**2~M-BWM0347** Rev. 1/2011 **tr~~~!!_** COMMONWEALTH

OF PENNSYLVANIA DEPARTMENT OF ENVIRONMENTAL PROTECTION BUREAU OF WASTE MANAGEMENT FORM26R CHEMICAL ANALYSIS OF RESIDUAL WASTE ANNUAL REPORT BY THE GENERA TOR be typed or legibly printed In the spaces provided. If additional space is necessary, Identify each atlached sheet as Fonn 26R, reference the Hem number and Identify the date prepared. The date on attached sheets needs to match the date noted below. 287.54 County c.

- 1 -2540.PM-BWM0347 Rev. 112011 of the the waste, as specified In the Instructions,
Is attached. b. A of the manufacturing as specified In the Instructions,
Is attached. c. If portions of the lnfonnation are the substantiation a confidentiality claim, as described In the Instructions,
Is attached. Address Line 1 Address Une 1 Address City State ZIP Municipality c. Facility Contact Name nue a. b. Address Une 1 Address Line 1 Address City State ZIP Municipality c. Facility Contact Name Title Phone d. waste
Email Address to processing or (check one) year. 0 cuyd D gal D lb D ton (check one) a. If "Yes" list the general penn it number or **~n•~rn\121** number. Volume of waste

0 ton (check one) -2-

No254Q.PM-BWM0347 Rev: 112011 I certify, under penalty of law, that

I have personally examined and am familiar with the lnfonnation submitted In this Annual Report and all attached documents and that based upon my Inquiry of those Individuals Immediately responsible for obtaining the Information,

I verify that the submitted Information Is true, accurate and complete to the best of my knowledge.

I understand that the submission of false Information herein is made subject to the penalties of 18 Pa. C.S. §4904, relating to unsworn falsification to authOrities, which Include fine and Imprisonment

.

· Check the following, If applicable: D

I certify the Information required in Section B-1, General Properties was supplied to the Department for the year _and has not changed. Form Submitted:

0 Form 26R 0 Other (specify) Date Submitted: D

I certify the Information required In Section B-2, Chemical Analysis was supplied to the Department for the year _and has not changed. Form Submitted:

0 Form 26R 0 Other (specify) Date Submitted: D

I certify the Information required In Section B-3, Process Description and Schematic, was supplied to the Department for the year_ and has not changed. Form Submitted:

0 Form 26R 0 Other (specify) Date Submitted: Name of Responsible Official Bernhardt Kissel Signature

Date 2-28-11February 8, 2011 Form 26R: Section B2b WASTE SAMPLING METHODS

I• All samples were obtained as grab type samples with a composite function which was maximized but sometimes limited by prevailing safety, site specific rational and/or environmental concerns. Brine fluids are composited within the storage production tank or tank battery at each well site where gas production is occurring. Each automatic or manual ejection of formation fluids is deposited into the tank(s) and added to the previously ejected and stored quantity

. Tanks are emptied into tank trucks for disposal at various PaDEP permitted waste disposal facilities on different schedules detennined by individual well characteristics. Grab samples of the composited fluids were obtained at the represented well pads directly from the storage tank drain ports. All drain ports had small "built in" containment and storage "buckets" capable of retaining small amounts of lost fluids. **Sa~ples**were obtained with bottle sets prepared at the laboratory which contained appropriate preservatives, as necessary, depending on the specific test run requested. All chain of custody and handling/holding time requirements were met. In some cases, a larger sample was broken into appropriate sampling containers and smaller aliquot portions at the laboratory. Flowback samples were composited to the extent possible during the flowback process primarily during times where safety issues did not override sample collection requirements. Generally,
a larger composite sample was broken into appropriate sampling containers and smaller aliquot portions at the laboratory or on the well location upon completion of the composite sampling process

. Samples were distributed into bottle sets prepared at the laboratory which contained appropriate preservatives, as necessary, depending on the specific test run requested. All chain of custody and handling/holding time requirements were met. Drill cuttings were composite sampled during the drilling process at various times and combined into a composite sample for analyses at the laboratory. On several wells, cuttings from the vertical portion of the well bore were segregated from cuttings from the target Marcellus Fonnation and separate testing was completed on both sample composites.
In some earlier cases during the utilization of open pits, composite samples were obtained from inactive drill pits. Safety concerns usually limited the randomness of the composite sample and composite grid sample positions were varied to the extent possible. Pit water (drill fluid) is currently discharged to closed containment and is re-conditioned and reused from well to well.I • February 9, 2011 Form 26R: Section B3a WASTE GENERATION PROCESS Pit Water "Drill Fluids" Remnant drill fluids are generated
in the well bore during the penetration of the drill stem as it intercepts both ground water and formation fluids. These fluids are brought to the surface along with the drill cuttings, pieces of the intercepted rock strata, by the return flow system of the drilling process. Drill cuttings and drill fluids are isolated into separate waste streams. Cuttings are mixed with sawdust to absorb remnant fluid and loaded out for disposal at a landfill. Fluids are currently stored in closed containers to be processed for reuse. Flowback: "Fracing Fluid" Flowback is produced from all fluids that flow back to surface during the "hydrofracing" process which occurs under pressure and results in the setting of a propant within the formation fractures. Production Fluid "Brine" During the production of natural gas, fonnation pressures bring remnant frac fluids, during the initial production phase, and formation fluids to the surface along with produced gas.WellI.D.#(various)WellI.D.#(various) ,,/ ,\/ -0.- -0- /·' /l' COUNTYA I\ I \/WellI.D.#(various) \I::b/ \I /II' \I/ \I// \I// .\I/ WellI.D.#(various)\1// '\// \I/ -0-/'\.. r----

-COUNTYB/**~o~--**(.**~** (Y"/**Fl"'"'~o..l ~7** **~oVd~** MobileTankTruck

**~t-o~vc..-\ro~t Ocu"tt\~~~**  \""ks::( **J~**Sbrine(TYP.) Note:. Processproducingwaste:Gaswellproduced fluids(brines)aretypicallyproducedin conjuctionwi.thnaturalgas.Thesefluids arebroughttothesurfaceutilizingeither .mechanicalorphysicalliftprocedures.
--------Landfill orTr!U.+M.U\f'PlCAAt

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.i**~~ ~** **~ ~** u·GEOCHEMICAL TESTING Environmental and Energy Analysis Wednesday, February 23, 2011 RICK BONAZZA RESOURCE MANAGEMENT SERVICES 65 FENTON ROAD INDIANA, PA 15701 RE: 26R Analysis Dear RICK BONAZZA: OrderNo.: 01101912 Geochemical Testing received
1 sample(s) on 1128/2011 for the analyses presented in the following report. There were no problems with the analyses and all QC data met NELAC, EPA, and laboratory specifications except where noted in the Case Narrative or Laboratory Results. If you have any questions regarding these tests results, please feel free to call. Sincerely, Timothy W. Bergstresser Director of Technical Services Page 1 of 7 2005 N Center Ave Somerset PA 15501 814/443-1671 814/445-6666 FAX: 814/445-6729Geochemical Testin2:

Date: 23-Feb-11 CLIENT: Project: Lab Order: RESOURCE MANAGEMENT SERVICES 26R Analysis Gll01912CASE NARRATIVE No problems were encountered during analysis of this workorder, except if noted in this report. The ethylene gycol analysis was subcontracted
to Free Col Labs. A copy of the subcontractor's laboratory report is enclosed with this Analytical Report. The radiological analysis was subcontracted
to Pace Analytical. A copy of the subcontractor's laboratory report is enclosed with this Analytical Report. Legend: ND- Not Detected at the Quantitation Limit J - Indicates an estimated value

.

·- ---
-----
·--·· ----------- .. - . --·- **-··-·- S-** **spik~ Recovery** outside accepted recovery limits U - The ana\yte was not detected at or above the I isted concentration, which is below the laboratory quantitation limit. B - Analyte detected in the associated Method Blank Q - Qualifier QL -Quantitation Limit DF- Dilution Factor R - RPD outside accepted recovery

l i mits E- Value above quantitation range **-Value exceeds Action Limit H - Method Hold Time Exceeded MCL- Contaminant Limit Page 2 of 7

\.D . 56-00306 PA DEPLaboratory Results Geochemical Testing

Date: 23-Feb-11 **-~- -·** **-·** -- ···--· - ----- · ''

. .

- -·· .. -- -. --- ... · ·· -·-·.-.

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o
o o CLIENT: Lab Order: RESOURCE MANAGEMENT SERVICES 01101912
Client Sample ID: Eckles Well 8590H FB RMS 111/28 Project: 26R Analysis Lab ID: 01101912-001 Matrix: AQUEOUS Analyses Result INORGANIC NON-METALS Acidity to pH 8 . 2

-38 INORGANIC NON-METALS Alkalinity to pH 4.5

150 PHYSICAL TESTS Specific Conductance 111000 PH BY SM 4500 H+B Lab pH

6 . 52 INORGANIC NON-METALS Total dissolved solids 97500 PHYSICAL TESTS Total suspended solids
545 INDICATOR ORGANIC PARAMETERS BOD 5-day
1350 Finish DatefTime 21212011 18

: 10 REACTIVE CYANIDE Reactive cyanide INDICATOR ORGANIC PARAMETERS Chemical Oxygen Demand INORGANIC NON-METALS Bromide Chloride Sulfate INORGANIC NON-METALS MBAS INORGANIC NON-METALS Ammonia Nitrogen

- Distilled INORGANIC NON-METALS N
i trate
- Nitrite INDICATOR ORGANIC PARAMETERS Phenolics REACTIVE SULFIDE Reactive sulfide INORGANIC NON-METALS

<0

. 25 5800 461 57100 < 100 < 0 . 25 69

. 1 0 . 53 < 100 0 . 50 Sampled By: Client Collection Date: 1/28/2011 1:10:00 PM Received Date: 1/28/2011
7 : 08:50 PM QL Q Units SM

· 23108(4A) 0 mgfLCaC03 SM 18 23208 5 mgfLCaC03 EPA 120.1 1Jmhos/cm SM4500-H+B 0 su SM 2540C 100 rng/L SM2540D 25 mgfl SM 5210 8 300 mgfl 0 mgfl SW846CH.7 0.25 mg/Kg HACH 8000 50 mgfl EPA 300.0 10

. 0 mgfl 50 mgfl 100 mgfl SM 5540C 0 . 25 H mg/L as LAS EPA 350.1 . 5 . 00 mgll as N EPA 353.2 0 . 05 mg/L as N EPA420.1 100 IJg/L SW846 CH.7 0 . 25 mg/Kg EPA 351.2 DF Date Analyzed Analyst: LNW 2/4/2011
9 : 44

: 00 AM Analyst: LNW 213/2011
4 : 50

: 00 PM Analyst: LNW

· 2/312011
4 : 50:00 PM Analyst: LNW 1 213/2011
4 : 50:00 PM Analyst: KLS 5 1/31/2011
7 : 10:00 AM Analyst: KLS 5 1/31/2011
7 : 17
: 04 AM Analyst: SAG 300 1/28/2011
6 : 50

: 00 PM 300 0 . 99 5 50 50 50 5 50 · 5 0 . 99 1/28/2011
6 : 50

: 00 PM Analyst: SAG 219/2011
4 : 58:00 .PM Analyst: MGV 211/2011 Analyst: CAS 1/31/2011
2 : 51:00 PM 1/31/2011 2:51:00 PM 1/31/20112

: 51

: 00 PM Analyst: CAS 21212011
2 : 30

: 00 PM Analyst: SLY 2/10/201112:51

: 01 PM Analyst: SLY 2/1/201110:14

: 21 AM Analyst: KMW 2/4/2011

1 : 05

: 00 PM Analyst: SLY 2/3/2011
2 : 50

: 00 PM Analyst: SLY ------------------·
-- ·--·· ·--·

· ---- -· ··-·-·

- · **~ ~** 

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% I.D 56-00306 PA DEP Page 3 of 7Laboratory Results Geochemical Testing

Date: 23-Feb-11 CLIENT: Lab Order: RESOURCE MANAGEMENT SERVICES Gll01912
Client Sample ID: Eckles Well 8590H FB RMS 111128 Project: 26R Analysis Lab ID: GIIOI912-00J Matrix: AQUEOUS Analyses INORGANIC NON-METALS Total Kjeldahl Nitrogen INORGANIC METALS Iron, dissolved INORGANIC METALS Mercury TCLP METALS Mercury TCLP METALS Arsenic Barium Cadmium Chromium Lead Selenium Silver INORGANIC METALS Aluminum Arsenic Barium Beryllium Boron Cadmium Calcium Chromium Cobalt Copper Iron Lead Lithium Magnesium Manganese Molybdenum N i ckel Selenium Silver Sodium Strontium Zinc Result 61

.4 10

.5 < 0.20 < 0 . 0002 <0.020 3190 < 0.002 < 0.010 < 0.020 < 0 . 020 < 0.005 < 1.0 < 0 .20 2850 < 0.010 2.58 <0.020 7470 < 0 .10 0.544 < 0 .10 46

.9 < 0 .20 60

.3 638 3 .47 < 0 .20 < 0 .10 < 0 .20 < 0 . 050 1510 1350 < 0 .10 Sampled By: Client Collection Date: 1128/2011

1 : 10:00 PM Received Date: 1/28/2011
7 : 08
: 50 PM QL Q EPA351.2 20.0 EPA 200.7 0.05 SM 31128 0 .20 EPA 7470 0 . 0002 EPA6010 0.020 150 0 . 002 0.010 0.020 0.020 0.005 EPA 200.7 1 .0 0 .20 5 .00 0.010 0.50 0.020 25.0 0 .10 0 . 050 0 .10 0 .50 0 .20 5 .00 1.0 0 .10 0 .20 0 .10 0 .20 0 . 050 100 2 .50 0 .10 Units mg/LasN !119/L !Jg/L rngll mgll mgll rngll mgll rngll mgll mgll mgll mgll mgll mgll mgll mg/L mgll mg/L mgll mgll mg/L mg/L mg/L mg/L mgll mg/l mg/l mg/L mg/l mgll mgll mgll DF 20 1 500 10 10 500 10 10 10 250 10 10 10 10 10 500 10 10 10 10 10 10 500 250 10 Date Anal _ yzed Analyst: SLY 211 Ji011 2:35

: 48 PM Analyst: MS 21112011 12:26:00 PM Analyst: JEK 211/2011 12
: 53

: 33 PM Analyst: JEK 21112011 12
: 49:15 PM Analyst: MS 211/201112

: 18:00 PM 213/201110

: 31

: 00AM 211/201112

: 18:00 PM 211/201112

: 18:00 PM 211/2011 12
: 18

: 00 PM 21112011 12
: 18:00 PM 211/2011 12:18:00 PM Analyst: MS 211/2011 12
: 22

: 00 PM 211/2011 12
: 22

: 00 PM 213/2011 10
: 35

: 00 AM 211/2011 12
: 22:00 PM 21112011 12
: 22

: 00 PM 211/2011 12
: 22

: 00 PM 213/2011 10
: 38:00 AM 211/2011 12
: 22

: 00 PM 211/2011 12
: 22:00 PM 211/201112

: 22:00 PM 2/1/201112

: 22

: 00 PM 2/1/2011 12
: 22

: 00 PM 2/3/2011
7 : 41 :00 PM 2/1/2011 12:22

: 00 PM 2/1/2011 12
: 22

: 00 PM 2/1/2011 12
: 22

: 00 PM 2/1/2011 12
: 22

: 00 PM 2/112011 12
: 22

: 00 PM 2/1/2011 12
: 22

: 00 PM 2/3/2011
7 : 41

: 00 PM 2/3/2011 10
: 38

: 00 AM 2/1/2011 12:22

: 00 PM .. - -·-- **·~-** - -·------ -- ----- ----.

------------- I.D 56-00306 PA DEP Page 4 of 7Laboratory Results Geochemical Testing

Date: 23-Feb-11

- CLIENT: RESOURCE MANAGEMENT SERVICES Client Sample ID: Eckles Well 8590H FB Lab Order: Gll01912

RMS 111/28 Project: 26R Analysis Sampled By: Client Lab ID: Gl101912-00I Collection Date: l/28/20lll

: IO : OOPM Matrix: AQUEOUS Received Date: 1/28/2011
7 : 08:50 PM Analyses Result QL Q Units DF Date Analyzed INORGANIC METALS EPA200

.7 Analyst: MS Hardness (SM 23408) 18500 10.0 mg/LCaC03
10 211/2011 12:22:00 PM INORGANIC METALS EPA200.8 Analyst: JEK Thorium
<200

. 200 IJ9/L 200 21812011 3:03:00 PM Uranium
<200 200 IJ9/L 200 21812011
3 : 03

: 00 PM TCLP HERBICIDES EPA8151 Analyst.: NPT 2,4

,5-T

<0

.0050

0 .0050 mgll 100 213/2011 10
: 39

: 30 PM 2.4-0

< 0 .020

0 .020 mgll 100 213/2011 10
: 39:30 PM Silvex

<0

.0050 0.0050 mg/L 100 21312011 10
: 39:30 PM Surr: 2,4-Dichlorophenyt acetic acid 74

.9 28.5
- 130 %REC 100 213/2011 10
: 39

: 30 PM TCLP PESTICIDES EPA8081 Analyst: NPT Chlordane

< 0.010 0.010 mgll
10 21212011 7:07:46 PM Endrin <0.00050

0 . 00050 mgiL
10 21212011 7:07

: 46 PM Lindane

< 0 . 00050

0 . 00050 mgll
10 21212011
7 : 07:46 PM Methoxychlor

< 0 . 00050 0.00050 mg/L
10 21212011
7 : 07:46 PM Toxaphene

< 0.020

0 .020 mg/L
10 21212011
7 : 07:46 PM Heptachlor (and its epoxide)

< 0.0010

0 .0010 mgll
10 21212011
7 : 07:46 PM Surr

: Decachlorobiphenyl

96

.3 5-156 %REC
10 21212011
7 : 07:46 PM Surr: Tetrachloro-m-xylene

64

.3 15

. 9-102 %REC
10 21212011
7 : 07:46 PM SEMI-VOLATILE COMPOUNDS: TCLP EPA8270 Analyst: JB 2-Methylphenol

< 100 100 IJg/L
10 21412011
6 : 48

: 00 AM 2,4-Dinitrotoluene

< 100 100 IJg/L
10 21412011
6 : 48:00 AM Hexachlorobenzene

< 100 100 j.lgll
10 21412011
6 : 48

: 00 AM Hexachlorobutadiene

< 100 100 jJgll
10 21412011
6 : 48:00 AM Hexachloroethane

< 100 100 IJg/L
10 214/2011
6 : 48

: 00 AM Nitrobenzene

< 100 100 IJg/L
10 214/2011
6 : 48

: 00 AM Pentachlorophenol

< 500 500 IJg/L
10 2/4/2011
6 : 48:00 AM Pyrid

i ne
<200 200 IJg/L
10 2/4/2011
6 : 48

: 00AM 2.4

, 5-Trichlorophenol

< 100 100 IJg/L
10 214/2011
6 : 48

: 00 AM 2,4,6-Trichlorophenol

< 100 100 IJg/L
10 2/4/2011
6 : 48

: 00 AM 3 , 4-Methylphenol

< 100 100 IJg/L
10 2/4/2011
6 : 4 _ 8:00 AM Surr

: 2,4,6-Tribromophenol

101 5-137 %REC
10 2/4/2011
6 : 48

: 00 AM Surr: 2-Fiuorobiphenyl

49

.3 27

.7-95

.1 %REC
10 214/2011 6:48

: 00 AM Surr

: . 2-Fiuorophenol
60.4 5-104 %REC
10 2/4/2011
6 : 48

: 00 AM Surr: Nitrobenzene-d5

86

.7 16-101 %REC
10 2/4/2011
6 : 48:00 AM Surr

: Phenol-d6

51.7 5-106 %REC
10 2/4/2011
6 : 48

: 00 AM Surr: p-Terphenyl-d14

38.8 25.4-133 %REC
10 2/4/2011
6 : 48

: 00 AM VOLATILE ORGANIC COMPOUNDS
EPA 8260 Analyst: SJM Benzene

< 1.0

1 .0 IJSIL 1/31/2011 7:02

: 00 PM -------

---------

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X I. D . 56-00306 PA DEP Page 5 of 7Laboratory Results Geochemical Testing

Date: 23-Feb-1
I CLIENT: RESOURCE MANAGEMENT SERVICES Client Sample ID: Lab Order: Gll01912 Project: 26R Analysis Lab ID: 01101912-001 Matrix: AQUEOUS Analyses Result VOLATILE ORGANIC COMPOUNDS Toluene Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr

: Toluene-dB VOLA TILE ORGANIC COMPOUNDS: TCLP Benzene Carbon Tetrachloride Chlorobenzene 1,1-Dichloroethene 1,2-Dichloroethane 1 A-Dichlorobenzene Trichloromethane Methyl Ethyl Ketone Tetrachloroethane Trichloroethane Vinyl Chloride Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr

: Toluene-dB INDICATOR ORGANIC PARAMETERS Oil & Grease NOTES:

1.1 10B 102 95.3 <50 <50 <50 <50 <50 <50 <50 < 250 <50 <50 <50 90.7 99

.7 92.0 97

. 0 436 Sampled By: Collection Date: Received Date: QL Q Units EPA8260 1.0 j.lg!L 70-130 %REC 70-130 %REC 70-130 %REC EPA8260 50 IJg/L 50 IJQ/L 50 IJg/L 50 IJg/L 50 IJQIL 50 !Jg/L 50 IJQIL 250 IJg/L 50 IJQ/L 50 IJ9/L 50 !Jg/L 70-130 %REC 70-130 %REC 70-130 %REC 70-130 %REC EPA 1664 5 . mg/L Eckles Well 8590H FB RMS 1/1/28 Client 1128/2011

1 : 10:00 PM 1/28/2011 7:08:50 PM DF 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 1.0B Date Analyzed Analyst: SJM 1/31/2011 7:02

: 00 PM 1/3112011
7 : 02

: 00 PM 1/31/2011
7 : 02

: 00 PM 1/31/2011 7:02

: 00 PM Analyst: JAW 21312011
4 : 31

: 00 AM 213/2011 4:31

: 00 AM 21312011
4 : 31

: 00 AM 213/2011
4 : 31

: 00 AM 2/3/2011
4 : 31

: 00 AM 213/2011
4 : 31

: 00 AM 213/2011 4:31

: 00 AM 213/2011
4 : 31

: 00 AM 2/3/2011 4:31

: 00AM 2/3/20114

: 31

: 00AM 2/3/2011
4 : 31:00 AM 21312011
4 : 31

: 00 AM 2/312011
4 : 31

: 00 AM 2/3/2011 4:31

: 00 AM 213/2011
4 : 31

: 00 AM Analyst: DSZ 2/1/2011 B:4B

: OO AM J- Unable to obtain a stable weight within specified limits due to sample matrix

. Value is estimated. VOLATILE ORGANIC COMPOUNDS Ethylene Glycol

< 550 RADIOLOGICAL TESTING Gross Alpha 7229 +- 1675 Gross Beta
104B +- 748 RADIOLOGICAL PARAMETERS Radium 226
163B +- 307 RADIOLOGICAL PARAMETERS Radium 22B

199 +- 39

.2 INORGANICS NON-METALS Corrosivity Characteristic
6.55 FLASH POINT EPA8015 550 mg/L EPA 900.0 3.00 pCill 4 . 00 pCi/L EPA 903.1 1 . 00 pCi/L EPA 904.0 1 . 00 pCi/L EPA 9040 1.00 su EPA 1010 Page 6 of 7 Analyst: SUB 2/712011 Analyst: SUB 2/10/2011 2/10/2011 Analyst: SUB 2/1B/2011 Analyst: SUB 2/1B/2011 Analyst: RLL 1/31/2011 Analyst: RLL I. D. 56-00306 PA DEPLaboratory Results Geochemical Testing

Date: 23-Feb-1
I CLIENT: Lab Order: RESOURCE MANAGEMENT SERVICES Gll01912
Client Sample ID: Eckles Well 8590H FB RMS lll/28 Project: 26R Analysis Lab ID: Gll01912-00l Matrix: AQUEOUS Analyses Result FLASH POINT Flashpoint

>200 TCLP ZHE EXTRACTION TCLP,ZHE

RL TCLP EXTRACTION Extraction Fluid Used

NA Final pH .

3.1 Initial pH

NA pH with HCI

NA pH with water

NA TCLP, non-volatile

NA TCLP,ZHE

NA Sampled By: Client Collection Date: l/28/20 II l: l 0:00 PM Received Date: l/2812011 7:08:50 PM ·------- ----·-- -- ------- --- ----
-- ·--- QL Q EPA 1010 10.0 EPA 1311 1.0 EPA 1311 0 1.0 1.0 1.0 1 . 0 0 0 Page 7 of 7 Units "F DF Date Analyzed Analyst: RLL 2/2/2011 Analyst: **R~L** 1131/2011 Analyst: RLL 1 . 1131/2011 1 1/31/2011 1131/2011 1 1/31/2011 1 1131/2011 1/31/2011 1/31/2011
I. D . 56-00306 PA DEP• 2540-PM-BWM0347 Rev. 1/2011 **~pennsylvania** - **DBWITMEHTOF~I'AOTECTION** COMMONWEALTH OF PENNSYLVANIA DEPARTMENT OF ENVIRONMENTAL PROTECTION BUREAU OF WASTE MANAGEMENT FORM26R CHEMICAL ANALYSIS OF RESIDUAL WASTE ANNUAL REPORT BY THE GENERATOR typed or legibly printed In the spaces provided. If additional space Is necessary, Identify each attached sheet as Fonn 26R, l'8ference the Item number and Identify the date prepared. The date on attached sheets needs to match the date noted below. General 287.54 DaUt Prepared/Revised 219/11 .Company c. Appearance Number of Solid or Uquid Phases of Separation Une2

No Describe each phase of separation

• **..::=:c~--------------;** -1 -2540-PM-BWM0347 Rev.1/2011 b. schematic of the as specified In the Instructions, Is attached. c. If portions of the
are a confidentiality claim, as described In the Instructions, Is attached. PA0095273 b. Facility Name c . a. Address Une 1 Address Une 1 Address City State ZIP Municipality Phone Solid b. Name c . b. Address Une 1 Address Une 1 Address City State ZIP Municipality Title Phone Volume of waste
being utilized. Oton - 2-

No (check one) (check one) (check one)2540-PM-BWM0347 Rev.112011 I certify, under penalty of law, that

I have personally examined and am familiar with the lnfonnation submitted In this Annual Report and all attached documents and that based upon my Inquiry of those Individuals Immediately responsible for obtaining the lnfonnation,

I verify that the submitted lnfonnatlon Is true, accurate and complete to the best of my knowledge.

I understand that the submission of false Information herein Is made subject to the penalties of 18 Pa. C.S. §4904, relating to unsworn falsification to authorities, which Include fine and Imprisonment. Check the following, If applicable: 0

I certify the Information required In Section B-1, General Properties was supplied to the Deparbnent for the year _and has not changed. Form Submitted:

0 Form 26R 0 Other (specify) ------------- Date Submitted: 0

I certify the Information required In Section B-2, Chemical Analysis was supplied to the Deparbnent for the year _and has not changed. Form Submitted:

0 Form26R 0 Other (specify) Date Submitted: 0

I certify the Information required In Section **~.**Process Description and Schematic, was supplied to the Department for the year_ and has not changed. Form Submitted:

0 Form 26R 0 Other (specify) Date Submitted: Name of Responsible Official

Title EH & S Marcellus Shale Bernhardt Signature

Date 2-28-11 -3-February 9, 2011 Form 26R: Section B 1 e GENERATOR KNOWLEDGE All Form 26R Waste Forms have been compiled, and future testing has been scheduled, to obtain samples of each waste stream on a PAD by PAD basis. Sample analyses will be conducted every 5 years for each waste stream unless the process that generates any particular waste stream is substantially altered. Attached analytical results for this waste stream have been obtained from
.a similar waste stream producing waste from the same geologic formation as this 26R Report. Additionally, the mud mixtures, chemical formulations and drilling process utilized at this well PAD are substantially the same as those utilized at the well where the attached waste analyticals were generated.February 8, 2011 Form 26R: Section B2b WASTE SAMPLING METHODS All samples were obtained as grab type samples with a composite function which was maximized but sometimes limited by prevailing safety, site specific rational and/or environmental concerns. Brine fluids are composited within the storage production tank or tank battery at each well site where gas production is occurring. Each automatic or manual ejection of formation fluids is deposited into the tank(s) and added to the previously ejected and stored quantity. Tanks are emptied into tank trucks for disposal at various PaDEP permitted waste disposal facilities on different schedules determined by individual well characteristics. Grab samples of the composited fluids were obtained at the represented well pads directly from the storage tank drain ports. All drain ports had small "built in" containment and storage "buckets" capable of retaining small amounts of lost fluids. Samples were obtained with bottle sets prepared at the laboratory which contained appropriate preservatives, as necessary, depending on the specific test run requested. All chain of custody and handling/holding time requirements were met. In some cases, a larger sample was broken into appropriate sampling containers and smaller aliquot portions at the laboratory. Flowback samples were composited to the extent possible during the flowback process primarily during times where safety issues did not override sample collection requirements. Generally,
a larger composite sample was broken into appropriate sampling containers and smaller aliquot portions at the laboratory or on the well location upon completion of the composite sampling process. Samples were distributed into bottle sets prepared at the laboratory which contained appropriate preservatives, as necessary, depending on the specific test run requested. All chain of custody and handling/holding time requirements were met. Drill cuttings were composite sampled during the drilling process at various times and combined into a composite sample for analyses at the laboratory. On several wells, cuttings from the vertical portion of the well bore were segregated from cuttings from the target Marcellus Formation and separate testing was completed on both sample composites.
In some earlier cases during the utilization of open pits, composite samples were obtained from inactive drill pits. Safety concerns usually limited the randomness of the composite sample and composite grid sample positions were varied to the extent possible. Pit water (drill fluid) is currently discharged to closed containment and is re-conditioned and reused from well to well.i· February 9, 2011 Form 26R: Section B3a WASTE GENERATION PROCESS Pit Water "Drill Fluids" Remnant drill fluids are generated in the well bore during the penetration of the drill stem as it intercepts both ground water and formation fluids. These fluids are brought to the surface along with the drill cuttings, pieces of the intercepted rock strata, by the return flow system of the drilling process. Drill cuttings and drill fluids are isolated into separate waste streams. Cuttings are mixed with sawdust to absorb remnant fluid and loaded out for disposal at a landfill. Fluids are currently stored in closed containers to be processed for reuse. Flowback: "Fracing Fluid" Flowback is produced from all fluids that flow back to surface during the "hydrofracing" process which occurs under pressure and results in the setting of a propant within the formation fractures. Production Fluid "Brine" During the production of natural gas, formation pressures bring remnant frac fluids, during the initial production phase, and formation fluids to the surface along with produced gas.WellI.D.#(various)WellI.·D.#.(various) '\/**~**

-0 **-~- /~,**  /1' I\ 1 \/WellI.D.#(various) \I::t)/ \I /II' \I/ \I// \I// ..\I/ WellI.D.#(various)\1// '\// \I/ -0-/",...--- **~-:../ '<'"0~~~;** **~o'fo,~**MobileTankTruck **~I"'O~vc**..:\-IOJ\Ocu**t\\~~.l**

COUNTYA COUNTYB\tM'..S::( ,·J1Sbrine(TYP.) ----Landfill or'

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**Tr«A.+~U\t**'PlGV\t. Note:Processproducingwaste:Gaswellproduced fluids(brines)aretypicallyproduced'in conjuctionwi.thnaturalgas.Thesefluids arebroughttothesurfaceutilizingeither mechanicalorphysicalliftprocedur.es. h**~·** n**~ ~**  BiGEOCHEMICAL TESTING Environmental and Energy Analysis Wednesday, February 23, 2011 RICK BONAZZA RESOURCE MANAGEMENT SERVICES 65 FENTON ROAD INDIANA, PA 15701 RE: 26R Analysis Dear RICK BONAZZA:OrderNo.: 01101912

. Geochemical Testing received

1 sarnple(s) on 1128/2011 for the analyses presented in the following report. There were no problems with the analyses and all QC data met NELAC, EPA, and laboratory specifications except where noted in the Case Narrative or Laboratory Results. If you have any questions regarding these tests results, please feel free to call. Sincerely, Timothy W. Bergstresser Director of Technical Services

2005 N Center Ave Somerset- PA 15501 814/443-1671 814/445-6666 FAX: 814/445-6729Geochemical Testinl! CLIENT: Project: Lab Order: RESOURCE MANAGEMENT SERVICES 26R Analysis G\101912

Date: 23-Feb-11 CASE NARRATIVE No problems were encountered during analysis of this workorder, except if noted in this report. The ethylene gycol analysis was subcontracted
to Free Col Labs. A copy of the subcontractor's laboratory report is enclosed with this Analytical Report. The radiological analysis was subcontracted to Pace Analytical. A copy of the subcontractor's laboratory report is enclosed with this Analytical Report. **~g~:d**

**·** - . --- **N;·~-~-~~ ~~~~d** at · ;; **~~~~t;~-n -~~~i~** 

. -----·-

. ----- -------------· ·s- : **Spik~ Re~~~~;;~utsi~** **~~~~t~d r;~~ry** **ii;its** J ·Indicates an estimated value.

R. RPD outside accepted recovery limits U ·The analyte was not detected at or above the listed concentration, which is below the laboratory quantitation limit. B • Analyte detected in the associated Method Blank Q ·Qualifier QL -Quantitation Limit DF ·Dilution Factor E ·Value above quantitation range **·Value exceeds Action Limit H • Method Hold Time Exceeded MCL. Contaminant Limit 1.0. 56..00306 PA DEPLaboratory Results Geochemical Testing

Date: 23-Feb-11 . **··· ·-** **~-= -·** · .. ··- . · :::-·
· . ··· _-:-: ·.-- ::- ..-.. : -· : - · :.: .: · .-.

- . ··------- ·.

• ·' • **~-** ·- .... _ - __···:_

· _·:
..·: ·.: .:;; :- .'.:

.··.: :- ·· -:· · :· .. ----- .. ---·--
. CLIENT: Lab Order: RESOURCE MANAGEMENT SERVICES GII01912
Client Sample ID: Eckles Well 8590H FB RMS 1/1/28 Project: 26R Analysis Lab ID: Gll01912·001 Matrix: AQUEOUS Analyses Result INORGANIC NON-METALS Acidity to pH 8.2

-38 INORGANIC NON-METALS Alkalinity to pH 4 .5
150 PHYSICAL TESTS Specific Conductance 111000 PH BY SM 4500 H+B Lab pH

6.52 INORGANIC NON-METALS Total dissolved solids 97500 PHYSICAL TESTS Total

· suspended solids
545 INDICATOR ORGANIC PARAMETERS BOD 5-day
1350 Finish Date/Time 2/21201118:10 REACTIVE CYANIDE Reactive cyanide INDICATOR ORGANIC PARAMETERS Chemical Oxygen Demand INORGANIC NON-METALS Bromide Chloride Sulfate INORGANIC NON-METALS MBAS INORGANIC NON-METALS Ammonia Nitrogen

- Distilled INORGANIC NON-METALS Nitrate

- Nitrite INDICATOR ORGANIC PARAMETERS Phenolics REACTIVE SULFIDE Reactive sulfide INORGANIC NON-METALS <0.25 5800 461 57100 < 100 < 0.25 69.1 0.53 < 100 0.50 Sampled By: Client Collection Date: l/28/2011 I: 10:00 PM Received Date: 1/28/2011 7:08:50 PM QL Q Units SM

· 2310B(4A) 0 mg/LCaC03 SM 18 23208 5 mgllCaC03 EPA 120.1 1Jrnhoslcm SM4500-H+B 0 su SM 2540 C 100 mgll SM 25400 25 mgll SM 5210 B 300 mgll 0 mgiL SW846CH.7 0 .25 mg/Kg HACH 8000 50 mgll EPA 300.0 10.0 mgll 50 mgll 100 mg/L SM5540C 0.25 H mg/L as LAS EPA 350.1 .5 .00 mgll as N EPA 353.2 0.05 mg/L as N EPA 420.1 100 IJQ/L SW846 CH.7 0.25 mg!Kg EPA351.2
DF Date Analyzed Analyst: LNW 1 21412011
9 : 44:00 AM Analyst: LNW 21312011 4:50

: 00 PM Analyst: LNW 21312011 4 : 50:00 PM Analyst: LNW 21312011 4:50:00 PM Analyst: KLS 5 1/31120117:10

: 00AM Analyst: KLS 5 1/3112011 7:17:04 AM 300 300 Analyst: SAG 1128/2011 6:50

: 00 PM 112812011 6:50

: 00 PM Analyst:

· SAG 0.99 21912011 4 : 58
: 00

.PM Analyst: MGV 5 21112011 Analyst: CAS 50 1/3112011
2 : 51
: 00 PM 50 113112011
2 : 51:00 PM 50 113112011
2 : 51:00 PM Analyst: CAS 5 21212011 2:30:00 PM Analyst: SLY 50 2110/201112:51

: 01 PM 0.99 Analyst: SLY 2/1/2011 10
: 14
: 21 AM Analyst: KMW 2/4/2011

1 : 05:00 PM Analyst: SLY 2/3/2011
2 : 50:00 PM Analyst: SLY -----

· -----

-----
------------- 4-• 4 ·----·····--·- I.D . 56-00306 PA DEPLaboratory Results Geochemical Testing CLIENT: Lab Order: RESOURCE MANAGEMENT SERVICES 01101912 Project: 26R Analysis Lab ID: GII01912-00I Matrix: AQUEOUS Analyses INORGANIC NON-METALS Total Kjeldahl Nitrogen INORGANIC METALS Iron, dissolved INORGANIC METALS Mercury TCLP METALS Mercury TCLP METALS Arsenic Barium Cadmium Chromium Lead Selenium Silver INORGANIC METALS Aluminum Arsenic Barium Beryllium Boron Cadmium Calcium Chromium Cobalt Copper Iron Lead Lithium Magnesium Manganese Molybdenum Nickel Selenium Silver Sodium Strontium Zinc **--~**

- · - - -· **··-· -------** **·--·-·-**

- --
· · - -- - - - - Result 61.4 10.5 <0.20 <0.0002 < 0.020 3190 <0.002 < 0.010 <0

. 020 <0

. 020 < 0.005 < 1.0 <0.20 2850 < 0.010 2.58 < 0.020 7470 <0.10 0 . 544 < 0 . 10 46.9 < 0.20 60.3 638 3.47 < 0.20 < 0.10 <0

