### Instructions for using the Emission Test Reporting Template for the Primary Aluminum Test Program

This Information Collection Request (ICR) spreadsheet is intended to be used to report emissions data from primary aluminum reduction facilities as an alternative to the Electronic Reporting Tool (ERT), as well as in cases where the test methods arenot currently supported by the ERT.**Data for multiple process units should be reported by using separate copies of the appropriate tabs of this spreadsheet.**  **Please Do Not delete rows or columns , addition of rows and columns is appropriate**  **as necessary.**
**Emission Data Worksheets** The emission data worksheets are provided for each test required for this testing program, although all facilities are not required to conduct all of the tests. On each worksheet,please enter process unit operating informationduring sampling and emission test results. The emission test results to be entered depends on the constituent. **Source Operating Information** 1. Please provide the Exhaust Flow Rate (acfm and dscfm) and the Exhaust Temperature (deg F). 2. Please provide the values of all requested parametersfor each of the sample testing periods in the appropriate cells. 3. Please provide any other supporting informationor commentsin the Other Supporting Informationfield.

# Primary Aluminum Testing: Hexavalent Chromium

**Parent company**

**name:** Alcoa 

## Facility **address:** Alcoa Massena Operations

East Plant 

## Description of source tested: Line 1 Method 14 Downcomer Massena, New York 13662

**Test Method Used (SW-846 M0061)**  **Data Flag**

**(A DL, BDL, DLL)**  **Test Method Comments**

1 4/30/2013 1043 4/30/2013 1501 SW-846 M0061 ADL 2 4/30/2013 1610 4/30/2013 2026 SW-846 M0061 ADL 3 5/1/2013 825 5/1/2013 1230 SW-846 M0061 BDL

**Moisture (%) CO2 (%)**  **O2 (%) Flow (acfm)**  **Temperature (°F)** 1 0.7 0.0 20.9 NA 83 2 1.0 0.0 20.9 NA 85 3 0.9 0.0 20.9 NA 85

**lb/hr lb/ton of** 

**throughput Ma** **terial Rate**  **(tons/hour)** 1 6.37E-04 1.24E-04Aluminum 5.12 2 2.06E-03 4.02E-04Aluminum 5.12 3 [<8.66E-04] [<1.69E-04]Aluminum 5.12 **Run Number**  **Calculated Emission Rate Production or Throughput**  3968169 Flow Rate is for total potroom 3584106 Flow Rate is for total potroom 3552880 Flow Rate is for total potroom 4.29E-02 5.30E-02 [<6.51E-02]

**Run Number**  **Exhaust Gas Other Supporting Information**  **Flow (dscfm) Run**  **Number Test Start** 

**Date Test Start** 

**Time Test End** 

**Date Test End** 

**Time Hexavalent Chromium Emission Test Results** 

**Concentration (ug/dscm)** 

# Primary Aluminum Testing: HAP Metals

**Parent company name:** Alcoa 

### Facility address: Alcoa Massena Operations East Plant 

### Description of source: Line 1 Downcomer Massena, New York 13662

**Pollutant Concentration** 

**(ug/dscm) Test Method Used** 

**(e.g. Method 29) Data Flag** 

**(A DL, BDL, DLL)**  **Test Method Comments**



### 1 30-Apr 1043 30-Apr 1501 

### Antimony [<0.16906] Method 29 BDL 

### 2 30-Apr 1610 30-Apr 2026

### Antimony [<0.16818] Method 29 BDL 

### 3 1-May 825 1-May 1230

### Antimony [<0.16909] Method 29 BDL 

### 1 30-Apr 1043 30-Apr 1501 

### Arsenic 2.46201 Method 29 ADL 2 30-Apr 1610 30-Apr 2026

### Arsenic 2.24943 Method 29 ADL 3 1-May 825 1-May 1230

### Arsenic 3.33951 Method 29 ADL 1 30-Apr 1043 30-Apr 1501 

### Beryllium [<0.04227] Method 29 BDL 2 30-Apr 1610 30-Apr 2026

### Beryllium [<0.04205] Method 29 BDL 3 1-May 825 1-May 1230 

### Beryllium [<0.04227] Method 29 BDL 1 30-Apr 1043 30-Apr 1501 

### Cadmium 0.06023 Method 29 ADL 2 30-Apr 1610 30-Apr 2026

### Cadmium 0.07989 Method 29 ADL 3 1-May 825 1-May 1230

### Cadmium 0.09089 Method 29 ADL 1 30-Apr 1043 30-Apr 1501 

### Chromium 0.85695 Method 29 ADL 2 30-Apr 1610 30-Apr 2026

### Chromium 7.71535 Method 29 ADL 3 1-May 825 1-May 1230

### Chromium 6.67902 Method 29 ADL 1 30-Apr 1043 30-Apr 1501 

### Cobalt 0.20393 Method 29 ADL 2 30-Apr 1610 30-Apr 2026

### Cobalt 0.30063 Method 29 ADL 3 1-May 825 1-May 1230

### Cobalt 0.40370Method 29 ADL 1 30-Apr 1043 30-Apr 1501 

### Lead 1.27010Method 29 ADL 2 30-Apr 1610 30-Apr 2026

### Lead 1.33915 Method 29 ADL 3 1-May 825 1-May 1230 

### Lead 1.42669 Method 29 ADL 1 30-Apr 1043 30-Apr 1501 

### Manganese 0.89816Method 29 ADL 2 30-Apr 1610 30-Apr 2026

### Manganese 3.46875 Method 29 ADL 3 1-May 825 1-May 1230 

### Manganese 3.38178Method 29 ADL 1 30-Apr 1043 30-Apr 1501 

### Nickel 10.21786Method 29 ADL 2 30-Apr 1610 30-Apr 2026

### Nickel 22.07388Method 29 ADL 3 1-May 825 1-May 1230 

### Nickel 21.98158Method 29 ADL 1 30-Apr 1043 30-Apr 1501 

### Selenium [<0.42266] Method 29 BDL 2 30-Apr 1610 30-Apr 2026

### Selenium [<0.42045] Method 29 BDL 3 1-May 825 1-May 1230

### Selenium [<0.42272] Method 29 BDL 1 30-Apr 1043 30-Apr 1501 

### Mercury 0.00412 Method 29 ADL 2 30-Apr 1610 30-Apr 2026

### Mercury 0.00673 Method 29 ADL 3 1-May 825 1-May 1230 

### Mercury 0.00486Method 29 ADL **Multiple Metals Emission Test Results Run**  **Number Test Start** 

**Date Test Start** 

**Time Test End** 

**Date Test End** 

**Time**

# Primary Aluminum Testing: HAP Metals

**Parent company name:** Alcoa 

### Facility address: Alcoa Massena Operations East Plant 

### Description of source: Line 1 Downcomer Massena, New York 13662

**lb/hr lb/ton of** 

**throughput Material**  **Rate (tons/hour)**  **Moisture**

**(%) CO** **2**

**(%) O** **2**

**(%) Flow** 

**(acfm) Flow** 

**(dscfm) Temp** 

**( °F)**  

### 1 [<0.00251] [<0.00049] Aluminum 5.12 0.8 0 20.9 NA 3965024 83 

### 2 [<0.00227] [<0.00044] Aluminum 5.12 0.6 0 20.9 NA 3601902 85 

### 3 [<0.00225] [<0.00044] Aluminum 5.12 1 0 20.9 NA 3550762 87 

### 1 0.03657 0.00714

### Aluminum 5.12 0.8 0 20.9 NA 3965024 83 

### 2 0.03035 0.00593

### Aluminum 5.12 0.6 0 20.9 NA 3601902 85 

### 3 0.04442 0.00868

### Aluminum 5.12 1 0 20.9 NA 3550762 87 

### 1 [<0.00063] [<0.00012] Aluminum 5.12 0.8 0 20.9 NA 3965024 83 

### 2 [<0.00057] [<0.00011] Aluminum 5.12 0.6 0 20.9 NA 3601902 85 

### 3 [<0.00056] [<0.00011] Aluminum 5.12 1 0 20.9 NA 3550762 87 

### 1 0.00089 0.00017

### Aluminum 5.12 0.8 0 20.9 NA 3965024 83 

### 2 0.00108 0.00021 

### Aluminum 5.12 0.6 0 20.9 NA 3601902 85 

### 3 0.00121 0.00024

### Aluminum 5.12 1 0 20.9 NA 3550762 87 

### 1 0.01273 0.00249

### Aluminum 5.12 0.8 0 20.9 NA 3965024 83 

### 2 0.10409 0.02033

### Aluminum 5.12 0.6 0 20.9 NA 3601902 85 

### 3 0.08883 0.01735

### Aluminum 5.12 1 0 20.9 NA 3550762 87 

### 1 0.00303 0.00059

### Aluminum 5.12 0.8 0 20.9 NA 3965024 83 

### 2 0.00406 0.00079

### Aluminum 5.12 0.6 0 20.9 NA 3601902 85 

### 3 0.00537 0.00105

### Aluminum 5.12 1 0 20.9 NA 3550762 87 

### 1 0.01886 0.00368

### Aluminum 5.12 0.8 0 20.9 NA 3965024 83 

### 2 0.01807 0.00353

### Aluminum 5.12 0.6 0 20.9 NA 3601902 85 

### 3 0.01898 0.00371 

### Aluminum 5.12 1 0 20.9 NA 3550762 87 

### 1 0.01334 0.00261 

### Aluminum 5.12 0.8 0 20.9 NA 3965024 83 

### 2 0.04680 0.00914

### Aluminum 5.12 0.6 0 20.9 NA 3601902 85 

### 3 0.04498 0.00878

### Aluminum 5.12 1 0 20.9 NA 3550762 87 

### 1 0.15176 0.02964

### Aluminum 5.12 0.8 0 20.9 NA 3965024 83 

### 2 0.29782 0.05817

### Aluminum 5.12 0.6 0 20.9 NA 3601902 85 

### 3 0.29236 0.05710

### Aluminum 5.12 1 0 20.9 NA 3550762 87 

### 1 [<0.00628] [<0.00123] 

### Aluminum 5.12 0.8 0 20.9 NA 3965024 83 

### 2 [<0.00567] [<0.00111] 

### Aluminum 5.12 0.6 0 20.9 NA 3601902 85 

### 3 [<0.00562] [<0.00110] 

### Aluminum 5.12 1 0 20.9 NA 3550762 87 

### 1 0.00006 0.000012

### Aluminum 5.12 0.8 0 20.9 NA 3965024 83 

### 2 0.00009 0.000018

### Aluminum 5.12 0.6 0 20.9 NA 3601902 85 

### 3 0.00006 0.000013

### Aluminum 5.12 1 0 20.9 NA 3550762 87 **Run Number**  **Calculated Emission Rate Production or Throughput**  **Exhaust Gas Other Supporting Information**