Dolan Chemical Laboratory 4001 Bixby Road Groveport, OH 43125 T: 614-836-4221, Audinet 210-4221 F: 614-836-4168, Audinet 210-4168 http://aepenv/labs 

### Water Analysis Form REP-703 Rev. 0, 4/2012



### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134633-001Date Collected:11/14/2013Date Received:11/15/2013 

### CPS Influent

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 49.0 0.05DPC EPA 200.8 0.01 11/20/2013 12:15 ug/L Arsenic, As 260 0.1 DPC EPA 200.8 0.03 11/20/2013 12:15 ug/L Barium, Ba 2240 0.1 DPC EPA 200.8 0.02 11/20/2013 12:15 ug/L Beryllium, Be 10 20 DAM EPA 200.7 5 11/20/2013 12:16 J ug/L Cadmium, Cd 248 0.05DPC EPA 200.8 0.01 11/20/2013 12:15 ug/L Chromium, Cr 1750 0.2 DPC EPA 200.8 0.04 11/20/2013 12:15 ug/L Cobalt, Co 293 0.02 DPC EPA 200.8 0.004 11/20/2013 12:15 ug/L Copper, Cu 719 0.05DPC EPA 200.8 0.01 11/20/2013 12:15 ug/L Lead, Pb 366 0.01 DPC EPA 200.8 0.002 11/20/2013 12:15 ng/L Mercury, Hg 165000 5000TLT EPA 1631E 2000 11/26/2013 ug/L Molybdenum, Mo 705 0.05DPC EPA 200.8 0.01 11/20/2013 12:15 ug/L Nickel, Ni 2720 0.2 DPC EPA 200.8 0.05 11/20/2013 12:15 ug/L Selenium, Se 1480 0.5 DPC EPA 200.8 0.2 11/20/2013 12:15 ug/L Silver, Ag 0.998 0.01 DPC EPA 200.8 0.002 11/20/2013 12:15 ug/L Thallium, Tl 17.9 0.05DPC EPA 200.8 0.002 11/20/2013 12:15 ug/L Tin, Sn < 100 500 DAM EPA 200.7 100 11/20/2013 12:17 U ug/L Titanium, Ti 851 100 DAM EPA 200.7 20 11/20/2013 12:17 ug/L Zinc, Zn 5910 0.5 DPC EPA 200.8 0.1 11/20/2013 12:15 mg/L Aluminum, Al 161 0.001DPC EPA 200.8 0.0003 11/20/2013 12:15 mg/L Boron, B 335 1 DAM EPA 200.7 0.2 11/20/2013 12:16 mg/L Calcium, Ca 5020 1 DAM EPA 200.7 0.2 11/20/2013 12:16 mg/L Iron, Fe 332 2 DAM EPA 200.7 0.5 11/20/2013 12:16 mg/L Magnesium, Mg 3690 0.5 DAM EPA 200.7 0.1 11/20/2013 12:16 mg/L Manganese, Mn 53.6 0.02DAM EPA 200.7 0.005 11/20/2013 12:16 mg/L Potassium, K 99.0 2 DAM EPA 200.7 0.4 11/20/2013 12:15 mg/L Sodium, Na 319 2 DAM EPA 200.7 0.4 11/20/2013 12:15 mg/L Strontium, Sr 47.1 0.05DAM EPA 200.7 0.02 11/20/2013 12:15 mg/L Ammonia, NH3, as N 0.79 0.05DMM EPA 350.1 0.02 11/19/2013 mg/L Total Kjeldahl Nitrogen, TKN as N10.0 5 DMM EPA 351.2 1 10/29/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N45.8 0.1 DMM SM20 4500NO3 H 0.02 11/19/2013

Mountaineer Plant, 134633 Page 1 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134633-001ADate Collected:11/14/2013Date Received:11/15/2013 

### CPS Influent Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 3.61 0.05DPC EPA 200.8 0.01 11/20/2013 12:20 ug/L Arsenic, As 2.89 0.1 DPC EPA 200.8 0.03 11/20/2013 12:20 ug/L Barium, Ba 83.2 0.1 DPC EPA 200.8 0.02 11/20/2013 12:20 ug/L Beryllium, Be 7 20 DAM EPA 200.7 5 11/20/2013 12:21 J ug/L Cadmium, Cd 162 0.05DPC EPA 200.8 0.01 11/20/2013 12:20 ug/L Chromium, Cr 3.5 0.2 DPC EPA 200.8 0.04 11/20/2013 12:20 ug/L Cobalt, Co 91.6 0.02DPC EPA 200.8 0.004 11/20/2013 12:20 ug/L Copper, Cu 7.70 0.05DPC EPA 200.8 0.01 11/20/2013 12:20 ug/L Lead, Pb 0.116 0.01 DPC EPA 200.8 0.002 11/20/2013 12:20 ng/L Mercury, Hg 697 500 TLT EPA 1631E 200 11/26/2013 ug/L Molybdenum, Mo 267 0.05DPC EPA 200.8 0.01 11/20/2013 12:20 ug/L Nickel, Ni 1520 0.2 DPC EPA 200.8 0.05 11/20/2013 12:20 ug/L Selenium, Se 797 0.5 DPC EPA 200.8 0.2 11/20/2013 12:20 ug/L Selenite, Se+4 (Hydride) 221 20 TLT AEP Method 4 12/04/2013 AEP Method for Se speciation is not accredited through any agency. Results are for internal use only. ug/L Silver, Ag 0.005 0.01 DPC EPA 200.8 0.002 11/20/2013 12:20 J ug/L Thallium, Tl 8.13 0.05DPC EPA 200.8 0.002 11/20/2013 12:20 ug/L Tin, Sn < 100 500 DAM EPA 200.7 100 11/20/2013 12:21 U ug/L Titanium, Ti < 20 100 DAM EPA 200.7 20 11/20/2013 12:21 U ug/L Zinc, Zn 1060 0.5 DPC EPA 200.8 0.1 11/20/2013 12:20 mg/L Aluminum, Al 0.120 0.001DPC EPA 200.8 0.0003 11/20/2013 12:20 mg/L Boron, B 333 1 DAM EPA 200.7 0.2 11/20/2013 12:21 mg/L Calcium, Ca 700 1 DAM EPA 200.7 0.2 11/20/2013 12:21 mg/L Iron, Fe < 0.5 2 DAM EPA 200.7 0.5 11/20/2013 12:21 U mg/L Magnesium, Mg 3320 0.5 DAM EPA 200.7 0.1 11/20/2013 12:21 mg/L Manganese, Mn 38.5 0.02DAM EPA 200.7 0.005 11/20/2013 12:21 mg/L Potassium, K 57.0 2 DAM EPA 200.7 0.4 11/20/2013 12:20 mg/L Sodium, Na 318 2 DAM EPA 200.7 0.4 11/20/2013 12:20 mg/L Strontium, Sr 9.02 0.05DAM EPA 200.7 0.02 11/20/2013 12:20

Mountaineer Plant, 134633 Page 2 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134633-002Date Collected:11/14/2013Date Received:11/15/2013 

### Primary Clarifier Effluent

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 3.41 0.05DPC EPA 200.8 0.01 11/20/2013 12:26 ug/L Arsenic, As 3.39 0.1 DPC EPA 200.8 0.03 11/20/2013 12:26 ug/L Barium, Ba 64.7 0.1 DPC EPA 200.8 0.02 11/20/2013 12:26 ug/L Beryllium, Be 2 5 DAM EPA 200.7 1 11/20/2013 12:26 J ug/L Cadmium, Cd 79.4 0.05DPC EPA 200.8 0.01 11/20/2013 12:26 ug/L Chromium, Cr 10.4 0.2 DPC EPA 200.8 0.04 11/20/2013 12:26 ug/L Cobalt, Co 27.1 0.02DPC EPA 200.8 0.004 11/20/2013 12:26 ug/L Copper, Cu 5.22 0.05DPC EPA 200.8 0.01 11/20/2013 12:26 ug/L Lead, Pb 0.773 0.01 DPC EPA 200.8 0.002 11/20/2013 12:26 ng/L Mercury, Hg 2650 50 TLT EPA 1631E 20 11/26/2013 ug/L Molybdenum, Mo 372 0.05DPC EPA 200.8 0.01 11/20/2013 12:26 ug/L Nickel, Ni 894 0.2 DPC EPA 200.8 0.05 11/20/2013 12:26 ug/L Selenium, Se 619 0.5 DPC EPA 200.8 0.2 11/20/2013 12:26 ug/L Silver, Ag 0.062 0.01 DPC EPA 200.8 0.002 11/20/2013 12:26 ug/L Thallium, Tl 7.76 0.05DPC EPA 200.8 0.002 11/20/2013 12:26 ug/L Tin, Sn < 20 100 DAM EPA 200.7 20 11/20/2013 12:26 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 11/20/2013 12:26 U ug/L Zinc, Zn 83.2 0.5 DPC EPA 200.8 0.1 11/20/2013 12:26 mg/L Aluminum, Al 0.195 0.001DPC EPA 200.8 0.0003 11/20/2013 12:26 mg/L Boron, B 275 0.2 DAM EPA 200.7 0.04 11/20/2013 12:25 mg/L Calcium, Ca 689 0.2 DAM EPA 200.7 0.04 11/20/2013 12:25 mg/L Iron, Fe 0.520 0.5 DAM EPA 200.7 0.1 11/20/2013 12:26 mg/L Magnesium, Mg 2710 0.1 DAM EPA 200.7 0.02 11/20/2013 12:25 mg/L Manganese, Mn 23.1 0.005DAM EPA 200.7 0.001 11/20/2013 12:25 mg/L Potassium, K 48.4 0.5 DAM EPA 200.7 0.07 11/20/2013 12:24 mg/L Sodium, Na 272 0.3 DAM EPA 200.7 0.08 11/20/2013 12:24 mg/L Strontium, Sr 7.95 0.01 DAM EPA 200.7 0.003 11/20/2013 12:24 mg/L Ammonia, NH3, as N 2.12 0.05DMM EPA 350.1 0.02 11/19/2013 mg/L Total Kjeldahl Nitrogen, TKN as N4.08 0.5 DMM EPA 351.2 0.1 10/29/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N31.8 0.1 DMM SM20 4500NO3 H 0.02 11/19/2013

Mountaineer Plant, 134633 Page 3 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134633-002ADate Collected:11/14/2013Date Received:11/15/2013 

