Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

-down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

-down boxes to fill in the units of

measure.Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

2324 Reid Gardner 1 bituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte

2324 Reid Gardner 1 As Received Higher Heating Value 2324 Reid Gardner 1 As Received % Moisture 2324 Reid Gardner 1 As Received % Ash 2324 Reid Gardner 1 As Received % Sulfur 2324 Reid Gardner 1 Dry basis Higher Heating Value 2324 Reid Gardner 1 Dry basis % Ash 2324 Reid Gardner 1 Dry basis % Sulfur 2324 Reid Gardner 1 Dry basis Antim ony 2324 Reid Gardner 1 Dry basis Arsenic 2324 Reid Gardner 1 Dry basis Beryllium 2324 Reid Gardner 1 Dry basis Cadmium 2324 Reid Gardner 1 Dry basis Chlorine 2324 Reid Gardner 1 Dry basis Chromium 2324 Reid Gardner 1 Dry basis Cobalt 2324 Reid Gardner 1 Dry basis Fluorine 2324 Reid Gardner 1 Dry basis Lead 2324 Reid Gardner 1 Dry basis Manganese 2324 Reid Gardner 1 Dry basis Mercury 2324 Reid Gardner 1 Dry basis Nickel 2324 Reid Gardner 1 Dry basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) ASTM D5865 ASTM D3302 ASTM D5142 ASTM D4239 Method B ASTM D5865 ASTM D5142 ASTM D4239 Method B ASTM D6357 ASTM D6357 ASTM D6357 ASTM D6357 ASTM D6721 ASTM D6357 ASTM D6357 ASTM D3761 ASTM D6357 ASTM D6357 ASTM D6722 ASTM D6357 SW-846 7740EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 2324 Reid Gardner 1 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 0745, 0845, 0945 5/5/2010 5/5/2010 12424.00 Btu/lb 1030, 1130, 1230 5/5/2010 5/5/2010 12288.00 Btu/lb 1330, 1430, 1510 5/5/2010 5/5/2010 12361.00 Btu/lb 0730, 0900, 1300 5/6/2010 5/6/2010 12009.00 Btu/lb 1000, 1130 1300 5/7/2010 5/7/2010 12216.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 8.05 8.38 1.02 13513 Btu/lb 9.11 1.11 8.67 8.72 1.05 13454 Btu/lb 9.55 1.15 8.46 8.36 0.99 13503 Btu/lb 9.13 1.08 8.83 9.46 1.01 13171 Btu/lb 10.38 1.1 7.49 9.33 1.2 13204 Btu/lb 10.08 1.3Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 380 ppm 0.04 μg/g [<1.0] μg/g [<1.0] μg/g 0.6 330 ppm 0.04 μg/g [<1.0] μg/g 1 μg/g 0.7 370 ppm 0.07 μg/g [<1.0] μg/g 5 μg/g 0.7 280 ppm 0.05 μg/g [<1.0] μg/g [<1.0] μg/g 0.6 240 ppm 0.07 μg/g [<1.0] μg/g [<1.0] μg/g 0.6Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units μg/g [<0.30] μg/g 9 μg/g 3 μg/g 12 μg/g μg/g [<0.30] μg/g 10 μg/g 3 μg/g 13 μg/g μg/g [<0.30] μg/g 10 μg/g 3 μg/g 12 μg/g μg/g [<0.30] μg/g 11 μg/g 3 μg/g 13 μg/g μg/g [<0.30] μg/g 13 μg/g 0 μg/g 14 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 6 μg/g 1 μg/g 96 ppm [<1.0] μg/g 8.05 7 μg/g 1 μg/g 100 ppm [<1.0] μg/g 8.67 6 μg/g 2 μg/g 110 ppm [<1.0] μg/g 8.46 7 μg/g 1 μg/g 130 ppm [<1.0] μg/g 8.83 7 μg/g 2 μg/g 110 ppm [<1.0] μg/g 7.49 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 39.68 9.11 51.21 74.68 5.03 1.54 1.11 39.73 9.55 50.72 74.16 5.03 1.51 1.15 39.82 9.13 51.05 74.9 5.06 1.54 1.08 39.9 10.38 49.72 71.56 4.93 1.43 1.1 40.2 10.08 49.72 72.99 5.02 1.46 1.3 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen

8.53 8.6 8.29 10.6 9.15EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 2324 Reid Gardner 1 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 0745, 0845, 0945 5/5/2010 5/5/2010 12424.00 Btu/lb 1030, 1130, 1230 5/5/2010 5/5/2010 12288.00 Btu/lb 1330, 1430, 1510 5/5/2010 5/5/2010 12361.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 8.05 8.38 1.02 13513 Btu/lb 9.11 1.11 8.67 8.72 1.05 13454 Btu/lb 9.55 1.15 8.46 8.36 0.99 13503 Btu/lb 9.13 1.08Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 380 ppm 0.04 μg/g [<1.0] μg/g [<1.0] μg/g 0.6 330 ppm 0.04 μg/g [<1.0] μg/g 1 μg/g 0.7 370 ppm 0.07 μg/g [<1.0] μg/g 5 μg/g 0.7Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units μg/g [<0.30] μg/g 9 μg/g 3 μg/g 12 μg/g μg/g [<0.30] μg/g 10 μg/g 3 μg/g 13 μg/g μg/g [<0.30] μg/g 10 μg/g 3 μg/g 12 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 6 μg/g 1 μg/g 96 ppm [<1.0] μg/g 7 μg/g 1 μg/g 100 ppm [<1.0] μg/g 6 μg/g 2 μg/g 110 ppm [<1.0] μg/gNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur

8.05 39.68 9.11 51.21 74.68 5.03 1.54 1.11 8.67 39.73 9.55 50.72 74.16 5.03 1.51 1.15 8.46 39.82 9.13 51.05 74.9 5.06 1.54 1.08 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 8.53 8.6 8.29EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 2324 Reid Gardner 1 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 0730, 0900, 1300 5/6/2010 5/6/2010 12009.00 Btu/lb 1000, 1130 1300 5/7/2010 5/7/2010 12216.00 Btu/lb 0800, 0930, 1100 5/8/2010 5/8/2010 12526.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 8.83 9.46 1.01 13171 Btu/lb 10.38 1.1 7.49 9.33 1.2 13204 Btu/lb 10.08 1.3 7.21 8.4 1.21 1.499 Btu/lb 9.05 1.3Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 280 ppm 0.05 μg/g [<1.0] μg/g [<1.0] μg/g 0.6 240 ppm 0.07 μg/g [<1.0] μg/g [<1.0] μg/g 0.6 410 ppm 0.07 μg/g [<1.0] μg/g 1 μg/g 0.6Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units μg/g [<0.30] μg/g 11 μg/g 3 μg/g 13 μg/g μg/g [<0.30] μg/g 13 μg/g 0 μg/g 14 μg/g μg/g [<0.30] μg/g 10 μg/g 3 μg/g 11 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 7 μg/g 1 μg/g 130 ppm [<1.0] μg/g 8.83 7 μg/g 2 μg/g 110 ppm [<1.0] μg/g 7.49 7 μg/g 1 μg/g 120 ppm [<1.0] μg/g 7.21 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 39.9 10.38 49.72 71.56 4.93 1.43 1.1 10.6 40.2 10.08 49.72 72.99 5.02 1.46 1.3 9.15 40.51 9.05 50.44 74.49 5.11 1.55 1.3 8.5 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 2324 Reid Gardner 1

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm