43-7 1-Methyl-3-n-propylbenzene 0.491 0.442 0.281 153.197

107.162 105-05-5 1,4-Diethylbenzene 0.188 0.168 0.107 58.495

107.380 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.147 0.130 0.084 45.929

107.624 135-01-3 1,2-Diethylbenzene 0.030 0.027 0.017 9.484

108.231 1074-17-5 1-Methyl-2-n-propylbenzene 0.053 0.047 0.031 16.653

109.076 1758-88-9 1,4,Dimethyl-2-ethylbenzene 0.119 0.105 0.068 37.101

109.235 874-41-9 1,3-Dimethyl-4-ethylbenzene 0.127 0.112 0.073 39.538

109.740 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.318 0.281 0.182 99.069

110.284 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.172 0.149 0.098 53.519

111.193 1-Methyl-4-t-butylbenzene 0.026 0.023 0.013 7.982

111.413 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.107 0.093 0.061 33.341

111.863 4218-48-8 1-Ethyl-4-i-propylbenzene 0.022 0.019 0.011 6.819

112.347 1,2,4,5-Tetramethylbenzene 0.254 0.222 0.145 79.201

112.613 527-53-7 1,2,3,5-Tetramethylbenzene 0.353 0.307 0.202 110.152

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C-455
Hydrocarbon Expert V4.7 Fri Aug 27 10:14:49 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91325 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91325

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 113.753 C11 - Aromatic - 3 0.040 0.035 0.021 12.375

114.069 1,2-Di-i-propylbenzene 0.039 0.034 0.019 12.169

114.284 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.057 0.049 0.029 17.602

114.440 C11 - Aromatic - 4 0.031 0.027 0.016 9.692

114.845 5161-04-6 Benzene, 1-methyl-4-(2-methylpropyl)-0.034 0.030 0.018 10.541

115.257 538-68-1 n-Pentylbenzene 0.013 0.012 0.007 4.185

115.484 tert-Pentylbenzene 0.060 0.052 0.031 18.533

115.797 577-55-9 1-Methyl-2-n-butylbenzene 0.027 0.023 0.014 8.262

115.906 C11 - Aromatic - 6 0.033 0.030 0.017 10.235

116.367 100-18-5 1,4-Di-i-propylbenzene 0.050 0.043 0.023 15.327

117.591 7364-19-4 1t-Butyl-4-ethylbenzene 0.009 0.008 0.004 2.898

117.893 1,3-Di-n-propylbenzene 0.044 0.038 0.021 13.687

118.004 C11 - Aromatic - 11 0.025 0.023 0.013 7.830

118.557 C11 - Aromatic - 12 0.017 0.016 0.009 5.315

119.485 102-25-0 1,3,5-Triethylbenzene 0.004 0.004 0.002 1.355

Naphthalenes 116.810 91-20-3 Naphthalene 0.118 0.089 0.071 38.577

123.438 91-57-6 2-Methylnaphthalene 0.009 0.007 0.005 2.903

124.304 90-12-0 1-Methylnaphthalene 0.005 0.004 0.003 1.589

Naphtheno/Olefino-Benzs 113.944 874-35-1 5-Methylindan 0.109 0.095 0.063 34.083

114.941 824-63-5 2-Methylindan 0.111 0.096 0.064 34.543

Indenes 105.042 Indan 0.119 0.095 0.077 37.792

105.638 Indene 0.374 0.300 0.243 119.045

109.393 2-Methylindan 0.040 0.032 0.023 12.672

114.693 824-22-6 4-Methylindan 0.147 0.128 0.085 45.715

117.006 4,7-Dimethyl Indane 0.005 0.004 0.003 1.713

117.250 1,1-Dimethyl Indane 0.015 0.012 0.008 4.934

117.412 Dimethyl Indane - 1 0.007 0.005 0.004 2.140

Naphthenes

Mono-Naphthenes 27.606 287-92-3 Cyclopentane 0.203 0.210 0.222 60.480

40.671 96-37-7 Methylcyclopentane 1.630 1.686 1.487 486.537

47.555 110-82-7 Cyclohexane 1.175 1.168 1.071 350.637

53.351 1759-58-6 1t,3-Dimethylcyclopentane 0.179 0.185 0.140 53.382

53.936 2532-58-3 1c,3-Dimethylcyclopentane 0.141 0.146 0.110 42.044

54.559 822-50-4 1t,2-Dimethylcyclopentane 0.206 0.213 0.161 61.581

59.64716491-15-9 Cyclopentene, 1,5-dimethyl- 0.018 0.018 0.014 5.299

61.519 108-87-2 Methylcyclohexane 1.134 1.141 0.887 338.516

62.457 4516-69-2 1,1,3-Trimethylcyclopentane 0.032 0.033 0.022 9.620

64.294 1640-89-7 Ethylcyclopentane 0.056 0.056 0.044 16.693

66.343 4850-28-6 1c,2t,4-Trimethylcyclopentane 0.032 0.032 0.022 9.483

67.85915890-40-1 1t,2c,3-Trimethylcyclopentane 0.028 0.028 0.019 8.316

73.223 1,3-dimethyl-t-cyclohexane 0.178 0.179 0.122 53.236

75.607 3c-Ethylmethylcyclopentane 0.010 0.010 0.007 3.089

75.823 3t-Ethylmethylcyclopentane 0.015 0.015 0.010 4.405

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C-456
Hydrocarbon Expert V4.7 Fri Aug 27 10:14:49 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91325 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91325

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Naphthenes 81.364 2207-01-4 1c,2-Dimethylcyclohexane 0.015 0.014 0.010 4.332

82.172 1678-91-7 Ethylcyclohexane 0.119 0.118 0.082 35.624

89.910 trans-1,3-Diethylcyclopentane 0.019 0.017 0.012 6.149

92.299 4926-90-3 1,1-Methylethylcyclohexane 0.013 0.012 0.008 3.841

101.548 1678-98-4 i-Butylcyclohexane 0.013 0.012 0.007 3.746

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.624 115-11-7 Isobutene 0.015 0.020 0.021 4.617

9.665 106-98-9 Butene-1 0.017 0.023 0.024 5.177

10.510 624-64-6 t-Butene-2 0.071 0.091 0.097 21.138

11.250 590-18-1 c-Butene-2 0.084 0.104 0.115 24.994

16.728 109-67-1 Pentene-1 0.324 0.392 0.355 96.787

19.235 646-04-8 t-Pentene-2 0.823 0.983 0.901 245.725

20.264 627-20-3 c-Pentene-2 0.451 0.533 0.494 134.738

33.448 592-41-6 Hexene-1 0.155 0.177 0.141 46.181

36.44413269-52-8 t-Hexene-3 0.254 0.288 0.232 75.829

36.913 4050-45-7 t-Hexene-2 0.391 0.443 0.356 116.663

38.740 7688-21-3 c-Hexene-2 0.207 0.231 0.189 61.700

55.466 592-76-7 Heptene-1 0.028 0.031 0.022 8.311

57.32914686-14-7 t-Heptene-3 0.031 0.034 0.024 9.204

58.272 7642-10-6 c-Heptene-3 0.024 0.026 0.019 7.071

59.17114686-13-6 t-Heptene-2 0.013 0.015 0.010 3.986

110.903 693-61-8 2-Undecene, (E)- 0.012 0.012 0.006 3.442

Iso-Olefins 13.454 563-45-1 3-Methylbutene-1 0.214 0.264 0.234 63.815

17.579 563-46-2 2-Methylbutene-1 0.492 0.586 0.539 146.973

20.946 513-35-9 2-Methylbutene-2 1.010 1.181 1.106 301.538

29.190 691-38-3 4-Methyl-c-pentene-2 0.045 0.051 0.041 13.314

29.836 674-76-0 4-Methyl-t-pentene-2 0.127 0.146 0.116 37.802

33.224 763-29-1 2-Methylpentene-1 0.216 0.245 0.197 64.584

35.649 760-21-4 2-Ethylbutene-1 0.057 0.063 0.052 16.939

37.405 625-27-4 2-Methylpentene-2 0.329 0.369 0.300 98.243

37.819 922-62-3 3-Methyl-c-pentene-2 0.255 0.282 0.232 75.981

40.086 3404-73-7 3,3-Dimethylpentene-1 0.297 0.328 0.232 88.758

42.529 594-56-9 2,3,3-Trimethylbutene-1 0.013 0.014 0.010 3.926

46.635 3404-61-3 3-Methylhexene-1 0.015 0.017 0.012 4.448

47.233 3524-73-0 5-Methylhexene-1 0.068 0.075 0.053 20.179

49.27015840-60-5 2-Methyl-c-hexene-3 0.039 0.043 0.030 11.625

49.617 3769-23-1 4-Methylhexene-1 0.010 0.011 0.008 3.058

50.265 3404-55-5 4-Methyl-t/c-hexene-2 0.049 0.054 0.038 14.576

54.839 C7 - Iso-Olefin - 2 0.021 0.023 0.017 6.409

56.799 4914-89-0 3-Methyl-c-hexene-3 0.013 0.014 0.011 4.010

57.681 6094-02-6 2-Methylhexene-1 0.055 0.061 0.043 16.479

58.546 2738-19-4 2-Methyl-2-hexene 0.025 0.027 0.020 7.518

58.79010574-36-4 3-Methyl-c-hexene-2 0.019 0.021 0.015 5.684

60.07520710-38-8 3-Methyl-t-hexene-2 0.015 0.016 0.012 4.412

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C-457
Hydrocarbon Expert V4.7 Fri Aug 27 10:14:49 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91325 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91325

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Iso-Olefins 60.858 4914-91-4 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.013 0.010 3.732

70.516 C8 - Diolefin - 1 0.012 0.012 0.008 3.613

80.905 C9 - IsoOlefin - 1 0.017 0.017 0.012 5.132

Naphtheno-Olefins 22.541 1574-41-0 1,3-Cyclopentadiene 0.007 0.008 0.008 2.088

25.745 142-29-0 Cyclopentene 0.191 0.192 0.215 58.746

37.040 1120-62-3 3-Methylcyclopentene 0.096 0.097 0.089 28.535

45.832 693-89-0 1-Methylcyclopentene 0.346 0.344 0.324 105.906

51.151 110-83-8 Cyclohexene 0.043 0.041 0.040 12.780

Di-Olefins 18.629 78-79-5 2-Methyl-1,3-Butadiene 0.010 0.012 0.011 3.130

21.271 2004-70-8 1t,3-Pentadiene 0.015 0.018 0.017 4.700

45.422 1528-30-9 C6-Diolefin-1 0.014 0.015 0.014 4.320

Oxygenates 13.136 64-17-5 Ethanol 21.878 21.468 36.452 2688.961

26.897 71-23-8 n-Propanol 0.076 0.073 0.096 15.782

48.053 71-36-3 n-Butanol 0.053 0.051 0.055 11.979

Unidentified 19.876 Unidentified 0.006 0.007 0.006 2.085

26.999 Unidentified 0.056 0.065 0.051 20.474

28.734 Unidentified 0.054 0.056 0.047 19.662

50.838 Unidentified 0.063 0.071 0.051 23.206

63.357 Unidentified 0.051 0.055 0.035 18.600

72.449 Unidentified 0.022 0.023 0.015 7.948

74.456 Unidentified 0.029 0.028 0.020 10.431

76.528 Unidentified 0.065 0.065 0.044 23.653

78.822 Unidentified 0.015 0.015 0.010 5.428

82.973 Unidentified 0.023 0.023 0.016 8.474

85.154 Unidentified 0.017 0.017 0.010 6.281

86.596 Unidentified 0.012 0.012 0.007 4.383

88.745 Unidentified 0.033 0.037 0.020 11.959

93.838 Unidentified 0.048 0.052 0.026 17.710

94.524 Unidentified 0.004 0.003 0.337 1.604

94.524 Unidentified 0.004 0.005 0.002 1.604

100.350 Unidentified 0.052 0.040 0.026 19.071

100.482 Unidentified 0.143 0.149 0.070 52.277

101.163 Unidentified 0.086 0.095 0.047 31.626

101.284 Unidentified 0.051 0.054 0.028 18.710

103.196 Unidentified 0.029 0.030 0.016 10.658

104.209 Unidentified 0.010 0.009 0.006 3.688

108.078 Unidentified 0.028 0.029 0.014 10.060

108.353 Unidentified 0.029 0.025 0.019 10.719

108.434 Unidentified 0.027 0.028 0.013 9.784

108.560 Unidentified 0.180 0.187 0.088 65.669

108.742 Unidentified 0.069 0.072 0.034 25.298

109.165 Unidentified 0.170 0.150 0.097 62.321

110.708 Unidentified 0.004 0.004 0.002 1.621

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C-458
Hydrocarbon Expert V4.7 Fri Aug 27 10:14:49 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91325 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91325

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Unidentified 111.037 Unidentified 0.016 0.017 0.009 5.995

111.971 Unidentified 0.010 0.009 0.005 3.782

113.481 Unidentified 0.013 0.013 0.006 4.607

115.144 Unidentified 0.010 0.010 0.005 3.652

130.001 Unidentified 0.003 0.002 0.001 1.023

Plus

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C-459
Hydrocarbon Expert V4.7 Fri Aug 27 10:14:49 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91325 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91325

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF

20.0 15.0 10.0 5.0 0.0

Propane

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

Ethanol

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

Unidentified

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

1,3-Cyclopentadiene

2,2-Dimethylbutane

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C-460
Hydrocarbon Expert V4.7 Fri Aug 27 10:14:49 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91325 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91325

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

n-Propanol Unidentified

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

2-Ethylbutene-1 n-Hexane

t-Hexene-3

t-Hexene-2 3-Methylcyclopentene

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane 2,3,3-Trimethylbutene-1 2,2,3-Trimethylbutane

C6-Diolefin-1 Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1

Cyclohexane

n-Butanol

2-Methyl-c-hexene-3

4-Methylhexene-1

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C-461
Hydrocarbon Expert V4.7 Fri Aug 27 10:14:49 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91325 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91325

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF

70.0 65.0 60.0 55.0 50.0

4-Methyl-t/c-hexene-2

2-Methylhexane Unidentified Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane C7 - Iso-Olefin - 2 2,2,4-Trimethylpentane

Heptene-1

3-Methyl-c-hexene-3

t-Heptene-3

2-Methylhexene-1

n-Heptane c-Heptene-3 2-Methyl-2-hexene 3-Methyl-c-hexene-2

t-Heptene-2

Cyclopentene, 1,5-dimethyl3-Methyl-t-hexene-2

2-Pentene, 3,4-dimethyl-, (Z)-

Methylcyclohexane

1,1,3-Trimethylcyclopentane

2,2-Dimethylhexane

Unidentified

Ethylcyclopentane

2,2,3-Trimethylpentane 2,5-Dimethylhexane

2,4-Dimethylhexane

1c,2t,4-Trimethylcyclopentane

3,3-Dimethylhexane

1t,2c,3-Trimethylcyclopentane

2,3,4-Trimethylpentane

Toluene

C8 - Diolefin - 1 2,3-Dimethylhexane

2-Methylheptane

Unidentified 4-Methylheptane

1,3-dimethyl-t-cyclohexane 3-Methylheptane 3-Ethylhexane

Unidentified

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C-462
Hydrocarbon Expert V4.7 Fri Aug 27 10:14:49 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91325 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91325

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF

95.0 90.0 85.0 80.0 75.0

2,2,5-Trimethylhexane

3c-Ethylmethylcyclopentane 3t-Ethylmethylcyclopentane

Unidentified

n-Octane

Unidentified

2,3,5-Trimethylhexane

C9 - IsoOlefin - 1

1c,2-Dimethylcyclohexane 2,4-Dimethylheptane

Ethylcyclohexane 2,6-Dimethylheptane

Unidentified

2,5-Dimethylheptane 3,5-Dimethylheptane

Ethylbenzene

Unidentified

m-Xylene p-Xylene

Unidentified 3,5-Dimethylheptane 3,3-Diethylpentane

4-Methyloctane 2-Methyloctane

Heptane, 3-ethyl- 3-Methyloctane

Unidentified o-Xylene

C10 - IsoParaffin - 1

trans-1,3-Diethylcyclopentane 2,2,4-trimethylheptane

n-Nonane

1,1-Methylethylcyclohexane

i-Propylbenzene

Unidentified 2,2-Dimethyloctane

Unidentified

2,5-Dimethyloctane C10 - IsoParaffin - 2 2,7-Dimethyloctane 2,4-Dimethyloctane

2,6-Dimethyloctane

n-Propylbenzene

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

5-Methylnonane 4-Methylnonane 2,2,6-Trimethyloctane 1-Methyl-2-ethylbenzene

3-Methylnonane

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C-463
Hydrocarbon Expert V4.7 Fri Aug 27 10:14:49 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91325 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91325

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified Unidentified C11-Isoparaffin-2 1,2,4-Trimethylbenzene Unidentified

i-Butylcyclohexane

3-Ethyl-3-methylheptane

i-Butylbenzene n-Decane Unidentified

1,2,3-Trimethylbenzene

Unidentified C11 Isoparaffin-4 1-Methyl-4-i-propylbenzene

Indan

Indene

C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene

1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

Unidentified 1-Methyl-2-n-propylbenzene

Unidentified Unidentified

1,4,Dimethyl-2-ethylbenzene 1,3-Dimethyl-4-ethylbenzene Unidentified 2-Methylindan

1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

Unidentified 2-Undecene, (E)- Unidentified 1-Methyl-4-t-butylbenzene 1,2-Dimethyl-3-ethylbenzene n-Undecane Unidentified 1-Ethyl-4-i-propylbenzene

1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene

Unidentified C11 - Aromatic - 3 5-Methylindan 1,2-Di-i-propylbenzene 1-methyl-4-(1-methylpropyl)be C11 - Aromatic - 4 4-Methylindan Benzene, 1-methyl-4-(2-methylpropyl)- 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene

1-Methyl-2-n-butylbenzene C11 - Aromatic - 6

1,4-Di-i-propylbenzene

Naphthalene 4,7-Dimethyl Indane 1,1-Dimethyl Indane Dimethyl Indane - 1 1t-Butyl-4-ethylbenzene

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

C11 - Aromatic - 12

1,3,5-Triethylbenzene

2-Methylnaphthalene

1-Methylnaphthalene

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C-464
Hydrocarbon Expert V4.7 Fri Aug 27 10:14:49 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF 25-Aug-10, 03:40:31

Sample: ODDB-91325 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91325

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000007.D\SIG2000007_FID2_B.CDF

145.0 140.0 135.0 130.0 125.0

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C-465
Hydrocarbon Expert V4.7 Fri Aug 27 15:20:34 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91326 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91326

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 8.270 9.957 9.435

I-Paraffins 37.267 39.763 27.546

Aromatics 19.014 16.000 13.683

Mono-Aromatics 18.147 15.327 13.148

Naphthalenes 0.092 0.066 0.054

Naphtheno/Olefino-Benzs 0.163 0.135 0.095

Indenes 0.612 0.473 0.386

Naphthenes 3.337 3.217 2.799

Mono-Naphthenes 3.337 3.217 2.799

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 7.296 7.918 7.342

n-Olefins 3.008 3.348 3.123

Iso-Olefins 3.545 3.863 3.479

Naphtheno-Olefins 0.702 0.664 0.698

Di-Olefins 0.041 0.043 0.043

Oxygenates 22.772 21.196 38.004

Unidentified 2.044 1.949 1.190

Plus 0.000 0.000 0.000

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C-466
Hydrocarbon Expert V4.7 Fri Aug 27 15:20:34 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91326 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91326

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C2 22.639 21.074 37.846

C3 0.084 0.081 0.111

C4 5.248 6.630 6.947

C5 9.128 10.531 9.868

C6 9.545 10.051 8.695

C7 10.587 10.042 8.522

C8 28.318 28.416 19.368

C9 7.751 7.149 4.835

C10 3.920 3.426 2.245

C11 0.621 0.553 0.318

C12 0.115 0.097 0.054

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C-467
Hydrocarbon Expert V4.7 Fri Aug 27 15:20:34 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91326 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91326

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C3 0.006 0.009 0.010

C4 4.928 6.253 6.530

C5 1.146 1.344 1.223

C6 0.789 0.879 0.705

C7 0.541 0.582 0.416

C8 0.522 0.546 0.352

C9 0.284 0.291 0.170

C10 0.024 0.024 0.013

C11 0.030 0.029 0.015

I-Paraffins C4 0.067 0.088 0.089

C5 4.174 4.948 4.455

C6 3.986 4.448 3.563

C7 2.762 2.989 2.123

C8 22.044 22.948 14.862

C9 2.973 3.073 1.785

C10 1.054 1.062 0.567

C11 0.195 0.192 0.096

C12 0.013 0.013 0.006

Mono-Aromatics C6 0.734 0.613 0.723

C7 5.209 4.413 4.354

C8 5.295 4.488 3.841

C9 4.388 3.701 2.812

C10 2.074 1.740 1.190

C11 0.344 0.287 0.179

C12 0.102 0.084 0.048

Naphthalenes C10 0.076 0.054 0.045

C11 0.017 0.012 0.009

Naphtheno/Olefino-Benzs C10 0.163 0.135 0.095

Indenes C9 0.072 0.055 0.047

C10 0.530 0.411 0.334

C11 0.009 0.007 0.005

Mono-Naphthenes C5 0.131 0.129 0.144

C6 1.434 1.390 1.312

C7 1.323 1.275 1.038

C8 0.415 0.394 0.285

C9 0.034 0.029 0.021

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C-468
Hydrocarbon Expert V4.7 Fri Aug 27 15:20:34 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91326 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91326

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Mono-Naphthenes

n-Olefins C4 0.198 0.238 0.271

C5 1.652 1.871 1.814

C6 1.034 1.111 0.946

C7 0.097 0.102 0.076

C11 0.026 0.026 0.015

Iso-Olefins C5 1.795 2.016 1.971

C6 1.069 1.140 0.978

C7 0.639 0.667 0.501

C8 0.043 0.040 0.028

Naphtheno-Olefins C5 0.204 0.195 0.231

C6 0.498 0.470 0.467

Di-Olefins C5 0.026 0.028 0.029

C7 0.015 0.015 0.014

Oxygenates C2 22.639 21.074 37.846

C3 0.079 0.072 0.101

C4 0.055 0.050 0.057

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C-469
Hydrocarbon Expert V4.7 Fri Aug 27 15:20:34 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91326 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91326

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 21.49 21.26

5% 31.02 28.77

10% 85.03 80.76

15% 134.41 97.26

20% 153.45 139.34

25% 172.30 155.96

30% 172.54 172.39

35% 172.78 172.65

40% 173.02 172.90

45% 173.26 173.16

50% 197.24 188.33

55% 209.70 209.37

60% 210.48 210.10

65% 230.77 227.37

70% 233.94 230.97

75% 237.17 236.05

80% 254.13 239.03

85% 280.02 268.42

90% 318.96 291.69

95% 343.56 335.66

FBP 392.15 387.69

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C-470
Hydrocarbon Expert V4.7 Fri Aug 27 15:20:34 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91326 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91326

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 7.553 74-98-6 P3 Propane 0.006 0.009 0.010 1.525

2 8.810 75-28-5 I4 i-Butane 0.067 0.088 0.089 17.580

3 9.624 115-11-7 K4 Isobutene 0.017 0.021 0.023 4.519

4 9.666 106-98-9 K4 Butene-1 0.018 0.023 0.025 4.989

5 10.025 106-97-8 P4 n-Butane 4.928 6.253 6.530 1292.516

6 10.512 624-64-6 K4 t-Butene-2 0.075 0.091 0.103 20.288

7 10.639 463-82-1 I5 2,2-Dimethylpropane 0.016 0.020 0.017 4.193

8 11.253 590-18-1 K4 c-Butene-2 0.088 0.104 0.121 23.903

9 13.135 64-17-5 X2 Ethanol 22.639 21.074 37.846 2532.266

10 13.454 563-45-1 C5 3-Methylbutene-1 0.241 0.282 0.264 65.368

11 15.084 78-78-4 I5 i-Pentane 4.158 4.929 4.438 1098.132

12 16.734 109-67-1 K5 Pentene-1 0.335 0.385 0.368 91.131

13 17.588 563-46-2 C5 2-Methylbutene-1 0.510 0.576 0.560 138.520

14 18.118 109-66-0 P5 n-Pentane 1.146 1.344 1.223 302.686

15 18.632 78-79-5 E5 2-Methyl-1,3-Butadiene 0.011 0.011 0.012 2.954

16 19.237 646-04-8 K5 t-Pentene-2 0.850 0.964 0.934 231.033

17 19.887 ? Unidentified 0.006 0.007 0.006 1.937

18 20.274 627-20-3 K5 c-Pentene-2 0.466 0.522 0.512 126.617

19 20.949 513-35-9 C5 2-Methylbutene-2 1.044 1.158 1.147 283.651

20 21.274 2004-70-8 E5 1t,3-Pentadiene 0.015 0.017 0.017 4.324

21 22.541 1574-41-0 B5 1,3-Cyclopentadiene 0.007 0.007 0.008 1.930

22 23.099 75-83-2 I6 2,2-Dimethylbutane 0.063 0.071 0.056 16.633

23 25.750 142-29-0 B5 Cyclopentene 0.197 0.187 0.223 55.099

24 26.907 71-23-8 X3 n-Propanol 0.079 0.072 0.101 14.942

25 26.998 ? Unidentified 0.057 0.063 0.052 19.089

26 27.615 287-92-3 M5 Cyclopentane 0.131 0.129 0.144 35.572

27 28.348 79-29-8 I6 2,3-Dimethylbutane 1.022 1.134 0.913 270.906

28 28.741 ? Unidentified 0.053 0.053 0.046 17.621

29 29.202 691-38-3 C6 4-Methyl-c-pentene-2 0.046 0.050 0.042 12.506

30 29.420 107-83-5 I6 2-Methylpentane 1.809 2.034 1.617 479.677

31 29.844 674-76-0 C6 4-Methyl-t-pentene-2 0.131 0.142 0.120 35.482

32 32.072 96-14-0 I6 3-Methylpentane 1.093 1.208 0.977 289.778

33 33.233 763-29-1 C6 2-Methylpentene-1 0.223 0.239 0.204 60.633

34 33.457 592-41-6 K6 Hexene-1 0.159 0.172 0.146 43.215

35 35.650 760-21-4 C6 2-Ethylbutene-1 0.069 0.073 0.063 18.777

36 35.809 110-54-3 P6 n-Hexane 0.789 0.879 0.705 209.313

37 36.44213269-52-8 K6 t-Hexene-3 0.261 0.281 0.238 70.789

38 36.923 4050-45-7 K6 t-Hexene-2 0.402 0.433 0.368 109.278

39 37.044 1120-62-3 B6 3-Methylcyclopentene 0.098 0.094 0.092 26.518

40 37.413 625-27-4 C6 2-Methylpentene-2 0.339 0.360 0.310 91.959

41 37.830 922-62-3 C6 3-Methyl-c-pentene-2 0.262 0.275 0.240 71.097

42 38.750 7688-21-3 K6 c-Hexene-2 0.212 0.225 0.194 57.641

43 40.091 3404-73-7 C7 3,3-Dimethylpentene-1 0.307 0.321 0.240 83.280

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C-471
Hydrocarbon Expert V4.7 Fri Aug 27 15:20:34 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91326 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91326

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 40.676 96-37-7 M6 Methylcyclopentane 0.998 0.979 0.913 271.044

45 42.237 108-08-7 I7 2,4-Dimethylpentane 0.817 0.892 0.628 217.607

46 42.539 594-56-9 C7 2,3,3-Trimethylbutene-1 0.013 0.013 0.010 3.496

47 42.787 464-06-2 I7 2,2,3-Trimethylbutane 0.051 0.054 0.039 13.581

48 45.436 1528-30-9 E7 C6-Diolefin-1 0.015 0.015 0.014 4.023

49 45.644 71-42-3 Q6 Benzene 0.734 0.613 0.723 214.653

50 45.841 693-89-0 B6 1-Methylcyclopentene 0.356 0.336 0.334 99.106

51 46.648 3404-61-3 C7 3-Methylhexene-1 0.015 0.016 0.012 4.180

52 47.236 3524-73-0 C7 5-Methylhexene-1 0.039 0.041 0.031 10.613

53 47.558 110-82-7 M6 Cyclohexane 0.436 0.412 0.399 118.491

54 48.064 71-36-3 X4 n-Butanol 0.055 0.050 0.057 11.294

55 49.27915840-60-5 C7 2-Methyl-c-hexene-3 0.040 0.042 0.031 10.864

56 49.627 3769-23-1 C7 4-Methylhexene-1 0.011 0.011 0.008 2.860

57 50.272 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.050 0.052 0.039 13.624

58 50.679 591-76-4 I7 2-Methylhexane 1.378 1.492 1.059 366.883

59 51.161 110-83-8 B6 Cyclohexene 0.044 0.040 0.041 11.959

60 52.501 589-34-4 I7 3-Methylhexane 0.515 0.551 0.396 137.192

61 53.361 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.147 0.144 0.115 39.807

62 53.948 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.112 0.111 0.088 30.441

63 54.573 822-50-4 M7 1t,2-Dimethylcyclopentane 0.152 0.148 0.119 41.231

64 54.896 C7 C7 - Iso-Olefin - 2 0.022 0.022 0.017 5.948

65 55.225 540-84-1 I8 2,2,4-Trimethylpentane 9.280 9.851 6.257 2475.508

66 55.484 592-76-7 K7 Heptene-1 0.029 0.030 0.022 7.773

67 56.811 4914-89-0 C7 3-Methyl-c-hexene-3 0.014 0.014 0.011 3.707

68 57.33914686-14-7 K7 t-Heptene-3 0.031 0.033 0.025 8.540

69 57.691 6094-02-6 C7 2-Methylhexene-1 0.056 0.059 0.044 15.264

70 58.063 142-82-5 P7 n-Heptane 0.541 0.582 0.416 144.113

71 58.281 7642-10-6 K7 c-Heptene-3 0.024 0.025 0.019 6.613

72 58.555 2738-19-4 C7 2-Methyl-2-hexene 0.026 0.027 0.020 6.985

73 58.79910574-36-4 C7 3-Methyl-c-hexene-2 0.020 0.020 0.015 5.312

74 59.18114686-13-6 K7 t-Heptene-2 0.013 0.013 0.010 3.520

75 59.65816491-15-9 M7 Cyclopentene, 1,5-dimethyl- 0.018 0.017 0.014 4.834

76 60.08420710-38-8 C7 3-Methyl-t-hexene-2 0.015 0.015 0.011 3.975

77 60.867 4914-91-4 C7 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.013 0.010 3.430

78 61.525 108-87-2 M7 Methylcyclohexane 0.848 0.809 0.665 230.275

79 62.466 4516-69-2 M8 1,1,3-Trimethylcyclopentane 0.026 0.025 0.018 7.022

80 62.856 590-73-8 I8 2,2-Dimethylhexane 0.025 0.026 0.017 6.634

81 63.369 ? Unidentified 0.053 0.054 0.037 17.607

82 64.302 1640-89-7 M7 Ethylcyclopentane 0.048 0.046 0.037 12.905

83 64.956 564-02-3 I8 2,2,3-Trimethylpentane 0.502 0.515 0.339 134.040

84 65.188 592-13-2 I8 2,5-Dimethylhexane 1.155 1.223 0.779 308.054

85 65.525 589-43-5 I8 2,4-Dimethylhexane 1.073 1.126 0.724 286.292

86 66.355 4850-28-6 M8 1c,2t,4-Trimethylcyclopentane 0.027 0.026 0.018 7.268

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C-472
Hydrocarbon Expert V4.7 Fri Aug 27 15:20:34 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91326 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91326

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 66.749 563-16-6 I8 3,3-Dimethylhexane 0.019 0.019 0.013 4.955

88 67.86715890-40-1 M8 1t,2c,3-Trimethylcyclopentane 0.024 0.023 0.016 6.434

89 68.512 565-75-3 I8 2,3,4-Trimethylpentane 3.896 3.980 2.627 1039.360

90 69.036 108-88-3 Q7 Toluene 5.209 4.413 4.354 1507.415

91 69.189 560-21-4 I8 2,3,3-Trimethylpentane 4.281 4.330 2.887 1142.059

92 70.520 C8 C8 - Diolefin - 1 0.010 0.010 0.007 2.847

93 70.805 584-94-1 I8 2,3-Dimethylhexane 1.062 1.095 0.716 283.229

94 72.053 592-27-8 I8 2-Methylheptane 0.248 0.261 0.167 66.153

95 72.316 589-53-7 I8 4-Methylheptane 0.181 0.189 0.122 48.361

96 72.456 ? Unidentified 0.085 0.087 0.057 28.284

97 73.230 M8 1,3-dimethyl-t-cyclohexane 0.168 0.160 0.115 45.514

98 73.366 589-81-1 I8 3-Methylheptane 0.215 0.223 0.145 57.248

99 73.567 619-99-8 I8 3-Ethylhexane 0.106 0.109 0.071 28.276

100 74.464 ? Unidentified 0.028 0.026 0.019 9.163

101 75.266 3522-94-9 I9 2,2,5-Trimethylhexane 1.986 2.063 1.193 530.957

102 75.615 M8 3c-Ethylmethylcyclopentane 0.010 0.009 0.007 2.631

103 75.832 M8 3t-Ethylmethylcyclopentane 0.014 0.013 0.010 3.783

104 76.239 ? Unidentified 0.014 0.014 0.010 4.791

105 76.538 ? Unidentified 0.066 0.062 0.045 21.873

106 77.875 111-65-9 P8 n-Octane 0.522 0.546 0.352 139.347

107 78.826 ? Unidentified 0.047 0.044 0.032 15.474

108 80.357 1069-53-0 I9 2,3,5-Trimethylhexane 0.311 0.316 0.187 83.136

109 80.911 C8 C9 - IsoOlefin - 1 0.018 0.017 0.013 5.020

110 81.372 2207-01-4 M8 1c,2-Dimethylcyclohexane 0.016 0.015 0.011 4.288

111 81.523 1071-26-7 I9 2,4-Dimethylheptane 0.071 0.073 0.042 18.897

112 82.177 1678-91-7 M8 Ethylcyclohexane 0.131 0.123 0.090 35.676

113 82.479 1072-05-5 I9 2,6-Dimethylheptane 0.114 0.118 0.068 30.466

114 82.978 ? Unidentified 0.030 0.029 0.021 10.067

115 83.409 I9 2,5-Dimethylheptane 0.205 0.211 0.123 54.806

116 83.588 926-82-9 I9 3,5-Dimethylheptane 0.026 0.027 0.016 7.053

117 84.733 100-41-4 Q8 Ethylbenzene 0.950 0.805 0.689 272.831

118 84.906 ? Unidentified 0.026 0.026 0.016 8.780

119 85.151 ? Unidentified 0.035 0.033 0.021 11.599

120 85.956 108-38-3 Q8 m-Xylene 2.418 2.055 1.754 694.470

121 86.103 106-42-3 Q8 p-Xylene 1.080 0.921 0.783 310.114

122 86.234 ? Unidentified 0.066 0.067 0.040 21.958

123 86.492 C8 C9-IsoOlefin-3 0.014 0.013 0.008 3.694

124 86.598 ? Unidentified 0.012 0.013 0.007 4.134

125 86.755 I9 3,5-Dimethylheptane 0.011 0.011 0.007 3.010

126 86.883 1067-20-5 I9 3,3-Diethylpentane 0.010 0.010 0.006 2.643

127 87.277 2216-34-4 I9 4-Methyloctane 0.063 0.064 0.038 16.803

128 87.408 3221-61-2 I9 2-Methyloctane 0.084 0.086 0.050 22.364

129 88.11015869-80-4 I9 Heptane, 3-ethyl- 0.011 0.012 0.007 3.041

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C-473
Hydrocarbon Expert V4.7 Fri Aug 27 15:20:34 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91326 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91326

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 88.271 2216-33-3 I9 3-Methyloctane 0.081 0.082 0.048 21.547

131 88.747 ? Unidentified 0.090 0.097 0.055 30.081

132 88.930 95-47-6 Q8 o-Xylene 0.847 0.707 0.615 243.280

133 89.325 I10 C10 - IsoParaffin - 1 0.310 0.313 0.168 83.102

134 89.913 M9 trans-1,3-Diethylcyclopentane 0.020 0.017 0.012 5.851

135 90.16714720-74-2 I10 2,2,4-trimethylheptane 0.226 0.229 0.123 60.660

136 91.735 111-84-2 P9 n-Nonane 0.284 0.291 0.170 75.892

137 92.299 4926-90-3 M9 1,1-Methylethylcyclohexane 0.013 0.012 0.008 3.652

138 93.096 98-82-8 Q9 i-Propylbenzene 0.031 0.027 0.020 8.883

139 93.842 ? Unidentified 0.046 0.047 0.025 15.448

140 94.06415869-87-1 I10 2,2-Dimethyloctane 0.018 0.018 0.010 4.886

141 94.86715869-89-3 I10 2,5-Dimethyloctane 0.013 0.013 0.007 3.380

142 95.071 I10 C10 - IsoParaffin - 2 0.008 0.008 0.004 2.043

143 95.507 2051-30-1 I10 2,4-Dimethyloctane 0.022 0.023 0.012 5.990

144 95.894 I10 2,6-Dimethyloctane 0.011 0.011 0.006 3.036

145 96.555 103-65-1 Q9 n-Propylbenzene 0.255 0.217 0.163 72.805

146 97.402 620-14-4 Q9 1-Methyl-3-ethylbenzene 0.969 0.824 0.621 276.614

147 97.635 622-96-8 Q9 1-Methyl-4-ethylbenzene 0.449 0.383 0.288 128.209

148 98.260 108-67-8 Q9 1,3,5-Trimethylbenzene 0.572 0.485 0.366 163.135

149 98.71815869-85-9 I10 5-Methylnonane 0.006 0.006 0.003 1.505

150 98.90817301-94-8 I10 4-Methylnonane 0.013 0.013 0.007 3.516

151 99.115 I10 2,2,6-Trimethyloctane 0.349 0.353 0.189 93.544

152 99.345 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.333 0.278 0.214 95.141

153 99.887 5911-04-6 I10 3-Methylnonane 0.015 0.016 0.008 4.151

154 100.351 ? Unidentified 0.023 0.017 0.011 7.560

155 100.483 ? Unidentified 0.060 0.059 0.030 20.050

156 100.699 I11 C11-Isoparaffin-2 0.033 0.032 0.016 8.782

157 100.976 95-63-6 Q9 1,2,4-Trimethylbenzene 1.574 1.320 1.009 449.228

158 101.164 ? Unidentified 0.042 0.044 0.023 13.901

159 101.286 ? Unidentified 0.024 0.024 0.013 7.974

160 102.33617302-01-1 I10 3-Ethyl-3-methylheptane 0.061 0.060 0.030 16.361

161 102.645 538-93-2 Q10 i-Butylbenzene 0.072 0.062 0.042 20.563

162 102.803 124-18-5 P10 n-Decane 0.024 0.024 0.013 6.388

163 102.899 ? Unidentified 0.014 0.012 0.008 4.764

164 103.199 ? Unidentified 0.017 0.017 0.009 5.778

165 103.851 526-73-8 Q9 1,2,3-Trimethylbenzene 0.203 0.167 0.130 57.981

166 104.222 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.009 0.008 0.005 2.564

167 104.410 I11 C11 Isoparaffin-4 0.009 0.009 0.004 2.435

168 104.617 99-87-6 Q10 1-Methyl-4-i-propylbenzene 0.062 0.053 0.036 17.648

169 105.046 J9 Indan 0.072 0.055 0.047 20.951

170 105.639 J10 Indene 0.367 0.280 0.239 106.527

171 106.355 I11 C11-Isoparaffin-7 0.153 0.151 0.075 41.018

172 106.548 141-93-5 Q10 1,3-Diethylbenzene 0.023 0.019 0.013 6.486

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C-474
Hydrocarbon Expert V4.7 Fri Aug 27 15:20:34 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91326 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91326

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 106.833 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 0.474 0.405 0.272 134.660

174 107.111 105-05-5 Q10 1,4-Diethylbenzene 0.173 0.147 0.099 49.056

175 107.383 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.095 0.079 0.054 26.889

176 107.622 135-01-3 Q10 1,2-Diethylbenzene 0.039 0.033 0.023 11.139

177 108.081 ? Unidentified 0.038 0.038 0.019 12.711

178 108.234 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.040 0.034 0.023 11.478

179 108.356 ? Unidentified 0.044 0.044 0.022 14.778

180 108.436 ? Unidentified 0.042 0.041 0.021 13.975

181 108.563 ? Unidentified 0.266 0.262 0.131 88.381

182 108.745 ? Unidentified 0.107 0.106 0.053 35.632

183 109.168 ? Unidentified 0.437 0.366 0.251 145.523

184 109.395 J10 2-Methylindan 0.055 0.042 0.032 16.018

185 109.741 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.247 0.208 0.142 70.137

186 110.286 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.321 0.265 0.184 91.206

187 110.711 ? Unidentified 0.010 0.009 0.005 3.492

188 110.905 693-61-8 K11 2-Undecene, (E)- 0.026 0.026 0.015 7.119

189 111.039 ? Unidentified 0.056 0.055 0.031 18.523

190 111.311 ? Unidentified 0.060 0.052 0.031 19.842

191 111.413 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.061 0.050 0.035 17.312

192 111.711 1120-21-4 P11 n-Undecane 0.030 0.029 0.015 7.946

193 111.864 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.041 0.034 0.022 11.719

194 111.973 ? Unidentified 0.024 0.020 0.012 7.916

195 112.349 Q10 1,2,4,5-Tetramethylbenzene 0.192 0.159 0.110 54.543

196 112.614 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.264 0.218 0.152 74.976

197 112.957 ? Unidentified 0.006 0.005 0.003 1.854

198 113.131 I12 C12 - IsoParaffin - 1 0.008 0.008 0.004 2.278

199 113.487 ? Unidentified 0.017 0.017 0.008 5.717

200 113.611 ? Unidentified 0.006 0.006 0.003 2.016

201 113.760 Q11 C11 - Aromatic - 3 0.052 0.043 0.027 14.775

202 113.946 874-35-1 H10 5-Methylindan 0.080 0.066 0.047 22.742

203 114.071 Q12 1,2-Di-i-propylbenzene 0.035 0.029 0.017 9.818

204 114.286 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.046 0.038 0.024 13.003

205 114.452 Q11 C11 - Aromatic - 4 0.030 0.024 0.015 8.373

206 114.695 824-22-6 J10 4-Methylindan 0.108 0.089 0.063 30.525

207 114.849 5161-04-6 Q11 Benzene, 1-methyl-4-(2-methylpropyl)-0.031 0.026 0.016 8.813

208 114.942 824-63-5 H10 2-Methylindan 0.083 0.068 0.048 23.516

209 115.146 ? Unidentified 0.010 0.010 0.005 3.399

210 115.259 538-68-1 Q11 n-Pentylbenzene 0.012 0.010 0.006 3.515

211 115.487 Q11 tert-Pentylbenzene 0.049 0.040 0.025 13.728

212 115.799 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.021 0.017 0.011 5.909

213 115.910 Q11 C11 - Aromatic - 7 0.035 0.030 0.018 9.767

214 116.251 I12 C12 - IsoParaffin - 4 0.004 0.004 0.002 1.221

215 116.370 100-18-5 Q12 1,4-Di-i-propylbenzene 0.037 0.031 0.018 10.549

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C-475
Hydrocarbon Expert V4.7 Fri Aug 27 15:20:34 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91326 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91326

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

216 116.810 91-20-3 G10 Naphthalene 0.076 0.054 0.045 22.459

217 116.944 ? Unidentified 0.012 0.012 0.006 4.091

218 117.127 ? Unidentified 0.004 0.003 0.002 1.225

219 117.241 J11 1,1-Dimethyl Indane 0.009 0.007 0.005 2.658

220 117.895 Q12 1,3-Di-n-propylbenzene 0.030 0.025 0.014 8.392

221 118.007 Q11 C11 - Aromatic - 11 0.016 0.013 0.008 4.407

222 118.559 Q11 C11 - Aromatic - 12 0.012 0.010 0.006 3.292

223 123.442 91-57-6 G11 2-Methylnaphthalene 0.011 0.008 0.006 3.353

224 124.309 90-12-0 G11 1-Methylnaphthalene 0.005 0.004 0.003 1.587

225 126.298 ? Unidentified 0.007 0.006 0.003 2.235

226 130.004 ? Unidentified 0.003 0.002 0.002 1.013

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C-476
Hydrocarbon Expert V4.7 Fri Aug 27 15:20:34 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91326 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91326

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 7.553 74-98-6 Propane 0.006 0.009 0.010 1.525

10.025 106-97-8 n-Butane 4.928 6.253 6.530 1292.516

18.118 109-66-0 n-Pentane 1.146 1.344 1.223 302.686

35.809 110-54-3 n-Hexane 0.789 0.879 0.705 209.313

58.063 142-82-5 n-Heptane 0.541 0.582 0.416 144.113

77.875 111-65-9 n-Octane 0.522 0.546 0.352 139.347

91.735 111-84-2 n-Nonane 0.284 0.291 0.170 75.892

102.803 124-18-5 n-Decane 0.024 0.024 0.013 6.388

111.711 1120-21-4 n-Undecane 0.030 0.029 0.015 7.946

I-Paraffins 8.810 75-28-5 i-Butane 0.067 0.088 0.089 17.580

10.639 463-82-1 2,2-Dimethylpropane 0.016 0.020 0.017 4.193

15.084 78-78-4 i-Pentane 4.158 4.929 4.438 1098.132

23.099 75-83-2 2,2-Dimethylbutane 0.063 0.071 0.056 16.633

28.348 79-29-8 2,3-Dimethylbutane 1.022 1.134 0.913 270.906

29.420 107-83-5 2-Methylpentane 1.809 2.034 1.617 479.677

32.072 96-14-0 3-Methylpentane 1.093 1.208 0.977 289.778

42.237 108-08-7 2,4-Dimethylpentane 0.817 0.892 0.628 217.607

42.787 464-06-2 2,2,3-Trimethylbutane 0.051 0.054 0.039 13.581

50.679 591-76-4 2-Methylhexane 1.378 1.492 1.059 366.883

52.501 589-34-4 3-Methylhexane 0.515 0.551 0.396 137.192

55.225 540-84-1 2,2,4-Trimethylpentane 9.280 9.851 6.257 2475.508

62.856 590-73-8 2,2-Dimethylhexane 0.025 0.026 0.017 6.634

64.956 564-02-3 2,2,3-Trimethylpentane 0.502 0.515 0.339 134.040

65.188 592-13-2 2,5-Dimethylhexane 1.155 1.223 0.779 308.054

65.525 589-43-5 2,4-Dimethylhexane 1.073 1.126 0.724 286.292

66.749 563-16-6 3,3-Dimethylhexane 0.019 0.019 0.013 4.955

68.512 565-75-3 2,3,4-Trimethylpentane 3.896 3.980 2.627 1039.360

69.189 560-21-4 2,3,3-Trimethylpentane 4.281 4.330 2.887 1142.059

70.805 584-94-1 2,3-Dimethylhexane 1.062 1.095 0.716 283.229

72.053 592-27-8 2-Methylheptane 0.248 0.261 0.167 66.153

72.316 589-53-7 4-Methylheptane 0.181 0.189 0.122 48.361

73.366 589-81-1 3-Methylheptane 0.215 0.223 0.145 57.248

73.567 619-99-8 3-Ethylhexane 0.106 0.109 0.071 28.276

75.266 3522-94-9 2,2,5-Trimethylhexane 1.986 2.063 1.193 530.957

80.357 1069-53-0 2,3,5-Trimethylhexane 0.311 0.316 0.187 83.136

81.523 1071-26-7 2,4-Dimethylheptane 0.071 0.073 0.042 18.897

82.479 1072-05-5 2,6-Dimethylheptane 0.114 0.118 0.068 30.466

83.409 2,5-Dimethylheptane 0.205 0.211 0.123 54.806

83.588 926-82-9 3,5-Dimethylheptane 0.026 0.027 0.016 7.053

86.755 3,5-Dimethylheptane 0.011 0.011 0.007 3.010

86.883 1067-20-5 3,3-Diethylpentane 0.010 0.010 0.006 2.643

87.277 2216-34-4 4-Methyloctane 0.063 0.064 0.038 16.803

87.408 3221-61-2 2-Methyloctane 0.084 0.086 0.050 22.364

88.11015869-80-4 Heptane, 3-ethyl- 0.011 0.012 0.007 3.041

88.271 2216-33-3 3-Methyloctane 0.081 0.082 0.048 21.547

89.325 C10 - IsoParaffin - 1 0.310 0.313 0.168 83.102

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C-477
Hydrocarbon Expert V4.7 Fri Aug 27 15:20:34 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91326 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91326

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

I-Paraffins 90.16714720-74-2 2,2,4-trimethylheptane 0.226 0.229 0.123 60.660

94.06415869-87-1 2,2-Dimethyloctane 0.018 0.018 0.010 4.886

94.86715869-89-3 2,5-Dimethyloctane 0.013 0.013 0.007 3.380

95.071 C10 - IsoParaffin - 2 0.008 0.008 0.004 2.043

95.507 2051-30-1 2,4-Dimethyloctane 0.022 0.023 0.012 5.990

95.894 2,6-Dimethyloctane 0.011 0.011 0.006 3.036

98.71815869-85-9 5-Methylnonane 0.006 0.006 0.003 1.505

98.90817301-94-8 4-Methylnonane 0.013 0.013 0.007 3.516

99.115 2,2,6-Trimethyloctane 0.349 0.353 0.189 93.544

99.887 5911-04-6 3-Methylnonane 0.015 0.016 0.008 4.151

100.699 C11-Isoparaffin-2 0.033 0.032 0.016 8.782

102.33617302-01-1 3-Ethyl-3-methylheptane 0.061 0.060 0.030 16.361

104.410 C11 Isoparaffin-4 0.009 0.009 0.004 2.435

106.355 C11-Isoparaffin-7 0.153 0.151 0.075 41.018

113.131 C12 - IsoParaffin - 1 0.008 0.008 0.004 2.278

116.251 C12 - IsoParaffin - 4 0.004 0.004 0.002 1.221

Aromatics

Mono-Aromatics 45.644 71-42-3 Benzene 0.734 0.613 0.723 214.653

69.036 108-88-3 Toluene 5.209 4.413 4.354 1507.415

84.733 100-41-4 Ethylbenzene 0.950 0.805 0.689 272.831

85.956 108-38-3 m-Xylene 2.418 2.055 1.754 694.470

86.103 106-42-3 p-Xylene 1.080 0.921 0.783 310.114

88.930 95-47-6 o-Xylene 0.847 0.707 0.615 243.280

93.096 98-82-8 i-Propylbenzene 0.031 0.027 0.020 8.883

96.555 103-65-1 n-Propylbenzene 0.255 0.217 0.163 72.805

97.402 620-14-4 1-Methyl-3-ethylbenzene 0.969 0.824 0.621 276.614

97.635 622-96-8 1-Methyl-4-ethylbenzene 0.449 0.383 0.288 128.209

98.260 108-67-8 1,3,5-Trimethylbenzene 0.572 0.485 0.366 163.135

99.345 611-14-3 1-Methyl-2-ethylbenzene 0.333 0.278 0.214 95.141

100.976 95-63-6 1,2,4-Trimethylbenzene 1.574 1.320 1.009 449.228

102.645 538-93-2 i-Butylbenzene 0.072 0.062 0.042 20.563

103.851 526-73-8 1,2,3-Trimethylbenzene 0.203 0.167 0.130 57.981

104.222 535-77-3 1-Methyl-3-i-propylbenzene 0.009 0.008 0.005 2.564

104.617 99-87-6 1-Methyl-4-i-propylbenzene 0.062 0.053 0.036 17.648

106.548 141-93-5 1,3-Diethylbenzene 0.023 0.019 0.013 6.486

106.833 1074-43-7 1-Methyl-3-n-propylbenzene 0.474 0.405 0.272 134.660

107.111 105-05-5 1,4-Diethylbenzene 0.173 0.147 0.099 49.056

107.383 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.095 0.079 0.054 26.889

107.622 135-01-3 1,2-Diethylbenzene 0.039 0.033 0.023 11.139

108.234 1074-17-5 1-Methyl-2-n-propylbenzene 0.040 0.034 0.023 11.478

109.741 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.247 0.208 0.142 70.137

110.286 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.321 0.265 0.184 91.206

111.413 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.061 0.050 0.035 17.312

111.864 4218-48-8 1-Ethyl-4-i-propylbenzene 0.041 0.034 0.022 11.719

112.349 1,2,4,5-Tetramethylbenzene 0.192 0.159 0.110 54.543

112.614 527-53-7 1,2,3,5-Tetramethylbenzene 0.264 0.218 0.152 74.976

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C-478
Hydrocarbon Expert V4.7 Fri Aug 27 15:20:34 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91326 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91326

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 113.760 C11 - Aromatic - 3 0.052 0.043 0.027 14.775

114.071 1,2-Di-i-propylbenzene 0.035 0.029 0.017 9.818

114.286 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.046 0.038 0.024 13.003

114.452 C11 - Aromatic - 4 0.030 0.024 0.015 8.373

114.849 5161-04-6 Benzene, 1-methyl-4-(2-methylpropyl)-0.031 0.026 0.016 8.813

115.259 538-68-1 n-Pentylbenzene 0.012 0.010 0.006 3.515

115.487 tert-Pentylbenzene 0.049 0.040 0.025 13.728

115.799 577-55-9 1-Methyl-2-n-butylbenzene 0.021 0.017 0.011 5.909

115.910 C11 - Aromatic - 7 0.035 0.030 0.018 9.767

116.370 100-18-5 1,4-Di-i-propylbenzene 0.037 0.031 0.018 10.549

117.895 1,3-Di-n-propylbenzene 0.030 0.025 0.014 8.392

118.007 C11 - Aromatic - 11 0.016 0.013 0.008 4.407

118.559 C11 - Aromatic - 12 0.012 0.010 0.006 3.292

Naphthalenes 116.810 91-20-3 Naphthalene 0.076 0.054 0.045 22.459

123.442 91-57-6 2-Methylnaphthalene 0.011 0.008 0.006 3.353

124.309 90-12-0 1-Methylnaphthalene 0.005 0.004 0.003 1.587

Naphtheno/Olefino-Benzs 113.946 874-35-1 5-Methylindan 0.080 0.066 0.047 22.742

114.942 824-63-5 2-Methylindan 0.083 0.068 0.048 23.516

Indenes 105.046 Indan 0.072 0.055 0.047 20.951

105.639 Indene 0.367 0.280 0.239 106.527

109.395 2-Methylindan 0.055 0.042 0.032 16.018

114.695 824-22-6 4-Methylindan 0.108 0.089 0.063 30.525

117.241 1,1-Dimethyl Indane 0.009 0.007 0.005 2.658

Naphthenes

Mono-Naphthenes 27.615 287-92-3 Cyclopentane 0.131 0.129 0.144 35.572

40.676 96-37-7 Methylcyclopentane 0.998 0.979 0.913 271.044

47.558 110-82-7 Cyclohexane 0.436 0.412 0.399 118.491

53.361 1759-58-6 1t,3-Dimethylcyclopentane 0.147 0.144 0.115 39.807

53.948 2532-58-3 1c,3-Dimethylcyclopentane 0.112 0.111 0.088 30.441

54.573 822-50-4 1t,2-Dimethylcyclopentane 0.152 0.148 0.119 41.231

59.65816491-15-9 Cyclopentene, 1,5-dimethyl- 0.018 0.017 0.014 4.834

61.525 108-87-2 Methylcyclohexane 0.848 0.809 0.665 230.275

62.466 4516-69-2 1,1,3-Trimethylcyclopentane 0.026 0.025 0.018 7.022

64.302 1640-89-7 Ethylcyclopentane 0.048 0.046 0.037 12.905

66.355 4850-28-6 1c,2t,4-Trimethylcyclopentane 0.027 0.026 0.018 7.268

67.86715890-40-1 1t,2c,3-Trimethylcyclopentane 0.024 0.023 0.016 6.434

73.230 1,3-dimethyl-t-cyclohexane 0.168 0.160 0.115 45.514

75.615 3c-Ethylmethylcyclopentane 0.010 0.009 0.007 2.631

75.832 3t-Ethylmethylcyclopentane 0.014 0.013 0.010 3.783

81.372 2207-01-4 1c,2-Dimethylcyclohexane 0.016 0.015 0.011 4.288

82.177 1678-91-7 Ethylcyclohexane 0.131 0.123 0.090 35.676

89.913 trans-1,3-Diethylcyclopentane 0.020 0.017 0.012 5.851

92.299 4926-90-3 1,1-Methylethylcyclohexane 0.013 0.012 0.008 3.652

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C-479
Hydrocarbon Expert V4.7 Fri Aug 27 15:20:34 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91326 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91326

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Naphthenes

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.624 115-11-7 Isobutene 0.017 0.021 0.023 4.519

9.666 106-98-9 Butene-1 0.018 0.023 0.025 4.989

10.512 624-64-6 t-Butene-2 0.075 0.091 0.103 20.288

11.253 590-18-1 c-Butene-2 0.088 0.104 0.121 23.903

16.734 109-67-1 Pentene-1 0.335 0.385 0.368 91.131

19.237 646-04-8 t-Pentene-2 0.850 0.964 0.934 231.033

20.274 627-20-3 c-Pentene-2 0.466 0.522 0.512 126.617

33.457 592-41-6 Hexene-1 0.159 0.172 0.146 43.215

36.44213269-52-8 t-Hexene-3 0.261 0.281 0.238 70.789

36.923 4050-45-7 t-Hexene-2 0.402 0.433 0.368 109.278

38.750 7688-21-3 c-Hexene-2 0.212 0.225 0.194 57.641

55.484 592-76-7 Heptene-1 0.029 0.030 0.022 7.773

57.33914686-14-7 t-Heptene-3 0.031 0.033 0.025 8.540

58.281 7642-10-6 c-Heptene-3 0.024 0.025 0.019 6.613

59.18114686-13-6 t-Heptene-2 0.013 0.013 0.010 3.520

110.905 693-61-8 2-Undecene, (E)- 0.026 0.026 0.015 7.119

Iso-Olefins 13.454 563-45-1 3-Methylbutene-1 0.241 0.282 0.264 65.368

17.588 563-46-2 2-Methylbutene-1 0.510 0.576 0.560 138.520

20.949 513-35-9 2-Methylbutene-2 1.044 1.158 1.147 283.651

29.202 691-38-3 4-Methyl-c-pentene-2 0.046 0.050 0.042 12.506

29.844 674-76-0 4-Methyl-t-pentene-2 0.131 0.142 0.120 35.482

33.233 763-29-1 2-Methylpentene-1 0.223 0.239 0.204 60.633

35.650 760-21-4 2-Ethylbutene-1 0.069 0.073 0.063 18.777

37.413 625-27-4 2-Methylpentene-2 0.339 0.360 0.310 91.959

37.830 922-62-3 3-Methyl-c-pentene-2 0.262 0.275 0.240 71.097

40.091 3404-73-7 3,3-Dimethylpentene-1 0.307 0.321 0.240 83.280

42.539 594-56-9 2,3,3-Trimethylbutene-1 0.013 0.013 0.010 3.496

46.648 3404-61-3 3-Methylhexene-1 0.015 0.016 0.012 4.180

47.236 3524-73-0 5-Methylhexene-1 0.039 0.041 0.031 10.613

49.27915840-60-5 2-Methyl-c-hexene-3 0.040 0.042 0.031 10.864

49.627 3769-23-1 4-Methylhexene-1 0.011 0.011 0.008 2.860

50.272 3404-55-5 4-Methyl-t/c-hexene-2 0.050 0.052 0.039 13.624

54.896 C7 - Iso-Olefin - 2 0.022 0.022 0.017 5.948

56.811 4914-89-0 3-Methyl-c-hexene-3 0.014 0.014 0.011 3.707

57.691 6094-02-6 2-Methylhexene-1 0.056 0.059 0.044 15.264

58.555 2738-19-4 2-Methyl-2-hexene 0.026 0.027 0.020 6.985

58.79910574-36-4 3-Methyl-c-hexene-2 0.020 0.020 0.015 5.312

60.08420710-38-8 3-Methyl-t-hexene-2 0.015 0.015 0.011 3.975

60.867 4914-91-4 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.013 0.010 3.430

70.520 C8 - Diolefin - 1 0.010 0.010 0.007 2.847

80.911 C9 - IsoOlefin - 1 0.018 0.017 0.013 5.020

86.492 C9-IsoOlefin-3 0.014 0.013 0.008 3.694

Naphtheno-Olefins 22.541 1574-41-0 1,3-Cyclopentadiene 0.007 0.007 0.008 1.930

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C-480
Hydrocarbon Expert V4.7 Fri Aug 27 15:20:34 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91326 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91326

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Naphtheno-Olefins 25.750 142-29-0 Cyclopentene 0.197 0.187 0.223 55.099

37.044 1120-62-3 3-Methylcyclopentene 0.098 0.094 0.092 26.518

45.841 693-89-0 1-Methylcyclopentene 0.356 0.336 0.334 99.106

51.161 110-83-8 Cyclohexene 0.044 0.040 0.041 11.959

Di-Olefins 18.632 78-79-5 2-Methyl-1,3-Butadiene 0.011 0.011 0.012 2.954

21.274 2004-70-8 1t,3-Pentadiene 0.015 0.017 0.017 4.324

45.436 1528-30-9 C6-Diolefin-1 0.015 0.015 0.014 4.023

Oxygenates 13.135 64-17-5 Ethanol 22.639 21.074 37.846 2532.266

26.907 71-23-8 n-Propanol 0.079 0.072 0.101 14.942

48.064 71-36-3 n-Butanol 0.055 0.050 0.057 11.294

Unidentified 19.887 Unidentified 0.006 0.007 0.006 1.937

26.998 Unidentified 0.057 0.063 0.052 19.089

28.741 Unidentified 0.053 0.053 0.046 17.621

63.369 Unidentified 0.053 0.054 0.037 17.607

72.456 Unidentified 0.085 0.087 0.057 28.284

74.464 Unidentified 0.028 0.026 0.019 9.163

76.239 Unidentified 0.014 0.014 0.010 4.791

76.538 Unidentified 0.066 0.062 0.045 21.873

78.826 Unidentified 0.047 0.044 0.032 15.474

82.978 Unidentified 0.030 0.029 0.021 10.067

84.906 Unidentified 0.026 0.026 0.016 8.780

85.151 Unidentified 0.035 0.033 0.021 11.599

86.234 Unidentified 0.066 0.067 0.040 21.958

86.598 Unidentified 0.012 0.013 0.007 4.134

88.747 Unidentified 0.090 0.097 0.055 30.081

93.842 Unidentified 0.046 0.047 0.025 15.448

100.351 Unidentified 0.023 0.017 0.011 7.560

100.483 Unidentified 0.060 0.059 0.030 20.050

101.164 Unidentified 0.042 0.044 0.023 13.901

101.286 Unidentified 0.024 0.024 0.013 7.974

102.899 Unidentified 0.014 0.012 0.008 4.764

103.199 Unidentified 0.017 0.017 0.009 5.778

108.081 Unidentified 0.038 0.038 0.019 12.711

108.356 Unidentified 0.044 0.044 0.022 14.778

108.436 Unidentified 0.042 0.041 0.021 13.975

108.563 Unidentified 0.266 0.262 0.131 88.381

108.745 Unidentified 0.107 0.106 0.053 35.632

109.168 Unidentified 0.437 0.366 0.251 145.523

110.711 Unidentified 0.010 0.009 0.005 3.492

111.039 Unidentified 0.056 0.055 0.031 18.523

111.311 Unidentified 0.060 0.052 0.031 19.842

111.973 Unidentified 0.024 0.020 0.012 7.916

112.957 Unidentified 0.006 0.005 0.003 1.854

113.487 Unidentified 0.017 0.017 0.008 5.717

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C-481
Hydrocarbon Expert V4.7 Fri Aug 27 15:20:34 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91326 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91326

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Unidentified 113.611 Unidentified 0.006 0.006 0.003 2.016

115.146 Unidentified 0.010 0.010 0.005 3.399

116.944 Unidentified 0.012 0.012 0.006 4.091

117.127 Unidentified 0.004 0.003 0.002 1.225

126.298 Unidentified 0.007 0.006 0.003 2.235

130.004 Unidentified 0.003 0.002 0.002 1.013

Plus

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C-482
Hydrocarbon Expert V4.7 Fri Aug 27 15:20:34 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91326 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91326

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF

20.0 15.0 10.0 5.0 0.0

Propane

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

Ethanol

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

Unidentified

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

1,3-Cyclopentadiene

2,2-Dimethylbutane

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C-483
Hydrocarbon Expert V4.7 Fri Aug 27 15:20:34 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91326 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91326

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

n-Propanol Unidentified

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

2-Ethylbutene-1 n-Hexane

t-Hexene-3

3-Methylcyclopentene t-Hexene-2

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane 2,3,3-Trimethylbutene-1 2,2,3-Trimethylbutane

C6-Diolefin-1 Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1 Cyclohexane

n-Butanol

2-Methyl-c-hexene-3

4-Methylhexene-1

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C-484
Hydrocarbon Expert V4.7 Fri Aug 27 15:20:34 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91326 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91326

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF

70.0 65.0 60.0 55.0 50.0

4-Methyl-t/c-hexene-2

2-Methylhexane

Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane

C7 - Iso-Olefin - 2

2,2,4-Trimethylpentane Heptene-1

3-Methyl-c-hexene-3

t-Heptene-3

2-Methylhexene-1

n-Heptane c-Heptene-3 2-Methyl-2-hexene 3-Methyl-c-hexene-2

t-Heptene-2

Cyclopentene, 1,5-dimethyl3-Methyl-t-hexene-2

2-Pentene, 3,4-dimethyl-, (Z)-

Methylcyclohexane

1,1,3-Trimethylcyclopentane

2,2-Dimethylhexane

Unidentified

Ethylcyclopentane

2,2,3-Trimethylpentane 2,5-Dimethylhexane

2,4-Dimethylhexane

1c,2t,4-Trimethylcyclopentane

3,3-Dimethylhexane

1t,2c,3-Trimethylcyclopentane

2,3,4-Trimethylpentane

Toluene 2,3,3-Trimethylpentane

C8 - Diolefin - 1 2,3-Dimethylhexane

2-Methylheptane

Unidentified 4-Methylheptane

1,3-dimethyl-t-cyclohexane 3-Methylheptane 3-Ethylhexane

Unidentified

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C-485
Hydrocarbon Expert V4.7 Fri Aug 27 15:20:34 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91326 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91326

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF

95.0 90.0 85.0 80.0 75.0

2,2,5-Trimethylhexane

3c-Ethylmethylcyclopentane 3t-Ethylmethylcyclopentane

Unidentified Unidentified

n-Octane

Unidentified

2,3,5-Trimethylhexane

C9 - IsoOlefin - 1

1c,2-Dimethylcyclohexane 2,4-Dimethylheptane

Ethylcyclohexane 2,6-Dimethylheptane

Unidentified

2,5-Dimethylheptane 3,5-Dimethylheptane

Ethylbenzene Unidentified

m-Xylene Unidentified p-Xylene

C9-IsoOlefin-3 Unidentified 3,5-Dimethylheptane 3,3-Diethylpentane

4-Methyloctane 2-Methyloctane

Heptane, 3-ethyl- 3-Methyloctane

Unidentified o-Xylene

C10 - IsoParaffin - 1

trans-1,3-Diethylcyclopentane 2,2,4-trimethylheptane

n-Nonane

1,1-Methylethylcyclohexane

i-Propylbenzene

Unidentified 2,2-Dimethyloctane

2,5-Dimethyloctane C10 - IsoParaffin - 2

2,4-Dimethyloctane

2,6-Dimethyloctane

n-Propylbenzene

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

5-Methylnonane 4-Methylnonane 2,2,6-Trimethyloctane 1-Methyl-2-ethylbenzene

3-Methylnonane

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C-486
Hydrocarbon Expert V4.7 Fri Aug 27 15:20:34 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91326 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91326

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified

C11-Isoparaffin-2 1,2,4-Trimethylbenzene Unidentified

3-Ethyl-3-methylheptane i-Butylbenzene Unidentified n-Decane

Unidentified

1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene C11 Isoparaffin-4 1-Methyl-4-i-propylbenzene

Indan

Indene

C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene 1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

Unidentified 1-Methyl-2-n-propylbenzene Unidentified Unidentified Unidentified

Unidentified 2-Methylindan

1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

Unidentified 2-Undecene, (E)- Unidentified Unidentified 1,2-Dimethyl-3-ethylbenzene n-Undecane Unidentified 1-Ethyl-4-i-propylbenzene

1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene

Unidentified C12 - IsoParaffin - 1

Unidentified C11 - Aromatic - 3 5-Methylindan 1,2-Di-i-propylbenzene 1-methyl-4-(1-methylpropyl)be C11 - Aromatic - 4 4-Methylindan Benzene, 1-methyl-4-(2-methylpropyl)- 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene 1-Methyl-2-n-butylbenzene C11 - Aromatic - 7

C12 - IsoParaffin - 4 1,4-Di-i-propylbenzene

Unidentified Naphthalene

1,1-Dimethyl Indane

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

C11 - Aromatic - 12

2-Methylnaphthalene

1-Methylnaphthalene

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C-487
Hydrocarbon Expert V4.7 Fri Aug 27 15:20:34 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF 26-Aug-10, 13:09:57

Sample: ODDB-91326 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91326

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000018.D\SIG2000018_FID2_B.CDF

145.0 140.0 135.0 130.0 125.0

Unidentified

Unidentified

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C-488
Hydrocarbon Expert V4.7 Fri Aug 27 10:28:47 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91327 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91327

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 8.179 9.359 7.395

I-Paraffins 26.371 29.191 20.475

Aromatics 24.723 21.232 17.409

Mono-Aromatics 22.468 19.457 15.965

Naphthalenes 0.110 0.081 0.066

Naphtheno/Olefino-Benzs 0.179 0.151 0.105

Indenes 1.966 1.542 1.273

Naphthenes 6.329 6.239 5.446

Mono-Naphthenes 6.329 6.239 5.446

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 7.197 7.993 7.271

n-Olefins 2.989 3.403 3.110

Iso-Olefins 3.457 3.856 3.408

Naphtheno-Olefins 0.709 0.688 0.708

Di-Olefins 0.043 0.046 0.046

Oxygenates 22.530 21.487 37.932

Unidentified 4.671 4.499 4.072

Plus 0.000 0.000 0.000

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C-489
Hydrocarbon Expert V4.7 Fri Aug 27 10:28:47 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91327 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91327

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C2 22.401 21.366 37.779

C3 0.082 0.081 0.109

C4 0.817 1.034 1.086

C5 8.195 9.640 8.951

C6 20.564 22.607 18.745

C7 11.762 11.416 9.542

C8 10.358 9.857 7.353

C9 6.421 5.759 4.103

C10 12.071 11.141 6.925

C11 2.520 2.479 1.268

C12 0.138 0.121 0.066

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C-490
Hydrocarbon Expert V4.7 Fri Aug 27 10:28:47 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91327 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91327

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C3 0.008 0.012 0.014

C4 0.504 0.656 0.674

C5 1.264 1.519 1.361

C6 4.274 4.878 3.854

C7 0.909 1.000 0.705

C8 0.810 0.867 0.551

C9 0.283 0.297 0.171

C10 0.041 0.043 0.023

C11 0.086 0.087 0.043

I-Paraffins C4 0.068 0.092 0.092

C5 3.123 3.794 3.364

C6 9.714 11.116 8.758

C7 2.492 2.756 1.932

C8 3.057 3.280 2.079

C9 0.863 0.908 0.523

C10 5.079 5.247 2.748

C11 1.949 1.971 0.969

C12 0.026 0.026 0.012

Mono-Aromatics C6 0.724 0.620 0.720

C7 5.523 4.794 4.657

C8 5.794 5.032 4.240

C9 5.097 4.406 3.295

C10 4.822 4.173 2.791

C11 0.400 0.341 0.210

C12 0.109 0.092 0.052

Naphthalenes C10 0.095 0.070 0.058

C11 0.015 0.011 0.008

Naphtheno/Olefino-Benzs C10 0.179 0.151 0.105

Indenes C9 0.106 0.083 0.070

C10 1.847 1.450 1.197

C11 0.009 0.007 0.005

C12 0.004 0.003 0.002

Mono-Naphthenes C5 0.235 0.237 0.260

C6 3.330 3.292 3.074

C7 2.043 2.015 1.617

C8 0.652 0.634 0.452

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C-491
Hydrocarbon Expert V4.7 Fri Aug 27 10:28:47 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91327 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91327

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Mono-Naphthenes C9 0.065 0.058 0.040

C10 0.003 0.003 0.002

n-Olefins C4 0.190 0.234 0.262

C5 1.615 1.873 1.789

C6 1.027 1.131 0.948

C7 0.096 0.103 0.076

C11 0.062 0.063 0.034

Iso-Olefins C5 1.730 1.990 1.917

C6 0.993 1.085 0.916

C7 0.685 0.733 0.542

C8 0.045 0.044 0.031

C10 0.004 0.004 0.002

Naphtheno-Olefins C5 0.201 0.196 0.229

C6 0.501 0.484 0.474

C9 0.007 0.007 0.004

Di-Olefins C5 0.027 0.030 0.031

C7 0.015 0.015 0.014

Oxygenates C2 22.401 21.366 37.779

C3 0.074 0.069 0.095

C4 0.055 0.052 0.058

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C-492
Hydrocarbon Expert V4.7 Fri Aug 27 10:28:47 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91327 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91327

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 28.74 26.29

5% 87.79 81.88

10% 134.95 101.07

15% 140.05 138.76

20% 152.92 144.52

25% 155.61 154.48

30% 172.32 159.22

35% 172.56 172.38

40% 172.80 172.63

45% 173.04 172.88

50% 173.28 173.14

55% 197.13 177.07

60% 228.60 209.01

65% 231.03 230.84

70% 277.05 245.71

75% 291.70 281.73

80% 329.25 321.71

85% 334.61 332.42

90% 358.04 352.22

95% 363.20 363.20

FBP 397.97 388.02

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C-493
Hydrocarbon Expert V4.7 Fri Aug 27 10:28:47 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91327 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91327

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 7.553 74-98-6 P3 Propane 0.008 0.012 0.014 2.117

2 8.810 75-28-5 I4 i-Butane 0.068 0.092 0.092 18.575

3 9.624 115-11-7 K4 Isobutene 0.016 0.020 0.022 4.438

4 9.665 106-98-9 K4 Butene-1 0.018 0.022 0.024 4.971

5 10.024 106-97-8 P4 n-Butane 0.504 0.656 0.674 136.813

6 10.510 624-64-6 K4 t-Butene-2 0.072 0.089 0.099 20.107

7 10.637 463-82-1 I5 2,2-Dimethylpropane 0.007 0.008 0.007 1.806

8 11.252 590-18-1 K4 c-Butene-2 0.085 0.102 0.117 23.755

9 13.136 64-17-5 X2 Ethanol 22.401 21.366 37.779 2592.448

10 13.454 563-45-1 C5 3-Methylbutene-1 0.212 0.255 0.235 59.661

11 15.077 78-78-4 I5 i-Pentane 3.117 3.786 3.356 851.694

12 16.730 109-67-1 K5 Pentene-1 0.327 0.384 0.362 91.959

13 17.580 563-46-2 C5 2-Methylbutene-1 0.496 0.574 0.550 139.529

14 18.117 109-66-0 P5 n-Pentane 1.264 1.519 1.361 345.443

15 18.627 78-79-5 E5 2-Methyl-1,3-Butadiene 0.012 0.013 0.014 3.463

16 19.236 646-04-8 K5 t-Pentene-2 0.831 0.965 0.921 233.676

17 19.879 ? Unidentified 0.006 0.007 0.006 1.988

18 20.267 627-20-3 K5 c-Pentene-2 0.456 0.523 0.505 128.173

19 20.944 513-35-9 C5 2-Methylbutene-2 1.021 1.161 1.132 287.088

20 21.271 2004-70-8 E5 1t,3-Pentadiene 0.015 0.017 0.017 4.436

21 22.538 1574-41-0 B5 1,3-Cyclopentadiene 0.007 0.007 0.008 1.971

22 23.092 75-83-2 I6 2,2-Dimethylbutane 0.216 0.251 0.195 59.275

23 25.740 142-29-0 B5 Cyclopentene 0.194 0.189 0.221 56.071

24 26.902 71-23-8 X3 n-Propanol 0.074 0.069 0.095 14.507

25 26.998 ? Unidentified 0.059 0.066 0.054 20.289

26 27.606 287-92-3 M5 Cyclopentane 0.235 0.237 0.260 66.074

27 28.338 79-29-8 I6 2,3-Dimethylbutane 1.008 1.147 0.909 276.570

28 28.734 ? Unidentified 0.052 0.053 0.046 17.890

29 29.197 691-38-3 C6 4-Methyl-c-pentene-2 0.045 0.050 0.041 12.606

30 29.436 107-83-5 I6 2-Methylpentane 5.203 5.995 4.691 1427.392

31 29.846 674-76-0 C6 4-Methyl-t-pentene-2 0.129 0.144 0.119 36.274

32 32.075 96-14-0 I6 3-Methylpentane 3.287 3.724 2.964 901.752

33 33.228 763-29-1 C6 2-Methylpentene-1 0.221 0.243 0.204 62.196

34 33.455 592-41-6 K6 Hexene-1 0.158 0.175 0.146 44.390

35 35.827 110-54-3 P6 n-Hexane 4.274 4.878 3.854 1172.592

36 36.44113269-52-8 K6 t-Hexene-3 0.260 0.287 0.240 73.101

37 36.917 4050-45-7 K6 t-Hexene-2 0.398 0.438 0.367 111.781

38 37.043 1120-62-3 B6 3-Methylcyclopentene 0.100 0.099 0.095 28.141

39 37.408 625-27-4 C6 2-Methylpentene-2 0.336 0.366 0.311 94.559

40 37.820 922-62-3 C6 3-Methyl-c-pentene-2 0.261 0.281 0.241 73.337

41 38.745 7688-21-3 K6 c-Hexene-2 0.212 0.230 0.195 59.449

42 40.089 3404-73-7 C7 3,3-Dimethylpentene-1 0.307 0.330 0.243 86.391

43 40.678 96-37-7 M6 Methylcyclopentane 1.892 1.902 1.746 531.671

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C-494
Hydrocarbon Expert V4.7 Fri Aug 27 10:28:47 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91327 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91327

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 42.233 108-08-7 I7 2,4-Dimethylpentane 0.431 0.483 0.334 118.818

45 42.533 594-56-9 C7 2,3,3-Trimethylbutene-1 0.014 0.015 0.011 3.887

46 42.781 464-06-2 I7 2,2,3-Trimethylbutane 0.053 0.058 0.041 14.724

47 45.426 1528-30-9 E7 C6-Diolefin-1 0.015 0.015 0.014 4.281

48 45.639 71-42-3 Q6 Benzene 0.724 0.620 0.720 219.241

49 45.833 693-89-0 B6 1-Methylcyclopentene 0.357 0.345 0.338 102.729

50 46.640 3404-61-3 C7 3-Methylhexene-1 0.016 0.017 0.013 4.507

51 47.236 3524-73-0 C7 5-Methylhexene-1 0.082 0.088 0.065 22.959

52 47.559 110-82-7 M6 Cyclohexane 1.438 1.391 1.328 404.294

53 48.059 71-36-3 X4 n-Butanol 0.055 0.052 0.058 11.742

54 49.27215840-60-5 C7 2-Methyl-c-hexene-3 0.040 0.043 0.032 11.193

55 49.622 3769-23-1 C7 4-Methylhexene-1 0.011 0.012 0.009 3.228

56 50.267 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.051 0.054 0.040 14.212

57 50.666 591-76-4 I7 2-Methylhexane 1.231 1.365 0.954 339.006

58 50.841 ? Unidentified 0.068 0.074 0.055 23.503

59 51.153 110-83-8 B6 Cyclohexene 0.044 0.041 0.042 12.426

60 52.493 589-34-4 I7 3-Methylhexane 0.776 0.850 0.602 213.780

61 53.353 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.194 0.195 0.154 54.572

62 53.939 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.154 0.156 0.122 43.326

63 54.561 822-50-4 M7 1t,2-Dimethylcyclopentane 0.234 0.234 0.185 65.793

64 54.847 C7 C7 - Iso-Olefin - 2 0.022 0.023 0.017 6.127

65 55.148 540-84-1 I8 2,2,4-Trimethylpentane 1.102 1.198 0.749 304.018

66 55.468 592-76-7 K7 Heptene-1 0.029 0.031 0.023 8.040

67 56.801 4914-89-0 C7 3-Methyl-c-hexene-3 0.014 0.014 0.011 3.872

68 57.33114686-14-7 K7 t-Heptene-3 0.031 0.034 0.025 8.804

69 57.684 6094-02-6 C7 2-Methylhexene-1 0.056 0.061 0.044 15.758

70 58.060 142-82-5 P7 n-Heptane 0.909 1.000 0.705 250.301

71 58.276 7642-10-6 K7 c-Heptene-3 0.023 0.025 0.019 6.599

72 58.547 2738-19-4 C7 2-Methyl-2-hexene 0.025 0.027 0.020 7.076

73 58.79210574-36-4 C7 3-Methyl-c-hexene-2 0.019 0.021 0.015 5.472

74 59.17314686-13-6 K7 t-Heptene-2 0.012 0.013 0.010 3.419

75 59.65016491-15-9 M7 Cyclopentene, 1,5-dimethyl- 0.018 0.018 0.015 5.183

76 60.07820710-38-8 C7 3-Methyl-t-hexene-2 0.016 0.016 0.012 4.415

77 60.860 4914-91-4 C7 2-Pentene, 3,4-dimethyl-, (Z)- 0.012 0.013 0.010 3.388

78 61.523 108-87-2 M7 Methylcyclohexane 1.377 1.347 1.089 386.953

79 62.459 4516-69-2 M8 1,1,3-Trimethylcyclopentane 0.041 0.041 0.028 11.386

80 62.848 590-73-8 I8 2,2-Dimethylhexane 0.034 0.037 0.023 9.453

81 63.359 ? Unidentified 0.054 0.057 0.038 18.669

82 64.297 1640-89-7 M7 Ethylcyclopentane 0.066 0.065 0.052 18.498

83 64.945 564-02-3 I8 2,2,3-Trimethylpentane 0.057 0.060 0.039 15.846

84 65.169 592-13-2 I8 2,5-Dimethylhexane 0.181 0.197 0.123 50.088

85 65.506 589-43-5 I8 2,4-Dimethylhexane 0.191 0.205 0.130 52.699

86 66.345 4850-28-6 M8 1c,2t,4-Trimethylcyclopentane 0.042 0.041 0.029 11.757

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C-495
Hydrocarbon Expert V4.7 Fri Aug 27 10:28:47 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91327 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91327

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 66.739 563-16-6 I8 3,3-Dimethylhexane 0.028 0.030 0.019 7.782

88 67.85815890-40-1 M8 1t,2c,3-Trimethylcyclopentane 0.038 0.037 0.026 10.575

89 68.470 565-75-3 I8 2,3,4-Trimethylpentane 0.409 0.428 0.278 112.781

90 69.019 108-88-3 Q7 Toluene 5.523 4.794 4.657 1653.405

91 70.512 C8 C8 - Diolefin - 1 0.017 0.016 0.012 4.679

92 70.791 584-94-1 I8 2,3-Dimethylhexane 0.160 0.169 0.109 44.175

93 72.049 592-27-8 I8 2-Methylheptane 0.330 0.355 0.224 90.953

94 72.301 589-53-7 I8 4-Methylheptane 0.126 0.135 0.086 34.844

95 72.450 ? Unidentified 0.013 0.014 0.009 4.570

96 73.225 M8 1,3-dimethyl-t-cyclohexane 0.263 0.257 0.182 73.975

97 73.362 589-81-1 I8 3-Methylheptane 0.278 0.297 0.189 76.791

98 73.563 619-99-8 I8 3-Ethylhexane 0.160 0.169 0.109 44.185

99 74.459 ? Unidentified 0.042 0.041 0.029 14.575

100 75.247 3522-94-9 I9 2,2,5-Trimethylhexane 0.178 0.190 0.108 49.329

101 75.609 M8 3c-Ethylmethylcyclopentane 0.015 0.015 0.011 4.346

102 75.825 M8 3t-Ethylmethylcyclopentane 0.022 0.022 0.015 6.221

103 76.530 ? Unidentified 0.100 0.097 0.069 34.502

104 77.875 111-65-9 P8 n-Octane 0.810 0.867 0.551 223.484

105 80.353 1069-53-0 I9 2,3,5-Trimethylhexane 0.030 0.031 0.018 8.275

106 80.908 C8 C9 - IsoOlefin - 1 0.029 0.028 0.020 8.016

107 81.366 2207-01-4 M8 1c,2-Dimethylcyclohexane 0.024 0.022 0.016 6.646

108 81.521 1071-26-7 I9 2,4-Dimethylheptane 0.046 0.048 0.028 12.595

109 82.175 1678-91-7 M8 Ethylcyclohexane 0.199 0.191 0.138 55.853

110 82.476 1072-05-5 I9 2,6-Dimethylheptane 0.088 0.093 0.053 24.338

111 82.976 ? Unidentified 0.041 0.040 0.029 14.247

112 83.406 I9 2,5-Dimethylheptane 0.116 0.122 0.070 32.038

113 83.605 926-82-9 I9 3,5-Dimethylheptane 0.028 0.029 0.017 7.803

114 84.731 100-41-4 Q8 Ethylbenzene 0.992 0.861 0.726 294.651

115 84.922 ? Unidentified 0.013 0.013 0.008 4.399

116 85.153 ? Unidentified 0.030 0.029 0.019 10.450

117 85.958 108-38-3 Q8 m-Xylene 2.730 2.378 1.998 811.298

118 86.104 106-42-3 Q8 p-Xylene 1.181 1.032 0.864 350.901

119 86.231 ? Unidentified 0.038 0.040 0.023 13.185

120 86.596 ? Unidentified 0.014 0.013 0.009 4.787

121 86.755 I9 3,5-Dimethylheptane 0.017 0.018 0.010 4.754

122 86.883 1067-20-5 I9 3,3-Diethylpentane 0.015 0.015 0.009 4.028

123 87.275 2216-34-4 I9 4-Methyloctane 0.091 0.095 0.055 25.046

124 87.407 3221-61-2 I9 2-Methyloctane 0.120 0.127 0.073 33.265

125 87.884 B9 C9 - NaphOlefin - 2 0.007 0.007 0.004 2.014

126 88.10815869-80-4 I9 Heptane, 3-ethyl- 0.017 0.018 0.010 4.694

127 88.270 2216-33-3 I9 3-Methyloctane 0.117 0.123 0.071 32.451

128 88.930 95-47-6 Q8 o-Xylene 0.891 0.762 0.652 264.656

129 89.322 I10 C10 - IsoParaffin - 1 0.025 0.026 0.014 6.861

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C-496
Hydrocarbon Expert V4.7 Fri Aug 27 10:28:47 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91327 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91327

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 89.756 3728-57-2 M8 Cyclopentane, 1-methyl-2-propyl- 0.009 0.008 0.007 2.677

131 89.912 M9 trans-1,3-Diethylcyclopentane 0.033 0.029 0.021 9.922

132 90.18214720-74-2 I10 2,2,4-trimethylheptane 0.046 0.047 0.025 12.611

133 91.748 111-84-2 P9 n-Nonane 0.283 0.297 0.171 78.269

134 92.324 4926-90-3 M9 1,1-Methylethylcyclohexane 0.028 0.026 0.017 7.878

135 93.095 98-82-8 Q9 i-Propylbenzene 0.035 0.031 0.023 10.407

136 93.273 ? Unidentified 0.008 0.008 0.005 2.876

137 93.273 ? Unidentified 0.008 0.009 0.005 2.876

138 93.273 ? Unidentified 0.008 0.006 0.005 2.876

139 93.387 696-29-7 M9 1-Methyl-2-propyl-cyclopentan 0.004 0.004 0.002 1.119

140 93.387 C10 C10-IsoOlefin-4 0.004 0.004 0.002 1.119

141 93.387 I10 C10-isoparaffin-x 0.000 0.000 0.000 1.119

142 93.843 ? Unidentified 0.150 0.156 0.082 51.658

143 94.06415869-87-1 I10 2,2-Dimethyloctane 0.054 0.056 0.029 14.888

144 94.526 ? Unidentified 0.019 0.014 1.470 6.512

145 94.526 ? Unidentified 0.019 0.020 0.010 6.512

146 94.722 ? Unidentified 0.022 0.021 0.014 7.613

147 94.86215869-89-3 I10 2,5-Dimethyloctane 0.093 0.096 0.051 25.784

148 95.068 I10 C10 - IsoParaffin - 2 0.014 0.015 0.008 3.942

149 95.326 2040-95-1 I10 2,7-Dimethyloctane 0.056 0.058 0.030 15.463

150 95.509 2051-30-1 I10 2,4-Dimethyloctane 0.242 0.251 0.132 67.191

151 95.896 I10 2,6-Dimethyloctane 0.075 0.077 0.041 20.711

152 96.060 I10 C10 Isoparaffin -1 0.005 0.005 0.003 1.419

153 96.555 103-65-1 Q9 n-Propylbenzene 0.315 0.275 0.204 93.069

154 96.754 I10 3-Methyl-5-ethylheptane 0.009 0.010 0.005 2.612

155 97.402 620-14-4 Q9 1-Methyl-3-ethylbenzene 1.105 0.962 0.714 326.178

156 97.635 622-96-8 Q9 1-Methyl-4-ethylbenzene 0.497 0.435 0.322 146.856

157 98.260 108-67-8 Q9 1,3,5-Trimethylbenzene 0.711 0.618 0.459 209.794

158 98.72515869-85-9 I10 5-Methylnonane 0.011 0.011 0.006 2.928

159 98.91517301-94-8 I10 4-Methylnonane 0.023 0.024 0.013 6.459

160 99.140 I10 2,2,6-Trimethyloctane 3.878 4.017 2.118 1074.551

161 99.346 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.363 0.310 0.235 107.124

162 99.710 ? Unidentified 0.012 0.012 0.007 4.150

163 99.890 5911-04-6 I10 3-Methylnonane 0.023 0.024 0.013 6.427

164 100.074 ? Unidentified 0.013 0.014 0.007 4.393

165 100.356 ? Unidentified 0.224 0.168 0.111 77.047

166 100.489 ? Unidentified 0.619 0.626 0.308 213.181

167 100.705 I11 C11-Isoparaffin-2 0.326 0.330 0.162 90.374

168 100.982 95-63-6 Q9 1,2,4-Trimethylbenzene 1.845 1.585 1.193 544.634

169 101.170 ? Unidentified 0.370 0.397 0.205 127.269

170 101.292 ? Unidentified 0.219 0.225 0.120 75.383

171 101.554 ? Unidentified 0.050 0.051 0.027 17.139

172 102.197 ? Unidentified 0.025 0.024 0.014 8.604

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C-497
Hydrocarbon Expert V4.7 Fri Aug 27 10:28:47 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91327 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91327

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 102.34117302-01-1 I10 3-Ethyl-3-methylheptane 0.525 0.531 0.261 145.746

174 102.546 ? Unidentified 0.130 0.131 0.064 44.638

175 102.690 538-93-2 Q10 i-Butylbenzene 0.408 0.360 0.236 119.797

176 102.890 124-18-5 P10 n-Decane 0.041 0.043 0.023 11.485

177 103.200 ? Unidentified 0.129 0.131 0.072 44.497

178 103.689 ? Unidentified 0.019 0.016 0.012 6.517

179 103.855 526-73-8 Q9 1,2,3-Trimethylbenzene 0.225 0.190 0.146 66.529

180 104.195 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.045 0.040 0.026 13.286

181 104.412 I11 C11 Isoparaffin-4 0.064 0.065 0.032 17.757

182 104.619 99-87-6 Q10 1-Methyl-4-i-propylbenzene 0.378 0.332 0.219 110.990

183 104.955 ? Unidentified 0.065 0.051 0.043 22.402

184 105.052 J9 Indan 0.106 0.083 0.070 31.900

185 105.265 I11 C11-Isoparaffin-5 0.026 0.026 0.013 7.143

186 105.652 J10 Indene 1.591 1.242 1.046 477.486

187 106.079 M10 n-ButylCyclohexane 0.003 0.003 0.002 0.819

188 106.205 ? Unidentified 0.011 0.011 0.006 3.946

189 106.363 I11 C11-Isoparaffin-7 0.572 0.578 0.284 158.540

190 106.552 141-93-5 Q10 1,3-Diethylbenzene 0.024 0.021 0.014 6.962

191 106.847 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 1.674 1.463 0.969 491.568

192 107.105 105-05-5 Q10 1,4-Diethylbenzene 0.415 0.362 0.240 121.806

193 107.385 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.104 0.089 0.060 30.440

194 107.621 135-01-3 Q10 1,2-Diethylbenzene 0.116 0.099 0.067 34.073

195 108.084 ? Unidentified 0.127 0.128 0.063 43.588

196 108.237 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.043 0.037 0.025 12.536

197 108.359 ? Unidentified 0.129 0.131 0.065 44.289

198 108.438 ? Unidentified 0.119 0.121 0.059 41.124

199 108.569 I11 C11- Isoparaffin-11 0.961 0.972 0.478 266.662

200 108.747 ? Unidentified 0.306 0.310 0.152 105.438

201 109.171 ? Unidentified 0.861 0.739 0.499 296.547

202 109.397 J10 2-Methylindan 0.142 0.111 0.084 42.717

203 109.743 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.309 0.265 0.179 90.595

204 109.875 ? Unidentified 0.041 0.035 0.024 14.031

205 110.288 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.734 0.620 0.425 215.546

206 110.712 ? Unidentified 0.025 0.023 0.013 8.746

207 110.906 693-61-8 K11 2-Undecene, (E)- 0.062 0.063 0.034 17.283

208 111.039 ? Unidentified 0.139 0.141 0.077 47.762

209 111.311 ? Unidentified 0.120 0.102 0.063 41.477

210 111.411 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.060 0.051 0.035 17.660

211 111.711 1120-21-4 P11 n-Undecane 0.086 0.087 0.043 23.760

212 111.862 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.100 0.084 0.052 29.208

213 111.974 ? Unidentified 0.066 0.056 0.034 22.649

214 112.349 Q10 1,2,4,5-Tetramethylbenzene 0.222 0.188 0.128 65.160

215 112.615 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.291 0.246 0.169 85.580

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C-498
Hydrocarbon Expert V4.7 Fri Aug 27 10:28:47 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91327 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91327

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

216 112.827 ? Unidentified 0.013 0.011 0.007 4.609

217 112.956 ? Unidentified 0.017 0.014 0.010 5.759

218 113.131 I12 C12 - IsoParaffin - 1 0.026 0.026 0.012 7.234

219 113.476 ? Unidentified 0.032 0.032 0.014 10.874

220 113.613 ? Unidentified 0.010 0.011 0.005 3.612

221 113.811 Q11 C11 - Aromatic - 3 0.060 0.051 0.032 17.574

222 113.946 874-35-1 H10 5-Methylindan 0.092 0.078 0.054 27.092

223 114.070 Q12 1,2-Di-i-propylbenzene 0.034 0.029 0.016 9.887

224 114.285 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.047 0.040 0.025 13.688

225 114.449 Q11 C11 - Aromatic - 4 0.031 0.026 0.016 9.126

226 114.695 824-22-6 J10 4-Methylindan 0.114 0.096 0.067 33.388

227 114.849 5161-04-6 Q11 Benzene, 1-methyl-4-(2-methylpropyl)-0.027 0.023 0.014 7.966

228 114.942 824-63-5 H10 2-Methylindan 0.087 0.073 0.051 25.506

229 115.145 ? Unidentified 0.010 0.008 0.005 3.392

230 115.258 538-68-1 Q11 n-Pentylbenzene 0.011 0.009 0.006 3.165

231 115.486 Q11 tert-Pentylbenzene 0.045 0.038 0.024 13.191

232 115.798 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.019 0.016 0.010 5.615

233 115.909 Q11 C11 - Aromatic - 7 0.027 0.024 0.014 7.936

234 116.369 100-18-5 Q12 1,4-Di-i-propylbenzene 0.036 0.030 0.017 10.472

235 116.811 91-20-3 G10 Naphthalene 0.095 0.070 0.058 29.213

236 117.248 J11 1,1-Dimethyl Indane 0.009 0.007 0.005 2.593

237 117.413 J12 Dimethyl Indane - 1 0.004 0.003 0.002 1.157

238 117.594 7364-19-4 Q12 1t-Butyl-4-ethylbenzene 0.005 0.004 0.003 1.535

239 117.895 Q12 1,3-Di-n-propylbenzene 0.033 0.028 0.016 9.732

240 118.005 Q11 C11 - Aromatic - 11 0.019 0.017 0.010 5.529

241 118.559 Q11 C11 - Aromatic - 12 0.014 0.012 0.007 3.968

242 123.440 91-57-6 G11 2-Methylnaphthalene 0.010 0.007 0.005 2.931

243 124.306 90-12-0 G11 1-Methylnaphthalene 0.005 0.004 0.003 1.546

244 130.003 ? Unidentified 0.003 0.002 0.002 1.064

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C-499
Hydrocarbon Expert V4.7 Fri Aug 27 10:28:47 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91327 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91327

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 7.553 74-98-6 Propane 0.008 0.012 0.014 2.117

10.024 106-97-8 n-Butane 0.504 0.656 0.674 136.813

18.117 109-66-0 n-Pentane 1.264 1.519 1.361 345.443

35.827 110-54-3 n-Hexane 4.274 4.878 3.854 1172.592

58.060 142-82-5 n-Heptane 0.909 1.000 0.705 250.301

77.875 111-65-9 n-Octane 0.810 0.867 0.551 223.484

91.748 111-84-2 n-Nonane 0.283 0.297 0.171 78.269

102.890 124-18-5 n-Decane 0.041 0.043 0.023 11.485

111.711 1120-21-4 n-Undecane 0.086 0.087 0.043 23.760

I-Paraffins 8.810 75-28-5 i-Butane 0.068 0.092 0.092 18.575

10.637 463-82-1 2,2-Dimethylpropane 0.007 0.008 0.007 1.806

15.077 78-78-4 i-Pentane 3.117 3.786 3.356 851.694

23.092 75-83-2 2,2-Dimethylbutane 0.216 0.251 0.195 59.275

28.338 79-29-8 2,3-Dimethylbutane 1.008 1.147 0.909 276.570

29.436 107-83-5 2-Methylpentane 5.203 5.995 4.691 1427.392

32.075 96-14-0 3-Methylpentane 3.287 3.724 2.964 901.752

42.233 108-08-7 2,4-Dimethylpentane 0.431 0.483 0.334 118.818

42.781 464-06-2 2,2,3-Trimethylbutane 0.053 0.058 0.041 14.724

50.666 591-76-4 2-Methylhexane 1.231 1.365 0.954 339.006

52.493 589-34-4 3-Methylhexane 0.776 0.850 0.602 213.780

55.148 540-84-1 2,2,4-Trimethylpentane 1.102 1.198 0.749 304.018

62.848 590-73-8 2,2-Dimethylhexane 0.034 0.037 0.023 9.453

64.945 564-02-3 2,2,3-Trimethylpentane 0.057 0.060 0.039 15.846

65.169 592-13-2 2,5-Dimethylhexane 0.181 0.197 0.123 50.088

65.506 589-43-5 2,4-Dimethylhexane 0.191 0.205 0.130 52.699

66.739 563-16-6 3,3-Dimethylhexane 0.028 0.030 0.019 7.782

68.470 565-75-3 2,3,4-Trimethylpentane 0.409 0.428 0.278 112.781

70.791 584-94-1 2,3-Dimethylhexane 0.160 0.169 0.109 44.175

72.049 592-27-8 2-Methylheptane 0.330 0.355 0.224 90.953

72.301 589-53-7 4-Methylheptane 0.126 0.135 0.086 34.844

73.362 589-81-1 3-Methylheptane 0.278 0.297 0.189 76.791

73.563 619-99-8 3-Ethylhexane 0.160 0.169 0.109 44.185

75.247 3522-94-9 2,2,5-Trimethylhexane 0.178 0.190 0.108 49.329

80.353 1069-53-0 2,3,5-Trimethylhexane 0.030 0.031 0.018 8.275

81.521 1071-26-7 2,4-Dimethylheptane 0.046 0.048 0.028 12.595

82.476 1072-05-5 2,6-Dimethylheptane 0.088 0.093 0.053 24.338

83.406 2,5-Dimethylheptane 0.116 0.122 0.070 32.038

83.605 926-82-9 3,5-Dimethylheptane 0.028 0.029 0.017 7.803

86.755 3,5-Dimethylheptane 0.017 0.018 0.010 4.754

86.883 1067-20-5 3,3-Diethylpentane 0.015 0.015 0.009 4.028

87.275 2216-34-4 4-Methyloctane 0.091 0.095 0.055 25.046

87.407 3221-61-2 2-Methyloctane 0.120 0.127 0.073 33.265

88.10815869-80-4 Heptane, 3-ethyl- 0.017 0.018 0.010 4.694

88.270 2216-33-3 3-Methyloctane 0.117 0.123 0.071 32.451

89.322 C10 - IsoParaffin - 1 0.025 0.026 0.014 6.861

90.18214720-74-2 2,2,4-trimethylheptane 0.046 0.047 0.025 12.611

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C-500
Hydrocarbon Expert V4.7 Fri Aug 27 10:28:47 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91327 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91327

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

I-Paraffins 93.387 C10-isoparaffin-x 0.000 0.000 0.000 1.119

94.06415869-87-1 2,2-Dimethyloctane 0.054 0.056 0.029 14.888

94.86215869-89-3 2,5-Dimethyloctane 0.093 0.096 0.051 25.784

95.068 C10 - IsoParaffin - 2 0.014 0.015 0.008 3.942

95.326 2040-95-1 2,7-Dimethyloctane 0.056 0.058 0.030 15.463

95.509 2051-30-1 2,4-Dimethyloctane 0.242 0.251 0.132 67.191

95.896 2,6-Dimethyloctane 0.075 0.077 0.041 20.711

96.060 C10 Isoparaffin -1 0.005 0.005 0.003 1.419

96.754 3-Methyl-5-ethylheptane 0.009 0.010 0.005 2.612

98.72515869-85-9 5-Methylnonane 0.011 0.011 0.006 2.928

98.91517301-94-8 4-Methylnonane 0.023 0.024 0.013 6.459

99.140 2,2,6-Trimethyloctane 3.878 4.017 2.118 1074.551

99.890 5911-04-6 3-Methylnonane 0.023 0.024 0.013 6.427

100.705 C11-Isoparaffin-2 0.326 0.330 0.162 90.374

102.34117302-01-1 3-Ethyl-3-methylheptane 0.525 0.531 0.261 145.746

104.412 C11 Isoparaffin-4 0.064 0.065 0.032 17.757

105.265 C11-Isoparaffin-5 0.026 0.026 0.013 7.143

106.363 C11-Isoparaffin-7 0.572 0.578 0.284 158.540

108.569 C11- Isoparaffin-11 0.961 0.972 0.478 266.662

113.131 C12 - IsoParaffin - 1 0.026 0.026 0.012 7.234

Aromatics

Mono-Aromatics 45.639 71-42-3 Benzene 0.724 0.620 0.720 219.241

69.019 108-88-3 Toluene 5.523 4.794 4.657 1653.405

84.731 100-41-4 Ethylbenzene 0.992 0.861 0.726 294.651

85.958 108-38-3 m-Xylene 2.730 2.378 1.998 811.298

86.104 106-42-3 p-Xylene 1.181 1.032 0.864 350.901

88.930 95-47-6 o-Xylene 0.891 0.762 0.652 264.656

93.095 98-82-8 i-Propylbenzene 0.035 0.031 0.023 10.407

96.555 103-65-1 n-Propylbenzene 0.315 0.275 0.204 93.069

97.402 620-14-4 1-Methyl-3-ethylbenzene 1.105 0.962 0.714 326.178

97.635 622-96-8 1-Methyl-4-ethylbenzene 0.497 0.435 0.322 146.856

98.260 108-67-8 1,3,5-Trimethylbenzene 0.711 0.618 0.459 209.794

99.346 611-14-3 1-Methyl-2-ethylbenzene 0.363 0.310 0.235 107.124

100.982 95-63-6 1,2,4-Trimethylbenzene 1.845 1.585 1.193 544.634

102.690 538-93-2 i-Butylbenzene 0.408 0.360 0.236 119.797

103.855 526-73-8 1,2,3-Trimethylbenzene 0.225 0.190 0.146 66.529

104.195 535-77-3 1-Methyl-3-i-propylbenzene 0.045 0.040 0.026 13.286

104.619 99-87-6 1-Methyl-4-i-propylbenzene 0.378 0.332 0.219 110.990

106.552 141-93-5 1,3-Diethylbenzene 0.024 0.021 0.014 6.962

106.847 1074-43-7 1-Methyl-3-n-propylbenzene 1.674 1.463 0.969 491.568

107.105 105-05-5 1,4-Diethylbenzene 0.415 0.362 0.240 121.806

107.385 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.104 0.089 0.060 30.440

107.621 135-01-3 1,2-Diethylbenzene 0.116 0.099 0.067 34.073

108.237 1074-17-5 1-Methyl-2-n-propylbenzene 0.043 0.037 0.025 12.536

109.743 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.309 0.265 0.179 90.595

110.288 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.734 0.620 0.425 215.546

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C-501
Hydrocarbon Expert V4.7 Fri Aug 27 10:28:47 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91327 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91327

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 111.411 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.060 0.051 0.035 17.660

111.862 4218-48-8 1-Ethyl-4-i-propylbenzene 0.100 0.084 0.052 29.208

112.349 1,2,4,5-Tetramethylbenzene 0.222 0.188 0.128 65.160

112.615 527-53-7 1,2,3,5-Tetramethylbenzene 0.291 0.246 0.169 85.580

113.811 C11 - Aromatic - 3 0.060 0.051 0.032 17.574

114.070 1,2-Di-i-propylbenzene 0.034 0.029 0.016 9.887

114.285 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.047 0.040 0.025 13.688

114.449 C11 - Aromatic - 4 0.031 0.026 0.016 9.126

114.849 5161-04-6 Benzene, 1-methyl-4-(2-methylpropyl)-0.027 0.023 0.014 7.966

115.258 538-68-1 n-Pentylbenzene 0.011 0.009 0.006 3.165

115.486 tert-Pentylbenzene 0.045 0.038 0.024 13.191

115.798 577-55-9 1-Methyl-2-n-butylbenzene 0.019 0.016 0.010 5.615

115.909 C11 - Aromatic - 7 0.027 0.024 0.014 7.936

116.369 100-18-5 1,4-Di-i-propylbenzene 0.036 0.030 0.017 10.472

117.594 7364-19-4 1t-Butyl-4-ethylbenzene 0.005 0.004 0.003 1.535

117.895 1,3-Di-n-propylbenzene 0.033 0.028 0.016 9.732

118.005 C11 - Aromatic - 11 0.019 0.017 0.010 5.529

118.559 C11 - Aromatic - 12 0.014 0.012 0.007 3.968

Naphthalenes 116.811 91-20-3 Naphthalene 0.095 0.070 0.058 29.213

123.440 91-57-6 2-Methylnaphthalene 0.010 0.007 0.005 2.931

124.306 90-12-0 1-Methylnaphthalene 0.005 0.004 0.003 1.546

Naphtheno/Olefino-Benzs 113.946 874-35-1 5-Methylindan 0.092 0.078 0.054 27.092

114.942 824-63-5 2-Methylindan 0.087 0.073 0.051 25.506

Indenes 105.052 Indan 0.106 0.083 0.070 31.900

105.652 Indene 1.591 1.242 1.046 477.486

109.397 2-Methylindan 0.142 0.111 0.084 42.717

114.695 824-22-6 4-Methylindan 0.114 0.096 0.067 33.388

117.248 1,1-Dimethyl Indane 0.009 0.007 0.005 2.593

117.413 Dimethyl Indane - 1 0.004 0.003 0.002 1.157

Naphthenes

Mono-Naphthenes 27.606 287-92-3 Cyclopentane 0.235 0.237 0.260 66.074

40.678 96-37-7 Methylcyclopentane 1.892 1.902 1.746 531.671

47.559 110-82-7 Cyclohexane 1.438 1.391 1.328 404.294

53.353 1759-58-6 1t,3-Dimethylcyclopentane 0.194 0.195 0.154 54.572

53.939 2532-58-3 1c,3-Dimethylcyclopentane 0.154 0.156 0.122 43.326

54.561 822-50-4 1t,2-Dimethylcyclopentane 0.234 0.234 0.185 65.793

59.65016491-15-9 Cyclopentene, 1,5-dimethyl- 0.018 0.018 0.015 5.183

61.523 108-87-2 Methylcyclohexane 1.377 1.347 1.089 386.953

62.459 4516-69-2 1,1,3-Trimethylcyclopentane 0.041 0.041 0.028 11.386

64.297 1640-89-7 Ethylcyclopentane 0.066 0.065 0.052 18.498

66.345 4850-28-6 1c,2t,4-Trimethylcyclopentane 0.042 0.041 0.029 11.757

67.85815890-40-1 1t,2c,3-Trimethylcyclopentane 0.038 0.037 0.026 10.575

73.225 1,3-dimethyl-t-cyclohexane 0.263 0.257 0.182 73.975

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C-502
Hydrocarbon Expert V4.7 Fri Aug 27 10:28:47 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91327 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91327

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Naphthenes 75.609 3c-Ethylmethylcyclopentane 0.015 0.015 0.011 4.346

75.825 3t-Ethylmethylcyclopentane 0.022 0.022 0.015 6.221

81.366 2207-01-4 1c,2-Dimethylcyclohexane 0.024 0.022 0.016 6.646

82.175 1678-91-7 Ethylcyclohexane 0.199 0.191 0.138 55.853

89.756 3728-57-2 Cyclopentane, 1-methyl-2-propyl- 0.009 0.008 0.007 2.677

89.912 trans-1,3-Diethylcyclopentane 0.033 0.029 0.021 9.922

92.324 4926-90-3 1,1-Methylethylcyclohexane 0.028 0.026 0.017 7.878

93.387 696-29-7 1-Methyl-2-propyl-cyclopentan 0.004 0.004 0.002 1.119

106.079 n-ButylCyclohexane 0.003 0.003 0.002 0.819

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.624 115-11-7 Isobutene 0.016 0.020 0.022 4.438

9.665 106-98-9 Butene-1 0.018 0.022 0.024 4.971

10.510 624-64-6 t-Butene-2 0.072 0.089 0.099 20.107

11.252 590-18-1 c-Butene-2 0.085 0.102 0.117 23.755

16.730 109-67-1 Pentene-1 0.327 0.384 0.362 91.959

19.236 646-04-8 t-Pentene-2 0.831 0.965 0.921 233.676

20.267 627-20-3 c-Pentene-2 0.456 0.523 0.505 128.173

33.455 592-41-6 Hexene-1 0.158 0.175 0.146 44.390

36.44113269-52-8 t-Hexene-3 0.260 0.287 0.240 73.101

36.917 4050-45-7 t-Hexene-2 0.398 0.438 0.367 111.781

38.745 7688-21-3 c-Hexene-2 0.212 0.230 0.195 59.449

55.468 592-76-7 Heptene-1 0.029 0.031 0.023 8.040

57.33114686-14-7 t-Heptene-3 0.031 0.034 0.025 8.804

58.276 7642-10-6 c-Heptene-3 0.023 0.025 0.019 6.599

59.17314686-13-6 t-Heptene-2 0.012 0.013 0.010 3.419

110.906 693-61-8 2-Undecene, (E)- 0.062 0.063 0.034 17.283

Iso-Olefins 13.454 563-45-1 3-Methylbutene-1 0.212 0.255 0.235 59.661

17.580 563-46-2 2-Methylbutene-1 0.496 0.574 0.550 139.529

20.944 513-35-9 2-Methylbutene-2 1.021 1.161 1.132 287.088

29.197 691-38-3 4-Methyl-c-pentene-2 0.045 0.050 0.041 12.606

29.846 674-76-0 4-Methyl-t-pentene-2 0.129 0.144 0.119 36.274

33.228 763-29-1 2-Methylpentene-1 0.221 0.243 0.204 62.196

37.408 625-27-4 2-Methylpentene-2 0.336 0.366 0.311 94.559

37.820 922-62-3 3-Methyl-c-pentene-2 0.261 0.281 0.241 73.337

40.089 3404-73-7 3,3-Dimethylpentene-1 0.307 0.330 0.243 86.391

42.533 594-56-9 2,3,3-Trimethylbutene-1 0.014 0.015 0.011 3.887

46.640 3404-61-3 3-Methylhexene-1 0.016 0.017 0.013 4.507

47.236 3524-73-0 5-Methylhexene-1 0.082 0.088 0.065 22.959

49.27215840-60-5 2-Methyl-c-hexene-3 0.040 0.043 0.032 11.193

49.622 3769-23-1 4-Methylhexene-1 0.011 0.012 0.009 3.228

50.267 3404-55-5 4-Methyl-t/c-hexene-2 0.051 0.054 0.040 14.212

54.847 C7 - Iso-Olefin - 2 0.022 0.023 0.017 6.127

56.801 4914-89-0 3-Methyl-c-hexene-3 0.014 0.014 0.011 3.872

57.684 6094-02-6 2-Methylhexene-1 0.056 0.061 0.044 15.758

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C-503
Hydrocarbon Expert V4.7 Fri Aug 27 10:28:47 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91327 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91327

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Iso-Olefins 58.547 2738-19-4 2-Methyl-2-hexene 0.025 0.027 0.020 7.076

58.79210574-36-4 3-Methyl-c-hexene-2 0.019 0.021 0.015 5.472

60.07820710-38-8 3-Methyl-t-hexene-2 0.016 0.016 0.012 4.415

60.860 4914-91-4 2-Pentene, 3,4-dimethyl-, (Z)- 0.012 0.013 0.010 3.388

70.512 C8 - Diolefin - 1 0.017 0.016 0.012 4.679

80.908 C9 - IsoOlefin - 1 0.029 0.028 0.020 8.016

93.387 C10-IsoOlefin-4 0.004 0.004 0.002 1.119

Naphtheno-Olefins 22.538 1574-41-0 1,3-Cyclopentadiene 0.007 0.007 0.008 1.971

25.740 142-29-0 Cyclopentene 0.194 0.189 0.221 56.071

37.043 1120-62-3 3-Methylcyclopentene 0.100 0.099 0.095 28.141

45.833 693-89-0 1-Methylcyclopentene 0.357 0.345 0.338 102.729

51.153 110-83-8 Cyclohexene 0.044 0.041 0.042 12.426

87.884 C9 - NaphOlefin - 2 0.007 0.007 0.004 2.014

Di-Olefins 18.627 78-79-5 2-Methyl-1,3-Butadiene 0.012 0.013 0.014 3.463

21.271 2004-70-8 1t,3-Pentadiene 0.015 0.017 0.017 4.436

45.426 1528-30-9 C6-Diolefin-1 0.015 0.015 0.014 4.281

Oxygenates 13.136 64-17-5 Ethanol 22.401 21.366 37.779 2592.448

26.902 71-23-8 n-Propanol 0.074 0.069 0.095 14.507

48.059 71-36-3 n-Butanol 0.055 0.052 0.058 11.742

Unidentified 19.879 Unidentified 0.006 0.007 0.006 1.988

26.998 Unidentified 0.059 0.066 0.054 20.289

28.734 Unidentified 0.052 0.053 0.046 17.890

50.841 Unidentified 0.068 0.074 0.055 23.503

63.359 Unidentified 0.054 0.057 0.038 18.669

72.450 Unidentified 0.013 0.014 0.009 4.570

74.459 Unidentified 0.042 0.041 0.029 14.575

76.530 Unidentified 0.100 0.097 0.069 34.502

82.976 Unidentified 0.041 0.040 0.029 14.247

84.922 Unidentified 0.013 0.013 0.008 4.399

85.153 Unidentified 0.030 0.029 0.019 10.450

86.231 Unidentified 0.038 0.040 0.023 13.185

86.596 Unidentified 0.014 0.013 0.009 4.787

93.273 Unidentified 0.008 0.008 0.005 2.876

93.273 Unidentified 0.008 0.009 0.005 2.876

93.273 Unidentified 0.008 0.006 0.005 2.876

93.843 Unidentified 0.150 0.156 0.082 51.658

94.526 Unidentified 0.019 0.014 1.470 6.512

94.526 Unidentified 0.019 0.020 0.010 6.512

94.722 Unidentified 0.022 0.021 0.014 7.613

99.710 Unidentified 0.012 0.012 0.007 4.150

100.074 Unidentified 0.013 0.014 0.007 4.393

100.356 Unidentified 0.224 0.168 0.111 77.047

100.489 Unidentified 0.619 0.626 0.308 213.181

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C-504
Hydrocarbon Expert V4.7 Fri Aug 27 10:28:47 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91327 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91327

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Unidentified 101.170 Unidentified 0.370 0.397 0.205 127.269

101.292 Unidentified 0.219 0.225 0.120 75.383

101.554 Unidentified 0.050 0.051 0.027 17.139

102.197 Unidentified 0.025 0.024 0.014 8.604

102.546 Unidentified 0.130 0.131 0.064 44.638

103.200 Unidentified 0.129 0.131 0.072 44.497

103.689 Unidentified 0.019 0.016 0.012 6.517

104.955 Unidentified 0.065 0.051 0.043 22.402

106.205 Unidentified 0.011 0.011 0.006 3.946

108.084 Unidentified 0.127 0.128 0.063 43.588

108.359 Unidentified 0.129 0.131 0.065 44.289

108.438 Unidentified 0.119 0.121 0.059 41.124

108.747 Unidentified 0.306 0.310 0.152 105.438

109.171 Unidentified 0.861 0.739 0.499 296.547

109.875 Unidentified 0.041 0.035 0.024 14.031

110.712 Unidentified 0.025 0.023 0.013 8.746

111.039 Unidentified 0.139 0.141 0.077 47.762

111.311 Unidentified 0.120 0.102 0.063 41.477

111.974 Unidentified 0.066 0.056 0.034 22.649

112.827 Unidentified 0.013 0.011 0.007 4.609

112.956 Unidentified 0.017 0.014 0.010 5.759

113.476 Unidentified 0.032 0.032 0.014 10.874

113.613 Unidentified 0.010 0.011 0.005 3.612

115.145 Unidentified 0.010 0.008 0.005 3.392

130.003 Unidentified 0.003 0.002 0.002 1.064

Plus

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C-505
Hydrocarbon Expert V4.7 Fri Aug 27 10:28:47 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91327 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91327

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF

20.0 15.0 10.0 5.0 0.0

Propane

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

Ethanol

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

Unidentified

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

1,3-Cyclopentadiene

2,2-Dimethylbutane

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C-506
Hydrocarbon Expert V4.7 Fri Aug 27 10:28:47 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91327 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91327

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

n-Propanol Unidentified

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

n-Hexane

t-Hexene-3

t-Hexene-2 3-Methylcyclopentene

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane 2,3,3-Trimethylbutene-1 2,2,3-Trimethylbutane

C6-Diolefin-1Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1 Cyclohexane

n-Butanol

2-Methyl-c-hexene-3

4-Methylhexene-1

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C-507
Hydrocarbon Expert V4.7 Fri Aug 27 10:28:47 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91327 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91327

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF

70.0 65.0 60.0 55.0 50.0

4-Methyl-t/c-hexene-2

2-Methylhexane Unidentified Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane C7 - Iso-Olefin - 22,2,4-Trimethylpentane

Heptene-1

3-Methyl-c-hexene-3

t-Heptene-3

2-Methylhexene-1

n-Heptane c-Heptene-3 2-Methyl-2-hexene 3-Methyl-c-hexene-2

t-Heptene-2

Cyclopentene, 1,5-dimethyl3-Methyl-t-hexene-2

2-Pentene, 3,4-dimethyl-, (Z)-

Methylcyclohexane

1,1,3-Trimethylcyclopentane

2,2-Dimethylhexane

Unidentified

Ethylcyclopentane

2,2,3-Trimethylpentane 2,5-Dimethylhexane

2,4-Dimethylhexane

1c,2t,4-Trimethylcyclopentane

3,3-Dimethylhexane

1t,2c,3-Trimethylcyclopentane

2,3,4-Trimethylpentane

Toluene

C8 - Diolefin - 1 2,3-Dimethylhexane

2-Methylheptane 4-Methylheptane Unidentified

1,3-dimethyl-t-cyclohexane 3-Methylheptane 3-Ethylhexane

Unidentified

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C-508
Hydrocarbon Expert V4.7 Fri Aug 27 10:28:47 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91327 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91327

