CLAIRTON MUNICIPAL AUTHORITY 

ALLEGHENY COUNTY, PENNSYLVANIA 

TECHNICAL EVALUATION OF THE IMPACT OF 

OIL AND GAS WELL WASTEWATERS ON THE 

CLAIRTON MUNICIPAL AUTHORITY 

WASTEWATER TREATMENT FACILITY 

NPDES PERMIT No. PA0026824 

FEBRUARY 2009 

KLH· 

ENGINEERS, INC. 

5173 CAMPBELLS RUN ROAD 

PITTSBURGH, PA 15205-9733 
Clairton Municipal Authority 

Technical Evaluation of the Impact of Oil and Gas Well Wastewaters on the 

Clairton Municipal Authority 

Wastewater Treatment Facility 

Table of Contents 

1.0 Purpose .......................................................................................................................................... 1 

2.0 Description ofCMA Treatment Processes .................................................................................... 1 

3.0 Evaluation of Total Dissolved Solids and Chlorides on Process Units ......................................... 3 

4.0 CMA Sludge Treatment and Disposal. .......................................................................................... 6 

5.0 Summary of Conclusions .............................................................................................................. 7 

Tables 

Table 1.0 

Appendices 

Appendix A 

AppendixB 

AppendixC 

AppendixD 

AppendixE 

AppendixF 

Clairton Municipal Authority 

Net Impact ofCMA Effluent on Background Levels of IDS and Chlorides 

Oil and Gas Wastewater Manifest Spreadsheet 

CMA Process Flow Diagram Detailing Sample Locations 

CMA Chloride and TDS Analytical Data 

Table 3-16 "Typical Composition of Untreated Domestic Wastewater," 

Metcalf & Eddy, Third Edition, Wastewater Engineering 

CMA BOD and TSS Inter Process Data and MACM Weekly Operations 

Reports 

Radiological Analysis ofCNX-1 and CNX-3 Wells 

Technical Evaluation of the Impact of Oil and Gas Well 

Wastewaters on the Wastewater Treatment Plant 

February 2009 Ref. No. 273-46 

1 KLH 

ENGINEERS, INC. 
---------------------------------------~ 

1.0 Purpose 

The Pennsylvania Department of Environmental Protection (P ADEP) issued an Administrative 

Order to the Clairton Municipal Authority (CMA) on October 23, 2008. The Adrrtinistrative 

Order sets forth a series of requirements prescribed to CMA, in order for CMA to continue 

acceptance of oil and gas well production wastewater for treatment and processing at the CMA 

Wastewater Treatment Plant (WWTP). The purpose of this document is to provide a written 

technical evaluation of potential impacts of oil and gas production wastewaters on the CMA 

treatment process. This evaluation will contain, as prescribed in the Order; an evaluation of the 

effects on each major unit process; an estimate of the maximum Total Dissolved Solids (IDS) 

that will occur in each process; a description of measures employed by CMA to monitor and 

minimize adverse effects on biological processes; quantitative estimates on anticipated changes 

to effluent characteristics for each new pollutant identified; a description of how CMA will 

assure that the WWTP sludge will not be classified as hazardous waste as a result of accepting 

this new waste stream, and any resulting constraints on sludge treatment and disposaL 

2.0 Description of CMA Treatment Processes 

The CMA WWTP is a conventional activated sludge, secondary wastewater treatment facility. 

The plant has a permitted hydraulically treatment capacity of 6.0 million gallons per day (mgd). 

The CMA 2007 Annual Chapter 94 Waste Load Management Report indicates the annual 

average flow to the WWTP in 2007 was 3.994 mgd. The maximum monthly average day flow 

was 5.46 mgd, occurring in March of 2007, and the minimum monthly average flow was 2.919 

mgd, occurring in October 2007. 

The Order requires CMA to immediately restrict the daily volume of oil and gas well 

production wastewater to 1 % of the average daily flow. To comply with this requirement CMA 

has limited the daily volume of Oil and Gas well production wastewater introduced into the 

WWTP to 1 % of the WWTP's forward flow rate on any given day. 

The CMA receives the oil and gas well production water at the influent manhole just up-stream 

of the influent pumping station. Water is received into the wet well and subsequently 

introduced into the WWTP process via the raw sewage pumps. Trucks discharge typically 

4,000 gallons of waste over a period of approximately ten to fifteen minutes. This translates to 

waste being introduced into the pumping station at a rate of between 267 and 400 gallons per 

minute. The actual volume of waste received is limited and does not exceed 1% of the 

estimated daily flow volume. Typically Clairton will accept up to 37,500 gallons during a one 

day period. 

Clairton Municipal Authority 

Technical Evaluation of the Impact of Oil and Gas Well 

Wastewaters on the Wastewater Treatment Plant 

February 2009 Ref. No. 273-46 

1 KLH 

ENGINEERS, INC. 
CMA monitors each individual waste load received from oil and gas well production 

wastewater sources. Included in this record is the date received at CMA; the hauling company 

transporting the waste to CMA; the manifest number identifying the load received at CMA; the 

well or point source from which the wastewater was generated; and the quantity of the 

wastewater received. CMA is currently purchasing testing equipment which will allow plant 

operational personnel to test and monitor the level of chlorides and IDS in the wastewater 

received in (mg/l). Once the testing equipment is obtained and staff trained in its operation 

chloride and IDS levels in each load will be monitored and recorded. The corresponding mass 

load of chlorides and IDS in the wastewater received will be determined and recorded, as well 

as the pH of the wastewater. This data is recorded and stored in a spreadsheet format by CMA 

operation staff. The information contained in this spreadsheet will be filed with the CMA 

monthly discharge monitoring report (DMR) to PADEP as required under the Order. A copy of 

the hauling records and data is contained in Appendix A of this report. 

By CMA monitoring chloride levels in the received wastewaters CMA will have the ability to 

control the quantity, rate and mass of chlorides introduced into the treatment process. This will 

provide CMA's operations staff with a level of control to protect the biological process from 

upset, and control the level of pass through to assure water quality criteria is met. CMA will 

also sample each load and store each sample for a period of five days. This sample will be 

available for complete analysis of all priority pollutants listed in PADEP's Administrative Order 

should any adverse effects be observed within the plant processes. 

CMA employ's Pennsylvania state licensed operators who monitor, regulate and control all 

aspects of the WWTP process twenty four hours a day, seven days per week, fifty two weeks 

per year. The professional training and experience of these state licensed wastewater treatment 

plant operators provides CMA another level of assurance the introduction of oil and gas well 

wastewaters can be conducted, monitored and controlled to achieve the desired water quality 

limits while preserving the biological treatment process, and plant performance. 

The CMA facility is comprised of the following treatment unit process: 

• Mechanical screening 

• Grit removal 

• Comminutor 

• Pre-aeration basins 

• Primary clarifier settling tanks 

• Activated sludge process tanks 

• Final clarifier settling tanks 

• Aerobic digestion 

• Sludge thickening tanks 

• Gravity belt thickener 

• Sludge dewatering (centrifuge) 

• Chlorine disinfection system 

Clairton Municipal Authority 

Technical Evaluation of the Impact of Oil and Gas Well 

Wastewaters on the Wastewater Treatment Plant 

February 2009 Ref. No. 273·46 

2 KLH 

ENGINEERS, INC. 
Oil and gas well production wastewaters received is applied to the raw sewage wet well at a 

rate no greater than 1% of the plants daily forward flow. In the wet well the oil and gas 

production water is combined with domestic raw sewage from Clairton, Jefferson Borough, 

South Park, Finleyville, Nottingham, Peters Township and Union Township. This combined 

waste stream is screened, de-gritted and comminuted prior to discharging into the pre-aeration 

tanks. Primary Settling of the waste stream occurs after pre-aeration. Solids that are removed 

during the primary settling process are sent to the sludge thickening and aerobic digestion 

processes for stabilization of the bio-solids. CMA conducts an annual priority pollutant scan on 

its produced sludge for all Form 43 listed parameters. 

After the primary clarification settling tanks the plants flow enters the activated sludge tanks. 

During this process the plant operators closely monitor control points for Sludge Volume Index 

(SVl), and Food to Micro-organism Ratio (F/M). By monitoring these control points regularly 

the plant operations staff can determine if any adverse effects to settling or treatment capability 

are observed. If any adverse effects were noticed the operating staff would immediately stop 

receiving the oil and gas well wastewater and have the most recent loads received analyzed for 

all priority pollutants listed in the PADEP Administrative Order to determine which load may 

be the source of a potential upset. A biological microscopic evaluation is also completed 

periodically by the operating staff. Samples of activated sludge mixed liquor are collected and 

analyzed under a high powered microscope to determine the overall health of the biological 

system. Any adverse effects noticed during the microscopic evaluation would also trigger 

CMA to stop the receipt of oil and gas production wastewater. 

When the forward flow leaves the activated sludge process it enters the final clarifier settling 

tanks. Here the mixed liquor activated sludge is settled and separated from the liquid stream 

and returned to the activated sludge tanks via the return activated sludge pump system. 

Periodically, as required to maintain the desired sludge age and to maintain proper settling 

characteristics; sludge will be wasted to and aerobic digesters. 

After final settling the treated water is conveyed to the chlorination system where pathogenic 

disinfection via chlorine gas injection is completed. After chlorination the flow is transferred 

into the chlorine contact tanks to provide sufficient contact time for the disinfection process to 

be completed prior to discharge into Peters Creek. CMA's effluent discharges into Peter's Creek 

approximately 2,000 feet from the mouth of Peters Creek where Peters Creek flows into the 

Monongahela River at River Mile Index 19.66. 

3.0 Evaluation of Total Dissolved Solids and Chlorides on Process Units 

CMA began to collect 24 hour flow proportional composite samples to evaluate the levels of 

chlorides and IDS which occur under normal waste load conditions and which occur during 

days which the WWTP is processing oil and gas well wastewater. CMA selected six sampling 

