# Quarterly Groundwater Monitoring Report – Outside (Non-Tunnel) Wells Red Hill Fuel Storage Facility Pearl Harbor, Oahu, Hawaii Latitude: 21 o 

# 22’15” N Longitude: 157 o 

# 53’33” W
HDOH Facility ID No. 9-102271 HDOH Release ID No. 99051, 010011, 020028
September 2009

Prepared by:

TEC Inc. 1001 Bishop St. Suite 1400 American Savings Bank Tower Honolulu, Hawaii 96813

Prepared for:

Commander Navy Region Hawaii Environmental Department, Code N45 850 Ticonderoga Street, Suite 110 Pearl Harbor, Hawaii 96860-5101

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility September 2009

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## i 

# Table of Contents
Table of Contents

............................................................................................................................. i Executive Summary......................................................................................................................... 1 1.0 Introduction .......................................................................................................................... 3 1.1 Project Objective ............................................................................................................. . 3 1.2 Previous Reports .............................................................................................................. 3 1.3 Background .................................................................................................................... .. 4 1.3.1 Site Description ......................................................................................................... 4 1.3.2 Facility Information .................................................................................................. 4 1.3.3 UST Information ....................................................................................................... 5 1.4 Regulatory Updates .......................................................................................................... 5 2.0 Sample Collection and Analyses.......................................................................................... 6 2.1 Monitoring Well Purging ................................................................................................. 6 2.2 Groundwater Sample Collection ...................................................................................... 6 2.3 Groundwater Sample Analyses ........................................................................................ 7 3.1 August 2009 Sample Analytical Results .......................................................................... 7 4.0 Summary and Conclusions ................................................................................................... 7 5.0 References.......................................................................................................................... 10
List of Tables Table 1 Monitoring Well Information ........................................................................................5 Table 2 Analytical Results for Quarte rly Groundwater Sampling (August 4, 2009) .................8 List of Figures Figure 1 Groundwater Monitoring Well Locations ......................................................................9 List of Appendices Appendix A – Laboratory Analytical Reports Appendix B – Monitoring Well Construction Logs

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## 1 

# Executive Summary This quarterly groundwater monitoring report presen ts the results of grou ndwater sampling (i.e., RHMW04, and OWDFMW01) conducted on August 4, 2009 at the United States (US) Navy Bulk Fuel Storage Facility at Red Hill, Oahu, Hawaii (the Facility). Due to access issues, sampling of the Halawa Deep Well 2253-03 ( 2253-03) was postponed (see Figure 1). The sampling and reporting was conducted by TEC Inc. (TEC) for the Fleet and Industrial Supply Center (FISC) at Pearl Harbor, Hawaii. This re port is part of a series of quarterly groundwater monitoring reports, supplemental to the groun dwater reports for the groundwater monitoring wells within the Facility, provided by the US Navy to the State of Hawaii Department of Health (HDOH) in accordance with HDOH’s release res ponse requirements. Cu rrently, there are 18 active and 2 inactive, 12.5 million gallon, field-c onstructed underground storage tanks (USTs) located at the Facility. Background In 2002, the US Navy installed a groundwater monitoring well (cur rently named RHMW01) into the basal aquifer, directly down-gradient from the Facility, within th e lower access tunnel. Groundwater samples from this wellindicated that petroleum from the Facility has migrated to the basal aquifer (AMEC, 2002). In 2005, the US Navy began quarterly monitoring of the aquifer to protect their down-grad ient drinking water resource a ssociated with the US Navy Well 2254-01. US Navy Well 2254-01 is located approxi mately 3,000 feet down-gradient from the Facility USTs and provides approximately 24 % of the potable water to the Pearl Harbor Water System (PHWS). By September 2005, the US Navy had installe d two more groundwater monitoring wells (RHMW02 and RHMW03) within the Facility US T system and a groundwater monitoring well within the US Navy Well 2254-01 infiltration gallery (RHMW2254-01). Since 2005, these wells have been sampled quarterly for Total Petrol eum Hydrocarbons (TPH) quantified as DieselRange Organics (DRO) and Gasoline Range Organics (GRO), Volatile Organic Compounds (VOCs), Polynuclear Aromatic Hydro carbons (PAHs), and dissolved lead. In response to increasing concen trations of contaminants of pot ential concern at the groundwater monitoring wells within the faci lity (specifically RHMW02) during 2008, plans were made to conduct quarterly sampling at the fo llowing monitoring well locations:

 RHMW04, up-gradient of the Facility;

 Oily Waste Disposal Facility monitoring well 01 (OWDFMW01), down-gradient of the Facility; and

 Halawa Deep Well 2253-03 (2253-03) During the summer and fall of 2008, HDOH updated their Environm ental Action Levels (EALs), which resulted in significant changes to the acti on levels associated withmethylnaphthalenes. The HDOH Drinking Water toxicity EAL for these compounds was 240  g/L. This concentration assumed that methylnaphthalenes were not human carcinogens. Once evidence emerged and was accepted by the US Environm ental Protection Agency (USEPA) that

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## 2 methylnaphthalenes are carcinogenic to humans, HDOH adopted more rigorous EALs of 4.7  g/L for 1-methylnaphthalene and 24  g/L for 2-methylnaphthalene (HDOH, 2008). The HDOH Drinking Water EAL for naphthalenewas also updated during this process. Previously, HDOH based their naphthalene EA L on USEPA Region 9 Preliminary Remediation Goal (USEPA PRG) of 6.2  g/L, which is associated with a non-cancer Hazard Index of 1. In deference to the California Department of Pub lic Health’s Drinking Water Notification Levels, (HDOH, 2008) HDOH updated their naphthalene drinking water EAL to 17  g/L. Finally, the HDOH Drinking Water EAL for TPH-DRO was increased from 100  g/L to 210  g/L, although the Groundwater Gross Cont amination EAL for TPH-DRO remains 100  g/L.
Current Results On August 4, 2009, two groundwater samples (i.e., RHMW04, and OWDFMW01), along with the required quality control samples (duplicate, matrix spike, spike duplicate, and trip blank) were collected for analysis. Samples were analyzed for TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved lead. No HDOH Drinking Water EALs were exceeded and no contaminants of concern were detected above the laboratory method dete ction limit (MDL), except for be nzene. At RHMW04, benzene was detected below the laborat ory reporting limit (RL) but above the MDL, at an estimated concentration of 0.25 μg/L in the duplicate sample only. Benzene was also detected in OWDFMW01 at 0.47 μg/L, just above the RL. The HDOH Drinking Water EAL and groundwater Gross Contamination EAL for ben zene are 5 μg/L and 170 μg/L, respectively.
Conclusions and Recommendations Based on the August 2009 sampling event, there is no indication of si gnificant contaminant migration up-gradient and down-gradient of th e Facility. Quarterly groundwater sampling for TPH-DRO, TPH-GRO, VOCs, PAHs, a nd dissolved lead will continue at the Facility until such time that data indicates that a differe nt monitoring plan is warranted.

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## 3 

# 1.0 Introduction This report presents the results of the first groundwater sampling event, conducted in August 2009 at two groundwater monitoring wells (i.e ., RHMW04, and OWDFMW 01), up-gradient and down-gradient from the Red Hill Fuel Storage Facility, Oahu, Hawaii (hereafter referred to as “the Facility”). The Facility consists of 18 active and 2 inactive USTs operated by FISC, Pearl Harbor. This groundwater sampling and analys is event is supplemental to the quarterly groundwater sampling and analysis at groundwater monitoring wells with in the Facility (i.e., part of the groundwater monitoring program for the US T site in response to past UST releases, previous environmental investigatio ns, and recommendations from the HDOH). 

# 1.1 Project Objective This groundwater sampling project was performed to evaluate the presence of chemicals of potential concern in groundwater up-gradient and down-gradient fr om the Facility. The project was conducted to ensure the Navy remains in compliance with HDOH UST release response requirements. The groundwater sampling program followed th e procedures described in Red Hill Bulk Fuel Storage Facil ity Groundwater Protection Plan [TEC Inc. (TEC), 2008], also referred to as “the Plan”. This groundwater sampling event was conducte d by TEC under US Navy Contract Number N47408-04-D-8514, Task Order No. 54, Amendment/Modification No. 01. 

# 1.2 Previous Reports This is the first groundwater sampling event for monitoring wells RHMW04 and OWDFMW01. Due to access issues, sampling of the Halawa Deep Well 2253-03 (2253-03) was postponed. This is a quarterly sampling event that is being conducted to supplement the quarterly groundwater sampling and analysis at groundwater monitoring wells within the Facility, which began in 2005. The following groundwater monito ring reports were previously submitted to the HDOH, for groundwater monitoring wells within the Facility:
1. Groundwater Sampling Report, First Quarter 2005 (submitted April 2005); 2. Groundwater Sampling Report, Second Quarter 2005 (submitted August 2005); 3. Groundwater Sampling Report, Third Quarter 2005 (submitted November 2005); 4. Groundwater Sampling Report, Fourth Quarter 2005 (submitted February 2006); 5. Groundwater Monitoring Results, July 2006 (submitted September 2006); 6. Groundwater Monitoring Results, December 2006 (submitted January 2007); 7. Groundwater Monitoring Results, March 2007 (submitted May 2007); 8. Groundwater Monitoring Results, June 2007 (submitted August 2007); 9. Groundwater Monitoring Results, September 2007 (submitted October 2007); 10. Groundwater Monitoring Results, January 2008 (submitted March 2008);

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## 4 11. Groundwater Monitoring Results, April 2008 (submitted May 2008); 12. Groundwater Monitoring Results, July 2008 (submitted October 2008); 13. Groundwater Monitoring Results, October and December 2008 (submitted February 2009); 14. Groundwater Monitoring Results, February 2009 (submitted May 2009); 15. Groundwater Monitoring Results, May 2009 (submitted July 2009); and 16. Groundwater Monitoring Results, July 2009 (submitted September 2009) 

# 1.3 Background The following sections provide a description of th e site and information on the Facility and USTs.
1.3.1 Site Description The Facility is located in Halawa Heights on Oahu, Hawaii. Land adjacen t to the north of the Facility is occupied by Halawa Correctional Faci lity and private businesses. Land to the south and west of the Facility includes the Coast Guar d Reservation. Moanalua Valley is located east of the Facility (Dawson, 2006). The Navy Public Works Department operates a pot able water infiltratio n tunnel approximately 1,550 feet hydraulically down-gradient from th e Facility (Dawson, 2006). The US Navy Well 2254-01 is located approximately 3,000 feet down-grad ient (west) of the Facility and provides approximately 24% of the potable water to th e Pearl Harbor Water System, which serves approximately 52,200 military consumers (TEC, 2008).
1.3.2 Facility Information The Facility consists of 18 active and 2 inactive USTs operate d by Navy FISC Pearl Harbor. Each UST has a capacity of 12.5 million gallons. The Facility is located approximately 100 feet above the basal aquifer (Dawson, 2006). In 2002, the US Navy installed a groundwater monitoring well (cur rently named RHMW01) into the basal aquifer, directly down-gradient from the Facility, within th e lower access tunnel. Groundwater samples from this wellindicated that petroleum from the Facility has migrated to the basal aquifer (AMEC, 2002). In 2005, the US Navy began quarterly monitoring of the aquifer to protect their down-grad ient drinking water resource a ssociated with the US Navy Well 2254-01. US Navy Well 2254-01 is located approxi mately 3,000 feet down-gradient from the Facility USTs and provides approximately 24 % of the potable water to the PHWS. By September 2005, the US Navy had installe d two more groundwater monitoring wells (RHMW02 and RHMW03) within the Facil ity UST system, a background groundwater monitoring well (RHMW04) up-gradient from the Facility adjacent to the US Navy Firing Range, and a groundwater monitoring well within the US Navy Well 2254-01 infiltration gallery (RHMW2254-01). Since 2005, RHMW01, RH MW02, RHMW03, and RHMW2254-01 have been sampled quarterly for TPH-DRO, TP H-GRO, VOCs, PAHs, and dissolved lead.

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## 5 Due to increasing concentrations of contamin ants of potential con cern at the groundwater monitoring wells within the Fa cility (specifically RHMW02) during 2008, response measures were warranted. In April 2009, another groundwater monitoring well (RHMW05) was installed down-gradient from the USTs, within the lower access tunnel between RHMW01 and RHMW2254-01. It was installed to identify the extent of contaminant migration down-gradient before it reaches the infiltration gallery at RHMW2254-01. Additionally, plans were made to sample three monitori ng wells RHMW04, OWDFMW01, and monitoring well 2253-03. RHMW04 is adjacent to the US Navy Firing Range, geographically up-gradient of the USTs. It wa s installed to provide geochemistry for water moving through the basal aquifer beneath the Facility. OWDFMW01 (originally known as MW08) was installed into the basal aquifer in 1998 for a Phase II Remedial Investigation/ Feasibility Study for the Red Hill Oily Waste Disposal Facility (Earth Tech Inc., 2000). It is located geographically down-gradient of the USTs and US Navy Well 2254-01. Monitori ng well 2253-03 is controlled by the State of Hawaii Commission on Water Resource Management. It is located cr oss-gradient of the Facility, between the Facility and the municipal drinking water supply well run by the City and County of Honolulu Board of Water Supply (Halaw a Shaft pumping station 2354-01). Table 1 summarizes basic gr oundwater monitoring well information, Figure 1 shows groundwater monitoring well locatio ns, and Appendix B includes th e well construction logs for RHMW04 and OWDFMW01. Table 1. Monitoring Well Information

Groundwater Well TOC Elevation (ft msl) DTW (ft) TD (ft)

RHMW04 313.03 293 320 OWDFMW01 138.94 120 142.8 Halawa Deep (2253-03) 225 210 1,575 Notes: DTW - Distance to water TD - Total depth of well TOC - Top of casing ft – Feet ft msl - Feet from mean sea level



## 1.3.3 UST Information The USTs were constructed in th e early 1940s. The tanks were c onstructed of steel and currently contain Jet Propulsion (JP)–5 fuel and F-76 (diesel marine fuel ). Previously, se veral tanks stored Navy Special Fuel Oil, Navy Distillate, aviati on gasoline, and motor gasoline. Each tank measures approximately 245 feet in height and 100 feet in diameter. The upper domes of the tanks lie at depths varying between approximately 100 feet and 200 feet below the existing ground surface (TEC, 2006). 

# 1.4 Regulatory Updates During the summer and fall of 2008, HDOH updated their EALs, which resulted in significant changes to the action levels associated with me thylnaphthalenes. The drinking water toxicity EAL for these compounds was 240  g/L. This concentration pres umed that methylnaphthalenes

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## 6 were non-carcinogenic. Evidence th at they are human carcinogens has now been accepted by the US Environmental Protection Agency (USEPA). As a result, HDOH adopted more rigorous EALs of 4.7  g/L for 1-methylnaphthalene and 24  g/L for 2-methylnaphthalene, corresponding to a residential tap water scenario, an d a 1 in a million cancer risk (HDOH, 2008). The drinking water EAL for naphthalene has also been updated during this process. Previously, HDOH based their naphthalene EAL on USEPA Region 9 Preliminary Remediation Goal (USEPA PRG) of 6.2  g/L, which is associated with a non-cancer Hazard Index of 1. HDOH has updated their naphthalen e drinking water EAL to 17  g/L, in deference to the California Department of Public Health’s Drinking Wate r Notification Levels, a Hazard Index of 2.7 (HDOH, 2008). Finally, the HDOH Drinking Water EAL for TPH-DRO was increased from 100  g/L to 210  g/L, although the HDOH Groundwat er Gross Contamination EAL for TPH-DRO remains 100  g/L. 

# 2.0 Sample Collection and Analyses Field activities relating to groundwater sample collection we re conducted on August 4, 2009. Groundwater samples were collected from two monitoring wells, one downgradient of the Facility and one upgradien t (OWDFMW01 and RHMW04, respectively). Groundwater monitoring well 2253-03 was not sampled duri ng this round of sampling due to problems obtaining access. Sampling and anal ysis were conducted according to Red Hill Bulk Fuel Storage Facility Groundwater Protection Plan (TEC, 2008). A total of five samples were collected as follows:

 one environmental sample from RHMW04 and OWDFMW01;

 one duplicate sample from RHMW04 (sampled as RHMWA01 and reported as RHMW04D); and

 one matrix spike and matrix sp ike duplicate from OWDFMW01. 

# 2.1 Monitoring Well Purging The groundwater monitoring wells were purged and sampled using a dedicated pump system. Well purging was considered complete when no less than three successive water quality parameter measurements had stabilized within ap proximately 10 percent. Field parameters were measured at regular intervals during well pur ging and included pH, temperature, specific conductivity, dissolved oxygen, and turbidity. 

# 2.2 Groundwater Sample Collection Each monitoring well was sampled immediately following purging. Both wells were sampled directly from their dedicatedbladder pump system. Samples were placed into sampling containers with appropriate pr eservatives [i.e., hydrochloric ac id (HCl) for volatile organic analysis, nitric acid (HNO 3 

## ) for dissolved lead]. Dissolved lead samples were filtered in the field and placed in preserved bottles. Sample cont ainers were labeled with the date, sample identification number, type of analysis, and samp ler’s name. The containers were placed on ice

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## 7 in sample coolers and transporte d under chain-of-custody procedur es to the certified laboratory for analysis. 

# 2.3 Groundwater Sample Analyses Groundwater samples were analyzed by SGS Environm ental Service, Inc. in Anchorage, Alaska for TPH-DRO and TPH-GRO by EPA Method 8015B, VOCs by EPA Method 8260B, PAHs by EPA Method 8270C SIM, and dissolved lead by EPA Method 6020. 

# 3.0 Groundwater Sample Analytical Results This section provides a summary of analytical results for groundwater samples collected from two monitoring wells, one downgradient of the Facility and one upgradient (OWDFMW01 and RHMW04, respectively). Duplicate sample result s from monitoring well RHMW04 are reported in this document as RHMW04D. A summary of groundwater analytical results for TPH-DRO and TPH-GRO, VOCs, PAHs, and dissolved lead is included in Table 2. Complete analytical laboratory reports are pr ovided in Appendix A. 

# 3.1 August 2009 Sample Analytical Results All groundwater samples were analyzed for TP H-DRO, TPH-GRO, VOCs, PAHs, and dissolved lead. The results for each groundwater monitoring well are discussed below.
RHMW04 Benzene was detected in the duplicate sample at an estimated concentrati on of 0.25 μg/L (i.e., the value is below the laboratory RL, but above the MDL), well below the HDOH Drinking Water EAL (i.e., 5 μg/L). Benzene was not de tected above the same laboratory MDL in the normal sample from RHMW04. No other potential chemical of concern wa s detected above the laboratory MDL (Table 2).
OWDFMW01 Benzene was detected at 0.47 μg /L just above the RL (i.e., 0.4 μg/L) in OWDFMW01. This concentration is well below the HDOH Drinking Wate r EAL (i.e., 5 μg/L). No other potential chemical of concern was detected above the laboratory MDL (Table 2). 

# 4.0 Summary and Conclusions Summary No potential chemicals of concern were dete cted above the HDOH Drinking Water or Gross Contamination EALs at RHMW04 or OWDFMW01. Only trace detections of benzene were detected.
Conclusions/Recommendations Based on the August 2009 sampling event, there is no indication of significant contaminant migration up-gradient or down-gradient of the Facility.Table 2. Analytical Results for Quarterly Groundwater Sampling (August 4, 2009)Red Hill Fuel Storage Facility, Pearl Harbor, HawaiiResult Q MDL RL Result Q MDL RL Result Q MDL RLTPH as DIESEL RANGE ORGANICS210 100 ND U 171 457 ND U 157 419 ND U 161 430TPH as GASOLINE RANGE ORGANICS100 100 ND U 30 100 ND U 30 100 ND U 30 1001-METHYLNAPHTHALENE4.7 10 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0167 0.05562-METHYLNAPHTHALENE24 10 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0167 0.0556ACENAPHTHENE370 20 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0167 0.0556ACENAPHTHYLENE240 2000 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0167 0.0556ANTHRACENE1800 22 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0167 0.0556BENZO(a)ANTHRACENE0.092 4.7 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0167 0.0556BENZO(a)PYRENE0.2 0.81 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0167 0.0556BENZO(b)FLUORANTHENE0.092 0.75 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0167 0.0556BENZO(g,h,i)PERYLENE1500 0.13 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0167 0.0556BENZO(k)FLUORANTHENE0.92 0.4 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0167 0.0556CHRYSENE9.2 1 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0167 0.0556DIBENZ( h)ANTHRACENE0 00920 52NDU0 01640 0546NDU0 01620 0541NDU0 01670 05568015B (Petroleum)8270C SIM(PAHs)August 4, 2009MethodHDOH Drinking WaterEALs1for Human ToxicityUG/LHDOH GroundwaterGross ContaminationEALs2UG/LChemicalOWDFMW01UG/LAugust 4, 2009 August 4, 2009RHMW04UG/LRHMW04DUG/LDIBENZ(a,h)ANTHRACENE0.0092 0.52 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0167 0.0556FLUORANTHENE1500 130 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0167 0.0556FLUORENE240 950 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0167 0.0556INDENO(1,2,3-c,d)PYRENE0.092 0.095 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0167 0.0556NAPHTHALENE17 21 ND U 0.0339 0.109 ND U 0.0335 0.108 ND U 0.0344 0.111PHENANTHRENE240 410 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0167 0.0556PYRENE180 68 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0167 0.05561,1,1,2-TETRACHLOROETHANE0.52 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.51,1,1-TRICHLOROETHANE200 970 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,1,2,2-TETRACHLOROETHANE0.067 500 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.51,1,2-TRICHLOROETHANE5 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,1-DICHLOROETHANE2.4 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,2,3-TRICHLOROPROPANE (TCP)0.6 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,2,4-TRICHLOROBENZENE70 3000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,2-DIBROMO-3-CHLOROPROPANE (DBCP)0.04 10 ND U 0.62 2 ND U 0.62 2 ND U 0.62 21,2-DIBROMOETHANE (EDB)0.0065 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,2-DICHLOROBENZENE600 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,2-DICHLOROETHANE0.15 7000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.51,2-DICHLOROPROPANE5 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,3-DICHLOROBENZENE180 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11 4 DICHLOROBENZENE755NDU0 150 5NDU0 150 5NDU0 150 51,4-DICHLOROBENZENE......ACETONE22000 20000 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10BENZENE5 170 0.47 0.12 0.4 ND U 0.12 0.4 0.25 F 0.12 0.4BROMODICHLOROMETHANE0.22 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5BROMOFORM100 510 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1BROMOMETHANE8.7 50000 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3CARBON TETRACHLORIDE5 520 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1CHLOROBENZENE100 50 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5CHLOROETHANE8600 16 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1CHLOROFORM70 2400 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1CHLOROMETHANE1.8 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1cis-1,2-DICHLOROETHYLENE70 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1cis-1,3-DICHLOROPROPENE0.43 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5DIBROMOCHLOROMETHANE0.16 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5ETHYLBENZENE700 30 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1HEXACHLOROBUTADIENE0.86 6 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1M,P-XYLENE (SUM OF ISOMERS)10000 20 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2METHYL ETHYL KETONE (2-BUTANONE)7100 8400 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10METHYL ISOBUTYL KETONE (4-METHYL-2-PENTANONE)2000 1300 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10METHYLENE CHLORIDE4.8 9100 ND U 1 5 ND U 1 5 ND U 1 5NAPHTHALENE1721NDU0.622NDU0.622NDU0.6228260B(VOCs)NAPHTHALENE1721NDU0.622NDU0.622NDU0.622STYRENE100 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1TETRACHLOROETHYLENE(PCE)5 170 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1TOLUENE1000 40 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1trans-1,2-DICHLOROETHENE100 260 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1TRICHLOROETHYLENE (TCE)5 310 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1VINYL CHLORIDE2 3400 ND U 0.31 1 ND U 0.31 1 ND U 0.31 16020LEAD15 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1PAHs - Polynuclear aromatic hydrocarbonsMDL - Method detection limitVOCs - Volatile organic compoundsRL - Reporting limitND - Indicates that the compound was not detected above the stated method detection limit TPH - Total petroleum hydrocarbonsQ - Data qualifierUG/L - Micrograms per LiterU - Indicates that the compound was analyzed for but not detected at or above the stated limitF - Indicates that the compound was identified but the concentration was above the MDL and below the RL-Result exceeds one or both HDOH EALs12Final Drinking Water Action Levels for Human Toxicity, Table D-3a,Screening for Environmental Concerns at Sites withContaminated Soil and Groundwater, HDOH, 2009Groundwater Gross Contamination Action Levels, Table G-1,Screening for Environmental Concerns at Sites withContaminated Soil and Groundwater, HDOH, 2009200Page 1 of 1Figure1GroundwaterMonitoringWellLocationsdilllSiliReHFuetorageFactyOahu,Hawaii

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## 10 

# 5.0 References AMEC. Red Hill Bulk Fuel Storage Facility Investigation Report , Prepared for NAVFAC Pacific, August 2002. Dawson Group, Inc. Fourth Quarter 2005 Groundwater Sam pling Report, Red Hill Fuel Storage Facility, Hawaii. February 2006. Earth Tech, Inc. Remedial Investigation Phase II, Volume I, Technical Report, Red Hill Oily Waste Disposal Facility, Halawa, Oahu, Hawaii . September 2000. Hawaii Administrative Rules, Titl e 11, Chapter 281, Subchapter 7.
HDOH. Screening for Environmental Concerns at Sites with Contaminated Soil and Groundwater, Summary Lookup Tables. March 2009.
HDOH. Use of May 2005 Environmental Action Levels (“EALs”) at Leaking Underground Storage Tank Sites . Memo. July 2005.
HDOH. Evaluation of Environmental Hazards at Sites with Contaminated Soil and Groundwater . Summer 2008 (updated October 2008).
TEC, Inc. Red Hill Bulk Fuel Storage Facility, Fi nal – Addendum Planning Documents, Pearl Harbor, Hawaii. May 2006.
TEC, Inc. Red Hill Bulk Fuel Storage Facility, Final Groundwater Protection Plan, Pearl Harbor, Hawaii. January 2008.

# Appendix A Laboratory Analytical Reports

## SGS Work Order:

Contents: Cover Page Case Narrative Final Report Pages Quality Control Summary Forms Chain of Custody/Sample Receipt Forms 

## Project: Client: 

# SGS North America Inc. Alaska Division Level II Laboratory Data Report

Released by:

Note: Unless otherwise noted, all quality assurance/quality control criteria is in compliance with the standards set forth by the proper regulatory authority, the SGS Quality Assurance Program Plan, and the National Environmental Accreditation Conference. 

## 3354-003 Red Hill BFSF The Environmental Company, Inc. (TEC) 1094021

## CASE NARRATIVE Print Date: 8/20/2009

Workorder No.: 1094021 Project Name: 3354-003 Red Hill BFSF Client Name: The Environmental Company, Inc. (TEC)

Lab Sample ID 

## Sample Comments

Sample Type Client Sample ID Refer to the sample receipt form for information on sample condition.

1094021002 8260B - MS/MSD recoveries for chloroethane and bromomethane do not meet QC criteria. These analytes were not

detected above the PQL in the associated samples BMS OWDFMW01-WG01 MS

1094021003 8260B - MS/MSD recoveries for chloroethane and bromomethane do not meet QC criteria. These analytes were not

detected above the PQL in the associated samples BMSD OWDFMW01-WG01 MSD

915596 8260B - LCS recovery for acetone does not meet QC criteria. This analyte was not detected above the PQL in the

associated samples LCS LCS for HBN 218335 [VXX/19797]

915597 8260B - LCS recovery for acetone does not meet QC criteria. This analyte was not detected above the PQL in the

associated samples LCSD LCSD for HBN 218335 [VXX/19797

915601 8260B - CCV recoveries for several analytes do not meet QC criteria. These analytes were not detected above the PQL in

the associated samples CCV CCV for HBN 218337 [VMS/10724]

915947 8260B - LCS recovery for 1,1-dichloropropene does not meet QC criteria. This analyte was not detected above the PQL in

the associated samples LCS LCS for HBN 218403 [VXX/19810]

915948 8260B - LCS recovery for 1,1-dichloropropene does not meet QC criteria. This analyte was not detected above the PQL in

the associated samples LCSD LCSD for HBN 218403 [VXX/19810

915950 8260B - CCV recoveries for 1,1-dichloropropene and bromomethane do not meet QC criteria. These analytes were not

detected above the PQL in the associated samples CCV CCV for HBN 218404 [VMS/10730]

916342 8260B - CCV recoveries for several analytes do not meet QC criteria. These analytes were not detected above the PQL in

the associated samples CCV CCV for HBN 218479 [VMS/10736]

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

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. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)Print Date: 8/20/2009 1:51 pm 

### Report of Manual Integrations
Laboratory ID Client Sample ID Analytical Batch Method Analyte Reason 914031 LCS for HBN 218011 [XXX/21374] XMS5029 8270D SIMS Benzo[g,h,i]perylene RSP 

### Manual Integration Reason Code Descriptions Code Description O Original Chromatogram M Modified Chromatogram SS Skimmed surrogate BLG Closed baseline gap RP Reassign peak name PIR Pattern integration required IT Included tail SP Split peak RSP Removed split peak FPS Forced peak start/stop BLC Baseline correction PNF Peak not found by software All DRO/RRO analysis are integrated per SOP.

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# Laboratory Analytical Report

Project: Client:

Workorder No.: The Environmental Company, Inc. (TEC)



### 1094021

Certification: I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, other than the conditions noted on the sample data sheet(s) and/or the case narrative. This certification applies only to the tested parameters and the specific sample(s) received at the laboratory. 1001 Bishop Street, Suite 1400 Honolulu, HI 96813

Attn: Rick Adkisson T: (808)528-1445 F:(808)528-0768

Tamara Rentz tamara.rentz@sgs.com Project Manager 

### 3354-003 Red Hill BFSF

If you have any questions regarding this report, or if we can be of further assistance, please contact your SGS Project Manager.

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

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. 5301 w w w . us. sgs.com M em ber of S G S G roupEnclosed are the analytical results associated with this workorder. As required by the state of Alaska and the USEPA, a formal Quality Assurance/Quality Control Program is maintained by SGS. A copy of our Quality Assurance Plan (QAP), which outlines this program is available at your request.
The Laboratory certification numbers are AK971-05 (DW), UTS-005 (CS) and AK00971 (Micro) for ADEC and AK100001 for NELAP (RCRA methods: 1020A, 1311, 6010B, 7470A, 7471A, 9040B, 9045C, 9056, 9060, 8015B, 8021B, 8081A/8082, 8260B, 8270C). Except as specifically noted, all statements and data in this report are in conformance to the provisions set forth by the SGS QAP, the National Environmental Laboratory Accreditation Program and, when applicable, other regulatory authorities. If you have any questions regarding this report or if we can be of any assistance, please contact your SGS Project Manager at 907-562-2343. 

### All work is being provided under SGS general terms and conditions (http://www.sgs.com/terms_and_conditions.htm)
The following descriptors may be found on your report which will serve to further qualify the data.

MDL Method Detection Limit PQL Practical Quantitation Limit (reporting limit). CL Control Limit U Indicates the analyte was analyzed for but not detected. F Indicates value that is greater than or equal to the MDL. J The quantitation is an estimation. ND Indicates the analyte is not detected B Indicates the analyte is found in a blank associated with the sample.

* The analyte has exceeded allowable regulatory or control limits. D The analyte concentration is the result of dilution. GT Greater Than LT Less Than Q QC parameter out of acceptance range. M A matrix effect was present. E The analyte result is above the calibrated range. R Rejected DF Analytical Dilution Factor JL The analyte was positively identified, but the quantitation is a low estimation. <Surr> Surrogate QC spiked standard <Surr/IS> Surrogate / Internal Standard QC spiked standard QC Quality Control QA Quality Assurance MB Method Blank LCS (D) Laboratory Control Sample (Duplicate) MS(D) Matrix Spike (Duplicate) BMS(D) Site Specific Matrix Spike (Duplicate) RPD Relative Percent Difference ICV Initial Calibration Verification CCV Continuous Calibration Verification MSA Method of Standard Addition Notes: Soil samples are reported on a dry weight basis unless otherwise specified Print Date: 8/20/2009

Notes: All DRO/RRO analyses are integrated per SOP.

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## SAMPLE SUMMARY Client Name: The Environmental Company, Inc. (TEC) Project Name: 3354-003 Red Hill BFSF Workorder No.: 1094021 

## Analytical Methods
Method Description Analytical Method 8270 PAH SIM Semi-Vol GC/MS Liq/Liq ext. 8270D SIMS AFCEE 3.1 8260 (W) SW8260B Dissolved Metals by ICP-MS SW6020 DRO by 8015B (W) SW8015C GRO (W) SW8015C Print Date: 8/20/2009 1:51 pm



## Sample ID Cross Reference
Client Sample ID Lab Sample ID 1094021001 OWDFMW01-WG01 1094021002 OWDFMW01-WG01 MS 1094021003 OWDFMW01-WG01 MSD 1094021004 RHMW04-WG01 1094021005 RHMWA01-WG01 1094021006 TB01-WG01

S G S N orth A m erica Inc

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### The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: 

### OWDFMW01-WG01 SGS Ref. #: 1094021001 Collection Date/Time: 08/04/09 15:45 Receipt Date/Time: 08/06/09 11:30 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 ug/L MMS6032 MXX22033 0.310 5
Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS6032 Analytical Method: SW6020 Analysis Date/Time: 08/18/09 19:35 Prep Batch: MXX22033 Prep Method: SW3010A Prep Date/Time: 08/12/09 19:00 Container ID:1094021001-G Dilution Factor: 5 Analyst: NRB

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2 343 f ( 907 ) 561

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### The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: 

### OWDFMW01-WG01 SGS Ref. #: 1094021001 Collection Date/Time: 08/04/09 15:45 Receipt Date/Time: 08/06/09 11:30 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

MDL DF
Gasoline Range Organics ND 100 ug/L VFC9606 VXX19837 30.0 1 4-Bromofluorobenzene <surr> 95.2 50-150 % VFC9606 VXX19837 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9606 Analytical Method: SW8015C Analysis Date/Time: 08/14/09 17:20 Prep Batch: VXX19837 Prep Method: SW5030B Prep Date/Time: 08/14/09 13:16 Container ID:1094021001-B Dilution Factor: 1 Analyst: KPW

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2 343 f ( 907 ) 561

. 5 301 w w w . us. sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: 

### OWDFMW01-WG01 SGS Ref. #: 1094021001 Collection Date/Time: 08/04/09 15:45 Receipt Date/Time: 08/06/09 11:30 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

MDL DF
Diesel Range Organics ND 0.457 mg/L XFC8762 XXX21370 0.171 1 5a Androstane <surr> 78.7 50-150 % XFC8762 XXX21370 1
Batch Information Initial Prep Wt./Vol.: 875 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC8762 Analytical Method: SW8015C Analysis Date/Time: 08/08/09 11:01 Prep Batch: XXX21370 Prep Method: SW3520C Prep Date/Time: 08/07/09 09:25 Container ID:1094021001-J Dilution Factor: 1 Analyst: KDC

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2 343 f ( 907 ) 561

. 5 301 w w w . us. sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: 

### OWDFMW01-WG01 SGS Ref. #: 1094021001 Collection Date/Time: 08/04/09 15:45 Receipt Date/Time: 08/06/09 11:30 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene 0.470 0.400 ug/L VMS10730 VXX19810 0.120 1 Toluene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 Ethylbenzene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 n-Butylbenzene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 1,4-Dichlorobenzene ND 0.500 ug/L VMS10730 VXX19810 0.150 1 1,2-Dichloroethane ND 0.500 ug/L VMS10730 VXX19810 0.150 1 1,3,5-Trimethylbenzene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 4-Chlorotoluene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 Chlorobenzene ND 0.500 ug/L VMS10730 VXX19810 0.150 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L VMS10730 VXX19810 3.10 1 cis-1,2-Dichloroethene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 4-Isopropyltoluene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 cis-1,3-Dichloropropene ND 0.500 ug/L VMS10730 VXX19810 0.150 1 n-Propylbenzene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 Styrene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 Dibromomethane ND 1.00 ug/L VMS10730 VXX19810 0.310 1 trans-1,3-Dichloropropene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 1,2,4-Trichlorobenzene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 Acetone ND 10.0 ug/L VMS10730 VXX19810 3.10 1 1,1,2,2-Tetrachloroethane ND 0.500 ug/L VMS10730 VXX19810 0.150 1 1,2-Dibromo-3-chloropropane ND 2.00 ug/L VMS10730 VXX19810 0.620 1 Methyl-t-butyl ether ND 5.00 ug/L VMS10730 VXX19810 1.50 1 Tetrachloroethene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 Dibromochloromethane ND 0.500 ug/L VMS10730 VXX19810 0.150 1 1,3-Dichloropropane ND 0.400 ug/L VMS10730 VXX19810 0.120 1 1,2-Dibromoethane ND 1.00 ug/L VMS10730 VXX19810 0.310 1 Carbon tetrachloride ND 1.00 ug/L VMS10730 VXX19810 0.310 1 1,1,1,2-Tetrachloroethane ND 0.500 ug/L VMS10730 VXX19810 0.150 1 Chloroform ND 1.00 ug/L VMS10730 VXX19810 0.300 1 Bromobenzene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 Chloromethane ND 1.00 ug/L VMS10730 VXX19810 0.310 1 1,2,3-Trichloropropane ND 1.00 ug/L VMS10730 VXX19810 0.310 1 Bromomethane ND 3.00 ug/L VMS10730 VXX19810 0.940 1 Bromochloromethane ND 1.00 ug/L VMS10730 VXX19810 0.310 1 Vinyl chloride ND 1.00 ug/L VMS10730 VXX19810 0.310 1 Dichlorodifluoromethane ND 1.00 ug/L VMS10730 VXX19810 0.310 1

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2 343 f ( 907 ) 561

. 5 301 w w w . us. sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: 

### OWDFMW01-WG01 SGS Ref. #: 1094021001 Collection Date/Time: 08/04/09 15:45 Receipt Date/Time: 08/06/09 11:30 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Chloroethane ND 1.00 ug/L VMS10730 VXX19810 0.310 1 sec-Butylbenzene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 Bromodichloromethane ND 0.500 ug/L VMS10730 VXX19810 0.150 1 1,1-Dichloroethene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 2-Butanone (MEK) ND 10.0 ug/L VMS10730 VXX19810 3.10 1 Methylene chloride ND 5.00 ug/L VMS10730 VXX19810 1.00 1 Trichlorofluoromethane ND 1.00 ug/L VMS10730 VXX19810 0.310 1 P & M -Xylene ND 2.00 ug/L VMS10730 VXX19810 0.620 1 Naphthalene ND 2.00 ug/L VMS10730 VXX19810 0.620 1 o-Xylene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 Bromoform ND 1.00 ug/L VMS10730 VXX19810 0.310 1 1-Chlorohexane ND 1.00 ug/L VMS10730 VXX19810 0.310 1 1,2,4-Trimethylbenzene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 tert-Butylbenzene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 1,1,1-Trichloroethane ND 1.00 ug/L VMS10730 VXX19810 0.310 1 1,1-Dichloroethane ND 1.00 ug/L VMS10730 VXX19810 0.310 1 2-Chlorotoluene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 Trichloroethene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 trans-1,2-Dichloroethene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 1,2-Dichlorobenzene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 2,2-Dichloropropane ND 1.00 ug/L VMS10730 VXX19810 0.310 1 Hexachlorobutadiene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 Isopropylbenzene (Cumene) ND 1.00 ug/L VMS10730 VXX19810 0.310 1 1,2-Dichloropropane ND 1.00 ug/L VMS10730 VXX19810 0.310 1 1,1-Dichloropropene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 1,1,2-Trichloroethane ND 1.00 ug/L VMS10730 VXX19810 0.310 1 1,3-Dichlorobenzene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 1,2,3-Trichlorobenzene ND 1.00 ug/L VMS10730 VXX19810 0.310 1 1,2-Dichloroethane-D4 <surr> 118 73-120 % VMS10730 VXX19810 1 Toluene-d8 <surr> 99.9 80-120 % VMS10730 VXX19810 1 4-Bromofluorobenzene <surr> 104 76-120 % VMS10730 VXX19810 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS10730 Analytical Method: SW8260B Analysis Date/Time: 08/13/09 22:27 Prep Batch: VXX19810 Prep Method: SW5030B Prep Date/Time: 08/13/09 08:26 Container ID:1094021001-A Dilution Factor: 1 Analyst: SCL

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### The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: 

### OWDFMW01-WG01 SGS Ref. #: 1094021001 Collection Date/Time: 08/04/09 15:45 Receipt Date/Time: 08/06/09 11:30 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0546 ug/L XMS5029 XXX21374 0.0164 1 Acenaphthene ND 0.0546 ug/L XMS5029 XXX21374 0.0164 1 Fluorene ND 0.0546 ug/L XMS5029 XXX21374 0.0164 1 Phenanthrene ND 0.0546 ug/L XMS5029 XXX21374 0.0164 1 Anthracene ND 0.0546 ug/L XMS5029 XXX21374 0.0164 1 Fluoranthene ND 0.0546 ug/L XMS5029 XXX21374 0.0164 1 Pyrene ND 0.0546 ug/L XMS5029 XXX21374 0.0164 1 Benzo(a)Anthracene ND 0.0546 ug/L XMS5029 XXX21374 0.0164 1 Chrysene ND 0.0546 ug/L XMS5029 XXX21374 0.0164 1 Benzo[b]Fluoranthene ND 0.0546 ug/L XMS5029 XXX21374 0.0164 1 Benzo[k]fluoranthene ND 0.0546 ug/L XMS5029 XXX21374 0.0164 1 Benzo[a]pyrene ND 0.0546 ug/L XMS5029 XXX21374 0.0164 1 Indeno[1,2,3-c,d] pyrene ND 0.0546 ug/L XMS5029 XXX21374 0.0164 1 Dibenzo[a,h]anthracene ND 0.0546 ug/L XMS5029 XXX21374 0.0164 1 Benzo[g,h,i]perylene ND 0.0546 ug/L XMS5029 XXX21374 0.0164 1 Naphthalene ND 0.109 ug/L XMS5029 XXX21374 0.0339 1 1-Methylnaphthalene ND 0.0546 ug/L XMS5029 XXX21374 0.0164 1 2-Methylnaphthalene ND 0.0546 ug/L XMS5029 XXX21374 0.0164 1 Terphenyl-d14 <surr> 102 50-135 % XMS5029 XXX21374 1
Batch Information Initial Prep Wt./Vol.: 915 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS5029 Analytical Method: 8270D SIMS Analysis Date/Time: 08/12/09 02:10 Prep Batch: XXX21374 Prep Method: SW3520C Prep Date/Time: 08/07/09 10:00 Container ID:1094021001-H Dilution Factor: 1 Analyst: JDH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

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### The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: 

### RHMW04-WG01 SGS Ref. #: 1094021004 Collection Date/Time: 08/04/09 12:35 Receipt Date/Time: 08/06/09 11:30 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 ug/L MMS6032 MXX22033 0.310 5
Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS6032 Analytical Method: SW6020 Analysis Date/Time: 08/18/09 19:48 Prep Batch: MXX22033 Prep Method: SW3010A Prep Date/Time: 08/12/09 19:00 Container ID:1094021004-G Dilution Factor: 5 Analyst: NRB

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2 343 f ( 907 ) 561

. 5 301 w w w . us. sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: 

### RHMW04-WG01 SGS Ref. #: 1094021004 Collection Date/Time: 08/04/09 12:35 Receipt Date/Time: 08/06/09 11:30 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

MDL DF
Gasoline Range Organics ND 100 ug/L VFC9606 VXX19837 30.0 1 4-Bromofluorobenzene <surr> 99.8 50-150 % VFC9606 VXX19837 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9606 Analytical Method: SW8015C Analysis Date/Time: 08/14/09 16:23 Prep Batch: VXX19837 Prep Method: SW5030B Prep Date/Time: 08/14/09 13:16 Container ID:1094021004-B Dilution Factor: 1 Analyst: KPW

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2 343 f ( 907 ) 561

. 5 301 w w w . us. sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: 

### RHMW04-WG01 SGS Ref. #: 1094021004 Collection Date/Time: 08/04/09 12:35 Receipt Date/Time: 08/06/09 11:30 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

MDL DF
Diesel Range Organics ND 0.419 mg/L XFC8762 XXX21370 0.157 1 5a Androstane <surr> 82.2 50-150 % XFC8762 XXX21370 1
Batch Information Initial Prep Wt./Vol.: 955 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC8762 Analytical Method: SW8015C Analysis Date/Time: 08/08/09 11:38 Prep Batch: XXX21370 Prep Method: SW3520C Prep Date/Time: 08/07/09 09:25 Container ID:1094021004-J Dilution Factor: 1 Analyst: KDC

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2 343 f ( 907 ) 561

. 5 301 w w w . us. sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: 

### RHMW04-WG01 SGS Ref. #: 1094021004 Collection Date/Time: 08/04/09 12:35 Receipt Date/Time: 08/06/09 11:30 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 ug/L VMS10724 VXX19797 0.120 1 Toluene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Ethylbenzene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 n-Butylbenzene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,4-Dichlorobenzene ND 0.500 ug/L VMS10724 VXX19797 0.150 1 1,2-Dichloroethane ND 0.500 ug/L VMS10724 VXX19797 0.150 1 1,3,5-Trimethylbenzene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 4-Chlorotoluene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Chlorobenzene ND 0.500 ug/L VMS10724 VXX19797 0.150 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L VMS10724 VXX19797 3.10 1 cis-1,2-Dichloroethene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 4-Isopropyltoluene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 cis-1,3-Dichloropropene ND 0.500 ug/L VMS10724 VXX19797 0.150 1 n-Propylbenzene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Styrene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Dibromomethane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 trans-1,3-Dichloropropene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,2,4-Trichlorobenzene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Acetone ND 10.0 ug/L VMS10724 VXX19797 3.10 1 1,1,2,2-Tetrachloroethane ND 0.500 ug/L VMS10724 VXX19797 0.150 1 1,2-Dibromo-3-chloropropane ND 2.00 ug/L VMS10724 VXX19797 0.620 1 Methyl-t-butyl ether ND 5.00 ug/L VMS10724 VXX19797 1.50 1 Tetrachloroethene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Dibromochloromethane ND 0.500 ug/L VMS10724 VXX19797 0.150 1 1,3-Dichloropropane ND 0.400 ug/L VMS10724 VXX19797 0.120 1 1,2-Dibromoethane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Carbon tetrachloride ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,1,1,2-Tetrachloroethane ND 0.500 ug/L VMS10724 VXX19797 0.150 1 Chloroform ND 1.00 ug/L VMS10724 VXX19797 0.300 1 Bromobenzene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Chloromethane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,2,3-Trichloropropane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Bromomethane ND 3.00 ug/L VMS10724 VXX19797 0.940 1 Bromochloromethane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Vinyl chloride ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Dichlorodifluoromethane ND 1.00 ug/L VMS10724 VXX19797 0.310 1

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2 343 f ( 907 ) 561

. 5 301 w w w . us. sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: 

### RHMW04-WG01 SGS Ref. #: 1094021004 Collection Date/Time: 08/04/09 12:35 Receipt Date/Time: 08/06/09 11:30 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Chloroethane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 sec-Butylbenzene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Bromodichloromethane ND 0.500 ug/L VMS10724 VXX19797 0.150 1 1,1-Dichloroethene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 2-Butanone (MEK) ND 10.0 ug/L VMS10724 VXX19797 3.10 1 Methylene chloride ND 5.00 ug/L VMS10724 VXX19797 1.00 1 Trichlorofluoromethane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 P & M -Xylene ND 2.00 ug/L VMS10724 VXX19797 0.620 1 Naphthalene ND 2.00 ug/L VMS10724 VXX19797 0.620 1 o-Xylene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Bromoform ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1-Chlorohexane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,2,4-Trimethylbenzene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 tert-Butylbenzene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,1,1-Trichloroethane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,1-Dichloroethane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 2-Chlorotoluene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Trichloroethene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 trans-1,2-Dichloroethene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,2-Dichlorobenzene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 2,2-Dichloropropane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Hexachlorobutadiene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Isopropylbenzene (Cumene) ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,2-Dichloropropane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,1-Dichloropropene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,1,2-Trichloroethane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,3-Dichlorobenzene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,2,3-Trichlorobenzene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,2-Dichloroethane-D4 <surr> 109 73-120 % VMS10724 VXX19797 1 Toluene-d8 <surr> 99.8 80-120 % VMS10724 VXX19797 1 4-Bromofluorobenzene <surr> 107 76-120 % VMS10724 VXX19797 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS10724 Analytical Method: SW8260B Analysis Date/Time: 08/13/09 00:01 Prep Batch: VXX19797 Prep Method: SW5030B Prep Date/Time: 08/12/09 08:21 Container ID:1094021004-A Dilution Factor: 1 Analyst: SCL

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2 343 f ( 907 ) 561

. 5 301 w w w . us. sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: 

### RHMW04-WG01 SGS Ref. #: 1094021004 Collection Date/Time: 08/04/09 12:35 Receipt Date/Time: 08/06/09 11:30 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0541 ug/L XMS5029 XXX21374 0.0162 1 Acenaphthene ND 0.0541 ug/L XMS5029 XXX21374 0.0162 1 Fluorene ND 0.0541 ug/L XMS5029 XXX21374 0.0162 1 Phenanthrene ND 0.0541 ug/L XMS5029 XXX21374 0.0162 1 Anthracene ND 0.0541 ug/L XMS5029 XXX21374 0.0162 1 Fluoranthene ND 0.0541 ug/L XMS5029 XXX21374 0.0162 1 Pyrene ND 0.0541 ug/L XMS5029 XXX21374 0.0162 1 Benzo(a)Anthracene ND 0.0541 ug/L XMS5029 XXX21374 0.0162 1 Chrysene ND 0.0541 ug/L XMS5029 XXX21374 0.0162 1 Benzo[b]Fluoranthene ND 0.0541 ug/L XMS5029 XXX21374 0.0162 1 Benzo[k]fluoranthene ND 0.0541 ug/L XMS5029 XXX21374 0.0162 1 Benzo[a]pyrene ND 0.0541 ug/L XMS5029 XXX21374 0.0162 1 Indeno[1,2,3-c,d] pyrene ND 0.0541 ug/L XMS5029 XXX21374 0.0162 1 Dibenzo[a,h]anthracene ND 0.0541 ug/L XMS5029 XXX21374 0.0162 1 Benzo[g,h,i]perylene ND 0.0541 ug/L XMS5029 XXX21374 0.0162 1 Naphthalene ND 0.108 ug/L XMS5029 XXX21374 0.0335 1 1-Methylnaphthalene ND 0.0541 ug/L XMS5029 XXX21374 0.0162 1 2-Methylnaphthalene ND 0.0541 ug/L XMS5029 XXX21374 0.0162 1 Terphenyl-d14 <surr> 103 50-135 % XMS5029 XXX21374 1
Batch Information Initial Prep Wt./Vol.: 925 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS5029 Analytical Method: 8270D SIMS Analysis Date/Time: 08/12/09 03:54 Prep Batch: XXX21374 Prep Method: SW3520C Prep Date/Time: 08/07/09 10:00 Container ID:1094021004-H Dilution Factor: 1 Analyst: JDH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2 343 f ( 907 ) 561