### Primary Clarifier Effluent Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 2.91 0.05DPC EPA 200.8 0.01 11/20/2013 12:31 ug/L Arsenic, As 2.57 0.1 DPC EPA 200.8 0.03 11/20/2013 12:31 ug/L Barium, Ba 54.2 0.1 DPC EPA 200.8 0.02 11/20/2013 12:31 ug/L Beryllium, Be < 1 5 DAM EPA 200.7 1 11/20/2013 14:02 U ug/L Cadmium, Cd 69.4 0.05DPC EPA 200.8 0.01 11/20/2013 12:31 ug/L Chromium, Cr 6.6 0.2 DPC EPA 200.8 0.04 11/20/2013 12:31 ug/L Cobalt, Co 23.4 0.02DPC EPA 200.8 0.004 11/20/2013 12:31 ug/L Copper, Cu 3.24 0.05DPC EPA 200.8 0.01 11/20/2013 12:31 ug/L Lead, Pb 0.024 0.01 DPC EPA 200.8 0.002 11/20/2013 12:31 ng/L Mercury, Hg 926 50 TLT EPA 1631E 20 11/26/2013 ug/L Molybdenum, Mo 322 0.05DPC EPA 200.8 0.01 11/20/2013 12:31 ug/L Nickel, Ni 782 0.2 DPC EPA 200.8 0.05 11/20/2013 12:31 ug/L Selenium, Se 537 0.5 DPC EPA 200.8 0.2 11/20/2013 12:31 ug/L Selenite, Se+4 (Hydride) 205 20 TLT AEP Method 4 12/04/2013 AEP Method for Se speciation is not accredited through any agency. Results are for internal use only. ug/L Silver, Ag 0.004 0.01 DPC EPA 200.8 0.002 11/20/2013 12:31 J ug/L Thallium, Tl 6.66 0.05DPC EPA 200.8 0.002 11/20/2013 12:31 ug/L Tin, Sn < 20 100 DAM EPA 200.7 20 11/20/2013 14:02 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 11/20/2013 14:02 U ug/L Zinc, Zn 65.8 0.5 DPC EPA 200.8 0.1 11/20/2013 12:31 mg/L Aluminum, Al 0.0261 0.001DPC EPA 200.8 0.0003 11/20/2013 12:31 mg/L Boron, B 277 0.2 DAM EPA 200.7 0.04 11/20/2013 14:02 mg/L Calcium, Ca 694 0.2 DAM EPA 200.7 0.04 11/20/2013 14:02 mg/L Iron, Fe < 0.1 0.5 DAM EPA 200.7 0.1 11/20/2013 14:02 U mg/L Magnesium, Mg 2710 0.1 DAM EPA 200.7 0.02 11/20/2013 14:02 mg/L Manganese, Mn 23.2 0.005DAM EPA 200.7 0.001 11/20/2013 14:02 mg/L Potassium, K 47.5 0.5 DAM EPA 200.7 0.07 11/20/2013 14:00 mg/L Sodium, Na 268 0.3 DAM EPA 200.7 0.08 11/20/2013 14:00 mg/L Strontium, Sr 7.91 0.01 DAM EPA 200.7 0.003 11/20/2013 14:00

Mountaineer Plant, 134633 Page 4 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134633-003Date Collected:11/14/2013Date Received:11/15/2013 

### CPS Effluent

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 2.65 0.05DPC EPA 200.8 0.01 11/20/2013 12:36 ug/L Arsenic, As 2.65 0.1 DPC EPA 200.8 0.03 11/20/2013 12:36 ug/L Barium, Ba 64.6 0.1 DPC EPA 200.8 0.02 11/20/2013 12:36 ug/L Beryllium, Be < 1 5 DAM EPA 200.7 1 11/20/2013 14:11 U ug/L Cadmium, Cd 25.9 0.05DPC EPA 200.8 0.01 11/20/2013 12:36 ug/L Chromium, Cr 7.8 0.2 DPC EPA 200.8 0.04 11/20/2013 12:36 ug/L Cobalt, Co 16.0 0.02DPC EPA 200.8 0.004 11/20/2013 12:36 ug/L Copper, Cu 1.92 0.05DPC EPA 200.8 0.01 11/20/2013 12:36 ug/L Lead, Pb 0.363 0.01 DPC EPA 200.8 0.002 11/20/2013 12:36 ng/L Mercury, Hg 1600 20 TLT EPA 1631E 8 11/26/2013 ug/L Molybdenum, Mo 324 0.05DPC EPA 200.8 0.01 11/20/2013 12:36 ug/L Nickel, Ni 654 0.2 DPC EPA 200.8 0.05 11/20/2013 12:36 ug/L Selenium, Se 491 0.5 DPC EPA 200.8 0.2 11/20/2013 12:36 ug/L Silver, Ag 0.012 0.01 DPC EPA 200.8 0.002 11/20/2013 12:36 ug/L Thallium, Tl 4.92 0.05DPC EPA 200.8 0.002 11/20/2013 12:36 ug/L Tin, Sn < 20 100 DAM EPA 200.7 20 11/20/2013 14:11 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 11/20/2013 14:11 U ug/L Zinc, Zn 54.5 0.5 DPC EPA 200.8 0.1 11/20/2013 12:36 mg/L Aluminum, Al 0.115 0.001DPC EPA 200.8 0.0003 11/20/2013 12:36 mg/L Boron, B 226 0.2 DAM EPA 200.7 0.04 11/20/2013 14:11 mg/L Calcium, Ca 580 0.2 DAM EPA 200.7 0.04 11/20/2013 14:11 mg/L Iron, Fe 0.2 0.5 DAM EPA 200.7 0.1 11/20/2013 14:11 J mg/L Magnesium, Mg 2190 0.1 DAM EPA 200.7 0.02 11/20/2013 14:11 mg/L Manganese, Mn 18.8 0.005DAM EPA 200.7 0.001 11/20/2013 14:11 mg/L Potassium, K 40.4 0.5 DAM EPA 200.7 0.07 11/20/2013 14:10 mg/L Sodium, Na 227 0.3 DAM EPA 200.7 0.08 11/20/2013 14:10 mg/L Strontium, Sr 6.57 0.01 DAM EPA 200.7 0.003 11/20/2013 14:10 mg/L Ammonia, NH3, as N 1.86 0.05DMM EPA 350.1 0.02 11/19/2013 mg/L Total Kjeldahl Nitrogen, TKN as N3.68 0.5 DMM EPA 351.2 0.1 10/29/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N25.4 0.1 DMM SM20 4500NO3 H 0.02 11/19/2013

Mountaineer Plant, 134633 Page 5 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134633-003ADate Collected:11/14/2013Date Received:11/15/2013 

### CPS Effluent Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 2.29 0.05DPC EPA 200.8 0.01 11/20/2013 12:41 ug/L Arsenic, As 2.13 0.1 DPC EPA 200.8 0.03 11/20/2013 12:41 ug/L Barium, Ba 56.1 0.1 DPC EPA 200.8 0.02 11/20/2013 12:41 ug/L Beryllium, Be < 1 5 DAM EPA 200.7 1 11/20/2013 14:21 U ug/L Cadmium, Cd 13.8 0.05DPC EPA 200.8 0.01 11/20/2013 12:41 ug/L Chromium, Cr 5.7 0.2 DPC EPA 200.8 0.04 11/20/2013 12:41 ug/L Cobalt, Co 12.2 0.02DPC EPA 200.8 0.004 11/20/2013 12:41 ug/L Copper, Cu 0.63 0.05DPC EPA 200.8 0.01 11/20/2013 12:41 ug/L Lead, Pb 0.019 0.01 DPC EPA 200.8 0.002 11/20/2013 12:41 ng/L Mercury, Hg 50.0 2 TLT EPA 1631E 0.8 11/26/2013 ug/L Molybdenum, Mo 285 0.05DPC EPA 200.8 0.01 11/20/2013 12:41 ug/L Nickel, Ni 561 0.2 DPC EPA 200.8 0.05 11/20/2013 12:41 ug/L Selenium, Se 434 0.5 DPC EPA 200.8 0.2 11/20/2013 12:41 ug/L Selenite, Se+4 (Hydride) 161 20 TLT AEP Method 4 12/04/2013 AEP Method for Se speciation is not accredited through any agency. Results are for internal use only. ug/L Silver, Ag 0.004 0.01 DPC EPA 200.8 0.002 11/20/2013 12:41 J ug/L Thallium, Tl 4.14 0.05DPC EPA 200.8 0.002 11/20/2013 12:41 ug/L Tin, Sn < 20 100 DAM EPA 200.7 20 11/20/2013 14:21 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 11/20/2013 14:21 U ug/L Zinc, Zn 45.5 0.5 DPC EPA 200.8 0.1 11/20/2013 12:41 mg/L Aluminum, Al 0.0289 0.001DPC EPA 200.8 0.0003 11/20/2013 12:41 mg/L Boron, B 212 0.2 DAM EPA 200.7 0.04 11/20/2013 14:21 mg/L Calcium, Ca 541 0.2 DAM EPA 200.7 0.04 11/20/2013 14:21 mg/L Iron, Fe < 0.1 0.5 DAM EPA 200.7 0.1 11/20/2013 14:21 U mg/L Magnesium, Mg 2050 0.1 DAM EPA 200.7 0.02 11/20/2013 14:21 mg/L Manganese, Mn 17.5 0.005DAM EPA 200.7 0.001 11/20/2013 14:21 mg/L Potassium, K 36.6 0.5 DAM EPA 200.7 0.07 11/20/2013 14:19 mg/L Sodium, Na 210 0.3 DAM EPA 200.7 0.08 11/20/2013 14:19 mg/L Strontium, Sr 6.11 0.01 DAM EPA 200.7 0.003 11/20/2013 14:19

Mountaineer Plant, 134633 Page 6 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134633-004Date Collected:11/14/2013Date Received:11/15/2013 

### Landfill Leachate

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 11.1 0.05DPC EPA 200.8 0.01 11/20/2013 12:46 ug/L Arsenic, As 34.0 0.1 DPC EPA 200.8 0.03 11/20/2013 12:46 ug/L Barium, Ba 35.2 0.1 DPC EPA 200.8 0.02 11/20/2013 12:46 ug/L Beryllium, Be < 1 5 DAM EPA 200.7 1 11/20/2013 14:35 U ug/L Cadmium, Cd 41.8 0.05DPC EPA 200.8 0.01 11/20/2013 12:46 ug/L Chromium, Cr 1.1 0.2 DPC EPA 200.8 0.04 11/20/2013 12:46 ug/L Cobalt, Co 51.5 0.02DPC EPA 200.8 0.004 11/20/2013 12:46 ug/L Copper, Cu 1.84 0.05DPC EPA 200.8 0.01 11/20/2013 12:46 ug/L Lead, Pb 0.088 0.01 DPC EPA 200.8 0.002 11/20/2013 12:46 ng/L Mercury, Hg 134 10 TLT EPA 1631E 4 11/26/2013 ug/L Molybdenum, Mo 6390 0.05DPC EPA 200.8 0.01 11/20/2013 12:46 ug/L Nickel, Ni 422 0.2 DPC EPA 200.8 0.05 11/20/2013 12:46 ug/L Selenium, Se 398 0.5 DPC EPA 200.8 0.2 11/20/2013 12:46 ug/L Silver, Ag 0.002 0.01 DPC EPA 200.8 0.002 11/20/2013 12:46 J ug/L Thallium, Tl 5.62 0.05DPC EPA 200.8 0.002 11/20/2013 12:46 ug/L Tin, Sn < 20 100 DAM EPA 200.7 20 11/20/2013 14:35 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 11/20/2013 14:35 U ug/L Zinc, Zn 117 0.5 DPC EPA 200.8 0.1 11/20/2013 12:46 mg/L Aluminum, Al 0.112 0.001DPC EPA 200.8 0.0003 11/20/2013 12:46 mg/L Boron, B 176 0.2 DAM EPA 200.7 0.04 11/20/2013 14:35 mg/L Calcium, Ca 515 0.2 DAM EPA 200.7 0.04 11/20/2013 14:35 mg/L Iron, Fe < 0.1 0.5 DAM EPA 200.7 0.1 11/20/2013 14:35 U mg/L Magnesium, Mg 1450 0.1 DAM EPA 200.7 0.02 11/20/2013 14:35 mg/L Manganese, Mn 19.9 0.005DAM EPA 200.7 0.001 11/20/2013 14:35 mg/L Potassium, K 121 0.5 DAM EPA 200.7 0.07 11/20/2013 14:33 mg/L Sodium, Na 1760 0.3 DAM EPA 200.7 0.08 11/20/2013 14:33 mg/L Strontium, Sr 7.02 0.01 DAM EPA 200.7 0.003 11/20/2013 14:33 mg/L Ammonia, NH3, as N 1.52 0.05DMM EPA 350.1 0.02 11/19/2013 mg/L Total Kjeldahl Nitrogen, TKN as N3.68 0.5 DMM EPA 351.2 0.1 10/29/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N16.3 0.1 DMM SM20 4500NO3 H 0.02 11/19/2013

Mountaineer Plant, 134633 Page 7 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134633-004ADate Collected:11/14/2013Date Received:11/15/2013 