. 20 < 0 . 050 1510 1350 < 0.10 QL Q EPA 351.2 20
. 0 EPA200.7 0.05 SM 31128 0.20 EPA 7470 0.0002 EPA6010 0 . 020 150 0.002 0.010 0 . 020 0 . 020 0.005 EPA200.7 1.0 0.20 5.00 0.010 0.50 0 . 020 25.0 0 . 10 0 . 050 0.10 0 . 50 0 . 20 5.00 1.0 0 . 10 0.20 0 . 10 0 . 20 0 . 050 100 2.50 0.10 Date: 23-Feb-11 Client Sample ID: Eckles Well 8590H FB RMS 1/1/28 Sampled By: Client Collection Date: 1/28/2011 1:10:00 PM Received Date: 1/28/2011 7:08:50 PM Units mg/Las N mgiL **~** mg/L mgll. mg/L mgll. mgiL mgiL mgiL mgiL mgll. mg/l. mgll. mgll. mgll. mgll mgiL mgiL mgiL mgll. mg/l. mg/L mgll. mg/L mgll. mg/L mgll. mg/L mgll. mg/L mg/L mg/L DF Date **Ana~yzed** 20 500 1 1 Analyst: SLY 2/1/2011 2:35:48 PM Analyst: MS 2/1/2011 12:26:00 PM Analyst: JEK 2/1/2011 12:53

: 33 PM Analyst: JEK 2/1/201112:49

: 15 PM Analyst: MS 2/1/2011 12:18:00 PM 213/201110:31:00AM 2/1/201112:18:00 PM 2/1/2011 12
: 18
: 00 PM 2/1/201112:18:00 PM 2/1/2011 12
: 18:00 PM 2/1/2011 12:18

: 00 PM Analyst: MS 10 2/1/2011 12:22:00 PM 10 2/1/201112:22:00 PM 500 213/2011 10:35:00 AM 10 2/1/2011 12:22:00 PM 10 2/1/2011 12:22

: 00 PM 10 2/1/201112:22:00 PM 250 2/3/2011 10:38

: 00 AM 10 2/1/2011 12
: 22:00 PM 10 2/1/2011 12:22

: 00 PM 10 2/1/201112

: 22
: 00PM 10 2/1/2011 12:22:00 PM 10 2/1/2011 12:22:00 PM 500 2/3/2011 7:41 :00 PM 10 2/1/2011 12:22:00 PM 10 2/1/2011 12:22:00 PM 10 2/1/201112:22:00 PM 10 2/1/2011 12
: 22
: 00 PM 1 0 2/1/2011 12
: 22
: 00 PM 10 2/1/2011 12
: 22
: 00 PM 500 2/3/2011 7:41

: 00 PM 250 2/3/2011 10:38:00 AM 10 2/1/2011 12:22:00 PM I. D. 56-00306 PA DEPLaboratory Results Geochemical Testing

Date: 23-Feb-11 . - CLIENT: RESOURCE MANAGEMENT SERVICES Client Sample ID: Eckles Wel18590H FB Lab Order: GIIOI912

RMS 111/28 Project: 26R Analysis Sampled By: Client Lab ID: Gll01912-001 Collection Date: 1/28/2011 1:10:00 PM Matrix: AQUEOUS Received Date: 112812011
7 : 08
: 50 PM Analyses Result QL Q Units DF Date Analyzed INORGANIC METALS EPA200.7 Analyst: MS Hardness (SM 2 . 340B) 18500 10.0 mgiLCaC03
10 2/1/2011 12
: 22:00 PM INORGANIC METALS

EPA 200

.8 Analyst: JEK Thorium
<200

' 200 **~IL** 200 2/812011 3:03:00 PM Uranium
<200 200 **~giL**200 2/812011
3 : 03

: 00 PM TCLP HERBICIDES

EPA 8151 Analyst

_: NPT 2,4

, 5-T

< 0.0050

0 . 0050 mg/L 100 2/312011 10
: 39

: 30 PM 2,4-0

< 0.020

0 . 020 mgll 100 2/3/2011 10:39:30 PM Silvex <0.0050 0.0050 mgiL 100 2/312011 10
: 39

: 30 PM Surr: 2.4-Dichlorophenyl acetic acid 74.9 28

. 5-130 %REC 100 2/312011 10:39

: 30 PM TCLP PESTICIDES EPA8081 Analyst: NPT Chlordane

< 0 . 010

0 . 010 mg/L
10 21212011
7 : 07:46 PM Endrin

<0

. 00050

0 . 00050 mgiL
10 21212011 7:07

: 46 PM Lindane

< 0 . 00050

0 . 00050 mgiL
10 2/212011
7 : 07:46 PM Methoxychlor

< 0.00050 0.00050 mg/L
10 21212011 7:07:46 PM Toxaphene

< 0.020

0 . 020 mgll
10 21212011
7 : 07

: 46 PM Heptachlor (and its epoxide)

< 0.0010 0.0010 mgll
10 21212011
7 : 07

: 46 PM Surr

: Decachlorobiphenyl

96.3 5-156 %REC
10 21212011 7:07:46 PM Surr: Tetrachloro-m-xylene

64

.3 15.9-102 %REC
10 21212011 7:07

: 46 PM SEMI-VOLATILE COMPOUNDS: TCLP EPA8270 Analyst: JB 2-Methylphenol

< 100 100 **~giL**
10 2/4/2011
6 : 48

: 00 Nil 2,4-Dinitrotoluene

< 100 100 **~giL**
10 2/4/2011 6:48

: 00 Nil Hexachlorobenzene

< 100 100 **~giL**
10 2/4/2011 6:48

: 00 AM Hexachlorobutadiene

< 100 100 J.19IL
10 2/4/2011 6:48

: 00 AM Hexachloroethane

< 100 100 IJQ/L
10 214/2011 6:48

: 00 AM Nitrobenzene

< 100 100 j.Jg/l
10 2/4/2011 6:48

: 00 AM Pentachlorophenol

< 500 500 **~ll**
10 2/4/2011 6:48

: 00 AM Pyridine
<200 200 j.Jg/L
10 2/4/2011
6 : 48

: 00

.AM 2,4,5-Trichlorophenol

< 100 100 IJg/L
10 2/4/2011 6:48

: 00 AM 2 , 4,6-Trichlorophenol

< 100 100 IJQ/L
10 214/2011
6 : 48

: 00 AM 3,4-Methylphenol

< 100 100 IJQ/l
10 2/4/2011 6:48

: 00 AM Surr

: 2,4,6-Tribromophenol

101 5-137 %REC
10 2/4/2011 6:48

: 00 AM Surr

: 2-Fiuorobiphenyl

49.3 27

. 7-95.1 %REC
10 2/4/2011 6:48

: 00 AM Surr
: 2-Fiuorophenol

60.4 5-104 %REC
10 2/4/2011 6:48

: 00 AM Surr

: Nitrobenzene-d5

86

.7 16-101 %REC
10 2/4/2011 6:48:00 AM Surr
: Phenol-d6

51

.7 5-106 %REC
10 2/4/2011
6 : 48:00 AM Surr: p-Terphenyl-d14

38

.8 25

. 4-133 %REC
10 2/4/2011
6 : 48

: 00 AM VOLATILE ORGANIC COMPOUNDS
EPA 8260 Analyst: SJM Benzene

< 1 .0

1 .0 IJQ/l 1/31120117

: 02:00 PM ---------------------

···---- ·--------
--··-----------------

-----
-------

----- **1\#.CColl(} ~** 

**~** u

**~** <

% 1.0 . 56 - 00306 PA OEPLaboratory Results Geochemical Testing

Date: 23-Feb-11 **-: .:** **.: ::-::::** **::: ====----**  **--~= ===-:** = CLIENT: Lab Order: RESOURCE MANAGEMENT SERVICES 01101912
Client Sample ID: Eckles Well 8590H FB RMS 111128 Project: 26R Analysis Sampled By: Client Lab ID: Gll01912-001 Collection Date: 1128/2011 1:10:00 PM Matrix: AQUEOUS Received Date: 1128/2011 7:08:50 PM ---------

-----··--------·····--· · **------ ---** **·- ··-** **--~----**

**-- ---** **-- -----** **····· ---** **·~-- --** **--**

**--**
**·**.. ·------

··--···- ·--- Analyses Result VOLATILE ORGANIC COMPOUNDS Toluene Surr
: 1 ,2-Dichloroethane-d4 Surr
: 4-Bromofluorobenzene Surr: Toluene-d8 VOLATILE ORGANIC COMPOUNDS: TCLP Benzene Carbon Tetrachloride Chlorobenzene 1 , 1-Dichloroethene 1 ,2-Dichloroethane 1 A-Dichlorobenzene Trichloromethane Methyl Ethyl Ketone Tetrachloroethane Trichloroethane Vinyl Chloride Surr: 1 ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-dB INDICATOR ORGANIC PARAMETERS Oii&Grease NOTES:

1.1 108 102 95.3 <50 <50 <50 <50 <50 <50 <50 < 250 <50 <50 <50 90.7 99.7 92.0 97.0 436 QL Q EPA8260 1.0 70-130 7Q-130 7Q-130 EPA8260 50 50 50 50 50 50 50 250 50 50 50 7Q-130 70-130 7Q-130 70-130 EPA 1664 5 Units **~** %REC %REC %REC **~giL ~**  **~giL ~g/L**  **~giL ~IL**  **~IL ~IL**  IJQIL **~giL** IJQIL %REC %REC %REC %REC mg/L DF 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 1.08 J -Unable to obtain a stable weight within specified limits due to sample matrix. Value is estimated. VOLATILE ORGANIC COMPOUNDS
EPA 8015 Ethylene Glycol <550 550 mg/L RADIOLOGICAL TESTING
EPA 900.0 Gross Alpha 7229 +- 1675 3.00 pCill **Gros~**Beta
1048
**~**748

4 .00 pCill RADIOLOGICAL PARAMETERS
EPA 903.1 Radium 226 1638 +- 307

1 .00 pCill RADIOLOGICAL PARAMETERS EPA904.0 Radium 228

199 +- 39.2

1 .00 pCi/L INORGANICS NON-METALS EPA9040 Corrosivity Characteristic

6 .55 100 su FLASH POINT

EPA 1010 Page 6 of 7 Date Analyzed Analyst: SJM 1/3112011
7 : 02
: 00 PM 1/31/2011 7:02

: 00 PM 1/31/2011
7 : 02
: 00 PM 1/31/2011
7 : 02
: 00 PM Analyst: JAW 213/2011 4:31

: 00 AM 213/20114:31

: 00AM 2/3120114

: 31:00AM 21312011 4:31:00 AM 213/2011 4:31:00 AM 21312011
4 : 31

: 00 AM 213/2011
4 : 31:00 AM 213/2011 4:31 :00 AM 21312011 4:31:00 AM 213/2011
4 : 31 :00 AM 21312011 4:31

: 00 AM 21312011
4 : 31
: 00 AM 21312011
4 : 31

: 00 AM 213/2011
4 : 31:00 AM 213/2011
4 : 31

: 00 AM Analyst: DSZ 211/2011
8 : 48

: 00 AM Analyst: SUB 217/2011 Analyst: SUB 2110/2011 2110/2011 Analyst: SUB 2118/2011 Analyst: SUB 2/18/2011 Analyst: RLL 1/31/2011 Analyst: RLL I. D. 56-00306 PA DEPLaboratory Results Geochemical Testing

Date: 23-Feb-11 CLIENT: Lab Order: RESOURCE MANAGEMENT SERVICES Gl101912
Client Sample ID: Eckles Well 8590H FB RMS 1/1/28 Project: 26R Analysis Lab ID: G1101912-001 Matrix: AQUEOUS Analyses FLASH POINT Flashpoint TCLP ZHE EXTRACTION TCLP,ZHE TCLP EXTRACTION Extraction Fluid Used Final pH . Initial pH pHwithHCI pH with water TCLP, non-volatile TCLP,ZHE Result >200 RL NA 3.1 NA NA NA NA NA Sampled By: Client Collection Date: 1/28/2011 1:10:00 PM Received Date: 1/28/2011 7:08:50 PM O
-

·**~--**

**-- ---·** **--•**
•• ·-·- -·- -· **-·--- ------** 

**~-**

-
- -

- -- ..
. --- HO QL Q EPA 1010 10.0 EPA 1311 1.0 EPA 1311 0 1.0 1.0 1.0 1.0 0 0 Units "F DF Date Analyzed Analyst: RLL 212/2011 Analyst: RLL 113112011 Analyst: RLL 1 . 1/3112011 1/3112011 113112011 1 1/3112011 1 1/31/2011 1 1131/2011 1 1/3112011 .... - · . ·-- ... ---··----- **~**. ···-- _,... - .. --- **~** - · . - ---·- 1.0. 56-00306 PA DEP o ........ ,.. 7 ,..,f. "72540-PM-BWM0347 Rev.1/2011 6 pennsylvania - llBWnMENT OF ENVIRONMENTAL PR0TECTJ0N COMMONWEALTH OF PENNSYLVANIA DEPARTMENT OF ENVIRONMENTAL PROTECTION BUREAU OF WASTE MANAGEMENT FORM26R CHEMICAL ANALYSIS OF RESIDUAL WASTE ANNUAL REPORT BY THE GENERATOR must and accurately completed. All required lnfonnation must be typed or legibly printed In the spaces provided. If additional space Is necessary, identify each attached sheet as Form 26R, reference the Item number and Identify the date prepared. The date on attached sheets needs to match the date noted below. General Reference 287.54 Date Prepared/Revised 219/11 c. Appearance2540-PM-BWM0347 Rev. 1/2011 a. b. A of the manufacturing as specified in the instructions, Is attached. c. If portions of the
ant a confidentiality claim, as described In the Instructions, Is attached. b. c. a. b. c. d. PA0091472 Name Add1"888 Une 1 Addl"888 Une 1 Address City State ZIP Municipality Address Une 1 Addl"888 Une 1 Add1"888 City State ZIP Municipality Title Phone Saltsburg waste shipped to processing or 0 cuyd 0 gal (check one) year. ton (check one) Oton (check one) -2-

NIA2540..PM-BWM0347 Rev.112011 I certify, under penalty of law, that

I have personally examined and am familiar with the lnfonnation submitted In this Annual Report and all attached documents and that based upon my Inquiry of those Individuals immediately responsible for obtaining the Information,

I verify that the submitted lnfonnation Is true, accurate and complete to the best of my knowledge.

I understand that the submission of false Information herein Is made subject to the penalties of 18 Pa. C.S. §4904, relating to unsworn falsification to authorities, which Include fine and Imprisonment Check the following, if applicable: 0

I certify the lnfonnation required In Section B-1, General Properties was supplied to the Department for the year _and has not changed. Fonn Submitted:

0 Form 26R 0 Other (specify) Date Submitted: 0

I certify the Information required in Section B-2, Chemical Analysis was supplied to the Department for the year _and has not changed. Form Submitted:

0 Fonn26R 0 **~(specify)**------------------------ Date Submitted: D

I certify the Information required In Section B-3, Process Description and Schematic, was supplied to the Deparbnent for the year_ and has not changed. Form Submitted:

0 Fonn26R 0 Other (specify) Date Submitted: Name of Responsible Official Bernhardt Signature

Date 2-28-11 -3-February 9, 2011 Fonn 26R: Section B1e GENERATOR KNOWLEDGE All Fonn 26R Waste Forms have been compiled, and future testing has been scheduled, to obtain samples of each waste stream on a PAD by PAD basis. Sample analyses will be conducted every 5 years for each waste stream unless the process that generates any particular waste stream is substantially altered. Attached analytical results for this waste stream have been obtained from a similar waste stream producing waste from the same geologic formation as this 26R Report. Additionally, the mud mixtures, chemical fonnulations and drilling process utilized at this well PAD are substantially the same as those utilized at the well where the attached waste analyticals were generated.February 8, 2011 Form 26R: Section B2b WASTE SAMPLING METHODS All samples were obtained as grab type samples with a composite function which was maximized but sometimes limited by prevailing safety, site specific rational and/or environmental concerns. Brine fluids are composited within the storage production tank or tank battery at each well site where gas production
is occurring. Each automatic or manual ejection of formation fluids is deposited into the tank(s) and added to the previously ejected and stored quantity. Tanks are emptied into tank trucks for disposal at various PaDEP permitted waste disposal facilities on different schedules determined by individual well characteristics. Grab samples of the composited fluids were obtained at the represented well pads directly **fro~**the storage tank drain ports. All drain ports had small ·built in• containment and storage •buckets• capable of retaining small amounts of lost fluids. Samples were obtained with bottle sets prepared at the laboratory which contained appropriate preservatives, as necessary, depending on the specific test run requested. All chain of custody and handlinglho!ding time requirements were met. In some cases, a larger sample was broken into appropriate sampling containers and smaller aliquot portions at the laboratory. Flowback samples were composited to the extent possible during the flowback process primarily during times where safety issues did not override sample collection requirements.

· Generally,
a larger composite sample was broken into appropriate sampling containers and smaller aliquot portions at the laboratory or on the well location upon completion of the composite sampling process. Samples were distributed into bottle sets prepared at the laboratory which contained appropriate preservatives, as necessary, depending on the specific test run requested. All chain of custody and handling/holding time requirements were met. Drill cuttings were composite sampled during the drilling process at various times and combined into a composite sample for analyses at the laboratory. On several wells, cuttings from the vertical portion of the well bore were segregated from cuttings from the target Marcellus Formation and separate testing was completed on both sample composites.
In some earlier cases during the utilization of open pits, composite samples were obtained from inactive drill pits. Safety concerns usually limited the randomness of the composite sample and composite grid sample positions were varied to the extent possible. Pit water (drill fluid) is currently discharged to closed containment and is re-conditioned and reused from well to well.j. February 9, 2011 Fonn 26R: Section 83a WASTE GENERATION PROCESS Pit Water "Drill Fluids" Remnant drill fluids are generated in the well bore during thE! penetration of the drill stem as it intercepts both ground water and fonnation fluids. These fluids are brought to the surface along with the drill cuttings, pieces of the intercepted rock strata, by the return flow system of the drilling process. Drill cuttings and drill fluids are isolated into separate waste streams. Cuttings are mixed with sawdust to absorb remnant fluid and loaded out for disposal at a landfill. Fluids are currently stored in closed containers to be processed for reuse. Flowback: "Fracing Fluid" Flowback is produced from all fluids that flow back to surface during the "hydrofracing" process which occurs under pressure and results in the setting of a propant within the fonnation fractures. Production Fluid "Brine" During the production of natural gas, fonnation pressures bring remnant frac fluids, during the initial production phase, and fonnation fluids to the surface along with produced gas.WellI.D.#(various)WellI.·D.#.(various) ,,/,,/

-0 _if'\\_ /v, /v, COUNTYA I\ 11 ',/WellI.D.#(various) \I::b/ \/ ///I' \I/ \ / \I/ / . . \I/ WellI.D.#(various)\1// '\// \I/ -a-,-" **~ ~~---** **~ ~**  --:r_1r**.,~_**-L'-**~ :--d~b,~**  **'fr-ob1vc..\t~/t**l**Oc~it,~~~**
COUNTYB\OAI<..s:·( -.**J~**5brine(TYP.)

_sRoadTransport Note:Processproducingwaste:Gaswellproduced fluids(brines)aretypicallyproduced·in conjuctionwithnaturalgas.Thesefluids arebroughttothesurfaceutilizingeither ·mechanicalorphysicalliftprocedur.es.
-----Landfill orTreu.+tv\(.J\t'?\CAllt

0**~**UJ:r:(.)CJ)z0**~**1-0::0Cl..CJ)z**~**1-**$~~11f ~~~~** **~**... t**~**

iI§I; **~~**s:id**~ ~**  ll8CJ- t!"2:S' I"**~ ~** I! **~ ~** **,~ I** **~ ~** GEOCHEMICAL TESTING Environmental and Energy Analysis Wednesday, February 23, 2011 RICK BONAZZA RESOURCE MANAGEMENT SERVICES 65 FENTON ROAD INDIANA, PA 15701 RE: 26R Analysis Dear RICK BONAZZA:OrderNo.: G1101912

. Geochemical Testing received
1 sample(s) on 1128/2011 for the analyses presented in the following report. There were no problems with the analyses and all QC data met NELAC, EPA, and laboratory specifications except where noted in the Case Narrative or Laboratory Results. If you have any questions regarding these tests results, please feel free to call. Sincerely, Timothy W. Bergstresser Director of Technical Services

2005 N 'Center Ave Somerset PA 15501 814/443-1671 814/445-6666 FAX: 814/445-6729Geochemical Testin2: CLIENT: Project: Lab Order: RESOURCE MANAGEMENT SERVICES 26R Analysis Gll01912

Date: 23-Feb-11 CASE NARRATIVE No problems were encoWltered during analysis of this workorder, except if noted in this report. The ethylene gycol analysis was subcontracted
to Free Col Labs. A copy of the subcontractor's laboratory report is enclosed with this Analytical Report. The radiological analysis was subcontracted to Pace Analytical. A copy of the subcontractor's laboratory report is enclosed with this Analytical Report. Legend: ND -Not Detected at the Quantitation Limit 1 - Indicates an estimated value

.

----------- **s=- sj;ik~** **Re~~~;r;,· ~iie** **~~~ ~Pt~** **~~~o~~ r),** **-ii~ its**  U - The analyte was not detected at or above the listed concentration. which is below the laboratory quantitation limit 8 - Analyte detected in the associated Method Blank Q- Qualifier QL -Quant

i tat i on Limit OF -Dilution Factor R - RPD outside accepted recovery limits E- Value above quantitation range u -Value exceeds Action Limit H -Method Hold Time Exceeded MCL
- Contaminant Limit
1.0 . 56--00306 PA DEPLaboratory Results Geochemical Testing

Date: 23-Feb-11 .. -·- -- **-~**.. -··- . -- . ·--
. - . -- .
: .. :-·;: ____: . _ -· : ..·:- ..-==: .··;:· ·--:- :.·._·_; __-: · -= : -:- _ - _-: ·- -· ..... --· .. **-~..**........ --- .. - -·- CLIENT: Lab Order: RESOURCE MANAGEMENT SERVICES 01101912
Client Sample 10: Eckles Well 8590H FB RMS 1/1128 Project: 26R Analysis Lab ID: GIIOI912-001 Matrix: AQUEOUS Analyses Result INORGANIC NON-METALS Acidity to pH 8.2

-38 INORGANIC NON-METALS Alkalinity to pH 4.5

150 PHYSICAL TESTS Specific Conductance 111000 PH BY SM 4500 H+B Lab pH

6 .52 INORGANIC NON-METALS Total dissolved solids 97500 PHYSICAL TESTS Total suspended solids
545 INDICATOR ORGANIC PARAMETERS BOD **5~ay**
1350 Finish Date!Time 2121201118

: 10 REACTIVE CYANIDE Reactive cyanide INDICATOR ORGANIC PARAMETERS Chemical Oxygen Demand INORGANIC NON-METALS Bromide Chloride Sulfate INORGANIC NON-METALS MBAS INORGANIC NON-METALS Ammonia Nitrogen

- Distilled INORGANIC NON-METALS Nitrate

- Nitrite INDICATOR ORGANIC PARAMETERS Phenolics REACTIVE SULFIDE Reactive sulfide INORGANIC NON-METALS

<0

.25 5800 461 57100 < 100 <0

.25 69.1 0.53 < 100 0 .50 Sampled By: Client Collection Date: 1128/2011 1:10

: 00 PM Received Date: 1/2812011 7:08:50 PM QL Q Units SM

· 231 OB(4A) 0 mgJLCaC03 SM 18 23208 5 mgJLCaC03 EPA 120.1 **~mhos/em** SM4500-H+B 0 su SM 2540 C 100 mgll SM2540D 25 mgll SM 5210 B 300 mgll 0 mgll SW846 CH.7 0 .25 mgiKg HACH 8000 50 -mgll EPA300.0 10.0 mgll 50 mgiL 100 mgiL SM 5540C 0 .25 H mgll as LAS EPA 350.1 ' 5 .00 mg/L as N EPA 353.2 0 .05 mg/L as N EPA420.1 100 **~g/L** SW846CH.7 0 .25 mg!Kg EPA 351.2 DF Date Analyzed Analyst: LNW 21412011
9 : 44

: 00 /WI Analyst: LNW 21312011 4:50

: 00 PM Analyst: LNW 2/312011
4 : 50

: 00 PM Analyst: LNW 21312011 4:50

: 00 PM Analyst:

.KLS 5 1/31120117:10:00/WI Analyst: KLS 5 1/31/2011
7 : 17:04 AM Analyst: SAG 300 1128/2011
6 : 50

: 00 PM 300 0 .99 5 50 50 50 5 50 ·5 0 .99 112812011
6 : 50

: 00 PM Analyst: SAG 219/2011
4 : 58:00 PM Analyst: MGV 21112011 Analyst: CAS 1/3112011 2:51

: 00 PM 1/3112011 2:51

: 00 PM 1/3112011 2:51

: 00 PM Analyst: CAS 21212011
2 : 30

: 00 PM Analyst: SLY 21101201112

: 51:01 PM Analyst: SLY 211/2011 10:14

: 21 AM Analyst: KMW 2/4/2011 1:05

: 00 PM Analyst: SLY 213/2011
2 : 50

: 00 PM Analyst: SLY --------

- · ---------------------- -·------- I. D. 56-00306 PA DEP n--- ,., ...,;. £ _,Laboratory Results Geochemical Testing

Date: 23-Feb-11 CLIENT: Lab Order: RESOURCE MANAGEMENT SERVICES Gll01912
Client Sample ID: Eckles We118590H FB RMS 1/1128 Project: 26R Analysis Lab ID: G1101912-00I Matrix: AQUEOUS Analyses INORGANIC NON-METALS Total Kjeldahl Nitrogen INORGANIC METALS Iron, dissolved INORGANIC METALS Mercury TCLP METALS Mercury TCLP METALS Arsenic Barium Cadmium Chromium Lead Selenium Silver INORGANIC METALS Aluminum Arsenic Barium Beryllium Boron Cadmium Calcium Chromium CobaH Copper Iron Lead lithium Magnesium Manganese Molybdenum Nickel Selenium Silver Sodium Strontium Zinc Result 61

.4 10
.5 < 0 .20 <0.0002 < 0 .020 3190 <0

.002 < 0 .010 < 0 .020 <0.020 < 0 .005 < 1.0 <0.20 2850 < 0 .010 2 .58 <0

.020 7470 < 0 .10 0.544 <0.10 46

.9 < 0 .20 60.3 638 3.47 < 0 .20 < 0.10 <0.20 < 0 .050 1510 1350 < 0 .10 Sampled By: Client Collection Date: 1/2812011 1:10

: 00 PM Received Date: 1128/2011 7:08

: 50 PM QL Q EPA351.2 20

.0 EPA200.7 0.05 SM 31128 0.20 EPA 7470 0 .0002 EPA6010 0.020 150 ** 0 .002 0 .010 0.020 0.020 0.005 EPA200.7 1 .0 0 .20 5.00 0.010 0.50 0 .020 25

.0 0 .10 0.050 0 .10 0 .50 0 .20 5 .00 1.0 0 .10 0 .20 0 .10 0 .20 0.050 100 2.50 0 .10 Units mg/L as N !T'gll **~giL** mgll mgll mg/L mg/L mgJL mgll mgll mg/L mgll mg/L mgll mgll mgll mg/L mg/L mg/L mgll mg/L mgll mgll mg/L mgll mg/L mg/L mg/L mg/L mg/L mgll mg/L mg/L DF 20 500 1 1 10 10 500 10 10 10 250 10 10 10 10 10 500 10 10 10 10 10 10 500 250 10 Date **Ana~yzed** Analyst: SLY 21112011
2 : 35:48 PM Analyst: MS 21112011 12
: 26
: 00 PM Analyst: JEK 2111201112

: 53
: 33 PM Analyst: JEK 2111201112

: 49
: 15 PM Analyst: MS 211/201112

: 18
: 00 PM 2131201110

: 31
: 00AM 211/201112

: 18
: 00 PM 21112011 12
: 18
: 00 PM 211/2011 12:18:00 PM 21112011 12:18

: 00 PM 21112011 12:18

: 00 PM Analyst: MS 21112011 12:22

: 00 PM 21112011 12
: 22:00 PM 213/2011 10:35

: 00 AM 21112011 12:22:00 PM 21112011 12:22

: 00 PM 211/2011 12:22

: 00 PM 213/2011 10
: 38:00 AM 21112011 12:22

: 00 PM 211/2011 12:22:00 PM 2/1/2011 12:22:00 PM 211/201112

: 22
: 00 PM 211/2011 12
: 22:00 PM 213/2011 7:41:00 PM 211/2011 12:22:00 PM 211/2011 12
: 22
: 00 PM 2/1/2011 12
: 22
: 00 PM 211/2011 12:22:00 PM 2/1/2011 12:22:00 PM 21112011 12
: 22:00 PM 2/3/20117