Clairton Municipal Authority 

Technical Evaluation of the Impact of Oil and Gas Well 

Wastewaters on the Wastewater Treatment Plant 

February 2009 Ref. No. 273-46 

3 KLH 

ENGINEERS, INC. 
~~~~~~~---------------~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~-

locations as key areas within the WWTP to monitor IDS and chloride levels. These sampling 

points can be seen on the CMA Process Flow Diagram included in Appendix B, which shows 

the location of each of the six sampling points. A complete listing of the sample results for IDS 

and chlorides at all six sampling locations is contained in Appendix C of this report. 

The first sampling location monitored by CMA is the influent sampling point. The purpose of 

collecting the influent sample is to provide CMA with the typical level of IDS and chlorides 

which occur in CMA's influent, with contributions from oil and gas well wastewater and 

domestic sewage prior to the waste stream entering CMA's process tanks. During the week 

long testing the influent test results for both IDS and chlorides were relatively consistent. IDS 

values in the influent ranged from 664 mg/l to 1980 mg/l. These levels of IDS would indicate 

concentrations that would be found in typical strong strength domestic sewage. Chloride levels 

in the influent samples ranged from 183 mg/l to 843 mg/l. Chloride levels of 100 mg/l are 

considered to be a strong concentration in untreated domestic sewage, according to Table 3-16, 

of Metcalf and Eddy. Third Edition. Wastewater Engineering. Table 3-16 is included in 

Appendix D of this report. 

Grab samples were also taken and analyzed for oil and gas well wastewaters received at CMA 

from the two well sources, CNX-1 and CNX-3. The analysis of CNX-1 and CNX-3 waste waters, 

as required under the Administrative Order, are also included in Appendix A. 

The results of the samples taken and analyzed through the CMA WWTP indicate that there is 

little to no reduction in concentration of IDS and chlorides through the plant processes. This is 

not unexpected as conventional sewage treatment facilities are not designed to remove 

dissolved constituents such as IDS and chlorides. 

Although there is no apparent reduction in IDS or chloride concentrations through the 

treatment process, the introduction of oil and gas well wastewaters has had no effect on the 

treatment ability of the CMA system to treat and remove conventional pollutants such as 

Biochemical Oxygen Demand (BODs) and Total Suspended Solids (TSS). Appendix E. contains 

effluent data for BODs and TSS through the CMA process during the introduction of oil and gas 

well waste water. The data contained in Appendix E shows the removal of BODs and TSS 

during the December 8, 2008 to December 12, 2008 testing period was consistently observed, 

producing an average effluent CBODs of 8.94 mg/l and an average effluent TSS of 8.36 mg/l. 

These levels of removal exceed the NPDES permit requirements for these pollutants and 

provide a good indication the process is performing well during the introduction of oil and gas 

well wastewater into the process. Microscopic analysis conducted periodically on the activated 

sludge mixed liquor has shown that the biological process has remained healthy and viable 

during the introduction and processing of oil and gas well waste waters. 

To evaluate the potential impacts that the discharge of IDS and chlorides may have on the 

Monongahela River, an evaluation utilizing the same analytical approach CMA would use to 

conduct a Head Works Loading analysis to development Local Limits has been utilized. 

Clairton Municipal Authority 

Technical Evaluation of the Impact of Oil and Gas Well 

Wastewaters on the Wastewater Treatment Plant 

February 2009 Ref. No. 273-46 

4 KLH 

ENGINEERS, INC. 
The following Monongahela River flows were utilized for the purpose of this evaluation: 

Chronic Evaluation: Q7-10 = 350 cfs, or 226 million gallons per day 

Acute Evaluation: Q,-10 = 494 cfs, or 319 million gallons per day 

Human Health: Harmonic Flow = 2860 cfs, or 1,847 million gallons per day 

By utilizing the CMA effluent data collected and analyzed for IDS and chlorides we can 

determine the effective impact these levels have on the Monongahela River during the above 

referenced flow periods. We will analyze the impact of the effluent IDS and chlorides at the 

maximum effluent levels and at the average levels recorded during the one week testing period 

and apply these loads to the various river flows to determine the net effect CMA's effluent has 

on the Monongahela River. 

Average IDS level = 974 mg/l 

Maximum IDS level = 1250 mg/l 

Average Chloride level = 347 mg/l 

Maximum Chloride level = 520 mg/l 

Applying each to the following formula the net effect for each can be determined at the various 

river flows. 

Effluent conc. Cmg/ll x Plant flow rate Cmgdl = Net effect to background level (mg/l) 

Monongahela River Flow Rate (mgd) 

Clairton Municipal Authority 

Technical Evaluation of the Impact of Oil and Gas Well 

Wastewaters on the Wastewater Treatment Plant 

February 2009 Ref. No. 273·46 

5 KLH 

ENGINEERS, INC. 
- - --- -- ----------- -------------

Table 1.0 

Net Impact of CMA Effluent on Background Levels of TDS and Chlorides 

Net Increase in Receiving Water Levels 

Max Avg Max Avg 

IDS IDS Chlorides Chlorides 

(mg/l) (mg/l) (mg/l) (mg/l) 

River 

Flow (mgd) 1250 974 520 347 

Q7-10 226 24.28 18.92 10.10 6.74 

Q,-,O 319 17.20 13.40 7.16 4.78 

Harmonic 1,847 2.97 2.32 1.24 0.83 

Note: Average daily plant flow of 4.39 mgd utilized for calculation 

Table 1.0 clearly shows the resulting increase in levels of IDS and Chlorides attributable to the 

CMA effluent on the Monongahela River during the most critical Q7-10 river flow is very small, 

less than 25 mg/l for IDS, and less than 11 mg/l for chlorides. The monthly average limit for 

potable water supply criteria in source waters for IDS is a monthly average of 500 mg/l and a 

maximum value of 750 mg/l. The net increase in IDS of 25 mg/l under Q7-10 conditions is only 

5% of this limitation and only 3.33% of the maximum allowed. The limit to meet potable water 

supply criteria for chlorides is 250 mg/l in source waters. The net increase from the CMA 

effluent of 11 mg/l under Q7-10 conditions is 4.4% of the limit. 

As a result of the data presented and the analysis conducted it is the opinion of KLH Engineers, 

Inc. that the introduction of oil and gas wastewaters under the conditions prescribed above 

causes no adverse effects to the CMAbiological treatment process and no discernable impact on 

the receiving waters of the Monongahela River. 

4.0 CMA Sludge Treatment and Disposal 

The CMA currently employs two (2) aerobic digesters to digest and stabilize biologically active 

waste solids for its treatment process. Once stabilized the solids are thickened and dewatered 

via a centrifuge. Dry, stabilized cake solids are then hauled to the Waste Management 

(Elizabeth) landfill for final disposal. Annually the CMA conducts a Form 43 analysis to 

maintain its permit with the landfill fro sludge disposal. To determine if the acceptance of oil 

and gas well wastewaters poses any harmful effects to CMA's current method of sludge 

stabilization and treatment a comparison of analytical data prior to the acceptance of oil and gas 

well waste water was and analytical data obtained after the acceptance of oil and gas well 

wastewater was conducted. 

Clairton Municipal Authority 

Technical Evaluation of the Impact of Oil and Gas Well 

Wastewaters on the Wastewater Treatment Plant 

February 2009 Ref. No. 273-46 

6 KLH 

ENGINEERS, INC. 
-----------------------------------------~-

Comparison of sludge data prior to the acceptance of oil and gas well wastewaters and sludge 

data after the acceptance of oil and gas well wastewaters indicates there is little change in the 

consistency, or quality of sludge at CMA. Should levels of any monitored substance in their 

sludge begin to increase to a level which would cause the sludge treatment or disposal practices 

to be come at risk CMA will limit or halt receiving oil and gas well wastewaters contributing to 

this increase. 

CMA sludge is screened for radioactivity at the Waste Management landfill prior to acceptance, 

but because low level, Normally Occurring Radioactive Materials (NORM) are known to be 

present in oil and gas well waste waters in certain areas, CMA has conducted radiological 

analysis of both the CNX-l and CNX-3 source wastewaters received from oil and gas well 

operations for NORM. The results of the radiological testing for CNX-l and CNX-3 oil and gas 

well wastewater, is contained in Appendix F of this report. CMA will continue to rely on the 

landfill monitoring of sludge received for NORM and will halt receipt of such wastes if it is 

determined to contain such materials. In addition, CMA requires that the generator certify that 

the wastewater being received is not classified as hazardous waste. 

By continuing to closely monitor their sludge for metals, PCB's, Herbicides, Pesticides, Volatile, 

Semi-volatile Organics, and NORM, CMA will be able to assure that the current methods 

utilized to treat, stabilize and dispose of their sludge are protected and maintained and that 

their sludge will not be classified as a hazardous waste. 

CMA has also limited oil and gas production water received from any individual source well to 

less than 25,000 gallons per day. 

5.0 Summary of Conclusions 

In conclusion, the current program for the acceptance of oil and gas well wastewater as it is 

currently being conducted at the CMA WWTP provides for both the protection of the CMA 

process, and the protection of the receiving waters of the Monongahela River for its intended 

use, and will not adversely impact the level of Total Dissolved Solids or Chlorides in the 

Monongahela River. CMA has instituted record keeping, quality control and process 

monitoring programs to assure it can sufficiently monitor the treatment plant process, and the 

effluent water quality to meet permit compliance. Monthly monitoring data for chlorides and 

IDS in CMA's effluent has been and will continue to be filed with CMA's monthly Discharge 

Monitoring Report (DMR). 

Clairton Municipal Authority 

Technical Evaluation of the Impact of Oil and Gas Well 

Wastewaters on the Wastewater Treatment Plant 

February 2009 Ref. No. 273-46 

7 KLH 

ENGINEERS, INC. 
ApPENDIX A 

OIL AND GAS WASTEWATER 

MANIFEST SPREADSHEET 
I'· 

J 

I 

MONTH: DECEMBER 

) CMA TRUCK HAULING TOTALS FOR SHIPMANS 

. \,:",:" i:&QUROl=i.t i\ . :MANIFEST4l", .', .... <.:DATE? ;, ~'''/i.:'':· , I.G.ALl.j$N$E' . .. ·%.$6LIDS··.······ : . . ___ "i-,o,,· __ _ ):,.',,'-':-." __ ::,--,'>5~<_ ~ 

dravosburg 9634 12/3/2008 4eee 

dravosburg 9636 12/3/2008 - 4gQg 

port-a-john 9290 12/5/2008 Ge6 

CNX#3 Pitwater 9678 1218/2008 4000 

CNX#3 Pitwater 8823 12/8/2008 4500 

CNX#3 Pitwater 9103 12/8/2008 4000 

CNX#3 Pitwater 9663 12/8/2008 4000 

CNX#3 Pitwater 9638 12/8/2008 4000 

CNX#3 Pitwater 9284 1218/2008 4000 

CNX#3 Pitwater 8824 12/8/2008 4500 

CNX#3 Pitwater 9640 12/8/2008 4000 

CNX#3 Pitwater 9105 12/8/2008 4000 

CNX#3 Pitwater 9106 12/9/2008 4000 

CNX#3 Pitwater 9641 12/9/2008 4000 

CNX#3 Pitwaler 8825 12/9/2008 4500 

port-a john 9696 12/9/2008 356 

CNX#3 Pitwaler 9107 12/9/2008 4000 

C NX#3 Pitwater 9331 12/9/2008 4000 

CNX#3 Pitwater 9643 12/9/2008 4000 

.CNX#3 Pitwater 8828 1219/2008 4500 

);NX#3 Pitwater 8827 1219/2008 4500 

CNX#3 Pitwater 9642 12/9/2008 4000 

CNX#3 Pitwater 9274 12/10/2008 3500 

port-a-john 9273 12110/2008 59Q 

CNX#3 Pitwater 8829 12110/2008 4500 

CNX#3 Pitwater 6944 12/10/2008 4000 

CNX#3 Pitwater 9287 12/10/2008 4000 

CNX#3 Pitwater 9335 12110/2008 4000 

CNX#3 Pitwater 9645 12/10/2008 4000 

dravosburg 9280 12/10/2008 qggO 

ONX#3 Pitwater 9334 12/10/2008 4000 

CNX#3 Pitwater 8830 12/10/2008 4500 

CNX#3 Pitwater 9281 12/11/2008 4000 

CNX#3 Pitwater 8831 12/11/2008 4500 

CNX#3 Pitwater 9370 12/11/2008 4000 

CNX#3 Pitwater 9647 12111/2008 4000 

CNX#3 Pitwater 9332 1211112008 4000 

CNX#3 Pitwater 9371 12/11/2008 4000 

CNX#3 Pitwater 9226 12111/2008 4000 

CNX#3 Pitwater 9404 12/11/2008 4000 

CNX#3 Pitwater 8833 12/11/2008 4500 

CNX#3 Pitwater 9224 12-Dec 4000 

CNX#3 Pitwater 9407 12/12/2008 4000 

CNX#3 Pitwater 9374 12/1212008 4000 

"-NX#3 Pitwater 9337 12/12/2008 4000 

~X#3 Pitwater 9409 12113/2008 4000 
CNX#3 Pitwater 9263 12/1312008 4000 

CNX#3 Pitwater 9376 1211312008 4000 

CNX#3 Pitwater 9341 12/1312008 4000 

CNX#3 Pitwater 9340 12113/2008 4500 

CNX#3 Pitwater 9431 12/1512008 4500 

CNX#3 Pitwater 9346 12/1512008 4000 

CNX#3 Pitwater 9271 12/1512008 4000 

CNX#3 Pitwater 9383 12/1512008 4000 

CNX#3 Pitwater 9345 12/1512008 4000 

CNX#3 Pitwater 9272 12/1512008 4000 

CNX#3 Pitwater 9430 1211512008 4500 

CNX#3 Pitwater 9384 12/1512008 4000 

port-a john 9447 12/1612008 -- 3~e 

CNX#3 Pitwater 9446 12/1612008 3700 

CNX#3 Pitwater 9386 12116/2008 4000 

CNX#3 Pitwater 9351 12/1612008 4000 

CNX#3 Pitwater 9680 12/16/2008 4000 

CNX#3 Pitwater 9434 12/16/2008 4500 

CNX#3 Pitwater 9435 12/1612008 4500 

CNX#3 Pitwater 9350 12/1612008 4000 

CNX#3 Pitwater 9388 12116/2008 4000 

CNX#3 Pitwater 9441 1211712008 4500 

CNX#3 Pitwater 9356 1211712008 4000 

CNX#3 Pitwater 9440 12117/2008 4500 

<::NX#3 Pitwater 9355 12/17/2008 4000 

':':NX#3 Pitwater 9354 12/17/2008 4000 

CNX#3 Pitwater 9439 12/17/2008 4500 

CNX#3 Pitwater 9353 12117/2008 4000 

CNX#3 Pitwater 9438 1211712008 4500 

CNX#3 Pitwater 9449 12117/2008 4000 

port-a-john 9505 12118/2008 see 

CNX#3 Pitwater 9357 . 12/18/2008 4000 

CNX#3 Pitwater 9506 12/1812008 4000 

CNX#1 Pitwater 9475 12/18/2008 4000 

GNX#1 Pitwater 9474 12/18/2008 4000 

CNX#1 Pitwater 9511 12/18/2008 4500 

CNX#1 Pitwater 9359 12/18/2008 4000 

CNX#1 Pitwater 9509 12/1812008 4500 

CNX#1 Pitwater 9508 12/18/2008 4500 

CNX#1 Pitwater 9358 12/18/2008 4000 

CNX#1 Pitwater ,9520 12/19/2008 4500 

CNX#1 Pitwater '9477 12119/2008 4000 

CNX#1 Pitwater 9476 12/19/2008 4000 

CNX#1 Pitwater 9519 12/1912008 4500 

port a-john 9293 12/19/2008 388 

CNX#1 Pitwater 9478 12/19/2008 4000 

CNX#1 Pitwater 9521 12/19/2008 4500 

CNX#1 Pitwater 9468 12/19/2008 4000 

CNX#1 Pitwater 9463 12/19/2008 4000 

\jX#1 Pitwater 9455 12119/2008 4000 

I~NX#3 Pitwater 9479 12120/2008 4000 

\CNX#3 Pitwater 9457 12/20/2008 4000 
CNX#3 Pitwater 9522 12120/2008 4500 

CNX#1 Pitwater 9393 12/20/2008 4000 

CNX#1 Pitwater 9480 12120/2008 4000 

CNX#1 Pitwater 9531 12/20/2008 4500 

CNX#1 Pitwater 9394 12120/2008 4000 

CNX#1 Pitwater 9532 12/20/2008 4500 

CNX#1 Pitwater 9481 12/20/2008 4000 

CNX#1 Pitwater . 9533 12/22/2008 4500 

CNX#1 Pitwater 9482 12/2212008 4000 

CNX#1 Pitwater 9534 12/22/2008 4500 

CNX#1 Pitwater 9483 12/22/2008 4000 

cNX#1 Pitwater 9484 12/22/2008 4000 

CNX#1 Pitwater 9535 12/22/2008 4500 

CNX#1 Pitwater 9485 12/22/2008 4000 

CNX#1 Pitwater 9536 12/22/2008 4500 

Zinkan Enterprise 9486 12123/2008 1008 

CNX # 1 Pitwater 9537 12/23/2008 4500 -- CNX#1 Pitwater 9487 12/23/2008 3000 

CNX#l Pitwater 9538 12/23/2008 4500 

dravosburg 9488 12/23/2008 4008 

- CNX#1 Pitwater 9489 12/23/2008 4000 

CNX#1 Pitwater 9539 12/23/2008 4500 

CNX#1 Pitwater 9523 12123/2008 4500 

CNX#1 Pitwater 9490 12/23/2008 4000 

~NX#1 Pitwater 9491 12/23/2008 4000 

CNX#1 Pitwater 9524 12/23/2008 4500 

CNX#1 Pitwater 9462 12/24/2008 4000 

CNX#1 Pitwater 9495 12124/2008 4000 

CNX#1 Pitwater 9526 12/24/2008 4500 

CNX#l Pitwater 9496 12/24/2008 4000 

CNX#1 Pitwater 9461 12124/2008 4000 

CNX#l Pitwater 9527 12/24/2008 4500 

CNX#1 Pitwater 9497 12124/2008 4000 

CNX#3 Pitwater 9225 12/1212008 4000 

CNX#3 Pitwater 9408 12112/2008 4000 

CNX#3 Pitwater 9375 12/1212008 4000 

CNX#3 Pitwater 9339 12/12/2008 4000 

port-a-john 9292 12/12/2008 -z68 

port a-john 9291 12/12/2008 200 

CNX#1 Pitwater 9512 12/26/2008 4500 

CNX#l Pitwater 9501 12126/2008 . 4000 

CNX#1 Pitwater 9396 12126/2008 4000 

CNX#1 Pitwater 9502 12126/2008 4000 

CNX#1 Pitwater 9504 12/26/2008 4000 

CNX#l Pitwater 9513 12/26/2008 4500 

CNX#1 Pitwater 9503 12/26/2008 4000 

CNX#l Pitwater 9397 12/26/2008 4000 

CNX#1 Pitwater 9515 12/27/2008 4500 

CNX#1 Pitwater 9401 12127/2008 4000 

\lX#1 Pitwater 9516 12127/2008 4500 

,~NX#1 Pitwater 9399 12/27/2008 4000 

ICNX#l Pitwater 9563 12/27/2008 4000 
'itwaler 9514 12127/2008 4500 

'itwaler 9562 12/27/2008 4000 

'itwater 9561 12/27/2008 4000 

'itwaler 9400 12127/2008 4000 

'itwaler 9560 12/29/2008 4000 

'itwaler 9559 12129/2008 4000 

'itwaler 9402 12/29/2008 4000 

'itwaler 9564 12/29/2008 4500 

'itwaler 9565 29-Dec 4500 

'itwaler 9566 12129/2008 4500 

'itwaler 9540 12/29/2008 4000 

'itwaler 9403 12/29/2008 4000 

'itwaler 9558 12/29/2008 4000 

'itwaler 9542 12/30/2008 4000 

'itwaler 9416 12/30/2008 4000 

'itwaler 9567 12/30/2008 4500 

'itwaler 9557 12/30/2008 4000 

itwaler 9458 12/30/2008 4000 

itwaler 9541 12/30/2008 4000 

itwaler 9556 12/30/2008 4000 

itwaler 9568 12/30/2008 4500 

itwaler 9459 12/30/2008 4000 

I 9588 12/30/2008 -.289 

itwaler 9552 12/31/2008 4000 

itwaler 9555 12131/2008 ' 4000 

itwaler 9570 12131/2008 4500 

itwaler 9571 12131/2008 4500 

itwaler 9460 12/31/2008 4000 

itwaler 9551 12/31/2008 , 4000 

itwaler 9543 12131/2008 4000 

itwaler 9418 12131/2008 4000 

itwaler 9569 12/31/2008 4500 
® Microbac Laboratories, Inc. Page 1 of2 

100 MARSHALL DRIVE 

WARRENDALE, PA 15086 

(724) 772-0610 FAX (724) 772-I 686 

TOM ZlERENBERG, MANAGING DIRECTOR 

http://www.microbac.com 

State Laboratory Certification Numbers: 

PADEP: 02-257, NC: 42703. WVDEP: 215,9951 CM KY: 90136 

C1iliMl~TK¥ . MlCKutIlULUV¥ . rUUU ~A.t<bT¥· CUN~UMbK.PKUUUCT~ 

WATbK· Alli.. WA~ThS . FOOD· .PHARMACbUTlCALS . NUTKACbUTlCALS 

CLAIRTON MUNICIPAL AUTHORITY 

MR. PATRICK CANAVAN 

I NORTH STATE STREET 

CLAIRTON, PA 15025 

Permjt No.: 

CustP.O.: 

SUBJECT: \Vastewater Sample fOT Analysis 

CERTIFICATE OF ANALYSIS 

Date Reported: 

Date Received: 

Order Number: 

Invoice No.: 

Cust#: 

Sample Date: 

Sample Time: 

Sampler/Temp: 

1/13/2009 

12/19/2008 

0812-01476 

38389 

CI23 

12/1912008 

11:25 

TEST METHOD UNITS DATE TECH 

Acidity (as CaC03) EPA 305.1 <1 mg/L 12/31/0B SFS 

Alkalinity (as CaC03) SM20 2320 341 mgjL 12/31/0B SFS 

Arr , ia, Distilled SM20 4500-NH3 B/D 29.4 mg/L 01/05/09 RDP 

BGe SM20 5210B 781 mg/L 12/19/0B SFS 

COD SM20 5220D 2,390 mg/L 12/31/0B RDP 

ChlOride EPA 325.2 44,700 mg/L 12/23/0B NAH 

Conductivity EPA 120.1 102,000 umhos/an 12/30/0B LLS 

Hardness by Calculation SM192340B 12,600 mgcaC03/L 12/30/08 LLS 

Nitrate-Nitrite as Nitrogen EPA 353.2 <0.10 mg/L 12/29/08 NAH 

Oil & Grease EPA 1664A 43 mg/L 12/30/08 ADS 

