### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1



### 1210003 Progress Energy Florida, Inc. 3 No.6 Fuel Oil (residual or bunker C) 1210004 Progress Energy Florida, Inc. 3 No.6 Fuel Oil (residual or bunker C) 1210005 Progress Energy Florida, Inc. 3 No.6 Fuel Oil (residual or bunker C) 1210006 Progress Energy Florida, Inc. 3 No.6 Fuel Oil (residual or bunker C) 1210007 Progress Energy Florida, Inc. 3 No.6 Fuel Oil (residual or bunker C) 1210008 Progress Energy Florida, Inc. 3 No.6 Fuel Oil (residual or bunker C) 1210009 Progress Energy Florida, Inc. 3 No.6 Fuel Oil (residual or bunker C) 1210010 Progress Energy Florida, Inc. 3 No.6 Fuel Oil (residual or bunker C) 1210011 Progress Energy Florida, Inc. 3 No.6 Fuel Oil (residual or bunker C) 1210012 Progress Energy Florida, Inc. 3 No.6 Fuel Oil (residual or bunker C) 1210013 Progress Energy Florida, Inc. 3 No.6 Fuel Oil (residual or bunker C)Fuel Type 2 Fuel Type 3 Other Fuel Description 

### No.6 Fuel Oil (residual or bunker C) No.6 Fuel Oil (residual or bunker C) No.6 Fuel Oil (residual or bunker C) No.6 Fuel Oil (residual or bunker C) No.6 Fuel Oil (residual or bunker C) No.6 Fuel Oil (residual or bunker C) No.6 Fuel Oil (residual or bunker C) No.6 Fuel Oil (residual or bunker C) No.6 Fuel Oil (residual or bunker C) No.6 Fuel Oil (residual or bunker C) No.6 Fuel Oil (residual or bunker C)EIA

Facility Code Facility Name Boiler ID Basis An alyte 

### 1210003 Progress Energy Florida, Inc. 3 As Received Higher Heating Value 

### 1210003 Progress Energy Florida, Inc. 3 As Received % Moisture 

### 1210003 Progress Energy Florida, Inc. 3 As Received % Ash 

### 1210003 Progress Energy Florida, Inc. 3 As Received % Sulfur 

### 1210003 Progress Energy Florida, Inc. 3 Dry basis Antim ony 

### 1210003 Progress Energy Florida, Inc. 3 Dry basis Arsenic 

### 1210003 Progress Energy Florida, Inc. 3 Dry basis Beryllium 

### 1210003 Progress Energy Florida, Inc. 3 Dry basis Cadmium 

### 1210003 Progress Energy Florida, Inc. 3 Dry basis Chlorine 

### 1210003 Progress Energy Florida, Inc. 3 Dry basis Chromium 

### 1210003 Progress Energy Florida, Inc. 3 Dry basis Cobalt 

### 1210003 Progress Energy Florida, Inc. 3 Dry basis Fluorine 

### 1210003 Progress Energy Florida, Inc. 3 Dry basis Lead 

### 1210003 Progress Energy Florida, Inc. 3 Dry basis Manganese 

### 1210003 Progress Energy Florida, Inc. 3 Dry basis Mercury 

### 1210003 Progress Energy Florida, Inc. 3 Dry basis Nickel 

### 1210003 Progress Energy Florida, Inc. 3 Dry basis Selenium 

### 1210003 Progress Energy Florida, Inc. 3 As Received Carbon 

### 1210003 Progress Energy Florida, Inc. 3 As Received Hydrogen 

### 1210003 Progress Energy Florida, Inc. 3 As Received NitrogenAn alysis M ethod for each Analyte

(example: ASTM D5865-04) ASTM D5865 ASTM D3173 ASTM D3174 ASTM D4239 ASTM D6357 ASTM D6357 ASTM D6357 ASTM D6357 ASTM D4208 ASTM D6357 ASTM D6357 ASTM D3761 ASTM D6357 ASTM D6357 ASTM D6722 ASTM D6357 ASTM D4606 ASTM D5373 ASTM D5373 ASTM D5373EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 1210003 Progress Energy Florida, Inc. 3 Dioxin/furan HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) 3 

### 2/23/2010 2/23/2010 17851 Btu/gallon <0.01 3 2/24/2010 2/24/2010 17885 Btu/gallon <0.01 3 2/25/2010 2/25/2010 17908 Btu/gallon <0.01 Fuel Testing Results% A sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units 

### 0.08 1.01 17851 Btu/gallon 0.08 1.01 77 ppm 0.03 1.00 17885 Btu/gallon 0.03 1.00 75 ppm 0.06 1.01 17908 Btu/gallon 0.06 1.01 187 ppmMercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) 

### 0.01 mg/g <0.01 mg/g 14.26 mg/g <0.01 mg/g 0.01 0.01 mg/g <0.01 mg/g 10.41 mg/g <0.01 mg/g <0.01 0.01 mg/g <0.01 mg/g 14.85 mg/g <0.1 mg/g 0.03Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units 

### mg/g <0.01 mg/g 31.84 mg/g <0.01 mg/g 1.9 mg/g mg/g <0.01 mg/g 22.39 mg/g <0.01 mg/g 0.37 mg/g mg/g <0.01 mg/g 31.81 mg/g <0.01 mg/g 0.18 mg/gNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles 

### <0.01 mg/g 15 ppm 0.09 mg/g <0.01 mg/g 12 ppm 0.07 mg/g <0.01 mg/g 13 ppm 0.17 mg/g Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

### 0.08 90.05% 6.05% 0.29% 0.03 88.75% 8.47 0.26 0.06 89.40% 8.39 0.17 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 1210003 Progress Energy Florida, Inc. 3 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units % Moisture (as received) 3 

### 2/26/2010 2/26/2010 17884 Btu/gallon <0.01 3 2/27/2010 2/27/2010 17808 Btu/gallon <0.01 Fuel Testing Results% A sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) 

### 0.04 1.02 17884 Btu/gallon 0.04 1.02 150 0.06 1.03 17808 Btu/gallon 0.06 1.03 141Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units 

### ppm 0.01 mg/g <0.01 mg/g 14.22 mg/g <0.01 mg/g ppm 0.01 mg/g <0.01 mg/g 14.18 mg/g <0.01 mg/gCadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) 

### 0.02 mg/g <0.01 mg/g 31.2 mg/g <0.01 mg/g 1.02 <0.01 mg/g <0.01 mg/g 30.27 mg/g <0.01 mg/g <0.01Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Nickel Units Selenium

(Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles 

### mg/g <0.01 mg/g 12 ppm <0.01 mg/g mg/g <0.01 mg/g 11 ppm <0.01 mg/g Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

### 0.04 89 8.76 0.11 0.06 89.97 8.44 0.12 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 1210003 Progress Energy Florida, Inc. 3 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) 3 

### 2/28/2010 2/28/2010 17974 Btu/gallon <0.01 3 3/4/2010 3/4/2010 17938 Btu/gallon <0.01 3 3/5/2010 3/5/2010 17894 Btu/gallon <0.01 Fuel Testing Results% A sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units 

### 0.09 0.98 17974 Btu/gallon 0.09 0.98 128 ppm 0.2 1.01 17938 Btu/gallon 0.2 1.01 105 ppm 0.07 0.99 17894 Btu/gallon 0.07 0.99 74 ppmMercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) 

### 0.01 mg/g <0.01 mg/g 8.99 mg/g <0.01 mg/g 0.03 0.02 mg/g <0.01 mg/g 14.83 mg/g <0.01 mg/g 0.02 0.01 mg/g <0.01 mg/g 14.52 mg/g <0.01 mg/g 0.04Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units 

### mg/g <0.01 mg/g 33.43 mg/g <0.01 mg/g 0.56 mg/g mg/g <0.01 mg/g 33.41 mg/g <0.01 mg/g 0.96 mg/g mg/g <0.01 mg/g 32.25 mg/g <0.01 mg/g 3.62 mg/gNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h 

### 0.01 mg/g 11 ppm 0.15 mg/g <0.01 0.09 <0.01 mg/g 12 ppm 0.17 mg/g <0.01 0.2 <0.01 mg/g 13 ppm 0.07 mg/g <0.01 0.07 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen



### 89.07 8.68 0.22 90.52 6.31 0.33 88.55 8.59 0.14

Ultimate Analy

ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 1210003 Progress Energy Florida, Inc. 3 Dioxin/furan HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) 3 

### 3/1/2010 3/1/2010 17968 Btu/gallon <0.01 3 3/2/2010 3/2/2010 17949 Btu/gallon <0.01 3 3/3/2010 3/3/2010 17941 Btu/gallon <0.01 Fuel Testing Results% A sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units 

### 0.05 1.00 17968 Btu/gallon 0.05 1.00 92 ppm 0.04 1.01 17949 Btu/gallon 0.04 1.01 100 ppm 0.1 1.02 17941 Btu/gallon 0.1 1.02 202 ppmMercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) 

### 0.01 mg/g <0.01 mg/g 13.91 mg/g <0.01 mg/g 0.05 0.01 mg/g <0.01 mg/g 14.86 mg/g <0.01 mg/g 0.05 0.01 mg/g <0.01 mg/g 13.81 mg/g <0.01 mg/g 0.09Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units 

### mg/g <0.01 mg/g 30.09 mg/g <0.01 mg/g 5.71 mg/g mg/g <0.01 mg/g 32.57 mg/g <0.01 mg/g 5.83 mg/g mg/g <0.01 mg/g 30.14 mg/g <0.01 mg/g 1.67 mg/gNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h 

### <0.01 mg/g 13 ppm <0.01 mg/g 0.05 <0.01 mg/g 14 ppm <0.01 mg/g 0.04 <0.01 mg/g 15 ppm 0.05 mg/g 0.1 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen



### 88.69 8.56 0.26 89.18 8.83 0.14 88.5 9.13 0.12 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm