# CLAIRTON MUNICIPAL AUTHORITY ALLEGHENY COUNTY, PENNSYLVANIA TECHNICAL EVALUATION OF THE IMPACT OF OIL AND GAS WELL WASTEWATERS ON THE CLAIRTON MUNICIPAL AUTHORITY WASTEWATER TREATMENT FACILITY NPDES PERMIT No. PA0026824 FEBRUARY 2009



# KLH· ENGINEERS, INC. 5173 CAMPBELLS RUN ROAD PITTSBURGH, 

### PA 15205-9733

### Clairton Municipal Authority Technical Evaluation ofthe Impact of Oil and Gas Well Wastewaters on the Clairton Municipal Authority Wastewater Treatment Facility
Table of Contents

1.0 Purpose

.......................................................................................................................................... 1 2.0 Description ofCMA Treatment Processes

.................................................................................... 1 3.0 Evaluation ofTotal Dissolved Solids and Chlorides on Process Units

......................................... 3 4.0 CMA Sludge Treatment and Disposal.

.......................................................................................... 6 5.0 Summary ofConclusions

..............................................................................................................7

Tables Table 1.0

Appendices Appendix A AppendixB AppendixC AppendixD AppendixE AppendixF

Clairton Municipal Authority 

### Net Impact ofCMA Effluent on Background Levels ofIDS and Chlorides

Oil and Gas Wastewater Manifest Spreadsheet CMA Process Flow Diagram Detailing Sample Locations CMA Chloride and TDS Analytical Data Table 3-16 "Typical Composition ofUntreated Domestic Wastewater," Metcalf& 

### Eddy, Third Edition, Wastewater Engineering CMA BOD and TSS Inter Process Data and MACM Weekly Operations Reports Radiological Analysis ofCNX-1 and CNX-3 Wells

Technical Evaluation of the Impact of Oil and Gas Well Wastewaters on the Wastewater Treatment Plant February 2009 Ref. No. 273-46 1 

## KLH ENGINEERS, INC.**---------------------------------------~**



## 1.0 Purpose
The Pennsylvania Department of Environmental Protection (PADEP) issued an Administrative Order to the Clairton Municipal Authority (CMA) on October 23, 2008. The Adrrtinistrative Order sets forth a series of requirements prescribed to CMA, in order for CMA to continue acceptance of oil and gas well production wastewater for treatment and processing at the CMA Wastewater Treatment Plant (WWTP). The purpose of this document is to provide a written technical evaluation of potential impacts of oil and gas production wastewaters on the CMA treatment process. This evaluation will 

### contain, as prescribed in the Order; an evaluation of the effects on each major unit process; an estimate of the maximum Total Dissolved Solids (IDS) that will occur in each process; a description of measures employed by CMA to monitor and minimize adverse effects on biological processes; quantitative estimates on anticipated changes to effluent characteristics for each new pollutant identified; a description of how CMA will assure that the WWTP sludge will not be classified as hazardous waste as a result of accepting this new waste stream, and any resulting constraints on sludge treatment and disposaL 

## 2.0 Description of CMA Treatment Processes
The CMA WWTP is a conventional activated sludge, secondary wastewater treatment facility. The planthas a permittedhydraulically treatment capacity of 6.0 million gallons per day (mgd). The CMA 2007 Annual Chapter 94 Waste Load Management Report indicates the annual average flow to the WWTP in 2007 was 3.994 mgd. The maximum monthly average day flow was 5.46 mgd, occurring in March of 2007, and the minimum monthly average flow was 2.919 mgd, occurring in October 2007.
The Order requires CMA to immediately restrict the daily volume of oil and gas well production wastewater to 1% 

### of the average daily flow. To comply with this requirement CMA has limited the daily volume of Oil and Gas well production wastewater introduced into the WWTP to 1%

### ofthe WWTP's forward flow rate on any given day.
The CMA receives the oil and gas well production water at the influent manholejustup-stream of the influent pumping station. Water is received into the wet well and subsequently introduced into the WWTP process via the raw sewage pumps. Trucks discharge typically 4,000 gallons of waste over a period of approximately ten to fifteen minutes. This translates to waste being introduced into the pumping station at a rate of between 267 and 400 gallons per minute. The actual volume of waste received is limited and does not exceed 1% of the estimated daily flow volume. Typically Clairton will accept up to 37,500 gallons during a one dayperiod.

Clairton Municipal Authority Technical Evaluation of the Impact of Oil and Gas Well Wastewaters on the Wastewater Treatment Plant February 2009 Ref. No. 273-46 

### 1 

## KLH ENGINEERS, INC.

### CMA monitors each individual waste load received from oil and gas well production wastewater sources. Included in this record is the date received at CMA; the hauling company transporting the waste to CMA; the manifest number identifying the load received at CMA; the well or point source from which the wastewater was generated; and the quantity of the wastewater received. CMA is 

### currently purchasing testing equipment which will allow plant operational personnel to test and monitor the level of chlorides and IDS in the wastewater received in (mg/l). Once the testing equipment is obtained and staff trained in its operation chloride and IDS levels in each load will be monitored and recorded. The corresponding mass load of chlorides and IDS in the wastewater received will

### be determined and recorded, as well as the pH of the wastewater. This data is 

### recorded and stored in a spreadsheet format by CMA operation staff. The information contained in this spreadsheet will be filed with the CMA monthly discharge monitoring report (DMR) to PADEP as required under the Order. A copy of thehaulingrecords and data is contained in Appendix A of this report. By CMA monitoring chloride levels in the received wastewaters CMA will have the ability to control the quantity, rate and mass of chlorides introduced into the treatment process. This will provide CMA's operations staff with a level of control to protect the biological process from upset, and control the level of pass through to assure water quality criteria is met. CMA will also sample each load and store each sample for a period of five days. This sample will 

### be available for complete analysis of all 

### priority pollutants listed in PADEP's Administrative Order should any adverse effects be observed within the plantprocesses. CMA employ's Pennsylvania state licensed operators who monitor, regulate and control all aspects of the WWTP process twenty four hours a day, seven days per week, fifty two weeks per year. The professional training and experience of these state licensed wastewater treatment plant operators provides CMA another level of assurance the introduction of oil and gas well wastewaters can be conducted, monitored and controlled to achieve the desired water quality limits while preserving the biological treatmentprocess, and plantperformance. The CMA facility is comprised of the following treatmentunit process:


## • Mechanical screening 

## • Gritremoval 

## • Comminutor 

## • Pre-aerationbasins 

## • Primary clarifier settling tanks 

## • Activated sludge process tanks 

## • Final clarifier settling tanks 

## • Aerobic digestion 

## • Sludge thickening tanks 

## • Gravitybeltthickener 

## • Sludge dewatering (centrifuge) 

## • Chlorine disinfection system
Clairton Municipal Authority Technical Evaluation ofthe Impact of Oil and Gas Well Wastewaters on the Wastewater Treatment Plant February 2009 Ref. No. 273·46 

### 2 

## KLH ENGINEERS, INC.

### Oil and gas well production wastewaters received is applied to the raw sewage wet well at a rate no greater than 1% of the plants daily forward flow. In the wet well the oil and gas production water is combined with domestic raw sewage from Clairton, Jefferson Borough, South Park, Finleyville, Nottingham, Peters Township and Union Township. This combined waste stream is screened, de-gritted and comminuted prior to discharging into the pre-aeration tanks. Primary Settling of the waste stream occurs after pre-aeration. Solids that are removed during the primary settling process are sent to the sludge thickening and aerobic digestion processes for stabilization of the bio-solids. CMA conducts an annual priority pollutant scan on its produced sludge for all Form 43 listed parameters. After the primary clarification settling tanks the plants flow enters the activated sludge tanks. During this process the plant operators closely monitor control points for Sludge Volume Index (SVl), and Food to Micro-organism Ratio (F/M). By monitoring these control points regularly the plant operations staff can determine if any adverse effects to settling or treatment capability are observed. If 

### any adverse effects were noticed the operating staff would immediately stop receiving the oil and gas well wastewater and have the most recent loads received analyzed for all priority pollutants listed in the PADEP Administrative Order to determine which load may be the source of a potential upset. A biological microscopic evaluation is also completed periodically by the operating staff. Samples of activated sludge mixed liquor are collected and analyzed under a high powered microscope to determine the overall health of the biological system. Any adverse effects noticed during the microscopic evaluation would also trigger CMA to stop the receipt of oil and gas productionwastewater. When the forward flow leaves the activated sludge process it enters the final clarifier settling tanks. Here the mixed liquor activated sludge is settled and separated from the liquid stream and returned to the activated sludge tanks via the return activated sludge pump system. Periodically, as required to maintain the desired sludge age and to maintain proper settling characteristics; sludge will be wasted to and aerobic digesters.
After final settling the treated water is conveyed to the chlorination system where pathogenic disinfection via chlorine gas injection is completed. After chlorination the flow is transferred into the chlorine contact tanks to provide sufficient contact time for the disinfection process to be completed prior to discharge into Peters Creek. CMA's effluent discharges into Peter's Creek approximately 2,000 feet from the mouth of Peters Creek where Peters Creek flows into the Monongahela River atRiver Mile Index 19.66. 

## 3.0 Evaluation of Total Dissolved Solids and Chlorides on Process Units
CMA began to collect 24 hour flow proportional composite samples to evaluate the levels of chlorides and IDS which occur under normal waste load conditions and which occur during days which the WWTP is processing oil and gas well wastewater. CMA selected six sampling

Clairton Municipal Authority Technical Evaluation of the Impact of Oil and GasWell Wastewaters on the Wastewater Treatment Plant February 2009 Ref. No. 273-46 

### 3 

## KLH ENGINEERS, INC.**~~~~~~~---------------~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~-**



### locations as key areas within the WWTP to monitor IDS and chloride levels. These sampling points can be seen on the CMA Process Flow Diagram included in Appendix B, which shows the location of each of the six sampling points. A complete listing of the sample results for IDS and chlorides at all six sampling locations is contained in Appendix C ofthis report.
The first sampling location monitored by CMA is the influent sampling point. The purpose of collecting the influent sample is to provide CMA with the typical level of IDS and chlorides which occur in CMA's influent, with contributions from oil and gas well wastewater and domestic sewage prior to the waste stream entering CMA's process tanks. During the week long testing the influent test results for both IDS and chlorides were relatively consistent. IDS values in the influent ranged from 664 mg/l to 1980 mg/l. These levels of IDS would indicate concentrations thatwould be found in typical strong strength domestic sewage. Chloride levels in the influent samples ranged from 183 mg/l to 843 mg/l. Chloride levels of 100 mg/l are considered to be a strong concentration in untreated domestic sewage, according to Table 3-16, of Metcalf and Eddy. Third Edition. Wastewater Engineering. Table 3-16 is included in Appendix D ofthis report.
Grab samples were also taken and analyzed for oil and gas well wastewaters received at CMA from the two well sources, CNX-1 and CNX-3. The analysis of CNX-1 and CNX-3 waste waters, as required under the Administrative Order, are also included in Appendix A.
The results of the samples taken and analyzed through the CMA WWTP indicate that there is little to no reduction in concentration of IDS and chlorides through the plant processes. This is not unexpected as conventional sewage treatment facilities are not designed to remove dissolved constituents such as IDS and chlorides. Although there is no apparent reduction in IDS or chloride concentrations through the treatment process, the introduction of oil and gas well wastewaters has had no effect on the treatment ability of the CMA system to treat and remove conventional pollutants such as Biochemical Oxygen Demand (BODs) and Total Suspended Solids (TSS). Appendix E. contains effluent data for BODs and TSS through the CMA process during the introduction of oil and gas well waste water. The data contained in Appendix E shows the removal of BODs and TSS during the December 8, 2008 to December 12, 2008 testing period was consistently observed, producing an average effluent CBODs of 8.94 mg/l and an average effluent TSS of 8.36 mg/l. These levels of removal exceed the NPDES permit requirements for these pollutants and provide a good indication the process is performing well during the introduction of oil and gas well wastewater into the process. Microscopic analysis conducted periodically on the activated sludge mixed liquor has shown that the biological process has remained healthy and viable during the introduction and processing of oil and gas well waste waters.
To evaluate the potential impacts that the discharge of IDS and chlorides may have on the Monongahela River, an evaluation utilizing the same analytical approach CMA would use to conduct a Head Works Loading analysis to developmentLocalLimits has beenutilized. Clairton Municipal Authority Technical Evaluation of the Impact of Oil and Gas Well Wastewaters on the Wastewater Treatment Plant February 2009 Ref. No. 273-46 

### 4 

## KLH ENGINEERS, INC.

### The following Monongahela River flows were utilized for the purpose of this evaluation:
Chronic Evaluation: Q7-10 = 

### 350 cfs, or 226 million gallons per day
Acute Evaluation: Q,-10 = 

### 494 cfs, or 319 million gallons per day
Human Health: Harmonic Flow = 

### 2860 cfs, or 1,847 million gallons per day By utilizing the CMA effluent data collected and analyzed for IDS and chlorides we can determine the effective impact these levels have on the Monongahela River during the above referenced flow periods. We will analyze the impact of the effluent IDS and chlorides at the maximum effluent levels and at the average levels recorded during the one week testing period and apply these loads to the various river flows to determine the net effect CMA's effluent has onthe Monongahela River. Average IDS level 

## = 974 mg/l
Maximum IDS level = 

### 1250 mg/l Average Chloride level 

## = 347 mg/l
Maximum Chloride level = 

### 520 mg/l
Applying each to the following formula the net effect for each can be determined at the various river flows.
Effluent conc. Cmg/ll x Plant flow rate Cmgdl = 

### Net effect to background level (mg/l) Monongahela River Flow Rate (mgd)

Clairton Municipal Authority Technical Evaluation of the Impact of Oil and Gas Well Wastewaters on the Wastewater Treatment Plant February 2009 Ref. No. 273·46 

### 5 

## KLH ENGINEERS, INC.- - --- -- ----------- -------------



### Table 1.0
Net Impact of CMA Effluent on BackgroundLevels of TDS and Chlorides
Net Increase in Receiving Water Levels Max Avg Max Avg IDS IDS Chlorides Chlorides (mg/l) (mg/l) (mg/l) (mg/l) River Flow (mgd) 1250 974 520 347 Q7-10 

### 226 24.28 18.92 10.10 6.74 Q,-,O 

### 319 17.20 13.40 7.16 4.78 Harmonic 1,847 2.97 2.32 1.24 0.83
Note: Average daily plant flow of4.39 mgd utilized for calculation
Table 1.0 clearly shows the resulting increase in levels of IDS and Chlorides attributable to the CMA effluent on the Monongahela River during the most critical Q7-10 

### river flow is very small, less than 25 mg/l for IDS, and less than 11 mg/l for chlorides. The monthly average limit for potable water supply criteria in source waters for IDS is 

### a monthly average of 500 mg/l and a maximum value of 750 mg/l. The net increase in IDS of 25 mg/l under Q7-10 

### conditions is only 5% of this limitation and only 3.33% of the maximum allowed. The limit to meet potable water supply criteria for chlorides is 250 mg/l in source waters. The net increase from the CMA effluent of 11 mg/lunder Q7-10 

### conditions is 4.4% of the limit.
As a result of the data presented and the analysis conducted it is the opinion of KLH Engineers, Inc. that the introduction of oil and gas wastewaters under the conditions prescribed above causes no adverse effects to the CMAbiological treatment process and no discernable impact on the receiving waters of the Monongahela River.
4.0 

### CMA Sludge Treatment and Disposal
The CMA currently employs two (2) aerobic digesters to digest and stabilize biologically active waste solids for its treatment process. Once stabilized the solids are thickened and dewatered via a centrifuge. Dry, stabilized cake solids are then hauled to the Waste Management (Elizabeth) landfill for final disposal. Annually the CMA conducts a Form 43 analysis to maintain its permit with the landfill fro sludge disposal. To determine if 

### the acceptance of oil and gas well wastewaters poses any harmful effects to CMA's current method of sludge stabilization and treatment a comparison of analytical data prior to the acceptance of oil and gas well waste water was and analytical data obtained after the acceptance of oil and gas well wastewater was conducted.

Clairton Municipal Authority Technical Evaluation of the Impact of Oil and Gas Well Wastewaters on the Wastewater Treatment Plant February 2009 Ref. No. 273-46 

### 6 

## KLH ENGINEERS, INC.**-----------------------------------------~-**



### Comparison of sludge data prior to the acceptance of oil and gas well wastewaters and sludge data after the acceptance of oil and gas well wastewaters indicates there is little change in the consistency, or quality of sludge at CMA. Should levels of any monitored substance in their sludge begin to increase to a level which would cause the sludge treatment or disposal practices to be come at risk CMA will limit or halt receiving oil and gas well wastewaters contributing to this increase.
CMA sludge is screened for radioactivity at the Waste Management landfill prior to acceptance, but because low level, Normally Occurring Radioactive Materials (NORM) are known to be present in oil and gas well waste waters in certain areas, CMA has conducted radiological analysis of both the CNX-l and CNX-3 source wastewaters received from oil and gas well operations for NORM. The results of the radiological testing for CNX-l and CNX-3 oil and gas well wastewater, is contained in Appendix F of this report. CMA will continue to rely on the landfill monitoring of sludge received for NORM and will halt receipt of such wastes if it is determined to contain such materials. 

## In addition, CMA requires that the generator certify that the wastewaterbeing received is not classified as hazardous waste. By continuing to closely monitor their sludge for metals, PCB's, Herbicides, Pesticides, Volatile, Semi-volatile Organics, and NORM, CMA will be able to assure that the current methods utilized to treat, stabilize and dispose of their sludge are protected and maintained and that their sludge will notbe classified as a hazardous waste.
CMA has also limited oil and gas production water received from any individual source well to less than25,000 gallons per day. 

## 5.0 Summary of Conclusions


## In conclusion, the current program for the acceptance of oil and gas well wastewater as it is currently being conducted at the CMA WWTP provides for both the protection of the CMA process, and the protection of the receiving waters of the Monongahela River for its intended use, and will not adversely impact the level of Total Dissolved Solids or Chlorides in the Monongahela River. CMA has instituted record keeping, quality control and process monitoring programs to assure it can sufficiently monitor the treatment plant process, and the effluent water quality to meet permit compliance. Monthly monitoring data for chlorides and IDS in CMA's effluent has been and will continue to be filed with CMA's monthly Discharge Monitoring Report (DMR).

Clairton Municipal Authority Technical Evaluation of the Impact of Oil and Gas Well Wastewaters on the Wastewater Treatment Plant February 2009 Ref. No. 273-46 

### 7 

### KLH ENGINEERS, INC.

### ApPENDIX A OIL AND GAS WASTEWATER MANIFEST SPREADSHEET

### I'·



# J 

# I MONTH: DECEMBER 

# )CMA TRUCK HAULING TOTALS FOR SHIPMANS

. \,:",:" 

# i:&QUROl=i.t i\

. 

# :MANIFEST4l", .',

.... 

# <.:DATE? ;, 

# I.G.ALl.j$N$E'

.

# ..·%.$6LIDS··.······**~'''/i.:'':·**, :. .___"i-,o,,·

__ _ ):,.',,'-':-."

__**::,--,'>5~<_ ~**  

### dravosburg 9634 12/3/2008 

# 4eee dravosburg 9636 12/3/2008



### - 4gQg port-a-john 9290 12/5/2008 

### Ge6 CNX#3 Pitwater 9678 1218/2008 

### 4000 CNX#3 Pitwater 8823 12/8/2008 

### 4500 CNX#3 Pitwater 9103 12/8/2008 

### 4000 CNX#3 Pitwater 9663 12/8/2008 

### 4000 CNX#3 Pitwater 9638 12/8/2008 

### 4000 CNX#3 Pitwater 9284 1218/2008 

### 4000 CNX#3 Pitwater 8824 12/8/2008 

### 4500 CNX#3 Pitwater 9640 12/8/2008 

### 4000 CNX#3 Pitwater 9105 12/8/2008 

### 4000 CNX#3 Pitwater 9106 12/9/2008 

### 4000 CNX#3 Pitwater 9641 12/9/2008 

### 4000 CNX#3 Pitwaler 8825 12/9/2008 

### 4500 port-a john 9696 12/9/2008 

### 356 CNX#3 Pitwaler 9107 12/9/2008 

### 4000 CNX#3 Pitwater 9331 12/9/2008 

### 4000 CNX#3 Pitwater 9643 12/9/2008 

### 4000 .CNX#3 Pitwater 8828 1219/2008 

### 4500

);NX#3 Pitwater 8827 1219/2008 

### 4500 CNX#3 Pitwater 9642 12/9/2008 

### 4000 CNX#3 Pitwater 9274 12/10/2008 

### 3500 port-a-john 9273 12110/2008 

### 59Q CNX#3 Pitwater 8829 12110/2008 

### 4500 CNX#3 Pitwater 6944 12/10/2008 

### 4000 CNX#3 Pitwater 9287 12/10/2008 

### 4000 CNX#3 Pitwater 9335 12110/2008 

### 4000 CNX#3 Pitwater 9645 12/10/2008 

### 4000 dravosburg 9280 12/10/2008 

### qggO ONX#3 Pitwater 9334 12/10/2008 

### 4000 CNX#3 Pitwater 8830 12/10/2008 

### 4500 CNX#3 Pitwater 9281 12/11/2008 

### 4000 CNX#3 Pitwater 8831 12/11/2008 

### 4500 CNX#3 Pitwater 9370 12/11/2008 

### 4000 CNX#3 Pitwater 9647 12111/2008 

### 4000 CNX#3 Pitwater 9332 1211112008 

### 4000 CNX#3 Pitwater 9371 12/11/2008 

### 4000 CNX#3 Pitwater 9226 12111/2008 

### 4000 CNX#3 Pitwater 9404 12/11/2008 

### 4000 CNX#3 Pitwater 8833 12/11/2008 

### 4500 CNX#3 Pitwater 9224 12-Dec 4000 CNX#3 Pitwater 9407 12/12/2008 

### 4000 CNX#3 Pitwater 9374 12/1212008 

### 4000 "-NX#3 Pitwater 9337 12/12/2008 

### 4000**~X#3** 

### Pitwater 9409 12113/2008 

### 4000

### CNX#3 Pitwater 9263 12/1312008 

### 4000 CNX#3 Pitwater 9376 1211312008 4000 CNX#3 Pitwater 9341 12/1312008 

### 4000 CNX#3 Pitwater 9340 12113/2008 

### 4500 CNX#3 Pitwater 9431 12/1512008 

### 4500 CNX#3 Pitwater 9346 12/1512008 

### 4000 CNX#3 Pitwater 9271 12/1512008 

### 4000 CNX#3 Pitwater 9383 12/1512008 

### 4000 CNX#3 Pitwater 9345 12/1512008 

### 4000 CNX#3 Pitwater 9272 12/1512008 

### 4000 CNX#3 Pitwater 9430 1211512008 4500 CNX#3 Pitwater 9384 12/1512008 

### 4000 port-a john 9447 12/1612008 

# --**3~e** 

### CNX#3 Pitwater 9446 12/1612008 

### 3700 CNX#3 Pitwater 9386 12116/2008 

### 4000 CNX#3 Pitwater 9351 12/1612008 

### 4000 CNX#3 Pitwater 9680 12/16/2008 

### 4000 CNX#3 Pitwater 9434 12/16/2008 

### 4500 CNX#3 Pitwater 9435 12/1612008 

### 4500 CNX#3 Pitwater 9350 12/1612008 

### 4000 CNX#3 Pitwater 9388 12116/2008 

### 4000 CNX#3 Pitwater 9441 1211712008 4500 CNX#3 Pitwater 9356 1211712008 4000 CNX#3 Pitwater 9440 12117/2008 

### 4500 <::NX#3 Pitwater 9355 12/17/2008 

### 4000 ':':NX#3 Pitwater 9354 12/17/2008 

### 4000 CNX#3 Pitwater 9439 12/17/2008 

### 4500 CNX#3 Pitwater 9353 12117/2008 

### 4000 CNX#3 Pitwater 9438 1211712008 4500 CNX#3 Pitwater 9449 12117/2008 

### 4000 port-a-john 9505 12118/2008 

## see CNX#3 Pitwater 9357

. 12/18/2008 

### 4000 CNX#3 Pitwater 9506 12/1812008 

### 4000 CNX#1 Pitwater 9475 12/18/2008 

### 4000 GNX#1 Pitwater 9474 12/18/2008 

### 4000 CNX#1 Pitwater 9511 12/18/2008 

### 4500 CNX#1 Pitwater 9359 12/18/2008 

### 4000 CNX#1 Pitwater 9509 12/1812008 

### 4500 CNX#1 Pitwater 9508 12/18/2008 

### 4500 CNX#1 Pitwater 9358 12/18/2008 

### 4000 CNX#1 Pitwater ,9520 12/19/2008 

### 4500 CNX#1 Pitwater '9477 12119/2008 

### 4000 CNX#1 Pitwater 9476 12/19/2008 

### 4000 CNX#1 Pitwater 9519 12/1912008 

### 4500 port a-john 9293 12/19/2008 

### 388 CNX#1 Pitwater 9478 12/19/2008 

### 4000 CNX#1 Pitwater 9521 12/19/2008 

### 4500 CNX#1 Pitwater 9468 12/19/2008 

### 4000 CNX#1 Pitwater 9463 12/19/2008 

### 4000

\jX#1 Pitwater 9455 12119/2008 

### 4000**I~NX#3** 

### Pitwater 9479 12120/2008 

### 4000 \CNX#3 Pitwater 9457 12/20/2008 

### 4000

### CNX#3 Pitwater 

### 9522 12120/2008 

### 4500 CNX#1 Pitwater 

### 9393 12/20/2008 

### 4000 CNX#1 Pitwater 

### 9480 12120/2008 

### 4000 CNX#1 Pitwater 

### 9531 12/20/2008 

### 4500 CNX#1 Pitwater 

### 9394 12120/2008 

### 4000 CNX#1 Pitwater 

### 9532 12/20/2008 

### 4500 CNX#1 Pitwater 

### 9481 12/20/2008 

### 4000 CNX#1 Pitwater

. 

### 9533 12/22/2008 

### 4500 CNX#1 Pitwater 

### 9482 12/2212008 

### 4000 CNX#1 Pitwater 

### 9534 12/22/2008 

### 4500 CNX#1 Pitwater 

### 9483 12/22/2008 

### 4000 cNX#1 Pitwater 

### 9484 12/22/2008 

### 4000 CNX#1 Pitwater 

### 9535 12/22/2008 

### 4500 CNX#1 Pitwater 

### 9485 12/22/2008 

### 4000 CNX#1 Pitwater 

### 9536 12/22/2008 

### 4500 Zinkan Enterprise 

### 9486 12123/2008 

### 1008 

# -- CNX # 1 Pitwater 

### 9537 12/23/2008 

### 4500 CNX#1 Pitwater 

### 9487 12/23/2008 

### 3000 CNX#l Pitwater 

### 9538 12/23/2008 

### 4500 dravosburg 

### 9488 12/23/2008 

### 4008 

# - CNX#1 Pitwater 

### 9489 12/23/2008 

### 4000 CNX#1 Pitwater 

### 9539 12/23/2008 

### 4500 CNX#1 Pitwater 

### 9523 12123/2008 

### 4500 CNX#1 Pitwater 

### 9490 12/23/2008 

### 4000**~NX#1** 

### Pitwater 

### 9491 12/23/2008 

### 4000 CNX#1 Pitwater 

### 9524 12/23/2008 

### 4500 CNX#1 Pitwater 

### 9462 12/24/2008 

### 4000 CNX#1 Pitwater 

### 9495 12124/2008 

### 4000 CNX#1 Pitwater 

### 9526 12/24/2008 

### 4500 CNX#l Pitwater 

### 9496 12/24/2008 

### 4000 CNX#1 Pitwater 

### 9461 12124/2008 

### 4000 CNX#l Pitwater 

### 9527 12/24/2008 

### 4500 CNX#1 Pitwater 

### 9497 12124/2008 

### 4000 CNX#3 Pitwater 

### 9225 12/1212008 

### 4000 CNX#3 Pitwater 

### 9408 12112/2008 

### 4000 CNX#3 Pitwater 

### 9375 12/1212008 

### 4000 CNX#3 Pitwater 

### 9339 12/12/2008 

### 4000 port-a-john 

### 9292 12/12/2008 

### -z68 port a-john 

### 9291 12/12/2008 

### 200 

### CNX#1 Pitwater 

### 9512 12/26/2008 

### 4500 CNX#l Pitwater 

### 9501 12126/2008


### . 4000 CNX#1 Pitwater 

### 9396 12126/2008 

### 4000 CNX#1 Pitwater 

### 9502 12126/2008 

### 4000 CNX#1 Pitwater 

### 9504 12/26/2008 

### 4000 CNX#l Pitwater 

### 9513 12/26/2008 

### 4500 CNX#1 Pitwater 

### 9503 12/26/2008 

### 4000 CNX#l Pitwater 

### 9397 12/26/2008 

### 4000 CNX#1 Pitwater 

### 9515 12/27/2008 

### 4500 CNX#1 Pitwater 

### 9401 12127/2008 

### 4000

\lX#1 Pitwater 

### 9516 12127/2008 

### 4500**,~NX#1** 

### Pitwater 

### 9399 12/27/2008 

### 4000 ICNX#l Pitwater 

### 9563 12/27/2008 

### 4000- ---------------------------



### 'itwaler 9514 12127/2008 

### 4500 'itwaler 9562 12/27/2008 

### 4000 'itwater 9561 12/27/2008 

### 4000 'itwaler 9400 12127/2008 

### 4000 'itwaler 9560 12/29/2008 

### 4000 'itwaler 9559 12129/2008 

### 4000 'itwaler 9402 12/29/2008 

### 4000 'itwaler 9564 12/29/2008 

### 4500 'itwaler 9565 29-Dec 4500 'itwaler 9566 12129/2008 

### 4500 'itwaler 9540 12/29/2008 

### 4000 'itwaler 9403 12/29/2008 

### 4000 'itwaler 9558 12/29/2008 

### 4000 'itwaler 9542 12/30/2008 

### 4000 'itwaler 9416 12/30/2008 

### 4000 'itwaler 9567 12/30/2008 

### 4500 'itwaler 9557 12/30/2008 

### 4000 itwaler 9458 12/30/2008 

### 4000 itwaler 9541 12/30/2008 

### 4000 itwaler 9556 12/30/2008 

### 4000 itwaler 9568 12/30/2008 

### 4500 itwaler 9459 12/30/2008 

### 4000 I 

### 9588 12/30/2008 

### -.289 

### itwaler 9552 12/31/2008 

### 4000 itwaler 9555 12131/2008 ' 

### 4000 itwaler 9570 12131/2008 

### 4500 itwaler 9571 12131/2008 

### 4500 itwaler 9460 12/31/2008 

### 4000 itwaler 9551 12/31/2008 , 

### 4000 itwaler 9543 12131/2008 

### 4000 itwaler 9418 12131/2008 

### 4000 itwaler 9569 12/31/2008 

### 4500

## ® 

## Microbac Laboratories, Inc. Page 1 of2 100 

### MARSHALL DRIVE WARRENDALE, PA 15086 (724) 772-0610 

### FAX (724) 772-

### I686 TOMZlERENBERG, MANAGING DIRECTOR http://www.microbac.com State Laboratory Certification Numbers: PADEP: 02-257, NC: 42703. WVDEP: 215,9951 CM KY: 90136**C1iliMl~TK¥** . MlCKutIlULUV¥

. rUUU**~A.t<bT¥· CUN~UMbK.PKUUUCT~**  WATbK· Alli..**WA~ThS** . FOOD· .PHARMACbUTlCALS

. NUTKACbUTlCALS

CLAIRTON MUNICIPAL AUTHORITY 

### MR. PATRICK CANAVAN I NORTH STATE STREET CLAIRTON, PA 15025

Permjt No.: CustP.O.: SUBJECT: \Vastewater Sample fOT Analysis 

### CERTIFICATE OF ANALYSIS
Date Reported: Date Received: Order Number: Invoice No.: Cust#: Sample Date: Sample Time: Sampler/Temp: 1/13/2009 12/19/2008 0812-01476 38389 CI23 12/1912008 11:25

TEST 

### METHOD UNITS 

### DATE TECH

Acidity (as CaC03) EPA 305.1 <1 mg/L 12/31/0B 

### SFS Alkalinity (as CaC03) SM20 2320 341 mgjL 12/31/0B 

### SFS Arr

, ia, Distilled SM20 4500-NH3 B/D 29.4 mg/L 01/05/09 

### RDP BGe SM20 5210B 781 mg/L 12/19/0B 

### SFS COD SM20 5220D 2,390 mg/L 12/31/0B 

### RDP ChlOride EPA 325.2 44,700 mg/L 12/23/0B 

### NAH Conductivity EPA 120.1 102,000 umhos/an 12/30/0B 

### LLS Hardness by Calculation SM192340B 12,600 mgcaC03/L 12/30/08 

### LLS Nitrate-Nitrite as Nitrogen EPA 353.2 <0.10 mg/L 12/29/08 

### NAH Oil & Grease EPA 1664A 43 mg/L 12/30/08 

### ADS Osmolality Cyroscope 2,400 mOsm/kg 12/23/08 

# *-. pH EPA 150.1 6.0 su 12/31/08 

### SFS Phendl1cs EPA 420.2 MOD 0.05 mg/L 12/31/0B 

### NAH Sulfate EPA 375.4 53 mg/L 01/03/09 

### SFS ;urfactants SM20 5540C 11.1 mg/L 12/19/0B 

### NAH rotal Dissolved Solids EPA 160.1 76,000 mg/L 12/22/0B 

### ADS rotal KjeJdahl Nitrogen SM20 4500-Norg-B 

### + NH3-D S2.5 mg/L 01/07/09 

### RDP lotal Suspended Solids EPA 160.2 1,600 mg/L 12/23/0B 

### ADS**~rsenjc** EPA 200.7 <0.10 mg/L 12/22/0S 

### LLS**~arium** EPA 200.7 294 mg/L 12/30/0B 

### LLS 'eryllium EPA 200.7 <0.005 mg/L 12/22/08 

### LLS ;oron EPA 200.7 0.71 mg/L 12/22/08 

### LLS :admium EPA 200.7 <0.005 mg/L 12/22/08 

### LLS :alcium EPA 200.7 3,060 mg/L 12/30/0S 

### LLS hromium EPA 200.7 0.02 mg/L 12/22/0S 

### LLS Dbalt EPA 200.7 <0.01 mg/L 12/22/08 

### LLS opper EPA 200.7 0.11 mg/L 12/22/0S 

### LLS un EPA 200.7 20.S mg/L 12/22/0S 

### LLS on,,.. 11ved EPA 200.7 1.20 mg/L 12/22/0S 

### LLS**~ad** EPA 200.7 <0.10 mg/L 12/22/08 

### LLS thlum EPA 200.7 0.13 mg/L 01/0S/09 CMG agnesium EPA 200.7 1,210 mg/L 12/30/0S 

### LLS

The data and information on this, and other accompanying documents, represent only the samplers) analyzed and is rendered upon condition MEMBER that it is not to be reproduced wnolly or In part for advertising or other purposes without approval From the laboratory. 

# 911**USDA~EPA-NIOSH** Testing Food Sanitation Consulting Dlemic:al and Microblo!ogical Analyses and Research

## Microbac Laboratories, Inc. 100 MARSHALL DRIVE WARRENDALE, PA 15086 Page2 of2

(724) 772-0610 

### FAX (724) 772-1686 TOMZIERENBERG, MANAGrnGDlRECTOR http)

### /www.microbac.com State Laboratory Certification Numbers: PADEP: 02-257, NC: 42703, WVDEP: 215,9951 CM KY: 90136**UiliMl~TKY** . MlCKUtHULUUY

. YUUJJ**~Aj'bTY** .**CUN~UMJjKl'KUJJUCT~** WATER' Alli.

. WASTES'

## l'uuD

.PHARMACbUl1CALS . NUTKACbUl1CALS



### CLAIRTON MUNICIPAL AUTHORITY 

### MR. PATRlCK CANA

### VAN 1 

### NORTH STATE STREET CLAIRTON, PA 15025

PemlitNo.: 

### CERTIFICATE OF ANALYSIS
Date Reported: Date Received: 

### Order Number: Invoice No.: 

### Cust#: Sample Date: Sample Time: Cust P.O.: Sampler/Temp: SUBJECT: Vlastewater Sample for Analysis 1113/2009 12119/2008 

### 0812-01476 38389 Cl23 12/1912008 

### 11:25

TEST METHOD RESULT UNTTS DATE TECH

v 

### EPA 245.1 0.0003 mg/L 12/23/0B Nil 

### EPA 200.7 <0.01 mg/L 12/22/08 Selenium 

### EPA 200.7 <0.10 mg/L 12/22/0B Sodium 

### EPA 200.7 B4,500 mg/L 01/02/09 Strontium 

### EPA 200.7 176 mg/L 01/0B/09 Zinc 

### EPA 200.7 0.53 mg/L 12/22/oB Glycols SW-846 801S6 01/07/09 

### Ethylene Glycol <50 mg/L 01/07/09 Total Volatiles 

### EPA 624 12/22/0B Benzene <5 ug/L 12/22/08 Tolue!le S ug/L 12/22/0B AlUminum 

### EPA 200.7 5.19 mg/L 12/22/08 Silver 

### EPA 200.7 <0.01 mg/L 12/22/0B BOD Analysis TIme lS:0o Hrs. 12/19/oB
***Osmolality analysis performed by Microbac Laboratories, Inc. - Erie Division.



### >ubmitted By:
om Zierenberg : Managing. Directo"r

The data and Information on this, and other accompanyIng documents, represent only the sample{s) analyzed and is rendered upon condition that it is not to be reproduced wholly or In part for advertising or other purposes without approval from the laboratory.**USDA~EPA-NIOSH** Testlng Food Sanil.ction Consulting O1emical and MicrobIological Analyses and Research 

### LLS LLS LLS LLS CMG LLS MSM MSM LAM 

### LAM LAM LLS LLS SFS

MEMBER

# ~~II

## .M1crobac Laboratones, lnc. 100 MARSHALL DRIVE WARRENDALE, PA 15086 rage lOlL



### (724) 772-0610 PAX 

### (724) 772-1686 TOMZIERENBERG, MANAGmGDIRECTOR http://www.microbac.com 

### State Laboratory Certification Numbers: PADEP: 02-257, NC: 

### 42703, WVDEP: 215,9951 CM KY: 90136**CHbMl~TKY** . MlCKU1HULU(jY

. !<'UUJJ ::;AYcTY' CU.N::;UMCKPKUJJUCT::; WATER' AIR· WASTcS

. !<'UOD

. PHAKlVlACEUTlCALS' NUTKACEUTlCALS



### CLAIRTON MUNIClPAL AUTHORITY MR. PATRICK CANAVAN I 

### NORTH STATE STREET CLAIRTON, PA 15025

PemJitNo.: Cust P.O.: SUBJECT: Wastewater SampJe for Analysis 

### CERTIFICATE OF ANALYSIS
Date Reported: Date Received: Order Number: Invoice No.: 

### CllSt 

### #: Sample Date: Sample 

### Time: Sampler/Temp: 12/23/2008 12/912008 

### 0812-00532 37371 C123 12/8/2008 

### 9:30

TEST METHOD RESULT UNITS DATE TECH 001 CNX-3 

### PitvvateJ".···

. Collected 12/8/08 Acidity (as CaC03) Alkalinity (as CaC03) Ammonia, Distilled 8oD5 C

r C Je Conductivity Hardness by Calculation Nitrate-Nitrite as Nitrogen Oil & Grease Osmolality pH Phenolics Sulfate Surtactants Total Dissolved Solids Total Kjeldahl Nitrogen Total Suspended Solids o,rsenic 3arium 3eryllium 30ron :admium :alcium :hrorilium :obalt :opper ron 

### ron l Dissolved .ead 

### itt lS9,·_.:.lum EPA 305.1 SM20 2320 SM20 4S00-NH3 8/D SM20 S2108 SM20 S220D EPA 32S.2 EPA 120.1 SM1923408 EPA 353.2 EPA 1664A Cyroscope EPA 150.1 EPA 420.2 MDD EPA 375.4 5M20 5540C EPA 160.1 SM20 4S00-Norg-8 

### + NH3-D EPA 160..2 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 <1 mg/L 12/16/08 2,100 mg/L 12/16/08

0.93 mg/L 12/12/08

29 mg/L 12/09/08 7Z mg/L 12/1S/08 534 mgjL 12/23/08 3,440 umhos/em 12/15/08 2,870 mg caC03/L 12/13/08

0.32 mg/L 12/19/08

<5 mg/L 12/16/08 36 mDsm/kg 12/11/08 11.9 su 12/12/08 <0.010 mg/L 12/17/08 73 mg/L 12/22/08 12.6 mg/L 12/10/08 1,350 mg/L 12/12/08 8.42 mg/L 12/12/08 8,110 mg/L 12/12/08 <0.10 mg/L 12/11/08

7.76 mg/l 12/13/08 0.009 mg/L 12/11/08 <0.10 mg/L 12/11/08 <0.005 mg/L 12/11/08

1,020 mg/L 12/13/08

0.S4 mg/L 12/11/08 0.07 mg/L 12/11/08 0.64 mg/L 12/11/08 211 mg/L 12/13/08 0.02 mg/L 12/11/08 0.24 mg/l 12/11/08

. 0.17 mg/L 12/12/08

83.3 mg/L 12/11/08

The data and Inforrnatlon on this, and other accompanying dOaJments, represent only the sample{s) analyzed and Is rendered upon condition that It is not to be reproduced wholly or In IBrt for advertising or other.purposes without approval from the laboratory.**USDA~EPA-NIOSH** Testing Food Sanitation Consultlng Dlemical and Microbiological Analyses and Re5"...arch 

### MEMBER SPS 

### SPS 

## RDP SFS 

## RDP NAB LLS CMC NAB ADS 

## *** SPS NAB SPS NAB ADS 

## RDP LLS CMC CMC CMC CMC CMC CMC CMC CMC CMC CMC CMC CMC CMC CMC

# r:.~I.- ----- ---------------- 

## :M:icrobac Laboratories, Inc. 100 MARSHALL DRIVE 

### WARRENDALE, PA 15086 Page2 of2

(724) 

### 772-0610 FAX (724) 

### 772-1686 TOM ZIERENBERG, MANAGrnG DIRECTOR http://www.rnicrobac.com State Laboratory Certification Numbers: 

### PADEP: 02-257, NC: 42703, WVDEP: 215,9951 CM KY: 90136 CHJ::;MlSTKY

. MlCKUl:HULUliY

. YUUlJ SAYbTY

. CUNSUMEKI'KUlJUCTS WATbK' ALK· WASTbS

. 1'OOlJ· I'HAKMACEUI1CALS' NUTKACbUT1CALS



### CLAIRTON MUN1CIP 

### AL AUTHORlTY MR. 

### PATRlCK CANAVAN I 

### NORTH STATE STREET CLAIRTON, PA 15025

Penllit No.: 

### Cust P.O.: SUBJECT: Wastewater Sample for Analysis 

### CERTIFICATE OF ANALYSIS
Date Reported: Date Received: 

### OrderNllIDber: Invoice No.: 

### Cust#: Sample Date: Sample Time: 

### Sampler/Temp: 12/2312008 12/912008 

### 0812-00532 37371 CI23 12/8/2008 9:30



### TEST METHOD RESULT umTS DATE TECH 001 CNX-3 Pitvvate(-· Collected 12/8/08

Manganese Mercury Nick.:>1 S( m SodIum Strontium Zinc Glycols Ethylene Glycol Total Volatiles Benzene Toluene Aluminum Silver BOD Analysis lime EPA 200.7 EPA 245.1 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 5W-845 80158
EPA 524

EPA 200.7 EPA 200.7

"'**Osmolality analysis performed by Microbac Laboratories, Inc. - Erie Division.



### ;ubrn.itted By: 7.20 mg/L 12/13/08 0.0011 mg/L 12/15108

0.25 mg/L 12/11/08 <0.10 mg/L 12/11/08

284 mg/L 12/13/08 4.98 mg/L 12/12/08 1.82 mg/L 12/11/08 12/12/08 23 mg/L 12/12/08 12/12/08 <5 ug/L 12/12/08 <5 ug/L 12/12/08 150 mg/L 12/13/08 <0.01 mg/L 12/11/08 15:00 Hrs. 12/09/08

The data and information on thIs, and other accompanying dorumenls, represent only the sample(s) analyzed and is rendered upon condition that it is not to be reproduced wholly or In part for advertising or other purposes without approval from the laboratory. USDA-EPA-NIOSH Testing Food Sanitation Consulting Chemical and Microbiological Analyses and Researd1 

### CMC LLS CMC CMC CMC CMC CMC MSM MSM LAM LAM LAM CMC CMC SFS

MEMBER

# ~~II**----------------------~**



### ApPENDIX 

## B CMA PROCESS FLOW DIAGRAM

DETAILING SAMPLE LOCATIONS........ _---_. __._-**----------~**



### AERATION TANKS---,

PRIMARYSETTLING TANKS PRE-AERATION\ TANKS SAMPLING] SAMPLING.

# 7' STATION STATION**!~"''-**

# SAMPLlNG~, STATION'**,..~-----.**


### COARSE BAR\l' 

### 1

# [~**l~~** 

# :**~ ]t~**  SCREEN 

# !.

. 1 1 ill , RETURNACTIVATED SLUDGE**~,,...,---**

## /~,----.l---,~'-l--e\+

# .... /1'-,

__ ;

__ ---'

_--i-_---I ! I 

### 4=-- ! 

# r - - --- - - - -'-
- - - --- - JjL
- - 

## J 

# \+-' ---' ,I, 

### -4-....J.....J 

# r--
_ --j 

### BY-PASS 

## ,1,_' 1'---'r FINAL SETTLING \ TANKS \
SAMPLING

# r---:-::=~~-'

SCREW PUMPS



## ,_1_; 1 

# i 1 ...., 1 

# \ ' 1**L-~-l----r-----~-** I 

### COMMINUTORS 

# L - -

__ - - 

# ....rf'--

- - - __- -1-

- -. 1 WASTE SLUDGE 

# I BY-PASS 

### 1 

# d RETURN 1 

### AND SCUM 

# 0
THICKENING 1 

### ACTIVATED \'------..,-----'---------

# ~: 14" F.M. 

# t TANK 

# l

__ Sl.UDGE

_____ __

# ~SAMPLlNG 

# >! 1 

# ! BY-PASS 

# i STATION -' ,-' ! 

## 11:11 

## Y -, '-.rI ' 

### ----j = J 

### OLD



## -- I 

### AERATED

# --,-tl I 1 

# i

# ~ I GRIT " I

# ~!**~MBER L-~iF.** **~** 1

## ~i PUMP STATION

MECHANICAL BAR SCREEN , 1 Q:: 

### i 

### III!

# ~ :s L _o--..J 

# !!i ',,' h-i,_

... 

# ...**~;** 

# b**~'-<-'**---' 

# .,.,, ( PUMP i. 

### STATION T**ri-~-"":'"**

### --'----. BAR SCREEN --T-- 

# 6 OXIDIZED SUP"ERNATANT SLUDGE

. HOLDING ! 

## I TANK

- 

# .**~GRA"TYBELT**

15'" ,,'

## ~THICKENER CENTRATE**--,,;----C----'-==~==-j** 

# ! CENTRIFUGE --_._+ 

# t '-----36'· INTERCEPTOR SOLiDS TO DISPOSAL 

# - - '--



# - -



# --



# - CHLORINE CONTACT TANKS

____ WASTEWATER

____ BYPASS

- - - WASTE SLUDGE

- , ,,- RETURN ACTIVATED SLUDGE 

# .. • 

## '" • " o

### :~ 

# '"**~** 

# , • , , 

## •**~** • 

### , 

# , < o 

## • 

# , 

# • , , , 

# , , " " 

## , 

# , , " 

## ,**~** E 

# ,

# ~~ ill ill 

# I**~** ..J [!I 

### V Z _11.1

Sheet No.



### xx of XX Drawing No. 

### Ii'IG26

### KLH**ENGINEERS~** INC. 51 '73 c ... M
..aE:L'-S RUN R",
... ", p,.,.,.....U,.
..H, pA 15Z05 ""ONE:,412-4"'4-1:1"'0

FAx, 412-494-0425 'NI'Q@><LHEONGINEERS.",QM ALLEGHENY COUI.,y, ?ENI,SYLVANIA "NPDES PERMIT # PA 0026824" LOCA TIOI,**I~AP** Drawing No.---------- ---------------------



### ApPENDIXC CMA CHLORIDE AND 

### TDS ANALYTICAL DATA

### Clairton Municipal Authority Interprocess Testing Data Total Dissolved Solids, Chlorides, and FOG

Date

12/8/2008 12/9/2008 12/10/2008 12/11/2008 12/12/2008 

### Average Maximum Minimum

Date

1218/2008 12/9/2008 12/10/2008 12/11/2008 12/12/2008 

### Average Maximum Minimum

Date

12/8/2008 12/9/2008 12/10/2008 12/11/2008 12/12/2008 

### Average Maximum Minimum

Date

12/8/2008 12/9/2008 12/10/2008 12/11/2008 12/12/2008 

### Average Maximum Minimum Flow (MGD)

3.08 3.04 4.97 5.21 5.67 4.39 

### 5.67 3.04

Flow (MGD)

3.08 3.04 4.97 5.21 5.67 4.39 

### 5.67 3.04

Flow (MGD)

3.08 3.04 4.97 5.21 5.67 

### 4.39 5.67 3.04

Flow (MGD)

3.08 3.04 4.97 5.21 5.67 

### 4.39 5.67 3.04 Chlorides (mg/l)

386 843 221 183 268 

### 380 843 183

Chlorides

(mg/l)

575 419 330 364 381 

### 414 575 330

Chlorides

(mg/l)

276 413 411 353 408 

### 372 413 276

Chlorides

(mg/l)

286 397 518 351 331 377 518 286 TDS (mg/l) 1080 1980 708 664 794 

### 1045 1980 664

TDS (mg/l) 1360 1140 876 942 952 

### 1054 1360 876

TDS (mg/l)

898 1190 1020 946 1020 

### 1015 1190 898

TDS (mglJ)

904 1100 1210 932 820 

### 993 1210 820 Location #1 FOG (mgll)

12 10 14 7 4 

### 9 

### 14 4 Chlorides (lbs/day)

9915 21373 9160 7952 12673 

### 12215 21373 7952 Location #2 FOG (mg/l)

10 11 14 7 4 

### 9 

### 14 4 Chlorides (Ibs/day)

14770 10623 13678 15816 18017 

### 14581 18017 10623 Location #3 FOG (mg/l)

10 9 7 5 4 

### 7 10 

### 4 Chlorides (lbs/day)

7090 10471 17036 15338 19293 

### 13846 19293 7090 Location 

### #4 FOG (mg/l)

17 16 16 16 16 

### 16 17 16 Chlorides (lbs/day)

7347 10065 21471 15251 15652 

### 13957 21471 7347**----~------~----------------**



### TDS (Ibs/day)

27742 50200 29346 28852 37547 

### 34737 50200 27742

TDS (Ibs/day)

34935 28903 36310 40931 45018 

### 37219 45018 28903

TDS (Ibs/day)

23067 30171 42279 41105 48234 

### 36971 48234 23067

TDS (Ibs/day)

23221 27889 50154 40497 38776 

### 36107 50154 23221 FOG (Ibs/day) 308 254 580 304 189 

### 327 580 189

FOG (Ibs/day) 257 279 580 304 189 

### 322 580 189

FOG (Ibs/day)

257 228 290 217 189 

### 236 290 189

FOG (Ibs/day)

437 406 663 695 757 

### 591 757 406

### bate 12/8/2008 12/9/2008 12/10/2008 12/11/2008 12/12/2008 

### Average Maximum Minimum

Date

1218/2008 12/9/2008 12/10/2008 12/11/2008 12/12/2008 

### Average Maximum Minimum Flow (MGD)

3.08 3.04 4.97 5.21 5.67 4.39 

### 5.67 3.04

Flow (MGD)

3.08 3.04 4.97 5.21 5.67 

### 4.39 5.67· 3.04 Chlorides (mg/l) 234 351 478 335 293 

### 338 478 234

Chlorides

(mg/l) 227 359 520 329 300 

### 347 520 227 TDS (mg/l) 862 1060 1190 954 804 

### 974 1190 804

TDS (mg/l) 844 1050 1250 948 780 

### 974 1250 780 Location #5 FOG (mg/l)

4 4 4 4 4 

### 4 

### 4 4 Chlorides (Ibs/day)

6011 8899 19813 14556 13855 

### 12627 19813 6011 Location #6 FOG (mg/l)

4 4 4 4 4 

### 4 4 4 Chlorides (lbs/day)

5831 9102 21554 14296 14186 

### 12994 21554 5831 TDS (Ibs/day)

22142 26875 49325 41453 38019 

### 35563 49325 22142

TDS (Ibs/day)

21680

. 26621 51812 41192 36884 

### 35638 51812 21680 FOG (lbs/d§Yl 103 101 166 174 189 

### 147 189 101

FOG (lbs/day) 103 101 166 174 189 

### 147 189 101

### JAN-05~2009 

# MON 09:47 PM CLAIRTON MUNICIPAL AUT
®Microbac Laboratories, Inc. 100 MARSHALL DRIVE WARRENDALE, PA 15086 (724)**772~061O** FAX (724) 772-1686 TOM

### ZIERENBERG, MANAGING DIRECTOR http://''''''''''_rnicxobac_com 

# P, 002

MEMBER



# - INVOICE Page 1 of I



## No. 36964

# i(·;~+;~~~·l~?i~;;.!~ifr;**:';::~t}~;.~~]~;~~~~J.~:~;m;~;·~w:~:::~tj ::,·;:~1'itt~~;·:** **~':' ;':'~;'~.** **j,~.(:.~:::** ! CUilRTONMUNlClPAL AUTHORlTY MR, PATRICK CANAVAN 

### Day 1 • Wastewater Samples forAnalysis


### 1NORTH 

### STATE STREET CLAlRTON,PA 15025

.



### 0812·00543

. 

### .**~** :. NET 30 DAYS 

### Day 1 • Wastewater Samples forAnalysis



### Please includ.e this Invoice Number and your Client AccountNumber with all remittances

CHEMISTRY'

. FOOD WATBR' AIR

- WASTES, FOOD

- PHARMACEUTICALS

- NUTRACEUTICALS 

### $264,00

$264.00



## - $264.00

# JAN-05-2009 MON 09:48 PM CLAIRTON MUNICIPAL AUT
®Microbac Laboratories, Inc. 100 MARSHALL DRIVE WARRENDALE, PA 15086 (724) 772-0610 FAX (724) 

### 772-)686 TOM ZIERENBERG, 

### M.

...



### NAGING DIRECTOR 

### http)/www.microb.c.com 

# P, 003

MEMBER

## ~ INVOICE Page 1 of]



### No. 36964

CLAIRTON MUNICIPAL 

### AUTHORITY MR. PATRlCK CANAVAN 

### Day 1
- Wastewater Samples for Analysis


### 1NORTH STATE STREET CLAlRTON,PA 15025



### 0812-()0543
Day 1
- Wastewater Samples forAnalysis



### Please include this Invoice Number and your Client AccountNumberwith all remittances

CHEMISTRY' MICROBIOLOGY' FOOD SAFETY· CONSUMERPRODUCTS

A .,. <"T""r> TTA ..... 6,0,., T AT '>.'N "T:"TT"" 

### $264.00

Total 

### $264.00

",

. i":,:.i!'· 

## 6.

# JAN-05-2009 MON 09:48 PM CLAIRTON MUNICIPAL AUT P, 004
® 

## Microbac Laboratories, Inc. Page 1 of2 

### 100 MARSHALL DRIVE WARRENDALE, PA 

### 15086 (724) 772-0610 FAX (724) 772-1686 TOMZIERENBERG, MANAGING DIRECTOR http://www.m.icrobac.com State Laboratory Certification Numbers: PADEP: 02-257, NC: 42703, WVDEP:. 215,9951 CM KY: 90136 C.tJJOMlt;TRY • MlCKUb!VLVUY

. t<VVlJ 

### SAl'l:dY· CVNt;UlVJbKJ:'KVlJUCTS 

### WATER· A.IR'**WAS'lli~·** 

### FUOD· J:'HARMACJ:iUTlCALS' NUTRACJ::U'l'JCALS 

### CERTIFICATE OF ANAL VSIS CLAIRTON

### MUNICIPAL AUTIlORlTY 

### MR..PATlUCK CANAVAN Date Reporred: Date Received: 

### 1NORTH STATE STREET CLAIRTON, PA 15025


### Perm.itNo,: CustP.O.: l SUBJECJ': Day 1

- Wastewater Samples fur Analysis
TEST

0,1 all &\;Irea:se Total Dissolved Solids

ChlorIde Oil 

### &. Grease Total D!ssolved Solids



### );1 & Grease rotal Dissolved Solids

:hloride iii & Grease 'ota' Jived Solids METHOD

EPA 3252 EPA 1664A EPA 160.1

EPA 325,2 EPA 1664A EPA 160.1

EPA 1664A EPA 160.1

EPA 325.2 EPA 1664A EPA 150.1 

### RESULT

386

12 1,080

575

10 1,360

10 898

26B



### 17 904 OrderNumber: Invoice No.: 

### Cust#: Sample Date: Sample Time: Sampler/Temp:



### UNITS 

### DATE

mg/L 12/17/08 

### mg/L 12/16/08 mg/L 12/12/08

mg/l 12/17/08 mg/L 12/16/0B 

### mg/l 12I12/0B

mg/l 12/17/08 mg/l 12/17/08 mg/l 12[12/0B

Thl:: dna ami lnfom;(loElon on !:hI", ;:!ncl other**aocom~nylng** documents,. rcpre:se:nt**Dnl~** the samp[e{s) tlni'llyzed and Is rendsred upon condition mat It is nut to be repr'l)::h,u:
.... ""'d whoUy or 111 D1trt for advertlsiflg Of o\:l1er pUfPOses wlthovt tlPproval from the**I~OOr"tt1ry.** USDA-EPA,NTn5;H T",sH..... 1=....,-.1**C::>~"""'I-T**...." ,.,.,,.,"',1"....

........**""~.1 ~~.1**  .....**~~**..**'~r~_'~~' ~** __1 ••_. -_... ,,_._-_.. 12/1812008 

### 12/912008 0812-00543 36964 C123 12/8/2008 0:00

TECH

NAH ADS ADS



### NAB ADS ADS

NAH ADS ADS



### NAB 

### ADS ADS

MEMBER '. 

# '1.'W.I

# JAN-05-2009 MON 09:48 PM CLAIRTON MUNICIPAL AUT p. 

# 005

® 

## Microbac Laboratories, Inc. Page 2 of2 

### 100 MARSHALL DRIVE WARRENDALE, PA 

### 15086 (724) 772-0610 FAX (724) 772-16&6 TOM 

### ZIERENBERG, MANAGING DIRECTOR http://www.micwbac.com State Laboratory Certification Numbers: PADEP: 02-257, NC: 42703, WVDEP: 215,9951 

### eM KYo 90136 L;liliMl::>TKY

. MlCKUJ:llULUl:iY 'I'UUJJ l:>AI'tl'!');"**WN~U.M.tlKPKUJ.)UCT~** 

### WA'l'hl{' A.lK'**WAS'lB~** 

### '1'00.0

.pHAl:tMACI;u-nCALS' NUTRACEUTICALS 

### CERTIFICATE OF ANALYSIS CLAIRTONMUNICIPAL AUTBOlUTY 

### MR. PATRICK CANAVAN 

### 1NORTH STATE STREET CLAIRTON,PA 15025

PenmtNo.: 

### CustP.o.: SUBJECT: Day 1

- Wastewater Samples for Analysis 

### T:EST METHOD

:hIDI.

__ EPA 325.2 Jil &. Grease EPA 1664A fotal Dissolved Solids EPA 160.1 

### .,>(!: 

## ., I': .:;": ":,'; 

### ',;



### .. '.;,1 .:; .,',. ,": ' ,11,**~,** ' ,., • TI· EPA 325.2 III & G"'ase EPA 1664A etal Plssolved Solids EPA 160.1



### iJmitted By: RESULT

234 <5 862



### ......:'i' :



### 227 <5 844 

### Date Reported: Date Received: OrderNumber: Invoice No.: Cust

### #: Sample Date: 

### Sample Time: SampJer/Temp:

UNITS DATE

mgJL 12/17/08 mg/L 12/17/08 mg/L 12/12/08

:;'.'.;



### . .. ·,'":.i

. ,: ,



### . ''',,\r

!<,'

,', 

### .. mg/L mg[L 12/17/08 mg/L 12/12/08

Thl: data and Informatlnn on this, and**D~l:r 2Iccampany!n~**  docum"-nts,**fe!JreS::f"I~** On!y the. samp!e(.s) "nalyzed anti b; render:eclLJPll!1 I;()ndltlof"l tnat It Is nDt to be n:produoed Wholly or 111 p:.rt for**adv~ing** or cIller pUrp;:lseEl wltl'lout approval. from th:; l2IooratClty. USDA-EPA-NIQSH re:s:tlnCl fond ""'nlr::oti"'" r""'Od'l...,, ""

__**I~! ~~** ... UI_'-I_I

__

'_· • .• • - . 

### 12/J

### 812008 12/9/2008 

### 0812-00543 36964 

### C[23' 12/8/2008 

### 0:00

TECH



### NAH 

### ADS ADS

NAH 

### ADS 

## ADS

MEMBER 

### iF

.....I

### itWQrKorder# 

## C:Th Id •5'4 i.-- 

### ISit€'-

. --,,;,.r-- --------. • -1iI'-

__**~,** __ 

### 100 Marshall Drlve, Warrendale, PA. 15086

.Phone (714)772·0610 Fax (724) 772-1686 

## Chain :ustody (Please Fill Dul Completely using perm anenl ink) 

# dt!l-,;,,:,w ""VN" 

## tfvi;'; PO#. x 

### Fax
IICO"1901 N2me: 

## &r..:""N -S,4Qt.,.;,r; Report .Yes No E·mall WATER DrinkIng Water DW LE MATRIX CODES SOUDS MISC.
SoIT SO· DII OL Ground ,"'

........... .....,

## .., <.'1,,-,- SL Wlpes 

### WP Slreet: Report Yes No l""OY I

...'

...... !::I'; IfBilling Infoll1lalion is dffi"e ,-- rent than Reporting ISLIrta[;e 

### Icity: RoullneTAT: Yes No InformaHon Please Indicate below (Waler Person:

IDEP PWS ID #: StatelZip: Ilfno, Speoify days below P"hGna: Rusb TAT Requesled(Davs): E-mail: <2 2·5 5-7

SAMPLE COLLECTED '-BOVE. R¥ No, OF**CONTAIN~l)** SAMPLE IDENTIFICATION

m 

# :r**~** DATE 

### I TIME

# 1/'~f-T/oA/" 

# I II?**J,,LvI7~~3** 

# f 

# :z. .2 

# InklcJ 7 

# :!;& f 

# < .I 

# IqkJ.81& ;,£ 

## '/ 2. 

# If lialn!

# ~I**fJ~g'k** 

# If 

# Z**~**

# k~b~Ig-~~= 11 Z

# G,**~2J",Lcl** f/ 

# ;;G

# ~ 2- Waste Water Trip8lank Field Blank

# ~"~~~It

Z**~ ~**  Z 0 Z 

# '" '"**~** 

### z 

## 8 o 0 Cl 

### m .". :c .- 

# L I 

# ! I 1 I I I 

# ) 

# J



# I I I ) J J SW
WW TB 

### FB



### if 

## 1< o "- < 00**~O**

### ~fJ 

## w .... Swabs SB liquid L Food FD Solids S Mh::;ro-bialogy Me

----- -



### " Analysis Requested



# T tlS}**C!l&,{:;.(i.f_~;'Gi'"w-t'**

....>_ ......**_~L** 

# '-V

Gals

### ~m' 

# 1"'001'"' ,( / "" ---.l--" 

# I**Oa~** 

# 1 ''''''**""IS;"'~"")** 

# /4z...**~;;:::,.** 

# /Z/t/.lJ**J-~.?** 

## c lY=1,' 

# 14: /t L:" 112

# J'!oJ> 1

# /O~:~**I=;~~~~u,")** 

# Irl fI 

# ? 7**rliffl'l(j±(~** i" 

# /7
T Oalll- 

## 1- 11m!! D<.!w ThnB Fe sampling-Notes:**EQUII'M~l'l'n'l[AflKS~AND** FIELD BLANKS-ARE USED FOR INTERNAL LAB USE ONLY!NDT BILLABI.EI. NOT REPORTED UNLESS REQUESTED llY**~amp** 100 By: CUSTOMER. GhlOJine Rs.dlng: Please deliver samoles to the lab as ,soon as possible after collection 10 ensure that holding 

# I:··'

,., ,**lag~in.** G ".'J( be met. Please fill GOC aut competely**to_expeDlle_~:all~~**

.....__ .....__"-_1 hi". I\An.t:n..t:1n,u:::: tUijJ;

RsII.;{1 Creeta{{ By:MAlJ

Dals;YJ11O .5**~** :to- 

### =

1 

### = =

1**~** 

### = = <0 

# "" = = = <0



# -- <0 -0 

# ""

C""> r- :to- 

## = -< 

## = = s::: 

### = = C""> -0 >- r- :to- 

### = -<

-:0 

### = = =

# JAN-05-2009 MON 09:49 PM CLAIRTON MUNICIPAL AUT

® 

# Microbac La

# boratories, Inc. 100 MARSHALL DRlVE WARRENPALE, PA 15086 

### (724) 772-0610 FAX (724) 772-1686 TOMZIERENBERG, MWAGlNG DIRECTOR http://www.microb.c.com 

## p. 

# 007**MEMB~~** 

# RII INVOICE Page 1 of!



## No. 36986

CLA1RTON 

### MllNICIPAL AUTHORITY MR. 

### PATRlCKCANAVAN Day 2
- Wastewater Samples for Analysis


### 1NORTH STATE STREET CLAIRTON,l'A 15025

, ..... 

### 0312-00544 ", ; : , r:-



### Day 2
- Wastewater Samples for Analysis



### Please include this Invoice Number and your Client AccountNumber with all remittances

WATER' AIR· 

### WASTES, FOOD' PHARMACEUTICAIJS

. NTJTR**~("P"TTf'A' ~**  

### .. ,.) . 

### $264.00

# JAN-05-2009 MON 09:49 PM CLAIRTON MUNICIPAL AUT


# ®Microbac Laboratories, Inc. 100 MARSHALL DRIVE WARRENDALE, PA 15086 

### (724)772"()610 FAX (724) 772-1686 

### TOM ZlERENBERG, MANAGING DIRECTOR http://www.rucrob.c.com 

## p. 

# 008

MJ:iMBER



# - INVOICE Page 1 of 1



## No. 36986

CLAIRTON MUNICIPAL AUTHORlTY MR. PATRlCK CANAVAN Day 2 - Wastewater Samples forAnalysis


### 1NORTH STATE STREET CLAIRTON,PA 15025

0!!12-00544
Day 2 - Wastewater Samples



### Please include this Invoice Number and your Client Account Numberwith all remittances

. MICROBIOLOGY'

. CONSUM:ERPR.DD1JCli'S WATER· AIR' WASTES' 

### FOOD· PHARMACEUTICALS·**NUTRAr.p.TTTrrAT.~** 

### Total 

### Prepaid " "" 

### $264.00



# $264.00

# JAN-05-2009 MON 09:49 PM CLAIRTON MUNICIPAL AUT p. 

# 009

® 

## Microbac Laboratories, luc. Page] of2 100 MARSHALL DRIVE 

### WARRENDALE, PA 

### 15086 (724)772-0610 FAX(724)77H686 

### TOM ZIERENBERG, MANAGING DIRECTOR httpJ/www-microbac.com 

### State Laboratory CertificationNumber,: PADEP: 02-257, NC: 

### 42703, WVDEP: 215,9951 CM KY: 90136 CllliMl;';TKY

. NUCKU1:SlULU(;iY

. ¥UUlJ ;';A.!'

. .t::T"i:'

. CUN;';UMJ:i.K J:'KUlJUCTS 

### WATER' AIR.· WASTES

. fOOD**·l'H.l\.KMAC.I'UTjCAL~·** NUJ'KA<.:.t::UT1CALS 

### CERTIFICATE OF ANALYSIS CLAIRTON MUNICIPAL AUTHORiTY MR. 

### PATRICK CANAVAN I NORTH STATE STREET 

### CLAlRTON, PA 15025



### PermitNo.: CustP.O.: 

### SUBJECT: Pay 2

- Wastewater Samples for Analysis 

### TEST METE:OD

Chlo' EPA 325.2 Oill**_~se** EPA 1664A Total Dissolved Solids EPA 160.1


## .'

.. 

## , '. >':";,";'



### " :hlotide EPA 325.2 )f/'&' Grease**E~A** 1664A 'otal Dissolved Solids: EPA 160.1 

### RESULT

843

10 1,980

419

11 1,140 

### Date Reported: DateReceived: Order Number: lnvoice No.: Cu,t#: 

### Sample Date: Sample Time: Sampler/Temp:

UNITS DATE

mg/L 12/17/08 mg/L 1'1./17/08 mg/L 12/12/08

mg/L 12/17(08 mg/L 12{17/0B mg/L 12/12/0B 

### ]2119/200& 

### 12/912008 0812-00544 36986 Cl23 

### 12/9/2008 

### 0:00



### TEeE:



## NAB ADS ADS

NAIl: 

## ADS ADS

"Ioride EPA 325.2 413 mg/l 12/17/0B 

### NAB jJ &. Grease )tal Dissolved Solids

londe &. Grease tal D' 'ved Solids EPA 1664A EPA 160,1

EPA 325.2 EPA 1664A EPA 160.1 9 1,190

397 <17 1,100 mg/L 12/17/0B 

## ADS mg(L 12/12/0B 

### ADS

mg(L mg/L mg/L 12/17/08 12{17/08 12/12/06 

### NAB 

## ADS ADS

The**d~** amllnformal:ion on this,. and other accompanylrl!:l dOOJlnents, re)Jl'eSl:!n\: only the**samp!~(Ir)** ana\y2ed**~nd** 19**rend~** upon O:JI1dltloo that: It Is not.ttl be**n:!prodll~** whony or In part for**Bdv~rtlElng O~**  other pUr'pQieS wIthoutapproval from rile**lab::l~lDry.** MEMBER ".;:;;;;;;;J i II**U.s[)A-EPA-NIOSH"'T~nll** FtIOrl**",,"nrh>~,,"** ,..........**~,,'''**... A
...... _-,_.**--~** ••• •

# j~'-----------------------::-P.0:10:-- I 

# JAN-05-2009 MON 09:50 PM CLAIRTON MUNICIPAL AUT
Microbac Laboratories, Inc. 100 MARSHALL DRIVE WARRENDALE, PA 

### 15086 Page 2 of2

(724) 

### 772-0610 FAX (724) 

### 772-1686 TOM ZlERENBERG, MANAGING DIRECTOR htrp:llwww.microbac.com 

### Stat. Laboratory Certification Numbers: PADEl': 02-257, NC: 42703, WVDEP: 215, ?951 CM KY: 90136**CHJ:£Ml~"J1<.¥** • MlCKU1HULUl:iY •¥U()J)**~At'bTY** .**C\)N~UlIlliK** l'KUJ)UCl"S 

### WATER· AlR· WASTES·**~'UOD'** 

### l'HAKMACI:UnCALB

. NU'J'RACEUTlCALS 

## CERTIFICATE OF ANALYSIS CLAlRTON MUNIClPAL AUTHORITY MR. PATRICK 

### CANAVAN 1NORTH STA1E STREET 

### CLAIRTON, PA 15025

Permit No.: 

### Cu,stP.O.: SUBJECT: Day 2 - Wastewater**Sampi~s** 

### for Analysis
TEST 

### METHOD

. '," 

### ..,' 

### ....

.,: :hloJ. E:PA 325,2 

## )a II. 

### Grease EPA 

### 1664A rotal Dissolved Solids EPA 160.1 

### RESULT

351 <5 1,060 

### Date :Reponed; Date Received: Order

### Number: Invoice No.: Cu,t#: 

### S1UIlple Date: S1UIlple Time: SampJertremp:

UNITS 

### nATE

mglL 12/17/08 mg/L 12/17/08 mg/L 12/12/08 

### 12119/2008 12/9/2008 

### 0812-00544 36986 

### C123 12/912008 0:00



### TECH

"",:",'



## NAH ADS ADS

hlo:ide EPA 325.2 359 mgjL 12/17108 NAB: il & Grease EPA 1664A <5 mglL 12/17/0B ADS >tal Dissolved Solids EPA 160.1 1,Q50 mg/L 1l/12/08 ADS



### )mittedBy:

The fll'Il;;;l ana Informl!!tlol'/ on this, ard other BC:O::lmpanying docwnenls,**repr~lt** only til::: .;amp)"",,s) anl!lltzad ilml Is reru:1c:re:d upon CtIndJtlon rhcrt: it IS nat to be**rcproau~** wholly or In part for eclvertlsing or ot:hm-**~** W/!tlout approval from the**lab[]~roN. U5[).I>,~EPA.-NrDg..!"'rl:><;};""**  ,,""'"''''--,
......- ---- '" -**MEMBE~** 0&

# I Yi"","rosrw 

# I**O~ Id.'~~**  

## .**Samp\m~** 

### SlteJprOj Special Instruction.: SAMPLE MATRIX CODeS

lvumpany:

### Lt~,~r..-.J "'oJ/J. Y-Iu 

## 17-/ PO;!I x WA1ER SOWDS MISC. 

# - Fax Drtnking tN.me: 

# &,'.'" oS(Kfil".-f/ Report Yes No Water DW Soil SO 011 Ol E-mail Ground Street: Report Yes No Wa.(er GW Sludge SL Wlpe8 WP ClIy: If Billing Infonmatlon 18 different !han Reporting Surface Routine TAT: Yes No Information Please indicate below Water 

### sw W,ste Swab, SB
Iphone: E-mail:

Matrix**~ECODES** If

### no. Specify d

### .ys below Contact Person: 

# I**Ru.~** TAT R.quested(Days): Phone#: <2 2-5 5-7 DEPPWSID#:

SAMPlE COLlEClEO :, tr)'Our**'~** nat SAMP LE IDENTIFICATION 

# I NO.OF COllTAI

_ ••Jed/y i ma1rlx DATE 

# l TIME 

# I! ! 

# to c.:,.". ,,"0 N 

# I 

# InAkflf:/c I xl j 

## J

# bUc'i~C)S 

# 111 I J 

# F!J9i.sI7 i% 

# IYI I 

# Y**p2h/.~** 7:52- 

# IXI ( 

# s**1/~bI7~S'O** 

# VI / fo 

# 1/2.lrkfl**~~CO** IYI I

Dala 11mEl

# ~J1-:J- 

# Ilzl;"g 

# 1/6**~~mic>** 

# // ;J'/ Dalll 

## 1---- Ttm9

- Samoled By: 

# I Plsase deliver samples to the Jab as soon as possible aft.er collEKitiQn to-enS'ure that holding 

# I:

.... limes will be mel Pleas. fill COG 

### out

### oomple1ely~expedae sample Log-in. C Tan:p:

.....__ ...._.uw_1 "-,_. niln

...**n.a:;;~n.ll~** 

### I

I

.

# 1~1:r :I: 

### z 

# I.**l~** 

# i g**~ ~** **_~Ji** 

# J I f
{ Waste a.1er WW liquid TJip.Blan«. TB So/"o!ds Field lIIank FB



# 19 I !!:l :

><,

lRuoolved 

# A-**;.t,2../~** lR-eooIYed

# ~I'/**IRI';II:;.at~1ld** L Food 

### FD 

### s Mk:ro-blofogy**M~**



### Analysis Requested 

# ()/L. 

# +G-/L



# I/z-h:kfl $ 

# T;'} 0 

# I --Oaill'- 

# I Tone 

# l'2..Iq,IA b0'>0 Datil TIml!
I Nates: EQUIPMENf St:ANKS-AND-FiELD BLANKS ARE USED FOR ""**~'"""''-** LAB USE: 0 NL YINOT BILLABLE). NOT REP ORTED UNLESS REQUESTE D BY ICUSTOMER.

Rsv.:<i Created a-t:M"ID

D.ata::JI3tKl .5**~** 

# "'"' =



# , =**~**



# , "" = = <.0 

### s:: 

## = = = <.0**~** 

### = -0 

# ""
" r- 

# "'"' :;0 -< 

### = = s:: 

### = = c-> -0 

# "'"' r- 

# "'"' = -<

-0 

### =WOrKorde, # 

# J 100 Marshall Drive

.SamplmgSltelPro ect: (f ...... _. 'W"

....""'

....... _,....Vl ClLV'I'CoO:!I, lilt"

...**r-11.~Durgn** UIVISJOn PaY9

__ Dl

__

. Customer Reporting Infonnatian

. Special In,lnlctions: SAMPLE MATRIX CODES 

### Company: 

## CU."/<-Tey.,J mVIJ. flJvTIfJ Pall



# --

# • '" Fa. Confact Name: Repol! Ves No E-mail 

### 8lIeet: Report Ves No**C~;** Routine TAT: Yes No SI.loIZip:. IfnD, Speony days below Phone: Rush TAT Reque.ted(Day,): E-mail: <2 2-5 5-7



## - SAMPLE Malrix SAMPLE C.Ol.1.ECTEO

. OS"EcaDES

ABOVE, Ifyou SAMPLE IDENTIFICATION maJ.ri:tis no1 IIsfed specify

. yoorrna1rb:" below DATE TIME 

# to**c:-~/o!,,.J** 

# j**1~&k8** L

## 1'2j~S ..] 

# tJ/Wof 

# y fo/gog 

# S :Zl.£

. 

# roy 

# "**12/W~** RelinqIJisJ)ed sy:(Slgnalura)



# - Oala**~Da!SI** Reinquished By:(S'gMlUr.a) 

# 14**d.~** :::> II:

.

# /;/"y

JRE!1il1i-l15hi!d By.::(Sfgn:abJrs) 

### / 

# 1"# Daht

Sampled So(. Chlorine Reading: PJeoase deliver samples to the lab as soon as possible after colts-eliOA to ensure that holding Urnes will be met. Please fiU COG out completely itt expBdne sample log·in.

1"1

__ ..........,......., 1\1

.....**t\lInli.llot;.1rtd:~** WATER SOUDS MISC. Drinking Water DW SoU SO all OL Ground Water 

## ow Sludge Sl Wipes WP IfBilling Inform ajlOll Is**d~ferenllhan** Reporting Surface Information Pleas.e Indicate below Water SW Wasle! Swell<! 5B COlltacl Perton: IWaste Water WW Liquid l Food 

### FD Phone II: T1Jp Biank TS SoJids S MlcllJ-biology 

### Me DEP PWS 10 II: ReM I?lartk FB Preservative

. 

# '" g N:Q. OF 0: 

### Analysis Requested Q C-OtfrAlNER5 Z c**~** m "- 

### z :J: :I: 

# '" 0 

## " 

# '" Z IlJ 0;'; a " 0 Z 

# '" ru :J: 

## '"**~o**

## ~**~** Z 0 0 0 0 0**~** 

### 5" m w 

# '" :I: r 

# '"**~.**

## ~ f t/

# r~s**cfl{~/O/£** 

# y.,;> { 

# Iv 

# J 't 

# I [/ 

# l**VI~** 

# I Iv**I~~** ( 

# It-' 

# 1/**~~** 

# (**~** 

# \y

lima RBaalvG'd 

# L**/{~** 

# ;zit**1i~** ay.{&gnilEull!l 

# . ;J,$'**6'~/:(' 11~**  ft1i!oeived 

# /// Dale TIfPB 

### /0**rt)~ ay:(sr{lnB~reJ**  

# "'"'**R.e~d** O,Is lima By;(Si9Ilo!1Wr.a) 

### > - Field SampJlng Notes:

. EQUIPMENT BLANI\S AND FJELD BLANKS ARE SED FOR

Cr.lHdmon: A,,!!.SlU11pia TelllJl: '0 INTERNAL LAB USE ONl Y(NOT BILLABLE). NOT REPORTED UNLESS REQUESTED BY CUSTOMER.



## - 

# - Cre-sted B.y:UAD

DaIE'l::!J311D5 

# J**~** ::<>- 

### =

I 

### =**~**

I 

## "" = = <0 

# "'" = 

# = = <0**~ ~**  ;s::

co**~** :»- 

# = -l 

### = = 

# "'" = = co**~** ",.**~** ",. 

### = -l**~** 

### = 

## ""

## JAN-05-2009 MON 09: 51 PM

',' " '. ;' : ',' :

..,:.' 

## CLAIRTON MUNICIPAL AUT 

# ®Microbac Laboratories, Inc. 100 MARSHALL DRIVE WARRENDALE, PA 15086 

### (724) 7n06]O FAX (724) 772·]686 

### TOM ZIERENBERG;MANAGING DIRECTOR http://www.microbac.com

"'1' ",**I~** ", :r",':" 

## P, 013 Page] of] 

### INVOICE No. 37078

CLAIRTONMUNICIPAL AUTHORITY MR. PATRICK CANAVAN Pay 3
- Wastewater Samples for Analysis


### 1NORTH STATE STREET CLAIRTON, PA )5025

',; .','; ,; 

### . :. 

### 0812·00788 Pay 3· Wastewater Sampiss for Analysis



## Please inclnde this InvoiceNumber lind your Client Account Number with all remittances .. : i $254.00

$264.00 

## $264.00

## JAN-05-2009 MON 09: 51 PM CLAIRTON MUNICIPAL AUT 

# ®Microbac Laboratories, Inc. 100 MARSHALL DRIVE WARRENDALE, PA 

### 15086 (724) 772-0610 FAX (724) 772-1686 

### TOM ZlERENBERG, MANAGING DIRECTOR hr<p://www.microbac.com

!"'"

. !,": 

## P, 014

MEMBBR 

# mo INVOICE Page I of!



## No. 37078

CLAIRTON 

### MUNIelP AL AUTHORITY 

### MR. PATlUCK CANAVAN Day 3 • Wastewater samples for Analysis


### 1NORTH STATE STREET CLAIRTON,PA 

### 15025

.: '::' 

### 0812-00788 12122/08



### . . , 

### ..,

### . 

## ';**:~** 

## >;**~:** 

## :. :.: ! .:, :. ".,:._'1,:,

, ,I r i

.. ':

.. :' ; 

### Day 3 - Wastewater Samples for Analysis

\



## Please include this Invoice Number andyour Client 

## AccountNumber with all remittances :.**~** I ',: '

..,.,' 

### $264.00

## JAN-05-2009**I~ON** 

## 09: 51 PM CLAIRTON MUNICIPAL AUT 

## p. 015
® 

## Microbac Laboratories, Inc. 100 MARSHALL DRIVE WARRENDALE, PA 15086 Page 1 of2

(724) 77:2-0610 FAX (724) 772-1686 

### TOM ZlERENBERG, MANAGING DIRECTOR http://www.microbac.com 

### State Laboratory CertificationNumbers: PADEP: 02--257, NC: 42703, WVDEP: 2)5,9951 CM KY: 90136 U-lli.MlS·l'KY • MlCRU1,UUJ.,UUY 'l'UUlJ**~A-":E'1':r** .**I,;UN~UNI.I:Kl'.KUlJUCTS** 

### WATER· AlR· W**ASTE~** 

### . 1'UOI)

. PHARMACEU'flt:Ut; . NUTRACEUTlCUS

CLAIRTON MUNlCIP 

### ALAUTHORlTY 

### MR.. PATRlCK CANAVAN 1 NORTH STATE STREET CLAIRTON, PA 15025

POlmitNo.: CustP.O.; 

### CERTIFICATE OF ANALYSIS

SUUJECT: Day 3

- Wastewater Sample, for Analysis Date Reported: Date Received: OrdecNumber: Invoice No.: 

### Cust#: Sample Date:**Salll~le** 

### Time: Sampler/Temp: 12122/:2008 

### 12/1112008 0812-00788 37078 Cl23 l21l0/Z008 0;00



### TEST METHOD RESULT UNITS 

### DATE TECn

Chloride 011 ,a50 Total ......rSSOlved Sands

.-.j'" :::. ,. 

### "::":', Chloride Oil &. Grease Total Dissolved Solids



### 103.::'



### ... ,. ".'
Chloride 011 & Greese Total Dissolved SDlids

:hlorlde )il & Grease rotal Dissolved Solids EPA 325.2 EPA 1664A**~PA** 160.1

EPA 325.2 EPA 1664A EPA 160.1

EPA 325.2 EPA 1664A E:PA 160.1

EPA 325.2 EPA 1664A EPA 160.1**'~1** 14 70S

330

14 

### 876

4).1



### 7 1,020



### 516 <17 1,210 mg{L 12{17/08 mg/L 12/18/08 mg/l 12/17/08

mg/L 12/17{08 mg/L 12(18{08 mg/L 12/17/08

mg/L 12/<7{08 mgfL 12/18/08 mg/L 12/17/08

mg/L l2{l7/0B mg/l 12/18/08 mg/l 12/17/08

ThE: data and InibrmatlQn on this, and othe.r accompenylng documents, repre52l1t o:'lly ItII: S/JmpleCs) analyzed and 19 rendeted upon comfltlon that It 19 not to Ix: reproduced wholly or In part fur**~;j\lf.:rfulno** or other purpose:; without <lPJlI1lval from the laboratory. USDA-EPA-Nf05H Th5l1nc food sanltatlcm Consulting Chemical and Mh;rob1oiog1cal AlTc'llyses and ReS"eaKh MEMtlER 

### NAB: ADS ADS



### NAB: 

### ADS ADS



## NAH 

## ADS ADS



## NAB ADS 

### ADS



# mill

# JAN-05-2009 MON 09:52 PM CLAIRTON MUNICIPAL AUT p. 

# 016
® 

## Microbac Laboratories, Inc. 100 MARSHALL DRIVE WARRENDALE, 

### PA 15086 Page 2 of2

(124) 

### 772-0610 FAX (7:24) 772·1686 

### TOMZIERENBERG, MANAGING DIRECTOR http://www.microb.c.com State Laboratory Certifioation Numbers: PADEP: 0.2-257, NC: 42703, WVDEP: 215,9951 CM KY: 90136**C.tiliM(~TKY** - M1CJ:<.Ul:I1ULUliY ·l:'UUV**~Al'],;rr** .**CUN~UMJ:iKPKUVUL:T~** WATjjj{' AIR' 

### WASTES' FOUJ)· I'HAKMACHU'flCALS· NUTI{ACjjUT1CALS



### CLAIRTON MlJNICIPALAUTHOlUTY 

### MR- PATRICK CANAVAN 1 NORTH STATE STREET 

### CLAIRTON, PA 15025



### Permit No.:



### . CustP.O.: 

### CERTIFICATE OF ANALYSIS

SUBJECT: Day 3 - Wastewater Samples for 

### Analysis Date Reported: 

### Date Received: OrdorNumber: Invoice**No_~** CU$t#; 

### Sample Date: 

### Sample Time: Sampler/Temp; 

### 1212212008 12111/200& 08)2-00788 37078 Cl23 1211012008 

### 0:00



## tEST Ml!:TI-IOD 

## RESULr UNITS DATE 

# TEcn

Chi· Oil**~** .=ase Tot,,1 Dissolved Solids
)06'<:'**':~~** :;:: .' 

### \':.:

.... :

### .. Chloride Oil & Grease rotal Dissolved Solld5



### lbmitted By: EPA 325.2 478 mg/L 12/17/08 EPA 1664A <5 mg/l 12/18/08 oPA 160.1**1,1~0** mg/l 12/17/08

EPA 325.2 520 mgjL 12/17/08 EPA 1664A <5 mg/L 12/1B/OB EPA 160.1 1.2S0 mg/L 1'l./17/08

The**dll~** ana InrormaliDn on !:hIS, emf other tlcmmpanylng docuYnents, repr-esent DIlIV**~h<:i:** sampb(!:) analyrd c:nd Is" tendered upon I:Uildltlon thBt It Is not 00' De repl'O(luced wholly or In part for advertising or other purposes without IJIJProval fmm the**rafxlfilto~)'. USbA~fPA-Nlo5H** **TE!~n!J** Food $oIrlt:2Itlon Ctruult:lng CIlemlQd and Mlo-obroioglcal Anall'Ses !!mtf**~8searc:h** 

### NAH 

### ADS ADS

NAH 

### ADS ADS

MEM1U'!R 

# tltlll**~**



### = D-

>- 

### = -< --' -< D- '-' 

### = 

### = :2 

### = 

## = >- 

## = -< --' '-'

::>' D- 

## ""**~** 

### = = 

### = 

## = :2 

### = = =**~**



## ,**~** 

### =



## , = -<**~** WemalUl Workora.,# 

## Microbac Laborator' ,Inc.
- Pittsburgh Division Pag"

__o' 

### 100 Marshall Drive, Warrendale, PA. 15L_A Phone (724)772-0610 Fax (724) 772-1686 

## OJ, (;).

- 

# 'I

# n; Chain of Custody am piing S;le/P roject: (please Fitl Out Completely using peITr1anent ink) Cusmmer Reporting lnfonnation Special instructions: SAMPLE MAlRIllCOOES Company: POiI

__

### x WATER SOLIDS MISC. Fax Dfinldlll Contacl Name: 

## C{.&'A../<>4**.~ild** 

## 11<117/ Report 

### Yes N. 

# iwalllr DW 5011 SO 

### on Ol E-mail GrooM SIreBl: Report Yes No Water 

### OW SluxIge Sl WIpeS WP 11 SWing infonnatlan is differe1lt than Reporting Surfa", City: RoUU"" TAT: Yes No lnfonnaoon Please fndTc:ate below 

### w_ sw Wasm SlItabs SB SlalelZip:. Hno, Specify days below C(mta.ct.Person: Phone: Rush TAT RequesledlDays): Phone #:. E-mail: <2 2-5 5-7 DEPPWSID#:
SAMPLE

Matrix SMl.!PLE COLLECTED SECODES MOVE. if)'Ou NlI. OF SAMPLE IDENTIFICATION 0 CONTAINERS ma1rb:'ts not 0 IisfBj spec""**~ ~**  mar.rix 

### g 

# !**~** belo" DATE TIME 

# 4<i47/W 

# I**f't~i** n!c 

# r**I~** 

# L L 

# iZJ/';63 7:S- 

# 1)( f;I 

## J 

# .J 

# 17/1-4-**7~'>o** 

# Ii**'~** 

# Z-.



# y kftolti**7;~u** 

# Ii i!t Z-**~** 

# '1k/eg**7~>O**

# I~**~** 

# Z- S. 

# r;, '¥j,f 1)5 0

# ~~**~** RelinlJ.li:9:lIe4 Hy;(Signalure) Da(i! l1rr,a

eincpJIsltad**B~stgi\'ilLura) D~'**  11,..
Relinquished B'(.lSlgnafure)

# ·h7~ 

# ria TI"", 

### .'2. 

### Ii 0.8**/~ ~** **o~** ,. Sampled By:**.~** Chlorine Reading: omfrtiot1: Please deliver 51lmples to (he lab as soon as possible after roliection to ensure that holding**~",g"Samp{e** Teffll: times will be met. Please fill coe out completely to**e)(J)ed~e** sample Log-in. , '0

1"10

__**""~...Jr**... 1 t..i

..... nllnl;J"JJ';1nlllF; 

### w
.... Water 

## Iww Ili<ruid l Food FD Trip Bfan, T8 Solids S**Micro-bi~ogy** Me Reld Blank fB 

## I Presernilli/ll 

### il'**~** 

# '" Analysis Requested 

## " ·z !!.



# .. z :r: 

# '" 0 :r: 

# '" z [J) ,,2: 0 

### z [J) 

# " :r: 

## '"**~o** Z 0 0 0 Cl 0 0"- m 

# '" ... :r: r- 

# '" >'il 

# Iii' ,/ 

# TV'S. 

# C/-Ic.c,.,.,t¥J 6/t.-{-C-;d! / 

# Iv Iv

V- 

# IV'" 

# /
il 

# Iv 

# I 't/ 

## Y 

# , /
V 

# Iv 

# ""

Recell.'Ed nw Tilne By:(,si-;lnarore)**Rooel~oo** 

# 4ltK 

# Iz1JoJ f( lilT¥! By;{6IlJl!i:ure)

### ~/;j**!Re~lo;E.d** 

## IB,'I""'''''''''l 

# I 

# /1' " 

# .. 11", Field Sampling Notes: EQUI PMENT BLANKS"AND FIELD BLANKS ARE USED FOR INTEl'\NAllAB USE DNLYlNOT BILLABLE). NOT REPORTED UNLESS REQUESTED BY

. CUSTOMER.

Re\r.:O Cl!;l0lllld BrJhAtJ IWam:dllsa 

## Mlcrobac Laboratori 100 Marshall Drive, Warrendale, PA.**150t.~** 

## Inc. - Pittsburgh Division Page

__ ol Wor1<ortler # 

## Phone (724}772-0610 Fax (724) 772-1686 

# :: I oQ 1::1.
- 

# S""lJ 0:. 

### Sampling 

### site/Pi Jec\: 

### r _l!Srunor 

### ; ,,1.t" 

# (utl1.1181\
;tName: 

### Slr.et

____________ 

## -1 city: 

# I phone:

____________ 

### -I E-mail:

Matrix**:SECODE~** 

# Chain of Custody (please Fill Out Completely "'lfl!j permanent ink) SpeciallnslrucUons:

, POiI X



# -- Fax Report Yes No 

### E-lnau Report 

### 'Yes 

### No
Routine TAT: Ye, No 

# r Bming information is different than Reportirn.i Information PleB.5e indlcate belo11l It no, Specify days below 

### rontad Person: Rush TAT R"'Iuested(Days): Phoneil:

<2 2-5 5-7 DEf' PWSID I/:

JI t= l'.l'Il E,lfl'OOlJ SAMPLE IDENTIFICATKlN 'NO. OF 

# potrr.

1- 

# = -<C -" -0: "- '-' 

### = = ::2 

### = = <--- 

# = -<C -" '-' ""b 

### not d 'pecify Jurma1rix. 

## It-. 

# CNX

# -3 11'L._L 

# 'I DATE 

# 1 TIME

# I~

# 1~1~1~1~lp \1.1-O'<j 

# I 'i']"Au

# I~-I~IJI 13 r 

# H SAMPLE MATRIX CODES 

### WATER 

# J SOUDS 

# ] MISe. Drinking Wal",

## ~~nd

ater

. Su.- WEtST Wasle Weier Top BI"" Fl<1d Bl!mk DW GW
SW WW TB FB

## ~**~** 

# a
0 

## 9**~o** 

# ."-**ll,~** Sci SO Oll 01 SludQe Sl Wipeo 

### WP
Wasta swab, S1l UqtBd L food 

### FO Soids S MiCllJ..biolagy 

### MC

Analysis Requested



# IJ.AJ.tfu

::2 Dam**~** R-I!09ilibd' 0at.9

-- --- --·TwX 

## "- It- 

# if**/()~lf(** /l.'"! Ily;ISi"".Im" 

# /t,o P''1)A'<**~** Re1:lli.y.;;d D:at.e Time 

### = 

# I;;' 

# "',(81,,,,,,,

..) 1;Z

# -'1.-.f: 

# Ii r;.1 0 

# = -**~~** 

### =**'''I'OIl"",~)** 

# 1"-/'/ 

# It 'I'l>b 

## = ::2

_ t7 F'eld Sampling Notes: EQUIPMENT BLANKs AND FIELD BLANKS E SED FOR 

### =

## ~ i@y..'lZd[e,!JL-l)-O,3''1]01WJ.INTERroIALLABUSEONLY(NOTBILLABLE), NOT REPORTED UNLESS REQUESTED BY

### ~ Sampled

### B~? .

### <!O~ I ' CUSTOMER,**~** Chlorine Read ng:**~** 

### =



## , = -<C**~** Please deliver sa.mples 10 the lab as S{]OD as po:.ssible after IXlllectiDII

# to ensure that hakllng \"--",.--

...r

. tlrnes will be

### meLi"leaoe fill CO C

### OU! completely to o"".rllle sample Log-In, "C

### ~,).-' Rev.=o Cro!1aled 8!(.MAD

# JAN-05-2009 MON 09:53 PM CLAIRTON MUNICIPAL AUT
®

# Microbac Laboratories, Inc. 100 MARSHALLDRlVE WARRENDALE, PA 15086 (724) 772-0610 FAX (724) 772-1686 TOMZlERENBERG, lvlANAGING DIRECTOR**http://WW\V.mi~obac.com**



### CLAIRTONMUNICIPAL AUTHORITY MR. PATIUCK CANAVAN 

### 1NORTH STATE STREET CLAIRTON, PA 15025



### . ': ::, 

### ,. "",:



### 0812-01064

" :": 

### .,..... : ;**~** ; 

### . ,.': 

### . " "; ; , . ',,!!; "'''.1; :

# ..... , 

## .
. '," t:· i' ('I •.· •• 

### f': :: samples for Analysis



## Please include this Invoice Number and your Client Account N1Ul.\ber with all remittances 

## p. 

# 019

MEM9ER: 

# DII INVOICE Page 1ofl



## No. 37372



### $528.00

# JAN-05-2009 MON 09:53 PM CLAIRTON MUNICIPAL AUT
® 

# Microbac Laboratories, Inc. 100 MARSHALL DRIVE WARRENDALE, PA 15086 (724)772-0610 FAX(724)772-1686 TOM ZIERENBERG, MANAGING DIRECTOR 

### http://www

. ...;crob.c.com 

# P, 020 Pago 1 of!



### No. 37372

. "1 .}

## \~',:,:: CLAIRTON 

### M:tJNICXPAL AUTHORITY 

### MR, PATRICK CANAVAN .Wastewater Samples forAnalysis


### I NORTH STATE STREET 

### CLAIRTON, 

### PA 15025

12123108


### Wastewater Samples forAnalysis



### Please include this Invoice Number and your Clieut AccountNumberwith all remittances ",

.**.~** 

### . 

### $528.00



## $528.00

## JAN-05-2009 MON 09: 54 PM 

## CLAIRTON MUNICIPAL AUT p, 

## 021 

## Microbac Laboratories, Inc. Page 1 of4



### 100 MARSHALL DRlVE WARRENDALE, PA 15086 (724) 772-0610 FAX (724) 772-1686 TOMZIERENBERG, MANAGING DIRECTOR 

### http://wwW.m1c{obac.c

# om State L.boratoIy Certificatioll Numbers: PADEI': 02-257, NC: 42703, WVDEP: 215,9951 CM KY: 90136 CHJ>M1S"U<.Y

. MICKU IULUt;iy' F()U)) SM' Tl'" CUNSUMI:ili. !tUlJUc-n; WA:l'l:iR' 

### l\..lli.' WASTES, t'OOJ)' PHAJ{MAC/:iUl1CALS' NUTKACEUTlCALS

CLAIRTON MUNIClPAL AUTHORITY 

### MR., PATRICK CA:NAVAN 1 NORTH STATE STREET CLAIRTON,PA 15025



### Permit No.: Cus!P.O.: 

### SUliJECl': Wastewater Samples for Analysis 

## CERTIFICATE OF ANALYSIS
Data Reported: Date Received: 

### OrderNumber: mvoice No.: Cust#: Sample Date: Sample Time: SamplerlTemp: 

### 12/23/2008 12115/2008 

### 0812-01064 

### 37372 Cl23 12/] 112008 0:00

TESl' 

### MEmO)) 

### RESULl' 

### UNITS 

### DATE U<CR

Chloride Oil ar.:rease Toti ;olved Solids

::hlorlde )jl &. Grease**'Ci~1** Dissolved Solids

13

.... I,,'



### ..: ....**~.** ;:',: 

### .

, 

### , II & Grease ,tal Dissolved Solids



### ,Iorio. "i1I. Grease tal Dissolved Solids EPA 325.2 EPA 1664A E:PA 160.1

EPA 325.2 EPA 1664A EPA 160.1

EPA 1664A EPA 160.1

EPA 325.2 EPA 1664A EPA 160.1 183 7 664

364



### 7 942

S 

### 946

351 <17 

### 932 mgfL 12/23/08 mg/L 12/'22/08 mg/L 1Z/19/0B

mg/L 12/23/08 mg/L 12/22/08 mg/L 12/19/08

mg/L



### mg/L 12/23/08 mgfL 12/22/08 mg/L 12/19/08

Tne. data anti Informstlon on**thl~,** and orh!lr I!ItOJmp.lftylng documents'. represerlt only the SlImple(s) 6ni:llyzed and Is re:ndered Upon cOi'ldrt!on that It Is not to be rop;uduced wholly**O~** In Pllrt fur advertlslng or Qther Pul'pCls:;5 wIthout !IPDrovall'rorn the labnrotory.

USDA-ePA-NIOSH Testing Food**.sanl~tlon** CC!l'3ultlng**a,~car** aM MlaoDlo)ogfcol Antllyses and RE$eafCh 

### MEMBER NAB: 

## RDP ADS



### NAB: 

## RDP ADS



### NAB: 

## RDP ADS



# hll

# JAN-05-2009 MON 09:54 PM CLAIRTON MUNICIPAL AUT p. 

# 022
® 

## Microbac Laboratories, Inc. Page 2 of4 100 MARSHALL DRIVE WARRENDALE, PA 

### 15086 (724) 

### 772-0610 FAX (724) 772-1686 TOMZIERENBERG, MANAGING DIRECTOR http://www.microbac.com State Laboratory Certification Numbers: PADEP: 02-257, NC: 42703, WYnEP: 215,9951 CM J(Y: 90136 CHt:M.ls·nc\,

. M.lCKUlllULUliY

. ¥UUJJ SA1:'bTY

. CUNOiU ·K.PKUJJULTt; WATbR' AIR·**WA~THS** '1'00))' PHARM/>.CtUDcALS

- NUTRAcEU'I'lCALS



### CLAIRTONMUNICIPAL AUTHORITY 

### MR. PATRICK CANAVAN 

### 1NORm STATE STREET CLAIRTON, PA 15025·

Permit No.: 

### CustP.O.: SUBJECT: Wastewater Samples 

### for Analysis 

### CERTIFICATE OF ANALYSIS
Date Reported: Date Received: OrderNumber: Invoice No.: 

### Cust#: Sample Date: 

### SBDlple Time: SamplerlTemp: 

### 12/23/2008 

### 1211512008 0812-01064 37372 

### CIZ3 12111/2008 0:00

TEST 

### METHOD 

## RESULT UNITS DATE TECH

Chic Olle.. .::!a;se Total Dissolved solids

)11 & Grease rota! Dissolved SoJlds



### :hlorlde )11 &. Grease 'otal 

### Dissolved Solids

hloride 'i1 & Grease 

### otal ". '0lved Solids


### 9/·Locati6d ' cPA 325.2 EPA 1664A EPA 160.1

EPA 1664A EPA 160.1

EPA 325.2 EPA 1664A EPA 160.1

EPA 325.2 EPA 1664A EPA 160.1 335 <5 954

<5 948

258 <5 794

381 <5 952 mg/l 12/23/08 mg/l 

### 12/n/08 mg/l 12(19(OS

mg/l 12/22/08 mgfl 12/19/09

mg/l 12/23/08 mg/l**12/~2/08** mg[l 12/19/06

mg[l 12/23[08 mg/l 12/22/08 mg/l 12/19/08

Tho;:: dllta and Inrorltltltlon on thJs, and**oth~r ell;comp~1n9**  dOC(lme:nts, repre5E!nt: Drily thIS: sample{s) analy.ted**~nd** Is rendered upnn conditJgn tlEt It I.!! !'JOt to be reproduced wholly or In part fot Bdvertlslng or oHler**pu~s** without approval frOm the lilbol<!toty. USDA-EPA-NJOSH Testlrlg Fo.cc Sl:Inltatton COnsultIng ChemIcal and M1C1OblologlcaJ Analrs!!S and**R~ord!** 

### Ml:MBcR 

## NAB RbP ADS

ADS

NAIf 

### RbP 

## ADS

NAIf 

## RDP ADS


# rtllJll

# JAN-05-2009 MON 09:55 PM CLAIRTON MUNICIPAL,AUT P, 023 Microbac Laboratories, Inc. Page 3 of4 100 MARSHALL DRIVE WARRENDALE, PA 15086 (724) 772-0610 FAX (724) 772-16&6 

### TOM ZlERENBERG; MANAGING 

### DIRECTOR http://\X!'WW,mio;obac:.c:om State Laboratory CertificationNumbers: 

### PADEP: 02-257, NC: 42703, 

### WVDEP: 215,9951 CM KY: 90136 Cl-lliMl:sa<.y • MlCKUHIULUliY • r'uuu**:;Al'J;lT~** • CUN:;UMJ>KYKUUUCn; 

### WATER· AlK

. WASTES' .FOOl)

. l'.tiAKMACEU·UCALS

. NUTRACEU'rlCALi;;

CLAIRTON MUNICIPAL AUTHORITY 

### MR. PATRICK 

### CANAVAN 

### 1NORTH STATE STREET CLAIRTON, PA 

### 15025

PelmitNo.: 

### CusIP.O.: SUBJECT: W.,tewater Samples for Analysis

Chloride 

### 011 ase Total vlSsolved Solids

Chloride Oil & Grease Total Dissolved Solids

)11 & Grease iotal Dissolved Solids

:hloHde 

### lil & 

### Grease ·otal Dissolved Solids EPA 32S.2 EPA 1654A EPA 160.1

EPA 325.2 EPA 1664A EPA 160.1

EPA 1664A EPA 160.1

EPA 32S.2 EPA 1664A EPA 160.1 

### CERTIFICATE OF ANALYSIS

408

<;5 1,020

331 <17 820

<5 

### 804

300 

### <5 780 DateReported: Date Received: OrderNumber: 

### Invoice No.: CUst#: Sample Date: Sample Time: Sampler/Tomp:

mg/L 12/23/08 mg/L 12/U/08 mg/L 12/19/08

mg/L 12/23/08 mg/L 12/22/08 mg/L 12/19/08

mg{L mg{L

mg/L 12/23/06 mg/L 12/22/08 mg/L 12/19/08

The det,t:! tmd Information on thiS', and oltu;r**~mllcmvlnll** documents,.**rep~l'lt** [lilly**th~** ':;;lImDI€(s) an<lI)lzed and I:i rendered upotl =ndll:Jnn th;:.t It 1:; not to be reproouced Wholly or In p;:lrt for advert1s:lng at' other PllI'pCJSes without approval from the laboratory. USDA-ePA-NlOSH Testing food**SBnJ~t1on** Consultln!l Chemical and MkrobloJoglCII! Am'll).':;es and**~arch** 

### 12123/2008 1211512008 0812-01064 37372 C123 12/11/2008 0;00



### MEMBER NAH 

## RDP ADS

NAH 

## RDP ADS

NAH 

## RDP ADS



# ratl

# JAN-05-2009 MON 09:56 PM CLAIRTON MUNICIPAL AUT p. 

# 024 ® 

## Microbac Laboratories, Inc. Page4 of4 100 MARSHALL DRIVE 

### WARRENDALE, PA 15086 

### (724) 772-0610 

### FAX (724) 772-1686 

### TOM ZlERENBERG, MANAGING 

### DlRECTOR http://wwtv...m1cI::obac..com StateLaboratory Certification Numbet·s:



### . PADEP: 02-257, NC:42703, WVDEP: 

### 215,9951 eM 

### KY: 90136 l.;j-lliMlS·lKY

. MlUKU,BJU.LU(jy : FUUl) SAl')':',,),'

. UUNljUMbKJ-'KUl)UCTS 

### WATER· AiR' 

### WASTES, FOOD 'l'HAlZMACEU'11CALS

. NUTRACBU'l'lCALS



### CLAIRTON MUNICIPAL AUTHORITY MR. PATRICK CANAVAN I NORTH STATE STREET CLAIRTON, PA 15025

PermitNQ.: 

### CustP.D.: SUBJECT: Wastewater Samples for Analysis 

### CERTIFICATE OF ANALYSIS
DateReported: Date Received; OrderNumber: Invoice No.: 

### Cust#: Sample Date: 

### SaInple Tim.: Sampler/Temp: 121:2.312008 12/15/2008 0812-01064 

### 3737:2. C123 1211 112008 0:00



### TEST METHOD RESULT UNITS 

### DATE TECH

The data lind Information 011 thiS, lmd othEr accompanVlng ODC1l11l!nts,**TEpre5!!n~(Inlv** the S3mpJe{s) analyzea end 1.$ rtm:ll3Tli!d upon condition HH[ ItIs notto**~** reproduced wholly or In p;,rt for adverttslng or o!:her purpose;: without approval from thE: laboratory.

U5DA-EPA-NIOSH TestIng food Srmll:zJt:lan Consulting ChamlCJ)\**~nd Mlcrob\o[og\~a\**  AI1a1ySc:s ;,nd R'23eardl MEMBER. 

# mill**~ ~** 



### = <>-

r- 

### = <C ---' <C <>- c> 

### = = :2 

### = 

### = r- 

# "" <C ---' c> 

# "'" <>- 

### =**~** 

### = 

### = 

# = = 

# "'" = = =**~**



# ,**~** 

### =



# , = <C**~** lntarnal U 1

# ci;;\Q~L{ Sampling SiteiProjact: '" .---- ... ----- --.--,-----.J ---'-"".--- .-.-.----- ..." Customer Reporting Infannat! on Special Ins.tructions: SAMPLE MAllWrCODES 

### I Company:

### cI.A/~7o~**MUNI~vjh** 1>OII._x WATER SOLIDS MISC_ Fax DrillktnlJ Contact Name: Report 

### Yes No Watfr 

## ow Soil 

## so O[ OL E-mail Ground Street Report Yes No Weter GW Sludge SL Wipes WP If Billing information is different tl1an Reporting Surfaoo City:**Rouffn~** TAT: Yes No Information Please indicate below Wafer SW 

### waste Swabs SB Waote SlatelZ.ip:

. If no, Spoec::iFy days below Contact Person: Water WW Liquid L RJOd FD Phone: Rush TAT RequesleIl(Days): Phone'ik Trip**f3~nk** T8 Solids S . M"KrobJology 

### Me E-mail: <2 2-5 5-7 DEPPWSIDfI.:**A~d** Blanf< 

### FS 

# J Preservalive SAMPLE

Matrlx SAPflE COLL.l:r:::TEO SECODES 

# "**~'.OF** m BOVE, ifyou "- SAMPLE IDENTIFICA110N**~** 

### Analysis Requested**~** FQtHA!NERS Z 

## " matrixis not a I!!. 

# " :c ID 

# " D&!ed gpeciIy Z 

## '"**~** :c N 

### z en o=:



### urmatnx a Gl 0 Z 01**~** 

### :c 

## '"**~c**

## ~**~** Z 0 0 0 (") 0**~** "- below DATE TIME m 

# '" 

# .,. :t r- 

# '" ll-iil 

# to**~r** 

### CiJ! I r,rJ 

# / iJIr;j(')[; 

# g:..;7" IX- 

# Z i/ V 

# Ttl 

# s;, 0)" 

## I-G-i'f 

# C'yW.,:c.c-d 

# z.. i2/;fk f;;('l-., 

# l>c 1 

# .J.**Iz.flf!.~** 

# 8',07 y 

## 2 

# r; ii/tlo

# g 

# t:rl6 y 2 

# S**2/1I1.~** 

# 8:0 :1 

# Ix**~** .:- 

# (0 

# i2J!t/of**~',O6** 

# Y 2-**R.elillqliRl~d** El'r.(S"gnal\J1l!)**",~** 

# """ Relinqti"&Iet1 B'r.(stgnahze)

# £.._d~ /2;,(&'"**"~ /6~6~** **R.elinqli~erl** B'r:(-Sigwdl.m) 

# /' 1/**D'~** 

### nma j. I**~**

- Sampled By: ChID ['ine Read ing: Comlilkm: Please deliver samples to the lab as Soon as p-ossible aller corfectioI1 to el1sure that holdin!1**j!o,'o'g.SalT1JleT~** times will be met Please fill 

## coe ou{ completely [0 expedi1e sample**Log~ln,** '0 

# 6,

'n
..... r ...",fno,llI.I,,· f'I,/InClll1;1nA&:: i/ 

# "" I"" v- 

# I

V V 

# I

1/ V 

# \

# // I"'" V" 

### ¥

iU!oohooo 

# £ " """ 11""**B~:(Sigrtalure)** 

### Jl--/:S"..:.j,

### R~ ReraNEd

# /~**.~~~** 

# GliS--Pd "Time 

# O "'I"""'

....) 

# /!tl Reteivw LJ ./ 0.", 

# ""'" By:(S4;!nall.l'e} field Sampling Notes: EQUIPMENT BLANKS AND FIELD Bl.ANKS ARE ",ED FOR INTERNAL LAB USE ONLY{NOT BILLABLE)_ NOT REPORTED UNLESS REQUESTED BY**.~** CUSTOMER.

Rell'.:(J CreatEd**RIf'J.f~n**Itrtflmal t.: 'I Workorder# 

## .'I1icrobac Laborator , Inc•• Pittsburgh Division Page

__ , 

### 100 

## Marshall Drive, Warrendale, PA. 

## 1511,,0 Phone (724)772-0610 

## Fax (724) 772-1686 <=**~** 

### = 0-**~** 

# = Chain of Custody (Please Fill Out Complete!;, usine permanent ink) ISpeGiaJ 

# :**c.tA.,4:~nW** 

# ;u,TlidtJ PO# 

### x Fa. Ves ,No

\Gontact Name: Rilport E-mail 

### street: Report Yes NQ**l'~i:HI:lJ II,;>~~**  I.;;IIUUYC HBilling information is different than R"1'orung Surfa". 

# Iclty:**-----~**________ _I Routioe TAT: Ves No Infarm.llon Please indlcate below 

### .."'C"""

___,_

\stateJZi P:' II no, 5peoify 

### d.ys below Pho"", Rush TAT Requesled(Days): E-mail: <2 2-5 f>.7

--
- SAMPLE

Matrix _SE CDDES**I~;;;;VE, ~you** **rm~lrlx** Is nat Sl>MPLE OOUECTED

,d spec;ry r rmrlrix SAMPlE IDENTIFICATION

DATE 

## ,

TIME

### ~ ,

# ~,af OIITAI 

# '"**~** :z :J:

### ~ Z r

# I~ a z (J> 

### 1) z 0 0 o 0 m 

### '" 

# ... :I: r- '" 

# Ir Analysis Requ ested 

# 'ftjJg g;2 0 

# If I 2- v' 

# v**~n-'** 

# 1.. , ((oN 

# '""" ---' 

## '""" 

# rps' CuW, 

# CMQn,.?>{(

0- eC> 

### = 

# = 

# "" = 

## =**~** 

# = '""" ---' co


# " "'-' <=**~** 

### = 

### = = L

'"'}'·l"'1I' 

## .:< 

# 12lJ'h,)J**8~/g** 

# III I J-.**~**

# l~zkS f;d 

# rl I 2- 

# r**;t.A/~ /?~/(,**  

# lXl I '2.. 

# S

# J.tj-%~ jJ;/() 

# y 'J, 

# 'f;r/r£ /" 

## I( 

# 2-**~-;~ ~'**  

### ,"
Dale To"",

# ~,4.~ DaLe--

.**-l-~me** 

# IiLjl'/',,!' /0

## ~oC> 

# I' 

# ftl I**D.~** l-: Torn, {/ 

## i/ V {/ 

### V 

### IRe"""'" tsy:(SlgMI 

### ;/ 

### 1-

;/
V 

### V 

## f/



# '" L /J::2j

## IRe~""_~-/BfZ?W'htU'P 

# 1"_'''''--. LV :J , j 

# I


# 17/ v 

# I ""'! 

# I T"", 

### !21!c/,\)f 

### of:,:. Q 

# b ;}{I,ft /l"H """**1l~ ~**  'freid Sampling Notes: EQUIPMENT BLANRln\NIJl'IEDJElIJIfIKS ARE USED FOR 

### = lNTERNAL LAB USE ONLY(NOT BILLABLt;j. NOT REPORTED UNLESS REQUESTED BY 

### = Sampled By: CUSTOMER. 

### =**~** Chi [}ri ne Readlng:**~** P(ease deliver samples to the lab as soon as possible after collection to enSllre that holdrng**~** limes will be met. PI.as.fill COC out completely!o experlile sample Log-in, 

## '"""**~** Rev.:D Cre;rtsd Bv:M4D**~ ~** 



### =**~**

>- 

### = <C -' <C**~** '-" 

### = = 

# "'" = 

## = >- 

# = <C -' '-" 

# "'"**~ ~** **~** 

### = = 

# = = :2 

### = = =**~**



## ,**~** 

### =

I 

# = -<C**~.** Inf.Dmllll Usr

# Oi\1--:\Q~l( IVlIl;.rVI.lc:n

... L.d.):.IUIQ.I,U11°- -, III

...... - T

... _ ........ ltJU

_ ... .--._u 

### 100 Marshall 

## Drive, Warrendale, PA. 15C Phone (724)772-0610 Fax (724) 772-1686 

# Chain of Custody**U"1~'I;f~** I' (please**Fi~** Out Completefy using permanent ink) 

### Cf4,'/I... 7(J",) fflt,)hJ, 

### ftfIvTJ 

## 1PV11 Fax Contact Name: Report E-mail Street Report 

# " Yes No Yes No Cil)': Rootin. TAT: Yes No S!ateJZip: Ifno, Specify days beiovi ISpecOil WATJ:'g

## ~:!n~ 

# low ·IGroUJH!

W-",",---- 

# I GW III BmUng In!omotion Is different th", Reporting s..rr.ce Information Please Indicate below

. WalE< SW Waste IContact Pe",oo: Wat.. 

## ww Phone: Rush TAT Reque,ted(Days): E-ffiai[:; <2 2-5 5-7 

# I phon.e.#:. • 

## ITilJl Blan!< 

# 1m 1

0

__ DEP PWSID #: Foe!d Blank FB
SAMPLE

Matrix**~** _"uut:::; JVE, ifYOUI 1U1X is oot 

### ,ct spedf)I**I~~r** matliK SAMPLE IDENllFICATION

## !~)CATI '"rJ ; 

## 2.. 

# ..1



# c; .5 

# Co SAtRE COllEClEO

DATE 

# I TIME

# I~ 

# 11**1~7Usl g~jy**  

# W**Vz;Id,~ g~iJ.**  

# jx

# 1/z/;'1.~18'iO71y

# li~lo& 

# IR:rl6 

# 1)(

# liz!tIIo~1 &';0

# ~ 

# 1)(**~~Jkl** f',oo 

# Ix IND. OF lCaNTAlI"c


# 2 1 

## 2 

## 2 2- 

## 2-

# I~**I~**

# I§**I~** 

# Ip k
v 

# !v 

# Iv 

# 11/ ltV Iv

t--



### v


## v j/



### v**~** 

# f c: c !'!. 

### Analysis Requested

# II~ It? S, 0 

# /C /-?/'t.**Cj,lC.v,.I~;;"(** 

# 1 / JJL :v D,r. 

# -:z. £ Tma**l~e~ad.** 

# I D,r. 

# I Time 

### 1,z-/s-e.J R;[465 

## -,. 

# ILdk D"'" 

# v,,"?

# ;.6R**Th~** 

### /0**~<l~** 

## D," 

# I' 

# /'1**~**..**~** 

# r: lim. 

# I Rat:aivild B,:13Jgna< 

# 1_'''''

# ~t.I.llk**~**

# ~;'r-d,?l' 

# ;i(Jo

o.r. Time Field Sampling Nill

..: EQUIPMENT I:ILANKS ANI) FlEW BLANKS ARE USED FOR INTERNAL LAB USE ONLY(NOT BILLABLE). NOT REPORTE.I) UNLgSS REQUESTED BY ui:L1111-'Jed By: CUSTOMER. Chlorine Reading:**Pl~se** deliver samples t() the lab as. soon as I'ossiille after coJlectlon to ensurn fha[ hol[Jing**~'L'g.S~6aTrr'/** Urnes will be met. Please fill COG (luI c.ompletely to**e~edite** sample Larrln. C 

## lO

____ RelJ.:O 

# n..... ............**+O-.-.~** hi

... • nJlfl.I:iOl;-{**ntI~** Craa1ed By:PMDIfnlcm_' Us

.. r IVn

....luu.Q:\# LClJJ'VIC('il.Vllr IJn

.... -I

..._ .......**,.~** •• _0

....__ ....." Womar,k 

### 100 Marshall Drive, Warrendale, PA. 150. Phone (724)772-0610 Fax (724) 772-1686 

## Chain of Custody = 

## "" (Please Fill Oul Completely using permenent Ink) 

### = Sampling.51telproject:**~c~u~~~o~m~.~r~Re~p~o~ru~'n~g~l~nro~rm~aH~·o~n~~~~~--~I~S~pe~cl~a~t~I"~SI~ru~ru~·o-n-s:----------------------~r-----------~SAM~~P~L~E~M~A~T~~~C~O"'DES** CL

>- 

### = <C --' <C CL '--' 

### = = :2 

### = 

## = >- 

# = <C --' C>

::2' CL**~ ~**  0> 

### = 

# = = ::2 0> 

### = = 

## ""



# ,**~** 

### =



## , = <C**~.** ny.

### c;t.4/fr~.,.J hi 

### UN 11 

### uTfi PO#

__x WATER 

# I SOUDS 

# I
- - -- MISC. 

### Fax o_g Contact Name: Report Yes No Water OW Soil SO OJ Ol E-mail Ground Street Report Y8S No !water GW 510008 SL Wipes WP HBilling infonnaUon Is dlHerem than Reporting Isurfa", CiIy: RoUline TAT, Yes No Information Please indicate below Iwater SW 

### waste Swabs S6 5talemp:. 

### Ilf no, Specify days 

### below Phone: Rush TAT Reque.lodIDeys): IWast. Conmel Pe.-son: Iwale, WW UqlIid L Food FD**~i<>gy** rip Blank 

### m Solids S 

### Me E-mail' <2 2.0 5-7

Matrix

_ SI: CODES IABOVE, II)", rbt Is not**dspecl~. lYIJ~rRl1l1rilf** 

,--- SAMPLE IDENTlFIGATION

## ~1(:W 

# / .{ 

# J. l( 

# s & SAMPLE: COl1.ECTED I

DATE TIME 

# VZJ-M 3;2 0

## I%~ 

# 2;;8**I~th~** fl;tf 

# Itjz/&**;~**

# /zJ;z/o~**?~!O** 

# 2/;'/r% /.**~1.~** Da'" IDEP PWSID#:.



# ,I

No. OF CONTA.I 

## '"**~**

### ~ 

# f I 2. till 

# :t 

# (I I 

# t.**~I** "" £,. 

# vi I ;A 

## \C 

# I**2~** 11m,

# ~/t.--1-**""~** 

# """ 

# \it?,;ld /Dr;cP 

# 1'7,1 

# "", Time 

## I· z

# I~J!IU~**~ I~** **IFi~d** 

## BlonklFil


# " R 

## g: !!!.**~o** 

# l°it**~** 

# s- --"-"- 

### Analysis Requested



## 1-,/ 

# Iv


# .IJ/'S o,'.;j(yt. cj;(Cyl/§(j 

# Iv 

# 1/ 

# I."" 

# \Y Iv Iv Iv v 

# Iv 

# IV'**1~~~'.h"S11** 

# _&**/l:::;L~\** 

# I Re

-**8~;(Sj;Jnal**

# ~!l~**~..,** 

# LV / / 

# 112. v !aLB! 

# I 11"" 

# I ::'<A,{\

## J ,f
--'" c:, 

# 19-**i9JA_Ltl~** Dala Tima.

, Field Sampling Noles: EQUIPMENT BLANKS AND FIELD BLANKS ARE USED FOR 

### i IN1ERNAL LAB USE ONLY{NOT BILLABLE). NOT REPORTED UNLESS REQUESTED BY Sampled 

## By, CUSTOMER. Chlorine Rea.ding: Please denver**.sampl~s** to Ole Jab as soon as possible after Gol!ection to ensure that holding**~ 1Jg..sa~fl1/P:**  times

### 'tVi~ be. mel Please fill 

### coe out completely to expedile sample LogMin. C 

## h (I

n..
.... ,........**~l** "-1

.... - nJlr.t::nt:.-1n,u:, Rey.:O Gra&:\Dd By:MAD**nJl""'lU~1m** Ii

### ApPENDIX 

# D TABLE 3-16: "TYPICAL COMPOSITION OF

UNTREATED DOMESTIC WASTEWATER" METCALF 

## &EDDY, THIRD EDITION, WASTEWATER ENGINEER3-5 WASTEWATER COMPOSITION 

### 109 TABLE 3-16 

### Typical composition 01 untreated domestic wastewater Concentration**~d** for Contaminants Unit Weak**Me~ium** Strong Solids, total (TS) mg/L 350 720 1200

Dissolved, total (TDS) mg/L 250 500 850

Fixed mg/L 145 300 525 [luent Volatile mg/L 105 200 325 i and Suspended solids (SS) mg/L 100 220 350 Fixed mg/L 20 55 75 eegate Volatile mg/L 80 165 275**~can** 10 Settleable solids mUL 5 20 )orary lteria, Biochemical oxygen demand, mg/L: 5-day, 20"C (BODs, 20"C) mg/L 110 220 400 water 

### w for Total organic carbon (TOC) mg/L 80 160 290 Chemical oxygen demand (COP) mg/L 250 500 1000 Nitrogen (total as N) mg/L 20 40 85

Organic mg/L 8 15 35 Free ammonia mg/L 12 25 50 Nitrites mg/L 0 0 0 I con- Nitrates mg/L 0 0 0 md in Phosphorus (total as P) mg/L 4 8 15 eed to Organic mg/L 3 5 

# w, Inorganic mg/L 3 5 10 .ap. oJ. Chloridesa mg/L 30 50 100 Sulfatea mg/L 20 30 50 Alkalinity (as CaCO,) mg/L 50 100 ZOO ported Grease mg/L 50 100 150 ater is Total coliformb no/100 mL 106_107 10'-10' 107-10 9 rations Volatile organic compounds (VOCs) 1'9/L <100 100-400 >400 i other <lValues should be increased by amount present in domestic water supply. ded to b'See Table 3·18 for typical values for other microorganisms. lced iJ1 Note: t.8(oq + 32 := of. ;pools. iations Some organisms (shigella, helminth eggs, protozoa cysts) are almost never looked for 'ptage. in a routine analysis. Great care should be exercised when reviewing reported virus values. In recent years, refinements in virus detection and enumeration methods have rendered most early results suspect. Thus, the date of the study is almost as important as the reported concentration values. lUnd in 

### Need for Specialized Analyses 'ported ed that In general, the constituents reported 

### in Table 3-16 are those that are analyzed more 

### !i [18]. or less rou$-ely. In the past, 

### it was believed that these constituents were sufficient

### ApPENDIX 

## E CMA BOD AND 

### TSS INTER PROCESS DATA AND 

### CMA WEEKLY OPERATIONS REPORTS

# ~**~**

0.:

0) 

# "" 0J (:0 (:0 (:0 0J 0J**~ ~**  X <C LL**~**



### >-f0-; 0:: 0 ::c f- :::> <C -l <C 0... 0-; (,) 0-; 

### :z :::> 

# "" :z 0f0:: 0-; <C -l (,)

f'- LD Gl**~** 

### w :::> f-**~** 0) (S) Gl 0J

I f'- 0J

I 

### :z <C -0 

# I II

II 

# II NOV 30 DEC 1 2 3 4 5 6

9 10 11 12 14 \6 16 17 18 19 20 21. 22 23 24 25 25 27 28 29 30 31 

# IItJ I.wJijj 

# II

..



# -""ti1i,.

.**~**

# ..**~-** CMA WASTE WATER TREATMENT NPDES REPORT

3.74 0.37 10.0 312 4.5 140 67 3.B9 0.02 10.7 

### 341 5.2 16B 13B 3.40 0.00 9.3 263 4.0 113 55 3.16 0.00 14.6 385 4.6 121 71 3.28 0.12 11.3 309 4.4 120 42 3.13 0.00 12.3 321 4.9 128 20 3.05 0.00 14.7 374 4.7 120 3\

3.04 0.01 11.9 3!l2 7.0 178 77 4.97 0.62 2.6 108 14.8 614 780 5.21 \.13 6.0 261 11.1 482 100 5.67 0.03 B.O 379 7.1**~~A** .oil 4.70 0.21 15.3 599 5.7 223 58 4.7S 0.12 16.0 638 4.8 191 50 4.79 0.01 1!J.B 423 5.9 236 4S 5.2B 0.3\ 11.3 49B 6.0 254 96 5.10 O.DO B.O 346 6.7 289 '84 5.57 1.54 9.0 418 11.1 516 

### BO 5.55 0.00 21.3 gaS 7.3 338 43 5.2:1 0.05 20.0 872 6.1 266 40 4.55 0.00 15.3 581 4.1\ 182 39 4.28 0.01 11.6 414 5.0 17B 55 5.71 1.45 22.!J 1047 7.2 343 60 5.90 0.00 16.6 B\6 6.1 300 140 5.60 0.76 8.6 402 5.1 236 77 6.07 0.01 13.3 674 B.2 314 90 5.63 0.02 14.6 686 5.\ 240 43 6.31 0.01 7.3 323 4.5 199 51 4.93 0.00 B.6 354 4.6 189 26 4.65 0.02 17.3 

### 659 5_3 143.9 6.67 15210 76BI 3.4 

### lI,B 330 

### 4.6 130 4.3 10.3 354 8.2 314 5,1 13.1 558 6.B 294 5.3 15.3 687 S.B 250 4.6 0.22 12.6 491 6.2 248 6.1 1.54 22.0 1047 14.B 

### 614 780.0 3.0 0.00 2.6 lOB 4.0 112 20.0 DEC 2008

7.0 0.30 7.0 3218 0.30 7.1 3236 0.33

# l:~' 

# " days 6.9 3330 0.30 6.9 330B 0.3\ MlSS = 3875 mgll 6.9 3294 0.32 6.9 3138 0.32 Flllt=_ 0.05

7.0 3486 0.25 

# II SEC. AERATION CAPACITY:: 1525920 gal,", 6.S 3456 0.2\ S=C.CLP-.RIFIER CAPACITY = 410064 Q01= 7.1 3360 0.32 AVE. WAS**PUMF~NG** RATE ::i 35915 gal'dBy 7. '1"':17A non AVE. I'IAS % SOLIDS. 0.47 % 

## " AVE. PRIMARY EFF. BOD '" 64.125 IT.Q:l 7.2 0.34 7.1 3995 0.34 7.1 3!f40 0.:12 7.0 3698 0.36 7.1 3936 0.35 7.1 4458 0.25 7.2 4114 0.38 7.1 0.34 7.2 4748 0.36 7.1 4982 0.27 7.0 444B 0.26 7.2 3614 0.37 7.1 4832 0.36 7.\ 4146 0.45 7.1 0.38 7.1 4484 0.32 7.2 4910 0.30

7.1 3875 0.33 7.2 4982 0.45 6.8 

### :1I3a 0.21**~~~ ~-----------------------,----------------** 



### ApPENDIX 

## F RADIOLOGICAL ANALYSIS OF 

### CNX-1 AND 

### CNX-3 WELLS

## JAN-21-2009(WED) 07:53 

# CLAIRTON MUNICIPi>L AUTHORITY (FAX)4122333249 P.0171029 ® 

## Microbac Laboratories, Inc. 100 MARSHALL DlUVE WARRENDALE, PA 15086 

### Page I ofI

(724) 772-0610 FAX (724) 772·1686 

### TOMZlERENBERG, MANAGING DIRECTOR htlp://www.microb-a<.<<>m State 

### Laboratory Certification Numbers: PADEP:02-257, NC:42703, WVDEP: 215,9951 

### CM KY: 90136 CHcM.I;;lKY • MICKVl;SlVLUIJY •**~VVU** :SAl'lOl'Y· CVN;;UMblU'KUJ..)UC 1:S WATER· 

### AIR' WASTES' 

### 1'001)' .!:'HAJ.{MACEUTJCALS· NUTRACJ,;UTICALS



### CLAIRTON MUNICIPAL AUTHORlTY MR. PATRlCK CANAVAN I NORTI-I STATE 

### STREET CLAIRTON, PA 15025



### PermitNo.: CustP.O.: 

## CERTIFICATE OF ANALYSIS

SUBJECT: Wa.,tewater 

### Samples lor

### Radiological Analysis 

### Date Reporled: DateReceived: 

### OrderNumber: 

### Invoice No,; Cust if; Sample 

### Da.te: Sample 

### Time: SamplerlTemp: 

### 111412009 1211912008 0812-01478 38431 CI23 

### 12/19/2008 11:25

TEST METHOD RESULT UNITS 

### DAT.E TECf(

Gross Alph. 6ro< :a EPA 900.0 EPA 900.0 See Attached See Attached pall 01106109 pCill 01/06109

""Analysis performed by GEL 

### Laboratories w;.

:ubmiltcd By: om Zicronborg Managlns. Dle-Bcta

TIl!! dl,r;!:llmd InforTJ1iltloo on mis, aM**o1h~** &eeomp.,nylna documents, represent only**tf,~** :.lImD'lc(:;:} 'lnClI)'Zed allllis**~lld~** IIjXIIl c:DfIdltlon lhl:!L**111~** not**~** be reproducea Wholty or In pout ror**~d'l:i1'tf~lna** or ott\[!f purposes**wltllou~** 1!pprQ'oli11 from !:TIe labcralnl'y_ USDA-EPA-i'HOSI'11cst1ng' fOocI Sanltatlcm Catl!>ulUrrg 0lc:mlc;,1 and MIi:robi01ClglCBI AJI,lIir..e:; lind**I~nn:h** 

# ••• •••

MEMBER 

# lWil

# I**",fUI~d lI~.**  Onl, 

### Microbac Laboratorles,lnc.- Pittsburgh Division Pago

__

## or



# --- 

# l
Workoodcf II 

### 100 Marshall Drive, Warrendale, PA. 150ar Phone (724)772-0610 Fax (724) 772-1686**~61 ';;I-~**  

# lID**~** 

## Chait. of Custody <iau'(I 

### '"9**Sj(e/Proje~t:** (please fill Out Compretely**U5~llg** permanent Ink) Customer Repnrfing t9formation Special Insfrucliof.ls: SMIPLE ldATlUX CODES f;.omfmny: 

# .:_L,';.' iO 

## rJ ;11I]1I;(_,r/1/**~ffflll:j** POil

__x WATER SOLIDS MISC_ Fax DllrlkJng**r;'::'flr~ct** Nallle: 

### {it.. ;,'1 {j.} 

### .f£t./!./::;s,' .,.' Report Ye.s Uo Wa1er (lW !ioil SO Oil (}L E-mail Ground**~jl** rE::::"t: 

### I {Ij")''l 

### rlJ SJiU"c: S/: Report Yes Uo W'.ata" 01N Sludge Sl**lA~pas** \NP

..**~** (_/11A.[:,.J if Billing Information is ilifiarent than Repor1ing Surface ely: Routine TAT: Ye:5 

### No Jnfonn.a'ion Please fndicate below Wi!lte:r "Vi Waste S

.....abs S8**~i!al<~JZ~r:** 

## .'-'I l 

### r**S-o~~;-** If no, Sp€oily days 

### b.low Conia[;1 PeISGn: ,-'IH1IIe-: '1" ,) 

### J j ) --. 

## J ,'/.. Lj .£ Rush TAT Request.d(Days): 

### Phone #: C-In<:L <2 2-5 5-7 DEPPWSIDI/:



### - J!li:drm;I' SAMPLE**iJ.!'~;': ~** ',:. 

### Malrl,**S~MPL.E** COLLECTED**,~;~; ~:**  L.lECODES AnOVE, if,',}I!! No. Of S!,MPLE IDENTIFICATIDN**.~), ~.~**  0 -CONTAlr.lERS m:=.t·l)( is nol, 0**::;~~::~~.** liste;1**srecif~** . 

# " 

# ..**~~b'~'::1~ ',\~,ur**  rna<:rilc Q <> 

# ..**~ 5,)"1l1~'1.**  DATE TIME "i tx:'.a

... •**~** I**-~** 

# ;.. ' 

# C;V·l- ,**6.1~**


## -- 

# lViI-II I

## Hi-oJ**1J:t~** 

## }! 

# lif

--- 

# -

---
-'"--."-- 

## --_.on<'llF·"f.ii:!.l.,.,l Dy:{Si"t'l.c.lu-.,.**[)aI~ ll~**  

# ,>:·.1',_"','**.!g.J(~**...} ;j-,**i~** 

### k'A(j::I)'-r 

# 11**'19';'~** /l'LI(A''-1

.

-..**lhlll.i~l~ (l.":(fi.~n;;.t,uty.**  

# 9.**'~:·.7J".,-:~;~~-c-:-~.-~** 0>1"**T~.** 

### Il-I'l-rJJ' 

### If

.**~.** ..:;. 

# .......'".**'~**

### ..**,~..!;"** I":"""'] r,i:(Si"'l

...**~.t"~l** - .. 

## )

..

## ::~):;:.{: Oal!! 

# It";"

- .'\



## .**'0·7(-·-~** 

# ,_. -fd./ ':./' ; .

### ---,.

# ....**~'-.-** 

## ......- ·'1 -,.. _ ,. C_' •



## .. .. 

## '

# •**~.;.~-. ~~~~** **~:;iln1plad** ri'f: j**:h'l,)nll~** R.ea·jiriil: Ca

..J.dili';:.r.: "/eil:if;; It-.:::1.lIer samples to the: lab as soon as possillte after colJecUon to ensure that holdi.ng**o!,vg.S3~lo1!** lEo1:p;**;~im,~~ 'o\'~'=llla**  me.t. Please fill CDC out comp!e-tEIY'1[) 6')(peDite sample 

### log-In

.. '0

### ~ 

## ';1 i:

........

...... _ •. r'"MI.-nI

....... · f'I.1n

..a<O:1CU." Was.te Waler 

## ww**lJLju~** l Food f() Trip Blank TB Solids 5 Micro--b!clogy 

### Me rteld a.lail..'< FB 

# I Preservative

:0 

### • o. fi 

### Analysis Requesled Z c 

# .. "- Z J: 

## .... 

# " J: 

# ... Z 

# '" 02: 0 

### z VI m 

### :r 

## ....**~** 0 Z 0 0 0 0 0 

### 1\s- m 

## '" 

# .. :J: r- 

# '"**~.** 

# (0 

# tL 9- 

# ? 

# Q41)5

.,

/

:'i6:ei'

.. w.i

# ~e.¢**C;l~** 

# J-r./**D.~** Tirr&l Bi:(.SigrAIu'eo} 

### /1-1'7-0;; 

### itt;!**-1"~** Rilca::Viid 

# .7r

.......**~ L·~"-·~~;'5'"""** 

## ..**D~'** lir't3 B:r.(S\lfl.3t-Jra)



## - ...-"''''''?;-?<-'::''

.....**~~y** . f" \ 

## ..

## -. ..,_.- ,_.. 

### t)·7?;·

... ,: /"':)-{}**C~ R~j.,w**  D

..;e T:rr,., B'I.(SiGni!.lJre) Field Sampliny Notes: EQUIPMENT BLANKS AND FIELD BLMIKS ARE USED FDR INTERNAL LAB USE 0 N L YIN DT BILLABLEI. NOT REPOR1EO U NLES5 REQUE5TE D ElY CUSTDl.IER_

.

Fie.·.'.:D**Craa.~ed** D'/,MO Data:J.'3'o'J 5 L J> 

### :z



# ,**~** 

# , N <Sl <Sl CD**~** 

# "" m CJ**~** <Sl --.J 

### en .".

("") 

### r :l> H ;J:J -l 0 

### :z 

# "" C 

### :z H 0 H "D :l> 

### r :l> C -l 

### :::r: 0 ;J:J H -l 

### -<**~** 

### -n :l> X**~** 

## ::; N N W W W N .". CD

CD

### Microbac Laboratories, Inc. Atlshurgh Division 

## SAMPLE BOHLE & 

## PRESERVATION RECORD**,"~,:,** . 

# , ., ..,·H._l.l(2.i,...j-L!2_ v-,",--_

"').' f<.l)v SOIL:

___**~_**



### !

. T. MET. 

# ---1

Ptl**---~----~---~--~----+----+----+---~----I----4----~--~** 

## --1-**~---+** 

## ·1 1---' 

# I

I I

. I**L-~** .L.- I,

__ 'J! Ii**!'F~ r::u~~,er'**  ..ative tlaS b-p.en**ch~r.}.;** llle 11 limber and hott!e**t~rpa** will be entered into Um appropraile column. The'slatE=mentlPreserved al Lab"**9hou~d** be Roted ne>...i to the sa:np'c {hat

. '·P.;**~'.~** lie preserved. '**;·.H'·~~i·rrs**

..' '.1**~i·',;.·ornsl.S;:lTnple·** Uollle Slleel PRESt=RVATION CHECKED BY: OilTE**Cr~ated** By: :"·1I\D Or.la: 03.112J05 

### R,;v. '1 n
........llr-ct

.... nl ("'"

...fl'"",1 t:l"

.**n~r'I.,.~,;;11C:-{'\**

# ~**~**

# ~**~ ~**  

# o**~** 

## <:5**~**

# ~ H

### ~

### ~

# ~ H 

# " H -0 

# F'

# ~ H 

## ::;!**~** 

### -n 

# ::<**~ ~**  f')

# ~**~**

:-0**~** 

### co

# ~

## i I



# - 

# I JAN-21-2009(WED) 07:54 

# CLAIRTON MUNICIPAL AUTHORITY (FAX)4122333249 P.020/029

.' ,,"'



### ..... ,r ....**'.\~**

### ..

. 'I 

### "**~;\~,:-;.r7c:}da]c.~** 

## P_\ 15056-7::'-; 

## PlwDe: 724-772-0610 Fax: 724-772-:1686
SAMPLE SUBMISSION FOKM 

### for OUTSIDE TESTING



### Senc**R.esLllt~.** 

### "T:J 

# 11M!.!

# \w~a'\tl-D'I**~**...

## ~iGi:J~ac**!....~:-2'r::b:i-;:.s** -[ 00 IV'larshaiJ Drive Warrandala, ?A 15086 

### PllDne: 724-T72-061 

### 0 Fax: 724-T72-1686 

### Invoice To: 

### (if different from**abov~)**

____ SAME.

__________ _

SAMPLE IDEHTIFICATIOH COLLECTED'



# .

as 8- lu-lK 

# t.o-il"11'6 

# I I

- 

# I ..

### -



# I

.. 

# I 

# I

I I**P~linquj-shed** 3vo 

### Dale: 

## j!



# I I

I I 

# I Data Submillad:

# _-"L~,,--.;!;-'\ i;;;,Cj",1<1,,-i

____ _ 

### Su::"mined 9v:**c,n~/' '.,----,~-_~**  

## "LI--"--" Or':ler No**·'-"I--'"\-~:;-;~"** 

## t
... ",.... r 1
..... '1:::;;,:'17,.
.... .,'\,. "))"'\1;' J r 

# o I. P!sass C!re::k 

### if**Addition~1** 

### ?$sistancG is 

### Nt:l::!d2C:

_____ · __ Rush Analysis Required 

### Phone Results 

### -------Fax Results

MATP.lX 

# ! I ANALYsiS REQUESTED 

# 100 

# lJW-1-ClJ!MlJ.- V 

# hLk I 

# • 

# . 

# I
I I



# I I 

# i i

SPECIAL INSTRUCTIONS: 

# I LA!30RATORY USE 

### ONI,Y -. 

# I**~:f~eived8y** ___

## '.''--_~---'- I**:::"CL~_~** 

### . 

## f I IlmB!1 emp.: 

### I 

# I j**~onditiDn:** 

### . 

# II'

yustomer.l"o__. 

# J R .,**~l** .
, apOrT

## ~O.:**'_'''''_'~''''"''''''_"''''''''&_** f

Revision: 0

## JAN-21-2009(WED) 07:54 

# CLAIRTON MUNICIPAL AUTHORITY (FAX)4122333249 P.021/029 

# t§1#lI!Ii Laboratories LLC

a**mOl~ber** 

### ofThe GEL Group 

### ING PO Box 30712 eil"I""lon. SC 29411 2040 S'''"flC Road Charl

.. ton. 

## se 29407 P843.555.8171 F843.766.117B
January 09. 2009 Ms. Polly McConahy Microbac Labs 100 Marshall Drive Wr1Irendale, Penosylvania 

### 15086 Re;**W~ndale** • Non 

### DE? Reportable WOI'k Order: 221666
Dc.r Ms, McConahy; GEl. L.l)ol'atol'ie

.. 

### LLC (GEL) appreciates the opportunity to provide the enclosed an.lyticnl results for the samplc(s) we received on December 22.2008. This original dum report h"" been prepared and reviewed in accordance 

### with GEL's .standard operating**pro~durc5.** Our policy is to provide high qillllity,**pCI~onalized** analytical services to cmlbJe you to. meeryour analytic:tl needs on tilnO every time. We trust llmt you willllnd eVerything 

### in order and to your sotisf.ctioD. Ifyou have any queslions, plo.so do nor. hesit.te to c:tll me at (843) 556-8171. ext, 4512.

Enclosures

problem solved Sincerely,

# ~ Ann Skradski**Proj~ct M~magcr** 



### Page 1 of 

### 10 www.gal.com

## JAN-21-2009(WED) 07:54 

# CLAIRTON MUNICIPAL AUTHORITY (FAX)4122333249

GEL LABORATORIES LLC 2040 

### Savage R03d CharleSlon SC 29407

- (843) 556-6171

- www.gel.com 

## Certificate of Analysis Report for MILA001 M:icrobac 

### Labs (STND) Client SDG: 221666 GEL Work Order: 221666
The Qu3liriers hI**tbi~** 

### report are defined n.< 

### e"uows: • A quality conlrol analyte recovery is outside of <pecificd acceptance criteria >i:'* 

### Analyte is a surrogate compound U Analyte was analyzed for. but not detecred above the MDL. MDA. orLOD., Whorethe analytical method has been pcrformed under NELAP certification. the analysis has mot all ofthe rcquircrncnL< ofthe NELAe standard UIlIe.

.. qualified on tho Certificatc ofAnalysis. 

## P.022/029

The designa.tion ND, 

### ifprcsenr .. appe<lI"s in the rc;sulr. column when the analyr:e**conC~l.rnlion** 

### is nor. der.ecr.ed above

. the delection limit. .



### This data report bas br:.en prepared and reviewed in nccorrhmcc with GEL LaborJtories 

### LtC smndard OpCf"dting procedures_ PI"as" 

### di«"t any questions 10 your ProjectM:magcr. Ann Skradsl::L

# ~------------**Review~dby**



### Page 2 of 10**JAN-21~2008(WED)** 

## 07:55 

# CLAIRTON MUNICIPAL AUTHORITY (FAX)4122333248 P.027/028

.GEL LABORATORIES LLC 2040 Savage Road Charleslon SC 29407';' (943) 556-8171

- www.gel.eom



## Certificate ofAnalysis

Company: Microb3c Labs Address: 100 M=hall Drive W""tClld.,\e, Pcnnsylv.nill 15086**Cont.o~** Ms. Polly MCCon.by Project: Wotrrcodtllc - Non DEP Report:.lb1c
Client Samplc ill: SampleLD: 

### Matri)" Collect Date: Rcccivo Date: 

### Colloctor: 0812-1478 

### 221666001 WnSTeWatl:r ·19-DEC-08 

### 12:00 22-DEC-08 

### Client QmdiLicr Result Uncert.:linlY DL Rad Gas Flow Proportiooa1 Ct"tUDting GF"PC. GrossAlB. liquid 'i1s**R~c(ttved"** Alpha U 'u ND 4230
The rullnwing AnalytieDJ Methods were performed Method DI$crlptlon 1 EPA 900.0 +/-155**~/-216** 254 215



### Page 3 of 10 RL Rcport Date: Januury 9. 2009



### ProiecT' MlLAOa104 Client ill: 

### Mil-AOOI

UJlilG

pCilL pCi/L lIF A.Daly,W.W Time Bateh Method

oXl'3 01/05109 21>6 828558 1

Amllytol Comments

## JNh21-2009(ifiJED) 07:55 

# CLAIRTON MUNICIPAL AUTHORITY (FAX)4122333249 

## P.028/029

GEL LABORATORIES LLC 2040 Savage Road CharlesTon. SC 29407
- (B43) 556-B171
- www.gel.com

Contact: Micmbil:c Lal)" 100 Mursbull Driyc**Warrendal~** Pl.!nn!f)'Jvania Ms. Polly McConahy WurknrdCl"! 221666 

## QCSummary

Parmn9lne

. __ .:.-'**J:N,!!O~M~**__**-2S'O!wn~p,!!I,,~--.\Ql!"U!!nl'!.....**__ Q!;

...,.. tlnits R'PD% oKlid Gm; Flow Bmch 8:!.8658 QCl:!01747181 221466UOl DUP Alpha.
Bota QC12017471R4 LCS Alph.

BelLI.. QCI20l747180 MB U

114
395 

### 0.977 U ·139 pCiIL 0 ,,·/·1.58 +1-1.29

21.7 21.9 pCi/L

...

/-4.QS +1·3.98 

### 110 pCi/L

..

1·11.6

354 pCiIL +1-14.9 RCDOrt Date: Janu03ry 9. ZllU9 l)age 1 of 2

REe%**·:R~~~L~.ls~.**__ Dat.e Time

. N/A DXF3 Ollllo/U921,50 (0% -100%)

97 (75%-1"5%) 01l06/o92U6
90 (15%·115%)
Alpha 0.552 pCiIL U 01l0fil0921,5U +1-1.26 I' 

### u 1.00 pCi/L ",·f·2.39 QC120174718:! 221466001 MS Alpha**l2~** U 0.977 271 pCiIL 119 (75%·125%) 01l06/0911:S0

...1-I.5R
...1-25.7 Beta 790 21.7 SS9 pCiIL 110 (75%-125%)**;~-4.05** -t/-'J.9.S QCI2017471B3 221466001 MSI) Alpha 

### 228 U 0.977 261 pCi/L 4 I1S (0%·20%) 01l06/0921:26

..

/·I.5R +/
..28.8 BeleL 

### 790 21.7 8.59 pCiIL 3 lD6 (0%·20%) ",/-4,05**.,.1-3~.9** NOles: 11,c QuaJiticO! in thili report ortl de:fined 3S follows: Analyt.e**h~** a surrog'l.llc compound 

### <**R~uh i~**  h::ss Us":l.n**v~lIe** reponed
> Result is f..rc..1tCf [han vahle**rep~rtecl** A Ttl.: TIC iN U**~uspcCled** :Udal-condensation product B FOr**Gell~** Chelllistry nnd Organic analysilj Lhe LurscL unulYlC WtlS dc1.t:C1.ed In the associafed blank. BD Results arc either below lhe

### MOe Or lr'.J.c;errcco'Ycry is low C AT1Ollyt(; hou; been confirmed by GC/MS**ruI~ysls** D**RC'~ulr-",.ate** reponed from udiluted aliquot of the s.1mpJc F ERtimalcd Value I-l Arut1ytical holding time was c:::t;:l:eded



### Page 5 of 10

### JAN-21~2008(WED) 

## 07:55 

# CLAIRTON MUNICIPAL AUTHORITY (FAX)4122333248

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407
- (843)556-8171 "www.gcl.com 

# QCSummary Womorder: Pannname

.._____"

____ --,N",O",M=_ J Vwuc is esrimated M M if .bo •• MOC and less ,Jmn ll.D M MaLtix**Rdn~d** Fililurc N/A RPD 

### or %Rcc[)vc:ry limits. do nor apply. 

### ND NJ R U ill 

### x y Analyle com::cnt.roLion is nOl· dl!fe.Clcd above the detection limil Consult**ew.~** Nan'::Itivc:, 'Data Sunumuy package. or Project MMilg!;.f cunct::rning mil>**'-Iualili~r** Sample fCljults o.rc: rejected**Anul:yl~** was an:l1yzcd for. but**nt~l** dc,ectcd ahove the MDt., MDA. or LOI). Gamma Spc

..t.roscopy-UnceIUl.in idcntitlclllion Consult Case NaJT;1Dvc., Datil SummuIy pack:i1Sc. Dr Project**M;ul!l~!:r** concernIng this qUi11itIc;r QC Somplcs were noL spiked wll.h !his compound REC%

h RPD ofs.mlple and dupllcal.c ev.ulUatt!ld uliiny -I-/

...RL. Cr.mccnlr.iltious arc .oXthe RI

.... Quolifie:t Nor Applicable for RaLiiochemisrry. Pn:parnr.ion tlr prcserv:n.i(ln holding time**~us** exceeded
indicares Llml.!:ipike recovery lill).j.rs do not apply wl1l;n Rample concenlrntiou exceed" lipikc CODe. by a rHetot of4 or more. 

