Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop‐down boxes, included. Gray fields are aut

filled from other fields.

Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop‐down boxes, included. Gray fields are aut

filled from other fields.

Please name each resulting spreadsheet with the following naming convention:

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop‐down boxes, included. Gray fields are aut

filled from other fields.

Please name each resulting spreadsheet with the following naming convention:

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.3. Please choose the type of fuel being sampled using the drop‐down in the fuel column of the Boiler Information

worksheet If you choose "other" please provide a description of the fuel in the Other Fuel Description column

Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop‐down boxes, included. Gray fields are aut

filled from other fields.

Please name each resulting spreadsheet with the following naming convention:

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.3. Please choose the type of fuel being sampled using the drop‐down in the fuel column of the Boiler Information

worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column.

4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "A

D5865‐04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If t

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange

highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksh

Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop‐down boxes, included. Gray fields are aut

filled from other fields.

Please name each resulting spreadsheet with the following naming convention:

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.3. Please choose the type of fuel being sampled using the drop‐down in the fuel column of the Boiler Information

worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column.

4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "A

D5865‐04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If t

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange

highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksh

6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell).

7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a mincomposite samples consisting of 3 combined grab samples each, but you are not limited to that number if you ha

collected more.

8. Provide the results of the analyses for each constituent requested. Use the drop‐down boxes to fill in the unit

Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop‐down boxes, included. Gray fields are aut

filled from other fields.

Please name each resulting spreadsheet with the following naming convention:

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.3. Please choose the type of fuel being sampled using the drop‐down in the fuel column of the Boiler Information

worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column.

4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "A

D5865‐04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If t

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange

highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksh

6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell).

7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a mincomposite samples consisting of 3 combined grab samples each, but you are not limited to that number if you ha

collected more.

8. Provide the results of the analyses for each constituent requested. Use the drop‐down boxes to fill in the unit

measure.
EIA Facility Code Facility Name Boiler ID Fuel Type 1

2107 Sioux 2 subbituminous
Fuel Type 2 Fuel Type 3 Other Fuel Description

bituminous
EIA Facility Code Facility Name Boiler ID Basis Analyte

2107 Sioux 2 As Received Higher Heating Value

2107 Sioux 2 As Received % Moisture

2107 Sioux 2 As Received % Ash

2107 Sioux 2 As Received % Sulfur

2107 Sioux 2 Dry basis Higher Heating Value

2107 Sioux 2 Dry basis % Ash

2107 Sioux 2 Dry basis % Sulfur

2107 Sioux 2 Dry basis Antimony

2107 Sioux 2 Dry basis Arsenic

2107 Sioux 2 Dry basis Beryllium

2107 Sioux 2 Dry basis Cadmium

2107 Sioux 2 Dry basis Chlorine

2107 Sioux 2 Dry basis Chromium

2107 Sioux 2 Dry basis Cobalt

2107 Sioux 2 Dry basis Fluorine

2107 Sioux 2 Dry basis Lead

2107 Sioux 2 Dry basis Manganese

2107 Sioux 2 Dry basis Mercury

2107 Sioux 2 Dry basis Nickel

2107 Sioux 2 Dry basis Selenium
Analysis Method for each Analyte 

(example: ASTM D5865-04)

ASTM D5865

ASTM D5142, ASTM D5373

ASTM D5142, ASTM D5373

ASTM D4239

ASTM D5142, ASTM D5373

ASTM D5142, ASTM D5373

ASTM D4239

ASTM D6357, ASTM D5987

ASTM D6357, ASTM D5987

ASTM D6357, ASTM D5987

ASTM D6357, ASTM D5987

ASTM D6721

ASTM D6357, ASTM D5987

ASTM D6357, ASTM D5987

ASTM D5987

ASTM D6357, ASTM D5987

ASTM D6357, ASTM D5987

ASTM D6722

ASTM D6357, ASTM D5987

ASTM D6357, ASTM D5987
EIA Facility Code Facility Name Boiler ID HAPs Test Group

2107 Sioux 2 Non‐dioxin/furan organic HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received) HHV Units

COAL SAMPLE 5   5/4/2010 5/4/2010

COAL SAMPLE 6   5/4/2010 5/4/2010

COAL SAMPLE 7   5/4/2010 5/4/2010

 Fuel Testing Results
% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

25.9494 12181 Btu/lb

26.22588 12213 Btu/lb

25.06807 12227 Btu/lb
Chlorine

(Dry Basis)

Chlorine 

Units

Mercury 

(Dry Basis)

Mercury 

Units

Antimony 

(Dry Basis)

Antimony 

Units

Arsenic (Dry 

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units
Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry 

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry 

Basis) Nickel Units
Note the P

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry 

Basis) Cobalt Units Total Moisture Volatiles

13.76 51.48

12.62 49.16

9.47 50.21

Proximate Analyses, %
roximate/Ultimate data below should be recorded on a dry basis (including ash).

Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

7.77 71.15 5.33 1.16 1.14 13.45

7.67 71.4 5.2 1.17 1.17 13.39

7.73 69.7 5.1 1.14 1.28 15.05

% by wt Ultimate Analyses, % by wt
EIA Facility Code Facility Name Boiler ID HAPs Test Group

2107 Sioux 2 Acid gas HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher 

Heating 

Value (HHV)

(as 

received) HHV Units

COAL SAMPLE 1   4/27/2010 4/27/2010

COAL SAMPLE 2   4/28/2010 4/28/2010

COAL SAMPLE 3   4/28/2010 4/28/2010

COAL SAMPLE 4   5/3/2010 5/3/2010

 Fuel Testing Results
% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

25.84255 12173 Btu/lb

26.04692 12277 Btu/lb

25.61881 12208 Btu/lb

26.32784 12058 Btu/lb
Chlorine

(Dry Basis)

Chlorine 

Units

Mercury 

(Dry Basis)

Mercury 

Units

Antimony 

(Dry Basis)

Antimony 

Units

Arsenic (Dry 

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

0.0196 % 0.066 μg/g 0.210295 μg/g 1.424753 μg/g 0.419268 μg/g

0.0182 % 0.043 μg/g 0.183904 μg/g 1.274356 μg/g 0.391781 μg/g

0.0193 % 0.056 μg/g 0.193793 μg/g 1.362075 μg/g 0.436343 μg/g

0.0196 % 0.057 μg/g 0.215 μg/g 1.22 μg/g 0.415 μg/g
Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry 

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry 

Basis) Nickel Units

0.095148 μg/g 8.211272 μg/g 3.252828 μg/g 17.71541 μg/g 6.860171 μg/g

0.086698 μg/g 6.783102 μg/g 3.144923 μg/g 19.46328 μg/g 6.270634 μg/g

0.075735 μg/g 7.340685 μg/g 3.072218 μg/g 17.76176 μg/g 6.311415 μg/g

0.103 μg/g 7.93 μg/g 3.09 μg/g 14.5 μg/g 5.81 μg/g
Note the Proximate/U

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry 

Basis) Cobalt Units Total Moisture Volatiles Ash

<1 μg/g 112 μg/g 2.123827 μg/g 13.22 50.59 7.56

<1 μg/g 87.9 μg/g 2.2777 μg/g 11.86 50.26 7.56

<1 μg/g 2.208608 μg/g 12.12 49.49 7.65

<1 μg/g 124 μg/g 2.08 μg/g 10.66 49.24 8.28

Proximate Analyses, % by wt
ltimate data below should be recorded on a dry basis (including ash).

Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

70.68 5.08 1.26 1.23 14.1704

71.22 5.35 1.32 1.19 13.3418

70.97 5.16 1.26 1.21 13.7307

70.32 5.24 1.21 1.11 13.8204

Ultimate Analyses, % by wt
EIA Facility Code Facility Name Boiler ID HAPs Test Group

2107 Sioux 2

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received) HHV Units

 Fuel Testing Results
% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)
Chlorine

(Dry Basis)

Chlorine 

Units

Mercury 

(Dry Basis)

Mercury 

Units

Antimony 

(Dry Basis)

Antimony 

Units

Arsenic (Dry 

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units
Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry 

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry 

Basis) Nickel Units
Note the Proximate/U

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry 

Basis) Cobalt Units Total Moisture Volatiles Ash

Proximate Analyses, % by w
ltimate data below should be recorded on a dry basis (including ash).

Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

wt Ultimate Analyses, % by wt
EIA Facility Code Facility Name Boiler ID HAPs Test Group

2107 Sioux 2 Mercury and non‐mercury metalic HAP

Sample Number 

(minimum of 3 

composite samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating Value 

(HHV)

(as received) HHV Units

COAL SAMPLE 1   4/27/2010 4/27/2010

COAL SAMPLE 2       4/28/2010 4/28/2010

COAL SAMPLE 4      5/3/2010 5/3/2010

COAL SAMPLE 5      5/4/2010 5/4/2010

 Fuel Testing Results
Ps

% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

25.84255 12173 Btu/lb

26.04692 12277 Btu/lb

26.32784 12058 Btu/lb

25.9494 12181 Btu/lb
Chlorine

(Dry Basis)

Chlorine 

Units

Mercury 

(Dry Basis)

Mercury 

Units

Antimony 

(Dry Basis)

Antimony 

Units

Arsenic (Dry 

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

0.0196 % 0.066 μg/g 0.210295 μg/g 1.424753 μg/g 0.419268

0.0182 % 0.043 μg/g 0.183904 μg/g 1.274356 μg/g 0.391781

0.0196 % 0.057 μg/g 0.215 μg/g 1.22 μg/g 0.415
Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry 

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

μg/g 0.095148 μg/g 8.211272 μg/g 3.252828 μg/g 17.71541 μg/g

μg/g 0.086698 μg/g 6.783102 μg/g 3.144923 μg/g 19.46328 μg/g

μg/g 0.103 μg/g 7.93 μg/g 3.09 μg/g 14.5 μg/g
Nickel (Dry 

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry 

Basis) Cobalt Units Total Moisture

6.860171 μg/g <1 μg/g 112 μg/g 2.123827 μg/g 13.22

6.270634 μg/g <1 μg/g 87.9 μg/g 2.2777 μg/g 11.86

5.81 μg/g <1 μg/g 124 μg/g 2.08 μg/g 10.66

13.76

Pr
Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur

50.59 7.56 70.68 5.08 1.26 1.23

50.26 7.56 71.22 5.35 1.32 1.19

49.24 8.28 70.32 5.24 1.21 1.11

51.48 7.77 71.15 5.33 1.16 1.14

roximate Analyses, % by wt Ultimate Analyses, % by wt
Oxygen

14.1704

13.3418

13.8204

13.45
Units of Measure Tables: Please do not modify these tables, except to add your own unit of measu

Fuel Units of Measure - HHV

anthracite Btu/lb

bituminous Btu/gallon

subbituminous

lignite

coal refuse (culm or gob)

No.2 Fuel Oil (distillate)

No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals

synfuel mg/g

petroleum coke μg/g

other mg/Kg
re to the orange hightlighted cell, if necessary.

Units of Measure - Cl, Fl

%

ppm