Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls(example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

-down in the fuel column of the Boiler Information worksheet.If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

-down boxes to fill in the units of

measure.Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet.If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

1943 Hoot Lake Plant 2 subbituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis Analyte

1943 Hoot Lake Plant 2 As Received Higher Heating Value 1943 Hoot Lake Plant 2 As Received % Moisture 1943 Hoot Lake Plant 2 As Received % Ash 1943 Hoot Lake Plant 2 As Received % Sulfur 1943 Hoot Lake Plant 2 Dry basis Higher Heating Value 1943 Hoot Lake Plant 2 Dry basis % Ash 1943 Hoot Lake Plant 2 Dry basis % Sulfur 1943 Hoot Lake Plant 2 Dry basis Antimony 1943 Hoot Lake Plant 2 Dry basis Arsenic 1943 Hoot Lake Plant 2 Dry basis Beryllium 1943 Hoot Lake Plant 2 Dry basis Cadmium 1943 Hoot Lake Plant 2 Dry basis Chlorine 1943 Hoot Lake Plant 2 Dry basis Chromium 1943 Hoot Lake Plant 2 Dry basis Cobalt 1943 Hoot Lake Plant 2 Dry basis Fluorine 1943 Hoot Lake Plant 2 Dry basis Lead 1943 Hoot Lake Plant 2 Dry basis Manganese 1943 Hoot Lake Plant 2 Dry basis Mercury 1943 Hoot Lake Plant 2 Dry basis Nickel 1943 Hoot Lake Plant 2 Dry basis SeleniumAnalysis Method for each Analyte

(example: ASTM D5865-04) ASTM D3172-89/D3176-89 ASTM D3172-89/D3176-89 ASTM D3172-89/D3176-89 ASTM D3172-89/D3176-89 ASTM D3172-89/D3176-89 ASTM D3172-89/D3176-89 ASTM D3172-89/D3176-89 SW846 6020A SW846 6020A SW846 6020A SW846 6020A ASTM D6721-01 SW846 6020A SW846 6020A ASTM D5987-96 (2002) SW846 6020A SW846 6020A ASTM D6722-01 SW846 6020A SW846 6020AEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 1943 Hoot Lake 2 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units % Moisture (as received) % A sh (as received) 1 - M29 5/24/2010 5/24/2010 9180.00 Btu/lb 26.17 3.77 2 - M29 5/25/2010 5/25/2010 9248.00 Btu/lb 25.96 3.81 3 - M29 5/26/2010 5/26/2010 9283.00 Btu/lb 25.76 3.70 1 - OTM 27/28 5/19/2010 5/19/2010 9243.00 Btu/lb 26.09 3.66 2 - OTM 27/28 5/20/2010 5/20/2010 9196.00 Btu/lb 25.95 4.15 3 - OTM 27/28 5/21/2010 5/21/2010 9205.00 Btu/lb 25.87 4.01 Fuel Testing ResultsMercury and non-mercury metalic HAPs

% Sulfur (as received) Higher Heating

Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units 0.32 12434 Btu/lb 5.11 0.43 < 27.1 μg/g 0.037 μg/g 0.32 12491 Btu/lb 5.15 0.43 < 27 μg/g 0.045 μg/g 0.34 12504 Btu/lb 4.98 0.46 < 26.9 μg/g 0.058 μg/g 0.28 12506 Btu/lb 4.95 0.38 38.0 μg/g 0.032 μg/g 0.34 12419 Btu/lb 5.60 0.46 < 27 μg/g 0.049 μg/g 0.36 12418 Btu/lb 5.41 0.49 < 27 μg/g 0.030 μg/gAntimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) < 0.26 ppm 1.22 ppm 0.18 ppm 0.06 ppm 2.58 < 0.25 ppm 1.25 ppm 0.19 ppm < 0.05 ppm 2.35 < 0.22 ppm 1.29 ppm 0.12 ppm 0.06 ppm 2.04 < 0.23 ppm 0.76 ppm 0.11 ppm < 0.05 ppm 2.04 < 0.26 ppm 1.11 ppm 0.13 ppm 0.05 ppm 2.37 < 0.24 ppm 1.07 ppm 0.20 ppm 0.05 ppm 2.16Chromium

Units Lead (Dry

Basis) Lead

Units Manganese

(Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) ppm 1.17 ppm 16.01 ppm 1.83 ppm 0.27 ppm ppm 1.15 ppm 14.22 ppm 1.70 ppm 0.29 ppm ppm 1.11 ppm 16.47 ppm 1.69 ppm 0.34 ppm ppm 1.20 ppm 13.40 ppm 1.43 ppm 0.24 ppm ppm 1.35 ppm 14.70 ppm 1.71 ppm 0.28 ppm ppm 1.20 ppm 13.74 ppm 1.62 ppm 0.26 ppmFluoride