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF

95.0 90.0 85.0 80.0 75.0

2,2,5-Trimethylhexane

3c-Ethylmethylcyclopentane 3t-Ethylmethylcyclopentane

Unidentified

n-Octane

2,3,5-Trimethylhexane

C9 - IsoOlefin - 1

1c,2-Dimethylcyclohexane 2,4-Dimethylheptane

Ethylcyclohexane 2,6-Dimethylheptane

Unidentified

2,5-Dimethylheptane 3,5-Dimethylheptane

Ethylbenzene Unidentified

m-Xylene Unidentified p-Xylene

Unidentified 3,5-Dimethylheptane 3,3-Diethylpentane

4-Methyloctane 2-Methyloctane

C9 - NaphOlefin - 2 Heptane, 3-ethyl- 3-Methyloctane

o-Xylene

C10 - IsoParaffin - 1

Cyclopentane, 1-methyl-2-propyl- trans-1,3-Diethylcyclopentane 2,2,4-trimethylheptane

n-Nonane

1,1-Methylethylcyclohexane

i-Propylbenzene Unidentified 1-Methyl-2-propyl-cyclopentan/C10-IsoOlefin-4/C10-isoparaffin-x

Unidentified 2,2-Dimethyloctane

Unidentified

2,5-Dimethyloctane C10 - IsoParaffin - 2 2,7-Dimethyloctane 2,4-Dimethyloctane

2,6-Dimethyloctane C10 Isoparaffin -1

n-Propylbenzene 3-Methyl-5-ethylheptane

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

5-Methylnonane 4-Methylnonane 2,2,6-Trimethyloctane 1-Methyl-2-ethylbenzene

Unidentified 3-Methylnonane

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C-509
Hydrocarbon Expert V4.7 Fri Aug 27 10:28:47 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91327 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91327

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified UnidentifiedUnidentified C11-Isoparaffin-2 1,2,4-Trimethylbenzene

Unidentified Unidentified

Unidentified

Unidentified3-Ethyl-3-methylheptane Unidentified i-Butylbenzene n-Decane Unidentified

Unidentified 1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene C11 Isoparaffin-4 1-Methyl-4-i-propylbenzene

Unidentified Indan C11-Isoparaffin-5

Indene

n-ButylCyclohexane UnidentifiedC11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene 1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

Unidentified 1-Methyl-2-n-propylbenzene Unidentified C11- Isoparaffin-11 Unidentified

Unidentified 2-Methylindan

Unidentified 1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

Unidentified 2-Undecene, (E)- Unidentified

1,2-Dimethyl-3-ethylbenzene Unidentified

n-Undecane Unidentified 1-Ethyl-4-i-propylbenzene

1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene Unidentified C12 - IsoParaffin - 1

Unidentified

C11 - Aromatic - 3 5-Methylindan 1,2-Di-i-propylbenzene 1-methyl-4-(1-methylpropyl)be C11 - Aromatic - 4 4-Methylindan Benzene, 1-methyl-4-(2-methylpropyl)- 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene

1-Methyl-2-n-butylbenzene C11 - Aromatic - 7

1,4-Di-i-propylbenzene

Naphthalene

1,1-Dimethyl Indane Dimethyl Indane - 1 1t-Butyl-4-ethylbenzene

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

C11 - Aromatic - 12

2-Methylnaphthalene

1-Methylnaphthalene

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C-510
Hydrocarbon Expert V4.7 Fri Aug 27 10:28:47 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF 25-Aug-10, 08:35:09

Sample: ODDB-91327 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91327

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000009.D\SIG2000009_FID2_B.CDF

145.0 140.0 135.0 130.0 125.0

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C-511
Hydrocarbon Expert V4.7 Fri Aug 27 11:26:13 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91328 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91328

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 8.442 10.248 9.404

I-Paraffins 28.876 31.453 21.590

Aromatics 23.029 19.560 16.025

Mono-Aromatics 20.934 17.927 14.709

Naphthalenes 0.092 0.067 0.054

Naphtheno/Olefino-Benzs 0.183 0.153 0.106

Indenes 1.820 1.413 1.156

Naphthenes 3.829 3.738 3.170

Mono-Naphthenes 3.829 3.738 3.170

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 7.571 8.311 7.472

n-Olefins 3.228 3.620 3.236

Iso-Olefins 3.585 3.960 3.487

Naphtheno-Olefins 0.716 0.687 0.705

Di-Olefins 0.042 0.044 0.044

Oxygenates 23.072 21.767 38.167

Unidentified 5.181 4.922 4.172

Plus 0.000 0.000 0.000

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C-512
Hydrocarbon Expert V4.7 Fri Aug 27 11:26:13 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91328 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91328

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C2 22.944 21.648 38.018

C3 0.078 0.077 0.102

C4 4.935 6.318 6.476

C5 9.429 11.020 10.102

C6 12.051 12.985 10.847

C7 10.196 9.729 8.152

C8 16.487 16.257 11.313

C9 6.308 5.658 3.949

C10 10.732 9.825 6.046

C11 1.504 1.427 0.751

C12 0.154 0.133 0.072

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C-513
Hydrocarbon Expert V4.7 Fri Aug 27 11:26:13 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91328 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91328

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C3 0.007 0.010 0.011

C4 4.614 5.935 6.060

C5 1.445 1.718 1.529

C6 0.910 1.027 0.806

C7 0.583 0.635 0.444

C8 0.536 0.568 0.358

C9 0.228 0.237 0.136

C10 0.039 0.040 0.021

C11 0.080 0.080 0.039

I-Paraffins C4 0.066 0.088 0.086

C5 4.094 4.919 4.331

C6 6.112 6.917 5.414

C7 2.180 2.390 1.661

C8 9.730 10.289 6.502

C9 1.206 1.261 0.718

C10 4.570 4.670 2.429

C11 0.890 0.891 0.435

C12 0.029 0.029 0.013

Mono-Aromatics C6 0.772 0.654 0.755

C7 5.223 4.484 4.327

C8 5.679 4.879 4.084

C9 4.729 4.044 3.004

C10 3.964 3.389 2.254

C11 0.442 0.372 0.228

C12 0.125 0.104 0.059

Naphthalenes C10 0.076 0.055 0.045

C11 0.016 0.012 0.009

Naphtheno/Olefino-Benzs C10 0.183 0.153 0.106

Indenes C9 0.099 0.076 0.064

C10 1.702 1.322 1.083

C11 0.019 0.015 0.010

Mono-Naphthenes C5 0.175 0.175 0.190

C6 1.607 1.578 1.457

C7 1.439 1.405 1.119

C8 0.512 0.493 0.348

C9 0.045 0.040 0.027

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C-514
Hydrocarbon Expert V4.7 Fri Aug 27 11:26:13 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91328 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91328

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Mono-Naphthenes C10 0.051 0.048 0.028

n-Olefins C4 0.200 0.244 0.271

C5 1.675 1.922 1.823

C6 1.053 1.147 0.955

C7 0.099 0.105 0.077

C10 0.144 0.145 0.078

C11 0.057 0.057 0.031

Iso-Olefins C5 1.807 2.056 1.967

C6 1.087 1.175 0.986

C7 0.657 0.696 0.511

C8 0.030 0.029 0.020

C10 0.004 0.004 0.002

Naphtheno-Olefins C5 0.207 0.201 0.232

C6 0.509 0.487 0.473

Di-Olefins C5 0.026 0.029 0.030

C7 0.015 0.015 0.014

Oxygenates C2 22.944 21.648 38.018

C3 0.072 0.067 0.091

C4 0.056 0.052 0.058

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C-515
Hydrocarbon Expert V4.7 Fri Aug 27 11:26:13 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91328 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91328

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 21.55 21.29

5% 55.00 29.21

10% 87.23 80.98

15% 134.26 97.23

20% 144.68 138.35

25% 161.44 146.09

30% 172.42 172.23

35% 172.66 172.48

40% 172.89 172.73

45% 173.13 172.98

50% 176.90 173.23

55% 209.58 197.14

60% 228.87 210.20

65% 231.05 230.83

70% 251.09 236.75

75% 281.64 277.01

80% 321.45 296.60

85% 332.47 332.04

90% 352.22 349.06

95% 363.20 363.20

FBP 399.20 388.21

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C-516
Hydrocarbon Expert V4.7 Fri Aug 27 11:26:13 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91328 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91328

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 7.554 74-98-6 P3 Propane 0.007 0.010 0.011 1.701

2 8.810 75-28-5 I4 i-Butane 0.066 0.088 0.086 17.158

3 9.623 115-11-7 K4 Isobutene 0.017 0.021 0.023 4.515

4 9.665 106-98-9 K4 Butene-1 0.019 0.023 0.025 5.019

5 10.024 106-97-8 P4 n-Butane 4.614 5.935 6.060 1204.963

6 10.510 624-64-6 K4 t-Butene-2 0.075 0.093 0.103 20.396

7 10.638 463-82-1 I5 2,2-Dimethylpropane 0.015 0.019 0.016 4.020

8 11.251 590-18-1 K4 c-Butene-2 0.089 0.107 0.121 24.042

9 13.131 64-17-5 X2 Ethanol 22.944 21.648 38.018 2555.264

10 13.452 563-45-1 C5 3-Methylbutene-1 0.232 0.275 0.252 62.689

11 15.076 78-78-4 I5 i-Pentane 4.078 4.900 4.315 1072.411

12 16.727 109-67-1 K5 Pentene-1 0.340 0.395 0.370 91.909

13 17.580 563-46-2 C5 2-Methylbutene-1 0.516 0.591 0.562 139.634

14 18.113 109-66-0 P5 n-Pentane 1.445 1.718 1.529 379.903

15 18.625 78-79-5 E5 2-Methyl-1,3-Butadiene 0.011 0.012 0.012 2.953

16 19.230 646-04-8 K5 t-Pentene-2 0.862 0.991 0.939 233.275

17 19.879 ? Unidentified 0.006 0.007 0.006 1.958

18 20.266 627-20-3 K5 c-Pentene-2 0.473 0.537 0.515 127.890

19 20.943 513-35-9 C5 2-Methylbutene-2 1.059 1.190 1.153 286.406

20 21.271 2004-70-8 E5 1t,3-Pentadiene 0.016 0.017 0.018 4.394

21 22.536 1574-41-0 B5 1,3-Cyclopentadiene 0.007 0.008 0.008 1.968

22 23.092 75-83-2 I6 2,2-Dimethylbutane 0.113 0.130 0.100 29.814

23 25.743 142-29-0 B5 Cyclopentene 0.200 0.193 0.224 55.693

24 26.906 71-23-8 X3 n-Propanol 0.072 0.067 0.091 13.578

25 26.995 ? Unidentified 0.063 0.070 0.057 20.863

26 27.608 287-92-3 M5 Cyclopentane 0.175 0.175 0.190 47.269

27 28.339 79-29-8 I6 2,3-Dimethylbutane 0.972 1.094 0.861 256.713

28 28.734 ? Unidentified 0.054 0.054 0.047 17.816

29 29.192 691-38-3 C6 4-Methyl-c-pentene-2 0.046 0.051 0.042 12.573

30 29.421 107-83-5 I6 2-Methylpentane 3.123 3.560 2.766 824.449

31 29.842 674-76-0 C6 4-Methyl-t-pentene-2 0.133 0.147 0.120 35.928

32 32.069 96-14-0 I6 3-Methylpentane 1.904 2.134 1.687 502.653

33 33.228 763-29-1 C6 2-Methylpentene-1 0.227 0.247 0.206 61.460

34 33.451 592-41-6 K6 Hexene-1 0.162 0.178 0.147 43.792

35 35.640 760-21-4 C6 2-Ethylbutene-1 0.069 0.074 0.063 18.732

36 35.803 110-54-3 P6 n-Hexane 0.910 1.027 0.806 240.197

37 36.44013269-52-8 K6 t-Hexene-3 0.266 0.291 0.242 72.033

38 36.917 4050-45-7 K6 t-Hexene-2 0.409 0.446 0.371 110.534

39 37.040 1120-62-3 B6 3-Methylcyclopentene 0.101 0.099 0.094 27.386

40 37.407 625-27-4 C6 2-Methylpentene-2 0.345 0.371 0.313 93.283

41 37.820 922-62-3 C6 3-Methyl-c-pentene-2 0.267 0.284 0.242 72.114

42 38.745 7688-21-3 K6 c-Hexene-2 0.216 0.233 0.196 58.516

43 40.088 3404-73-7 C7 3,3-Dimethylpentene-1 0.313 0.332 0.244 84.790

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C-517
Hydrocarbon Expert V4.7 Fri Aug 27 11:26:13 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91328 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91328

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 40.670 96-37-7 M6 Methylcyclopentane 1.090 1.084 0.988 294.735

45 42.232 108-08-7 I7 2,4-Dimethylpentane 0.601 0.665 0.457 159.170

46 42.534 594-56-9 C7 2,3,3-Trimethylbutene-1 0.014 0.014 0.011 3.697

47 42.781 464-06-2 I7 2,2,3-Trimethylbutane 0.040 0.043 0.030 10.557

48 45.426 1528-30-9 E7 C6-Diolefin-1 0.015 0.015 0.014 4.127

49 45.640 71-42-3 Q6 Benzene 0.772 0.654 0.755 224.957

50 45.831 693-89-0 B6 1-Methylcyclopentene 0.363 0.347 0.338 100.596

51 46.640 3404-61-3 C7 3-Methylhexene-1 0.016 0.017 0.012 4.332

52 47.229 3524-73-0 C7 5-Methylhexene-1 0.042 0.045 0.033 11.398

53 47.552 110-82-7 M6 Cyclohexane 0.517 0.494 0.469 139.804

54 48.062 71-36-3 X4 n-Butanol 0.056 0.052 0.058 11.447

55 49.27315840-60-5 C7 2-Methyl-c-hexene-3 0.041 0.044 0.032 11.021

56 49.621 3769-23-1 C7 4-Methylhexene-1 0.012 0.012 0.009 3.163

57 50.266 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.051 0.054 0.040 13.783

58 50.668 591-76-4 I7 2-Methylhexane 1.029 1.129 0.784 272.854

59 50.839 ? Unidentified 0.043 0.046 0.034 14.280

60 51.153 110-83-8 B6 Cyclohexene 0.045 0.041 0.042 12.089

61 52.493 589-34-4 I7 3-Methylhexane 0.510 0.553 0.389 135.220

62 53.353 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.157 0.156 0.122 42.341

63 53.940 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.120 0.120 0.094 32.543

64 54.564 822-50-4 M7 1t,2-Dimethylcyclopentane 0.165 0.163 0.128 44.508

65 54.862 C7 C7 - Iso-Olefin - 2 0.023 0.024 0.018 6.144

66 55.178 540-84-1 I8 2,2,4-Trimethylpentane 4.298 4.625 2.872 1141.598

67 55.472 592-76-7 K7 Heptene-1 0.030 0.032 0.023 7.979

68 56.802 4914-89-0 C7 3-Methyl-c-hexene-3 0.014 0.014 0.011 3.774

69 57.33314686-14-7 K7 t-Heptene-3 0.032 0.034 0.025 8.645

70 57.684 6094-02-6 C7 2-Methylhexene-1 0.058 0.061 0.045 15.564

71 58.058 142-82-5 P7 n-Heptane 0.583 0.635 0.444 154.512

72 58.275 7642-10-6 K7 c-Heptene-3 0.025 0.026 0.019 6.714

73 58.548 2738-19-4 C7 2-Methyl-2-hexene 0.026 0.028 0.020 7.127

74 58.79310574-36-4 C7 3-Methyl-c-hexene-2 0.020 0.021 0.016 5.430

75 59.17414686-13-6 K7 t-Heptene-2 0.012 0.013 0.010 3.370

76 59.65116491-15-9 M7 Cyclopentene, 1,5-dimethyl- 0.018 0.018 0.014 4.977

77 60.07720710-38-8 C7 3-Methyl-t-hexene-2 0.015 0.015 0.012 4.029

78 60.861 4914-91-4 C7 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.014 0.010 3.566

79 61.519 108-87-2 M7 Methylcyclohexane 0.929 0.899 0.722 251.207

80 62.460 4516-69-2 M8 1,1,3-Trimethylcyclopentane 0.028 0.027 0.019 7.456

81 62.848 590-73-8 I8 2,2-Dimethylhexane 0.026 0.027 0.017 6.784

82 63.362 ? Unidentified 0.054 0.055 0.037 17.764

83 64.297 1640-89-7 M7 Ethylcyclopentane 0.051 0.049 0.039 13.665

84 64.948 564-02-3 I8 2,2,3-Trimethylpentane 0.210 0.218 0.140 55.721

85 65.174 592-13-2 I8 2,5-Dimethylhexane 0.521 0.559 0.348 138.296

86 65.511 589-43-5 I8 2,4-Dimethylhexane 0.515 0.548 0.344 136.793

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C-518
Hydrocarbon Expert V4.7 Fri Aug 27 11:26:13 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91328 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91328

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 66.347 4850-28-6 M8 1c,2t,4-Trimethylcyclopentane 0.028 0.028 0.019 7.682

88 66.741 563-16-6 I8 3,3-Dimethylhexane 0.019 0.020 0.013 5.176

89 67.86115890-40-1 M8 1t,2c,3-Trimethylcyclopentane 0.025 0.024 0.017 6.762

90 68.482 565-75-3 I8 2,3,4-Trimethylpentane 1.575 1.631 1.052 418.284

91 69.022 108-88-3 Q7 Toluene 5.223 4.484 4.327 1504.641

92 69.155 560-21-4 I8 2,3,3-Trimethylpentane 1.461 1.497 0.976 387.960

93 70.515 C8 C8 - Diolefin - 1 0.011 0.011 0.008 3.012

94 70.794 584-94-1 I8 2,3-Dimethylhexane 0.448 0.468 0.299 119.005

95 72.048 592-27-8 I8 2-Methylheptane 0.231 0.247 0.155 61.459

96 72.305 589-53-7 I8 4-Methylheptane 0.118 0.125 0.079 31.458

97 72.450 ? Unidentified 0.034 0.035 0.023 11.233

98 73.225 M8 1,3-dimethyl-t-cyclohexane 0.174 0.168 0.118 47.086

99 73.361 589-81-1 I8 3-Methylheptane 0.199 0.210 0.133 52.857

100 73.563 619-99-8 I8 3-Ethylhexane 0.108 0.113 0.072 28.780

101 74.459 ? Unidentified 0.028 0.027 0.019 9.378

102 75.250 3522-94-9 I9 2,2,5-Trimethylhexane 0.614 0.647 0.366 163.444

103 75.610 M8 3c-Ethylmethylcyclopentane 0.010 0.010 0.007 2.811

104 75.826 M8 3t-Ethylmethylcyclopentane 0.015 0.014 0.010 4.004

105 76.531 2207-03-6 M8 1t,3-Dimethylcyclohexane 0.081 0.077 0.055 21.835

106 77.871 111-65-9 P8 n-Octane 0.536 0.568 0.358 142.302

107 78.825 ? Unidentified 0.015 0.014 0.010 4.921

108 80.353 1069-53-0 I9 2,3,5-Trimethylhexane 0.091 0.094 0.054 24.323

109 80.907 C8 C9 - IsoOlefin - 1 0.019 0.018 0.013 5.122

110 81.367 2207-01-4 M8 1c,2-Dimethylcyclohexane 0.016 0.015 0.011 4.345

111 81.521 1071-26-7 I9 2,4-Dimethylheptane 0.042 0.044 0.025 11.173

112 82.175 1678-91-7 M8 Ethylcyclohexane 0.135 0.128 0.092 36.557

113 82.476 1072-05-5 I9 2,6-Dimethylheptane 0.071 0.074 0.042 18.848

114 82.976 ? Unidentified 0.029 0.028 0.020 9.515

115 83.405 I9 2,5-Dimethylheptane 0.109 0.113 0.065 28.886

116 83.599 926-82-9 I9 3,5-Dimethylheptane 0.021 0.022 0.013 5.632

117 84.731 100-41-4 Q8 Ethylbenzene 1.023 0.879 0.736 292.627

118 85.151 ? Unidentified 0.035 0.033 0.021 11.579

119 85.955 108-38-3 Q8 m-Xylene 2.607 2.245 1.874 745.305

120 86.102 106-42-3 Q8 p-Xylene 1.167 1.009 0.839 333.671

121 86.231 ? Unidentified 0.035 0.036 0.021 11.662

122 86.597 ? Unidentified 0.013 0.012 0.008 4.302

123 86.754 I9 3,5-Dimethylheptane 0.012 0.012 0.007 3.080

124 86.881 1067-20-5 I9 3,3-Diethylpentane 0.010 0.010 0.006 2.658

125 87.274 2216-34-4 I9 4-Methyloctane 0.062 0.064 0.037 16.590

126 87.406 3221-61-2 I9 2-Methyloctane 0.083 0.086 0.049 21.964

127 88.10715869-80-4 I9 Heptane, 3-ethyl- 0.011 0.012 0.007 3.059

128 88.269 2216-33-3 I9 3-Methyloctane 0.080 0.083 0.048 21.320

129 88.745 ? Unidentified 0.020 0.022 0.012 6.576

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C-519
Hydrocarbon Expert V4.7 Fri Aug 27 11:26:13 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91328 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91328

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 88.929 95-47-6 Q8 o-Xylene 0.882 0.746 0.634 252.297

131 89.321 I10 C10 - IsoParaffin - 1 0.079 0.081 0.043 21.135

132 89.910 M9 trans-1,3-Diethylcyclopentane 0.020 0.017 0.012 5.700

133 90.16814720-74-2 I10 2,2,4-trimethylheptane 0.076 0.077 0.041 20.149

134 91.741 111-84-2 P9 n-Nonane 0.228 0.237 0.136 60.760

135 92.337 4926-90-3 M9 1,1-Methylethylcyclohexane 0.022 0.020 0.013 5.903

136 93.094 98-82-8 Q9 i-Propylbenzene 0.032 0.028 0.020 9.119

137 93.272 ? Unidentified 0.009 0.008 0.005 2.922

138 93.272 ? Unidentified 0.009 0.009 0.005 2.922

139 93.272 ? Unidentified 0.009 0.007 0.005 2.922

140 93.383 696-29-7 M9 1-Methyl-2-propyl-cyclopentan 0.004 0.003 0.002 0.964

141 93.383 C10 C10-IsoOlefin-4 0.004 0.004 0.002 0.964

142 93.383 I10 C10-isoparaffin-x 0.000 0.000 0.000 0.964

143 93.842 ? Unidentified 0.145 0.149 0.078 47.973

144 94.06415869-87-1 I10 2,2-Dimethyloctane 0.054 0.055 0.029 14.377

145 94.526 ? Unidentified 0.018 0.013 1.379 5.984

146 94.526 ? Unidentified 0.018 0.019 0.010 5.984

147 94.723 ? Unidentified 0.012 0.011 0.007 3.928

148 94.86115869-89-3 I10 2,5-Dimethyloctane 0.074 0.075 0.040 19.743

149 95.325 2040-95-1 I10 2,7-Dimethyloctane 0.047 0.048 0.025 12.470

150 95.508 2051-30-1 I10 2,4-Dimethyloctane 0.220 0.225 0.118 58.706

151 95.894 I10 2,6-Dimethyloctane 0.068 0.070 0.037 18.212

152 96.058 I10 C10 Isoparaffin -1 0.006 0.006 0.003 1.626

153 96.555 103-65-1 Q9 n-Propylbenzene 0.291 0.251 0.185 82.590

154 96.753 I10 3-Methyl-5-ethylheptane 0.007 0.007 0.004 1.939

155 97.400 620-14-4 Q9 1-Methyl-3-ethylbenzene 1.011 0.871 0.642 287.357

156 97.634 622-96-8 Q9 1-Methyl-4-ethylbenzene 0.459 0.397 0.292 130.475

157 98.259 108-67-8 Q9 1,3,5-Trimethylbenzene 0.654 0.562 0.415 185.717

158 98.72115869-85-9 I10 5-Methylnonane 0.009 0.009 0.005 2.455

159 98.91317301-94-8 I10 4-Methylnonane 0.020 0.020 0.011 5.312

160 99.135 I10 2,2,6-Trimethyloctane 3.428 3.513 1.839 914.097

161 99.345 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.339 0.287 0.215 96.348

162 99.707 ? Unidentified 0.011 0.011 0.006 3.555

163 99.888 5911-04-6 I10 3-Methylnonane 0.020 0.021 0.011 5.423

164 100.073 ? Unidentified 0.011 0.012 0.006 3.778

165 100.354 ? Unidentified 0.201 0.150 0.098 66.600

166 100.487 ? Unidentified 0.542 0.542 0.265 179.602

167 100.702 I11 C11-Isoparaffin-2 0.287 0.287 0.140 76.574

168 100.978 95-63-6 Q9 1,2,4-Trimethylbenzene 1.723 1.465 1.094 489.529

169 101.168 ? Unidentified 0.328 0.348 0.179 108.674

170 101.290 ? Unidentified 0.194 0.197 0.104 64.374

171 101.552 1678-98-4 M10 i-Butylcyclohexane 0.051 0.048 0.028 13.834

172 102.194 ? Unidentified 0.020 0.019 0.011 6.790

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C-520
Hydrocarbon Expert V4.7 Fri Aug 27 11:26:13 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91328 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91328

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 102.33917302-01-1 I10 3-Ethyl-3-methylheptane 0.461 0.461 0.225 123.016

174 102.545 ? Unidentified 0.118 0.118 0.058 39.022

175 102.689 538-93-2 Q10 i-Butylbenzene 0.347 0.302 0.197 97.929

176 102.890 124-18-5 P10 n-Decane 0.039 0.040 0.021 10.415

177 103.199 K10 3-Decene 0.144 0.145 0.078 38.585

178 103.688 ? Unidentified 0.016 0.013 0.010 5.353

179 103.853 526-73-8 Q9 1,2,3-Trimethylbenzene 0.220 0.183 0.140 62.413

180 104.194 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.034 0.029 0.019 9.531

181 104.410 I11 C11 Isoparaffin-4 0.053 0.053 0.026 14.271

182 104.618 99-87-6 Q10 1-Methyl-4-i-propylbenzene 0.319 0.277 0.182 90.254

183 104.955 ? Unidentified 0.053 0.041 0.034 17.430

184 105.051 J9 Indan 0.099 0.076 0.064 28.493

185 105.264 I11 C11-Isoparaffin-5 0.023 0.023 0.011 6.189

186 105.649 J10 Indene 1.454 1.123 0.939 419.908

187 106.203 ? Unidentified 0.010 0.009 0.005 3.239

188 106.361 I11 C11-Isoparaffin-7 0.527 0.527 0.257 140.559

189 106.551 141-93-5 Q10 1,3-Diethylbenzene 0.026 0.022 0.015 7.353

190 106.845 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 1.510 1.306 0.859 426.818

191 107.104 ? Unidentified 0.330 0.285 0.188 109.282

192 107.385 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.097 0.082 0.055 27.534

193 107.619 ? Unidentified 0.086 0.073 0.049 28.581

194 108.083 ? Unidentified 0.112 0.112 0.055 37.220

195 108.236 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.042 0.035 0.024 11.738

196 108.358 ? Unidentified 0.119 0.119 0.059 39.323

197 108.437 ? Unidentified 0.109 0.109 0.053 36.190

198 108.567 ? Unidentified 0.712 0.712 0.348 235.829

199 108.746 ? Unidentified 0.277 0.277 0.135 91.656

200 109.170 ? Unidentified 0.809 0.686 0.460 267.972

201 109.396 J10 2-Methylindan 0.129 0.099 0.074 37.142

202 109.742 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.308 0.262 0.175 86.893

203 109.875 ? Unidentified 0.038 0.032 0.021 12.507

204 110.287 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.677 0.566 0.385 191.360

205 110.711 ? Unidentified 0.024 0.021 0.012 7.789

206 110.906 693-61-8 K11 2-Undecene, (E)- 0.057 0.057 0.031 15.290

207 111.039 ? Unidentified 0.130 0.130 0.071 42.983

208 111.310 ? Unidentified 0.115 0.096 0.059 38.040

209 111.410 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.068 0.057 0.039 19.159

210 111.711 1120-21-4 P11 n-Undecane 0.080 0.080 0.039 21.346

211 111.862 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.093 0.078 0.048 26.102

212 111.974 ? Unidentified 0.062 0.052 0.032 20.511

213 112.350 Q10 1,2,4,5-Tetramethylbenzene 0.230 0.193 0.131 64.991

214 112.614 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.306 0.256 0.174 86.457

215 112.824 ? Unidentified 0.013 0.011 0.007 4.221

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C-521
Hydrocarbon Expert V4.7 Fri Aug 27 11:26:13 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91328 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91328

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

216 112.956 ? Unidentified 0.016 0.014 0.009 5.448

217 113.131 I12 C12 - IsoParaffin - 1 0.024 0.024 0.011 6.451

218 113.478 ? Unidentified 0.030 0.030 0.013 9.950

219 113.612 ? Unidentified 0.011 0.011 0.005 3.506

220 113.807 Q11 C11 - Aromatic - 3 0.068 0.057 0.035 19.167

221 113.945 874-35-1 H10 5-Methylindan 0.092 0.077 0.053 25.988

222 114.070 Q12 1,2-Di-i-propylbenzene 0.040 0.033 0.019 11.173

223 114.285 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.055 0.046 0.028 15.382

224 114.453 Q11 C11 - Aromatic - 4 0.035 0.029 0.018 9.711

225 114.695 824-22-6 J10 4-Methylindan 0.119 0.100 0.069 33.675

226 114.848 5161-04-6 Q11 Benzene, 1-methyl-4-(2-methylpropyl)-0.034 0.029 0.018 9.688

227 114.942 824-63-5 H10 2-Methylindan 0.091 0.076 0.053 25.695

228 115.145 ? Unidentified 0.012 0.010 0.006 3.878

229 115.259 538-68-1 Q11 n-Pentylbenzene 0.014 0.011 0.007 3.821

230 115.487 Q11 tert-Pentylbenzene 0.054 0.045 0.028 15.200

231 115.798 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.023 0.019 0.012 6.497

232 115.909 Q11 C11 - Aromatic - 7 0.037 0.033 0.019 10.467

233 116.250 I12 C12 - IsoParaffin - 4 0.005 0.005 0.002 1.358

234 116.368 100-18-5 Q12 1,4-Di-i-propylbenzene 0.044 0.037 0.021 12.304

235 116.810 91-20-3 G10 Naphthalene 0.076 0.055 0.045 22.500

236 116.944 ? Unidentified 0.010 0.010 0.005 3.372

237 117.241 J11 1,1-Dimethyl Indane 0.019 0.015 0.010 5.459

238 117.594 7364-19-4 Q12 1t-Butyl-4-ethylbenzene 0.009 0.007 0.004 2.392

239 117.893 Q12 1,3-Di-n-propylbenzene 0.033 0.027 0.015 9.141

240 118.005 Q11 C11 - Aromatic - 11 0.018 0.016 0.009 5.002

241 118.558 Q11 C11 - Aromatic - 12 0.012 0.010 0.006 3.343

242 123.441 91-57-6 G11 2-Methylnaphthalene 0.011 0.008 0.006 3.218

243 124.306 90-12-0 G11 1-Methylnaphthalene 0.005 0.004 0.003 1.499

244 126.297 ? Unidentified 0.004 0.004 0.002 1.445

245 126.297 ? Unidentified 0.004 0.004 0.002 1.445

246 126.297 ? Unidentified 0.004 0.004 0.002 1.445

247 130.003 ? Unidentified 0.003 0.002 0.002 1.030

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C-522
Hydrocarbon Expert V4.7 Fri Aug 27 11:26:13 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91328 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91328

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 7.554 74-98-6 Propane 0.007 0.010 0.011 1.701

10.024 106-97-8 n-Butane 4.614 5.935 6.060 1204.963

18.113 109-66-0 n-Pentane 1.445 1.718 1.529 379.903

35.803 110-54-3 n-Hexane 0.910 1.027 0.806 240.197

58.058 142-82-5 n-Heptane 0.583 0.635 0.444 154.512

77.871 111-65-9 n-Octane 0.536 0.568 0.358 142.302

91.741 111-84-2 n-Nonane 0.228 0.237 0.136 60.760

102.890 124-18-5 n-Decane 0.039 0.040 0.021 10.415

111.711 1120-21-4 n-Undecane 0.080 0.080 0.039 21.346

I-Paraffins 8.810 75-28-5 i-Butane 0.066 0.088 0.086 17.158

10.638 463-82-1 2,2-Dimethylpropane 0.015 0.019 0.016 4.020

15.076 78-78-4 i-Pentane 4.078 4.900 4.315 1072.411

23.092 75-83-2 2,2-Dimethylbutane 0.113 0.130 0.100 29.814

28.339 79-29-8 2,3-Dimethylbutane 0.972 1.094 0.861 256.713

29.421 107-83-5 2-Methylpentane 3.123 3.560 2.766 824.449

32.069 96-14-0 3-Methylpentane 1.904 2.134 1.687 502.653

42.232 108-08-7 2,4-Dimethylpentane 0.601 0.665 0.457 159.170

42.781 464-06-2 2,2,3-Trimethylbutane 0.040 0.043 0.030 10.557

50.668 591-76-4 2-Methylhexane 1.029 1.129 0.784 272.854

52.493 589-34-4 3-Methylhexane 0.510 0.553 0.389 135.220

55.178 540-84-1 2,2,4-Trimethylpentane 4.298 4.625 2.872 1141.598

62.848 590-73-8 2,2-Dimethylhexane 0.026 0.027 0.017 6.784

64.948 564-02-3 2,2,3-Trimethylpentane 0.210 0.218 0.140 55.721

65.174 592-13-2 2,5-Dimethylhexane 0.521 0.559 0.348 138.296

65.511 589-43-5 2,4-Dimethylhexane 0.515 0.548 0.344 136.793

66.741 563-16-6 3,3-Dimethylhexane 0.019 0.020 0.013 5.176

68.482 565-75-3 2,3,4-Trimethylpentane 1.575 1.631 1.052 418.284

69.155 560-21-4 2,3,3-Trimethylpentane 1.461 1.497 0.976 387.960

70.794 584-94-1 2,3-Dimethylhexane 0.448 0.468 0.299 119.005

72.048 592-27-8 2-Methylheptane 0.231 0.247 0.155 61.459

72.305 589-53-7 4-Methylheptane 0.118 0.125 0.079 31.458

73.361 589-81-1 3-Methylheptane 0.199 0.210 0.133 52.857

73.563 619-99-8 3-Ethylhexane 0.108 0.113 0.072 28.780

75.250 3522-94-9 2,2,5-Trimethylhexane 0.614 0.647 0.366 163.444

80.353 1069-53-0 2,3,5-Trimethylhexane 0.091 0.094 0.054 24.323

81.521 1071-26-7 2,4-Dimethylheptane 0.042 0.044 0.025 11.173

82.476 1072-05-5 2,6-Dimethylheptane 0.071 0.074 0.042 18.848

83.405 2,5-Dimethylheptane 0.109 0.113 0.065 28.886

83.599 926-82-9 3,5-Dimethylheptane 0.021 0.022 0.013 5.632

86.754 3,5-Dimethylheptane 0.012 0.012 0.007 3.080

86.881 1067-20-5 3,3-Diethylpentane 0.010 0.010 0.006 2.658

87.274 2216-34-4 4-Methyloctane 0.062 0.064 0.037 16.590

87.406 3221-61-2 2-Methyloctane 0.083 0.086 0.049 21.964

88.10715869-80-4 Heptane, 3-ethyl- 0.011 0.012 0.007 3.059

88.269 2216-33-3 3-Methyloctane 0.080 0.083 0.048 21.320

89.321 C10 - IsoParaffin - 1 0.079 0.081 0.043 21.135

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C-523
Hydrocarbon Expert V4.7 Fri Aug 27 11:26:13 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91328 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91328

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

I-Paraffins 90.16814720-74-2 2,2,4-trimethylheptane 0.076 0.077 0.041 20.149

93.383 C10-isoparaffin-x 0.000 0.000 0.000 0.964

94.06415869-87-1 2,2-Dimethyloctane 0.054 0.055 0.029 14.377

94.86115869-89-3 2,5-Dimethyloctane 0.074 0.075 0.040 19.743

95.325 2040-95-1 2,7-Dimethyloctane 0.047 0.048 0.025 12.470

95.508 2051-30-1 2,4-Dimethyloctane 0.220 0.225 0.118 58.706

95.894 2,6-Dimethyloctane 0.068 0.070 0.037 18.212

96.058 C10 Isoparaffin -1 0.006 0.006 0.003 1.626

96.753 3-Methyl-5-ethylheptane 0.007 0.007 0.004 1.939

98.72115869-85-9 5-Methylnonane 0.009 0.009 0.005 2.455

98.91317301-94-8 4-Methylnonane 0.020 0.020 0.011 5.312

99.135 2,2,6-Trimethyloctane 3.428 3.513 1.839 914.097

99.888 5911-04-6 3-Methylnonane 0.020 0.021 0.011 5.423

100.702 C11-Isoparaffin-2 0.287 0.287 0.140 76.574

102.33917302-01-1 3-Ethyl-3-methylheptane 0.461 0.461 0.225 123.016

104.410 C11 Isoparaffin-4 0.053 0.053 0.026 14.271

105.264 C11-Isoparaffin-5 0.023 0.023 0.011 6.189

106.361 C11-Isoparaffin-7 0.527 0.527 0.257 140.559

113.131 C12 - IsoParaffin - 1 0.024 0.024 0.011 6.451

116.250 C12 - IsoParaffin - 4 0.005 0.005 0.002 1.358

Aromatics

Mono-Aromatics 45.640 71-42-3 Benzene 0.772 0.654 0.755 224.957

69.022 108-88-3 Toluene 5.223 4.484 4.327 1504.641

84.731 100-41-4 Ethylbenzene 1.023 0.879 0.736 292.627

85.955 108-38-3 m-Xylene 2.607 2.245 1.874 745.305

86.102 106-42-3 p-Xylene 1.167 1.009 0.839 333.671

88.929 95-47-6 o-Xylene 0.882 0.746 0.634 252.297

93.094 98-82-8 i-Propylbenzene 0.032 0.028 0.020 9.119

96.555 103-65-1 n-Propylbenzene 0.291 0.251 0.185 82.590

97.400 620-14-4 1-Methyl-3-ethylbenzene 1.011 0.871 0.642 287.357

97.634 622-96-8 1-Methyl-4-ethylbenzene 0.459 0.397 0.292 130.475

98.259 108-67-8 1,3,5-Trimethylbenzene 0.654 0.562 0.415 185.717

99.345 611-14-3 1-Methyl-2-ethylbenzene 0.339 0.287 0.215 96.348

100.978 95-63-6 1,2,4-Trimethylbenzene 1.723 1.465 1.094 489.529

102.689 538-93-2 i-Butylbenzene 0.347 0.302 0.197 97.929

103.853 526-73-8 1,2,3-Trimethylbenzene 0.220 0.183 0.140 62.413

104.194 535-77-3 1-Methyl-3-i-propylbenzene 0.034 0.029 0.019 9.531

104.618 99-87-6 1-Methyl-4-i-propylbenzene 0.319 0.277 0.182 90.254

106.551 141-93-5 1,3-Diethylbenzene 0.026 0.022 0.015 7.353

106.845 1074-43-7 1-Methyl-3-n-propylbenzene 1.510 1.306 0.859 426.818

107.385 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.097 0.082 0.055 27.534

108.236 1074-17-5 1-Methyl-2-n-propylbenzene 0.042 0.035 0.024 11.738

109.742 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.308 0.262 0.175 86.893

110.287 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.677 0.566 0.385 191.360

111.410 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.068 0.057 0.039 19.159

111.862 4218-48-8 1-Ethyl-4-i-propylbenzene 0.093 0.078 0.048 26.102

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C-524
Hydrocarbon Expert V4.7 Fri Aug 27 11:26:13 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91328 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91328

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 112.350 1,2,4,5-Tetramethylbenzene 0.230 0.193 0.131 64.991

112.614 527-53-7 1,2,3,5-Tetramethylbenzene 0.306 0.256 0.174 86.457

113.807 C11 - Aromatic - 3 0.068 0.057 0.035 19.167

114.070 1,2-Di-i-propylbenzene 0.040 0.033 0.019 11.173

114.285 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.055 0.046 0.028 15.382

114.453 C11 - Aromatic - 4 0.035 0.029 0.018 9.711

114.848 5161-04-6 Benzene, 1-methyl-4-(2-methylpropyl)-0.034 0.029 0.018 9.688

115.259 538-68-1 n-Pentylbenzene 0.014 0.011 0.007 3.821

115.487 tert-Pentylbenzene 0.054 0.045 0.028 15.200

115.798 577-55-9 1-Methyl-2-n-butylbenzene 0.023 0.019 0.012 6.497

115.909 C11 - Aromatic - 7 0.037 0.033 0.019 10.467

116.368 100-18-5 1,4-Di-i-propylbenzene 0.044 0.037 0.021 12.304

117.594 7364-19-4 1t-Butyl-4-ethylbenzene 0.009 0.007 0.004 2.392

117.893 1,3-Di-n-propylbenzene 0.033 0.027 0.015 9.141

118.005 C11 - Aromatic - 11 0.018 0.016 0.009 5.002

118.558 C11 - Aromatic - 12 0.012 0.010 0.006 3.343

Naphthalenes 116.810 91-20-3 Naphthalene 0.076 0.055 0.045 22.500

123.441 91-57-6 2-Methylnaphthalene 0.011 0.008 0.006 3.218

124.306 90-12-0 1-Methylnaphthalene 0.005 0.004 0.003 1.499

Naphtheno/Olefino-Benzs 113.945 874-35-1 5-Methylindan 0.092 0.077 0.053 25.988

114.942 824-63-5 2-Methylindan 0.091 0.076 0.053 25.695

Indenes 105.051 Indan 0.099 0.076 0.064 28.493

105.649 Indene 1.454 1.123 0.939 419.908

109.396 2-Methylindan 0.129 0.099 0.074 37.142

114.695 824-22-6 4-Methylindan 0.119 0.100 0.069 33.675

117.241 1,1-Dimethyl Indane 0.019 0.015 0.010 5.459

Naphthenes

Mono-Naphthenes 27.608 287-92-3 Cyclopentane 0.175 0.175 0.190 47.269

40.670 96-37-7 Methylcyclopentane 1.090 1.084 0.988 294.735

47.552 110-82-7 Cyclohexane 0.517 0.494 0.469 139.804

53.353 1759-58-6 1t,3-Dimethylcyclopentane 0.157 0.156 0.122 42.341

53.940 2532-58-3 1c,3-Dimethylcyclopentane 0.120 0.120 0.094 32.543

54.564 822-50-4 1t,2-Dimethylcyclopentane 0.165 0.163 0.128 44.508

59.65116491-15-9 Cyclopentene, 1,5-dimethyl- 0.018 0.018 0.014 4.977

61.519 108-87-2 Methylcyclohexane 0.929 0.899 0.722 251.207

62.460 4516-69-2 1,1,3-Trimethylcyclopentane 0.028 0.027 0.019 7.456

64.297 1640-89-7 Ethylcyclopentane 0.051 0.049 0.039 13.665

66.347 4850-28-6 1c,2t,4-Trimethylcyclopentane 0.028 0.028 0.019 7.682

67.86115890-40-1 1t,2c,3-Trimethylcyclopentane 0.025 0.024 0.017 6.762

73.225 1,3-dimethyl-t-cyclohexane 0.174 0.168 0.118 47.086

75.610 3c-Ethylmethylcyclopentane 0.010 0.010 0.007 2.811

75.826 3t-Ethylmethylcyclopentane 0.015 0.014 0.010 4.004

76.531 2207-03-6 1t,3-Dimethylcyclohexane 0.081 0.077 0.055 21.835

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C-525
Hydrocarbon Expert V4.7 Fri Aug 27 11:26:13 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91328 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91328

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Naphthenes 81.367 2207-01-4 1c,2-Dimethylcyclohexane 0.016 0.015 0.011 4.345

82.175 1678-91-7 Ethylcyclohexane 0.135 0.128 0.092 36.557

89.910 trans-1,3-Diethylcyclopentane 0.020 0.017 0.012 5.700

92.337 4926-90-3 1,1-Methylethylcyclohexane 0.022 0.020 0.013 5.903

93.383 696-29-7 1-Methyl-2-propyl-cyclopentan 0.004 0.003 0.002 0.964

101.552 1678-98-4 i-Butylcyclohexane 0.051 0.048 0.028 13.834

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.623 115-11-7 Isobutene 0.017 0.021 0.023 4.515

9.665 106-98-9 Butene-1 0.019 0.023 0.025 5.019

10.510 624-64-6 t-Butene-2 0.075 0.093 0.103 20.396

11.251 590-18-1 c-Butene-2 0.089 0.107 0.121 24.042

16.727 109-67-1 Pentene-1 0.340 0.395 0.370 91.909

19.230 646-04-8 t-Pentene-2 0.862 0.991 0.939 233.275

20.266 627-20-3 c-Pentene-2 0.473 0.537 0.515 127.890

33.451 592-41-6 Hexene-1 0.162 0.178 0.147 43.792

36.44013269-52-8 t-Hexene-3 0.266 0.291 0.242 72.033

36.917 4050-45-7 t-Hexene-2 0.409 0.446 0.371 110.534

38.745 7688-21-3 c-Hexene-2 0.216 0.233 0.196 58.516

55.472 592-76-7 Heptene-1 0.030 0.032 0.023 7.979

57.33314686-14-7 t-Heptene-3 0.032 0.034 0.025 8.645

58.275 7642-10-6 c-Heptene-3 0.025 0.026 0.019 6.714

59.17414686-13-6 t-Heptene-2 0.012 0.013 0.010 3.370

103.199 3-Decene 0.144 0.145 0.078 38.585

110.906 693-61-8 2-Undecene, (E)- 0.057 0.057 0.031 15.290

Iso-Olefins 13.452 563-45-1 3-Methylbutene-1 0.232 0.275 0.252 62.689

17.580 563-46-2 2-Methylbutene-1 0.516 0.591 0.562 139.634

20.943 513-35-9 2-Methylbutene-2 1.059 1.190 1.153 286.406

29.192 691-38-3 4-Methyl-c-pentene-2 0.046 0.051 0.042 12.573

29.842 674-76-0 4-Methyl-t-pentene-2 0.133 0.147 0.120 35.928

33.228 763-29-1 2-Methylpentene-1 0.227 0.247 0.206 61.460

35.640 760-21-4 2-Ethylbutene-1 0.069 0.074 0.063 18.732

37.407 625-27-4 2-Methylpentene-2 0.345 0.371 0.313 93.283

37.820 922-62-3 3-Methyl-c-pentene-2 0.267 0.284 0.242 72.114

40.088 3404-73-7 3,3-Dimethylpentene-1 0.313 0.332 0.244 84.790

42.534 594-56-9 2,3,3-Trimethylbutene-1 0.014 0.014 0.011 3.697

46.640 3404-61-3 3-Methylhexene-1 0.016 0.017 0.012 4.332

47.229 3524-73-0 5-Methylhexene-1 0.042 0.045 0.033 11.398

49.27315840-60-5 2-Methyl-c-hexene-3 0.041 0.044 0.032 11.021

49.621 3769-23-1 4-Methylhexene-1 0.012 0.012 0.009 3.163

50.266 3404-55-5 4-Methyl-t/c-hexene-2 0.051 0.054 0.040 13.783

54.862 C7 - Iso-Olefin - 2 0.023 0.024 0.018 6.144

56.802 4914-89-0 3-Methyl-c-hexene-3 0.014 0.014 0.011 3.774

57.684 6094-02-6 2-Methylhexene-1 0.058 0.061 0.045 15.564

58.548 2738-19-4 2-Methyl-2-hexene 0.026 0.028 0.020 7.127

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C-526
Hydrocarbon Expert V4.7 Fri Aug 27 11:26:13 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91328 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91328

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Iso-Olefins 58.79310574-36-4 3-Methyl-c-hexene-2 0.020 0.021 0.016 5.430

60.07720710-38-8 3-Methyl-t-hexene-2 0.015 0.015 0.012 4.029

60.861 4914-91-4 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.014 0.010 3.566

70.515 C8 - Diolefin - 1 0.011 0.011 0.008 3.012

80.907 C9 - IsoOlefin - 1 0.019 0.018 0.013 5.122

93.383 C10-IsoOlefin-4 0.004 0.004 0.002 0.964

Naphtheno-Olefins 22.536 1574-41-0 1,3-Cyclopentadiene 0.007 0.008 0.008 1.968

25.743 142-29-0 Cyclopentene 0.200 0.193 0.224 55.693

37.040 1120-62-3 3-Methylcyclopentene 0.101 0.099 0.094 27.386

45.831 693-89-0 1-Methylcyclopentene 0.363 0.347 0.338 100.596

51.153 110-83-8 Cyclohexene 0.045 0.041 0.042 12.089

Di-Olefins 18.625 78-79-5 2-Methyl-1,3-Butadiene 0.011 0.012 0.012 2.953

21.271 2004-70-8 1t,3-Pentadiene 0.016 0.017 0.018 4.394

45.426 1528-30-9 C6-Diolefin-1 0.015 0.015 0.014 4.127

Oxygenates 13.131 64-17-5 Ethanol 22.944 21.648 38.018 2555.264

26.906 71-23-8 n-Propanol 0.072 0.067 0.091 13.578

48.062 71-36-3 n-Butanol 0.056 0.052 0.058 11.447

Unidentified 19.879 Unidentified 0.006 0.007 0.006 1.958

26.995 Unidentified 0.063 0.070 0.057 20.863

28.734 Unidentified 0.054 0.054 0.047 17.816

50.839 Unidentified 0.043 0.046 0.034 14.280

63.362 Unidentified 0.054 0.055 0.037 17.764

72.450 Unidentified 0.034 0.035 0.023 11.233

74.459 Unidentified 0.028 0.027 0.019 9.378

78.825 Unidentified 0.015 0.014 0.010 4.921

82.976 Unidentified 0.029 0.028 0.020 9.515

85.151 Unidentified 0.035 0.033 0.021 11.579

86.231 Unidentified 0.035 0.036 0.021 11.662

86.597 Unidentified 0.013 0.012 0.008 4.302

88.745 Unidentified 0.020 0.022 0.012 6.576

93.272 Unidentified 0.009 0.008 0.005 2.922

93.272 Unidentified 0.009 0.009 0.005 2.922

93.272 Unidentified 0.009 0.007 0.005 2.922

93.842 Unidentified 0.145 0.149 0.078 47.973

94.526 Unidentified 0.018 0.013 1.379 5.984

94.526 Unidentified 0.018 0.019 0.010 5.984

94.723 Unidentified 0.012 0.011 0.007 3.928

99.707 Unidentified 0.011 0.011 0.006 3.555

100.073 Unidentified 0.011 0.012 0.006 3.778

100.354 Unidentified 0.201 0.150 0.098 66.600

100.487 Unidentified 0.542 0.542 0.265 179.602

101.168 Unidentified 0.328 0.348 0.179 108.674

101.290 Unidentified 0.194 0.197 0.104 64.374

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C-527
Hydrocarbon Expert V4.7 Fri Aug 27 11:26:13 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91328 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91328

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Unidentified 102.194 Unidentified 0.020 0.019 0.011 6.790

102.545 Unidentified 0.118 0.118 0.058 39.022

103.688 Unidentified 0.016 0.013 0.010 5.353

104.955 Unidentified 0.053 0.041 0.034 17.430

106.203 Unidentified 0.010 0.009 0.005 3.239

107.104 Unidentified 0.330 0.285 0.188 109.282

107.619 Unidentified 0.086 0.073 0.049 28.581

108.083 Unidentified 0.112 0.112 0.055 37.220

108.358 Unidentified 0.119 0.119 0.059 39.323

108.437 Unidentified 0.109 0.109 0.053 36.190

108.567 Unidentified 0.712 0.712 0.348 235.829

108.746 Unidentified 0.277 0.277 0.135 91.656

109.170 Unidentified 0.809 0.686 0.460 267.972

109.875 Unidentified 0.038 0.032 0.021 12.507

110.711 Unidentified 0.024 0.021 0.012 7.789

111.039 Unidentified 0.130 0.130 0.071 42.983

111.310 Unidentified 0.115 0.096 0.059 38.040

111.974 Unidentified 0.062 0.052 0.032 20.511

112.824 Unidentified 0.013 0.011 0.007 4.221

112.956 Unidentified 0.016 0.014 0.009 5.448

113.478 Unidentified 0.030 0.030 0.013 9.950

113.612 Unidentified 0.011 0.011 0.005 3.506

115.145 Unidentified 0.012 0.010 0.006 3.878

116.944 Unidentified 0.010 0.010 0.005 3.372

126.297 Unidentified 0.004 0.004 0.002 1.445

126.297 Unidentified 0.004 0.004 0.002 1.445

126.297 Unidentified 0.004 0.004 0.002 1.445

130.003 Unidentified 0.003 0.002 0.002 1.030

Plus

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C-528
Hydrocarbon Expert V4.7 Fri Aug 27 11:26:13 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91328 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91328

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF

20.0 15.0 10.0 5.0 0.0

Propane

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

Ethanol

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

Unidentified

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

1,3-Cyclopentadiene

2,2-Dimethylbutane

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C-529
Hydrocarbon Expert V4.7 Fri Aug 27 11:26:13 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91328 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91328

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

n-Propanol Unidentified

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

2-Ethylbutene-1 n-Hexane

t-Hexene-3

t-Hexene-2 3-Methylcyclopentene

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane 2,3,3-Trimethylbutene-1 2,2,3-Trimethylbutane

C6-Diolefin-1 Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1

Cyclohexane

n-Butanol

2-Methyl-c-hexene-3

4-Methylhexene-1

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C-530
Hydrocarbon Expert V4.7 Fri Aug 27 11:26:13 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91328 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91328

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF

70.0 65.0 60.0 55.0 50.0

4-Methyl-t/c-hexene-2

2-Methylhexane Unidentified Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane C7 - Iso-Olefin - 2

2,2,4-Trimethylpentane Heptene-1

3-Methyl-c-hexene-3

t-Heptene-3

2-Methylhexene-1

n-Heptane c-Heptene-3 2-Methyl-2-hexene 3-Methyl-c-hexene-2

t-Heptene-2

Cyclopentene, 1,5-dimethyl3-Methyl-t-hexene-2

2-Pentene, 3,4-dimethyl-, (Z)-

Methylcyclohexane

1,1,3-Trimethylcyclopentane

2,2-Dimethylhexane

Unidentified

Ethylcyclopentane

2,2,3-Trimethylpentane 2,5-Dimethylhexane

2,4-Dimethylhexane

1c,2t,4-Trimethylcyclopentane

3,3-Dimethylhexane

1t,2c,3-Trimethylcyclopentane

2,3,4-Trimethylpentane

Toluene 2,3,3-Trimethylpentane

C8 - Diolefin - 1 2,3-Dimethylhexane

2-Methylheptane

Unidentified 4-Methylheptane

1,3-dimethyl-t-cyclohexane 3-Methylheptane 3-Ethylhexane

Unidentified

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C-531
Hydrocarbon Expert V4.7 Fri Aug 27 11:26:13 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91328 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91328

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF

95.0 90.0 85.0 80.0 75.0

2,2,5-Trimethylhexane

3c-Ethylmethylcyclopentane 3t-Ethylmethylcyclopentane

1t,3-Dimethylcyclohexane

n-Octane

Unidentified

2,3,5-Trimethylhexane

C9 - IsoOlefin - 1

1c,2-Dimethylcyclohexane 2,4-Dimethylheptane

Ethylcyclohexane 2,6-Dimethylheptane

Unidentified

2,5-Dimethylheptane 3,5-Dimethylheptane

Ethylbenzene

Unidentified

m-Xylene Unidentified p-Xylene

Unidentified 3,5-Dimethylheptane 3,3-Diethylpentane

4-Methyloctane 2-Methyloctane

Heptane, 3-ethyl- 3-Methyloctane

Unidentifiedo-Xylene

C10 - IsoParaffin - 1

trans-1,3-Diethylcyclopentane 2,2,4-trimethylheptane

n-Nonane

1,1-Methylethylcyclohexane

i-Propylbenzene Unidentified 1-Methyl-2-propyl-cyclopentan/C10-IsoOlefin-4/C10-isoparaffin-x

Unidentified 2,2-Dimethyloctane

Unidentified

2,5-Dimethyloctane

2,7-Dimethyloctane 2,4-Dimethyloctane

2,6-Dimethyloctane C10 Isoparaffin -1

n-Propylbenzene 3-Methyl-5-ethylheptane

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

5-Methylnonane 4-Methylnonane 2,2,6-Trimethyloctane 1-Methyl-2-ethylbenzene

Unidentified 3-Methylnonane

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C-532
Hydrocarbon Expert V4.7 Fri Aug 27 11:26:13 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91328 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91328

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified Unidentified Unidentified C11-Isoparaffin-2 1,2,4-Trimethylbenzene Unidentified Unidentified

i-Butylcyclohexane

Unidentified 3-Ethyl-3-methylheptane Unidentified i-Butylbenzene n-Decane 3-Decene

Unidentified 1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene C11 Isoparaffin-4 1-Methyl-4-i-propylbenzene

Unidentified Indan C11-Isoparaffin-5

Indene

Unidentified C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene Unidentified 1,3-Dimethyl-5-ethylbenzene Unidentified

Unidentified 1-Methyl-2-n-propylbenzene UnidentifiedUnidentified Unidentified

Unidentified 2-Methylindan

Unidentified 1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

Unidentified 2-Undecene, (E)- Unidentified

1,2-Dimethyl-3-ethylbenzene n-Undecane Unidentified 1-Ethyl-4-i-propylbenzene

1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene Unidentified C12 - IsoParaffin - 1

Unidentified

C11 - Aromatic - 3 5-Methylindan 1,2-Di-i-propylbenzene 1-methyl-4-(1-methylpropyl)be C11 - Aromatic - 4 4-Methylindan Benzene, 1-methyl-4-(2-methylpropyl)- 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene 1-Methyl-2-n-butylbenzene C11 - Aromatic - 7

C12 - IsoParaffin - 4 1,4-Di-i-propylbenzene

Unidentified Naphthalene

1,1-Dimethyl Indane

1t-Butyl-4-ethylbenzene

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

C11 - Aromatic - 12

2-Methylnaphthalene

1-Methylnaphthalene

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C-533
Hydrocarbon Expert V4.7 Fri Aug 27 11:26:13 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF 25-Aug-10, 11:02:54

Sample: ODDB-91328 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91328

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000010.D\SIG2000010_FID2_B.CDF

145.0 140.0 135.0 130.0 125.0

Unidentified

Unidentified

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C-534
Hydrocarbon Expert V4.7 Fri Aug 27 13:42:53 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91329 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91329

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 7.734 9.847 9.087

I-Paraffins 15.447 18.031 13.525

Aromatics 42.903 37.798 30.294

Mono-Aromatics 40.715 36.014 28.953

Naphthalenes 0.247 0.186 0.147

Naphtheno/Olefino-Benzs 0.452 0.391 0.263

Indenes 1.488 1.207 0.930

Naphthenes 2.071 2.109 1.891

Mono-Naphthenes 2.071 2.109 1.891

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 7.117 8.087 7.143

n-Olefins 2.978 3.467 3.071

Iso-Olefins 3.403 3.886 3.339

Naphtheno-Olefins 0.696 0.690 0.690

Di-Olefins 0.040 0.044 0.043

Oxygenates 21.900 21.350 36.487

Unidentified 2.828 2.779 1.573

Plus 0.000 0.000 0.000

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C-535
Hydrocarbon Expert V4.7 Fri Aug 27 13:42:53 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91329 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91329

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C2 21.767 21.222 36.330

C3 0.079 0.077 0.102

C4 5.147 6.809 6.803

C5 7.109 8.510 7.701

C6 16.997 19.240 15.334

C7 13.609 12.576 11.220

C8 11.480 10.212 8.311

C9 10.903 9.604 6.977

C10 7.580 6.595 4.398

C11 2.142 2.065 1.082

C12 0.358 0.312 0.170

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C-536
Hydrocarbon Expert V4.7 Fri Aug 27 13:42:53 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91329 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91329

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C3 0.001 0.001 0.001

C4 4.881 6.487 6.457

C5 0.812 0.997 0.865

C6 1.796 2.095 1.603

C7 0.126 0.142 0.097

C8 0.023 0.025 0.015

C9 0.013 0.014 0.008

C11 0.083 0.085 0.041

I-Paraffins C4 0.021 0.030 0.028

C5 2.497 3.100 2.661

C6 10.368 12.139 9.251

C7 1.132 1.280 0.869

C8 0.047 0.052 0.032

C10 0.258 0.269 0.133

C11 1.099 1.136 0.541

C12 0.025 0.026 0.011

Mono-Aromatics C6 0.762 0.667 0.750

C7 11.289 10.016 9.421

C8 11.410 10.136 8.264

C9 10.632 9.384 6.802

C10 5.464 4.802 3.130

C11 0.846 0.739 0.439

C12 0.312 0.270 0.148

Naphthalenes C10 0.233 0.175 0.140

C11 0.014 0.011 0.008

Naphtheno/Olefino-Benzs C10 0.452 0.391 0.263

Indenes C9 0.258 0.206 0.168

C10 1.162 0.947 0.726

C11 0.048 0.038 0.025

C12 0.020 0.016 0.011

Mono-Naphthenes C5 0.244 0.251 0.267

C6 1.503 1.527 1.373

C7 0.313 0.320 0.245

C10 0.011 0.011 0.006

n-Olefins C4 0.190 0.240 0.261

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C-537
Hydrocarbon Expert V4.7 Fri Aug 27 13:42:53 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91329 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91329

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

n-Olefins C5 1.615 1.916 1.771

C6 1.023 1.151 0.935

C7 0.096 0.105 0.075

C11 0.053 0.055 0.029

Iso-Olefins C5 1.716 2.017 1.881

C6 1.049 1.171 0.958

C7 0.638 0.698 0.500

Naphtheno-Olefins C5 0.200 0.200 0.226

C6 0.496 0.490 0.464

Di-Olefins C5 0.026 0.029 0.029

C7 0.015 0.015 0.014

Oxygenates C2 21.767 21.222 36.330

C3 0.078 0.075 0.100

C4 0.055 0.052 0.057

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C-538
Hydrocarbon Expert V4.7 Fri Aug 27 13:42:53 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91329 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91329

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 21.61 21.35

5% 33.33 28.59

10% 97.17 81.80

15% 138.01 111.42

20% 140.53 138.65

25% 154.40 143.99

30% 172.29 154.33

35% 172.54 172.27

40% 172.79 172.53

45% 173.04 172.78

50% 173.28 173.03

55% 221.36 173.29

60% 226.27 221.51

65% 253.49 227.05

70% 281.21 270.68

75% 282.37 281.68

80% 323.14 321.06

85% 335.32 334.04

90% 358.22 352.22

95% 370.41 368.42

FBP 404.60 404.60

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C-539
Hydrocarbon Expert V4.7 Fri Aug 27 13:42:53 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91329 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91329

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 7.554 74-98-6 P3 Propane 0.001 0.001 0.001 0.187

2 8.810 75-28-5 I4 i-Butane 0.021 0.030 0.028 5.549

3 9.623 115-11-7 K4 Isobutene 0.016 0.020 0.022 4.228

4 9.664 106-98-9 K4 Butene-1 0.018 0.023 0.024 4.729

5 10.024 106-97-8 P4 n-Butane 4.881 6.487 6.457 1264.928

6 10.510 624-64-6 K4 t-Butene-2 0.072 0.092 0.099 19.355

7 10.637 463-82-1 I5 2,2-Dimethylpropane 0.006 0.008 0.007 1.616

8 11.250 590-18-1 K4 c-Butene-2 0.085 0.105 0.116 22.797

9 13.124 64-17-5 X2 Ethanol 21.767 21.222 36.330 2405.814

10 13.454 563-45-1 C5 3-Methylbutene-1 0.197 0.242 0.216 52.954

11 15.073 78-78-4 I5 i-Pentane 2.491 3.092 2.654 649.939

12 16.730 109-67-1 K5 Pentene-1 0.328 0.393 0.359 87.931

13 17.577 563-46-2 C5 2-Methylbutene-1 0.497 0.588 0.545 133.516

14 18.111 109-66-0 P5 n-Pentane 0.812 0.997 0.865 211.846

15 18.628 78-79-5 E5 2-Methyl-1,3-Butadiene 0.010 0.012 0.012 2.816

16 19.232 646-04-8 K5 t-Pentene-2 0.832 0.987 0.912 223.252

17 19.882 ? Unidentified 0.006 0.007 0.006 1.907

18 20.263 627-20-3 K5 c-Pentene-2 0.456 0.535 0.500 122.419

19 20.940 513-35-9 C5 2-Methylbutene-2 1.021 1.186 1.120 274.156

20 21.269 2004-70-8 E5 1t,3-Pentadiene 0.015 0.018 0.017 4.261

21 22.534 1574-41-0 B5 1,3-Cyclopentadiene 0.007 0.008 0.008 1.879

22 23.089 75-83-2 I6 2,2-Dimethylbutane 0.264 0.313 0.235 69.147

23 25.739 142-29-0 B5 Cyclopentene 0.194 0.193 0.219 53.497

24 26.906 71-23-8 X3 n-Propanol 0.078 0.075 0.100 14.745

25 26.991 ? Unidentified 0.056 0.064 0.051 18.364

26 27.604 287-92-3 M5 Cyclopentane 0.244 0.251 0.267 65.362

27 28.334 79-29-8 I6 2,3-Dimethylbutane 1.068 1.242 0.953 279.771

28 28.733 ? Unidentified 0.052 0.054 0.045 17.036

29 29.194 691-38-3 C6 4-Methyl-c-pentene-2 0.044 0.051 0.041 11.916

30 29.438 107-83-5 I6 2-Methylpentane 6.069 7.148 5.415 1589.994

31 29.843 674-76-0 C6 4-Methyl-t-pentene-2 0.128 0.147 0.117 34.450

32 32.074 96-14-0 I6 3-Methylpentane 2.968 3.437 2.648 777.561

33 33.233 763-29-1 C6 2-Methylpentene-1 0.220 0.247 0.201 59.096

34 33.450 592-41-6 K6 Hexene-1 0.157 0.178 0.144 42.227

35 35.642 760-21-4 C6 2-Ethylbutene-1 0.062 0.069 0.057 16.747

36 35.806 110-54-3 P6 n-Hexane 1.796 2.095 1.603 470.606

37 36.43913269-52-8 K6 t-Hexene-3 0.258 0.291 0.236 69.365

38 36.916 4050-45-7 K6 t-Hexene-2 0.397 0.447 0.363 106.583

39 37.042 1120-62-3 B6 3-Methylcyclopentene 0.098 0.099 0.092 26.242

40 37.406 625-27-4 C6 2-Methylpentene-2 0.335 0.373 0.306 89.849

41 37.820 922-62-3 C6 3-Methyl-c-pentene-2 0.259 0.285 0.236 69.441

42 38.742 7688-21-3 K6 c-Hexene-2 0.210 0.234 0.192 56.392

43 40.086 3404-73-7 C7 3,3-Dimethylpentene-1 0.306 0.336 0.240 82.196

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C-540
Hydrocarbon Expert V4.7 Fri Aug 27 13:42:53 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91329 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91329

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 40.671 96-37-7 M6 Methylcyclopentane 1.055 1.085 0.964 283.306

45 42.239 108-08-7 I7 2,4-Dimethylpentane 0.209 0.239 0.160 54.905

46 42.532 594-56-9 C7 2,3,3-Trimethylbutene-1 0.013 0.014 0.010 3.544

47 42.778 464-06-2 I7 2,2,3-Trimethylbutane 0.019 0.021 0.015 4.979

48 45.429 1528-30-9 E7 C6-Diolefin-1 0.015 0.015 0.014 3.975

49 45.637 71-42-3 Q6 Benzene 0.762 0.667 0.750 220.346

50 45.833 693-89-0 B6 1-Methylcyclopentene 0.354 0.349 0.331 97.257

51 46.637 3404-61-3 C7 3-Methylhexene-1 0.016 0.017 0.012 4.167

52 47.230 3524-73-0 C7 5-Methylhexene-1 0.038 0.042 0.030 10.241

53 47.552 110-82-7 M6 Cyclohexane 0.448 0.442 0.409 120.162

54 48.062 71-36-3 X4 n-Butanol 0.055 0.052 0.057 11.090

55 49.27215840-60-5 C7 2-Methyl-c-hexene-3 0.040 0.044 0.031 10.677

56 49.619 3769-23-1 C7 4-Methylhexene-1 0.011 0.012 0.008 2.867

57 50.266 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.050 0.055 0.039 13.442

58 50.661 591-76-4 I7 2-Methylhexane 0.552 0.626 0.423 145.154

59 50.840 ? Unidentified 0.024 0.027 0.019 7.980

60 51.152 110-83-8 B6 Cyclohexene 0.044 0.042 0.041 11.800

61 52.491 589-34-4 I7 3-Methylhexane 0.352 0.395 0.270 92.708

62 53.352 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.100 0.103 0.078 26.826

63 53.938 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.068 0.070 0.053 18.197

64 54.563 822-50-4 M7 1t,2-Dimethylcyclopentane 0.069 0.070 0.054 18.403

65 54.842 C7 C7 - Iso-Olefin - 2 0.022 0.023 0.017 5.868

66 55.468 592-76-7 K7 Heptene-1 0.027 0.030 0.021 7.291

67 56.801 4914-89-0 C7 3-Methyl-c-hexene-3 0.014 0.015 0.011 3.660

68 57.33214686-14-7 K7 t-Heptene-3 0.031 0.034 0.025 8.413

69 57.683 6094-02-6 C7 2-Methylhexene-1 0.056 0.062 0.044 15.137

70 58.053 142-82-5 P7 n-Heptane 0.126 0.142 0.097 33.207

71 58.274 7642-10-6 K7 c-Heptene-3 0.025 0.027 0.019 6.665

72 58.548 2738-19-4 C7 2-Methyl-2-hexene 0.026 0.028 0.020 6.845

73 58.79310574-36-4 C7 3-Methyl-c-hexene-2 0.019 0.021 0.015 5.209

74 59.17414686-13-6 K7 t-Heptene-2 0.013 0.014 0.010 3.395

75 59.65016491-15-9 M7 Cyclopentene, 1,5-dimethyl- 0.018 0.019 0.014 4.888

76 60.07720710-38-8 C7 3-Methyl-t-hexene-2 0.015 0.016 0.012 3.985

77 60.859 4914-91-4 C7 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.014 0.010 3.431

78 61.507 108-87-2 M7 Methylcyclohexane 0.058 0.058 0.046 15.648

79 63.361 ? Unidentified 0.057 0.061 0.040 18.873

80 69.069 108-88-3 Q7 Toluene 11.289 10.016 9.421 3227.774

81 72.046 592-27-8 I8 2-Methylheptane 0.019 0.020 0.012 4.877

82 72.299 589-53-7 I8 4-Methylheptane 0.010 0.011 0.007 2.552

83 73.361 589-81-1 I8 3-Methylheptane 0.019 0.021 0.013 5.011

84 77.869 111-65-9 P8 n-Octane 0.023 0.025 0.015 6.005

85 84.742 100-41-4 Q8 Ethylbenzene 2.126 1.886 1.540 603.262

86 85.983 108-38-3 Q8 m-Xylene 5.424 4.828 3.928 1539.029

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C-541
Hydrocarbon Expert V4.7 Fri Aug 27 13:42:53 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91329 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91329

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 86.124 106-42-3 Q8 p-Xylene 2.466 2.203 1.786 699.626

88 88.935 95-47-6 Q8 o-Xylene 1.395 1.219 1.010 395.859

89 91.739 111-84-2 P9 n-Nonane 0.013 0.014 0.008 3.421

90 93.095 98-82-8 Q9 i-Propylbenzene 0.035 0.031 0.023 9.924

91 93.842 ? Unidentified 0.015 0.015 0.008 4.781

92 94.86015869-89-3 I10 2,5-Dimethyloctane 0.009 0.010 0.005 2.416

93 95.508 2051-30-1 I10 2,4-Dimethyloctane 0.032 0.034 0.017 8.411

94 95.898 I10 2,6-Dimethyloctane 0.010 0.010 0.005 2.548

95 96.557 103-65-1 Q9 n-Propylbenzene 0.546 0.487 0.349 153.898

96 97.412 620-14-4 Q9 1-Methyl-3-ethylbenzene 2.190 1.948 1.401 617.332

97 97.643 622-96-8 Q9 1-Methyl-4-ethylbenzene 1.026 0.916 0.656 289.162

98 98.268 108-67-8 Q9 1,3,5-Trimethylbenzene 1.319 1.173 0.844 371.949

99 98.72415869-85-9 I10 5-Methylnonane 0.009 0.010 0.005 2.453

100 98.91317301-94-8 I10 4-Methylnonane 0.022 0.023 0.012 5.861

101 99.119 ? Unidentified 0.568 0.601 0.307 186.648

102 99.349 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.795 0.694 0.509 224.157

103 99.568 5881-17-4 I10 3-Ethyloctane 0.004 0.005 0.002 1.185

104 99.889 5911-04-6 I10 3-Methylnonane 0.031 0.033 0.017 8.312

105 100.353 ? Unidentified 0.045 0.034 0.022 14.684

106 100.487 ? Unidentified 0.128 0.132 0.063 42.031

107 100.701 I11 C11-Isoparaffin-2 0.068 0.070 0.033 18.003

108 100.998 95-63-6 Q9 1,2,4-Trimethylbenzene 4.010 3.522 2.565 1130.624

109 101.165 ? Unidentified 0.085 0.094 0.047 28.053

110 101.287 ? Unidentified 0.050 0.052 0.027 16.373

111 101.551 1678-98-4 M10 i-Butylcyclohexane 0.011 0.011 0.006 3.000

112 102.33817302-01-1 I10 3-Ethyl-3-methylheptane 0.140 0.145 0.069 37.096

113 102.636 538-93-2 Q10 i-Butylbenzene 0.210 0.189 0.120 58.832

114 102.901 ? Unidentified 0.048 0.043 0.028 15.814

115 103.200 ? Unidentified 0.035 0.036 0.017 11.499

116 103.855 526-73-8 Q9 1,2,3-Trimethylbenzene 0.711 0.612 0.455 200.480

117 104.234 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.024 0.022 0.014 6.805

118 104.411 I11 C11 Isoparaffin-4 0.019 0.020 0.010 5.146

119 104.617 99-87-6 Q10 1-Methyl-4-i-propylbenzene 0.134 0.121 0.077 37.701

120 105.046 J9 Indan 0.258 0.206 0.168 74.055

121 105.643 J10 Indene 0.733 0.585 0.477 210.012

122 106.358 I11 C11-Isoparaffin-7 0.318 0.329 0.156 84.204

123 106.549 141-93-5 Q10 1,3-Diethylbenzene 0.097 0.086 0.055 27.102

124 106.834 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 1.138 1.017 0.652 319.151

125 107.167 105-05-5 Q10 1,4-Diethylbenzene 0.420 0.375 0.240 117.726

126 107.385 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.301 0.264 0.173 84.543

127 107.626 135-01-3 Q10 1,2-Diethylbenzene 0.079 0.069 0.045 22.122

128 108.083 ? Unidentified 0.080 0.082 0.039 26.142

129 108.235 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.103 0.091 0.059 28.968

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C-542
Hydrocarbon Expert V4.7 Fri Aug 27 13:42:53 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91329 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91329

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 108.358 ? Unidentified 0.091 0.094 0.045 29.838

131 108.437 ? Unidentified 0.083 0.086 0.041 27.434

132 108.566 I11 C11- Isoparaffin-11 0.694 0.717 0.341 183.768

133 108.746 ? Unidentified 0.224 0.232 0.110 73.628

134 109.084 1758-88-9 Q10 1,4,Dimethyl-2-ethylbenzene 0.209 0.183 0.120 58.511

135 109.170 ? Unidentified 0.812 0.712 0.465 266.890

136 109.397 J10 2-Methylindan 0.127 0.102 0.074 36.451

137 109.745 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.691 0.608 0.396 193.699

138 110.287 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.627 0.541 0.359 175.760

139 110.711 ? Unidentified 0.022 0.020 0.011 7.130

140 110.906 693-61-8 K11 2-Undecene, (E)- 0.053 0.055 0.029 14.139

141 111.040 ? Unidentified 0.101 0.105 0.055 33.160

142 111.192 Q11 1-Methyl-4-t-butylbenzene 0.041 0.037 0.021 11.322

143 111.314 ? Unidentified 0.100 0.087 0.052 32.932

144 111.415 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.163 0.140 0.093 45.632

145 111.712 1120-21-4 P11 n-Undecane 0.083 0.085 0.041 21.905

146 111.864 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.090 0.078 0.047 25.236

147 111.975 ? Unidentified 0.057 0.050 0.030 18.882

148 112.352 Q10 1,2,4,5-Tetramethylbenzene 0.538 0.467 0.308 150.976

149 112.618 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.730 0.631 0.418 204.853

150 112.821 ? Unidentified 0.012 0.010 0.006 3.858

151 112.958 ? Unidentified 0.015 0.013 0.009 4.849

152 113.132 I12 C12 - IsoParaffin - 1 0.020 0.020 0.009 5.230

153 113.482 ? Unidentified 0.035 0.037 0.017 11.625

154 113.613 ? Unidentified 0.007 0.007 0.003 2.309

155 113.757 Q11 C11 - Aromatic - 3 0.096 0.083 0.050 26.882

156 113.947 874-35-1 H10 5-Methylindan 0.229 0.198 0.133 64.313

157 114.072 Q12 1,2-Di-i-propylbenzene 0.083 0.072 0.039 23.143

158 114.286 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.119 0.103 0.062 33.241

159 114.443 Q11 C11 - Aromatic - 4 0.068 0.059 0.035 18.949

160 114.696 824-22-6 J10 4-Methylindan 0.302 0.261 0.175 84.586

161 114.847 5161-04-6 Q11 Benzene, 1-methyl-4-(2-methylpropyl)-0.071 0.061 0.037 19.699

162 114.944 824-63-5 H10 2-Methylindan 0.223 0.192 0.130 62.446

163 115.146 ? Unidentified 0.022 0.023 0.010 7.192

164 115.259 538-68-1 Q11 n-Pentylbenzene 0.028 0.024 0.015 7.833

165 115.486 Q11 tert-Pentylbenzene 0.123 0.107 0.064 34.466

166 115.799 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.055 0.048 0.029 15.369

167 115.908 Q11 C11 - Aromatic - 7 0.070 0.064 0.037 19.675

168 116.238 I12 C12 - IsoParaffin - 4 0.005 0.006 0.002 1.513

169 116.369 100-18-5 Q12 1,4-Di-i-propylbenzene 0.109 0.094 0.052 30.323

170 116.813 91-20-3 G10 Naphthalene 0.233 0.175 0.140 68.466

171 117.007 J11 4,7-Dimethyl Indane 0.011 0.009 0.006 3.158

172 117.252 J11 1,1-Dimethyl Indane 0.037 0.029 0.019 10.480

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C-543
Hydrocarbon Expert V4.7 Fri Aug 27 13:42:53 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91329 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91329

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 117.414 J12 Dimethyl Indane - 1 0.015 0.012 0.008 4.273

174 117.593 7364-19-4 Q12 1t-Butyl-4-ethylbenzene 0.017 0.015 0.008 4.694

175 117.733 J12 Dimethyl Indane - 2 0.005 0.004 0.003 1.536

176 117.895 Q12 1,3-Di-n-propylbenzene 0.090 0.078 0.043 25.039

177 118.005 Q11 C11 - Aromatic - 11 0.051 0.046 0.026 14.158

178 118.559 Q11 C11 - Aromatic - 12 0.034 0.030 0.017 9.389

179 119.487 102-25-0 Q12 1,3,5-Triethylbenzene 0.009 0.008 0.004 2.415

180 120.147 Q12 C12 - Aromatic - 1 0.005 0.004 0.002 1.299

181 123.439 91-57-6 G11 2-Methylnaphthalene 0.009 0.007 0.005 2.635

182 124.306 90-12-0 G11 1-Methylnaphthalene 0.005 0.004 0.003 1.476

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C-544
Hydrocarbon Expert V4.7 Fri Aug 27 13:42:53 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91329 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91329

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 7.554 74-98-6 Propane 0.001 0.001 0.001 0.187

10.024 106-97-8 n-Butane 4.881 6.487 6.457 1264.928

18.111 109-66-0 n-Pentane 0.812 0.997 0.865 211.846

35.806 110-54-3 n-Hexane 1.796 2.095 1.603 470.606

58.053 142-82-5 n-Heptane 0.126 0.142 0.097 33.207

77.869 111-65-9 n-Octane 0.023 0.025 0.015 6.005

91.739 111-84-2 n-Nonane 0.013 0.014 0.008 3.421

111.712 1120-21-4 n-Undecane 0.083 0.085 0.041 21.905

I-Paraffins 8.810 75-28-5 i-Butane 0.021 0.030 0.028 5.549

10.637 463-82-1 2,2-Dimethylpropane 0.006 0.008 0.007 1.616

15.073 78-78-4 i-Pentane 2.491 3.092 2.654 649.939

23.089 75-83-2 2,2-Dimethylbutane 0.264 0.313 0.235 69.147

28.334 79-29-8 2,3-Dimethylbutane 1.068 1.242 0.953 279.771

29.438 107-83-5 2-Methylpentane 6.069 7.148 5.415 1589.994

32.074 96-14-0 3-Methylpentane 2.968 3.437 2.648 777.561

42.239 108-08-7 2,4-Dimethylpentane 0.209 0.239 0.160 54.905

42.778 464-06-2 2,2,3-Trimethylbutane 0.019 0.021 0.015 4.979

50.661 591-76-4 2-Methylhexane 0.552 0.626 0.423 145.154

52.491 589-34-4 3-Methylhexane 0.352 0.395 0.270 92.708

72.046 592-27-8 2-Methylheptane 0.019 0.020 0.012 4.877

72.299 589-53-7 4-Methylheptane 0.010 0.011 0.007 2.552

73.361 589-81-1 3-Methylheptane 0.019 0.021 0.013 5.011

94.86015869-89-3 2,5-Dimethyloctane 0.009 0.010 0.005 2.416

95.508 2051-30-1 2,4-Dimethyloctane 0.032 0.034 0.017 8.411

95.898 2,6-Dimethyloctane 0.010 0.010 0.005 2.548

98.72415869-85-9 5-Methylnonane 0.009 0.010 0.005 2.453

98.91317301-94-8 4-Methylnonane 0.022 0.023 0.012 5.861

99.568 5881-17-4 3-Ethyloctane 0.004 0.005 0.002 1.185

99.889 5911-04-6 3-Methylnonane 0.031 0.033 0.017 8.312

100.701 C11-Isoparaffin-2 0.068 0.070 0.033 18.003

102.33817302-01-1 3-Ethyl-3-methylheptane 0.140 0.145 0.069 37.096

104.411 C11 Isoparaffin-4 0.019 0.020 0.010 5.146

106.358 C11-Isoparaffin-7 0.318 0.329 0.156 84.204

108.566 C11- Isoparaffin-11 0.694 0.717 0.341 183.768

113.132 C12 - IsoParaffin - 1 0.020 0.020 0.009 5.230

116.238 C12 - IsoParaffin - 4 0.005 0.006 0.002 1.513

Aromatics

Mono-Aromatics 45.637 71-42-3 Benzene 0.762 0.667 0.750 220.346

69.069 108-88-3 Toluene 11.289 10.016 9.421 3227.774

84.742 100-41-4 Ethylbenzene 2.126 1.886 1.540 603.262

85.983 108-38-3 m-Xylene 5.424 4.828 3.928 1539.029

86.124 106-42-3 p-Xylene 2.466 2.203 1.786 699.626

88.935 95-47-6 o-Xylene 1.395 1.219 1.010 395.859

93.095 98-82-8 i-Propylbenzene 0.035 0.031 0.023 9.924

96.557 103-65-1 n-Propylbenzene 0.546 0.487 0.349 153.898

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C-545
Hydrocarbon Expert V4.7 Fri Aug 27 13:42:53 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91329 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91329

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 97.412 620-14-4 1-Methyl-3-ethylbenzene 2.190 1.948 1.401 617.332

97.643 622-96-8 1-Methyl-4-ethylbenzene 1.026 0.916 0.656 289.162

98.268 108-67-8 1,3,5-Trimethylbenzene 1.319 1.173 0.844 371.949

99.349 611-14-3 1-Methyl-2-ethylbenzene 0.795 0.694 0.509 224.157

100.998 95-63-6 1,2,4-Trimethylbenzene 4.010 3.522 2.565 1130.624

102.636 538-93-2 i-Butylbenzene 0.210 0.189 0.120 58.832

103.855 526-73-8 1,2,3-Trimethylbenzene 0.711 0.612 0.455 200.480

104.234 535-77-3 1-Methyl-3-i-propylbenzene 0.024 0.022 0.014 6.805

104.617 99-87-6 1-Methyl-4-i-propylbenzene 0.134 0.121 0.077 37.701

106.549 141-93-5 1,3-Diethylbenzene 0.097 0.086 0.055 27.102

106.834 1074-43-7 1-Methyl-3-n-propylbenzene 1.138 1.017 0.652 319.151

107.167 105-05-5 1,4-Diethylbenzene 0.420 0.375 0.240 117.726

107.385 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.301 0.264 0.173 84.543

107.626 135-01-3 1,2-Diethylbenzene 0.079 0.069 0.045 22.122

108.235 1074-17-5 1-Methyl-2-n-propylbenzene 0.103 0.091 0.059 28.968

109.084 1758-88-9 1,4,Dimethyl-2-ethylbenzene 0.209 0.183 0.120 58.511

109.745 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.691 0.608 0.396 193.699

110.287 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.627 0.541 0.359 175.760

111.192 1-Methyl-4-t-butylbenzene 0.041 0.037 0.021 11.322

111.415 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.163 0.140 0.093 45.632

111.864 4218-48-8 1-Ethyl-4-i-propylbenzene 0.090 0.078 0.047 25.236

112.352 1,2,4,5-Tetramethylbenzene 0.538 0.467 0.308 150.976

112.618 527-53-7 1,2,3,5-Tetramethylbenzene 0.730 0.631 0.418 204.853

113.757 C11 - Aromatic - 3 0.096 0.083 0.050 26.882

114.072 1,2-Di-i-propylbenzene 0.083 0.072 0.039 23.143

114.286 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.119 0.103 0.062 33.241

114.443 C11 - Aromatic - 4 0.068 0.059 0.035 18.949

114.847 5161-04-6 Benzene, 1-methyl-4-(2-methylpropyl)-0.071 0.061 0.037 19.699

115.259 538-68-1 n-Pentylbenzene 0.028 0.024 0.015 7.833

115.486 tert-Pentylbenzene 0.123 0.107 0.064 34.466

115.799 577-55-9 1-Methyl-2-n-butylbenzene 0.055 0.048 0.029 15.369

115.908 C11 - Aromatic - 7 0.070 0.064 0.037 19.675

116.369 100-18-5 1,4-Di-i-propylbenzene 0.109 0.094 0.052 30.323

117.593 7364-19-4 1t-Butyl-4-ethylbenzene 0.017 0.015 0.008 4.694

117.895 1,3-Di-n-propylbenzene 0.090 0.078 0.043 25.039

118.005 C11 - Aromatic - 11 0.051 0.046 0.026 14.158

118.559 C11 - Aromatic - 12 0.034 0.030 0.017 9.389

119.487 102-25-0 1,3,5-Triethylbenzene 0.009 0.008 0.004 2.415

120.147 C12 - Aromatic - 1 0.005 0.004 0.002 1.299

Naphthalenes 116.813 91-20-3 Naphthalene 0.233 0.175 0.140 68.466

123.439 91-57-6 2-Methylnaphthalene 0.009 0.007 0.005 2.635

124.306 90-12-0 1-Methylnaphthalene 0.005 0.004 0.003 1.476

Naphtheno/Olefino-Benzs 113.947 874-35-1 5-Methylindan 0.229 0.198 0.133 64.313

114.944 824-63-5 2-Methylindan 0.223 0.192 0.130 62.446

Indenes 105.046 Indan 0.258 0.206 0.168 74.055

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C-546
Hydrocarbon Expert V4.7 Fri Aug 27 13:42:53 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91329 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91329

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Indenes 105.643 Indene 0.733 0.585 0.477 210.012

109.397 2-Methylindan 0.127 0.102 0.074 36.451

114.696 824-22-6 4-Methylindan 0.302 0.261 0.175 84.586

117.007 4,7-Dimethyl Indane 0.011 0.009 0.006 3.158

117.252 1,1-Dimethyl Indane 0.037 0.029 0.019 10.480

117.414 Dimethyl Indane - 1 0.015 0.012 0.008 4.273

117.733 Dimethyl Indane - 2 0.005 0.004 0.003 1.536

Naphthenes

Mono-Naphthenes 27.604 287-92-3 Cyclopentane 0.244 0.251 0.267 65.362

40.671 96-37-7 Methylcyclopentane 1.055 1.085 0.964 283.306

47.552 110-82-7 Cyclohexane 0.448 0.442 0.409 120.162

53.352 1759-58-6 1t,3-Dimethylcyclopentane 0.100 0.103 0.078 26.826

53.938 2532-58-3 1c,3-Dimethylcyclopentane 0.068 0.070 0.053 18.197

54.563 822-50-4 1t,2-Dimethylcyclopentane 0.069 0.070 0.054 18.403

59.65016491-15-9 Cyclopentene, 1,5-dimethyl- 0.018 0.019 0.014 4.888

61.507 108-87-2 Methylcyclohexane 0.058 0.058 0.046 15.648

101.551 1678-98-4 i-Butylcyclohexane 0.011 0.011 0.006 3.000

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.623 115-11-7 Isobutene 0.016 0.020 0.022 4.228

9.664 106-98-9 Butene-1 0.018 0.023 0.024 4.729

10.510 624-64-6 t-Butene-2 0.072 0.092 0.099 19.355

11.250 590-18-1 c-Butene-2 0.085 0.105 0.116 22.797

16.730 109-67-1 Pentene-1 0.328 0.393 0.359 87.931

19.232 646-04-8 t-Pentene-2 0.832 0.987 0.912 223.252

20.263 627-20-3 c-Pentene-2 0.456 0.535 0.500 122.419

33.450 592-41-6 Hexene-1 0.157 0.178 0.144 42.227

36.43913269-52-8 t-Hexene-3 0.258 0.291 0.236 69.365

36.916 4050-45-7 t-Hexene-2 0.397 0.447 0.363 106.583

38.742 7688-21-3 c-Hexene-2 0.210 0.234 0.192 56.392

55.468 592-76-7 Heptene-1 0.027 0.030 0.021 7.291

57.33214686-14-7 t-Heptene-3 0.031 0.034 0.025 8.413

58.274 7642-10-6 c-Heptene-3 0.025 0.027 0.019 6.665

59.17414686-13-6 t-Heptene-2 0.013 0.014 0.010 3.395

110.906 693-61-8 2-Undecene, (E)- 0.053 0.055 0.029 14.139

Iso-Olefins 13.454 563-45-1 3-Methylbutene-1 0.197 0.242 0.216 52.954

17.577 563-46-2 2-Methylbutene-1 0.497 0.588 0.545 133.516

20.940 513-35-9 2-Methylbutene-2 1.021 1.186 1.120 274.156

29.194 691-38-3 4-Methyl-c-pentene-2 0.044 0.051 0.041 11.916

29.843 674-76-0 4-Methyl-t-pentene-2 0.128 0.147 0.117 34.450

33.233 763-29-1 2-Methylpentene-1 0.220 0.247 0.201 59.096

35.642 760-21-4 2-Ethylbutene-1 0.062 0.069 0.057 16.747

37.406 625-27-4 2-Methylpentene-2 0.335 0.373 0.306 89.849

37.820 922-62-3 3-Methyl-c-pentene-2 0.259 0.285 0.236 69.441

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C-547
Hydrocarbon Expert V4.7 Fri Aug 27 13:42:53 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91329 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91329

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Iso-Olefins 40.086 3404-73-7 3,3-Dimethylpentene-1 0.306 0.336 0.240 82.196

42.532 594-56-9 2,3,3-Trimethylbutene-1 0.013 0.014 0.010 3.544

46.637 3404-61-3 3-Methylhexene-1 0.016 0.017 0.012 4.167

47.230 3524-73-0 5-Methylhexene-1 0.038 0.042 0.030 10.241

49.27215840-60-5 2-Methyl-c-hexene-3 0.040 0.044 0.031 10.677

49.619 3769-23-1 4-Methylhexene-1 0.011 0.012 0.008 2.867

50.266 3404-55-5 4-Methyl-t/c-hexene-2 0.050 0.055 0.039 13.442

54.842 C7 - Iso-Olefin - 2 0.022 0.023 0.017 5.868

56.801 4914-89-0 3-Methyl-c-hexene-3 0.014 0.015 0.011 3.660

57.683 6094-02-6 2-Methylhexene-1 0.056 0.062 0.044 15.137

58.548 2738-19-4 2-Methyl-2-hexene 0.026 0.028 0.020 6.845

58.79310574-36-4 3-Methyl-c-hexene-2 0.019 0.021 0.015 5.209

60.07720710-38-8 3-Methyl-t-hexene-2 0.015 0.016 0.012 3.985

60.859 4914-91-4 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.014 0.010 3.431

Naphtheno-Olefins 22.534 1574-41-0 1,3-Cyclopentadiene 0.007 0.008 0.008 1.879

25.739 142-29-0 Cyclopentene 0.194 0.193 0.219 53.497

37.042 1120-62-3 3-Methylcyclopentene 0.098 0.099 0.092 26.242

45.833 693-89-0 1-Methylcyclopentene 0.354 0.349 0.331 97.257

51.152 110-83-8 Cyclohexene 0.044 0.042 0.041 11.800

Di-Olefins 18.628 78-79-5 2-Methyl-1,3-Butadiene 0.010 0.012 0.012 2.816

21.269 2004-70-8 1t,3-Pentadiene 0.015 0.018 0.017 4.261

45.429 1528-30-9 C6-Diolefin-1 0.015 0.015 0.014 3.975

Oxygenates 13.124 64-17-5 Ethanol 21.767 21.222 36.330 2405.814

26.906 71-23-8 n-Propanol 0.078 0.075 0.100 14.745

48.062 71-36-3 n-Butanol 0.055 0.052 0.057 11.090

Unidentified 19.882 Unidentified 0.006 0.007 0.006 1.907

26.991 Unidentified 0.056 0.064 0.051 18.364

28.733 Unidentified 0.052 0.054 0.045 17.036

50.840 Unidentified 0.024 0.027 0.019 7.980

63.361 Unidentified 0.057 0.061 0.040 18.873

93.842 Unidentified 0.015 0.015 0.008 4.781

99.119 Unidentified 0.568 0.601 0.307 186.648

100.353 Unidentified 0.045 0.034 0.022 14.684

100.487 Unidentified 0.128 0.132 0.063 42.031

101.165 Unidentified 0.085 0.094 0.047 28.053

101.287 Unidentified 0.050 0.052 0.027 16.373

102.901 Unidentified 0.048 0.043 0.028 15.814

103.200 Unidentified 0.035 0.036 0.017 11.499

108.083 Unidentified 0.080 0.082 0.039 26.142

108.358 Unidentified 0.091 0.094 0.045 29.838

108.437 Unidentified 0.083 0.086 0.041 27.434

108.746 Unidentified 0.224 0.232 0.110 73.628

109.170 Unidentified 0.812 0.712 0.465 266.890

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C-548
Hydrocarbon Expert V4.7 Fri Aug 27 13:42:53 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91329 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91329

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Unidentified 110.711 Unidentified 0.022 0.020 0.011 7.130

111.040 Unidentified 0.101 0.105 0.055 33.160

111.314 Unidentified 0.100 0.087 0.052 32.932

111.975 Unidentified 0.057 0.050 0.030 18.882

112.821 Unidentified 0.012 0.010 0.006 3.858

112.958 Unidentified 0.015 0.013 0.009 4.849

113.482 Unidentified 0.035 0.037 0.017 11.625

113.613 Unidentified 0.007 0.007 0.003 2.309

115.146 Unidentified 0.022 0.023 0.010 7.192

Plus

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C-549
Hydrocarbon Expert V4.7 Fri Aug 27 13:42:53 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91329 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91329

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF

20.0 15.0 10.0 5.0 0.0

Propane

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

Ethanol

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

Unidentified

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

1,3-Cyclopentadiene

2,2-Dimethylbutane

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C-550
Hydrocarbon Expert V4.7 Fri Aug 27 13:42:53 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91329 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91329

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

n-Propanol Unidentified

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

2-Ethylbutene-1 n-Hexane

t-Hexene-3

t-Hexene-2 3-Methylcyclopentene

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane 2,3,3-Trimethylbutene-1 2,2,3-Trimethylbutane

C6-Diolefin-1 Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1

Cyclohexane

n-Butanol

2-Methyl-c-hexene-3

4-Methylhexene-1

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C-551
Hydrocarbon Expert V4.7 Fri Aug 27 13:42:53 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91329 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91329

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF

70.0 65.0 60.0 55.0 50.0

4-Methyl-t/c-hexene-2

2-Methylhexane Unidentified Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane C7 - Iso-Olefin - 2

Heptene-1

3-Methyl-c-hexene-3

t-Heptene-3

2-Methylhexene-1

n-Heptane c-Heptene-3 2-Methyl-2-hexene 3-Methyl-c-hexene-2

t-Heptene-2

Cyclopentene, 1,5-dimethyl3-Methyl-t-hexene-2

2-Pentene, 3,4-dimethyl-, (Z)-

Methylcyclohexane

Unidentified

Toluene

2-Methylheptane 4-Methylheptane

3-Methylheptane

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C-552
Hydrocarbon Expert V4.7 Fri Aug 27 13:42:53 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91329 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91329

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF

95.0 90.0 85.0 80.0 75.0

n-Octane

Ethylbenzene

m-Xylene p-Xylene

o-Xylene

n-Nonane

i-Propylbenzene

Unidentified

2,5-Dimethyloctane

2,4-Dimethyloctane

2,6-Dimethyloctane

n-Propylbenzene

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

5-Methylnonane 4-Methylnonane Unidentified 1-Methyl-2-ethylbenzene 3-Ethyloctane

3-Methylnonane

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C-553
Hydrocarbon Expert V4.7 Fri Aug 27 13:42:53 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91329 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91329

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified Unidentified C11-Isoparaffin-2 1,2,4-Trimethylbenzene Unidentified

i-Butylcyclohexane

3-Ethyl-3-methylheptane i-Butylbenzene Unidentified Unidentified

1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene C11 Isoparaffin-4 1-Methyl-4-i-propylbenzene

Indan

Indene

C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene

1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

Unidentified 1-Methyl-2-n-propylbenzene Unidentified C11- Isoparaffin-11 Unidentified

1,4,Dimethyl-2-ethylbenzene Unidentified 2-Methylindan

1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

Unidentified 2-Undecene, (E)- Unidentified 1-Methyl-4-t-butylbenzene Unidentified 1,2-Dimethyl-3-ethylbenzene n-Undecane Unidentified 1-Ethyl-4-i-propylbenzene

1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene Unidentified C12 - IsoParaffin - 1

Unidentified C11 - Aromatic - 3 5-Methylindan 1,2-Di-i-propylbenzene 1-methyl-4-(1-methylpropyl)be C11 - Aromatic - 4 4-Methylindan Benzene, 1-methyl-4-(2-methylpropyl)- 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene

1-Methyl-2-n-butylbenzene C11 - Aromatic - 7

C12 - IsoParaffin - 4 1,4-Di-i-propylbenzene

Naphthalene 4,7-Dimethyl Indane 1,1-Dimethyl Indane Dimethyl Indane - 1

Dimethyl Indane - 2 1t-Butyl-4-ethylbenzene

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

C11 - Aromatic - 12

1,3,5-Triethylbenzene

C12 - Aromatic - 1

2-Methylnaphthalene

1-Methylnaphthalene

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C-554
Hydrocarbon Expert V4.7 Fri Aug 27 13:42:53 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF 25-Aug-10, 13:30:15

Sample: ODDB-91329 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91329

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000011.D\SIG2000011_FID2_B.CDF

145.0 140.0 135.0 130.0 125.0

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C-555
Hydrocarbon Expert V4.7 Fri Aug 27 13:48:42 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91330 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91330

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 3.580 4.480 4.343

I-Paraffins 26.765 31.493 26.304

Aromatics 43.296 37.521 31.368

Mono-Aromatics 41.011 35.674 29.940

Naphthalenes 0.336 0.248 0.208

Naphtheno/Olefino-Benzs 0.627 0.533 0.378

Indenes 1.323 1.066 0.842

Naphthenes 1.425 1.438 1.364

Mono-Naphthenes 1.425 1.438 1.364

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 7.192 8.040 7.486

n-Olefins 2.990 3.428 3.204

Iso-Olefins 3.439 3.863 3.497

Naphtheno-Olefins 0.722 0.705 0.740

Di-Olefins 0.041 0.044 0.045

Oxygenates 16.442 15.774 28.362

Unidentified 1.299 1.253 0.773

Plus 0.000 0.000 0.000

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C-556
Hydrocarbon Expert V4.7 Fri Aug 27 13:48:42 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91330 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91330

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C2 16.311 15.650 28.202

C3 0.075 0.071 0.100

C4 2.371 3.069 3.242

C5 16.690 20.062 18.558

C6 17.331 19.450 16.176

C7 12.679 11.479 10.842

C8 11.410 9.988 8.557

C9 10.612 9.198 7.035

C10 8.720 7.509 5.212

C11 2.026 1.866 1.069

C12 0.476 0.406 0.235

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C-557
Hydrocarbon Expert V4.7 Fri Aug 27 13:48:42 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91330 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91330

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C4 2.109 2.758 2.890

C5 0.838 1.014 0.926

C6 0.413 0.474 0.382

C7 0.096 0.107 0.077

C8 0.020 0.022 0.014

C9 0.006 0.007 0.004

C10 0.033 0.034 0.018

C11 0.063 0.064 0.032

I-Paraffins C4 0.017 0.023 0.023

C5 11.941 14.589 13.183

C6 12.756 14.704 11.791

C7 0.827 0.920 0.657

C8 0.046 0.050 0.032

C10 0.440 0.456 0.243

C11 0.719 0.732 0.367

C12 0.018 0.019 0.009

Mono-Aromatics C6 0.726 0.626 0.741

C7 10.715 9.355 9.262

C8 11.343 9.915 8.510

C9 10.358 8.996 6.864

C10 6.308 5.442 3.744

C11 1.130 0.973 0.607

C12 0.430 0.366 0.211

Naphthalenes C10 0.320 0.237 0.199

C11 0.015 0.011 0.008

Naphtheno/Olefino-Benzs C10 0.627 0.533 0.378

Indenes C9 0.248 0.195 0.167

C10 0.984 0.801 0.626

C11 0.063 0.049 0.034

C12 0.027 0.021 0.015

Mono-Naphthenes C5 0.313 0.318 0.355

C6 0.809 0.815 0.765

C7 0.297 0.299 0.240

C10 0.007 0.006 0.004

n-Olefins C4 0.189 0.235 0.269

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C-558
Hydrocarbon Expert V4.7 Fri Aug 27 13:48:42 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91330 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91330

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

n-Olefins C5 1.637 1.911 1.859

C6 1.044 1.156 0.988

C7 0.084 0.091 0.068

C11 0.035 0.036 0.020

Iso-Olefins C5 1.731 2.001 1.965

C6 1.077 1.183 1.019

C7 0.631 0.679 0.512

Naphtheno-Olefins C5 0.204 0.201 0.239

C6 0.506 0.491 0.490

C7 0.013 0.012 0.011

Di-Olefins C5 0.026 0.029 0.031

C7 0.015 0.015 0.015

Oxygenates C2 16.311 15.650 28.202

C3 0.075 0.071 0.100

C4 0.056 0.053 0.060

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C-559
Hydrocarbon Expert V4.7 Fri Aug 27 13:48:42 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91330 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91330

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 22.89 22.31

5% 79.44 79.16

10% 80.80 80.27

15% 86.39 81.38

20% 134.21 96.99

25% 138.99 135.70

30% 144.35 139.00

35% 159.47 143.92

40% 172.48 154.03

45% 172.81 172.40

50% 173.14 172.74

55% 220.09 173.09

60% 225.26 197.38

65% 230.43 225.20

70% 280.63 243.86

75% 282.22 281.36

80% 322.54 291.87

85% 335.29 329.33

90% 359.24 352.03

95% 374.16 372.02

FBP 410.01 404.60

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C-560
Hydrocarbon Expert V4.7 Fri Aug 27 13:48:42 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91330 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91330

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 8.809 75-28-5 I4 i-Butane 0.017 0.023 0.023 5.177

2 9.621 115-11-7 K4 Isobutene 0.016 0.020 0.022 5.023

3 9.663 106-98-9 K4 Butene-1 0.017 0.022 0.025 5.591

4 10.023 106-97-8 P4 n-Butane 2.109 2.758 2.890 655.608

5 10.509 624-64-6 K4 t-Butene-2 0.072 0.090 0.102 23.066

6 10.637 463-82-1 I5 2,2-Dimethylpropane 0.008 0.010 0.009 2.511

7 11.251 590-18-1 K4 c-Butene-2 0.085 0.103 0.120 27.303

8 13.111 64-17-5 X2 Ethanol 16.311 15.650 28.202 2162.315

9 13.451 563-45-1 C5 3-Methylbutene-1 0.190 0.230 0.216 61.273

10 15.097 78-78-4 I5 i-Pentane 11.933 14.579 13.174 3735.075

11 16.728 109-67-1 K5 Pentene-1 0.331 0.392 0.376 106.701

12 17.580 563-46-2 C5 2-Methylbutene-1 0.504 0.586 0.572 162.173

13 18.112 109-66-0 P5 n-Pentane 0.838 1.014 0.926 262.437

14 18.625 78-79-5 E5 2-Methyl-1,3-Butadiene 0.010 0.012 0.012 3.456

15 19.232 646-04-8 K5 t-Pentene-2 0.843 0.985 0.958 271.448

16 19.879 ? Unidentified 0.006 0.007 0.007 2.292

17 20.266 627-20-3 K5 c-Pentene-2 0.463 0.534 0.525 148.936

18 20.944 513-35-9 C5 2-Methylbutene-2 1.037 1.185 1.177 333.713

19 21.270 2004-70-8 E5 1t,3-Pentadiene 0.016 0.018 0.018 5.211

20 22.535 1574-41-0 B5 1,3-Cyclopentadiene 0.007 0.008 0.008 2.314

21 23.092 75-83-2 I6 2,2-Dimethylbutane 0.369 0.430 0.341 115.862

22 25.740 142-29-0 B5 Cyclopentene 0.197 0.193 0.230 65.328

23 26.904 71-23-8 X3 n-Propanol 0.075 0.071 0.100 16.972

24 26.995 ? Unidentified 0.059 0.067 0.056 23.426

25 27.606 287-92-3 M5 Cyclopentane 0.313 0.318 0.355 100.758

26 28.342 79-29-8 I6 2,3-Dimethylbutane 1.375 1.573 1.270 431.949

27 28.734 ? Unidentified 0.053 0.054 0.048 20.912

28 29.204 691-38-3 C6 4-Methyl-c-pentene-2 0.045 0.050 0.042 14.401

29 29.461 107-83-5 I6 2-Methylpentane 7.744 8.976 7.158 2433.703

30 29.850 674-76-0 C6 4-Methyl-t-pentene-2 0.131 0.147 0.124 42.030

31 32.083 96-14-0 I6 3-Methylpentane 3.269 3.725 3.021 1027.171

32 33.230 763-29-1 C6 2-Methylpentene-1 0.224 0.248 0.212 72.191

33 33.454 592-41-6 K6 Hexene-1 0.160 0.179 0.152 51.582

34 35.641 760-21-4 C6 2-Ethylbutene-1 0.072 0.079 0.068 23.300

35 35.802 110-54-3 P6 n-Hexane 0.413 0.474 0.382 129.877

36 36.43913269-52-8 K6 t-Hexene-3 0.263 0.292 0.249 84.733

37 36.918 4050-45-7 K6 t-Hexene-2 0.406 0.450 0.384 130.707

38 37.040 1120-62-3 B6 3-Methylcyclopentene 0.099 0.098 0.096 31.759

39 37.408 625-27-4 C6 2-Methylpentene-2 0.341 0.374 0.323 109.806

40 37.823 922-62-3 C6 3-Methyl-c-pentene-2 0.264 0.286 0.250 84.946

41 38.745 7688-21-3 K6 c-Hexene-2 0.214 0.235 0.203 69.017

42 40.091 3404-73-7 C7 3,3-Dimethylpentene-1 0.311 0.335 0.252 100.051

43 40.670 96-37-7 M6 Methylcyclopentane 0.740 0.748 0.700 238.146

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C-561
Hydrocarbon Expert V4.7 Fri Aug 27 13:48:42 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91330 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91330

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 42.243 108-08-7 I7 2,4-Dimethylpentane 0.146 0.164 0.116 46.060

45 42.534 594-56-9 C7 2,3,3-Trimethylbutene-1 0.009 0.010 0.007 2.897

46 44.495 7459-71-4 B7 3,5-Dimethylcyclopentene 0.013 0.012 0.011 4.125

47 45.429 1528-30-9 E7 C6-Diolefin-1 0.015 0.015 0.015 4.875

48 45.640 71-42-3 Q6 Benzene 0.726 0.626 0.741 251.866

49 45.836 693-89-0 B6 1-Methylcyclopentene 0.362 0.351 0.351 119.252

50 46.643 3404-61-3 C7 3-Methylhexene-1 0.016 0.018 0.013 5.217

51 47.229 3524-73-0 C7 5-Methylhexene-1 0.023 0.025 0.018 7.340

52 47.553 110-82-7 M6 Cyclohexane 0.069 0.067 0.065 22.211

53 48.058 71-36-3 X4 n-Butanol 0.056 0.053 0.060 13.663

54 49.27415840-60-5 C7 2-Methyl-c-hexene-3 0.041 0.044 0.033 13.058

55 49.621 3769-23-1 C7 4-Methylhexene-1 0.011 0.012 0.009 3.672

56 50.268 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.051 0.055 0.042 16.512

57 50.661 591-76-4 I7 2-Methylhexane 0.405 0.452 0.322 127.777

58 50.841 ? Unidentified 0.020 0.022 0.017 7.883

59 51.153 110-83-8 B6 Cyclohexene 0.045 0.042 0.044 14.542

60 52.493 589-34-4 I7 3-Methylhexane 0.276 0.304 0.220 87.130

61 53.354 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.097 0.098 0.078 31.087

62 53.940 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.064 0.065 0.052 20.739

63 54.566 822-50-4 M7 1t,2-Dimethylcyclopentane 0.059 0.059 0.048 18.891

64 54.843 C7 C7 - Iso-Olefin - 2 0.023 0.024 0.018 7.276

65 55.470 592-76-7 K7 Heptene-1 0.014 0.015 0.011 4.427

66 55.604 M7 C7 - MonoNaph - 1 0.014 0.013 0.010 4.429

67 56.803 4914-89-0 C7 3-Methyl-c-hexene-3 0.014 0.015 0.011 4.505

68 57.33314686-14-7 K7 t-Heptene-3 0.032 0.035 0.026 10.417

69 57.685 6094-02-6 C7 2-Methylhexene-1 0.058 0.063 0.047 18.603

70 58.055 142-82-5 P7 n-Heptane 0.096 0.107 0.077 30.404

71 58.276 7642-10-6 K7 c-Heptene-3 0.026 0.028 0.021 8.302

72 58.550 2738-19-4 C7 2-Methyl-2-hexene 0.026 0.028 0.021 8.482

73 58.79410574-36-4 C7 3-Methyl-c-hexene-2 0.020 0.021 0.016 6.457

74 59.17614686-13-6 K7 t-Heptene-2 0.012 0.013 0.010 3.954

75 59.65316491-15-9 M7 Cyclopentene, 1,5-dimethyl- 0.019 0.019 0.015 6.028

76 60.07820710-38-8 C7 3-Methyl-t-hexene-2 0.015 0.016 0.012 4.946

77 60.862 4914-91-4 C7 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.014 0.011 4.178

78 61.503 108-87-2 M7 Methylcyclohexane 0.045 0.044 0.037 14.529

79 63.365 ? Unidentified 0.045 0.047 0.032 17.677

80 69.082 108-88-3 Q7 Toluene 10.715 9.355 9.262 3674.563

81 72.047 592-27-8 I8 2-Methylheptane 0.018 0.019 0.012 5.541

82 72.301 589-53-7 I8 4-Methylheptane 0.010 0.010 0.007 3.071

83 73.362 589-81-1 I8 3-Methylheptane 0.019 0.021 0.013 6.059

84 77.870 111-65-9 P8 n-Octane 0.020 0.022 0.014 6.465

85 84.746 100-41-4 Q8 Ethylbenzene 2.111 1.843 1.584 718.518

86 85.993 108-38-3 Q8 m-Xylene 5.389 4.721 4.043 1834.259

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C-562
Hydrocarbon Expert V4.7 Fri Aug 27 13:48:42 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91330 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91330

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 86.132 106-42-3 Q8 p-Xylene 2.444 2.149 1.834 831.977

88 88.939 95-47-6 Q8 o-Xylene 1.398 1.202 1.049 475.836

89 91.751 111-84-2 P9 n-Nonane 0.006 0.007 0.004 1.995

90 93.096 98-82-8 Q9 i-Propylbenzene 0.037 0.032 0.024 12.472

91 95.508 2051-30-1 I10 2,4-Dimethyloctane 0.009 0.009 0.005 2.705

92 96.558 103-65-1 Q9 n-Propylbenzene 0.530 0.466 0.351 179.330

93 97.417 620-14-4 Q9 1-Methyl-3-ethylbenzene 2.130 1.865 1.411 720.185

94 97.646 622-96-8 Q9 1-Methyl-4-ethylbenzene 0.998 0.877 0.661 337.491

95 98.271 108-67-8 Q9 1,3,5-Trimethylbenzene 1.274 1.114 0.844 430.727

96 98.72515869-85-9 I10 5-Methylnonane 0.009 0.009 0.005 2.729

97 98.91417301-94-8 I10 4-Methylnonane 0.021 0.021 0.011 6.508

98 99.118 I10 2,2,6-Trimethyloctane 0.297 0.310 0.167 94.413

99 99.351 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.778 0.669 0.516 263.055

100 99.570 5881-17-4 I10 3-Ethyloctane 0.006 0.006 0.003 1.815

101 99.890 5911-04-6 I10 3-Methylnonane 0.031 0.032 0.017 9.723

102 100.354 ? Unidentified 0.020 0.015 0.010 7.865

103 100.488 ? Unidentified 0.059 0.060 0.030 23.427

104 100.701 I11 C11-Isoparaffin-2 0.033 0.033 0.017 10.410

105 101.004 95-63-6 Q9 1,2,4-Trimethylbenzene 3.904 3.375 2.587 1320.248

106 101.166 ? Unidentified 0.042 0.046 0.024 16.645

107 101.288 ? Unidentified 0.025 0.026 0.014 9.938

108 101.551 1678-98-4 M10 i-Butylcyclohexane 0.007 0.006 0.004 2.107

109 102.33817302-01-1 I10 3-Ethyl-3-methylheptane 0.069 0.070 0.035 21.809

110 102.627 538-93-2 Q10 i-Butylbenzene 0.110 0.098 0.065 37.102

111 102.806 124-18-5 P10 n-Decane 0.033 0.034 0.018 10.422

112 102.902 ? Unidentified 0.044 0.039 0.026 17.297

113 103.200 ? Unidentified 0.019 0.019 0.010 7.375

114 103.856 526-73-8 Q9 1,2,3-Trimethylbenzene 0.707 0.599 0.469 239.171

115 104.244 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.021 0.018 0.012 6.930

116 104.412 I11 C11 Isoparaffin-4 0.012 0.012 0.006 3.736

117 104.617 99-87-6 Q10 1-Methyl-4-i-propylbenzene 0.081 0.071 0.048 27.192

118 105.047 J9 Indan 0.248 0.195 0.167 85.272

119 105.643 J10 Indene 0.460 0.362 0.310 158.236

120 106.358 I11 C11-Isoparaffin-7 0.206 0.209 0.105 65.361

121 106.549 141-93-5 Q10 1,3-Diethylbenzene 0.110 0.097 0.066 37.149

122 106.827 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 0.889 0.782 0.528 299.094

123 107.170 105-05-5 Q10 1,4-Diethylbenzene 0.353 0.310 0.209 118.667

124 107.267 104-51-8 Q10 n-Butylbenzene 0.067 0.059 0.040 22.570

125 107.387 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.396 0.341 0.235 133.245

126 107.644 135-01-3 Q10 1,2-Diethylbenzene 0.061 0.053 0.036 20.540

127 108.084 ? Unidentified 0.052 0.053 0.027 20.644

128 108.236 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.137 0.119 0.081 46.093

129 108.358 ? Unidentified 0.061 0.062 0.031 23.957

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C-563
Hydrocarbon Expert V4.7 Fri Aug 27 13:48:42 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91330 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91330

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 108.439 ? Unidentified 0.056 0.056 0.028 21.899

131 108.566 I11 C11- Isoparaffin-11 0.469 0.477 0.239 149.073

132 108.747 ? Unidentified 0.152 0.154 0.077 59.856

133 109.084 1758-88-9 Q10 1,4,Dimethyl-2-ethylbenzene 0.325 0.280 0.193 109.194

134 109.172 ? Unidentified 0.403 0.347 0.239 158.793

135 109.244 874-41-9 Q10 1,3-Dimethyl-4-ethylbenzene 0.361 0.312 0.214 121.545

136 109.397 J10 2-Methylindan 0.100 0.079 0.060 34.463

137 109.748 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.890 0.770 0.528 299.351

138 110.288 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.451 0.384 0.268 151.731

139 110.712 ? Unidentified 0.013 0.012 0.007 4.976

140 110.907 693-61-8 K11 2-Undecene, (E)- 0.035 0.036 0.020 11.152

141 111.042 ? Unidentified 0.046 0.047 0.026 17.953

142 111.197 Q11 1-Methyl-4-t-butylbenzene 0.077 0.068 0.041 25.643

143 111.418 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.306 0.259 0.181 102.803

144 111.714 1120-21-4 P11 n-Undecane 0.063 0.064 0.032 20.072

145 111.868 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.068 0.058 0.037 22.807

146 111.976 ? Unidentified 0.034 0.029 0.018 13.307

147 112.083 Q11 C11 - Aromatic - 1 0.007 0.006 0.004 2.456

148 112.356 Q10 1,2,4,5-Tetramethylbenzene 0.739 0.630 0.439 248.541

149 112.623 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 1.011 0.860 0.600 340.155

150 112.813 ? Unidentified 0.009 0.007 0.005 3.466

151 112.962 ? Unidentified 0.011 0.010 0.007 4.451

152 113.134 I12 C12 - IsoParaffin - 1 0.013 0.013 0.006 4.048

153 113.486 ? Unidentified 0.040 0.041 0.019 15.583

154 113.757 Q11 C11 - Aromatic - 3 0.116 0.098 0.062 38.766

155 113.949 874-35-1 H10 5-Methylindan 0.317 0.269 0.191 106.484

156 114.073 Q12 1,2-Di-i-propylbenzene 0.115 0.097 0.056 38.230

157 114.288 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.165 0.140 0.088 55.136

158 114.443 Q11 C11 - Aromatic - 4 0.091 0.077 0.049 30.433

159 114.698 824-22-6 J10 4-Methylindan 0.424 0.360 0.255 142.501

160 114.848 5161-04-6 Q11 Benzene, 1-methyl-4-(2-methylpropyl)-0.098 0.084 0.053 32.973

161 114.946 824-63-5 H10 2-Methylindan 0.310 0.264 0.187 104.407

162 115.146 ? Unidentified 0.030 0.030 0.014 11.648

163 115.260 538-68-1 Q11 n-Pentylbenzene 0.039 0.033 0.021 13.066

164 115.487 Q11 tert-Pentylbenzene 0.172 0.146 0.092 57.548

165 115.800 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.077 0.066 0.041 25.841

166 115.909 Q11 C11 - Aromatic - 7 0.095 0.084 0.051 31.740

167 116.239 I12 C12 - IsoParaffin - 4 0.006 0.006 0.003 1.924

168 116.370 100-18-5 Q12 1,4-Di-i-propylbenzene 0.149 0.127 0.073 49.736

169 116.815 91-20-3 G10 Naphthalene 0.320 0.237 0.199 112.847

170 117.008 J11 4,7-Dimethyl Indane 0.014 0.011 0.007 4.651

171 117.253 J11 1,1-Dimethyl Indane 0.049 0.039 0.027 16.938

172 117.415 J12 Dimethyl Indane - 1 0.020 0.016 0.011 6.967

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C-564
Hydrocarbon Expert V4.7 Fri Aug 27 13:48:42 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91330 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91330

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 117.593 7364-19-4 Q12 1t-Butyl-4-ethylbenzene 0.023 0.020 0.011 7.679

174 117.733 J12 Dimethyl Indane - 2 0.007 0.006 0.004 2.412

175 117.895 Q12 1,3-Di-n-propylbenzene 0.125 0.107 0.062 41.855

176 118.006 Q11 C11 - Aromatic - 11 0.071 0.063 0.038 23.710

177 118.559 Q11 C11 - Aromatic - 12 0.047 0.042 0.025 15.884

178 119.189 Q11 C11 - Aromatic - 13 0.007 0.007 0.004 2.459

179 119.487 102-25-0 Q12 1,3,5-Triethylbenzene 0.012 0.010 0.006 4.107

180 120.146 Q12 C12 - Aromatic - 1 0.006 0.005 0.003 2.105

181 123.440 91-57-6 G11 2-Methylnaphthalene 0.010 0.007 0.006 3.469

182 124.306 90-12-0 G11 1-Methylnaphthalene 0.005 0.004 0.003 1.842

183 130.001 ? Unidentified 0.003 0.002 0.001 1.142

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C-565
Hydrocarbon Expert V4.7 Fri Aug 27 13:48:42 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91330 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91330

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 10.023 106-97-8 n-Butane 2.109 2.758 2.890 655.608

18.112 109-66-0 n-Pentane 0.838 1.014 0.926 262.437

35.802 110-54-3 n-Hexane 0.413 0.474 0.382 129.877

58.055 142-82-5 n-Heptane 0.096 0.107 0.077 30.404

77.870 111-65-9 n-Octane 0.020 0.022 0.014 6.465

91.751 111-84-2 n-Nonane 0.006 0.007 0.004 1.995

102.806 124-18-5 n-Decane 0.033 0.034 0.018 10.422

111.714 1120-21-4 n-Undecane 0.063 0.064 0.032 20.072

I-Paraffins 8.809 75-28-5 i-Butane 0.017 0.023 0.023 5.177

10.637 463-82-1 2,2-Dimethylpropane 0.008 0.010 0.009 2.511

15.097 78-78-4 i-Pentane 11.933 14.579 13.174 3735.075

23.092 75-83-2 2,2-Dimethylbutane 0.369 0.430 0.341 115.862

28.342 79-29-8 2,3-Dimethylbutane 1.375 1.573 1.270 431.949

29.461 107-83-5 2-Methylpentane 7.744 8.976 7.158 2433.703

32.083 96-14-0 3-Methylpentane 3.269 3.725 3.021 1027.171

42.243 108-08-7 2,4-Dimethylpentane 0.146 0.164 0.116 46.060

50.661 591-76-4 2-Methylhexane 0.405 0.452 0.322 127.777

52.493 589-34-4 3-Methylhexane 0.276 0.304 0.220 87.130

72.047 592-27-8 2-Methylheptane 0.018 0.019 0.012 5.541

72.301 589-53-7 4-Methylheptane 0.010 0.010 0.007 3.071

73.362 589-81-1 3-Methylheptane 0.019 0.021 0.013 6.059

95.508 2051-30-1 2,4-Dimethyloctane 0.009 0.009 0.005 2.705

98.72515869-85-9 5-Methylnonane 0.009 0.009 0.005 2.729

98.91417301-94-8 4-Methylnonane 0.021 0.021 0.011 6.508

99.118 2,2,6-Trimethyloctane 0.297 0.310 0.167 94.413

99.570 5881-17-4 3-Ethyloctane 0.006 0.006 0.003 1.815

99.890 5911-04-6 3-Methylnonane 0.031 0.032 0.017 9.723

100.701 C11-Isoparaffin-2 0.033 0.033 0.017 10.410

102.33817302-01-1 3-Ethyl-3-methylheptane 0.069 0.070 0.035 21.809

104.412 C11 Isoparaffin-4 0.012 0.012 0.006 3.736

106.358 C11-Isoparaffin-7 0.206 0.209 0.105 65.361

108.566 C11- Isoparaffin-11 0.469 0.477 0.239 149.073

113.134 C12 - IsoParaffin - 1 0.013 0.013 0.006 4.048

116.239 C12 - IsoParaffin - 4 0.006 0.006 0.003 1.924

Aromatics

Mono-Aromatics 45.640 71-42-3 Benzene 0.726 0.626 0.741 251.866

69.082 108-88-3 Toluene 10.715 9.355 9.262 3674.563

84.746 100-41-4 Ethylbenzene 2.111 1.843 1.584 718.518

85.993 108-38-3 m-Xylene 5.389 4.721 4.043 1834.259

86.132 106-42-3 p-Xylene 2.444 2.149 1.834 831.977

88.939 95-47-6 o-Xylene 1.398 1.202 1.049 475.836

93.096 98-82-8 i-Propylbenzene 0.037 0.032 0.024 12.472

96.558 103-65-1 n-Propylbenzene 0.530 0.466 0.351 179.330

97.417 620-14-4 1-Methyl-3-ethylbenzene 2.130 1.865 1.411 720.185

97.646 622-96-8 1-Methyl-4-ethylbenzene 0.998 0.877 0.661 337.491

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C-566
Hydrocarbon Expert V4.7 Fri Aug 27 13:48:42 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91330 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91330

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 98.271 108-67-8 1,3,5-Trimethylbenzene 1.274 1.114 0.844 430.727

99.351 611-14-3 1-Methyl-2-ethylbenzene 0.778 0.669 0.516 263.055

101.004 95-63-6 1,2,4-Trimethylbenzene 3.904 3.375 2.587 1320.248

102.627 538-93-2 i-Butylbenzene 0.110 0.098 0.065 37.102

103.856 526-73-8 1,2,3-Trimethylbenzene 0.707 0.599 0.469 239.171

104.244 535-77-3 1-Methyl-3-i-propylbenzene 0.021 0.018 0.012 6.930

104.617 99-87-6 1-Methyl-4-i-propylbenzene 0.081 0.071 0.048 27.192

106.549 141-93-5 1,3-Diethylbenzene 0.110 0.097 0.066 37.149

106.827 1074-43-7 1-Methyl-3-n-propylbenzene 0.889 0.782 0.528 299.094

107.170 105-05-5 1,4-Diethylbenzene 0.353 0.310 0.209 118.667

107.267 104-51-8 n-Butylbenzene 0.067 0.059 0.040 22.570

107.387 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.396 0.341 0.235 133.245

107.644 135-01-3 1,2-Diethylbenzene 0.061 0.053 0.036 20.540

108.236 1074-17-5 1-Methyl-2-n-propylbenzene 0.137 0.119 0.081 46.093

109.084 1758-88-9 1,4,Dimethyl-2-ethylbenzene 0.325 0.280 0.193 109.194

109.244 874-41-9 1,3-Dimethyl-4-ethylbenzene 0.361 0.312 0.214 121.545

109.748 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.890 0.770 0.528 299.351

110.288 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.451 0.384 0.268 151.731

111.197 1-Methyl-4-t-butylbenzene 0.077 0.068 0.041 25.643

111.418 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.306 0.259 0.181 102.803

111.868 4218-48-8 1-Ethyl-4-i-propylbenzene 0.068 0.058 0.037 22.807

112.083 C11 - Aromatic - 1 0.007 0.006 0.004 2.456

112.356 1,2,4,5-Tetramethylbenzene 0.739 0.630 0.439 248.541

112.623 527-53-7 1,2,3,5-Tetramethylbenzene 1.011 0.860 0.600 340.155

113.757 C11 - Aromatic - 3 0.116 0.098 0.062 38.766

114.073 1,2-Di-i-propylbenzene 0.115 0.097 0.056 38.230

114.288 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.165 0.140 0.088 55.136

114.443 C11 - Aromatic - 4 0.091 0.077 0.049 30.433

114.848 5161-04-6 Benzene, 1-methyl-4-(2-methylpropyl)-0.098 0.084 0.053 32.973

115.260 538-68-1 n-Pentylbenzene 0.039 0.033 0.021 13.066

115.487 tert-Pentylbenzene 0.172 0.146 0.092 57.548

115.800 577-55-9 1-Methyl-2-n-butylbenzene 0.077 0.066 0.041 25.841

115.909 C11 - Aromatic - 7 0.095 0.084 0.051 31.740

116.370 100-18-5 1,4-Di-i-propylbenzene 0.149 0.127 0.073 49.736

117.593 7364-19-4 1t-Butyl-4-ethylbenzene 0.023 0.020 0.011 7.679

117.895 1,3-Di-n-propylbenzene 0.125 0.107 0.062 41.855

118.006 C11 - Aromatic - 11 0.071 0.063 0.038 23.710

118.559 C11 - Aromatic - 12 0.047 0.042 0.025 15.884

119.189 C11 - Aromatic - 13 0.007 0.007 0.004 2.459

119.487 102-25-0 1,3,5-Triethylbenzene 0.012 0.010 0.006 4.107

120.146 C12 - Aromatic - 1 0.006 0.005 0.003 2.105

Naphthalenes 116.815 91-20-3 Naphthalene 0.320 0.237 0.199 112.847

123.440 91-57-6 2-Methylnaphthalene 0.010 0.007 0.006 3.469

124.306 90-12-0 1-Methylnaphthalene 0.005 0.004 0.003 1.842

Naphtheno/Olefino-Benzs 113.949 874-35-1 5-Methylindan 0.317 0.269 0.191 106.484

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C-567
Hydrocarbon Expert V4.7 Fri Aug 27 13:48:42 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91330 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91330

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Naphtheno/Olefino-Benzs 114.946 824-63-5 2-Methylindan 0.310 0.264 0.187 104.407

Indenes 105.047 Indan 0.248 0.195 0.167 85.272

105.643 Indene 0.460 0.362 0.310 158.236

109.397 2-Methylindan 0.100 0.079 0.060 34.463

114.698 824-22-6 4-Methylindan 0.424 0.360 0.255 142.501

117.008 4,7-Dimethyl Indane 0.014 0.011 0.007 4.651

117.253 1,1-Dimethyl Indane 0.049 0.039 0.027 16.938

117.415 Dimethyl Indane - 1 0.020 0.016 0.011 6.967

117.733 Dimethyl Indane - 2 0.007 0.006 0.004 2.412

Naphthenes

Mono-Naphthenes 27.606 287-92-3 Cyclopentane 0.313 0.318 0.355 100.758

40.670 96-37-7 Methylcyclopentane 0.740 0.748 0.700 238.146

47.553 110-82-7 Cyclohexane 0.069 0.067 0.065 22.211

53.354 1759-58-6 1t,3-Dimethylcyclopentane 0.097 0.098 0.078 31.087

53.940 2532-58-3 1c,3-Dimethylcyclopentane 0.064 0.065 0.052 20.739

54.566 822-50-4 1t,2-Dimethylcyclopentane 0.059 0.059 0.048 18.891

55.604 C7 - MonoNaph - 1 0.014 0.013 0.010 4.429

59.65316491-15-9 Cyclopentene, 1,5-dimethyl- 0.019 0.019 0.015 6.028

61.503 108-87-2 Methylcyclohexane 0.045 0.044 0.037 14.529

101.551 1678-98-4 i-Butylcyclohexane 0.007 0.006 0.004 2.107

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.621 115-11-7 Isobutene 0.016 0.020 0.022 5.023

9.663 106-98-9 Butene-1 0.017 0.022 0.025 5.591

10.509 624-64-6 t-Butene-2 0.072 0.090 0.102 23.066

11.251 590-18-1 c-Butene-2 0.085 0.103 0.120 27.303

16.728 109-67-1 Pentene-1 0.331 0.392 0.376 106.701

19.232 646-04-8 t-Pentene-2 0.843 0.985 0.958 271.448

20.266 627-20-3 c-Pentene-2 0.463 0.534 0.525 148.936

33.454 592-41-6 Hexene-1 0.160 0.179 0.152 51.582

36.43913269-52-8 t-Hexene-3 0.263 0.292 0.249 84.733

36.918 4050-45-7 t-Hexene-2 0.406 0.450 0.384 130.707

38.745 7688-21-3 c-Hexene-2 0.214 0.235 0.203 69.017

55.470 592-76-7 Heptene-1 0.014 0.015 0.011 4.427

57.33314686-14-7 t-Heptene-3 0.032 0.035 0.026 10.417

58.276 7642-10-6 c-Heptene-3 0.026 0.028 0.021 8.302

59.17614686-13-6 t-Heptene-2 0.012 0.013 0.010 3.954

110.907 693-61-8 2-Undecene, (E)- 0.035 0.036 0.020 11.152

Iso-Olefins 13.451 563-45-1 3-Methylbutene-1 0.190 0.230 0.216 61.273

17.580 563-46-2 2-Methylbutene-1 0.504 0.586 0.572 162.173

20.944 513-35-9 2-Methylbutene-2 1.037 1.185 1.177 333.713

29.204 691-38-3 4-Methyl-c-pentene-2 0.045 0.050 0.042 14.401

29.850 674-76-0 4-Methyl-t-pentene-2 0.131 0.147 0.124 42.030

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C-568
Hydrocarbon Expert V4.7 Fri Aug 27 13:48:42 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91330 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91330

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Iso-Olefins 33.230 763-29-1 2-Methylpentene-1 0.224 0.248 0.212 72.191

35.641 760-21-4 2-Ethylbutene-1 0.072 0.079 0.068 23.300

37.408 625-27-4 2-Methylpentene-2 0.341 0.374 0.323 109.806

37.823 922-62-3 3-Methyl-c-pentene-2 0.264 0.286 0.250 84.946

40.091 3404-73-7 3,3-Dimethylpentene-1 0.311 0.335 0.252 100.051

42.534 594-56-9 2,3,3-Trimethylbutene-1 0.009 0.010 0.007 2.897

46.643 3404-61-3 3-Methylhexene-1 0.016 0.018 0.013 5.217

47.229 3524-73-0 5-Methylhexene-1 0.023 0.025 0.018 7.340

49.27415840-60-5 2-Methyl-c-hexene-3 0.041 0.044 0.033 13.058

49.621 3769-23-1 4-Methylhexene-1 0.011 0.012 0.009 3.672

50.268 3404-55-5 4-Methyl-t/c-hexene-2 0.051 0.055 0.042 16.512

54.843 C7 - Iso-Olefin - 2 0.023 0.024 0.018 7.276

56.803 4914-89-0 3-Methyl-c-hexene-3 0.014 0.015 0.011 4.505

57.685 6094-02-6 2-Methylhexene-1 0.058 0.063 0.047 18.603

58.550 2738-19-4 2-Methyl-2-hexene 0.026 0.028 0.021 8.482

58.79410574-36-4 3-Methyl-c-hexene-2 0.020 0.021 0.016 6.457

60.07820710-38-8 3-Methyl-t-hexene-2 0.015 0.016 0.012 4.946

60.862 4914-91-4 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.014 0.011 4.178

Naphtheno-Olefins 22.535 1574-41-0 1,3-Cyclopentadiene 0.007 0.008 0.008 2.314

25.740 142-29-0 Cyclopentene 0.197 0.193 0.230 65.328

37.040 1120-62-3 3-Methylcyclopentene 0.099 0.098 0.096 31.759

44.495 7459-71-4 3,5-Dimethylcyclopentene 0.013 0.012 0.011 4.125

45.836 693-89-0 1-Methylcyclopentene 0.362 0.351 0.351 119.252

51.153 110-83-8 Cyclohexene 0.045 0.042 0.044 14.542

Di-Olefins 18.625 78-79-5 2-Methyl-1,3-Butadiene 0.010 0.012 0.012 3.456

21.270 2004-70-8 1t,3-Pentadiene 0.016 0.018 0.018 5.211

45.429 1528-30-9 C6-Diolefin-1 0.015 0.015 0.015 4.875

Oxygenates 13.111 64-17-5 Ethanol 16.311 15.650 28.202 2162.315

26.904 71-23-8 n-Propanol 0.075 0.071 0.100 16.972

48.058 71-36-3 n-Butanol 0.056 0.053 0.060 13.663

Unidentified 19.879 Unidentified 0.006 0.007 0.007 2.292

26.995 Unidentified 0.059 0.067 0.056 23.426

28.734 Unidentified 0.053 0.054 0.048 20.912

50.841 Unidentified 0.020 0.022 0.017 7.883

63.365 Unidentified 0.045 0.047 0.032 17.677

100.354 Unidentified 0.020 0.015 0.010 7.865

100.488 Unidentified 0.059 0.060 0.030 23.427

101.166 Unidentified 0.042 0.046 0.024 16.645

101.288 Unidentified 0.025 0.026 0.014 9.938

102.902 Unidentified 0.044 0.039 0.026 17.297

103.200 Unidentified 0.019 0.019 0.010 7.375

108.084 Unidentified 0.052 0.053 0.027 20.644

108.358 Unidentified 0.061 0.062 0.031 23.957

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C-569
Hydrocarbon Expert V4.7 Fri Aug 27 13:48:42 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91330 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91330

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Unidentified 108.439 Unidentified 0.056 0.056 0.028 21.899

108.747 Unidentified 0.152 0.154 0.077 59.856

109.172 Unidentified 0.403 0.347 0.239 158.793

110.712 Unidentified 0.013 0.012 0.007 4.976

111.042 Unidentified 0.046 0.047 0.026 17.953

111.976 Unidentified 0.034 0.029 0.018 13.307

112.813 Unidentified 0.009 0.007 0.005 3.466

112.962 Unidentified 0.011 0.010 0.007 4.451

113.486 Unidentified 0.040 0.041 0.019 15.583

115.146 Unidentified 0.030 0.030 0.014 11.648

130.001 Unidentified 0.003 0.002 0.001 1.142

Plus

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C-570
Hydrocarbon Expert V4.7 Fri Aug 27 13:48:42 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91330 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91330

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF

20.0 15.0 10.0 5.0 0.0

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

Ethanol

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

Unidentified

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

1,3-Cyclopentadiene

2,2-Dimethylbutane

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C-571
Hydrocarbon Expert V4.7 Fri Aug 27 13:48:42 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91330 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91330

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

n-Propanol Unidentified

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

2-Ethylbutene-1 n-Hexane

t-Hexene-3

t-Hexene-2 3-Methylcyclopentene

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane 2,3,3-Trimethylbutene-1

3,5-Dimethylcyclopentene

C6-Diolefin-1 Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1

Cyclohexane

n-Butanol

2-Methyl-c-hexene-3

4-Methylhexene-1

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C-572
Hydrocarbon Expert V4.7 Fri Aug 27 13:48:42 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91330 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91330

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF

70.0 65.0 60.0 55.0 50.0

4-Methyl-t/c-hexene-2

2-Methylhexane Unidentified Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane C7 - Iso-Olefin - 2

C7 - MonoNaph - 1 Heptene-1

3-Methyl-c-hexene-3

t-Heptene-3

2-Methylhexene-1

n-Heptane c-Heptene-3 2-Methyl-2-hexene 3-Methyl-c-hexene-2

t-Heptene-2

Cyclopentene, 1,5-dimethyl3-Methyl-t-hexene-2

2-Pentene, 3,4-dimethyl-, (Z)-

Methylcyclohexane

Unidentified

Toluene

2-Methylheptane 4-Methylheptane

3-Methylheptane

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C-573
Hydrocarbon Expert V4.7 Fri Aug 27 13:48:42 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91330 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91330

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF

95.0 90.0 85.0 80.0 75.0

n-Octane

Ethylbenzene

m-Xylene p-Xylene

o-Xylene

n-Nonane

i-Propylbenzene

2,4-Dimethyloctane

n-Propylbenzene

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

5-Methylnonane 4-Methylnonane 2,2,6-Trimethyloctane 1-Methyl-2-ethylbenzene 3-Ethyloctane

3-Methylnonane

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C-574
Hydrocarbon Expert V4.7 Fri Aug 27 13:48:42 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91330 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91330

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified

C11-Isoparaffin-2 1,2,4-Trimethylbenzene Unidentified

i-Butylcyclohexane

3-Ethyl-3-methylheptane i-Butylbenzene n-Decane Unidentified Unidentified

1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene C11 Isoparaffin-4 1-Methyl-4-i-propylbenzene

Indan

Indene

C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene

n-Butylbenzene 1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

Unidentified 1-Methyl-2-n-propylbenzene

C11- Isoparaffin-11 Unidentified

1,4,Dimethyl-2-ethylbenzene 1,3-Dimethyl-4-ethylbenzene Unidentified 2-Methylindan

1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

Unidentified 2-Undecene, (E)- Unidentified 1-Methyl-4-t-butylbenzene 1,2-Dimethyl-3-ethylbenzene n-Undecane Unidentified 1-Ethyl-4-i-propylbenzene C11 - Aromatic - 1 1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene Unidentified

C12 - IsoParaffin - 1

Unidentified C11 - Aromatic - 3 5-Methylindan 1,2-Di-i-propylbenzene

C11 - Aromatic - 4 1-methyl-4-(1-methylpropyl)be

4-Methylindan Benzene, 1-methyl-4-(2-methylpropyl)- 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene 1-Methyl-2-n-butylbenzene C11 - Aromatic - 7

C12 - IsoParaffin - 4 1,4-Di-i-propylbenzene

Naphthalene 4,7-Dimethyl Indane 1,1-Dimethyl Indane Dimethyl Indane - 1

Dimethyl Indane - 2 1t-Butyl-4-ethylbenzene

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

C11 - Aromatic - 12

C11 - Aromatic - 13 1,3,5-Triethylbenzene

C12 - Aromatic - 1

2-Methylnaphthalene

1-Methylnaphthalene

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C-575
Hydrocarbon Expert V4.7 Fri Aug 27 13:48:42 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF 25-Aug-10, 15:57:03

Sample: ODDB-91330 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91330

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000012.D\SIG2000012_FID2_B.CDF

145.0 140.0 135.0 130.0 125.0

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C-576
Hydrocarbon Expert V4.7 Fri Aug 27 13:56:25 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91331 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91331

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 4.083 4.804 4.540

I-Paraffins 42.647 45.728 33.265

Aromatics 22.281 18.909 17.099

Mono-Aromatics 20.011 17.143 15.521

Naphthalenes 0.136 0.099 0.088

Naphtheno/Olefino-Benzs 0.173 0.145 0.110

Indenes 1.961 1.522 1.380

Naphthenes 1.643 1.617 1.575

Mono-Naphthenes 1.643 1.617 1.575

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 7.614 8.382 8.395

n-Olefins 3.191 3.600 3.619

Iso-Olefins 3.641 4.026 3.921

Naphtheno-Olefins 0.739 0.710 0.805

Di-Olefins 0.043 0.046 0.050

Oxygenates 16.687 15.756 30.495

Unidentified 5.045 4.805 4.631

Plus 0.000 0.000 0.000

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C-577
Hydrocarbon Expert V4.7 Fri Aug 27 13:56:25 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91331 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91331

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C2 16.550 15.628 30.318

C3 0.079 0.074 0.111

C4 1.683 2.133 2.436

C5 9.089 10.633 10.772

C6 9.900 10.643 9.871

C7 8.867 8.457 7.866

C8 26.247 26.680 19.665

C9 8.277 7.632 5.683

C10 11.654 10.790 7.227

C11 2.439 2.378 1.332

C12 0.171 0.149 0.088

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C-578
Hydrocarbon Expert V4.7 Fri Aug 27 13:56:25 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91331 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91331

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C4 1.395 1.796 2.025

C5 0.876 1.042 1.025

C6 0.963 1.088 0.943

C7 0.112 0.122 0.094

C8 0.026 0.028 0.020

C9 0.279 0.290 0.184

C10 0.303 0.309 0.180

C11 0.124 0.124 0.067

C12 0.005 0.005 0.003

I-Paraffins C4 0.021 0.028 0.031

C5 4.282 5.150 5.008

C6 4.383 4.957 4.292

C7 2.569 2.824 2.163

C8 21.317 22.433 15.749

C9 2.671 2.804 1.758

C10 5.502 5.627 3.238

C11 1.868 1.870 1.008

C12 0.034 0.034 0.017

Mono-Aromatics C6 0.720 0.610 0.778

C7 5.106 4.388 4.676

C8 4.880 4.197 3.879

C9 5.060 4.326 3.553

C10 3.757 3.210 2.362

C11 0.363 0.307 0.207

C12 0.125 0.105 0.065

Naphthalenes C10 0.117 0.085 0.077

C11 0.019 0.014 0.011

Naphtheno/Olefino-Benzs C10 0.173 0.145 0.110

Indenes C9 0.223 0.172 0.159

C10 1.721 1.337 1.211

C11 0.011 0.009 0.007

C12 0.006 0.005 0.004

Mono-Naphthenes C5 0.099 0.098 0.119

C6 1.107 1.094 1.110

C7 0.304 0.301 0.262

C8 0.014 0.013 0.010

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C-579
Hydrocarbon Expert V4.7 Fri Aug 27 13:56:25 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91331 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91331

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Mono-Naphthenes C9 0.043 0.039 0.029

C10 0.076 0.071 0.046

n-Olefins C4 0.209 0.255 0.314

C5 1.745 2.004 2.100

C6 1.083 1.180 1.086

C7 0.101 0.107 0.087

C11 0.054 0.054 0.032

Iso-Olefins C5 1.845 2.099 2.220

C6 1.120 1.212 1.123

C7 0.661 0.700 0.568

C8 0.010 0.010 0.007

C10 0.005 0.006 0.003

Naphtheno-Olefins C5 0.215 0.209 0.267

C6 0.524 0.501 0.538

Di-Olefins C5 0.028 0.030 0.034

C7 0.016 0.016 0.016

Oxygenates C2 16.550 15.628 30.318

C3 0.079 0.074 0.111

C4 0.058 0.054 0.066

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C-580
Hydrocarbon Expert V4.7 Fri Aug 27 13:56:25 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91331 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91331

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 23.97 23.13

5% 81.07 80.38

10% 100.74 97.08

15% 144.48 137.87

20% 168.76 154.06

25% 172.53 172.35

30% 172.86 172.69

35% 173.18 173.04

40% 193.37 176.58

45% 209.85 209.42

50% 228.40 210.31

55% 230.67 229.99

60% 235.00 232.43

65% 238.04 236.99

70% 261.54 243.44

75% 291.66 281.24

80% 326.97 320.72

85% 334.28 332.34

90% 352.22 352.22

95% 363.20 363.20

FBP 402.05 388.39

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C-581
Hydrocarbon Expert V4.7 Fri Aug 27 13:56:25 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91331 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91331

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 8.806 75-28-5 I4 i-Butane 0.021 0.028 0.031 5.320

2 9.619 115-11-7 K4 Isobutene 0.017 0.022 0.026 4.527

3 9.661 106-98-9 K4 Butene-1 0.019 0.024 0.029 5.030

4 10.020 106-97-8 P4 n-Butane 1.395 1.796 2.025 348.622

5 10.506 624-64-6 K4 t-Butene-2 0.079 0.097 0.119 20.405

6 10.634 463-82-1 I5 2,2-Dimethylpropane 0.016 0.020 0.018 3.956

7 11.247 590-18-1 K4 c-Butene-2 0.093 0.112 0.140 24.087

8 13.087 64-17-5 X2 Ethanol 16.550 15.628 30.318 1763.987

9 13.448 563-45-1 C5 3-Methylbutene-1 0.205 0.244 0.247 53.090

10 15.074 78-78-4 I5 i-Pentane 4.266 5.130 4.990 1073.609

11 16.726 109-67-1 K5 Pentene-1 0.355 0.413 0.427 91.857

12 17.578 563-46-2 C5 2-Methylbutene-1 0.538 0.617 0.648 139.330

13 18.110 109-66-0 P5 n-Pentane 0.876 1.042 1.025 220.468

14 18.624 78-79-5 E5 2-Methyl-1,3-Butadiene 0.011 0.012 0.014 2.981

15 19.230 646-04-8 K5 t-Pentene-2 0.898 1.032 1.081 232.434

16 19.876 ? Unidentified 0.006 0.007 0.007 1.963

17 20.264 627-20-3 K5 c-Pentene-2 0.492 0.559 0.592 127.403

18 20.942 513-35-9 C5 2-Methylbutene-2 1.101 1.239 1.325 285.046

19 21.266 2004-70-8 E5 1t,3-Pentadiene 0.016 0.018 0.020 4.394

20 22.532 1574-41-0 B5 1,3-Cyclopentadiene 0.007 0.008 0.009 1.969

21 23.105 75-83-2 I6 2,2-Dimethylbutane 0.029 0.033 0.028 7.201

22 25.738 142-29-0 B5 Cyclopentene 0.208 0.201 0.258 55.399

23 26.901 71-23-8 X3 n-Propanol 0.079 0.074 0.111 14.373

24 26.992 ? Unidentified 0.062 0.069 0.062 19.690

25 27.606 287-92-3 M5 Cyclopentane 0.099 0.098 0.119 25.503

26 28.339 79-29-8 I6 2,3-Dimethylbutane 1.335 1.504 1.308 337.344

27 28.734 ? Unidentified 0.056 0.056 0.053 17.614

28 29.192 691-38-3 C6 4-Methyl-c-pentene-2 0.048 0.053 0.048 12.495

29 29.415 107-83-5 I6 2-Methylpentane 1.825 2.082 1.787 461.124

30 29.842 674-76-0 C6 4-Methyl-t-pentene-2 0.137 0.152 0.138 35.495

31 32.065 96-14-0 I6 3-Methylpentane 1.194 1.339 1.169 301.639

32 33.229 763-29-1 C6 2-Methylpentene-1 0.234 0.254 0.234 60.522

33 33.453 592-41-6 K6 Hexene-1 0.167 0.183 0.167 43.147

34 35.642 760-21-4 C6 2-Ethylbutene-1 0.071 0.076 0.071 18.449

35 35.804 110-54-3 P6 n-Hexane 0.963 1.088 0.943 243.400

36 36.44113269-52-8 K6 t-Hexene-3 0.274 0.299 0.274 70.847

37 36.916 4050-45-7 K6 t-Hexene-2 0.421 0.459 0.422 108.872

38 37.041 1120-62-3 B6 3-Methylcyclopentene 0.104 0.101 0.107 26.877

39 37.409 625-27-4 C6 2-Methylpentene-2 0.355 0.383 0.356 91.931

40 37.823 922-62-3 C6 3-Methyl-c-pentene-2 0.274 0.293 0.275 71.033

41 38.745 7688-21-3 K6 c-Hexene-2 0.222 0.239 0.223 57.500

42 40.088 3404-73-7 C7 3,3-Dimethylpentene-1 0.322 0.342 0.277 83.413

43 40.669 96-37-7 M6 Methylcyclopentane 0.891 0.887 0.893 230.581

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C-582
Hydrocarbon Expert V4.7 Fri Aug 27 13:56:25 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91331 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91331

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 42.235 108-08-7 I7 2,4-Dimethylpentane 1.014 1.123 0.854 257.280

45 42.536 594-56-9 C7 2,3,3-Trimethylbutene-1 0.014 0.015 0.012 3.753

46 42.782 464-06-2 I7 2,2,3-Trimethylbutane 0.067 0.073 0.057 17.116

47 45.429 1528-30-9 E7 C6-Diolefin-1 0.016 0.016 0.016 4.066

48 45.638 71-42-3 Q6 Benzene 0.720 0.610 0.778 200.638

49 45.835 693-89-0 B6 1-Methylcyclopentene 0.374 0.357 0.384 99.075

50 46.641 3404-61-3 C7 3-Methylhexene-1 0.016 0.017 0.014 4.230

51 47.232 3524-73-0 C7 5-Methylhexene-1 0.030 0.032 0.025 7.664

52 47.554 110-82-7 M6 Cyclohexane 0.216 0.207 0.217 56.017

53 48.061 71-36-3 X4 n-Butanol 0.058 0.054 0.066 11.331

54 49.27515840-60-5 C7 2-Methyl-c-hexene-3 0.041 0.044 0.036 10.725

55 49.625 3769-23-1 C7 4-Methylhexene-1 0.012 0.013 0.010 3.119

56 50.270 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.052 0.055 0.045 13.559

57 50.674 591-76-4 I7 2-Methylhexane 1.123 1.233 0.946 284.818

58 51.155 110-83-8 B6 Cyclohexene 0.046 0.042 0.047 11.959

59 52.494 589-34-4 I7 3-Methylhexane 0.364 0.395 0.307 92.357

60 53.356 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.101 0.100 0.086 26.025

61 53.942 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.068 0.068 0.058 17.525

62 54.568 822-50-4 M7 1t,2-Dimethylcyclopentane 0.066 0.065 0.057 17.051

63 54.881 C7 C7 - Iso-Olefin - 2 0.023 0.024 0.020 6.017

64 55.204 540-84-1 I8 2,2,4-Trimethylpentane 7.529 8.108 5.563 1913.792

65 55.476 592-76-7 K7 Heptene-1 0.030 0.032 0.025 7.655

66 56.806 4914-89-0 C7 3-Methyl-c-hexene-3 0.014 0.015 0.012 3.690

67 57.33514686-14-7 K7 t-Heptene-3 0.033 0.035 0.028 8.520

68 57.686 6094-02-6 C7 2-Methylhexene-1 0.059 0.063 0.051 15.271

69 58.056 142-82-5 P7 n-Heptane 0.112 0.122 0.094 28.296

70 58.277 7642-10-6 K7 c-Heptene-3 0.026 0.028 0.022 6.743

71 58.550 2738-19-4 C7 2-Methyl-2-hexene 0.027 0.028 0.023 6.901

72 58.79510574-36-4 C7 3-Methyl-c-hexene-2 0.020 0.021 0.017 5.247

73 59.17814686-13-6 K7 t-Heptene-2 0.012 0.013 0.010 3.158

74 59.65316491-15-9 M7 Cyclopentene, 1,5-dimethyl- 0.019 0.018 0.016 4.821

75 60.07820710-38-8 C7 3-Methyl-t-hexene-2 0.015 0.016 0.013 3.970

76 60.862 4914-91-4 C7 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.014 0.011 3.439

77 61.506 108-87-2 M7 Methylcyclohexane 0.052 0.050 0.044 13.334

78 63.373 ? Unidentified 0.044 0.046 0.034 14.036

79 64.954 564-02-3 I8 2,2,3-Trimethylpentane 0.564 0.587 0.417 143.318

80 65.183 592-13-2 I8 2,5-Dimethylhexane 1.172 1.260 0.866 298.008

81 65.522 589-43-5 I8 2,4-Dimethylhexane 1.022 1.087 0.755 259.674

82 68.511 565-75-3 I8 2,3,4-Trimethylpentane 4.452 4.613 3.289 1131.566

83 69.030 108-88-3 Q7 Toluene 5.106 4.388 4.676 1407.813

84 69.192 560-21-4 I8 2,3,3-Trimethylpentane 5.238 5.374 3.870 1331.407

85 70.802 584-94-1 I8 2,3-Dimethylhexane 1.110 1.161 0.820 282.159

86 72.047 592-27-8 I8 2-Methylheptane 0.057 0.061 0.042 14.536

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C-583
Hydrocarbon Expert V4.7 Fri Aug 27 13:56:25 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91331 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91331

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 72.320 589-53-7 I8 4-Methylheptane 0.122 0.129 0.090 31.045

88 72.451 ? Unidentified 0.090 0.093 0.066 28.487

89 73.362 589-81-1 I8 3-Methylheptane 0.051 0.053 0.037 12.876

90 75.263 3522-94-9 I9 2,2,5-Trimethylhexane 2.047 2.156 1.347 521.317

91 76.237 ? Unidentified 0.015 0.015 0.012 4.900

92 77.870 111-65-9 P8 n-Octane 0.026 0.028 0.020 6.728

93 78.822 ? Unidentified 0.045 0.044 0.034 14.354

94 80.354 1069-53-0 I9 2,3,5-Trimethylhexane 0.319 0.329 0.210 81.284

95 81.520 1071-26-7 I9 2,4-Dimethylheptane 0.043 0.045 0.028 11.027

96 82.166 1678-91-7 M8 Ethylcyclohexane 0.014 0.013 0.010 3.605

97 82.476 1072-05-5 I9 2,6-Dimethylheptane 0.057 0.060 0.037 14.420

98 83.407 I9 2,5-Dimethylheptane 0.138 0.143 0.091 35.048

99 84.730 100-41-4 Q8 Ethylbenzene 0.898 0.771 0.714 245.642

100 84.900 ? Unidentified 0.021 0.021 0.014 6.649

101 85.146 ? Unidentified 0.022 0.021 0.015 6.955

102 85.951 108-38-3 Q8 m-Xylene 2.242 1.932 1.782 613.395

103 86.099 106-42-3 Q8 p-Xylene 1.019 0.881 0.810 278.756

104 86.231 ? Unidentified 0.044 0.045 0.029 13.865

105 86.489 C8 C9-IsoOlefin-3 0.010 0.010 0.007 2.627

106 86.597 ? Unidentified 0.009 0.009 0.006 2.721

107 87.274 2216-34-4 I9 4-Methyloctane 0.017 0.017 0.011 4.248

108 87.406 3221-61-2 I9 2-Methyloctane 0.024 0.025 0.016 6.186

109 88.269 2216-33-3 I9 3-Methyloctane 0.027 0.028 0.018 6.814

110 88.745 ? Unidentified 0.102 0.111 0.068 32.383

111 88.927 95-47-6 Q8 o-Xylene 0.722 0.611 0.574 197.643

112 89.323 I10 C10 - IsoParaffin - 1 0.333 0.341 0.197 84.964

113 89.911 M9 trans-1,3-Diethylcyclopentane 0.013 0.011 0.009 3.649

114 90.16614720-74-2 I10 2,2,4-trimethylheptane 0.238 0.244 0.141 60.744

115 91.726 111-84-2 P9 n-Nonane 0.279 0.290 0.184 71.166

116 92.334 4926-90-3 M9 1,1-Methylethylcyclohexane 0.025 0.023 0.016 6.368

117 93.094 98-82-8 Q9 i-Propylbenzene 0.029 0.025 0.020 7.776

118 93.273 ? Unidentified 0.012 0.012 0.008 3.868

119 93.273 ? Unidentified 0.012 0.013 0.007 3.868

120 93.273 ? Unidentified 0.012 0.009 0.007 3.868

121 93.385 696-29-7 M9 1-Methyl-2-propyl-cyclopentan 0.005 0.005 0.003 1.355

122 93.385 C10 C10-IsoOlefin-4 0.005 0.006 0.003 1.355

123 93.385 I10 C10-isoparaffin-x 0.000 0.000 0.000 1.355

124 93.842 ? Unidentified 0.173 0.178 0.103 54.945

125 94.06315869-87-1 I10 2,2-Dimethyloctane 0.074 0.076 0.044 18.961

126 94.525 ? Unidentified 0.019 0.014 1.612 6.055

127 94.525 ? Unidentified 0.019 0.020 0.011 6.055

128 94.724 ? Unidentified 0.023 0.021 0.015 7.282

129 94.86315869-89-3 I10 2,5-Dimethyloctane 0.108 0.110 0.064 27.484

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C-584
Hydrocarbon Expert V4.7 Fri Aug 27 13:56:25 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91331 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91331

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 95.068 I10 C10 - IsoParaffin - 2 0.019 0.019 0.011 4.821

131 95.331 2040-95-1 I10 2,7-Dimethyloctane 0.061 0.062 0.036 15.533

132 95.508 2051-30-1 I10 2,4-Dimethyloctane 0.232 0.238 0.138 59.220

133 95.894 I10 2,6-Dimethyloctane 0.092 0.094 0.055 23.570

134 96.061 I10 C10 Isoparaffin -1 0.010 0.010 0.006 2.525

135 96.351 ? Unidentified 0.008 0.008 0.005 2.424

136 96.555 103-65-1 Q9 n-Propylbenzene 0.295 0.255 0.207 80.142

137 96.752 I10 3-Methyl-5-ethylheptane 0.009 0.009 0.005 2.338

138 97.400 620-14-4 Q9 1-Methyl-3-ethylbenzene 0.996 0.858 0.699 270.675

139 97.634 622-96-8 Q9 1-Methyl-4-ethylbenzene 0.456 0.395 0.321 124.111

140 98.259 108-67-8 Q9 1,3,5-Trimethylbenzene 0.672 0.579 0.472 182.761

141 98.72415869-85-9 I10 5-Methylnonane 0.031 0.032 0.018 7.957

142 98.91417301-94-8 I10 4-Methylnonane 0.066 0.067 0.039 16.814

143 99.135 I10 2,2,6-Trimethyloctane 3.660 3.754 2.171 934.022

144 99.345 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.361 0.305 0.253 98.153

145 99.564 5881-17-4 I10 3-Ethyloctane 0.009 0.009 0.005 2.360

146 99.707 ? Unidentified 0.012 0.012 0.007 3.720

147 99.888 5911-04-6 I10 3-Methylnonane 0.071 0.072 0.042 18.184

148 100.068 ? Unidentified 0.017 0.018 0.010 5.267

149 100.354 ? Unidentified 0.215 0.160 0.116 68.306

150 100.488 ? Unidentified 0.577 0.578 0.312 183.068

151 100.702 I11 C11-Isoparaffin-2 0.311 0.311 0.168 79.444

152 100.979 95-63-6 Q9 1,2,4-Trimethylbenzene 1.910 1.625 1.341 519.303

153 101.168 ? Unidentified 0.358 0.380 0.215 113.423

154 101.290 ? Unidentified 0.209 0.213 0.124 66.388

155 101.550 1678-98-4 M10 i-Butylcyclohexane 0.065 0.061 0.039 16.878

156 102.195 ? Unidentified 0.023 0.021 0.014 7.253

157 102.33917302-01-1 I10 3-Ethyl-3-methylheptane 0.489 0.489 0.264 124.873

158 102.546 ? Unidentified 0.123 0.108 0.077 39.065

159 102.688 ? Unidentified 0.281 0.281 0.152 89.115

160 102.805 124-18-5 P10 n-Decane 0.303 0.309 0.180 77.288

161 103.199 ? Unidentified 0.122 0.122 0.066 38.704

162 103.687 ? Unidentified 0.018 0.015 0.013 5.691

163 103.853 526-73-8 Q9 1,2,3-Trimethylbenzene 0.342 0.285 0.240 92.961

164 104.195 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.045 0.039 0.028 12.146

165 104.412 I11 C11 Isoparaffin-4 0.070 0.070 0.038 17.967

166 104.618 99-87-6 Q10 1-Methyl-4-i-propylbenzene 0.347 0.302 0.218 93.954

167 105.048 J9 Indan 0.223 0.172 0.159 61.520

168 105.262 I11 C11-Isoparaffin-5 0.048 0.048 0.026 12.185

169 105.649 J10 Indene 1.481 1.145 1.058 409.309

170 106.064 M10 n-ButylCyclohexane 0.011 0.010 0.007 2.821

171 106.204 ? Unidentified 0.010 0.009 0.006 3.057

172 106.361 I11 C11-Isoparaffin-7 0.537 0.538 0.290 137.170

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C-585
Hydrocarbon Expert V4.7 Fri Aug 27 13:56:25 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91331 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91331

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 106.549 141-93-5 Q10 1,3-Diethylbenzene 0.043 0.037 0.027 11.639

174 106.843 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 1.575 1.363 0.991 426.067

175 107.104 ? Unidentified 0.345 0.298 0.217 109.291

176 107.384 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.120 0.101 0.075 32.393

177 107.619 135-01-3 Q10 1,2-Diethylbenzene 0.115 0.098 0.072 31.144

178 107.898 I11 C11-Isoparaffin-8 0.010 0.010 0.005 2.564

179 108.082 ? Unidentified 0.120 0.120 0.065 37.905

180 108.237 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.051 0.044 0.032 13.838

181 108.354 ? Unidentified 0.135 0.135 0.073 42.788

182 108.436 ? Unidentified 0.106 0.107 0.057 33.726

183 108.566 I11 C11- Isoparaffin-11 0.867 0.869 0.468 221.590

184 108.745 ? Unidentified 0.268 0.268 0.145 84.927

185 108.896 I11 C11- IsoParaffin - 13 0.024 0.025 0.013 6.250

186 109.169 ? Unidentified 0.773 0.657 0.486 245.109

187 109.398 J10 2-Methylindan 0.134 0.104 0.086 37.045

188 109.741 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.288 0.245 0.181 77.768

189 109.868 ? Unidentified 0.036 0.030 0.022 11.326

190 110.286 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.633 0.529 0.398 171.135

191 110.710 ? Unidentified 0.025 0.023 0.013 7.816

192 110.904 693-61-8 K11 2-Undecene, (E)- 0.054 0.054 0.032 13.734

193 111.039 ? Unidentified 0.120 0.121 0.072 38.197

194 111.309 ? Unidentified 0.110 0.096 0.063 34.817

195 111.410 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.062 0.052 0.039 16.741

196 111.698 1120-21-4 P11 n-Undecane 0.124 0.124 0.067 31.591

197 111.861 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.087 0.073 0.050 23.484

198 111.972 ? Unidentified 0.059 0.049 0.033 18.652

199 112.347 Q10 1,2,4,5-Tetramethylbenzene 0.210 0.176 0.132 56.718

200 112.613 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.268 0.224 0.169 72.491

201 112.956 ? Unidentified 0.031 0.026 0.020 9.948

202 113.130 I12 C12 - IsoParaffin - 1 0.026 0.026 0.013 6.726

203 113.483 ? Unidentified 0.034 0.034 0.017 10.663

204 113.609 ? Unidentified 0.012 0.012 0.006 3.772

205 113.811 ? Unidentified 0.056 0.047 0.032 17.887

206 113.944 874-35-1 H10 5-Methylindan 0.089 0.075 0.057 24.087

207 114.069 Q12 1,2-Di-i-propylbenzene 0.033 0.028 0.017 8.818

208 114.284 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.048 0.040 0.028 13.018

209 114.462 Q11 C11 - Aromatic - 4 0.038 0.032 0.021 10.160

210 114.694 824-22-6 J10 4-Methylindan 0.105 0.088 0.067 28.525

211 114.848 5161-04-6 Q11 Benzene, 1-methyl-4-(2-methylpropyl)-0.033 0.028 0.019 8.868

212 114.941 824-63-5 H10 2-Methylindan 0.084 0.070 0.053 22.604

213 115.144 ? Unidentified 0.011 0.009 0.006 3.591

214 115.256 538-68-1 Q11 n-Pentylbenzene 0.015 0.012 0.008 3.959

215 115.485 Q11 tert-Pentylbenzene 0.049 0.041 0.028 13.280

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C-586
Hydrocarbon Expert V4.7 Fri Aug 27 13:56:25 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91331 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91331

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

216 115.798 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.020 0.017 0.011 5.358

217 115.911 Q11 C11 - Aromatic - 7 0.033 0.029 0.019 8.977

218 116.090 ? Unidentified 0.005 0.005 0.003 1.663

219 116.245 I12 C12 - IsoParaffin - 4 0.008 0.008 0.004 2.181

220 116.368 100-18-5 Q12 1,4-Di-i-propylbenzene 0.038 0.032 0.020 10.112

221 116.809 91-20-3 G10 Naphthalene 0.117 0.085 0.077 33.249

222 116.942 ? Unidentified 0.018 0.018 0.009 5.791

223 117.124 ? Unidentified 0.006 0.004 0.003 1.756

224 117.247 J11 1,1-Dimethyl Indane 0.011 0.009 0.007 3.176

225 117.410 J12 Dimethyl Indane - 1 0.006 0.005 0.004 1.731

226 117.594 7364-19-4 Q12 1t-Butyl-4-ethylbenzene 0.010 0.008 0.005 2.586

227 117.893 Q12 1,3-Di-n-propylbenzene 0.038 0.032 0.020 10.157

228 118.004 Q11 C11 - Aromatic - 11 0.021 0.018 0.012 5.675

229 118.409 112-40-3 P12 n-Dodecane 0.005 0.005 0.003 1.356

230 118.558 Q11 C11 - Aromatic - 12 0.019 0.016 0.011 5.033

231 122.671 877-44-1 Q12 1,2,4-Triethylbenzene 0.007 0.006 0.004 1.884

232 123.441 91-57-6 G11 2-Methylnaphthalene 0.013 0.009 0.008 3.636

233 124.307 90-12-0 G11 1-Methylnaphthalene 0.006 0.004 0.003 1.644

234 126.296 ? Unidentified 0.009 0.009 0.004 2.982

235 127.262 ? Unidentified 0.003 0.002 0.002 0.932

236 130.003 ? Unidentified 0.003 0.003 0.002 1.043

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C-587
Hydrocarbon Expert V4.7 Fri Aug 27 13:56:25 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91331 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91331

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 10.020 106-97-8 n-Butane 1.395 1.796 2.025 348.622

18.110 109-66-0 n-Pentane 0.876 1.042 1.025 220.468

35.804 110-54-3 n-Hexane 0.963 1.088 0.943 243.400

58.056 142-82-5 n-Heptane 0.112 0.122 0.094 28.296

77.870 111-65-9 n-Octane 0.026 0.028 0.020 6.728

91.726 111-84-2 n-Nonane 0.279 0.290 0.184 71.166

102.805 124-18-5 n-Decane 0.303 0.309 0.180 77.288

111.698 1120-21-4 n-Undecane 0.124 0.124 0.067 31.591

118.409 112-40-3 n-Dodecane 0.005 0.005 0.003 1.356

I-Paraffins 8.806 75-28-5 i-Butane 0.021 0.028 0.031 5.320

10.634 463-82-1 2,2-Dimethylpropane 0.016 0.020 0.018 3.956

15.074 78-78-4 i-Pentane 4.266 5.130 4.990 1073.609

23.105 75-83-2 2,2-Dimethylbutane 0.029 0.033 0.028 7.201

28.339 79-29-8 2,3-Dimethylbutane 1.335 1.504 1.308 337.344

29.415 107-83-5 2-Methylpentane 1.825 2.082 1.787 461.124

32.065 96-14-0 3-Methylpentane 1.194 1.339 1.169 301.639

42.235 108-08-7 2,4-Dimethylpentane 1.014 1.123 0.854 257.280

42.782 464-06-2 2,2,3-Trimethylbutane 0.067 0.073 0.057 17.116

50.674 591-76-4 2-Methylhexane 1.123 1.233 0.946 284.818

52.494 589-34-4 3-Methylhexane 0.364 0.395 0.307 92.357

55.204 540-84-1 2,2,4-Trimethylpentane 7.529 8.108 5.563 1913.792

64.954 564-02-3 2,2,3-Trimethylpentane 0.564 0.587 0.417 143.318

65.183 592-13-2 2,5-Dimethylhexane 1.172 1.260 0.866 298.008

65.522 589-43-5 2,4-Dimethylhexane 1.022 1.087 0.755 259.674

68.511 565-75-3 2,3,4-Trimethylpentane 4.452 4.613 3.289 1131.566

69.192 560-21-4 2,3,3-Trimethylpentane 5.238 5.374 3.870 1331.407

70.802 584-94-1 2,3-Dimethylhexane 1.110 1.161 0.820 282.159

72.047 592-27-8 2-Methylheptane 0.057 0.061 0.042 14.536

72.320 589-53-7 4-Methylheptane 0.122 0.129 0.090 31.045

73.362 589-81-1 3-Methylheptane 0.051 0.053 0.037 12.876

75.263 3522-94-9 2,2,5-Trimethylhexane 2.047 2.156 1.347 521.317

80.354 1069-53-0 2,3,5-Trimethylhexane 0.319 0.329 0.210 81.284

81.520 1071-26-7 2,4-Dimethylheptane 0.043 0.045 0.028 11.027

82.476 1072-05-5 2,6-Dimethylheptane 0.057 0.060 0.037 14.420

83.407 2,5-Dimethylheptane 0.138 0.143 0.091 35.048

87.274 2216-34-4 4-Methyloctane 0.017 0.017 0.011 4.248

87.406 3221-61-2 2-Methyloctane 0.024 0.025 0.016 6.186

88.269 2216-33-3 3-Methyloctane 0.027 0.028 0.018 6.814

89.323 C10 - IsoParaffin - 1 0.333 0.341 0.197 84.964

90.16614720-74-2 2,2,4-trimethylheptane 0.238 0.244 0.141 60.744

93.385 C10-isoparaffin-x 0.000 0.000 0.000 1.355

94.06315869-87-1 2,2-Dimethyloctane 0.074 0.076 0.044 18.961

94.86315869-89-3 2,5-Dimethyloctane 0.108 0.110 0.064 27.484

95.068 C10 - IsoParaffin - 2 0.019 0.019 0.011 4.821

95.331 2040-95-1 2,7-Dimethyloctane 0.061 0.062 0.036 15.533

95.508 2051-30-1 2,4-Dimethyloctane 0.232 0.238 0.138 59.220

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C-588
Hydrocarbon Expert V4.7 Fri Aug 27 13:56:25 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91331 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91331

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

I-Paraffins 95.894 2,6-Dimethyloctane 0.092 0.094 0.055 23.570

96.061 C10 Isoparaffin -1 0.010 0.010 0.006 2.525

96.752 3-Methyl-5-ethylheptane 0.009 0.009 0.005 2.338

98.72415869-85-9 5-Methylnonane 0.031 0.032 0.018 7.957

98.91417301-94-8 4-Methylnonane 0.066 0.067 0.039 16.814

99.135 2,2,6-Trimethyloctane 3.660 3.754 2.171 934.022

99.564 5881-17-4 3-Ethyloctane 0.009 0.009 0.005 2.360

99.888 5911-04-6 3-Methylnonane 0.071 0.072 0.042 18.184

100.702 C11-Isoparaffin-2 0.311 0.311 0.168 79.444

102.33917302-01-1 3-Ethyl-3-methylheptane 0.489 0.489 0.264 124.873

104.412 C11 Isoparaffin-4 0.070 0.070 0.038 17.967

105.262 C11-Isoparaffin-5 0.048 0.048 0.026 12.185

106.361 C11-Isoparaffin-7 0.537 0.538 0.290 137.170

107.898 C11-Isoparaffin-8 0.010 0.010 0.005 2.564

108.566 C11- Isoparaffin-11 0.867 0.869 0.468 221.590

108.896 C11- IsoParaffin - 13 0.024 0.025 0.013 6.250

113.130 C12 - IsoParaffin - 1 0.026 0.026 0.013 6.726

116.245 C12 - IsoParaffin - 4 0.008 0.008 0.004 2.181

Aromatics

Mono-Aromatics 45.638 71-42-3 Benzene 0.720 0.610 0.778 200.638

69.030 108-88-3 Toluene 5.106 4.388 4.676 1407.813

84.730 100-41-4 Ethylbenzene 0.898 0.771 0.714 245.642

85.951 108-38-3 m-Xylene 2.242 1.932 1.782 613.395

86.099 106-42-3 p-Xylene 1.019 0.881 0.810 278.756

88.927 95-47-6 o-Xylene 0.722 0.611 0.574 197.643

93.094 98-82-8 i-Propylbenzene 0.029 0.025 0.020 7.776

96.555 103-65-1 n-Propylbenzene 0.295 0.255 0.207 80.142

97.400 620-14-4 1-Methyl-3-ethylbenzene 0.996 0.858 0.699 270.675

97.634 622-96-8 1-Methyl-4-ethylbenzene 0.456 0.395 0.321 124.111

98.259 108-67-8 1,3,5-Trimethylbenzene 0.672 0.579 0.472 182.761

99.345 611-14-3 1-Methyl-2-ethylbenzene 0.361 0.305 0.253 98.153

100.979 95-63-6 1,2,4-Trimethylbenzene 1.910 1.625 1.341 519.303

103.853 526-73-8 1,2,3-Trimethylbenzene 0.342 0.285 0.240 92.961

104.195 535-77-3 1-Methyl-3-i-propylbenzene 0.045 0.039 0.028 12.146

104.618 99-87-6 1-Methyl-4-i-propylbenzene 0.347 0.302 0.218 93.954

106.549 141-93-5 1,3-Diethylbenzene 0.043 0.037 0.027 11.639

106.843 1074-43-7 1-Methyl-3-n-propylbenzene 1.575 1.363 0.991 426.067

107.384 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.120 0.101 0.075 32.393

107.619 135-01-3 1,2-Diethylbenzene 0.115 0.098 0.072 31.144

108.237 1074-17-5 1-Methyl-2-n-propylbenzene 0.051 0.044 0.032 13.838

109.741 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.288 0.245 0.181 77.768

110.286 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.633 0.529 0.398 171.135

111.410 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.062 0.052 0.039 16.741

111.861 4218-48-8 1-Ethyl-4-i-propylbenzene 0.087 0.073 0.050 23.484

112.347 1,2,4,5-Tetramethylbenzene 0.210 0.176 0.132 56.718

112.613 527-53-7 1,2,3,5-Tetramethylbenzene 0.268 0.224 0.169 72.491

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C-589
Hydrocarbon Expert V4.7 Fri Aug 27 13:56:25 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91331 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91331

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 114.069 1,2-Di-i-propylbenzene 0.033 0.028 0.017 8.818

114.284 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.048 0.040 0.028 13.018

114.462 C11 - Aromatic - 4 0.038 0.032 0.021 10.160

114.848 5161-04-6 Benzene, 1-methyl-4-(2-methylpropyl)-0.033 0.028 0.019 8.868

115.256 538-68-1 n-Pentylbenzene 0.015 0.012 0.008 3.959

115.485 tert-Pentylbenzene 0.049 0.041 0.028 13.280

115.798 577-55-9 1-Methyl-2-n-butylbenzene 0.020 0.017 0.011 5.358

115.911 C11 - Aromatic - 7 0.033 0.029 0.019 8.977

116.368 100-18-5 1,4-Di-i-propylbenzene 0.038 0.032 0.020 10.112

117.594 7364-19-4 1t-Butyl-4-ethylbenzene 0.010 0.008 0.005 2.586

117.893 1,3-Di-n-propylbenzene 0.038 0.032 0.020 10.157

118.004 C11 - Aromatic - 11 0.021 0.018 0.012 5.675

118.558 C11 - Aromatic - 12 0.019 0.016 0.011 5.033

122.671 877-44-1 1,2,4-Triethylbenzene 0.007 0.006 0.004 1.884

Naphthalenes 116.809 91-20-3 Naphthalene 0.117 0.085 0.077 33.249

123.441 91-57-6 2-Methylnaphthalene 0.013 0.009 0.008 3.636

124.307 90-12-0 1-Methylnaphthalene 0.006 0.004 0.003 1.644

Naphtheno/Olefino-Benzs 113.944 874-35-1 5-Methylindan 0.089 0.075 0.057 24.087

114.941 824-63-5 2-Methylindan 0.084 0.070 0.053 22.604

Indenes 105.048 Indan 0.223 0.172 0.159 61.520

105.649 Indene 1.481 1.145 1.058 409.309

109.398 2-Methylindan 0.134 0.104 0.086 37.045

114.694 824-22-6 4-Methylindan 0.105 0.088 0.067 28.525

117.247 1,1-Dimethyl Indane 0.011 0.009 0.007 3.176

117.410 Dimethyl Indane - 1 0.006 0.005 0.004 1.731

Naphthenes

Mono-Naphthenes 27.606 287-92-3 Cyclopentane 0.099 0.098 0.119 25.503

40.669 96-37-7 Methylcyclopentane 0.891 0.887 0.893 230.581

47.554 110-82-7 Cyclohexane 0.216 0.207 0.217 56.017

53.356 1759-58-6 1t,3-Dimethylcyclopentane 0.101 0.100 0.086 26.025

53.942 2532-58-3 1c,3-Dimethylcyclopentane 0.068 0.068 0.058 17.525

54.568 822-50-4 1t,2-Dimethylcyclopentane 0.066 0.065 0.057 17.051

59.65316491-15-9 Cyclopentene, 1,5-dimethyl- 0.019 0.018 0.016 4.821

61.506 108-87-2 Methylcyclohexane 0.052 0.050 0.044 13.334

82.166 1678-91-7 Ethylcyclohexane 0.014 0.013 0.010 3.605

89.911 trans-1,3-Diethylcyclopentane 0.013 0.011 0.009 3.649

92.334 4926-90-3 1,1-Methylethylcyclohexane 0.025 0.023 0.016 6.368

93.385 696-29-7 1-Methyl-2-propyl-cyclopentan 0.005 0.005 0.003 1.355

101.550 1678-98-4 i-Butylcyclohexane 0.065 0.061 0.039 16.878

106.064 n-ButylCyclohexane 0.011 0.010 0.007 2.821

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.619 115-11-7 Isobutene 0.017 0.022 0.026 4.527

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C-590
Hydrocarbon Expert V4.7 Fri Aug 27 13:56:25 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91331 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91331

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

n-Olefins 9.661 106-98-9 Butene-1 0.019 0.024 0.029 5.030

10.506 624-64-6 t-Butene-2 0.079 0.097 0.119 20.405

11.247 590-18-1 c-Butene-2 0.093 0.112 0.140 24.087

16.726 109-67-1 Pentene-1 0.355 0.413 0.427 91.857

19.230 646-04-8 t-Pentene-2 0.898 1.032 1.081 232.434

20.264 627-20-3 c-Pentene-2 0.492 0.559 0.592 127.403

33.453 592-41-6 Hexene-1 0.167 0.183 0.167 43.147

36.44113269-52-8 t-Hexene-3 0.274 0.299 0.274 70.847

36.916 4050-45-7 t-Hexene-2 0.421 0.459 0.422 108.872

38.745 7688-21-3 c-Hexene-2 0.222 0.239 0.223 57.500

55.476 592-76-7 Heptene-1 0.030 0.032 0.025 7.655

57.33514686-14-7 t-Heptene-3 0.033 0.035 0.028 8.520

58.277 7642-10-6 c-Heptene-3 0.026 0.028 0.022 6.743

59.17814686-13-6 t-Heptene-2 0.012 0.013 0.010 3.158

110.904 693-61-8 2-Undecene, (E)- 0.054 0.054 0.032 13.734

Iso-Olefins 13.448 563-45-1 3-Methylbutene-1 0.205 0.244 0.247 53.090

17.578 563-46-2 2-Methylbutene-1 0.538 0.617 0.648 139.330

20.942 513-35-9 2-Methylbutene-2 1.101 1.239 1.325 285.046

29.192 691-38-3 4-Methyl-c-pentene-2 0.048 0.053 0.048 12.495

29.842 674-76-0 4-Methyl-t-pentene-2 0.137 0.152 0.138 35.495

33.229 763-29-1 2-Methylpentene-1 0.234 0.254 0.234 60.522

35.642 760-21-4 2-Ethylbutene-1 0.071 0.076 0.071 18.449

37.409 625-27-4 2-Methylpentene-2 0.355 0.383 0.356 91.931

37.823 922-62-3 3-Methyl-c-pentene-2 0.274 0.293 0.275 71.033

40.088 3404-73-7 3,3-Dimethylpentene-1 0.322 0.342 0.277 83.413

42.536 594-56-9 2,3,3-Trimethylbutene-1 0.014 0.015 0.012 3.753

46.641 3404-61-3 3-Methylhexene-1 0.016 0.017 0.014 4.230

47.232 3524-73-0 5-Methylhexene-1 0.030 0.032 0.025 7.664

49.27515840-60-5 2-Methyl-c-hexene-3 0.041 0.044 0.036 10.725

49.625 3769-23-1 4-Methylhexene-1 0.012 0.013 0.010 3.119

50.270 3404-55-5 4-Methyl-t/c-hexene-2 0.052 0.055 0.045 13.559

54.881 C7 - Iso-Olefin - 2 0.023 0.024 0.020 6.017

56.806 4914-89-0 3-Methyl-c-hexene-3 0.014 0.015 0.012 3.690

57.686 6094-02-6 2-Methylhexene-1 0.059 0.063 0.051 15.271

58.550 2738-19-4 2-Methyl-2-hexene 0.027 0.028 0.023 6.901

58.79510574-36-4 3-Methyl-c-hexene-2 0.020 0.021 0.017 5.247

60.07820710-38-8 3-Methyl-t-hexene-2 0.015 0.016 0.013 3.970

60.862 4914-91-4 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.014 0.011 3.439

86.489 C9-IsoOlefin-3 0.010 0.010 0.007 2.627

93.385 C10-IsoOlefin-4 0.005 0.006 0.003 1.355

Naphtheno-Olefins 22.532 1574-41-0 1,3-Cyclopentadiene 0.007 0.008 0.009 1.969

25.738 142-29-0 Cyclopentene 0.208 0.201 0.258 55.399

37.041 1120-62-3 3-Methylcyclopentene 0.104 0.101 0.107 26.877

45.835 693-89-0 1-Methylcyclopentene 0.374 0.357 0.384 99.075

51.155 110-83-8 Cyclohexene 0.046 0.042 0.047 11.959

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C-591
Hydrocarbon Expert V4.7 Fri Aug 27 13:56:25 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91331 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91331

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Naphtheno-Olefins

Di-Olefins 18.624 78-79-5 2-Methyl-1,3-Butadiene 0.011 0.012 0.014 2.981

21.266 2004-70-8 1t,3-Pentadiene 0.016 0.018 0.020 4.394

45.429 1528-30-9 C6-Diolefin-1 0.016 0.016 0.016 4.066

Oxygenates 13.087 64-17-5 Ethanol 16.550 15.628 30.318 1763.987

26.901 71-23-8 n-Propanol 0.079 0.074 0.111 14.373

48.061 71-36-3 n-Butanol 0.058 0.054 0.066 11.331

Unidentified 19.876 Unidentified 0.006 0.007 0.007 1.963

26.992 Unidentified 0.062 0.069 0.062 19.690

28.734 Unidentified 0.056 0.056 0.053 17.614

63.373 Unidentified 0.044 0.046 0.034 14.036

72.451 Unidentified 0.090 0.093 0.066 28.487

76.237 Unidentified 0.015 0.015 0.012 4.900

78.822 Unidentified 0.045 0.044 0.034 14.354

84.900 Unidentified 0.021 0.021 0.014 6.649

85.146 Unidentified 0.022 0.021 0.015 6.955

86.231 Unidentified 0.044 0.045 0.029 13.865

86.597 Unidentified 0.009 0.009 0.006 2.721

88.745 Unidentified 0.102 0.111 0.068 32.383

93.273 Unidentified 0.012 0.012 0.008 3.868

93.273 Unidentified 0.012 0.013 0.007 3.868

93.273 Unidentified 0.012 0.009 0.007 3.868

93.842 Unidentified 0.173 0.178 0.103 54.945

94.525 Unidentified 0.019 0.014 1.612 6.055

94.525 Unidentified 0.019 0.020 0.011 6.055

94.724 Unidentified 0.023 0.021 0.015 7.282

96.351 Unidentified 0.008 0.008 0.005 2.424

99.707 Unidentified 0.012 0.012 0.007 3.720

100.068 Unidentified 0.017 0.018 0.010 5.267

100.354 Unidentified 0.215 0.160 0.116 68.306

100.488 Unidentified 0.577 0.578 0.312 183.068

101.168 Unidentified 0.358 0.380 0.215 113.423

101.290 Unidentified 0.209 0.213 0.124 66.388

102.195 Unidentified 0.023 0.021 0.014 7.253

102.546 Unidentified 0.123 0.108 0.077 39.065

102.688 Unidentified 0.281 0.281 0.152 89.115

103.199 Unidentified 0.122 0.122 0.066 38.704

103.687 Unidentified 0.018 0.015 0.013 5.691

106.204 Unidentified 0.010 0.009 0.006 3.057

107.104 Unidentified 0.345 0.298 0.217 109.291

108.082 Unidentified 0.120 0.120 0.065 37.905

108.354 Unidentified 0.135 0.135 0.073 42.788

108.436 Unidentified 0.106 0.107 0.057 33.726

108.745 Unidentified 0.268 0.268 0.145 84.927

109.169 Unidentified 0.773 0.657 0.486 245.109

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C-592
Hydrocarbon Expert V4.7 Fri Aug 27 13:56:25 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91331 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91331

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Unidentified 109.868 Unidentified 0.036 0.030 0.022 11.326

110.710 Unidentified 0.025 0.023 0.013 7.816

111.039 Unidentified 0.120 0.121 0.072 38.197

111.309 Unidentified 0.110 0.096 0.063 34.817

111.972 Unidentified 0.059 0.049 0.033 18.652

112.956 Unidentified 0.031 0.026 0.020 9.948

113.483 Unidentified 0.034 0.034 0.017 10.663

113.609 Unidentified 0.012 0.012 0.006 3.772

113.811 Unidentified 0.056 0.047 0.032 17.887

115.144 Unidentified 0.011 0.009 0.006 3.591

116.090 Unidentified 0.005 0.005 0.003 1.663

116.942 Unidentified 0.018 0.018 0.009 5.791

117.124 Unidentified 0.006 0.004 0.003 1.756

126.296 Unidentified 0.009 0.009 0.004 2.982

127.262 Unidentified 0.003 0.002 0.002 0.932

130.003 Unidentified 0.003 0.003 0.002 1.043

Plus

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C-593
Hydrocarbon Expert V4.7 Fri Aug 27 13:56:25 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91331 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91331

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF

20.0 15.0 10.0 5.0 0.0

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

Ethanol

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

Unidentified

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

1,3-Cyclopentadiene

2,2-Dimethylbutane

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C-594
Hydrocarbon Expert V4.7 Fri Aug 27 13:56:25 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91331 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91331

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

n-Propanol Unidentified

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

2-Ethylbutene-1 n-Hexane

t-Hexene-3

t-Hexene-2 3-Methylcyclopentene

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane 2,3,3-Trimethylbutene-1 2,2,3-Trimethylbutane

C6-Diolefin-1 Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1

Cyclohexane

n-Butanol

2-Methyl-c-hexene-3

4-Methylhexene-1

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C-595
Hydrocarbon Expert V4.7 Fri Aug 27 13:56:25 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91331 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91331

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF

70.0 65.0 60.0 55.0 50.0

4-Methyl-t/c-hexene-2

2-Methylhexane

Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane C7 - Iso-Olefin - 2

2,2,4-Trimethylpentane Heptene-1

3-Methyl-c-hexene-3

t-Heptene-3

2-Methylhexene-1

n-Heptane c-Heptene-3 2-Methyl-2-hexene 3-Methyl-c-hexene-2

t-Heptene-2

Cyclopentene, 1,5-dimethyl3-Methyl-t-hexene-2

2-Pentene, 3,4-dimethyl-, (Z)-

Methylcyclohexane

Unidentified

2,2,3-Trimethylpentane 2,5-Dimethylhexane

2,4-Dimethylhexane

2,3,4-Trimethylpentane

Toluene2,3,3-Trimethylpentane

2,3-Dimethylhexane

2-Methylheptane

Unidentified 4-Methylheptane

3-Methylheptane

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C-596
Hydrocarbon Expert V4.7 Fri Aug 27 13:56:25 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91331 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91331

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF

95.0 90.0 85.0 80.0 75.0

2,2,5-Trimethylhexane

Unidentified

n-Octane

Unidentified

2,3,5-Trimethylhexane

2,4-Dimethylheptane

Ethylcyclohexane 2,6-Dimethylheptane

2,5-Dimethylheptane

Ethylbenzene Unidentified

m-Xylene Unidentified p-Xylene

C9-IsoOlefin-3 Unidentified

4-Methyloctane 2-Methyloctane

3-Methyloctane

Unidentified o-Xylene

C10 - IsoParaffin - 1

trans-1,3-Diethylcyclopentane 2,2,4-trimethylheptane

n-Nonane

1,1-Methylethylcyclohexane

i-Propylbenzene Unidentified 1-Methyl-2-propyl-cyclopentan/C10-IsoOlefin-4/C10-isoparaffin-x

Unidentified 2,2-Dimethyloctane

Unidentified

2,5-Dimethyloctane C10 - IsoParaffin - 2 2,7-Dimethyloctane 2,4-Dimethyloctane

2,6-Dimethyloctane C10 Isoparaffin -1 Unidentified n-Propylbenzene 3-Methyl-5-ethylheptane

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

5-Methylnonane 4-Methylnonane 2,2,6-Trimethyloctane 1-Methyl-2-ethylbenzene 3-Ethyloctane Unidentified 3-Methylnonane

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C-597
Hydrocarbon Expert V4.7 Fri Aug 27 13:56:25 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91331 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91331

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified UnidentifiedUnidentified C11-Isoparaffin-2 1,2,4-Trimethylbenzene

Unidentified Unidentified

i-Butylcyclohexane

Unidentified3-Ethyl-3-methylheptane Unidentified Unidentified n-Decane

Unidentified

Unidentified 1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene C11 Isoparaffin-4 1-Methyl-4-i-propylbenzene

Indan C11-Isoparaffin-5

Indene

n-ButylCyclohexane Unidentified C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene Unidentified 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene C11-Isoparaffin-8 Unidentified 1-Methyl-2-n-propylbenzene Unidentified C11- Isoparaffin-11

C11- IsoParaffin - 13 Unidentified

Unidentified 2-Methylindan

Unidentified 1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

Unidentified 2-Undecene, (E)- Unidentified

1,2-Dimethyl-3-ethylbenzene Unidentified

n-Undecane Unidentified 1-Ethyl-4-i-propylbenzene

1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene

Unidentified C12 - IsoParaffin - 1

Unidentified

5-Methylindan 1,2-Di-i-propylbenzene 1-methyl-4-(1-methylpropyl)be C11 - Aromatic - 4 4-Methylindan Benzene, 1-methyl-4-(2-methylpropyl)- 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene

1-Methyl-2-n-butylbenzene C11 - Aromatic - 7 Unidentified C12 - IsoParaffin - 4 1,4-Di-i-propylbenzene

Unidentified Naphthalene

1,1-Dimethyl Indane Dimethyl Indane - 1 1t-Butyl-4-ethylbenzene

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

n-Dodecane C11 - Aromatic - 12

1,2,4-Triethylbenzene

2-Methylnaphthalene

1-Methylnaphthalene

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C-598
Hydrocarbon Expert V4.7 Fri Aug 27 13:56:25 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF 25-Aug-10, 18:24:02

Sample: ODDB-91331 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91331

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000013.D\SIG2000013_FID2_B.CDF

145.0 140.0 135.0 130.0 125.0

Unidentified

Unidentified

Unidentified

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C-599
Hydrocarbon Expert V4.7 Fri Aug 27 14:12:51 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91332 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91332

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 4.593 5.646 5.278

I-Paraffins 28.265 31.378 22.549

Aromatics 40.492 35.745 32.614

Mono-Aromatics 39.596 35.016 32.025

Naphthalenes 0.141 0.105 0.090

Naphtheno/Olefino-Benzs 0.207 0.178 0.130

Indenes 0.549 0.446 0.369

Naphthenes 1.856 1.885 1.807

Mono-Naphthenes 1.856 1.885 1.807

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 7.240 8.217 7.872

n-Olefins 3.005 3.497 3.371

Iso-Olefins 3.491 3.979 3.701

Naphtheno-Olefins 0.703 0.695 0.753

Di-Olefins 0.041 0.045 0.047

Oxygenates 16.089 15.652 28.934

Unidentified 1.465 1.477 0.946

Plus 0.000 0.000 0.000

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C-600
Hydrocarbon Expert V4.7 Fri Aug 27 14:12:51 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91332 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91332

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C2 15.958 15.526 28.767

C3 0.076 0.073 0.106

C4 1.974 2.586 2.814

C5 7.736 9.294 9.038

C6 10.273 11.364 10.073

C7 18.347 16.895 16.346

C8 30.682 30.120 23.155

C9 8.701 8.307 5.872

C10 3.813 3.452 2.354

C11 0.809 0.761 0.444

C12 0.165 0.143 0.084

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C-601
Hydrocarbon Expert V4.7 Fri Aug 27 14:12:51 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91332 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91332

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C4 1.703 2.259 2.433

C5 0.821 1.007 0.945

C6 1.709 1.990 1.647

C7 0.120 0.135 0.100

C8 0.021 0.023 0.015

C9 0.177 0.189 0.115

C10 0.016 0.017 0.009

C11 0.025 0.026 0.013

I-Paraffins C4 0.018 0.025 0.026

C5 3.155 3.909 3.631

C6 3.831 4.467 3.692

C7 1.733 1.960 1.436

C8 15.266 16.448 11.099

C9 3.087 3.339 1.999

C10 0.843 0.888 0.490

C11 0.322 0.332 0.171

C12 0.010 0.010 0.005

Mono-Aromatics C6 0.685 0.598 0.728

C7 15.435 13.667 13.912

C8 15.380 13.636 12.031

C9 5.317 4.683 3.674

C10 2.219 1.944 1.373

C11 0.413 0.360 0.231

C12 0.148 0.127 0.076

Naphthalenes C10 0.124 0.093 0.081

C11 0.016 0.012 0.009

Naphtheno/Olefino-Benzs C10 0.207 0.178 0.130

Indenes C9 0.120 0.096 0.084

C10 0.404 0.331 0.271

C11 0.018 0.014 0.010

C12 0.007 0.006 0.004

Mono-Naphthenes C5 0.093 0.096 0.111

C6 1.456 1.477 1.437

C7 0.306 0.313 0.259

n-Olefins C4 0.199 0.250 0.294

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C-602
Hydrocarbon Expert V4.7 Fri Aug 27 14:12:51 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91332 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91332

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

n-Olefins C5 1.659 1.964 1.965

C6 1.033 1.160 1.020

C7 0.098 0.107 0.083

C11 0.015 0.016 0.009

Iso-Olefins C5 1.777 2.085 2.104

C6 1.060 1.182 1.046

C7 0.640 0.698 0.541

C8 0.014 0.014 0.009

Naphtheno-Olefins C5 0.205 0.204 0.250

C6 0.498 0.491 0.504

Di-Olefins C5 0.026 0.030 0.032

C7 0.015 0.015 0.015

Oxygenates C2 15.958 15.526 28.767

C3 0.076 0.073 0.106

C4 0.055 0.053 0.061

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C-603
Hydrocarbon Expert V4.7 Fri Aug 27 14:12:51 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91332 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91332

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 23.40 22.65

5% 81.59 80.51

10% 133.56 97.90

15% 153.07 140.21

20% 172.26 155.11

25% 172.60 172.38

30% 172.94 172.72

35% 173.28 173.07

40% 209.60 183.48

45% 229.89 210.36

50% 230.30 230.02

55% 230.71 230.48

60% 231.64 230.95

65% 236.93 235.22

70% 246.00 238.21

75% 276.56 254.85

80% 281.23 279.18

85% 282.10 281.80

90% 320.72 301.96

95% 341.62 336.07

FBP 403.54 399.00

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C-604
Hydrocarbon Expert V4.7 Fri Aug 27 14:12:51 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91332 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91332

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 8.809 75-28-5 I4 i-Butane 0.018 0.025 0.026 5.016

2 9.622 115-11-7 K4 Isobutene 0.017 0.021 0.025 4.824

3 9.663 106-98-9 K4 Butene-1 0.018 0.024 0.027 5.339

4 10.022 106-97-8 P4 n-Butane 1.703 2.259 2.433 476.606

5 10.507 624-64-6 K4 t-Butene-2 0.075 0.096 0.111 21.798

6 10.635 463-82-1 I5 2,2-Dimethylpropane 0.008 0.010 0.009 2.207

7 11.249 590-18-1 K4 c-Butene-2 0.088 0.109 0.131 25.652

8 13.095 64-17-5 X2 Ethanol 15.958 15.526 28.767 1904.669

9 13.450 563-45-1 C5 3-Methylbutene-1 0.219 0.268 0.259 63.429

10 15.072 78-78-4 I5 i-Pentane 3.147 3.899 3.622 886.785

11 16.725 109-67-1 K5 Pentene-1 0.337 0.404 0.400 97.817

12 17.577 563-46-2 C5 2-Methylbutene-1 0.512 0.604 0.606 148.347

13 18.109 109-66-0 P5 n-Pentane 0.821 1.007 0.945 231.436

14 18.624 78-79-5 E5 2-Methyl-1,3-Butadiene 0.011 0.012 0.013 3.169

15 19.230 646-04-8 K5 t-Pentene-2 0.854 1.011 1.011 247.513

16 19.875 ? Unidentified 0.006 0.007 0.007 2.072

17 20.263 627-20-3 K5 c-Pentene-2 0.468 0.548 0.554 135.641

18 20.940 513-35-9 C5 2-Methylbutene-2 1.046 1.213 1.239 303.329

19 21.266 2004-70-8 E5 1t,3-Pentadiene 0.016 0.018 0.019 4.692

20 22.531 1574-41-0 B5 1,3-Cyclopentadiene 0.007 0.008 0.009 2.115

21 23.100 75-83-2 I6 2,2-Dimethylbutane 0.028 0.033 0.027 7.928

22 25.738 142-29-0 B5 Cyclopentene 0.198 0.196 0.241 58.959

23 26.899 71-23-8 X3 n-Propanol 0.076 0.073 0.106 15.497

24 26.990 ? Unidentified 0.059 0.067 0.058 20.797

25 27.603 287-92-3 M5 Cyclopentane 0.093 0.096 0.111 27.060

26 28.334 79-29-8 I6 2,3-Dimethylbutane 0.704 0.817 0.678 199.158

27 28.732 ? Unidentified 0.053 0.055 0.050 18.695

28 29.190 691-38-3 C6 4-Methyl-c-pentene-2 0.046 0.052 0.045 13.302

29 29.413 107-83-5 I6 2-Methylpentane 1.771 2.082 1.707 501.176

30 29.840 674-76-0 C6 4-Methyl-t-pentene-2 0.130 0.148 0.129 37.750

31 32.064 96-14-0 I6 3-Methylpentane 1.328 1.535 1.280 375.725

32 33.226 763-29-1 C6 2-Methylpentene-1 0.222 0.249 0.219 64.428

33 33.449 592-41-6 K6 Hexene-1 0.162 0.184 0.160 47.021

34 35.642 760-21-4 C6 2-Ethylbutene-1 0.063 0.070 0.062 18.264

35 35.807 110-54-3 P6 n-Hexane 1.709 1.990 1.647 483.546

36 36.43713269-52-8 K6 t-Hexene-3 0.260 0.293 0.257 75.488

37 36.913 4050-45-7 K6 t-Hexene-2 0.399 0.449 0.394 115.739

38 37.039 1120-62-3 B6 3-Methylcyclopentene 0.099 0.100 0.101 28.830

39 37.407 625-27-4 C6 2-Methylpentene-2 0.338 0.375 0.333 97.894

40 37.820 922-62-3 C6 3-Methyl-c-pentene-2 0.261 0.287 0.257 75.630

41 38.741 7688-21-3 K6 c-Hexene-2 0.211 0.234 0.209 61.253

42 40.086 3404-73-7 C7 3,3-Dimethylpentene-1 0.307 0.335 0.259 88.880

43 40.668 96-37-7 M6 Methylcyclopentane 1.035 1.061 1.021 299.897

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C-605
Hydrocarbon Expert V4.7 Fri Aug 27 14:12:51 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91332 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91332

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 42.230 108-08-7 I7 2,4-Dimethylpentane 0.524 0.598 0.434 148.880

45 42.531 594-56-9 C7 2,3,3-Trimethylbutene-1 0.014 0.015 0.012 4.048

46 42.780 464-06-2 I7 2,2,3-Trimethylbutane 0.040 0.045 0.033 11.375

47 45.424 1528-30-9 E7 C6-Diolefin-1 0.015 0.015 0.015 4.336

48 45.635 71-42-3 Q6 Benzene 0.685 0.598 0.728 213.697

49 45.832 693-89-0 B6 1-Methylcyclopentene 0.355 0.349 0.359 105.295

50 46.637 3404-61-3 C7 3-Methylhexene-1 0.016 0.017 0.013 4.523

51 47.227 3524-73-0 C7 5-Methylhexene-1 0.037 0.041 0.031 10.776

52 47.550 110-82-7 M6 Cyclohexane 0.422 0.416 0.416 122.239

53 48.057 71-36-3 X4 n-Butanol 0.055 0.053 0.061 12.019

54 49.27115840-60-5 C7 2-Methyl-c-hexene-3 0.040 0.044 0.034 11.593

55 49.616 3769-23-1 C7 4-Methylhexene-1 0.012 0.013 0.010 3.344

56 50.264 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.050 0.054 0.042 14.460

57 50.663 591-76-4 I7 2-Methylhexane 0.805 0.911 0.667 228.761

58 51.151 110-83-8 B6 Cyclohexene 0.044 0.042 0.044 12.745

59 52.490 589-34-4 I7 3-Methylhexane 0.364 0.406 0.301 103.273

60 53.349 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.100 0.102 0.084 28.855

61 53.936 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.067 0.069 0.057 19.418

62 54.563 822-50-4 M7 1t,2-Dimethylcyclopentane 0.068 0.069 0.057 19.620

63 54.855 C7 C7 - Iso-Olefin - 2 0.022 0.024 0.019 6.500

64 55.165 540-84-1 I8 2,2,4-Trimethylpentane 2.988 3.315 2.172 850.410

65 55.470 592-76-7 K7 Heptene-1 0.028 0.031 0.024 8.182

66 56.801 4914-89-0 C7 3-Methyl-c-hexene-3 0.014 0.015 0.012 3.947

67 57.33014686-14-7 K7 t-Heptene-3 0.032 0.035 0.027 9.157

68 57.683 6094-02-6 C7 2-Methylhexene-1 0.056 0.062 0.048 16.309

69 58.052 142-82-5 P7 n-Heptane 0.120 0.135 0.100 34.163

70 58.272 7642-10-6 K7 c-Heptene-3 0.025 0.027 0.021 7.277

71 58.546 2738-19-4 C7 2-Methyl-2-hexene 0.026 0.028 0.022 7.459

72 58.79010574-36-4 C7 3-Methyl-c-hexene-2 0.020 0.021 0.017 5.684

73 59.17314686-13-6 K7 t-Heptene-2 0.013 0.014 0.011 3.821

74 59.64916491-15-9 M7 Cyclopentene, 1,5-dimethyl- 0.018 0.018 0.015 5.243

75 60.07520710-38-8 C7 3-Methyl-t-hexene-2 0.015 0.016 0.013 4.288

76 60.857 4914-91-4 C7 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.013 0.011 3.646

77 61.504 108-87-2 M7 Methylcyclohexane 0.054 0.054 0.046 15.625

78 63.367 ? Unidentified 0.043 0.045 0.032 15.132

79 64.950 564-02-3 I8 2,2,3-Trimethylpentane 0.448 0.481 0.326 127.584

80 65.178 592-13-2 I8 2,5-Dimethylhexane 0.836 0.925 0.608 237.908

81 65.515 589-43-5 I8 2,4-Dimethylhexane 0.739 0.810 0.537 210.382

82 68.522 565-75-3 I8 2,3,4-Trimethylpentane 4.183 4.466 3.041 1190.681

83 69.115 108-88-3 Q7 Toluene 15.435 13.667 13.912 4765.873

84 69.232 560-21-4 I8 2,3,3-Trimethylpentane 4.730 5.001 3.439 1346.437

85 70.803 584-94-1 I8 2,3-Dimethylhexane 1.102 1.188 0.802 313.800

86 72.047 592-27-8 I8 2-Methylheptane 0.059 0.064 0.043 16.668

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C-606
Hydrocarbon Expert V4.7 Fri Aug 27 14:12:51 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91332 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91332

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 72.319 589-53-7 I8 4-Methylheptane 0.129 0.140 0.094 36.671

88 72.450 ? Unidentified 0.096 0.102 0.070 34.095

89 73.361 589-81-1 I8 3-Methylheptane 0.052 0.057 0.038 14.812

90 75.266 3522-94-9 I9 2,2,5-Trimethylhexane 2.367 2.569 1.533 675.055

91 76.236 ? Unidentified 0.018 0.018 0.014 6.488

92 77.868 111-65-9 P8 n-Octane 0.021 0.023 0.015 6.018

93 78.821 ? Unidentified 0.058 0.058 0.043 20.616

94 80.354 1069-53-0 I9 2,3,5-Trimethylhexane 0.394 0.419 0.255 112.325

95 81.519 1071-26-7 I9 2,4-Dimethylheptane 0.053 0.058 0.035 15.215

96 82.476 1072-05-5 I9 2,6-Dimethylheptane 0.064 0.070 0.042 18.307

97 83.411 I9 2,5-Dimethylheptane 0.187 0.201 0.121 53.362

98 84.749 100-41-4 Q8 Ethylbenzene 2.851 2.524 2.230 873.669

99 84.901 ? Unidentified 0.025 0.026 0.017 8.888

100 85.148 ? Unidentified 0.022 0.022 0.014 7.758

101 86.001 108-38-3 Q8 m-Xylene 7.294 6.479 5.706 2235.133

102 86.140 106-42-3 Q8 p-Xylene 3.389 3.022 2.651 1038.534

103 86.490 C8 C9-IsoOlefin-3 0.014 0.014 0.009 4.152

104 86.597 ? Unidentified 0.012 0.012 0.008 4.181

105 87.408 3221-61-2 I9 2-Methyloctane 0.013 0.014 0.009 3.763

106 88.271 2216-33-3 I9 3-Methyloctane 0.008 0.009 0.005 2.421

107 88.747 ? Unidentified 0.142 0.160 0.093 50.369

108 88.940 95-47-6 Q8 o-Xylene 1.846 1.610 1.444 565.783

109 89.323 I10 C10 - IsoParaffin - 1 0.446 0.471 0.260 127.480

110 90.16614720-74-2 I10 2,2,4-trimethylheptane 0.301 0.317 0.176 85.947

111 91.710 111-84-2 P9 n-Nonane 0.177 0.189 0.115 50.450

112 93.094 98-82-8 Q9 i-Propylbenzene 0.033 0.029 0.023 9.953

113 93.272 ? Unidentified 0.012 0.012 0.008 4.271

114 93.272 ? Unidentified 0.012 0.013 0.007 4.271

115 93.272 ? Unidentified 0.012 0.009 0.007 4.271

116 93.840 ? Unidentified 0.052 0.055 0.030 18.549

117 94.06415869-87-1 I10 2,2-Dimethyloctane 0.017 0.018 0.010 4.769

118 94.86515869-89-3 I10 2,5-Dimethyloctane 0.007 0.008 0.004 2.051

119 95.505 2051-30-1 I10 2,4-Dimethyloctane 0.012 0.013 0.007 3.396

120 96.553 103-65-1 Q9 n-Propylbenzene 0.279 0.248 0.193 84.939

121 97.401 620-14-4 Q9 1-Methyl-3-ethylbenzene 1.081 0.960 0.747 329.098

122 97.633 622-96-8 Q9 1-Methyl-4-ethylbenzene 0.508 0.453 0.351 154.647

123 98.259 108-67-8 Q9 1,3,5-Trimethylbenzene 0.640 0.568 0.442 194.829

124 98.90717301-94-8 I10 4-Methylnonane 0.009 0.009 0.005 2.482

125 99.112 ? Unidentified 0.167 0.176 0.097 59.137

126 99.344 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.406 0.354 0.280 123.552

127 99.885 5911-04-6 I10 3-Methylnonane 0.014 0.015 0.008 4.114

128 100.350 ? Unidentified 0.012 0.010 0.007 4.414

129 100.481 ? Unidentified 0.036 0.037 0.019 12.795

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C-607
Hydrocarbon Expert V4.7 Fri Aug 27 14:12:51 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91332 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91332

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 100.696 I11 C11-Isoparaffin-2 0.020 0.021 0.011 5.777

131 100.978 95-63-6 Q9 1,2,4-Trimethylbenzene 2.005 1.757 1.385 610.371

132 101.162 ? Unidentified 0.025 0.027 0.015 8.880

133 101.283 ? Unidentified 0.014 0.015 0.008 5.113

134 102.33417302-01-1 I10 3-Ethyl-3-methylheptane 0.037 0.039 0.020 10.675

135 102.623 538-93-2 Q10 i-Butylbenzene 0.059 0.053 0.036 17.756

136 102.803 124-18-5 P10 n-Decane 0.016 0.017 0.009 4.591

137 102.899 ? Unidentified 0.024 0.022 0.015 8.680

138 103.197 ? Unidentified 0.010 0.010 0.005 3.529

139 103.849 526-73-8 Q9 1,2,3-Trimethylbenzene 0.366 0.314 0.253 111.433

140 104.241 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.008 0.007 0.005 2.498

141 104.614 99-87-6 Q10 1-Methyl-4-i-propylbenzene 0.037 0.033 0.023 11.304

142 105.043 J9 Indan 0.120 0.096 0.084 37.159

143 105.636 J10 Indene 0.227 0.181 0.159 70.184

144 106.352 I11 C11-Isoparaffin-7 0.094 0.097 0.050 26.762

145 106.546 141-93-5 Q10 1,3-Diethylbenzene 0.048 0.043 0.030 14.676

146 106.822 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 0.394 0.351 0.244 119.298

147 107.163 105-05-5 Q10 1,4-Diethylbenzene 0.147 0.131 0.091 44.524

148 107.260 104-51-8 Q10 n-Butylbenzene 0.030 0.027 0.019 9.170

149 107.381 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.146 0.128 0.091 44.342

150 107.633 135-01-3 Q10 1,2-Diethylbenzene 0.027 0.024 0.017 8.215

151 108.079 ? Unidentified 0.023 0.024 0.012 8.213

152 108.232 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.057 0.050 0.035 17.204

153 108.353 ? Unidentified 0.028 0.029 0.015 9.989

154 108.434 ? Unidentified 0.025 0.026 0.014 9.025

155 108.560 I11 C11- Isoparaffin-11 0.208 0.215 0.111 59.571

156 108.742 ? Unidentified 0.067 0.070 0.036 23.919

157 109.076 1758-88-9 Q10 1,4,Dimethyl-2-ethylbenzene 0.116 0.102 0.072 35.244

158 109.165 ? Unidentified 0.291 0.255 0.180 103.406

159 109.393 J10 2-Methylindan 0.042 0.033 0.026 12.981

160 109.739 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.309 0.271 0.191 93.639

161 110.284 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.206 0.178 0.128 62.501

162 110.708 ? Unidentified 0.006 0.005 0.003 2.063

163 110.902 693-61-8 K11 2-Undecene, (E)- 0.015 0.016 0.009 4.387

164 111.036 ? Unidentified 0.022 0.023 0.013 7.718

165 111.195 Q11 1-Methyl-4-t-butylbenzene 0.029 0.026 0.016 8.774

166 111.311 ? Unidentified 0.033 0.029 0.019 11.746

167 111.412 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.083 0.071 0.051 25.007

168 111.707 1120-21-4 P11 n-Undecane 0.025 0.026 0.013 7.254

169 111.863 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.027 0.024 0.015 8.251

170 111.972 ? Unidentified 0.014 0.012 0.008 5.004

171 112.346 Q10 1,2,4,5-Tetramethylbenzene 0.235 0.204 0.146 71.287

172 112.612 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.315 0.272 0.195 95.358

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C-608
Hydrocarbon Expert V4.7 Fri Aug 27 14:12:51 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91332 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91332

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 112.955 J10 C1-Indane - 1 0.005 0.004 0.003 1.440

174 113.131 I12 C12 - IsoParaffin - 1 0.006 0.007 0.003 1.846

175 113.483 ? Unidentified 0.019 0.019 0.009 6.582

176 113.754 Q11 C11 - Aromatic - 3 0.044 0.038 0.025 13.348

177 113.944 874-35-1 H10 5-Methylindan 0.103 0.089 0.065 31.260

178 114.069 Q12 1,2-Di-i-propylbenzene 0.038 0.032 0.019 11.303

179 114.284 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.053 0.046 0.030 15.967

180 114.441 Q11 C11 - Aromatic - 4 0.034 0.029 0.019 10.274

181 114.693 824-22-6 J10 4-Methylindan 0.131 0.113 0.082 39.591

182 114.845 5161-04-6 Q11 Benzene, 1-methyl-4-(2-methylpropyl)-0.039 0.034 0.022 11.910

183 114.940 824-63-5 H10 2-Methylindan 0.103 0.089 0.065 31.331

184 115.144 ? Unidentified 0.011 0.011 0.005 3.825

185 115.256 538-68-1 Q11 n-Pentylbenzene 0.017 0.015 0.010 5.183

186 115.485 Q11 tert-Pentylbenzene 0.058 0.050 0.033 17.591

187 115.797 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.026 0.022 0.014 7.743

188 115.908 Q11 C11 - Aromatic - 7 0.036 0.032 0.020 10.827

189 116.242 I12 C12 - IsoParaffin - 4 0.004 0.004 0.002 1.108

190 116.367 100-18-5 Q12 1,4-Di-i-propylbenzene 0.050 0.043 0.025 14.889

191 116.809 91-20-3 G10 Naphthalene 0.124 0.093 0.081 39.466

192 116.944 ? Unidentified 0.009 0.010 0.005 3.310

193 117.250 J11 1,1-Dimethyl Indane 0.018 0.014 0.010 5.443

194 117.412 J12 Dimethyl Indane - 1 0.007 0.006 0.004 2.186

195 117.592 7364-19-4 Q12 1t-Butyl-4-ethylbenzene 0.007 0.006 0.004 2.097

196 117.892 Q12 1,3-Di-n-propylbenzene 0.048 0.041 0.025 14.409

197 118.003 Q11 C11 - Aromatic - 11 0.027 0.025 0.015 8.211

198 118.557 Q11 C11 - Aromatic - 12 0.021 0.019 0.012 6.334

199 119.486 102-25-0 Q12 1,3,5-Triethylbenzene 0.006 0.005 0.003 1.670

200 123.439 91-57-6 G11 2-Methylnaphthalene 0.011 0.008 0.006 3.387

201 124.305 90-12-0 G11 1-Methylnaphthalene 0.005 0.004 0.003 1.653

202 126.296 ? Unidentified 0.004 0.004 0.002 1.351

203 130.002 ? Unidentified 0.003 0.002 0.002 1.015

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C-609
Hydrocarbon Expert V4.7 Fri Aug 27 14:12:51 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91332 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91332

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 10.022 106-97-8 n-Butane 1.703 2.259 2.433 476.606

18.109 109-66-0 n-Pentane 0.821 1.007 0.945 231.436

35.807 110-54-3 n-Hexane 1.709 1.990 1.647 483.546

58.052 142-82-5 n-Heptane 0.120 0.135 0.100 34.163

77.868 111-65-9 n-Octane 0.021 0.023 0.015 6.018

91.710 111-84-2 n-Nonane 0.177 0.189 0.115 50.450

102.803 124-18-5 n-Decane 0.016 0.017 0.009 4.591

111.707 1120-21-4 n-Undecane 0.025 0.026 0.013 7.254

I-Paraffins 8.809 75-28-5 i-Butane 0.018 0.025 0.026 5.016

10.635 463-82-1 2,2-Dimethylpropane 0.008 0.010 0.009 2.207

15.072 78-78-4 i-Pentane 3.147 3.899 3.622 886.785

23.100 75-83-2 2,2-Dimethylbutane 0.028 0.033 0.027 7.928

28.334 79-29-8 2,3-Dimethylbutane 0.704 0.817 0.678 199.158

29.413 107-83-5 2-Methylpentane 1.771 2.082 1.707 501.176

32.064 96-14-0 3-Methylpentane 1.328 1.535 1.280 375.725

42.230 108-08-7 2,4-Dimethylpentane 0.524 0.598 0.434 148.880

42.780 464-06-2 2,2,3-Trimethylbutane 0.040 0.045 0.033 11.375

50.663 591-76-4 2-Methylhexane 0.805 0.911 0.667 228.761

52.490 589-34-4 3-Methylhexane 0.364 0.406 0.301 103.273

55.165 540-84-1 2,2,4-Trimethylpentane 2.988 3.315 2.172 850.410

64.950 564-02-3 2,2,3-Trimethylpentane 0.448 0.481 0.326 127.584

65.178 592-13-2 2,5-Dimethylhexane 0.836 0.925 0.608 237.908

65.515 589-43-5 2,4-Dimethylhexane 0.739 0.810 0.537 210.382

68.522 565-75-3 2,3,4-Trimethylpentane 4.183 4.466 3.041 1190.681

69.232 560-21-4 2,3,3-Trimethylpentane 4.730 5.001 3.439 1346.437

70.803 584-94-1 2,3-Dimethylhexane 1.102 1.188 0.802 313.800

72.047 592-27-8 2-Methylheptane 0.059 0.064 0.043 16.668

72.319 589-53-7 4-Methylheptane 0.129 0.140 0.094 36.671

73.361 589-81-1 3-Methylheptane 0.052 0.057 0.038 14.812

75.266 3522-94-9 2,2,5-Trimethylhexane 2.367 2.569 1.533 675.055

80.354 1069-53-0 2,3,5-Trimethylhexane 0.394 0.419 0.255 112.325

81.519 1071-26-7 2,4-Dimethylheptane 0.053 0.058 0.035 15.215

82.476 1072-05-5 2,6-Dimethylheptane 0.064 0.070 0.042 18.307

83.411 2,5-Dimethylheptane 0.187 0.201 0.121 53.362

87.408 3221-61-2 2-Methyloctane 0.013 0.014 0.009 3.763

88.271 2216-33-3 3-Methyloctane 0.008 0.009 0.005 2.421

89.323 C10 - IsoParaffin - 1 0.446 0.471 0.260 127.480

90.16614720-74-2 2,2,4-trimethylheptane 0.301 0.317 0.176 85.947

94.06415869-87-1 2,2-Dimethyloctane 0.017 0.018 0.010 4.769

94.86515869-89-3 2,5-Dimethyloctane 0.007 0.008 0.004 2.051

95.505 2051-30-1 2,4-Dimethyloctane 0.012 0.013 0.007 3.396

98.90717301-94-8 4-Methylnonane 0.009 0.009 0.005 2.482

99.885 5911-04-6 3-Methylnonane 0.014 0.015 0.008 4.114

100.696 C11-Isoparaffin-2 0.020 0.021 0.011 5.777

102.33417302-01-1 3-Ethyl-3-methylheptane 0.037 0.039 0.020 10.675

106.352 C11-Isoparaffin-7 0.094 0.097 0.050 26.762

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C-610
Hydrocarbon Expert V4.7 Fri Aug 27 14:12:51 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91332 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91332

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

I-Paraffins 108.560 C11- Isoparaffin-11 0.208 0.215 0.111 59.571

113.131 C12 - IsoParaffin - 1 0.006 0.007 0.003 1.846

116.242 C12 - IsoParaffin - 4 0.004 0.004 0.002 1.108

Aromatics

Mono-Aromatics 45.635 71-42-3 Benzene 0.685 0.598 0.728 213.697

69.115 108-88-3 Toluene 15.435 13.667 13.912 4765.873

84.749 100-41-4 Ethylbenzene 2.851 2.524 2.230 873.669

86.001 108-38-3 m-Xylene 7.294 6.479 5.706 2235.133

86.140 106-42-3 p-Xylene 3.389 3.022 2.651 1038.534

88.940 95-47-6 o-Xylene 1.846 1.610 1.444 565.783

93.094 98-82-8 i-Propylbenzene 0.033 0.029 0.023 9.953

96.553 103-65-1 n-Propylbenzene 0.279 0.248 0.193 84.939

97.401 620-14-4 1-Methyl-3-ethylbenzene 1.081 0.960 0.747 329.098

97.633 622-96-8 1-Methyl-4-ethylbenzene 0.508 0.453 0.351 154.647

98.259 108-67-8 1,3,5-Trimethylbenzene 0.640 0.568 0.442 194.829

99.344 611-14-3 1-Methyl-2-ethylbenzene 0.406 0.354 0.280 123.552

100.978 95-63-6 1,2,4-Trimethylbenzene 2.005 1.757 1.385 610.371

102.623 538-93-2 i-Butylbenzene 0.059 0.053 0.036 17.756

103.849 526-73-8 1,2,3-Trimethylbenzene 0.366 0.314 0.253 111.433

104.241 535-77-3 1-Methyl-3-i-propylbenzene 0.008 0.007 0.005 2.498

104.614 99-87-6 1-Methyl-4-i-propylbenzene 0.037 0.033 0.023 11.304

106.546 141-93-5 1,3-Diethylbenzene 0.048 0.043 0.030 14.676

106.822 1074-43-7 1-Methyl-3-n-propylbenzene 0.394 0.351 0.244 119.298

107.163 105-05-5 1,4-Diethylbenzene 0.147 0.131 0.091 44.524

107.260 104-51-8 n-Butylbenzene 0.030 0.027 0.019 9.170

107.381 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.146 0.128 0.091 44.342

107.633 135-01-3 1,2-Diethylbenzene 0.027 0.024 0.017 8.215

108.232 1074-17-5 1-Methyl-2-n-propylbenzene 0.057 0.050 0.035 17.204

109.076 1758-88-9 1,4,Dimethyl-2-ethylbenzene 0.116 0.102 0.072 35.244

109.739 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.309 0.271 0.191 93.639

110.284 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.206 0.178 0.128 62.501

111.195 1-Methyl-4-t-butylbenzene 0.029 0.026 0.016 8.774

111.412 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.083 0.071 0.051 25.007

111.863 4218-48-8 1-Ethyl-4-i-propylbenzene 0.027 0.024 0.015 8.251

112.346 1,2,4,5-Tetramethylbenzene 0.235 0.204 0.146 71.287

112.612 527-53-7 1,2,3,5-Tetramethylbenzene 0.315 0.272 0.195 95.358

113.754 C11 - Aromatic - 3 0.044 0.038 0.025 13.348

114.069 1,2-Di-i-propylbenzene 0.038 0.032 0.019 11.303

114.284 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.053 0.046 0.030 15.967

114.441 C11 - Aromatic - 4 0.034 0.029 0.019 10.274

114.845 5161-04-6 Benzene, 1-methyl-4-(2-methylpropyl)-0.039 0.034 0.022 11.910

115.256 538-68-1 n-Pentylbenzene 0.017 0.015 0.010 5.183

115.485 tert-Pentylbenzene 0.058 0.050 0.033 17.591

115.797 577-55-9 1-Methyl-2-n-butylbenzene 0.026 0.022 0.014 7.743

115.908 C11 - Aromatic - 7 0.036 0.032 0.020 10.827

116.367 100-18-5 1,4-Di-i-propylbenzene 0.050 0.043 0.025 14.889

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C-611
Hydrocarbon Expert V4.7 Fri Aug 27 14:12:51 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91332 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91332

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 117.592 7364-19-4 1t-Butyl-4-ethylbenzene 0.007 0.006 0.004 2.097

117.892 1,3-Di-n-propylbenzene 0.048 0.041 0.025 14.409

118.003 C11 - Aromatic - 11 0.027 0.025 0.015 8.211

118.557 C11 - Aromatic - 12 0.021 0.019 0.012 6.334

119.486 102-25-0 1,3,5-Triethylbenzene 0.006 0.005 0.003 1.670

Naphthalenes 116.809 91-20-3 Naphthalene 0.124 0.093 0.081 39.466

123.439 91-57-6 2-Methylnaphthalene 0.011 0.008 0.006 3.387

124.305 90-12-0 1-Methylnaphthalene 0.005 0.004 0.003 1.653

Naphtheno/Olefino-Benzs 113.944 874-35-1 5-Methylindan 0.103 0.089 0.065 31.260

114.940 824-63-5 2-Methylindan 0.103 0.089 0.065 31.331

Indenes 105.043 Indan 0.120 0.096 0.084 37.159

105.636 Indene 0.227 0.181 0.159 70.184

109.393 2-Methylindan 0.042 0.033 0.026 12.981

112.955 C1-Indane - 1 0.005 0.004 0.003 1.440

114.693 824-22-6 4-Methylindan 0.131 0.113 0.082 39.591

117.250 1,1-Dimethyl Indane 0.018 0.014 0.010 5.443

117.412 Dimethyl Indane - 1 0.007 0.006 0.004 2.186

Naphthenes

Mono-Naphthenes 27.603 287-92-3 Cyclopentane 0.093 0.096 0.111 27.060

40.668 96-37-7 Methylcyclopentane 1.035 1.061 1.021 299.897

47.550 110-82-7 Cyclohexane 0.422 0.416 0.416 122.239

53.349 1759-58-6 1t,3-Dimethylcyclopentane 0.100 0.102 0.084 28.855

53.936 2532-58-3 1c,3-Dimethylcyclopentane 0.067 0.069 0.057 19.418

54.563 822-50-4 1t,2-Dimethylcyclopentane 0.068 0.069 0.057 19.620

59.64916491-15-9 Cyclopentene, 1,5-dimethyl- 0.018 0.018 0.015 5.243

61.504 108-87-2 Methylcyclohexane 0.054 0.054 0.046 15.625

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.622 115-11-7 Isobutene 0.017 0.021 0.025 4.824

9.663 106-98-9 Butene-1 0.018 0.024 0.027 5.339

10.507 624-64-6 t-Butene-2 0.075 0.096 0.111 21.798

11.249 590-18-1 c-Butene-2 0.088 0.109 0.131 25.652

16.725 109-67-1 Pentene-1 0.337 0.404 0.400 97.817

19.230 646-04-8 t-Pentene-2 0.854 1.011 1.011 247.513

20.263 627-20-3 c-Pentene-2 0.468 0.548 0.554 135.641

33.449 592-41-6 Hexene-1 0.162 0.184 0.160 47.021

36.43713269-52-8 t-Hexene-3 0.260 0.293 0.257 75.488

36.913 4050-45-7 t-Hexene-2 0.399 0.449 0.394 115.739

38.741 7688-21-3 c-Hexene-2 0.211 0.234 0.209 61.253

55.470 592-76-7 Heptene-1 0.028 0.031 0.024 8.182

57.33014686-14-7 t-Heptene-3 0.032 0.035 0.027 9.157

58.272 7642-10-6 c-Heptene-3 0.025 0.027 0.021 7.277

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C-612
Hydrocarbon Expert V4.7 Fri Aug 27 14:12:51 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91332 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91332

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

n-Olefins 59.17314686-13-6 t-Heptene-2 0.013 0.014 0.011 3.821

110.902 693-61-8 2-Undecene, (E)- 0.015 0.016 0.009 4.387

Iso-Olefins 13.450 563-45-1 3-Methylbutene-1 0.219 0.268 0.259 63.429

17.577 563-46-2 2-Methylbutene-1 0.512 0.604 0.606 148.347

20.940 513-35-9 2-Methylbutene-2 1.046 1.213 1.239 303.329

29.190 691-38-3 4-Methyl-c-pentene-2 0.046 0.052 0.045 13.302

29.840 674-76-0 4-Methyl-t-pentene-2 0.130 0.148 0.129 37.750

33.226 763-29-1 2-Methylpentene-1 0.222 0.249 0.219 64.428

35.642 760-21-4 2-Ethylbutene-1 0.063 0.070 0.062 18.264

37.407 625-27-4 2-Methylpentene-2 0.338 0.375 0.333 97.894

37.820 922-62-3 3-Methyl-c-pentene-2 0.261 0.287 0.257 75.630

40.086 3404-73-7 3,3-Dimethylpentene-1 0.307 0.335 0.259 88.880

42.531 594-56-9 2,3,3-Trimethylbutene-1 0.014 0.015 0.012 4.048

46.637 3404-61-3 3-Methylhexene-1 0.016 0.017 0.013 4.523

47.227 3524-73-0 5-Methylhexene-1 0.037 0.041 0.031 10.776

49.27115840-60-5 2-Methyl-c-hexene-3 0.040 0.044 0.034 11.593

49.616 3769-23-1 4-Methylhexene-1 0.012 0.013 0.010 3.344

50.264 3404-55-5 4-Methyl-t/c-hexene-2 0.050 0.054 0.042 14.460

54.855 C7 - Iso-Olefin - 2 0.022 0.024 0.019 6.500

56.801 4914-89-0 3-Methyl-c-hexene-3 0.014 0.015 0.012 3.947

57.683 6094-02-6 2-Methylhexene-1 0.056 0.062 0.048 16.309

58.546 2738-19-4 2-Methyl-2-hexene 0.026 0.028 0.022 7.459

58.79010574-36-4 3-Methyl-c-hexene-2 0.020 0.021 0.017 5.684

60.07520710-38-8 3-Methyl-t-hexene-2 0.015 0.016 0.013 4.288

60.857 4914-91-4 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.013 0.011 3.646

86.490 C9-IsoOlefin-3 0.014 0.014 0.009 4.152

Naphtheno-Olefins 22.531 1574-41-0 1,3-Cyclopentadiene 0.007 0.008 0.009 2.115

25.738 142-29-0 Cyclopentene 0.198 0.196 0.241 58.959

37.039 1120-62-3 3-Methylcyclopentene 0.099 0.100 0.101 28.830

45.832 693-89-0 1-Methylcyclopentene 0.355 0.349 0.359 105.295

51.151 110-83-8 Cyclohexene 0.044 0.042 0.044 12.745

Di-Olefins 18.624 78-79-5 2-Methyl-1,3-Butadiene 0.011 0.012 0.013 3.169

21.266 2004-70-8 1t,3-Pentadiene 0.016 0.018 0.019 4.692

45.424 1528-30-9 C6-Diolefin-1 0.015 0.015 0.015 4.336

Oxygenates 13.095 64-17-5 Ethanol 15.958 15.526 28.767 1904.669

26.899 71-23-8 n-Propanol 0.076 0.073 0.106 15.497

48.057 71-36-3 n-Butanol 0.055 0.053 0.061 12.019

Unidentified 19.875 Unidentified 0.006 0.007 0.007 2.072

26.990 Unidentified 0.059 0.067 0.058 20.797

28.732 Unidentified 0.053 0.055 0.050 18.695

63.367 Unidentified 0.043 0.045 0.032 15.132

72.450 Unidentified 0.096 0.102 0.070 34.095

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C-613
Hydrocarbon Expert V4.7 Fri Aug 27 14:12:51 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91332 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91332

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Unidentified 76.236 Unidentified 0.018 0.018 0.014 6.488

78.821 Unidentified 0.058 0.058 0.043 20.616

84.901 Unidentified 0.025 0.026 0.017 8.888

85.148 Unidentified 0.022 0.022 0.014 7.758

86.597 Unidentified 0.012 0.012 0.008 4.181

88.747 Unidentified 0.142 0.160 0.093 50.369

93.272 Unidentified 0.012 0.012 0.008 4.271

93.272 Unidentified 0.012 0.013 0.007 4.271

93.272 Unidentified 0.012 0.009 0.007 4.271

93.840 Unidentified 0.052 0.055 0.030 18.549

99.112 Unidentified 0.167 0.176 0.097 59.137

100.350 Unidentified 0.012 0.010 0.007 4.414

100.481 Unidentified 0.036 0.037 0.019 12.795

101.162 Unidentified 0.025 0.027 0.015 8.880

101.283 Unidentified 0.014 0.015 0.008 5.113

102.899 Unidentified 0.024 0.022 0.015 8.680

103.197 Unidentified 0.010 0.010 0.005 3.529

108.079 Unidentified 0.023 0.024 0.012 8.213

108.353 Unidentified 0.028 0.029 0.015 9.989

108.434 Unidentified 0.025 0.026 0.014 9.025

108.742 Unidentified 0.067 0.070 0.036 23.919

109.165 Unidentified 0.291 0.255 0.180 103.406

110.708 Unidentified 0.006 0.005 0.003 2.063

111.036 Unidentified 0.022 0.023 0.013 7.718

111.311 Unidentified 0.033 0.029 0.019 11.746

111.972 Unidentified 0.014 0.012 0.008 5.004

113.483 Unidentified 0.019 0.019 0.009 6.582

115.144 Unidentified 0.011 0.011 0.005 3.825

116.944 Unidentified 0.009 0.010 0.005 3.310

126.296 Unidentified 0.004 0.004 0.002 1.351

130.002 Unidentified 0.003 0.002 0.002 1.015

Plus

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C-614
Hydrocarbon Expert V4.7 Fri Aug 27 14:12:51 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91332 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91332

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF

20.0 15.0 10.0 5.0 0.0

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

Ethanol

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

Unidentified

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

1,3-Cyclopentadiene

2,2-Dimethylbutane

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C-615
Hydrocarbon Expert V4.7 Fri Aug 27 14:12:51 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91332 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91332

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

n-Propanol Unidentified

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-22-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

2-Ethylbutene-1 n-Hexane

t-Hexene-3

t-Hexene-2 3-Methylcyclopentene

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane 2,3,3-Trimethylbutene-1 2,2,3-Trimethylbutane

C6-Diolefin-1 Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1 Cyclohexane

n-Butanol

2-Methyl-c-hexene-3

4-Methylhexene-1

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C-616
Hydrocarbon Expert V4.7 Fri Aug 27 14:12:51 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91332 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91332

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF

70.0 65.0 60.0 55.0 50.0

4-Methyl-t/c-hexene-2

2-Methylhexane

Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane C7 - Iso-Olefin - 2

2,2,4-Trimethylpentane Heptene-1

3-Methyl-c-hexene-3

t-Heptene-3

2-Methylhexene-1

n-Heptane c-Heptene-3 2-Methyl-2-hexene 3-Methyl-c-hexene-2

t-Heptene-2

Cyclopentene, 1,5-dimethyl3-Methyl-t-hexene-2

2-Pentene, 3,4-dimethyl-, (Z)-

Methylcyclohexane

Unidentified

2,2,3-Trimethylpentane 2,5-Dimethylhexane

2,4-Dimethylhexane

2,3,4-Trimethylpentane

2,3,3-Trimethylpentane Toluene

2,3-Dimethylhexane

2-Methylheptane

Unidentified 4-Methylheptane

3-Methylheptane

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C-617
Hydrocarbon Expert V4.7 Fri Aug 27 14:12:51 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91332 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91332

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF

95.0 90.0 85.0 80.0 75.0

2,2,5-Trimethylhexane

Unidentified

n-Octane

Unidentified

2,3,5-Trimethylhexane

2,4-Dimethylheptane

2,6-Dimethylheptane

2,5-Dimethylheptane

Unidentified Ethylbenzene

m-Xylene p-Xylene

C9-IsoOlefin-3 Unidentified

2-Methyloctane

3-Methyloctane

Unidentified o-Xylene

C10 - IsoParaffin - 1

2,2,4-trimethylheptane

n-Nonane

i-Propylbenzene Unidentified

Unidentified 2,2-Dimethyloctane

2,5-Dimethyloctane

2,4-Dimethyloctane

n-Propylbenzene

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

4-Methylnonane Unidentified 1-Methyl-2-ethylbenzene

3-Methylnonane

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C-618
Hydrocarbon Expert V4.7 Fri Aug 27 14:12:51 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91332 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91332

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified

C11-Isoparaffin-2 1,2,4-Trimethylbenzene Unidentified

3-Ethyl-3-methylheptane i-Butylbenzene n-Decane Unidentified Unidentified

1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene

1-Methyl-4-i-propylbenzene

Indan

Indene

C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene

n-Butylbenzene 1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

Unidentified 1-Methyl-2-n-propylbenzene

C11- Isoparaffin-11 Unidentified

1,4,Dimethyl-2-ethylbenzene Unidentified 2-Methylindan

1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

Unidentified 2-Undecene, (E)- Unidentified 1-Methyl-4-t-butylbenzene Unidentified 1,2-Dimethyl-3-ethylbenzene n-Undecane Unidentified 1-Ethyl-4-i-propylbenzene

1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene

C1-Indane - 1 C12 - IsoParaffin - 1

Unidentified C11 - Aromatic - 3 5-Methylindan 1,2-Di-i-propylbenzene 1-methyl-4-(1-methylpropyl)be C11 - Aromatic - 4 4-Methylindan Benzene, 1-methyl-4-(2-methylpropyl)- 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene

1-Methyl-2-n-butylbenzene C11 - Aromatic - 7

C12 - IsoParaffin - 4 1,4-Di-i-propylbenzene

Unidentified Naphthalene

1,1-Dimethyl Indane Dimethyl Indane - 1 1t-Butyl-4-ethylbenzene

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

C11 - Aromatic - 12

1,3,5-Triethylbenzene

2-Methylnaphthalene

1-Methylnaphthalene

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C-619
Hydrocarbon Expert V4.7 Fri Aug 27 14:12:51 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF 25-Aug-10, 20:51:55

Sample: ODDB-91332 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91332

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000014.D\SIG2000014_FID2_B.CDF

145.0 140.0 135.0 130.0 125.0

Unidentified

Unidentified

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C-620
Hydrocarbon Expert V4.7 Fri Aug 27 14:24:58 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000015.D\SIG2000015_FID2_B.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91333 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91333

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 4.061 5.099 2.937

I-Paraffins 5.798 6.839 3.314

Aromatics 6.677 5.948 3.273

Mono-Aromatics 6.588 5.876 3.238

Naphthalenes 0.033 0.025 0.012

Naphtheno/Olefino-Benzs 0.014 0.013 0.005

Indenes 0.042 0.035 0.018

Naphthenes 0.715 0.733 0.423

Mono-Naphthenes 0.715 0.733 0.423

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 0.443 0.549 0.359

n-Olefins 0.337 0.429 0.295

Iso-Olefins 0.106 0.120 0.063

Naphtheno-Olefins 0.000 0.000 0.000

Di-Olefins 0.000 0.000 0.000

Oxygenates 82.109 80.620 89.603

Unidentified 0.197 0.213 0.091

Plus 0.000 0.000 0.000

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C-621
Hydrocarbon Expert V4.7 Fri Aug 27 14:24:58 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000015.D\SIG2000015_FID2_B.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91333 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91333

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C2 82.109 80.620 89.603

C3 0.007 0.010 0.007

C4 2.040 2.725 1.774

C5 3.749 4.624 2.617

C6 2.008 2.282 1.184

C7 3.810 3.679 2.027

C8 4.280 4.206 1.966

C9 1.459 1.336 0.605

C10 0.300 0.267 0.113

C11 0.042 0.039 0.014

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C-622
Hydrocarbon Expert V4.7 Fri Aug 27 14:24:58 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000015.D\SIG2000015_FID2_B.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91333 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91333

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C3 0.007 0.010 0.007

C4 1.528 2.045 1.321

C5 1.652 2.044 1.151

C6 0.399 0.469 0.233

C7 0.289 0.327 0.145

C8 0.138 0.153 0.061

C9 0.036 0.039 0.014

C10 0.008 0.008 0.003

C11 0.004 0.004 0.001

I-Paraffins C4 0.212 0.295 0.183

C5 1.843 2.304 1.284

C6 1.190 1.403 0.694

C7 0.674 0.766 0.338

C8 1.665 1.839 0.733

C9 0.171 0.185 0.067

C10 0.023 0.025 0.008

C11 0.020 0.021 0.007

Mono-Aromatics C6 0.142 0.125 0.091

C7 2.551 2.280 1.392

C8 2.446 2.184 1.158

C9 1.230 1.093 0.514

C10 0.219 0.194 0.082

Naphthalenes C10 0.016 0.012 0.006

C11 0.017 0.013 0.006

Naphtheno/Olefino-Benzs C10 0.014 0.013 0.005

Indenes C9 0.022 0.018 0.009

C10 0.020 0.017 0.008

Mono-Naphthenes C5 0.177 0.184 0.127

C6 0.268 0.274 0.160

C7 0.240 0.244 0.123

C8 0.030 0.030 0.014

n-Olefins C4 0.300 0.385 0.269

C5 0.037 0.044 0.026

Iso-Olefins C5 0.041 0.048 0.029

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C-623
Hydrocarbon Expert V4.7 Fri Aug 27 14:24:58 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000015.D\SIG2000015_FID2_B.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91333 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91333

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Iso-Olefins C6 0.009 0.010 0.005

C7 0.056 0.062 0.029

Oxygenates C2 82.109 80.620 89.603

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C-624
Hydrocarbon Expert V4.7 Fri Aug 27 14:24:58 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000015.D\SIG2000015_FID2_B.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91333 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91333

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 21.70 20.80

5% 93.97 81.46

10% 171.55 171.51

15% 171.66 171.62

20% 171.77 171.74

25% 171.88 171.85

30% 171.99 171.96

35% 172.10 172.07

40% 172.21 172.18

45% 172.32 172.29

50% 172.43 172.41

55% 172.54 172.52

60% 172.65 172.63

65% 172.76 172.74

70% 172.87 172.85

75% 172.98 172.96

80% 173.09 173.07

85% 173.20 173.19

90% 178.77 173.30

95% 235.25 231.00

FBP 336.22 335.51

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C-625
Hydrocarbon Expert V4.7 Fri Aug 27 14:24:58 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000015.D\SIG2000015_FID2_B.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91333 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91333

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 7.476 ? Unidentified 0.001 0.002 0.001 0.379

2 7.554 74-98-6 P3 Propane 0.007 0.010 0.007 1.953

3 8.808 75-28-5 I4 i-Butane 0.212 0.295 0.183 64.086

4 9.621 115-11-7 K4 Isobutene 0.073 0.095 0.065 22.829

5 9.662 106-98-9 K4 Butene-1 0.055 0.071 0.049 17.123

6 10.021 106-97-8 P4 n-Butane 1.528 2.045 1.321 461.498

7 10.506 624-64-6 K4 t-Butene-2 0.107 0.137 0.096 33.454

8 10.634 463-82-1 I5 2,2-Dimethylpropane 0.009 0.012 0.006 2.810

9 11.247 590-18-1 K4 c-Butene-2 0.066 0.082 0.059 20.543

10 13.405 64-17-5 X2 Ethanol 82.109 80.620 89.603 10578.776

11 15.067 78-78-4 I5 i-Pentane 1.833 2.292 1.277 557.689

12 16.723 109-67-1 K5 Pentene-1 0.008 0.010 0.006 2.513

13 17.574 563-46-2 C5 2-Methylbutene-1 0.014 0.017 0.010 4.365

14 18.105 109-66-0 P5 n-Pentane 1.652 2.044 1.151 502.540

15 19.225 646-04-8 K5 t-Pentene-2 0.019 0.022 0.013 5.850

16 20.258 627-20-3 K5 c-Pentene-2 0.010 0.012 0.007 3.111

17 20.935 513-35-9 C5 2-Methylbutene-2 0.027 0.032 0.019 8.449

18 23.079 75-83-2 I6 2,2-Dimethylbutane 0.069 0.082 0.040 20.959

19 27.595 287-92-3 M5 Cyclopentane 0.177 0.184 0.127 55.278

20 28.325 79-29-8 I6 2,3-Dimethylbutane 0.147 0.172 0.086 44.870

21 29.399 107-83-5 I6 2-Methylpentane 0.632 0.750 0.369 193.017

22 32.051 96-14-0 I6 3-Methylpentane 0.342 0.399 0.200 104.569

23 35.789 110-54-3 P6 n-Hexane 0.399 0.469 0.233 121.978

24 37.397 625-27-4 C6 2-Methylpentene-2 0.009 0.010 0.005 2.835

25 40.078 3404-73-7 C7 3,3-Dimethylpentene-1 0.009 0.010 0.004 2.745

26 40.654 96-37-7 M6 Methylcyclopentane 0.201 0.208 0.120 62.791

27 42.217 108-08-7 I7 2,4-Dimethylpentane 0.074 0.085 0.037 22.613

28 45.625 71-42-3 Q6 Benzene 0.142 0.125 0.091 47.875

29 47.219 3524-73-0 C7 5-Methylhexene-1 0.022 0.024 0.011 6.770

30 47.541 110-82-7 M6 Cyclohexane 0.067 0.067 0.040 20.976

31 50.650 591-76-4 I7 2-Methylhexane 0.323 0.369 0.162 99.136

32 52.480 589-34-4 I7 3-Methylhexane 0.277 0.312 0.139 84.930

33 53.343 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.025 0.026 0.013 7.722

34 53.929 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.022 0.023 0.011 6.930

35 54.555 822-50-4 M7 1t,2-Dimethylcyclopentane 0.029 0.030 0.015 9.026

36 54.670 C7 2-Ethylpentene-1 0.025 0.028 0.013 7.944

37 55.134 540-84-1 I8 2,2,4-Trimethylpentane 0.666 0.745 0.293 204.506

38 58.045 142-82-5 P7 n-Heptane 0.289 0.327 0.145 88.539

39 61.501 108-87-2 M7 Methylcyclohexane 0.094 0.095 0.048 29.471

40 62.839 590-73-8 I8 2,2-Dimethylhexane 0.013 0.015 0.006 4.028

41 63.330 ? Unidentified 0.196 0.211 0.090 75.213

42 64.168 1640-89-7 M7 Ethylcyclopentane 0.070 0.071 0.036 22.047

43 64.936 564-02-3 I8 2,2,3-Trimethylpentane 0.024 0.026 0.011 7.456

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C-626
Hydrocarbon Expert V4.7 Fri Aug 27 14:24:58 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000015.D\SIG2000015_FID2_B.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91333 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91333

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 65.159 592-13-2 I8 2,5-Dimethylhexane 0.084 0.094 0.037 25.953

45 65.497 589-43-5 I8 2,4-Dimethylhexane 0.108 0.120 0.048 33.221

46 66.334 4850-28-6 M8 1c,2t,4-Trimethylcyclopentane 0.009 0.010 0.004 2.959

47 66.731 563-16-6 I8 3,3-Dimethylhexane 0.016 0.017 0.007 4.848

48 68.455 565-75-3 I8 2,3,4-Trimethylpentane 0.277 0.298 0.122 84.965

49 68.984 108-88-3 Q7 Toluene 2.551 2.280 1.392 850.318

50 70.783 584-94-1 I8 2,3-Dimethylhexane 0.091 0.099 0.040 28.040

51 72.038 592-27-8 I8 2-Methylheptane 0.120 0.133 0.053 36.872

52 72.293 589-53-7 I8 4-Methylheptane 0.078 0.086 0.034 23.923

53 73.354 589-81-1 I8 3-Methylheptane 0.153 0.168 0.067 47.044

54 73.519 619-99-8 I8 3-Ethylhexane 0.035 0.038 0.015 10.738

55 75.241 3522-94-9 I9 2,2,5-Trimethylhexane 0.046 0.050 0.018 14.140

56 75.602 M8 3c-Ethylmethylcyclopentane 0.005 0.005 0.002 1.493

57 77.864 111-65-9 P8 n-Octane 0.138 0.153 0.061 42.513

58 80.347 1069-53-0 I9 2,3,5-Trimethylhexane 0.008 0.008 0.003 2.314

59 81.516 1071-26-7 I9 2,4-Dimethylheptane 0.009 0.010 0.003 2.694

60 82.159 1678-91-7 M8 Ethylcyclohexane 0.016 0.016 0.007 5.021

61 82.471 1072-05-5 I9 2,6-Dimethylheptane 0.011 0.012 0.004 3.299

62 83.399 I9 2,5-Dimethylheptane 0.016 0.018 0.006 4.984

63 84.721 100-41-4 Q8 Ethylbenzene 0.402 0.359 0.190 132.895

64 85.937 108-38-3 Q8 m-Xylene 1.042 0.934 0.493 344.612

65 86.087 106-42-3 Q8 p-Xylene 0.441 0.397 0.209 145.825

66 87.270 2216-34-4 I9 4-Methyloctane 0.021 0.023 0.008 6.551

67 87.401 3221-61-2 I9 2-Methyloctane 0.024 0.026 0.010 7.490

68 88.10115869-80-4 I9 Heptane, 3-ethyl- 0.006 0.006 0.002 1.820

69 88.265 2216-33-3 I9 3-Methyloctane 0.030 0.033 0.012 9.307

70 88.922 95-47-6 Q8 o-Xylene 0.562 0.494 0.266 185.747

71 89.316 I10 C10 - IsoParaffin - 1 0.006 0.006 0.002 1.702

72 91.744 111-84-2 P9 n-Nonane 0.036 0.039 0.014 11.157

73 93.091 98-82-8 Q9 i-Propylbenzene 0.022 0.020 0.009 7.355

74 96.548 103-65-1 Q9 n-Propylbenzene 0.077 0.069 0.032 25.188

75 97.389 620-14-4 Q9 1-Methyl-3-ethylbenzene 0.271 0.243 0.113 89.025

76 97.625 622-96-8 Q9 1-Methyl-4-ethylbenzene 0.119 0.107 0.050 38.990

77 98.250 108-67-8 Q9 1,3,5-Trimethylbenzene 0.127 0.114 0.053 41.883

78 99.111 I10 2,2,6-Trimethyloctane 0.018 0.019 0.006 5.417

79 99.338 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.098 0.086 0.041 32.243

80 100.960 95-63-6 Q9 1,2,4-Trimethylbenzene 0.425 0.376 0.178 139.747

81 102.802 124-18-5 P10 n-Decane 0.008 0.008 0.003 2.335

82 103.843 526-73-8 Q9 1,2,3-Trimethylbenzene 0.091 0.078 0.038 29.778

83 105.039 J9 Indan 0.022 0.018 0.009 7.373

84 105.632 J10 Indene 0.012 0.009 0.005 3.869

85 106.349 I11 C11-Isoparaffin-7 0.005 0.005 0.002 1.504

86 106.542 141-93-5 Q10 1,3-Diethylbenzene 0.009 0.008 0.003 2.822

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C-627
Hydrocarbon Expert V4.7 Fri Aug 27 14:24:58 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000015.D\SIG2000015_FID2_B.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91333 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91333

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 106.803 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 0.036 0.033 0.014 11.915

88 107.159 105-05-5 Q10 1,4-Diethylbenzene 0.018 0.016 0.007 5.822

89 107.377 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.025 0.022 0.009 8.046

90 108.230 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.007 0.006 0.003 2.314

91 108.558 I11 C11- Isoparaffin-11 0.016 0.016 0.005 4.816

92 109.071 1758-88-9 Q10 1,4,Dimethyl-2-ethylbenzene 0.017 0.015 0.006 5.486

93 109.234 874-41-9 Q10 1,3-Dimethyl-4-ethylbenzene 0.023 0.020 0.009 7.558

94 109.736 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.029 0.026 0.011 9.449

95 110.282 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.009 0.008 0.003 2.930

96 111.411 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.006 0.005 0.002 1.946

97 111.687 1120-21-4 P11 n-Undecane 0.004 0.004 0.001 1.281

98 112.343 Q10 1,2,4,5-Tetramethylbenzene 0.017 0.015 0.006 5.526

99 112.608 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.024 0.021 0.009 7.747

100 113.942 874-35-1 H10 5-Methylindan 0.006 0.005 0.002 1.846

101 114.691 824-22-6 J10 4-Methylindan 0.009 0.007 0.003 2.806

102 114.939 824-63-5 H10 2-Methylindan 0.009 0.008 0.003 2.852

103 116.809 91-20-3 G10 Naphthalene 0.016 0.012 0.006 5.344

104 123.439 91-57-6 G11 2-Methylnaphthalene 0.012 0.009 0.004 4.131

105 124.304 90-12-0 G11 1-Methylnaphthalene 0.005 0.004 0.002 1.679

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C-628
Hydrocarbon Expert V4.7 Fri Aug 27 14:24:58 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000015.D\SIG2000015_FID2_B.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91333 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91333

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 7.554 74-98-6 Propane 0.007 0.010 0.007 1.953

10.021 106-97-8 n-Butane 1.528 2.045 1.321 461.498

18.105 109-66-0 n-Pentane 1.652 2.044 1.151 502.540

35.789 110-54-3 n-Hexane 0.399 0.469 0.233 121.978

58.045 142-82-5 n-Heptane 0.289 0.327 0.145 88.539

77.864 111-65-9 n-Octane 0.138 0.153 0.061 42.513

91.744 111-84-2 n-Nonane 0.036 0.039 0.014 11.157

102.802 124-18-5 n-Decane 0.008 0.008 0.003 2.335

111.687 1120-21-4 n-Undecane 0.004 0.004 0.001 1.281

I-Paraffins 8.808 75-28-5 i-Butane 0.212 0.295 0.183 64.086

10.634 463-82-1 2,2-Dimethylpropane 0.009 0.012 0.006 2.810

15.067 78-78-4 i-Pentane 1.833 2.292 1.277 557.689

23.079 75-83-2 2,2-Dimethylbutane 0.069 0.082 0.040 20.959

28.325 79-29-8 2,3-Dimethylbutane 0.147 0.172 0.086 44.870

29.399 107-83-5 2-Methylpentane 0.632 0.750 0.369 193.017

32.051 96-14-0 3-Methylpentane 0.342 0.399 0.200 104.569

42.217 108-08-7 2,4-Dimethylpentane 0.074 0.085 0.037 22.613

50.650 591-76-4 2-Methylhexane 0.323 0.369 0.162 99.136

52.480 589-34-4 3-Methylhexane 0.277 0.312 0.139 84.930

55.134 540-84-1 2,2,4-Trimethylpentane 0.666 0.745 0.293 204.506

62.839 590-73-8 2,2-Dimethylhexane 0.013 0.015 0.006 4.028

64.936 564-02-3 2,2,3-Trimethylpentane 0.024 0.026 0.011 7.456

65.159 592-13-2 2,5-Dimethylhexane 0.084 0.094 0.037 25.953

65.497 589-43-5 2,4-Dimethylhexane 0.108 0.120 0.048 33.221

66.731 563-16-6 3,3-Dimethylhexane 0.016 0.017 0.007 4.848

68.455 565-75-3 2,3,4-Trimethylpentane 0.277 0.298 0.122 84.965

70.783 584-94-1 2,3-Dimethylhexane 0.091 0.099 0.040 28.040

72.038 592-27-8 2-Methylheptane 0.120 0.133 0.053 36.872

72.293 589-53-7 4-Methylheptane 0.078 0.086 0.034 23.923

73.354 589-81-1 3-Methylheptane 0.153 0.168 0.067 47.044

73.519 619-99-8 3-Ethylhexane 0.035 0.038 0.015 10.738

75.241 3522-94-9 2,2,5-Trimethylhexane 0.046 0.050 0.018 14.140

80.347 1069-53-0 2,3,5-Trimethylhexane 0.008 0.008 0.003 2.314

81.516 1071-26-7 2,4-Dimethylheptane 0.009 0.010 0.003 2.694

82.471 1072-05-5 2,6-Dimethylheptane 0.011 0.012 0.004 3.299

83.399 2,5-Dimethylheptane 0.016 0.018 0.006 4.984

87.270 2216-34-4 4-Methyloctane 0.021 0.023 0.008 6.551

87.401 3221-61-2 2-Methyloctane 0.024 0.026 0.010 7.490

88.10115869-80-4 Heptane, 3-ethyl- 0.006 0.006 0.002 1.820

88.265 2216-33-3 3-Methyloctane 0.030 0.033 0.012 9.307

89.316 C10 - IsoParaffin - 1 0.006 0.006 0.002 1.702

99.111 2,2,6-Trimethyloctane 0.018 0.019 0.006 5.417

106.349 C11-Isoparaffin-7 0.005 0.005 0.002 1.504

108.558 C11- Isoparaffin-11 0.016 0.016 0.005 4.816

Aromatics

Mono-Aromatics 45.625 71-42-3 Benzene 0.142 0.125 0.091 47.875

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C-629
Hydrocarbon Expert V4.7 Fri Aug 27 14:24:58 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000015.D\SIG2000015_FID2_B.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91333 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91333

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 68.984 108-88-3 Toluene 2.551 2.280 1.392 850.318

84.721 100-41-4 Ethylbenzene 0.402 0.359 0.190 132.895

85.937 108-38-3 m-Xylene 1.042 0.934 0.493 344.612

86.087 106-42-3 p-Xylene 0.441 0.397 0.209 145.825

88.922 95-47-6 o-Xylene 0.562 0.494 0.266 185.747

93.091 98-82-8 i-Propylbenzene 0.022 0.020 0.009 7.355

96.548 103-65-1 n-Propylbenzene 0.077 0.069 0.032 25.188

97.389 620-14-4 1-Methyl-3-ethylbenzene 0.271 0.243 0.113 89.025

97.625 622-96-8 1-Methyl-4-ethylbenzene 0.119 0.107 0.050 38.990

98.250 108-67-8 1,3,5-Trimethylbenzene 0.127 0.114 0.053 41.883

99.338 611-14-3 1-Methyl-2-ethylbenzene 0.098 0.086 0.041 32.243

100.960 95-63-6 1,2,4-Trimethylbenzene 0.425 0.376 0.178 139.747

103.843 526-73-8 1,2,3-Trimethylbenzene 0.091 0.078 0.038 29.778

106.542 141-93-5 1,3-Diethylbenzene 0.009 0.008 0.003 2.822

106.803 1074-43-7 1-Methyl-3-n-propylbenzene 0.036 0.033 0.014 11.915

107.159 105-05-5 1,4-Diethylbenzene 0.018 0.016 0.007 5.822

107.377 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.025 0.022 0.009 8.046

108.230 1074-17-5 1-Methyl-2-n-propylbenzene 0.007 0.006 0.003 2.314

109.071 1758-88-9 1,4,Dimethyl-2-ethylbenzene 0.017 0.015 0.006 5.486

109.234 874-41-9 1,3-Dimethyl-4-ethylbenzene 0.023 0.020 0.009 7.558

109.736 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.029 0.026 0.011 9.449

110.282 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.009 0.008 0.003 2.930

111.411 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.006 0.005 0.002 1.946

112.343 1,2,4,5-Tetramethylbenzene 0.017 0.015 0.006 5.526

112.608 527-53-7 1,2,3,5-Tetramethylbenzene 0.024 0.021 0.009 7.747

Naphthalenes 116.809 91-20-3 Naphthalene 0.016 0.012 0.006 5.344

123.439 91-57-6 2-Methylnaphthalene 0.012 0.009 0.004 4.131

124.304 90-12-0 1-Methylnaphthalene 0.005 0.004 0.002 1.679

Naphtheno/Olefino-Benzs 113.942 874-35-1 5-Methylindan 0.006 0.005 0.002 1.846

114.939 824-63-5 2-Methylindan 0.009 0.008 0.003 2.852

Indenes 105.039 Indan 0.022 0.018 0.009 7.373

105.632 Indene 0.012 0.009 0.005 3.869

114.691 824-22-6 4-Methylindan 0.009 0.007 0.003 2.806

Naphthenes

Mono-Naphthenes 27.595 287-92-3 Cyclopentane 0.177 0.184 0.127 55.278

40.654 96-37-7 Methylcyclopentane 0.201 0.208 0.120 62.791

47.541 110-82-7 Cyclohexane 0.067 0.067 0.040 20.976

53.343 1759-58-6 1t,3-Dimethylcyclopentane 0.025 0.026 0.013 7.722

53.929 2532-58-3 1c,3-Dimethylcyclopentane 0.022 0.023 0.011 6.930

54.555 822-50-4 1t,2-Dimethylcyclopentane 0.029 0.030 0.015 9.026

61.501 108-87-2 Methylcyclohexane 0.094 0.095 0.048 29.471

64.168 1640-89-7 Ethylcyclopentane 0.070 0.071 0.036 22.047

66.334 4850-28-6 1c,2t,4-Trimethylcyclopentane 0.009 0.010 0.004 2.959

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C-630
Hydrocarbon Expert V4.7 Fri Aug 27 14:24:58 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000015.D\SIG2000015_FID2_B.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91333 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91333

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Naphthenes 75.602 3c-Ethylmethylcyclopentane 0.005 0.005 0.002 1.493

82.159 1678-91-7 Ethylcyclohexane 0.016 0.016 0.007 5.021

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.621 115-11-7 Isobutene 0.073 0.095 0.065 22.829

9.662 106-98-9 Butene-1 0.055 0.071 0.049 17.123

10.506 624-64-6 t-Butene-2 0.107 0.137 0.096 33.454

11.247 590-18-1 c-Butene-2 0.066 0.082 0.059 20.543

16.723 109-67-1 Pentene-1 0.008 0.010 0.006 2.513

19.225 646-04-8 t-Pentene-2 0.019 0.022 0.013 5.850

20.258 627-20-3 c-Pentene-2 0.010 0.012 0.007 3.111

Iso-Olefins 17.574 563-46-2 2-Methylbutene-1 0.014 0.017 0.010 4.365

20.935 513-35-9 2-Methylbutene-2 0.027 0.032 0.019 8.449

37.397 625-27-4 2-Methylpentene-2 0.009 0.010 0.005 2.835

40.078 3404-73-7 3,3-Dimethylpentene-1 0.009 0.010 0.004 2.745

47.219 3524-73-0 5-Methylhexene-1 0.022 0.024 0.011 6.770

54.670 2-Ethylpentene-1 0.025 0.028 0.013 7.944

Naphtheno-Olefins

Di-Olefins

Oxygenates 13.405 64-17-5 Ethanol 82.109 80.620 89.603 10578.776

Unidentified 7.476 Unidentified 0.001 0.002 0.001 0.379

63.330 Unidentified 0.196 0.211 0.090 75.213

Plus

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C-631
Hydrocarbon Expert V4.7 Fri Aug 27 14:24:58 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000015.D\SIG2000015_FID2_B.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91333 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91333

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000015.D\SIG2000015_FID2_B.CDF

20.0 15.0 10.0 5.0 0.0

Unidentified Propane

i-Butane

Butene-1 Isobutene

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

Ethanol

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

t-Pentene-2

c-Pentene-2

2-Methylbutene-2

2,2-Dimethylbutane

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C-632
Hydrocarbon Expert V4.7 Fri Aug 27 14:24:58 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000015.D\SIG2000015_FID2_B.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91333 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91333

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000015.D\SIG2000015_FID2_B.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentane

2,3-Dimethylbutane

2-Methylpentane

3-Methylpentane

n-Hexane

2-Methylpentene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane

Benzene

5-Methylhexene-1

Cyclohexane

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C-633
Hydrocarbon Expert V4.7 Fri Aug 27 14:24:58 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000015.D\SIG2000015_FID2_B.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91333 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91333

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000015.D\SIG2000015_FID2_B.CDF

70.0 65.0 60.0 55.0 50.0

2-Methylhexane

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane 2-Ethylpentene-1

2,2,4-Trimethylpentane

n-Heptane

Methylcyclohexane

2,2-Dimethylhexane

Unidentified

Ethylcyclopentane

2,2,3-Trimethylpentane 2,5-Dimethylhexane

2,4-Dimethylhexane

1c,2t,4-Trimethylcyclopentane

3,3-Dimethylhexane

2,3,4-Trimethylpentane

Toluene

2,3-Dimethylhexane

2-Methylheptane 4-Methylheptane

3-Methylheptane 3-Ethylhexane

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C-634
Hydrocarbon Expert V4.7 Fri Aug 27 14:24:58 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000015.D\SIG2000015_FID2_B.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91333 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91333

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000015.D\SIG2000015_FID2_B.CDF

95.0 90.0 85.0 80.0 75.0

2,2,5-Trimethylhexane

3c-Ethylmethylcyclopentane

n-Octane

2,3,5-Trimethylhexane

2,4-Dimethylheptane

Ethylcyclohexane 2,6-Dimethylheptane

2,5-Dimethylheptane

Ethylbenzene

m-Xylene p-Xylene

4-Methyloctane 2-Methyloctane

Heptane, 3-ethyl- 3-Methyloctane

o-Xylene

C10 - IsoParaffin - 1

n-Nonane

i-Propylbenzene

n-Propylbenzene

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

2,2,6-Trimethyloctane 1-Methyl-2-ethylbenzene

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C-635
Hydrocarbon Expert V4.7 Fri Aug 27 14:24:58 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000015.D\SIG2000015_FID2_B.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91333 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91333

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000015.D\SIG2000015_FID2_B.CDF

120.0 115.0 110.0 105.0 100.0

1,2,4-Trimethylbenzene

n-Decane

1,2,3-Trimethylbenzene

Indan

Indene

C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene

1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene

1-Methyl-2-n-propylbenzene

C11- Isoparaffin-11

1,4,Dimethyl-2-ethylbenzene 1,3-Dimethyl-4-ethylbenzene

1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

1,2-Dimethyl-3-ethylbenzene n-Undecane

1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene

5-Methylindan

4-Methylindan 2-Methylindan

Naphthalene

2-Methylnaphthalene

1-Methylnaphthalene

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C-636
Hydrocarbon Expert V4.7 Fri Aug 27 14:24:58 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000015.D\SIG2000015_FID2_B.CDF 25-Aug-10, 23:27:47

Sample: ODDB-91333 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91333

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000015.D\SIG2000015_FID2_B.CDF

145.0 140.0 135.0 130.0 125.0

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C-637
Hydrocarbon Expert V4.7 Fri Aug 27 15:26:31 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000019.D\SIG2000019_FID2_B.CDF 26-Aug-10, 15:36:26

Sample: ODDB-91334 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91334

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 3.648 4.505 4.628

I-Paraffins 33.536 38.748 34.013

Aromatics 42.295 36.165 32.537

Mono-Aromatics 40.946 35.096 31.657

Naphthalenes 0.185 0.135 0.118

Naphtheno/Olefino-Benzs 0.327 0.274 0.204

Indenes 0.837 0.661 0.557

Naphthenes 1.465 1.456 1.471

Mono-Naphthenes 1.465 1.456 1.471

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 7.367 8.109 7.962

n-Olefins 3.084 3.481 3.432

Iso-Olefins 3.516 3.888 3.710

Naphtheno-Olefins 0.725 0.696 0.772

Di-Olefins 0.042 0.045 0.048

Oxygenates 10.419 9.834 18.599

Unidentified 1.270 1.182 0.790

Plus 0.000 0.000 0.000

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C-638
Hydrocarbon Expert V4.7 Fri Aug 27 15:26:31 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000019.D\SIG2000019_FID2_B.CDF 26-Aug-10, 15:36:26

Sample: ODDB-91334 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91334

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C2 10.286 9.710 18.431

C3 0.077 0.072 0.106

C4 2.499 3.184 3.542

C5 17.835 21.096 20.549

C6 23.350 25.952 22.530

C7 14.022 12.449 12.442

C8 12.205 10.510 9.486

C9 12.010 10.266 8.250

C10 4.945 4.214 3.065

C11 1.263 1.163 0.687

C12 0.240 0.202 0.122

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C-639
Hydrocarbon Expert V4.7 Fri Aug 27 15:26:31 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000019.D\SIG2000019_FID2_B.CDF 26-Aug-10, 15:36:26

Sample: ODDB-91334 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91334

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C4 2.216 2.852 3.148

C5 0.832 0.990 0.952

C6 0.415 0.469 0.398

C7 0.091 0.100 0.075

C8 0.020 0.021 0.014

C10 0.039 0.040 0.023

C11 0.034 0.034 0.018

I-Paraffins C4 0.027 0.037 0.039

C5 12.911 15.523 14.772

C6 18.731 21.232 17.943

C7 0.833 0.913 0.687

C8 0.045 0.047 0.032

C10 0.402 0.410 0.231

C11 0.574 0.575 0.303

C12 0.011 0.011 0.005

Mono-Aromatics C6 0.712 0.603 0.752

C7 12.074 10.373 10.817

C8 12.140 10.442 9.440

C9 11.874 10.161 8.155

C10 3.346 2.843 2.058

C11 0.581 0.492 0.323

C12 0.219 0.183 0.111

Naphthalenes C10 0.171 0.124 0.110

C11 0.015 0.011 0.008

Naphtheno/Olefino-Benzs C10 0.327 0.274 0.204

Indenes C9 0.135 0.105 0.095

C10 0.660 0.524 0.439

C11 0.031 0.024 0.018

C12 0.010 0.008 0.006

Mono-Naphthenes C5 0.375 0.374 0.441

C6 0.811 0.805 0.796

C7 0.279 0.277 0.235

n-Olefins C4 0.199 0.243 0.293

C5 1.698 1.950 1.999

C6 1.063 1.158 1.042

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C-640
Hydrocarbon Expert V4.7 Fri Aug 27 15:26:31 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000019.D\SIG2000019_FID2_B.CDF 26-Aug-10, 15:36:26

Sample: ODDB-91334 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91334

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

n-Olefins C7 0.096 0.102 0.081

C11 0.028 0.028 0.016

Iso-Olefins C5 1.782 2.026 2.097

C6 1.102 1.192 1.081

C7 0.632 0.670 0.532

Naphtheno-Olefins C5 0.210 0.203 0.255

C6 0.515 0.493 0.518

Di-Olefins C5 0.027 0.029 0.033

C7 0.015 0.015 0.015

Oxygenates C2 10.286 9.710 18.431

C3 0.077 0.072 0.106

C4 0.056 0.052 0.063

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C-641
Hydrocarbon Expert V4.7 Fri Aug 27 15:26:31 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000019.D\SIG2000019_FID2_B.CDF 26-Aug-10, 15:36:26

Sample: ODDB-91334 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91334

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 22.72 22.20

5% 79.36 79.11

10% 80.61 80.16

15% 81.87 81.20

20% 111.52 88.92

25% 138.02 126.40

30% 139.43 138.13

35% 144.11 139.37

40% 148.77 143.79

45% 172.39 145.53

50% 172.91 170.61

55% 191.00 172.77

60% 223.52 174.24

65% 228.11 222.92

70% 272.95 228.26

75% 281.53 277.87

80% 289.20 281.91

85% 323.48 321.57

90% 335.37 334.25

95% 363.20 359.41

FBP 404.60 404.60

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C-642
Hydrocarbon Expert V4.7 Fri Aug 27 15:26:31 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000019.D\SIG2000019_FID2_B.CDF 26-Aug-10, 15:36:26

Sample: ODDB-91334 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91334

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 8.809 75-28-5 I4 i-Butane 0.027 0.037 0.039 6.805

2 9.623 115-11-7 K4 Isobutene 0.017 0.021 0.024 4.281

3 9.665 106-98-9 K4 Butene-1 0.018 0.023 0.027 4.773

4 10.023 106-97-8 P4 n-Butane 2.216 2.852 3.148 552.220

5 10.510 624-64-6 K4 t-Butene-2 0.075 0.093 0.111 19.435

6 10.638 463-82-1 I5 2,2-Dimethylpropane 0.028 0.035 0.031 6.902

7 11.251 590-18-1 K4 c-Butene-2 0.089 0.107 0.131 22.971

8 13.050 64-17-5 X2 Ethanol 10.286 9.710 18.431 1093.007

9 13.455 563-45-1 C5 3-Methylbutene-1 0.184 0.218 0.216 47.445

10 15.097 78-78-4 I5 i-Pentane 12.884 15.488 14.741 3232.534

11 16.734 109-67-1 K5 Pentene-1 0.345 0.401 0.406 88.991

12 17.587 563-46-2 C5 2-Methylbutene-1 0.524 0.600 0.617 135.298

13 18.116 109-66-0 P5 n-Pentane 0.832 0.990 0.952 208.786

14 18.633 78-79-5 E5 2-Methyl-1,3-Butadiene 0.011 0.012 0.013 2.853

15 19.239 646-04-8 K5 t-Pentene-2 0.874 1.005 1.029 225.599

16 19.882 ? Unidentified 0.006 0.007 0.007 1.934

17 20.268 627-20-3 K5 c-Pentene-2 0.479 0.544 0.564 123.646

18 20.950 513-35-9 C5 2-Methylbutene-2 1.074 1.207 1.264 277.069

19 21.279 2004-70-8 E5 1t,3-Pentadiene 0.016 0.018 0.020 4.276

20 22.540 1574-41-0 B5 1,3-Cyclopentadiene 0.007 0.008 0.009 1.931

21 23.093 75-83-2 I6 2,2-Dimethylbutane 0.520 0.597 0.498 130.983

22 25.745 142-29-0 B5 Cyclopentene 0.203 0.195 0.246 53.820

23 26.904 71-23-8 X3 n-Propanol 0.077 0.072 0.106 13.895

24 27.005 ? Unidentified 0.062 0.069 0.060 19.450

25 27.607 287-92-3 M5 Cyclopentane 0.375 0.374 0.441 96.657

26 28.353 79-29-8 I6 2,3-Dimethylbutane 1.877 2.113 1.798 472.714

27 28.748 ? Unidentified 0.054 0.054 0.051 17.060

28 29.207 691-38-3 C6 4-Methyl-c-pentene-2 0.046 0.051 0.045 11.836

29 29.474 107-83-5 I6 2-Methylpentane 10.806 12.324 10.351 2721.985

30 29.857 674-76-0 C6 4-Methyl-t-pentene-2 0.134 0.148 0.132 34.623

31 32.101 96-14-0 I6 3-Methylpentane 5.529 6.199 5.296 1392.728

32 33.239 763-29-1 C6 2-Methylpentene-1 0.230 0.250 0.226 59.348

33 33.460 592-41-6 K6 Hexene-1 0.164 0.180 0.161 42.260

34 35.645 760-21-4 C6 2-Ethylbutene-1 0.074 0.080 0.073 19.187

35 35.807 110-54-3 P6 n-Hexane 0.415 0.469 0.398 104.594

36 36.44313269-52-8 K6 t-Hexene-3 0.269 0.293 0.264 69.349

37 36.921 4050-45-7 K6 t-Hexene-2 0.411 0.449 0.404 106.182

38 37.048 1120-62-3 B6 3-Methylcyclopentene 0.104 0.101 0.104 26.770

39 37.413 625-27-4 C6 2-Methylpentene-2 0.349 0.376 0.342 89.939

40 37.828 922-62-3 C6 3-Methyl-c-pentene-2 0.269 0.287 0.264 69.485

41 38.748 7688-21-3 K6 c-Hexene-2 0.219 0.236 0.215 56.473

42 40.094 3404-73-7 C7 3,3-Dimethylpentene-1 0.316 0.335 0.266 81.530

43 40.674 96-37-7 M6 Methylcyclopentane 0.746 0.743 0.732 192.624

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C-643
Hydrocarbon Expert V4.7 Fri Aug 27 15:26:31 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000019.D\SIG2000019_FID2_B.CDF 26-Aug-10, 15:36:26

Sample: ODDB-91334 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91334

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 42.246 108-08-7 I7 2,4-Dimethylpentane 0.149 0.165 0.123 37.719

45 42.544 594-56-9 C7 2,3,3-Trimethylbutene-1 0.010 0.010 0.008 2.467

46 45.435 1528-30-9 E7 C6-Diolefin-1 0.015 0.015 0.015 3.958

47 45.645 71-42-3 Q6 Benzene 0.712 0.603 0.752 197.767

48 45.839 693-89-0 B6 1-Methylcyclopentene 0.366 0.350 0.368 96.741

49 46.649 3404-61-3 C7 3-Methylhexene-1 0.016 0.017 0.013 4.014

50 47.234 3524-73-0 C7 5-Methylhexene-1 0.023 0.024 0.019 5.891

51 47.557 110-82-7 M6 Cyclohexane 0.065 0.062 0.064 16.744

52 48.061 71-36-3 X4 n-Butanol 0.056 0.052 0.063 10.967

53 49.27815840-60-5 C7 2-Methyl-c-hexene-3 0.041 0.044 0.035 10.648

54 49.626 3769-23-1 C7 4-Methylhexene-1 0.011 0.012 0.009 2.828

55 50.272 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.052 0.055 0.043 13.320

56 50.665 591-76-4 I7 2-Methylhexane 0.407 0.447 0.335 102.965

57 50.847 ? Unidentified 0.020 0.022 0.017 6.343

58 51.158 110-83-8 B6 Cyclohexene 0.045 0.042 0.046 11.738

59 52.498 589-34-4 I7 3-Methylhexane 0.277 0.300 0.228 70.106

60 53.360 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.096 0.096 0.081 24.869

61 53.946 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.064 0.064 0.054 16.633

62 54.569 822-50-4 M7 1t,2-Dimethylcyclopentane 0.058 0.058 0.049 15.086

63 54.849 C7 C7 - Iso-Olefin - 2 0.023 0.024 0.019 5.866

64 55.475 592-76-7 K7 Heptene-1 0.028 0.030 0.024 7.257

65 56.808 4914-89-0 C7 3-Methyl-c-hexene-3 0.014 0.015 0.012 3.625

66 57.33814686-14-7 K7 t-Heptene-3 0.032 0.034 0.027 8.202

67 57.690 6094-02-6 C7 2-Methylhexene-1 0.056 0.060 0.047 14.491

68 58.060 142-82-5 P7 n-Heptane 0.091 0.100 0.075 23.135

69 58.280 7642-10-6 K7 c-Heptene-3 0.024 0.026 0.020 6.264

70 58.555 2738-19-4 C7 2-Methyl-2-hexene 0.025 0.026 0.021 6.456

71 58.79910574-36-4 C7 3-Methyl-c-hexene-2 0.019 0.020 0.016 5.028

72 59.18214686-13-6 K7 t-Heptene-2 0.012 0.013 0.010 3.067

73 59.65716491-15-9 M7 Cyclopentene, 1,5-dimethyl- 0.018 0.018 0.015 4.736

74 60.08020710-38-8 C7 3-Methyl-t-hexene-2 0.014 0.015 0.012 3.723

75 60.865 4914-91-4 C7 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.013 0.011 3.326

76 61.506 108-87-2 M7 Methylcyclohexane 0.042 0.040 0.035 10.727

77 63.401 ? Unidentified 0.024 0.025 0.018 7.719

78 69.076 108-88-3 Q7 Toluene 12.074 10.373 10.817 3319.113

79 72.051 592-27-8 I8 2-Methylheptane 0.017 0.018 0.012 4.247

80 72.304 589-53-7 I8 4-Methylheptane 0.009 0.010 0.007 2.396

81 73.365 589-81-1 I8 3-Methylheptane 0.018 0.019 0.013 4.670

82 77.873 111-65-9 P8 n-Octane 0.020 0.021 0.014 4.996

83 84.745 100-41-4 Q8 Ethylbenzene 2.190 1.881 1.703 597.451

84 85.987 108-38-3 Q8 m-Xylene 5.749 4.955 4.470 1568.548

85 86.128 106-42-3 Q8 p-Xylene 2.663 2.304 2.071 726.622

86 88.939 95-47-6 Q8 o-Xylene 1.538 1.301 1.196 419.492

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C-644
Hydrocarbon Expert V4.7 Fri Aug 27 15:26:31 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000019.D\SIG2000019_FID2_B.CDF 26-Aug-10, 15:36:26

Sample: ODDB-91334 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91334

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 93.098 98-82-8 Q9 i-Propylbenzene 0.033 0.028 0.023 8.880

88 95.511 2051-30-1 I10 2,4-Dimethyloctane 0.007 0.007 0.004 1.770

89 96.560 103-65-1 Q9 n-Propylbenzene 0.650 0.562 0.446 176.160

90 97.418 620-14-4 Q9 1-Methyl-3-ethylbenzene 2.697 2.324 1.852 731.111

91 97.648 622-96-8 Q9 1-Methyl-4-ethylbenzene 1.258 1.088 0.864 340.892

92 98.273 108-67-8 Q9 1,3,5-Trimethylbenzene 1.623 1.397 1.115 439.949

93 98.72615869-85-9 I10 5-Methylnonane 0.011 0.011 0.006 2.827

94 98.91517301-94-8 I10 4-Methylnonane 0.027 0.027 0.016 6.863

95 99.120 I10 2,2,6-Trimethyloctane 0.253 0.259 0.147 64.384

96 99.353 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.898 0.760 0.617 243.466

97 99.570 5881-17-4 I10 3-Ethyloctane 0.008 0.008 0.005 1.975

98 99.891 5911-04-6 I10 3-Methylnonane 0.042 0.042 0.024 10.561

99 100.356 ? Unidentified 0.016 0.012 0.008 5.086

100 100.489 ? Unidentified 0.048 0.048 0.025 15.084

101 100.702 I11 C11-Isoparaffin-2 0.026 0.026 0.014 6.682

102 101.001 95-63-6 Q9 1,2,4-Trimethylbenzene 4.291 3.649 2.947 1163.089

103 101.167 ? Unidentified 0.034 0.036 0.020 10.723

104 101.288 ? Unidentified 0.019 0.020 0.011 6.145

105 102.33917302-01-1 I10 3-Ethyl-3-methylheptane 0.055 0.055 0.029 13.971

106 102.628 538-93-2 Q10 i-Butylbenzene 0.085 0.074 0.052 22.871

107 102.806 124-18-5 P10 n-Decane 0.039 0.040 0.023 9.913

108 102.904 ? Unidentified 0.032 0.027 0.019 10.000

109 103.201 ? Unidentified 0.015 0.015 0.008 4.695

110 103.853 526-73-8 Q9 1,2,3-Trimethylbenzene 0.425 0.354 0.292 115.180

111 104.234 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.010 0.009 0.006 2.715

112 104.413 I11 C11 Isoparaffin-4 0.009 0.009 0.005 2.283

113 104.618 99-87-6 Q10 1-Methyl-4-i-propylbenzene 0.065 0.057 0.040 17.541

114 105.047 J9 Indan 0.135 0.105 0.095 37.283

115 105.641 J10 Indene 0.368 0.285 0.257 101.478

116 106.356 I11 C11-Isoparaffin-7 0.161 0.162 0.085 41.103

117 106.550 141-93-5 Q10 1,3-Diethylbenzene 0.038 0.033 0.024 10.361

118 106.833 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 0.590 0.510 0.363 159.044

119 107.166 105-05-5 Q10 1,4-Diethylbenzene 0.245 0.212 0.151 66.072

120 107.385 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.190 0.161 0.117 51.327

121 107.628 135-01-3 Q10 1,2-Diethylbenzene 0.044 0.037 0.027 11.820

122 108.083 ? Unidentified 0.042 0.042 0.022 13.315

123 108.235 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.072 0.062 0.044 19.503

124 108.358 ? Unidentified 0.049 0.049 0.026 15.380

125 108.438 ? Unidentified 0.045 0.045 0.024 14.313

126 108.565 I11 C11- Isoparaffin-11 0.378 0.378 0.200 96.240

127 108.747 ? Unidentified 0.122 0.123 0.065 38.687

128 109.082 1758-88-9 Q10 1,4,Dimethyl-2-ethylbenzene 0.160 0.136 0.099 43.236

129 109.170 ? Unidentified 0.490 0.416 0.301 154.966

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C-645
Hydrocarbon Expert V4.7 Fri Aug 27 15:26:31 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000019.D\SIG2000019_FID2_B.CDF 26-Aug-10, 15:36:26

Sample: ODDB-91334 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91334

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 109.397 J10 2-Methylindan 0.073 0.057 0.046 20.219

131 109.744 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.471 0.401 0.289 126.903

132 110.288 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.354 0.296 0.218 95.396

133 110.712 ? Unidentified 0.010 0.010 0.006 3.315

134 110.907 693-61-8 K11 2-Undecene, (E)- 0.028 0.028 0.016 7.032

135 111.040 ? Unidentified 0.052 0.052 0.031 16.400

136 111.195 Q11 1-Methyl-4-t-butylbenzene 0.029 0.025 0.016 7.809

137 111.316 ? Unidentified 0.053 0.044 0.030 16.787

138 111.417 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.117 0.098 0.072 31.536

139 111.712 1120-21-4 P11 n-Undecane 0.034 0.034 0.018 8.659

140 111.865 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.045 0.038 0.025 12.199

141 111.975 ? Unidentified 0.024 0.020 0.014 7.681

142 112.351 Q10 1,2,4,5-Tetramethylbenzene 0.379 0.318 0.233 102.212

143 112.617 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.525 0.439 0.323 141.640

144 112.959 ? Unidentified 0.013 0.010 0.007 4.086

145 113.133 I12 C12 - IsoParaffin - 1 0.011 0.011 0.005 2.821

146 113.484 ? Unidentified 0.024 0.024 0.011 7.467

147 113.757 Q11 C11 - Aromatic - 3 0.064 0.054 0.036 17.194

148 113.947 874-35-1 H10 5-Methylindan 0.164 0.138 0.103 44.325

149 114.072 Q12 1,2-Di-i-propylbenzene 0.059 0.050 0.030 15.887

150 114.287 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.084 0.071 0.047 22.642

151 114.443 Q11 C11 - Aromatic - 4 0.048 0.040 0.026 12.772

152 114.697 824-22-6 J10 4-Methylindan 0.218 0.183 0.136 58.850

153 114.848 5161-04-6 Q11 Benzene, 1-methyl-4-(2-methylpropyl)-0.051 0.042 0.028 13.633

154 114.944 824-63-5 H10 2-Methylindan 0.163 0.136 0.101 43.821

155 115.147 ? Unidentified 0.015 0.013 0.009 4.850

156 115.260 538-68-1 Q11 n-Pentylbenzene 0.020 0.017 0.011 5.378

157 115.486 Q11 tert-Pentylbenzene 0.089 0.074 0.049 23.773

158 115.800 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.039 0.033 0.022 10.571

159 115.909 Q11 C11 - Aromatic - 7 0.049 0.043 0.028 13.270

160 116.370 100-18-5 Q12 1,4-Di-i-propylbenzene 0.074 0.062 0.037 19.711

161 116.814 91-20-3 G10 Naphthalene 0.171 0.124 0.110 48.212

162 117.008 J11 4,7-Dimethyl Indane 0.009 0.007 0.005 2.362

163 117.252 J11 1,1-Dimethyl Indane 0.023 0.018 0.013 6.308

164 117.414 J12 Dimethyl Indane - 1 0.010 0.008 0.006 2.783

165 117.594 7364-19-4 Q12 1t-Butyl-4-ethylbenzene 0.014 0.012 0.007 3.784

166 117.896 Q12 1,3-Di-n-propylbenzene 0.065 0.055 0.033 17.435

167 118.006 Q11 C11 - Aromatic - 11 0.037 0.033 0.021 9.982

168 118.560 Q11 C11 - Aromatic - 12 0.025 0.022 0.014 6.718

169 119.488 102-25-0 Q12 1,3,5-Triethylbenzene 0.007 0.005 0.003 1.752

170 123.441 91-57-6 G11 2-Methylnaphthalene 0.010 0.007 0.005 2.665

171 124.308 90-12-0 G11 1-Methylnaphthalene 0.005 0.004 0.003 1.418

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C-646
Hydrocarbon Expert V4.7 Fri Aug 27 15:26:31 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000019.D\SIG2000019_FID2_B.CDF 26-Aug-10, 15:36:26

Sample: ODDB-91334 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91334

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 10.023 106-97-8 n-Butane 2.216 2.852 3.148 552.220

18.116 109-66-0 n-Pentane 0.832 0.990 0.952 208.786

35.807 110-54-3 n-Hexane 0.415 0.469 0.398 104.594

58.060 142-82-5 n-Heptane 0.091 0.100 0.075 23.135

77.873 111-65-9 n-Octane 0.020 0.021 0.014 4.996

102.806 124-18-5 n-Decane 0.039 0.040 0.023 9.913

111.712 1120-21-4 n-Undecane 0.034 0.034 0.018 8.659

I-Paraffins 8.809 75-28-5 i-Butane 0.027 0.037 0.039 6.805

10.638 463-82-1 2,2-Dimethylpropane 0.028 0.035 0.031 6.902

15.097 78-78-4 i-Pentane 12.884 15.488 14.741 3232.534

23.093 75-83-2 2,2-Dimethylbutane 0.520 0.597 0.498 130.983

28.353 79-29-8 2,3-Dimethylbutane 1.877 2.113 1.798 472.714

29.474 107-83-5 2-Methylpentane 10.806 12.324 10.351 2721.985

32.101 96-14-0 3-Methylpentane 5.529 6.199 5.296 1392.728

42.246 108-08-7 2,4-Dimethylpentane 0.149 0.165 0.123 37.719

50.665 591-76-4 2-Methylhexane 0.407 0.447 0.335 102.965

52.498 589-34-4 3-Methylhexane 0.277 0.300 0.228 70.106

72.051 592-27-8 2-Methylheptane 0.017 0.018 0.012 4.247

72.304 589-53-7 4-Methylheptane 0.009 0.010 0.007 2.396

73.365 589-81-1 3-Methylheptane 0.018 0.019 0.013 4.670

95.511 2051-30-1 2,4-Dimethyloctane 0.007 0.007 0.004 1.770

98.72615869-85-9 5-Methylnonane 0.011 0.011 0.006 2.827

98.91517301-94-8 4-Methylnonane 0.027 0.027 0.016 6.863

99.120 2,2,6-Trimethyloctane 0.253 0.259 0.147 64.384

99.570 5881-17-4 3-Ethyloctane 0.008 0.008 0.005 1.975

99.891 5911-04-6 3-Methylnonane 0.042 0.042 0.024 10.561

100.702 C11-Isoparaffin-2 0.026 0.026 0.014 6.682

102.33917302-01-1 3-Ethyl-3-methylheptane 0.055 0.055 0.029 13.971

104.413 C11 Isoparaffin-4 0.009 0.009 0.005 2.283

106.356 C11-Isoparaffin-7 0.161 0.162 0.085 41.103

108.565 C11- Isoparaffin-11 0.378 0.378 0.200 96.240

113.133 C12 - IsoParaffin - 1 0.011 0.011 0.005 2.821

Aromatics

Mono-Aromatics 45.645 71-42-3 Benzene 0.712 0.603 0.752 197.767

69.076 108-88-3 Toluene 12.074 10.373 10.817 3319.113

84.745 100-41-4 Ethylbenzene 2.190 1.881 1.703 597.451

85.987 108-38-3 m-Xylene 5.749 4.955 4.470 1568.548

86.128 106-42-3 p-Xylene 2.663 2.304 2.071 726.622

88.939 95-47-6 o-Xylene 1.538 1.301 1.196 419.492

93.098 98-82-8 i-Propylbenzene 0.033 0.028 0.023 8.880

96.560 103-65-1 n-Propylbenzene 0.650 0.562 0.446 176.160

97.418 620-14-4 1-Methyl-3-ethylbenzene 2.697 2.324 1.852 731.111

97.648 622-96-8 1-Methyl-4-ethylbenzene 1.258 1.088 0.864 340.892

98.273 108-67-8 1,3,5-Trimethylbenzene 1.623 1.397 1.115 439.949

99.353 611-14-3 1-Methyl-2-ethylbenzene 0.898 0.760 0.617 243.466

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C-647
Hydrocarbon Expert V4.7 Fri Aug 27 15:26:31 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000019.D\SIG2000019_FID2_B.CDF 26-Aug-10, 15:36:26

Sample: ODDB-91334 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91334

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 101.001 95-63-6 1,2,4-Trimethylbenzene 4.291 3.649 2.947 1163.089

102.628 538-93-2 i-Butylbenzene 0.085 0.074 0.052 22.871

103.853 526-73-8 1,2,3-Trimethylbenzene 0.425 0.354 0.292 115.180

104.234 535-77-3 1-Methyl-3-i-propylbenzene 0.010 0.009 0.006 2.715

104.618 99-87-6 1-Methyl-4-i-propylbenzene 0.065 0.057 0.040 17.541

106.550 141-93-5 1,3-Diethylbenzene 0.038 0.033 0.024 10.361

106.833 1074-43-7 1-Methyl-3-n-propylbenzene 0.590 0.510 0.363 159.044

107.166 105-05-5 1,4-Diethylbenzene 0.245 0.212 0.151 66.072

107.385 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.190 0.161 0.117 51.327

107.628 135-01-3 1,2-Diethylbenzene 0.044 0.037 0.027 11.820

108.235 1074-17-5 1-Methyl-2-n-propylbenzene 0.072 0.062 0.044 19.503

109.082 1758-88-9 1,4,Dimethyl-2-ethylbenzene 0.160 0.136 0.099 43.236

109.744 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.471 0.401 0.289 126.903

110.288 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.354 0.296 0.218 95.396

111.195 1-Methyl-4-t-butylbenzene 0.029 0.025 0.016 7.809

111.417 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.117 0.098 0.072 31.536

111.865 4218-48-8 1-Ethyl-4-i-propylbenzene 0.045 0.038 0.025 12.199

112.351 1,2,4,5-Tetramethylbenzene 0.379 0.318 0.233 102.212

112.617 527-53-7 1,2,3,5-Tetramethylbenzene 0.525 0.439 0.323 141.640

113.757 C11 - Aromatic - 3 0.064 0.054 0.036 17.194

114.072 1,2-Di-i-propylbenzene 0.059 0.050 0.030 15.887

114.287 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.084 0.071 0.047 22.642

114.443 C11 - Aromatic - 4 0.048 0.040 0.026 12.772

114.848 5161-04-6 Benzene, 1-methyl-4-(2-methylpropyl)-0.051 0.042 0.028 13.633

115.260 538-68-1 n-Pentylbenzene 0.020 0.017 0.011 5.378

115.486 tert-Pentylbenzene 0.089 0.074 0.049 23.773

115.800 577-55-9 1-Methyl-2-n-butylbenzene 0.039 0.033 0.022 10.571

115.909 C11 - Aromatic - 7 0.049 0.043 0.028 13.270

116.370 100-18-5 1,4-Di-i-propylbenzene 0.074 0.062 0.037 19.711

117.594 7364-19-4 1t-Butyl-4-ethylbenzene 0.014 0.012 0.007 3.784

117.896 1,3-Di-n-propylbenzene 0.065 0.055 0.033 17.435

118.006 C11 - Aromatic - 11 0.037 0.033 0.021 9.982

118.560 C11 - Aromatic - 12 0.025 0.022 0.014 6.718

119.488 102-25-0 1,3,5-Triethylbenzene 0.007 0.005 0.003 1.752

Naphthalenes 116.814 91-20-3 Naphthalene 0.171 0.124 0.110 48.212

123.441 91-57-6 2-Methylnaphthalene 0.010 0.007 0.005 2.665

124.308 90-12-0 1-Methylnaphthalene 0.005 0.004 0.003 1.418

Naphtheno/Olefino-Benzs 113.947 874-35-1 5-Methylindan 0.164 0.138 0.103 44.325

114.944 824-63-5 2-Methylindan 0.163 0.136 0.101 43.821

Indenes 105.047 Indan 0.135 0.105 0.095 37.283

105.641 Indene 0.368 0.285 0.257 101.478

109.397 2-Methylindan 0.073 0.057 0.046 20.219

114.697 824-22-6 4-Methylindan 0.218 0.183 0.136 58.850

117.008 4,7-Dimethyl Indane 0.009 0.007 0.005 2.362

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C-648
Hydrocarbon Expert V4.7 Fri Aug 27 15:26:31 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000019.D\SIG2000019_FID2_B.CDF 26-Aug-10, 15:36:26

Sample: ODDB-91334 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91334

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Indenes 117.252 1,1-Dimethyl Indane 0.023 0.018 0.013 6.308

117.414 Dimethyl Indane - 1 0.010 0.008 0.006 2.783

Naphthenes

Mono-Naphthenes 27.607 287-92-3 Cyclopentane 0.375 0.374 0.441 96.657

40.674 96-37-7 Methylcyclopentane 0.746 0.743 0.732 192.624

47.557 110-82-7 Cyclohexane 0.065 0.062 0.064 16.744

53.360 1759-58-6 1t,3-Dimethylcyclopentane 0.096 0.096 0.081 24.869

53.946 2532-58-3 1c,3-Dimethylcyclopentane 0.064 0.064 0.054 16.633

54.569 822-50-4 1t,2-Dimethylcyclopentane 0.058 0.058 0.049 15.086

59.65716491-15-9 Cyclopentene, 1,5-dimethyl- 0.018 0.018 0.015 4.736

61.506 108-87-2 Methylcyclohexane 0.042 0.040 0.035 10.727

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.623 115-11-7 Isobutene 0.017 0.021 0.024 4.281

9.665 106-98-9 Butene-1 0.018 0.023 0.027 4.773

10.510 624-64-6 t-Butene-2 0.075 0.093 0.111 19.435

11.251 590-18-1 c-Butene-2 0.089 0.107 0.131 22.971

16.734 109-67-1 Pentene-1 0.345 0.401 0.406 88.991

19.239 646-04-8 t-Pentene-2 0.874 1.005 1.029 225.599

20.268 627-20-3 c-Pentene-2 0.479 0.544 0.564 123.646

33.460 592-41-6 Hexene-1 0.164 0.180 0.161 42.260

36.44313269-52-8 t-Hexene-3 0.269 0.293 0.264 69.349

36.921 4050-45-7 t-Hexene-2 0.411 0.449 0.404 106.182

38.748 7688-21-3 c-Hexene-2 0.219 0.236 0.215 56.473

55.475 592-76-7 Heptene-1 0.028 0.030 0.024 7.257

57.33814686-14-7 t-Heptene-3 0.032 0.034 0.027 8.202

58.280 7642-10-6 c-Heptene-3 0.024 0.026 0.020 6.264

59.18214686-13-6 t-Heptene-2 0.012 0.013 0.010 3.067

110.907 693-61-8 2-Undecene, (E)- 0.028 0.028 0.016 7.032

Iso-Olefins 13.455 563-45-1 3-Methylbutene-1 0.184 0.218 0.216 47.445

17.587 563-46-2 2-Methylbutene-1 0.524 0.600 0.617 135.298

20.950 513-35-9 2-Methylbutene-2 1.074 1.207 1.264 277.069

29.207 691-38-3 4-Methyl-c-pentene-2 0.046 0.051 0.045 11.836

29.857 674-76-0 4-Methyl-t-pentene-2 0.134 0.148 0.132 34.623

33.239 763-29-1 2-Methylpentene-1 0.230 0.250 0.226 59.348

35.645 760-21-4 2-Ethylbutene-1 0.074 0.080 0.073 19.187

37.413 625-27-4 2-Methylpentene-2 0.349 0.376 0.342 89.939

37.828 922-62-3 3-Methyl-c-pentene-2 0.269 0.287 0.264 69.485

40.094 3404-73-7 3,3-Dimethylpentene-1 0.316 0.335 0.266 81.530

42.544 594-56-9 2,3,3-Trimethylbutene-1 0.010 0.010 0.008 2.467

46.649 3404-61-3 3-Methylhexene-1 0.016 0.017 0.013 4.014

47.234 3524-73-0 5-Methylhexene-1 0.023 0.024 0.019 5.891

49.27815840-60-5 2-Methyl-c-hexene-3 0.041 0.044 0.035 10.648

49.626 3769-23-1 4-Methylhexene-1 0.011 0.012 0.009 2.828

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C-649
Hydrocarbon Expert V4.7 Fri Aug 27 15:26:31 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000019.D\SIG2000019_FID2_B.CDF 26-Aug-10, 15:36:26

Sample: ODDB-91334 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91334

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Iso-Olefins 50.272 3404-55-5 4-Methyl-t/c-hexene-2 0.052 0.055 0.043 13.320

54.849 C7 - Iso-Olefin - 2 0.023 0.024 0.019 5.866

56.808 4914-89-0 3-Methyl-c-hexene-3 0.014 0.015 0.012 3.625

57.690 6094-02-6 2-Methylhexene-1 0.056 0.060 0.047 14.491

58.555 2738-19-4 2-Methyl-2-hexene 0.025 0.026 0.021 6.456

58.79910574-36-4 3-Methyl-c-hexene-2 0.019 0.020 0.016 5.028

60.08020710-38-8 3-Methyl-t-hexene-2 0.014 0.015 0.012 3.723

60.865 4914-91-4 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.013 0.011 3.326