. 5 301 w w w . us. sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: 

### RHMWA01-WG01 SGS Ref. #: 1094021005 Collection Date/Time: 08/04/09 12:05 Receipt Date/Time: 08/06/09 11:30 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 ug/L MMS6032 MXX22033 0.310 5
Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS6032 Analytical Method: SW6020 Analysis Date/Time: 08/18/09 19:50 Prep Batch: MXX22033 Prep Method: SW3010A Prep Date/Time: 08/12/09 19:00 Container ID:1094021005-G Dilution Factor: 5 Analyst: NRB

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2 343 f ( 907 ) 561

. 5 301 w w w . us. sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: 

### RHMWA01-WG01 SGS Ref. #: 1094021005 Collection Date/Time: 08/04/09 12:05 Receipt Date/Time: 08/06/09 11:30 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

MDL DF
Gasoline Range Organics ND 100 ug/L VFC9606 VXX19837 30.0 1 4-Bromofluorobenzene <surr> 94.2 50-150 % VFC9606 VXX19837 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9606 Analytical Method: SW8015C Analysis Date/Time: 08/14/09 16:42 Prep Batch: VXX19837 Prep Method: SW5030B Prep Date/Time: 08/14/09 13:16 Container ID:1094021005-B Dilution Factor: 1 Analyst: KPW

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2 343 f ( 907 ) 561

. 5 301 w w w . us. sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: 

### RHMWA01-WG01 SGS Ref. #: 1094021005 Collection Date/Time: 08/04/09 12:05 Receipt Date/Time: 08/06/09 11:30 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

MDL DF
Diesel Range Organics ND 0.430 mg/L XFC8762 XXX21370 0.161 1 5a Androstane <surr> 79.9 50-150 % XFC8762 XXX21370 1
Batch Information Initial Prep Wt./Vol.: 930 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC8762 Analytical Method: SW8015C Analysis Date/Time: 08/08/09 11:48 Prep Batch: XXX21370 Prep Method: SW3520C Prep Date/Time: 08/07/09 09:25 Container ID:1094021005-J Dilution Factor: 1 Analyst: KDC

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2 343 f ( 907 ) 561

. 5 301 w w w . us. sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: 

### RHMWA01-WG01 SGS Ref. #: 1094021005 Collection Date/Time: 08/04/09 12:05 Receipt Date/Time: 08/06/09 11:30 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene 0.250 J 0.400 ug/L VMS10724 VXX19797 0.120 1 Toluene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Ethylbenzene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 n-Butylbenzene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,4-Dichlorobenzene ND 0.500 ug/L VMS10724 VXX19797 0.150 1 1,2-Dichloroethane ND 0.500 ug/L VMS10724 VXX19797 0.150 1 1,3,5-Trimethylbenzene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 4-Chlorotoluene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Chlorobenzene ND 0.500 ug/L VMS10724 VXX19797 0.150 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L VMS10724 VXX19797 3.10 1 cis-1,2-Dichloroethene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 4-Isopropyltoluene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 cis-1,3-Dichloropropene ND 0.500 ug/L VMS10724 VXX19797 0.150 1 n-Propylbenzene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Styrene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Dibromomethane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 trans-1,3-Dichloropropene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,2,4-Trichlorobenzene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Acetone ND 10.0 ug/L VMS10724 VXX19797 3.10 1 1,1,2,2-Tetrachloroethane ND 0.500 ug/L VMS10724 VXX19797 0.150 1 1,2-Dibromo-3-chloropropane ND 2.00 ug/L VMS10724 VXX19797 0.620 1 Methyl-t-butyl ether ND 5.00 ug/L VMS10724 VXX19797 1.50 1 Tetrachloroethene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Dibromochloromethane ND 0.500 ug/L VMS10724 VXX19797 0.150 1 1,3-Dichloropropane ND 0.400 ug/L VMS10724 VXX19797 0.120 1 1,2-Dibromoethane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Carbon tetrachloride ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,1,1,2-Tetrachloroethane ND 0.500 ug/L VMS10724 VXX19797 0.150 1 Chloroform ND 1.00 ug/L VMS10724 VXX19797 0.300 1 Bromobenzene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Chloromethane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,2,3-Trichloropropane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Bromomethane ND 3.00 ug/L VMS10724 VXX19797 0.940 1 Bromochloromethane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Vinyl chloride ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Dichlorodifluoromethane ND 1.00 ug/L VMS10724 VXX19797 0.310 1

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2 343 f ( 907 ) 561

. 5 301 w w w . us. sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: 

### RHMWA01-WG01 SGS Ref. #: 1094021005 Collection Date/Time: 08/04/09 12:05 Receipt Date/Time: 08/06/09 11:30 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Chloroethane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 sec-Butylbenzene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Bromodichloromethane ND 0.500 ug/L VMS10724 VXX19797 0.150 1 1,1-Dichloroethene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 2-Butanone (MEK) ND 10.0 ug/L VMS10724 VXX19797 3.10 1 Methylene chloride ND 5.00 ug/L VMS10724 VXX19797 1.00 1 Trichlorofluoromethane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 P & M -Xylene ND 2.00 ug/L VMS10724 VXX19797 0.620 1 Naphthalene ND 2.00 ug/L VMS10724 VXX19797 0.620 1 o-Xylene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Bromoform ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1-Chlorohexane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,2,4-Trimethylbenzene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 tert-Butylbenzene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,1,1-Trichloroethane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,1-Dichloroethane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 2-Chlorotoluene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Trichloroethene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 trans-1,2-Dichloroethene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,2-Dichlorobenzene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 2,2-Dichloropropane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Hexachlorobutadiene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 Isopropylbenzene (Cumene) ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,2-Dichloropropane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,1-Dichloropropene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,1,2-Trichloroethane ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,3-Dichlorobenzene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,2,3-Trichlorobenzene ND 1.00 ug/L VMS10724 VXX19797 0.310 1 1,2-Dichloroethane-D4 <surr> 106 73-120 % VMS10724 VXX19797 1 Toluene-d8 <surr> 101 80-120 % VMS10724 VXX19797 1 4-Bromofluorobenzene <surr> 103 76-120 % VMS10724 VXX19797 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS10724 Analytical Method: SW8260B Analysis Date/Time: 08/13/09 02:49 Prep Batch: VXX19797 Prep Method: SW5030B Prep Date/Time: 08/12/09 08:21 Container ID:1094021005-A Dilution Factor: 1 Analyst: SCL

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2 343 f ( 907 ) 561

. 5 301 w w w . us. sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: 

### RHMWA01-WG01 SGS Ref. #: 1094021005 Collection Date/Time: 08/04/09 12:05 Receipt Date/Time: 08/06/09 11:30 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0556 ug/L XMS5029 XXX21374 0.0167 1 Acenaphthene ND 0.0556 ug/L XMS5029 XXX21374 0.0167 1 Fluorene ND 0.0556 ug/L XMS5029 XXX21374 0.0167 1 Phenanthrene ND 0.0556 ug/L XMS5029 XXX21374 0.0167 1 Anthracene ND 0.0556 ug/L XMS5029 XXX21374 0.0167 1 Fluoranthene ND 0.0556 ug/L XMS5029 XXX21374 0.0167 1 Pyrene ND 0.0556 ug/L XMS5029 XXX21374 0.0167 1 Benzo(a)Anthracene ND 0.0556 ug/L XMS5029 XXX21374 0.0167 1 Chrysene ND 0.0556 ug/L XMS5029 XXX21374 0.0167 1 Benzo[b]Fluoranthene ND 0.0556 ug/L XMS5029 XXX21374 0.0167 1 Benzo[k]fluoranthene ND 0.0556 ug/L XMS5029 XXX21374 0.0167 1 Benzo[a]pyrene ND 0.0556 ug/L XMS5029 XXX21374 0.0167 1 Indeno[1,2,3-c,d] pyrene ND 0.0556 ug/L XMS5029 XXX21374 0.0167 1 Dibenzo[a,h]anthracene ND 0.0556 ug/L XMS5029 XXX21374 0.0167 1 Benzo[g,h,i]perylene ND 0.0556 ug/L XMS5029 XXX21374 0.0167 1 Naphthalene ND 0.111 ug/L XMS5029 XXX21374 0.0344 1 1-Methylnaphthalene ND 0.0556 ug/L XMS5029 XXX21374 0.0167 1 2-Methylnaphthalene ND 0.0556 ug/L XMS5029 XXX21374 0.0167 1 Terphenyl-d14 <surr> 99.7 50-135 % XMS5029 XXX21374 1
Batch Information Initial Prep Wt./Vol.: 900 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS5029 Analytical Method: 8270D SIMS Analysis Date/Time: 08/12/09 04:28 Prep Batch: XXX21374 Prep Method: SW3520C Prep Date/Time: 08/07/09 10:00 Container ID:1094021005-H Dilution Factor: 1 Analyst: JDH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2 343 f ( 907 ) 561

. 5 301 w w w . us. sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: 

### TB01-WG01 SGS Ref. #: 1094021006 Collection Date/Time: 08/04/09 08:00 Receipt Date/Time: 08/06/09 11:30 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

MDL DF
Gasoline Range Organics ND 100 ug/L VFC9606 VXX19837 30.0 1 4-Bromofluorobenzene <surr> 93.9 50-150 % VFC9606 VXX19837 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9606 Analytical Method: SW8015C Analysis Date/Time: 08/14/09 17:01 Prep Batch: VXX19837 Prep Method: SW5030B Prep Date/Time: 08/14/09 13:16 Container ID:1094021006-C Dilution Factor: 1 Analyst: KPW

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2 343 f ( 907 ) 561

. 5 301 w w w . us. sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: 

### TB01-WG01 SGS Ref. #: 1094021006 Collection Date/Time: 08/04/09 08:00 Receipt Date/Time: 08/06/09 11:30 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 ug/L VMS10728 VXX19797 0.120 1 Toluene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 Ethylbenzene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 n-Butylbenzene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 1,4-Dichlorobenzene ND 0.500 ug/L VMS10728 VXX19797 0.150 1 1,2-Dichloroethane ND 0.500 ug/L VMS10728 VXX19797 0.150 1 1,3,5-Trimethylbenzene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 4-Chlorotoluene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 Chlorobenzene ND 0.500 ug/L VMS10728 VXX19797 0.150 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L VMS10728 VXX19797 3.10 1 cis-1,2-Dichloroethene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 4-Isopropyltoluene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 cis-1,3-Dichloropropene ND 0.500 ug/L VMS10728 VXX19797 0.150 1 n-Propylbenzene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 Styrene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 Dibromomethane ND 1.00 ug/L VMS10728 VXX19797 0.310 1 trans-1,3-Dichloropropene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 1,2,4-Trichlorobenzene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 Acetone 3.33 J 10.0 ug/L VMS10736 VXX19816 3.10 1 1,1,2,2-Tetrachloroethane ND 0.500 ug/L VMS10728 VXX19797 0.150 1 1,2-Dibromo-3-chloropropane ND 2.00 ug/L VMS10728 VXX19797 0.620 1 Methyl-t-butyl ether ND 5.00 ug/L VMS10728 VXX19797 1.50 1 Tetrachloroethene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 Dibromochloromethane ND 0.500 ug/L VMS10728 VXX19797 0.150 1 1,3-Dichloropropane ND 0.400 ug/L VMS10728 VXX19797 0.120 1 1,2-Dibromoethane ND 1.00 ug/L VMS10728 VXX19797 0.310 1 Carbon tetrachloride ND 1.00 ug/L VMS10728 VXX19797 0.310 1 1,1,1,2-Tetrachloroethane ND 0.500 ug/L VMS10728 VXX19797 0.150 1 Chloroform ND 1.00 ug/L VMS10728 VXX19797 0.300 1 Bromobenzene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 Chloromethane ND 1.00 ug/L VMS10728 VXX19797 0.310 1 1,2,3-Trichloropropane ND 1.00 ug/L VMS10728 VXX19797 0.310 1 Bromomethane ND 3.00 ug/L VMS10728 VXX19797 0.940 1 Bromochloromethane ND 1.00 ug/L VMS10728 VXX19797 0.310 1 Vinyl chloride ND 1.00 ug/L VMS10728 VXX19797 0.310 1 Dichlorodifluoromethane ND 1.00 ug/L VMS10728 VXX19797 0.310 1

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2 343 f ( 907 ) 561

. 5 301 w w w . us. sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: 

### TB01-WG01 SGS Ref. #: 1094021006 Collection Date/Time: 08/04/09 08:00 Receipt Date/Time: 08/06/09 11:30 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Chloroethane ND 1.00 ug/L VMS10728 VXX19797 0.310 1 sec-Butylbenzene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 Bromodichloromethane ND 0.500 ug/L VMS10728 VXX19797 0.150 1 1,1-Dichloroethene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 2-Butanone (MEK) ND 10.0 ug/L VMS10736 VXX19816 3.10 1 Methylene chloride ND 5.00 ug/L VMS10728 VXX19797 1.00 1 Trichlorofluoromethane ND 1.00 ug/L VMS10728 VXX19797 0.310 1 P & M -Xylene ND 2.00 ug/L VMS10728 VXX19797 0.620 1 Naphthalene ND 2.00 ug/L VMS10728 VXX19797 0.620 1 o-Xylene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 Bromoform ND 1.00 ug/L VMS10728 VXX19797 0.310 1 1-Chlorohexane ND 1.00 ug/L VMS10728 VXX19797 0.310 1 1,2,4-Trimethylbenzene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 tert-Butylbenzene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 1,1,1-Trichloroethane ND 1.00 ug/L VMS10728 VXX19797 0.310 1 1,1-Dichloroethane ND 1.00 ug/L VMS10728 VXX19797 0.310 1 2-Chlorotoluene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 Trichloroethene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 trans-1,2-Dichloroethene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 1,2-Dichlorobenzene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 2,2-Dichloropropane ND 1.00 ug/L VMS10728 VXX19797 0.310 1 Hexachlorobutadiene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 Isopropylbenzene (Cumene) ND 1.00 ug/L VMS10728 VXX19797 0.310 1 1,2-Dichloropropane ND 1.00 ug/L VMS10728 VXX19797 0.310 1 1,1-Dichloropropene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 1,1,2-Trichloroethane ND 1.00 ug/L VMS10728 VXX19797 0.310 1 1,3-Dichlorobenzene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 1,2,3-Trichlorobenzene ND 1.00 ug/L VMS10728 VXX19797 0.310 1 1,2-Dichloroethane-D4 <surr> 106 73-120 % VMS10728 VXX19797 1 Toluene-d8 <surr> 101 80-120 % VMS10728 VXX19797 1 4-Bromofluorobenzene <surr> 102 76-120 % VMS10728 VXX19797 1

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2 343 f ( 907 ) 561

. 5 301 w w w . us. sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: 

### TB01-WG01 SGS Ref. #: 1094021006 Collection Date/Time: 08/04/09 08:00 Receipt Date/Time: 08/06/09 11:30 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS10728 Analytical Method: SW8260B Analysis Date/Time: 08/14/09 03:46 Prep Batch: VXX19797 Prep Method: SW5030B Prep Date/Time: 08/12/09 08:21 Container ID:1094021006-B Dilution Factor: 1 Analyst: SCL Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS10736 Analytical Method: SW8260B Analysis Date/Time: 08/14/09 22:41 Prep Batch: VXX19816 Prep Method: SW5030B Prep Date/Time: 08/14/09 08:51 Container ID:1094021006-A Dilution Factor: 1 Analyst: SCL

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2 343 f ( 907 ) 561

. 5 301 w w w . us. sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)Matrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 914006 Method Blank The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) XXX21370 SW3520C 08/07/2009 QC results affect the following production samples: 

### 1094021001, 1094021004, 1094021005

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Semivolatile Organic Fuels Department 

### Diesel Range Organics 0.190 J 0.400 mg/L 08/08/09 

### 0.150 Surrogates


### 5a Androstane <surr> 88.5 60-120 % 08/08/09

Instrument Method Batch XFC8762

SW8015C HP 6890 Series II FID SV D RMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 914030 Method Blank The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) XXX21374 SW3520C 08/07/2009 QC results affect the following production samples: 

### 1094021001, 1094021004, 1094021005

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Polynuclear Aromatics GC/MS 

### Acenaphthylene ND 0.0500 ug/L 08/12/09 

### 0.0150 Acenaphthene ND 0.0500 ug/L 08/12/09 

### 0.0150 Fluorene ND 0.0500 ug/L 08/12/09 

### 0.0150 Phenanthrene ND 0.0500 ug/L 08/12/09 

### 0.0150 Anthracene ND 0.0500 ug/L 08/12/09 

### 0.0150 Fluoranthene ND 0.0500 ug/L 08/12/09 

### 0.0150 Pyrene ND 0.0500 ug/L 08/12/09 

### 0.0150 Benzo(a)Anthracene ND 0.0500 ug/L 08/12/09 

### 0.0150 Chrysene ND 0.0500 ug/L 08/12/09 

### 0.0150 Benzo[b]Fluoranthene ND 0.0500 ug/L 08/12/09 

### 0.0150 Benzo[k]fluoranthene ND 0.0500 ug/L 08/12/09 

### 0.0150 Benzo[a]pyrene ND 0.0500 ug/L 08/12/09 

### 0.0150 Indeno[1,2,3-c,d] pyrene ND 0.0500 ug/L 08/12/09 

### 0.0150 Dibenzo[a,h]anthracene ND 0.0500 ug/L 08/12/09 

### 0.0150 Benzo[g,h,i]perylene ND 0.0500 ug/L 08/12/09 

### 0.0150 Naphthalene ND 0.100 ug/L 08/12/09 

### 0.0310 1-Methylnaphthalene ND 0.0500 ug/L 08/12/09 

### 0.0150 2-Methylnaphthalene ND 0.0500 ug/L 08/12/09 

### 0.0150 Surrogates 

### Terphenyl-d14 <surr> 105 50-135 % 08/12/09

Instrument Method Batch XMS5029

8270D SIMS HP 6890/5973 MS SVQAMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 915442 Method Blank The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) MXX22033 SW3010A 08/12/2009 QC results affect the following production samples: 

### 1094021001, 1094021004, 1094021005

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Metals by ICP/MS



### Lead ND 1.00 ug/L 08/18/09 

### 0.310

Instrument Method Batch MMS6032

SW6020 Perkin Elmer Sciex ICP-MS P3Matrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 915595 Method Blank The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19797 SW5030B 08/12/2009 QC results affect the following production samples: 

### 1094021004, 1094021005, 1094021006

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Volatile Gas Chromatography/Mass SpectroscopyMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 915595 Method Blank The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19797 SW5030B 08/12/2009

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Volatile Gas Chromatography/Mass Spectroscopy



### Benzene ND 0.400 ug/L 08/12/09 

### 0.120 Toluene ND 1.00 ug/L 08/12/09 

### 0.310 Ethylbenzene ND 1.00 ug/L 08/12/09 

### 0.310 n-Butylbenzene ND 1.00 ug/L 08/12/09 

### 0.310 1,4-Dichlorobenzene ND 0.500 ug/L 08/12/09 

### 0.150 1,2-Dichloroethane ND 0.500 ug/L 08/12/09 

### 0.150 1,3,5-Trimethylbenzene ND 1.00 ug/L 08/12/09 

### 0.310 4-Chlorotoluene ND 1.00 ug/L 08/12/09 

### 0.310 Chlorobenzene ND 0.500 ug/L 08/12/09 

### 0.150 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L 08/12/09 

### 3.10 cis-1,2-Dichloroethene ND 1.00 ug/L 08/12/09 

### 0.310 4-Isopropyltoluene ND 1.00 ug/L 08/12/09 

### 0.310 cis-1,3-Dichloropropene ND 0.500 ug/L 08/12/09 

### 0.150 n-Propylbenzene ND 1.00 ug/L 08/12/09 

### 0.310 Styrene ND 1.00 ug/L 08/12/09 

### 0.310 Dibromomethane ND 1.00 ug/L 08/12/09 

### 0.310 trans-1,3-Dichloropropene ND 1.00 ug/L 08/12/09 

### 0.310 1,2,4-Trichlorobenzene ND 1.00 ug/L 08/12/09 

### 0.310 Acetone ND 10.0 ug/L 08/12/09 

### 3.10 1,1,2,2-Tetrachloroethane ND 0.500 ug/L 08/12/09 

### 0.150 1,2-Dibromo-3-chloropropane ND 2.00 ug/L 08/12/09 

### 0.620 Methyl-t-butyl ether ND 5.00 ug/L 08/12/09 

### 1.50 Tetrachloroethene ND 1.00 ug/L 08/12/09 

### 0.310 Dibromochloromethane ND 0.500 ug/L 08/12/09 

### 0.150 1,3-Dichloropropane ND 0.400 ug/L 08/12/09 

### 0.120 1,2-Dibromoethane ND 1.00 ug/L 08/12/09 

### 0.310 Carbon tetrachloride ND 1.00 ug/L 08/12/09 

### 0.310 1,1,1,2-Tetrachloroethane ND 0.500 ug/L 08/12/09 

### 0.150 Chloroform ND 1.00 ug/L 08/12/09 

### 0.300 Bromobenzene ND 1.00 ug/L 08/12/09 

### 0.310 Chloromethane ND 1.00 ug/L 08/12/09 

### 0.310 1,2,3-Trichloropropane ND 1.00 ug/L 08/12/09 

### 0.310 Bromomethane ND 3.00 ug/L 08/12/09 

### 0.940 Bromochloromethane ND 1.00 ug/L 08/12/09 

### 0.310 Vinyl chloride ND 1.00 ug/L 08/12/09 

### 0.310 Dichlorodifluoromethane ND 1.00 ug/L 08/12/09 

### 0.310 Chloroethane ND 1.00 ug/L 08/12/09 

### 0.310 sec-Butylbenzene ND 1.00 ug/L 08/12/09 

### 0.310 Bromodichloromethane ND 0.500 ug/L 08/12/09 

### 0.150Matrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 915595 Method Blank The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19797 SW5030B 08/12/2009

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Volatile Gas Chromatography/Mass Spectroscopy


### 1,1-Dichloroethene ND 1.00 ug/L 08/12/09 

### 0.310 2-Butanone (MEK) ND 10.0 ug/L 08/12/09 

### 3.10 Methylene chloride ND 5.00 ug/L 08/12/09 

### 1.00 Trichlorofluoromethane ND 1.00 ug/L 08/12/09 

### 0.310 P & M -Xylene ND 2.00 ug/L 08/12/09 

### 0.620 Naphthalene ND 2.00 ug/L 08/12/09 

### 0.620 o-Xylene ND 1.00 ug/L 08/12/09 

### 0.310 Bromoform ND 1.00 ug/L 08/12/09 

### 0.310 1-Chlorohexane ND 1.00 ug/L 08/12/09 

### 0.310 1,2,4-Trimethylbenzene ND 1.00 ug/L 08/12/09 

### 0.310 tert-Butylbenzene ND 1.00 ug/L 08/12/09 

### 0.310 1,1,1-Trichloroethane ND 1.00 ug/L 08/12/09 

### 0.310 1,1-Dichloroethane ND 1.00 ug/L 08/12/09 

### 0.310 2-Chlorotoluene ND 1.00 ug/L 08/12/09 

### 0.310 Trichloroethene ND 1.00 ug/L 08/12/09 

### 0.310 trans-1,2-Dichloroethene ND 1.00 ug/L 08/12/09 

### 0.310 1,2-Dichlorobenzene ND 1.00 ug/L 08/12/09 

### 0.310 2,2-Dichloropropane ND 1.00 ug/L 08/12/09 

### 0.310 Hexachlorobutadiene ND 1.00 ug/L 08/12/09 

### 0.310 Isopropylbenzene (Cumene) ND 1.00 ug/L 08/12/09 

### 0.310 1,2-Dichloropropane ND 1.00 ug/L 08/12/09 

### 0.310 1,1-Dichloropropene ND 1.00 ug/L 08/12/09 

### 0.310 1,1,2-Trichloroethane ND 1.00 ug/L 08/12/09 

### 0.310 1,3-Dichlorobenzene ND 1.00 ug/L 08/12/09 

### 0.310 1,2,3-Trichlorobenzene ND 1.00 ug/L 08/12/09 

### 0.310 Surrogates 

### 1,2-Dichloroethane-D4 <surr> 108 73-120 % 08/12/09 

### Toluene-d8 <surr> 101 80-120 % 08/12/09 

### 4-Bromofluorobenzene <surr> 103 76-120 % 08/12/09

Instrument Method Batch VMS10724

SW8260B HP 5890 Series II MS3 VNAMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 915946 Method Blank The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19810 SW5030B 08/13/2009 QC results affect the following production samples: 

### 1094021001

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Volatile Gas Chromatography/Mass SpectroscopyMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 915946 Method Blank The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19810 SW5030B 08/13/2009

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Volatile Gas Chromatography/Mass Spectroscopy



### Benzene ND 0.400 ug/L 08/13/09 

### 0.120 Toluene ND 1.00 ug/L 08/13/09 

### 0.310 Ethylbenzene ND 1.00 ug/L 08/13/09 

### 0.310 n-Butylbenzene ND 1.00 ug/L 08/13/09 

### 0.310 1,4-Dichlorobenzene ND 0.500 ug/L 08/13/09 

### 0.150 1,2-Dichloroethane ND 0.500 ug/L 08/13/09 

### 0.150 1,3,5-Trimethylbenzene ND 1.00 ug/L 08/13/09 

### 0.310 4-Chlorotoluene ND 1.00 ug/L 08/13/09 

### 0.310 Chlorobenzene ND 0.500 ug/L 08/13/09 

### 0.150 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L 08/13/09 

### 3.10 cis-1,2-Dichloroethene ND 1.00 ug/L 08/13/09 

### 0.310 4-Isopropyltoluene ND 1.00 ug/L 08/13/09 

### 0.310 cis-1,3-Dichloropropene ND 0.500 ug/L 08/13/09 

### 0.150 n-Propylbenzene ND 1.00 ug/L 08/13/09 

### 0.310 Styrene ND 1.00 ug/L 08/13/09 

### 0.310 Dibromomethane ND 1.00 ug/L 08/13/09 

### 0.310 trans-1,3-Dichloropropene ND 1.00 ug/L 08/13/09 

### 0.310 1,2,4-Trichlorobenzene ND 1.00 ug/L 08/13/09 

### 0.310 Acetone ND 10.0 ug/L 08/13/09 

### 3.10 1,1,2,2-Tetrachloroethane ND 0.500 ug/L 08/13/09 

### 0.150 1,2-Dibromo-3-chloropropane ND 2.00 ug/L 08/13/09 

### 0.620 Methyl-t-butyl ether ND 5.00 ug/L 08/13/09 

### 1.50 Tetrachloroethene ND 1.00 ug/L 08/13/09 

### 0.310 Dibromochloromethane ND 0.500 ug/L 08/13/09 

### 0.150 1,3-Dichloropropane ND 0.400 ug/L 08/13/09 

### 0.120 1,2-Dibromoethane ND 1.00 ug/L 08/13/09 

### 0.310 Carbon tetrachloride ND 1.00 ug/L 08/13/09 

### 0.310 1,1,1,2-Tetrachloroethane ND 0.500 ug/L 08/13/09 

### 0.150 Chloroform ND 1.00 ug/L 08/13/09 

### 0.300 Bromobenzene ND 1.00 ug/L 08/13/09 

### 0.310 Chloromethane ND 1.00 ug/L 08/13/09 

### 0.310 1,2,3-Trichloropropane ND 1.00 ug/L 08/13/09 

### 0.310 Bromomethane ND 3.00 ug/L 08/13/09 

### 0.940 Bromochloromethane ND 1.00 ug/L 08/13/09 

### 0.310 Vinyl chloride ND 1.00 ug/L 08/13/09 

### 0.310 Dichlorodifluoromethane ND 1.00 ug/L 08/13/09 

### 0.310 Chloroethane ND 1.00 ug/L 08/13/09 

### 0.310 sec-Butylbenzene ND 1.00 ug/L 08/13/09 

### 0.310 Bromodichloromethane ND 0.500 ug/L 08/13/09 

### 0.150Matrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 915946 Method Blank The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19810 SW5030B 08/13/2009

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Volatile Gas Chromatography/Mass Spectroscopy


### 1,1-Dichloroethene ND 1.00 ug/L 08/13/09 

### 0.310 2-Butanone (MEK) ND 10.0 ug/L 08/13/09 

### 3.10 Methylene chloride ND 5.00 ug/L 08/13/09 

### 1.00 Trichlorofluoromethane ND 1.00 ug/L 08/13/09 

### 0.310 P & M -Xylene ND 2.00 ug/L 08/13/09 

### 0.620 Naphthalene ND 2.00 ug/L 08/13/09 

### 0.620 o-Xylene ND 1.00 ug/L 08/13/09 

### 0.310 Bromoform ND 1.00 ug/L 08/13/09 

### 0.310 1-Chlorohexane ND 1.00 ug/L 08/13/09 

### 0.310 1,2,4-Trimethylbenzene ND 1.00 ug/L 08/13/09 

### 0.310 tert-Butylbenzene ND 1.00 ug/L 08/13/09 

### 0.310 1,1,1-Trichloroethane ND 1.00 ug/L 08/13/09 

### 0.310 1,1-Dichloroethane ND 1.00 ug/L 08/13/09 

### 0.310 2-Chlorotoluene ND 1.00 ug/L 08/13/09 

### 0.310 Trichloroethene ND 1.00 ug/L 08/13/09 

### 0.310 trans-1,2-Dichloroethene ND 1.00 ug/L 08/13/09 

### 0.310 1,2-Dichlorobenzene ND 1.00 ug/L 08/13/09 

### 0.310 2,2-Dichloropropane ND 1.00 ug/L 08/13/09 

### 0.310 Hexachlorobutadiene ND 1.00 ug/L 08/13/09 

### 0.310 Isopropylbenzene (Cumene) ND 1.00 ug/L 08/13/09 

### 0.310 1,2-Dichloropropane ND 1.00 ug/L 08/13/09 

### 0.310 1,1-Dichloropropene ND 1.00 ug/L 08/13/09 

### 0.310 1,1,2-Trichloroethane ND 1.00 ug/L 08/13/09 

### 0.310 1,3-Dichlorobenzene ND 1.00 ug/L 08/13/09 

### 0.310 1,2,3-Trichlorobenzene ND 1.00 ug/L 08/13/09 

### 0.310 Surrogates 

### 1,2-Dichloroethane-D4 <surr> 117 73-120 % 08/13/09 

### Toluene-d8 <surr> 99.3 80-120 % 08/13/09 

### 4-Bromofluorobenzene <surr> 103 76-120 % 08/13/09

Instrument Method Batch VMS10730

SW8260B HP 5890 Series II MS3 VNAMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 916338 Method Blank The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19816 SW5030B 08/14/2009 QC results affect the following production samples: 

### 1094021006

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Volatile Gas Chromatography/Mass Spectroscopy



### Acetone ND 10.0 ug/L 08/14/09 

### 3.10 2-Butanone (MEK) ND 10.0 ug/L 08/14/09 

### 3.10 Surrogates 

### 1,2-Dichloroethane-D4 <surr> 108 73-120 % 08/14/09 

### Toluene-d8 <surr> 99.1 80-120 % 08/14/09 

### 4-Bromofluorobenzene <surr> 103 76-120 % 08/14/09

Instrument Method Batch VMS10736

SW8260B HP 5890 Series II MS3 VNAMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 917244 Method Blank The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19837 SW5030B 08/14/2009 QC results affect the following production samples: 

### 1094021001, 1094021004, 1094021005, 1094021006

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Volatile Fuels Department 

### Gasoline Range Organics ND 100 ug/L 08/14/09 

### 30.0 Surrogates


### 4-Bromofluorobenzene <surr> 93.7 50-150 % 08/14/09

Instrument Method Batch VFC9606

SW8015C HP 5890 Series II PID+HECD VBAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 914008 Lab Control Sample 914009 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) XXX21370 SW3520C 08/07/2009

QC results affect the following production samples: 

### 1094021001, 1094021004, 1094021005

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Semivolatile Organic Fuels Department 

### Diesel Range Organics LCS 4.40 88 ( 75-125 ) 5 mg/L 08/08/2009 LCSD 4.25 85 4 (< 20 ) 5 mg/L 08/08/2009

Surrogates 

### 5a Androstane <surr> LCS 93 ( 60-120 ) 08/08/2009 LCSD 90 3 08/08/2009

Batch Method Instrument 

### XFC8762

SW8015C HP 6890 Series II FID SV D RMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 914031 Lab Control Sample
The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) XXX21374 SW3520C 08/07/2009

QC results affect the following production samples: 

### 1094021001, 1094021004, 1094021005

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Polynuclear Aromatics GC/MSMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 914031 Lab Control Sample
The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) XXX21374 SW3520C 08/07/2009

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Polynuclear Aromatics GC/MS 

### Acenaphthylene LCS 0.429 86 ( 50-105 ) 0.5 ug/L 08/12/2009
Acenaphthene LCS 0.415 83 ( 45-110 ) 0.5 ug/L 08/12/2009

Fluorene LCS 0.452 90 ( 50-110 ) 0.5 ug/L 08/12/2009

Phenanthrene LCS 0.453 91 ( 50-115 ) 0.5 ug/L 08/12/2009

Anthracene LCS 0.480 96 ( 55-110 ) 0.5 ug/L 08/12/2009

Fluoranthene LCS 0.510 102 ( 55-125 ) 0.5 ug/L 08/12/2009
Pyrene LCS 0.486 97 ( 50-130 ) 0.5 ug/L 08/12/2009
Benzo(a)Anthracene LCS 0.536 107 ( 55-120 ) 0.5 ug/L 08/12/2009
Chrysene LCS 0.489 98 ( 55-120 ) 0.5 ug/L 08/12/2009
Benzo[b]Fluoranthene LCS 0.524 105 ( 46-130 ) 0.5 ug/L 08/12/2009
Benzo[k]fluoranthene LCS 0.518 104 ( 60-125 ) 0.5 ug/L 08/12/2009
Benzo[a]pyrene LCS 0.515 103 ( 55-120 ) 0.5 ug/L 08/12/2009
Indeno[1,2,3-c,d] pyrene LCS 0.479 96 ( 45-125 ) 0.5 ug/L 08/12/2009
Dibenzo[a,h]anthracene LCS 0.483 97 ( 41-140 ) 0.5 ug/L 08/12/2009
Benzo[g,h,i]perylene LCS 0.503 101 ( 46-125 ) 0.5 ug/L 08/12/2009
Naphthalene LCS 0.391 78 ( 42-100 ) 0.5 ug/L 08/12/2009
1-Methylnaphthalene LCS 0.387 78 ( 46-115 ) 0.5 ug/L 08/12/2009
2-Methylnaphthalene LCS 0.389 78 ( 45-105 ) 0.5 ug/L 08/12/2009

