U.S. DEPARTMEiWjRSii

National Butsau of Standards

NBS Special Publication 699

A Bibliography of Sources of

Thermodynamic Data for the Systems:

CO2+NH3+H2O, CO2+H2S+H2O,

H2S+NH3+H2O, and CO2+NH3+H2S+H2O

R. N. Goldberg and D. K. Steckler

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NBS Special Publication 699

A Bibliography of Sources of

Thermodynamic Data for the Systems:

C02+NH^^H20, C02+H2S^H20,

H2S+NH^+H20, and C02+NH^^H2S+H20

R. N. Goldberg and D. K. Steckler Center for Chemical Physics

National Measurement Laboratory

National Bureau of Standards

Gaiihersburg, MD 20899

Sponsored by:

Design Institute for Physical Property Data

Project 811 American Institute of Chemical Engineers

New York, N Y

May 1985

U.S. Department of Commerce

Malcolm Baldrige, Secretary National Bureau of Standards

Ernest Ambler, Director
Library of Congress U.S. Government Printing Office Catalog Card Number: 85-600545 Washington: 1985 National Bureau of Standards

Special Publication 699

Natl. Bur. Stand. (U.S.), Spec. Publ. 699, 37 pages (May 1985) CODEN: XNBSAV

For sale by the Superintendent

of Documents,

U.S. Government Printing Office, Washington. DC 20402
ABSTRACT

Contained herein is a bibliography of sources of experimental and

correlated thermodynamic data for the systems CO2 + NH^ + H2O, CO2 + H2S +

H2O, H2S + NH3 + H2O, and CO2 + NH3 + H2S + H2O. The types of data in this

bibliography include all types of equilibrium data, including both equilibria

in solution and vapor-liquid equilibrium data, enthalpies, heat capacities,

and densities. There are 215 references cited.

KEY WORDS: ammonia; ammonium carbamate; bibliography; carbon dioxide;

enthalpy; equilibrium constants; heat capacity; hydrogen sulfide;

sour water; thermodynamics; urea; vapor-liquid equilibria; water.

iii

INTRODUCTION

The thermodynamics of mixtures of CO2 + NH3 + H2O, CO2 + H2S + H2O, NH3

+ H2S + H2O, and CO2 + NH3 + H2S + H2O are of importance for a variety of

industrial applications which include the synthesis of urea, the utilization

of sour water systems, gas production, and environmental concerns. The

purpose of this bibliography is to identify papers which contain either

experimental thermodynamic data for these systems or reviews or correlations

of this data. The thermodynamic properties of interest include all types of

equilibrium data, including both equilibria in solution and vapor-liquid

equilibrium data, enthalpies, heat capacities, and densities. The principal

0 2- 0 0 - 2-

species in aqueous solutions are CO^, CO^ , HCO^, H^CO^, NH^, NHJ, HS , S ,

C0(NH2)2, and ammonium carbamate, NH2C00NHi|. Our search of the literature

was based upon a search of the following sources: a computer aided one of

Chemical Abstracts from 1967 to 1983, the Bulletin of Chemical Thermodynamics

[1] from 1960 to 1981, the files of the Chemical Thermodynamics Data Center

at the National Bureau of Standards, and, finally, of the references found in

the papers identified in the search itself. The authors would appreciate

learning of any papers which we have missed in our search.

The papers are listed alphabetically by first author. Each

bibliographic citation includes a brief reference citation (the year and

three letters from the names of the first two authors), the authors names,

the title of the article and the source. In one instance only an abstract

was available and there we have also given the Chemical Abstracts citation.

The last column contains a capital letter(s) which serves to identify which

systems are found in the paper. The letter codes used are: (A) CO2 + H2S +

H2O, (B) CO2 + NH3 + H2O, (C) H2S + NH3 + H2O, and (D) CO2 + H2S + NH3 + H2O.
Each paper has been annotated to show the type of data, the temperature

range and, if appropriate, the pressure, solution composition, and pH. The

property codes which we have used are from the Bulletin of Chemical

Thermodynamics [1]; they are reproduced in Table I. In specifying the

compositions of ternary systems, we have frequently used the quantities L and

W, which are defined to be the mole ratios m^/C02 and H2O/CO2, respectively.

Note that, using existing conventions, the value of W can be negative [2].

We have attempted to adhere to the journal abbreviations used in the Chemical

Abstracts Service Source Index [3].

The Japanese, Russian, and Polish titles have been translated into

English. These translations come, by preference, from the papers themselves

or from Chemical Abstracts. The titles from the latter source may be

condensations of the originals.

This bibliography was sponsored by the Design Institute for Physical

Property Data (DIPPR) of the American Institute of Chemical Engineers.

Bibliographies on the binary systems CO2 + H2O, NH^ + H2O, and H2S + H2O have

also been compiled for DIPPR under the direction of Drs. David Garvin, David

Smith-Magowan, and Bert R. Staples. These bibliographies have been used in

developing the present listing, but those papers which treat only the

binaries have not been repeated here. We thank Mr. T. B. Selover of the

Standard Oil Company for bringing several references to our attention for

inclusion in this bibliography. Dr. Hideo Okabe for his assistance with the

papers written in Japanese, and Dr. Ewa Gajewski for her help with the papers

in Polish.

2
REFERENCES

[1] Bulletin of Chemical Thermodynamic, R. D. Freeman, editor.

Thermochemistry, Inc., Stillwater, OK, 1977 to 1981.

[2] Durisch, W. ; Lemkowitz, S. M. ; van den Berg, P. J.; Chimia; *34, 314

(1980); "Constituent and Component Measurements and Calculations of the

Vapor/Liquid Equilibrium of the Ternary System Carbon

Dioxide-Ammonia-Water under Urea Synthesis Conditions."

C3] Chemical Abstracts Service Source Index: 1907-1979 Cumulative, in two

volumes; American Chemical Society, Washington, DC, 1979.

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U.S. OEPT. or COM>^.. 1. PUBLICATION OR 2. Performing Organ. Report No. 3. Poblication Date BIBLIOGRAPHIC DATA

REPORT NO. SHEET (See instructions NBS/SP-699 May 1985

4. TITLE AND SUBTITLE

A Bibliography of Sources of Thermodynamic Data for the Systems: + NH^ + H^O,

CO. + H^S + H^O, H^S + NH3 + H2O, and CO^ + NH3 + H^S + H^O

5. AUTHOR(S',

R. N. Goldberg and D. K. Steckler

6. PERFORMING ORGANIZATION (if joint or other than NBS, see instructions^

NATIONAL BUREAU OF STANDARDS

U.S. DEPARTMENT OF COMMERCE

GAITHERSBURG, MD 20899

7. Contract/Gram No.

8. Type of Report & Period Covered

Final

9. SPONSORING ORGANIZATION NAME AND COMPLETE ADDRESS (Street. City. Slate, ZIP)

Design Institute for Physical Property Data

Project 811

American Institute of Chemical Engineers

New York. NY

10. SUPPLEMENTARY NOTES

Library of Congress Catalog Card Number: 85-600545

|~ - Document describes a compute' program; SF-185, FlPS Software Summary, is attached.

11. ABSTRACT l A 200-wora o' /ess foctuoi summary of most si gnificant information. If document includes a significant

b' bi lOgroony o' iiteroture survey, mention it here; Contained herein is a bibliography of sources of experimental and correlated

thermodynamic data for the systems CO/ + NH^ + H^O, CO^ + H^S + H^O, H^S + NH2 + H^O,

and COo + NH^ + HpS + H2O. The types of data in this DibliOgraphy incfude all types

of equilibrium data, including both eqilibria in solution and vapor-liquid equilibrium

date, enthalpies, heat capacities, and densities. There are 216 references cited.

12. KEY WORDS (Sj* to twelve entries; alphabeti cal order; capitalize only proper names; and separate key words by semicolons)

ammonia; ammonium carbamate; bibliography; carbon dioxide; enthalpy; equilibrium

constants; heat capacity; hydrogen sulfide; sour water; thermodynamics; urea;

vapor-1 i qui d equilibria; water

13. AVAILABILITY

Unlimited

I

i For Official Distribution, Do Not Release to NTIS

I Xi Order From Superintendent of Documents, U.S. Government Printing Office, Washington, D.C. 20402.

I ! Order From National Technical Information Service (NTIS), Springfield, VA. 22161

14. NO. OF

PRINTED PAGES

37

15. Price

USCOMM-DC 6043-P80

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and supplements are available from ACS, 1155 Sb(teenth St., NW, Washington, DC 20056.

Building Science Series—Disseminates technical information developed at the Bureau on building materials,

components, systems, and whole structures. The series presents research results, test methods, and perfor- mance criteria related to the structural and environmental functions and the durability and safety

characteristics of building elements and systems.

Technical Notes—Studies or repons which are complete in themselves but restrictive in their treatment of a

subject. Analogous to monographs but not so comprehensive in scope or definitive in treatment of the subject

area. Often serve as a vehicle for fmal reports of work performed at NBS under the sponsorship of other government agencies.

Voiuntar> Product Standards—Developed under procedures published by the Department of Commerce in Part 10, Title 15, of the Code of Federal Regulations. The standards establish nationally recognized re- quirements for products, and provide all concerned interests with a basis for common understanding of the

characteristics of the products. NBS administers this program as a supplement to the activities of i e sector standardizing organizations.

Consumer Information Series—Practical information, based on NBS research and experience, co\ - of interest to the consumer. Easily understandable language and illustrations provide useful ba - knowledge for shopping in today's technological marketplace.

Order the above NBS publications from: Superintendent of Documents, Govern x'e, Washington, DC 20402. Order the following NBS publications—FIPS and NBSIR 's—from the National Tec

vice, Springfield, VA 22161.

Federal Information Processing Standards Publications (FIPS PLU)—Publications in this series collecti\ely constitute the Federal Information Processing Standards Register. The Register serves as i- ^ of

information in the Federal Government regarding standards issued by NBS pursuant to i and Administrative Services Act of 1949 as amended. Public Law 89-306 (79 Stat. 1

^ by Executive Order 1 1717 (38 FR 12315, dated May 11, 1973) and Part 6 of Title 1: Regulations).

NBS Interagency Reports (NBSIR)—A special series of interim or final reports on work perfo NBS

for outside sponsors (both government and non-government). In general, initial distribution i:- ^\ the sponsor; public distribution is by the National Technical Information Service, Springfield ^r

copy or microfiche form.
U.S. Department of Commerce

National Bureau of Standards

Gaithersburg. MD 20899

Official Business

Penalty for Private Use $300