Exhaust Emissions Sampling 

Dal Italia, LLC., Muskogee, OK 

Spray Dryer, Kiln Scrubber, and Trim Kiln Exhausts 

. December 6 - 8, 2005 

Arrnstrong Environmental, Inc. 

Project W-2485-05 

Report Prepared For: 

Bob Hurt 

Daltile 

7834 C. F. Hawn Freeway 

Dallas, TX 75217 

Report Prepared December 21, 2005 By: 

Armstrong Environmental, Inc. 

7715 Sovereign Row 

Dallas, Texas 75247 

(214) 631-0021 
TABLE OF CONTENTS 

I. Introduction 

U. Summary 

III. Procedures 

I'V. Appendices 

A. Calculation Summaries 

B. Continuous Emissions Monitor Summaries 

C. Analytical Summaries 

D. Field Data Sheets 

E. Equipment Calibrations 

F. Standard Gas Certifications 

G. S02 Interfernce Summaries 

Page 

1 

2-9 

10- 16 

17 -.34 

35 - 129 

130 - 217 

218 -238 

~ 239 - 252 

253 - 264 

265 - 323 
SUMMARY OF EMISSIONS TEST DATA 

Table : 4 

Plant : Daltile, Muskogee, OK 

Location : Kiln Scrubber Exhaust 

Operator : D. Barrera 

Test Date : 7•Dec•05 

Repetition : 1 2 3 

STACK GAS 

Temperature, F 138.3 138.4 138.2 

Velocity, fps 29.06 29.06 29.67 

Volume Flow, acfm 33664.7 33669.9 34368.6 

scfm 22612.7 22453.4 22833.2 

scfh 1356762 1347206 1369993 

Moisture, % 23.80% 24.33% 24.40% 

CO2, % 3.00 3.00 3.00 

02, % 16.00 16.00 16.00 

SAMPLE 

Start Time, hrs:min 10:10 AM 12:22 PM 2:05 PM 

Finish Time, hrs:rnin 11:17 AM 1:26 PM 3:10 PM 

Sample Volume, scf 39.247 38.933 36.583 

Isokinetic Ratio, % 104.802 104.7015 96.745 

CARBON MONOXIDE 

Concentration, ppm 234.48 230.63 

Emissions, Ibs/hr 23.12497 22.58507 

NITROGEN OXIDE AS NO2 

Concentration, ppm 33.02 33.23 

Emissions, Ibs/hr 5.34998 5.346085 

VOC AS C31-18 

Concentration, ppm as C3H8, WET 47.17 45.70 

Concentration, ppm as C3H8, WET 61.9013 60.39667 

Emissions, Ibs/hr as C3H8 9.593337 9.294228 

Emissions, Ibs/hr as C 7.849094 7.604368 

SULFUR DIOXIDE 

Concentration, ppm 0.073 0.225 

Emissions, Ibs/hr 0.016456 0.050363 

HYDROGEN FLUORIDE 

Sample Weight, mg 0.22 0.72 0.24 

Concentration, ppm 0.235891 0.789733 0.280929 

Emissions, Ibs/hr 0.016617 0.055241 0.019983 

CHLORINE 

Sample Weight, mg 0.00 0.00 0.00 

Concentration, ppm 0 0 0 

Emissions, Ibs/hr 0 0 0 

HYDROGEN CHLORIDE 

Sample Weight, mg 0.87 0.70 0.64 

Concentration, ppm 0.515243 0.415995 0.40519 

Emissions, Ibs/hr - 0.06624 0.053104 0.0526 

-n 
SUMMARY OF EMISSIONS TEST DATA 

138.4 

29.24 

33881.2 

22583.6 

1355016 

24.37% 

3.00 

16.00 

1 

10:10 AM 

11:17 AM 

39.193 

105.0612 

66.74 

0.026275 

. 5.087779 

4.48 

0.001764 

0.341523 

5.429302 

Table : 3 

Plant : Daltile, Muskogee, OK 

Location : Kiln Scrubber Exhausi 

Operator : R. Taylor 

Test Date : 7•Dec•05 

Repetition : 

STACK GAS 

Temperature, F 

Velocity, fps 

Volume Flow, acfm 

scfm 

scfh 

Moisture, % 

CO2, % 

02, % 

SAMPLE 

Start Time, hrs:min 

Finish Time, hrs:min 

Sample Volume, scf 

Isokinetic Ratio, % 

PARTICVLATE 

"ront Half 

amp e Weight, mg 

Concentration, gr/scf 

Emissions, Ibs/hr 

Back Half 

Sample Weight, mg 

Concentration, gr/scf 

Emissions, Ibs/hr 

Total Particulate, Ibs/hr 

CARBON MONOXIDE 

Concentration, ppm 

Emissions, Ibs/hr 

NITROGEN OXIDE AS NO2 

Concentration, ppm 

Emissions, Ibs/hr 

VOC AS C31-18 

Concentration, ppm as C31-18, WET 

Concentration, ppm as C3H8, WET 

Emissions, Ibs/hr as C3H8 

Emissions, Ibs/hr as C 

SULFUR DIOXIDE 

Concentration, ppm 

Emissions, Ibs/hr 

3 

137.0 

30.38 

35191.8 

23764.2 

1425855 

23.31% 

3.00 

16.00 

2:05 PM 

3:10 PM 

40.964 

104.3513 

52.80 

0.019888 

4.052464 

8.20 

0.003089 

0.62936 

4.681824 

236.52 

24.51404 

33.07 

5.630942 

46.13 

60.15022 

9.79668 

8.015465 

0.482 

0.114187 

2 

137.1 

28.73 

33283.3 

22204.8 

1332289 

24.47% 

3.00 

16.00 

12:22 PM 

1:26 PM 

38.815 

105.821 

55.37 

0.022011 

4.190704 

13.38 

0.005319 

1.012671 

5.203375 

7 
SUMMARY OF EMISSIONS TEST DATA 

Table : 5 

Plant : Daltile, Muskogee, OK 

Location : Trim Kiln Exhaust 

Operator : R. Taylor 

Test Date : 8•Dec•05 

Repetition : 1 2 3 

STACK GAS 

Temperature, F 485.0 486,2 486.5 

Velocity, fps 79.43 77.96 79.05 

Volume Flow, acfm 15602.0 15312.9 15527.1 

scfm 8251.9 8097.6 8072.2 " 

scfh 495113 485857 484334 

Moisture, % 5.50% 5.40% 6.97% 

CO2, % 2.50 2.50 2.50 

02, % 17.50 17.00 17.00 

SAMPLE 

Start Time, hrs:min 11:20 AM 12:50 PM 2:20 PM 

Finish Time, hrs:min 11:24 AM 1:53 PM 3:22 PM 

Sample Volume, scf 51.241 49.860 50.057 

Isokinetic Ratio, % 98.90241 98.06889 98.76648 

PARTICULATE 

Front Half 

Sample Weight, mg 30.30 29.31 31.01 

Concentration, gr/scf 0.009124 0.009071 0.009559 

Emissions, Ibs/hr 0,645556 0.629771 0.661595 

Back Half 

Sample Weight, mg 26.33 24.41 20.19 

Concentration, gr/scf 0.007929 0.007554 0.006224 

Emissions, Ibs/hr 0.560973 0.524487 0.430751 

Total Particulate, Ibs/hr 1.20653 1.154258 1.092346 

CARBON MONOXIDE 

Concentration, ppm 165.54 171.36 

Emissions, Ibs/hr 5.957706 6.032906 

NITROGEN OXIDE AS NO2 

Concentration, ppm 30.29 30.92 

Emissions, Ibs/hr 1.790916 1.788366 

VOC AS C31-18 

Concentration, ppm as C3H8, WET 138.61 128.32 

Concentration, ppm as C3H8, DRY 146.6825 137.9369 

Emissions, Ibs/hr as C3H8 8.295623 7.631187 

Emissions, Ibs/hr as C 6.787328 6.243698 

SULFUR DIOXIDE 

Concentration, ppm 85.25 77.13 

Emissions, Ibs/hr 7.012816 6.206723 

: 
2 

485.1 

78.24 

15369.3 

8160.6 

489636 

5.13°Jo 

2.50 

17.00 

12:50 PM 

1:53 PM 

49.488 

97.36155 

168.04 

5.980783 

29.59 

1.730175 

122.48 

129.0969 

7.220312 

5.907528 

71.45 

5.812588 

65.60 

56.29141 

1.431065 

3 

487.0. 

78.26 

15372.5 

8053.7 

483223 

6.20% 

2.50 

17.00 

2:20 PM 

3:22 PM 

49.298 

98.27505 

66.29 

57.10798 

1.43281 

0.89 0.35 

0.215143 0.083962 

0.019417 0.007478 

SUMMARY OF EMISSIONS TEST DATA 

Table : 6 

Plant : Daltile, Muskogee, OK 

Location : Trim Kiln Exhaust 

Operator : D. Barrera 

Test Date : 8•Dec•05 

Repetition 

STACK GAS 

Temperature, F 

Velocity, fps 

Volume Flow, acfm 

scfm 

scfh 

Moisture, % 

CO2, o'fo 

02, % 

SAMPLE 

Start Time, hrs:min 11:20 AM 

Finish Time, hrs:min 11:24 AM 

Sample Volume, scf 49.306 

I soki netic Ratio, % 96.81248 

CARBON MONOXIDE 

Concentration, ppm 

Emissions, Ibs/hr 

1 

484.3 

78.48 

15415.3 

8176.6 

490598 

5.30% 

2.50 

17.00 

NITROGEN OXIDE AS NO2 

Concentration, ppm 

Emissions, Ibs/hr 

VOC AS C31-18 

Concentration, ppm as C3H8, WET 

Concentration, ppm as C31-18, DRY 

Emissions, Ibs/hr as C3118 

Emissions, Ibs/hr as C 

SULFUR DIOXIDE 

Concentration, ppm 

Emissions, lbs/hr 

HYDROGEN FLUORIDE 

Sample Weight, mg 

Concentration, ppm 

Emissions, Ibs/hr 

CHLORINE 

Sample Weight, mg 

Concentration, ppm 

Emissions, Ibs/hr 

73.10 

62.96225 

1.603799 

0.48 

0.115733 

0.010465 

HYDROGEN CHLORIDE 

Sample Weight, mg 92.77 92.97 85.60 

Concentration, ppm 43.78239 43.71502 40.40418 

Emissions, Ibs/hr 2.035316 2.028201 1.850039 

2 
III. PROCEDURES 

The procedure for emissions sampling followed USEPA test methods as detailed in Title 

40: Code of Federal Regulations. The following methods were used: 

Method Title 

1 Sample and Velocity Traverses for Stationary Sources 

2 Determination of Stack Gas Velocity and Volumetric Flow Rate (Type S 

Pitot Tube) 

3 Gas Analysis for CO2, 02, Excess Air and Dry Molecular Weight 

5 Determination of Particulate Emissions from Stationary Sources 

6C Determination of Sulfur Dioxide Emissions from Stationary Sources 

(Instrumental Analyzer Procedure) 

7E Determination of Nitrogen Oxides Emissions from Stationary Sources 

(Instrumental Analyzer Procedure) 

10 Determination of Carbon Monoxide Emissions from Stationary Sources 

25A Determination of Total Gaseous Organic Concentration using a Flame 

Ionization Analyzer 

26A Determination of Hydrogen Halides and Halogens Emissions from 

Stationary Sources 

202 Determination of Condensible Particulate Bmissions from Stationary 

Sources 

02 and CO2 were determined using FyRite Analyzers. 

Velocity and volumetric flow rates were determined at each locations as follows: 

~ '^ 

~ , ~ F~~~Y~~~~ ~~ ~~~~ • a~~~e~'~fiA~'o~ ~s'> ~~N ~ ~ ~: ,. . t: " ~N~~~n~~u~ess 

..~r RQiR ~

Spray Dryer 24 12 per traverse 2.5 

Kil.n Scrubber 20 10 per traverse 3.0 

Trim Kiln 12 6 per traverse 5.0 

HF, HCI, and Chlorine sampling was performed for a duration of 60 minutes. The 

sampling train was configured as follows: 

0 
Glass Sampling Nozzle 

Heated Glass Lined Probe 

Heated teflon filter 

Impinger #1 - 100 mis 0.1 N H2SO4 

Impinger #2 - 100 mis 0.1 N H2SO4 

Impinger #3 -100 mis 0.1 N NaOH 

Impinger #4 - 100 rnls 0.1 N NaOH 

Impinger #5 - 200 grams silica Gel 

Analysis for HF and HCl analysis was performed on the solution from the 1 st and 2nd 

impinger. Analysis for C12 was performed on the solution from the 3rd and 4th 

impingers. Analysis was performed using a Dionex LC20 IC/HPLC. 

PM sampling was performed for a duration of 60 minutes. The sampling train was 

configured as follows: 

Stainless Steel Sampling Nozzle 

Heated Glass Lined Probe 

Heated Glass Fiber Filter (Teflon Filter for Trim Kiln) 

Impinger # 1- 100 mis H20 

Impinger #2 - 100 mis H20 

Impinger #3 - 100 mis H20 

Impinger #4 - Empty 

Impinger #5 200 grams silica gel 

"Front-Half 'particulate analysis was performed on the probe wash, prefilter glassware, 

and the filter. "Back-half' particulate anaiysis was performed on the impinger solutions 

and related glassware by Methylene Chloride extractions of the impinger solutions 

(evaporated at room temperature) and total solids in the impinger solutions (evaporated at 

105 degrees C). 

Continuous emissions were monitored for the Spray Dryer as follows: 

r~"✓'?:y ' —P'~~i,~c`.

•~{, r .yi 

_ .~1 r.~?e.4i~Y.1i~~p2..-' 

jT,iy^ ~ ~~+'~ - •~ •-•~;7,~,.

, ~y..si 

~ `r '-'.k~~.`.y,ia - a ~~ '.fi'y ~'1.~ ::;.~t~;4,~i..tx~^~;i7~iLYfili'~~~ 

yf`"y ~ ~Y.q, 

+~ b~-~~ A . I, _ 

Fuji 3300 CO a.nalyzer 0- 100 49.9 ppm, 99.1 ppm CO in N2 

EPA Protocol 1 

EcoPhysics 70S Nox Analyzer 0-60 25.5 ppm, 51.0 ppm Nox in N2 

EPA Protocol 1 

Western Research 721-AT S02 0- 110 50.1 ppm, 101 pprn S02 in N2 

Anal zer EPA Protocol 1- 

ThermoEnvironmental 51 FID 0- 100 28.8 ppm, 48.8 ppm, and 89.2 

analyzer ppm C3H8 in Air EPA Protocol 1 

Continuous emissions were monitored for the Kiln Scrubber as follows: 

11 
,+fT~~ 

YV .'{ 7 ~ 

' d ';: ~^ w 

~.r. .`'f.M ~~ { ~ Y,i l

. 1 - I . 

, 

, -

~ I. 

't .- t Ais - YN L •.1 , _. 

~ ~ •t"' o ~ - ?:*S :t` e, f ~ >..,1 [ i. 1 a i 

Fuji 3300 CO analyzer 0- 500 200 ppm, 494 ppm CO in N2 

EPA Protocol 1 

EcoPhysics 70S Nox Analyzer 0-60 25.5 ppm, 51.0 ppm Nox in N2 

EPA Protocol 1 

Western Research 721-AT S02 0- 110 50.1 ppm, 101 ppm S02 in N2 

Analyzer EPA Protocol 1 

ThenmoEnvironmenta151 FID 0- 100 28.8 ppm, 48.8 ppm, and 89.2 

analyzer ppm C3H8 in Air EPA Protocol 1 

Continuous emissions were monitored for the Trim Kiln as follows: 

;{•f F y'ik' ~~.1 k .7. ~'^f a 4, k- . y•,. - ~'~"'~X ii `t [ ~ i - ~w.1.~ ~a y'Q, 

Fuji 3300 CO analyzer 0- 500 200 ppm, 494 ppm CO in N2 

EPA Protocol 1 

EcoPhysics 70S Nox Analyzer 0-60 25.5 ppm, 51.0 ppm Nox in N2 

EPA Protocol 1 

Westem Research 721-AT S02 0- 110 50.1 ppm, 101 ppm S02 in N2 

Analyzer EPA Protocol 1 

ThermoEnvironmental 51 FID 0- 250 48.8 ppm, 89.2 ppm, and 200 

analyzer ppm C3H8 in Air EPA Protocol I 

Sampling nozzles were measured with a microcaliper onsite prior to sampling. 

The CO analyzer was operated following procedures in Method 6C. No ascai -ite or silica 

gel was using inline of the sample. 

The NOx converter was checked prior to sampling on the Spray Dryer and is documented 

in Appendix B. The trailer was then moved, and another converter check performed for 

both the Kiln Scrubber and Trim Kiln, since the analyzer was not turned off between 

tests. 

Schematics of the sampling locations are shown in Figures 1- 3. The schematic of the 

continuous emission monitor configuration is shown in Figure 4. 

12 
Figure 2 - Kiln Scrubber Zxhaust 

St-ick Diameter - 59.5 inches 

Point #1 -1.5 inches 

Point #2 - 4.9 inches. 

Point #3 - 8.7 inches 

Point #4 - 13.4 inches 

Point #5 - 20.3 inches 

Point #6 - 39.1 inciies 

Point #7 - 46.1 inches 

Point #8 - 50.8 inches 

Point #9 - 54.6 incties 

Point #10 - 58 inches 

r-► 

~ 
Figure 3- Trim Kiin Exhaust 

so1= 

1801, 

1-1 

Ln 

Stack Diameter - 24.5 Inches 

Po'mt #1 -1.1 inches 

Poin# #2 - 3.6 inches 

Poirk #3 - 7.25 inches 

Point #4 -1725 inches 

Poirtt #5 - 20.9 inches 

Point #6 - 23,4 irtches 
Figure 4 - CEM Configuration 

Instack Filter, Heated Probe 

CO Anafyzer 

Heated 

Sampfe Line 

FID Analyaer I NOx Anafyzer 

S02 Anafyaer 

Heated Manifold 

I Sample I I 

To interfernce Train Processor Calibration Poird 

Pump 

1-." 

(31 

Bias Calibration Span l.ine 

\,-,/ Sample processor consists of two short stem impirrgers followed by a 0.3 

puynp micron filter 

EMISSION TEST SUMMARY 

PLANT : Dal;ile, MuskoAee, OK 

DATE : 7-Dec•05 

PLACE : Kiin Scrubber ExN,aust 

RUN# : 1 i4 j~" 

TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 26^.4 

NOZZLE DIAMETER (INCH.) : 0.3127 PARTICULATE WEIGHT (Front half mg) : 0 

METER COEFFICIENT (Y) : 0.989 PARTICULATE WEIGHT (Back half mg) : 0 

PITOT COEFFICIENT (Cp) : 0.84- STATIC PRESSURE (in. H20) : .0.2 

GAS METER VOL.(Cu.Ft.) : 37.828 PERCENT CO2 3 

BAROMETRIC PRESSURE 29.9 PERCENT 02 16 

PERCENT CO 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 59.5 STACK LENGTH(inchs) : 

STACK AREA (Sq.Ft.) : 19.30907 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0.000533 STACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 19.30907 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 39.2473 

VOLUME OF WATER VAPOR (STD. CU .FT.): 12.2570 

FRACTIONAL MOISTURE CONTENT {aJo): 0.2380 

DRY BASE: 81.0000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1200 

MOLECULAR WT. OF STACK GAS (WET BASE): 26.4737 

STACK PRESSURE (inch Hg): 29.8853 

STACK GAS VELOCITY (ft/sec.): 29.0578 

ACTUAL STACK GAS FLOW RATE (ACFM): 33664.7445 

STANDARD STACK GAS FLOW RATE (SCFH): 1356761.65 

ISOKINETIC RATIO (%): 104.8020 

POINTS STACK T. DEL T A P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 137 0.12 0.34641 0.50 38 37 

2 138 0.15 0.387298 0.70 44 38 

3 138 0.17 0.412311 0.80 46 38 

4 138 0.18 0.424264 0.80 47 39 

5 139 0.18 0.424264 0.80 47 39 

6 139 0.19 0.43589 0.90 47 40 

7 139 0.21 0.458258 1.00 47 40 

8 139 0.24 0.489898 1.10 47 40 

9 139 0.28 0.52915 1.30 47 41 

10 138 0.30 0.547723 1.40 48 41 

11 137 0.24 0.489898 1. i 0 44 4 i 

12 139 0.30 0.547723 1.40 46 42 

13 138 0.30 0.547723 1.40 48 42 

14 138 0.29 0.538516 1.30 48 42 

15 138 0.21 0.458258 1.00 48 42 

16 139 0.19 0.43589 0.90 49 413 

17 138 0.20 0.447214 0.90 49 43 

18 138 0.21 0.458258 1.00 51 44 

19 138 0.22 0.469042 1.00 50 ' 4 

20 139 0.21 0.458258 1.00 50 44 

138.3 0.4653 1.0150 47.0500 41.0000 44.0250 

P3 
EMISSION TEST SUMMARY 

PLANT : Daltile, Iviuskogee, CP, 

DATE : 7•Dec•05 

PLACE : Kiln ScrubbEr Exhaust 

RUN# : 2 t4 F 

TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mts) : 26 ~ 

NOZZLE DIAMETER (INCH.) : 0.3127 PARTICULATE WElGHT (Front half mg) : '} 

METER COEFFIClENT (Y) : 0.989 PARTICULATE WEIGHT (Back half mg) 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : •C.?_ 

GAS METER VOL.(Cu.Ft.) : 37.411 PERCENT CO2 . 3 

BAROMETRIC PRESSURE 29.9 PERCENT 02 lo 

PERCENT CO 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 59.5 STACK LENGTH(inches) : 

STACK AREA (Sq.Ft.) : 19.30907 STACK WIDTH(inches) : 

NOZZLE AREA (feet): 0.000533 STACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 19.30907 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 38.9335 

VOLUME OF WATER VAPOR (STD. CU .FT.): 12.5206 

FRACTIONAL MOISTURE CONTENT (%): 0.2433 

DRY BASE: 81.0000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1200 

MOLECULAR WT. OF STACK GAS (WET BASE): 26.4141 

STACK PRESSURE (inch Hg): 29.8853 

STACK GAS VELOCITY (ft/sec.): 29.0622 

ACTUAL STACK GAS FLOW RATE (ACFM): 33669.8511 

STANDARD STACK GAS FLOW RATE (SCFH): 1347205.83 

ISOKINETIC RAT10 (%): 104.7015 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 138 0.25 0.5 1.20 41 41 

2 138 0.27 0.519615 1.20 44 40 

3 139 0.29 0.538516 1.30 45 40 

4 139 0.28 0.52915 1.30 45 40 

5 139 0.25 0.5 1.20 45 40 

6 139 0.20 0.447214 0.96 45 40 

7 139 0.19 0.43589 0.91 45 40 

8 139 0.19 0.43589 0.91 45 40 

9 139 0:21 0.458258 1.00 45 40 

10 138 0.22 0.469042 1.00 4•6 40 

11 137 0.14 0.374166 0.67 43 40 

12 138 0.16 0.4 0.77 44 40 

13 138 0.19 0.43589 0.90 46 40 

14 138 0.20 0.447214 0.96 46 40 

15 139 0.18 0.424264 0.86 46 40 

16 139 0.19 0.43589 0.91 45 /_0 

17 138 0.20 0.447214 0.96 45 40 

18 138 0.22 0.469042 1.00 46 40 

19 138 0.25 0.5 1.20 46 40 

20 138 0.28 0.52915 1.30 46 40 

138.4 0.4648 1.0255 44.9500 40.0500 42.5000 

?4 
EMISSION TEST SUMMARY 

PLANT : Daltile, Miuskogee, OK 

DATE : 7•Dec•05 

PLACE : Kiln Scrubber Exhaust 

RUN# : 3 ~ F 

TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 250.8 

NOZZLE DIAMETER (INCH.) : 0.3127 PARTICULATE WEIGHT (Front half mg) : 0 

METER COEFFICIENT (Y) : 0.989 PARTICULATE WEIGHT (Back half mg) : ;? 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : J.2 

GAS METER VOL.(Cu.Ft.) : 34.996 PERCENT CO2 3 

BAROMETRIC PRESSURE 29.8 PERCENT 02 16 

PERCENT CO 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 59.5 STACK LENGTH(inchs) : 

STACK AREA (Sq.Ft.) : 19.30907 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0.000533 STACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 19.30907 

F'LOWS 

SAMPLED VOLUME (STD. CU .FT.): 36.5833 

VOLUME OF WATER VAPOR (STD. CU .FT.): 11.8052 

FRACTIONAL MOISTURE CONTENT (%): 0.2440 

DRY BASE: 81 .0000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1200 

MOLECULAR WT. OF STACK GAS (WET BASE): 26.4071 

STACK PRESSURE (inch Hg): 29.7853 

STACK GAS VELOCITY (ft/sec.): 29.6653 

ACTUAL STACK GAS FLOW RATE (ACFM): 34368.6052 

STANDARD STACK GAS FLOW RATE (SCFH): 1369993.29 

ISOKINETIC RATIO (aJo): 96.7450 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 135 0.15 0.387298 0.72 40 38 

2 138 0.18 0.424264 0.86 42 38 

3 138 0.18 0.424264 0.86 42 38 

4 139 0.20 0.447214 0.96 43 38 

5 138 0.21 0.458258 1.00 43 38 

6 138 0.21 0.458258 1.00 43 37 

7 138 0.22 0.469042 1.00 42 37 

8 139 0.25 0.5 1.20 42 37 

9 139 0.27 0.519615 1.20 42 37 

10 138 0.30 0.547723 1.40 41 37 

11 138 0.24 0.489898 1.20 39 36 

12 138 0.28 0.52915 1.40 40 36 

13 138 0.30 0.547723 1.40 40 36 

14 138 0.29 0.538516 -1.30 40 36 

15 138 0.26 0.509902 1.20 40 36 

16 139 0.20 0.447214 0.96 39 36 

17 139 0.18 0.424264 0.86 39 36 

18 139 0.18 0.424264 0.86 38 36 

19 138 0.21 0.458258 1.00 38 36 

20 138 0.22 0.469042 1.10 38 36 

138.15 0.4737 1.0740 40.5500 36.7500 38.6500 

?5 
EMISSION TEST SUMMARY 

PLANT : Daltile, Muskogee, OK 

DATE : 7-Dec•05 

PLACE : Kiln Scrubl-,er Exhaust 

RUN# : 1 ?m 

TEST DURATION (MINUTES) : 60 LiQUID COLLECTED (mis) : 268.3 

NOZZLE DIAMETER (lNCH.) : 0.3123 PARTICULATE WEIGHT (Front half mg) : 66.74 

METER COEFFICIENT (Y) : 1.005 PARTICULATE WEIGHT (Back hatf mg) : 4.48 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : •0.2 

GAS METER VOL.(Cu.Ft.) : 37.326 PERCENT CO2 3 

BAROMETRiC PRESSURE 29.9 PERCENT 02 16 

PERCENT CO 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 59.5 STACK LENGTH(inchs) : 

STACK AREA (Sq.Ft.) : 19.30907 STACK WIDTH(inchs) : 

NOZZLE AREA (teet): 0.000532 STACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 19.30907 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 39.1932 

VOLUME OF WATER VAPOR (STD. CU .FT,): 12.6289 

FRACTIONAL MOISTURE CONTENT (V: 0.2437 

DRY BASE: 81.0000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1200 

MOLECULAR WT. OF STACK GAS (WET BASE): 26.4101 

STACK PRESSURE (inch Hg): 29.8853 

STACK GAS VELOCITY (tt/sec.): 29.2447 

ACTUAL STACK GAS FLOW RATE (ACFM): 33881.2229 

STANDARD STACK GAS FLOW RATE (SCFH): 1355016.48 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF): 0.0263 

PARTICULATE CONCENTRATION (LBS/SCF): 3.75E.06 

PARTICULATE EMISSION (LBS/HR): 5.0878 

BACK HALF 

PARTICULATE CONCENTRATION (GR./SCF): 0.0018 

PARTICULATE CONCENTRATION (LBS/SCF): 2.52E•07 

PARTICULATE EMISSION (LBS/HR): 0.3415 

ISOKINETIC RATIO (gb): 105.0612 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 138 0.21 0.458258 0.92 42 40 

2 139 0.20 0.447214 0.88 47 40 

3 138 0.20 0.447214 0.88 47 41 

4 139 0.18 0.424264 0.79 48 41 

5 139 0.17 0.412311 0.75 48 41 

6 139 0.22 0.469042 0.97 48 41 

7 138 0.26 0.509902 1.15 48 42 

8 138 0.28 0.52915 1.20 49 43 

9 139 0.28 0.52915 1.20 49 43 

10 138 0.25 0.5 1.20 49 43 

11 138 0.31 0.556776 1.40 44 43 

12 138 0.29 0.538516 1.30 49 43 

13 139 0.26 0.509902 1.10 50 43 

14 139 0.22 0.469042 0.97 51 44 

15 139 0.20 0.447214 0.88 51 44 

16 138 0.19 0.43589 0.84 51 44 

17 138 0.19 0.43589 0.84 52 45 

18 138 0.19 0.43589 0.84 53 45 

19 138 0.18 0.424264 0.79 54 45 

20 138 0.14 0.374166 0.62 54 46 

138.4 0.4677 0.9710 49.2000 42.8500 46.0250 

Me 
EMISSION TEST SUMMARY 

PLANT : Daltile. Muskogee, OK 

DATE : 7•Dec•05 

PLACE : Kiln Scrubber =xhiust 

RUN3i : 2 p ft) 

TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 

NOZZLE DIAMETER (INCH.) : 0.3123 PARTICULATE WEIGHT (Front half mg) : 

METER COEFFICiENT (Y) : 1.005 PARTICULATE WEIGHT (Back half mg) : 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : 

GAS METER VOL.(Cu.Ft.) : 36.702 PERCENT CO2 

BAROMETRIC PRESSURE 29.9 PERCENT 02 

PERCENT CO 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 59.5 STACK LENGTH(inches) : 

STACK AREA (Sq.Ft.) : 19.30907 STACK WIDTH(inches) : 

NOZZLE AREA (feet): 0.000532 STACK AREA (Sq.Ft.) : 

ENTER THE STACK AREA SHOWN ABOVE: 19.30907 

FLOwS 

SAMPLED VOLUME (STD. CU .FT.): 38.8145 

VOLUME OF WATER VAPOR (STD. CU .FT.): 12.5771 

FRACTIONAL MOISTURE CONTENT 0.2447 

DRY BASE: 81.0000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1200 

MOLECULAR WT. OF STACK GAS (WET BASE): 26.3986 

STACK PRESSURE (inch Hg): 29.8853 

STACK GAS VELOCITY (ft/sec.): 28.7285 

ACTUAL STACK GAS FLOW RATE (ACFM): 33283.2664 

STANDARD STACK GAS FLOW RA T E(SCFH): 1332288.54 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF): 0.0220 

PARTICULATE CONCENTRATION (LBS/SCF): 3.15E•06 

PARTICULATE EMISSION (LBS/HR): 4.1907 

BACK HALF 

PARTICULATE CONCENTRATION (GR./SCF): 0.0053 

PARTICULATE CONCENTRATION (LBS/SCF): 7.60E.07 

PARTICULATE EMISSION (LBS/HR): 1.0127 

ISOKINETIC RATIO (%): 105.8210 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 137 0.29 0.538516 1.30 42 41 

2 137 0.28 0.52915 1.20 46 41 

3 137 0.25 0.5 1.10 45 41 

4 1.37 0.20 0.447214 0.88 45 41 

5 137 0.18 0.424264 0.79 45 41 

6 137 0.17 0.412311 0.74 45 40 

7 138 0.18 0.424264 0.79 45 40 

8 137 0.18 0.424264 0.79 45 40 

9 137 0.17 0.412311 0.75 46 40 

10 136 0.15 0.387298 0.66 45 40 

11 138 0.22 0.469042 0.98 41 40 

12 138 0.21 0.458258 0.92 45 40 

13 137 0.19 0.43589 0.83 45 40 

14 137 0.17 0.412311 0.75 44 40 

15 138 0.18 0.424264 0.79 44 40 

16 137 0.22 0.469042 0.97 45 39 

17 137 0.25 0.5 1.10 44 40 

18 137 0.26 0.509902 1.10 44 40 

19 137 0.28 0,52915 1.20 45 40 

20 135 0.24 0.489898 1.05 45 40 

137.05 0.4599 0.9345 44.5500 40.2000 42.3750 

267.2 

55.37 

13.38 

•0.2 

3 

16 

0 

n 

p 7 
EMISSION TEST SUMMARY 

PLANT : Daltile. Muskogee. OK 

DATE : 7•Dec•05 

PLACE : Kiln Scrubber Exhaus'. 

RUNit : 3 

r 

y~~~ 

TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 264.5 

NOZZLE DIAMETER (INCH.) : 0.3123 PARTICULATE WEIGHT (Front half mg) : 52.8 

METER COEFFICIENT (Y) : 1.005 PARTICULATE WEIGHT (Back half mg) : 8.2 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : •0.2 

GAS METER VOL.(Cu.Ft.) : 38.588 PERCENT CO2 3 

BAROMETRIC PRESSURE 29.8 PERCENT 02 16 

PERCENT CO 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 59.5 STACK LENGTH(inchs) : 

STACK AREA (Sq.Ft.) : 19.30907 - STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0.000532 STACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 19.30907 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 40.9636 

VOLUME OF WATER VAPOR (STD. CU.FT.): 12.4500 

FRACTIONAL MOISTURE CONTENT (gi;): 0.2331 

DRY BASE: 81.0000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1200 

MOLECULAR WT. OF STACK GAS (WET BASE): 26.5281 

STACK PRESSURE (inch Hg): 29.7853 

STACK GAS VELOCITY (ft/sec.): 30.3759 

ACTUAL STACK GAS FLOW RATE (ACFM): 35191.8041 

STANDARD STACK GAS FLOW RATE (SCFH): 1425854.86 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF): 0.0199 

PARTICULATE CONCENTRATION (LBS/SCF): 2.84E•06 

PARTICULATE EMISSION (LBS/HR): 4.0525 

BACK HALF 

PARTICULATE CONCENTRATION (GR./SCF): 0.0031 

PARTICULATE CONCENTRATION (LBS/SCF): 4.41E•07 

PARTICULATE EMISSION (LBS/HR): 0.6294 

ISOKINETIC RATIO (%): 104.3513 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 137 0.23 0.479583 1.00 39 37 

2 137 0.22 0.469042 0.97 41 38 

3 137 0.21 0.458258 0.92 42 37 

4 137 0.19 0.43589 0.83 42 38 

5 137 0.18 0.424264 0.79 42 37 

6 137 0.24 0.489898 0.84 42 37 

7 137 0.27 0.519615 1.20 42 37 

8 137 0.29 0.538516 1.30 42 37 

9 137 0.28 0.52915 1.20 42 37 

10 136 0.25 0.5 1.10 42 37 

11 137 0.30 0.547723 1.30 39 36 

12 137 0.31 0.556776 1.30 40 37 

13 137 0.30 0.547723 1.30 41 37 

14 137 0.25 0.5 1.10 41 36 

15 137 0.23 0.479583 1.00 41 36 

16 137 0.22 0.469042 0.96 41 36 

17 137 0.21 0.458258 0.91 41 36 

18 137 0.21 0.458258 0.91 41 36 

19 137 0.20 0.447214 0.86 41 36 

20 137 0.18 0.424264 0.78 41 36 

136.95 0.4867 1.0285 41.1500 36.7000 38.9250 

• 
EMISSION TEST SUMMARY 

PLANT : Daltile, Muskogee, nK 

DATE : 8-Dec-05 

PLACE : Trim Kiln Exhaust 

RUN# : 1 IK 0 I'" 

TEST DURATION (MINUTES) : 

NOZZLE DIAMETER (INCH.) : 

METER COEFFICIENT (Y) : 

PITOT COEFFICIENT (Cp) : 

GAS METER VOL.(Cu.Ft.) : 

BAROMETRIC PRESSURE 

60 LIQUID COLLECTED (mis) : 

0.2497 PARTICULATE 1NEIGHT (Front half mg) : 

0.989 PARTICULATE WEIGHT (Back half mg) : 

0.84 STATIC PRESSURE (in. H20) : 

47.101 PERCENT CO2 . 

30 PERCENT 02 : 

PERCENT CO 

58.6 

0 

0 

0.38 

2.5 

17 

0 

0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 24.5 STACK LENGTH(inchs) : 

STACK AREA (Sq.Ft.) : 3.273856 STACK WIDTH(inchs) ; 

NOZZLE AREA (feet): 0.00034 STACK AREA (Sq.Ft.) : 

ENTER THE STACK AREA SHOWN ABOVE: 3.273856 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 49.3056 

VOLUME OF WATER VAPOR (STD. CU .FT.): 2.7583 

FRACTIONAL MOISTURE CONTENT (¢Jo}: 0.0530 

DRY BASE: 80.5000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.0800 

MOLECULAR WT. OF STACK GAS (WET BASE): 28.4930 

STACK PRESSURE (inch Hg): 29.9721 

STACK GAS VELOCITY (ft/sec.): 78.4767 

ACTUAL STACK GAS FLOW RATE (ACFM): 15415.2827 

STANDARD STACK GAS FL01N RATE (SCFH): 490598.094 

ISOKINETIC RATIO (%): 96.8125 

POINTS STACK T. DELTA P SQUAR D.P DELTA H 

, 

METER T. 'METER T. 

deg F INLET OUTLET 

1 481 0.87 0.932738 1.30 39 38 

2 486 1.00 1 1.50 44 38 

3 486 1.20 1.095445 1.80 45 39 

4 485 1.20 1.095445 1.80 44 39 

5 486 1.20 1.095445 1.80 44 39 

6 484 1.00 1 1.50 44 40 

7 480 0.84 0.916515 1.20 42 40 

8 485 1.00 1 1.50 45 40 

9 487 1.20 1.095445 1.80 46 40 

10 486 1.20 1.095445 1.80 46 41 

11 485 1.20 1.095445 1.80 46 41 

12 481 1.10 1.048809 1.60 46 41 

484.33333 1.0392 1.6167 44.2500 39.6667 41.9583 

P9 
EMISSION TEST SUMMARY 

PLANT : Daltile, tViuskogee, OK 

DATE : 8-Dec-05 

PLACE : Trim Kiln Exhaust 

RUN# : 2 #0 14r 

TEST DURATION (MINUTES) : 

NOZZLE DIAMETER (INCH.) : 

METER COEFFICIENT (Y) : 

PITOT COEFFICIENT (Cp) : 

GAS METER VOL.(Cu.Ft.) : 

BAROMETRIC PRESSURE . 

