Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop-down boxes, included. Gray fields are aut

filled from other fields.

Please name each resulting spreadsheet with the following naming convention: 

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.

3. Please choose the type of fuel being sampled using the drop-down in the fuel column of the Boiler Informatio

worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column.

4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "A

04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If t

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange 

highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksh

6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell)

7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a min

composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you ha

more.

8. Provide the results of the analyses for each constituent requested. Use the drop-down boxes to fill in the unit

measure.
Information

ormation about chemical analyses of fuels 

hlorine, fluorine, and metals, such as 

 selenium. This spreadsheet is intended to 

) fuel analyses at that specific boiler. This 

or all 4 HAP surrogates were being tested. 

Fields that are highlighted in yellow are 

xes, included. Gray fields are automatically 

 on the Boiler Information worksheet.

el column of the Boiler Information 

e Other Fuel Description column.

hods worksheet. For example: "ASTM D5865-

cklist worksheet (orange tab). If the units of

ease fill them in the blank, orange 

n the Fuels Sample Results worksheet.

range highlighted cell).

orksheet. You must provide a minimum of 3 

t limited to that number if you have collected 

down boxes to fill in the units of 
EIA Facility Code Facility Name Boiler ID Fuel Type 1

1210003 Progress Energy Florida, Inc. 3 No.6 Fuel Oil (residual or bunker C)

1210004 Progress Energy Florida, Inc. 3 No.6 Fuel Oil (residual or bunker C)

1210005 Progress Energy Florida, Inc. 3 No.6 Fuel Oil (residual or bunker C)

1210006 Progress Energy Florida, Inc. 3 No.6 Fuel Oil (residual or bunker C)

1210007 Progress Energy Florida, Inc. 3 No.6 Fuel Oil (residual or bunker C)

1210008 Progress Energy Florida, Inc. 3 No.6 Fuel Oil (residual or bunker C)

1210009 Progress Energy Florida, Inc. 3 No.6 Fuel Oil (residual or bunker C)

1210010 Progress Energy Florida, Inc. 3 No.6 Fuel Oil (residual or bunker C)

1210011 Progress Energy Florida, Inc. 3 No.6 Fuel Oil (residual or bunker C)

1210012 Progress Energy Florida, Inc. 3 No.6 Fuel Oil (residual or bunker C)

1210013 Progress Energy Florida, Inc. 3 No.6 Fuel Oil (residual or bunker C)
Fuel Type 2 Fuel Type 3 Other Fuel Description

 or bunker C)

 or bunker C)

 or bunker C)

 or bunker C)

 or bunker C)

 or bunker C)

 or bunker C)

 or bunker C)

 or bunker C)

 or bunker C)

 or bunker C)
EIA Facility Code Facility Name Boiler ID Basis Analyte

1210003 Progress Energy Florida, Inc.3 As Received Higher Heating Value

1210003 Progress Energy Florida, Inc.3 As Received % Moisture

1210003 Progress Energy Florida, Inc.3 As Received % Ash

1210003 Progress Energy Florida, Inc.3 As Received % Sulfur

1210003 Progress Energy Florida, Inc.3 Dry basis Antimony

1210003 Progress Energy Florida, Inc.3 Dry basis Arsenic

1210003 Progress Energy Florida, Inc.3 Dry basis Beryllium

1210003 Progress Energy Florida, Inc.3 Dry basis Cadmium

1210003 Progress Energy Florida, Inc.3 Dry basis Chlorine

1210003 Progress Energy Florida, Inc.3 Dry basis Chromium

1210003 Progress Energy Florida, Inc.3 Dry basis Cobalt

1210003 Progress Energy Florida, Inc.3 Dry basis Fluorine

1210003 Progress Energy Florida, Inc.3 Dry basis Lead

1210003 Progress Energy Florida, Inc.3 Dry basis Manganese

1210003 Progress Energy Florida, Inc.3 Dry basis Mercury

1210003 Progress Energy Florida, Inc.3 Dry basis Nickel

1210003 Progress Energy Florida, Inc.3 Dry basis Selenium

1210003 Progress Energy Florida, Inc.3 As Received Carbon

1210003 Progress Energy Florida, Inc.3 As Received Hydrogen

1210003 Progress Energy Florida, Inc.3 As Received Nitrogen
Analysis Method for each Analyte 

(example: ASTM D5865-04)

ASTM D5865

ASTM D3173

ASTM D3174

ASTM D4239

ASTM D6357

ASTM D6357

ASTM D6357

ASTM D6357

ASTM D4208

ASTM D6357

ASTM D6357

ASTM D3761

ASTM D6357

ASTM D6357

ASTM D6722

ASTM D6357

ASTM D4606

ASTM D5373

ASTM D5373

ASTM D5373
EIA Facility Code Facility Name Boiler ID HAPs Test Group

1210003 Progress Energy Florida, Inc. 3 Dioxin/furan HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating Value 

(HHV)

(as received) HHV Units

% Moisture

(as received)

3 2/23/2010 2/23/2010 17851 Btu/gallon <0.01

3 2/24/2010 2/24/2010 17885 Btu/gallon <0.01

3 2/25/2010 2/25/2010 17908 Btu/gallon <0.01

 Fuel Testing Results


% Ash

(as received)

% Sulfur

(as received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

0.08 1.01 17851 Btu/gallon 0.08 1.01 77 ppm

0.03 1.00 17885 Btu/gallon 0.03 1.00 75 ppm

0.06 1.01 17908 Btu/gallon 0.06 1.01 187 ppm


Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

0.01 mg/g <0.01 mg/g 14.26 mg/g <0.01 mg/g 0.01

0.01 mg/g <0.01 mg/g 10.41 mg/g <0.01 mg/g <0.01

0.01 mg/g <0.01 mg/g 14.85 mg/g <0.1 mg/g 0.03


Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units

mg/g <0.01 mg/g 31.84 mg/g <0.01 mg/g 1.9 mg/g

mg/g <0.01 mg/g 22.39 mg/g <0.01 mg/g 0.37 mg/g

mg/g <0.01 mg/g 31.81 mg/g <0.01 mg/g 0.18 mg/g


Note the Proximate/Ultimate data 

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles

<0.01 mg/g 15 ppm 0.09 mg/g

<0.01 mg/g 12 ppm 0.07 mg/g

<0.01 mg/g 13 ppm 0.17 mg/g

Proximate Analyses, % by wt


Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

0.08 90.05% 6.05% 0.29%

0.03 88.75% 8.47 0.26

0.06 89.40% 8.39 0.17

ximate Analyses, % by wt Ultimate Analyses, % by wt


EIA Facility Code Facility Name Boiler ID HAPs Test Group

1210003 Progress Energy Florida, Inc. 3 Non-dioxin/furan organic HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received) HHV Units

% Moisture

(as received)

3 2/26/2010 2/26/2010 17884 Btu/gallon <0.01

3 2/27/2010 2/27/2010 17808 Btu/gallon <0.01

 Fuel Testing Results


% Ash

(as received)

% Sulfur

(as received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

0.04 1.02 17884 Btu/gallon 0.04 1.02 150

0.06 1.03 17808 Btu/gallon 0.06 1.03 141


Chlorine 

Units

Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

ppm 0.01 mg/g <0.01 mg/g 14.22 mg/g <0.01 mg/g

ppm 0.01 mg/g <0.01 mg/g 14.18 mg/g <0.01 mg/g


Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis)

0.02 mg/g <0.01 mg/g 31.2 mg/g <0.01 mg/g 1.02

<0.01 mg/g <0.01 mg/g 30.27 mg/g <0.01 mg/g <0.01


Note the Proximate/Ult

Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles

mg/g <0.01 mg/g 12 ppm <0.01 mg/g

mg/g <0.01 mg/g 11 ppm <0.01 mg/g

Proximate Analyses, % by wt


Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

0.04 89 8.76 0.11

0.06 89.97 8.44 0.12

mate Analyses, % by wt Ultimate Analyses, % by wt


EIA Facility Code Facility Name Boiler ID HAPs Test Group

1210003 Progress Energy Florida, Inc. 3 Acid gas HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher 

Heating 

Value (HHV)

(as 

received) HHV Units

% Moisture

(as received)

3 2/28/2010 2/28/2010 17974 Btu/gallon <0.01

3 3/4/2010 3/4/2010 17938 Btu/gallon <0.01

3 3/5/2010 3/5/2010 17894 Btu/gallon <0.01

 Fuel Testing Results


% Ash

(as received)

% Sulfur

(as received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

0.09 0.98 17974 Btu/gallon 0.09 0.98 128 ppm

0.2 1.01 17938 Btu/gallon 0.2 1.01 105 ppm

0.07 0.99 17894 Btu/gallon 0.07 0.99 74 ppm


Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

0.01 mg/g <0.01 mg/g 8.99 mg/g <0.01 mg/g 0.03

0.02 mg/g <0.01 mg/g 14.83 mg/g <0.01 mg/g 0.02

0.01 mg/g <0.01 mg/g 14.52 mg/g <0.01 mg/g 0.04


Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units

mg/g <0.01 mg/g 33.43 mg/g <0.01 mg/g 0.56 mg/g

mg/g <0.01 mg/g 33.41 mg/g <0.01 mg/g 0.96 mg/g

mg/g <0.01 mg/g 32.25 mg/g <0.01 mg/g 3.62 mg/g


Note the Proximate/Ultimate data 

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Ash

0.01 mg/g 11 ppm 0.15 mg/g <0.01 0.09

<0.01 mg/g 12 ppm 0.17 mg/g <0.01 0.2

<0.01 mg/g 13 ppm 0.07 mg/g <0.01 0.07

Proximate Analyses, % by wt


roximate/Ultimate data below should be recorded on a dry basis (including ash).

Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

89.07 8.68 0.22

90.52 6.31 0.33

88.55 8.59 0.14

Ultimate Analyses, % by wt


EIA Facility Code Facility Name Boiler ID HAPs Test Group

1210003 Progress Energy Florida, Inc. 3 Dioxin/furan HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received) HHV Units

% Moisture

(as received)

3 3/1/2010 3/1/2010 17968 Btu/gallon <0.01

3 3/2/2010 3/2/2010 17949 Btu/gallon <0.01

3 3/3/2010 3/3/2010 17941 Btu/gallon <0.01

 Fuel Testing Results


% Ash

(as received)

% Sulfur

(as received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

0.05 1.00 17968 Btu/gallon 0.05 1.00 92 ppm

0.04 1.01 17949 Btu/gallon 0.04 1.01 100 ppm

0.1 1.02 17941 Btu/gallon 0.1 1.02 202 ppm


Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

0.01 mg/g <0.01 mg/g 13.91 mg/g <0.01 mg/g 0.05

0.01 mg/g <0.01 mg/g 14.86 mg/g <0.01 mg/g 0.05

0.01 mg/g <0.01 mg/g 13.81 mg/g <0.01 mg/g 0.09


Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units

mg/g <0.01 mg/g 30.09 mg/g <0.01 mg/g 5.71 mg/g

mg/g <0.01 mg/g 32.57 mg/g <0.01 mg/g 5.83 mg/g

mg/g <0.01 mg/g 30.14 mg/g <0.01 mg/g 1.67 mg/g


Note the Proximate/Ultimate data belo

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Ash

<0.01 mg/g 13 ppm <0.01 mg/g 0.05

<0.01 mg/g 14 ppm <0.01 mg/g 0.04

<0.01 mg/g 15 ppm 0.05 mg/g 0.1

Proximate Analyses, % by wt


roximate/Ultimate data below should be recorded on a dry basis (including ash).

Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

88.69 8.56 0.26

89.18 8.83 0.14

88.5 9.13 0.12

alyses, % by wt Ultimate Analyses, % by wt


Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the 

Fuel Units of Measure - HHV

anthracite Btu/lb

bituminous Btu/gallon

subbituminous

lignite

coal refuse (culm or gob)

No.2 Fuel Oil (distillate)

No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals

synfuel mg/g

petroleum coke μg/g

other mg/Kg

nit of measure to the orange hightlighted cell, if necessary.

Units of Measure - Cl, Fl

%

ppm