Surrogates 

### Terphenyl-d14 <surr> LCS 98 ( 50-135 ) 08/12/2009Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 914031 Lab Control Sample
The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) XXX21374 SW3520C 08/07/2009

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Polynuclear Aromatics GC/MS

Batch Method Instrument 

### XMS5029

8270D SIMS HP 6890/5973 MS SVQAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 915443 Lab Control Sample
The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) MXX22033 SW3010A 08/12/2009

QC results affect the following production samples: 

### 1094021001, 1094021004, 1094021005

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Metals by ICP/MS


### Lead LCS 1030 103 ( 80-120 ) 1000 ug/L 08/18/2009

Batch Method Instrument 

### MMS6032

SW6020 Perkin Elmer Sciex ICP-MS P3Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 915596 Lab Control Sample 915597 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19797 SW5030B 08/12/2009

QC results affect the following production samples: 

### 1094021004, 1094021005, 1094021006

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass SpectroscopyMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 915596 Lab Control Sample 915597 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19797 SW5030B 08/12/2009

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy


### Benzene LCS 28.8 96 ( 80-120 ) 30 ug/L 08/12/2009 LCSD 27.9 93 3 (< 20 ) 30 ug/L 08/12/2009

Toluene LCS 29.7 99 ( 77-120 ) 30 ug/L 08/12/2009 LCSD 28.8 96 3 (< 20 ) 30 ug/L 08/12/2009
Ethylbenzene LCS 32.0 107 ( 80-120 ) 30 ug/L 08/12/2009 LCSD 30.6 102 5 (< 20 ) 30 ug/L 08/12/2009
n-Butylbenzene LCS 33.7 112 ( 80-124 ) 30 ug/L 08/12/2009 LCSD 33.2 111 1 (< 20 ) 30 ug/L 08/12/2009
1,4-Dichlorobenzene LCS 29.8 99 ( 80-120 ) 30 ug/L 08/12/2009 LCSD 29.5 98 1 (< 20 ) 30 ug/L 08/12/2009
1,2-Dichloroethane LCS 31.7 106 ( 80-129 ) 30 ug/L 08/12/2009 LCSD 30.6 102 4 (< 20 ) 30 ug/L 08/12/2009
1,3,5-Trimethylbenzene LCS 31.4 105 ( 80-128 ) 30 ug/L 08/12/2009 LCSD 30.7 102 2 (< 20 ) 30 ug/L 08/12/2009

4-Chlorotoluene LCS 30.4 101 ( 79-128 ) 30 ug/L 08/12/2009 LCSD 30.0 100 2 (< 20 ) 30 ug/L 08/12/2009

Chlorobenzene LCS 30.2 101 ( 80-120 ) 30 ug/L 08/12/2009 LCSD 29.7 99 1 (< 20 ) 30 ug/L 08/12/2009
4-Methyl-2-pentanone (MIBK) LCS 81.9 91 ( 69-134 ) 90 ug/L 08/12/2009 LCSD 84.5 94 3 (< 20 ) 90 ug/L 08/12/2009
cis-1,2-Dichloroethene LCS 29.7 99 ( 80-125 ) 30 ug/L 08/12/2009 LCSD 29.1 97 2 (< 20 ) 30 ug/L 08/12/2009
4-Isopropyltoluene LCS 32.7 109 ( 80-125 ) 30 ug/L 08/12/2009 LCSD 31.9 106 3 (< 20 ) 30 ug/L 08/12/2009
cis-1,3-Dichloropropene LCS 28.7 96 ( 80-120 ) 30 ug/L 08/12/2009 LCSD 28.2 94 2 (< 20 ) 30 ug/L 08/12/2009
n-Propylbenzene LCS 31.3 104 ( 80-129 ) 30 ug/L 08/12/2009 LCSD 30.9 103 1 (< 20 ) 30 ug/L 08/12/2009Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 915596 Lab Control Sample 915597 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19797 SW5030B 08/12/2009

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### Styrene LCS 32.4 108 ( 80-120 ) 30 ug/L 08/12/2009 LCSD 31.6 105 3 (< 20 ) 30 ug/L 08/12/2009

Dibromomethane LCS 30.2 101 ( 80-120 ) 30 ug/L 08/12/2009 LCSD 29.1 97 4 (< 20 ) 30 ug/L 08/12/2009
trans-1,3-Dichloropropene LCS 29.2 97 ( 80-124 ) 30 ug/L 08/12/2009 LCSD 28.6 95 2 (< 20 ) 30 ug/L 08/12/2009
1,2,4-Trichlorobenzene LCS 27.9 93 ( 80-120 ) 30 ug/L 08/12/2009 LCSD 28.4 95 2 (< 20 ) 30 ug/L 08/12/2009

Acetone LCS 146 162 ( 50-135 ) * 90 ug/L 08/12/2009 LCSD 126 140 * 14 (< 20 ) 90 ug/L 08/12/2009
1,1,2,2-Tetrachloroethane LCS 28.8 96 ( 76-123 ) 30 ug/L 08/12/2009 LCSD 28.7 96 0 (< 20 ) 30 ug/L 08/12/2009
1,2-Dibromo-3-chloropropane LCS 26.4 88 ( 73-130 ) 30 ug/L 08/12/2009 LCSD 28.1 94 6 (< 20 ) 30 ug/L 08/12/2009
Methyl-t-butyl ether LCS 43.2 96 ( 80-120 ) 45 ug/L 08/12/2009 LCSD 43.5 97 1 (< 20 ) 45 ug/L 08/12/2009

Tetrachloroethene LCS 31.4 105 ( 79-122 ) 30 ug/L 08/12/2009 LCSD 30.7 102 2 (< 20 ) 30 ug/L 08/12/2009

Dibromochloromethane LCS 28.5 95 ( 80-120 ) 30 ug/L 08/12/2009 LCSD 28.8 96 1 (< 20 ) 30 ug/L 08/12/2009
1,3-Dichloropropane LCS 30.1 100 ( 80-121 ) 30 ug/L 08/12/2009 LCSD 29.6 99 2 (< 20 ) 30 ug/L 08/12/2009
1,2-Dibromoethane LCS 30.7 102 ( 80-120 ) 30 ug/L 08/12/2009 LCSD 30.6 102 0 (< 20 ) 30 ug/L 08/12/2009

Carbon tetrachloride LCS 31.2 104 ( 80-126 ) 30 ug/L 08/12/2009 LCSD 29.6 99 5 (< 20 ) 30 ug/L 08/12/2009
1,1,1,2-Tetrachloroethane LCS 34.4 115 ( 80-120 ) 30 ug/L 08/12/2009Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 915596 Lab Control Sample 915597 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19797 SW5030B 08/12/2009

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### LCSD 33.1 110 4 (< 20 ) 30 ug/L 08/12/2009

Chloroform LCS 31.4 105 ( 80-124 ) 30 ug/L 08/12/2009 LCSD 30.5 102 3 (< 20 ) 30 ug/L 08/12/2009

Bromobenzene LCS 28.8 96 ( 80-120 ) 30 ug/L 08/12/2009 LCSD 28.7 96 0 (< 20 ) 30 ug/L 08/12/2009

Chloromethane LCS 35.1 117 ( 67-125 ) 30 ug/L 08/12/2009 LCSD 33.4 111 5 (< 20 ) 30 ug/L 08/12/2009
1,2,3-Trichloropropane LCS 28.9 96 ( 80-120 ) 30 ug/L 08/12/2009 LCSD 28.8 96 0 (< 20 ) 30 ug/L 08/12/2009

Bromomethane LCS 39.2 131 ( 30-140 ) 30 ug/L 08/12/2009 LCSD 37.9 126 3 (< 20 ) 30 ug/L 08/12/2009

Bromochloromethane LCS 31.1 104 ( 77-129 ) 30 ug/L 08/12/2009 LCSD 30.0 100 4 (< 20 ) 30 ug/L 08/12/2009
Vinyl chloride LCS 38.9 130 ( 72-145 ) 30 ug/L 08/12/2009 LCSD 37.5 125 4 (< 20 ) 30 ug/L 08/12/2009

Dichlorodifluoromethane LCS 40.3 134 ( 62-153 ) 30 ug/L 08/12/2009 LCSD 38.9 130 4 (< 20 ) 30 ug/L 08/12/2009

Chloroethane LCS 38.1 127 ( 67-133 ) 30 ug/L 08/12/2009 LCSD 34.2 114 11 (< 20 ) 30 ug/L 08/12/2009
sec-Butylbenzene LCS 32.4 108 ( 80-120 ) 30 ug/L 08/12/2009 LCSD 31.5 105 3 (< 20 ) 30 ug/L 08/12/2009

Bromodichloromethane LCS 35.0 117 ( 80-120 ) 30 ug/L 08/12/2009 LCSD 33.8 113 4 (< 20 ) 30 ug/L 08/12/2009
1,1-Dichloroethene LCS 32.9 110 ( 76-130 ) 30 ug/L 08/12/2009 LCSD 31.8 106 4 (< 20 ) 30 ug/L 08/12/2009
2-Butanone (MEK) LCS 104 116 ( 66-136 ) 90 ug/L 08/12/2009 LCSD 96.4 107 8 (< 20 ) 90 ug/L 08/12/2009Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 915596 Lab Control Sample 915597 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19797 SW5030B 08/12/2009

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy 

### Methylene chloride LCS 32.9 110 ( 63-131 ) 30 ug/L 08/12/2009 LCSD 32.4 108 2 (< 20 ) 30 ug/L 08/12/2009

Trichlorofluoromethane LCS 40.5 135 ( 68-145 ) 30 ug/L 08/12/2009 LCSD 38.3 128 6 (< 20 ) 30 ug/L 08/12/2009
P & M -Xylene LCS 64.4 107 ( 80-120 ) 60 ug/L 08/12/2009 LCSD 62.5 104 3 (< 20 ) 60 ug/L 08/12/2009
Naphthalene LCS 26.4 88 ( 75-120 ) 30 ug/L 08/12/2009 LCSD 27.3 91 4 (< 20 ) 30 ug/L 08/12/2009
o-Xylene LCS 30.9 103 ( 80-120 ) 30 ug/L 08/12/2009 LCSD 30.3 101 2 (< 20 ) 30 ug/L 08/12/2009

Bromoform LCS 30.6 102 ( 80-120 ) 30 ug/L 08/12/2009 LCSD 30.9 103 1 (< 20 ) 30 ug/L 08/12/2009

1-Chlorohexane LCS 50.9 113 ( 70-125 ) 45 ug/L 08/12/2009 LCSD 47.8 106 6 (< 20 ) 45 ug/L 08/12/2009
1,2,4-Trimethylbenzene LCS 31.2 104 ( 80-125 ) 30 ug/L 08/12/2009 LCSD 30.5 102 2 (< 20 ) 30 ug/L 08/12/2009
tert-Butylbenzene LCS 31.3 104 ( 80-122 ) 30 ug/L 08/12/2009 LCSD 30.6 102 2 (< 20 ) 30 ug/L 08/12/2009
1,1,1-Trichloroethane LCS 33.3 111 ( 80-122 ) 30 ug/L 08/12/2009 LCSD 31.9 106 4 (< 20 ) 30 ug/L 08/12/2009
1,1-Dichloroethane LCS 33.1 110 ( 80-120 ) 30 ug/L 08/12/2009 LCSD 31.9 106 4 (< 20 ) 30 ug/L 08/12/2009

2-Chlorotoluene LCS 30.2 101 ( 80-125 ) 30 ug/L 08/12/2009 LCSD 29.8 100 1 (< 20 ) 30 ug/L 08/12/2009

Trichloroethene LCS 31.3 104 ( 80-125 ) 30 ug/L 08/12/2009 LCSD 29.8 100 5 (< 20 ) 30 ug/L 08/12/2009
trans-1,2-Dichloroethene LCS 31.6 105 ( 79-132 ) 30 ug/L 08/12/2009 LCSD 30.4 101 4 (< 20 ) 30 ug/L 08/12/2009Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 915596 Lab Control Sample 915597 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19797 SW5030B 08/12/2009

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### 1,2-Dichlorobenzene LCS 29.6 99 ( 80-120 ) 30 ug/L 08/12/2009 LCSD 29.0 97 2 (< 20 ) 30 ug/L 08/12/2009
2,2-Dichloropropane LCS 36.0 120 ( 80-132 ) 30 ug/L 08/12/2009 LCSD 33.7 112 7 (< 20 ) 30 ug/L 08/12/2009

Hexachlorobutadiene LCS 32.3 108 ( 77-125 ) 30 ug/L 08/12/2009 LCSD 31.9 106 1 (< 20 ) 30 ug/L 08/12/2009
Isopropylbenzene (Cumene) LCS 33.0 110 ( 80-121 ) 30 ug/L 08/12/2009 LCSD 31.7 106 4 (< 20 ) 30 ug/L 08/12/2009
1,2-Dichloropropane LCS 30.4 101 ( 80-121 ) 30 ug/L 08/12/2009 LCSD 29.7 99 2 (< 20 ) 30 ug/L 08/12/2009
1,1-Dichloropropene LCS 32.1 107 ( 80-122 ) 30 ug/L 08/12/2009 LCSD 30.5 102 5 (< 20 ) 30 ug/L 08/12/2009
1,1,2-Trichloroethane LCS 29.2 98 ( 77-120 ) 30 ug/L 08/12/2009 LCSD 28.8 96 2 (< 20 ) 30 ug/L 08/12/2009
1,3-Dichlorobenzene LCS 29.5 99 ( 80-120 ) 30 ug/L 08/12/2009 LCSD 29.4 98 1 (< 20 ) 30 ug/L 08/12/2009
1,2,3-Trichlorobenzene LCS 27.1 90 ( 77-120 ) 30 ug/L 08/12/2009 LCSD 27.5 92 1 (< 20 ) 30 ug/L 08/12/2009

Surrogates 

### 1,2-Dichloroethane-D4 <surr> LCS 106 ( 73-120 ) 08/12/2009 LCSD 104 2 08/12/2009

Toluene-d8 <surr> LCS 99 ( 80-120 ) 08/12/2009 LCSD 99 1 08/12/2009

4-Bromofluorobenzene <surr> LCS 96 ( 76-120 ) 08/12/2009 LCSD 98 2 08/12/2009Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 915596 Lab Control Sample 915597 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19797 SW5030B 08/12/2009

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy

Batch Method Instrument 

### VMS10724

SW8260B HP 5890 Series II MS3 VNAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 915947 Lab Control Sample 915948 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19810 SW5030B 08/13/2009

QC results affect the following production samples: 

### 1094021001

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass SpectroscopyMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 915947 Lab Control Sample 915948 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19810 SW5030B 08/13/2009

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy


### Benzene LCS 29.5 99 ( 80-120 ) 30 ug/L 08/13/2009 LCSD 28.4 95 4 (< 20 ) 30 ug/L 08/13/2009

Toluene LCS 30.9 103 ( 77-120 ) 30 ug/L 08/13/2009 LCSD 29.6 99 4 (< 20 ) 30 ug/L 08/13/2009
Ethylbenzene LCS 32.5 108 ( 80-120 ) 30 ug/L 08/13/2009 LCSD 31.0 103 5 (< 20 ) 30 ug/L 08/13/2009
n-Butylbenzene LCS 34.0 113 ( 80-124 ) 30 ug/L 08/13/2009 LCSD 32.3 108 5 (< 20 ) 30 ug/L 08/13/2009
1,4-Dichlorobenzene LCS 31.0 103 ( 80-120 ) 30 ug/L 08/13/2009 LCSD 29.3 98 6 (< 20 ) 30 ug/L 08/13/2009
1,2-Dichloroethane LCS 32.0 107 ( 80-129 ) 30 ug/L 08/13/2009 LCSD 31.8 106 1 (< 20 ) 30 ug/L 08/13/2009
1,3,5-Trimethylbenzene LCS 32.6 109 ( 80-128 ) 30 ug/L 08/13/2009 LCSD 31.4 105 4 (< 20 ) 30 ug/L 08/13/2009

4-Chlorotoluene LCS 31.3 104 ( 79-128 ) 30 ug/L 08/13/2009 LCSD 30.2 101 4 (< 20 ) 30 ug/L 08/13/2009

Chlorobenzene LCS 31.3 104 ( 80-120 ) 30 ug/L 08/13/2009 LCSD 30.2 101 3 (< 20 ) 30 ug/L 08/13/2009
4-Methyl-2-pentanone (MIBK) LCS 84.8 94 ( 69-134 ) 90 ug/L 08/13/2009 LCSD 78.1 87 8 (< 20 ) 90 ug/L 08/13/2009
cis-1,2-Dichloroethene LCS 30.7 102 ( 80-125 ) 30 ug/L 08/13/2009 LCSD 30.5 102 1 (< 20 ) 30 ug/L 08/13/2009
4-Isopropyltoluene LCS 33.7 112 ( 80-125 ) 30 ug/L 08/13/2009 LCSD 32.4 108 4 (< 20 ) 30 ug/L 08/13/2009
cis-1,3-Dichloropropene LCS 32.5 108 ( 80-120 ) 30 ug/L 08/13/2009 LCSD 32.7 109 1 (< 20 ) 30 ug/L 08/13/2009
n-Propylbenzene LCS 32.3 108 ( 80-129 ) 30 ug/L 08/13/2009 LCSD 31.1 104 4 (< 20 ) 30 ug/L 08/13/2009Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 915947 Lab Control Sample 915948 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19810 SW5030B 08/13/2009

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### Styrene LCS 33.3 111 ( 80-120 ) 30 ug/L 08/13/2009 LCSD 32.3 108 3 (< 20 ) 30 ug/L 08/13/2009

Dibromomethane LCS 30.3 101 ( 80-120 ) 30 ug/L 08/13/2009 LCSD 30.6 102 1 (< 20 ) 30 ug/L 08/13/2009
trans-1,3-Dichloropropene LCS 33.3 111 ( 80-124 ) 30 ug/L 08/13/2009 LCSD 32.9 110 1 (< 20 ) 30 ug/L 08/13/2009
1,2,4-Trichlorobenzene LCS 30.1 100 ( 80-120 ) 30 ug/L 08/13/2009 LCSD 28.3 94 6 (< 20 ) 30 ug/L 08/13/2009

Acetone LCS 90.6 101 ( 50-135 ) 90 ug/L 08/13/2009 LCSD 87.0 97 4 (< 20 ) 90 ug/L 08/13/2009
1,1,2,2-Tetrachloroethane LCS 30.4 101 ( 76-123 ) 30 ug/L 08/13/2009 LCSD 28.4 95 7 (< 20 ) 30 ug/L 08/13/2009
1,2-Dibromo-3-chloropropane LCS 29.1 97 ( 73-130 ) 30 ug/L 08/13/2009 LCSD 27.9 93 4 (< 20 ) 30 ug/L 08/13/2009
Methyl-t-butyl ether LCS 44.5 99 ( 80-120 ) 45 ug/L 08/13/2009 LCSD 43.3 96 3 (< 20 ) 45 ug/L 08/13/2009

Tetrachloroethene LCS 31.3 104 ( 79-122 ) 30 ug/L 08/13/2009 LCSD 30.2 101 4 (< 20 ) 30 ug/L 08/13/2009

Dibromochloromethane LCS 31.6 105 ( 80-120 ) 30 ug/L 08/13/2009 LCSD 30.8 103 3 (< 20 ) 30 ug/L 08/13/2009
1,3-Dichloropropane LCS 31.2 104 ( 80-121 ) 30 ug/L 08/13/2009 LCSD 30.6 102 2 (< 20 ) 30 ug/L 08/13/2009
1,2-Dibromoethane LCS 31.1 104 ( 80-120 ) 30 ug/L 08/13/2009 LCSD 30.6 102 2 (< 20 ) 30 ug/L 08/13/2009

Carbon tetrachloride LCS 34.4 115 ( 80-126 ) 30 ug/L 08/13/2009 LCSD 34.4 115 0 (< 20 ) 30 ug/L 08/13/2009
1,1,1,2-Tetrachloroethane LCS 30.0 100 ( 80-120 ) 30 ug/L 08/13/2009Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 915947 Lab Control Sample 915948 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19810 SW5030B 08/13/2009

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### LCSD 29.6 99 1 (< 20 ) 30 ug/L 08/13/2009

Chloroform LCS 33.2 111 ( 80-124 ) 30 ug/L 08/13/2009 LCSD 32.8 109 1 (< 20 ) 30 ug/L 08/13/2009

Bromobenzene LCS 29.5 98 ( 80-120 ) 30 ug/L 08/13/2009 LCSD 28.3 94 4 (< 20 ) 30 ug/L 08/13/2009

Chloromethane LCS 31.2 104 ( 67-125 ) 30 ug/L 08/13/2009 LCSD 27.8 93 11 (< 20 ) 30 ug/L 08/13/2009
1,2,3-Trichloropropane LCS 29.7 99 ( 80-120 ) 30 ug/L 08/13/2009 LCSD 28.0 93 6 (< 20 ) 30 ug/L 08/13/2009

Bromomethane LCS 38.8 129 ( 30-140 ) 30 ug/L 08/13/2009 LCSD 40.7 136 5 (< 20 ) 30 ug/L 08/13/2009

Bromochloromethane LCS 31.0 103 ( 77-129 ) 30 ug/L 08/13/2009 LCSD 30.2 101 3 (< 20 ) 30 ug/L 08/13/2009
Vinyl chloride LCS 32.9 110 ( 72-145 ) 30 ug/L 08/13/2009 LCSD 30.2 101 8 (< 20 ) 30 ug/L 08/13/2009

Dichlorodifluoromethane LCS 32.1 107 ( 62-153 ) 30 ug/L 08/13/2009 LCSD 30.2 101 6 (< 20 ) 30 ug/L 08/13/2009

Chloroethane LCS 34.5 115 ( 67-133 ) 30 ug/L 08/13/2009 LCSD 31.6 105 9 (< 20 ) 30 ug/L 08/13/2009
sec-Butylbenzene LCS 33.3 111 ( 80-120 ) 30 ug/L 08/13/2009 LCSD 32.0 107 4 (< 20 ) 30 ug/L 08/13/2009

Bromodichloromethane LCS 32.1 107 ( 80-120 ) 30 ug/L 08/13/2009 LCSD 32.6 109 2 (< 20 ) 30 ug/L 08/13/2009
1,1-Dichloroethene LCS 33.1 110 ( 76-130 ) 30 ug/L 08/13/2009 LCSD 32.4 108 2 (< 20 ) 30 ug/L 08/13/2009
2-Butanone (MEK) LCS 87.2 97 ( 66-136 ) 90 ug/L 08/13/2009 LCSD 89.6 100 3 (< 20 ) 90 ug/L 08/13/2009Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 915947 Lab Control Sample 915948 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19810 SW5030B 08/13/2009

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy 

### Methylene chloride LCS 31.3 104 ( 63-131 ) 30 ug/L 08/13/2009 LCSD 29.6 99 5 (< 20 ) 30 ug/L 08/13/2009

Trichlorofluoromethane LCS 35.6 119 ( 68-145 ) 30 ug/L 08/13/2009 LCSD 32.9 110 8 (< 20 ) 30 ug/L 08/13/2009
P & M -Xylene LCS 65.6 109 ( 80-120 ) 60 ug/L 08/13/2009 LCSD 63.7 106 3 (< 20 ) 60 ug/L 08/13/2009
Naphthalene LCS 28.5 95 ( 75-120 ) 30 ug/L 08/13/2009 LCSD 26.7 89 7 (< 20 ) 30 ug/L 08/13/2009
o-Xylene LCS 32.7 109 ( 80-120 ) 30 ug/L 08/13/2009 LCSD 31.7 106 3 (< 20 ) 30 ug/L 08/13/2009

Bromoform LCS 31.8 106 ( 80-120 ) 30 ug/L 08/13/2009 LCSD 31.2 104 2 (< 20 ) 30 ug/L 08/13/2009

1-Chlorohexane LCS 52.3 116 ( 70-125 ) 45 ug/L 08/13/2009 LCSD 49.7 110 5 (< 20 ) 45 ug/L 08/13/2009
1,2,4-Trimethylbenzene LCS 32.6 109 ( 80-125 ) 30 ug/L 08/13/2009 LCSD 31.0 103 5 (< 20 ) 30 ug/L 08/13/2009
tert-Butylbenzene LCS 32.7 109 ( 80-122 ) 30 ug/L 08/13/2009 LCSD 31.6 105 3 (< 20 ) 30 ug/L 08/13/2009
1,1,1-Trichloroethane LCS 33.7 112 ( 80-122 ) 30 ug/L 08/13/2009 LCSD 33.9 113 1 (< 20 ) 30 ug/L 08/13/2009
1,1-Dichloroethane LCS 34.9 116 ( 80-120 ) 30 ug/L 08/13/2009 LCSD 33.7 112 4 (< 20 ) 30 ug/L 08/13/2009

2-Chlorotoluene LCS 31.5 105 ( 80-125 ) 30 ug/L 08/13/2009 LCSD 30.0 100 5 (< 20 ) 30 ug/L 08/13/2009

Trichloroethene LCS 31.1 104 ( 80-125 ) 30 ug/L 08/13/2009 LCSD 30.4 101 2 (< 20 ) 30 ug/L 08/13/2009
trans-1,2-Dichloroethene LCS 31.9 106 ( 79-132 ) 30 ug/L 08/13/2009 LCSD 31.5 105 1 (< 20 ) 30 ug/L 08/13/2009Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 915947 Lab Control Sample 915948 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19810 SW5030B 08/13/2009

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### 1,2-Dichlorobenzene LCS 30.3 101 ( 80-120 ) 30 ug/L 08/13/2009 LCSD 29.0 97 5 (< 20 ) 30 ug/L 08/13/2009
2,2-Dichloropropane LCS 33.0 110 ( 80-132 ) 30 ug/L 08/13/2009 LCSD 33.3 111 1 (< 20 ) 30 ug/L 08/13/2009

Hexachlorobutadiene LCS 31.3 104 ( 77-125 ) 30 ug/L 08/13/2009 LCSD 30.5 102 3 (< 20 ) 30 ug/L 08/13/2009
Isopropylbenzene (Cumene) LCS 34.5 115 ( 80-121 ) 30 ug/L 08/13/2009 LCSD 33.2 111 4 (< 20 ) 30 ug/L 08/13/2009
1,2-Dichloropropane LCS 31.0 103 ( 80-121 ) 30 ug/L 08/13/2009 LCSD 30.0 100 3 (< 20 ) 30 ug/L 08/13/2009
1,1-Dichloropropene LCS 37.7 126 ( 80-122 ) * 30 ug/L 08/13/2009 LCSD 37.0 123 * 2 (< 20 ) 30 ug/L 08/13/2009
1,1,2-Trichloroethane LCS 31.5 105 ( 77-120 ) 30 ug/L 08/13/2009 LCSD 30.6 102 3 (< 20 ) 30 ug/L 08/13/2009
1,3-Dichlorobenzene LCS 30.4 101 ( 80-120 ) 30 ug/L 08/13/2009 LCSD 29.2 97 4 (< 20 ) 30 ug/L 08/13/2009
1,2,3-Trichlorobenzene LCS 29.2 97 ( 77-120 ) 30 ug/L 08/13/2009 LCSD 27.8 93 5 (< 20 ) 30 ug/L 08/13/2009

Surrogates 

### 1,2-Dichloroethane-D4 <surr> LCS 103 ( 73-120 ) 08/13/2009 LCSD 108 5 08/13/2009

Toluene-d8 <surr> LCS 100 ( 80-120 ) 08/13/2009 LCSD 101 1 08/13/2009

4-Bromofluorobenzene <surr> LCS 98 ( 76-120 ) 08/13/2009 LCSD 98 1 08/13/2009Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 915947 Lab Control Sample 915948 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19810 SW5030B 08/13/2009

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy

Batch Method Instrument 

### VMS10730

SW8260B HP 5890 Series II MS3 VNAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 916339 Lab Control Sample 916340 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19816 SW5030B 08/14/2009

QC results affect the following production samples: 

### 1094021006

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy


### Acetone LCS 104 116 ( 50-135 ) 90 ug/L 08/14/2009 LCSD 97.6 108 7 (< 20 ) 90 ug/L 08/14/2009
2-Butanone (MEK) LCS 84.6 94 ( 66-136 ) 90 ug/L 08/14/2009 LCSD 81.8 91 3 (< 20 ) 90 ug/L 08/14/2009

Surrogates 

### 1,2-Dichloroethane-D4 <surr> LCS 106 ( 73-120 ) 08/14/2009 LCSD 103 2 08/14/2009

Toluene-d8 <surr> LCS 99 ( 80-120 ) 08/14/2009 LCSD 99 0 08/14/2009

4-Bromofluorobenzene <surr> LCS 94 ( 76-120 ) 08/14/2009 LCSD 95 1 08/14/2009

Batch Method Instrument 

### VMS10736

SW8260B HP 5890 Series II MS3 VNAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Prep 

### 917245 Lab Control Sample 917246 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19837 SW5030B 08/14/2009

QC results affect the following production samples: 

### 1094021001, 1094021004, 1094021005, 1094021006

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Fuels Department 

### Gasoline Range Organics LCS 197 98 ( 79-108 ) 200 ug/L 08/14/2009 LCSD 193 96 2 (< 20 ) 200 ug/L 08/14/2009

Surrogates 

### 4-Bromofluorobenzene <surr> LCS 96 ( 50-150 ) 08/14/2009 LCSD 97 2 08/14/2009

Batch Method Instrument 

### VFC9606

SW8015C HP 5890 Series II PID+HECD VBAMatrix SGS Ref.# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Original Prep 

### 1094021002 Billable Matrix Spike 1094021003 Billable Matrix Spike Dup.

1094021001 Water (Surface, Eff., Ground) MXX22033 3010 H20 Digest for Metals ICP-MS 08/12/2009

QC results affect the following production samples:

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Dissolved Metals by ICP/MS


### Lead BMS ND 999 100 ( 80-120 ) 1000 ug/L 08/18/2009 BMSD 989 99 1 (< 15 ) 1000 ug/L 08/18/2009
Batch Method Instrument 

### MMS6032

SW6020 Perkin Elmer Sciex ICP-MS P3

Volatile Fuels Department 

### Gasoline Range Organics BMS ND 432 96 ( 79-108 ) 450 ug/L 08/14/2009 BMSD 455 101 5 (< 20 ) 450 ug/L 08/14/2009 Surrogates 

### 4-Bromofluorobenzene <surr> BMS 50.8 102 ( 50-150 ) 08/14/2009 BMSD 50.4 101 1 08/14/2009
Batch Method Instrument 

### VFC9606

SW8015C HP 5890 Series II PID+HECD VBA

Semivolatile Organic Fuels Department 

### Diesel Range Organics BMS ND 4.82 81 ( 75-125 ) 5.99 mg/L 08/08/2009 BMSD 4.89 82 1 (< 30 ) 5.99 mg/L 08/08/2009 Surrogates 

### 5a Androstane <surr> BMS .1 84 ( 50-150 ) 08/08/2009 BMSD 0.103 86 3 08/08/2009
Batch Method Instrument 

### XFC8762

SW8015C HP 6890 Series II FID SV D R

Volatile Gas Chromatography/Mass SpectroscopyMatrix SGS Ref.# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Original Prep 

### 1094021002 Billable Matrix Spike 1094021003 Billable Matrix Spike Dup.

1094021001 Water (Surface, Eff., Ground) VXX19810 Volatiles Extraction AFCEE 3.1 8260 (W) 08/13/2009

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy


### Benzene BMS 0.470 29.2 96 ( 80-120 ) 30.0 ug/L 08/13/2009 BMSD 28.3 93 3 (< 20 ) 30.0 ug/L 08/13/2009 Toluene BMS ND 29.8 99 ( 77-120 ) 30.0 ug/L 08/13/2009 BMSD 28.9 96 3 (< 20 ) 30.0 ug/L 08/13/2009 Ethylbenzene BMS ND 31.3 104 ( 80-120 ) 30.0 ug/L 08/13/2009 BMSD 30.3 101 3 (< 20 ) 30.0 ug/L 08/13/2009 n-Butylbenzene BMS ND 33.3 111 ( 80-124 ) 30.0 ug/L 08/13/2009 BMSD 32.7 109 2 (< 20 ) 30.0 ug/L 08/13/2009 1,4-Dichlorobenzene BMS ND 29.7 99 ( 80-120 ) 30.0 ug/L 08/13/2009 BMSD 29.5 98 1 (< 20 ) 30.0 ug/L 08/13/2009 1,2-Dichloroethane BMS ND 32.5 108 ( 80-129 ) 30.0 ug/L 08/13/2009 BMSD 31.9 106 2 (< 20 ) 30.0 ug/L 08/13/2009 1,3,5-Trimethylbenzene BMS ND 31.6 105 ( 80-128 ) 30.0 ug/L 08/13/2009 BMSD 30.6 102 3 (< 20 ) 30.0 ug/L 08/13/2009 4-Chlorotoluene BMS ND 30.5 102 ( 79-128 ) 30.0 ug/L 08/13/2009 BMSD 29.8 99 3 (< 20 ) 30.0 ug/L 08/13/2009 Chlorobenzene BMS ND 30.1 100 ( 80-120 ) 30.0 ug/L 08/13/2009 BMSD 29.6 99 2 (< 20 ) 30.0 ug/L 08/13/2009 4-Methyl-2-pentanone (MIBK) BMS ND 84.3 94 ( 69-134 ) 90.0 ug/L 08/13/2009 BMSD 85.4 95 1 (< 20 ) 90.0 ug/L 08/13/2009 cis-1,2-Dichloroethene BMS ND 30.7 102 ( 80-125 ) 30.0 ug/L 08/13/2009 BMSD 30.0 100 2 (< 20 ) 30.0 ug/L 08/13/2009 4-Isopropyltoluene BMS ND 32.8 109 ( 80-125 ) 30.0 ug/L 08/13/2009 BMSD 32.1 107 2 (< 20 ) 30.0 ug/L 08/13/2009 cis-1,3-Dichloropropene BMS ND 32.7 109 ( 80-120 ) 30.0 ug/L 08/13/2009 BMSD 32.3 108 1 (< 20 ) 30.0 ug/L 08/13/2009 n-Propylbenzene BMS ND 32 107 ( 80-129 ) 30.0 ug/L 08/13/2009 BMSD 31.0 103 3 (< 20 ) 30.0 ug/L 08/13/2009 Styrene BMS ND 28.3 94 ( 80-120 ) 30.0 ug/L 08/13/2009 BMSD 26.9 90 5 (< 20 ) 30.0 ug/L 08/13/2009 Dibromomethane BMS ND 31.5 105 ( 80-120 ) 30.0 ug/L 08/13/2009 BMSD 31.6 105 0 (< 20 ) 30.0 ug/L 08/13/2009 trans-1,3-Dichloropropene BMS ND 32.6 109 ( 80-124 ) 30.0 ug/L 08/13/2009 BMSD 32.4 108 1 (< 20 ) 30.0 ug/L 08/13/2009 1,2,4-Trichlorobenzene BMS ND 29.6 99 ( 80-120 ) 30.0 ug/L 08/13/2009 BMSD 28.7 96 3 (< 20 ) 30.0 ug/L 08/13/2009 Acetone BMS ND 91 101 ( 50-135 ) 90.0 ug/L 08/13/2009 BMSD 90.0 100 1 (< 20 ) 90.0 ug/L 08/13/2009 1,1,2,2-Tetrachloroethane BMS ND 29.7 99 ( 76-123 ) 30.0 ug/L 08/13/2009 BMSD 29.6 99 0 (< 20 ) 30.0 ug/L 08/13/2009Matrix SGS Ref.# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Original Prep 