Units Cobalt (Dry

Basis) Cobalt Units 0.77 ppm 0.77 ppm 0.79 ppm 0.64 ppm 0.78 ppm 0.73 ppmEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 1943 Hoot Lake Plant 2 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 1 - CTM 033 5/18/2010 5/18/2010 9086.00 Btu/lb 2 - CTM 033 5/18/2010 5/18/2010 9106.00 Btu/lb 3 - CTM 033 5/19/2010 5/19/2010 9173.00 Btu/lb 1 - M26A 5/24/2010 5/24/2010 9104.00 Btu/lb 2 - M26A 5/25/2010 5/25/2010 9247.00 Btu/lb 3 - M26A 5/26/2010 5/26/2010 9236.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units 26.67 3.60 0.26 12391 Btu/lb 4.91 0.35 < 27.3 μg/g 26.60 3.55 0.26 12406 Btu/lb 4.84 0.35 < 27.2 μg/g 25.93 3.96 0.27 12384 Btu/lb 5.35 0.36 31.2 μg/g 26.34 4.17 0.32 12360 Btu/lb 5.66 0.43 < 27.2 μg/g 26.41 3.87 0.32 12565 Btu/lb 5.26 0.43 < 27.2 μg/g 25.61 3.86 0.35 12415 Btu/lb 5.19 0.47 < 26.9 μg/gMercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis)Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel UnitsSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units 41.0 μg/g 46.0 μg/g 45.0 μg/g 52.0 μg/g 47.0 μg/g 48.9 μg/gEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 1943 Hoot Lake Plant 2 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 1 - M25A 5/27/2010 5/27/2010 9223 Btu/lb 2 - M25A 5/27/2010 5/27/2010 9167 Btu/lb 3 - M25A 5/27/2010 5/27/2010 9220 Btu/lb 1 - M0011 5/24/2010 5/24/2010 9236 Btu/lb 2 - M0011 5/25/2010 5/25/2010 9207 Btu/lb 3 - M0011 5/25/2010 5/25/2010 9257 Btu/lb 1 - M0031 5/20/2010 5/20/2010 9214 Btu/lb 2 - M0031 5/20/2010 5/20/2010 9112 Btu/lb 3 - M0031 5/21/2010 5/21/2010 9151 Btu/lb 1 - M10 5/25/2010 5/25/2010 9180 Btu/lb 2 - M10 5/26/2010 5/26/2010 9270 Btu/lb 3 - M10 5/26/2010 5/26/2010 9187 Btu/lb 1 - M0010 5/20/2010 5/20/2010 9171 Btu/lb 2 - M0010 5/21/2010 5/21/2010 9140 Btu/lb 3 - M0010 5/26/2010 5/26/2010 9274 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units 26.12 3.80 0.34 12484 Btu/lb 5.14 0.46 26.42 3.68 0.33 12459 Btu/lb 5.00 0.45 26.57 3.63 0.35 12556 Btu/lb 4.94 0.48 25.94 3.67 0.31 12471 Btu/lb 4.96 0.42 25.99 4.08 0.31 12440 Btu/lb 5.51 0.42 25.8 4.11 0.31 12476 Btu/lb 5.54 0.42 25.95 4.06 0.32 12443 Btu/lb 5.48 0.43 26.08 4.44 0.36 12326 Btu/lb 6.01 0.49 26.28 4.05 0.34 12413 Btu/lb 5.49 0.46 25.78 4.05 0.35 12369 Btu/lb 5.46 0.47 25.69 3.90 0.39 12475 Btu/lb 5.25 0.52 26.07 3.90 0.35 12427 Btu/lb 5.28 0.47 26.04 4.43 0.34 12400 Btu/lb 5.99 0.46 26.14 4.22 0.33 12375 Btu/lb 5.71 0.45 25.29 3.88 0.38 12413 Btu/lb 5.19 0.51Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis)Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel UnitsSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 1943 Hoot Lake Plant 2 Dioxin/furan HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 1 - M23 5/17/2010 5/17/2010 9153.00 Btu/lb 2 - M23 5/18/2010 5/18/2010 9149.00 Btu/lb 3 - M23 5/19/2010 5/19/2010 9158.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units 26.28 4.24 0.28 12416 Btu/lb 5.75 0.38 < 27.1 μg/g 26.31 3.47 0.26 12416 Btu/lb 4.71 0.35 < 27.1 μg/g 26.17 3.87 0.29 12405 Btu/lb 5.24 0.39 < 27.1 μg/gMercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis)Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel UnitsSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units