## P.029/028**~** Relati'\lc Percent DiITerellCC (RPD) obtained from ilic s::unplQ duplicate (1)tJP) is cva1u:nc:d ngainst the**~cceplance** criterill when the sample is gJ.'LAuer thnn five limes (5X) the canrmcr required detcl;(.;on limit (RL). In**Cill:i~** wbere ciLhcr!he s.1il1ple or duplicate value is less thun 5X lhe iUJt a oontrollirnir. (If4-/

.. 11le RL is**lll'~d l~**  e\laluarc t.he DUP J.'esult•

... TnLiitAltes**rh~t** tl Qufiliry Control parameter ",lUI nOl wirhin**~pecifications.** ForPS. ?SD, llnd SD.ll

.. T results. tbe: vwucs listed arc the mC:3surcd amounts, !lorfinn\ concc:mr;n.iom;,. 

### where [.he an:liytiC::ll mJ:thod hilS been performed under NEJ

...

### AP certific.d.;on, 

### the ana!YS1S has l1ll:t a.ll 

### ofrhe re(l"ir.mellts ofLb. NELAC su.ndard unIoss qualified on I\'" QC SUIDlllary_



### Page 6 of 10

## JAN-21 -2009**(I~ED)** 

## 07: 54 

# CLAIRTON MUNICIPAL AUTHORITY (FAX)4122333249



# MICROBAC L.u30RATORI.l:::S, INC. 100 Ma.rshallDrive 

## Warrendale, FA 15086-7554 Phone: 724-772-0610 Fax: 724-772-1686 

## P.023/029

SAMPLE SUBMISSION FORM for 

### OUrsIDE; TESTING Page

__ of

__ _
Send Results To 

## COmpiiny: Address:

# g~~~ar~~ 100 Marnhall Drive Warrendale, 

### PA 15086 Phone: 724-772-0610 Fax: 724-772-1686 Invoic" To: (if different from 

### above)



### _______**.SN~E** 

### __**~**

### ________ _

.. SAMPLE IDENTIFICATION COLLECTED



# .cg Jd.- \lflK !!:tll"l

# ~

Re/inquishe;d By:

. 

# Ciwou:J-.-- 

# .I SPECIAL INSTRUCTIONS:

.



## ==. ;: =

FDrm Cowo] l'"D.: 0202051630 Date Submitted: 

# (8.\I'lf'i

. Submitted Bv:**~** 

## *--**PurchOl~e** Order 

### No.: 

# W**.UIil(~** 

## .... 

# ry
. Please CheCK ifAdditional Assistance is Needed:

______Rush Analysis Required

______ ,Phone Results



### ______ ,Fax Results

. MATRIX ANALYSIS REQUESTED 

# 1;)0

# ~ nV.dtL

# ~ 

# Ada:

.

Rovjsion: 0 !:ia.t: : 020205 I I



### ,

## JAN-21-2009(WED) 07:54 

# CLAIRTON MUNICIPAL AUTHORITY (FAX)4122333249



# },HCROBAC 

# LABORlHOPJES, INC. 100 Marshall Drive Warrendale; PA 15086-7554 

## Phone: 724-772-0610 Fax:**724-772~1686** 

## P.024J029

SAMPLE SUBMISSION FORM 

### for OUTSIDE TESTING 

### Page.

___ ,of

__
Send Results 

### To 

### Company: Address:

# M~r~datl~~s 1DO**Marsh~1I** Drive· Warrendale, PA 15086 

### Phone: .724-772-0610 Fax: 724-772-16B6 

### Invoice To: (if 

### different from OIbove)

______**SAME,_~**_____________ _

SAMPLE IDENTIFICATION COLLECTED 

### ()'9. 

## 1:1- 

## I

# t..\

# 40

. .

## 1a..II{r~



# ..

Relinquished By: Date:
SPECIAL INSTRUCTIONS: Date Submitted: 

### _-IIr<:lir<./!.t.:I'l1.llu[t.,-

___ _ Submitted By:**c..~** 

### Purchase Order No.:

### t'15~&-. 

## - 

# .:uII 

## h

-- Please 

### Check 

### ifAdditional Assistanoe is 

### Needed:

_______ :Rush Analysis Required



### _______ Phone Results



### ____ -'--_Fax Results

MATRIX ANALYSIS REQUESTED 

# Ilkl',",**~(lOMI~** 

# t- 

# RlJtc
I



### ,



# -----,------------,-'----,--....;...-- 

# I LABORATORY

## U~**ON~**

# ~;~:i~ed)Y:**J(i'o"6J~:**

# I~m"'~' 

# , ,Condition: , '



# , . -.!!**,Custome~** 

### No.: Report No.: 

# L

form Convoll'o.: 0202051630**R~vision:** 

### 0 Dart: 02G2GS

## JAN-21-2009(WED) 07:55 

# CLAIRTON MUNICIPAL AUTHORITY (FP,X)4122333249 P.025/029



# . m3!

# I Laboratories LlC SAMPLE RECEIPl' & 

## REVIEWFORM 

# (t):c.r

.....



# h..r . 

## ,,",,,,,,**~~** 

# lLr. (" 

# "'1,,- IBy: 

## R('1S !Dsle:

## I~ 

# 1-.:>-\1

....'1:



### Hazard

### Wormation**~** 

## :@**.~. 'x2~rca**  I 

### not matI:ed • contact 

# .. ...**'~>r~"**•. :! 

## ,J, , CotQIlS 

# ,".**~** 

# nor III

### bvRSo1 ,/ Qr. h ('r-.r"," .,. ,marked



### .PcBs? f 

### lasaDOT: / 

### UN//:



# ..

# , ;sO;i1 

# , . 

### SampleReeeipt Cdteria 

# ;: II**~** Crunn>cntslQuaIir",,,, (Required 

### forNon-Conrormingf!enzS)**'~L'.** 

## _,. coul:liners =civet!intactand 

### [; 

# """".ro'" 1**~'** 

## ./ damaged enntaillCl"**~_1>i1ur** o!b:< (d=ribo)

''''**requirin~** coldpresClVation 

# / blue leo

### dryJ~**~:** .IborCo=ibc) icc ""'" 

# :2 Iwithin 0 S 6 deg. C? 

## IS'"

3 

### IChain of

### CU!llOdy documents included

lwith shipment? 

## ICin:lo. 

# .--
4 containers intactand scalcd7**~**

# """'""""**bl:iIJi'~ o[bcr(~~)** 

, .... 0<l0<I

..... 

# 1/ 5 atproperpm 

# ... .. ,
{; VOA vialsftee ofbeads pace (defmed os 

## ./ <: 6mm bubble)?

. 

## / ,.. . CI. 

### 7 A**~** 1>,,",,", contain=present? 

# !8 ='ved within bolclln& 

### titne? 

### I,". .1. 

### ID's on COC IJl3.Il:b

# ro'. on Is

# """".8>·,

. 

# ,.-
.9 1 

## "",u"", IOate &.limcon COC mall:b <lao:: & time 

# ISIullp"**~**

# .ffoc'''''' 110 Ion bottlcs7

• 0 

### containers received march**.~**. • "",=Cd: ,11 

### on COC? COCfom> is properlysigned in 

# / III sectiOnS?

.

# ~'.**~b** 

# (,5" ')..51> 

# 7Yo/A

.

. r-ag'"**~** 

### or 1

## Q DoO:: 

### \'7./.,,-ll

## I**~02** 

### revieW: :Initials

## ~1>'\.." PM(orPMA)

# JAN-21-2008(IfIJED) 07:55 CLAIRTON MUNICIPAL AUTHORITY (FAX)4122333248

Lid or**curr~nl** 

### GEL Certifications ,... 

### of

### (19 Jonuary 

### 20&9 Stale

CLlA**~.ofNavy ~da-NELAP**  O.t)rgi. L,eorg'. DW

Haw.ii ISO 17U25

I<labo

,NELAP Inobn. 

# M",a,

- Nl;!LAP .-NELAP

Nov.d. NewJ.n<.y

- NELAP 

### New MeX,co**~'York-** NJ;LAP North NOrtll ( ,DW

South 

### 'exas

- NELAP 

# r-'u"",

..s"'.Dcpr, 

# of Jtail-NELAP Virginia



### Page 10 of 10 01151CA OEL PH-<l169 NFESC413

.WO::.15.1

E87156 ES7156 .AI" 967 N/A 2567.01

_2lJUU2" C-SC-OI

90129 03046



### 270**Nl-~'-Ul"** SCOO0l2 SCOUZ Fl. 715.§,

. 11501 233 

### 4$709 9904 1012000lI10IZOOU2 TN 02934

GEL VTS?156

_00151 CIMI 

## P,026/028

## Microbac Laboratories, Inc. Page I 

# of I 100 MARSfIALL DRIVE WARRENDALE, PA 15086 (724) 772-0610 FAX (724) 772-1686 TOM ZlERENBERG, MANAGING DIRECTOR http://www.microbac.com State Laboratory Certification Nmnbers: PADEP: 02-257, 

### NC: 42703,WVDEP: 215,9951 CM KY: 90136 CHbMlo"lKY

. MlCKUHlULUliY

. l'UUJJ OiAFbTY

.. CUNOiUMbK PKUJJUCrOi WATbK· 

### AJ:K. WASTbS· l'UUD· PHARMACbU'11CALS· NUTKACbUTICALS

CLAIRTON :MUNICIPAL AUTHORITY 

### MR. PATRICK CANA VAN I NORTH STATE STREET CLAIRTON, PA 15025

Permit 

### No.: Cust P.O.: 

### CERTIFICATE OF ANALYSIS

SUBJECT: Wastewater Samples for Radiological Analysis Date Reported: Date Received: Order Number: Invoice No.: Cust 

### #: Sample Date: Sample Time: Sampler/Temp: lII4/2009 121912008 0812-00540 38430 CI23 12/8/2008 9:30

TEST METHOD RESULT UNITS DATE TECH 001 CNk3 Pitwater Collected 

### 12/8/08@
Gross Alpha Gross Beta

SubmlttedBy: EPA 900.0 EPA 900.0

Managing Direct·o See Attached See Attached pOlL 01/03/09 pCi(L 01/03/09

The data and information on thiS, and other accompanying documents, represent only the sample(s) analyzed and is rendered upon condition that it is not to be reproduced wholly or in part for advertising or other Pl.Il'pOSeS without approval from the laboratory. U5DA-EPA-NIOSH Testing Food Sanitation Consulting Ch'emical and Microbiological Analyses and Research 

### MEMBER 

# '4{111*** ***

# [i1§Q ILaboratories LLC

a member of The GEL Group 

### INC PO 80x 30712 Charleston, SC 29417 2040 Savage Road Charleston, SC 29407 P843.556.8171 F843.766.1178
Januery 12. 2009
Ms. Polly McConahy Microbac Labs 100 Marshall Drive Warrendale, Pennsylvania 15086
Re: Warrendale

- Non DEP Reportable Work Order: 2210II Dear Ms. McConahy: GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on December 11, 2008. This original data report has been prepared and reviewed in ac.cordance with GEL's standard operating procedures. Our policy is to provide high quality, personalized analytical services to enable yOll to. meet your analytical needs on time every time. ,Ve trust that you will fInd everything in order and to your satisfaction. Ifyou have any guestions, please do not hesitate to call me at (843) 556-8171, ext. 4512.
Sincerely,

# ~ Ann Skradski Project Manager

Enclosures



## Page 1 of 9 problem solved www.geLcom

## GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407
- (843) 556-8171
- www.gel.com 

## Certificate of Analysis Report for

. MILA001 Microbac Labs (STND) Client SDG: 221011 GEL Work Order: 221011
The Qualifiers in this report are defined as follows: 

## " A quality control analyte recovery is outside of specified acceptance criteria 

### ** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above th"e 1vi[)L, MDA, orLOD. "\Vbere the analytical method has been performed under NELAP certification, the analysis has met all ofthe requirements ofthe NELAC standard unJess qualified on the Certificate ofAnalysis. The designation 1\11), ifpresent, appears in the result column when the analyte concentration is not detected above the detection limit. This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures. Please wect any questions to your Project Manager, Ann Skradski.

Reviewedby



### Page 2 of9

# GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407

- (843) 556-8171

- www.gel.com



## Certificate ofAnalysis

Company: Microbac Labs Address: 100 Marshall Drive Warrendale, Pennsylvania 15086 Contact: Ms. PollyMcConahy Project Warrendale

- Non DEP Reportable

Client Sample ID: Sample ID: 

### Matrix: Collect Date: 

### Recejve Date: Collector: 0812540 221011001 Waste Water OS-DEC-08 12:00 lJ-DEC-08 Client Parameter Qualifier Result Uncertainty 

### DL Rad Gas Flow Proportional Counting GFPC, GrossAlB, l.iquid ''As Received" Alpha Beta 33.2 140 The following Analytical Methods were performed Method Description EPA 900.0 +/-9.67 +/-11.8 7.13 8.94



### Page 3 of9 RL

5.00 5.00 Report Date: January 12, 2009

Proiect: MlLAOOI04 Client ID: MlLAOO 1

Units

pCiIL pCiIL DF AnalystDate Time Batch Method

DXF3 01/03/09 2135 825351

Analyst Comments

## GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407

- (843) 556-8171

- www.gel.com

Contact: "rorkorder: Parmname Rad Gas Flow M1crobac Labs 100 Marshall Drive Warrendale, Pennsylvania Ms. Polly McConahy 221011 

### NOM

Batch 825351 QC1201739437 220707001 DUP Alpha
Beta QCJ201739440 LCS Alpha 57.0
Bela 198 QC1201739436 MB Alpha
Beta QC1201739438 22070700] MS Alpha 114 Beta 395 QC1201739439 220707001 MSD Alpha 114
Beta 395

N:Jtes: The Qualifiers in this report are defined as follows:



## ** Analyte is a surrogate compound
< Result is less than value :reported
> Result is greaterthan value reported A The TIC is a suspected aldol-condensation product 

# QCSummary**Sam~le** Qua] QC Units RPD%

10.4 11.8 pCilL 13 +/-3.09 +/-2.96 17.8 12.5 pCilL 35 

### * +/-2.68 +/-2.14
57.0 pCifL +/-6.14 195 pCilL +/-7.67 U 0.313 pCifL +/-0.529 U 0.996 pCifL +/-0.993 lOA 92.1 pCifL +/-3.09 +/-9.31 17.8 421 pCifL +/-2.68 +/-11.6
10.4 120 pCifL 26 * +/-3.09 +/-11.4 17.8 409 pCifL 3 +/-2.68 +/-11.8

B For General Chemistry and Organic analysis the target analyte was detected inthe associated blank. 

### BD Results are eitherbelow the MDC ortracerrecovery is low C Analyte has been confirmed by GCfMS analysis 

### D Results are reported from a diluted aliquot ofthe sample F Estimated Value H Analytical holding time was exceeded



### Page 4 of 9 ReDort Date: January 12, 2009 Page lof 2

REC% Range AnI,!

(0%

- 100%) D)(F3

(0%

- 20%)

100 (75%-12S%)
99 (75%-125%)

72* (75%-125%)
102 (75%-125%)

96 (0%-20%)
99 (0%-20%) Date Time

01103/0921:34

01106/09 1859

01/03/0921:34

01103/0921:34

01103/0921:34

## GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407
- (843) 556-8171
- www.gei.com


## QCSummary Workorder: 221011 Page 2 of 2 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time J Value is estimated M M ifabove MDe and less than LLD M Matrix Related Failure NI

A RPD or %Recovery limits do not apply. ND Analyte concentration is not detected above the detection limit NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier R SampJe results are rejected U Analyte was analyzed for, but Dot.detected above the MDL, MDA, or LOD. til Gamma Spectroscopy--Unccrtain identification X Consult Case Narrative, Data Sununary package, or Project Manager concerning this qualifier Y QC SampJes were not spiked with this compound RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. b Preparation or preservation bolcling time was exceeded

N/

A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of4 or more. "Tfle Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sampleis greater than**~** times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5XtheRL, a control limit of+/- the KL is used to evaluate the DUP result. *" Indicates that a Quallty Control parameter was not within specifications. For PS, PSD, and Snll..T results, the values listed are the measured amounts, not frnal concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all ofthe requirements ofthe NELAC standard unless qualified on the QC Su=ary.



### Page 5 of 9

### r---------

GEL Laboratories LLC Form GEL-NCR Rev. 06/05

Mo.Day Yr. OB-JAN-09 Instrument Type: GFPC Batch )0: 825351 COMPANY

- WIDE NONCONFORMANCE REPORT
Division: Quality Criteria: Radiochemistry Specifications Test / Method: Matrix Type: EPA 900.0 Liquid Sample Numbers: See Below NCR Report No.: 646092 Revision No.:

Type: Process Client Code: MILA, NFSR, RHOD

Potentially affected work order(s)(SOG): 220706(OB-CAH-1 09),220707(08-CAH-1 07),220709(08-CAH-1 08),221 011 ,221099 Application Issues: Failed Recovery for MS/PS Specification and Requirements 

# I NRG Disposition: Nonconformance Description:

1. The matrix spike 1201739438 did not meet the alpha recovery 1. Reporting results. requirement. The matrix spike duplicate 1201739439 did meet the recovery requirement. The matrix spike and the matrix spike duplicate have a relative error ration of 1.7582.

Originator'S Name: Data Validator/Group Leader: Nat Long OB-JAN-09 Heather McCarty 12-JAN-09 Quality Review:

Director:



### Page 6 of 9--rc------ --- 

# /

MICROBAC 

# LABORATORIES, INC. 100 Marshall Drive Warrendale, PA 15086-7554**~~IDII** 

## Phone: 724-772-0610 Fax: 724-772-1686 SAMPLE SUBMISSION FORM for OUTSIDE TESTING Page.

__ ---'of,

__ _ Send Results To Company: Address: 

# Poli1**flWb~** Microbac Laboratories 100 Marshall Drive Warrendale, PA 

### 15086 Phone: 724-772-0610 Fax: 724-772-1686 Invoice To: (if different from above)

_______SAME.

________________ ___

SAMPLE IDENTIFICATION COLLECTED 

# (fA!d- 

# 540**\~\~k** Date Submitted: 

# loil 11 

# r Submitted By: 

# DtYiL Purchase Order No.: 

# cof"i'»)i.A-eaPlease Check if Additional Assistance is Needed:

_______Rush Analysis Required

_______ .Phone Results

_______ F,ax Results

MATRIX ANALYSIS REQUESTED 

# WW r

# Jh fiJJ).- ()

# 0 d J. 

# 'F.It! J 

# 11 '>



### -

Relinquished

### By: Date:
SPECIAL INSTRUCTIONS:

II

.

Fonn Control No.: 0202051630 LABORATORY

### ~**ONL~** Received By:

### ~ 

# fl'ltY'-- Date: 

## I**~-I** 

## -0 TimefTemp.: Condition: Customer No.: Report No.:

Revision: 0 Dale: 020205

## ~~Q I 

## , d(IMlla)

# mag Laboratories LLC 

## SAMPLE RECEIPI' & REVIEWFORM 

# -rn ;(I/l 

### 0

## hrxl' 7**~,.** c:uc/'**cOrd.~** - 

# 2Z1(fll' By: 

# ?4.f\ fi.l. 

# Iz·I)-O'(**~** 

### t

# r~:' -Dun,.

# >~:::;**~** 01 • ' DOl marl:ed •contact 

### Hazard Information ;:.. 

# Z

,marked as. 

# " ,Counts' , 

# r:z () (ij;>(Y\ ,IIor

### III by RSO? 

# v: ;marked 

# :pCsS? V lasaOOT 

### ,/ IClass UN#:

,as! 

### ,Soil? ,/ SampleReceipt Criteria 

# :! ;2' Z Comments/Qualifiers (RequiredforNoo-Conforming Item<)

1 containers JeCeived intact and 

# J £bm3ged CCIi:lbiDer**~** 

# ,.**~** COJll.ainer Otbr::r (de:$cribe)
requiringcold preservation dryic:e

# ~1y~,(O=rireJ ice bog> '2 

# j blue ice 

### IWithin 0 :; 6 deg. C?

,
3 !Chain ofcustody documents included



### 'with shipment? 

# j ICUclo Applical>k: ' 

# ,.,..,_on

4**~** damaged cootaioec

.. 1caDng=- alba(dc,aibe) containers intact and sealed?


# - IJ 5 requiring chemical ". p<opex pH? added,.LotOo
VOA vials free ofheadsP= I •• 

### 6 

### < 6rombubble)? ' 

# I.J

7 Are EOCOi"e containers present? 

# V Id'.od

# tests,_

'8 leceived within holdiDg time? 

# ,-

.**~'.** on CDC match ID', on , . '9 

## 1"'''''-><**~** 

### 110jDare & rime on CDC match 

### date -Ik time 

# I 

# Nof'htd1Cm.v f,:)f\ \f)f\1(J\ VI 

### QA 

### Ion hottles? , 

## 'v, , match 

# ' I (lflf'tf(f

# ~fl0 

## 1 

# Pet-O J1f{J ,J 

## III indicated on

## cae?

112 ICue

### ~ is p<opedy

### 'i~eiI in :;ecbons?

# r~6{ I 

# '](Y(i5'

# Z?:15 

# zwqg

I**~** 

## (-'age 8 

## ot!i Dare 

### / ..;)-//1 

### 10";<
, y, orP.MA) review: Initials**~** E I PM(List of current GEL Certifications as of 12 January 2009 State 

# r Arizona**~** 88-0651 CLIA

i- 01151CA GEl pj:i: 1"i;9 Dept. ofNavy NFESC413 EPA Region 5 Florida

- NELAP 

### E87i56 Georgia E87156 (Fj GeorgiaDW 967

Hawaii 

### N7A ISO 17025 2567.01

Idaho SCOOO12 Ilhnois

- NELAP 200029 Indiana -OiL-VJ Kansas

- NELAP 90129 -NELAP 

### 03046 270
Nevada New Jersey

- NELAP SC002 New Mexico 

## m APE87156 New York

- NELAP 

### J.15Ol North ' 

### 233 North ,DW 45769 9904 ·NELAP South 

### 7I'

T, TN 02934 Texas

- NELAP T U.S. Dept. of S-52597 .AP 

### GEL VT871S{ Virginia 00151 C1641



### Page 9 of9