. ..

**~·** .. 2540-PM-BWM0347 Rev. 1/2011 **,~pennsylvania** • DEPAA1MENT OF EIMRONMBITAL PROTECTION COMMONWEALTH OF PENNSYLVANIA DEPARTMENT OF ENVIRONMENTAL PROTECTION BUREAU OF WASTE MANAGEMENT FORM26R CHEMICAL ANALYSIS OF RESIDUAL WASTE ANNUAL REPORT BY THE GENERA TOR This must be fully and accurately completed.

**~~ ~=:**  typed or legibly printed In the spaces provided. If additional space is necessary, Identify each attached sheet as Fonn 26R, reference the Item number and identify the date prepared. The date on attached sheets needs to match the date noted below. General Reference 287.54 Date Prepared/Revi8ed 219/11 c. Phytslcal Appearance Company County Indiana Address Une 2 Number of Solid or Uquid Phases of Separation

Ext No Describe each phase of separatlon

• .=s.:=----------------1 - 1 -2540.PM-BWM0347 Rev.1/2011 c. a. b. c. d . b. Address Une 1 Address Une 1 Address City State ZIP Municipality Facility Title Name Address Une 1 Address Une 1 Address City State ZIP Municipality Title Phone

Indiana (check one) Oton (check one) -2-2540-PM-BWM0347 Rev.112011 I certify, under penalty of law, that

I have personally examined and am familiar wi1h the Information submitted In this Annual Report and all attached documents and that based upon my Inquiry of those Individuals Immediately responsible for obtaining the Information,

I verify that the submitted Information Is true, accurate and complete to the best of my knowledge.

I understand that the submission of false Information herein Is made subject to the penalties of 18 Pa. C.S. §4904, relating to unsworn falsification to authorities, which lnctude fine and Imprisonment Check the following, If applicable: D

I certify the Information required In Section B-1, General Properties was supplied to the Department for the year _and has not changed. Form Submitted:
D Fonn 26R D Other (specify) Date Submitted: D

I certify the Information required In Section B-2, Chemical Analysis was supplied to the Department for the year _and has not changed. Form Submitted:
D Form26R D other (specify) Date Submitted: D

I certify the Information required In Section B-3, Process Description and Schematic, was supplied to the Department for the year_ and has not changed. Form Submitted:
D Fonn 26R D Other (specify) Date Submitted: Name of Respo_pslble Official

Date 2-28-11 -3-February 9, 2011 Form 26R: Section B 1 e GENERATOR KNOWLEDGE All Form 26R Waste Forms have been compiled, and Mure testing has been scheduled, to obtain samples of each waste stream on a PAD by PAD basis. Sample analyses will be conducted every 5 years for each waste stream unless the process that generates any particular waste stream is substantially altered. Attached analytical results for this waste stream have been obtained from a similar waste stream producing waste from the same geologic formation as this 26R Report. Additionally, the mud mixtures, chemical formulations and drilling process utilized at this well PAD are substantially the same as those utilized at the well where the attached waste analyticals were generated.February 8, 2011 Form 26R: Section B2b WASTE SAMPLING METHODS All samples were obtained as grab type samples with a composite function which was maximized but sometimes limited by prevailing safety, site specific rational and/or environmental concerns.

- Brine fluids are composited within the storage production tank or tank battery at each well site where gas production
is occurring. Each automatic or manual ejection of formation fluids is deposited into the tank(s) and added to the previously ejected and stored quantity. Tanks are emptied into tank trucks for disposal at various PaDEP permitted waste disposal facilities on different schedules determined by individual well characteristics. Grab samples of the com posited fluids were obtained at the represented well pads directly from the storage tank drain ports. All drain ports had small "built in" containment and storage "buckets" capable of retaining small amounts of lost fluids. Samples were obtained with bottle sets prepared at the laboratory which contained appropriate preservatives, as necessary, depending on the specific test run requested. All chain of custody and handling/holding time requirements were met. In some cases, a larger sample was broken into appropriate sampling containers and smaller aliquot portions at the laboratory. Flowback samples were composited to the extent possible during the flowback process primarily during times where safety issues did not override sample collection requirements. Generally,
a larger composite sample was broken into appropriate sampling containers and smaller aliquot portions at the laboratory or on the well location upon completion of the composite sampling process. Samples were distributed into bottle sets prepared at the laboratory which contained appropriate preservatives, as necessary, depending on the specific test run requested. All chain of custody and handling/holding time requirements were met. Drill cuttings were composite sampled during the drilling process at various times and combined into a composite sample for analyses at the laboratory. On several wells, cuttings from the vertical portion of the well bore were segregated from cuttings from the target Marcellus Formation and separate testing was completed on both sample composites.
In some earlier cases during the utilization of open pits, composite samples were obtained from inactive drill pits. Safety concerns usually limited the randomness of the composite sample and composite grid sample positions were varied to the extent possible. Pit water (drill fluid) is currently discharged to closed containment and is re-conditioned and reused from well to well.i·February9,2011Form26R:Section83aWASTEGENERATIONPROCESSPitWater"DrillFluids"Remnantdrillfluidsaregeneratedinthewellboreduringthepenetrationofthedrillstemasitinterceptsbothgroundwaterandformationfluids.Thesefluidsarebroughttothesurfacealongwiththedrillcuttings,piecesoftheinterceptedrockstrata,bythereturnflowsystemofthedrillingprocess.Drillcuttingsanddrillfluidsareisolatedintoseparatewastestreams.Cuttingsaremixedwithsawdusttoabsorbremnantfluidandloadedoutfordisposalatalandfill.Fluidsarecurrentlystoredinclosedcontainerstobeprocessedforreuse.Flowback:"FracingFluid"Flowbackisproducedfromallfluidsthatflowbacktosurfaceduringthe"hydrofracing"processwhichoccursunderpressureandresultsinthesettingofapropantwithintheformationfractures.ProductionFluid"Brine"Duringtheproductionofnaturalgas,formationpressuresbringremnantfracfluids,duringtheinitialproductionphase,andformationfluidstothesurfacealongwithproducedgas.WellI.D.# (various) WellI.· D.#.(various) '\/*

**~** -)V,- **~~~** /1' COUNTYA I\ I \ / WellI.D.# (various) \ I:::b/ \ I /II' \ I / \ I // \I // . \I/ WellI.D.# (various) \I//

-COUNTYB '-\/ / \I/ -0.-/' /**~**...,...-_ . u"I **of!~....\..~;~** Mobile TankTruck 'fr-oc\h.-\ 10"Ocu

**1\\i..~-\ \OA~S** :!(USbrine('TYP.) Note: . Process producing waste:Gaswell produced fluids (brines)aretypically produced·in conjuction withnaturalgas.Thesefluids arebroughttothesurface utilizing either mechanical orphysicallift procedures.
-----Landfill or**Tru.J~v.+** 'P\Wlt.

()**~**UJ:I:()CJ)z0**~ ~** 00..CJ)z**~**1-**~II**If. **~~~-**j...

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giI ilGEOCHEMICAL TESTING Environmental and Energy Analysis Wednesday, February 23, 2011 RICK BONAZZA RESOURCE MANAGEMENT SERVICES 65 FENTON ROAD INDIANA, PA 15701 RE: 26R Analysis Dear RICK BONAZZA:
Order No.: 01101912

. Geochemical Testing received

I sample(s) on 1/28/2011 for the analyses presented in the following report. There were no problems with the analyses and all QC data met NELAC, EPA, and laboratory specifications except where noted in the Case Narrative or Laboratory Results. If you have any questions regarding these tests results, please feel free to call. Sincerely, Timothy W. Bergstresser Director of Technical Services

.. ,..,
2005 N Center A.ve Somerset PA 15501 814/443-1671 814/445-6666 FAX: 814/445-6729Geochemical Testin2 CLIENT: Project: Lab Order: RESOURCE MANAGEMENT SERVICES 26R Analysis Gll0l9l2

Date: 23-Feb-1
I CASE NARRATIVE No problems were encountered during analysis of this workorder, except if noted in this report. The ethylene gycol analysis was subcontracted
to Free Col Labs. A copy of the subcontractor's laboratory report is enclosed with this Analytical Report. The radiological analysis was subcontracted
to Pace Analytical. A copy of the subcontractor's laboratory report is enclosed with this Analytical Report. J - Indicates an estimated value. U -The analyte was not detected at or above the listed concentration, which is below the laboratory quantitation lim i t B - Analyte detected in the associated Method Blank Q- Qualifier QL -Quantitation Limit DF - Dilution Factor R - RPD outside accepted recovery limits E - Value above quantitation range ••- Value exceeds Action Limit H - Method Hold Time Exceeded MCL

- Contaminant Limit

I. D . 56-00306 PA DEPLaboratory Results Geochemical Testing

Date: 23-Feb-11 CLIENT: RESOURCE MANAGEMENT SERVICES Client Sample ID: Eckles Weli8590H FB Lab Order: Gll01912

RMS 1/1/28 Project: Lab ID: Matrix: Analyses 26R Analysis Gli01912-00I AQUEOUS INORGANIC NON-METALS Acidity to pH 8.2 INORGANIC NON-METALS Alkalinity to pH 4.5 PHYSICAL TESTS Specific Conductance PH BY SM 4500 H+B lab pH INORGANIC NON-METALS Total dissolved solids PHYSICAL TESTS Total suspended solids INDICATOR ORGANIC PARAMETERS Result -38 150 111000 6.52 97500 545 BOD 5-day

1350 Finish Date/Time 212/2011 18
: 10 REACTIVE CYANIDE Reactive cyanide INDICATOR ORGANIC PARAMETERS Chemical Oxygen Demand INORGANIC NON-METALS Bromide Chloride Sulfate INORGANIC NON-METALS MBAS INORGANIC NON-METALS Ammonia Nitrogen

- Distilled INORGANIC NON-METALS Nitrate

- Nitrite INDICATOR ORGANIC PARAMETERS Phenolics REACTIVE SULFIDE Reactive sulfide INORGANIC NON-METALS

< 0.25 5800 461 57100 < 100 < 0 . 25 69.1 0 . 53 < 100 0 . 50 Sampled By: Client Collection Date: 1/28/2011

1 : 10:00 PM Received Date: 1/28/2011 7:08:50 PM QL Q Units DF Date Analyzed SM

· 2310B(4A) Analyst: LNW 0 mg!LCaC03 2/412011 9:44:00 AM SM 18 23208 Analyst: LNW 5 mgll.CaC03 2/312011 4:50

: 00 PM EPA 120.1 Analyst: LNW **~hos/an** 21312011
4 : 50

: 00 PM SM4500-H+B Analyst: LNW 0 su 2/3/2011 4:50:00 PM SM 2540C Analyst:

· KLS 100 mg/L

5 1/3112011 7:10:00 AM SM 2540D Analyst: KLS 25 mg!L

5 113112011
7 : 17
: 04 AM SM 5210 B Analyst: SAG 300 mg/l 300 112812011
6 : 50

: 00 PM 0 mgll. 300 112812011 6:50:00 PM SW846 CH.7 Analyst: SAG 0 . 25 mg/Kg 0.99 219/2011 4:58:00

. PM HACH 8000 Analyst: MGV 50 mg/L

5 2/112011 EPA300.0 Analyst: CAS 10

. 0 mg/L
50 1/3112011
2 : 51

: 00 PM 50 mg/L
50 113112011
2 : 51:00 PM 100 mgll
50 1/31/2011 2:51

: 00 PM SM 5540C Analyst: CAS 0 . 25 H mgll as LAS

5 2/2/2011
2 : 30

: 00 PM EPA 350.1 Analyst: SLY . 5 . 00 mg/L as N 50 2/10/2011 12
: 51

: 01 PM EPA 353.2 Analyst: SLY 0 . 05 mgll as N 2/1/2011 10
: 14
: 21 AM EPA420.1 Analyst: KMW 100 IJ9/L

·s 2/4/20111

: 05

: 00 PM SW846 CH.7 Analyst: SLY 0 . 25 mg/Kg 0.99 2/3/2011 2:50

: 00 PM EPA 351.2 Analyst: SLY - · ----

- - --- ---- - -·-···- -· . . ·--- **~ ~** 

.. ...

* u "Laboratory Results Geochemical Testing

Date: 23-Feb-11 CLIENT: Lab Order: RESOURCE MANAGEMENT SERVICES Gll01912
Client Sample ID: Eckles Wei18590H FB RMS 1/1/28 Project: 26R Analysis Sampled By: Client Lab ID: 01101912-00t Collection Date: l/28120 11 1:10:00 PM Matrix: AQUEOUS Received Date: 1/2812011 7:08:50 PM • • •• • -

-

' o o o n-

•
• • ••• ••• •• •••- -• • Analyses Result QL Q Units DF Date Anal _ yzed INORGANIC NON-METALS

EPA 351.2 Analyst: SLY Total Kjeldahl Nitrogen
61.4 20.0 mg/L as N

2 . 0 2/1/2011 2:35:48 PM INORGANIC METALS EPA200.7 Analyst: MS . Iron, dissolved

10.5 0.05 !l19'l 2/1/2011 12:26:00 PM INORGANIC METALS

SM 31128 Analyst: JEK Mercury
<0.20 0.20 IJg/1,. 2/1/201112:53:33 PM TCLP METALS

EPA 7470 Analyst: JEK Mercury <0.0002 0.0002 mgll

1 2/1/2011 12:49:15 PM TCLP METALS EPA6010 Analyst: MS Arsenic

< 0 . 020 0.020 mgll

1 2/1/201112:18

: 00PM Barium

3190 150 ** mg/L 500 21312011 10:31:00 AM Cadmium <0.002 0.002 mg/L 2/1/2011 12:18

: 00 PM Chromium

< 0 . 010 0.010 mg/L 2/1/2011 12:18

: 00 PM Lead

< 0.020 0.020 mg/L 2/1/201112:18:00 PM Selenium

< 0.020 0.020 mgll

1 2/1/201112:18:00 PM Silver <0.005 0.005 mg/L

1 2/1/201112:18

: 00 PM INORGANIC METALS EPA200.7 Analyst: MS Aluminum

< 1.0 1.0 mg/L
10 2/1/201112:22:00 PM Arsenic
<0.20 0.20 mg/L
10 2/1/2011 12:22:00 PM Barium

2850 5.00 mgiL 500 21312011 10:35:00 AM Beryllium

< 0.010

0 . 010 mg/L
10 2/1/2011 12:22:00 PM Boron

2.58

0 . 50 mg/L
10 2/1/2011 12:22:00 PM Cadmium

< 0.020 0.020 mg/L
10 2/1/2011 12:22:00 PM Calcium

7470 25.0 mgll 250 213/2011 10
: 38:00 AM Chromium

< 0.10

0 . 10 mgll
10 2/1/201112:22:00 PM Cobalt
0.544 0.050 mg/L
10 2/112011 12:22:00 PM Copper

< 0.10 0.10 mg/L
10 2/112011 12:22:00 PM Iron

46.9

0 . 50 mgll
10 2/1/2011 12:22:00 PM Lead
<0.20

0 . 20 mg/l
10 2/1/2011 12
: 22:00 PM Lithium

60

. 3

5 . 00 mg/L 500 2/3/2011 7:41:00 PM Magnesium

638 1.0 mgll
10 2/1/2011 12:22:00 PM Manganese

3.47

0 . 10 mg/L
10 2/1/2011 12
: 22:00 PM Molybdenum
<0.20 0.20 mg/L
10 2/1/2011 12

: 22

: 00 PM Nickel

< 0.10

0 . 10 mg/l
10 2/1/2011 12:22

: 00 PM Selenium

< 0.20 0.20 mg/L
10 2/1/201112:22:00 PM Silver

< 0.050

0 . 050 mg/L
10 2/1/2011 12:22:00 PM Sodium

1510 100 mg/L 500 2/3/2011 7:41 :00 PM Strontium

1350

2 . 50 mgll 250 2/3/2011 10
: 38:00 AM Zinc

< 0.10 0.10 mg/L
10 2/1/2011 12:22

: 00 PM **-- ---~-** 

- · ---· -·-· - --- --- .. . ... ----·· - · ··· - - .

· · · ---·
· ·--------
-- -----

·· · ··- ----- --- -- ---- ------

- --·-···--·----

-- ----- ---· ----- -- - -·· ·- ·-- - **~** .:;>

.. **~**

* <.o

- "

-Laboratory Results Geochemical Testing

Date: 23-Feb-11 CLIENT: Lab Order: RESOURCE MANAGEMENT SERVICES 01101912
Client Sample ID: Eckles Well 8590H FB RMS 1/1128 Project: 26R Analysis Lab ID: 01101912-001 Matrix: AQUEOUS Analyses INORGANIC METALS Hardness (SM 23408) INORGANIC METALS Thorium · Uranium TCLP HERBICIDES 2,4,5-T 2,4-0 Silvex Surr: 2,4-Dichlorophenyt acetic acid TCLP PESTICIDES Chlordane Endrin Lindane Methoxychlor Toxaphene Heptachlor (and its epoxide) Surr: Decachlorobiphenyt Surr: Tetrachloro-m-xytene SEMI-VOLATILE COMPOUNDS: TCLP 2-Methylphenol 2,4-0initrotoluene Hexachlorobenzene Hexachlorobutadiene Hexachloroethane Nitrobenzene Pentachlorophenol Pyridine 2 , 4 , 5 - Trichlorophenol 2,4

, 6-Trichlorophenol 3.4-Methytphenol Surr
: 2,4,6-Tribromophenol Surr
: 2-Fiuorobiphenyt Surr
: 2-Fiuorophenol Surr: Nitrobenzene-d5 Surr
: Phenol-d6 Surr
: p - Terphenyl-d14 VOLATILE ORGANIC COMPOUNDS Benzene Result 18500 <200 <200 < 0.0050 < 0.020 <0.0050 74.9 < 0.010 <0

. 00050 < 0.00050 < 0 . 00050 < 0 . 020 < 0.0010 96

. 3 64.3 < 100 < 100 < 100 < 100 < 100 < 100 < 500 <200 < 100 < 100 < 100 101 49

. 3 60

. 4 86.7 51

. 7 38

. 8 < 1.0 Sampled By: Client Collection Date: 1128/2011 1:10:00 PM Received Date: 1128/2011 7:08:50 PM QL Q Units DF Date Analyzed EPA200.7 Analyst: MS 10.0 mgJLCaC03
10 211/201112

: ?2
: 00 PM EPA200.8 Analyst: JEK . 200 IJg/L 200 21812011 3:03

: 00 PM 200 IJg/L 200 21812011
3 : 03:00 PM EPA 8151 Analyst.: NPT 0.0050 mgll 100 213/2011 10
: 39

: 30 PM 0.020 mg/L 100 213/201110:39:30 PM 0 . 0050 mg/L 100 213/2011 10:39

: 30 PM 28

. 5-130 %REC 100 213/2011 10:39:30 PM EPA8081 Analyst: NPT 0.010 mgll
10 21212011
7 : 07
: 46 PM 0.00050 mgll
10 2!212011 7:07

: 46 PM 0 . 00050 mg/L
10 21212011
7 : 07:46 PM 0 . 00050 mg/L
10 21212011
7 : 07:46 PM 0 . 020 mgll
10 21212011
7 : 07

: 46 PM 0.0010 mg/L
10 21212011 7:07:46 PM 5-156 %REC
10 21212011
7 : 07
: 46 PM 15.9-102 %REC
10 21212011
7 : 07

: 46 PM EPA8270 Analyst: JB 100 IJg/L
10 214/2011 6:48:00 /lN. 100 IJg/L
10 214/2011 6:48

: 00 /lN. 100 IJQ/L
10 214/2011 6:48

: 00 /lN. 100 IJg/L
10 214/2011
6 : 48:00 /lN. 100 IIQIL
10 214/2011 6:48:00 AM 100 1J91L
10 214/2011 6:48:00 AM 500 IJg/L
10 214/2011 6:48:00 /lN. 200 IJQIL
10 214/2011
6 : 48:00

. AM 100 IJQ/L
10 214/2011
6 : 48

: 00 AM 100 IJg/L
10 214/2011
6 : 48

: 00 AM 100 119/L
10 214/2011
6 : 4.8

: 00 AM 5-137 %REC

10 214/2011
6 : 48

: 00 AM 27.7-95.1 %REC
10 2/4/2011
6 : 48

: 00 AM 5-104 %REC
10 214/2011
6 : 48

: 00 AM 16-101 o/oREC
10 214/2011
6 : 48

: 00 AM 5-106 %REC

10 214/2011
6 : 48

: 00 AM 25.4-133 %REC
10 2/4/2011
6 : 48

: 00 AM EPA8260 Analyst: SJM 1 . 0 119/L

. 1/31/2011 7:02:00 PM -------- -- -------------

---·· -------------

--·- ---- ------- **~** ..

... «

**~** "

**~** "

**~**<

**~** 1.0 . 56-00306 PA DEP Paae 5 of 7Laboratory Results Geochemical Testing

Date: 23-Feb-11 ------·-----·-

---- ==== ===- - --: :::- CLIENT: RESOURCE MANAGEMENT SERVICES Client Sample ID: Eckles Weli8590H FB Lab Order: GIJ01912

RMS 111/28 Project: 26R Analysis Sampled By: Client Lab ID: Gll01912-00I Collection Date: l/28/20lll:IO:OO PM Matrix: AQUEOUS Received Date: 1/28/20ll 7:08:50 PM ---- ---·----- --- -·· --
· ----

- ----------

· --------------------- --------

- . - -· Analyses VOLA TILE ORGANIC COMPOUNDS Toluene Surr: 1,2-Dichloroethane--d4 Surr: 4-Bromofluorobenzene Surr: Toluene-d8 Result 1.1 10S 102 95.3 VOLATILE ORGANIC COMPOUNDS: TCLP **~nz~**

<00 Carbon Tetrachloride

< 00 Chlorobenzene

< 00 1,1-Dichloroethene

< 50 1,2-Dichloroethane

< 50 1,4-Dichlorobenzene

< 00 Trichloromethane

< 50 Methyl Ethyl Ketone

< 250 Tetrachloroethene

< 00 Trichloroethene

< 50 Vinyl Chloride

< 50 surr: 1,2-Dichloroethane-<14

90.7 Surr: 4-Bromofluorobenzene

99.7 Surr: Dibromofluoromethane

92.0 Surr: Toluene-d8

97

. 0 INDICATOR ORGANIC PARAMETERS Oil & Grease

436 NOTES:

QL Q EPA 8260 1.0 70-130 70-130 70-130 EPA8260 50 50 50 50 50 50 50 250 50 50 50 70-130 70-130 70-130 70-130 EPA 1664 5 Units ll91L %REC %REC %REC J.I9IL J.191l J.lg/L J.lg/L ll91L J.19IL J.191l J.191l J.IQIL J.I9IL J.I9IL %REC %REC %REC %REC mgll DF Date Analyzed Analyst: SJM 113112011 7:02

: 00 PM 113112011
7 : 02

: 00 PM 113112011 7:02:00 PM 1/3112011 7:02

: 00 PM Analyst: JAW 50 2/312011 4:31

: 00 AM 50 2/3120114:31

: 00AM 50 21312011 4:31:00 AM 50 21312011 4:31 :00 AM 50 213120114:31:00AM 50 2/3/2011 4:31:00 AM 50 2/312011 4:31

: 00 AM 50 213/20114

: 31

: 00AM 50 2/3/20114:31:00AM 50 213120114:31

: 00AM 50 21312011 4:31:00 AM 50 213120114:31:00AM 50 21312011 4:31 :00 AM 50 21312011 4:31 :00 AM 50 213/2011 4:31:00 AM Analyst: DSZ 1.08 21112011 8:48:00 AM J- Unable to obtain a stable weight within specified limits due to sample matrix. Value is estimated. VOLA TILE ORGANIC COMPOUNDS Ethylene Glycol

< 550 RADIOLOGICAL TESTING Gross Alpha 7229 +- 1675 Gross Beta
1048 + -- 748 RADIOLOGICAL PARAMETERS Radium 226
1638 +- 307 RADIOLOGICAL PARAMETERS Radium 228

199 +- 39

. 2 INORGANICS NON-METALS Corrosivity Characteristic

6 . 55 FLASH POINT EPA8015 550 EPA 900.0 3 . 00 4.00 EPA 903.1 1 . 00 EPA 904.0 1.00 EPA 9040 1.00 EPA 1010 **P~nA**R nf7 mgll pCVL pCill pCill pCill su Analyst: SUB 217/2011 Analyst: SUB 2110/2011 2110/2011 Analyst: SUB 211812011 Analyst: SUB 2/1812011 Analyst: RLL 1131/2011 Analyst: RLL 1.0. 56-00306 PA DEPLaboratory Results Geochemical Testing

Date: 23-Feb-11 CLIENT: Lab Order: RESOURCE MANAGEMENT SERVICES Gll019l2
Client Sample ID: Eckles Well 8590H FB RMS l/1128 Project: 26R Analysis Sampled By: Client Lab ID: Gli01912-00I Collection Date: l/28/2011 1:10:00 PM Matrix: AQUEOUS Received Date: 1/2812011 7:08

: 50 PM **-- ·~~** **--- --** **--** ----·- ---·· ·· -··· ---------··- --------------------- -· .. - · . ------· ------- ----
--- ----- ------

----- -- --------- ...
. . -- Analyses FLASH POINT Flashpoint TCLP ZHE EXTRACTION TCLP,ZHE TCLP EXTRACTION Extraction Fluid Used Final pH . Initial pH pH with HCI pH with water TCLP, non-volatile TCLP, ZHE Result QL Q EPA 1010 >200 10
. 0 EPA 1311 RL 1.0 EPA 1311 NA

0 3 . 1 1.0 NA 1.0 NA 1.0 NA

1 : 0 NA

0 NA

0 Units •f DF Date Analyzed Analyst: RLL 2/212011 Analyst: RLL 1/3112011 Analyst: RLL 1 . 1/3112011 1 . 1/31/2011 1/3112011 1/3112011 1 1/3112011 1 1131/2011 1/31/2011 • •• ••

··

-

- •• -· -····-·-

· --

- --

· --·-··.

- -- -- -- --- ·-·

- --·- -·

- -- ·-

-

0

• •

--

. I. D . 56-00306 PA DEP Pace 7 of 7