Initial to indicate certification as to information on this page (full text of certification is on page one). Date INSTRUCTIONS: Please type or print in ink. Please read carefully the attached instructions and supply the information requested on this form. Use additional sheet(s) if necessary. 2. Case # and Name 3. Date and Type of DCI and Number

4. EPA Product Registration 5. I wish to cancel this product registration voluntarily 6. Generic Data 7. Product Specific Data 6a. I am claiming a Generic Data Exemption because I obtain the active ingredient from the source EPA registration number listed below. 6b. I agree to satisfy Generic Data Requirements as indicated on the attached form entitled "Requirements Status and Registrant's Response." 7a. My product is an MUP and I agree to satisfy the MUP requirement on the attached form entitled "Requirements Status and Registrant's Response." 7b. My product is an EUP and I agree to satisfy the EUP requirement on the attached form entitled "Requirements Status and Registrant's Response." OMB Approval 2070-0174 EPA FORM 6300-4

1. Company Name and Address ADAMA AGAN LTD. 3120 HIGHWOODS BLVD., SUITE 100 RALEIGH, NC 27604 2490 - Oxyfluorfen Chemical # and Name: 111601 Oxyfluorfen 12-Jan-2016 GENERIC ID # GDCI-111601-1515 

### United States Environmental Protection Agency

Washington, D.C. 20460 DATA CALL-IN RESPONSE 1 Page of 1

11603-29

8. Certification: I certify that the statements made on this form and all attachments are true, accurate, and complete. I acknowledge that any knowingly false or misleading statement may be punishable by fine, imprisonment or both under applicable law. Signature and Title of Company's Authorized Representative ______________________________________________________ 10. Name of Company N/A N/A

9. Date
11. Phone NumberInitial to indicate certification as to information on this page (full text of certification is on page one) 13. Phone Number 10. Certification: I certify that the statements made on this form and all attachments are true, accurate, and complete. I acknowledge that any knowingly false or misleading statement may be punishable by fine, imprisonment or both under applicable law. 12. Name of Company 11. Date OMB Approval 2070-0174 EPA FORM 6300-3 

### United States Environmental Protection Agency

Washington, D.C. 20460 REQUIREMENTS STATUS AND REGISTRANT'S RESPONSE INSTRUCTIONS: Please type or print in ink. Please read carefully the attached instructions and supply the information requested on this form. Use additional sheet(s) if necessary.

4. Guideline Requirement Number 5. Study Title Progress Reports



### 2 3 1 6. Use

Pattern 7. Test Substance 8. Time Frame (Months) 9. Registrant

Response P R O T O C O L 1. Company Name and Address 2. Case # and Name 3. Date and Type of DCI and Number

Signature and Title of Company's Authorized Representative _________________________________________________________________ ADAMA AGAN LTD. 3120 HIGHWOODS BLVD., SUITE 100 RALEIGH, NC 27604

Environmental Fate Data Requirements (Conventional Chemical)

Post-Application Exposure Data Requirements (Conventional Chemical) Terrestrial and Aquatic Nontarget Organisms Data Requirements (Conventional Chemical) 835.2240 835.4300 835.4400

875.2100

850.1075 850.1400 Direct photolysis rate of parent and degradates in

water Aerobic aquatic metabolism Anaerobic aquatic metabolism
Foliar dislodgeable residue dissipation
Fish acute toxicity test, freshwater and marine Fish early-life stage toxicity test 2490 - Oxyfluorfen Chemical # and Name: 111601 Oxyfluorfen 12-Jan-2016 GENERIC ID # GDCI-111601-1515

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J,U,I,M,II,Q,C,R,A
J,U,I,M,II,Q,C,R,A J,U,I,M,II,Q,C,R,A TGAI TGAI TGAI

TEP

TGAI TGAI 12 24 24

12

12 12 1 of Page

(13) (13)
(1)
(7) (6, 14) N

N N

Y

N N 3OMB Approval 2070-0174 EPA FORM 6300-3 

### United States Environmental Protection Agency

Washington, D.C. 20460 REQUIREMENTS STATUS AND REGISTRANT'S RESPONSE INSTRUCTIONS: Please type or print in ink. Please read carefully the attached instructions and supply the information requested on this form. Use additional sheet(s) if necessary.

4. Guideline Requirement Number 5. Study Title Progress Reports



### 2 3 1 6. Use

Pattern 7. Test Substance 8. Time Frame (Months) 9. Registrant

Response P R O T O C O L 1. Company Name and Address 2. Case # and Name 3. Date and Type of DCI and Number ADAMA AGAN LTD. 3120 HIGHWOODS BLVD., SUITE 100 RALEIGH, NC 27604

Terrestrial and Aquatic Nontarget Organisms Data Requirements (Conventional Chemical)
Toxicology Data Requirements (Conventional Chemical) 850.2100 850.3040
870.3200

850.6100 SS-1113 SS-1311 Avian acute oral toxicity test

Field testing for pollinators 21/28-day dermal toxicity Environmental Chemistry Methods and Associated Independent Laboratory Validation Residue Analysis of Nectar and Pollen in Flowering Crops Honey bee adult acute oral toxicity 2490 - Oxyfluorfen Chemical # and Name: 111601 Oxyfluorfen 12-Jan-2016 GENERIC ID # GDCI-111601-1515

J,U,I,M,II,Q,C,R,A J,U,I,M,II,Q,C,R,A
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N

N Y Y 3Date OMB Approval 2070-0174 EPA FORM 6300-3 

### United States Environmental Protection Agency

Washington, D.C. 20460 REQUIREMENTS STATUS AND REGISTRANT'S RESPONSE INSTRUCTIONS: Please type or print in ink. Please read carefully the attached instructions and supply the information requested on this form. Use additional sheet(s) if necessary.

4. Guideline Requirement Number 5. Study Title Progress Reports



### 2 3 1 6. Use

Pattern 7. Test Substance 8. Time Frame (Months) 9. Registrant

Response P R O T O C O L 1. Company Name and Address 2. Case # and Name 3. Date and Type of DCI and Number ADAMA AGAN LTD. 3120 HIGHWOODS BLVD., SUITE 100 RALEIGH, NC 27604

SS-1312 SS-1313 SS-1314 SS-1319 Honey bee larvae acute oral toxicity

Honey bee adult chronic oral toxicity Honey bee larvae chronic oral toxicity Semi-field testing for pollinators (tunnel or colony feeding studies) 2490 - Oxyfluorfen Chemical # and Name: 111601 Oxyfluorfen 12-Jan-2016 GENERIC ID # GDCI-111601-1515

J,U,I,M,II,Q,C,R,A J,U,I,M,II,Q,C,R,A J,U,I,M,II,Q,C,R,A J,U,I,M,II,Q,C,R,A TGAI TGAI TGAI TEP 12 12 12 24 3 of Page

(11) (9) (10) (3, 13) Y

Y Y Y 3

### United States Environmental Protection Agency Washington, D.C. 20460 FOOTNOTES AND KEY DEFINITIONS FOR GUIDELINE REQUIREMENTS 2490 - Oxyfluorfen GDCI-111601-1515

1 2 3

4 Key: Residue of Concern = Residue of Concern; TEP = Typical End Use Product [TEP]; TGAI = Technical Grade Active Ingredient [TGAI]; TGAI/PAIRA = Technical Grade of the Active Ingredient or Pure Active Ingredient, Radio Labelled; TGAI, TEP = Technical Grade of the Active Ingredient or Technical End-Use Product; TGAI/PAI = Technical Grade Active Ingredient, Pure Active Ingredient

This study is to be completed using a bulb vegetable crop; see the Scoping Document for details. Protocols must be submitted for approval prior to the initiation of the study. Details for developing protocols are available from the Agency at http://www.epa.gov/pesticide-science-and-assessing-pesticide-risks/test-guidelines-pesticide-data-requirements. This study and its requirements (ECM/ILV) is needed for both soil and water. The need for a semi-field test for pollinators (i.e., either a field-feeding test or a tunnel test) will be determined based upon lower-tiered tests and/or other lines of evidence, and the need for a refined pollinator risk assessment. Formal guidelines for semi-field tests do not yet exist; however, information that can help guide the development of either a semi-field tunnel test protocol can be found at OECD 75, see: OECD. 2007. Series on Testing and Assessment Number 75. Guidance document on the honey bee (Apis mellifera L.) brood test under semi-field conditions. Environmental Directorate Joint Meeting of the Chemicals Committee and the Working Party on Chemicals, Pesticides and Biotechnology. ENV/JM/MONO(2007)22. 31-Aug-2007. http://www.oecd.org/officialdocuments/publicdisplaydocumentpdf/?cote=env/jm/mono(2007)22&doclanguage=en. For field-feeding studies see: Oomen et al. 1992: Oomen, P. A. A. DeRuijter and J. Van der Steen. 1992. Method for honey bee brood feeding tests with insect growth-regulating insecticides. Bul OEPP/EPPO Bulletin 22: 613 ¿ 616. See also the guidance identified in the EPA document, Guidance Implementation of Exposure and Effects Testing for Assessing Risks to Bees, Appendix 2. A study protocol must be submitted to, and reviewed by EPA, prior to study initiation. The need for a field test for pollinators will be determined based upon lower-tiered tests and/or other lines of data and the need for a refined pollinator risk assessment. Case # and Name: DCI Number: 1 Page: of

