Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### EIA

Facility Code Facility Name Boiler ID Fuel Type 1

3131 Shawville Common Stack 

## bituminous

### Fuel Type 2 Fuel Type 3 Other Fuel Description

### EIA

Facility Code Facility Name Boiler ID Basis An alyte



## 3131 Shawville Common Stack As Received Higher Heating Value 

## 3131 Shawville Common Stack As Received % Moisture 

## 3131 Shawville Common Stack As Received % Ash 

## 3131 Shawville Common Stack As Received % Sulfur 

## 3131 Shawville Common Stack Dry basis Higher Heating Value 

## 3131 Shawville Common Stack Dry basis % Ash 

## 3131 Shawville Common Stack Dry basis % Sulfur 

## 3131 Shawville Common Stack Dry basis Antim ony 

## 3131 Shawville Common Stack Dry basis Arsenic 

## 3131 Shawville Common Stack Dry basis Bery llium 

## 3131 Shawville Common Stack Dry basis Cadmium 

## 3131 Shawville Common Stack Dry basis Chlorine 

## 3131 Shawville Common Stack Dry basis Chromium 

## 3131 Shawville Common Stack Dry basis Cobalt 

## 3131 Shawville Common Stack Dry basis Fluorine 

## 3131 Shawville Common Stack Dry basis Lead 

## 3131 Shawville Common Stack Dry basis Manganese 

## 3131 Shawville Common Stack Dry basis Mercury 

## 3131 Shawville Common Stack Dry basis Nickel 

## 3131 Shawville Common Stack Dry basis Selenium

### An alysis M ethod for each A nalyte

(example: ASTM D5865-04) 

## ASTM D5865 ASTM D3172 ASTM D3172 ASTM D4239-02 ASTM D5865 ASTM D3172 ASTM D4239-02 ASTM D-6357 ASTM D-6357 ASTM D-6357 ASTM D-6357 ASTM D4208-02 ASTM D-6357 ASTM D-6357 ASTM D3761-02 ASTM D-6357 ASTM D-6357 ASTM D-6722 ASTM D-6357 ASTM D-4606 / D-6357EIA

Facility Code Facility

Name Boiler ID 

### HA Ps Test Group 

## 3131 Shawville Common Stack Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### 1 

## 6/2/2010 6/2/2010 11941.00 Btu/lb 2 6/2/2010 6/2/2010 12045.00 Btu/lb 3 6/2/2010 6/2/2010 12082.00 Btu/lb Fuel Testing Results

## 12099.58

% Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

## 7.35 13.34 1.98 12888 Btu/lb 14.4 2.13 7.07 13.27 2.04 12961 Btu/lb 14.28 2.19 6.74 13.22 2.14 12955 Btu/lb 14.17 2.3Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis) 

## 720 ppm 754 ppm 715 ppmBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

## 41 ppm 7.35 37 ppm 7.07 35 ppm 6.74 Proximate Analy

ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 

## 27.68 14.4 57.92 72.58 4.36 1.52 2.13 27.21 14.28 58.51 72.75 4.33 1.46 2.19 27.65 14.17 58.18 72.68 4.36 1.49 2.3 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen



## 5.01 4.99 5EIA

Facility Code Facility

Name Boiler ID 

### HA Ps Test Group 

## 3131 Shawville Common Stack Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 

### 1 

## 6/8/2010 6/8/2010 12206.00 Btu/lb 2 6/8/2010 6/8/2010 12155.00 Btu/lb 3 6/8/2010 6/8/2010 12341.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

## 6.99 12.54 1.87 13123 Btu/lb 13.48 2.01 5.9 13.79 2.02 12917 Btu/lb 14.65 2.15 5.99 12.64 1.93 13127 Btu/lb 13.45 2.05Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis) 

## 798 ppm 670 ppm 743 ppmBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur



## 6.99 27.32 13.48 59.2 73.7 4.39 1.43 2.01 5.9 27.38 14.65 57.97 72.72 4.37 1.41 2.15 5.99 27.94 13.45 58.61 73.79 4.48 1.46 2.05 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 

## 4.99 4.7 4.77EIA

Facility Code Facility

Name Boiler ID 

### HA Ps Test Group 

## 3131 Shawville Common Stack Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### 1 

## 6/3/2010 6/3/2010 12006.00 Btu/lb 2 6/3/2010 6/3/2010 11949.00 Btu/lb 3 6/4/2010 6/4/2010 11955.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

## 6.29 14.09 1.8 12812 Btu/lb 15.04 1.92 6.78 14.18 1.89 12818 Btu/lb 15.21 2.03 6.98 13.75 2.08 12852 Btu/lb 14.78 2.24Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis) 

## 719 ppm 0.431 mg/Kg 1.75 mg/Kg 30.4 mg/Kg 2.06 728 ppm 0.48 mg/Kg 1.78 mg/Kg 38.7 mg/Kg 2.05 765 ppm 0.52 mg/Kg 1.82 mg/Kg 40.5 mg/Kg 2.01Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

## mg/Kg 0.15 mg/Kg 23.6 mg/Kg 11.1 mg/Kg 39 mg/Kg mg/Kg 0.17 mg/Kg 23.3 mg/Kg 11.6 mg/Kg 37.6 mg/Kg mg/Kg 0.2 mg/Kg 22.6 mg/Kg 12.1 mg/Kg 45.9 mg/KgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

## 17.5 mg/Kg 4.19 mg/Kg 47 ppm 8.24 mg/Kg 6.29 17.5 mg/Kg 4.62 mg/Kg 50 ppm 8.38 mg/Kg 6.78 18.4 mg/Kg 5.15 mg/Kg 45 ppm 8.5 mg/Kg 6.98 Proximate Analy

ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

## 27.61 15.04 57.35 71.91 4.32 1.46 1.92 5.35 26.98 15.21 57.81 72.24 4.3 1.44 2.03 4.78 27.79 14.78 57.43 72.07 4.42 1.48 2.24 5.01 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID 

### HA Ps Test Group 

## 3131 Shawville Common Stack Dioxin/furan HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### 1 

## 6/7/2010 6/7/2010 12443.00 Btu/lb 2 6/9/2010 6/9/2010 11832.00 Btu/lb 3 6/9/2010 6/9/2010 12240.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

## 5.33 12.65 2.02 13143 Btu/lb 13.36 2.14 6.1 15.46 2.14 12601 Btu/lb 16.47 2.28 5.61 13.61 2.28 12968 Btu/lb 14.42 2.41Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis) 

## 732 709 714Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

## 5.33 6.1 5.61 Proximate Analy ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

## 27.96 13.36 58.68 73.52 4.43 1.47 2.14 5.08 25.96 16.47 57.57 71.13 4.23 1.41 2.28 4.48 27.24 14.42 58.34 72.79 4.38 1.46 2.41 4.54 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wt

### Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals sy nfuel mg /g petroleum coke μg/g other mg /Kg

### Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm