### Instructions for filling Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

-04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected more. 7. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being Fields that are highlighted in down boxes, included. Gray fields are

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Test Date

1642 West Springfield 3 3/29/2010Fuel Type 1 Fuel Type 2 Fuel Type 3

No.6 Fuel Oil (residual or bunker C)Other Fuel DescriptionEIA Facility Code Facility Name Boiler ID Basis An alyte An alysis M ethod for each Analyte (example: ASTM D5865-04) 1642 West Springfield 3 As Received Higher Heating Value ASTM D-282 1642 West Springfield 3 As Received % Moisture ASTM D-6304 1642 West Springfield 3 As Received % Ash ASTM D-482 1642 West Springfield 3 As Received % Sulfur ASTM D-1552 1642 West Springfield 3 Dry basis Higher Heating Value ASTM D-282 1642 West Springfield 3 Dry basis % Moisture ASTM D-6304 1642 West Springfield 3 Dry basis % Ash ASTM D-482 1642 West Springfield 3 Dry basis % Sulfur ASTM D-1552 1642 West Springfield 3 Dry basis Antim ony EPA 200.9 1642 West Springfield 3 Dry basis Arsenic SW 846-7060 1642 West Springfield 3 Dry basis Beryllium SW 846-6010B 1642 West Springfield 3 Dry basis Cadmium SW 846-6010B 1642 West Springfield 3 Dry basis Chlorine SW 846-9076 1642 West Springfield 3 Dry basis Chromium SW 846-6010B 1642 West Springfield 3 Dry basis Cobalt SW 846-6010B 1642 West Springfield 3 Dry basis Fluorine SW 846-9076 1642 West Springfield 3 Dry basis Lead SW 846-6010B 1642 West Springfield 3 Dry basis Manganese SW 846-6010B 1642 West Springfield 3 Dry basis Mercury SW 846-7470 1642 West Springfield 3 Dry basis Nickel SW 846-6010B 1642 West Springfield 3 Dry basis Selenium SW 846-6010BSample Number

(minimum of 3 composite samples) Sample Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) % A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) 1 3/29/2010 151530.00 Btu/gallon 0.2 0.07 0.86 151530.00 2 3/31/2010 150720.00 Btu/gallon 0.23 0.05 0.84 150720.00 3 3/30/2010 150340.00 Btu/gallon 0.26 0.07 0.84 150340.00 Fuel Testing ResultsHHV Units % Moisture (Dry Basis) % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Arsenic (Dry

Basis) Arsenic Units Beryllium (Dry Basis) Btu/gallon 0.2 0.07 0.2 124 ppm <0.02 mg/Kg <0.60 ppm <1.00 Btu/gallon 0.23 0.05 0.23 237 ppm <0.02 mg/Kg <0.50 ppm <1.00 Btu/gallon 0.26 0.07 0.26 153 ppm <0.02 mg/Kg <0.50 ppm <1.00Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) ppm <1.00 ppm <1.00 ppm <1.00 ppm 2.5 ppm 26.6 ppm 0.88 ppm <1.00 ppm <1.00 ppm <1.00 ppm <1.00 ppm 27.5 ppm <0.50 ppm <1.00 ppm <1.00 ppm <1.00 ppm <1.00 ppm 26.8 ppm <0.50Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units ppm <0.10 ppm 1.65 ppm ppm <0.10 ppm <1.11 ppm ppm <0.10 ppm 1.14 ppmUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/Kg ppmUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm