Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.
1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

-down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected
more. 8. Provide the results of the analyses for each constituent requested. Use the drop

-down boxes to fill in the units of
measure.Information
This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

130 Santee Cooper-Cross Unit 3 bituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte An alysis M ethod for each Analyte (example: ASTM D5865-04) 130 Santee Cooper-Cross Unit 3 As Received Higher Heating Value ASTM D 240 130 Santee Cooper-Cross Unit 3 As Received % Moisture ASTM D 2216 130 Santee Cooper-Cross Unit 3 As Received Antim ony SW846 3050B/6020A 130 Santee Cooper-Cross Unit 3 As Received Arsenic SW846 3050B/6020A 130 Santee Cooper-Cross Unit 3 As Received Beryllium SW846 3050B/6020A 130 Santee Cooper-Cross Unit 3 As Received Cadmium SW846 3050B/6020A 130 Santee Cooper-Cross Unit 3 As Received Chlorine SW846 5050/9056A 130 Santee Cooper-Cross Unit 3 As Received Chromium SW846 3050B/6020A 130 Santee Cooper-Cross Unit 3 As Received Cobalt SW846 3050B/6020A 130 Santee Cooper-Cross Unit 3 As Received Fluorine SW846 5050/9056A 130 Santee Cooper-Cross Unit 3 As Received Lead SW846 3050B/6020A 130 Santee Cooper-Cross Unit 3 As Received Manganese SW846 3050B/6020A 130 Santee Cooper-Cross Unit 3 As Received Mercury SW846 7471B 130 Santee Cooper-Cross Unit 3 As Received Nickel SW846 3050B/6020A 130 Santee Cooper-Cross Unit 3 As Received Selenium SW846 3050B/6020AEIA

Facility Code Facility

Name Boiler ID 130 Santee Cooper-Cross Unit 3

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units % Moisture (as received) Chlorine

(Dry Basis) RUN 1 6/18/2010 6/18/2010 11900.00 Btu/lb 6.14 1120000 RUN 2 6/18/2010 6/18/2010 13300.00 Btu/lb 5.55 1050000 RUN 3 6/18/2010 6/18/2010 14500.00 Btu/lb 5.70 940000 HAPs Test Group Mercury and non-mercury metalic HAPs

Fuel Testing ResultsChlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units μg/Kg 17.6 μg/Kg <587 μg/Kg 24800 μg/Kg 1130 μg/Kg μg/Kg 13.3 μg/Kg 106 μg/Kg 10800 μg/Kg 818 μg/Kg μg/Kg 15.5 μg/Kg <576 μg/Kg 13200 μg/Kg 876 μg/KgCadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel

(Dry Basis) 71.6 μg/Kg 5360 μg/Kg 4740 μg/Kg 11200 μg/Kg 7670 66.5 μg/Kg 4740 μg/Kg 4750 μg/Kg 9700 μg/Kg 8390 70.2 μg/Kg 4470 μg/Kg 4870 μg/Kg 10900 μg/Kg 7590Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units μg/Kg 2280 μg/Kg 65300 μg/Kg 3210 μg/Kg μg/Kg 1830 μg/Kg 78100 μg/Kg 3310 μg/Kg μg/Kg 1910 μg/Kg 70900 μg/Kg 3710 μg/KgEIA

Facility Code Facility

Name Boiler ID 130 Santee Cooper-Cross Unit 3

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) Chlorine

(Dry Basis) RUN 1 6/17/2010 6/17/2010 12800.00 Btu/lb 5.74 1220000 RUN 2 6/17/2010 6/17/2010 18000.00 Btu/lb 5.48 1050000 RUN 3 6/17/2010 6/17/2010 11700.00 Btu/lb 5.88 1070000 HAPs Test Group

Fuel Testing Results Acid gas HAPsChlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units μg/Kg 10.4 μg/Kg 109 μg/Kg 16300 μg/Kg 908 μg/Kg μg/Kg 19.8 μg/Kg 111 μg/Kg 12100 μg/Kg 1010 μg/Kg μg/Kg 16.1 μg/Kg 114 μg/Kg 14200 μg/Kg 947 μg/KgCadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel

(Dry Basis) 94.8 μg/Kg 5480 μg/Kg 4210 μg/Kg 17100 μg/Kg 11700 99.6 μg/Kg 6120 μg/Kg 4970 μg/Kg 17400 μg/Kg 9680 67.1 μg/Kg 4760 μg/Kg 3660 μg/Kg 15100 μg/Kg 7760Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units μg/Kg 2280 μg/Kg 87200 μg/Kg 3820 μg/Kg μg/Kg 4290 μg/Kg 67400 μg/Kg 3870 μg/Kg μg/Kg 1900 μg/Kg 66600 μg/Kg 3070 μg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/Kg μg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm μg/Kg