Osmolality Cyroscope 2,400 mOsm/kg 12/23/08 *-. pH EPA 150.1 6.0 su 12/31/08 SFS 

Phendl1cs EPA 420.2 MOD 0.05 mg/L 12/31/0B NAH 

Sulfate EPA 375.4 53 mg/L 01/03/09 SFS 

;urfactants SM20 5540C 11.1 mg/L 12/19/0B NAH 

rotal Dissolved Solids EPA 160.1 76,000 mg/L 12/22/0B ADS 

rotal KjeJdahl Nitrogen SM20 4500-Norg-B + NH3-D S2.5 mg/L 01/07/09 RDP 

lotal Suspended Solids EPA 160.2 1,600 mg/L 12/23/0B ADS ~rsenjc EPA 200.7 <0.10 mg/L 12/22/0S LLS ~arium EPA 200.7 294 mg/L 12/30/0B LLS 

'eryllium EPA 200.7 <0.005 mg/L 12/22/08 LLS 

;oron EPA 200.7 0.71 mg/L 12/22/08 LLS 

:admium EPA 200.7 <0.005 mg/L 12/22/08 LLS 

:alcium EPA 200.7 3,060 mg/L 12/30/0S LLS 

hromium EPA 200.7 0.02 mg/L 12/22/0S LLS 

Dbalt EPA 200.7 <0.01 mg/L 12/22/08 LLS 

opper EPA 200.7 0.11 mg/L 12/22/0S LLS un EPA 200.7 20.S mg/L 12/22/0S LLS 

on,,.. 11ved EPA 200.7 1.20 mg/L 12/22/0S LLS ~ad EPA 200.7 <0.10 mg/L 12/22/08 LLS 

thlum EPA 200.7 0.13 mg/L 01/0S/09 CMG 

agnesium EPA 200.7 1,210 mg/L 12/30/0S LLS 

The data and information on this, and other accompanying documents, represent only the samplers) analyzed and is rendered upon condition MEMBER 

that it is not to be reproduced wnolly or In part for advertising or other purposes without approval From the laboratory. 911 USDA~EPA-NIOSH Testing Food Sanitation Consulting Dlemic:al and Microblo!ogical Analyses and Research 
Microbac Laboratories, Inc. 

100 MARSHALL DRIVE 

WARRENDALE, PA 15086 

Page 2 of2 

(724) 772-0610 FAX (724) 772-1686 

TOM ZIERENBERG, MANAGrnG DlRECTOR 

http) /www.microbac.com 

State Laboratory Certification Numbers: 

PADEP: 02-257, NC: 42703, WVDEP: 215,9951 CM KY: 90136 

UiliMl~TKY . MlCKUtHULUUY . YUUJJ ~Aj'bTY . CUN~UMJjKl'KUJJUCT~ 

WATER' Alli. . WASTES' l'uuD . P HARMACbUl1CALS . N UTKACbUl1CALS 

CLAIRTON MUNICIPAL AUTHORITY 

MR. PATRlCK CANA VAN 

1 NORTH STATE STREET 

CLAIRTON, PA 15025 

PemlitNo.: 

CERTIFICATE OF ANALYSIS 

Date Reported: 

Date Received: 

Order Number: 

Invoice No.: 

Cust#: 

Sample Date: 

Sample Time: 

Cust P.O.: Sampler/Temp: 

SUBJECT: Vlastewater Sample for Analysis 

1113/2009 

12119/2008 

0812-01476 

38389 

Cl23 

12/1912008 

11:25 

TEST METHOD RESULT UNTTS DATE TECH 

v EPA 245.1 0.0003 mg/L 12/23/0B 

Nil EPA 200.7 <0.01 mg/L 12/22/08 

Selenium EPA 200.7 <0.10 mg/L 12/22/0B 

Sodium EPA 200.7 B4,500 mg/L 01/02/09 

Strontium EPA 200.7 176 mg/L 01/0B/09 

Zinc EPA 200.7 0.53 mg/L 12/22/oB 

Glycols SW-846 801S6 01/07/09 

Ethylene Glycol <50 mg/L 01/07/09 

Total Volatiles EPA 624 12/22/0B 

Benzene <5 ug/L 12/22/08 

Tolue!le S ug/L 12/22/0B 

AlUminum EPA 200.7 5.19 mg/L 12/22/08 

Silver EPA 200.7 <0.01 mg/L 12/22/0B 

BOD Analysis TIme lS:0o Hrs. 12/19/oB 

***Osmolality analysis performed by Microbac Laboratories, Inc. - Erie Division. 

>ubmitted By: 

om Zierenberg : 

Managing. Directo"r 

The data and Information on this, and other accompanyIng documents, represent only the sample{s) analyzed and is rendered upon condition 

that it is not to be reproduced wholly or In part for advertising or other purposes without approval from the laboratory. 

USDA~EPA-NIOSH Testlng Food Sanil.ction Consulting O1emical and MicrobIological Analyses and Research 

LLS 

LLS 

LLS 

LLS 

CMG 

LLS 

MSM 

MSM 

LAM 

LAM 

LAM 

LLS 

LLS 

SFS 

MEMBER 

~~II 
.M1crobac Laboratones, lnc. 

100 MARSHALL DRIVE 

WARRENDALE, PA 15086 

rage lOlL 

(724) 772-0610 PAX (724) 772-1686 

TOM ZIERENBERG, MANAGmG DIRECTOR 

http://www.microbac.com 

State Laboratory Certification Numbers: 

PADEP: 02-257, NC: 42703, WVDEP: 215,9951 CM KY: 90136 

CHbMl~TKY . MlCKU1HULU(jY . !<'UUJJ ::;AYcTY' CU.N::;UMCKPKUJJUCT::; 

WATER' AIR· WASTcS . !<'UOD . PHAKlVlACEUTlCALS' NUTKACEUTlCALS 

CLAIRTON MUNIClPAL AUTHORITY 

MR. PATRICK CANAVAN 

I NORTH STATE STREET 

CLAIRTON, PA 15025 

PemJitNo.: 

Cust P.O.: 

SUBJECT: Wastewater SampJe for Analysis 

CERTIFICATE OF ANALYSIS 

Date Reported: 

Date Received: 

Order Number: 

Invoice No.: 

CllSt #: 

Sample Date: 

Sample Time: 

Sampler/Temp: 

12/23/2008 

12/912008 

0812-00532 

37371 

C123 

12/8/2008 

9:30 

TEST METHOD RESULT UNITS DATE TECH 

001 CNX-3 PitvvateJ".··· 

. Collected 12/8/08 

Acidity (as CaC03) 

Alkalinity (as CaC03) 

Ammonia, Distilled 

8oD5 

Cr 

C Je 

Conductivity 

Hardness by Calculation 

Nitrate-Nitrite as Nitrogen 

Oil & Grease 

Osmolality 

pH 

Phenolics 

Sulfate 

Surtactants 

Total Dissolved Solids 

Total Kjeldahl Nitrogen 

Total Suspended Solids 

o,rsenic 

3arium 

3eryllium 

30ron 

:admium 

:alcium 

:hrorilium 

:obalt 

:opper 

ron 

ronl Dissolved 

.ead 

itt 

lS9,·_.:.lum 

EPA 305.1 

SM20 2320 

SM20 4S00-NH3 8/D 

SM20 S2108 

SM20 S220D 

EPA 32S.2 

EPA 120.1 

SM1923408 

EPA 353.2 

EPA 1664A 

Cyroscope 

EPA 150.1 

EPA 420.2 MDD 

EPA 375.4 

5M20 5540C 

EPA 160.1 

SM20 4S00-Norg-8 + NH3-D 

EPA 160..2 

EPA 200.7 

EPA 200.7 

EPA 200.7 

EPA 200.7 

EPA 200.7 

EPA 200.7 

EPA 200.7 

EPA 200.7 

EPA 200.7 

EPA 200.7 

EPA 200.7 

EPA 200.7 

EPA 200.7 

EPA 200.7 

<1 mg/L 12/16/08 

2,100 mg/L 12/16/08 

0.93 mg/L 12/12/08 

29 mg/L 12/09/08 

7Z mg/L 12/1S/08 

534 mgjL 12/23/08 

3,440 umhos/em 12/15/08 

2,870 mg caC03/L 12/13/08 

0.32 mg/L 12/19/08 

<5 mg/L 12/16/08 

36 mDsm/kg 12/11/08 

11.9 su 12/12/08 

<0.010 mg/L 12/17/08 

73 mg/L 12/22/08 

12.6 mg/L 12/10/08 

1,350 mg/L 12/12/08 

8.42 mg/L 12/12/08 

8,110 mg/L 12/12/08 

<0.10 mg/L 12/11/08 

7.76 mg/l 12/13/08 

0.009 mg/L 12/11/08 

<0.10 mg/L 12/11/08 

<0.005 mg/L 12/11/08 

1,020 mg/L 12/13/08 

0.S4 mg/L 12/11/08 

0.07 mg/L 12/11/08 

0.64 mg/L 12/11/08 

211 mg/L 12/13/08 

0.02 mg/L 12/11/08 

0.24 mg/l 12/11/08 

. 0.17 mg/L 12/12/08 

83.3 mg/L 12/11/08 

The data and Inforrnatlon on this, and other accompanying dOaJments, represent only the sample{s) analyzed and Is rendered upon condition 

that It is not to be reproduced wholly or In IBrt for advertising or other.purposes without approval from the laboratory. 

USDA~EPA-NIOSH Testing Food Sanitation Consultlng Dlemical and Microbiological Analyses and Re5"...arch 

MEMBER 

SPS 

SPS 

RDP 

SFS 

RDP 

NAB 

LLS 

CMC 

NAB 

ADS 

*** 

SPS 

NAB 

SPS 

NAB 

ADS 

RDP 

LLS 

CMC 

CMC 

CMC 

CMC 

CMC 

CMC 

CMC 

CMC 

CMC 

CMC 

CMC 

CMC 

CMC 

CMC 

r:.~I. 
- ----- ----------------

:M:icrobac Laboratories, Inc. 

100 MARSHALL DRIVE 

WARRENDALE, PA 15086 

Page 2 of2 

(724) 772-0610 FAX (724) 772-1686 

TOM ZIERENBERG, MANAGrnG DIRECTOR 

http://www.rnicrobac.com 

State Laboratory Certification Numbers: 

PADEP: 02-257, NC: 42703, WVDEP: 215,9951 CM KY: 90136 

CHJ::;MlSTKY . MlCKUl:HULUliY . YUUlJ SAYbTY . CUNSUMEKI'KUlJUCTS 

WATbK' ALK· WASTbS . 1'OOlJ· I'HAKMACEUI1CALS' NUTKACbUT1CALS 

CLAIRTON MUN1CIP AL AUTHORlTY 

MR. PATRlCK CANAVAN 

I NORTH STATE STREET 

CLAIRTON, PA 15025 

Penllit No.: 

Cust P.O.: 

SUBJECT: Wastewater Sample for Analysis 

CERTIFICATE OF ANALYSIS 

Date Reported: 

Date Received: 

Order NllIDber: 

Invoice No.: 

Cust#: 

Sample Date: 

Sample Time: 

Sampler/Temp: 

12/2312008 

12/912008 

0812-00532 

37371 

CI23 

12/8/2008 

9:30 

TEST METHOD RESULT umTS DATE TECH 

001 CNX -3 Pitvvate(-· 

Collected 12/8/08 

Manganese 

Mercury 

Nick.:>1 

S( m 

SodIum 

Strontium 

Zinc 

Glycols 

Ethylene Glycol 

Total Volatiles 

Benzene 

Toluene 

Aluminum 

Silver 

BOD Analysis lime 

EPA 200.7 

EPA 245.1 

EPA 200.7 

EPA 200.7 

EPA 200.7 

EPA 200.7 

EPA 200.7 

5W-845 80158 

EPA 524 

EPA 200.7 

EPA 200.7 

"'**Osmolality analysis performed by Microbac Laboratories, Inc. - Erie Division. 

;ubrn.itted By: 

7.20 mg/L 12/13/08 

0.0011 mg/L 12/15108 

0.25 mg/L 12/11/08 

<0.10 mg/L 12/11/08 

284 mg/L 12/13/08 

4.98 mg/L 12/12/08 

1.82 mg/L 12/11/08 

12/12/08 

23 mg/L 12/12/08 

12/12/08 

<5 ug/L 12/12/08 

<5 ug/L 12/12/08 

150 mg/L 12/13/08 

<0.01 mg/L 12/11/08 

15:00 Hrs. 12/09/08 

The data and information on thIs, and other accompanying dorumenls, represent only the sample(s) analyzed and is rendered upon condition 

that it is not to be reproduced wholly or In part for advertising or other purposes without approval from the laboratory. 

USDA-EPA-NIOSH Testing Food Sanitation Consulting Chemical and Microbiological Analyses and Researd1 

CMC 

LLS 

CMC 

CMC 

CMC 

CMC 

CMC 

MSM 

MSM 

LAM 

LAM 

LAM 

CMC 

CMC 

SFS 

MEMBER 

~~II 
----------------------~ 

ApPENDIX B 

CMA PROCESS FLOW DIAGRAM 

DETAILING SAMPLE LOCATIONS 
........ _

_. __ ._- ----------~ 

AERATION TANKS---, 

PRIMARY SETTLING 

TANKS 

PRE-AERATION \ 

TANKS SAMPLING] SAMPLING. 7' STATION STATION !~"''-

SAMPLlNG~, STATION' ,..~-----. 

COARSE 

SCREEN 

BAR\l' 

ill 

!. 1 [~ . 

l~~ 1 : ~ ]t~ 1 

, 

RETURN ACTIVATED 

SLUDGE 

~,,...,---

/~,----.l---,~'-l--e\+ .... /1'-, __ ; __ ---' 

_--i-_---I 

! I 4=--

! r - - --- - - - -'-- - - --- - JjL - - J \+-' ---' ,I, -4-....J.....J r-- _ --j BY-PASS ,1,_' 1'---'r 

FINAL SETTLING \ 

TANKS \ 

SAMPLING r---:-::=~~-' 

SCREW 

PUMPS 

,_1_; 1 i 1 ...., 1 

\ ' 1 L-~-l----r-----~- I COMMINUTORS L - - __ - - ....rf'-- - - - __ - -1- - -. 

1 WASTE SLUDGE I BY-PASS 1 d RETURN 

1 AND SCUM 0 THICKENING 1 ACTIVATED \'------..,-----'---------

~: 14" F.M. t TANK l __ Sl.UDGE _____ __ ~SAMPLlNG 

>! 1 ! BY-PASS i STATION 

-' ,-'! 11:11 Y -, '-. 

rI

' ----j OLD = J -- I 

AERATED --,-tl I 1 i ~ I 

GRIT " I ~! ~MBER L-~iF. ~ 1 ~i 

PUMP 

STATION 

MECHANICAL 

BAR 

SCREEN 

, 1 Q:: i 

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.,., , 

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PUMP 

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SCREEN 

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SUP"ERNATANT SLUDGE 

. HOLDING 

! I TANK 

- . 

~GRA"TYBELT 

15'" 

,,' CENTRATE ~THICKENER --,,;----C----'-==~==-j 

! CENTRIFUGE --_._+ 

t 

'-----36'· INTERCEPTOR SOLiDS TO DISPOSAL 

- - '--

- - -- -

CHLORINE 

CONTACT 

TANKS 

____ WASTEWATER 

____ BYPASS 

- - - WASTE SLUDGE 

- , ,,- RETURN 

ACTIVATED 

SLUDGE 

.. 

• 

'" 

• 

" 

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, 

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ill 

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_11.1 

Sheet No. 

xx of XX 

Drawing No. 

Ii'IG26 
KLH 

ENGINEERS~ INC. 

51 '73 c ... M .. aE:L'-S RUN R", ... ", 

p,.,.,. .... U,. .. H, pA 15Z05 

""ONE:,412-4"'4-1:1"'0 

FAx, 412-494-0425 

'NI'Q@><LHEONGINEERS.",QM 

ALLEGHENY COUI.,y, ?ENI,SYLVANIA 

"NPDES PERMIT # PA 0026824" 

LOCA TIOI, I~AP 

Drawing No. 
---------- ---------------------

ApPENDIXC 

CMA CHLORIDE AND TDS 

ANALYTICAL DATA 
Clairton Municipal Authority 

Interprocess Testing Data 

Total Dissolved Solids, Chlorides, and FOG 

Date 

12/8/2008 

12/9/2008 

12/10/2008 

12/11/2008 

12/12/2008 

Average 

Maximum 

Minimum 

Date 

1218/2008 

12/9/2008 

12/10/2008 

12/11/2008 

12/12/2008 

Average 

Maximum 

Minimum 

Date 

12/8/2008 

12/9/2008 

12/10/2008 

12/11/2008 

12/12/2008 

Average 

Maximum 

Minimum 

Date 

12/8/2008 

12/9/2008 

12/10/2008 

12/11/2008 

12/12/2008 

Average 

Maximum 

Minimum 

Flow 

(MGD) 

3.08 

3.04 

4.97 

5.21 

5.67 

4.39 

5.67 

3.04 

Flow 

(MGD) 

3.08 

3.04 

4.97 

5.21 

5.67 

4.39 

5.67 

3.04 

Flow 

(MGD) 

3.08 

3.04 

4.97 

5.21 

5.67 

4.39 

5.67 

3.04 

Flow 

(MGD) 

3.08 

3.04 

4.97 

5.21 

5.67 

4.39 

5.67 

3.04 

Chlorides 

(mg/l) 

386 

843 

221 

183 

268 

380 

843 

183 

Chlorides 

(mg/l) 

575 

419 

330 

364 

381 

414 

575 

330 

Chlorides 

(mg/l) 

276 

413 

411 

353 

408 

372 

413 

276 

Chlorides 

(mg/l) 

286 

397 

518 

351 

331 

377 

518 

286 

TDS 

(mg/l) 

1080 

1980 

708 

664 

794 

1045 

1980 

664 

TDS 

(mg/l) 

1360 

1140 

876 

942 

952 

1054 

1360 

876 

TDS 

(mg/l) 

898 

1190 

1020 

946 

1020 

1015 

1190 

898 

TDS 

(mglJ) 

904 

1100 

1210 

932 

820 

993 

1210 

820 

Location #1 

FOG 

(mgll) 

12 

10 

14 

7 

4 

9 

14 

4 

Chlorides 

(lbs/day) 

9915 

21373 

9160 

7952 

12673 

12215 

21373 

7952 

Location #2 

FOG 

(mg/l) 

10 

11 

14 

7 

4 

9 

14 

4 

Chlorides 

(Ibs/day) 

14770 

10623 

13678 

15816 

18017 

14581 

18017 

10623 

Location #3 

FOG 

(mg/l) 

10 

9 

7 

5 

4 

7 

10 

4 

Chlorides 

(lbs/day) 

7090 

10471 

17036 

15338 

19293 

13846 

19293 

7090 

Location #4 

FOG 

(mg/l) 

17 

16 

16 

16 

16 

16 

17 

16 

Chlorides 

(lbs/day) 

7347 

10065 

21471 

15251 

15652 

13957 

21471 

7347 

----~------~----------------

TDS 

(Ibs/day) 

27742 

50200 

29346 

28852 

37547 

34737 

50200 

27742 

TDS 

(Ibs/day) 

34935 

28903 

36310 

40931 

45018 

37219 

45018 

28903 

TDS 

(Ibs/day) 

23067 

30171 

42279 

41105 

48234 

36971 

48234 

23067 

TDS 

(Ibs/day) 

23221 

27889 

50154 

40497 

38776 

36107 

50154 

23221 

FOG 

(Ibs/day) 

308 

254 

580 

304 

189 

327 

580 

189 

FOG 

(Ibs/day) 

257 

279 

580 

304 

189 

322 

580 

189 

FOG 

(Ibs/day) 

257 

228 

290 

217 

189 

236 

290 

189 

FOG 

(Ibs/day) 

437 

406 

663 

695 

757 

591 

757 

406 
bate 

12/8/2008 

12/9/2008 

12/10/2008 

12/11/2008 

12/12/2008 

Average 

Maximum 

Minimum 

Date 

1218/2008 

12/9/2008 

12/10/2008 

12/11/2008 

12/12/2008 

Average 

Maximum 

Minimum 

Flow 

(MGD) 

3.08 

3.04 

4.97 

5.21 

5.67 

4.39 

5.67 

3.04 

Flow 

(MGD) 

3.08 

3.04 

4.97 

5.21 

5.67 

4.39 

5.67· 

3.04 

Chlorides 

(mg/l) 

234 

351 

478 

335 

293 

338 

478 

234 

Chlorides 

(mg/l) 

227 

359 

520 

329 

300 

347 

520 

227 

TDS 

(mg/l) 

862 

1060 

1190 

954 

804 

974 

1190 

804 

TDS 

(mg/l) 

844 

1050 

1250 

948 

780 

974 

1250 

780 

Location #5 

FOG 

(mg/l) 

4 

4 

4 

4 

4 

4 

4 

4 

Chlorides 

(Ibs/day) 

6011 

8899 

19813 

14556 

13855 

12627 

19813 

6011 

Location #6 

FOG 

(mg/l) 

4 

4 

4 

4 

4 

4 

4 

4 

Chlorides 

(lbs/day) 

5831 

9102 

21554 

14296 

14186 

12994 

21554 

5831 

TDS 

(Ibs/day) 

22142 

26875 

49325 

41453 

38019 

35563 

49325 

22142 

TDS 

(Ibs/day) 

21680 . 

26621 

51812 

41192 

36884 

35638 

51812 

21680 

FOG 

(lbs/d§Yl 

103 

101 

166 

174 

189 

147 

189 

101 

FOG 

(lbs/day) 

103 

101 

166 

174 

189 

147 

189 

101 
JAN-05~2009 MON 09:47 PM CLAIRTON MUNICIPAL AUT 

®Microbac Laboratories, Inc. 

100 MARSHALL DRIVE 

WARRENDALE, PA 15086 

(724) 772~061O FAX (724) 772-1686 

TOM ZIERENBERG, MANAGING DIRECTOR 

http://''''''''''_rnicxobac_com 

P, 002 

MEMBER 

- INVOICE 

Page 1 of I 

No. 36964 

i(·;~+;~~~·l~?i~;;.!~ifr; :';::~t}~;.~~]~;~~~~J.~:~;m;~;·~w:~:::~tj ::,·;:~1'itt~~;·: ~':' ;':'~;'~. j,~.(:.~::: ! 

CUilRTON MUNlClPAL AUTHORlTY 

MR, PATRICK CANAVAN 

Day 1 • Wastewater Samples for Analysis 

1 NORTH STATE STREET 

CLAlRTON,PA 15025 . 

0812·00543 

. . ~ :. 

NET 30 DAYS 

Day 1 • Wastewater Samples for Analysis 

Please includ.e this Invoice Number and your Client 

Account Number with all remittances 

CHEMISTRY' . FOOD 

WATBR' AIR - WASTES, FOOD - PHARMACEUTICALS - NUTRACEUTICALS 

$264,00 

$264.00 

- $264.00 
JAN-05-2009 MON 09:48 PM CLAIRTON MUNICIPAL AUT 

®Microbac Laboratories, Inc. 

100 MARSHALL DRIVE 

WARRENDALE, PA 15086 

(724) 772-0610 FAX (724) 772-)686 

TOM ZIERENBERG, M. ... NAGING DIRECTOR 

http)/www.microb.c.com 

P, 003 

MEMBER 

~ INVOICE 

Page 1 of] 

No. 36964 

CLAIRTON MUNICIPAL AUTHORITY 

MR. PATRlCK CANAVAN 

Day 1 - Wastewater Samples for Analysis 

1 NORTH STATE STREET 

CLAlRTON,PA 15025 

0812-()0543 

Day 1 - Wastewater Samples for Analysis 

Please include this Invoice Number and your Client 

Account Number with all remittances 

CHEMISTRY' MICROBIOLOGY' FOOD SAFETY· CONSUMER PRODUCTS A .,. <"T""r> TTA ..... 6,0,., T AT '>.'N "T:"TT"" 

$264.00 

Total $264.00 

", . i":,:.i!'· 6. 
JAN-05-2009 MON 09:48 PM CLAIRTON MUNICIPAL AUT P, 004 

® Microbac Laboratories, Inc. Page 1 of2 

100 MARSHALL DRIVE 

WARRENDALE, PA 15086 

(724) 772-0610 FAX (724) 772-1686 

TOM ZIERENBERG, MANAGING DIRECTOR 

http://www.m.icrobac.com 

State Laboratory Certification Numbers: 

PADEP: 02-257, NC: 42703, WVDEP:. 215,9951 CM KY: 90136 

C.tJJOMlt;TRY • MlCKUb!VLVUY . t<VVlJ SAl'l:dY· CVNt;UlVJbKJ:'KVlJUCTS 

WATER· A.IR' WAS'lli~· FUOD· J:'HARMACJ:iUTlCALS' NUTRACJ::U'l'JCALS 

CERTIFICATE OF ANAL VSIS 

CLAIRTON MUNICIPAL AUTIlORlTY 

MR..PATlUCK CANAVAN 

Date Reporred: 

Date Received: 

1 NORTH STATE STREET 

CLAIRTON, PA 15025 

Perm.itNo,: 

CustP.O.: 

l 

SUBJECJ': Day 1 - Wastewater Samples fur Analysis 

TEST 

0,1 

all &\;Irea:se 

Total Dissolved Solids 

ChlorIde 

Oil &. Grease 

Total D!ssolved Solids 

);1 & Grease 

rotal Dissolved Solids 

:hloride 

iii & Grease 

'ota' Jived Solids 

METHOD 

EPA 3252 

EPA 1664A 

EPA 160.1 

EPA 325,2 

EPA 1664A 

EPA 160.1 

EPA 1664A 

EPA 160.1 

EPA 325.2 

EPA 1664A 

EPA 150.1 

RESULT 

386 

12 

1,080 

575 

10 

1,360 

10 

898 

26B 

17 

904 

Order Number: 

Invoice No.: 

Cust#: 

Sample Date: 

Sample Time: 

Sampler/Temp: 

UNITS DATE 

mg/L 12/17/08 

mg/L 12/16/08 

mg/L 12/12/08 

mg/l 12/17/08 

mg/L 12/16/0B 

mg/l 12I12/0B 

mg/l 12/17/08 

mg/l 12/17/08 

mg/l 12[12/0B 

Thl:: dna ami lnfom;(loElon on !:hI", ;:!ncl other aocom~nylng documents,. rcpre:se:nt Dnl~ the samp[e{s) tlni'llyzed and Is rendsred upon condition 

mat It is nut to be repr'l)::h,u: .... ""'d whoUy or 111 D1trt for advertlsiflg Of o\:l1er pUfPOses wlthovt tlPproval from the I~OOr"tt1ry. 

USDA-EPA,NTn5;H T",sH..... 1=....,-.1 C::>~"""'I-T .... " ,.,.,,.,"',1".... ...... .. ""~.1 ~~.1 ..... ~~ .. '~r~_'~~' ~ __ 1 •• _. -_ ... ,,_._-_ .. 

12/1812008 

12/912008 

0812-00543 

36964 

C123 

12/8/2008 

0:00 

TECH 

NAH 

ADS 

ADS 

NAB 

ADS 

ADS 

NAH 

ADS 

ADS 

NAB 

ADS 

ADS 

MEMBER '. '1.'W.I 
JAN-05-2009 MON 09:48 PM CLAIRTON MUNICIPAL AUT p. 005 

® Microbac Laboratories, Inc. Page 2 of2 

100 MARSHALL DRIVE 

WARRENDALE, PA 15086 

(724) 772-0610 FAX (724) 772-16&6 

TOM ZIERENBERG, MANAGING DIRECTOR 

http://www.micwbac.com 

State Laboratory Certification Numbers: 

PADEP: 02-257, NC: 42703, WVDEP: 215,9951 eM KYo 90136 

L;liliMl::>TKY . MlCKUJ:llULUl:iY 'I'UUJJ l:>AI'tl'!');" WN~U.M.tlKPKUJ.)UCT~ 

WA'l'hl{' A.lK' WAS'lB~ '1'00.0 . pHAl:tMACI;u-nCALS' NUTRACEUTICALS 

CERTIFICATE OF ANALYSIS 

CLAIRTON MUNICIPAL AUTBOlUTY 

MR. PATRICK CANAVAN 

1 NORTH STATE STREET 

CLAIRTON,PA 15025 

PenmtNo.: 

CustP.o.: 

SUBJECT: Day 1 - Wastewater Samples for Analysis 

T:EST METHOD 

:hIDI. __ EPA 325.2 

Jil &. Grease EPA 1664A 

fotal Dissolved Solids EPA 160.1 

.,>(!: . , .:;": I': ":,'; ',; .. 

'.;,1 .:; .,',. ,": ' 

,11, ,., • TI· ~, ' 

EPA 325.2 

III & G"'ase EPA 1664A 

etal Plssolved Solids EPA 160.1 

iJmitted By: 

RESULT 

234 

<5 

862 

...... :'i' : 

227 

<5 

844 

Date Reported: 

Date Received: 

Order Number: 

Invoice No.: 

Cust #: 

Sample Date: 

Sample Time: 

SampJer/Temp: 

UNITS DATE 

mgJL 12/17/08 

mg/L 12/17/08 

mg/L 12/12/08 

:;'.'.; 

. .. ·,'":.i . ,: , 

. ''',,\r 

!<,' ,', .. mg/L 

mg[L 12/17/08 

mg/L 12/12/08 

Thl: data and Informatlnn on this, and D~l:r 2Iccampany!n~ docum"-nts, fe!JreS::f"I~ On!y the. samp!e(.s) "nalyzed anti b; render:eclLJPll!1 I;()ndltlof"l 

tnat It Is nDt to be n:produoed Wholly or 111 p:.rt for adv~ing or cIller pUrp;:lseEl wltl'lout approval. from th:; l2IooratClty. 

USDA-EPA-NIQSH re:s:tlnCl fond ""'nlr::oti"'" r""'Od'l ... ,, "" __ I~! ~~ ... UI_'-I_I __ '_· • .• • - . 

12/J 812008 

12/9/2008 

0812-00543 

36964 

C[23' 

12/8/2008 

0:00 

TECH 

NAH 

ADS 

ADS 

NAH 

ADS 

ADS 

MEMBER 

iF ..... I it 
WQrKorder# 

C:Th I d • 5'4 i.--

ISit€'- . 

--,,;,.r-- --------. • -1iI'- __ ~, __ 

100 Marshall Drlve, Warrendale, PA. 15086 . Phone (714)772·0610 Fax (724) 772-1686 

Chain :ustody 

(Please Fill Dul Completely using perm anenl ink) 

dt!l-,;,,:,w ""VN" tfvi;'; PO#. x 

Fax 

IICO"1901 N2me: &r..:""N -S,4Qt.,.;,r; Report .Yes No 

E·mall 

WATER 

DrinkIng 

Water DW 

LE MATRIX CODES 

SOUDS MISC. 

SoIT SO· DII OL 

Ground 

,"' ........... ..... , .. , <.'1,,-,- Slreet: Report Yes No SL Wlpes WP l""OY I ... ' ...... !::I'; 

If Billing Infoll1lalion is dffi"e ,-- rent than Reporting ISLIrta[;e 

Icity: Roullne TAT: Yes No InformaHon Please Indicate below (Waler 

Person: 

IDEP PWS ID #: 

StatelZip: Ilf no, Speoify days below 

P"hGna: Rusb TAT Requesled(Davs): 

E-mail: <2 2·5 5-7 

SAMPLE COLLECTED 

'-BOVE. R¥ No, OF 

CONTAIN~l) SAMPLE IDENTIFICATION 

m 

:r DATE I TIME ~ 

1/'~f-T/oA/" I II? J,,LvI7~~3 f :z. 

.2 InklcJ 7 :!;& f < 

.I IqkJ.81& ;,£ '/ 2. 

If lialn! ~I fJ~g'k If Z ~ k~b~Ig-~~= 11 ZG, ~2J",Lcl f/ ;;G ~ 2-

Waste 

Water 

Trip8lank 

Field Blank 

~"~~~It 

Z ~ ~ Z 

0 Z 

z '" '" ~ 8 o 0 Cl 

m .". :c .-

L I 

! I 1 I I I 

) J 

I I 

I ) 

J J 

SW 

WW 

TB 

FB 

if 

1< 

o 

"-

< 00 

~O 

~fJ 

w .... Swabs SB 

liquid L Food FD 

Solids S 

Mh::;ro-bialogy Me ----- -

" Analysis Requested 

T tlS} C!l&,{:;.(i.f_~;'Gi'"w-t' 

....>_ ...... _~L 

'-V Gals ~m' 1"'001'"' ,( /"" ---.l--" I Oa~ 1 '''''' ""IS;"'~"") /4z... ~;;:::,. /Z/t/.lJ J-~.? c lY=1,' 14: /t L:" 112 J'!oJ> 1 /O~:~ I=;~~~~u,") I rl fI ? 7 rliffl'l(j±(~ 

i" /7 T Oalll- 1- 11m!! D<.!w ThnB 

Fe sampling-Notes: EQUII'M~l'l'n'l[AflKS~AND FIELD BLANKS-ARE USED FOR 

INTERNAL LAB USE ONLY!NDT BILLABI.EI. NOT REPORTED UNLESS REQUESTED llY 

~amp 100 By: CUSTOMER. 

GhlOJine Rs.dlng: 

Please deliver samoles to the lab as ,soon as possible after collection 10 ensure that holding I:··' ,., , lag~in. G ".'J( be met. Please fill GOC aut competely to_expeDlle_~:all~~ 

..... __ ..... __ "-_1 hi". I\An.t:n..t:1n,u:::: 

tUijJ; 

RsII.;{1 

Creeta{{ By:MAlJ 

Dals;YJ11O .5 

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= 

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JAN-05-2009 MON 09:49 PM CLAIRTON MUNICIPAL AUT 

® Microbac La bora tories, Inc. 

100 MARSHALL DRlVE 

WARRENPALE, PA 15086 

(724) 772-0610 FAX (724) 772-1686 

TOM ZIERENBERG, MWAGlNG DIRECTOR 

http://www.microb.c.com 

p. 007 

MEMB~~ 

RII INVOICE 

Page 1 of! 

No. 36986 

CLA1RTON MllNICIP AL AUTHORITY 

MR. PATRlCKCANAVAN 

Day 2 - Wastewater Samples for Analysis 

1 NORTH STATE STREET 

CLAIRTON,l'A 15025 

, ..... 

0312-00544 

", ; : , r:-

Day 2 - Wastewater Samples for Analysis 

Please include this Invoice Number and your Client 

Account Number with all remittances 

WATER' AIR· WASTES, FOOD' PHARMACEUTICAIJS . NTJTR ~("P"TTf'A' ~ 

.. ,.) . 

$264.00 
JAN-05-2009 MON 09:49 PM CLAIRTON MUNICIPAL AUT 

®Microbac Laboratories, Inc. 

100 MARSHALL DRIVE 

WARRENDALE, PA 15086 

(724)772"()610 FAX (724) 772-1686 

TOM ZlERENBERG, MANAGING DIRECTOR 

http://www.rucrob.c.com 

p. 008 

MJ:iMBER 

- INVOICE 

Page 1 of 1 

No. 36986 

CLAIRTON MUNICIPAL AUTHORlTY 

MR. PATRlCK CANAVAN 

Day 2 - Wastewater Samples for Analysis 

1 NORTH STATE STREET 

CLAIRTON,PA 15025 

0!!12-00544 

Day 2 - Wastewater Samples 

Please include this Invoice Number and your Client 

Account Number with all remittances 

. MICROBIOLOGY' . CONSUM:ERPR.DD1JCli'S 

WATER· AIR' WASTES' FOOD· PHARMACEUTICALS· NUTRAr.p.TTTrrAT.~ 

Total 

Prepaid 

" "" 

$264.00 

$264.00 
JAN-05-2009 MON 09:49 PM CLAIRTON MUNICIPAL AUT p. 009 

® Microbac Laboratories, luc. Page] of2 

100 MARSHALL DRIVE 

WARRENDALE, PA 15086 

(724)772-0610 FAX(724)77H686 

TOM ZIERENBERG, MANAGING DIRECTOR 

httpJ/www-microbac.com 

State Laboratory Certification Number,: 

PADEP: 02-257, NC: 42703, WVDEP: 215,9951 CM KY: 90136 

CllliMl;';TKY . NUCKU1:SlULU(;iY . ¥UUlJ ;';A.!' . .t::T"i:' . CUN;';UMJ:i.K J:'KUlJUCTS 

WATER' AIR.· WASTES . fOOD ·l'H.l\.KMAC.I'UTjCAL~· NUJ'KA<.:.t::UT1CALS 

CERTIFICATE OF ANALYSIS 

CLAIRTON MUNICIPAL AUTHORiTY 

MR. PATRICK CANAVAN 

I NORTH STATE STREET 

CLAlRTON, PA 15025 

Permit No.: 

CustP.O.: 

SUBJECT: Pay 2 - Wastewater Samples for Analysis 

TEST METE:OD 

Chlo' EPA 325.2 

Oill _~se EPA 1664A 

Total Dissolved Solids EPA 160.1 

.' .. , 

'. >':";,";' 

" 

:hlotide EPA 325.2 

)f/'&' Grease E~A 1664A 

'otal Dissolved Solids: EPA 160.1 

RESULT 

843 

10 

1,980 

419 

11 

1,140 

Date Reported: 

Date Received: 

Order Number: 

lnvoice No.: 

Cu,t#: 

Sample Date: 

Sample Time: 

Sampler/Temp: 

UNITS DATE 

mg/L 12/17/08 

mg/L 1'1./17/08 

mg/L 12/12/08 

mg/L 12/17(08 

mg/L 12{17/0B 

mg/L 12/12/0B 

]2119/200& 

12/912008 

0812-00544 

36986 

Cl23 

12/9/2008 

0:00 

TEeE: 

NAB 

ADS 

ADS 

NAIl: 

ADS 

ADS 

"Ioride EPA 325.2 413 mg/l 12/17/0B NAB 

jJ &. Grease 

)tal Dissolved Solids 

londe 

&. Grease 

tal D' 'ved Solids 

EPA 1664A 

EPA 160,1 

EPA 325.2 

EPA 1664A 

EPA 160.1 

9 

1,190 

397 

<17 

1,100 

mg/L 12/17/0B ADS 

mg(L 12/12/0B ADS 

mg(L 

mg/L 

mg/L 

12/17/08 

12{17/08 

12/12/06 

NAB 

ADS 

ADS 

The d~ amllnformal:ion on this,. and other accompanylrl!:l dOOJlnents, re)Jl'eSl:!n\: only the samp!~(Ir) ana\y2ed ~nd 19 rend~ upon O:JI1dltloo 

that: It Is not.ttl be n:!prodll~ whony or In part for Bdv~rtlElng O~ other pUr'pQieS wIthout approval from rile lab::l~lDry. 

MEMBER 

".;:;;;;;;;J i II U.s[)A-EPA-NIOSH"'T~nll FtIOrl ",,"nrh>~,," ,... ....... ~,,''' ... A ...... _-,_. --~ ••• • 
j~' 

::P.0:10:

I JAN-05-2009 MON 09:50 PM CLAIRTON MUNICIPAL AUT 

Microbac Laboratories, Inc. 

100 MARSHALL DRIVE 

WARRENDALE, PA 15086 

Page 2 of2 

(724) 772-0610 FAX (724) 772-1686 

TOM ZlERENBERG, MANAGING DIRECTOR 

htrp:llwww.microbac.com 

Stat. Laboratory Certification Numbers: 

PADEl': 02-257, NC: 42703, WVDEP: 215, ?951 CM KY: 90136 

CHJ:£Ml~"J1<.¥ • MlCKU1HULUl:iY • ¥U()J) ~At'bTY . C\)N~UlIlliK l'KUJ)UCl"S 

WATER· AlR· WASTES· ~'UOD' l'HAKMACI:UnCALB . NU'J'RACEUTlCALS 

CERTIFICATE OF ANALYSIS 

CLAlRTON MUNIClP AL AUTHORITY 

MR. PATRICK CANAVAN 

1 NORTH STA 1E STREET 

CLAIRTON, PA 15025 

Permit No.: 

Cu,stP.O.: 

SUBJECT: Day 2 - Wastewater Sampi~s for Analysis 

TEST METHOD . '," .. ,' .... 

.,: 

:hloJ. E:PA 325,2 

)a II. Grease EPA 1664A 

rotal Dissolved Solids EPA 160.1 

RESULT 

351 

<5 

1,060 

Date :Reponed; 

Date Received: 

Order Number: 

Invoice No.: 

Cu,t#: 

S1UIlple Date: 

S1UIlple Time: 

SampJertremp: 

UNITS nATE 

mglL 12/17/08 

mg/L 12/17/08 

mg/L 12/12/08 

12119/2008 

12/9/2008 

0812-00544 

36986 

C123 

12/912008 

0:00 

TECH 

"",:",' 

NAH 

ADS 

ADS 

hlo:ide EPA 325.2 359 mgjL 12/17108 NAB: 

il & Grease EPA 1664A <5 mglL 12/17/0B ADS 

>tal Dissolved Solids EPA 160.1 1,Q50 mg/L 1l/12/08 ADS 

)mittedBy: 

The fll'Il;;;l ana Informl!!tlol'/ on this, ard other BC:O::lmpanying docwnenls, repr~lt only til::: .;amp)"",,s) anl!lltzad ilml Is reru:1c:re:d upon CtIndJtlon 

rhcrt: it IS nat to be rcproau~ wholly or In part for eclvertlsing or ot:hm-~ W/!tlout approval from the lab[]~roN. 

U5[).I>,~EPA.-NrDg..!"'rl:><;};"" ,,""'"''''--, ...... - ---- '" -

MEMBE~ 

0& 
I Yi"","rosrw I O~ Id.'~~ . Samp\m~ SlteJprOj 

Special Instruction.: SAMPLE MATRIX CODeS 

lvumpany: Lt~,~r..-.J "'oJ/J. Y-Iu 17-/ PO;!I x WA1ER SOWDS MISC. 

- Fax Drtnking tN.me: &,'.'" oS (Kfil".-f / Report Yes No Water DW Soil SO 011 Ol E-mail Ground Street: Report Yes No Wa.(er GW Sludge SL Wlpe8 WP 

ClIy: 

If Billing Infonmatlon 18 different !han Reporting Surface 

Routine TAT: Yes No Information Please indicate below Water sw W,ste Swab, SB 

Iphone: 

E-mail: 

Matrix 

~ECODES 

If no. Specify d .ys below Contact Person: I Ru.~ TAT R.quested(Days): Phone#: 

<2 2-5 5-7 DEPPWSID#: 

SAMPlE COLlEClEO 

:, tr)'Our 

'~ nat SAMP LE IDENTIFICATION I

NO.OF 

COllTAI 

_ •• Jed/y 

i ma1rlx 

DATE l TIME I! 

! to c.:,.". ,,"0 N I InAkflf:/c I xl j 

J bUc'i~C)S 111 I 

J F!J9i.sI7 i% IYI I 

Y p2h/.~ 7:52- IXI ( 

s 1/~bI7~S'O VI / 

fo 1/2.lrkfl ~~CO IYI I 

Dala 11mEl 

~J1-:J- Ilzl;"g 1/6 ~~mic> // ;J'/ Dalll 1---- Ttm9 

-

Samoled By: 

I

Plsase deliver samples to the Jab as soon as possible aft.er collEKitiQn to-enS'ure that holding I: .... limes will be mel Pleas. fill COG out oomple1ely~expedae sample Log-in. C 

Tan:p: 

..... __ .... _.uw_1 "-,_. niln ... n.a:;;~n.ll~ 

I 

I . 

1~1:r :I: z I. l~ i g ~ ~ _~Ji 

J 

I 

f 

{ 

Waste 

a.1er WW liquid 

TJip.Blan«. TB So/"o!ds 

Field lIIank FB 

19 I !!:l : ><, 

lRuoolved A- ;.t,2../~ lR-eooIYed 

IRI';II:;.at~1ld 

~I'/ 

L Food FD 

s Mk:ro-blofogy M~ 

Analysis Requested 

()/L. + G-/L 

I/z-h:kfl $ T;'} 0 

I --Oaill'- I Tone 

l'2..Iq,IA b0'>0 

Datil TIml! 

I Nates: EQUIPMENf St:ANKS-AND-FiELD BLANKS ARE USED FOR 

"" ~'"""''- LAB US E: 0 NL YIN OT BILLABLE). NOT REP ORTED UNLESS REQUESTE D BY 

ICUSTOMER. 

Rsv.:<i 

Created a-t:M"ID 

D.ata::JI3tKl .5 

~ 

= "'"' , 

= 

~ 

, 

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= <.0 

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. SamplmgSltelPro ect: (f 

...... _. 'W" .... ""' ....... _,....Vl ClLV'I'CoO:!I, lilt" ... r-11.~Durgn UIVISJOn PaY9 __ Dl __ 

. Customer Reporting Infonnatian . Special In,lnlctions: SAMPLE MATRIX CODES 

Company: CU."/<-Tey.,J mVIJ. flJvTIfJ Pall --• '" 

Fa. 

Confact Name: Repol! Ves No 

E-mail 

8lIeet: Report Ves No 

C~; Routine TAT: Yes No 

SI.loIZip:. If n D, Speony days below 

Phone: Rush TAT Reque.ted(Day,): 

E-mail: <2 2-5 5-7 

- SAMPLE 

Malrix SAMPLE C.Ol.1.ECTEO 

. OS"EcaDES 

ABOVE, If you SAMPLE IDENTIFICATION 

maJ.ri:tis no1 

IIsfed specify 

. yoorrna1rb:" 

below DATE TIME 

to c:-~/o!,,.J j 1~&k8 

L 1'2j~S 

..] tJ/Wof 

y fo/gog 

S :Zl.£ . roy 

" 12/W~ 

RelinqIJisJ)ed sy:(Slgnalura) - Oala 

Reinquished By:(S'gMlUr.a) ~Da!SI 14 d.~ :::> II: . /;/"y JRE!1il1i-l15hi!d By.::(Sfgn:abJrs) / 1"# Daht 

Sampled So(. 

Chlorine Reading: 

PJeoase deliver samples to the lab as soon as possible after colts-eliOA to ensure that holding 

Urnes will be met. Please fiU COG out completely itt expBdne sample log·in. 

1"1 __ ........ .., ....... , 1\1 ..... t\lInli.llot;.1rtd:~ 

WATER SOUDS MISC. 

Drinking 

Water DW SoU SO all OL 

Ground 

Water ow Sludge Sl Wipes WP 

If Billing Inform ajlOll Is d~ferenllhan Reporting Surface 

Information Pleas.e Indicate below Water SW Wasle! Swell<! 5B 

COlltacl Perton: 

IWaste 

Water WW Liquid l Food FD 

Phone II: T1Jp Biank TS SoJids S MlcllJ-biology 

Me 

DEP PWS 10 II: ReM I?lartk FB 

Preservative 

. 

'" g N:Q. OF 0: Q C-OtfrAlNER5 Analysis Requested Z c 

~ m "- z :J: :I: '" 0 " '" Z IlJ 0;'; a " 0 Z '" ru :J: '" ~o 

~ ~ Z 0 0 0 m w 0 0 ~ 5" '" :I: r '" ~. 

~ f t/ r~s cfl{~/O/£ 

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/0 rt)~ ay:(sr{lnB~reJ 

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By;(Si9Ilo!1Wr.a) 

> - Field SampJlng Notes: . EQUIPMENT BLANI\S AND FJELD BLANKS ARE SED FOR 

Cr.lHdmon: 

A,,!!.SlU11pia TelllJl: 

'0 

INTERNAL LAB USE ONl Y(NOT BILLABLE). NOT REPORTED UNLESS REQUESTED BY 

CUSTOMER. 

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DaIE'l::!J311D5 

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"" 
JAN-05-2009 MON 09: 51 PM 

',' " '. 

;' : ',' : .. ,:.' 

CLAIRTON MUNICIPAL AUT 

®Microbac Laboratories, Inc. 

100 MARSHALL DRIVE 

WARRENDALE, PA 15086 

(724) 7n06]O FAX (724) 772·]686 

TOM ZIERENBERG;MANAGING DIRECTOR 

http://www.microbac.com 

"'1' 

", I~ 

", :r",':" 

P, 013 

Page] of] 

INVOICE 

No. 37078 

CLAIRTON MUNICIPAL AUTHORITY 

MR. PATRICK CANAVAN 

Pay 3 - Wastewater Samples for Analysis 

1 NORTH STATE STREET 

CLAIRTON, PA )5025 

',; .','; ,; . :. 

0812·00788 

Pay 3· Wastewater Sam piss for Analysis 

Please inclnde this Invoice Number lind your Client 

Account Number with all remittances 

.. : i 

$254.00 

$264.00 

$264.00 
JAN-05-2009 MON 09: 51 PM CLAIRTON MUNICIPAL AUT 

®Microbac Laboratories, Inc. 

100 MARSHALL DRIVE 

WARRENDALE, PA 15086 

(724) 772-0610 FAX (724) 772-1686 

TOM ZlERENBERG, MANAGING DIRECTOR 

hr<p://www.microbac.com 

!"'" . !,": 

P, 014 

MEMBBR 

mo INVOICE 

Page I of! 

No. 37078 

CLAIRTON MUNIelP AL AUTHORITY 

MR. PATlUCK CANAVAN 

Day 3 • Wastewater samples for Analysis 

1 NORTH STATE STREET 

CLAIRTON,PA 15025 

.: '::' 

0812-00788 12122/08 

. . , .., . '; :~ > ; ~: :. : .: ! .:, :. ".,:._'1,:, 

, ,I r i .. ': .. :' ; 

Day 3 - Wastewater Samples for Analysis 

\ 

Please include this Invoice Number and your Client 

Account Number with all remittances 

:. ~ I ',: ' 

..,.,' 

$264.00 
JAN-05-2009 I~ON 09: 51 PM CLAIRTON MUNICIPAL AUT p. 015 

® Microbac Laboratories, Inc. 

100 MARSHALL DRIVE 

WARRENDALE, PA 15086 

Page 1 of2 

(724) 77:2-0610 FAX (724) 772-1686 

TOM ZlERENBERG, MANAGING DIRECTOR 

http://www.microbac.com 

State Laboratory Certification Numbers: 

PADEP: 02--257, NC: 42703, WVDEP: 2)5,9951 CM KY: 90136 

U-lli.MlS·l'KY • MlCRU1,UUJ.,UUY 'l'UUlJ ~A-":E'1':r . I,;UN~UNI.I:Kl'.KUlJUCTS 

WATER· AlR· W ASTE~ . 1'UOI) . PHARMACEU'flt:Ut; . N UTRACEUTlCUS 

CLAIRTON MUNlCIP AL AUTHORlTY 

MR.. PATRlCK CANAVAN 

1 NORTH STATE STREET 

CLAIRTON, PA 15025 

POlmitNo.: 

CustP.O.; 

CERTIFICATE OF ANALYSIS 

SUUJECT: Day 3 - Wastewater Sample, for Analysis 

Date Reported: 

Date Received: 

OrdecNumber: 

Invoice No.: 

Cust#: 

Sample Date: 

Salll~le Time: 

Sampler/Temp: 

12122/:2008 

12/1112008 

0812-00788 

37078 

Cl23 

l21l0/Z008 

0;00 

TEST METHOD RESULT UNITS DATE TECn 

Chloride 

011 ,a50 

Total ...... rSSOlved Sands 

.-.j'" 

:::. 

,. 

"::":', 

Chloride 

Oil &. Grease 

Total Dissolved Solids 

103.::' ... ,. ".' 

Chloride 

011 & Greese 

Total Dissolved SDlids 

:hlorlde 

)il & Grease 

rotal Dissolved Solids 

EPA 325.2 

EPA 1664A 

~PA 160.1 

EPA 325.2 

EPA 1664A 

EPA 160.1 

EPA 325.2 

EPA 1664A 

E:PA 160.1 

EPA 325.2 

EPA 1664A 

EPA 160.1 

'~1 

14 

70S 

330 

14 

876 

4).1 

7 

1,020 

516 

<17 

1,210 

mg{L 12{17/08 

mg/L 12/18/08 

mg/l 12/17/08 

mg/L 12/17{08 

mg/L 12(18{08 

mg/L 12/17/08 

mg/L 12/<7{08 

mgfL 12/18/08 

mg/L 12/17/08 

mg/L l2{l7/0B 

mg/l 12/18/08 

mg/l 12/17/08 

ThE: data and InibrmatlQn on this, and othe.r accompenylng documents, repre52l1t o:'lly ItII: S/JmpleCs) analyzed and 19 rendeted upon comfltlon 

that It 19 not to Ix: reproduced wholly or In part fur ~;j\lf.:rfulno or other purpose:; without <lPJlI1lval from the laboratory. 

USDA-EPA-Nf05H Th5l1nc food sanltatlcm Consulting Chemical and Mh;rob1oiog1cal AlTc'llyses and ReS"eaKh 

MEMtlER 

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JAN-05-2009 MON 09:52 PM CLAIRTON MUNICIPAL AUT p. 016 

® Microbac Laboratories, Inc. 

100 MARSHALL DRIVE 

WARRENDALE, PA 15086 

Page 2 of2 

(124) 772-0610 FAX (7:24) 772·1686 

TOM ZIERENBERG, MANAGING DIRECTOR 

http://www.microb.c.com 

State Laboratory Certifioation Numbers: 

PADEP: 0.2-257, NC: 42703, WVDEP: 215,9951 CM KY: 90136 

C.tiliM(~TKY - M1CJ:<.Ul:I1ULUliY ·l:'UUV ~Al'],;rr . CUN~UMJ:iKPKUVUL:T~ 

WATjjj{' AIR' WASTES' FOUJ)· I'HAKMACHU'flCALS· NUTI{ACjjUT1CALS 

CLAIRTON MlJNICIP AL AUTHOlUTY 

MR- PATRICK CANAVAN 

1 NORTH STATE STREET 

CLAIRTON, PA 15025 

Permit No.: 

. CustP.O.: 

CERTIFICATE OF ANALYSIS 

SUBJECT: Day 3 - Wastewater Samples for Analysis 

Date Reported: 

Date Received: 

OrdorNumber: 

Invoice No_~ 

CU$t#; 

Sample Date: 

Sample Time: 

Sampler/Temp; 

1212212008 

12111/200& 

08)2-00788 

37078 

Cl23 

1211012008 

0:00 

tEST Ml!:TI-IOD RESULr UNITS DATE TEcn 

Chi· 

Oil ~ .=ase 

Tot,,1 Dissolved Solids 

)06'<:' 

':~~ :;:: .' 

\':.: .... : .. 

Chloride 

Oil & Grease 

rotal Dissolved Solld5 

lbmitted By: 

EPA 325.2 478 mg/L 12/17/08 

EPA 1664A <5 mg/l 12/18/08 

oPA 160.1 1,1~0 mg/l 12/17/08 

EPA 325.2 520 mgjL 12/17/08 

EPA 1664A <5 mg/L 12/1B/OB 

EPA 160.1 1.2S0 mg/L 1'l./17/08 

The dll~ ana InrormaliDn on !:hIS, emf other tlcmmpanylng docuYnents, repr-esent DIlIV ~h<:i: sampb(!:) analyrd c:nd Is" tendered upon I:Uildltlon 

thBt It Is not 00' De repl'O(luced wholly or In part for advertising or other purposes without IJIJProval fmm the rafxlfilto~)'. 

USbA~fPA-Nlo5H TE!~n!J Food $oIrlt:2Itlon Ctruult:lng CIlemlQd and Mlo-obroioglcal Anall'Ses !!mtf ~8searc:h 

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Microbac Laborator' ,Inc. - Pittsburgh Division Pag" __ o' 

100 Marshall Drive, Warrendale, PA. 15L_A Phone (724)772-0610 Fax (724) 772-1686 

OJ, (;). - 'I n; Chain of Custody 

am piing S;le/P roject: (please Fitl Out Completely using peITr1anent ink) 

Cusmmer Reporting lnfonnation Special instructions: SAMPLE MAlRIll COOES 

Company: POiI __ x WATER SOLIDS MISC. 

Fax Dfinldlll 

Contacl Name: C{.&'A../<>4 .~ild 11<117/ Report Yes N. iwalllr DW 5011 SO on Ol 

E-mail GrooM 

SIreBl: Report Yes No Water OW SluxIge Sl WIpeS WP 

11 SWing infonnatlan is differe1lt than Reporting Surfa", 

City: RoUU"" TAT: Yes No lnfonnaoon Please fndTc:ate below w_ sw Wasm SlItabs SB 

SlalelZip:. H no, Specify days below C(mta.ct. Person: 

Phone: Rush TAT RequesledlDays): Phone #:. 

E-mail: <2 2-5 5-7 DEPPWSID#: 

SAMPLE 

Matrix SMl.!PLE COLLECTED 

SECODES 

MOVE. if)'Ou NlI. OF SAMPLE IDENTIFICATION 0 CONTAINERS ma1rb:'ts not 0 

IisfBj spec"" ~ ~ 

mar.rix g 

belo" DATE TIME ~ ! 

4<i47/W I f't~i n!c r I~ L 

L iZJ/';63 7:S- 1)( f;I J 

.J 17/1-4- 7~'>o Ii '~ Z-. 

y kftolti 7;~u Ii i!t Z- ~ '1k/eg 7~>O I~ ~ Z- S. 

r;, '¥j,f 1)50 ~~ ~ RelinlJ.li:9:lIe4 Hy;(Signalure) Da(i! l1rr,a 

eincpJIsltad B~stgi\'ilLura) D~' 11,.. 

Relinquished B'(.lSlgnafure) 

·h7~ ria TI"", 

.'2. Ii 0.8 /~ ~ o~ ,. 

Sampled By: .~ 

Chlorine Reading: omfrtiot1: 

Please deliver 51lmples to (he lab as soon as possible after roliection to ensure that holding ~",g"Samp{e Teffll: 

times will be met. Please fill coe out completely to e)(J)ed~e sample Log-in. , '0 

1"10 __ ""~...Jr ... 1 t..i ..... nllnl;J"JJ';1nlllF; 

w .... 

Water Iww Ili<ruid l Food FD 

Trip Bfan, T8 Solids S Micro-bi~ogy 

Me 

Reld Blank fB I 

Presernilli/ll 

il' 

~ 

'" Analysis Requested " ·z 

.. !!. 

z :r: '" 0 :r: '" z [J) ,,2: 0 z [J) " :r: '" ~o 

Z 0 0 0 Cl 0 0"-

m '" ... :r: r- '" >'il 

Iii' ,/ TV'S. C/-Ic.c,.,.,t¥J 6/t.-{-C-;d! / 

Iv Iv 

V- IV'" / 

il Iv I 

't/ Y , / 

V Iv "" Recell.'Ed nw Tilne 

By:(,si-;lnarore) 

Rooel~oo 4ltK Iz1JoJ f( lilT¥! By;{6IlJl!i:ure) ~/;j 

!Re~lo;E.d 

IB,'I""'''''''''l I /1' " .. 11", 

Field Sampling Notes: EQUI PMENT BLANKS" AND FIELD BLANKS ARE USED FOR 

INTEl'\NAllAB USE DNLYlNOT BILLABLE). NOT REPORTED UNLESS REQUESTED BY 

. CUSTOMER. 

Re\r.:O 

Cl!;l0lllld BrJhAtJ 

I 
Wam:dllsa Mlcrobac Laboratori 

100 Marshall Drive, Warrendale, PA. 150t.~ 

Inc. - Pittsburgh Division Page __ ol 

Wor1<ortler # Phone (724}772-0610 Fax (724) 772-1686 

:: I oQ 1::1. - S""lJ 

0:. Sampling site/Pi Jec\: 

r _l!Srunor 

; ,,1.t" ( utl1.1181\ 

;tName: 

Slr.et ____________ -1 

city: 

I

phone: ____________ -I 

E-mail: 

Matrix 

:SECODE~ 

Chain of Custody 

(please Fill Out Completely "'lfl!j permanent ink) 

SpeciallnslrucUons: , 

POiI X -- Fax 

Report Yes No 

E-lnau 

Report 'Yes No 

Routine TAT: Ye, No 

r Bming information is different than Reportirn.i 

Information PleB.5e indlcate belo11l 

It no, Specify days below rontad Person: 

Rush TAT R"'Iuested(Days): Phoneil: 

<2 2-5 5-7 DEf' PWSID I/: 

JI t= l'.l'Il 

E,lfl'OOlJ SAMPLE IDENTIFICATKlN 'NO. OF potrr. 

1-

= -<C 

-" 

-0: 

"-

'-' 

= 

= ::2 

= 

= 

<---

= 

-<C 

-" 

'-' 

""b not 

d 'pecify 

Jurma1rix. 

It-. 

CNX -3 11'L._L 

'I DATE 1 TIME I~ 1~1~1~1~lp \1.1 -O'<j I 'i']"Au I~-I~IJI 13 

r H 

SAMPLE MATRIX CODES 

WATER J SOUDS ] MISe. 

Drinking 

Wal", 

~~nd ater . 

Su.-

WEtST 

Wasle 

Weier 

Top BI"" 

Fl<1d Bl!mk 

DW 

GW 

SW 

WW 

TB 

FB 

~ ~ 

a 

0 9 ~o 

. "- ll,~ 

Sci SO Oll 01 

SludQe Sl Wipeo WP 

Wasta swab, S1l 

UqtBd L food FO 

Soids S 

MiCllJ..biolagy 

MC 

Analysis Requested 

I J.AJ.tfu 

::2 Dam ~ R-I!09ilibd' 0at.9 -- --- --·TwX 

"- It- if /()~lf( /l.'"! Ily;ISi"".Im" /t,o P''1)A'< ~ Re1:lli.y.;;d D:at.e Time 

= I;;' "',(81,,,,,,, .. ) 1;Z -'1.-. f: Ii r;.1 0 

= 

= -'''I'OIl"",~) 1"-/'/ ~~ It 'I' l>b 

= ::2 _ t7 F'eld Sampling Notes: EQUIPMENT BLANKs AND FIELD BLANKS E SED FOR 

= ~ i@y..'lZd[e,!JL-l)-O,3''1]01WJ.INTERroIALLABUSEONLY(NOTBILLABLE), NOT REPORTED UNLESS REQUESTED BY 

~ Sampled B~? . <!O~ I ' CUSTOMER, 

~ Chlorine Read ng: ~ 

= , 

= -<C 

~ 

Please deliver sa.mples 10 the lab as S{]OD as po:.ssible after IXlllectiDII to ensure that hakllng \"--",.--... r 

. tlrnes will be meLi"leaoe fill CO C OU! completely to o"".rllle sample Log-In, "C ~,).-' 

Rev.=o 

Cro!1aled 8!(.MAD 
JAN-05-2009 MON 09:53 PM CLAIRTON MUNICIPAL AUT 

® Microbac Laboratories, Inc. 

100 MARSHALLDRlVE 

WARRENDALE, PA 15086 

(724) 772-0610 FAX (724) 772-1686 

TOM ZlERENBERG, lvlANAGING DIRECTOR 

http://WW\V.mi~obac.com 

CLAIRTON MUNICIPAL AUTHORITY 

MR. PATIUCK CANAVAN 

1 NORTH STATE STREET 

CLAIRTON, PA 15025 

. ': ::, ,. 

"",: 

0812-01064 

" :": ., ..... : ; ~ ; . ,.': . " "; ; , . ',,!!; "'''.1; 

: ..... , . . '," t:· i' ('I •. · •• f': :: 

samples for Analysis 

Please include this Invoice Number and your Client 

Account N1Ul.\ber with all remittances 

p. 019 

MEM9ER: 

DII INVOICE 

Page 1 ofl 

No. 37372 

$528.00 
JAN-05-2009 MON 09:53 PM CLAIRTON MUNICIPAL AUT 

® Microbac Laboratories, Inc. 

1 00 MARSHALL DRIVE 

WARRENDALE, PA 15086 

(724)772-0610 FAX(724)772-1686 

TOM ZIERENBERG, MANAGING DIRECTOR 

http://www . ...;crob.c.com 

P, 020 

Pago 1 of! 

No. 37372 

. "1 .} \~',:,:: 

CLAIRTON M:tJNICXPAL AUTHORITY 

MR, PATRICK CANAVAN 

.Wastewater Samples for Analysis 

I NORTH STATE STREET 

CLAIRTON, PA 15025 

12123108 

Wastewater Samples for Analysis 

Please include this Invoice Number and your Clieut 

Account Number with all remittances 

", . .~ . 

$528.00 

$528.00 
JAN-05-2009 MON 09: 54 PM CLAIRTON MUNICIPAL AUT p, 021 

Microbac Laboratories, Inc. Page 1 of4 

100 MARSHALL DRlVE 

WARRENDALE, PA 15086 

(724) 772-0610 FAX (724) 772-1686 

TOM ZIERENBERG, MANAGING DIRECTOR 

http://wwW.m1c{obac.com 

State L.boratoIy Certificatioll Numbers: 

PADEI': 02-257, NC: 42703, WVDEP: 215,9951 CM KY: 90136 

CHJ>M1S"U<.Y . MICKU IULUt;iy' F()U)) SM' Tl'" CUNSUMI:ili. !tUlJUc-n; 

WA:l'l:iR' l\..lli.' WASTES, t'OOJ)' PHAJ{MAC/:iUl1CALS' NUTKACEUTlCALS 

CLAIRTON MUNIClP AL AUTHORITY 

MR., PATRICK CA:NAVAN 

1 NORTH STATE STREET 

CLAIRTON,PA 15025 

Permit No.: 

Cus!P.O.: 

SUliJECl': Wastewater Samples for Analysis 

CERTIFICATE OF ANALYSIS 

Data Reported: 

Date Received: 

Order Number: 

mvoice No.: 

Cust#: 

Sample Date: 

Sample Time: 

SamplerlTemp: 

12/23/2008 

12115/2008 

0812-01064 

37372 

Cl23 

12/] 112008 

0:00 

TESl' MEmO)) RESULl' UNITS DATE U<CR 

Chloride 

Oil ar.:rease 

Toti ;olved Solids 

::hlorlde 

)jl &. Grease 

'Ci~1 Dissolved Solids 

13 .... I,,' 

.. : .... ~. 

;:',: . , , 

II & Grease 

,tal Dissolved Solids 

,Iorio. 

"i1I. Grease 

tal Dissolved Solids 

EPA 325.2 

EPA 1664A 

E:PA 160.1 

EPA 325.2 

EPA 1664A 

EPA 160.1 

EPA 1664A 

EPA 160.1 

EPA 325.2 

EPA 1664A 

EPA 160.1 

183 

7 

664 

364 

7 

942 

S 

946 

351 

<17 

932 

mgfL 12/23/08 

mg/L 12/'22/08 

mg/L 1Z/19/0B 

mg/L 12/23/08 

mg/L 12/22/08 

mg/L 12/19/08 

mg/L 

mg/L 12/23/08 

mgfL 12/22/08 

mg/L 12/19/08 

Tne. data anti Informstlon on thl~, and orh!lr I!ItOJmp.lftylng documents'. represerlt only the SlImple(s) 6ni:llyzed and Is re:ndered Upon cOi'ldrt!on 

that It Is not to be rop;uduced wholly O~ In Pllrt fur advertlslng or Qther Pul'pCls:;5 wIthout !IPDrovall'rorn the labnrotory. 

USDA-ePA-NIOSH Testing Food .sanl~tlon CC!l'3ultlng a,~car aM MlaoDlo)ogfcol Antllyses and RE$eafCh 

MEMBER 

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JAN-05-2009 MON 09:54 PM CLAIRTON MUNICIPAL AUT p. 022 

® Microbac Laboratories, Inc. Page 2 of4 

100 MARSHALL DRIVE 

WARRENDALE, PA 15086 

(724) 772-0610 FAX (724) 772-1686 

TOM ZIERENBERG, MANAGING DIRECTOR 

http://www.microbac.com 

State Laboratory Certification Numbers: 

PADEP: 02-257, NC: 42703, WYnEP: 215,9951 CM J(Y: 90136 

CHt:M.ls·nc\, . M.lCKUlllULUliY . ¥UUJJ SA1:'bTY . CUNOiU ·K.PKUJJULTt; 

WATbR' AIR· WA~THS '1'00))' PHARM/>.CtUDcALS - NUTRAcEU'I'lCALS 

CLAIRTON MUNICIPAL AUTHORITY 

MR. PATRICK CANAVAN 

1 NORm STATE STREET 

CLAIRTON, PA 15025· 

Permit No.: 

CustP.O.: 

SUBJECT: Wastewater Samples for Analysis 

CERTIFICATE OF ANALYSIS 

Date Reported: 

Date Received: 

Order Number: 

Invoice No.: 

Cust#: 

Sample Date: 

SBDlple Time: 

SamplerlTemp: 

12/23/2008 

1211512008 

0812-01064 

37372 

CIZ3 

12111/2008 

0:00 

TEST METHOD RESULT UNITS DATE TECH 

Chic 

Olle.. .::!a;se 

Total Dissolved solids 

)11 & Grease 

rota! Dissolved SoJlds 

:hlorlde 

)11 &. Grease 

'otal Dissolved Solids 

hloride 

'i1 & Grease 

otal ". '0lved Solids 

9 /·Locati6d ' 

cPA 325.2 

EPA 1664A 

EPA 160.1 

EPA 1664A 

EPA 160.1 

EPA 325.2 

EPA 1664A 

EPA 160.1 

EPA 325.2 

EPA 1664A 

EPA 160.1 

335 

<5 

954 

<5 

948 

258 

<5 

794 

381 

<5 

952 

mg/l 12/23/08 

mg/l 12/n/08 

mg/l 12(19(OS 

mg/l 12/22/08 

mgfl 12/19/09 

mg/l 12/23/08 

mg/l 12/~2/08 

mg[l 12/19/06 

mg[l 12/23[08 

mg/l 12/22/08 

mg/l 12/19/08 

Tho;:: dllta and Inrorltltltlon on thJs, and oth~r ell;comp~1n9 dOC(lme:nts, repre5E!nt: Drily thIS: sample{s) analy.ted ~nd Is rendered upnn conditJgn 

tlEt It I.!! !'JOt to be reproduced wholly or In part fot Bdvertlslng or oHler pu~s without approval frOm the lilbol<!toty. 

USDA-EPA-NJOSH Testlrlg Fo.cc Sl:Inltatton COnsultIng ChemIcal and M1C1OblologlcaJ Analrs!!S and R~ord! 

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JAN-05-2009 MON 09:55 PM CLAIRTON MUNICIPAL,AUT P, 023 

Microbac Laboratories, Inc. Page 3 of4 

100 MARSHALL DRIVE 

WARRENDALE, PA 15086 

(724) 772-0610 FAX (724) 772-16&6 

TOM ZlERENBERG; MANAGING DIRECTOR 

http://\X!'WW,mio;obac:.c:om 

State Laboratory Certification Numbers: 

PADEP: 02-257, NC: 42703, WVDEP: 215,9951 CM KY: 90136 

Cl-lliMl:sa<.y • MlCKUHIULUliY • r'uuu :;Al'J;lT~ • CUN:;UMJ>KYKUUUCn; 

WATER· AlK . WASTES' .FOOl) . l'.tiAKMACEU·UCALS . NUTRACEU'rlCALi;; 

CLAIRTON MUNICIPAL AUTHORITY 

MR. PATRICK CANAVAN 

1 NORTH STATE STREET 

CLAIRTON, PA 15025 

PelmitNo.: 

CusIP.O.: 

SUBJECT: W.,tewater Samples for Analysis 

Chloride 

011 ase 

Total vlSsolved Solids 

Chloride 

Oil & Grease 

Total Dissolved Solids 

)11 & Grease 

iotal Dissolved Solids 

:hloHde 

lil & Grease 

·otal Dissolved Solids 

EPA 32S.2 

EPA 1654A 

EPA 160.1 

EPA 325.2 

EPA 1664A 

EPA 160.1 

EPA 1664A 

EPA 160.1 

EPA 32S.2 

EPA 1664A 

EPA 160.1 

CERTIFICATE OF ANALYSIS 

408 

<;5 

1,020 

331 

<17 

820 

<5 

804 

300 

<5 

780 

Date Reported: 

Date Received: 

Order Number: 

Invoice No.: 

CUst#: 

S ample Date: 

Sample Time: 

Sampler/Tomp: 

mg/L 12/23/08 

mg/L 12/U/08 

mg/L 12/19/08 

mg/L 12/23/08 

mg/L 12/22/08 

mg/L 12/19/08 

mg{L 

mg{L 

mg/L 12/23/06 

mg/L 12/22/08 

mg/L 12/19/08 

The det,t:! tmd Information on thiS', and oltu;r ~mllcmvlnll documents,. rep~l'lt [lilly th~ ':;;lImDI€(s) an<lI)lzed and I:i rendered upotl =ndll:Jnn 

th;:.t It 1:; not to be reproouced Wholly or In p;:lrt for advert1s:lng at' other PllI'pCJSes without approval from the laboratory. 

USDA-ePA-NlOSH Testing food SBnJ~t1on Consultln!l Chemical and MkrobloJoglCII! Am'll).':;es and ~arch 

12123/2008 

1211512008 

0812-01064 

37372 

C123 

12/11/2008 

0;00 

MEMBER 

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JAN-05-2009 MON 09:56 PM CLAIRTON MUNICIPAL AUT p. 024 

® Microbac Laboratories, Inc. Page 4 of4 

100 MARSHALL DRIVE 

WARRENDALE, PA 15086 

(724) 772-0610 FAX (724) 772-1686 

TOM ZlERENBERG, MANAGING DlRECTOR 

http://wwtv...m1cI::obac..com 

State Laboratory Certification Numbet·s: 

. PADEP: 02-257, NC:42703, WVDEP: 215,9951 eM KY: 90136 

l.;j-lliMlS·lKY . MlUKU,BJU.LU(jy : FUUl) SAl')':',,),' . UUNljUMbKJ-'KUl)UCTS 

WATER· AiR' WASTES, FOOD 'l'HAlZMACEU'11CALS . NUTRACBU'l'lCALS 

CLAIRTON MUNICIPAL AUTHORITY 

MR. PATRICK CANAVAN 

I NORTH STATE STREET 

CLAIRTON, PA 15025 

PermitNQ.: 

CustP.D.: 

SUBJECT: Wastewater Samples for Analysis 

CERTIFICATE OF ANALYSIS 

Date Reported: 

Date Received; 

Order Number: 

Invoice No.: 

Cust#: 

Sample Date: 

SaInple Tim.: 

Sampler/Temp: 

121:2.312008 

12/15/2008 

0812-01064 

3737:2. 

C123 

1211 112008 

0:00 

TEST METHOD RESULT UNITS DATE TECH 

The data lind Information 011 thiS, lmd othEr accompanVlng ODC1l11l!nts, TEpre5!!n~(Inlv the S3mpJe{s) analyzea end 1.$ rtm:ll3Tli!d upon condition 

HH[ It Is not to ~ reproduced wholly or In p;,rt for adverttslng or o!:her purpose;: without approval from thE: laboratory. 

U5DA-EPA-NIOSH TestIng food Srmll:zJt:lan Consulting ChamlCJ)\ ~nd Mlcrob\o[og\~a\ AI1a1ySc:s ;,nd R'23eardl 

MEMBER. 

mill 
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If Billing information is different tl1an Reporting Surfaoo 

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Waote 

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Phone: Rush TAT RequesleIl(Days): Phone'ik Trip f3~nk T8 Solids S . M"KrobJology Me 

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times will be met Please fill coe ou{ completely [0 expedi1e sample Log~ln, '0 6, 

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field Sampling Notes: EQUIPMENT BLANKS AND FIELD Bl.ANKS ARE ",ED FOR 

INTERNAL LAB USE ONLY{NOT BILLABLE)_ NOT REPORTED UNLESS REQUESTED BY 

.~ CUSTOMER. 

Rell'.:(J 

CreatEd RIf'J.f~n 
Itrtflmal t.: 'I 

Workorder# 

.'I1icrobac Laborator , Inc •• Pittsburgh Division Page __ , 

100 Marshall Drive, Warrendale, PA. 1511,,0 Phone (724)772-0610 Fax (724) 772-1686 <= 

~ 

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stateJZiP:' II no, 5peoify d.ys below 

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= lNTERNAL LAB USE ONLY(NOT BILLABLt;j. NOT REPORTED UNLESS REQUESTED BY 

= Sampled By: CUSTOMER. 

= 

~ Chi [}ri ne Readlng: 

~ P(ease deliver samples to the lab as soon as possible after collection to enSllre that holdrng 

~ limes will be met. PI.as. fill COC out completely!o experlile sample Log-in, 

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Chain of Custody U"1~'I;f~ I' (please Fi~ Out Completefy using permanent ink) 

Cf4,'/I... 7(J",) fflt,)hJ, ftfIvTJ 1PV11 

Fax 

Contact Name: Report 

E-mail 

Street Report 

" 

Yes No 

Yes No 

Cil)': Rootin. TAT: Yes No 

S!ateJZip: If no, Specify days beiovi 

ISpecOil 

WATJ:'g 

~:!n~ low 

·IGroUJH! 

W-",",---- I GW 

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Information Please Indicate below . WalE< SW 

Waste 

IContact Pe",oo: Wat.. ww 

Phone: Rush TAT Reque,ted(Days): 

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phon. e.#:. • ITilJl Blan!< 1m 10 __ 

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INTERNAL LAB USE ONLY(NOT BILLABLE). NOT REPORTE.I) UNLgSS REQUESTED BY 

ui:L1111-'Jed By: CUSTOMER. 

Chlorine Reading: 

Pl~se deliver samples t() the lab as. soon as I'ossiille after coJlectlon to ensurn fha[ hol[Jing ~'L'g.S~6aTrr'/ 

Urnes will be met. Please fill COG (luI c.ompletely to e~edite sample Larrln. C lO ___ _ 

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Womar,k 100 Marshall Drive, Warrendale, PA. 150. Phone (724)772-0610 Fax (724) 772-1686 

= Chain of Custody 

= "" Sampling. 51telp roject: (Please Fill Oul Completely using permenent Ink) 

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1-,/ Iv . IJ/'S o,'.;j(yt. cj;(Cyl/§(j 

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i IN1ERNAL LAB USE ONLY{NOT BILLABLE). NOT REPORTED UNLESS REQUESTED BY 

Sampled By, CUSTOMER. 

Chlorine Rea.ding: 

Please denver .sampl~s to Ole Jab as soon as possible after Gol!ection to ensure that holding ~ 1Jg..sa~fl1/P: 

times 'tVi~ be. mel P lease fill coe out completely to expedile sample LogMin. C h ( I 

n.. .... ,... ..... ~l "-1 .... - nJlr.t::nt:.-1n,u:, 

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nJl""'lU~1m Ii 
ApPENDIX D 

TABLE 3-16: "TYPICAL COMPOSITION OF 

UNTREATED DOMESTIC WASTEWATER" 

METCALF & EDDY, THIRD EDITION, 

WASTEWATER ENGINEER 
3-5 WASTEWATER COMPOSITION 109 

TABLE 3-16 

Typical composition 01 untreated domestic wastewater 

Concentration 

~d for Contaminants Unit Weak Me~ium Strong 

Solids, total (TS) mg/L 350 720 1200 

Dissolved, total (TDS) mg/L 250 500 850 

Fixed mg/L 145 300 525 

[luent Volatile mg/L 105 200 325 

i and Suspended solids (SS) mg/L 100 220 350 

Fixed mg/L 20 55 75 

eegate Volatile mg/L 80 165 275 ~can 

Settleable solids mUL 5 10 20 )orary 

lteria, Biochemical oxygen demand, mg/L: 

5-day, 20"C (BODs, 20"C) mg/L 110 220 400 

water 

w for Total organic carbon (TOC) mg/L 80 160 290 

Chemical oxygen demand (COP) mg/L 250 500 1000 

Nitrogen (total as N) mg/L 20 40 85 

Organic mg/L 8 15 35 

Free ammonia mg/L 12 25 50 

Nitrites mg/L 0 0 0 

I con- Nitrates mg/L 0 0 0 

md in Phosphorus (total as P) mg/L 4 8 15 

eed to Organic mg/L 3 5 

w, Inorganic mg/L 3 5 10 

.ap. oJ. Chloridesa mg/L 30 50 100 

Sulfatea mg/L 20 30 50 

Alkalinity (as CaCO,) mg/L 50 100 ZOO 

ported Grease mg/L 50 100 150 

ater is Total coliformb no/100 mL 106_107 10'-10' 107-109 

rations Volatile organic compounds (VOCs) 1'9/L <100 100-400 >400 

i other <lValues should be increased by amount present in domestic water supply. 

ded to b'See Table 3·18 for typical values for other microorganisms. 

lced iJ1 Note: t.8(oq + 32 := of. 

;pools. 

iations Some organisms (shigella, helminth eggs, protozoa cysts) are almost never looked for 

'ptage. in a routine analysis. Great care should be exercised when reviewing reported virus 

values. In recent years, refinements in virus detection and enumeration methods have 

rendered most early results suspect. Thus, the date of the study is almost as important 

as the reported concentration values. 

lUnd in 

Need for Specialized Analyses 'ported 

ed that In general, the constituents reported in Table 3-16 are those that are analyzed more 

!i [18]. or less rou$-ely. In the past, it was believed that these constituents were sufficient 
ApPENDIX E 

CMA BOD AND TSS 

INTER PROCESS DATA AND 

CMA WEEKLY OPERATIONS REPORTS 
~ ~ 

0.: 

0) 

"" 0J 

(:0 

(:0 

(:0 

0J 

0J 

~ ~ 

X 

<C 

LL 

~ 

>- f0-; 

0:: 

0 

::c 

f-

:::> 

<C 

-l 

<C 

0... 

0-; 

(,) 

0-; 

:z 

:::> 

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0 

f0:: 

0-; 

<C 

-l 

(,) 

f'-

LD 

Gl 

~ 

w 

:::> 

f-

~ 

0) 

(S) 

Gl 

0J 

I 

f'-

0J 

I 

:z 

<C 

-0 

I 

II 

II 

II 

NOV 30 

DEC 1 

2 

3 

4 

5 

6 

9 

10 

11 

12 

14 

\6 

16 

17 

18 

19 

20 

21. 

22 

23 

24 

25 

25 

27 

28 

29 

30 

31 

IItJ I.wJijj 

II .. 

-

~ ""ti1i,. . .. ~-

CMA WASTE WATER TREATMENT NPDES REPORT 

3.74 0.37 10.0 312 4.5 140 67 

3.B9 0.02 10.7 341 5.2 16B 13B 

3.40 0.00 9.3 263 4.0 113 55 

3.16 0.00 14.6 385 4.6 121 71 

3.28 0.12 11.3 309 4.4 120 42 

3.13 0.00 12.3 321 4.9 128 20 

3.05 0.00 14.7 374 4.7 120 3\ 

3.04 0.01 11.9 3!l2 7.0 178 77 

4.97 0.62 2.6 108 14.8 614 780 

5.21 \.13 6.0 261 11.1 482 100 

5.67 0.03 B.O 379 7.1 ~~A .oil 

4.70 0.21 15.3 599 5.7 223 58 

4.7S 0.12 16.0 638 4.8 191 50 

4.79 0.01 1!J.B 423 5.9 236 4S 

5.2B 0.3\ 11.3 49B 6.0 254 96 

5.10 O.DO B.O 346 6.7 289 '84 

5.57 1.54 9.0 418 11.1 516 BO 

5.55 0.00 21.3 gaS 7.3 338 43 

5.2:1 0.05 20.0 872 6.1 266 40 

4.55 0.00 15.3 581 4.1\ 182 39 

4.28 0.01 11.6 414 5.0 17B 55 

5.71 1.45 22.!J 1047 7.2 343 60 

5.90 0.00 16.6 B\6 6.1 300 140 

5.60 0.76 8.6 402 5.1 236 77 

6.07 0.01 13.3 674 B.2 314 90 

5.63 0.02 14.6 686 5.\ 240 43 

6.31 0.01 7.3 323 4.5 199 51 

4.93 0.00 B.6 354 4.6 189 26 

4.65 0.02 17.3 659 5_3 

143.9 6.67 15210 76BI 

3.4 lI,B 330 4.6 130 

4.3 10.3 354 8.2 314 

5,1 13.1 558 6.B 294 

5.3 15.3 687 S.B 250 

4.6 0.22 12.6 491 6.2 248 

6.1 1.54 22.0 1047 14.B 614 780.0 

3.0 0.00 2.6 lOB 4.0 112 20.0 

DEC 2008 

7.0 0.30 

7.0 3218 0.30 

7.1 3236 0.33 

l:~' " days 

6.9 3330 0.30 

6.9 330B 0.3\ MlSS = 3875 mgll 

6.9 3294 0.32 

6.9 3138 0.32 Flllt=_ 0.05 

7.0 3486 0.25 

II 

SEC. AERATION CAPACITY:: 1525920 gal,", 

6.S 3456 0.2\ S=C.CLP-.RIFIER CAPACITY = 410064 Q01= 

7.1 3360 0.32 AVE. WAS PUMF~NG RATE ::i 35915 gal'dBy 7. '1"':17A non AVE. I'IAS % SOLIDS. 0.47 % 

" AVE. PRIMARY EFF. BOD '" 64.125 IT.Q:l 

7.2 0.34 

7.1 3995 0.34 

7.1 3!f40 0.:12 

7.0 3698 0.36 

7.1 3936 0.35 

7.1 4458 0.25 

7.2 4114 0.38 

7.1 0.34 

7.2 4748 0.36 

7.1 4982 0.27 

7.0 444B 0.26 

7.2 3614 0.37 

7.1 4832 0.36 

7.\ 4146 0.45 

7.1 0.38 

7.1 4484 0.32 

7.2 4910 0.30 

7.1 3875 0.33 

7.2 4982 0.45 

6.8 :1I3a 0.21 
~~~ ~-----------------------,----------------

