Quarterly Groundwater Monitoring Report – Outside 

(Non-Tunnel) Wells 

Red Hill Fuel Storage Facility 

Pearl Harbor, Oahu, Hawaii 

Latitude: 21o

22’15” N 

Longitude: 157o

53’33” W 

HDOH Facility ID No. 9-102271 

HDOH Release ID No. 99051, 010011, 020028 

September 2009 

Prepared by: 

TEC Inc. 

1001 Bishop St. Suite 1400 

American Savings Bank Tower 

Honolulu, Hawaii 96813 

Prepared for: 

Commander 

Navy Region Hawaii 

Environmental Department, Code N45 

850 Ticonderoga Street, Suite 110 

Pearl Harbor, Hawaii 96860-5101 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility September 2009 

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i 

Table of Contents 

Table of Contents ............................................................................................................................. i

Executive Summary ......................................................................................................................... 1

1.0 Introduction.......................................................................................................................... 3

1.1 Project Objective .............................................................................................................. 3

1.2 Previous Reports .............................................................................................................. 3

1.3 Background ...................................................................................................................... 4

1.3.1 Site Description ......................................................................................................... 4

1.3.2 Facility Information .................................................................................................. 4

1.3.3 UST Information ....................................................................................................... 5

1.4 Regulatory Updates .......................................................................................................... 5

2.0 Sample Collection and Analyses .......................................................................................... 6

2.1 Monitoring Well Purging ................................................................................................. 6

2.2 Groundwater Sample Collection ...................................................................................... 6

2.3 Groundwater Sample Analyses ........................................................................................ 7

3.1 August 2009 Sample Analytical Results .......................................................................... 7

4.0 Summary and Conclusions ................................................................................................... 7

5.0 References .......................................................................................................................... 10

List of Tables 

Table 1 Monitoring Well Information ........................................................................................5 

Table 2 Analytical Results for Quarterly Groundwater Sampling (August 4, 2009) .................8 

List of Figures 

Figure 1 Groundwater Monitoring Well Locations ......................................................................9 

List of Appendices 

Appendix A – Laboratory Analytical Reports 

Appendix B – Monitoring Well Construction Logs
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility September 2009 

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1 

Executive Summary 

This quarterly groundwater monitoring report presents the results of groundwater sampling (i.e., 

RHMW04, and OWDFMW01) conducted on August 4, 2009 at the United States (US) Navy 

Bulk Fuel Storage Facility at Red Hill, Oahu, Hawaii (the Facility). Due to access issues, 

sampling of the Halawa Deep Well 2253-03 (2253-03) was postponed (see Figure 1). The 

sampling and reporting was conducted by TEC Inc. (TEC) for the Fleet and Industrial Supply 

Center (FISC) at Pearl Harbor, Hawaii. This report is part of a series of quarterly groundwater 

monitoring reports, supplemental to the groundwater reports for the groundwater monitoring 

wells within the Facility, provided by the US Navy to the State of Hawaii Department of Health 

(HDOH) in accordance with HDOH’s release response requirements. Currently, there are 18 

active and 2 inactive, 12.5 million gallon, field-constructed underground storage tanks (USTs) 

located at the Facility. 

Background 

In 2002, the US Navy installed a groundwater monitoring well (currently named RHMW01) into 

the basal aquifer, directly down-gradient from the Facility, within the lower access tunnel. 

Groundwater samples from this well indicated that petroleum from the Facility has migrated to 

the basal aquifer (AMEC, 2002). In 2005, the US Navy began quarterly monitoring of the 

aquifer to protect their down-gradient drinking water resource associated with the US Navy Well 

2254-01. US Navy Well 2254-01 is located approximately 3,000 feet down-gradient from the 

Facility USTs and provides approximately 24 % of the potable water to the Pearl Harbor Water 

System (PHWS). 

By September 2005, the US Navy had installed two more groundwater monitoring wells 

(RHMW02 and RHMW03) within the Facility UST system and a groundwater monitoring well 

within the US Navy Well 2254-01 infiltration gallery (RHMW2254-01). Since 2005, these wells 

have been sampled quarterly for Total Petroleum Hydrocarbons (TPH) quantified as DieselRange Organics (DRO) and Gasoline Range Organics (GRO), Volatile Organic Compounds 

(VOCs), Polynuclear Aromatic Hydrocarbons (PAHs), and dissolved lead. 

In response to increasing concentrations of contaminants of potential concern at the groundwater 

monitoring wells within the facility (specifically RHMW02) during 2008, plans were made to 

conduct quarterly sampling at the following monitoring well locations: 

 RHMW04, up-gradient of the Facility; 

 Oily Waste Disposal Facility monitoring well 01 (OWDFMW01), down-gradient of the 

Facility; and 

 Halawa Deep Well 2253-03 (2253-03) 

During the summer and fall of 2008, HDOH updated their Environmental Action Levels (EALs), 

which resulted in significant changes to the action levels associated with methylnaphthalenes. 

The HDOH Drinking Water toxicity EAL for these compounds was 240 g/L. This 

concentration assumed that methylnaphthalenes were not human carcinogens. Once evidence 

emerged and was accepted by the US Environmental Protection Agency (USEPA) that 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility September 2009 

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methylnaphthalenes are carcinogenic to humans, HDOH adopted more rigorous EALs of 4.7 

g/L for 1-methylnaphthalene and 24 g/L for 2-methylnaphthalene (HDOH, 2008). 

The HDOH Drinking Water EAL for naphthalene was also updated during this process. 

Previously, HDOH based their naphthalene EAL on USEPA Region 9 Preliminary Remediation 

Goal (USEPA PRG) of 6.2 g/L, which is associated with a non-cancer Hazard Index of 1. In 

deference to the California Department of Public Health’s Drinking Water Notification Levels, 

(HDOH, 2008) HDOH updated their naphthalene drinking water EAL to 17 g/L. 

Finally, the HDOH Drinking Water EAL for TPH-DRO was increased from 100 g/L to 210 

g/L, although the Groundwater Gross Contamination EAL for TPH-DRO remains 100 g/L. 

Current Results 

On August 4, 2009, two groundwater samples (i.e., RHMW04, and OWDFMW01), along with 

the required quality control samples (duplicate, matrix spike, spike duplicate, and trip blank) 

were collected for analysis. Samples were analyzed for TPH-DRO, TPH-GRO, VOCs, PAHs, 

and dissolved lead. 

No HDOH Drinking Water EALs were exceeded and no contaminants of concern were detected 

above the laboratory method detection limit (MDL), except for benzene. At RHMW04, benzene 

was detected below the laboratory reporting limit (RL) but above the MDL, at an estimated 

concentration of 0.25 μg/L in the duplicate sample only. Benzene was also detected in 

OWDFMW01 at 0.47 μg/L, just above the RL. The HDOH Drinking Water EAL and 

groundwater Gross Contamination EAL for benzene are 5 μg/L and 170 μg/L, respectively. 

Conclusions and Recommendations 

Based on the August 2009 sampling event, there is no indication of significant contaminant 

migration up-gradient and down-gradient of the Facility. Quarterly groundwater sampling for 

TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved lead will continue at the Facility until such 

time that data indicates that a different monitoring plan is warranted. 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility September 2009 

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1.0 Introduction

This report presents the results of the first groundwater sampling event, conducted in August 

2009 at two groundwater monitoring wells (i.e., RHMW04, and OWDFMW01), up-gradient and 

down-gradient from the Red Hill Fuel Storage Facility, Oahu, Hawaii (hereafter referred to as 

“the Facility”). The Facility consists of 18 active and 2 inactive USTs operated by FISC, Pearl 

Harbor. This groundwater sampling and analysis event is supplemental to the quarterly 

groundwater sampling and analysis at groundwater monitoring wells within the Facility (i.e., part 

of the groundwater monitoring program for the UST site in response to past UST releases, 

previous environmental investigations, and recommendations from the HDOH). 

1.1 Project Objective 

This groundwater sampling project was performed to evaluate the presence of chemicals of 

potential concern in groundwater up-gradient and down-gradient from the Facility. The project 

was conducted to ensure the Navy remains in compliance with HDOH UST release response 

requirements. The groundwater sampling program followed the procedures described in Red 

Hill Bulk Fuel Storage Facility Groundwater Protection Plan [TEC Inc. (TEC), 2008], also 

referred to as “the Plan”. 

This groundwater sampling event was conducted by TEC under US Navy Contract Number 

N47408-04-D-8514, Task Order No. 54, Amendment/Modification No. 01. 

1.2 Previous Reports 

This is the first groundwater sampling event for monitoring wells RHMW04 and OWDFMW01. 

Due to access issues, sampling of the Halawa Deep Well 2253-03 (2253-03) was postponed. 

This is a quarterly sampling event that is being conducted to supplement the quarterly 

groundwater sampling and analysis at groundwater monitoring wells within the Facility, which 

began in 2005. The following groundwater monitoring reports were previously submitted to the 

HDOH, for groundwater monitoring wells within the Facility: 

1. Groundwater Sampling Report, First Quarter 2005 (submitted April 2005); 

2. Groundwater Sampling Report, Second Quarter 2005 (submitted August 2005); 

3. Groundwater Sampling Report, Third Quarter 2005 (submitted November 2005); 

4. Groundwater Sampling Report, Fourth Quarter 2005 (submitted February 2006); 

5. Groundwater Monitoring Results, July 2006 (submitted September 2006); 

6. Groundwater Monitoring Results, December 2006 (submitted January 2007); 

7. Groundwater Monitoring Results, March 2007 (submitted May 2007); 

8. Groundwater Monitoring Results, June 2007 (submitted August 2007); 

9. Groundwater Monitoring Results, September 2007 (submitted October 2007); 

10. Groundwater Monitoring Results, January 2008 (submitted March 2008); 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility September 2009 

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11. Groundwater Monitoring Results, April 2008 (submitted May 2008); 

12. Groundwater Monitoring Results, July 2008 (submitted October 2008); 

13. Groundwater Monitoring Results, October and December 2008 (submitted February 

2009); 

14. Groundwater Monitoring Results, February 2009 (submitted May 2009); 

15. Groundwater Monitoring Results, May 2009 (submitted July 2009); and 

16. Groundwater Monitoring Results, July 2009 (submitted September 2009) 

1.3 Background 

The following sections provide a description of the site and information on the Facility and USTs. 

1.3.1 Site Description 

The Facility is located in Halawa Heights on Oahu, Hawaii. Land adjacent to the north of the 

Facility is occupied by Halawa Correctional Facility and private businesses. Land to the south 

and west of the Facility includes the Coast Guard Reservation. Moanalua Valley is located east 

of the Facility (Dawson, 2006). 

The Navy Public Works Department operates a potable water infiltration tunnel approximately 

1,550 feet hydraulically down-gradient from the Facility (Dawson, 2006). The US Navy Well 

2254-01 is located approximately 3,000 feet down-gradient (west) of the Facility and provides 

approximately 24% of the potable water to the Pearl Harbor Water System, which serves 

approximately 52,200 military consumers (TEC, 2008). 

1.3.2 Facility Information 

The Facility consists of 18 active and 2 inactive USTs operated by Navy FISC Pearl Harbor. 

Each UST has a capacity of 12.5 million gallons. The Facility is located approximately 100 feet 

above the basal aquifer (Dawson, 2006). 

In 2002, the US Navy installed a groundwater monitoring well (currently named RHMW01) into 

the basal aquifer, directly down-gradient from the Facility, within the lower access tunnel. 

Groundwater samples from this well indicated that petroleum from the Facility has migrated to 

the basal aquifer (AMEC, 2002). In 2005, the US Navy began quarterly monitoring of the 

aquifer to protect their down-gradient drinking water resource associated with the US Navy Well 

2254-01. US Navy Well 2254-01 is located approximately 3,000 feet down-gradient from the 

Facility USTs and provides approximately 24 % of the potable water to the PHWS. 

By September 2005, the US Navy had installed two more groundwater monitoring wells 

(RHMW02 and RHMW03) within the Facility UST system, a background groundwater 

monitoring well (RHMW04) up-gradient from the Facility adjacent to the US Navy Firing Range, 

and a groundwater monitoring well within the US Navy Well 2254-01 infiltration gallery 

(RHMW2254-01). Since 2005, RHMW01, RHMW02, RHMW03, and RHMW2254-01 have 

been sampled quarterly for TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved lead. 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility September 2009 

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Due to increasing concentrations of contaminants of potential concern at the groundwater 

monitoring wells within the Facility (specifically RHMW02) during 2008, response measures 

were warranted. In April 2009, another groundwater monitoring well (RHMW05) was installed 

down-gradient from the USTs, within the lower access tunnel between RHMW01 and 

RHMW2254-01. It was installed to identify the extent of contaminant migration down-gradient 

before it reaches the infiltration gallery at RHMW2254-01. 

Additionally, plans were made to sample three monitoring wells RHMW04, OWDFMW01, and 

monitoring well 2253-03. RHMW04 is adjacent to the US Navy Firing Range, geographically 

up-gradient of the USTs. It was installed to provide geochemistry for water moving through the 

basal aquifer beneath the Facility. OWDFMW01 (originally known as MW08) was installed into 

the basal aquifer in 1998 for a Phase II Remedial Investigation/ Feasibility Study for the Red Hill 

Oily Waste Disposal Facility (Earth Tech Inc., 2000). It is located geographically down-gradient 

of the USTs and US Navy Well 2254-01. Monitoring well 2253-03 is controlled by the State of 

Hawaii Commission on Water Resource Management. It is located cross-gradient of the Facility, 

between the Facility and the municipal drinking water supply well run by the City and County of 

Honolulu Board of Water Supply (Halawa Shaft pumping station 2354-01). 

Table 1 summarizes basic groundwater monitoring well information, Figure 1 shows 

groundwater monitoring well locations, and Appendix B includes the well construction logs for 

RHMW04 and OWDFMW01. 

Table 1. Monitoring Well Information 

Groundwater Well TOC Elevation 

(ft msl) 

DTW (ft) TD (ft) 

RHMW04 313.03 293 320 

OWDFMW01 138.94 120 142.8 

Halawa Deep (2253-03) 225 210 1,575 

Notes: 

 DTW - Distance to water 

 TD - Total depth of well 

 TOC - Top of casing 

ft – Feet 

ft msl - Feet from mean sea level 

1.3.3 UST Information 

The USTs were constructed in the early 1940s. The tanks were constructed of steel and currently 

contain Jet Propulsion (JP)–5 fuel and F-76 (diesel marine fuel). Previously, several tanks stored 

Navy Special Fuel Oil, Navy Distillate, aviation gasoline, and motor gasoline. Each tank 

measures approximately 245 feet in height and 100 feet in diameter. The upper domes of the 

tanks lie at depths varying between approximately 100 feet and 200 feet below the existing 

ground surface (TEC, 2006). 

1.4 Regulatory Updates 

During the summer and fall of 2008, HDOH updated their EALs, which resulted in significant 

changes to the action levels associated with methylnaphthalenes. The drinking water toxicity 

EAL for these compounds was 240 g/L. This concentration presumed that methylnaphthalenes 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility September 2009 

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6 

were non-carcinogenic. Evidence that they are human carcinogens has now been accepted by the 

US Environmental Protection Agency (USEPA). As a result, HDOH adopted more rigorous 

EALs of 4.7 g/L for 1-methylnaphthalene and 24 g/L for 2-methylnaphthalene, corresponding 

to a residential tap water scenario, and a 1 in a million cancer risk (HDOH, 2008). 

The drinking water EAL for naphthalene has also been updated during this process. Previously, 

HDOH based their naphthalene EAL on USEPA Region 9 Preliminary Remediation Goal 

(USEPA PRG) of 6.2 g/L, which is associated with a non-cancer Hazard Index of 1. HDOH 

has updated their naphthalene drinking water EAL to 17 g/L, in deference to the California 

Department of Public Health’s Drinking Water Notification Levels, a Hazard Index of 2.7 

(HDOH, 2008). 

Finally, the HDOH Drinking Water EAL for TPH-DRO was increased from 100 g/L to 210 

g/L, although the HDOH Groundwater Gross Contamination EAL for TPH-DRO remains 100 

g/L. 

2.0 Sample Collection and Analyses 

Field activities relating to groundwater sample collection were conducted on August 4, 2009. 

Groundwater samples were collected from two monitoring wells, one downgradient of the 

Facility and one upgradient (OWDFMW01 and RHMW04, respectively). Groundwater 

monitoring well 2253-03 was not sampled during this round of sampling due to problems 

obtaining access. Sampling and analysis were conducted according to Red Hill Bulk Fuel 

Storage Facility Groundwater Protection Plan (TEC, 2008). A total of five samples were 

collected as follows: 

 one environmental sample from RHMW04 and OWDFMW01; 

 one duplicate sample from RHMW04 (sampled as RHMWA01 and reported as 

RHMW04D); and 

 one matrix spike and matrix spike duplicate from OWDFMW01. 

2.1 Monitoring Well Purging

The groundwater monitoring wells were purged and sampled using a dedicated pump system. 

Well purging was considered complete when no less than three successive water quality 

parameter measurements had stabilized within approximately 10 percent. Field parameters were 

measured at regular intervals during well purging and included pH, temperature, specific 

conductivity, dissolved oxygen, and turbidity. 

2.2 Groundwater Sample Collection 

Each monitoring well was sampled immediately following purging. Both wells were sampled 

directly from their dedicated bladder pump system. Samples were placed into sampling 

containers with appropriate preservatives [i.e., hydrochloric acid (HCl) for volatile organic 

analysis, nitric acid (HNO3) for dissolved lead]. Dissolved lead samples were filtered in the field 

and placed in preserved bottles. Sample containers were labeled with the date, sample 

identification number, type of analysis, and sampler’s name. The containers were placed on ice 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility September 2009 

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in sample coolers and transported under chain-of-custody procedures to the certified laboratory 

for analysis. 

2.3 Groundwater Sample Analyses 

Groundwater samples were analyzed by SGS Environmental Service, Inc. in Anchorage, Alaska 

for TPH-DRO and TPH-GRO by EPA Method 8015B, VOCs by EPA Method 8260B, PAHs by 

EPA Method 8270C SIM, and dissolved lead by EPA Method 6020. 

3.0 Groundwater Sample Analytical Results 

This section provides a summary of analytical results for groundwater samples collected from 

two monitoring wells, one downgradient of the Facility and one upgradient (OWDFMW01 and 

RHMW04, respectively). Duplicate sample results from monitoring well RHMW04 are reported 

in this document as RHMW04D. A summary of groundwater analytical results for TPH-DRO 

and TPH-GRO, VOCs, PAHs, and dissolved lead is included in Table 2. Complete analytical 

laboratory reports are provided in Appendix A. 

3.1 August 2009 Sample Analytical Results 

All groundwater samples were analyzed for TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved 

lead. The results for each groundwater monitoring well are discussed below. 

RHMW04

Benzene was detected in the duplicate sample at an estimated concentration of 0.25 μg/L (i.e., 

the value is below the laboratory RL, but above the MDL), well below the HDOH Drinking 

Water EAL (i.e., 5 μg/L). Benzene was not detected above the same laboratory MDL in the 

normal sample from RHMW04. No other potential chemical of concern was detected above the 

laboratory MDL (Table 2). 

OWDFMW01

Benzene was detected at 0.47 μg/L just above the RL (i.e., 0.4 μg/L) in OWDFMW01. This 

concentration is well below the HDOH Drinking Water EAL (i.e., 5 μg/L). No other potential 

chemical of concern was detected above the laboratory MDL (Table 2). 

4.0 Summary and Conclusions 

Summary

No potential chemicals of concern were detected above the HDOH Drinking Water or Gross 

Contamination EALs at RHMW04 or OWDFMW01. Only trace detections of benzene were 

detected. 

Conclusions/Recommendations

Based on the August 2009 sampling event, there is no indication of significant contaminant 

migration up-gradient or down-gradient of the Facility.
Table 2. Analytical Results for Quarterly Groundwater Sampling (August 4, 2009)

Red Hill Fuel Storage Facility, Pearl Harbor, Hawaii

Result Q MDL RL Result Q MDL RL Result Q MD

TPH as DIESEL RANGE ORGANICS 210 100 ND U 171 457 ND U 157 419 ND U 16TPH as GASOLINE RANGE ORGANICS 100 100 ND U 30 100 ND U 30 100 ND U 31-METHYLNAPHTHALENE 4.7 10 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.02-METHYLNAPHTHALENE 24 10 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0ACENAPHTHENE 370 20 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0ACENAPHTHYLENE 240 2000 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0ANTHRACENE 1800 22 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0BENZO(a)ANTHRACENE 0.092 4.7 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0BENZO(a)PYRENE 0.2 0.81 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0BENZO(b)FLUORANTHENE 0.092 0.75 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0BENZO(g,h,i)PERYLENE 1500 0.13 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0BENZO(k)FLUORANTHENE 0.92 0.4 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0CHRYSENE 9.2 1 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0

DIBENZ( h)ANTHRACENE 0 0092 0 52 ND U 0 0164 0 0546 ND U 0 0162 0 0541 ND U 0 0

8015B (Petroleum)

8270C SIM 

(PAHs)

August 4, 2009 Method

HDOH Drinking Water 

EALs1

for Human Toxicity 

UG/L

HDOH Groundwater 

Gross Contamination 

EALs2

UG/L

Chemical

OWDFMW01

UG/L

August 4, 2009 August 4, 

RHMW04

UG/L

RHMW0

UG/L

DIBENZ(a,h)ANTHRACENE 0.0092 0.52 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0FLUORANTHENE 1500 130 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0FLUORENE 240 950 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0INDENO(1,2,3-c,d)PYRENE 0.092 0.095 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0NAPHTHALENE 17 21 ND U 0.0339 0.109 ND U 0.0335 0.108 ND U 0.0PHENANTHRENE 240 410 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.0PYRENE 180 68 ND U 0.0164 0.0546 ND U 0.0162 0.0541 ND U 0.01,1,1,2-TETRACHLOROETHANE 0.52 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.1,1,1-TRICHLOROETHANE 200 970 ND U 0.31 1 ND U 0.31 1 ND U 0.1,1,2,2-TETRACHLOROETHANE 0.067 500 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.1,1,2-TRICHLOROETHANE 5 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.1,1-DICHLOROETHANE 2.4 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.1,2,3-TRICHLOROPROPANE (TCP) 0.6 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.1,2,4-TRICHLOROBENZENE 70 3000 ND U 0.31 1 ND U 0.31 1 ND U 0.1,2-DIBROMO-3-CHLOROPROPANE (DBCP) 0.04 10 ND U 0.62 2 ND U 0.62 2 ND U 0.1,2-DIBROMOETHANE (EDB) 0.0065 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.1,2-DICHLOROBENZENE 600 10 ND U 0.31 1 ND U 0.31 1 ND U 0.1,2-DICHLOROETHANE 0.15 7000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.1,2-DICHLOROPROPANE 5 10 ND U 0.31 1 ND U 0.31 1 ND U 0.1,3-DICHLOROBENZENE 180 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.1 4 DICHLOROBENZENE 1,4-DICHLOROBENZENE 75 5 ND U 0 15 . 0 5. ND U 0 15 . 0 5. ND U 0 

. 

ACETONE 22000 20000 ND U 3.1 10 ND U 3.1 10 ND U 3BENZENE 5 170 0.47 0.12 0.4 ND U 0.12 0.4 0.25 F 0.BROMODICHLOROMETHANE 0.22 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.BROMOFORM 100 510 ND U 0.31 1 ND U 0.31 1 ND U 0.BROMOMETHANE 8.7 50000 ND U 0.94 3 ND U 0.94 3 ND U 0.CARBON TETRACHLORIDE 5 520 ND U 0.31 1 ND U 0.31 1 ND U 0.CHLOROBENZENE 100 50 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.CHLOROETHANE 8600 16 ND U 0.31 1 ND U 0.31 1 ND U 0.CHLOROFORM 70 2400 ND U 0.3 1 ND U 0.3 1 ND U 0CHLOROMETHANE 1.8 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.cis-1,2-DICHLOROETHYLENE 70 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.cis-1,3-DICHLOROPROPENE 0.43 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.DIBROMOCHLOROMETHANE 0.16 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.ETHYLBENZENE 700 30 ND U 0.31 1 ND U 0.31 1 ND U 0.HEXACHLOROBUTADIENE 0.86 6 ND U 0.31 1 ND U 0.31 1 ND U 0.M,P-XYLENE (SUM OF ISOMERS) 10000 20 ND U 0.62 2 ND U 0.62 2 ND U 0.METHYL ETHYL KETONE (2-BUTANONE) 7100 8400 ND U 3.1 10 ND U 3.1 10 ND U 3METHYL ISOBUTYL KETONE (4-METHYL-2-PENTANONE) 2000 1300 ND U 3.1 10 ND U 3.1 10 ND U 3METHYLENE CHLORIDE 4.8 9100 ND U 1 5 ND U 1 5 ND U 1 NAPHTHALENE 17 21 ND U 0.62 2 ND U 0.62 2 ND U 0.

8260B 

(VOCs)

NAPHTHALENE 17 21 ND U 0.62 2 ND U 0.62 2 ND U 0.STYRENE 100 10 ND U 0.31 1 ND U 0.31 1 ND U 0.TETRACHLOROETHYLENE(PCE) 5 170 ND U 0.31 1 ND U 0.31 1 ND U 0.TOLUENE 1000 40 ND U 0.31 1 ND U 0.31 1 ND U 0.trans-1,2-DICHLOROETHENE 100 260 ND U 0.31 1 ND U 0.31 1 ND U 0.TRICHLOROETHYLENE (TCE) 5 310 ND U 0.31 1 ND U 0.31 1 ND U 0.VINYL CHLORIDE 2 3400 ND U 0.31 1 ND U 0.31 1 ND U 0.

6020 LEAD 15 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.

PAHs - Polynuclear aromatic hydrocarbons MDL - Method detection limit

VOCs - Volatile organic compounds RL - Reporting limit

ND - Indicates that the compound was not detected above the stated method detection limit TPH - Total petroleum hydrocarbons 

Q - Data qualifier UG/L - Micrograms per Liter

U - Indicates that the compound was analyzed for but not detected at or above the stated limit

F - Indicates that the compound was identified but the concentration was above the MDL and below the RL

- Result exceeds one or both HDOH EALs

12

Final Drinking Water Action Levels for Human Toxicity, Table D-3a, Screening for Environmental Concerns at Sites with Contaminated Soil and Groundwater, HDOH, 2009Groundwater Gross Contamination Action Levels, Table G-1, Screening for Environmental Concerns at Sites with Contaminated Soil and Groundwater, HDOH, 2009

200

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Red Hill Fuel Storage Facility September 2009 

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5.0 References 

AMEC. Red Hill Bulk Fuel Storage Facility Investigation Report, Prepared for NAVFAC 

Pacific, August 2002. 

Dawson Group, Inc. Fourth Quarter 2005 Groundwater Sampling Report, Red Hill Fuel 

Storage Facility, Hawaii. February 2006. 

Earth Tech, Inc. Remedial Investigation Phase II, Volume I, Technical Report, Red Hill Oily 

Waste Disposal Facility, Halawa, Oahu, Hawaii. September 2000. 

Hawaii Administrative Rules, Title 11, Chapter 281, Subchapter 7. 

HDOH. Screening for Environmental Concerns at Sites with Contaminated Soil and 

Groundwater, Summary Lookup Tables. March 2009. 

HDOH. Use of May 2005 Environmental Action Levels (“EALs”) at Leaking Underground 

Storage Tank Sites. Memo. July 2005. 

HDOH. Evaluation of Environmental Hazards at Sites with Contaminated Soil and 

Groundwater. Summer 2008 (updated October 2008). 

TEC, Inc. Red Hill Bulk Fuel Storage Facility, Final – Addendum Planning Documents, Pearl 

Harbor, Hawaii. May 2006. 

TEC, Inc. Red Hill Bulk Fuel Storage Facility, Final Groundwater Protection Plan, Pearl 

Harbor, Hawaii. January 2008. 
Appendix A 

Laboratory Analytical Reports 
SGS Work Order:

Contents:

Cover Page

Case Narrative

Final Report Pages

Quality Control Summary Forms

Chain of Custody/Sample Receipt Forms

Project:

Client:

SGS North America Inc.

 Alaska Division

Level II Laboratory Data Report

Released by: 

Note:

Unless otherwise noted, all quality assurance/quality control criteria is in compliance with the standards set forth by the proper regulatory authority, the 

SGS Quality Assurance Program Plan, and the National Environmental Accreditation Conference.

3354-003 Red Hill BFSF

The Environmental Company, Inc. (TEC)

1094021

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CASE NARRATIVE Print Date: 8/20/2009

Workorder No.: 1094021

Project Name: 3354-003 Red Hill BFSF

Client Name: The Environmental Company, Inc. (TEC)

Lab Sample ID

Sample Comments

Sample Type Client Sample ID

Refer to the sample receipt form for information on sample condition.

1094021002

8260B - MS/MSD recoveries for chloroethane and bromomethane do not meet QC criteria. These analytes were not 

detected above the PQL in the associated samples

BMS OWDFMW01-WG01 MS

1094021003

8260B - MS/MSD recoveries for chloroethane and bromomethane do not meet QC criteria. These analytes were not 

detected above the PQL in the associated samples

BMSD OWDFMW01-WG01 MSD

915596

8260B - LCS recovery for acetone does not meet QC criteria. This analyte was not detected above the PQL in the 

associated samples

LCS LCS for HBN 218335 [VXX/19797]

915597

8260B - LCS recovery for acetone does not meet QC criteria. This analyte was not detected above the PQL in the 

associated samples

LCSD LCSD for HBN 218335 [VXX/19797

915601

8260B - CCV recoveries for several analytes do not meet QC criteria. These analytes were not detected above the PQL in 

the associated samples

CCV CCV for HBN 218337 [VMS/10724]

915947

8260B - LCS recovery for 1,1-dichloropropene does not meet QC criteria. This analyte was not detected above the PQL in 

the associated samples

LCS LCS for HBN 218403 [VXX/19810]

915948

8260B - LCS recovery for 1,1-dichloropropene does not meet QC criteria. This analyte was not detected above the PQL in 

the associated samples

LCSD LCSD for HBN 218403 [VXX/19810

915950

8260B - CCV recoveries for 1,1-dichloropropene and bromomethane do not meet QC criteria. These analytes were not 

detected above the PQL in the associated samples

CCV CCV for HBN 218404 [VMS/10730]

916342

8260B - CCV recoveries for several analytes do not meet QC criteria. These analytes were not detected above the PQL in 

the associated samples

CCV CCV for HBN 218479 [VMS/10736]

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Report of Manual Integrations Print Date: 8/20/2009 1:51 pm

Laboratory ID Client Sample ID Analytical Batch Method Analyte Reason

914031 LCS for HBN 218011 [XXX/21374] XMS5029 8270D SIMS Benzo[g,h,i]perylene RSP

Manual Integration Reason Code Descriptions

Code Description

O Original Chromatogram

M Modified Chromatogram

SS Skimmed surrogate

BLG Closed baseline gap

RP Reassign peak name

PIR Pattern integration required

IT Included tail

SP Split peak

RSP Removed split peak

FPS Forced peak start/stop

BLC Baseline correction

PNF Peak not found by software

All DRO/RRO analysis are integrated per SOP.

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Laboratory Analytical Report

Project:

Client:

Workorder No.:

The Environmental Company, Inc. (TEC)

1094021

Certification:

I certify that this data package is in compliance with the terms and conditions of the contract, 

both technically and for completeness, other than the conditions noted on the sample data 

sheet(s) and/or the case narrative. This certification applies only to the tested parameters and 

the specific sample(s) received at the laboratory.

1001 Bishop Street, Suite 1400

Honolulu, HI 96813

Attn: Rick Adkisson

T: (808)528-1445 F:(808)528-0768

Tamara Rentz

tamara.rentz@sgs.com

Project Manager

3354-003 Red Hill BFSF

If you have any questions regarding this report, or if we can be of further assistance, please 

contact your SGS Project Manager.

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Enclosed are the analytical results associated with this workorder.

As required by the state of Alaska and the USEPA, a formal Quality Assurance/Quality Control Program is maintained by SGS. A copy of 

our Quality Assurance Plan (QAP), which outlines this program is available at your request.

The Laboratory certification numbers are AK971-05 (DW), UTS-005 (CS) and AK00971 (Micro) for ADEC and AK100001 for NELAP (RCRA 

methods: 1020A, 1311, 6010B, 7470A, 7471A, 9040B, 9045C, 9056, 9060, 8015B, 8021B, 8081A/8082, 8260B, 8270C).

Except as specifically noted, all statements and data in this report are in conformance to the provisions set forth by the SGS QAP, the 

National Environmental Laboratory Accreditation Program and, when applicable, other regulatory authorities.

If you have any questions regarding this report or if we can be of any assistance, please contact your SGS Project Manager at 

907-562-2343. All work is being provided under SGS general terms and conditions (http://www.sgs.com/terms_and_conditions.htm) 

The following descriptors may be found on your report which will serve to further qualify the data.

MDL Method Detection Limit

PQL Practical Quantitation Limit (reporting limit).

CL Control Limit

U Indicates the analyte was analyzed for but not detected.

F Indicates value that is greater than or equal to the MDL.

J The quantitation is an estimation.

ND Indicates the analyte is not detected

B Indicates the analyte is found in a blank associated with the sample.

* The analyte has exceeded allowable regulatory or control limits.

D The analyte concentration is the result of dilution.

GT Greater Than

LT Less Than

Q QC parameter out of acceptance range.

M A matrix effect was present.

E The analyte result is above the calibrated range.

R Rejected

DF Analytical Dilution Factor

JL The analyte was positively identified, but the quantitation is a low estimation.

<Surr> Surrogate QC spiked standard

<Surr/IS> Surrogate / Internal Standard QC spiked standard

QC Quality Control

QA Quality Assurance

MB Method Blank

LCS (D) Laboratory Control Sample (Duplicate)

MS(D) Matrix Spike (Duplicate)

BMS(D) Site Specific Matrix Spike (Duplicate)

RPD Relative Percent Difference

ICV Initial Calibration Verification

CCV Continuous Calibration Verification

MSA Method of Standard Addition

Notes: Soil samples are reported on a dry weight basis unless otherwise specified

Print Date: 8/20/2009

Notes: All DRO/RRO analyses are integrated per SOP.

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SAMPLE SUMMARY

Client Name: The Environmental Company, Inc. (TEC)

Project Name: 3354-003 Red Hill BFSF

Workorder No.: 1094021

Analytical Methods

Method Description Analytical Method

8270 PAH SIM Semi-Vol GC/MS Liq/Liq ext. 8270D SIMS

AFCEE 3.1 8260 (W) SW8260B

Dissolved Metals by ICP-MS SW6020

DRO by 8015B (W) SW8015C

GRO (W) SW8015C

Print Date: 8/20/2009 1:51 pm

Sample ID Cross Reference

Lab Sample ID Client Sample ID

1094021001 OWDFMW01-WG01

1094021002 OWDFMW01-WG01 MS

1094021003 OWDFMW01-WG01 MSD

1094021004 RHMW04-WG01

1094021005 RHMWA01-WG01

1094021006 TB01-WG01

S G S N orth A m erica Inc . A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

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The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: OWDFMW01-WG01

SGS Ref. #: 1094021001 Collection Date/Time: 08/04/09 15:45

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 08/06/09 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS6032 MXX22033

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6032

Analytical Method: SW6020

Analysis Date/Time: 08/18/09 19:35

Prep Batch: MXX22033

Prep Method: SW3010A

Prep Date/Time: 08/12/09 19:00 Container ID:1094021001-G

Dilution Factor: 5 Analyst: NRB

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

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The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: OWDFMW01-WG01

SGS Ref. #: 1094021001 Collection Date/Time: 08/04/09 15:45

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 08/06/09 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 30.0 ug/L 1 VFC9606 VXX19837

4-Bromofluorobenzene <surr> 95.2 50-150 % 1 VFC9606 VXX19837

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9606

Analytical Method: SW8015C

Analysis Date/Time: 08/14/09 17:20

Prep Batch: VXX19837

Prep Method: SW5030B

Prep Date/Time: 08/14/09 13:16 Container ID:1094021001-B

Dilution Factor: 1 Analyst: KPW

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

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The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: OWDFMW01-WG01

SGS Ref. #: 1094021001 Collection Date/Time: 08/04/09 15:45

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 08/06/09 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics ND 0.457 0.171 mg/L 1 XFC8762 XXX21370

5a Androstane <surr> 78.7 50-150 % 1 XFC8762 XXX21370

Batch Information

Initial Prep Wt./Vol.: 875 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8762

Analytical Method: SW8015C

Analysis Date/Time: 08/08/09 11:01

Prep Batch: XXX21370

Prep Method: SW3520C

Prep Date/Time: 08/07/09 09:25 Container ID:1094021001-J

Dilution Factor: 1 Analyst: KDC

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

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The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: OWDFMW01-WG01

SGS Ref. #: 1094021001 Collection Date/Time: 08/04/09 15:45

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 08/06/09 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene 0.470 0.400 0.120 ug/L 1 VMS10730 VXX19810

Toluene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10730 VXX19810

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10730 VXX19810

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10730 VXX19810

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10730 VXX19810

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10730 VXX19810

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

Styrene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

Acetone ND 10.0 3.10 ug/L 1 VMS10730 VXX19810

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10730 VXX19810

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10730 VXX19810

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10730 VXX19810

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10730 VXX19810

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10730 VXX19810

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10730 VXX19810

Chloroform ND 1.00 0.300 ug/L 1 VMS10730 VXX19810

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

Chloromethane ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

Bromomethane ND 3.00 0.940 ug/L 1 VMS10730 VXX19810

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

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The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: OWDFMW01-WG01

SGS Ref. #: 1094021001 Collection Date/Time: 08/04/09 15:45

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 08/06/09 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10730 VXX19810

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10730 VXX19810

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10730 VXX19810

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10730 VXX19810

Naphthalene ND 2.00 0.620 ug/L 1 VMS10730 VXX19810

o-Xylene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

Bromoform ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10730 VXX19810

1,2-Dichloroethane-D4 <surr> 118 73-120 % 1 VMS10730 VXX19810

Toluene-d8 <surr> 99.9 80-120 % 1 VMS10730 VXX19810

4-Bromofluorobenzene <surr> 104 76-120 % 1 VMS10730 VXX19810

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10730

Analytical Method: SW8260B

Analysis Date/Time: 08/13/09 22:27

Prep Batch: VXX19810

Prep Method: SW5030B

Prep Date/Time: 08/13/09 08:26 Container ID:1094021001-A

Dilution Factor: 1 Analyst: SCL

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The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: OWDFMW01-WG01

SGS Ref. #: 1094021001 Collection Date/Time: 08/04/09 15:45

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 08/06/09 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0546 0.0164 ug/L 1 XMS5029 XXX21374

Acenaphthene ND 0.0546 0.0164 ug/L 1 XMS5029 XXX21374

Fluorene ND 0.0546 0.0164 ug/L 1 XMS5029 XXX21374

Phenanthrene ND 0.0546 0.0164 ug/L 1 XMS5029 XXX21374

Anthracene ND 0.0546 0.0164 ug/L 1 XMS5029 XXX21374

Fluoranthene ND 0.0546 0.0164 ug/L 1 XMS5029 XXX21374

Pyrene ND 0.0546 0.0164 ug/L 1 XMS5029 XXX21374

Benzo(a)Anthracene ND 0.0546 0.0164 ug/L 1 XMS5029 XXX21374

Chrysene ND 0.0546 0.0164 ug/L 1 XMS5029 XXX21374

Benzo[b]Fluoranthene ND 0.0546 0.0164 ug/L 1 XMS5029 XXX21374

Benzo[k]fluoranthene ND 0.0546 0.0164 ug/L 1 XMS5029 XXX21374

Benzo[a]pyrene ND 0.0546 0.0164 ug/L 1 XMS5029 XXX21374

Indeno[1,2,3-c,d] pyrene ND 0.0546 0.0164 ug/L 1 XMS5029 XXX21374

Dibenzo[a,h]anthracene ND 0.0546 0.0164 ug/L 1 XMS5029 XXX21374

Benzo[g,h,i]perylene ND 0.0546 0.0164 ug/L 1 XMS5029 XXX21374

Naphthalene ND 0.109 0.0339 ug/L 1 XMS5029 XXX21374

1-Methylnaphthalene ND 0.0546 0.0164 ug/L 1 XMS5029 XXX21374

2-Methylnaphthalene ND 0.0546 0.0164 ug/L 1 XMS5029 XXX21374

Terphenyl-d14 <surr> 102 50-135 % 1 XMS5029 XXX21374

Batch Information

Initial Prep Wt./Vol.: 915 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5029

Analytical Method: 8270D SIMS

Analysis Date/Time: 08/12/09 02:10

Prep Batch: XXX21374

Prep Method: SW3520C

Prep Date/Time: 08/07/09 10:00 Container ID:1094021001-H

Dilution Factor: 1 Analyst: JDH

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The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: RHMW04-WG01

SGS Ref. #: 1094021004 Collection Date/Time: 08/04/09 12:35

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 08/06/09 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS6032 MXX22033

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6032

Analytical Method: SW6020

Analysis Date/Time: 08/18/09 19:48

Prep Batch: MXX22033

Prep Method: SW3010A

Prep Date/Time: 08/12/09 19:00 Container ID:1094021004-G

Dilution Factor: 5 Analyst: NRB

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t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

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The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: RHMW04-WG01

SGS Ref. #: 1094021004 Collection Date/Time: 08/04/09 12:35

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 08/06/09 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 30.0 ug/L 1 VFC9606 VXX19837

4-Bromofluorobenzene <surr> 99.8 50-150 % 1 VFC9606 VXX19837

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9606

Analytical Method: SW8015C

Analysis Date/Time: 08/14/09 16:23

Prep Batch: VXX19837

Prep Method: SW5030B

Prep Date/Time: 08/14/09 13:16 Container ID:1094021004-B

Dilution Factor: 1 Analyst: KPW

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

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The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: RHMW04-WG01

SGS Ref. #: 1094021004 Collection Date/Time: 08/04/09 12:35

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 08/06/09 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics ND 0.419 0.157 mg/L 1 XFC8762 XXX21370

5a Androstane <surr> 82.2 50-150 % 1 XFC8762 XXX21370

Batch Information

Initial Prep Wt./Vol.: 955 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8762

Analytical Method: SW8015C

Analysis Date/Time: 08/08/09 11:38

Prep Batch: XXX21370

Prep Method: SW3520C

Prep Date/Time: 08/07/09 09:25 Container ID:1094021004-J

Dilution Factor: 1 Analyst: KDC

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

15 of 75
The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: RHMW04-WG01

SGS Ref. #: 1094021004 Collection Date/Time: 08/04/09 12:35

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 08/06/09 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10724 VXX19797

Toluene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10724 VXX19797

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10724 VXX19797

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10724 VXX19797

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10724 VXX19797

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10724 VXX19797

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Styrene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Acetone ND 10.0 3.10 ug/L 1 VMS10724 VXX19797

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10724 VXX19797

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10724 VXX19797

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10724 VXX19797

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10724 VXX19797

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10724 VXX19797

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10724 VXX19797

Chloroform ND 1.00 0.300 ug/L 1 VMS10724 VXX19797

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Chloromethane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Bromomethane ND 3.00 0.940 ug/L 1 VMS10724 VXX19797

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

16 of 75
The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: RHMW04-WG01

SGS Ref. #: 1094021004 Collection Date/Time: 08/04/09 12:35

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 08/06/09 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10724 VXX19797

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10724 VXX19797

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10724 VXX19797

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10724 VXX19797

Naphthalene ND 2.00 0.620 ug/L 1 VMS10724 VXX19797

o-Xylene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Bromoform ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,2-Dichloroethane-D4 <surr> 109 73-120 % 1 VMS10724 VXX19797

Toluene-d8 <surr> 99.8 80-120 % 1 VMS10724 VXX19797

4-Bromofluorobenzene <surr> 107 76-120 % 1 VMS10724 VXX19797

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10724

Analytical Method: SW8260B

Analysis Date/Time: 08/13/09 00:01

Prep Batch: VXX19797

Prep Method: SW5030B

Prep Date/Time: 08/12/09 08:21 Container ID:1094021004-A

Dilution Factor: 1 Analyst: SCL

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

17 of 75
The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: RHMW04-WG01

SGS Ref. #: 1094021004 Collection Date/Time: 08/04/09 12:35

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 08/06/09 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0541 0.0162 ug/L 1 XMS5029 XXX21374

Acenaphthene ND 0.0541 0.0162 ug/L 1 XMS5029 XXX21374

Fluorene ND 0.0541 0.0162 ug/L 1 XMS5029 XXX21374

Phenanthrene ND 0.0541 0.0162 ug/L 1 XMS5029 XXX21374

Anthracene ND 0.0541 0.0162 ug/L 1 XMS5029 XXX21374

Fluoranthene ND 0.0541 0.0162 ug/L 1 XMS5029 XXX21374

Pyrene ND 0.0541 0.0162 ug/L 1 XMS5029 XXX21374

Benzo(a)Anthracene ND 0.0541 0.0162 ug/L 1 XMS5029 XXX21374

Chrysene ND 0.0541 0.0162 ug/L 1 XMS5029 XXX21374

Benzo[b]Fluoranthene ND 0.0541 0.0162 ug/L 1 XMS5029 XXX21374

Benzo[k]fluoranthene ND 0.0541 0.0162 ug/L 1 XMS5029 XXX21374

Benzo[a]pyrene ND 0.0541 0.0162 ug/L 1 XMS5029 XXX21374

Indeno[1,2,3-c,d] pyrene ND 0.0541 0.0162 ug/L 1 XMS5029 XXX21374

Dibenzo[a,h]anthracene ND 0.0541 0.0162 ug/L 1 XMS5029 XXX21374

Benzo[g,h,i]perylene ND 0.0541 0.0162 ug/L 1 XMS5029 XXX21374

Naphthalene ND 0.108 0.0335 ug/L 1 XMS5029 XXX21374

1-Methylnaphthalene ND 0.0541 0.0162 ug/L 1 XMS5029 XXX21374

2-Methylnaphthalene ND 0.0541 0.0162 ug/L 1 XMS5029 XXX21374

Terphenyl-d14 <surr> 103 50-135 % 1 XMS5029 XXX21374

Batch Information

Initial Prep Wt./Vol.: 925 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5029

Analytical Method: 8270D SIMS

Analysis Date/Time: 08/12/09 03:54

Prep Batch: XXX21374

Prep Method: SW3520C

Prep Date/Time: 08/07/09 10:00 Container ID:1094021004-H

Dilution Factor: 1 Analyst: JDH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

18 of 75
The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: RHMWA01-WG01

SGS Ref. #: 1094021005 Collection Date/Time: 08/04/09 12:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 08/06/09 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS6032 MXX22033

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6032

Analytical Method: SW6020

Analysis Date/Time: 08/18/09 19:50

Prep Batch: MXX22033

Prep Method: SW3010A

Prep Date/Time: 08/12/09 19:00 Container ID:1094021005-G

Dilution Factor: 5 Analyst: NRB

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

19 of 75
The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: RHMWA01-WG01

SGS Ref. #: 1094021005 Collection Date/Time: 08/04/09 12:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 08/06/09 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 30.0 ug/L 1 VFC9606 VXX19837

4-Bromofluorobenzene <surr> 94.2 50-150 % 1 VFC9606 VXX19837

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9606

Analytical Method: SW8015C

Analysis Date/Time: 08/14/09 16:42

Prep Batch: VXX19837

Prep Method: SW5030B

Prep Date/Time: 08/14/09 13:16 Container ID:1094021005-B

Dilution Factor: 1 Analyst: KPW

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

20 of 75
The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: RHMWA01-WG01

SGS Ref. #: 1094021005 Collection Date/Time: 08/04/09 12:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 08/06/09 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics ND 0.430 0.161 mg/L 1 XFC8762 XXX21370

5a Androstane <surr> 79.9 50-150 % 1 XFC8762 XXX21370

Batch Information

Initial Prep Wt./Vol.: 930 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8762

Analytical Method: SW8015C

Analysis Date/Time: 08/08/09 11:48

Prep Batch: XXX21370

Prep Method: SW3520C

Prep Date/Time: 08/07/09 09:25 Container ID:1094021005-J

Dilution Factor: 1 Analyst: KDC

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

21 of 75
The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: RHMWA01-WG01

SGS Ref. #: 1094021005 Collection Date/Time: 08/04/09 12:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 08/06/09 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene 0.250 J 0.400 0.120 ug/L 1 VMS10724 VXX19797

Toluene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10724 VXX19797

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10724 VXX19797

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10724 VXX19797

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10724 VXX19797

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10724 VXX19797

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Styrene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Acetone ND 10.0 3.10 ug/L 1 VMS10724 VXX19797

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10724 VXX19797

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10724 VXX19797

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10724 VXX19797

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10724 VXX19797

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10724 VXX19797

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10724 VXX19797

Chloroform ND 1.00 0.300 ug/L 1 VMS10724 VXX19797

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Chloromethane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Bromomethane ND 3.00 0.940 ug/L 1 VMS10724 VXX19797

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

22 of 75
The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: RHMWA01-WG01

SGS Ref. #: 1094021005 Collection Date/Time: 08/04/09 12:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 08/06/09 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10724 VXX19797

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10724 VXX19797

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10724 VXX19797

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10724 VXX19797

Naphthalene ND 2.00 0.620 ug/L 1 VMS10724 VXX19797

o-Xylene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Bromoform ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10724 VXX19797

1,2-Dichloroethane-D4 <surr> 106 73-120 % 1 VMS10724 VXX19797

Toluene-d8 <surr> 101 80-120 % 1 VMS10724 VXX19797

4-Bromofluorobenzene <surr> 103 76-120 % 1 VMS10724 VXX19797

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10724

Analytical Method: SW8260B

Analysis Date/Time: 08/13/09 02:49

Prep Batch: VXX19797

Prep Method: SW5030B

Prep Date/Time: 08/12/09 08:21 Container ID:1094021005-A

Dilution Factor: 1 Analyst: SCL

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

23 of 75
The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: RHMWA01-WG01

SGS Ref. #: 1094021005 Collection Date/Time: 08/04/09 12:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 08/06/09 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0556 0.0167 ug/L 1 XMS5029 XXX21374

Acenaphthene ND 0.0556 0.0167 ug/L 1 XMS5029 XXX21374

Fluorene ND 0.0556 0.0167 ug/L 1 XMS5029 XXX21374

Phenanthrene ND 0.0556 0.0167 ug/L 1 XMS5029 XXX21374

Anthracene ND 0.0556 0.0167 ug/L 1 XMS5029 XXX21374

Fluoranthene ND 0.0556 0.0167 ug/L 1 XMS5029 XXX21374

Pyrene ND 0.0556 0.0167 ug/L 1 XMS5029 XXX21374

Benzo(a)Anthracene ND 0.0556 0.0167 ug/L 1 XMS5029 XXX21374

Chrysene ND 0.0556 0.0167 ug/L 1 XMS5029 XXX21374

Benzo[b]Fluoranthene ND 0.0556 0.0167 ug/L 1 XMS5029 XXX21374

Benzo[k]fluoranthene ND 0.0556 0.0167 ug/L 1 XMS5029 XXX21374

Benzo[a]pyrene ND 0.0556 0.0167 ug/L 1 XMS5029 XXX21374

Indeno[1,2,3-c,d] pyrene ND 0.0556 0.0167 ug/L 1 XMS5029 XXX21374

Dibenzo[a,h]anthracene ND 0.0556 0.0167 ug/L 1 XMS5029 XXX21374

Benzo[g,h,i]perylene ND 0.0556 0.0167 ug/L 1 XMS5029 XXX21374

Naphthalene ND 0.111 0.0344 ug/L 1 XMS5029 XXX21374

1-Methylnaphthalene ND 0.0556 0.0167 ug/L 1 XMS5029 XXX21374

2-Methylnaphthalene ND 0.0556 0.0167 ug/L 1 XMS5029 XXX21374

Terphenyl-d14 <surr> 99.7 50-135 % 1 XMS5029 XXX21374

Batch Information

Initial Prep Wt./Vol.: 900 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5029

Analytical Method: 8270D SIMS

Analysis Date/Time: 08/12/09 04:28

Prep Batch: XXX21374

Prep Method: SW3520C

Prep Date/Time: 08/07/09 10:00 Container ID:1094021005-H

Dilution Factor: 1 Analyst: JDH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

24 of 75
The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: TB01-WG01

SGS Ref. #: 1094021006 Collection Date/Time: 08/04/09 08:00

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 08/06/09 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 30.0 ug/L 1 VFC9606 VXX19837

4-Bromofluorobenzene <surr> 93.9 50-150 % 1 VFC9606 VXX19837

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9606

Analytical Method: SW8015C

Analysis Date/Time: 08/14/09 17:01

Prep Batch: VXX19837

Prep Method: SW5030B

Prep Date/Time: 08/14/09 13:16 Container ID:1094021006-C

Dilution Factor: 1 Analyst: KPW

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

25 of 75
The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: TB01-WG01

SGS Ref. #: 1094021006 Collection Date/Time: 08/04/09 08:00

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 08/06/09 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10728 VXX19797

Toluene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10728 VXX19797

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10728 VXX19797

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10728 VXX19797

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10728 VXX19797

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10728 VXX19797

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

Styrene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

Acetone 3.33 J 10.0 3.10 ug/L 1 VMS10736 VXX19816

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10728 VXX19797

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10728 VXX19797

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10728 VXX19797

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10728 VXX19797

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10728 VXX19797

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10728 VXX19797

Chloroform ND 1.00 0.300 ug/L 1 VMS10728 VXX19797

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

Chloromethane ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

Bromomethane ND 3.00 0.940 ug/L 1 VMS10728 VXX19797

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

26 of 75
The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: TB01-WG01

SGS Ref. #: 1094021006 Collection Date/Time: 08/04/09 08:00

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 08/06/09 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10728 VXX19797

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10736 VXX19816

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10728 VXX19797

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10728 VXX19797

Naphthalene ND 2.00 0.620 ug/L 1 VMS10728 VXX19797

o-Xylene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

Bromoform ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10728 VXX19797

1,2-Dichloroethane-D4 <surr> 106 73-120 % 1 VMS10728 VXX19797

Toluene-d8 <surr> 101 80-120 % 1 VMS10728 VXX19797

4-Bromofluorobenzene <surr> 102 76-120 % 1 VMS10728 VXX19797

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

27 of 75
The Environmental Company, Inc. (TEC) Print Date: 8/20/2009 1:51 pm

Client Sample ID: TB01-WG01

SGS Ref. #: 1094021006 Collection Date/Time: 08/04/09 08:00

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 08/06/09 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10728

Analytical Method: SW8260B

Analysis Date/Time: 08/14/09 03:46

Prep Batch: VXX19797

Prep Method: SW5030B

Prep Date/Time: 08/12/09 08:21 Container ID:1094021006-B

Dilution Factor: 1 Analyst: SCL

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10736

Analytical Method: SW8260B

Analysis Date/Time: 08/14/09 22:41

Prep Batch: VXX19816

Prep Method: SW5030B

Prep Date/Time: 08/14/09 08:51 Container ID:1094021006-A

Dilution Factor: 1 Analyst: SCL

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

28 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

914006 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX21370

SW3520C

08/07/2009

QC results affect the following production samples:

1094021001, 1094021004, 1094021005

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Semivolatile Organic Fuels Department

Diesel Range Organics 0.190 J 0.400 0.150 mg/L 08/08/09

Surrogates 

5a Androstane <surr> 88.5 60-120 % 08/08/09

Instrument

Method

Batch XFC8762

SW8015C

HP 6890 Series II FID SV D R

29 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

914030 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX21374

SW3520C

08/07/2009

QC results affect the following production samples:

1094021001, 1094021004, 1094021005

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Polynuclear Aromatics GC/MS

Acenaphthylene ND 0.0500 0.0150 ug/L 08/12/09

Acenaphthene ND 0.0500 0.0150 ug/L 08/12/09

Fluorene ND 0.0500 0.0150 ug/L 08/12/09

Phenanthrene ND 0.0500 0.0150 ug/L 08/12/09

Anthracene ND 0.0500 0.0150 ug/L 08/12/09

Fluoranthene ND 0.0500 0.0150 ug/L 08/12/09

Pyrene ND 0.0500 0.0150 ug/L 08/12/09

Benzo(a)Anthracene ND 0.0500 0.0150 ug/L 08/12/09

Chrysene ND 0.0500 0.0150 ug/L 08/12/09

Benzo[b]Fluoranthene ND 0.0500 0.0150 ug/L 08/12/09

Benzo[k]fluoranthene ND 0.0500 0.0150 ug/L 08/12/09

Benzo[a]pyrene ND 0.0500 0.0150 ug/L 08/12/09

Indeno[1,2,3-c,d] pyrene ND 0.0500 0.0150 ug/L 08/12/09

Dibenzo[a,h]anthracene ND 0.0500 0.0150 ug/L 08/12/09

Benzo[g,h,i]perylene ND 0.0500 0.0150 ug/L 08/12/09

Naphthalene ND 0.100 0.0310 ug/L 08/12/09

1-Methylnaphthalene ND 0.0500 0.0150 ug/L 08/12/09

2-Methylnaphthalene ND 0.0500 0.0150 ug/L 08/12/09

Surrogates 

Terphenyl-d14 <surr> 105 50-135 % 08/12/09

Instrument

Method

Batch XMS5029

8270D SIMS

HP 6890/5973 MS SVQA

30 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

915442 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

MXX22033

SW3010A

08/12/2009

QC results affect the following production samples:

1094021001, 1094021004, 1094021005

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Metals by ICP/MS

Lead ND 1.00 0.310 ug/L 08/18/09

Instrument

Method

Batch MMS6032

SW6020

Perkin Elmer Sciex ICP-MS P3

31 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

915595 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19797

SW5030B

08/12/2009

QC results affect the following production samples:

1094021004, 1094021005, 1094021006

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy

32 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

915595 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19797

SW5030B

08/12/2009

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy

Benzene ND 0.400 0.120 ug/L 08/12/09

Toluene ND 1.00 0.310 ug/L 08/12/09

Ethylbenzene ND 1.00 0.310 ug/L 08/12/09

n-Butylbenzene ND 1.00 0.310 ug/L 08/12/09

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 08/12/09

1,2-Dichloroethane ND 0.500 0.150 ug/L 08/12/09

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 08/12/09

4-Chlorotoluene ND 1.00 0.310 ug/L 08/12/09

Chlorobenzene ND 0.500 0.150 ug/L 08/12/09

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 08/12/09

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 08/12/09

4-Isopropyltoluene ND 1.00 0.310 ug/L 08/12/09

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 08/12/09

n-Propylbenzene ND 1.00 0.310 ug/L 08/12/09

Styrene ND 1.00 0.310 ug/L 08/12/09

Dibromomethane ND 1.00 0.310 ug/L 08/12/09

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 08/12/09

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 08/12/09

Acetone ND 10.0 3.10 ug/L 08/12/09

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 08/12/09

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 08/12/09

Methyl-t-butyl ether ND 5.00 1.50 ug/L 08/12/09

Tetrachloroethene ND 1.00 0.310 ug/L 08/12/09

Dibromochloromethane ND 0.500 0.150 ug/L 08/12/09

1,3-Dichloropropane ND 0.400 0.120 ug/L 08/12/09

1,2-Dibromoethane ND 1.00 0.310 ug/L 08/12/09

Carbon tetrachloride ND 1.00 0.310 ug/L 08/12/09

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 08/12/09

Chloroform ND 1.00 0.300 ug/L 08/12/09

Bromobenzene ND 1.00 0.310 ug/L 08/12/09

Chloromethane ND 1.00 0.310 ug/L 08/12/09

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 08/12/09

Bromomethane ND 3.00 0.940 ug/L 08/12/09

Bromochloromethane ND 1.00 0.310 ug/L 08/12/09

Vinyl chloride ND 1.00 0.310 ug/L 08/12/09

Dichlorodifluoromethane ND 1.00 0.310 ug/L 08/12/09

Chloroethane ND 1.00 0.310 ug/L 08/12/09

sec-Butylbenzene ND 1.00 0.310 ug/L 08/12/09

Bromodichloromethane ND 0.500 0.150 ug/L 08/12/09

33 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

915595 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19797

SW5030B

08/12/2009

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy

1,1-Dichloroethene ND 1.00 0.310 ug/L 08/12/09

2-Butanone (MEK) ND 10.0 3.10 ug/L 08/12/09

Methylene chloride ND 5.00 1.00 ug/L 08/12/09

Trichlorofluoromethane ND 1.00 0.310 ug/L 08/12/09

P & M -Xylene ND 2.00 0.620 ug/L 08/12/09

Naphthalene ND 2.00 0.620 ug/L 08/12/09

o-Xylene ND 1.00 0.310 ug/L 08/12/09

Bromoform ND 1.00 0.310 ug/L 08/12/09

1-Chlorohexane ND 1.00 0.310 ug/L 08/12/09

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 08/12/09

tert-Butylbenzene ND 1.00 0.310 ug/L 08/12/09

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 08/12/09

1,1-Dichloroethane ND 1.00 0.310 ug/L 08/12/09

2-Chlorotoluene ND 1.00 0.310 ug/L 08/12/09

Trichloroethene ND 1.00 0.310 ug/L 08/12/09

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 08/12/09

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 08/12/09

2,2-Dichloropropane ND 1.00 0.310 ug/L 08/12/09

Hexachlorobutadiene ND 1.00 0.310 ug/L 08/12/09

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 08/12/09

1,2-Dichloropropane ND 1.00 0.310 ug/L 08/12/09

1,1-Dichloropropene ND 1.00 0.310 ug/L 08/12/09

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 08/12/09

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 08/12/09

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 08/12/09

Surrogates 

1,2-Dichloroethane-D4 <surr> 108 73-120 % 08/12/09

Toluene-d8 <surr> 101 80-120 % 08/12/09

4-Bromofluorobenzene <surr> 103 76-120 % 08/12/09

Instrument

Method

Batch VMS10724

SW8260B

HP 5890 Series II MS3 VNA

34 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

915946 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19810

SW5030B

08/13/2009

QC results affect the following production samples:

1094021001

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy

35 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

915946 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19810

SW5030B

08/13/2009

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy

Benzene ND 0.400 0.120 ug/L 08/13/09

Toluene ND 1.00 0.310 ug/L 08/13/09

Ethylbenzene ND 1.00 0.310 ug/L 08/13/09

n-Butylbenzene ND 1.00 0.310 ug/L 08/13/09

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 08/13/09

1,2-Dichloroethane ND 0.500 0.150 ug/L 08/13/09

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 08/13/09

4-Chlorotoluene ND 1.00 0.310 ug/L 08/13/09

Chlorobenzene ND 0.500 0.150 ug/L 08/13/09

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 08/13/09

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 08/13/09

4-Isopropyltoluene ND 1.00 0.310 ug/L 08/13/09

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 08/13/09

n-Propylbenzene ND 1.00 0.310 ug/L 08/13/09

Styrene ND 1.00 0.310 ug/L 08/13/09

Dibromomethane ND 1.00 0.310 ug/L 08/13/09

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 08/13/09

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 08/13/09

Acetone ND 10.0 3.10 ug/L 08/13/09

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 08/13/09

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 08/13/09

Methyl-t-butyl ether ND 5.00 1.50 ug/L 08/13/09

Tetrachloroethene ND 1.00 0.310 ug/L 08/13/09

Dibromochloromethane ND 0.500 0.150 ug/L 08/13/09

1,3-Dichloropropane ND 0.400 0.120 ug/L 08/13/09

1,2-Dibromoethane ND 1.00 0.310 ug/L 08/13/09

Carbon tetrachloride ND 1.00 0.310 ug/L 08/13/09

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 08/13/09

Chloroform ND 1.00 0.300 ug/L 08/13/09

Bromobenzene ND 1.00 0.310 ug/L 08/13/09

Chloromethane ND 1.00 0.310 ug/L 08/13/09

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 08/13/09

Bromomethane ND 3.00 0.940 ug/L 08/13/09

Bromochloromethane ND 1.00 0.310 ug/L 08/13/09

Vinyl chloride ND 1.00 0.310 ug/L 08/13/09

Dichlorodifluoromethane ND 1.00 0.310 ug/L 08/13/09

Chloroethane ND 1.00 0.310 ug/L 08/13/09

sec-Butylbenzene ND 1.00 0.310 ug/L 08/13/09

Bromodichloromethane ND 0.500 0.150 ug/L 08/13/09

36 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

915946 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19810

SW5030B

08/13/2009

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy

1,1-Dichloroethene ND 1.00 0.310 ug/L 08/13/09

2-Butanone (MEK) ND 10.0 3.10 ug/L 08/13/09

Methylene chloride ND 5.00 1.00 ug/L 08/13/09

Trichlorofluoromethane ND 1.00 0.310 ug/L 08/13/09

P & M -Xylene ND 2.00 0.620 ug/L 08/13/09

Naphthalene ND 2.00 0.620 ug/L 08/13/09

o-Xylene ND 1.00 0.310 ug/L 08/13/09

Bromoform ND 1.00 0.310 ug/L 08/13/09

1-Chlorohexane ND 1.00 0.310 ug/L 08/13/09

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 08/13/09

tert-Butylbenzene ND 1.00 0.310 ug/L 08/13/09

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 08/13/09

1,1-Dichloroethane ND 1.00 0.310 ug/L 08/13/09

2-Chlorotoluene ND 1.00 0.310 ug/L 08/13/09

Trichloroethene ND 1.00 0.310 ug/L 08/13/09

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 08/13/09

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 08/13/09

2,2-Dichloropropane ND 1.00 0.310 ug/L 08/13/09

Hexachlorobutadiene ND 1.00 0.310 ug/L 08/13/09

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 08/13/09

1,2-Dichloropropane ND 1.00 0.310 ug/L 08/13/09

1,1-Dichloropropene ND 1.00 0.310 ug/L 08/13/09

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 08/13/09

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 08/13/09

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 08/13/09

Surrogates 

1,2-Dichloroethane-D4 <surr> 117 73-120 % 08/13/09

Toluene-d8 <surr> 99.3 80-120 % 08/13/09

4-Bromofluorobenzene <surr> 103 76-120 % 08/13/09

Instrument

Method

Batch VMS10730

SW8260B

HP 5890 Series II MS3 VNA

37 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

916338 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19816

SW5030B

08/14/2009

QC results affect the following production samples:

1094021006

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy

Acetone ND 10.0 3.10 ug/L 08/14/09

2-Butanone (MEK) ND 10.0 3.10 ug/L 08/14/09

Surrogates 

1,2-Dichloroethane-D4 <surr> 108 73-120 % 08/14/09

Toluene-d8 <surr> 99.1 80-120 % 08/14/09

4-Bromofluorobenzene <surr> 103 76-120 % 08/14/09

Instrument

Method

Batch VMS10736

SW8260B

HP 5890 Series II MS3 VNA

38 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

917244 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19837

SW5030B

08/14/2009

QC results affect the following production samples:

1094021001, 1094021004, 1094021005, 1094021006

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Fuels Department

Gasoline Range Organics ND 100 30.0 ug/L 08/14/09

Surrogates 

4-Bromofluorobenzene <surr> 93.7 50-150 % 08/14/09

Instrument

Method

Batch VFC9606

SW8015C

HP 5890 Series II PID+HECD VBA

39 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

914008 Lab Control Sample

914009 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX21370

SW3520C

08/07/2009

QC results affect the following production samples:

1094021001, 1094021004, 1094021005

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Semivolatile Organic Fuels Department

Diesel Range Organics LCS 4.40 88 ( 75-125 ) 5 mg/L 08/08/2009

LCSD 4.25 85 4 (< 20 ) 5 mg/L 08/08/2009

Surrogates 

5a Androstane <surr> LCS 93 ( 60-120 ) 08/08/2009

LCSD 90 3 08/08/2009

Batch

Method

Instrument

XFC8762

SW8015C

HP 6890 Series II FID SV D R

40 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

914031 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX21374

SW3520C

08/07/2009

QC results affect the following production samples:

1094021001, 1094021004, 1094021005

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

41 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

914031 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX21374

SW3520C

08/07/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Acenaphthylene LCS 0.429 86 ( 50-105 ) 0.5 ug/L 08/12/2009

Acenaphthene LCS 0.415 83 ( 45-110 ) 0.5 ug/L 08/12/2009

Fluorene LCS 0.452 90 ( 50-110 ) 0.5 ug/L 08/12/2009

Phenanthrene LCS 0.453 91 ( 50-115 ) 0.5 ug/L 08/12/2009

Anthracene LCS 0.480 96 ( 55-110 ) 0.5 ug/L 08/12/2009

Fluoranthene LCS 0.510 102 ( 55-125 ) 0.5 ug/L 08/12/2009

Pyrene LCS 0.486 97 ( 50-130 ) 0.5 ug/L 08/12/2009

Benzo(a)Anthracene LCS 0.536 107 ( 55-120 ) 0.5 ug/L 08/12/2009

Chrysene LCS 0.489 98 ( 55-120 ) 0.5 ug/L 08/12/2009

Benzo[b]Fluoranthene LCS 0.524 105 ( 46-130 ) 0.5 ug/L 08/12/2009

Benzo[k]fluoranthene LCS 0.518 104 ( 60-125 ) 0.5 ug/L 08/12/2009

Benzo[a]pyrene LCS 0.515 103 ( 55-120 ) 0.5 ug/L 08/12/2009

Indeno[1,2,3-c,d] pyrene LCS 0.479 96 ( 45-125 ) 0.5 ug/L 08/12/2009

Dibenzo[a,h]anthracene LCS 0.483 97 ( 41-140 ) 0.5 ug/L 08/12/2009

Benzo[g,h,i]perylene LCS 0.503 101 ( 46-125 ) 0.5 ug/L 08/12/2009

Naphthalene LCS 0.391 78 ( 42-100 ) 0.5 ug/L 08/12/2009

1-Methylnaphthalene LCS 0.387 78 ( 46-115 ) 0.5 ug/L 08/12/2009

2-Methylnaphthalene LCS 0.389 78 ( 45-105 ) 0.5 ug/L 08/12/2009

Surrogates 

Terphenyl-d14 <surr> LCS 98 ( 50-135 ) 08/12/2009

42 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

914031 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX21374

SW3520C

08/07/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Batch

Method

Instrument

XMS5029

8270D SIMS

HP 6890/5973 MS SVQA

43 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

915443 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

MXX22033

SW3010A

08/12/2009

QC results affect the following production samples:

1094021001, 1094021004, 1094021005

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Metals by ICP/MS

Lead LCS 1030 103 ( 80-120 ) 1000 ug/L 08/18/2009

Batch

Method

Instrument

MMS6032

SW6020

Perkin Elmer Sciex ICP-MS P3

44 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

915596 Lab Control Sample

915597 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19797

SW5030B

08/12/2009

QC results affect the following production samples:

1094021004, 1094021005, 1094021006

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

45 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

915596 Lab Control Sample

915597 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19797

SW5030B

08/12/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Benzene LCS 28.8 96 ( 80-120 ) 30 ug/L 08/12/2009

LCSD 27.9 93 3 (< 20 ) 30 ug/L 08/12/2009

Toluene LCS 29.7 99 ( 77-120 ) 30 ug/L 08/12/2009

LCSD 28.8 96 3 (< 20 ) 30 ug/L 08/12/2009

Ethylbenzene LCS 32.0 107 ( 80-120 ) 30 ug/L 08/12/2009

LCSD 30.6 102 5 (< 20 ) 30 ug/L 08/12/2009

n-Butylbenzene LCS 33.7 112 ( 80-124 ) 30 ug/L 08/12/2009

LCSD 33.2 111 1 (< 20 ) 30 ug/L 08/12/2009

1,4-Dichlorobenzene LCS 29.8 99 ( 80-120 ) 30 ug/L 08/12/2009

LCSD 29.5 98 1 (< 20 ) 30 ug/L 08/12/2009

1,2-Dichloroethane LCS 31.7 106 ( 80-129 ) 30 ug/L 08/12/2009

LCSD 30.6 102 4 (< 20 ) 30 ug/L 08/12/2009

1,3,5-Trimethylbenzene LCS 31.4 105 ( 80-128 ) 30 ug/L 08/12/2009

LCSD 30.7 102 2 (< 20 ) 30 ug/L 08/12/2009

4-Chlorotoluene LCS 30.4 101 ( 79-128 ) 30 ug/L 08/12/2009

LCSD 30.0 100 2 (< 20 ) 30 ug/L 08/12/2009

Chlorobenzene LCS 30.2 101 ( 80-120 ) 30 ug/L 08/12/2009

LCSD 29.7 99 1 (< 20 ) 30 ug/L 08/12/2009

4-Methyl-2-pentanone (MIBK) LCS 81.9 91 ( 69-134 ) 90 ug/L 08/12/2009

LCSD 84.5 94 3 (< 20 ) 90 ug/L 08/12/2009

cis-1,2-Dichloroethene LCS 29.7 99 ( 80-125 ) 30 ug/L 08/12/2009

LCSD 29.1 97 2 (< 20 ) 30 ug/L 08/12/2009

4-Isopropyltoluene LCS 32.7 109 ( 80-125 ) 30 ug/L 08/12/2009

LCSD 31.9 106 3 (< 20 ) 30 ug/L 08/12/2009

cis-1,3-Dichloropropene LCS 28.7 96 ( 80-120 ) 30 ug/L 08/12/2009

LCSD 28.2 94 2 (< 20 ) 30 ug/L 08/12/2009

n-Propylbenzene LCS 31.3 104 ( 80-129 ) 30 ug/L 08/12/2009

LCSD 30.9 103 1 (< 20 ) 30 ug/L 08/12/2009

46 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

915596 Lab Control Sample

915597 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19797

SW5030B

08/12/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Styrene LCS 32.4 108 ( 80-120 ) 30 ug/L 08/12/2009

LCSD 31.6 105 3 (< 20 ) 30 ug/L 08/12/2009

Dibromomethane LCS 30.2 101 ( 80-120 ) 30 ug/L 08/12/2009

LCSD 29.1 97 4 (< 20 ) 30 ug/L 08/12/2009

trans-1,3-Dichloropropene LCS 29.2 97 ( 80-124 ) 30 ug/L 08/12/2009

LCSD 28.6 95 2 (< 20 ) 30 ug/L 08/12/2009

1,2,4-Trichlorobenzene LCS 27.9 93 ( 80-120 ) 30 ug/L 08/12/2009

LCSD 28.4 95 2 (< 20 ) 30 ug/L 08/12/2009

Acetone LCS 146 162 * ( 50-135 ) 90 ug/L 08/12/2009

LCSD 126 140 * 14 (< 20 ) 90 ug/L 08/12/2009

1,1,2,2-Tetrachloroethane LCS 28.8 96 ( 76-123 ) 30 ug/L 08/12/2009

LCSD 28.7 96 0 (< 20 ) 30 ug/L 08/12/2009

1,2-Dibromo-3-chloropropane LCS 26.4 88 ( 73-130 ) 30 ug/L 08/12/2009

LCSD 28.1 94 6 (< 20 ) 30 ug/L 08/12/2009

Methyl-t-butyl ether LCS 43.2 96 ( 80-120 ) 45 ug/L 08/12/2009

LCSD 43.5 97 1 (< 20 ) 45 ug/L 08/12/2009

Tetrachloroethene LCS 31.4 105 ( 79-122 ) 30 ug/L 08/12/2009

LCSD 30.7 102 2 (< 20 ) 30 ug/L 08/12/2009

Dibromochloromethane LCS 28.5 95 ( 80-120 ) 30 ug/L 08/12/2009

LCSD 28.8 96 1 (< 20 ) 30 ug/L 08/12/2009

1,3-Dichloropropane LCS 30.1 100 ( 80-121 ) 30 ug/L 08/12/2009

LCSD 29.6 99 2 (< 20 ) 30 ug/L 08/12/2009

1,2-Dibromoethane LCS 30.7 102 ( 80-120 ) 30 ug/L 08/12/2009

LCSD 30.6 102 0 (< 20 ) 30 ug/L 08/12/2009

Carbon tetrachloride LCS 31.2 104 ( 80-126 ) 30 ug/L 08/12/2009

LCSD 29.6 99 5 (< 20 ) 30 ug/L 08/12/2009

1,1,1,2-Tetrachloroethane LCS 34.4 115 ( 80-120 ) 30 ug/L 08/12/2009

47 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

915596 Lab Control Sample

915597 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19797

SW5030B

08/12/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

LCSD 33.1 110 4 (< 20 ) 30 ug/L 08/12/2009

Chloroform LCS 31.4 105 ( 80-124 ) 30 ug/L 08/12/2009

LCSD 30.5 102 3 (< 20 ) 30 ug/L 08/12/2009

Bromobenzene LCS 28.8 96 ( 80-120 ) 30 ug/L 08/12/2009

LCSD 28.7 96 0 (< 20 ) 30 ug/L 08/12/2009

Chloromethane LCS 35.1 117 ( 67-125 ) 30 ug/L 08/12/2009

LCSD 33.4 111 5 (< 20 ) 30 ug/L 08/12/2009

1,2,3-Trichloropropane LCS 28.9 96 ( 80-120 ) 30 ug/L 08/12/2009

LCSD 28.8 96 0 (< 20 ) 30 ug/L 08/12/2009

Bromomethane LCS 39.2 131 ( 30-140 ) 30 ug/L 08/12/2009

LCSD 37.9 126 3 (< 20 ) 30 ug/L 08/12/2009

Bromochloromethane LCS 31.1 104 ( 77-129 ) 30 ug/L 08/12/2009

LCSD 30.0 100 4 (< 20 ) 30 ug/L 08/12/2009

Vinyl chloride LCS 38.9 130 ( 72-145 ) 30 ug/L 08/12/2009

LCSD 37.5 125 4 (< 20 ) 30 ug/L 08/12/2009

Dichlorodifluoromethane LCS 40.3 134 ( 62-153 ) 30 ug/L 08/12/2009

LCSD 38.9 130 4 (< 20 ) 30 ug/L 08/12/2009

Chloroethane LCS 38.1 127 ( 67-133 ) 30 ug/L 08/12/2009

LCSD 34.2 114 11 (< 20 ) 30 ug/L 08/12/2009

sec-Butylbenzene LCS 32.4 108 ( 80-120 ) 30 ug/L 08/12/2009

LCSD 31.5 105 3 (< 20 ) 30 ug/L 08/12/2009

Bromodichloromethane LCS 35.0 117 ( 80-120 ) 30 ug/L 08/12/2009

LCSD 33.8 113 4 (< 20 ) 30 ug/L 08/12/2009

1,1-Dichloroethene LCS 32.9 110 ( 76-130 ) 30 ug/L 08/12/2009

LCSD 31.8 106 4 (< 20 ) 30 ug/L 08/12/2009

2-Butanone (MEK) LCS 104 116 ( 66-136 ) 90 ug/L 08/12/2009

LCSD 96.4 107 8 (< 20 ) 90 ug/L 08/12/2009

48 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

915596 Lab Control Sample

915597 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19797

SW5030B

08/12/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Methylene chloride LCS 32.9 110 ( 63-131 ) 30 ug/L 08/12/2009

LCSD 32.4 108 2 (< 20 ) 30 ug/L 08/12/2009

Trichlorofluoromethane LCS 40.5 135 ( 68-145 ) 30 ug/L 08/12/2009

LCSD 38.3 128 6 (< 20 ) 30 ug/L 08/12/2009

P & M -Xylene LCS 64.4 107 ( 80-120 ) 60 ug/L 08/12/2009

LCSD 62.5 104 3 (< 20 ) 60 ug/L 08/12/2009

Naphthalene LCS 26.4 88 ( 75-120 ) 30 ug/L 08/12/2009

LCSD 27.3 91 4 (< 20 ) 30 ug/L 08/12/2009

o-Xylene LCS 30.9 103 ( 80-120 ) 30 ug/L 08/12/2009

LCSD 30.3 101 2 (< 20 ) 30 ug/L 08/12/2009

Bromoform LCS 30.6 102 ( 80-120 ) 30 ug/L 08/12/2009

LCSD 30.9 103 1 (< 20 ) 30 ug/L 08/12/2009

1-Chlorohexane LCS 50.9 113 ( 70-125 ) 45 ug/L 08/12/2009

LCSD 47.8 106 6 (< 20 ) 45 ug/L 08/12/2009

1,2,4-Trimethylbenzene LCS 31.2 104 ( 80-125 ) 30 ug/L 08/12/2009

LCSD 30.5 102 2 (< 20 ) 30 ug/L 08/12/2009

tert-Butylbenzene LCS 31.3 104 ( 80-122 ) 30 ug/L 08/12/2009

LCSD 30.6 102 2 (< 20 ) 30 ug/L 08/12/2009

1,1,1-Trichloroethane LCS 33.3 111 ( 80-122 ) 30 ug/L 08/12/2009

LCSD 31.9 106 4 (< 20 ) 30 ug/L 08/12/2009

1,1-Dichloroethane LCS 33.1 110 ( 80-120 ) 30 ug/L 08/12/2009

LCSD 31.9 106 4 (< 20 ) 30 ug/L 08/12/2009

2-Chlorotoluene LCS 30.2 101 ( 80-125 ) 30 ug/L 08/12/2009

LCSD 29.8 100 1 (< 20 ) 30 ug/L 08/12/2009

Trichloroethene LCS 31.3 104 ( 80-125 ) 30 ug/L 08/12/2009

LCSD 29.8 100 5 (< 20 ) 30 ug/L 08/12/2009

trans-1,2-Dichloroethene LCS 31.6 105 ( 79-132 ) 30 ug/L 08/12/2009

LCSD 30.4 101 4 (< 20 ) 30 ug/L 08/12/2009

49 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

915596 Lab Control Sample

915597 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19797

SW5030B

08/12/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

1,2-Dichlorobenzene LCS 29.6 99 ( 80-120 ) 30 ug/L 08/12/2009

LCSD 29.0 97 2 (< 20 ) 30 ug/L 08/12/2009

2,2-Dichloropropane LCS 36.0 120 ( 80-132 ) 30 ug/L 08/12/2009

LCSD 33.7 112 7 (< 20 ) 30 ug/L 08/12/2009

Hexachlorobutadiene LCS 32.3 108 ( 77-125 ) 30 ug/L 08/12/2009

LCSD 31.9 106 1 (< 20 ) 30 ug/L 08/12/2009

Isopropylbenzene (Cumene) LCS 33.0 110 ( 80-121 ) 30 ug/L 08/12/2009

LCSD 31.7 106 4 (< 20 ) 30 ug/L 08/12/2009

1,2-Dichloropropane LCS 30.4 101 ( 80-121 ) 30 ug/L 08/12/2009

LCSD 29.7 99 2 (< 20 ) 30 ug/L 08/12/2009

1,1-Dichloropropene LCS 32.1 107 ( 80-122 ) 30 ug/L 08/12/2009

LCSD 30.5 102 5 (< 20 ) 30 ug/L 08/12/2009

1,1,2-Trichloroethane LCS 29.2 98 ( 77-120 ) 30 ug/L 08/12/2009

LCSD 28.8 96 2 (< 20 ) 30 ug/L 08/12/2009

1,3-Dichlorobenzene LCS 29.5 99 ( 80-120 ) 30 ug/L 08/12/2009

LCSD 29.4 98 1 (< 20 ) 30 ug/L 08/12/2009

1,2,3-Trichlorobenzene LCS 27.1 90 ( 77-120 ) 30 ug/L 08/12/2009

LCSD 27.5 92 1 (< 20 ) 30 ug/L 08/12/2009

Surrogates 

1,2-Dichloroethane-D4 <surr> LCS 106 ( 73-120 ) 08/12/2009

LCSD 104 2 08/12/2009

Toluene-d8 <surr> LCS 99 ( 80-120 ) 08/12/2009

LCSD 99 1 08/12/2009

4-Bromofluorobenzene <surr> LCS 96 ( 76-120 ) 08/12/2009

LCSD 98 2 08/12/2009

50 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

915596 Lab Control Sample

915597 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19797

SW5030B

08/12/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Batch

Method

Instrument

VMS10724

SW8260B

HP 5890 Series II MS3 VNA

51 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

915947 Lab Control Sample

915948 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19810

SW5030B

08/13/2009

QC results affect the following production samples:

1094021001

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

52 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

915947 Lab Control Sample

915948 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19810

SW5030B

08/13/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Benzene LCS 29.5 99 ( 80-120 ) 30 ug/L 08/13/2009

LCSD 28.4 95 4 (< 20 ) 30 ug/L 08/13/2009

Toluene LCS 30.9 103 ( 77-120 ) 30 ug/L 08/13/2009

LCSD 29.6 99 4 (< 20 ) 30 ug/L 08/13/2009

Ethylbenzene LCS 32.5 108 ( 80-120 ) 30 ug/L 08/13/2009

LCSD 31.0 103 5 (< 20 ) 30 ug/L 08/13/2009

n-Butylbenzene LCS 34.0 113 ( 80-124 ) 30 ug/L 08/13/2009

LCSD 32.3 108 5 (< 20 ) 30 ug/L 08/13/2009

1,4-Dichlorobenzene LCS 31.0 103 ( 80-120 ) 30 ug/L 08/13/2009

LCSD 29.3 98 6 (< 20 ) 30 ug/L 08/13/2009

1,2-Dichloroethane LCS 32.0 107 ( 80-129 ) 30 ug/L 08/13/2009

LCSD 31.8 106 1 (< 20 ) 30 ug/L 08/13/2009

1,3,5-Trimethylbenzene LCS 32.6 109 ( 80-128 ) 30 ug/L 08/13/2009

LCSD 31.4 105 4 (< 20 ) 30 ug/L 08/13/2009

4-Chlorotoluene LCS 31.3 104 ( 79-128 ) 30 ug/L 08/13/2009

LCSD 30.2 101 4 (< 20 ) 30 ug/L 08/13/2009

Chlorobenzene LCS 31.3 104 ( 80-120 ) 30 ug/L 08/13/2009

LCSD 30.2 101 3 (< 20 ) 30 ug/L 08/13/2009

4-Methyl-2-pentanone (MIBK) LCS 84.8 94 ( 69-134 ) 90 ug/L 08/13/2009

LCSD 78.1 87 8 (< 20 ) 90 ug/L 08/13/2009

cis-1,2-Dichloroethene LCS 30.7 102 ( 80-125 ) 30 ug/L 08/13/2009

LCSD 30.5 102 1 (< 20 ) 30 ug/L 08/13/2009

4-Isopropyltoluene LCS 33.7 112 ( 80-125 ) 30 ug/L 08/13/2009

LCSD 32.4 108 4 (< 20 ) 30 ug/L 08/13/2009

cis-1,3-Dichloropropene LCS 32.5 108 ( 80-120 ) 30 ug/L 08/13/2009

LCSD 32.7 109 1 (< 20 ) 30 ug/L 08/13/2009

n-Propylbenzene LCS 32.3 108 ( 80-129 ) 30 ug/L 08/13/2009

LCSD 31.1 104 4 (< 20 ) 30 ug/L 08/13/2009

53 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

915947 Lab Control Sample

915948 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19810

SW5030B

08/13/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Styrene LCS 33.3 111 ( 80-120 ) 30 ug/L 08/13/2009

LCSD 32.3 108 3 (< 20 ) 30 ug/L 08/13/2009

Dibromomethane LCS 30.3 101 ( 80-120 ) 30 ug/L 08/13/2009

LCSD 30.6 102 1 (< 20 ) 30 ug/L 08/13/2009

trans-1,3-Dichloropropene LCS 33.3 111 ( 80-124 ) 30 ug/L 08/13/2009

LCSD 32.9 110 1 (< 20 ) 30 ug/L 08/13/2009

1,2,4-Trichlorobenzene LCS 30.1 100 ( 80-120 ) 30 ug/L 08/13/2009

LCSD 28.3 94 6 (< 20 ) 30 ug/L 08/13/2009

Acetone LCS 90.6 101 ( 50-135 ) 90 ug/L 08/13/2009

LCSD 87.0 97 4 (< 20 ) 90 ug/L 08/13/2009

1,1,2,2-Tetrachloroethane LCS 30.4 101 ( 76-123 ) 30 ug/L 08/13/2009

LCSD 28.4 95 7 (< 20 ) 30 ug/L 08/13/2009

1,2-Dibromo-3-chloropropane LCS 29.1 97 ( 73-130 ) 30 ug/L 08/13/2009

LCSD 27.9 93 4 (< 20 ) 30 ug/L 08/13/2009

Methyl-t-butyl ether LCS 44.5 99 ( 80-120 ) 45 ug/L 08/13/2009

LCSD 43.3 96 3 (< 20 ) 45 ug/L 08/13/2009

Tetrachloroethene LCS 31.3 104 ( 79-122 ) 30 ug/L 08/13/2009

LCSD 30.2 101 4 (< 20 ) 30 ug/L 08/13/2009

Dibromochloromethane LCS 31.6 105 ( 80-120 ) 30 ug/L 08/13/2009

LCSD 30.8 103 3 (< 20 ) 30 ug/L 08/13/2009

1,3-Dichloropropane LCS 31.2 104 ( 80-121 ) 30 ug/L 08/13/2009

LCSD 30.6 102 2 (< 20 ) 30 ug/L 08/13/2009

1,2-Dibromoethane LCS 31.1 104 ( 80-120 ) 30 ug/L 08/13/2009

LCSD 30.6 102 2 (< 20 ) 30 ug/L 08/13/2009

Carbon tetrachloride LCS 34.4 115 ( 80-126 ) 30 ug/L 08/13/2009

LCSD 34.4 115 0 (< 20 ) 30 ug/L 08/13/2009

1,1,1,2-Tetrachloroethane LCS 30.0 100 ( 80-120 ) 30 ug/L 08/13/2009

54 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

915947 Lab Control Sample

915948 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19810

SW5030B

08/13/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

LCSD 29.6 99 1 (< 20 ) 30 ug/L 08/13/2009

Chloroform LCS 33.2 111 ( 80-124 ) 30 ug/L 08/13/2009

LCSD 32.8 109 1 (< 20 ) 30 ug/L 08/13/2009

Bromobenzene LCS 29.5 98 ( 80-120 ) 30 ug/L 08/13/2009

LCSD 28.3 94 4 (< 20 ) 30 ug/L 08/13/2009

Chloromethane LCS 31.2 104 ( 67-125 ) 30 ug/L 08/13/2009

LCSD 27.8 93 11 (< 20 ) 30 ug/L 08/13/2009

1,2,3-Trichloropropane LCS 29.7 99 ( 80-120 ) 30 ug/L 08/13/2009

LCSD 28.0 93 6 (< 20 ) 30 ug/L 08/13/2009

Bromomethane LCS 38.8 129 ( 30-140 ) 30 ug/L 08/13/2009

LCSD 40.7 136 5 (< 20 ) 30 ug/L 08/13/2009

Bromochloromethane LCS 31.0 103 ( 77-129 ) 30 ug/L 08/13/2009

LCSD 30.2 101 3 (< 20 ) 30 ug/L 08/13/2009

Vinyl chloride LCS 32.9 110 ( 72-145 ) 30 ug/L 08/13/2009

LCSD 30.2 101 8 (< 20 ) 30 ug/L 08/13/2009

Dichlorodifluoromethane LCS 32.1 107 ( 62-153 ) 30 ug/L 08/13/2009

LCSD 30.2 101 6 (< 20 ) 30 ug/L 08/13/2009

Chloroethane LCS 34.5 115 ( 67-133 ) 30 ug/L 08/13/2009

LCSD 31.6 105 9 (< 20 ) 30 ug/L 08/13/2009

sec-Butylbenzene LCS 33.3 111 ( 80-120 ) 30 ug/L 08/13/2009

LCSD 32.0 107 4 (< 20 ) 30 ug/L 08/13/2009

Bromodichloromethane LCS 32.1 107 ( 80-120 ) 30 ug/L 08/13/2009

LCSD 32.6 109 2 (< 20 ) 30 ug/L 08/13/2009

1,1-Dichloroethene LCS 33.1 110 ( 76-130 ) 30 ug/L 08/13/2009

LCSD 32.4 108 2 (< 20 ) 30 ug/L 08/13/2009

2-Butanone (MEK) LCS 87.2 97 ( 66-136 ) 90 ug/L 08/13/2009

LCSD 89.6 100 3 (< 20 ) 90 ug/L 08/13/2009

55 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

915947 Lab Control Sample

915948 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19810

SW5030B

08/13/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Methylene chloride LCS 31.3 104 ( 63-131 ) 30 ug/L 08/13/2009

LCSD 29.6 99 5 (< 20 ) 30 ug/L 08/13/2009

Trichlorofluoromethane LCS 35.6 119 ( 68-145 ) 30 ug/L 08/13/2009

LCSD 32.9 110 8 (< 20 ) 30 ug/L 08/13/2009

P & M -Xylene LCS 65.6 109 ( 80-120 ) 60 ug/L 08/13/2009

LCSD 63.7 106 3 (< 20 ) 60 ug/L 08/13/2009

Naphthalene LCS 28.5 95 ( 75-120 ) 30 ug/L 08/13/2009

LCSD 26.7 89 7 (< 20 ) 30 ug/L 08/13/2009

o-Xylene LCS 32.7 109 ( 80-120 ) 30 ug/L 08/13/2009

LCSD 31.7 106 3 (< 20 ) 30 ug/L 08/13/2009

Bromoform LCS 31.8 106 ( 80-120 ) 30 ug/L 08/13/2009

LCSD 31.2 104 2 (< 20 ) 30 ug/L 08/13/2009

1-Chlorohexane LCS 52.3 116 ( 70-125 ) 45 ug/L 08/13/2009

LCSD 49.7 110 5 (< 20 ) 45 ug/L 08/13/2009

1,2,4-Trimethylbenzene LCS 32.6 109 ( 80-125 ) 30 ug/L 08/13/2009

LCSD 31.0 103 5 (< 20 ) 30 ug/L 08/13/2009

tert-Butylbenzene LCS 32.7 109 ( 80-122 ) 30 ug/L 08/13/2009

LCSD 31.6 105 3 (< 20 ) 30 ug/L 08/13/2009

1,1,1-Trichloroethane LCS 33.7 112 ( 80-122 ) 30 ug/L 08/13/2009

LCSD 33.9 113 1 (< 20 ) 30 ug/L 08/13/2009

1,1-Dichloroethane LCS 34.9 116 ( 80-120 ) 30 ug/L 08/13/2009

LCSD 33.7 112 4 (< 20 ) 30 ug/L 08/13/2009

2-Chlorotoluene LCS 31.5 105 ( 80-125 ) 30 ug/L 08/13/2009

LCSD 30.0 100 5 (< 20 ) 30 ug/L 08/13/2009

Trichloroethene LCS 31.1 104 ( 80-125 ) 30 ug/L 08/13/2009

LCSD 30.4 101 2 (< 20 ) 30 ug/L 08/13/2009

trans-1,2-Dichloroethene LCS 31.9 106 ( 79-132 ) 30 ug/L 08/13/2009

LCSD 31.5 105 1 (< 20 ) 30 ug/L 08/13/2009

56 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

915947 Lab Control Sample

915948 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19810

SW5030B

08/13/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

1,2-Dichlorobenzene LCS 30.3 101 ( 80-120 ) 30 ug/L 08/13/2009

LCSD 29.0 97 5 (< 20 ) 30 ug/L 08/13/2009

2,2-Dichloropropane LCS 33.0 110 ( 80-132 ) 30 ug/L 08/13/2009

LCSD 33.3 111 1 (< 20 ) 30 ug/L 08/13/2009

Hexachlorobutadiene LCS 31.3 104 ( 77-125 ) 30 ug/L 08/13/2009

LCSD 30.5 102 3 (< 20 ) 30 ug/L 08/13/2009

Isopropylbenzene (Cumene) LCS 34.5 115 ( 80-121 ) 30 ug/L 08/13/2009

LCSD 33.2 111 4 (< 20 ) 30 ug/L 08/13/2009

1,2-Dichloropropane LCS 31.0 103 ( 80-121 ) 30 ug/L 08/13/2009

LCSD 30.0 100 3 (< 20 ) 30 ug/L 08/13/2009

1,1-Dichloropropene LCS 37.7 126 * ( 80-122 ) 30 ug/L 08/13/2009

LCSD 37.0 123 * 2 (< 20 ) 30 ug/L 08/13/2009

1,1,2-Trichloroethane LCS 31.5 105 ( 77-120 ) 30 ug/L 08/13/2009

LCSD 30.6 102 3 (< 20 ) 30 ug/L 08/13/2009

1,3-Dichlorobenzene LCS 30.4 101 ( 80-120 ) 30 ug/L 08/13/2009

LCSD 29.2 97 4 (< 20 ) 30 ug/L 08/13/2009

1,2,3-Trichlorobenzene LCS 29.2 97 ( 77-120 ) 30 ug/L 08/13/2009

LCSD 27.8 93 5 (< 20 ) 30 ug/L 08/13/2009

Surrogates 

1,2-Dichloroethane-D4 <surr> LCS 103 ( 73-120 ) 08/13/2009

LCSD 108 5 08/13/2009

Toluene-d8 <surr> LCS 100 ( 80-120 ) 08/13/2009

LCSD 101 1 08/13/2009

4-Bromofluorobenzene <surr> LCS 98 ( 76-120 ) 08/13/2009

LCSD 98 1 08/13/2009

57 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

915947 Lab Control Sample

915948 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19810

SW5030B

08/13/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Batch

Method

Instrument

VMS10730

SW8260B

HP 5890 Series II MS3 VNA

58 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

916339 Lab Control Sample

916340 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19816

SW5030B

08/14/2009

QC results affect the following production samples:

1094021006

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Acetone LCS 104 116 ( 50-135 ) 90 ug/L 08/14/2009

LCSD 97.6 108 7 (< 20 ) 90 ug/L 08/14/2009

2-Butanone (MEK) LCS 84.6 94 ( 66-136 ) 90 ug/L 08/14/2009

LCSD 81.8 91 3 (< 20 ) 90 ug/L 08/14/2009

Surrogates 

1,2-Dichloroethane-D4 <surr> LCS 106 ( 73-120 ) 08/14/2009

LCSD 103 2 08/14/2009

Toluene-d8 <surr> LCS 99 ( 80-120 ) 08/14/2009

LCSD 99 0 08/14/2009

4-Bromofluorobenzene <surr> LCS 94 ( 76-120 ) 08/14/2009

LCSD 95 1 08/14/2009

Batch

Method

Instrument

VMS10736

SW8260B

HP 5890 Series II MS3 VNA

59 of 75
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Prep

917245 Lab Control Sample

917246 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19837

SW5030B

08/14/2009

QC results affect the following production samples:

1094021001, 1094021004, 1094021005, 1094021006

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Fuels Department

Gasoline Range Organics LCS 197 98 ( 79-108 ) 200 ug/L 08/14/2009

LCSD 193 96 2 (< 20 ) 200 ug/L 08/14/2009

Surrogates 

4-Bromofluorobenzene <surr> LCS 96 ( 50-150 ) 08/14/2009

LCSD 97 2 08/14/2009

Batch

Method

Instrument

VFC9606

SW8015C

HP 5890 Series II PID+HECD VBA

60 of 75
Matrix

SGS Ref.# Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Original

Prep

1094021002 Billable Matrix Spike

1094021003 Billable Matrix Spike Dup.

1094021001

Water (Surface, Eff., Ground)

MXX22033

3010 H20 Digest for Metals ICP-MS

08/12/2009

QC results affect the following production samples:

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Dissolved Metals by ICP/MS

Lead BMS ND 999 100 ( 80-120 ) 1000 ug/L 08/18/2009

BMSD 989 99 1 (< 15 ) 1000 ug/L 08/18/2009

Batch

Method

Instrument

MMS6032

SW6020

Perkin Elmer Sciex ICP-MS P3

Volatile Fuels Department

Gasoline Range Organics BMS ND 432 96 ( 79-108 ) 450 ug/L 08/14/2009

BMSD 455 101 5 (< 20 ) 450 ug/L 08/14/2009

Surrogates 

4-Bromofluorobenzene <surr> BMS 50.8 102 ( 50-150 ) 08/14/2009

BMSD 50.4 101 1 08/14/2009

Batch

Method

Instrument

VFC9606

SW8015C

HP 5890 Series II PID+HECD VBA

Semivolatile Organic Fuels Department

Diesel Range Organics BMS ND 4.82 81 ( 75-125 ) 5.99 mg/L 08/08/2009

BMSD 4.89 82 1 (< 30 ) 5.99 mg/L 08/08/2009

Surrogates 

5a Androstane <surr> BMS .1 84 ( 50-150 ) 08/08/2009

BMSD 0.103 86 3 08/08/2009

Batch

Method

Instrument

XFC8762

SW8015C

HP 6890 Series II FID SV D R

Volatile Gas Chromatography/Mass Spectroscopy

61 of 75
Matrix

SGS Ref.# Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Original

Prep

1094021002 Billable Matrix Spike

1094021003 Billable Matrix Spike Dup.

1094021001

Water (Surface, Eff., Ground)

VXX19810

Volatiles Extraction AFCEE 3.1 8260 (

08/13/2009

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

Benzene BMS 0.470 29.2 96 ( 80-120 ) 30.0 ug/L 08/13/2009

BMSD 28.3 93 3 (< 20 ) 30.0 ug/L 08/13/2009

Toluene BMS ND 29.8 99 ( 77-120 ) 30.0 ug/L 08/13/2009

BMSD 28.9 96 3 (< 20 ) 30.0 ug/L 08/13/2009

Ethylbenzene BMS ND 31.3 104 ( 80-120 ) 30.0 ug/L 08/13/2009

BMSD 30.3 101 3 (< 20 ) 30.0 ug/L 08/13/2009

n-Butylbenzene BMS ND 33.3 111 ( 80-124 ) 30.0 ug/L 08/13/2009

BMSD 32.7 109 2 (< 20 ) 30.0 ug/L 08/13/2009

1,4-Dichlorobenzene BMS ND 29.7 99 ( 80-120 ) 30.0 ug/L 08/13/2009

BMSD 29.5 98 1 (< 20 ) 30.0 ug/L 08/13/2009

1,2-Dichloroethane BMS ND 32.5 108 ( 80-129 ) 30.0 ug/L 08/13/2009

BMSD 31.9 106 2 (< 20 ) 30.0 ug/L 08/13/2009

1,3,5-Trimethylbenzene BMS ND 31.6 105 ( 80-128 ) 30.0 ug/L 08/13/2009

BMSD 30.6 102 3 (< 20 ) 30.0 ug/L 08/13/2009

4-Chlorotoluene BMS ND 30.5 102 ( 79-128 ) 30.0 ug/L 08/13/2009

BMSD 29.8 99 3 (< 20 ) 30.0 ug/L 08/13/2009

Chlorobenzene BMS ND 30.1 100 ( 80-120 ) 30.0 ug/L 08/13/2009

BMSD 29.6 99 2 (< 20 ) 30.0 ug/L 08/13/2009

4-Methyl-2-pentanone (MIBK) BMS ND 84.3 94 ( 69-134 ) 90.0 ug/L 08/13/2009

BMSD 85.4 95 1 (< 20 ) 90.0 ug/L 08/13/2009

cis-1,2-Dichloroethene BMS ND 30.7 102 ( 80-125 ) 30.0 ug/L 08/13/2009

BMSD 30.0 100 2 (< 20 ) 30.0 ug/L 08/13/2009

4-Isopropyltoluene BMS ND 32.8 109 ( 80-125 ) 30.0 ug/L 08/13/2009

BMSD 32.1 107 2 (< 20 ) 30.0 ug/L 08/13/2009

cis-1,3-Dichloropropene BMS ND 32.7 109 ( 80-120 ) 30.0 ug/L 08/13/2009

BMSD 32.3 108 1 (< 20 ) 30.0 ug/L 08/13/2009

n-Propylbenzene BMS ND 32 107 ( 80-129 ) 30.0 ug/L 08/13/2009

BMSD 31.0 103 3 (< 20 ) 30.0 ug/L 08/13/2009

Styrene BMS ND 28.3 94 ( 80-120 ) 30.0 ug/L 08/13/2009

BMSD 26.9 90 5 (< 20 ) 30.0 ug/L 08/13/2009

Dibromomethane BMS ND 31.5 105 ( 80-120 ) 30.0 ug/L 08/13/2009

BMSD 31.6 105 0 (< 20 ) 30.0 ug/L 08/13/2009

trans-1,3-Dichloropropene BMS ND 32.6 109 ( 80-124 ) 30.0 ug/L 08/13/2009

BMSD 32.4 108 1 (< 20 ) 30.0 ug/L 08/13/2009

1,2,4-Trichlorobenzene BMS ND 29.6 99 ( 80-120 ) 30.0 ug/L 08/13/2009

BMSD 28.7 96 3 (< 20 ) 30.0 ug/L 08/13/2009

Acetone BMS ND 91 101 ( 50-135 ) 90.0 ug/L 08/13/2009

BMSD 90.0 100 1 (< 20 ) 90.0 ug/L 08/13/2009

1,1,2,2-Tetrachloroethane BMS ND 29.7 99 ( 76-123 ) 30.0 ug/L 08/13/2009

BMSD 29.6 99 0 (< 20 ) 30.0 ug/L 08/13/2009

62 of 75
Matrix

SGS Ref.# Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Original

Prep

1094021002 Billable Matrix Spike

1094021003 Billable Matrix Spike Dup.

1094021001

Water (Surface, Eff., Ground)

VXX19810

Volatiles Extraction AFCEE 3.1 8260 (

08/13/2009

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

1,2-Dibromo-3-chloropropane BMS ND 29 97 ( 73-130 ) 30.0 ug/L 08/13/2009

BMSD 28.4 95 2 (< 20 ) 30.0 ug/L 08/13/2009

Methyl-t-butyl ether BMS ND 45 100 ( 80-120 ) 45.0 ug/L 08/13/2009

BMSD 44.4 99 1 (< 20 ) 45.0 ug/L 08/13/2009

Tetrachloroethene BMS ND 30 100 ( 79-122 ) 30.0 ug/L 08/13/2009

BMSD 29.4 98 2 (< 20 ) 30.0 ug/L 08/13/2009

Dibromochloromethane BMS ND 31.4 105 ( 80-120 ) 30.0 ug/L 08/13/2009

BMSD 30.7 102 2 (< 20 ) 30.0 ug/L 08/13/2009

1,3-Dichloropropane BMS ND 30.7 102 ( 80-121 ) 30.0 ug/L 08/13/2009

BMSD 29.6 99 4 (< 20 ) 30.0 ug/L 08/13/2009

1,2-Dibromoethane BMS ND 30.7 102 ( 80-120 ) 30.0 ug/L 08/13/2009

BMSD 30.2 101 2 (< 20 ) 30.0 ug/L 08/13/2009

Carbon tetrachloride BMS ND 35.8 119 ( 80-126 ) 30.0 ug/L 08/13/2009

BMSD 34.4 115 4 (< 20 ) 30.0 ug/L 08/13/2009

1,1,1,2-Tetrachloroethane BMS ND 29.3 98 ( 80-120 ) 30.0 ug/L 08/13/2009

BMSD 29.2 97 0 (< 20 ) 30.0 ug/L 08/13/2009

Chloroform BMS ND 33.2 111 ( 80-124 ) 30.0 ug/L 08/13/2009

BMSD 32.8 109 1 (< 20 ) 30.0 ug/L 08/13/2009

Bromobenzene BMS ND 28.9 96 ( 80-120 ) 30.0 ug/L 08/13/2009

BMSD 28.3 94 2 (< 20 ) 30.0 ug/L 08/13/2009

Chloromethane BMS ND 28.7 96 ( 67-125 ) 30.0 ug/L 08/13/2009

BMSD 28.4 95 1 (< 20 ) 30.0 ug/L 08/13/2009

1,2,3-Trichloropropane BMS ND 29.8 99 ( 80-120 ) 30.0 ug/L 08/13/2009

BMSD 28.8 96 4 (< 20 ) 30.0 ug/L 08/13/2009

Bromomethane BMS ND 44.2 147* ( 30-140 ) 30.0 ug/L 08/13/2009

BMSD 45.9 153* 4 (< 20 ) 30.0 ug/L 08/13/2009

Bromochloromethane BMS ND 30.8 103 ( 77-129 ) 30.0 ug/L 08/13/2009

BMSD 30.1 100 3 (< 20 ) 30.0 ug/L 08/13/2009

Vinyl chloride BMS ND 30.6 102 ( 72-145 ) 30.0 ug/L 08/13/2009

BMSD 29.9 100 2 (< 20 ) 30.0 ug/L 08/13/2009

Dichlorodifluoromethane BMS ND 31.7 106 ( 62-153 ) 30.0 ug/L 08/13/2009

BMSD 30.2 101 5 (< 20 ) 30.0 ug/L 08/13/2009

Chloroethane BMS ND 46.1 154* ( 67-133 ) 30.0 ug/L 08/13/2009

BMSD 44.5 148* 4 (< 20 ) 30.0 ug/L 08/13/2009

sec-Butylbenzene BMS ND 32.4 108 ( 80-120 ) 30.0 ug/L 08/13/2009

BMSD 31.8 106 2 (< 20 ) 30.0 ug/L 08/13/2009

Bromodichloromethane BMS ND 33.3 111 ( 80-120 ) 30.0 ug/L 08/13/2009

BMSD 32.6 109 2 (< 20 ) 30.0 ug/L 08/13/2009

1,1-Dichloroethene BMS ND 31.6 105 ( 76-130 ) 30.0 ug/L 08/13/2009

BMSD 31.2 104 1 (< 20 ) 30.0 ug/L 08/13/2009

63 of 75
Matrix

SGS Ref.# Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Original

Prep

1094021002 Billable Matrix Spike

1094021003 Billable Matrix Spike Dup.

1094021001

Water (Surface, Eff., Ground)

VXX19810

Volatiles Extraction AFCEE 3.1 8260 (

08/13/2009

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

2-Butanone (MEK) BMS ND 94.1 105 ( 66-136 ) 90.0 ug/L 08/13/2009

BMSD 93.9 104 0 (< 20 ) 90.0 ug/L 08/13/2009

Methylene chloride BMS ND 29.6 99 ( 63-131 ) 30.0 ug/L 08/13/2009

BMSD 28.8 96 3 (< 20 ) 30.0 ug/L 08/13/2009

Trichlorofluoromethane BMS ND 36.7 122 ( 68-145 ) 30.0 ug/L 08/13/2009

BMSD 35.8 119 3 (< 20 ) 30.0 ug/L 08/13/2009

P & M -Xylene BMS ND 62.8 105 ( 80-120 ) 60.0 ug/L 08/13/2009

BMSD 61.7 103 2 (< 20 ) 60.0 ug/L 08/13/2009

Naphthalene BMS ND 28.6 95 ( 75-120 ) 30.0 ug/L 08/13/2009

BMSD 27.9 93 2 (< 20 ) 30.0 ug/L 08/13/2009

o-Xylene BMS ND 31.5 105 ( 80-120 ) 30.0 ug/L 08/13/2009

BMSD 30.7 102 3 (< 20 ) 30.0 ug/L 08/13/2009

Bromoform BMS ND 32 107 ( 80-120 ) 30.0 ug/L 08/13/2009

BMSD 31.5 105 1 (< 20 ) 30.0 ug/L 08/13/2009

1-Chlorohexane BMS ND 50.7 113 ( 70-125 ) 45.0 ug/L 08/13/2009

BMSD 48.2 107 5 (< 20 ) 45.0 ug/L 08/13/2009

1,2,4-Trimethylbenzene BMS ND 31.3 104 ( 80-125 ) 30.0 ug/L 08/13/2009

BMSD 30.5 102 3 (< 20 ) 30.0 ug/L 08/13/2009

tert-Butylbenzene BMS ND 32.2 107 ( 80-122 ) 30.0 ug/L 08/13/2009

BMSD 31.3 104 3 (< 20 ) 30.0 ug/L 08/13/2009

1,1,1-Trichloroethane BMS ND 34.8 116 ( 80-122 ) 30.0 ug/L 08/13/2009

BMSD 34.0 113 3 (< 20 ) 30.0 ug/L 08/13/2009

1,1-Dichloroethane BMS ND 34.1 114 ( 80-120 ) 30.0 ug/L 08/13/2009

BMSD 32.9 110 3 (< 20 ) 30.0 ug/L 08/13/2009

2-Chlorotoluene BMS ND 30.6 102 ( 80-125 ) 30.0 ug/L 08/13/2009

BMSD 29.8 99 3 (< 20 ) 30.0 ug/L 08/13/2009

Trichloroethene BMS ND 31.1 104 ( 80-125 ) 30.0 ug/L 08/13/2009

BMSD 30.0 100 4 (< 20 ) 30.0 ug/L 08/13/2009

trans-1,2-Dichloroethene BMS ND 32.2 107 ( 79-132 ) 30.0 ug/L 08/13/2009

BMSD 31.4 105 3 (< 20 ) 30.0 ug/L 08/13/2009

1,2-Dichlorobenzene BMS ND 29.1 97 ( 80-120 ) 30.0 ug/L 08/13/2009

BMSD 28.6 95 2 (< 20 ) 30.0 ug/L 08/13/2009

2,2-Dichloropropane BMS ND 35.3 118 ( 80-132 ) 30.0 ug/L 08/13/2009

BMSD 34.0 113 4 (< 20 ) 30.0 ug/L 08/13/2009

Hexachlorobutadiene BMS ND 31.1 104 ( 77-125 ) 30.0 ug/L 08/13/2009

BMSD 30.8 103 1 (< 20 ) 30.0 ug/L 08/13/2009

Isopropylbenzene (Cumene) BMS ND 33.4 111 ( 80-121 ) 30.0 ug/L 08/13/2009

BMSD 32.5 108 3 (< 20 ) 30.0 ug/L 08/13/2009

1,2-Dichloropropane BMS ND 30.5 102 ( 80-121 ) 30.0 ug/L 08/13/2009

BMSD 29.7 99 3 (< 20 ) 30.0 ug/L 08/13/2009

64 of 75
Matrix

SGS Ref.# Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Original

Prep

1094021002 Billable Matrix Spike

1094021003 Billable Matrix Spike Dup.

1094021001

Water (Surface, Eff., Ground)

VXX19810

Volatiles Extraction AFCEE 3.1 8260 (

08/13/2009

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

1,1-Dichloropropene BMS ND 32.5 108 ( 80-122 ) 30.0 ug/L 08/13/2009

BMSD 32.1 107 1 (< 20 ) 30.0 ug/L 08/13/2009

1,1,2-Trichloroethane BMS ND 30.7 102 ( 77-120 ) 30.0 ug/L 08/13/2009

BMSD 30.2 101 1 (< 20 ) 30.0 ug/L 08/13/2009

1,3-Dichlorobenzene BMS ND 29.4 98 ( 80-120 ) 30.0 ug/L 08/13/2009

BMSD 28.9 96 2 (< 20 ) 30.0 ug/L 08/13/2009

1,2,3-Trichlorobenzene BMS ND 29 97 ( 77-120 ) 30.0 ug/L 08/13/2009

BMSD 29.1 97 0 (< 20 ) 30.0 ug/L 08/13/2009

Surrogates 

1,2-Dichloroethane-D4 <surr> BMS 33.3 111 ( 73-120 ) 08/13/2009

BMSD 34.2 114 3 08/13/2009

Toluene-d8 <surr> BMS 29.5 98 ( 80-120 ) 08/13/2009

BMSD 29.7 99 1 08/13/2009

4-Bromofluorobenzene <surr> BMS 29.6 99 ( 76-120 ) 08/13/2009

BMSD 29.1 97 2 08/13/2009

Batch

Method

Instrument

VMS10730

SW8260B

HP 5890 Series II MS3 VNA

Polynuclear Aromatics GC/MS

65 of 75
Matrix

SGS Ref.# Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Original

Prep

1094021002 Billable Matrix Spike

1094021003 Billable Matrix Spike Dup.

1094021001

Water (Surface, Eff., Ground)

XXX21374

3520 Liquid/Liquid Ext for 8270 SIM

08/07/2009

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Polynuclear Aromatics GC/MS

Acenaphthylene BMS ND .539 92 ( 50-105 ) 0.585 ug/L 08/12/2009

BMSD 0.541 96 0 (< 30 ) 0.565 ug/L 08/12/2009

Acenaphthene BMS ND .497 85 ( 45-110 ) 0.585 ug/L 08/12/2009

BMSD 0.487 86 2 (< 30 ) 0.565 ug/L 08/12/2009

Fluorene BMS ND .539 92 ( 50-110 ) 0.585 ug/L 08/12/2009

BMSD 0.532 94 1 (< 30 ) 0.565 ug/L 08/12/2009

Phenanthrene BMS ND .544 93 ( 50-115 ) 0.585 ug/L 08/12/2009

BMSD 0.549 97 1 (< 30 ) 0.565 ug/L 08/12/2009

Anthracene BMS ND .596 102 ( 55-110 ) 0.585 ug/L 08/12/2009

BMSD 0.583 103 2 (< 30 ) 0.565 ug/L 08/12/2009

Fluoranthene BMS ND .603 103 ( 55-125 ) 0.585 ug/L 08/12/2009

BMSD 0.589 104 2 (< 30 ) 0.565 ug/L 08/12/2009

Pyrene BMS ND .58 99 ( 50-130 ) 0.585 ug/L 08/12/2009

BMSD 0.562 100 3 (< 30 ) 0.565 ug/L 08/12/2009

Benzo(a)Anthracene BMS ND .649 111 ( 55-120 ) 0.585 ug/L 08/12/2009

BMSD 0.609 108 6 (< 30 ) 0.565 ug/L 08/12/2009

Chrysene BMS ND .587 100 ( 55-120 ) 0.585 ug/L 08/12/2009

BMSD 0.545 97 8 (< 30 ) 0.565 ug/L 08/12/2009

Benzo[b]Fluoranthene BMS ND .63 108 ( 46-130 ) 0.585 ug/L 08/12/2009

BMSD 0.596 105 6 (< 30 ) 0.565 ug/L 08/12/2009

Benzo[k]fluoranthene BMS ND .605 103 ( 60-125 ) 0.585 ug/L 08/12/2009

BMSD 0.608 108 1 (< 30 ) 0.565 ug/L 08/12/2009

Benzo[a]pyrene BMS ND .64 109 ( 55-120 ) 0.585 ug/L 08/12/2009

BMSD 0.638 113 0 (< 30 ) 0.565 ug/L 08/12/2009

Indeno[1,2,3-c,d] pyrene BMS ND .591 101 ( 45-125 ) 0.585 ug/L 08/12/2009

BMSD 0.584 103 1 (< 30 ) 0.565 ug/L 08/12/2009

Dibenzo[a,h]anthracene BMS ND .6 103 ( 41-140 ) 0.585 ug/L 08/12/2009

BMSD 0.605 107 1 (< 30 ) 0.565 ug/L 08/12/2009

Benzo[g,h,i]perylene BMS ND .598 102 ( 46-125 ) 0.585 ug/L 08/12/2009

BMSD 0.604 107 1 (< 30 ) 0.565 ug/L 08/12/2009

Naphthalene BMS ND .494 84 ( 42-100 ) 0.585 ug/L 08/12/2009

BMSD 0.472 84 5 (< 30 ) 0.565 ug/L 08/12/2009

1-Methylnaphthalene BMS ND .492 84 ( 46-115 ) 0.585 ug/L 08/12/2009

BMSD 0.486 86 1 (< 30 ) 0.565 ug/L 08/12/2009

2-Methylnaphthalene BMS ND .459 78 ( 45-105 ) 0.585 ug/L 08/12/2009

BMSD 0.462 82 1 (< 30 ) 0.565 ug/L 08/12/2009

Surrogates 

Terphenyl-d14 <surr> BMS .596 102 ( 50-135 ) 08/12/2009

BMSD 0.568 101 5 08/12/2009

66 of 75
Matrix

SGS Ref.# Printed Date/Time 08/20/2009 13:51

Batch

Method

Date

Original

Prep

1094021002 Billable Matrix Spike

1094021003 Billable Matrix Spike Dup.

1094021001

Water (Surface, Eff., Ground)

XXX21374

3520 Liquid/Liquid Ext for 8270 SIM

08/07/2009

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Polynuclear Aromatics GC/MS

Batch

Method

Instrument

XMS5029

8270D SIMS

HP 6890/5973 MS SVQA

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