Naphtheno-Olefins 22.540 1574-41-0 1,3-Cyclopentadiene 0.007 0.008 0.009 1.931

25.745 142-29-0 Cyclopentene 0.203 0.195 0.246 53.820

37.048 1120-62-3 3-Methylcyclopentene 0.104 0.101 0.104 26.770

45.839 693-89-0 1-Methylcyclopentene 0.366 0.350 0.368 96.741

51.158 110-83-8 Cyclohexene 0.045 0.042 0.046 11.738

Di-Olefins 18.633 78-79-5 2-Methyl-1,3-Butadiene 0.011 0.012 0.013 2.853

21.279 2004-70-8 1t,3-Pentadiene 0.016 0.018 0.020 4.276

45.435 1528-30-9 C6-Diolefin-1 0.015 0.015 0.015 3.958

Oxygenates 13.050 64-17-5 Ethanol 10.286 9.710 18.431 1093.007

26.904 71-23-8 n-Propanol 0.077 0.072 0.106 13.895

48.061 71-36-3 n-Butanol 0.056 0.052 0.063 10.967

Unidentified 19.882 Unidentified 0.006 0.007 0.007 1.934

27.005 Unidentified 0.062 0.069 0.060 19.450

28.748 Unidentified 0.054 0.054 0.051 17.060

50.847 Unidentified 0.020 0.022 0.017 6.343

63.401 Unidentified 0.024 0.025 0.018 7.719

100.356 Unidentified 0.016 0.012 0.008 5.086

100.489 Unidentified 0.048 0.048 0.025 15.084

101.167 Unidentified 0.034 0.036 0.020 10.723

101.288 Unidentified 0.019 0.020 0.011 6.145

102.904 Unidentified 0.032 0.027 0.019 10.000

103.201 Unidentified 0.015 0.015 0.008 4.695

108.083 Unidentified 0.042 0.042 0.022 13.315

108.358 Unidentified 0.049 0.049 0.026 15.380

108.438 Unidentified 0.045 0.045 0.024 14.313

108.747 Unidentified 0.122 0.123 0.065 38.687

109.170 Unidentified 0.490 0.416 0.301 154.966

110.712 Unidentified 0.010 0.010 0.006 3.315

111.040 Unidentified 0.052 0.052 0.031 16.400

111.316 Unidentified 0.053 0.044 0.030 16.787

111.975 Unidentified 0.024 0.020 0.014 7.681

112.959 Unidentified 0.013 0.010 0.007 4.086

113.484 Unidentified 0.024 0.024 0.011 7.467

115.147 Unidentified 0.015 0.013 0.009 4.850

Plus

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C-650
Hydrocarbon Expert V4.7 Fri Aug 27 15:26:31 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000019.D\SIG2000019_FID2_B.CDF 26-Aug-10, 15:36:26

Sample: ODDB-91334 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91334

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000019.D\SIG2000019_FID2_B.CDF

20.0 15.0 10.0 5.0 0.0

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

Ethanol

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

Unidentified

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

1,3-Cyclopentadiene

2,2-Dimethylbutane

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C-651
Hydrocarbon Expert V4.7 Fri Aug 27 15:26:31 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000019.D\SIG2000019_FID2_B.CDF 26-Aug-10, 15:36:26

Sample: ODDB-91334 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91334

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000019.D\SIG2000019_FID2_B.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

n-Propanol Unidentified

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

2-Ethylbutene-1 n-Hexane

t-Hexene-3

t-Hexene-2 3-Methylcyclopentene

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane 2,3,3-Trimethylbutene-1

C6-Diolefin-1 Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1

Cyclohexane

n-Butanol

2-Methyl-c-hexene-3

4-Methylhexene-1

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C-652
Hydrocarbon Expert V4.7 Fri Aug 27 15:26:31 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000019.D\SIG2000019_FID2_B.CDF 26-Aug-10, 15:36:26

Sample: ODDB-91334 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91334

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000019.D\SIG2000019_FID2_B.CDF

70.0 65.0 60.0 55.0 50.0

4-Methyl-t/c-hexene-2

2-Methylhexane Unidentified Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane C7 - Iso-Olefin - 2

Heptene-1

3-Methyl-c-hexene-3

t-Heptene-3

2-Methylhexene-1

n-Heptane c-Heptene-3 2-Methyl-2-hexene 3-Methyl-c-hexene-2

t-Heptene-2

Cyclopentene, 1,5-dimethyl3-Methyl-t-hexene-2

2-Pentene, 3,4-dimethyl-, (Z)-

Methylcyclohexane

Unidentified

Toluene

2-Methylheptane 4-Methylheptane

3-Methylheptane

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C-653
Hydrocarbon Expert V4.7 Fri Aug 27 15:26:31 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000019.D\SIG2000019_FID2_B.CDF 26-Aug-10, 15:36:26

Sample: ODDB-91334 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91334

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000019.D\SIG2000019_FID2_B.CDF

95.0 90.0 85.0 80.0 75.0

n-Octane

Ethylbenzene

m-Xylene p-Xylene

o-Xylene

i-Propylbenzene

2,4-Dimethyloctane

n-Propylbenzene

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

5-Methylnonane 4-Methylnonane 2,2,6-Trimethyloctane 1-Methyl-2-ethylbenzene 3-Ethyloctane

3-Methylnonane

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C-654
Hydrocarbon Expert V4.7 Fri Aug 27 15:26:31 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000019.D\SIG2000019_FID2_B.CDF 26-Aug-10, 15:36:26

Sample: ODDB-91334 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91334

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000019.D\SIG2000019_FID2_B.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified

C11-Isoparaffin-2 1,2,4-Trimethylbenzene Unidentified

3-Ethyl-3-methylheptane i-Butylbenzene n-Decane Unidentified Unidentified

1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene C11 Isoparaffin-4 1-Methyl-4-i-propylbenzene

Indan

Indene

C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene

1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

Unidentified 1-Methyl-2-n-propylbenzene

C11- Isoparaffin-11 Unidentified

1,4,Dimethyl-2-ethylbenzene Unidentified 2-Methylindan

1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

Unidentified 2-Undecene, (E)- Unidentified 1-Methyl-4-t-butylbenzene Unidentified 1,2-Dimethyl-3-ethylbenzene n-Undecane Unidentified 1-Ethyl-4-i-propylbenzene

1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene

Unidentified C12 - IsoParaffin - 1

Unidentified C11 - Aromatic - 3 5-Methylindan 1,2-Di-i-propylbenzene

C11 - Aromatic - 4 1-methyl-4-(1-methylpropyl)be

4-Methylindan Benzene, 1-methyl-4-(2-methylpropyl)- 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene

1-Methyl-2-n-butylbenzene C11 - Aromatic - 7

1,4-Di-i-propylbenzene

Naphthalene 4,7-Dimethyl Indane 1,1-Dimethyl Indane Dimethyl Indane - 1 1t-Butyl-4-ethylbenzene

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

C11 - Aromatic - 12

1,3,5-Triethylbenzene

2-Methylnaphthalene

1-Methylnaphthalene

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C-655
Hydrocarbon Expert V4.7 Fri Aug 27 15:26:31 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000019.D\SIG2000019_FID2_B.CDF 26-Aug-10, 15:36:26

Sample: ODDB-91334 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91334

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000019.D\SIG2000019_FID2_B.CDF

145.0 140.0 135.0 130.0 125.0

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C-656
Hydrocarbon Expert V4.7 Fri Aug 27 15:05:52 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91335 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91335

LIMS Id: 

Summary by Group

Recovery = 100.00

Group %Wgt %Vol %Mol

Paraffin 4.688 5.657 4.647

I-Paraffins 19.280 22.413 16.416

Aromatics 42.279 37.515 30.678

Mono-Aromatics 40.739 36.253 29.721

Naphthalenes 0.183 0.138 0.110

Naphtheno/Olefino-Benzs 0.325 0.283 0.191

Indenes 1.031 0.842 0.656

Naphthenes 3.320 3.381 2.938

Mono-Naphthenes 3.320 3.381 2.938

Di/Bicyclo-Naphthenes 0.000 0.000 0.000

Olefins 7.121 8.142 7.242

n-Olefins 2.939 3.445 3.081

Iso-Olefins 3.447 3.961 3.423

Naphtheno-Olefins 0.693 0.691 0.694

Di-Olefins 0.041 0.045 0.044

Oxygenates 21.875 21.438 36.824

Unidentified 1.438 1.453 1.255

Plus 0.000 0.000 0.000

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C-657
Hydrocarbon Expert V4.7 Fri Aug 27 15:05:52 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91335 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91335

LIMS Id: 

Summary by Carbon

Recovery = 100.00

C# %Wgt %Vol %Mol

C2 21.748 21.315 36.673

C3 0.075 0.073 0.098

C4 0.867 1.127 1.153

C5 9.339 11.313 10.185

C6 16.286 18.463 14.855

C7 16.039 14.994 13.321

C8 13.867 12.747 10.049

C9 11.815 10.625 7.607

C10 7.003 6.446 4.035

C11 1.266 1.219 0.647

C12 0.257 0.224 0.123

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C-658
Hydrocarbon Expert V4.7 Fri Aug 27 15:05:52 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91335 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91335

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Paraffin C3 0.002 0.003 0.004

C4 0.597 0.797 0.797

C5 1.763 2.178 1.899

C6 1.573 1.845 1.418

C7 0.376 0.425 0.292

C8 0.201 0.221 0.136

C9 0.110 0.118 0.066

C10 0.040 0.042 0.022

C11 0.027 0.028 0.014

I-Paraffins C4 0.025 0.035 0.034

C5 3.668 4.578 3.949

C6 9.602 11.302 8.656

C7 1.318 1.498 1.022

C8 1.536 1.672 1.044

C9 0.671 0.730 0.406

C10 1.824 1.936 0.988

C11 0.631 0.655 0.313

C12 0.005 0.005 0.002

Mono-Aromatics C6 0.734 0.646 0.730

C7 12.625 11.261 10.644

C8 11.926 10.650 8.727

C9 10.809 9.596 6.987

C10 3.834 3.389 2.219

C11 0.569 0.501 0.298

C12 0.242 0.211 0.116

Naphthalenes C10 0.169 0.128 0.103

C11 0.014 0.011 0.008

Naphtheno/Olefino-Benzs C10 0.325 0.283 0.191

Indenes C9 0.219 0.175 0.144

C10 0.794 0.651 0.503

C11 0.009 0.007 0.005

C12 0.010 0.008 0.005

Mono-Naphthenes C5 0.305 0.316 0.338

C6 1.822 1.858 1.682

C7 0.965 0.980 0.763

C8 0.204 0.204 0.141

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C-659
Hydrocarbon Expert V4.7 Fri Aug 27 15:05:52 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91335 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91335

LIMS Id: 

Composite by Carbon

Recovery = 100.00

Group C# %Wgt %Vol %Mol

Mono-Naphthenes C9 0.007 0.006 0.004

C10 0.018 0.018 0.010

n-Olefins C4 0.191 0.242 0.265

C5 1.616 1.926 1.790

C6 1.017 1.151 0.939

C7 0.099 0.109 0.078

C11 0.017 0.017 0.009

Iso-Olefins C5 1.762 2.084 1.951

C6 1.044 1.172 0.964

C7 0.641 0.706 0.508

Naphtheno-Olefins C5 0.200 0.201 0.228

C6 0.493 0.490 0.466

Di-Olefins C5 0.026 0.030 0.030

C7 0.015 0.015 0.014

Oxygenates C2 21.748 21.315 36.673

C3 0.073 0.070 0.094

C4 0.054 0.053 0.057

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C-660
Hydrocarbon Expert V4.7 Fri Aug 27 15:05:52 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91335 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91335

LIMS Id: 

Calculated Boiling Point

Recovery = 100.00

%Off WBP(F) VBP(F)

IBP 28.34 26.13

5% 83.73 81.27

10% 111.94 97.25

15% 139.18 137.76

20% 145.62 140.07

25% 161.49 152.27

30% 172.44 169.42

35% 172.68 172.46

40% 172.93 172.72

45% 173.18 172.97

50% 196.17 173.22

55% 230.80 201.59

60% 230.94 230.82

65% 231.16 230.98

70% 278.20 257.01

75% 281.80 281.22

80% 318.15 291.63

85% 327.67 323.18

90% 335.83 334.98

95% 363.20 362.49

FBP 404.60 404.60

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C-661
Hydrocarbon Expert V4.7 Fri Aug 27 15:05:52 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91335 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91335

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

1 7.553 74-98-6 P3 Propane 0.002 0.003 0.004 0.583

2 8.809 75-28-5 I4 i-Butane 0.025 0.035 0.034 6.870

3 9.621 115-11-7 K4 Isobutene 0.016 0.021 0.022 4.502

4 9.662 106-98-9 K4 Butene-1 0.018 0.023 0.024 4.962

5 10.021 106-97-8 P4 n-Butane 0.597 0.797 0.797 162.290

6 10.507 624-64-6 K4 t-Butene-2 0.072 0.092 0.100 20.328

7 10.635 463-82-1 I5 2,2-Dimethylpropane 0.009 0.012 0.010 2.601

8 11.247 590-18-1 K4 c-Butene-2 0.085 0.106 0.118 24.035

9 13.125 64-17-5 X2 Ethanol 21.748 21.315 36.673 2523.196

10 13.445 563-45-1 C5 3-Methylbutene-1 0.245 0.302 0.271 68.928

11 15.073 78-78-4 I5 i-Pentane 3.658 4.566 3.939 1002.166

12 16.725 109-67-1 K5 Pentene-1 0.328 0.396 0.363 92.420

13 17.577 563-46-2 C5 2-Methylbutene-1 0.498 0.592 0.551 140.212

14 18.107 109-66-0 P5 n-Pentane 1.763 2.178 1.899 483.060

15 18.621 78-79-5 E5 2-Methyl-1,3-Butadiene 0.011 0.012 0.012 3.164

16 19.228 646-04-8 K5 t-Pentene-2 0.832 0.992 0.921 234.391

17 19.873 ? Unidentified 0.005 0.006 0.006 1.873

18 20.261 627-20-3 K5 c-Pentene-2 0.456 0.538 0.505 128.401

19 20.941 513-35-9 C5 2-Methylbutene-2 1.019 1.190 1.129 287.222

20 21.266 2004-70-8 E5 1t,3-Pentadiene 0.015 0.018 0.018 4.495

21 22.527 1574-41-0 B5 1,3-Cyclopentadiene 0.007 0.008 0.008 1.979

22 23.085 75-83-2 I6 2,2-Dimethylbutane 0.296 0.353 0.267 81.465

23 25.736 142-29-0 B5 Cyclopentene 0.193 0.193 0.220 55.939

24 26.899 71-23-8 X3 n-Propanol 0.073 0.070 0.094 14.306

25 26.983 ? Unidentified 0.059 0.068 0.054 20.285

26 27.596 287-92-3 M5 Cyclopentane 0.305 0.316 0.338 85.857

27 28.336 79-29-8 I6 2,3-Dimethylbutane 1.015 1.187 0.915 279.232

28 28.726 ? Unidentified 0.055 0.057 0.048 18.827

29 29.196 691-38-3 C6 4-Methyl-c-pentene-2 0.044 0.050 0.040 12.346

30 29.429 107-83-5 I6 2-Methylpentane 5.593 6.623 5.042 1538.314

31 29.838 674-76-0 C6 4-Methyl-t-pentene-2 0.128 0.147 0.118 35.957

32 32.074 96-14-0 I6 3-Methylpentane 2.697 3.140 2.431 741.781

33 33.221 763-29-1 C6 2-Methylpentene-1 0.220 0.249 0.203 62.043

34 33.446 592-41-6 K6 Hexene-1 0.158 0.180 0.146 44.508

35 35.633 760-21-4 C6 2-Ethylbutene-1 0.064 0.071 0.059 17.898

36 35.799 110-54-3 P6 n-Hexane 1.573 1.845 1.418 432.616

37 36.43513269-52-8 K6 t-Hexene-3 0.257 0.291 0.237 72.378

38 36.909 4050-45-7 K6 t-Hexene-2 0.394 0.446 0.363 110.939

39 37.033 1120-62-3 B6 3-Methylcyclopentene 0.098 0.099 0.093 27.611

40 37.401 625-27-4 C6 2-Methylpentene-2 0.333 0.372 0.307 93.747

41 37.815 922-62-3 C6 3-Methyl-c-pentene-2 0.256 0.284 0.237 72.243

42 38.737 7688-21-3 K6 c-Hexene-2 0.209 0.233 0.193 58.832

43 40.080 3404-73-7 C7 3,3-Dimethylpentene-1 0.305 0.336 0.242 86.052

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C-662
Hydrocarbon Expert V4.7 Fri Aug 27 15:05:52 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91335 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91335

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

44 40.665 96-37-7 M6 Methylcyclopentane 1.205 1.245 1.112 339.547

45 42.235 108-08-7 I7 2,4-Dimethylpentane 0.207 0.238 0.161 57.207

46 42.525 594-56-9 C7 2,3,3-Trimethylbutene-1 0.013 0.015 0.011 3.749

47 42.773 464-06-2 I7 2,2,3-Trimethylbutane 0.020 0.022 0.015 5.432

48 45.422 1528-30-9 E7 C6-Diolefin-1 0.015 0.015 0.014 4.177

49 45.631 71-42-3 Q6 Benzene 0.734 0.646 0.730 222.725

50 45.828 693-89-0 B6 1-Methylcyclopentene 0.351 0.349 0.332 101.379

51 46.634 3404-61-3 C7 3-Methylhexene-1 0.016 0.017 0.012 4.389

52 47.225 3524-73-0 C7 5-Methylhexene-1 0.043 0.048 0.034 12.223

53 47.550 110-82-7 M6 Cyclohexane 0.617 0.613 0.569 173.801

54 48.053 71-36-3 X4 n-Butanol 0.054 0.053 0.057 11.594

55 49.26815840-60-5 C7 2-Methyl-c-hexene-3 0.040 0.044 0.031 11.166

56 49.614 3769-23-1 C7 4-Methylhexene-1 0.011 0.012 0.009 3.054

57 50.261 3404-55-5 C7 4-Methyl-t/c-hexene-2 0.050 0.055 0.039 14.019

58 50.654 591-76-4 I7 2-Methylhexane 0.651 0.742 0.505 179.828

59 50.835 ? Unidentified 0.041 0.046 0.034 14.321

60 51.147 110-83-8 B6 Cyclohexene 0.044 0.042 0.041 12.323

61 52.488 589-34-4 I7 3-Methylhexane 0.440 0.495 0.341 121.523

62 53.349 1759-58-6 M7 1t,3-Dimethylcyclopentane 0.137 0.141 0.108 38.547

63 53.934 2532-58-3 M7 1c,3-Dimethylcyclopentane 0.102 0.106 0.081 28.707

64 54.556 822-50-4 M7 1t,2-Dimethylcyclopentane 0.131 0.134 0.103 36.801

65 54.838 C7 C7 - Iso-Olefin - 2 0.022 0.024 0.018 6.235

66 55.140 540-84-1 I8 2,2,4-Trimethylpentane 0.054 0.060 0.037 14.924

67 55.464 592-76-7 K7 Heptene-1 0.028 0.031 0.022 7.935

68 56.799 4914-89-0 C7 3-Methyl-c-hexene-3 0.014 0.015 0.011 3.819

69 57.32814686-14-7 K7 t-Heptene-3 0.031 0.034 0.025 8.787

70 57.679 6094-02-6 C7 2-Methylhexene-1 0.056 0.062 0.044 15.773

71 58.051 142-82-5 P7 n-Heptane 0.376 0.425 0.292 103.846

72 58.270 7642-10-6 K7 c-Heptene-3 0.024 0.027 0.019 6.871

73 58.545 2738-19-4 C7 2-Methyl-2-hexene 0.026 0.028 0.020 7.199

74 58.78810574-36-4 C7 3-Methyl-c-hexene-2 0.019 0.021 0.015 5.494

75 59.17014686-13-6 K7 t-Heptene-2 0.015 0.017 0.012 4.257

76 59.64616491-15-9 M7 Cyclopentene, 1,5-dimethyl- 0.017 0.018 0.014 4.867

77 60.07320710-38-8 C7 3-Methyl-t-hexene-2 0.014 0.015 0.011 4.032

78 60.857 4914-91-4 C7 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.014 0.010 3.544

79 61.513 108-87-2 M7 Methylcyclohexane 0.542 0.544 0.428 152.583

80 62.456 4516-69-2 M8 1,1,3-Trimethylcyclopentane 0.015 0.015 0.010 4.114

81 62.845 590-73-8 I8 2,2-Dimethylhexane 0.012 0.014 0.008 3.451

82 63.356 ? Unidentified 0.057 0.062 0.041 19.817

83 64.289 1640-89-7 M7 Ethylcyclopentane 0.036 0.037 0.029 10.269

84 64.942 564-02-3 I8 2,2,3-Trimethylpentane 0.064 0.069 0.043 17.634

85 65.167 592-13-2 I8 2,5-Dimethylhexane 0.133 0.148 0.090 36.796

86 65.503 589-43-5 I8 2,4-Dimethylhexane 0.123 0.136 0.084 34.156

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C-663
Hydrocarbon Expert V4.7 Fri Aug 27 15:05:52 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91335 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91335

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

87 66.343 4850-28-6 M8 1c,2t,4-Trimethylcyclopentane 0.014 0.014 0.010 3.951

88 67.85915890-40-1 M8 1t,2c,3-Trimethylcyclopentane 0.012 0.012 0.008 3.360

89 68.478 565-75-3 I8 2,3,4-Trimethylpentane 0.662 0.712 0.450 183.050

90 69.077 108-88-3 Q7 Toluene 12.625 11.261 10.644 3789.205

91 70.790 584-94-1 I8 2,3-Dimethylhexane 0.185 0.201 0.126 51.197

92 72.044 592-27-8 I8 2-Methylheptane 0.105 0.116 0.071 29.018

93 72.303 589-53-7 I8 4-Methylheptane 0.058 0.063 0.039 15.932

94 72.447 ? Unidentified 0.017 0.019 0.012 6.014

95 73.222 M8 1,3-dimethyl-t-cyclohexane 0.070 0.070 0.048 19.722

96 73.358 589-81-1 I8 3-Methylheptane 0.093 0.102 0.063 25.804

97 73.558 619-99-8 I8 3-Ethylhexane 0.047 0.051 0.032 12.962

98 74.457 ? Unidentified 0.011 0.011 0.008 3.870

99 75.247 3522-94-9 I9 2,2,5-Trimethylhexane 0.427 0.467 0.259 118.324

100 76.528 2207-03-6 M8 1t,3-Dimethylcyclohexane 0.031 0.030 0.021 8.620

101 77.868 111-65-9 P8 n-Octane 0.201 0.221 0.136 55.524

102 78.821 M8 C8 - MonoNaph - 3 0.015 0.015 0.010 4.185

103 80.350 1069-53-0 I9 2,3,5-Trimethylhexane 0.077 0.083 0.047 21.429

104 81.519 1071-26-7 I9 2,4-Dimethylheptane 0.018 0.020 0.011 5.059

105 82.172 1678-91-7 M8 Ethylcyclohexane 0.048 0.047 0.033 13.412

106 82.475 1072-05-5 I9 2,6-Dimethylheptane 0.032 0.034 0.019 8.764

107 82.974 ? Unidentified 0.009 0.009 0.006 3.065

108 83.407 I9 2,5-Dimethylheptane 0.049 0.053 0.030 13.705

109 84.740 100-41-4 Q8 Ethylbenzene 2.131 1.901 1.559 634.694

110 85.150 ? Unidentified 0.009 0.009 0.005 3.004

111 85.985 108-38-3 Q8 m-Xylene 5.649 5.055 4.134 1682.769

112 86.126 106-42-3 Q8 p-Xylene 2.623 2.356 1.920 781.401

113 87.275 2216-34-4 I9 4-Methyloctane 0.019 0.020 0.011 5.163

114 87.407 3221-61-2 I9 2-Methyloctane 0.025 0.027 0.015 6.835

115 88.269 2216-33-3 I9 3-Methyloctane 0.024 0.026 0.015 6.708

116 88.745 ? Unidentified 0.031 0.035 0.019 10.638

117 88.935 95-47-6 Q8 o-Xylene 1.523 1.338 1.115 453.684

118 89.320 I10 C10 - IsoParaffin - 1 0.099 0.105 0.054 27.411

119 89.911 M9 trans-1,3-Diethylcyclopentane 0.007 0.006 0.004 1.997

120 90.16414720-74-2 I10 2,2,4-trimethylheptane 0.073 0.078 0.040 20.361

121 91.730 111-84-2 P9 n-Nonane 0.110 0.118 0.066 30.373

122 93.094 98-82-8 Q9 i-Propylbenzene 0.030 0.027 0.020 8.966

123 93.840 ? Unidentified 0.060 0.064 0.033 20.831

124 94.06415869-87-1 I10 2,2-Dimethyloctane 0.022 0.023 0.012 6.080

125 94.524 ? Unidentified 0.005 0.004 0.419 1.862

126 94.524 ? Unidentified 0.005 0.006 0.003 1.862

127 94.86115869-89-3 I10 2,5-Dimethyloctane 0.024 0.025 0.013 6.623

128 95.325 2040-95-1 I10 2,7-Dimethyloctane 0.018 0.019 0.010 5.110

129 95.507 2051-30-1 I10 2,4-Dimethyloctane 0.080 0.085 0.044 22.279

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C-664
Hydrocarbon Expert V4.7 Fri Aug 27 15:05:52 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91335 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91335

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

130 95.898 I10 2,6-Dimethyloctane 0.025 0.026 0.014 6.909

131 96.556 103-65-1 Q9 n-Propylbenzene 0.549 0.493 0.355 162.621

132 97.413 620-14-4 Q9 1-Methyl-3-ethylbenzene 2.289 2.048 1.480 677.453

133 97.643 622-96-8 Q9 1-Methyl-4-ethylbenzene 1.072 0.963 0.693 317.369

134 98.268 108-67-8 Q9 1,3,5-Trimethylbenzene 1.443 1.290 0.933 427.024

135 98.72315869-85-9 I10 5-Methylnonane 0.011 0.012 0.006 3.091

136 98.91317301-94-8 I10 4-Methylnonane 0.027 0.028 0.015 7.394

137 99.121 I10 2,2,6-Trimethyloctane 1.242 1.323 0.678 345.124

138 99.349 611-14-3 Q9 1-Methyl-2-ethylbenzene 0.786 0.690 0.508 232.631

139 99.567 5881-17-4 I10 3-Ethyloctane 0.005 0.005 0.003 1.365

140 99.889 5911-04-6 I10 3-Methylnonane 0.036 0.038 0.019 9.883

141 100.353 ? Unidentified 0.071 0.055 0.035 24.509

142 100.487 ? Unidentified 0.191 0.198 0.095 65.824

143 100.701 I11 C11-Isoparaffin-2 0.102 0.106 0.051 28.437

144 100.999 95-63-6 Q9 1,2,4-Trimethylbenzene 4.057 3.583 2.622 1200.810

145 101.165 ? Unidentified 0.116 0.128 0.064 39.963

146 101.287 ? Unidentified 0.069 0.073 0.038 23.913

147 101.550 1678-98-4 M10 i-Butylcyclohexane 0.018 0.018 0.010 5.091

148 102.193 ? Unidentified 0.007 0.006 0.004 2.278

149 102.33717302-01-1 I10 3-Ethyl-3-methylheptane 0.162 0.169 0.081 45.156

150 102.643 538-93-2 Q10 i-Butylbenzene 0.194 0.176 0.112 57.190

151 102.798 124-18-5 P10 n-Decane 0.040 0.042 0.022 10.990

152 102.900 ? Unidentified 0.042 0.038 0.025 14.638

153 103.199 ? Unidentified 0.039 0.041 0.020 13.581

154 103.688 ? Unidentified 0.006 0.005 0.004 1.946

155 103.853 526-73-8 Q9 1,2,3-Trimethylbenzene 0.582 0.503 0.376 172.206

156 104.217 535-77-3 Q10 1-Methyl-3-i-propylbenzene 0.028 0.026 0.016 8.359

157 104.410 I11 C11 Isoparaffin-4 0.022 0.023 0.011 6.062

158 104.617 99-87-6 Q10 1-Methyl-4-i-propylbenzene 0.112 0.101 0.065 33.084

159 105.045 J9 Indan 0.219 0.175 0.144 65.778

160 105.640 J10 Indene 0.519 0.416 0.341 156.008

161 106.356 I11 C11-Isoparaffin-7 0.192 0.199 0.095 53.323

162 106.547 141-93-5 Q10 1,3-Diethylbenzene 0.068 0.061 0.040 20.121

163 106.829 1074-43-7 Q10 1-Methyl-3-n-propylbenzene 0.705 0.633 0.408 207.476

164 107.166 105-05-5 Q10 1,4-Diethylbenzene 0.237 0.212 0.137 69.632

165 107.262 104-51-8 Q10 n-Butylbenzene 0.037 0.033 0.022 10.962

166 107.383 934-74-7 Q10 1,3-Dimethyl-5-ethylbenzene 0.222 0.195 0.128 65.332

167 107.625 135-01-3 Q10 1,2-Diethylbenzene 0.045 0.039 0.026 13.226

168 108.081 ? Unidentified 0.039 0.041 0.019 13.531

169 108.234 1074-17-5 Q10 1-Methyl-2-n-propylbenzene 0.077 0.068 0.044 22.563

170 108.355 ? Unidentified 0.042 0.043 0.021 14.353

171 108.435 ? Unidentified 0.038 0.040 0.019 13.148

172 108.563 I11 C11- Isoparaffin-11 0.315 0.327 0.156 87.528

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C-665
Hydrocarbon Expert V4.7 Fri Aug 27 15:05:52 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91335 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91335

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

173 108.744 ? Unidentified 0.098 0.102 0.049 33.803

174 109.080 1758-88-9 Q10 1,4,Dimethyl-2-ethylbenzene 0.173 0.153 0.100 51.036

175 109.168 ? Unidentified 0.236 0.208 0.137 81.546

176 109.239 874-41-9 Q10 1,3-Dimethyl-4-ethylbenzene 0.187 0.164 0.108 54.928

177 109.395 J10 2-Methylindan 0.057 0.046 0.034 17.206

178 109.743 934-80-5 Q10 1,2-Dimethyl-4-ethylbenzene 0.459 0.406 0.266 135.093

179 110.285 2870-04-4 Q10 1,3-Dimethyl-2-ethylbenzene 0.239 0.208 0.138 70.408

180 110.710 ? Unidentified 0.006 0.006 0.003 2.147

181 110.905 693-61-8 K11 2-Undecene, (E)- 0.017 0.017 0.009 4.613

182 111.039 ? Unidentified 0.023 0.024 0.013 7.855

183 111.195 Q11 1-Methyl-4-t-butylbenzene 0.037 0.034 0.020 10.963

184 111.415 933-98-2 Q10 1,2-Dimethyl-3-ethylbenzene 0.154 0.134 0.089 45.420

185 111.710 1120-21-4 P11 n-Undecane 0.027 0.028 0.014 7.561

186 111.866 4218-48-8 Q11 1-Ethyl-4-i-propylbenzene 0.031 0.027 0.016 9.050

187 111.974 ? Unidentified 0.015 0.013 0.008 5.064

188 112.349 Q10 1,2,4,5-Tetramethylbenzene 0.375 0.327 0.217 110.320

189 112.616 527-53-7 Q10 1,2,3,5-Tetramethylbenzene 0.521 0.452 0.302 153.348

190 113.132 I12 C12 - IsoParaffin - 1 0.005 0.005 0.002 1.451

191 113.483 ? Unidentified 0.020 0.021 0.009 6.737

192 113.755 Q11 C11 - Aromatic - 3 0.059 0.052 0.031 17.430

193 113.946 874-35-1 H10 5-Methylindan 0.163 0.141 0.096 47.931

194 114.071 Q12 1,2-Di-i-propylbenzene 0.059 0.051 0.028 17.265

195 114.286 1595-16-0 Q11 1-methyl-4-(1-methylpropyl)be 0.085 0.074 0.045 24.946

196 114.442 Q11 C11 - Aromatic - 4 0.047 0.041 0.025 13.773

197 114.695 824-22-6 J10 4-Methylindan 0.218 0.189 0.128 64.103

198 114.846 5161-04-6 Q11 Benzene, 1-methyl-4-(2-methylpropyl)-0.051 0.044 0.027 14.827

199 114.943 824-63-5 H10 2-Methylindan 0.162 0.141 0.095 47.781

200 115.146 ? Unidentified 0.015 0.016 0.007 5.194

201 115.259 538-68-1 Q11 n-Pentylbenzene 0.020 0.017 0.010 5.869

202 115.486 Q11 tert-Pentylbenzene 0.088 0.077 0.046 25.921

203 115.798 577-55-9 Q11 1-Methyl-2-n-butylbenzene 0.039 0.034 0.021 11.513

204 115.908 Q11 C11 - Aromatic - 6 0.049 0.045 0.026 14.427

205 116.369 100-18-5 Q12 1,4-Di-i-propylbenzene 0.073 0.064 0.035 21.437

206 116.813 91-20-3 G10 Naphthalene 0.169 0.128 0.103 52.159

207 117.008 J11 4,7-Dimethyl Indane 0.009 0.007 0.005 2.624

208 117.251 Q12 C12-Aromatic-1 0.023 0.021 0.011 6.871

209 117.414 J12 Dimethyl Indane - 1 0.010 0.008 0.005 3.038

210 117.593 7364-19-4 Q12 1t-Butyl-4-ethylbenzene 0.014 0.013 0.007 4.212

211 117.895 Q12 1,3-Di-n-propylbenzene 0.065 0.057 0.031 19.021

212 118.005 Q11 C11 - Aromatic - 11 0.037 0.034 0.019 10.824

213 118.559 Q11 C11 - Aromatic - 12 0.025 0.023 0.013 7.278

214 119.487 102-25-0 Q12 1,3,5-Triethylbenzene 0.006 0.005 0.003 1.823

215 123.440 91-57-6 G11 2-Methylnaphthalene 0.009 0.007 0.005 2.774

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C-666
Hydrocarbon Expert V4.7 Fri Aug 27 15:05:52 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91335 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91335

LIMS Id: 

Component List

Recovery = 100.00

Pk# Time CASNO Group Component %Wgt %Vol %Mol Area

216 124.306 90-12-0 G11 1-Methylnaphthalene 0.005 0.004 0.003 1.501

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C-667
Hydrocarbon Expert V4.7 Fri Aug 27 15:05:52 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91335 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91335

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Paraffin 7.553 74-98-6 Propane 0.002 0.003 0.004 0.583

10.021 106-97-8 n-Butane 0.597 0.797 0.797 162.290

18.107 109-66-0 n-Pentane 1.763 2.178 1.899 483.060

35.799 110-54-3 n-Hexane 1.573 1.845 1.418 432.616

58.051 142-82-5 n-Heptane 0.376 0.425 0.292 103.846

77.868 111-65-9 n-Octane 0.201 0.221 0.136 55.524

91.730 111-84-2 n-Nonane 0.110 0.118 0.066 30.373

102.798 124-18-5 n-Decane 0.040 0.042 0.022 10.990

111.710 1120-21-4 n-Undecane 0.027 0.028 0.014 7.561

I-Paraffins 8.809 75-28-5 i-Butane 0.025 0.035 0.034 6.870

10.635 463-82-1 2,2-Dimethylpropane 0.009 0.012 0.010 2.601

15.073 78-78-4 i-Pentane 3.658 4.566 3.939 1002.166

23.085 75-83-2 2,2-Dimethylbutane 0.296 0.353 0.267 81.465

28.336 79-29-8 2,3-Dimethylbutane 1.015 1.187 0.915 279.232

29.429 107-83-5 2-Methylpentane 5.593 6.623 5.042 1538.314

32.074 96-14-0 3-Methylpentane 2.697 3.140 2.431 741.781

42.235 108-08-7 2,4-Dimethylpentane 0.207 0.238 0.161 57.207

42.773 464-06-2 2,2,3-Trimethylbutane 0.020 0.022 0.015 5.432

50.654 591-76-4 2-Methylhexane 0.651 0.742 0.505 179.828

52.488 589-34-4 3-Methylhexane 0.440 0.495 0.341 121.523

55.140 540-84-1 2,2,4-Trimethylpentane 0.054 0.060 0.037 14.924

62.845 590-73-8 2,2-Dimethylhexane 0.012 0.014 0.008 3.451

64.942 564-02-3 2,2,3-Trimethylpentane 0.064 0.069 0.043 17.634

65.167 592-13-2 2,5-Dimethylhexane 0.133 0.148 0.090 36.796

65.503 589-43-5 2,4-Dimethylhexane 0.123 0.136 0.084 34.156

68.478 565-75-3 2,3,4-Trimethylpentane 0.662 0.712 0.450 183.050

70.790 584-94-1 2,3-Dimethylhexane 0.185 0.201 0.126 51.197

72.044 592-27-8 2-Methylheptane 0.105 0.116 0.071 29.018

72.303 589-53-7 4-Methylheptane 0.058 0.063 0.039 15.932

73.358 589-81-1 3-Methylheptane 0.093 0.102 0.063 25.804

73.558 619-99-8 3-Ethylhexane 0.047 0.051 0.032 12.962

75.247 3522-94-9 2,2,5-Trimethylhexane 0.427 0.467 0.259 118.324

80.350 1069-53-0 2,3,5-Trimethylhexane 0.077 0.083 0.047 21.429

81.519 1071-26-7 2,4-Dimethylheptane 0.018 0.020 0.011 5.059

82.475 1072-05-5 2,6-Dimethylheptane 0.032 0.034 0.019 8.764

83.407 2,5-Dimethylheptane 0.049 0.053 0.030 13.705

87.275 2216-34-4 4-Methyloctane 0.019 0.020 0.011 5.163

87.407 3221-61-2 2-Methyloctane 0.025 0.027 0.015 6.835

88.269 2216-33-3 3-Methyloctane 0.024 0.026 0.015 6.708

89.320 C10 - IsoParaffin - 1 0.099 0.105 0.054 27.411

90.16414720-74-2 2,2,4-trimethylheptane 0.073 0.078 0.040 20.361

94.06415869-87-1 2,2-Dimethyloctane 0.022 0.023 0.012 6.080

94.86115869-89-3 2,5-Dimethyloctane 0.024 0.025 0.013 6.623

95.325 2040-95-1 2,7-Dimethyloctane 0.018 0.019 0.010 5.110

95.507 2051-30-1 2,4-Dimethyloctane 0.080 0.085 0.044 22.279

95.898 2,6-Dimethyloctane 0.025 0.026 0.014 6.909

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C-668
Hydrocarbon Expert V4.7 Fri Aug 27 15:05:52 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91335 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91335

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

I-Paraffins 98.72315869-85-9 5-Methylnonane 0.011 0.012 0.006 3.091

98.91317301-94-8 4-Methylnonane 0.027 0.028 0.015 7.394

99.121 2,2,6-Trimethyloctane 1.242 1.323 0.678 345.124

99.567 5881-17-4 3-Ethyloctane 0.005 0.005 0.003 1.365

99.889 5911-04-6 3-Methylnonane 0.036 0.038 0.019 9.883

100.701 C11-Isoparaffin-2 0.102 0.106 0.051 28.437

102.33717302-01-1 3-Ethyl-3-methylheptane 0.162 0.169 0.081 45.156

104.410 C11 Isoparaffin-4 0.022 0.023 0.011 6.062

106.356 C11-Isoparaffin-7 0.192 0.199 0.095 53.323

108.563 C11- Isoparaffin-11 0.315 0.327 0.156 87.528

113.132 C12 - IsoParaffin - 1 0.005 0.005 0.002 1.451

Aromatics

Mono-Aromatics 45.631 71-42-3 Benzene 0.734 0.646 0.730 222.725

69.077 108-88-3 Toluene 12.625 11.261 10.644 3789.205

84.740 100-41-4 Ethylbenzene 2.131 1.901 1.559 634.694

85.985 108-38-3 m-Xylene 5.649 5.055 4.134 1682.769

86.126 106-42-3 p-Xylene 2.623 2.356 1.920 781.401

88.935 95-47-6 o-Xylene 1.523 1.338 1.115 453.684

93.094 98-82-8 i-Propylbenzene 0.030 0.027 0.020 8.966

96.556 103-65-1 n-Propylbenzene 0.549 0.493 0.355 162.621

97.413 620-14-4 1-Methyl-3-ethylbenzene 2.289 2.048 1.480 677.453

97.643 622-96-8 1-Methyl-4-ethylbenzene 1.072 0.963 0.693 317.369

98.268 108-67-8 1,3,5-Trimethylbenzene 1.443 1.290 0.933 427.024

99.349 611-14-3 1-Methyl-2-ethylbenzene 0.786 0.690 0.508 232.631

100.999 95-63-6 1,2,4-Trimethylbenzene 4.057 3.583 2.622 1200.810

102.643 538-93-2 i-Butylbenzene 0.194 0.176 0.112 57.190

103.853 526-73-8 1,2,3-Trimethylbenzene 0.582 0.503 0.376 172.206

104.217 535-77-3 1-Methyl-3-i-propylbenzene 0.028 0.026 0.016 8.359

104.617 99-87-6 1-Methyl-4-i-propylbenzene 0.112 0.101 0.065 33.084

106.547 141-93-5 1,3-Diethylbenzene 0.068 0.061 0.040 20.121

106.829 1074-43-7 1-Methyl-3-n-propylbenzene 0.705 0.633 0.408 207.476

107.166 105-05-5 1,4-Diethylbenzene 0.237 0.212 0.137 69.632

107.262 104-51-8 n-Butylbenzene 0.037 0.033 0.022 10.962

107.383 934-74-7 1,3-Dimethyl-5-ethylbenzene 0.222 0.195 0.128 65.332

107.625 135-01-3 1,2-Diethylbenzene 0.045 0.039 0.026 13.226

108.234 1074-17-5 1-Methyl-2-n-propylbenzene 0.077 0.068 0.044 22.563

109.080 1758-88-9 1,4,Dimethyl-2-ethylbenzene 0.173 0.153 0.100 51.036

109.239 874-41-9 1,3-Dimethyl-4-ethylbenzene 0.187 0.164 0.108 54.928

109.743 934-80-5 1,2-Dimethyl-4-ethylbenzene 0.459 0.406 0.266 135.093

110.285 2870-04-4 1,3-Dimethyl-2-ethylbenzene 0.239 0.208 0.138 70.408

111.195 1-Methyl-4-t-butylbenzene 0.037 0.034 0.020 10.963

111.415 933-98-2 1,2-Dimethyl-3-ethylbenzene 0.154 0.134 0.089 45.420

111.866 4218-48-8 1-Ethyl-4-i-propylbenzene 0.031 0.027 0.016 9.050

112.349 1,2,4,5-Tetramethylbenzene 0.375 0.327 0.217 110.320

112.616 527-53-7 1,2,3,5-Tetramethylbenzene 0.521 0.452 0.302 153.348

113.755 C11 - Aromatic - 3 0.059 0.052 0.031 17.430

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C-669
Hydrocarbon Expert V4.7 Fri Aug 27 15:05:52 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91335 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91335

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Aromatics 114.071 1,2-Di-i-propylbenzene 0.059 0.051 0.028 17.265

114.286 1595-16-0 1-methyl-4-(1-methylpropyl)be 0.085 0.074 0.045 24.946

114.442 C11 - Aromatic - 4 0.047 0.041 0.025 13.773

114.846 5161-04-6 Benzene, 1-methyl-4-(2-methylpropyl)-0.051 0.044 0.027 14.827

115.259 538-68-1 n-Pentylbenzene 0.020 0.017 0.010 5.869

115.486 tert-Pentylbenzene 0.088 0.077 0.046 25.921

115.798 577-55-9 1-Methyl-2-n-butylbenzene 0.039 0.034 0.021 11.513

115.908 C11 - Aromatic - 6 0.049 0.045 0.026 14.427

116.369 100-18-5 1,4-Di-i-propylbenzene 0.073 0.064 0.035 21.437

117.251 C12-Aromatic-1 0.023 0.021 0.011 6.871

117.593 7364-19-4 1t-Butyl-4-ethylbenzene 0.014 0.013 0.007 4.212

117.895 1,3-Di-n-propylbenzene 0.065 0.057 0.031 19.021

118.005 C11 - Aromatic - 11 0.037 0.034 0.019 10.824

118.559 C11 - Aromatic - 12 0.025 0.023 0.013 7.278

119.487 102-25-0 1,3,5-Triethylbenzene 0.006 0.005 0.003 1.823

Naphthalenes 116.813 91-20-3 Naphthalene 0.169 0.128 0.103 52.159

123.440 91-57-6 2-Methylnaphthalene 0.009 0.007 0.005 2.774

124.306 90-12-0 1-Methylnaphthalene 0.005 0.004 0.003 1.501

Naphtheno/Olefino-Benzs 113.946 874-35-1 5-Methylindan 0.163 0.141 0.096 47.931

114.943 824-63-5 2-Methylindan 0.162 0.141 0.095 47.781

Indenes 105.045 Indan 0.219 0.175 0.144 65.778

105.640 Indene 0.519 0.416 0.341 156.008

109.395 2-Methylindan 0.057 0.046 0.034 17.206

114.695 824-22-6 4-Methylindan 0.218 0.189 0.128 64.103

117.008 4,7-Dimethyl Indane 0.009 0.007 0.005 2.624

117.414 Dimethyl Indane - 1 0.010 0.008 0.005 3.038

Naphthenes

Mono-Naphthenes 27.596 287-92-3 Cyclopentane 0.305 0.316 0.338 85.857

40.665 96-37-7 Methylcyclopentane 1.205 1.245 1.112 339.547

47.550 110-82-7 Cyclohexane 0.617 0.613 0.569 173.801

53.349 1759-58-6 1t,3-Dimethylcyclopentane 0.137 0.141 0.108 38.547

53.934 2532-58-3 1c,3-Dimethylcyclopentane 0.102 0.106 0.081 28.707

54.556 822-50-4 1t,2-Dimethylcyclopentane 0.131 0.134 0.103 36.801

59.64616491-15-9 Cyclopentene, 1,5-dimethyl- 0.017 0.018 0.014 4.867

61.513 108-87-2 Methylcyclohexane 0.542 0.544 0.428 152.583

62.456 4516-69-2 1,1,3-Trimethylcyclopentane 0.015 0.015 0.010 4.114

64.289 1640-89-7 Ethylcyclopentane 0.036 0.037 0.029 10.269

66.343 4850-28-6 1c,2t,4-Trimethylcyclopentane 0.014 0.014 0.010 3.951

67.85915890-40-1 1t,2c,3-Trimethylcyclopentane 0.012 0.012 0.008 3.360

73.222 1,3-dimethyl-t-cyclohexane 0.070 0.070 0.048 19.722

76.528 2207-03-6 1t,3-Dimethylcyclohexane 0.031 0.030 0.021 8.620

78.821 C8 - MonoNaph - 3 0.015 0.015 0.010 4.185

82.172 1678-91-7 Ethylcyclohexane 0.048 0.047 0.033 13.412

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C-670
Hydrocarbon Expert V4.7 Fri Aug 27 15:05:52 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91335 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91335

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Mono-Naphthenes 89.911 trans-1,3-Diethylcyclopentane 0.007 0.006 0.004 1.997

101.550 1678-98-4 i-Butylcyclohexane 0.018 0.018 0.010 5.091

Di/Bicyclo-Naphthenes

Olefins

n-Olefins 9.621 115-11-7 Isobutene 0.016 0.021 0.022 4.502

9.662 106-98-9 Butene-1 0.018 0.023 0.024 4.962

10.507 624-64-6 t-Butene-2 0.072 0.092 0.100 20.328

11.247 590-18-1 c-Butene-2 0.085 0.106 0.118 24.035

16.725 109-67-1 Pentene-1 0.328 0.396 0.363 92.420

19.228 646-04-8 t-Pentene-2 0.832 0.992 0.921 234.391

20.261 627-20-3 c-Pentene-2 0.456 0.538 0.505 128.401

33.446 592-41-6 Hexene-1 0.158 0.180 0.146 44.508

36.43513269-52-8 t-Hexene-3 0.257 0.291 0.237 72.378

36.909 4050-45-7 t-Hexene-2 0.394 0.446 0.363 110.939

38.737 7688-21-3 c-Hexene-2 0.209 0.233 0.193 58.832

55.464 592-76-7 Heptene-1 0.028 0.031 0.022 7.935

57.32814686-14-7 t-Heptene-3 0.031 0.034 0.025 8.787

58.270 7642-10-6 c-Heptene-3 0.024 0.027 0.019 6.871

59.17014686-13-6 t-Heptene-2 0.015 0.017 0.012 4.257

110.905 693-61-8 2-Undecene, (E)- 0.017 0.017 0.009 4.613

Iso-Olefins 13.445 563-45-1 3-Methylbutene-1 0.245 0.302 0.271 68.928

17.577 563-46-2 2-Methylbutene-1 0.498 0.592 0.551 140.212

20.941 513-35-9 2-Methylbutene-2 1.019 1.190 1.129 287.222

29.196 691-38-3 4-Methyl-c-pentene-2 0.044 0.050 0.040 12.346

29.838 674-76-0 4-Methyl-t-pentene-2 0.128 0.147 0.118 35.957

33.221 763-29-1 2-Methylpentene-1 0.220 0.249 0.203 62.043

35.633 760-21-4 2-Ethylbutene-1 0.064 0.071 0.059 17.898

37.401 625-27-4 2-Methylpentene-2 0.333 0.372 0.307 93.747

37.815 922-62-3 3-Methyl-c-pentene-2 0.256 0.284 0.237 72.243

40.080 3404-73-7 3,3-Dimethylpentene-1 0.305 0.336 0.242 86.052

42.525 594-56-9 2,3,3-Trimethylbutene-1 0.013 0.015 0.011 3.749

46.634 3404-61-3 3-Methylhexene-1 0.016 0.017 0.012 4.389

47.225 3524-73-0 5-Methylhexene-1 0.043 0.048 0.034 12.223

49.26815840-60-5 2-Methyl-c-hexene-3 0.040 0.044 0.031 11.166

49.614 3769-23-1 4-Methylhexene-1 0.011 0.012 0.009 3.054

50.261 3404-55-5 4-Methyl-t/c-hexene-2 0.050 0.055 0.039 14.019

54.838 C7 - Iso-Olefin - 2 0.022 0.024 0.018 6.235

56.799 4914-89-0 3-Methyl-c-hexene-3 0.014 0.015 0.011 3.819

57.679 6094-02-6 2-Methylhexene-1 0.056 0.062 0.044 15.773

58.545 2738-19-4 2-Methyl-2-hexene 0.026 0.028 0.020 7.199

58.78810574-36-4 3-Methyl-c-hexene-2 0.019 0.021 0.015 5.494

60.07320710-38-8 3-Methyl-t-hexene-2 0.014 0.015 0.011 4.032

60.857 4914-91-4 2-Pentene, 3,4-dimethyl-, (Z)- 0.013 0.014 0.010 3.544

Naphtheno-Olefins 22.527 1574-41-0 1,3-Cyclopentadiene 0.007 0.008 0.008 1.979

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C-671
Hydrocarbon Expert V4.7 Fri Aug 27 15:05:52 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91335 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91335

LIMS Id: 

Components by Group

Recovery = 100.00

Group Time CASNO Component %Wgt %Vol %Mol Area

Naphtheno-Olefins 25.736 142-29-0 Cyclopentene 0.193 0.193 0.220 55.939

37.033 1120-62-3 3-Methylcyclopentene 0.098 0.099 0.093 27.611

45.828 693-89-0 1-Methylcyclopentene 0.351 0.349 0.332 101.379

51.147 110-83-8 Cyclohexene 0.044 0.042 0.041 12.323

Di-Olefins 18.621 78-79-5 2-Methyl-1,3-Butadiene 0.011 0.012 0.012 3.164

21.266 2004-70-8 1t,3-Pentadiene 0.015 0.018 0.018 4.495

45.422 1528-30-9 C6-Diolefin-1 0.015 0.015 0.014 4.177

Oxygenates 13.125 64-17-5 Ethanol 21.748 21.315 36.673 2523.196

26.899 71-23-8 n-Propanol 0.073 0.070 0.094 14.306

48.053 71-36-3 n-Butanol 0.054 0.053 0.057 11.594

Unidentified 19.873 Unidentified 0.005 0.006 0.006 1.873

26.983 Unidentified 0.059 0.068 0.054 20.285

28.726 Unidentified 0.055 0.057 0.048 18.827

50.835 Unidentified 0.041 0.046 0.034 14.321

63.356 Unidentified 0.057 0.062 0.041 19.817

72.447 Unidentified 0.017 0.019 0.012 6.014

74.457 Unidentified 0.011 0.011 0.008 3.870

82.974 Unidentified 0.009 0.009 0.006 3.065

85.150 Unidentified 0.009 0.009 0.005 3.004

88.745 Unidentified 0.031 0.035 0.019 10.638

93.840 Unidentified 0.060 0.064 0.033 20.831

94.524 Unidentified 0.005 0.004 0.419 1.862

94.524 Unidentified 0.005 0.006 0.003 1.862

100.353 Unidentified 0.071 0.055 0.035 24.509

100.487 Unidentified 0.191 0.198 0.095 65.824

101.165 Unidentified 0.116 0.128 0.064 39.963

101.287 Unidentified 0.069 0.073 0.038 23.913

102.193 Unidentified 0.007 0.006 0.004 2.278

102.900 Unidentified 0.042 0.038 0.025 14.638

103.199 Unidentified 0.039 0.041 0.020 13.581

103.688 Unidentified 0.006 0.005 0.004 1.946

108.081 Unidentified 0.039 0.041 0.019 13.531

108.355 Unidentified 0.042 0.043 0.021 14.353

108.435 Unidentified 0.038 0.040 0.019 13.148

108.744 Unidentified 0.098 0.102 0.049 33.803

109.168 Unidentified 0.236 0.208 0.137 81.546

110.710 Unidentified 0.006 0.006 0.003 2.147

111.039 Unidentified 0.023 0.024 0.013 7.855

111.974 Unidentified 0.015 0.013 0.008 5.064

113.483 Unidentified 0.020 0.021 0.009 6.737

115.146 Unidentified 0.015 0.016 0.007 5.194

Plus

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C-672
Hydrocarbon Expert V4.7 Fri Aug 27 15:05:52 2010 Page 1

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91335 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91335

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF

20.0 15.0 10.0 5.0 0.0

Propane

i-Butane

Isobutene Butene-1

n-Butane

t-Butene-2 2,2-Dimethylpropane

c-Butene-2

Ethanol

3-Methylbutene-1

i-Pentane

Pentene-1

2-Methylbutene-1

n-Pentane

2-Methyl-1,3-Butadiene

t-Pentene-2

Unidentified

c-Pentene-2

2-Methylbutene-2

1t,3-Pentadiene

1,3-Cyclopentadiene

2,2-Dimethylbutane

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C-673
Hydrocarbon Expert V4.7 Fri Aug 27 15:05:52 2010 Page 2

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91335 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91335

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF

45.0 40.0 35.0 30.0 25.0

Cyclopentene

n-Propanol Unidentified

Cyclopentane

2,3-Dimethylbutane

Unidentified

4-Methyl-c-pentene-2 2-Methylpentane

4-Methyl-t-pentene-2

3-Methylpentane

2-Methylpentene-1 Hexene-1

2-Ethylbutene-1 n-Hexane

t-Hexene-3

t-Hexene-2 3-Methylcyclopentene

2-Methylpentene-2

3-Methyl-c-pentene-2

c-Hexene-2

3,3-Dimethylpentene-1

Methylcyclopentane

2,4-Dimethylpentane 2,3,3-Trimethylbutene-1 2,2,3-Trimethylbutane

C6-Diolefin-1 Benzene 1-Methylcyclopentene

3-Methylhexene-1

5-Methylhexene-1 Cyclohexane

n-Butanol

2-Methyl-c-hexene-3

4-Methylhexene-1

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C-674
Hydrocarbon Expert V4.7 Fri Aug 27 15:05:52 2010 Page 3

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91335 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91335

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF

70.0 65.0 60.0 55.0 50.0

4-Methyl-t/c-hexene-2

2-Methylhexane Unidentified Cyclohexene

3-Methylhexane

1t,3-Dimethylcyclopentane

1c,3-Dimethylcyclopentane

1t,2-Dimethylcyclopentane C7 - Iso-Olefin - 2 2,2,4-Trimethylpentane

Heptene-1

3-Methyl-c-hexene-3

t-Heptene-3

2-Methylhexene-1

n-Heptane c-Heptene-3 2-Methyl-2-hexene 3-Methyl-c-hexene-2

t-Heptene-2

Cyclopentene, 1,5-dimethyl3-Methyl-t-hexene-2

2-Pentene, 3,4-dimethyl-, (Z)-

Methylcyclohexane

1,1,3-Trimethylcyclopentane

2,2-Dimethylhexane

Unidentified

Ethylcyclopentane

2,2,3-Trimethylpentane 2,5-Dimethylhexane

2,4-Dimethylhexane

1c,2t,4-Trimethylcyclopentane

1t,2c,3-Trimethylcyclopentane

2,3,4-Trimethylpentane

Toluene

2,3-Dimethylhexane

2-Methylheptane

Unidentified 4-Methylheptane

1,3-dimethyl-t-cyclohexane 3-Methylheptane 3-Ethylhexane

Unidentified

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C-675
Hydrocarbon Expert V4.7 Fri Aug 27 15:05:52 2010 Page 4

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91335 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91335

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF

95.0 90.0 85.0 80.0 75.0

2,2,5-Trimethylhexane

1t,3-Dimethylcyclohexane

n-Octane

C8 - MonoNaph - 3

2,3,5-Trimethylhexane

2,4-Dimethylheptane

Ethylcyclohexane 2,6-Dimethylheptane

Unidentified

2,5-Dimethylheptane

Ethylbenzene

Unidentified

m-Xylene p-Xylene

4-Methyloctane 2-Methyloctane

3-Methyloctane

Unidentified o-Xylene

C10 - IsoParaffin - 1

trans-1,3-Diethylcyclopentane 2,2,4-trimethylheptane

n-Nonane

i-Propylbenzene

Unidentified 2,2-Dimethyloctane

Unidentified

2,5-Dimethyloctane

2,7-Dimethyloctane 2,4-Dimethyloctane

2,6-Dimethyloctane

n-Propylbenzene

1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene

1,3,5-Trimethylbenzene

5-Methylnonane 4-Methylnonane 2,2,6-Trimethyloctane 1-Methyl-2-ethylbenzene 3-Ethyloctane

3-Methylnonane

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C-676
Hydrocarbon Expert V4.7 Fri Aug 27 15:05:52 2010 Page 5

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91335 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91335

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF

120.0 115.0 110.0 105.0 100.0

Unidentified Unidentified C11-Isoparaffin-2 1,2,4-Trimethylbenzene Unidentified

i-Butylcyclohexane

Unidentified 3-Ethyl-3-methylheptane i-Butylbenzene n-Decane Unidentified Unidentified

Unidentified1,2,3-Trimethylbenzene

1-Methyl-3-i-propylbenzene C11 Isoparaffin-4 1-Methyl-4-i-propylbenzene

Indan

Indene

C11-Isoparaffin-7 1,3-Diethylbenzene 1-Methyl-3-n-propylbenzene

n-Butylbenzene 1,4-Diethylbenzene 1,3-Dimethyl-5-ethylbenzene 1,2-Diethylbenzene

Unidentified 1-Methyl-2-n-propylbenzene

C11- Isoparaffin-11 Unidentified

1,4,Dimethyl-2-ethylbenzene 1,3-Dimethyl-4-ethylbenzene Unidentified 2-Methylindan

1,2-Dimethyl-4-ethylbenzene

1,3-Dimethyl-2-ethylbenzene

Unidentified 2-Undecene, (E)- Unidentified 1-Methyl-4-t-butylbenzene 1,2-Dimethyl-3-ethylbenzene n-Undecane Unidentified 1-Ethyl-4-i-propylbenzene

1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene

C12 - IsoParaffin - 1

Unidentified C11 - Aromatic - 3 5-Methylindan 1,2-Di-i-propylbenzene 1-methyl-4-(1-methylpropyl)be C11 - Aromatic - 4 4-Methylindan Benzene, 1-methyl-4-(2-methylpropyl)- 2-Methylindan Unidentified n-Pentylbenzene tert-Pentylbenzene

1-Methyl-2-n-butylbenzene C11 - Aromatic - 6

1,4-Di-i-propylbenzene

Naphthalene 4,7-Dimethyl Indane C12-Aromatic-1 Dimethyl Indane - 1 1t-Butyl-4-ethylbenzene

C11 - Aromatic - 11 1,3-Di-n-propylbenzene

C11 - Aromatic - 12

1,3,5-Triethylbenzene

2-Methylnaphthalene

1-Methylnaphthalene

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C-677
Hydrocarbon Expert V4.7 Fri Aug 27 15:05:52 2010 Page 6

File: C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF 26-Aug-10, 10:43:13

Sample: ODDB-91335 Operator: AAD

Parameter: C:\Chem32\SeparationSystems\HCE4\ODDB-91335

LIMS Id: 

Sample Chromatogram

C:\Chem32\1\DATA\8-24-10\TEST_NC 2010-08-24 12-47-46\SIG2000017.D\SIG2000017_FID2_B.CDF

145.0 140.0 135.0 130.0 125.0

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