Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility 

Pearl Harbor, Oahu, Hawaii 

Latitude: 21o

22’15” N 

Longitude: 157o

53’33” W 

HDOH Facility ID No. 9-102271 

HDOH Release ID No. 99051, 010011, 020028 

May 2010 

Prepared by: 

TEC Inc. 

1003 Bishop St. Suite 1505 

Pauahi Tower 

Honolulu, Hawaii 96813 

Prepared for: 

Commander 

Navy Region Hawaii 

Environmental Department, Code N45 

850 Ticonderoga Street, Suite 110 

Pearl Harbor, Hawaii 96860-5101 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility May 2010 

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Table of Contents 

Table of Contents ............................................................................................................................. i

Executive Summary ......................................................................................................................... 1

1.0 Introduction.......................................................................................................................... 3

1.1 Project Objective .............................................................................................................. 3

1.2 Previous Reports .............................................................................................................. 3

1.3 Background ...................................................................................................................... 4

1.3.1 Site Description ......................................................................................................... 4

1.3.2 Facility Information .................................................................................................. 4

1.3.3 UST Information ....................................................................................................... 4

1.4 Previous Environmental Investigations ............................................................................ 4

1.5 Regulatory Updates .......................................................................................................... 8

1.6 RHMW05 Installation ...................................................................................................... 8

2.0 Sample Collection and Analyses .......................................................................................... 8

2.1 Monitoring Well Purging ................................................................................................. 8

2.2 Groundwater Sample Collection ...................................................................................... 9

2.3 Groundwater Sample Analyses ........................................................................................ 9

3.1 April 2010 Sample Analytical Results ............................................................................. 9

3.2 Groundwater Contaminant Trend ................................................................................... 11

3.3 Results of Oil/Water Interface Measurements ............................................................... 13

3.4 Groundwater Status ........................................................................................................ 14

4.0 Summary and Conclusions ................................................................................................. 17

5.0 References .......................................................................................................................... 21

List of Tables 

Table 1 Analytical Results for Quarterly Groundwater Sampling Release Response Report ..10 

Table 2 Oil/Water Interface Measurements ..............................................................................13 

Table 3 Action Levels for Compounds of Concern ..................................................................14 

Table 4 Results Categories and Responses to Groundwater Monitoring Results .....................15 

List of Figures 

Figure 1 TPH Trends in Groundwater, Round 19 (April 13, 2010) ...........................................19 

Figure 2 PAH Trends in Groundwater, Round 19 (April 13, 2010) ..........................................20 

List of Appendices 

Appendix A – Laboratory Analytical Reports 
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Executive Summary 

Introduction

There are 18 active and two inactive, 12.5 million gallon, field-constructed underground storage 

tanks (USTs) located at the Red Hill Fuel Storage Facility (the Facility). Previous environmental 

site investigations indicated a release has occurred and contaminated the groundwater underlying 

the Facility. 

The United Stated (US) Navy implemented a groundwater monitoring program, which includes 

collecting groundwater samples quarterly from US Navy Well 2254-01 (RHMW2254-01) and 

four wells installed in the Facility lower access tunnel (RHMW01, RHMW02, RHMW03, and 

RHMW05). The US Navy Well 2254-01 is located approximately 3,000 feet downgradient from 

the Facility and provides approximately 24 percent of the potable water to the Pearl Harbor 

Water System (PHWS). The groundwater samples were analyzed for petroleum constituents and 

compared against State of Hawaii Department of Health (HDOH) Drinking Water 

Environmental Action Levels (EALs) (HDOH, 2008). 

This groundwater monitoring report presents the analytical results and compares them to HDOH 

Drinking Water EALs for samples collected on April 13, 2010. Contaminant trends that have 

exceeded HDOH Drinking Water EALs are also provided in this report. 

April 2010 Sampling Event Results 

Laboratory analytical results from the April 2010 sampling event indicate Total Petroleum 

Hydrocarbons (TPH) as Diesel Range Organics (TPH-DRO), Polynuclear Aromatic 

Hydrocarbons (PAHs), and Volatile Organic Hydrocarbons (VOCs) are present in the 

groundwater beneath the Facility at concentrations that exceed HDOH Drinking Water EALs. 

Specifically, TPH-DRO was detected in RHMW01 at 377F μg/L [F indicates that the compound 

was identified, but the concentration was above the laboratory method detection limit (MDL) and 

below the reporting limit (RL), therefore is considered an estimate]. At RHMW02, TPH-DRO 

was detected at 2,215 μg/L (i.e., the average of normal and duplicate samples). The HDOH 

Drinking Water EAL for TPH-DRO is 210 μg/L. Also during the April 2010 sampling event, 1-

methylnaphthalene was detected at RHMW02 above the HDOH Drinking Water EAL at an 

average concentration of 6.26 μg/L (HDOH Drinking Water EAL is 4.7 μg/L). Naphthalene was 

also detected at RHMW02 above the HDOH Drinking Water EAL at an average concentration of 

21 μg/L (HDOH Drinking Water EAL is 17 μg/L). 

Conversely, during the April 2010 sampling event at RHMW2254-01 and RHMW03, no 

compounds were detected above the laboratory MDLs. In addition, at RHMW05, only trace 

concentrations of 1-methylnaphthalene and Naphthalene were detected at concentrations 

significantly below the respective HDOH Drinking Water EALs. 

TPH-DRO Contaminant Trends 

Regarding TPH-DRO contaminant trends, since January 2008, TPH-DRO at RHMW01 has 

fluctuated between the historical range established from September 2005 through September 
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2007. At RHMW02, TPH-DRO concentrations were relatively stable prior to 2008, after which 

significant variations in the measured concentrations occurred. However, in April 2010 at 

RHMW02, TPH-DRO showed a decrease in concentration approaching the lower end of its 

historical range. Since February 2009, TPH-DRO at RHMW03 has not been detected above the 

MDL. At RHMW05, TPH-DRO had been increasing since it was first sampled in May 2009. 

However, in April 2010, TPH-DRO at RHMW05 was not detected above the laboratory MDL. 

Other Contaminant Trends

Regarding other contaminant trends, the concentrations of three PAHs detected at RHMW02 are 

discussed. Since October 2008, the concentration of 2-methylnaphthalene has remained below 

the HDOH Drinking Water EAL. In addition, Naphthalene and 1-methylnaphthalene 

concentrations decreased to below the HDOH Drinking Water EALs in May 2009 and October 

2009, respectively. However, concentrations for Naphthalene and 1-methylnaphthalene have 

since increased and remained just above their respective HDOH Drinking Water EALs through 

the April 2010 sampling event. 

Summary

At RHMW01 and RHMW02, TPH-DRO concentrations have fluctuated, but remain within their 

historical ranges. At RHMW03 and RHMW2254-01 during April 2010, no compounds were 

detected above laboratory MDLs. At RHMW05, as of the April 2010 sampling, the TPH-DRO 

concentration drastically decreased to below the laboratory MDL. Finally, no light-non aqueous 

phased liquid (LNAPL), otherwise known as “free product”, has been observed in any of the 

Facility groundwater monitoring wells since January 2008. 

Based on the results of the April 2010 sampling event, continued quarterly groundwater 

monitoring is warranted so that overall groundwater quality trends may be observed and 

proactive action taken if the groundwater quality shows evidence of deterioration. In addition, 

monthly oil/water interface measurements and soil vapor monitoring should continue within the 

Facility. Although the US Navy Well 2254-01 is not imminently threatened at this time, 

monitoring should continue to assess contaminant migration from up-gradient locations. 

 
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Red Hill Fuel Storage Facility May 2010 

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1.0 Introduction

This report presents the results of the 19th groundwater sampling event, conducted in April 2010 

at the Red Hill Fuel Storage Facility, Oahu, Hawaii (hereafter referred to as “the Facility”). The 

Facility consists of 18 active and two inactive underground storage tanks (USTs) operated by the 

Fleet and Industrial Supply Center (FISC), Pearl Harbor. The groundwater sampling and 

analysis event is part of a groundwater monitoring program for the UST site in response to past 

UST releases, previous environmental investigations, and recommendations from the State of 

Hawaii Department of Health (HDOH). 

1.1 Project Objective 

This groundwater sampling project was performed to evaluate the presence of chemicals of 

potential concern in groundwater underlying the Facility. The project was conducted to ensure 

the Navy remains in compliance with HDOH UST release response requirements as described in 

Hawaii Administrative Rules (HAR) 11-281 Subchapter 7, Release Response Action. The 

groundwater sampling program followed the procedures described in Red Hill Bulk Fuel Storage 

Facility Groundwater Protection Plan [TEC Inc. (TEC), 2008 updated in 2009], also referred to 

as “the Plan”. 

This groundwater sampling event was conducted by TEC under United States (US) Navy 

Contract Number N47408-04-D-8514, Task Order No. 54. 

1.2 Previous Reports 

The following groundwater monitoring reports were previously submitted to the HDOH: 

1. Groundwater Sampling Report, First Quarter 2005 (submitted April 2005); 

2. Groundwater Sampling Report, Second Quarter 2005 (submitted August 2005); 

3. Groundwater Sampling Report, Third Quarter 2005 (submitted November 2005); 

4. Groundwater Sampling Report, Fourth Quarter 2005 (submitted February 2006); 

5. Groundwater Monitoring Results, July 2006 (submitted September 2006); 

6. Groundwater Monitoring Results, December 2006 (submitted January 2007); 

7. Groundwater Monitoring Results, March 2007 (submitted May 2007); 

8. Groundwater Monitoring Results, June 2007 (submitted August 2007); 

9. Groundwater Monitoring Results, September 2007 (submitted October 2007); 

10. Groundwater Monitoring Results, January 2008 (submitted March 2008); 

11. Groundwater Monitoring Results, April 2008 (submitted May 2008); 

12. Groundwater Monitoring Results, July 2008 (submitted October 2008); 

13. Groundwater Monitoring Results, October and December 2008 (submitted February 

2009); 
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14. Groundwater Monitoring Results, February 2009 (submitted May 2009); 

15. Groundwater Monitoring Results, May 2009 (submitted July 2009); 

16. Groundwater Monitoring Results, July 2009 (submitted September 2009); 

17. Groundwater Monitoring Results, October 2009 (submitted December 2009); and 

18. Groundwater Monitoring Results, January, February, and March 2010 (submitted April 

2010). 

1.3 Background 

The following sections provide a description of the site and information on the Facility and USTs. 

1.3.1 Site Description 

The Facility is located in Red Hill, Oahu, Hawaii. Land adjacent to the north of the Facility is 

occupied by Halawa Correctional Facility and private businesses. Land to the south and west of 

the Facility includes the Coast Guard Reservation. Moanalua Valley is located east of the 

Facility (Dawson, 2006). 

The Navy Public Works Department operates a potable water infiltration tunnel approximately 

1,550 feet downgradient from the Facility (Dawson, 2006). The US Navy Well 2254-01 is 

located approximately 3,000 feet down-gradient (west) of the Facility and provides 

approximately 24% of the potable water to the Pearl Harbor Water System (PHWS), which 

serves approximately 52,200 military consumers (TEC, 2008). 

1.3.2 Facility Information 

The Facility consists of 18 active and two inactive USTs operated by Navy FISC Pearl Harbor. 

Each UST has a capacity of 12.5 million gallons. The bottom of the USTs is located 

approximately 100 feet above the basal aquifer (Dawson, 2006). 

1.3.3 UST Information 

The USTs were constructed in the early 1940s. The tanks were fabricated from steel and 

currently contain Jet Propulsion (JP)–5 fuel, JP-8, and F-76 (diesel marine fuel). Previously, 

several tanks stored Navy Special Fuel Oil, Navy Distillate, aviation gasoline, and motor 

gasoline. Each tank measures approximately 245 feet in height and 100 feet in diameter. The 

upper domes of the tanks lie at depths varying between approximately 100 feet and 200 feet 

below the existing ground surface (TEC, 2006). 

1.4 Previous Environmental Investigations 

1998 to 2001: From 1998 to 2001, the Navy conducted an investigation at the Facility to assess 

potential releases from the fuel storage USTs and piping systems. In February 2001, the Navy 

installed a one-inch diameter RHMW01 (previously known as MW-V1D) to monitor for 

contamination of the basal aquifer underlying the Facility. The well was installed and completed 

at approximately 100 feet below grade within the lower access tunnel. At the time of well 

completion, depth to water in RHMW01 was measured at 86 feet below grade (Dawson, 2006). 
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In February 2001, groundwater samples collected from RHMW01 contained total petroleum 

hydrocarbons (TPH) concentrations ranging from 883 micrograms per liter (g/L) to 1,050 g/L 

and total lead ranging from 10.4 g/L to 15 g/L. The maximum total lead concentration in the 

samples was equal to the primary drinking water standard of 15 g/L for lead and exceeded the 

HDOH Tier 1 groundwater action level of 5.6 g/L (Dawson, 2006). 

2005 – Groundwater Sampling: The Navy began quarterly groundwater sampling at existing 

monitoring wells in 2005. Dawson Group, Inc. collected groundwater samples from RHMW01 

and the Red Hill Navy Pump Station (US Navy Well 2254-01) in February, June, September, and 

December 2005. 

Samples collected in February and June 2005 were not filtered in the field prior to analysis for 

lead. Analytical results for samples collected from RHMW01 indicated concentrations of total 

lead were above the HDOH Tier 1 action level of 5.6 g/L. The results were not considered 

appropriate for risk assessment since the sample had not been filtered. In addition, lead was not 

a component of fuels from the tanks near RHMW01, but was a component is fuels stored in other 

tanks during the history of the Facility. Lead may have been part of the Facility construction 

material (TEC, 2007). Previous sampling efforts showed elevated lead when analyzed as 

unfiltered samples. Subsequent efforts where the lead samples were filtered has resolved this 

issue. 

Samples were filtered in September and December 2005, and dissolved lead concentrations were 

below the HDOH Tier 1 action level. Concentrations of all other contaminants of potential 

concern were below HDOH Tier 1 action levels. 

2005 – Site Investigation: As part of a site investigation, TEC installed three groundwater 

monitoring wells at the Facility between June and September 2005. Well RHMW02 was 

installed in the lower access tunnel near Tanks 5 and 6. Well RHMW03 was installed in the 

lower access tunnel near Tanks 13 and 14. Well RHMW04 was installed north of UST tank 20 

to provide contaminant chemistry data for water moving through the basal aquifer beneath the 

Facility. Wells RHMW02 and RHMW03 were completed to depths of approximately 125 feet 

below the tunnel floor, and well RHMW04 was completed to a depth of approximately 300 feet 

below ground surface outside the tunnel. Groundwater samples were collected from the three 

newly installed wells and two existing wells (RHMW01 and RHMW2254-01) in September 

2005. 

Naphthalene and trichloroethylene were detected in samples collected from RHMW02 at 

concentrations greater than the HDOH Tier 1 action levels. Lead was detected in the sample 

collected from RHMW01 at a concentration greater than the HDOH Tier 1 action level; 

however, the sample was not filtered in the field prior to analysis. Analytical results for filtered 

samples obtained by Dawson during the same period indicated concentrations of dissolved lead 

were below the HDOH Tier 1 action level. 

2006 – Site Investigation: Dedicated sampling pumps were installed in five wells (RHMW01, 

RHMW02, RHMW03, RHMW04, and US Navy Well 2254-01). TEC collected groundwater 
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samples from the wells in July 2006. The groundwater samples were analyzed for petroleum 

constituents. Naphthalene was detected in samples collected from RHMW02 at concentrations 

above the HDOH Tier 1 action level. 

In September 2005, with concurrence from the HDOH, the Navy decided to use the newer 

HDOH Environmental Action Levels (EALs) for the Red Hill Site Investigation and Risk 

Assessment project. The EALs provide action levels for more chemicals, and are more useful 

for conducting screening risk assessments. Since the HDOH (HDOH May 2005) Policy Letter 

stated that the two sets of action levels should not be mixed, the Tier 1 screening levels presented 

in HAR Section 11-281-78 would no longer be used to evaluate environmental impact at the 

Facility. 

An overall summary of Facility groundwater sampling data by year follows: 

2006 – Groundwater Sampling: Groundwater samples were collected in December 2006. 

Analytical results indicated the following: 

 No chemicals were detected in groundwater from US Navy Well 2254-01 or RHMW03; 

 TPH as diesel range organics (TPH-DRO) was detected in groundwater above the HDOH 

Drinking Water EALs in RHMW01; and 

 TPH as gasoline range organics (TPH-GRO), TPH-DRO, and naphthalene were detected 

in groundwater above the HDOH Drinking Water EALs in RHMW02. 

2007 – Groundwater Sampling: Groundwater samples were collected in March, June, and 

September 2007. Analytical results indicated the following: 

 No chemicals were detected above HDOH Drinking Water EALs at US Navy Well 

2254-01; 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW01 during all three 

sampling events; 

 TPH-GRO exceeded HDOH Drinking Water EALs at RHMW02 in March; 

 TPH-DRO and naphthalene exceeded HDOH Drinking Water EALs at RHMW02 during 

all three sampling events; 

 1-methylnaphthalene and 2-methylnaphthalene exceeded the HDOH Groundwater Gross 

Contamination EAL at RHMW02 during all three sampling events; and 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW03 in June. 

2008 – Groundwater Sampling: Groundwater samples were collected in January, April, July, 

and October 2008. Analytical results indicated the following: 

 No chemicals were detected above HDOH Drinking Water EALs at US Navy Well 

2254-01; 

 Trace detections of 1-methylnaphthalene and naphthalene prompted a resample event in 

December at US Navy Well 2254-01, no chemicals were detected above the laboratory 

method detection limit (MDL); 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW01 during all four sampling 

events; 

 TPH-GRO did not exceed HDOH Drinking Water EALs at RHMW02; 
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 TPH-DRO, naphthalene, 1-methylnaphthalene, and 2-methylnaphthalene exceeded 

HDOH Drinking Water EALs at RHMW02. Additionally, the SSRBL of 4,500 g/L for 

TPH-DRO was exceed in the October sampling event; and 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW03 during all four sampling 

events. 

2009 – Groundwater Sampling: Groundwater samples were collected in February, May, July, 

and October 2009. Analytical results indicated the following: 

 No chemicals have been detected above HDOH Drinking Water EALs at US Navy Well 

2254-01; 

 Trace TPH-GRO at US Navy Well 2254-01 was detected above the laboratory MDL and 

significantly below the laboratory reporting limit and HDOH Drinking Water EAL, in 

February and May 2009; 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW01 during all four sampling 

events; 

 TPH-GRO has not exceed HDOH Drinking Water EALs at RHMW02; 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW02 during all four sampling 

events; 

 Naphthalene, 1-methylnaphthalene, and 2-methylnaphthalene exceeded HDOH Drinking 

Water EALs at RHMW02 in February 2009, however only 1-methylnaphthalene 

exceeded the HDOH Drinking Water EALs in May and July 2009 and only naphthalene 

exceeded the HDOH Drinking Water EAL in October 2009; 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW03 in February, but not in 

May, July, or October; and 

 TPH-DRO exceeded HDOH Drinking Water EAL at RHMW05 during the July and 

October 2009 sampling events. 

2010 – Groundwater Sampling: Groundwater samples were collected in January 2010 (and 

TPH-DRO was resampled for at RHMW02 in February and March, 2010). Analytical results 

indicated the following: 

 No chemicals have been detected above HDOH Drinking Water EALs at US Navy Well 

2254-01; 

 Trace naphthalene at US Navy Well 2254-01 was detected above the laboratory MDL 

and significantly below the laboratory reporting limit and HDOH Drinking Water EAL, 

in January; 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW01; 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW02 in January, February, 

and March, however, significant increases in January and February were attributed to 

tentatively identified compounds (TICs) apparently not associated with petroleum from 

the Facility; 

 Naphthalene and 1-methylnaphthalene exceeded HDOH Drinking Water EALs in 

RHMW02 in January; 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW05 in January, however, 

the significant increase was attributed to TICs apparently not associated with petroleum 

from the Facility; and 
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 TPH-DRO at RHMW03 has not been detected above the laboratory MDL. 

1.5 Regulatory Updates 

During the summer and fall of 2008, HDOH updated their EALs, which resulted in significant 

changes to the action levels associated with methylnaphthalenes. The drinking water toxicity 

EAL for these compounds was 240 g/L. This concentration presumed that methylnaphthalenes 

were non-carcinogenic. Evidence that they are human carcinogens has now been accepted by the 

US Environmental Protection Agency (USEPA). As a result, HDOH adopted more rigorous 

EALs of 4.7 g/L for 1-methylnaphthalene and 24 g/L for 2-methylnaphthalene, corresponding 

to a residential tap water scenario, and a 1 in a million cancer risk (HDOH, 2008). 

Also, the drinking water EAL for naphthalene was increased from 6.2 g/L to 17 g/L (HDOH, 

2008). Finally, the HDOH Drinking Water EAL for TPH-DRO was increased from 100 g/L to 

210 g/L, although the HDOH Groundwater Gross Contamination EAL for TPH-DRO remains 

100 g/L. 

1.6 RHMW05 Installation 

In April 2009, a new groundwater monitoring well, RHMW05, was installed by TEC under US 

Navy Contract Number N47408-04-D-8514, Task Order No. 54. RHMW05 is located within the 

lower access tunnel between RHMW01 and RHMW2254-01(located at the US Navy Well 2254-

01). It was installed to identify any contamination migrating past RHMW01 prior to it reaching 

the US Navy Well 2254-01. 

2.0 Sample Collection and Analyses 

Field activities relating to groundwater sample collection were conducted on April 13, 2010. 

Groundwater samples were collected from four monitoring wells located inside the Facility 

lower access tunnel and one monitoring well located at the US Navy Pump Station. Sampling 

and analysis were conducted according to Red Hill Bulk Fuel Storage Facility Groundwater 

Protection Plan (TEC, 2009). A total of eight samples were collected as follows: 

 one environmental sample from RHMW2254-01 (i.e., located at the US Navy Well 

2254-01), RHMW01, RHMW02, RHMW03, and RHMW05; 

 one duplicate sample from RHMW02 (sampled as RHMWA01 and reported as 

RHMW02D); and 

 one matrix spike and matrix spike duplicate from RHMW2254-01. 

2.1 Monitoring Well Purging

All groundwater monitoring wells were purged and sampled using a dedicated pump system. 

Well purging was considered complete when no less than three successive water quality 

parameter measurements had stabilized within approximately 10 percent. Field parameters were 

measured at regular intervals during well purging and included pH, temperature, specific 

conductivity, dissolved oxygen, and turbidity. Purge water was collected and disposed in the 

Facility oil/water separator system. 
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2.2 Groundwater Sample Collection 

Each monitoring well was sampled immediately following purging. All wells were sampled 

directly from their dedicated bladder pump system. Samples were placed into sampling 

containers with appropriate preservatives [i.e., hydrochloric acid (HCl) for volatile organic 

analysis, nitric acid (HNO3) for dissolved lead]. Dissolved lead samples were filtered in the field 

and placed in preserved bottles. Sample containers were labeled with the date, sample 

identification number, type of analysis, and sampler’s name. The containers were placed on ice 

in sample coolers and transported under chain-of-custody procedures to the certified laboratory 

for analysis. 

2.3 Groundwater Sample Analyses 

Groundwater samples were analyzed by SGS Environmental Service, Inc. in Anchorage, Alaska 

for TPH-DRO and TPH-GRO by EPA Method 8015B, VOCs by EPA Method 8260B, PAHs by 

EPA Method 8270C SIM, and dissolved lead by EPA Method 6020. 

3.0 Groundwater Sample Analytical Results 

This section provides a summary of analytical results for groundwater samples collected from 

four monitoring wells located in the lower access tunnel of the Facility and one monitoring well 

located at the US Navy Pump Station. Duplicate sample results from monitoring well RHMW02 

are reported in this document as RHMW02D. A summary of groundwater analytical results for 

TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved lead is included in Table 1. Complete 

analytical laboratory reports are provided in Appendix A. 

3.1 April 2010 Sample Analytical Results 

Groundwater samples were analyzed for TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved 

lead. Data qualifier “F” indicates the result is between the laboratory MDL and reporting limit 

(RL), therefore, should be considered an estimated value. The results for each groundwater 

monitoring well are discussed below. 

RHMW01

TPH-DRO at 377F μg/L exceeded the HDOH Drinking Water EALs of 210 μg/L. Estimated 

trace concentrations of acenaphthene and flourene were detected at 0.045F μg/L and 0.0455F 

μg/L, respectfully (Table 1). These concentrations are significantly below the HDOH Drinking 

Water EALs for each constituent. No other constituents were detected above the laboratory 

MDL. 
Table 1. Analytical Results for Quarterly Groundwater Monitoring Release Response Report (April 13, 2010)

Red Hill Fuel Storage Facility, Pearl Harbor, Hawaii

Result Q MDL RL Result Q MDL RL Result Q MDL RL Result 

TPH as DIESEL RANGE ORGANICS 210 100 377 F 163 435 2350 160 426 2080 161 430 ND 

TPH as GASOLINE RANGE ORGANICS 100 100 ND U 30 100 39.3 F 30 100 39 F 30 100 ND 1-METHYLNAPHTHALENE 4.7 10 ND U 0.0161 0.0538 6.61 0.161 0.538 5.9 0.165 0.549 ND 2-METHYLNAPHTHALENE 24 10 ND U 0.0161 0.0538 1.69 0.161 0.538 1.9 0.0165 0.0549 ND ACENAPHTHENE 370 20 0.045 F 0.0161 0.0538 0.426 0.0161 0.0538 0.429 0.0165 0.0549 ND ACENAPHTHYLENE 240 2000 ND U 0.0161 0.0538 ND U 0.0161 0.0538 ND U 0.0165 0.0549 ND 

ANTHRACENE 1800 22 ND U 0.0161 0.0538 ND U 0.0161 0.0538 ND U 0.0165 0.0549 ND 

BENZO(a)ANTHRACENE 0.092 4.7 ND U 0.0161 0.0538 ND U 0.0161 0.0538 ND U 0.0165 0.0549 ND 

BENZO(a)PYRENE 0.2 0.81 ND U 0.0161 0.0538 ND U 0.0161 0.0538 ND U 0.0165 0.0549 ND 

BENZO(b)FLUORANTHENE 0.092 0.75 ND U 0.0161 0.0538 ND U 0.0161 0.0538 ND U 0.0165 0.0549 ND 

BENZO(g,h,i)PERYLENE 1500 0.13 ND U 0.0161 0.0538 ND U 0.0161 0.0538 ND U 0.0165 0.0549 ND 

BENZO(k)FLUORANTHENE 0.92 0.4 ND U 0.0161 0.0538 ND U 0.0161 0.0538 ND U 0.0165 0.0549 ND 

CHRYSENE 9.2 1 ND U 0.0161 0.0538 ND U 0.0161 0.0538 ND U 0.0165 0.0549 ND DIBENZ(a,h)ANTHRACENE 0.0092 0.52 ND U 0.0161 0.0538 ND U 0.0161 0.0538 ND U 0.0165 0.0549 ND FLUORANTHENE 1500 130 ND U 0.0161 0.0538 ND U 0.0161 0.0538 ND U 0.0165 0.0549 ND 

Method

HDOH Drinking Water 

EALs1

for Human Toxicity 

UG/L

HDOH Groundwater 

Gross Contamination 

EALs2

UG/L

Chemical

RHMW01

UG/L

RHMW02

UG/L

RHMW02D

UG/L

8015B (Petroleum)

8270C SIM 

(PAHs)

April 13, 2010 April 13, 2010 April 13, 2010

FLUORENE 240 950 0.0455 F 0.0161 0.0538 0.224 0.0161 0.0538 0.23 0.0165 0.0549 ND INDENO(1,2,3-c,d)PYRENE 0.092 0.095 ND U 0.0161 0.0538 ND U 0.0161 0.0538 ND U 0.0165 0.0549 ND NAPHTHALENE 17 21 ND U 0.0333 0.108 14.3 0.333 1.08 12.7 0.341 1.1 ND PHENANTHRENE 240 410 ND U 0.0161 0.0538 ND U 0.0161 0.0538 ND U 0.0165 0.0549 ND 

PYRENE 180 68 ND U 0.0161 0.0538 ND U 0.0161 0.0538 ND U 0.0165 0.0549 ND 1,1,1,2-TETRACHLOROETHANE 0.52 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND 1,1,1-TRICHLOROETHANE 200 970 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 1,1,2,2-TETRACHLOROETHANE 0.067 500 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND 1,1,2-TRICHLOROETHANE 5 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 1,1-DICHLOROETHANE 2.4 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 1,2,3-TRICHLOROPROPANE (TCP) 0.6 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 1,2,4-TRICHLOROBENZENE 70 3000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 1,2-DIBROMO-3-CHLOROPROPANE (DBCP) 0.04 10 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND 1,2-DIBROMOETHANE (EDB) 0.0065 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 1,2-DICHLOROBENZENE 600 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 1,2-DICHLOROETHANE 0.15 7000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND 1,2-DICHLOROPROPANE 5 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 1,3-DICHLOROBENZENE 180 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 1,4-DICHLOROBENZENE 75 5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND ACETONE 22000 20000 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND BENZENE 5 170 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND 

BROMODICHLOROMETHANE 0.22 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND BROMOFORM 100 510 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND BROMOMETHANE 8.7 50000 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3 ND CARBON TETRACHLORIDE 5 520 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND CHLOROBENZENE 100 50 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND CHLOROETHANE 8600 16 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND CHLOROFORM 70 2400 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1 ND CHLOROMETHANE 1.8 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND cis-1,2-DICHLOROETHYLENE 70 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND cis-1,3-DICHLOROPROPENE 0.43 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND DIBROMOCHLOROMETHANE 0.16 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND ETHYLBENZENE 700 30 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND HEXACHLOROBUTADIENE 0.86 6 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND M,P-XYLENE (SUM OF ISOMERS) 10000 20 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND METHYL ETHYL KETONE (2-BUTANONE) 7100 8400 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND METHYL ISOBUTYL KETONE (4-METHYL-2-PENTANONE) 2000 1300 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND METHYLENE CHLORIDE 4.8 9100 ND U 1 5 ND U 1 5 ND U 1 5 ND NAPHTHALENE 17 21 ND U 0.62 2 20.6 0.62 2 21.4 0.62 2 ND 

STYRENE 100 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND TETRACHLOROETHYLENE(PCE) 5 170 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND TOLUENE 1000 40 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND t 1 2 DICHLOROETHENE 100 260 ND U 0 31 1 ND U 0 31 1 ND U 0 31 1 ND 

8260B 

(VOCs)

trans-1,2-DICHLOROETHENE 100 260 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND TRICHLOROETHYLENE (TCE) 5 310 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND VINYL CHLORIDE 2 3400 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND XYLENES, TOTAL 10000 20 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3 ND 

6020 LEAD 15 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 

PAHs - Polynuclear aromatic hydrocarbons MDL - Method detection limit

VOCs - Volatile organic compounds RL - Reporting limit

UG/L - Micrograms per Liter TPH - Total petroleum hydrocarbons 

Q - Data qualifier ND - Indicates that the compound was not detected above the stated method dete

U - Indicates that the compound was analyzed for but not detected at or above the stated limit NA - not analyzed

F - Indicates that the compound was identified but the concentration was above the MDL and below the RL

- Result exceeds one or both HDOH EALs

12

Final Drinking Water Action Levels for Human Toxicity, Table D-3a, Screening for Environmental Concerns at Sites with Contaminated Soil and Groundwater , HDOH, 2009Groundwater Gross Contamination Action Levels, Table G-1, Screening for Environmental Concerns at Sites with Contaminated Soil and Groundwater , HDOH, 2009

200

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Red Hill Fuel Storage Facility May 2010 

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11 

RHMW02

In April 2010, TPH-DRO was detected in RHMW02 in the normal and duplicate samples at 

2,350 μg/L and 2,080 μg/L, respectively. These results exceeded the HDOH Drinking Water 

EAL of 210 μg/L, but not the site-specific risk based level (SSRBL) of 4,500 μg/L. The average 

concentration between the normal and duplicate samples for TPH-DRO was 2,215 μg/L, slightly 

less than half of the SSRBL. The concentration of TPH-GRO detected in the normal and 

duplicate sample from RHMW02 averaged 39.2F μg/L, less than the HDOH Drinking Water 

EAL of 100 μg/L. 

Naphthalene was analyzed by USEPA Method 8270C SIM and USEPA Method 8260B. USEPA 

Method 8260B produced the highest naphthalene concentrations, which averaged 21 μg/L from 

the normal and duplicate sample (HDOH Drinking Water EAL is 17 μg/L). In addition, 1-

methylnaphthalene, 2-methylnaphthalene, acenaphthene, and flourene were detected in the 

normal and duplicate samples at averaged concentrations of 6.26 μg/L, 1.795 μg/L, 0.428 μg/L, 

and 0.227 μg/L, respectively (Table 1). All of these concentrations are below the HDOH 

Drinking Water EALs for each constituent, except for 1-methylnaphthalene (HDOH Drinking 

Water EAL is 4.7 μg/L). No other constituents were detected above the laboratory MDL.

RHMW03

No parameters were detected above the laboratory MDLs in RHMW03 (Table 1). 

RHMW05

1-methylnaphthalene and naphthalene were detected above the laboratory MDL, but below the 

RL, at estimated concentrations of 0.0335F μg/L and 0.0752F μg/L, respectively. These 

concentrations are below the HDOH Drinking Water EAL for each compound. No other 

constituents were detected above the laboratory MDL (Table 1). 

US Navy Well 2254-01

No parameters were detected above the laboratory MDLs in RHMW2254-01 (Table 1). 

3.2 Groundwater Contaminant Trend 

Groundwater samples have been collected and analyzed by TEC since September 2005. Figure 1 

shows TPH trends in groundwater at the Facility. Figure 2 shows PAH trends in groundwater at 

the Facility. In these figures, open icons (without data) represent locations where the compounds 

being analyzed were not detected. 

The following is a discussion of compounds that exceeded HDOH Drinking Water EALs during 

two or more recent consecutive sampling events of increasing or decreasing concentrations, thus 

establishing a trend: 

 

RHMW01

At RHMW01, concentrations of TPH-DRO have been greater than the HDOH Drinking Water 

EAL since September 2005, but less than 25 percent of the SSRBL of 4,500 g/L. TPH-DRO 

had exhibited a decreasing trend since October 2008 with the lowest concentration (i.e., 248 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility May 2010 

 ____________________________________________________________________________________________ 

12 

μg/L) recorded in July 2009. Since July 2009, this trend began increasing with 299F μg/L, 312F 

μg/L, and 377 μg/L detected in October 2009, January 2010, and April 2010, respectively. 