### Landfill Leachate Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 10.3 0.05DPC EPA 200.8 0.01 11/20/2013 12:51 ug/L Arsenic, As 28.7 0.1 DPC EPA 200.8 0.03 11/20/2013 12:51 ug/L Barium, Ba 30.7 0.1 DPC EPA 200.8 0.02 11/20/2013 12:51 ug/L Beryllium, Be < 1 5 DAM EPA 200.7 1 11/20/2013 14:39 U ug/L Cadmium, Cd 38.1 0.05DPC EPA 200.8 0.01 11/20/2013 12:51 ug/L Chromium, Cr 0.7 0.2 DPC EPA 200.8 0.04 11/20/2013 12:51 ug/L Cobalt, Co 45.8 0.02DPC EPA 200.8 0.004 11/20/2013 12:51 ug/L Copper, Cu 1.37 0.05DPC EPA 200.8 0.01 11/20/2013 12:51 ug/L Lead, Pb 0.011 0.01 DPC EPA 200.8 0.002 11/20/2013 12:51 ng/L Mercury, Hg 53.7 2 TLT EPA 1631E 0.8 11/26/2013 ug/L Molybdenum, Mo 5860 0.05DPC EPA 200.8 0.01 11/20/2013 12:51 ug/L Nickel, Ni 382 0.2 DPC EPA 200.8 0.05 11/20/2013 12:51 ug/L Selenium, Se 361 0.5 DPC EPA 200.8 0.2 11/20/2013 12:51 ug/L Selenite, Se+4 (Hydride) 285 20 TLT AEP Method 4 12/04/2013 AEP Method for Se speciation is not accredited through any agency. Results are for internal use only. ug/L Silver, Ag < 0.002 0.01 DPC EPA 200.8 0.002 11/20/2013 12:51 U ug/L Thallium, Tl 5.02 0.05DPC EPA 200.8 0.002 11/20/2013 12:51 ug/L Tin, Sn < 20 100 DAM EPA 200.7 20 11/20/2013 14:40 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 11/20/2013 14:39 U ug/L Zinc, Zn 97.2 0.5 DPC EPA 200.8 0.1 11/20/2013 12:51 mg/L Aluminum, Al 0.0318 0.001DPC EPA 200.8 0.0003 11/20/2013 12:51 mg/L Boron, B 173 0.2 DAM EPA 200.7 0.04 11/20/2013 14:39 mg/L Calcium, Ca 504 0.2 DAM EPA 200.7 0.04 11/20/2013 14:39 mg/L Iron, Fe < 0.1 0.5 DAM EPA 200.7 0.1 11/20/2013 14:40 U mg/L Magnesium, Mg 1430 0.1 DAM EPA 200.7 0.02 11/20/2013 14:39 mg/L Manganese, Mn 19.2 0.005DAM EPA 200.7 0.001 11/20/2013 14:39 mg/L Potassium, K 119 0.5 DAM EPA 200.7 0.07 11/20/2013 14:38 mg/L Sodium, Na 1750 0.3 DAM EPA 200.7 0.08 11/20/2013 14:38 mg/L Strontium, Sr 6.97 0.01 DAM EPA 200.7 0.003 11/20/2013 14:38

Mountaineer Plant, 134633 Page 8 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134633-005Date Collected:11/14/2013Date Received:11/15/2013 

### 1st Stage Feed

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 6.67 0.05DPC EPA 200.8 0.01 11/20/2013 13:52 ug/L Arsenic, As 17.4 0.1 DPC EPA 200.8 0.03 11/20/2013 13:52 ug/L Barium, Ba 50.0 0.1 DPC EPA 200.8 0.02 11/20/2013 13:52 ug/L Beryllium, Be < 1 5 DAM EPA 200.7 1 11/20/2013 14:44 U ug/L Cadmium, Cd 34.2 0.05DPC EPA 200.8 0.01 11/20/2013 13:52 ug/L Chromium, Cr 5.3 0.2 DPC EPA 200.8 0.04 11/20/2013 13:52 ug/L Cobalt, Co 33.2 0.02DPC EPA 200.8 0.004 11/20/2013 13:52 ug/L Copper, Cu 2.03 0.05DPC EPA 200.8 0.01 11/20/2013 13:52 ug/L Lead, Pb 0.302 0.01 DPC EPA 200.8 0.002 11/20/2013 13:52 ng/L Mercury, Hg 921 10 TLT EPA 1631E 4 11/26/2013 ug/L Molybdenum, Mo 3300 0.05DPC EPA 200.8 0.01 11/20/2013 13:52 ug/L Nickel, Ni 544 0.2 DPC EPA 200.8 0.05 11/20/2013 13:52 ug/L Selenium, Se 436 0.5 DPC EPA 200.8 0.2 11/20/2013 13:52 ug/L Silver, Ag 0.012 0.01 DPC EPA 200.8 0.002 11/20/2013 13:52 ug/L Thallium, Tl 4.92 0.05DPC EPA 200.8 0.002 11/20/2013 13:52 ug/L Tin, Sn < 20 100 DAM EPA 200.7 20 11/20/2013 14:44 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 11/20/2013 14:44 U ug/L Zinc, Zn 87.8 0.5 DPC EPA 200.8 0.1 11/20/2013 13:52 mg/L Aluminum, Al 0.239 0.001DPC EPA 200.8 0.0003 11/20/2013 13:52 mg/L Boron, B 208 0.2 DAM EPA 200.7 0.04 11/20/2013 14:44 mg/L Calcium, Ca 563 0.2 DAM EPA 200.7 0.04 11/20/2013 14:44 mg/L Iron, Fe 0.4 0.5 DAM EPA 200.7 0.1 11/20/2013 14:44 J mg/L Magnesium, Mg 1910 0.1 DAM EPA 200.7 0.02 11/20/2013 14:44 mg/L Manganese, Mn 19.7 0.005DAM EPA 200.7 0.001 11/20/2013 14:44 mg/L Potassium, K 78.0 0.5 DAM EPA 200.7 0.07 11/20/2013 14:42 mg/L Sodium, Na 947 0.3 DAM EPA 200.7 0.08 11/20/2013 14:42 mg/L Strontium, Sr 7.00 0.01 DAM EPA 200.7 0.003 11/20/2013 14:42 mg/L Ammonia, NH3, as N 1.62 0.05DMM EPA 350.1 0.02 11/19/2013 mg/L Total Kjeldahl Nitrogen, TKN as N3.15 0.5 DMM EPA 351.2 0.1 10/29/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N25.4 0.1 DMM SM20 4500NO3 H 0.02 11/19/2013

Mountaineer Plant, 134633 Page 9 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134633-005ADate Collected:11/14/2013Date Received:11/15/2013 

### 1st Stage Feed Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 6.33 0.05DPC EPA 200.8 0.01 11/20/2013 13:57 ug/L Arsenic, As 14.3 0.1 DPC EPA 200.8 0.03 11/20/2013 13:57 ug/L Barium, Ba 45.8 0.1 DPC EPA 200.8 0.02 11/20/2013 13:57 ug/L Beryllium, Be < 1 5 DAM EPA 200.7 1 11/20/2013 14:53 U ug/L Cadmium, Cd 26.9 0.05DPC EPA 200.8 0.01 11/20/2013 13:57 ug/L Chromium, Cr 3.7 0.2 DPC EPA 200.8 0.04 11/20/2013 13:57 ug/L Cobalt, Co 29.8 0.02DPC EPA 200.8 0.004 11/20/2013 13:57 ug/L Copper, Cu 0.97 0.05DPC EPA 200.8 0.01 11/20/2013 13:57 ug/L Lead, Pb 0.017 0.01 DPC EPA 200.8 0.002 11/20/2013 13:57 ng/L Mercury, Hg 45.4 2 TLT EPA 1631E 0.8 11/26/2013 ug/L Molybdenum, Mo 3140 0.05DPC EPA 200.8 0.01 11/20/2013 13:57 ug/L Nickel, Ni 502 0.2 DPC EPA 200.8 0.05 11/20/2013 13:57 ug/L Selenium, Se 415 0.5 DPC EPA 200.8 0.2 11/20/2013 13:57 ug/L Selenite, Se+4 (Hydride) 222 20 TLT AEP Method 4 12/04/2013 AEP Method for Se speciation is not accredited through any agency. Results are for internal use only. ug/L Silver, Ag < 0.002 0.01 DPC EPA 200.8 0.002 11/20/2013 13:57 U ug/L Thallium, Tl 4.67 0.05DPC EPA 200.8 0.002 11/20/2013 13:57 ug/L Tin, Sn < 20 100 DAM EPA 200.7 20 11/20/2013 14:54 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 11/20/2013 14:54 U ug/L Zinc, Zn 74.8 0.5 DPC EPA 200.8 0.1 11/20/2013 13:57 mg/L Aluminum, Al 0.0327 0.001DPC EPA 200.8 0.0003 11/20/2013 13:57 mg/L Boron, B 204 0.2 DAM EPA 200.7 0.04 11/20/2013 14:53 mg/L Calcium, Ca 550 0.2 DAM EPA 200.7 0.04 11/20/2013 14:53 mg/L Iron, Fe < 0.1 0.5 DAM EPA 200.7 0.1 11/20/2013 14:54 U mg/L Magnesium, Mg 1870 0.1 DAM EPA 200.7 0.02 11/20/2013 14:53 mg/L Manganese, Mn 19.1 0.005DAM EPA 200.7 0.001 11/20/2013 14:53 mg/L Potassium, K 76.0 0.5 DAM EPA 200.7 0.07 11/20/2013 14:52 mg/L Sodium, Na 923 0.3 DAM EPA 200.7 0.08 11/20/2013 14:52 mg/L Strontium, Sr 6.81 0.01 DAM EPA 200.7 0.003 11/20/2013 14:52

Mountaineer Plant, 134633 Page 10 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134633-006Date Collected:11/14/2013Date Received:11/15/2013 

### 2nd Stage Feed

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 2.49 0.05DPC EPA 200.8 0.01 11/20/2013 14:02 ug/L Arsenic, As 18.4 0.1 DPC EPA 200.8 0.03 11/20/2013 14:02 ug/L Barium, Ba 45.0 0.1 DPC EPA 200.8 0.02 11/20/2013 14:02 ug/L Beryllium, Be < 1 5 DAM EPA 200.7 1 11/20/2013 15:03 U ug/L Cadmium, Cd 1.03 0.05DPC EPA 200.8 0.01 11/20/2013 14:02 ug/L Chromium, Cr 1.3 0.2 DPC EPA 200.8 0.04 11/20/2013 14:02 ug/L Cobalt, Co 33.9 0.02DPC EPA 200.8 0.004 11/20/2013 14:02 ug/L Copper, Cu 0.38 0.05DPC EPA 200.8 0.01 11/20/2013 14:02 ug/L Lead, Pb 0.023 0.01 DPC EPA 200.8 0.002 11/20/2013 14:02 ng/L Mercury, Hg 114 2 TLT EPA 1631E 0.8 11/26/2013 ug/L Molybdenum, Mo 2500 0.05DPC EPA 200.8 0.01 11/20/2013 14:02 ug/L Nickel, Ni 318 0.2 DPC EPA 200.8 0.05 11/20/2013 14:02 ug/L Selenium, Se 26.4 0.5 DPC EPA 200.8 0.2 11/20/2013 14:02 ug/L Silver, Ag 0.008 0.01 DPC EPA 200.8 0.002 11/20/2013 14:02 J ug/L Thallium, Tl 0.40 0.05DPC EPA 200.8 0.002 11/20/2013 14:02 ug/L Tin, Sn < 20 100 DAM EPA 200.7 20 11/20/2013 15:03 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 11/20/2013 15:03 U ug/L Zinc, Zn 8.5 0.5 DPC EPA 200.8 0.1 11/20/2013 14:02 mg/L Aluminum, Al 0.566 0.001DPC EPA 200.8 0.0003 11/20/2013 14:02 mg/L Boron, B 208 0.2 DAM EPA 200.7 0.04 11/20/2013 15:03 mg/L Calcium, Ca 529 0.2 DAM EPA 200.7 0.04 11/20/2013 15:03 mg/L Iron, Fe 1.34 0.5 DAM EPA 200.7 0.1 11/20/2013 15:03 mg/L Magnesium, Mg 1830 0.1 DAM EPA 200.7 0.02 11/20/2013 15:03 mg/L Manganese, Mn 21.9 0.005DAM EPA 200.7 0.001 11/20/2013 15:03 mg/L Potassium, K 75.0 0.5 DAM EPA 200.7 0.07 11/20/2013 15:01 mg/L Sodium, Na 786 0.3 DAM EPA 200.7 0.08 11/20/2013 15:01 mg/L Strontium, Sr 6.34 0.01 DAM EPA 200.7 0.003 11/20/2013 15:01 mg/L Ammonia, NH3, as N 1.19 0.05DMM EPA 350.1 0.02 11/19/2013 mg/L Total Kjeldahl Nitrogen, TKN as N7.40 0.5 DMM EPA 351.2 0.1 10/29/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N0.38 0.1 DMM SM20 4500NO3 H 0.02 11/19/2013