### 1094021002 Billable Matrix Spike 1094021003 Billable Matrix Spike Dup.

1094021001 Water (Surface, Eff., Ground) VXX19810 Volatiles Extraction AFCEE 3.1 8260 (W) 08/13/2009

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy 

### 1,2-Dibromo-3-chloropropane BMS ND 29 97 ( 73-130 ) 30.0 ug/L 08/13/2009 BMSD 28.4 95 2 (< 20 ) 30.0 ug/L 08/13/2009 Methyl-t-butyl ether BMS ND 45 100 ( 80-120 ) 45.0 ug/L 08/13/2009 BMSD 44.4 99 1 (< 20 ) 45.0 ug/L 08/13/2009 Tetrachloroethene BMS ND 30 100 ( 79-122 ) 30.0 ug/L 08/13/2009 BMSD 29.4 98 2 (< 20 ) 30.0 ug/L 08/13/2009 Dibromochloromethane BMS ND 31.4 105 ( 80-120 ) 30.0 ug/L 08/13/2009 BMSD 30.7 102 2 (< 20 ) 30.0 ug/L 08/13/2009 1,3-Dichloropropane BMS ND 30.7 102 ( 80-121 ) 30.0 ug/L 08/13/2009 BMSD 29.6 99 4 (< 20 ) 30.0 ug/L 08/13/2009 1,2-Dibromoethane BMS ND 30.7 102 ( 80-120 ) 30.0 ug/L 08/13/2009 BMSD 30.2 101 2 (< 20 ) 30.0 ug/L 08/13/2009 Carbon tetrachloride BMS ND 35.8 119 ( 80-126 ) 30.0 ug/L 08/13/2009 BMSD 34.4 115 4 (< 20 ) 30.0 ug/L 08/13/2009 1,1,1,2-Tetrachloroethane BMS ND 29.3 98 ( 80-120 ) 30.0 ug/L 08/13/2009 BMSD 29.2 97 0 (< 20 ) 30.0 ug/L 08/13/2009 Chloroform BMS ND 33.2 111 ( 80-124 ) 30.0 ug/L 08/13/2009 BMSD 32.8 109 1 (< 20 ) 30.0 ug/L 08/13/2009 Bromobenzene BMS ND 28.9 96 ( 80-120 ) 30.0 ug/L 08/13/2009 BMSD 28.3 94 2 (< 20 ) 30.0 ug/L 08/13/2009 Chloromethane BMS ND 28.7 96 ( 67-125 ) 30.0 ug/L 08/13/2009 BMSD 28.4 95 1 (< 20 ) 30.0 ug/L 08/13/2009 1,2,3-Trichloropropane BMS ND 29.8 99 ( 80-120 ) 30.0 ug/L 08/13/2009 BMSD 28.8 96 4 (< 20 ) 30.0 ug/L 08/13/2009 Bromomethane BMS ND 44.2 147 * ( 30-140 ) 30.0 ug/L 08/13/2009 BMSD 45.9 153 * 4 (< 20 ) 30.0 ug/L 08/13/2009 Bromochloromethane BMS ND 30.8 103 ( 77-129 ) 30.0 ug/L 08/13/2009 BMSD 30.1 100 3 (< 20 ) 30.0 ug/L 08/13/2009 Vinyl chloride BMS ND 30.6 102 ( 72-145 ) 30.0 ug/L 08/13/2009 BMSD 29.9 100 2 (< 20 ) 30.0 ug/L 08/13/2009 Dichlorodifluoromethane BMS ND 31.7 106 ( 62-153 ) 30.0 ug/L 08/13/2009 BMSD 30.2 101 5 (< 20 ) 30.0 ug/L 08/13/2009 Chloroethane BMS ND 46.1 154 * ( 67-133 ) 30.0 ug/L 08/13/2009 BMSD 44.5 148 * 4 (< 20 ) 30.0 ug/L 08/13/2009 sec-Butylbenzene BMS ND 32.4 108 ( 80-120 ) 30.0 ug/L 08/13/2009 BMSD 31.8 106 2 (< 20 ) 30.0 ug/L 08/13/2009 Bromodichloromethane BMS ND 33.3 111 ( 80-120 ) 30.0 ug/L 08/13/2009 BMSD 32.6 109 2 (< 20 ) 30.0 ug/L 08/13/2009 1,1-Dichloroethene BMS ND 31.6 105 ( 76-130 ) 30.0 ug/L 08/13/2009 BMSD 31.2 104 1 (< 20 ) 30.0 ug/L 08/13/2009Matrix SGS Ref.# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Original Prep 

### 1094021002 Billable Matrix Spike 1094021003 Billable Matrix Spike Dup.

1094021001 Water (Surface, Eff., Ground) VXX19810 Volatiles Extraction AFCEE 3.1 8260 (W) 08/13/2009

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy 

### 2-Butanone (MEK) BMS ND 94.1 105 ( 66-136 ) 90.0 ug/L 08/13/2009 BMSD 93.9 104 0 (< 20 ) 90.0 ug/L 08/13/2009 Methylene chloride BMS ND 29.6 99 ( 63-131 ) 30.0 ug/L 08/13/2009 BMSD 28.8 96 3 (< 20 ) 30.0 ug/L 08/13/2009 Trichlorofluoromethane BMS ND 36.7 122 ( 68-145 ) 30.0 ug/L 08/13/2009 BMSD 35.8 119 3 (< 20 ) 30.0 ug/L 08/13/2009 P & M -Xylene BMS ND 62.8 105 ( 80-120 ) 60.0 ug/L 08/13/2009 BMSD 61.7 103 2 (< 20 ) 60.0 ug/L 08/13/2009 Naphthalene BMS ND 28.6 95 ( 75-120 ) 30.0 ug/L 08/13/2009 BMSD 27.9 93 2 (< 20 ) 30.0 ug/L 08/13/2009 o-Xylene BMS ND 31.5 105 ( 80-120 ) 30.0 ug/L 08/13/2009 BMSD 30.7 102 3 (< 20 ) 30.0 ug/L 08/13/2009 Bromoform BMS ND 32 107 ( 80-120 ) 30.0 ug/L 08/13/2009 BMSD 31.5 105 1 (< 20 ) 30.0 ug/L 08/13/2009 1-Chlorohexane BMS ND 50.7 113 ( 70-125 ) 45.0 ug/L 08/13/2009 BMSD 48.2 107 5 (< 20 ) 45.0 ug/L 08/13/2009 1,2,4-Trimethylbenzene BMS ND 31.3 104 ( 80-125 ) 30.0 ug/L 08/13/2009 BMSD 30.5 102 3 (< 20 ) 30.0 ug/L 08/13/2009 tert-Butylbenzene BMS ND 32.2 107 ( 80-122 ) 30.0 ug/L 08/13/2009 BMSD 31.3 104 3 (< 20 ) 30.0 ug/L 08/13/2009 1,1,1-Trichloroethane BMS ND 34.8 116 ( 80-122 ) 30.0 ug/L 08/13/2009 BMSD 34.0 113 3 (< 20 ) 30.0 ug/L 08/13/2009 1,1-Dichloroethane BMS ND 34.1 114 ( 80-120 ) 30.0 ug/L 08/13/2009 BMSD 32.9 110 3 (< 20 ) 30.0 ug/L 08/13/2009 2-Chlorotoluene BMS ND 30.6 102 ( 80-125 ) 30.0 ug/L 08/13/2009 BMSD 29.8 99 3 (< 20 ) 30.0 ug/L 08/13/2009 Trichloroethene BMS ND 31.1 104 ( 80-125 ) 30.0 ug/L 08/13/2009 BMSD 30.0 100 4 (< 20 ) 30.0 ug/L 08/13/2009 trans-1,2-Dichloroethene BMS ND 32.2 107 ( 79-132 ) 30.0 ug/L 08/13/2009 BMSD 31.4 105 3 (< 20 ) 30.0 ug/L 08/13/2009 1,2-Dichlorobenzene BMS ND 29.1 97 ( 80-120 ) 30.0 ug/L 08/13/2009 BMSD 28.6 95 2 (< 20 ) 30.0 ug/L 08/13/2009 2,2-Dichloropropane BMS ND 35.3 118 ( 80-132 ) 30.0 ug/L 08/13/2009 BMSD 34.0 113 4 (< 20 ) 30.0 ug/L 08/13/2009 Hexachlorobutadiene BMS ND 31.1 104 ( 77-125 ) 30.0 ug/L 08/13/2009 BMSD 30.8 103 1 (< 20 ) 30.0 ug/L 08/13/2009 Isopropylbenzene (Cumene) BMS ND 33.4 111 ( 80-121 ) 30.0 ug/L 08/13/2009 BMSD 32.5 108 3 (< 20 ) 30.0 ug/L 08/13/2009 1,2-Dichloropropane BMS ND 30.5 102 ( 80-121 ) 30.0 ug/L 08/13/2009 BMSD 29.7 99 3 (< 20 ) 30.0 ug/L 08/13/2009Matrix SGS Ref.# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Original Prep 

### 1094021002 Billable Matrix Spike 1094021003 Billable Matrix Spike Dup.

1094021001 Water (Surface, Eff., Ground) VXX19810 Volatiles Extraction AFCEE 3.1 8260 (W) 08/13/2009

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy 

### 1,1-Dichloropropene BMS ND 32.5 108 ( 80-122 ) 30.0 ug/L 08/13/2009 BMSD 32.1 107 1 (< 20 ) 30.0 ug/L 08/13/2009 1,1,2-Trichloroethane BMS ND 30.7 102 ( 77-120 ) 30.0 ug/L 08/13/2009 BMSD 30.2 101 1 (< 20 ) 30.0 ug/L 08/13/2009 1,3-Dichlorobenzene BMS ND 29.4 98 ( 80-120 ) 30.0 ug/L 08/13/2009 BMSD 28.9 96 2 (< 20 ) 30.0 ug/L 08/13/2009 1,2,3-Trichlorobenzene BMS ND 29 97 ( 77-120 ) 30.0 ug/L 08/13/2009 BMSD 29.1 97 0 (< 20 ) 30.0 ug/L 08/13/2009 Surrogates 

### 1,2-Dichloroethane-D4 <surr> BMS 33.3 111 ( 73-120 ) 08/13/2009 BMSD 34.2 114 3 08/13/2009 Toluene-d8 <surr> BMS 29.5 98 ( 80-120 ) 08/13/2009 BMSD 29.7 99 1 08/13/2009 4-Bromofluorobenzene <surr> BMS 29.6 99 ( 76-120 ) 08/13/2009 BMSD 29.1 97 2 08/13/2009
Batch Method Instrument 

### VMS10730

SW8260B HP 5890 Series II MS3 VNA

Polynuclear Aromatics GC/MSMatrix SGS Ref.# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Original Prep 

### 1094021002 Billable Matrix Spike 1094021003 Billable Matrix Spike Dup.

1094021001 Water (Surface, Eff., Ground) XXX21374 3520 Liquid/Liquid Ext for 8270 SIM 08/07/2009

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Polynuclear Aromatics GC/MS 

### Acenaphthylene BMS ND .539 92 ( 50-105 ) 0.585 ug/L 08/12/2009 BMSD 0.541 96 0 (< 30 ) 0.565 ug/L 08/12/2009 Acenaphthene BMS ND .497 85 ( 45-110 ) 0.585 ug/L 08/12/2009 BMSD 0.487 86 2 (< 30 ) 0.565 ug/L 08/12/2009 Fluorene BMS ND .539 92 ( 50-110 ) 0.585 ug/L 08/12/2009 BMSD 0.532 94 1 (< 30 ) 0.565 ug/L 08/12/2009 Phenanthrene BMS ND .544 93 ( 50-115 ) 0.585 ug/L 08/12/2009 BMSD 0.549 97 1 (< 30 ) 0.565 ug/L 08/12/2009 Anthracene BMS ND .596 102 ( 55-110 ) 0.585 ug/L 08/12/2009 BMSD 0.583 103 2 (< 30 ) 0.565 ug/L 08/12/2009 Fluoranthene BMS ND .603 103 ( 55-125 ) 0.585 ug/L 08/12/2009 BMSD 0.589 104 2 (< 30 ) 0.565 ug/L 08/12/2009 Pyrene BMS ND .58 99 ( 50-130 ) 0.585 ug/L 08/12/2009 BMSD 0.562 100 3 (< 30 ) 0.565 ug/L 08/12/2009 Benzo(a)Anthracene BMS ND .649 111 ( 55-120 ) 0.585 ug/L 08/12/2009 BMSD 0.609 108 6 (< 30 ) 0.565 ug/L 08/12/2009 Chrysene BMS ND .587 100 ( 55-120 ) 0.585 ug/L 08/12/2009 BMSD 0.545 97 8 (< 30 ) 0.565 ug/L 08/12/2009 Benzo[b]Fluoranthene BMS ND .63 108 ( 46-130 ) 0.585 ug/L 08/12/2009 BMSD 0.596 105 6 (< 30 ) 0.565 ug/L 08/12/2009 Benzo[k]fluoranthene BMS ND .605 103 ( 60-125 ) 0.585 ug/L 08/12/2009 BMSD 0.608 108 1 (< 30 ) 0.565 ug/L 08/12/2009 Benzo[a]pyrene BMS ND .64 109 ( 55-120 ) 0.585 ug/L 08/12/2009 BMSD 0.638 113 0 (< 30 ) 0.565 ug/L 08/12/2009 Indeno[1,2,3-c,d] pyrene BMS ND .591 101 ( 45-125 ) 0.585 ug/L 08/12/2009 BMSD 0.584 103 1 (< 30 ) 0.565 ug/L 08/12/2009 Dibenzo[a,h]anthracene BMS ND .6 103 ( 41-140 ) 0.585 ug/L 08/12/2009 BMSD 0.605 107 1 (< 30 ) 0.565 ug/L 08/12/2009 Benzo[g,h,i]perylene BMS ND .598 102 ( 46-125 ) 0.585 ug/L 08/12/2009 BMSD 0.604 107 1 (< 30 ) 0.565 ug/L 08/12/2009 Naphthalene BMS ND .494 84 ( 42-100 ) 0.585 ug/L 08/12/2009 BMSD 0.472 84 5 (< 30 ) 0.565 ug/L 08/12/2009 1-Methylnaphthalene BMS ND .492 84 ( 46-115 ) 0.585 ug/L 08/12/2009 BMSD 0.486 86 1 (< 30 ) 0.565 ug/L 08/12/2009 2-Methylnaphthalene BMS ND .459 78 ( 45-105 ) 0.585 ug/L 08/12/2009 BMSD 0.462 82 1 (< 30 ) 0.565 ug/L 08/12/2009 Surrogates 

### Terphenyl-d14 <surr> BMS .596 102 ( 50-135 ) 08/12/2009 BMSD 0.568 101 5 08/12/2009Matrix SGS Ref.# Printed Date/Time 

### 08/20/2009 13:51 Batch Method Date Original Prep 

### 1094021002 Billable Matrix Spike 1094021003 Billable Matrix Spike Dup.

1094021001 Water (Surface, Eff., Ground) XXX21374 3520 Liquid/Liquid Ext for 8270 SIM 08/07/2009

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Polynuclear Aromatics GC/MS

Batch Method Instrument 

### XMS5029

8270D SIMS HP 6890/5973 MS SVQA