RHMW02

At RHMW02, from September 2005 through February 2009, TPH-DRO exceeded the HDOH 

Drinking Water EAL and was greater than 50 percent of the SSRBL (estimated solubility limit of 

4,500 g/L). Specifically, the concentration of TPH-DRO was relatively stable at RHMW02 

until July 2008, ranging from 2,250 to 2,995 μg/L. However, during the July and October 2008 

sampling events, these average concentrations increased. The July 2008 average concentration 

was 4,055 μg/L and the October 2008 average concentration was 5,420 μg/L. Both of these 

values were significantly above the HDOH Drinking Water EAL of 210 μg/L, with the October 

2008 average also exceeding the SSRBL of 4,500 μg/L. 

However, TPH-DRO at RHMW02 had shown a decreasing trend from October 2008 through 

July 2009. In May and July 2009, TPH-DRO remained above the HDOH Drinking Water EAL, 

but was below 50 percent of the SSRBL of 4,500 μg/L. In October 2009, TPH-DRO began an 

increasing trend greater than 50 percent of the SSRBL which continued through February 2010 

when it exceeded the SSRBL due to tentatively identified compounds (TICs) apparently not 

associated with petroleum from the Facility (TEC, 2010). In March and April 2010, TPH-DRO 

has exhibited a decreasing trend and the TICs detected in the two previous sampling events were 

not observed. During April 2010, TPH-DRO concentrations at RHMW02 decreased to an 

averaged concentration of 2,215 μg/L, just below 50 percent of the SSRBL. 

 

For other parameters, the average concentration for 1-methylnaphthalene (i.e., 6.26 g/L) 

exhibited a decrease from the January 2010 average concentration (i.e., 8.65 g/L) that was 

above the HDOH Drinking Water EAL of 4.7 g/L. Naphthalene had shown an increasing trend 

since its lowest concentration in May 2009. However since October 2009, average naphthalene 

concentrations in RHMW02 have remained relatively stable between 20 μg/L and 22 μg/L, 

exceeding the HDOH Drinking Water EAL of 17 μg/L. 

RHMW03

At RHMW03, historically, concentrations of TPH-DRO have fluctuated around the HDOH 

Drinking Water EAL, but have been significantly lower than corresponding values observed at 

RHMW01 and RHMW02. However, the measured concentrations decreased since October 2008 

dropping below the laboratory MDL in May 2009. There has been no detectable TPH-DRO 

result since May 2009. 

RHMW05

At RHMW05 there has been an increasing trend for TPH-DRO since it was first sampled in May 

2009. Since July 2009, TPH-DRO concentrations at RHMW05 were greater than the HDOH 

Drinking Water EAL (i.e., 210 μg/L). However, in April 2010 TPH-DRO concentrations 

exhibited a significant decrease and was not detected above the laboratory MDL. 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility May 2010 

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13 

US Navy Well 2254-01

At US Navy Well 2254-01, no compounds were detected above the laboratory MDLs during 

April 2010. Additionally, no compounds have ever been detected at this sample location at 

concentrations greater than any HDOH Drinking Water EALs. 

3.3 Results of Oil/Water Interface Measurements 

The presence and thickness of light-non aqueous phased liquids (LNAPL), otherwise known as 

“free product”, released from the USTs is monitored at the Facility (see Table 2). Static water 

levels and fuel thickness is measured to a precision of ± 0.01 feet. 

In January 2008, fuel was measured in monitoring wells RHMW01 and RHMW02 at a thickness 

of less than 0.01 ft, but has not been observed in other monitoring wells. Measurements to 

determine the presence and thickness of fuel were conducted at RHMW01, RHMW02, 

RHMW03, and RHMW05 following the April 2010 sampling round. Since January 2008, no 

free product has been observed in any of these Facility wells (Table 2). 

Table 2. Oil/Water Interface Measurements 

            

Date 

RHMW01 RHMW02 RHMW03 RHMW05 

SWL 

(ft) 

LNAPL 

(ft) 

SWL 

(ft) 

LNAPL 

(ft) 

SWL 

(ft) 

LNAPL 

(ft) 

SWL6 

(ft) 

LNAPL 

(ft) 

 January 2008 17.74 < 0.01 18.78 < 0.01 NT1 NT1 ---- ---- 

 July 2008 19.04 0.00 18.91 0.00 18.86 0.00 ---- ---- 

October 2008 18.61 0.00 18.56 0.00 18.82 0.00 ---- ---- 

November 2008 18.50 0.00 18.45 0.00 18.51 0.00 ---- ---- 

January 2009 19.28 0.00 19.22 0.00 19.27 0.00 ---- ---- 

February 2009 NT2 NT2 18.66 0.00 18.75 0.00 ---- ---- 

March 2009 18.59 0.00 18.57 0.00 18.67 0.00 ---- ---- 

May 20093 18.69 0.00 18.64 0.00 18.72 0.00 NT5 NT5

May 2009 18.91 0.00 18.86 0.00 18.90 0.00 NT5 NT5

July 20094 18.66 0.00 18.59 0.00 18.64 0.00 18.63 0.00 

August 2009 18.37 0.00 18.30 0.00 18.47 0.00 18.21 0.00 

September 2009 18.20 0.00 18.17 0.00 18.24 0.00 18.11 0.00 

October 2009 18.17 0.00 18.14 0.00 18.24 0.00 18.10 0.00 

November 2009 18.50 0.00 18.45 0.00 18.50 0.00 18.47 0.00 

December 2009 18.29 0.00 18.26 0.00 18.31 0.00 18.19 0.00 

January 2010 18.05 0.00 18.01 0.00 18.09 0.00 17.97 0.00 

February 2010 18.17 0.00 18.12 0.00 18.17 0.00 18.12 0.00 

March 2010 17.88 0.00 17.86 0.00 17.93 0.00 17.76 0.00 

April 2010 17.66 0.00 17.64 0.00 17.71 0.00 17.55 0.00 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility May 2010 

 ____________________________________________________________________________________________ 

14 

SWL - Static water level, elevation above mean sea level 

LNAPL - Light Non-Aqueous Phased Liquid, fuel product on groundwater attributed to the Facility 

ft - Feet 

NT - Not Taken 1

 - The January 2008 measurement at RHMW03 was not taken due to equipment malfunction 2 - During the February 2009 measurements, RHMW01 was inaccessible due to extensive work being conducted at Tank 02 3

 - The measurements scheduled for April 2009 were postponed until May 6, 2009 due to RHMW05 drilling activities 4

 – The June 2009 measurements were skipped due to the installation of dedicated oil/water interface probes 5 - Oil/water interface measurements were not taken at RHMW05 until the installation of the oil/water interface probe was completed 6 – Elevation at RHMW05 is estimated from the difference between RHMW01 and RHMW05 during a survey conducted in January 2010 

---- - Time period prior to the installation of RHMW05 

Oil/water interface measurements were not taken in April 2008 

3.4 Groundwater Status 

Facility-specific contaminants of concern are defined as petroleum-related chemicals that have 

been observed in the groundwater samples above the HDOH Drinking Water EALs. In 

accordance with the Red Hill Bulk Fuel Storage Facility Final Groundwater Protection Plan

(TEC, 2008), Table 3 defines these Facility-specific compounds and their associated SSRBLs 

and updated EALs (HDOH 2008). 

Table 3. Action Levels for Contaminants of Concern 

Chemical EAL (μg/L) SSRBL (μg/L) 

Petroleum Mixtures 

TPH-DRO 210 4,500 

TPH-GRO 100 4,500 

Semi-Volatile Compounds 

1-Methylnaphthalene 4.7 NA 

2-Methylnaphthalene 24 NA 

Naphthalene 17 NA 

NA – Not applicable or not determined 

SSRBLs are applicable at RHMW01, RHMW02, RHMW03, and RHMW05 

EALs are applicable at US Navy Well 2254-01 

In addition, the Plan defines four Results Categories of groundwater status for the Facility, based 

on concentrations of constituents of concern in RHMW01, RHMW02, RHMW03, RHMW05 

and the US Navy Well 2254-01, and requires specific responses when these categories are 

observed during quarterly groundwater sampling. Table 4 describes each of the four Results 

Categories and identifies response actions to be taken in accordance with the Plan. 

 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility May 2010 

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15 

Table 4. Results Categories and Response Actions to Changes in Groundwater Status 

Results Category RHMW02 

RHMW03 or 

RHMW05* 

RHMW01 US Navy Pumping 

Well 2254-01 

Results Category 1: Result above 

detection limit but below drinking 

water EAL and trend for all 

compounds stable or decreasing 

A A A,D,M,E 

Results Category 2: Trend for any 

compound increasing or drinking 

water EAL exceeded 

A, B A, B A,B,C,D,E,F,G,K, 

L,O 

Results Category 3: Result 

Between 1/10X SSRBL and 

SSRBL for benzene, or between 

1/2X SSRBL and SSRBL for TPH 

A,B,G,H,I,J A,B,E,G,H,I,J A,B,C,D,E,F,G,I,J,

K,L,O 

Results Category 4: Result 

Exceeding any SSRBL or 

petroleum product observed 

A,C,D,E,F,I,J, 

K,M,N 

A,C,D,E,F,I, 

J,K,M,N,O 

A,C,D,E,F,G,I,J,K,

L,O 

*RHMW05 was installed in April 2009 and has been subsequently been added to this Table. 

Specific Responses: 

A. Send quarterly reports to HDOH. 

B. Begin program to determine the source of leak. 

C. Notify HDOH verbally within 1 day and follow with written notification in 30 days. 

D. Notify FISC Chain of Command within 1 day. 

E. Send Type 1 Report (see box below) to HDOH. 

F. Send Type 2 Report (see box below) to HDOH. 

G. Increase monitoring frequency to once per month (if concentrations increasing). 

H. Notify HDOH verbally within 7 days and follow with written notification in 30 days. 

I. Remove sampling pumps, measure product in pertinent wells with interface probe, re-install 

pumps if product is not detected. 

J. Immediately determine leaking tank. 

K. Collect samples from nearby Halawa Deep Monitoring Well (2253-03) and OWDF MW01. 

L. Provide alternative water source at 2254-01. 

M. Prepare for alternative water source at US Navy Well 2254-01. 

N. Re-measure for product every month with reports to HDOH. 

O. Install additional monitoring well downgradient. 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility May 2010 

 ____________________________________________________________________________________________ 

16 

Report Types 

HDOH Type 1 Report 

 Re-evaluate Tier 3 Risk Assessment/groundwater model results 

 Proposal to HDOH on a course of action 

HDOH Type 2 Report 

 Proposal for groundwater treatment 

Free Product Measurements

In response to the previous Category 3 status at RHMW02, free product measurements have 

been collected at the Facility monitoring wells. As Table 2 indicates, free product has been 

observed only during the January 2008 monitoring event (i.e., at both RHMW01 and RHMW02 

at less than 0.01 foot each). 

US Navy Well 2254-01

Based upon the April 2010 sampling event, the US Navy Well 2254-01 is not eligible for any 

category status change since no compounds were detected above the laboratory MDLs. 

RHMW03

Based upon the April 2010 sampling event, RHMW03 is not eligible for any category status 

change since no compounds were detected above the laboratory MDLs. 

Category 1 Status Locations

There are no Category 1 status locations based upon the April 2010 event. 

Category 2 Status Locations

RHMW01 

The April 2010 sampling event indicates that RHMW01 should remain in Category 2 status. 

This is because the TPH-DRO concentration of 377F g/L is greater than the HDOH Drinking 

Water EAL (210 g/L), but less than half the SSRBL of 4,500 g/L (estimated solubility limit of 

JP-5). 

RHMW02

Based upon the April 2010 sampling event, RHMW02 has been downgraded to Category 2 status. 

Although TPH-DRO concentrations remain greater than the HDOH Drinking Water EAL (210 

g/L), the April 2010 averaged concentration (2,215 g/L) is less than half the SSRBL of 4,500 

g/L. 

RHMW05

Based upon the April 2010 sampling event, RHMW05 should remain in a Category 2 status. 

This is because estimated trace concentrations of 1-methylnaphthalene have demonstrated a 

slight increasing trend (i.e., two or more consecutive sampling events of increasing 

concentrations) starting with the January 2010 sampling event. 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility May 2010 

 ____________________________________________________________________________________________ 

17 

 

Category 2 for RHMW01, RHMW02, and RHMW05 requires: 

1. Quarterly reports to be sent to HDOH; and 

2. Initiation of a leak determination program to identify if tanks are leaking. 

Category 3 Status Locations

There are no Category 3 status locations. 

 

Category 4 Status Locations

There are no Category 4 status locations. 

4.0 Summary and Conclusions 

Summary

There is no indication of an immediate threat of disruption to drinking water resources of the US 

Navy Well 2254-01 as a result of the April 2010 data. Based on the April 2010 sampling event, 

the US Navy Well 2254-01 does not fall into any Results Category of the Plan. 

RHMW01 is exhibiting an increasing trend for TPH-DRO relative to the concentrations observed 

in the most recent sampling events. However, the April 2010 results from RHMW01 are still at 

concentration levels within the historical range. Also during April 2010, TPH-DRO 

concentrations for RHMW02 and RHMW05 decreased relative to the previous respective 

sampling events. Specifically, in April 2010, TPH-DRO at RHMW05 was not detected above 

the laboratory MDL (Table 1). 

Conclusions/Recommendations

 To date, fuel on the groundwater has been observed only once (i.e., in January 2008 in 

RHMW01 and RHMW02 at less than 0.01 ft.). Continued monitoring of Facility wells 

for the presence of fuel on groundwater is recommended. 

 The concentration of TPH-DRO measured in the newest monitoring well, RHMW05, has 

drastically declined since exhibiting an increasing trend during all the previous sampling 

events at this location. 

 RHMW01 has exhibited a slightly increasing TPH-DRO trend while TPH-DRO at 

RHMW02 has slightly decreased since March 2010. However, April 2010 TPH-DRO 

concentrations are within the historical ranges for both RHMW01 and RHMW02. It is 

recommended that quarterly monitoring of the Facility wells continue so that overall 

groundwater quality trends may be evaluated and proactive action taken if the 

groundwater quality shows evidence of deterioration. 

 The US Navy Well 2254-01 is not imminently threatened at this time; however, sampling 

should continue to monitor and assess contaminant migration from up-gradient locations. 

 Consideration should be given to having future samples analyzed using both 

Massachusetts Department of Environmental Protection (MADEP) analytical methods in 

addition to TPH-GRO and TPH-DRO analytical methods. 

 The following activities are in process to monitor and/or clarify the groundwater 

contamination situation at the Facility: 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility May 2010 

 ____________________________________________________________________________________________ 

18 

1. Continue monthly free product measurements at RHMW01, RHMW02, 

RHMW03, and RHMW05; 

2. Continue monthly soil vapor monitoring; and 

3. Continue quarterly groundwater monitoring of Facility wells for TPH-DRO, TPHGRO, VOCs, PAHs, and lead until such time that new data indicates that a 

different monitoring program is warranted. 
The HDOH toxicity EALs were updated in •TPH DRO Residential Tap Water EAL is 21•TPH-DRO Residential Tap Water EAL is 21•TPH-GRO Residential Tap Water EAL is 10(HDOH, 2008).
The HDOH toxicity EALs were updated in • Naphthalene Residential Tap Water EAL 

1 th l hth l R id ti l T W t 

• 1-methylnaphthalene 

Residential Tap 

Wat

• 2- methylnaphthalene Residential Tap Wa(HDOH, 2008).
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility May 2010 

 ____________________________________________________________________________________________ 

21 

5.0 References 

AMEC. Red Hill Bulk Fuel Storage Facility Investigation Report, Prepared for NAVFAC 

Pacific, August 2002. 

Dawson Group, Inc. Fourth Quarter 2005 Groundwater Sampling Report, Red Hill Fuel 

Storage Facility, Hawaii. February 2006. 

Hawaii Administrative Rules, Title 11, Chapter 281, Subchapter 7. 

HDOH. Screening for Environmental Concerns at Sites with Contaminated Soil and 

Groundwater, Summary Lookup Tables. March 2009. 

HDOH. Use of May 2005 Environmental Action Levels (“EALs”) at Leaking Underground 

Storage Tank Sites. Memo. July 2005. 

HDOH. Evaluation of Environmental Hazards at Sites with Contaminated Soil and 

Groundwater. Summer 2008 (updated October 2008). 

Massachusetts Department of Environmental Protection (MADEP). Implementation of the 

MADEP VPH/EPH Approach. Final Policy, October 2002 

The Environmental Company, Inc. and AMEC. Red Hill Bulk Fuel Storage Facility Work Plan, 

Pearl Harbor, Hawaii. June 2005. 

TEC, Inc. Red Hill Bulk Fuel Storage Facility, Final – Addendum Planning Documents, Pearl 

Harbor, Hawaii. May 2006. 

TEC, Inc. Red Hill Bulk Fuel Storage Facility, Final Technical Report, Pearl Harbor, Hawaii. 

August 2007. 

TEC, Inc. Red Hill Bulk Fuel Storage Facility, Final Groundwater Protection Plan, Pearl 

Harbor, Hawaii. January 2008 revised in December 2009. 

TEC, Inc. Quarterly Groundwater Monitoring Report, Red Hill Fuel Storage Facility, Pearl 

Harbor, Hawaii. April 2010. 
Appendix A 

Laboratory Analytical Reports
SGS Work Order:

Contents:

Cover Page

Case Narrative

Final Report Pages

Quality Control Summary Forms

Chain of Custody/Sample Receipt Forms

Project:

Client:

SGS North America Inc.

 Alaska Division

Level II Laboratory Data Report

Released by: 

Note:

Unless otherwise noted, all quality assurance/quality control criteria is in compliance with the standards set forth by the proper regulatory authority, the 

SGS Quality Assurance Program Plan, and the National Environmental Accreditation Conference.

3354-003 Red Hill BFSF

The Environmental Company, Inc. (TEC)

1101584

1 of 97
CASE NARRATIVE Print Date: 4/30/2010

Workorder No.: 1101584

Project Name: 3354-003 Red Hill BFSF

Client Name: The Environmental Company, Inc. (TEC)

Lab Sample ID

Sample Comments

Sample Type Client Sample ID

Refer to the sample receipt form for information on sample condition.

1101584002

8270D SIM - MS recovery for mutliple analytes is outside of QC criteria (biased high). Refer to LCS for accuracy.

* BMS RHMW2254-WG19 MS

1101584004

8270D SIM - LCS recovery for multiple analytes is outside of QC criteria (biased high) due to concentration of the spike.

PS RHMW03-WG19

1101584005

8270D SIM - LCS recovery for multiple analytes is outside of QC criteria (biased high) due to concentration of the spike.

8015C - The pattern is consistent with a weathered middle distillate.

PS RHMW02-WG19

1101584006

8270D SIM - LCS recovery for multiple analytes is outside of QC criteria (biased high) due to concentration of the spike.

8015C - The pattern is consistent with a weathered middle distillate.

PS RHMWA01-WG19

1101584007

8270D SIM - LCS recovery for multiple analytes is outside of QC criteria (biased high) due to concentration of the spike.

PS RHMW01-WG19

1101584008

8270D SIM - LCS recovery for multiple analytes is outside of QC criteria (biased high) due to concentration of the spike.

PS RHMW05-WG19

956904

8270D SIM - LCS recovery for multiple analytes is outside of QC criteria (biased high) due to concentration of the spike.

* LCS LCS for HBN 227260 [XXX/22499]

956905

8270D SIM - LCSD recovery for multiple analytes is outside of QC criteria (biased high). These analytes were not detected 

above the LOQ in the associated samples.

* LCSD LCSD for HBN 227260 [XXX/22499

956911

8270D SIM - MS recovery for is outside of QC criteria (biased high). Refer to LCS for accuracy.

* MS RHMW2254-WG19 MS(1101584002MS)

957642

8260B - ICV recovery for chloromethane and bromomethane does not meet QC criteria (biased high). These analytes were 

not detected above LOQ in the associated samples.

* CCV CCV for HBN 227420 [VMS/11176]

* QC comments may be associated with the field samples found in this report. When applicable, comments will be applied to

 associated field samples.

SG S N o rth A m eric a Inc . En vir onm enta l D ivision 200 W e st Potter D rive A nc hora ge A K 99518 t(907 )562.2343 f( 907)561 .5301 w w w .us.sgs.com M em ber of SG S Group

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3354-003 Red Hill BFSF

Project Manager

jennifer.serna@sgs.com

Jennifer Serna

T: (808)528-1445 F:(808)528-0768

Attn: Rick Adkisson

1003 Bishop Street,

Pauahi Tower Suite 1550

Honolulu, HI 96813

Certification:

This data package is in compliance with the terms and conditions of the contract, both 

technically and for completeness, unless otherwise noted on the sample data sheet(s) and/or 

case narrative. This certification applies only to the tested parameters and the specific 

sample(s) received at the laboratory. If you have any questions regarding this report, or if we 

can be of further assistance, please contact your SGS Project Manager.

1101584

The Environmental Company, Inc. (TEC)

Workorder No.:

Client:

Project:

Laboratory Analytical Report

Contents (Bookmarked in PDF):

Cover Page

Glossary

Sample Summary Forms

Case Narrative

Sample Results Forms

Batch Summary Forms (by method)

Quality Control Summary Forms (by method)

Chain of Custody/Sample Receipt Forms

Attachments (if applicable)

SGS No rth Americ a Inc . En vir onmenta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com Member of SG S Group

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Enclosed are the analytical results associated with the above work order. All results are intended to be used in their entirety and SGS is not 

responsible for use of less than the complete report. If you have any questions regarding this report, or if we can be of any other assistance, please 

contact your SGS Project Manager at 907-562-2343. All work is provided under SGS general terms and conditions 

(<http://www.sgs.com/terms_and_conditions.htm>), unless other written agreements have been accepted by both parties.

SGS maintains a formal Quality Assurance/Quality Control (QA/QC) program. A copy of our Quality Assurance Plan (QAP), which outlines this 

program, is available at your request. The laboratory certification numbers are AK00971 (DW Chemistry & Microbiology) & UST-005 (CS) for 

ADEC and AK100001 for NELAP (RCRA methods: 1020A, 1311, 3010A, 3050B, 3520C, 3550C, 5030B, 5035B, 6010B, 6020, 7470A, 7471B, 

8021B, 8081B, 8082A, 8260B, 8270D, 8270D-SIM, 9040B, 9045C, 9056A, 9060A, AK101 and AK102/103). Except as specifically noted, all 

statements and data in this report are in conformance to the provisions set forth by the SGS QAP and, when applicable, the National Environmental 

Laboratory Accreditation Program and other regulatory authorities. The following descriptors or qualifiers may be found in your report:

* The analyte has exceeded allowable regulatory or control limits.

! Surrogate out of control limits.

B Indicates the analyte is found in a blank associated with the sample.

CCV Continuing Calibration Verification

CL Control Limit

D The analyte concentration is the result of a dilution.

DF Dilution Factor

DL Detection Limit (i.e., maximum method detection limit)

E The analyte result is above the calibrated range.

F Indicates value that is greater than or equal to the DL

GT Greater Than

ICV Initial Calibration Verification

J The quantitation is an estimation.

JL The analyte was positively identified, but the quantitation is a low estimation.

LCS(D) Laboratory Control Spike (Duplicate)

LOD Limit of Detection (i.e., 2xDL)

LOQ Limit of Quantitation (i.e., reporting or practical quantitation limit)

LT Less Than

M A matrix effect was present.

MB Method Blank

MS(D) Matrix Spike (Duplicate)

ND Indicates the analyte is not detected.

Q QC parameter out of acceptance range.

R Rejected

RL Reporting Limit

RPD Relative Percent Difference

U Indicates the analyte was analyzed for but not detected.

Note: Sample summaries which include a result for "Total Solids" have already been adjusted for moisture content.

All DRO/RRO analyses are integrated per SOP.

Print Date: 4/30/2010

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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SAMPLE SUMMARY

Client Name: The Environmental Company, Inc. (TEC)

Project Name: 3354-003 Red Hill BFSF

Workorder No.: 1101584

Analytical Methods

Method Description Analytical Method

8270 PAH SIM Semi-Vol GC/MS Liq/Liq ext. 8270D SIMS

AFCEE 3.1 8260 (W) SW8260B

Dissolved Metals by ICP-MS SW6020

DRO by 8015C (W) SW8015C

GRO (W) SW8015C

Print Date: 4/30/2010 10:42 am

Sample ID Cross Reference

Lab Sample ID Client Sample ID

1101584001 RHMW2254-WG19

1101584002 RHMW2254-WG19 MS

1101584003 RHMW2254-WG19 MSD

1101584004 RHMW03-WG19

1101584005 RHMW02-WG19

1101584006 RHMWA01-WG19

1101584007 RHMW01-WG19

1101584008 RHMW05-WG19

1101584009 TB01-WG19

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW2254-WG19

SGS Ref. #: 1101584001 Collection Date/Time: 04/13/10 11:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 0.310 ug/L 5 MMS6398 MXX22905

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6398

Analytical Method: SW6020

Analysis Date/Time: 04/21/10 11:38

Prep Batch: MXX22905

Prep Method: SW3010A

Prep Date/Time: 04/19/10 12:10 Container ID:1101584001-G

Dilution Factor: 5 Analyst: NRB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW2254-WG19

SGS Ref. #: 1101584001 Collection Date/Time: 04/13/10 11:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 30.0 ug/L 1 VFC9900 VXX20571

4-Bromofluorobenzene <surr> 105 50-150 % 1 VFC9900 VXX20571

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9900

Analytical Method: SW8015C

Analysis Date/Time: 04/16/10 11:48

Prep Batch: VXX20571

Prep Method: SW5030B

Prep Date/Time: 04/16/10 09:20 Container ID:1101584001-A

Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW2254-WG19

SGS Ref. #: 1101584001 Collection Date/Time: 04/13/10 11:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 0.320 U 0.426 0.160 mg/L 1 XFC9164 XXX22502

5a Androstane <surr> 88.8 50-150 % 1 XFC9164 XXX22502

Batch Information

Initial Prep Wt./Vol.: 940 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC9164

Analytical Method: SW8015C

Analysis Date/Time: 04/28/10 14:02

Prep Batch: XXX22502

Prep Method: SW3520C

Prep Date/Time: 04/19/10 10:30 Container ID:1101584001-H

Dilution Factor: 1 Analyst: LCE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW2254-WG19

SGS Ref. #: 1101584001 Collection Date/Time: 04/13/10 11:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11176 VXX20578

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11176 VXX20578

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1-Chlorohexane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11176 VXX20578

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11176 VXX20578

Acetone 6.20 U 10.0 3.10 ug/L 1 VMS11176 VXX20578

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11176 VXX20578

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11176 VXX20578

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW2254-WG19

SGS Ref. #: 1101584001 Collection Date/Time: 04/13/10 11:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11176 VXX20578

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11176 VXX20578

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11176 VXX20578

Naphthalene 1.24 U 2.00 0.620 ug/L 1 VMS11176 VXX20578

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

o-Xylene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11176 VXX20578

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Xylenes (total) 1.88 U 3.00 0.940 ug/L 1 VMS11176 VXX20578

1,2-Dichloroethane-D4 <surr> 101 73-120 % 1 VMS11176 VXX20578

4-Bromofluorobenzene <surr> 101 76-120 % 1 VMS11176 VXX20578

Toluene-d8 <surr> 97.6 80-120 % 1 VMS11176 VXX20578

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW2254-WG19

SGS Ref. #: 1101584001 Collection Date/Time: 04/13/10 11:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11176

Analytical Method: SW8260B

Analysis Date/Time: 04/21/10 16:37

Prep Batch: VXX20578

Prep Method: SW5030B

Prep Date/Time: 04/21/10 11:58 Container ID:1101584001-D

Dilution Factor: 1 Analyst: DSH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW2254-WG19

SGS Ref. #: 1101584001 Collection Date/Time: 04/13/10 11:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

DL DF

1-Methylnaphthalene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5373 XXX22498

2-Methylnaphthalene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5373 XXX22498

Acenaphthene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5373 XXX22498

Acenaphthylene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5373 XXX22498

Anthracene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5373 XXX22498

Benzo(a)Anthracene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5373 XXX22498

Benzo[a]pyrene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5373 XXX22498

Benzo[b]Fluoranthene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5373 XXX22498

Benzo[g,h,i]perylene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5373 XXX22498

Benzo[k]fluoranthene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5373 XXX22498

Chrysene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5373 XXX22498

Dibenzo[a,h]anthracene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5373 XXX22498

Fluoranthene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5373 XXX22498

Fluorene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5373 XXX22498

Indeno[1,2,3-c,d] pyrene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5373 XXX22498

Naphthalene 0.0682 U 0.110 0.0341 ug/L 1 XMS5373 XXX22498

Phenanthrene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5373 XXX22498

Pyrene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5373 XXX22498

Terphenyl-d14 <surr> 101 50-126 % 1 XMS5373 XXX22498

Batch Information

Initial Prep Wt./Vol.: 910 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5373

Analytical Method: 8270D SIMS

Analysis Date/Time: 04/26/10 06:57

Prep Batch: XXX22498

Prep Method: SW3520C

Prep Date/Time: 04/16/10 09:50 Container ID:1101584001-J

Dilution Factor: 1 Analyst: JDH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW03-WG19

SGS Ref. #: 1101584004 Collection Date/Time: 04/13/10 14:55

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 0.310 ug/L 5 MMS6398 MXX22905

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6398

Analytical Method: SW6020

Analysis Date/Time: 04/21/10 11:48

Prep Batch: MXX22905

Prep Method: SW3010A

Prep Date/Time: 04/19/10 12:10 Container ID:1101584004-G

Dilution Factor: 5 Analyst: NRB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW03-WG19

SGS Ref. #: 1101584004 Collection Date/Time: 04/13/10 14:55

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 30.0 ug/L 1 VFC9900 VXX20571

4-Bromofluorobenzene <surr> 110 50-150 % 1 VFC9900 VXX20571

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9900

Analytical Method: SW8015C

Analysis Date/Time: 04/16/10 13:28

Prep Batch: VXX20571

Prep Method: SW5030B

Prep Date/Time: 04/16/10 09:20 Container ID:1101584004-A

Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

14 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW03-WG19

SGS Ref. #: 1101584004 Collection Date/Time: 04/13/10 14:55

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 0.320 U 0.426 0.160 mg/L 1 XFC9164 XXX22502

5a Androstane <surr> 95.7 50-150 % 1 XFC9164 XXX22502

Batch Information

Initial Prep Wt./Vol.: 940 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC9164

Analytical Method: SW8015C

Analysis Date/Time: 04/28/10 15:05

Prep Batch: XXX22502

Prep Method: SW3520C

Prep Date/Time: 04/19/10 10:30 Container ID:1101584004-H

Dilution Factor: 1 Analyst: LCE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW03-WG19

SGS Ref. #: 1101584004 Collection Date/Time: 04/13/10 14:55

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11176 VXX20578

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11176 VXX20578

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1-Chlorohexane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11176 VXX20578

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11176 VXX20578

Acetone 6.20 U 10.0 3.10 ug/L 1 VMS11176 VXX20578

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11176 VXX20578

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11176 VXX20578

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

16 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW03-WG19

SGS Ref. #: 1101584004 Collection Date/Time: 04/13/10 14:55

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11176 VXX20578

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11176 VXX20578

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11176 VXX20578

Naphthalene 1.24 U 2.00 0.620 ug/L 1 VMS11176 VXX20578

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

o-Xylene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11176 VXX20578

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Xylenes (total) 1.88 U 3.00 0.940 ug/L 1 VMS11176 VXX20578

1,2-Dichloroethane-D4 <surr> 99.5 73-120 % 1 VMS11176 VXX20578

4-Bromofluorobenzene <surr> 100 76-120 % 1 VMS11176 VXX20578

Toluene-d8 <surr> 98.7 80-120 % 1 VMS11176 VXX20578

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

17 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW03-WG19

SGS Ref. #: 1101584004 Collection Date/Time: 04/13/10 14:55

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11176

Analytical Method: SW8260B

Analysis Date/Time: 04/21/10 17:04

Prep Batch: VXX20578

Prep Method: SW5030B

Prep Date/Time: 04/21/10 11:58 Container ID:1101584004-D

Dilution Factor: 1 Analyst: DSH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

18 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW03-WG19

SGS Ref. #: 1101584004 Collection Date/Time: 04/13/10 14:55

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

DL DF

1-Methylnaphthalene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

2-Methylnaphthalene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Acenaphthene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Acenaphthylene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Anthracene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Benzo(a)Anthracene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Benzo[a]pyrene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Benzo[b]Fluoranthene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Benzo[g,h,i]perylene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Benzo[k]fluoranthene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Chrysene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Dibenzo[a,h]anthracene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Fluoranthene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Fluorene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Indeno[1,2,3-c,d] pyrene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Naphthalene 0.0666 U 0.108 0.0333 ug/L 1 XMS5372 XXX22499

Phenanthrene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Pyrene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Terphenyl-d14 <surr> 98.5 50-126 % 1 XMS5372 XXX22499

Batch Information

Initial Prep Wt./Vol.: 930 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5372

Analytical Method: 8270D SIMS

Analysis Date/Time: 04/23/10 16:55

Prep Batch: XXX22499

Prep Method: SW3520C

Prep Date/Time: 04/16/10 10:30 Container ID:1101584004-J

Dilution Factor: 1 Analyst: JDH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

19 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW02-WG19

SGS Ref. #: 1101584005 Collection Date/Time: 04/13/10 16:10

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 0.310 ug/L 5 MMS6398 MXX22905

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6398

Analytical Method: SW6020

Analysis Date/Time: 04/21/10 11:50

Prep Batch: MXX22905

Prep Method: SW3010A

Prep Date/Time: 04/19/10 12:10 Container ID:1101584005-G

Dilution Factor: 5 Analyst: NRB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

20 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW02-WG19

SGS Ref. #: 1101584005 Collection Date/Time: 04/13/10 16:10

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 39.3J 100 30.0 ug/L 1 VFC9900 VXX20571

4-Bromofluorobenzene <surr> 122 50-150 % 1 VFC9900 VXX20571

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9900

Analytical Method: SW8015C

Analysis Date/Time: 04/16/10 13:47

Prep Batch: VXX20571

Prep Method: SW5030B

Prep Date/Time: 04/16/10 09:20 Container ID:1101584005-A

Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

21 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW02-WG19

SGS Ref. #: 1101584005 Collection Date/Time: 04/13/10 16:10

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 2.35 0.426 0.160 mg/L 1 XFC9164 XXX22502

5a Androstane <surr> 83.2 50-150 % 1 XFC9164 XXX22502

Batch Information

Initial Prep Wt./Vol.: 940 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC9164

Analytical Method: SW8015C

Analysis Date/Time: 04/28/10 15:28

Prep Batch: XXX22502

Prep Method: SW3520C

Prep Date/Time: 04/19/10 10:30 Container ID:1101584005-H

Dilution Factor: 1 Analyst: LCE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

22 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW02-WG19

SGS Ref. #: 1101584005 Collection Date/Time: 04/13/10 16:10

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11176 VXX20578

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11176 VXX20578

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1-Chlorohexane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11176 VXX20578

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11176 VXX20578

Acetone 6.20 U 10.0 3.10 ug/L 1 VMS11176 VXX20578

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11176 VXX20578

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11176 VXX20578

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

23 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW02-WG19

SGS Ref. #: 1101584005 Collection Date/Time: 04/13/10 16:10

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11176 VXX20578

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Isopropylbenzene (Cumene) 4.15 1.00 0.310 ug/L 1 VMS11176 VXX20578

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11176 VXX20578

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11176 VXX20578

Naphthalene 20.6 2.00 0.620 ug/L 1 VMS11176 VXX20578

n-Butylbenzene 3.40 1.00 0.310 ug/L 1 VMS11176 VXX20578

n-Propylbenzene 6.24 1.00 0.310 ug/L 1 VMS11176 VXX20578

o-Xylene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11176 VXX20578

sec-Butylbenzene 4.33 1.00 0.310 ug/L 1 VMS11176 VXX20578

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

tert-Butylbenzene 0.840J 1.00 0.310 ug/L 1 VMS11176 VXX20578

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Xylenes (total) 1.88 U 3.00 0.940 ug/L 1 VMS11176 VXX20578

1,2-Dichloroethane-D4 <surr> 100 73-120 % 1 VMS11176 VXX20578

4-Bromofluorobenzene <surr> 101 76-120 % 1 VMS11176 VXX20578

Toluene-d8 <surr> 96.9 80-120 % 1 VMS11176 VXX20578

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

24 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW02-WG19

SGS Ref. #: 1101584005 Collection Date/Time: 04/13/10 16:10

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11176

Analytical Method: SW8260B

Analysis Date/Time: 04/21/10 17:31

Prep Batch: VXX20578

Prep Method: SW5030B

Prep Date/Time: 04/21/10 11:58 Container ID:1101584005-D

Dilution Factor: 1 Analyst: DSH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

25 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW02-WG19

SGS Ref. #: 1101584005 Collection Date/Time: 04/13/10 16:10

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

DL DF

1-Methylnaphthalene 6.61 0.538 0.161 ug/L 10 XMS5373 XXX22499

2-Methylnaphthalene 1.69 0.538 0.161 ug/L 10 XMS5373 XXX22499

Acenaphthene 0.426 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Acenaphthylene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Anthracene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Benzo(a)Anthracene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Benzo[a]pyrene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Benzo[b]Fluoranthene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Benzo[g,h,i]perylene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Benzo[k]fluoranthene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Chrysene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Dibenzo[a,h]anthracene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Fluoranthene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Fluorene 0.224 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Indeno[1,2,3-c,d] pyrene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Naphthalene 14.3 1.08 0.333 ug/L 10 XMS5373 XXX22499

Phenanthrene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Pyrene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Terphenyl-d14 <surr> 104 50-126 % 1 XMS5372 XXX22499

Batch Information

Initial Prep Wt./Vol.: 930 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5372

Analytical Method: 8270D SIMS

Analysis Date/Time: 04/23/10 17:14

Prep Batch: XXX22499

Prep Method: SW3520C

Prep Date/Time: 04/16/10 10:30 Container ID:1101584005-J

Dilution Factor: 1 Analyst: JDH

Initial Prep Wt./Vol.: 930 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5373

Analytical Method: 8270D SIMS

Analysis Date/Time: 04/25/10 21:53

Prep Batch: XXX22499

Prep Method: SW3520C

Prep Date/Time: 04/16/10 10:30 Container ID:1101584005-J

Dilution Factor: 10 Analyst: JDH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

26 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMWA01-WG19

SGS Ref. #: 1101584006 Collection Date/Time: 04/13/10 12:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 0.310 ug/L 5 MMS6398 MXX22905

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6398

Analytical Method: SW6020

Analysis Date/Time: 04/21/10 11:52

Prep Batch: MXX22905

Prep Method: SW3010A

Prep Date/Time: 04/19/10 12:10 Container ID:1101584006-G

Dilution Factor: 5 Analyst: NRB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

27 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMWA01-WG19

SGS Ref. #: 1101584006 Collection Date/Time: 04/13/10 12:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 39.0J 100 30.0 ug/L 1 VFC9900 VXX20571

4-Bromofluorobenzene <surr> 120 50-150 % 1 VFC9900 VXX20571

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9900

Analytical Method: SW8015C

Analysis Date/Time: 04/16/10 14:06

Prep Batch: VXX20571

Prep Method: SW5030B

Prep Date/Time: 04/16/10 09:20 Container ID:1101584006-A

Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

28 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMWA01-WG19

SGS Ref. #: 1101584006 Collection Date/Time: 04/13/10 12:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 2.08 0.430 0.161 mg/L 1 XFC9164 XXX22502

5a Androstane <surr> 77.8 50-150 % 1 XFC9164 XXX22502

Batch Information

Initial Prep Wt./Vol.: 930 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC9164

Analytical Method: SW8015C

Analysis Date/Time: 04/28/10 15:49

Prep Batch: XXX22502

Prep Method: SW3520C

Prep Date/Time: 04/19/10 10:30 Container ID:1101584006-H

Dilution Factor: 1 Analyst: LCE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

29 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMWA01-WG19

SGS Ref. #: 1101584006 Collection Date/Time: 04/13/10 12:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11176 VXX20578

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11176 VXX20578

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1-Chlorohexane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11176 VXX20578

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11176 VXX20578

Acetone 6.20 U 10.0 3.10 ug/L 1 VMS11176 VXX20578

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11176 VXX20578

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11176 VXX20578

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

30 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMWA01-WG19

SGS Ref. #: 1101584006 Collection Date/Time: 04/13/10 12:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11176 VXX20578

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Isopropylbenzene (Cumene) 4.08 1.00 0.310 ug/L 1 VMS11176 VXX20578

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11176 VXX20578

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11176 VXX20578

Naphthalene 21.4 2.00 0.620 ug/L 1 VMS11176 VXX20578

n-Butylbenzene 3.56 1.00 0.310 ug/L 1 VMS11176 VXX20578

n-Propylbenzene 6.44 1.00 0.310 ug/L 1 VMS11176 VXX20578

o-Xylene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11176 VXX20578

sec-Butylbenzene 4.34 1.00 0.310 ug/L 1 VMS11176 VXX20578

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

tert-Butylbenzene 0.790J 1.00 0.310 ug/L 1 VMS11176 VXX20578

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Xylenes (total) 1.88 U 3.00 0.940 ug/L 1 VMS11176 VXX20578

1,2-Dichloroethane-D4 <surr> 102 73-120 % 1 VMS11176 VXX20578

4-Bromofluorobenzene <surr> 105 76-120 % 1 VMS11176 VXX20578

Toluene-d8 <surr> 98 80-120 % 1 VMS11176 VXX20578

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

31 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMWA01-WG19

SGS Ref. #: 1101584006 Collection Date/Time: 04/13/10 12:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11176

Analytical Method: SW8260B

Analysis Date/Time: 04/21/10 17:57

Prep Batch: VXX20578

Prep Method: SW5030B

Prep Date/Time: 04/21/10 11:58 Container ID:1101584006-D

Dilution Factor: 1 Analyst: DSH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

32 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMWA01-WG19

SGS Ref. #: 1101584006 Collection Date/Time: 04/13/10 12:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

DL DF

1-Methylnaphthalene 5.90 0.549 0.165 ug/L 10 XMS5373 XXX22499

2-Methylnaphthalene 1.90 0.0549 0.0165 ug/L 1 XMS5372 XXX22499

Acenaphthene 0.429 0.0549 0.0165 ug/L 1 XMS5372 XXX22499

Acenaphthylene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5372 XXX22499

Anthracene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5372 XXX22499

Benzo(a)Anthracene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5372 XXX22499

Benzo[a]pyrene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5372 XXX22499

Benzo[b]Fluoranthene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5372 XXX22499

Benzo[g,h,i]perylene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5372 XXX22499

Benzo[k]fluoranthene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5372 XXX22499

Chrysene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5372 XXX22499

Dibenzo[a,h]anthracene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5372 XXX22499

Fluoranthene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5372 XXX22499

Fluorene 0.230 0.0549 0.0165 ug/L 1 XMS5372 XXX22499

Indeno[1,2,3-c,d] pyrene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5372 XXX22499

Naphthalene 12.7 1.10 0.341 ug/L 10 XMS5373 XXX22499

Phenanthrene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5372 XXX22499

Pyrene 0.0330 U 0.0549 0.0165 ug/L 1 XMS5372 XXX22499

Terphenyl-d14 <surr> 93.6 50-126 % 1 XMS5372 XXX22499

Batch Information

Initial Prep Wt./Vol.: 910 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5372

Analytical Method: 8270D SIMS

Analysis Date/Time: 04/23/10 17:32

Prep Batch: XXX22499

Prep Method: SW3520C

Prep Date/Time: 04/16/10 10:30 Container ID:1101584006-J

Dilution Factor: 1 Analyst: JDH

Initial Prep Wt./Vol.: 910 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5373

Analytical Method: 8270D SIMS

Analysis Date/Time: 04/25/10 22:12

Prep Batch: XXX22499

Prep Method: SW3520C

Prep Date/Time: 04/16/10 10:30 Container ID:1101584006-J

Dilution Factor: 10 Analyst: JDH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

33 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW01-WG19

SGS Ref. #: 1101584007 Collection Date/Time: 04/13/10 18:40

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 0.310 ug/L 5 MMS6398 MXX22905

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6398

Analytical Method: SW6020

Analysis Date/Time: 04/21/10 11:54

Prep Batch: MXX22905

Prep Method: SW3010A

Prep Date/Time: 04/19/10 12:10 Container ID:1101584007-G

Dilution Factor: 5 Analyst: NRB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

34 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW01-WG19

SGS Ref. #: 1101584007 Collection Date/Time: 04/13/10 18:40

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 30.0 ug/L 1 VFC9900 VXX20571

4-Bromofluorobenzene <surr> 105 50-150 % 1 VFC9900 VXX20571

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9900

Analytical Method: SW8015C

Analysis Date/Time: 04/16/10 14:25

Prep Batch: VXX20571

Prep Method: SW5030B

Prep Date/Time: 04/16/10 09:20 Container ID:1101584007-A

Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

35 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW01-WG19

SGS Ref. #: 1101584007 Collection Date/Time: 04/13/10 18:40

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 0.377J 0.435 0.163 mg/L 1 XFC9164 XXX22502

5a Androstane <surr> 98.8 50-150 % 1 XFC9164 XXX22502

Batch Information

Initial Prep Wt./Vol.: 920 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC9164

Analytical Method: SW8015C

Analysis Date/Time: 04/28/10 16:10

Prep Batch: XXX22502

Prep Method: SW3520C

Prep Date/Time: 04/19/10 10:30 Container ID:1101584007-H

Dilution Factor: 1 Analyst: LCE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

36 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW01-WG19

SGS Ref. #: 1101584007 Collection Date/Time: 04/13/10 18:40

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11176 VXX20578

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11176 VXX20578

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1-Chlorohexane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11176 VXX20578

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11176 VXX20578

Acetone 6.20 U 10.0 3.10 ug/L 1 VMS11176 VXX20578

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11176 VXX20578

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11176 VXX20578

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

37 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW01-WG19

SGS Ref. #: 1101584007 Collection Date/Time: 04/13/10 18:40

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11176 VXX20578

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11176 VXX20578

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11176 VXX20578

Naphthalene 1.24 U 2.00 0.620 ug/L 1 VMS11182 VXX20584

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

o-Xylene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11176 VXX20578

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Xylenes (total) 1.88 U 3.00 0.940 ug/L 1 VMS11176 VXX20578

1,2-Dichloroethane-D4 <surr> 104 73-120 % 1 VMS11176 VXX20578

4-Bromofluorobenzene <surr> 97.3 76-120 % 1 VMS11176 VXX20578

Toluene-d8 <surr> 98.9 80-120 % 1 VMS11176 VXX20578

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

38 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW01-WG19

SGS Ref. #: 1101584007 Collection Date/Time: 04/13/10 18:40

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11176

Analytical Method: SW8260B

Analysis Date/Time: 04/21/10 18:24

Prep Batch: VXX20578

Prep Method: SW5030B

Prep Date/Time: 04/21/10 11:58 Container ID:1101584007-D

Dilution Factor: 1 Analyst: DSH

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11182

Analytical Method: SW8260B

Analysis Date/Time: 04/22/10 15:42

Prep Batch: VXX20584

Prep Method: SW5030B

Prep Date/Time: 04/22/10 11:17 Container ID:1101584007-E

Dilution Factor: 1 Analyst: JDB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

39 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW01-WG19

SGS Ref. #: 1101584007 Collection Date/Time: 04/13/10 18:40

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

DL DF

1-Methylnaphthalene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

2-Methylnaphthalene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Acenaphthene 0.0450J 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Acenaphthylene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Anthracene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Benzo(a)Anthracene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Benzo[a]pyrene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Benzo[b]Fluoranthene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Benzo[g,h,i]perylene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Benzo[k]fluoranthene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Chrysene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Dibenzo[a,h]anthracene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Fluoranthene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Fluorene 0.0455J 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Indeno[1,2,3-c,d] pyrene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Naphthalene 0.0666 U 0.108 0.0333 ug/L 1 XMS5372 XXX22499

Phenanthrene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Pyrene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5372 XXX22499

Terphenyl-d14 <surr> 98.1 50-126 % 1 XMS5372 XXX22499

Batch Information

Initial Prep Wt./Vol.: 930 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5372

Analytical Method: 8270D SIMS

Analysis Date/Time: 04/23/10 17:50

Prep Batch: XXX22499

Prep Method: SW3520C

Prep Date/Time: 04/16/10 10:30 Container ID:1101584007-J

Dilution Factor: 1 Analyst: JDH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

40 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW05-WG19

SGS Ref. #: 1101584008 Collection Date/Time: 04/13/10 13:20

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 0.310 ug/L 5 MMS6398 MXX22905

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6398

Analytical Method: SW6020

Analysis Date/Time: 04/21/10 12:06

Prep Batch: MXX22905

Prep Method: SW3010A

Prep Date/Time: 04/19/10 12:10 Container ID:1101584008-G

Dilution Factor: 5 Analyst: NRB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

41 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW05-WG19

SGS Ref. #: 1101584008 Collection Date/Time: 04/13/10 13:20

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 30.0 ug/L 1 VFC9900 VXX20571

4-Bromofluorobenzene <surr> 99.5 50-150 % 1 VFC9900 VXX20571

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9900

Analytical Method: SW8015C

Analysis Date/Time: 04/16/10 14:44

Prep Batch: VXX20571

Prep Method: SW5030B

Prep Date/Time: 04/16/10 09:20 Container ID:1101584008-A

Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

42 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW05-WG19

SGS Ref. #: 1101584008 Collection Date/Time: 04/13/10 13:20

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 0.300 U 0.400 0.150 mg/L 1 XFC9164 XXX22502

5a Androstane <surr> 94.3 50-150 % 1 XFC9164 XXX22502

Batch Information

Initial Prep Wt./Vol.: 1000 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC9164

Analytical Method: SW8015C

Analysis Date/Time: 04/28/10 16:52

Prep Batch: XXX22502

Prep Method: SW3520C

Prep Date/Time: 04/19/10 10:30 Container ID:1101584008-H

Dilution Factor: 1 Analyst: LCE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

43 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW05-WG19

SGS Ref. #: 1101584008 Collection Date/Time: 04/13/10 13:20

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11176 VXX20578

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11176 VXX20578

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1-Chlorohexane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11176 VXX20578

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11176 VXX20578

Acetone 6.20 U 10.0 3.10 ug/L 1 VMS11176 VXX20578

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11176 VXX20578

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11176 VXX20578

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

44 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW05-WG19

SGS Ref. #: 1101584008 Collection Date/Time: 04/13/10 13:20

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11176 VXX20578

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11176 VXX20578

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11176 VXX20578

Naphthalene 1.24 U 2.00 0.620 ug/L 1 VMS11176 VXX20578

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

o-Xylene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11176 VXX20578

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Xylenes (total) 1.88 U 3.00 0.940 ug/L 1 VMS11176 VXX20578

1,2-Dichloroethane-D4 <surr> 99.6 73-120 % 1 VMS11176 VXX20578

4-Bromofluorobenzene <surr> 105 76-120 % 1 VMS11176 VXX20578

Toluene-d8 <surr> 97.8 80-120 % 1 VMS11176 VXX20578

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

45 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW05-WG19

SGS Ref. #: 1101584008 Collection Date/Time: 04/13/10 13:20

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11176

Analytical Method: SW8260B

Analysis Date/Time: 04/21/10 18:50

Prep Batch: VXX20578

Prep Method: SW5030B

Prep Date/Time: 04/21/10 11:58 Container ID:1101584008-D

Dilution Factor: 1 Analyst: DSH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

46 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: RHMW05-WG19

SGS Ref. #: 1101584008 Collection Date/Time: 04/13/10 13:20

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

DL DF

1-Methylnaphthalene 0.0335J 0.0543 0.0163 ug/L 1 XMS5372 XXX22499

2-Methylnaphthalene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5372 XXX22499

Acenaphthene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5372 XXX22499

Acenaphthylene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5372 XXX22499

Anthracene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5372 XXX22499

Benzo(a)Anthracene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5372 XXX22499

Benzo[a]pyrene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5372 XXX22499

Benzo[b]Fluoranthene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5372 XXX22499

Benzo[g,h,i]perylene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5372 XXX22499

Benzo[k]fluoranthene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5372 XXX22499

Chrysene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5372 XXX22499

Dibenzo[a,h]anthracene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5372 XXX22499

Fluoranthene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5372 XXX22499

Fluorene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5372 XXX22499

Indeno[1,2,3-c,d] pyrene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5372 XXX22499

Naphthalene 0.0752J 0.109 0.0337 ug/L 1 XMS5372 XXX22499

Phenanthrene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5372 XXX22499

Pyrene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5372 XXX22499

Terphenyl-d14 <surr> 101 50-126 % 1 XMS5372 XXX22499

Batch Information

Initial Prep Wt./Vol.: 920 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5372

Analytical Method: 8270D SIMS

Analysis Date/Time: 04/23/10 18:09

Prep Batch: XXX22499

Prep Method: SW3520C

Prep Date/Time: 04/16/10 10:30 Container ID:1101584008-J

Dilution Factor: 1 Analyst: JDH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

47 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: TB01-WG19

SGS Ref. #: 1101584009 Collection Date/Time: 04/13/10 08:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 30.0 ug/L 1 VFC9900 VXX20571

4-Bromofluorobenzene <surr> 112 50-150 % 1 VFC9900 VXX20571

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9900

Analytical Method: SW8015C

Analysis Date/Time: 04/16/10 11:29

Prep Batch: VXX20571

Prep Method: SW5030B

Prep Date/Time: 04/16/10 09:20 Container ID:1101584009-A

Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

48 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: TB01-WG19

SGS Ref. #: 1101584009 Collection Date/Time: 04/13/10 08:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11176 VXX20578

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11176 VXX20578

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

1-Chlorohexane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11176 VXX20578

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11176 VXX20578

Acetone 6.20 U 10.0 3.10 ug/L 1 VMS11176 VXX20578

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11176 VXX20578

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11176 VXX20578

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

49 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: TB01-WG19

SGS Ref. #: 1101584009 Collection Date/Time: 04/13/10 08:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11176 VXX20578

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11176 VXX20578

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11176 VXX20578

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11176 VXX20578

Naphthalene 1.24 U 2.00 0.620 ug/L 1 VMS11176 VXX20578

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

o-Xylene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11176 VXX20578

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11176 VXX20578

Xylenes (total) 1.88 U 3.00 0.940 ug/L 1 VMS11176 VXX20578

1,2-Dichloroethane-D4 <surr> 96.6 73-120 % 1 VMS11176 VXX20578

4-Bromofluorobenzene <surr> 103 76-120 % 1 VMS11176 VXX20578

Toluene-d8 <surr> 98.1 80-120 % 1 VMS11176 VXX20578

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

50 of 97
The Environmental Company, Inc. (TEC) Print Date: 4/30/2010 10:42 am

Client Sample ID: TB01-WG19

SGS Ref. #: 1101584009 Collection Date/Time: 04/13/10 08:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 04/15/10 11:10

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11176

Analytical Method: SW8260B

Analysis Date/Time: 04/21/10 16:11

Prep Batch: VXX20578

Prep Method: SW5030B

Prep Date/Time: 04/21/10 11:58 Container ID:1101584009-B

Dilution Factor: 1 Analyst: DSH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

51 of 97
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Prep

956901 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX22498

SW3520C

04/16/2010

QC results affect the following production samples:

1101584001

Parameter Results LOQ/CL Units

Analysis

DL Date

Polynuclear Aromatics GC/MS

1-Methylnaphthalene 0.0300 U 0.0500 0.0150 ug/L 04/26/10

2-Methylnaphthalene 0.0300 U 0.0500 0.0150 ug/L 04/26/10

Acenaphthene 0.0300 U 0.0500 0.0150 ug/L 04/26/10

Acenaphthylene 0.0300 U 0.0500 0.0150 ug/L 04/26/10

Anthracene 0.0300 U 0.0500 0.0150 ug/L 04/26/10

Benzo(a)Anthracene 0.0300 U 0.0500 0.0150 ug/L 04/26/10

Benzo[a]pyrene 0.0300 U 0.0500 0.0150 ug/L 04/26/10

Benzo[b]Fluoranthene 0.0300 U 0.0500 0.0150 ug/L 04/26/10

Benzo[g,h,i]perylene 0.0300 U 0.0500 0.0150 ug/L 04/26/10

Benzo[k]fluoranthene 0.0300 U 0.0500 0.0150 ug/L 04/26/10

Chrysene 0.0300 U 0.0500 0.0150 ug/L 04/26/10

Dibenzo[a,h]anthracene 0.0300 U 0.0500 0.0150 ug/L 04/26/10

Fluoranthene 0.0300 U 0.0500 0.0150 ug/L 04/26/10

Fluorene 0.0300 U 0.0500 0.0150 ug/L 04/26/10

Indeno[1,2,3-c,d] pyrene 0.0300 U 0.0500 0.0150 ug/L 04/26/10

Naphthalene 0.0620 U 0.100 0.0310 ug/L 04/26/10

Phenanthrene 0.0300 U 0.0500 0.0150 ug/L 04/26/10

Pyrene 0.0300 U 0.0500 0.0150 ug/L 04/26/10

Surrogates 

Terphenyl-d14 <surr> 103 50-126 % 04/26/10

Instrument

Method

Batch XMS5373

8270D SIMS

HP 6890/5973 MS SVQA

52 of 97
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Prep

956903 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX22499

SW3520C

04/16/2010

QC results affect the following production samples:

1101584004, 1101584005, 1101584006, 1101584007, 1101584008

Parameter Results LOQ/CL Units

Analysis

DL Date

Polynuclear Aromatics GC/MS

1-Methylnaphthalene 0.0300 U 0.0500 0.0150 ug/L 04/23/10

2-Methylnaphthalene 0.0300 U 0.0500 0.0150 ug/L 04/23/10

Acenaphthene 0.0300 U 0.0500 0.0150 ug/L 04/23/10

Acenaphthylene 0.0300 U 0.0500 0.0150 ug/L 04/23/10

Anthracene 0.0300 U 0.0500 0.0150 ug/L 04/23/10

Benzo(a)Anthracene 0.0300 U 0.0500 0.0150 ug/L 04/23/10

Benzo[a]pyrene 0.0300 U 0.0500 0.0150 ug/L 04/23/10

Benzo[b]Fluoranthene 0.0300 U 0.0500 0.0150 ug/L 04/23/10

Benzo[g,h,i]perylene 0.0300 U 0.0500 0.0150 ug/L 04/23/10

Benzo[k]fluoranthene 0.0300 U 0.0500 0.0150 ug/L 04/23/10

Chrysene 0.0300 U 0.0500 0.0150 ug/L 04/23/10

Dibenzo[a,h]anthracene 0.0300 U 0.0500 0.0150 ug/L 04/23/10

Fluoranthene 0.0300 U 0.0500 0.0150 ug/L 04/23/10

Fluorene 0.0300 U 0.0500 0.0150 ug/L 04/23/10

Indeno[1,2,3-c,d] pyrene 0.0300 U 0.0500 0.0150 ug/L 04/23/10

Naphthalene 0.0620 U 0.100 0.0310 ug/L 04/23/10

Phenanthrene 0.0300 U 0.0500 0.0150 ug/L 04/23/10

Pyrene 0.0300 U 0.0500 0.0150 ug/L 04/23/10

Surrogates 

Terphenyl-d14 <surr> 111 50-126 % 04/23/10

Instrument

Method

Batch XMS5372

8270D SIMS

HP 6890/5973 MS SVQA

53 of 97
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Prep

957070 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20571

SW5030B

04/16/2010

QC results affect the following production samples:

1101584001, 1101584004, 1101584005, 1101584006, 1101584007, 1101584008, 1101584009

Parameter Results LOQ/CL Units

Analysis

DL Date

Volatile Fuels Department

Gasoline Range Organics 60.0 U 100 30.0 ug/L 04/16/10

Surrogates 

4-Bromofluorobenzene <surr> 107 50-150 % 04/16/10

Instrument

Method

Batch VFC9900

SW8015C

HP 5890 Series II PID+FID VCA

54 of 97
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Prep

957073 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX22502

SW3520C

04/19/2010

QC results affect the following production samples:

1101584001, 1101584004, 1101584005, 1101584006, 1101584007, 1101584008

Parameter Results LOQ/CL Units

Analysis

DL Date

Semivolatile Organic Fuels Department

Diesel Range Organics 0.300 U 0.400 0.150 mg/L 04/28/10

Surrogates 

5a Androstane <surr> 86.2 60-120 % 04/28/10

Instrument

Method

Batch XFC9164

SW8015C

HP 7890A FID SV E R

55 of 97
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Prep

957189 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

MXX22905

SW3010A

04/19/2010

QC results affect the following production samples:

1101584001, 1101584004, 1101584005, 1101584006, 1101584007, 1101584008

Parameter Results LOQ/CL Units

Analysis

DL Date

Metals by ICP/MS

Lead 0.620 U 1.00 0.310 ug/L 04/21/10

Instrument

Method

Batch MMS6398

SW6020

Perkin Elmer Sciex ICP-MS P3

56 of 97
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Prep

957639 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20578

SW5030B

04/21/2010

QC results affect the following production samples:

1101584001, 1101584004, 1101584005, 1101584006, 1101584007, 1101584008, 1101584009

Parameter Results LOQ/CL Units

Analysis

DL Date

Volatile Gas Chromatography/Mass Spectroscopy

57 of 97
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Prep

957639 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20578

SW5030B

04/21/2010

Parameter Results LOQ/CL Units

Analysis

DL Date

Volatile Gas Chromatography/Mass Spectroscopy

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 04/21/10

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 04/21/10

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 04/21/10

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 04/21/10

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 04/21/10

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 04/21/10

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 04/21/10

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 04/21/10

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 04/21/10

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 04/21/10

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 04/21/10

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 04/21/10

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 04/21/10

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 04/21/10

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 04/21/10

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 04/21/10

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 04/21/10

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 04/21/10

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 04/21/10

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 04/21/10

1-Chlorohexane 0.620 U 1.00 0.310 ug/L 04/21/10

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 04/21/10

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 04/21/10

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 04/21/10

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 04/21/10

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 04/21/10

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 04/21/10

Acetone 6.20 U 10.0 3.10 ug/L 04/21/10

Benzene 0.240 U 0.400 0.120 ug/L 04/21/10

Bromobenzene 0.620 U 1.00 0.310 ug/L 04/21/10

Bromochloromethane 0.620 U 1.00 0.310 ug/L 04/21/10

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 04/21/10

Bromoform 0.620 U 1.00 0.310 ug/L 04/21/10

Bromomethane 1.88 U 3.00 0.940 ug/L 04/21/10

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 04/21/10

Chlorobenzene 0.300 U 0.500 0.150 ug/L 04/21/10

Chloroethane 0.620 U 1.00 0.310 ug/L 04/21/10

Chloroform 0.600 U 1.00 0.300 ug/L 04/21/10

Chloromethane 0.620 U 1.00 0.310 ug/L 04/21/10

58 of 97
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Prep

957639 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20578

SW5030B

04/21/2010

Parameter Results LOQ/CL Units

Analysis

DL Date

Volatile Gas Chromatography/Mass Spectroscopy

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 04/21/10

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 04/21/10

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 04/21/10

Dibromomethane 0.620 U 1.00 0.310 ug/L 04/21/10

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 04/21/10

Ethylbenzene 0.620 U 1.00 0.310 ug/L 04/21/10

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 04/21/10

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 04/21/10

Methylene chloride 2.00 U 5.00 1.00 ug/L 04/21/10

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 04/21/10

Naphthalene 1.24 U 2.00 0.620 ug/L 04/21/10

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 04/21/10

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 04/21/10

o-Xylene 0.620 U 1.00 0.310 ug/L 04/21/10

P & M -Xylene 1.24 U 2.00 0.620 ug/L 04/21/10

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 04/21/10

Styrene 0.620 U 1.00 0.310 ug/L 04/21/10

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 04/21/10

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 04/21/10

Toluene 0.620 U 1.00 0.310 ug/L 04/21/10

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 04/21/10

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 04/21/10

Trichloroethene 0.620 U 1.00 0.310 ug/L 04/21/10

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 04/21/10

Vinyl chloride 0.620 U 1.00 0.310 ug/L 04/21/10

Xylenes (total) 1.88 U 3.00 0.940 ug/L 04/21/10

Surrogates 

1,2-Dichloroethane-D4 <surr> 99.7 73-120 % 04/21/10

4-Bromofluorobenzene <surr> 99.8 76-120 % 04/21/10

Toluene-d8 <surr> 101 80-120 % 04/21/10

Instrument

Method

Batch VMS11176

SW8260B

HP 5890 Series II MS1 VJA

59 of 97
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Prep

957825 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20584

SW5030B

04/22/2010

QC results affect the following production samples:

1101584007

Parameter Results LOQ/CL Units

Analysis

DL Date

Volatile Gas Chromatography/Mass Spectroscopy

Naphthalene 1.24 U 2.00 0.620 ug/L 04/22/10

Surrogates 

1,2-Dichloroethane-D4 <surr> 97.7 73-120 % 04/22/10

4-Bromofluorobenzene <surr> 99 76-120 % 04/22/10

Toluene-d8 <surr> 100 80-120 % 04/22/10

Instrument

Method

Batch VMS11182

SW8260B

HP 5890 Series II MS1 VJA

60 of 97
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Prep

956902 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX22498

SW3520C

04/16/2010

QC results affect the following production samples:

1101584001

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

1-Methylnaphthalene LCS 0.424 85 ( 42-92 ) 0.5 ug/L 04/26/2010

2-Methylnaphthalene LCS 0.370 74 ( 45-89 ) 0.5 ug/L 04/26/2010

Acenaphthene LCS 0.416 83 ( 45-93 ) 0.5 ug/L 04/26/2010

Acenaphthylene LCS 0.457 92 ( 50-101 ) 0.5 ug/L 04/26/2010

Anthracene LCS 0.484 97 ( 55-105 ) 0.5 ug/L 04/26/2010

Benzo(a)Anthracene LCS 0.478 96 ( 55-120 ) 0.5 ug/L 04/26/2010

Benzo[a]pyrene LCS 0.404 81 ( 57-110 ) 0.5 ug/L 04/26/2010

Benzo[b]Fluoranthene LCS 0.487 97 ( 45-120 ) 0.5 ug/L 04/26/2010

Benzo[g,h,i]perylene LCS 0.400 80 ( 49-116 ) 0.5 ug/L 04/26/2010

Benzo[k]fluoranthene LCS 0.430 86 ( 56-112 ) 0.5 ug/L 04/26/2010

Chrysene LCS 0.508 102 ( 56-109 ) 0.5 ug/L 04/26/2010

Dibenzo[a,h]anthracene LCS 0.447 89 ( 54-113 ) 0.5 ug/L 04/26/2010

Fluoranthene LCS 0.494 99 ( 58-109 ) 0.5 ug/L 04/26/2010

Fluorene LCS 0.453 91 ( 50-98 ) 0.5 ug/L 04/26/2010

Indeno[1,2,3-c,d] pyrene LCS 0.427 85 ( 55-111 ) 0.5 ug/L 04/26/2010

Naphthalene LCS 0.355 71 ( 44-89 ) 0.5 ug/L 04/26/2010

Phenanthrene LCS 0.506 101 ( 50-104 ) 0.5 ug/L 04/26/2010

Pyrene LCS 0.483 97 ( 56-105 ) 0.5 ug/L 04/26/2010

Surrogates 

Terphenyl-d14 <surr> LCS 94 ( 50-126 ) 04/26/2010

61 of 97
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Prep

956902 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX22498

SW3520C

04/16/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Batch

Method

Instrument

XMS5373

8270D SIMS

HP 6890/5973 MS SVQA

62 of 97
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Prep

956904 Lab Control Sample

956905 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX22499

SW3520C

04/16/2010

QC results affect the following production samples:

1101584004, 1101584005, 1101584006, 1101584007, 1101584008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

63 of 97
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Prep

956904 Lab Control Sample

956905 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX22499

SW3520C

04/16/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

1-Methylnaphthalene LCS 0.462 92 ( 42-92 ) * 0.5 ug/L 04/23/2010

LCSD 0.453 91 2 (< 30 ) 0.5 ug/L 04/23/2010

2-Methylnaphthalene LCS 0.449 90 ( 45-89 ) * 0.5 ug/L 04/23/2010

LCSD 0.462 92 * 3 (< 30 ) 0.5 ug/L 04/23/2010

Acenaphthene LCS 0.476 95 ( 45-93 ) * 0.5 ug/L 04/23/2010

LCSD 0.449 90 6 (< 30 ) 0.5 ug/L 04/23/2010

Acenaphthylene LCS 0.483 97 ( 50-101 ) 0.5 ug/L 04/23/2010

LCSD 0.461 92 5 (< 30 ) 0.5 ug/L 04/23/2010

Anthracene LCS 0.505 101 ( 55-105 ) 0.5 ug/L 04/23/2010

LCSD 0.477 95 6 (< 30 ) 0.5 ug/L 04/23/2010

Benzo(a)Anthracene LCS 0.562 112 ( 55-120 ) 0.5 ug/L 04/23/2010

LCSD 0.542 108 4 (< 30 ) 0.5 ug/L 04/23/2010

Benzo[a]pyrene LCS 0.508 102 ( 57-110 ) 0.5 ug/L 04/23/2010

LCSD 0.517 103 2 (< 30 ) 0.5 ug/L 04/23/2010

Benzo[b]Fluoranthene LCS 0.566 113 ( 45-120 ) 0.5 ug/L 04/23/2010

LCSD 0.550 110 3 (< 30 ) 0.5 ug/L 04/23/2010

Benzo[g,h,i]perylene LCS 0.544 109 ( 49-116 ) 0.5 ug/L 04/23/2010

LCSD 0.580 116 6 (< 30 ) 0.5 ug/L 04/23/2010

Benzo[k]fluoranthene LCS 0.547 109 ( 56-112 ) 0.5 ug/L 04/23/2010

LCSD 0.547 109 0 (< 30 ) 0.5 ug/L 04/23/2010

Chrysene LCS 0.562 112 ( 56-109 ) * 0.5 ug/L 04/23/2010

LCSD 0.551 110 * 2 (< 30 ) 0.5 ug/L 04/23/2010

Dibenzo[a,h]anthracene LCS 0.540 108 ( 54-113 ) 0.5 ug/L 04/23/2010

LCSD 0.580 116 * 7 (< 30 ) 0.5 ug/L 04/23/2010

Fluoranthene LCS 0.565 113 ( 58-109 ) * 0.5 ug/L 04/23/2010

LCSD 0.577 115 * 2 (< 30 ) 0.5 ug/L 04/23/2010

Fluorene LCS 0.482 97 ( 50-98 ) 0.5 ug/L 04/23/2010

LCSD 0.465 93 4 (< 30 ) 0.5 ug/L 04/23/2010

64 of 97
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Prep

956904 Lab Control Sample

956905 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX22499

SW3520C

04/16/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Indeno[1,2,3-c,d] pyrene LCS 0.542 108 ( 55-111 ) 0.5 ug/L 04/23/2010

LCSD 0.582 116 * 7 (< 30 ) 0.5 ug/L 04/23/2010

Naphthalene LCS 0.404 81 ( 44-89 ) 0.5 ug/L 04/23/2010

LCSD 0.402 80 1 (< 30 ) 0.5 ug/L 04/23/2010

Phenanthrene LCS 0.515 103 ( 50-104 ) 0.5 ug/L 04/23/2010

LCSD 0.491 98 5 (< 30 ) 0.5 ug/L 04/23/2010

Pyrene LCS 0.543 109 ( 56-105 ) * 0.5 ug/L 04/23/2010

LCSD 0.550 110 * 1 (< 30 ) 0.5 ug/L 04/23/2010

Surrogates 

Terphenyl-d14 <surr> LCS 100 ( 50-126 ) 04/23/2010

LCSD 105 5 04/23/2010

Batch

Method

Instrument

XMS5372

8270D SIMS

HP 6890/5973 MS SVQA

65 of 97
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Prep

957071 Lab Control Sample

957072 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20571

SW5030B

04/16/2010

QC results affect the following production samples:

1101584001, 1101584004, 1101584005, 1101584006, 1101584007, 1101584008, 1101584009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Fuels Department

Gasoline Range Organics LCS 216 108 ( 79-108 ) 200 ug/L 04/16/2010

LCSD 205 102 5 (< 20 ) 200 ug/L 04/16/2010

Surrogates 

4-Bromofluorobenzene <surr> LCS 108 ( 50-150 ) 04/16/2010

LCSD 105 3 04/16/2010

Batch

Method

Instrument

VFC9900

SW8015C

HP 5890 Series II PID+FID VCA

66 of 97
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Prep

957190 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

MXX22905

SW3010A

04/19/2010

QC results affect the following production samples:

1101584001, 1101584004, 1101584005, 1101584006, 1101584007, 1101584008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Metals by ICP/MS

Lead LCS 1010 101 ( 80-120 ) 1000 ug/L 04/21/2010

Batch

Method

Instrument

MMS6398

SW6020

Perkin Elmer Sciex ICP-MS P3

67 of 97
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Prep

957640 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20578

SW5030B

04/21/2010

QC results affect the following production samples:

1101584001, 1101584004, 1101584005, 1101584006, 1101584007, 1101584008, 1101584009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

68 of 97
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Prep

957640 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20578

SW5030B

04/21/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

1,1,1,2-Tetrachloroethane LCS 27.5 92 ( 80-120 ) 30 ug/L 04/21/2010

1,1,1-Trichloroethane LCS 31.2 104 ( 80-122 ) 30 ug/L 04/21/2010

1,1,2,2-Tetrachloroethane LCS 32.4 108 ( 76-123 ) 30 ug/L 04/21/2010

1,1,2-Trichloroethane LCS 29.7 99 ( 77-120 ) 30 ug/L 04/21/2010

1,1-Dichloroethane LCS 32.2 107 ( 80-120 ) 30 ug/L 04/21/2010

1,1-Dichloroethene LCS 33.9 113 ( 76-130 ) 30 ug/L 04/21/2010

1,1-Dichloropropene LCS 31.7 106 ( 80-122 ) 30 ug/L 04/21/2010

1,2,3-Trichlorobenzene LCS 28.1 94 ( 77-120 ) 30 ug/L 04/21/2010

1,2,3-Trichloropropane LCS 30.9 103 ( 80-120 ) 30 ug/L 04/21/2010

1,2,4-Trichlorobenzene LCS 29.4 98 ( 80-120 ) 30 ug/L 04/21/2010

1,2,4-Trimethylbenzene LCS 30.6 102 ( 80-125 ) 30 ug/L 04/21/2010

1,2-Dibromo-3-chloropropane LCS 31.4 105 ( 73-130 ) 30 ug/L 04/21/2010

1,2-Dibromoethane LCS 30.4 101 ( 80-120 ) 30 ug/L 04/21/2010

1,2-Dichlorobenzene LCS 29.3 98 ( 80-120 ) 30 ug/L 04/21/2010

1,2-Dichloroethane LCS 31.9 106 ( 80-129 ) 30 ug/L 04/21/2010

1,2-Dichloropropane LCS 31.3 104 ( 80-121 ) 30 ug/L 04/21/2010

1,3,5-Trimethylbenzene LCS 30.8 103 ( 80-128 ) 30 ug/L 04/21/2010

1,3-Dichlorobenzene LCS 29.6 99 ( 80-120 ) 30 ug/L 04/21/2010

1,3-Dichloropropane LCS 29.1 97 ( 80-121 ) 30 ug/L 04/21/2010

1,4-Dichlorobenzene LCS 30.1 100 ( 80-120 ) 30 ug/L 04/21/2010

1-Chlorohexane LCS 47.9 106 ( 70-125 ) 45 ug/L 04/21/2010

69 of 97
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Prep

957640 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20578

SW5030B

04/21/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

2,2-Dichloropropane LCS 33.6 112 ( 80-132 ) 30 ug/L 04/21/2010

2-Butanone (MEK) LCS 102 113 ( 66-136 ) 90 ug/L 04/21/2010

2-Chlorotoluene LCS 30.4 101 ( 80-125 ) 30 ug/L 04/21/2010

4-Chlorotoluene LCS 30.8 103 ( 79-128 ) 30 ug/L 04/21/2010

4-Isopropyltoluene LCS 29.4 98 ( 80-125 ) 30 ug/L 04/21/2010

4-Methyl-2-pentanone (MIBK) LCS 93.9 104 ( 69-134 ) 90 ug/L 04/21/2010

Acetone LCS 93.6 104 ( 50-135 ) 90 ug/L 04/21/2010

Benzene LCS 32.0 107 ( 80-120 ) 30 ug/L 04/21/2010

Bromobenzene LCS 29.8 99 ( 80-120 ) 30 ug/L 04/21/2010

Bromochloromethane LCS 30.6 102 ( 77-129 ) 30 ug/L 04/21/2010

Bromodichloromethane LCS 29.7 99 ( 80-120 ) 30 ug/L 04/21/2010

Bromoform LCS 27.0 90 ( 80-120 ) 30 ug/L 04/21/2010

Bromomethane LCS 26.9 90 ( 30-140 ) 30 ug/L 04/21/2010

Carbon tetrachloride LCS 30.7 102 ( 80-126 ) 30 ug/L 04/21/2010

Chlorobenzene LCS 29.7 99 ( 80-120 ) 30 ug/L 04/21/2010

Chloroethane LCS 30.7 102 ( 67-133 ) 30 ug/L 04/21/2010

Chloroform LCS 31.4 105 ( 80-124 ) 30 ug/L 04/21/2010

Chloromethane LCS 32.0 107 ( 67-125 ) 30 ug/L 04/21/2010

cis-1,2-Dichloroethene LCS 32.1 107 ( 80-125 ) 30 ug/L 04/21/2010

cis-1,3-Dichloropropene LCS 29.7 99 ( 80-120 ) 30 ug/L 04/21/2010

70 of 97
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Prep

957640 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20578

SW5030B

04/21/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Dibromochloromethane LCS 27.7 92 ( 80-120 ) 30 ug/L 04/21/2010

Dibromomethane LCS 32.4 108 ( 80-120 ) 30 ug/L 04/21/2010

Dichlorodifluoromethane LCS 30.5 102 ( 62-153 ) 30 ug/L 04/21/2010

Ethylbenzene LCS 29.6 99 ( 80-120 ) 30 ug/L 04/21/2010

Hexachlorobutadiene LCS 26.3 88 ( 77-125 ) 30 ug/L 04/21/2010

Isopropylbenzene (Cumene) LCS 29.0 97 ( 80-121 ) 30 ug/L 04/21/2010

Methylene chloride LCS 30.1 100 ( 63-131 ) 30 ug/L 04/21/2010

Methyl-t-butyl ether LCS 49.5 110 ( 80-120 ) 45 ug/L 04/21/2010

Naphthalene LCS 30.1 100 ( 75-120 ) 30 ug/L 04/21/2010

n-Butylbenzene LCS 31.1 104 ( 80-124 ) 30 ug/L 04/21/2010

n-Propylbenzene LCS 30.8 103 ( 80-129 ) 30 ug/L 04/21/2010

o-Xylene LCS 29.3 98 ( 80-120 ) 30 ug/L 04/21/2010

P & M -Xylene LCS 60.8 101 ( 80-120 ) 60 ug/L 04/21/2010

sec-Butylbenzene LCS 29.1 97 ( 80-120 ) 30 ug/L 04/21/2010

Styrene LCS 29.7 99 ( 80-120 ) 30 ug/L 04/21/2010

tert-Butylbenzene LCS 30.1 100 ( 80-122 ) 30 ug/L 04/21/2010

Tetrachloroethene LCS 29.0 97 ( 79-122 ) 30 ug/L 04/21/2010

Toluene LCS 30.2 101 ( 77-120 ) 30 ug/L 04/21/2010

trans-1,2-Dichloroethene LCS 33.0 110 ( 79-132 ) 30 ug/L 04/21/2010

trans-1,3-Dichloropropene LCS 27.9 93 ( 80-124 ) 30 ug/L 04/21/2010

Trichloroethene LCS 31.4 105 ( 80-125 ) 30 ug/L 04/21/2010

71 of 97
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Prep

957640 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20578

SW5030B

04/21/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Trichlorofluoromethane LCS 31.0 103 ( 68-145 ) 30 ug/L 04/21/2010

Vinyl chloride LCS 29.5 98 ( 72-145 ) 30 ug/L 04/21/2010

Xylenes (total) LCS 90.1 100 ( 80-120 ) 90 ug/L 04/21/2010

Surrogates 

1,2-Dichloroethane-D4 <surr> LCS 98 ( 73-120 ) 04/21/2010

4-Bromofluorobenzene <surr> LCS 102 ( 76-120 ) 04/21/2010

Toluene-d8 <surr> LCS 97 ( 80-120 ) 04/21/2010

Batch

Method

Instrument

VMS11176

SW8260B

HP 5890 Series II MS1 VJA

72 of 97
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Prep

957826 Lab Control Sample

957827 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20584

SW5030B

04/22/2010

QC results affect the following production samples:

1101584007

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Naphthalene LCS 29.2 97 ( 75-120 ) 30 ug/L 04/22/2010

LCSD 31.2 104 7 (< 20 ) 30 ug/L 04/22/2010

Surrogates 

1,2-Dichloroethane-D4 <surr> LCS 98 ( 73-120 ) 04/22/2010

LCSD 96 1 04/22/2010

4-Bromofluorobenzene <surr> LCS 98 ( 76-120 ) 04/22/2010

LCSD 97 0 04/22/2010

Toluene-d8 <surr> LCS 97 ( 80-120 ) 04/22/2010

LCSD 97 1 04/22/2010

Batch

Method

Instrument

VMS11182

SW8260B

HP 5890 Series II MS1 VJA

73 of 97
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Prep

958549 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX22502

SW3520C

04/19/2010

QC results affect the following production samples:

1101584001, 1101584004, 1101584005, 1101584006, 1101584007, 1101584008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Semivolatile Organic Fuels Department

Diesel Range Organics LCS 4.00 80 ( 75-125 ) 5 mg/L 04/28/2010

Surrogates 

5a Androstane <surr> LCS 82 ( 60-120 ) 04/28/2010

Batch

Method

Instrument

XFC9164

SW8015C

HP 7890A FID SV E R

74 of 97
Matrix

SGS Ref.# Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Original

Prep

1101584002 Billable Matrix Spike

1101584003 Billable Matrix Spike Dup.

1101584001

Water (Surface, Eff., Ground)

MXX22905

3010 H20 Digest for Metals ICP-MS

04/19/2010

QC results affect the following production samples:

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Dissolved Metals by ICP/MS

Lead BMS (0.620) U 969 97 ( 80-120 ) 1000 ug/L 04/21/2010

BMSD 994 99 3 (< 15 ) 1000 ug/L 04/21/2010

Batch

Method

Instrument

MMS6398

SW6020

Perkin Elmer Sciex ICP-MS P3

Volatile Fuels Department

Gasoline Range Organics BMS (60.0) U 475 106 ( 79-108 ) 450 ug/L 04/16/2010

BMSD 487 108 3 (< 20 ) 450 ug/L 04/16/2010

Surrogates 

4-Bromofluorobenzene <surr> BMS 58.9 118 ( 50-150 ) 04/16/2010

BMSD 56.1 112 5 04/16/2010

Batch

Method

Instrument

VFC9900

SW8015C

HP 5890 Series II PID+FID VCA

Semivolatile Organic Fuels Department

Diesel Range Organics BMS (0.320) U 4.9 91 ( 75-125 ) 5.38 mg/L 04/28/2010

BMSD 4.55 87 8 (< 30 ) 5.26 mg/L 04/28/2010

Surrogates 

5a Androstane <surr> BMS .104 97 ( 50-150 ) 04/28/2010

BMSD 0.0993 94 5 04/28/2010

Batch

Method

Instrument

XFC9164

SW8015C

HP 7890A FID SV E R

Volatile Gas Chromatography/Mass Spectroscopy

75 of 97
Matrix

SGS Ref.# Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Original

Prep

1101584002 Billable Matrix Spike

1101584003 Billable Matrix Spike Dup.

1101584001

Water (Surface, Eff., Ground)

VXX20578

Volatiles Extraction AFCEE 3.1 8260 (

04/21/2010

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

1,1,1,2-Tetrachloroethane BMS (0.300) U 26 87 ( 80-120 ) 30.0 ug/L 04/21/2010

BMSD 27.8 93 7 (< 20 ) 30.0 ug/L 04/21/2010

1,1,1-Trichloroethane BMS (0.620) U 31.1 104 ( 80-122 ) 30.0 ug/L 04/21/2010

BMSD 31.0 103 0 (< 20 ) 30.0 ug/L 04/21/2010

1,1,2,2-Tetrachloroethane BMS (0.300) U 27.9 93 ( 76-123 ) 30.0 ug/L 04/21/2010

BMSD 31.0 103 10 (< 20 ) 30.0 ug/L 04/21/2010

1,1,2-Trichloroethane BMS (0.620) U 27.9 93 ( 77-120 ) 30.0 ug/L 04/21/2010

BMSD 30.1 100 8 (< 20 ) 30.0 ug/L 04/21/2010

1,1-Dichloroethane BMS (0.620) U 31.1 104 ( 80-120 ) 30.0 ug/L 04/21/2010

BMSD 32.1 107 3 (< 20 ) 30.0 ug/L 04/21/2010

1,1-Dichloroethene BMS (0.620) U 32.9 110 ( 76-130 ) 30.0 ug/L 04/21/2010

BMSD 32.4 108 1 (< 20 ) 30.0 ug/L 04/21/2010

1,1-Dichloropropene BMS (0.620) U 30.8 103 ( 80-122 ) 30.0 ug/L 04/21/2010

BMSD 31.3 104 2 (< 20 ) 30.0 ug/L 04/21/2010

1,2,3-Trichlorobenzene BMS (0.620) U 27.1 90 ( 77-120 ) 30.0 ug/L 04/21/2010

BMSD 28.9 96 6 (< 20 ) 30.0 ug/L 04/21/2010

1,2,3-Trichloropropane BMS (0.620) U 27 90 ( 80-120 ) 30.0 ug/L 04/21/2010

BMSD 29.8 99 10 (< 20 ) 30.0 ug/L 04/21/2010

1,2,4-Trichlorobenzene BMS (0.620) U 28.4 95 ( 80-120 ) 30.0 ug/L 04/21/2010

BMSD 29.6 99 4 (< 20 ) 30.0 ug/L 04/21/2010

1,2,4-Trimethylbenzene BMS (0.620) U 29 97 ( 80-125 ) 30.0 ug/L 04/21/2010

BMSD 30.5 102 5 (< 20 ) 30.0 ug/L 04/21/2010

1,2-Dibromo-3-chloropropane BMS (1.24) U 26.9 90 ( 73-130 ) 30.0 ug/L 04/21/2010

BMSD 30.8 103 13 (< 20 ) 30.0 ug/L 04/21/2010

1,2-Dibromoethane BMS (0.620) U 28.2 94 ( 80-120 ) 30.0 ug/L 04/21/2010

BMSD 30.4 101 7 (< 20 ) 30.0 ug/L 04/21/2010

1,2-Dichlorobenzene BMS (0.620) U 27.9 93 ( 80-120 ) 30.0 ug/L 04/21/2010

BMSD 29.0 97 4 (< 20 ) 30.0 ug/L 04/21/2010

1,2-Dichloroethane BMS (0.300) U 29.5 98 ( 80-129 ) 30.0 ug/L 04/21/2010

BMSD 31.0 103 5 (< 20 ) 30.0 ug/L 04/21/2010

1,2-Dichloropropane BMS (0.620) U 30.1 100 ( 80-121 ) 30.0 ug/L 04/21/2010

BMSD 31.7 106 5 (< 20 ) 30.0 ug/L 04/21/2010

1,3,5-Trimethylbenzene BMS (0.620) U 29.1 97 ( 80-128 ) 30.0 ug/L 04/21/2010

BMSD 30.8 103 6 (< 20 ) 30.0 ug/L 04/21/2010

1,3-Dichlorobenzene BMS (0.620) U 28.6 96 ( 80-120 ) 30.0 ug/L 04/21/2010

BMSD 29.8 99 4 (< 20 ) 30.0 ug/L 04/21/2010

1,3-Dichloropropane BMS (0.240) U 27 90 ( 80-121 ) 30.0 ug/L 04/21/2010

BMSD 29.0 97 7 (< 20 ) 30.0 ug/L 04/21/2010

1,4-Dichlorobenzene BMS (0.300) U 29.1 97 ( 80-120 ) 30.0 ug/L 04/21/2010

BMSD 30.2 101 4 (< 20 ) 30.0 ug/L 04/21/2010

76 of 97
Matrix

SGS Ref.# Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Original

Prep

1101584002 Billable Matrix Spike

1101584003 Billable Matrix Spike Dup.

1101584001

Water (Surface, Eff., Ground)

VXX20578

Volatiles Extraction AFCEE 3.1 8260 (

04/21/2010

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

1-Chlorohexane BMS (0.620) U 45.3 101 ( 70-125 ) 45.0 ug/L 04/21/2010

BMSD 48.1 107 6 (< 20 ) 45.0 ug/L 04/21/2010

2,2-Dichloropropane BMS (0.620) U 30.5 102 ( 80-132 ) 30.0 ug/L 04/21/2010

BMSD 34.3 114 12 (< 20 ) 30.0 ug/L 04/21/2010

2-Butanone (MEK) BMS (6.20) U 83.8 93 ( 66-136 ) 90.0 ug/L 04/21/2010

BMSD 96.5 107 14 (< 20 ) 90.0 ug/L 04/21/2010

2-Chlorotoluene BMS (0.620) U 28.7 96 ( 80-125 ) 30.0 ug/L 04/21/2010

BMSD 30.3 101 6 (< 20 ) 30.0 ug/L 04/21/2010

4-Chlorotoluene BMS (0.620) U 29 97 ( 79-128 ) 30.0 ug/L 04/21/2010

BMSD 30.9 103 6 (< 20 ) 30.0 ug/L 04/21/2010

4-Isopropyltoluene BMS (0.620) U 28.2 94 ( 80-125 ) 30.0 ug/L 04/21/2010

BMSD 29.3 98 4 (< 20 ) 30.0 ug/L 04/21/2010

4-Methyl-2-pentanone (MIBK) BMS (6.20) U 80.3 89 ( 69-134 ) 90.0 ug/L 04/21/2010

BMSD 89.9 100 11 (< 20 ) 90.0 ug/L 04/21/2010

Acetone BMS (6.20) U 77.7 86 ( 50-135 ) 90.0 ug/L 04/21/2010

BMSD 84.5 94 8 (< 20 ) 90.0 ug/L 04/21/2010

Benzene BMS (0.240) U 30.3 101 ( 80-120 ) 30.0 ug/L 04/21/2010

BMSD 31.3 104 3 (< 20 ) 30.0 ug/L 04/21/2010

Bromobenzene BMS (0.620) U 28.6 95 ( 80-120 ) 30.0 ug/L 04/21/2010

BMSD 29.8 99 4 (< 20 ) 30.0 ug/L 04/21/2010

Bromochloromethane BMS (0.620) U 29.8 99 ( 77-129 ) 30.0 ug/L 04/21/2010

BMSD 30.1 100 1 (< 20 ) 30.0 ug/L 04/21/2010

Bromodichloromethane BMS (0.300) U 28.7 96 ( 80-120 ) 30.0 ug/L 04/21/2010

BMSD 30.1 100 5 (< 20 ) 30.0 ug/L 04/21/2010

Bromoform BMS (0.620) U 26 87 ( 80-120 ) 30.0 ug/L 04/21/2010

BMSD 27.5 92 6 (< 20 ) 30.0 ug/L 04/21/2010

Bromomethane BMS (1.88) U 34.1 114 ( 30-140 ) 30.0 ug/L 04/21/2010

BMSD 34.5 115 1 (< 20 ) 30.0 ug/L 04/21/2010

Carbon tetrachloride BMS (0.620) U 31 103 ( 80-126 ) 30.0 ug/L 04/21/2010

BMSD 31.2 104 0 (< 20 ) 30.0 ug/L 04/21/2010

Chlorobenzene BMS (0.300) U 29.2 97 ( 80-120 ) 30.0 ug/L 04/21/2010

BMSD 30.5 102 5 (< 20 ) 30.0 ug/L 04/21/2010

Chloroethane BMS (0.620) U 28.8 96 ( 67-133 ) 30.0 ug/L 04/21/2010

BMSD 30.0 100 4 (< 20 ) 30.0 ug/L 04/21/2010

Chloroform BMS (0.600) U 30.9 103 ( 80-124 ) 30.0 ug/L 04/21/2010

BMSD 31.5 105 2 (< 20 ) 30.0 ug/L 04/21/2010

Chloromethane BMS (0.620) U 28.7 96 ( 67-125 ) 30.0 ug/L 04/21/2010

BMSD 30.5 102 6 (< 20 ) 30.0 ug/L 04/21/2010

cis-1,2-Dichloroethene BMS (0.620) U 31.5 105 ( 80-125 ) 30.0 ug/L 04/21/2010

BMSD 32.3 108 3 (< 20 ) 30.0 ug/L 04/21/2010

77 of 97
Matrix

SGS Ref.# Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Original

Prep

1101584002 Billable Matrix Spike

1101584003 Billable Matrix Spike Dup.

1101584001

Water (Surface, Eff., Ground)

VXX20578

Volatiles Extraction AFCEE 3.1 8260 (

04/21/2010

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

cis-1,3-Dichloropropene BMS (0.300) U 28.5 95 ( 80-120 ) 30.0 ug/L 04/21/2010

BMSD 30.4 101 7 (< 20 ) 30.0 ug/L 04/21/2010

Dibromochloromethane BMS (0.300) U 26.9 90 ( 80-120 ) 30.0 ug/L 04/21/2010

BMSD 28.3 94 5 (< 20 ) 30.0 ug/L 04/21/2010

Dibromomethane BMS (0.620) U 30.9 103 ( 80-120 ) 30.0 ug/L 04/21/2010

BMSD 32.2 107 4 (< 20 ) 30.0 ug/L 04/21/2010

Dichlorodifluoromethane BMS (0.620) U 25.9 86 ( 62-153 ) 30.0 ug/L 04/21/2010

BMSD 26.4 88 2 (< 20 ) 30.0 ug/L 04/21/2010

Ethylbenzene BMS (0.620) U 28.3 94 ( 80-120 ) 30.0 ug/L 04/21/2010

BMSD 29.8 99 5 (< 20 ) 30.0 ug/L 04/21/2010

Hexachlorobutadiene BMS (0.620) U 26.6 89 ( 77-125 ) 30.0 ug/L 04/21/2010

BMSD 27.4 91 3 (< 20 ) 30.0 ug/L 04/21/2010

Isopropylbenzene (Cumene) BMS (0.620) U 28.3 94 ( 80-121 ) 30.0 ug/L 04/21/2010

BMSD 29.6 99 5 (< 20 ) 30.0 ug/L 04/21/2010

Methylene chloride BMS (2.00) U 29.7 99 ( 63-131 ) 30.0 ug/L 04/21/2010

BMSD 30.3 101 2 (< 20 ) 30.0 ug/L 04/21/2010

Methyl-t-butyl ether BMS (3.00) U 44.4 99 ( 80-120 ) 45.0 ug/L 04/21/2010

BMSD 47.8 106 7 (< 20 ) 45.0 ug/L 04/21/2010

Naphthalene BMS (1.24) U 27 90 ( 75-120 ) 30.0 ug/L 04/21/2010

BMSD 30.6 102 13 (< 20 ) 30.0 ug/L 04/21/2010

n-Butylbenzene BMS (0.620) U 29.1 97 ( 80-124 ) 30.0 ug/L 04/21/2010

BMSD 30.7 102 5 (< 20 ) 30.0 ug/L 04/21/2010

n-Propylbenzene BMS (0.620) U 29.1 97 ( 80-129 ) 30.0 ug/L 04/21/2010

BMSD 30.6 102 5 (< 20 ) 30.0 ug/L 04/21/2010

o-Xylene BMS (0.620) U 28.3 95 ( 80-120 ) 30.0 ug/L 04/21/2010

BMSD 29.6 99 4 (< 20 ) 30.0 ug/L 04/21/2010

P & M -Xylene BMS (1.24) U 58.5 98 ( 80-120 ) 60.0 ug/L 04/21/2010

BMSD 61.1 102 4 (< 20 ) 60.0 ug/L 04/21/2010

sec-Butylbenzene BMS (0.620) U 27.6 92 ( 80-120 ) 30.0 ug/L 04/21/2010

BMSD 29.2 97 6 (< 20 ) 30.0 ug/L 04/21/2010

Styrene BMS (0.620) U 28.2 94 ( 80-120 ) 30.0 ug/L 04/21/2010

BMSD 30.0 100 6 (< 20 ) 30.0 ug/L 04/21/2010

tert-Butylbenzene BMS (0.620) U 28.7 96 ( 80-122 ) 30.0 ug/L 04/21/2010

BMSD 30.0 100 4 (< 20 ) 30.0 ug/L 04/21/2010

Tetrachloroethene BMS (0.620) U 29.1 97 ( 79-122 ) 30.0 ug/L 04/21/2010

BMSD 29.4 98 1 (< 20 ) 30.0 ug/L 04/21/2010

Toluene BMS (0.620) U 29.4 98 ( 77-120 ) 30.0 ug/L 04/21/2010

BMSD 30.8 103 5 (< 20 ) 30.0 ug/L 04/21/2010

trans-1,2-Dichloroethene BMS (0.620) U 32.4 108 ( 79-132 ) 30.0 ug/L 04/21/2010

BMSD 32.6 109 0 (< 20 ) 30.0 ug/L 04/21/2010

78 of 97
Matrix

SGS Ref.# Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Original

Prep

1101584002 Billable Matrix Spike

1101584003 Billable Matrix Spike Dup.

1101584001

Water (Surface, Eff., Ground)

VXX20578

Volatiles Extraction AFCEE 3.1 8260 (

04/21/2010

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

trans-1,3-Dichloropropene BMS (0.620) U 25.4 85 ( 80-124 ) 30.0 ug/L 04/21/2010

BMSD 29.1 97 14 (< 20 ) 30.0 ug/L 04/21/2010

Trichloroethene BMS (0.620) U 30.4 101 ( 80-125 ) 30.0 ug/L 04/21/2010

BMSD 31.0 103 2 (< 20 ) 30.0 ug/L 04/21/2010

Trichlorofluoromethane BMS (0.620) U 30.3 101 ( 68-145 ) 30.0 ug/L 04/21/2010

BMSD 30.1 100 1 (< 20 ) 30.0 ug/L 04/21/2010

Vinyl chloride BMS (0.620) U 27.3 91 ( 72-145 ) 30.0 ug/L 04/21/2010

BMSD 28.2 94 3 (< 20 ) 30.0 ug/L 04/21/2010

Xylenes (total) BMS (1.88) U 86.8 97 ( 80-120 ) 90.0 ug/L 04/21/2010

BMSD 90.7 101 4 (< 20 ) 90.0 ug/L 04/21/2010

Surrogates 

1,2-Dichloroethane-D4 <surr> BMS 29.5 98 ( 73-120 ) 04/21/2010

BMSD 29.1 97 1 04/21/2010

4-Bromofluorobenzene <surr> BMS 29.8 99 ( 76-120 ) 04/21/2010

BMSD 30.0 100 1 04/21/2010

Toluene-d8 <surr> BMS 29.3 98 ( 80-120 ) 04/21/2010

BMSD 29.4 98 1 04/21/2010

Batch

Method

Instrument

VMS11176

SW8260B

HP 5890 Series II MS1 VJA

Polynuclear Aromatics GC/MS

79 of 97
Matrix

SGS Ref.# Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Original

Prep

1101584002 Billable Matrix Spike

1101584003 Billable Matrix Spike Dup.

1101584001

Water (Surface, Eff., Ground)

XXX22498

3520 Liquid/Liquid Ext for 8270 SIM

04/16/2010

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Polynuclear Aromatics GC/MS

1-Methylnaphthalene BMS (0.0330) U .504 95* ( 42-92 ) 0.532 ug/L 04/26/2010

BMSD 0.471 88 7 (< 30 ) 0.538 ug/L 04/26/2010

2-Methylnaphthalene BMS (0.0330) U .445 84 ( 45-89 ) 0.532 ug/L 04/26/2010

BMSD 0.435 81 2 (< 30 ) 0.538 ug/L 04/26/2010

Acenaphthene BMS (0.0330) U .522 98* ( 45-93 ) 0.532 ug/L 04/26/2010

BMSD 0.472 88 10 (< 30 ) 0.538 ug/L 04/26/2010

Acenaphthylene BMS (0.0330) U .53 100 ( 50-101 ) 0.532 ug/L 04/26/2010

BMSD 0.490 91 8 (< 30 ) 0.538 ug/L 04/26/2010

Anthracene BMS (0.0330) U .584 110* ( 55-105 ) 0.532 ug/L 04/26/2010

BMSD 0.529 98 10 (< 30 ) 0.538 ug/L 04/26/2010

Benzo(a)Anthracene BMS (0.0330) U .561 106 ( 55-120 ) 0.532 ug/L 04/26/2010

BMSD 0.520 97 8 (< 30 ) 0.538 ug/L 04/26/2010

Benzo[a]pyrene BMS (0.0330) U .491 92 ( 57-110 ) 0.532 ug/L 04/26/2010

BMSD 0.451 84 9 (< 30 ) 0.538 ug/L 04/26/2010

Benzo[b]Fluoranthene BMS (0.0330) U .589 111 ( 45-120 ) 0.532 ug/L 04/26/2010

BMSD 0.535 100 10 (< 30 ) 0.538 ug/L 04/26/2010

Benzo[g,h,i]perylene BMS (0.0330) U .495 93 ( 49-116 ) 0.532 ug/L 04/26/2010

BMSD 0.454 85 9 (< 30 ) 0.538 ug/L 04/26/2010

Benzo[k]fluoranthene BMS (0.0330) U .544 102 ( 56-112 ) 0.532 ug/L 04/26/2010

BMSD 0.489 91 11 (< 30 ) 0.538 ug/L 04/26/2010

Chrysene BMS (0.0330) U .615 116* ( 56-109 ) 0.532 ug/L 04/26/2010

BMSD 0.565 105 9 (< 30 ) 0.538 ug/L 04/26/2010

Dibenzo[a,h]anthracene BMS (0.0330) U .538 101 ( 54-113 ) 0.532 ug/L 04/26/2010

BMSD 0.501 93 7 (< 30 ) 0.538 ug/L 04/26/2010

Fluoranthene BMS (0.0330) U .571 107 ( 58-109 ) 0.532 ug/L 04/26/2010

BMSD 0.544 101 5 (< 30 ) 0.538 ug/L 04/26/2010

Fluorene BMS (0.0330) U .553 104* ( 50-98 ) 0.532 ug/L 04/26/2010

BMSD 0.495 92 11 (< 30 ) 0.538 ug/L 04/26/2010

Indeno[1,2,3-c,d] pyrene BMS (0.0330) U .512 96 ( 55-111 ) 0.532 ug/L 04/26/2010

BMSD 0.468 87 9 (< 30 ) 0.538 ug/L 04/26/2010

Naphthalene BMS (0.0682) U .426 80 ( 44-89 ) 0.532 ug/L 04/26/2010

BMSD 0.415 77 3 (< 30 ) 0.538 ug/L 04/26/2010

Phenanthrene BMS (0.0330) U .601 113* ( 50-104 ) 0.532 ug/L 04/26/2010

BMSD 0.549 102 9 (< 30 ) 0.538 ug/L 04/26/2010

Pyrene BMS (0.0330) U .559 105 ( 56-105 ) 0.532 ug/L 04/26/2010

BMSD 0.528 98 6 (< 30 ) 0.538 ug/L 04/26/2010

Surrogates 

Terphenyl-d14 <surr> BMS .531 100 ( 50-126 ) 04/26/2010

BMSD 0.505 94 5 04/26/2010

80 of 97
Matrix

SGS Ref.# Printed Date/Time 04/30/2010 10:42

Batch

Method

Date

Original

Prep

1101584002 Billable Matrix Spike

1101584003 Billable Matrix Spike Dup.

1101584001

Water (Surface, Eff., Ground)

XXX22498

3520 Liquid/Liquid Ext for 8270 SIM

04/16/2010

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Polynuclear Aromatics GC/MS

Batch

Method

Instrument

XMS5373

8270D SIMS

HP 6890/5973 MS SVQA

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