ApPENDIX F 

RADIOLOGICAL ANALYSIS OF CNX-1 

AND CNX-3 WELLS 
JAN-21-2009(WED) 07:53 CLAIRTON MUNICIPi>L AUTHORITY (FAX)4122333249 P.0171029 

® Microbac Laboratories, Inc. 

100 MARSHALL DlUVE 

WARRENDALE, PA 15086 

Page I of I 

(724) 772-0610 FAX (724) 772·1686 

TOM ZlERENBERG, MANAGING DIRECTOR 

htlp:/ /www.microb-a<.<<>m 

State Laboratory Certification Numbers: 

PADEP:02-257, NC:42703, WVDEP: 215,9951 CM KY: 90136 

CHcM.I;;lKY • MICKVl;SlVLUIJY • ~VVU :SAl'lOl'Y· CVN;;UMblU'KUJ..)UC 1:S 

WATER· AIR' WASTES' 1'001)' .!:'HAJ.{MACEUTJCALS· NUTRACJ,;UTICALS 

CLAIRTON MUNICIPAL AUTHORlTY 

MR. PATRlCK CANAVAN 

I NORTI-I STATE STREET 

CLAIRTON, PA 15025 

PermitNo.: 

CustP.O.: 

CERTIFICATE OF ANALYSIS 

SUBJECT: Wa.,tewater Samples lor Radiological Analysis 

Date Reporled: 

Date Received: 

Order Number: 

Invoice No,; 

Cust if; 

Sample Da.te: 

Sample Time: 

SamplerlTemp: 

111412009 

1211 912008 

0812-01478 

38431 

CI23 

12/19/2008 

11:25 

TEST METHOD RESULT UNITS DAT.E TECf( 

Gross Alph. 

6ro< :a 

EPA 900.0 

EPA 900.0 

See Attached 

See Attached 

pall 01106109 

pCill 01/06109 

""Analysis performed by GEL Laboratories w;. 

:ubmiltcd By: 

om Zicronborg 

Managlns. Dle-Bcta 

TIl!! dl,r;!:llmd InforTJ1iltloo on mis, aM o1h~ &eeomp.,nylna documents, represent only tf,~ :.lImD'lc(:;:} 'lnClI)'Zed allllis ~lld~ IIjXIIl c:DfIdltlon 

lhl:!L 111~ not ~ be reproducea Wholty or In pout ror ~d'l:i1'tf~lna or ott\[!f purposes wltllou~ 1!pprQ'oli11 from !:TIe labcralnl'y_ 

USDA-EPA-i'HOSI'11cst1ng' fOocI Sanltatlcm Catl!>ulUrrg 0lc:mlc;,1 and MIi:robi01ClglCBI AJI,lIir..e:; lind I~nn:h 

••• 

••• 

MEMBER 

lWil 
I ",fUI~d lI~. Onl, Microbac Laboratorles,lnc.- Pittsburgh Division Pago __ or --- l Workoodcf II 100 Marshall Drive, Warrendale, PA. 150ar Phone (724)772-0610 Fax (724) 772-1686 

~61 ';;I-~ lID ~ Chait. of Custody 

<iau'(I '"9 Sj(e/Proje~t: (please fill Out Compretely U5~llg permanent Ink) 

Customer Repnrfing t9formation Special Insfrucliof.ls: SMIPLE ldATlUX CODES 

f ;.om fmny: .:_L,';.' iO rJ ;11I]1I;(_,r/1/ ~ffflll:j POil __ x WATER SOLIDS MISC_ 

Fax DllrlkJng 

r;'::'flr~ct Nallle: {it.. ;,'1 {j.} .f£t./!./::;s,' .,.' Report Ye.s Uo Wa1er (lW !ioil SO Oil (}L 

E-mail Ground 

~jl rE::::"t: I {Ij")''l rlJ SJiU"c: S/: Report Yes Uo W'.ata" 01N Sludge Sl lA~pas \NP 

.. ~ (_/11A.[ :,.J 

if Billing Information is ilifiarent than Repor1ing Surface 

ely: Routine TAT: Ye:5 No Jnfonn.a'ion Please fndicate below Wi!lte:r "Vi Waste S ..... abs S8 

~i!al<~JZ~r: . '-'I l r S-o~~;- If no, Sp€oily days b.low Conia [;1 PeISGn: 

,-'IH1IIe-: '1" ,) J j ) --. J ,'/.. Lj .£ Rush TAT Request.d(Days): Phone #: 

C-In<:L <2 2-5 5-7 DEPPWSIDI/: -

J!li:drm;I' SAMPLE 

iJ.!'~;': ~ ',:. Malrl, S~MPL.E COLLECTED 

,~;~; ~: L .lECODES 

AnOVE, if,',}I!! No. Of S!,MPLE IDENTIFICATIDN .~), ~.~ 0 m:=.t· -CONTAlr.lERS l)( is nol, 0 

::;~~::~~. liste;1 srecif~ . " .. ~~b'~'::1~ ',\~,ur rna<:rilc Q 

.. <> 

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j :h'l,)nll~ R.ea·jiriil: Ca .. J.dili';:.r.: 

"/eil:if;; It-.:::1.lIer samples to the: lab as soon as possillte after colJecUon to ensure that holdi.ng o!,vg.S3~lo1! lEo1:p; 

;~im,~~ 'o\'~'=llla me.t. Please fill CDC out comp!e-tEIY'1[) 6')(peDite sample log-In .. '0 ~ i: ';1 ........ 

...... _ •. r'"MI.-nI ....... · f'I.1n .. a<O:1CU." 

Was.te 

Waler ww lJLju~ l Food f() 

Trip Blank TB Solids 5 Micro--b!clogy Me 

rteld a.lail..'< FB I 

Preservative 

:0 • o. 

fi Analysis Requesled Z c 

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Z J: .... " J: ... Z '" 02: 0 z VI m :r .... ~ 0 

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R~j.,w D .. ;e T:rr,., 

B'I.(SiGni!.lJre) 

Field Sam pliny Notes: EQUIPMENT BLANKS AND FIELD BLMIKS ARE USED FDR 

INTERNAL LAB USE 0 N L YIN DT BILLAB LEI. NOT REPOR1EO U NLES5 REQUE5TE D ElY 

CUSTDl.IER_ . 

Fie.·.'.:D 

Craa.~ed D'/,MO 

Data:J.'3'o'J 5 

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CD 
Microbac Laboratories, Inc. Atlshurgh Division 

SAMPLE BOHLE & PRESERVATION RECORD ,"~,:, . 

, ., .. ,·H._l.l(2.i,...j-L!2_v-,",--_ 

"').' f<.l)v SOIL: ___ ~_ 

! . 

T. MET. 

---1 

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'J! Ii !'F~ r::u~~,er' .. ative tlaS b-p.en ch~r.}.; llle 11 limber and hott!e t~rpa will be entered into Um appropraile column. The'slatE=mentlPreserved al Lab" 9hou~d be Roted ne>...i to the sa:np'c {hat 

. '·P.; ~'.~ lie preserved. ' 

;·.H'·~~i·rrs 

.. ' '.1 ~i·',;.·ornsl.S;:lTnple· Uollle Slleel 

PRESt=RVATION CHECKED BY: OilTE 

Cr~ated By: :"·1I\D 

Or.la: 03.112J05 

R,;v. '1 

n ........ llr-ct .... nl ("'" ... fl'"",1 t:l" . n~r'I.,.~,;;11C:-{'\ 

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JAN-21-2009(WED) 07:54 CLAIRTON MUNICIPAL AUTHORITY (FAX)4122333249 P.020/029 

.' ,,"' 

..... ,r .... '.\~ .. . 'I 

" 

~;\~,:-;.r7c:}da]c.~ P_\ 15056-7::'-; 

PlwDe: 724-772-0610 Fax: 724-772-:1686 

SAMPLE SUBMISSION FOKM for OUTSIDE TESTING 

Senc R.esLllt~. "T:J 11M!.! \w~a'\tl-D'I ~ ... ~iGi:J~ac !....~:-2'r::b:i-;:.s -[ 00 IV'larshaiJ Drive 

Warrandala, ?A 15086 

PllDne: 724-T72-061 0 

Fax: 724-T72-1686 

Invoice To: (if different from abov~) ____ SAME. __________ _ 

SAMPLE IDEHTIFICATIOH COLLECTED' 

. as 8- lu-lK t.o-il "11'6 

I 

I -

I 

.. -

I .. 

I 

I 

I 

I 

P~linquj-shed 3vo Dale: 

j! 

I 

I 

I 

I 

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Data Submillad: _-"L~,,--.;!;-'\ i;;;,Cj",1 <1,,-i ____ _ 

Su::"mined 9v: c,n~/' '.,----,~-_~ "LI--"--" Or':ler No ·'-"I--'"\-~:;-;~" t ... ",.... r 1 ..... '1:::;;,:'17,. .... .,'\,. "))"'\1;' J r 

o I. 

P!sass C!re::k if Addition~1 ?$sistancG is Nt:l::!d2C: _____ · __ Rush Analysis Required 

Phone Results 

-------Fax Results 

MATP.lX ! I ANALYsiS REQUESTED 

100 lJW-1-ClJ!MlJ.- V hLk 

I 

• . 

I 

I 

I 

I 

I 

i 

i 

SPECIAL INSTRUCTIONS: I LA!30RATORY USE ONI, Y -. I ~:f~eived8y ___ '.''--_~---'- I :::"CL~_~ . f 

I IlmB!1 emp.: I I 

j ~onditiDn: . 

II' yustomer.l"o__. J R ., ~l . 

, apOrT ~O.: '_'''''_'~''''"''''''_"''''''''&_ f 

Revision: 0 
JAN-21-2009(WED) 07:54 CLAIRTON MUNICIPAL AUTHORITY (FAX)4122333249 P.021/029 

t§1#lI!Ii Laboratories LLC 

a mOl~ber of The GEL Group ING PO Box 30712 eil"I""lon. SC 29411 

2040 S'''"flC Road Charl .. ton. se 29407 

P 843.555.8171 F 843.766.117B 

January 09. 2009 

Ms. Polly McConahy 

Microbac Labs 

100 Marshall Drive 

Wr1Irendale, Penosylvania 15086 

Re; W~ndale • Non DE? Reportable 

WOI'k Order: 221666 

Dc.r Ms, McConahy; 

GEl. L.l)ol'atol'ie .. LLC (GEL) appreciates the opportunity to provide the enclosed an.lyticnl results for the 

samplc(s) we received on December 22.2008. This original dum report h"" been prepared and reviewed in 

accordance with GEL's .standard operating pro~durc5. 

Our policy is to provide high qillllity, pCI~onalized analytical services to cmlbJe you to. meeryour analytic:tl 

needs on tilnO every time. We trust llmt you willllnd eVerything in order and to your sotisf.ctioD. If you have 

any queslions, plo.so do nor. hesit.te to c:tll me at (843) 556-8171. ext, 4512. 

Enclosures 

problem solved 

~ 

Sincerely, 

Ann Skradski 

Proj~ct M~magcr 

Page 1 of 10 

www.gal.com 
JAN-21-2009(WED) 07:54 CLAIRTON MUNICIPAL AUTHORITY (FAX)4122333249 

GEL LABORATORIES LLC 

2040 Savage R03d CharleSlon SC 29407 - (843) 556-6171 - www.gel.com 

Certificate of Analysis Report 

for 

MILA001 M:icrobac Labs (STND) 

Client SDG: 221666 GEL Work Order: 221666 

The Qu3liriers hI tbi~ report are defined n.< e"uows: 

• A quality conlrol analyte recovery is outside of <pecificd acceptance criteria 

>i:'* Analyte is a surrogate compound 

U Analyte was analyzed for. but not detecred above the MDL. MDA. or LOD., 

Whore the analytical method has been pcrformed under NELAP certification. the analysis has mot all of the 

rcquircrncnL< of the NELAe standard UIlIe. .. qualified on tho Certificatc of Analysis. 

P.022/029 

The designa.tion ND, if prcsenr .. appe<lI"s in the rc;sulr. column when the analyr:e conC~l.rnlion is nor. der.ecr.ed above 

. the delection limit. . 

This data report bas br:.en prepared and reviewed in nccorrhmcc with GEL LaborJtories LtC 

smndard OpCf"dting procedures_ PI"as" di«"t any questions 10 your Project M:magcr. Ann Skradsl::L 

~------------ Review~dby 

Page 2 of 10 
JAN-21~2008(WED) 07:55 CLAIRTON MUNICIPAL AUTHORITY (FAX)4122333248 P.027/028 

. GEL LABORATORIES LLC 

2040 Savage Road Charleslon SC 29407';' (943) 556-8171 - www.gel.eom 

Certificate of Analysis 

Company: Microb3c Labs 

Address: 100 M=hall Drive 

W""tClld.,\e, Pcnnsylv.nill 15086 

Cont.o~ Ms. Polly MCCon.by 

Project: Wotrrcodtllc - Non DEP Report:.lb1c 

Client Samplc ill: 

SampleLD: 

Matri)" 

Collect Date: 

Rccci vo Date: 

Colloctor: 

0812-1478 

221666001 

WnSTeWatl:r 

·19-DEC-08 12:00 

22-DEC-08 

Client 

QmdiLicr Result Uncert.:linlY DL 

Rad Gas Flow Proportiooa1 Ct"tUDting 

GF"PC. Gross AlB. liquid 'i1s R~c(ttved" 

Alpha U 

'u 

ND 

4230 

The rullnwing AnalytieDJ Methods were performed 

Method DI$crlptlon 

1 EPA 900.0 

+/-155 

~/-216 

254 

215 

Page 3 of 10 

RL 

Rcport Date: Januury 9. 2009 

ProiecT' MlLAOa 104 

Client ill: Mil-AOOI 

UJlilG 

pCilL 

pCi/L 

lIF A.Daly,W.W Time Bateh Method 

oXl'3 01/05109 21>6 828558 1 

Amllytol Comments 
JNh21-2009(ifiJED) 07:55 CLAIRTON MUNICIPAL AUTHORITY (FAX)4122333249 P.028/029 

GEL LABORATORIES LLC 

2040 Savage Road CharlesTon. SC 29407 - (B43) 556-B171 - www.gel.com 

Contact: 

Micmbil:c Lal)" 

100 Mursbull Driyc 

Warrendal~ Pl.!nn!f)'Jvania 

Ms. Polly McConahy 

WurknrdCl"! 221666 

QCSummary 

Parmn9lne . __ .:.-' J:N,!!O~M~ __ -2S'O!wn~p,!!I,,~--.\Ql!"U!!nl'!..... __ Q!; ... ,.. tlnits R'PD% 

oKlid Gm; Flow 

Bmch 8:!.8658 

QCl:!01747181 221466UOl DUP 

Alpha. 

Bota 

QC12017471R4 LCS 

Alph. 

BelLI.. 

QCI20l747180 MB 

U 

114 

395 

0.977 U ·139 pCiIL 0 

,,·/·1.58 +1-1.29 

21.7 21.9 pCi/L 

... /-4.QS +1·3.98 

110 pCi/L 

.. 1·11.6 

354 pCiIL 

+1-14.9 

RCDOrt Date: Janu03ry 9. ZllU9 

l)age 1 of 2 

REe% ·:R~~~L~.ls~. __ Dat.e Time 

. N/A DXF3 Ollllo/U921,50 

(0% -100%) 

97 (75%-1"5%) 01l06/o92U6 

90 (15%·115%) 

Alpha U 0.552 pCiIL 01l0fil0921,5U 

+1-1.26 

I' u 1.00 pCi/L 

",·f·2.39 

QC120174718:! 221466001 MS 

Alpha l2~ U 0.977 271 pCiIL 119 (75%·125%) 01l06/0911:S0 

... 1-I.5R ... 1-25.7 

Beta 790 21.7 SS9 pCiIL 110 (75%-125%) 

;~-4.05 -t/-'J.9.S 

QCI2017471B3 221466001 MSI) 

Alpha 228 U 0.977 261 pCi/L 4 I1S (0%·20%) 01l06/0921:26 

.. /·I.5R +/ .. 28.8 

BeleL 790 21.7 8.59 pCiIL 3 lD6 (0%·20%) 

",/-4,05 .,.1-3~.9 

NOles: 

11,c QuaJiticO! in thili report ortl de:fined 3S follows: 

Analyt.e h~ a surrog'l.llc compound 

< R~uh i~ h::ss Us":l.n v~lIe reponed 

> Result is f..rc..1tCf [han vahle rep~rtecl 

A Ttl.: TIC iN U ~uspcCled :Udal-condensation product 

B FOr Gell~ Chelllistry nnd Organic analysilj Lhe LurscL unulYlC WtlS dc1.t:C1.ed In the associafed blank. 

BD Results arc either below lhe MOe Or lr'.J.c;errcco'Ycry is low 

C AT1Ollyt(; hou; been confirmed by GC/MS ruI~ysls 

D RC'~ulr-",.ate reponed from u diluted aliquot of the s.1mpJc 

F ERtimalcd Value 

I-l Arut1ytical holding time was c:::t;:l:eded 

Page 5 of 10 
JAN-21~2008(WED) 07:55 CLAIRTON MUNICIPAL AUTHORITY (FAX)4122333248 

GEL LABORATORIES LLC 

2040 Savage Road Charleston, SC 29407 - (843)556-8171 "www.gcl.com 

QCSummary 

Womorder: 

Pannname .. _____ " ____ --,N",O",M=_ 

J Vwuc is esrimated 

M M if .bo •• MOC and less ,Jmn ll.D 

M MaLtix Rdn~d Fililurc 

N/A RPD or %Rcc[)vc:ry limits. do nor apply. 

ND 

NJ 

R 

U 

ill 

x 

y 

Analyle com::cnt.roLion is nOl· dl!fe.Clcd above the detection limil 

Consult ew.~ Nan'::Itivc:, 'Data Sunumuy package. or Project MMilg!;.f cunct::rning mil> '-Iualili~r 

Sample fCljults o.rc: rejected 

Anul:yl~ was an:l1yzcd for. but nt~l dc,ectcd ahove the MDt., MDA. or LOI). 

Gamma Spc .. t.roscopy-UnceIUl.in idcntitlclllion 

Consult Case NaJT;1Dvc., Datil SummuIy pack:i1Sc. Dr Project M;ul!l~!:r concernIng this qUi11itIc;r 

QC Somplcs were noL spiked wll.h !his compound 

REC% 

h 

RPD of s.mlple and dupllcal.c ev.ulUatt!ld uliiny -I-/ ... RL. Cr.mccnlr.iltious arc .oX the RI .... Quolifie:t Nor Applicable for RaLiiochemisrry. 

Pn:parnr.ion tlr prcserv:n.i(ln holding time ~us exceeded 

indicares Llml.!:ipike recovery lill).j.rs do not apply wl1l;n Rample concenlrntiou exceed" lipikc CODe. by a rHetot of 4 or more. 

P.029/028 

~ Relati'\lc Percent DiITerellCC (RPD) obtained from ilic s::unplQ duplicate (1)tJP) is cva1u:nc:d ngainst the ~cceplance criterill when the sample is gJ.'LAuer thnn 

five limes (5X) the canrmcr required detcl;(.;on limit (RL). In Cill:i~ wbere ciLhcr!he s.1il1ple or duplicate value is less thun 5X lhe iUJt a oontrollirnir. (If 4-/ .. 11le 

RL is lll'~d l~ e\laluarc t.he DUP J.'esult • 

... TnLiitAltes rh~t tl Qufiliry Control parameter ",lUI nOl wirhin ~pecifications. 

For PS. ?SD, llnd SD.ll .. T results. tbe: vwucs listed arc the mC:3surcd amounts, !lor finn\ concc:mr;n.iom;,. 

where [.he an:liytiC::ll mJ:thod hilS been performed under NEJ ... AP certific.d.;on, the ana!YS1S has l1ll:t a.ll of rhe 

re(l"ir.mellts of Lb. NELAC su.ndard unIoss qualified on I\'" QC SUIDlllary_ 

Page 6 of 10 
JAN-21 -2009 (I~ED) 07: 54 CLAIRTON MUNICIPAL AUTHORITY (FAX)4122333249 

MICROBAC L.u30RATORI.l:::S, INC. 

100 Ma.rshall Drive 

Warrendale, FA 15086-7554 

Phone: 724-772-0610 Fax: 724-772-1686 

P.023/029 

SAMPLE SUBMISSION FORM for OUrs IDE; TESTING Page __ of __ _ 

Send Results To 

COmpiiny: 

Address: 

g~~~ar~~ 100 Marnhall Drive 

Warrendale, PA 15086 

Phone: 724-772-0610 

Fax: 724-772-1686 

Invoic" To: (if different from above) _______ .SN~E __ ~ ________ _ 

.. 

SAMPLE IDENTIFICATION COLLECTED 

. cg Jd.- \lflK !!:tll"l ~ 

Re/inquishe;d By: . Ciw ou:J-.--

.I SPECIAL INSTRUCTIONS: . 

==. ;: = 

FDrm Cowo] l'"D.: 0202051630 

Date Submitted: (8.\I'lf'i . Submitted Bv: ~ *-- PurchOl~e Order No.: W .UIil(~ .... ry . Please CheCK if Additional Assistance is Needed: 

______ Rush Analysis Required 

______ ,Phone Results 

______ ,Fax Results 

. 

MATRIX ANALYSIS REQUESTED 

1;)0 ~ nV.dtL ~ Ada: 

. 

Rovjsion: 0 

!:ia.t: : 020205 

I I 

, 
JAN-21-2009(WED) 07:54 CLAIRTON MUNICIPAL AUTHORITY (FAX)4122333249 

},HCROBAC LABORlHOPJES, INC. 

100 Marshall Drive 

Warrendale; P A 15086-7554 

Phone: 724-772-0610 Fax: 724-772~1686 

P.024J029 

SAMPLE SUBMISSION FORM for OUTSIDE TESTING Page. ___ ,of __ 

Send Results To 

Company: 

Address: 

M~r~datl~~s 1 DO Marsh~1I Drive· 

Warrendale, PA 15086 

Phone: .724-772-0610 

Fax: 724-772-1 6B6 

Invoice To: (if different from OIbove) ______ SAME,_~ _____________ _ 

SAMPLE IDENTIFICATION COLLECTED 

()'9. 1:1- I t..\ 40 . . 1a..II{r~ 

.. 

Relinquished By: Date: 

SPECIAL INSTRUCTIONS: 

Date Submitted: _-IIr<:lir<./!.t.:I'l1.llu[t.,-___ _ 

Submitted By: c..~ 

Purchase Order No.: t'15~&-. - .:u II 

h -- Please Check if Additional Assistanoe is Needed: _______ :Rush Analysis Required 

_______ Phone Results 

____ -'--_Fax Results 

MATRIX ANALYSIS REQUESTED 

Ilkl',", ~(lOMI~ t- RlJtc 

I 

, 

-----,------------,-'----,--....;...-- I LABORATORY U~ ON~ 

~;~:i~ed)Y: J(i'o"6J~: 

I~m"'~' ,Condition: , , ' 

, . -.!! 

,Custome~ No.: L Report No.: 

form Convoll'o.: 0202051630 R~vision: 0 

Dart: 02G2GS 
JAN-21-2009(WED) 07:55 CLAIRTON MUNICIPAL AUTHORITY (FP,X)4122333249 P.025/029 

. m3! I Laboratories LlC SAMPLE RECEIPl' & REVIEW FORM 

(t):c.r ..... h..r . ,,",,,,,, ~~ lLr. (" "'1,,-

IBy: R('1S !Dsle: I~ 1-.:>-\1 .... '1: 

Hazard Wormation ~ 

.. :@ .~. 'x2~rca I not matI:ed • contact 

... '~>r~" •. :! ,J, , CotQIlS 

, ". ~ n or III bvRSo1 ,/ Qr. h 

('r-.r"," .,. ,marked . PcBs? f 

lasaDOT: / UN//: .. , ;sO;i1 , . 

Sample Reeeipt Cdteria ;: II ~ Crunn>cntslQuaIir",,,, (Required for Non-Conrorming f!enzS) 

'~L'. _,. coul:liners =civet! intact and [; """".ro'" 

1 ~' ./ damaged enntaillCl" ~_1>i1ur o!b:< (d=ribo) 

'''' requirin~ cold presClVation / blue leo dryJ~ ~: .IborCo=ibc) 

icc ""'" 

:2 Iwithin 0 S 6 deg. C? IS'" 

3 

IChain of CU!llOdy documents included 

lwith shipment? 

I Cin:lo. .--

4 containers intact and scalcd7 ~ """'"""" bl:iIJi'~ o[bcr(~~) 

, .... 0<l0<I ..... 

5 1/ at proper pm .. , ... 

{; 

VOA vials ftee of beads pace (defmed os ./ 

<: 6mm bubble)? . 

/ ,.. . CI. 

7 A ~ 1>,,",,", contain= present? 

!8 ='ved within bolclln& titne? 

I,". .1. ID's on COC IJl3.Il:b ro'. on 

Is"""".8>·, . ,.-

.9 1 "",u"" , 

IOate &.limc on COC mall:b <lao:: & time 

ISIullp" ~ .ffoc'''''' 

1

10 Ion bottlcs7 

• 0 containers received march .~ . • "",=Cd: 

,11 on COC? 

COC fom> is properly signed in / 

III sectiOnS? 

. 

~'. ~b (,5" ')..51> 7Yo/A . . 

r-ag'" ~ or 1 Q DoO:: \ '7./.,,-ll I ~02 

revieW: :Initials ~ 1>'\.." PM (orPMA) 
JAN-21-2008(IfIJED) 07:55 CLAIRTON MUNICIPAL AUTHORITY (FAX)4122333248 

Lid or curr~nl GEL Certifications ,... of (19 Jonuary 20&9 

Stale 

CLlA 

~.ofNavy 

~da-NELAP 

O.t)rgi. 

L,eorg'. DW 

Haw.ii 

ISO 17U25 

I<labo 

,NELAP 

Inobn. 

M",a, - Nl;!LAP 

.-NELAP 

Nov.d. 

New J.n<.y - NELAP 

New MeX,co 

~'York- NJ;LAP 

North 

NOrtll ( ,DW 

South 

'exas - NELAP 

r-'u"", .. s"'.Dcpr, of 

Jtail-NELAP 

Virginia 

Page 10 of 10 

01151CA 

OEL 

PH-<l169 

NFESC413 

. WO::.15.1 

E87156 

ES7156 .AI" 

967 

N/A 

2567.01 

_ 2lJUU2" 

C-SC-OI 

90129 

03046 

270 

Nl-~'-Ul" 

SCOO0l2 

SCOUZ 

Fl. 715.§, 

. 11501 

233 

4$709 

9904 

1012000 lI10IZOOU2 

TN 02934 

GEL 

VTS?156 

_ 00151 

CIMI 

P,026/028 
Microbac Laboratories, Inc. Page I of I 

100 MARSfIALL DRIVE 

WARRENDALE, PA 15086 

(724) 772-0610 FAX (724) 772-1686 

TOM ZlERENBERG, MANAGING DIRECTOR 

http://www.microbac.com 

State Laboratory Certification Nmnbers: 

PADEP: 02-257, NC: 42703,WVDEP: 215,9951 CM KY: 90136 

CHbMlo"lKY . MlCKUHlULUliY . l'UUJJ OiAFbTY .. CUNOiUMbK PKUJJUCrOi 

WATbK· AJ:K. WASTbS· l'UUD· PHARMACbU'11CALS· NUTKACbUTICALS 

CLAIRTON :MUNICIPAL AUTHORITY 

MR. PATRICK CANA VAN 

I NORTH STATE STREET 

CLAIRTON, PA 15025 

Permit No.: 

Cust P.O.: 

CERTIFICATE OF ANALYSIS 

SUBJECT: Wastewater Samples for Radiological Analysis 

Date Reported: 

Date Received: 

Order Number: 

Invoice No.: 

Cust #: 

Sample Date: 

Sample Time: 

Sampler/Temp: 

lII4/2009 

121912008 

0812-00540 

38430 

CI23 

12/8/2008 

9:30 

TEST METHOD RESULT UNITS DATE TECH 

001 CNk3 Pitwater 

Collected 12/8/08@ 

Gross Alpha 

Gross Beta 

Submltted By: 

EPA 900.0 

EPA 900.0 

Managing Direct·o 

See Attached 

See Attached 

pOlL 01/03/09 

pCi(L 01/03/09 

The data and information on thiS, and other accompanying documents, represent only the sample(s) analyzed and is rendered upon condition 

that it is not to be reproduced wholly or in part for advertising or other Pl.Il'pOSeS without approval from the laboratory. 

U5DA-EPA-NIOSH Testing Food Sanitation Consulting Ch'emical and Microbiological Analyses and Research 

MEMBER 

'4{111 

*** 

*** 
[i1§Q I Laboratories LLC 

a member of The GEL Group INC PO 80x 30712 Charleston, SC 29417 

2040 Savage Road Charleston, SC 29407 

P 843.556.8171 F 843.766.1178 

J anuery 12. 2009 

Ms. Polly McConahy 

Microbac Labs 

100 Marshall Drive 

Warrendale, Pennsylvania 15086 

Re: Warrendale - Non DEP Reportable 

Work Order: 2210 II 

Dear Ms. McConahy: 

GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the 

sample(s) we received on December 11, 2008. This original data report has been prepared and reviewed in 

ac.cordance with GEL's standard operating procedures. 

Our policy is to provide high quality, personalized analytical services to enable yOll to. meet your analytical 

needs on time every time. ,Ve trust that you will fInd everything in order and to your satisfaction. If you have 

any guestions, please do not hesitate to call me at (843) 556-8171, ext. 4512. 

Sincerely, 

~ Ann Skradski 

Project Manager 

Enclosures 

Page 1 of 9 

problem solved 

www.geLcom 
GEL LABORATORIES LLC 

2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com 

Certificate of Analysis Report for . 

MILA001 Microbac Labs (STND) 

Client SDG: 221011 GEL Work Order: 221011 

The Qualifiers in this report are defined as follows: 

" A quality control analyte recovery is outside of specified acceptance criteria 

** Analyte is a surrogate compound 

U Analyte was analyzed for, but not detected above th"e 1vi[)L, MDA, or LOD. 

"\Vbere the analytical method has been performed under NELAP certification, the analysis has met all of the 

requirements of the NELAC standard unJess qualified on the Certificate of Analysis. 

The designation 1\11), if present, appears in the result column when the analyte concentration is not detected above 

the detection limit. 

This data report has been prepared and reviewed in accordance with GEL Laboratories LLC 

standard operating procedures. Please wect any questions to your Project Manager, Ann Skradski. 

Reviewed by 

Page 2 of9 
GEL LABORATORIES LLC 

2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com 

Certificate of Analysis 

Company: Microbac Labs 

Address: 100 Marshall Drive 

Warrendale, Pennsylvania 15086 

Contact: Ms. Polly McConahy 

Project Warrendale - Non DEP Reportable 

Client Sample ID: 

Sample ID: 

Matrix: 

Collect Date: 

Recejve Date: 

Collector: 

0812540 

221011001 

Waste Water 

OS-DEC-08 12:00 

lJ-DEC-08 

Client 

Parameter Qualifier Result Uncertainty DL 

Rad Gas Flow Proportional Counting 

GFPC, Gross AlB, l.iquid ''As Received" 

Alpha 

Beta 

33.2 

140 

The following Analytical Methods were performed 

Method Description 

EPA 900.0 

+/-9.67 

+/-11.8 

7.13 

8.94 

Page 3 of9 

RL 

5.00 

5.00 

Report Date: January 12, 2009 

Proiect: MlLAOOI04 

Client ID: MlLAOO 1 

Units 

pCiIL 

pCiIL 

DF AnalystDate Time Batch Method 

DXF3 01/03/09 2135 825351 

Analyst Comments 
GEL LABORATORIES LLC 

2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com 

Contact: 

"rorkorder: 

Parmname 

Rad Gas Flow 

M1crobac Labs 

100 Marshall Drive 

Warrendale, Pennsylvania 

Ms. Polly McConahy 

221011 

NOM 

Batch 825351 

QC1201739437 220707001 DUP 

Alpha 

Beta 

QCJ201739440 LCS 

Alpha 57.0 

Bela 198 

QC1201739436 MB 

Alpha 

Beta 

QC1201739438 22070700] MS 

Alpha 114 

Beta 395 

QC1201739439 220707001 MSD 

Alpha 114 

Beta 395 

N:Jtes: 

The Qualifiers in this report are defined as follows: 

** Analyte is a surrogate compound 

< Result is less than value :reported 

> Result is greater than value reported 

A The TIC is a suspected aldol-condensation product 

QCSummary 

Sam~le Qua] QC Units RPD% 

10.4 11.8 pCilL 13 

+/-3.09 +/-2.96 

17.8 12.5 pCilL 35 * 

+/-2.68 +/-2.14 

57.0 pCifL 

+/-6.14 

195 pCilL 

+/-7.67 

U 0.313 pCifL 

+/-0.529 

U 0.996 pCifL 

+/-0.993 

lOA 92.1 pCifL 

+/-3.09 +/-9.31 

17.8 421 pCifL 

+/-2.68 +/-11.6 

10.4 120 pCifL 26 * 

+/-3.09 +/-11.4 

17.8 409 pCifL 3 

+/-2.68 +/-11.8 

B For General Chemistry and Organic analysis the target analyte was detected in the associated blank. 

BD Results are either below the MDC or tracer recovery is low 

C Analyte has been confirmed by GCfMS analysis 

D Results are reported from a diluted aliquot of the sample 

F Estimated Value 

H Analytical holding time was exceeded 

Page 4 of 9 

ReDort Date: January 12, 2009 

Page lof 2 

REC% Range AnI,! 

(0% - 100%) D)(F3 

(0% - 20%) 

100 (75%-12S%) 

99 (75%-125%) 

72* (75%-125%) 

102 (75%-125%) 

96 (0%-20%) 

99 (0%-20%) 

Date Time 

01103/0921:34 

01106/09 1859 

01/03/0921:34 

01103/0921:34 

01103/0921:34 
GEL LABORATORIES LLC 

2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gei.com 

QCSummary 

Workorder: 221011 Page 2 of 2 

Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time 

J Value is estimated 

M M if above MDe and less than LLD 

M Matrix Related Failure 

NI A RPD or %Recovery limits do not apply. 

ND Analyte concentration is not detected above the detection limit 

NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier 

R SampJe results are rejected 

U Analyte was analyzed for, but Dot.detected above the MDL, MDA, or LOD. 

til Gamma Spectroscopy--Unccrtain identification 

X Consult Case Narrative, Data Sununary package, or Project Manager concerning this qualifier 

Y QC SampJes were not spiked with this compound 

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. 

b Preparation or preservation bolcling time was exceeded 

N/ A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more. 

"Tfle Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than 

~ times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X theRL, a control limit of +/- the 

KL is used to evaluate the DUP result. 

*" Indicates that a Quallty Control parameter was not within specifications. 

For PS, PSD, and Snll..T results, the values listed are the measured amounts, not frnal concentrations. 

Where the analytical method has been performed under NELAP certification, the analysis has met all of the 

requirements of the NELAC standard unless qualified on the QC Su=ary. 

Page 5 of 9 
r---------

GEL Laboratories LLC 

Form GEL-NCR 

Rev. 06/05 

Mo.Day Yr. 

OB-JAN-09 

Instrument Type: 

GFPC 

Batch )0: 

825351 

COMPANY - WIDE NONCONFORMANCE REPORT 

Division: Quality Criteria: 

Radiochemistry Specifications 

Test / Method: Matrix Type: 

EPA 900.0 Liquid 

Sample Numbers: 

See Below 

NCR Report No.: 646092 

Revision No.: 

Type: 

Process 

Client Code: 

MILA, NFSR, RHOD 

Potentially affected work order(s)(SOG): 220706(OB-CAH-1 09),220707(08-CAH-1 07),220709(08-CAH-1 08),221 011 ,221099 

Application Issues: 

Failed Recovery for MS/PS 

Specification and Requirements 

I 

NRG Disposition: 

Nonconformance Description: 

1. The matrix spike 1201739438 did not meet the alpha recovery 1. Reporting results. 

requirement. The matrix spike duplicate 1201739439 did meet the 

recovery requirement. The matrix spike and the matrix spike duplicate 

have a relative error ration of 1.7582. 

Originator'S Name: Data Validator/Group Leader: 

Nat Long OB-JAN-09 Heather McCarty 12-JAN-09 

Quality Review: 

Director: 

Page 6 of 9 
--rc------ ---

/ 

MICROBAC LABORATORIES, INC. 

100 Marshall Drive 

Warrendale, PA 15086-7554 

Phone: 724-772-0610 Fax: 724-772-1686 ~~IDII 

SAMPLE SUBMISSION FORM for OUTSIDE TESTING Page. __ ---'of, __ _ 

Send Results To 

Company: 

Address: 

Poli1 flWb~ Microbac Laboratories 

100 Marshall Drive 

Warrendale, PA 15086 

Phone: 724-772-0610 

Fax: 724-772-1686 

Invoice To: (if different from above) _______ SAME. ________________ ___ 

SAMPLE IDENTIFICATION COLLECTED 

(fA!d- 540 \~\~k 

Date S ubm itted: loil 11 r 

Submitted By: DtYiL 

Purchase Order No.: cof"i'»)i.A-eaPlease Check if Additional Assistance is Needed: 

_______ Rush Analysis Required 

_______ .Phone Results 

_______ F,ax Results 

MATRIX ANALYSIS REQUESTED 

WW r Jh fiJJ).- () 0 d J. 'F.It! J 11 '> 

-

Relinquished By: Date: 

SPECIAL INSTRUCTIONS: 

II . 

Fonn Control No.: 0202051630 

LABORATORY ~ ONL~ Received By: ~ fl'ltY'--

Date: I ~-I -0 

TimefTemp.: 

Condition: 

Customer No.: 

Report No.: 

Revision: 0 

Dale: 020205 

~~Q I , d ( IMlla) 
mag Laboratories LLC SAMPLE RECEIPI' & REVIEW FORM 

-rn ;(I/l 0 hrxl' 7 ~,. c:uc/' cOrd.~ - 2Z1(fll' 

By: ?4.f\ fi.l. Iz·I)-O'( ~ 

t r~:' -Dun,. >~:::; ~ 01 • 

' DOl marl:ed • contact Hazard Information ;:.. Z 

,marked as. " ,Counts' , r:z () (ij;>(Y\ 

,II or III by RSO? v: 

; marked :pCsS? V 

lasaOOT ,/ I Class UN#: 

, as! , Soil? ,/ 

Sample Receipt Criteria :! ;2' Z Comments/Qualifiers (Required for Noo-Conforming Item<) 

1 

containers JeCeived intact and J £bm3ged CCIi:lbiDer 

~ ,. ~ COJll.ainer Otbr::r (de:$cribe) 

requiring cold preservation dryic:e ~1y~,(O=rireJ ice bog> 

'2 j blue ice 

IWithin 0 :; 6 deg. C? , 

3 

!Chain of custody documents included 

'with shipment? 

j I CUclo Applical>k: ' 

,.,.., _on 

4 

~ damaged cootaioec .. 1caDng=- alba (dc,aibe) 

containers intact and sealed? 

-

IJ 5 requiring chemical 

". p<opex pH? added,. LotOo 

VOA vials free ofheadsP= I •• 

6 < 6rom bubble)? ' I.J 

7 Are EOCOi"e containers present? V 

Id'.od tests,_ 

'8 leceived within holdiDg time? 

. ~'. on CDC match ID', on , . ,-

'9 

1"'''''->< ~ 

110 

jDare & rime on CDC match date -Ik time I No f'htd1Cm.v f,:)f\ \f)f\1(J \ VI QA Ion hottles? , 

'v, , match ' I (lflf'tf(f ~ fl 0 1 Pet-O J1 f{J ,J III indicated on cae? 

112 

ICue ~ is p<opedy 'i~eiI in 

:;ecbons? 

r~6{ I 

'](Y(i5' Z?:15 zwqg 

I ~ (-'age 8 ot!i Dare / ..;)-//1 10";< , y, 

or P.MA) review: Initials ~ E I 

PM( 
List of current GEL Certifications as of 12 January 2009 

State r 

Arizona ~ 

88-0651 

CLIA 

i- 01151CA 

GEl 

pj:i: 1"i;9 

Dept. of Navy NFESC413 

EPA Region 5 

Florida - NELAP E87i56 

Georgia E87156 (Fj 

GeorgiaDW 967 

Hawaii N7A 

ISO 17025 2567.01 

Idaho SCOOO12 

Ilhnois - NELAP 200029 

Indiana -OiL-VJ 

Kansas - NELAP 

90129 

-NELAP 03046 

270 

Nevada 

New Jersey - NELAP SC002 

New Mexico m APE87156 

New York - NELAP J.15Ol 

North ' 233 

North ,DW 45769 

9904 

·NELAP 

South 7I' 

T, TN 02934 

Texas - NELAP T 

U.S. Dept. of S-52597 

.AP GEL 

VT871S{ 

Virginia 00151 

C1641 

Page 9 of9