Mountaineer Plant, 134633 Page 11 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134633-006ADate Collected:11/14/2013Date Received:11/15/2013 

### 2nd Stage Feed Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 2.15 0.05DPC EPA 200.8 0.01 11/20/2013 14:07 ug/L Arsenic, As 16.4 0.1 DPC EPA 200.8 0.03 11/20/2013 14:07 ug/L Barium, Ba 41.9 0.1 DPC EPA 200.8 0.02 11/20/2013 14:07 ug/L Beryllium, Be < 1 5 DAM EPA 200.7 1 11/20/2013 15:12 U ug/L Cadmium, Cd 0.33 0.05DPC EPA 200.8 0.01 11/20/2013 14:07 ug/L Chromium, Cr 1.1 0.2 DPC EPA 200.8 0.04 11/20/2013 14:07 ug/L Cobalt, Co 31.4 0.02DPC EPA 200.8 0.004 11/20/2013 14:07 ug/L Copper, Cu 0.22 0.05DPC EPA 200.8 0.01 11/20/2013 14:07 ug/L Lead, Pb 0.022 0.01 DPC EPA 200.8 0.002 11/20/2013 14:07 ng/L Mercury, Hg 14.6 1 TLT EPA 1631E 0.4 11/26/2013 ug/L Molybdenum, Mo 2330 0.05DPC EPA 200.8 0.01 11/20/2013 14:07 ug/L Nickel, Ni 295 0.2 DPC EPA 200.8 0.05 11/20/2013 14:07 ug/L Selenium, Se 14.9 0.5 DPC EPA 200.8 0.2 11/20/2013 14:07 ug/L Selenite, Se+4 (Hydride) 2 2 TLT AEP Method 0.4 12/04/2013 J AEP Method for Se speciation is not accredited through any agency. Results are for internal use only. ug/L Silver, Ag 0.003 0.01 DPC EPA 200.8 0.002 11/20/2013 14:07 J ug/L Thallium, Tl 0.34 0.05DPC EPA 200.8 0.002 11/20/2013 14:07 ug/L Tin, Sn < 20 100 DAM EPA 200.7 20 11/20/2013 15:13 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 11/20/2013 15:12 U ug/L Zinc, Zn 12.6 0.5 DPC EPA 200.8 0.1 11/20/2013 14:07 mg/L Aluminum, Al 0.530 0.001DPC EPA 200.8 0.0003 11/20/2013 14:07 mg/L Boron, B 215 0.2 DAM EPA 200.7 0.04 11/20/2013 15:12 mg/L Calcium, Ca 544 0.2 DAM EPA 200.7 0.04 11/20/2013 15:12 mg/L Iron, Fe 1.21 0.5 DAM EPA 200.7 0.1 11/20/2013 15:13 mg/L Magnesium, Mg 1910 0.1 DAM EPA 200.7 0.02 11/20/2013 15:12 mg/L Manganese, Mn 22.6 0.005DAM EPA 200.7 0.001 11/20/2013 15:12 mg/L Potassium, K 78.7 0.5 DAM EPA 200.7 0.07 11/20/2013 15:11 mg/L Sodium, Na 826 0.3 DAM EPA 200.7 0.08 11/20/2013 15:11 mg/L Strontium, Sr 6.58 0.01 DAM EPA 200.7 0.003 11/20/2013 15:11

Mountaineer Plant, 134633 Page 12 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134633-007Date Collected:11/14/2013Date Received:11/15/2013 

### Bioreactor Effluent

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 0.17 0.05DPC EPA 200.8 0.01 11/20/2013 14:12 ug/L Arsenic, As 0.86 0.1 DPC EPA 200.8 0.03 11/20/2013 14:12 ug/L Barium, Ba 45.2 0.1 DPC EPA 200.8 0.02 11/20/2013 14:12 ug/L Beryllium, Be 2 5 DAM EPA 200.7 1 11/20/2013 15:22 J ug/L Cadmium, Cd 0.18 0.05DPC EPA 200.8 0.01 11/20/2013 14:12 ug/L Chromium, Cr 1.1 0.2 DPC EPA 200.8 0.04 11/20/2013 14:12 ug/L Cobalt, Co 0.178 0.02DPC EPA 200.8 0.004 11/20/2013 14:12 ug/L Copper, Cu 0.17 0.05DPC EPA 200.8 0.01 11/20/2013 14:12 ug/L Lead, Pb 0.014 0.01 DPC EPA 200.8 0.002 11/20/2013 14:12 ng/L Mercury, Hg 26.5 1 TLT EPA 1631E 0.4 11/26/2013 ug/L Molybdenum, Mo 94.1 0.05DPC EPA 200.8 0.01 11/20/2013 14:12 ug/L Nickel, Ni 7.01 0.2 DPC EPA 200.8 0.05 11/20/2013 14:12 ug/L Selenium, Se 3.4 0.5 DPC EPA 200.8 0.2 11/20/2013 14:12 ug/L Silver, Ag 0.003 0.01 DPC EPA 200.8 0.002 11/20/2013 14:12 J ug/L Thallium, Tl 0.02 0.05DPC EPA 200.8 0.002 11/20/2013 14:12 J ug/L Tin, Sn < 20 100 DAM EPA 200.7 20 11/20/2013 15:22 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 11/20/2013 15:22 U ug/L Zinc, Zn 1.5 0.5 DPC EPA 200.8 0.1 11/20/2013 14:12 mg/L Aluminum, Al 1.75 0.001DPC EPA 200.8 0.0003 11/20/2013 14:12 mg/L Boron, B 262 0.2 DAM EPA 200.7 0.04 11/20/2013 15:22 mg/L Calcium, Ca 553 0.2 DAM EPA 200.7 0.04 11/20/2013 15:22 mg/L Iron, Fe 1.51 0.5 DAM EPA 200.7 0.1 11/20/2013 15:22 mg/L Magnesium, Mg 2000 0.1 DAM EPA 200.7 0.02 11/20/2013 15:22 mg/L Manganese, Mn 27.4 0.005DAM EPA 200.7 0.001 11/20/2013 15:22 mg/L Potassium, K 83.4 0.5 DAM EPA 200.7 0.07 11/20/2013 15:20 mg/L Sodium, Na 839 0.3 DAM EPA 200.7 0.08 11/20/2013 15:20 mg/L Strontium, Sr 6.63 0.01 DAM EPA 200.7 0.003 11/20/2013 15:20 mg/L Ammonia, NH3, as N 0.35 0.05DMM EPA 350.1 0.02 11/19/2013 mg/L Total Kjeldahl Nitrogen, TKN as N5.79 0.5 DMM EPA 351.2 0.1 10/29/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N0.22 0.1 DMM SM20 4500NO3 H 0.02 11/19/2013

Mountaineer Plant, 134633 Page 13 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134633-007ADate Collected:11/14/2013Date Received:11/15/2013 

### Bioreactor Effluent Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 0.12 0.05DPC EPA 200.8 0.01 11/20/2013 14:17 ug/L Arsenic, As 0.76 0.1 DPC EPA 200.8 0.03 11/20/2013 14:17 ug/L Barium, Ba 42.7 0.1 DPC EPA 200.8 0.02 11/20/2013 14:17 ug/L Beryllium, Be < 1 5 DAM EPA 200.7 1 11/20/2013 15:45 U ug/L Cadmium, Cd 0.08 0.05DPC EPA 200.8 0.01 11/20/2013 14:17 ug/L Chromium, Cr 1.0 0.2 DPC EPA 200.8 0.04 11/20/2013 14:17 ug/L Cobalt, Co 0.134 0.02DPC EPA 200.8 0.004 11/20/2013 14:17 ug/L Copper, Cu 0.08 0.05DPC EPA 200.8 0.01 11/20/2013 14:17 ug/L Lead, Pb 0.012 0.01 DPC EPA 200.8 0.002 11/20/2013 14:17 ng/L Mercury, Hg 8.6 0.5 TLT EPA 1631E 0.2 11/26/2013 ug/L Molybdenum, Mo 84.2 0.05DPC EPA 200.8 0.01 11/20/2013 14:17 ug/L Nickel, Ni 6.45 0.2 DPC EPA 200.8 0.05 11/20/2013 14:17 ug/L Selenium, Se 2.6 0.5 DPC EPA 200.8 0.2 11/20/2013 14:17 ug/L Selenite, Se+4 (Hydride)< 0.08 0.4 TLT AEP Method 0.08 12/04/2013 U AEP Method for Se speciation is not accredited through any agency. Results are for internal use only. ug/L Silver, Ag < 0.002 0.01 DPC EPA 200.8 0.002 11/20/2013 14:17 U ug/L Thallium, Tl 0.02 0.05DPC EPA 200.8 0.002 11/20/2013 14:17 J ug/L Tin, Sn < 20 100 DAM EPA 200.7 20 11/20/2013 15:46 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 11/20/2013 15:45 U ug/L Zinc, Zn 2.1 0.5 DPC EPA 200.8 0.1 11/20/2013 14:17 mg/L Aluminum, Al 1.65 0.001DPC EPA 200.8 0.0003 11/20/2013 14:17 mg/L Boron, B 265 0.2 DAM EPA 200.7 0.04 11/20/2013 15:45 mg/L Calcium, Ca 558 0.2 DAM EPA 200.7 0.04 11/20/2013 15:45 mg/L Iron, Fe 1.51 0.5 DAM EPA 200.7 0.1 11/20/2013 15:46 mg/L Magnesium, Mg 2030 0.1 DAM EPA 200.7 0.02 11/20/2013 15:45 mg/L Manganese, Mn 27.7 0.005DAM EPA 200.7 0.001 11/20/2013 15:45 mg/L Potassium, K 84.8 0.5 DAM EPA 200.7 0.07 11/20/2013 15:44 mg/L Sodium, Na 852 0.3 DAM EPA 200.7 0.08 11/20/2013 15:44 mg/L Strontium, Sr 6.76 0.01 DAM EPA 200.7 0.003 11/20/2013 15:44



### Sample Number:134633-008Date Collected:11/14/2013Date Received:11/15/2013 

### Field Blank

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ng/L Mercury, Hg < 0.2 0.5 TLT EPA 1631E 0.2 11/26/2013 U

THIS TEST REPORT RELATES ONLY TO THE ITEMS TESTED AND SHALL NOT BE REPRODUCED EXCEPT IN FULL WITHOUT WRITTEN APPROVAL OF THE LABORATORY. ALL TEST RESULTS MEET ALL OF THE REQUIREMENTS OF THE ACCREDITING AUTHORITY, UNLESS OTHERWISE NOTED. U: Analyte was analyzed and not detected at or above adjusted Method Detection Limit J: Analyte was positively identified, though the quantitation was below Reporting Limit.

Brian Snyder, Chemist II Email bssnyder@aep.comTel. 614-836-4224

Fax 614-836-4168Audinet 210-4224

Mountaineer Plant, 134633 Page 14 of 14