Footnotes: The following footnotes are referenced in column two (5. Study Title) of the Requirements Status and Registrant's Response form. These footnotes apply in addition to any test notes included in 40 CFR Part 158 with respect to the particular data requirement. Use Categories Key: A - Terrestrial food crop C - Terrestrial nonfood crop I - Greenhouse nonfood crop J - Forestry use M - Indoor nonfood use Q - Residential outdoor use R - Agricultural premises and equipment U - Residential and public access premises II - Residential Use Conventional Chemical 3

### United States Environmental Protection Agency Washington, D.C. 20460 FOOTNOTES AND KEY DEFINITIONS FOR GUIDELINE REQUIREMENTS 2490 - Oxyfluorfen GDCI-111601-1515

5 6 7 8

9

10 Key: Residue of Concern = Residue of Concern; TEP = Typical End Use Product [TEP]; TGAI = Technical Grade Active Ingredient [TGAI]; TGAI/PAIRA = Technical Grade of the Active Ingredient or Pure Active Ingredient, Radio Labelled; TGAI, TEP = Technical Grade of the Active Ingredient or Technical End-Use Product; TGAI/PAI = Technical Grade Active Ingredient, Pure Active Ingredient

See information and guidance identified in the EPA documents, (i) USEPA. 2012. White Paper in Support of the Proposed Risk Assessment Process for Bees. Submitted to the FIFRA Scientific Advisory Panel for Review and Comment September 11 ¿ 14, 2012. Office of Chemical Safety and Pollution Prevention Office of Pesticide Programs Environmental Fate and Effects Division, Environmental Protection Agency, Washington DC; Environmental Assessment Directorate, Pest Management Regulatory Agency, Health Canada, Ottawa, CN; California Department of Pesticide Regulation http://www.regulations.gov/#!documentDetail;D=EPA-HQ-OPP-2012-0543-0004; (ii) 2014 Guidance for Assessing Pesticide Risks to Bees. Office of Pesticide Programs United States Environmental Protection Agency, Health Canada Pest Management Regulatory Agency, California Department of Pesticide Regulation. June 19, 2014. http://www2.epa.gov/sites/production/files/2014-06/documents/pollinator_risk_assessment_guidance_06_19_14.pdf ; and, (iii) EPAs Guidance Implementation of Exposure and Effects Testing for Assessing Risks to Bees, Appendix 3. USEPA. 2012c. ¿Field Testing for Pollinators.¿ Ecological Effects Test Guidelines OCSPP 850.3040. EPA 712-C-017. Web. http://www.regulations.gov/#!documentDetail;D=EPA-HQ-OPPT-2009- 0154-0018 A study protocol must be submitted to, and reviewed by EPA, prior to study initiation. Test is for a passerine species only. Study is being request only for estuarine/marine fish. Specific requirements for this study can be found in table 11-3 of the problem formulation (PF) for oxyfluorfen. The Agency is requesting an estuarine/marine fish study, or a freshwater study specifically with the fathead minnow, not both studies as indicated in the study title.See the OECD 213: OECD Guidelines for the Testing of Chemicals. Honeybees, Acute Oral Toxicity Test. 213. http://lysander.sourceoecd.org/vl=5988235/cl=12/nw=1/rpsv/cgibin/fulltextew.pl?prpsv=/ij/oecdjournals/1607310x/v1n2/s14/p1.idx A study protocol must be submitted to, and reviewed by EPA, prior to study initiation. OECD has not yet finalized test guidelines for chronic studies, and efforts are underway to develop standardized guidelines for assessing the effects from chronic exposure to adult and larvae in the laboratory. Discussion of the study design elements for the 10-day adult toxicity test can be found in Appendix O of the European Food Safety Authority (EFSA) guidance document: EFSA. Guidance on the risk assessment of plant protection products on bees (Apis mellifera, Bombus spp. and solitary bees. EFSA Journal 2013;11(7):3295, 266 pp. doi:10.2903/j.efsa.2013.3295. Available online at: http://www.efsa.europa.eu/en/efsajournal/doc/3295.pdf. A study protocol must be submitted to, and reviewed by EPA, prior to study initiation. OECD has not yet finalized test guidelines for chronic studies with honey bee larvae. OECD draft guidance has is being developed, see OECD 2013b. OECD Draft Guidance Document Honey Bee (Apis mellifera) Larval Toxicity Test, Repeated Exposure. http://www.oecd.org/env/ehs/testing/Draft_GD_honeybees_rep_exp_for_2nd_CR_25_November_2013.pdf In some cases, information pertaining to acute toxicity to honey bee larvae may be obtained with the chronic honey bee larvae test thereby negating the need for separate acute and chronic larval toxicity tests. See also the guidance identified in the EPA document, Guidance Implementation of Exposure and Effects Testing for Assessing Risks to Bees, Appendix 1. A study protocol must be submitted to, and reviewed by EPA, prior to study initiation. Case # and Name: DCI Number: 2 Page: of 3

### United States Environmental Protection Agency Washington, D.C. 20460 FOOTNOTES AND KEY DEFINITIONS FOR GUIDELINE REQUIREMENTS 2490 - Oxyfluorfen GDCI-111601-1515

11

12

13 14 Key: Residue of Concern = Residue of Concern; TEP = Typical End Use Product [TEP]; TGAI = Technical Grade Active Ingredient [TGAI]; TGAI/PAIRA = Technical Grade of the Active Ingredient or Pure Active Ingredient, Radio Labelled; TGAI, TEP = Technical Grade of the Active Ingredient or Technical End-Use Product; TGAI/PAI = Technical Grade Active Ingredient, Pure Active Ingredient

OECD Test Guideline 237 may be used to develop a protocol for this study (OECD. 2013 Guidelines for Testing Chemicals. Honey bee (Apis mellifera) larval toxicity test, single exposure.) See: http://www.oecd-ilibrary.org/environment/test-no-237-honey-bee-apis-mellifera-larval-toxicity-test-single-exposure_9789264203723-en In some cases, information pertaining to acute toxicity to honey bee larvae may be obtained with the chronic honey bee larvae test thereby negating the need for separate acute and chronic larval toxicity tests. A study protocol must be submitted to, and reviewed by EPA, prior to study initiation. Measurements of residues in the pollen/nectar are needed based upon lower-tiered tests and/or other lines of evidence, and the need for a refined pollinator risk assessment. A study protocol must be submitted to, and reviewed by EPA, prior to study initiation. The following elements should be considered when developing study protocol(s) for the monitoring of residues in pollen/nectar. Consideration of the range of application methods and environmental conditions (e.g., soil and hydric regimes) that the target crop(s) may be under. Consideration of the attractiveness of the selected crop to pollinators Consideration of a collection schedule sufficient to allow for an understanding of the character of residues, in the pollen/nectar and/or plant tissues, over time. Consideration of data sufficient to determine whether residues of the active ingredient and/or degradation product(s) accumulates in soil and is/are bioavailable for plant to uptake in a following planting, and therefore result in potential exposure to pollinators. Consideration of the market proportion of the selected target crop(s). A study protocol must be submitted to, and reviewed by EPA, prior to study initiation. For each study having a 24-month time frame, a progress report at 9 months and 18 months is required to be submitted to the Agency. Data are preferred on sheepshead minnow (Cypinodon variegatus). Case # and Name: DCI Number: 3 Page: of 3

### United States Environmental Protection Agency Washington, D.C. 20460 LIST OF ALL REGISTRANTS SENT THIS DATA CALL-IN NOTICE 2490 - Oxyfluorfen Case # and Name: 1 Page: of 1

87283 62719 70506 11603 42750 WILLOWOOD OXYFLUORFEN, LLC

DOW AGROSCIENCES LLC UNITED PHOSPHORUS, INC ADAMA AGAN LTD. ALBAUGH, LLC Co. Nr. Company Name Agent For Company PYXIS REGULATORY CONSULTING, INC.

MAKHTESHIM-AGAN OF NORTH AMERICA INC 4110 136TH STREET, NW 9330 ZIONSVILLE RD 308/2E 630 FREEDOM BUSINESS CENTER, SUITE 402 3120 HIGHWOODS BLVD., SUITE 100 P.O. Box 2127 Address City ZIP GIG HARBOR INDIANAPOLIS KING OF PRUSSIA RALEIGH VALDOSTA 98332 462681054 19406 27604 316042127 OMB Approval 2070-0174

State WA IN PA NC GA DCI Number: GDCI-111601-1515

### United States Environmental Protection Agency Washington, D.C. 20460 LIST OF ALL REGISTRANTS SENT THIS DATA CALL-IN NOTICE 2490 - Oxyfluorfen Case # and Name: 1 Page: of 1

87283 62719 70506 11603 42750 WILLOWOOD OXYFLUORFEN, LLC

DOW AGROSCIENCES LLC UNITED PHOSPHORUS, INC ADAMA AGAN LTD. ALBAUGH, LLC Co. Nr. Company Name Agent For Company PYXIS REGULATORY CONSULTING, INC.

MAKHTESHIM-AGAN OF NORTH AMERICA INC 4110 136TH STREET, NW 9330 ZIONSVILLE RD 308/2E 630 FREEDOM BUSINESS CENTER, SUITE 402 3120 HIGHWOODS BLVD., SUITE 100 P.O. Box 2127 Address City ZIP GIG HARBOR INDIANAPOLIS KING OF PRUSSIA RALEIGH VALDOSTA 98332 462681054 19406 27604 316042127 OMB Approval 2070-0174

State WA IN PA NC GA DCI Number: GDCI-111601-1515

### United States Environmental Protection Agency Washington, D.C. 20460 LIST OF ALL REGISTRANTS SENT THIS DATA CALL-IN NOTICE 2490 - Oxyfluorfen Case # and Name: 1 Page: of 1

87283 62719 70506 11603 42750 WILLOWOOD OXYFLUORFEN, LLC

DOW AGROSCIENCES LLC UNITED PHOSPHORUS, INC ADAMA AGAN LTD. ALBAUGH, LLC Co. Nr. Company Name Agent For Company PYXIS REGULATORY CONSULTING, INC.

MAKHTESHIM-AGAN OF NORTH AMERICA INC 4110 136TH STREET, NW 9330 ZIONSVILLE RD 308/2E 630 FREEDOM BUSINESS CENTER, SUITE 402 3120 HIGHWOODS BLVD., SUITE 100 P.O. Box 2127 Address City ZIP GIG HARBOR INDIANAPOLIS KING OF PRUSSIA RALEIGH VALDOSTA 98332 462681054 19406 27604 316042127 OMB Approval 2070-0174

State WA IN PA NC GA DCI Number: GDCI-111601-1515

### United States Environmental Protection Agency Washington, D.C. 20460 LIST OF ALL REGISTRANTS SENT THIS DATA CALL-IN NOTICE 2490 - Oxyfluorfen Case # and Name: 1 Page: of 1

87283 62719 70506 11603 42750 WILLOWOOD OXYFLUORFEN, LLC

DOW AGROSCIENCES LLC UNITED PHOSPHORUS, INC ADAMA AGAN LTD. ALBAUGH, LLC Co. Nr. Company Name Agent For Company PYXIS REGULATORY CONSULTING, INC.

MAKHTESHIM-AGAN OF NORTH AMERICA INC 4110 136TH STREET, NW 9330 ZIONSVILLE RD 308/2E 630 FREEDOM BUSINESS CENTER, SUITE 402 3120 HIGHWOODS BLVD., SUITE 100 P.O. Box 2127 Address City ZIP GIG HARBOR INDIANAPOLIS KING OF PRUSSIA RALEIGH VALDOSTA 98332 462681054 19406 27604 316042127 OMB Approval 2070-0174

State WA IN PA NC GA DCI Number: GDCI-111601-1515

### United States Environmental Protection Agency Washington, D.C. 20460 LIST OF ALL REGISTRANTS SENT THIS DATA CALL-IN NOTICE 2490 - Oxyfluorfen Case # and Name: 1 Page: of 1

87283 62719 70506 11603 42750 WILLOWOOD OXYFLUORFEN, LLC

DOW AGROSCIENCES LLC UNITED PHOSPHORUS, INC ADAMA AGAN LTD. ALBAUGH, LLC Co. Nr. Company Name Agent For Company PYXIS REGULATORY CONSULTING, INC.

MAKHTESHIM-AGAN OF NORTH AMERICA INC 4110 136TH STREET, NW 9330 ZIONSVILLE RD 308/2E 630 FREEDOM BUSINESS CENTER, SUITE 402 3120 HIGHWOODS BLVD., SUITE 100 P.O. Box 2127 Address City ZIP GIG HARBOR INDIANAPOLIS KING OF PRUSSIA RALEIGH VALDOSTA 98332 462681054 19406 27604 316042127 OMB Approval 2070-0174

State WA IN PA NC GA DCI Number: GDCI-111601-1515