: 41:00PM 213/2011 10
: 38:00 AM 211/2011 12
: 22
: 00 PM -- ·.--- ---·· ···
····--- ---,_..._-

·-···--·-- ---

·-··------·-··------------
-·· ·-- . ---·- 1.0. 56-00306 PA DEPLaboratory Results Geochemical Testing

Date: 23-Feb-11 CLIENT: Lab Order: RESOURCE MANAGEMENT SERVICES Gll01912
Client Sample ID: Eckles Well 8590H FB RMS 111128 Project: 26R Analysis Lab ID: Gll01912-001 Matrix: AQUEOUS Analyses INORGANIC METALS Hardness (SM 2340B) INORGANIC METALS Thorium · Uranium TCLP HERBICIDES 2,4,5-T 2,4-D Silvex Surr: 2,4-Dichlorophenyl acetic acid TCLP PESTICIDES Chlordane Endrin Lindane Methoxychlor Toxaphene Heptachlor (and Its epoxide) Surr: Decachlorobiphenyl Surr: Tetrachloro-m-xytene SEMI-VOLATILE COMPOUNDS: TCLP 2-Methylphenol 2,4-Dinitrotoluene Hexachlorobenzene Hexachlorobutadiene Hexachloroethane Nitrobenzene Pentachlorophenol Pyridine 2,4,5-Trichlorophenol 2,4 ,6- Trichlorophenol 3,4-Methylphenol Surr

: 2,4,6-Tribromophenol Surr: 2-Fiuorobiphenyl Surr:
- 2-Fiuorophenol Surr: Nitrobenzene-<:15 Surr: Phenol-<:16 Surr

: p-Terphenyl-<:114 VOLATILE ORGANIC COMPOUNDS Benzene Result 18500 < 200 <200 < 0.0050 < 0.020 <0.0050 74.9 < 0 . 010 < 0.00050 < 0.00050 < 0.00050 < 0.020 <0.0010 96.3 64.3 < 100 < 100 < 100 < 100 < 100 < 100 < 500 < 200 < 100 < 100 < 100 101 49.3 60.4 86.7 51.7 38

.8 < 1.0 Sampled By: Client Collection Date: 1/28/2011
1: 10:00 PM Received Date: 1/28/2011 7:08:50 PM QL Q Units DF Date Analyzed EPA200.7 Analyst: MS 10.0 mgllCaC03
10 211/201112

: ?2:00 PM EPA200.8 Analyst: JEK . 200 **~giL**200 21812011 3:03:00 PM 200 **~giL**200 21812011
3 : 03

: 00 PM EPA8151 Analyst: NPT 0.0050 rng/l 100 21312011 10
: 39:30 PM 0 . 020 mg/L 100 21312011 10:39:30 PM 0.0050 mgll 100 21312011 10:39:30 PM 28.5-130 %REC 100 21312011 10:39:30 PM EPA8081 Analyst: NPT 0.010 mg/L
10 21212011
7 : 07:46 PM 0.00050 rng/l
10 21212011
7 : 07:46 PM 0.00050 rng/L
10 21212011
7 : 07

: 46 PM 0.00050 mg/L
10 21212011 7:07:46 PM 0.020 mg/L
10 21212011 7:07:46 PM 0 . 0010 mg/L
10 21212011 7:07:46 PM 5-156 %REC
10 21212011 7:07:46 PM 15.9 - 102 %REC
10 21212()11 7:07

: 46 PM EPA 8270 Analyst: JB 100 **~giL**
10 21412011 6:48

: 00 AM 100 **~**
10 21412011 6:48

: 00 AM 100 **~giL**
10 21412011 6:48:00 AM 100 **~giL**
10 21412011 6:48:00 AM 100 **~ll**
10 21412011 6:48

: 00 AM 100 **~g/L**
10 214/2011 6:48

: 00 AM 500 **~giL**
10 21412011
6 : 48

: 00 AM 200 **~/L**
10 214/2011
6 : 48

: 00 AM 100 **~giL**
10 21412011 6:48:00 AM 100 **~giL**
10 2/412011 6:48

: 00 AM 100 **~giL**
10 2/4/2011
6 : 48

: 00 AM 5-137 %REC
10 21412011 6:48

: 00 AM 27.7-95.1 %REC
10 2/4/2011 6:48:00 AM 5-104 %REC
10 21412011
6 : 48:00 AM 16-101 %REC
10 214/2011 6:48:00 AM 5-106 %REC
10 21412011 6:48:00 AM 25

. 4-133 %REC
10 214/2011 6:48:00 AM EPA 8260 Analyst: SJM 1 .0 **~g/L** 1/3112011 7:02:00 PM --·-

· ----------------------··

------·-· ------------- -----------------------

------ **~ ~** 

**~** u

**~** <

% 1 .0 . 56-00306 PA pEPLaboratory Results Geochemical Testing

Date: 23-Feb-1

I CLIENT: Lab Order: RESOURCE MANAGEMENT SERVICES Gl101912
Client Sample ID: Eckles Well 8590H FB RMS 1/1/28 Project: 26R Analysis Sampled By: Client Lab ID: 01101912-001 Collection Date: 1/28/2011 1:10:00 PM Matrix: AQUEOUS Received Date: 1/28/2011 7:08:50 PM ----·----
------··----···-

-
· ·-----------------------··--··------

-----------···--------------------

····- ·---

-- -··- Analyses Result QL Q Units DF Date Analyzed VOLA TILE ORGANIC COMPOUNDS
EPA 8260 Analyst: SJM Toluene

1.1

1 .0 IJgll 1/3112011 7:02:00 PM Surr

: 1,2-Dichloroethane-<14

108 70-130 o/oREC

1 1/3112011 7:02:00 PM Surr

: 4-Bromofluorobenzene

102 70-130 o/oREC

1 1/3112011 7:02

: 00 PM Surr: Toluene-<18

95

.3 70-130 o/oREC 1/3112011 7:02:00 PM VOLA TILE ORGANIC COMPOUNDS: TCLP EPA 8260 Analyst: JAW Benzene

<50 50 1J91l
50 21312011 4:31:00 AM Carbon Tetrachloride
<50 50 ll91L
50 213/20114:31:00AM Chlorobenzene

<50 50 ll9IL
50 21312011 4:31:00 AM 1, 1-0ichloroethene

<50 50 1-19/L
50 21312011 4:31 :00 AM 1,2-0ichloroethane

<50 50 ll91L
50 213/2011 4:31 :00 AM 1.4-0ichlorobenzene

<50 50 1-19/L
50 21312011 4:31:00AM Trichloromethane

<50 50 ll91L
50 2/312011 4:31 :00 AM Methyl Ethyl Ketone <250 250 ll91L
50 213/2011 4:31:00 AM Tetrachloroethene

<50 50 ll91L
50 213/2011 4:31 :00 AM Trichloroethene

<50 50 1J91l
50 21312011 4:31:00 AM Vinyl Chloride

<50 50 IJ9/L
50 213/2011 4:31:00 AM surr: 1,2-Dichloroethane-d4

90.7 70-130 o/oREC
50 213/2011 4:31:00 AM Surr: 4-Bromofluorobenzene

99.7 70-130 %REC
50 21312011 4:31 :00 AM Surr

: Dibromofluoromethane

92

.0 70-130 o/oREC
50 21312011 4:31:00 AM Surr: Toluene-d8
97.0 70-130 o/oREC
50 21312011
4 : 31:00 AM INDICATOR ORGANIC PARAMETERS
EPA 1664 Analyst: DSZ Oil & Grease

436

5 . mgiL 1.08 21112011
8 : 48

: 00 AM NOTES: J - Unable to obtain a stable weight within specified limits due to sample matrix. Value Is estimated. VOLATILE ORGANIC COMPOUNDS
EPA 8015 Analyst: SUB Ethylene Glycol

< 550 550 mgiL 2/7/2011 RADIOLOGICAL TESTING EPA900.0 Analyst: SUB Gross Alpha 7229 +-1675 3.00 pCill 2110/2011 Gross Beta
1048 +-748 4.00 pCill 2110/2011 RADIOLOGICAL PARAMETERS
EPA 903.1 Analyst: SUB Radium 226 1638 +- 307

1 .00 pCi!L 2118/2011 RADIOLOGICAL PARAMETERS
EPA 904.0 Analyst: SUB Radium 228

199 +- 39.2 1.00 pCi/L 2/18/2011 INORGANICS NON-METALS

EPA 9040 Analyst: RLL Corrosivity Characteristic

6 .55

1 .00 su 1/3112011 FLASH POINT

EPA 1010 Analyst: RLL **~**

+ .,

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% 1.0 . 56-00306 PA DEP P::::tno A nf 7Laboratory Results Geochemical Testing

Date: 23-Feb-11 CLIENT: Lab Order: RESOURCE MANAGEMENT SERVICES G1101912
Client Sample ID: Eckles Well 8590H FB RMS 1/1128 Project: 26R Analysis Lab ID: GIIOI912-001 Matrix: AQUEOUS Analyses FLASH POINT Flash point TCLPZHEEXTRACTION TCLP,ZHE TCLP EXTRACTION Extraction Fluid Used Final pH . Initial pH pH with HCI pH with water TCLP, non-volatile TCLP,ZHE Result >200 RL NA 3 . 1 NA NA NA NA NA Sampled By: Client Collection Date: 112812011 1:10:00 PM Received Date: 112812011 7:08:50 PM . . . .. _.... ------ --
------------- --

--- ···- - - - -- -· --- ·- · QL Q EPA 1010 10.0 EPA 1311 1.0 EPA 1311 0 1.0 1.0 1.0 1.0 0 0 Units "F DF Date Analyzed Analyst: RLL 212/2011 Analyst: Rl:-L 1131/2011 Analyst: RLL 113112011 1/3112011 1/3112011 1 1/3112011 1 113112011 1/3112011 1/3112011 .. - --·--····--
··· ·----···----- -- ···--···-

-------- -·· .. --· · I. D. 56-00306 PA DEP