60 LIQUID COLLECTED (mis) : 

0.2497 PARTICULATE WEIGHT (Front half mg) 

0.989 PARTICULATE WEIGHT (Back half mg) : 

0.84 STATIC PRESSURE (in. H20) : 

47.601 PERCENT CO2 . 

30 PERCENT 02 

PERCENT CO : 

56.8 

0 

0 

-0.38 

2.5 

17 

0 

0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 24.5 STACK LENGTH(inches) : 

STACK AREA (Sq.Ft.) : 3.273856 STACK WIDTH(inches) : 

NOZZLE AREA (feet): 0.00034 STACK AREA (Sq.Ft.) : 

ENTER THE STACK AREA SHOWN ABOVE: 3.273856 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 49.4880 

VOLUME OF WATER VAPOR (STD. CU .FT.): 2.6736 

FRACTIONAL MOISTURE CONTENT (%): 0.0513 

DRY BASE: 80.5000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.0800 

MOLECULAR WT. OF STACK GAS (WET BASE): 28.5121 

STACK PRESSURE (inch Hg): 29.9721 

STACK GAS VELOCITY (ft/sec.): 78.2426 

ACTUAL STACK GAS FLOW RATE (ACFM): 15369.309 

STANDARD STACK GAS FLOW RATE (SCFH): 489636.299 

ISOKINETIC RATIO (%): 97.3615 

PQINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 470 0.86 0.927362 1.30 43 43 

2 487 1.00 1 1.50 46 43 

3 488 1.20 1.095445 1.80 46 44 

4 488 1.20 1.095445 1.80 46 44 

5 487 1.20 1.095445 1.80 46 45 

6 481 1.00 1 1.50 46 45 

7 484 0.87 0.932738 1.30 45 45 

8 487 1.00 1 1.50 45 45 

9 488 1.20 1.095445 1.80 46 45 

10 488 1.20 1.095445 1.80 48 46 

11 487 1.20 1.095445 1.80 48 46 

12 486 1.00 1 1.50 48 46 

485.08333 1.0361 1.6167 46.0833 44.7500 45.4167 

30 
EMISSION TEST SUMiVIARY 

PLANT : Daltile, Muskogee, OK 

DATE : 8•Dec-05 

PLACE : Trim Kiln Exhaust 

RUN#: 3 ~ 14- 

TEST DURATION (MINUTES) : 

NOZZLE DIAMETER (INCH.) : 

M ETER COEFFICI ENT (Y) ; 

PITOT COEFFICIENT (Cp) : 

GAS METER VOL.(Cu.Ft.) ; 

BAROMETRIC PRESSURE . 

60 LIQUID COLLECTED (mis) : 

0.2497 PARTICULATE WEIGHT (Front half mg) : 

0.989 PARTICULATE WEIGHT (Back half mg) : 

0.84 STATIC PRESSURE (in. H20) : 

47.556 PERCENT CO2 . 

30 PERCENT 02 . 

PERCENT CO : 

69.2 

0 

0 

0.38 

2.5 

17 

0 

~~, 

J 

FOR CIRCU LAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 24.5 STACK LENGTH(inchs) : 

STACK AREA (Sq.Ft.) : 3.273856 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0.00034 STACK AREA (Sq.Ft.) : 

ENTER THE STACK AREA SHOWN ABOVE: 3.273856 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 49.2980 

VOLUME OF WATER VAPOR (STD. CU .FT.): 3.2572 

FRACTIONAL MOISTURE CONTENT 0.0620 

DRY BASE: 80.5000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.0800 

MOLECU LAR WT. OF STACK GAS (WET BASE): 28.3933 

STACK PRESSURE (inch Hg): 29.9721 

STACK GAS VELOCITY (ft/sec.): 78.2589 

ACTUAL STACK GAS FLOW RATE (ACFM): 15372.5021 

STANDARD STACK GAS FL01N RATE (SCFH): 483223.42.5 

ISOKINETIC RATIO (~Jo): 98.2751 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 478 0.88 0.938083 1.30 45 4-6 

2 488 1.00 1 1.50 49 46 

3 489 1.20 1.095445 1.80 50 46 

4 488 1.20 1.095445 1.80 50 46 

5 489 1.10 1.048809 1.70 49 46 

6 486 1.00 1 1.50 48 47 

7 481 0.87 0.932738 1.30 47 47 

8 489 1.00 1 1. 50- 48 46 

9 489 1.20 1.095445 1.80 47 48 

10 490 1.20 1.095445 1.80 46 46 

11 489 1.20 1.095445 1.80 46 45 

12 488 1.00 1 1.50 46 45 

487 1.0331 1.6083 47.5833 46.1667 46.8750 

3, 1 
EMISSION TEST SUMMARY 

PLANT : Daltile, Muskogee, OK 

DATE : 8-Dec-05 

PLACE : Trim Kiln Exhaust 

RUN# : 1 1(J/11 

TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 63.4 

NOZZLE DIAMETER (INCH.) : 0.2507 PARTICULATE WEIGHT (Front half mg) : 30.3 

METER*COEFFICIENT (Y) : 1.005 PARTICULATE WEIGHT (Back half mg) : 26.33 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : •0.38 

GAS METER VOL.(Cu.Ft.) : 47.939 PERCENT CO2 . 2.5 

BAROMETRIC PRESSURE . 30 PERCENT 02 17.5 

PERCENT CO . 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 24.5 STACK LENGTH(inchs) : 

STACK AREA (Sq.Ft.) : 3.273856 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0.000343 STACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 3.273856 

FLOwS 

SAMPLED VOLUME (STD. CU .FT.): 51.2415 

VOLUME OF WATER VAPOR (STD. CU .FT.): 2.9842 

FRACTIONAL MOISTURE CONTENT (%): 0.0550 

DRY BASE: 80.0000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1000 

MOLECULAR WT. OF STACK GAS (WET BASE): 28.4891 

STACK PRESSURE (inch Hg): 29,9721 

STACK GAS VELOCITY (ft/sec.): 79.4271 

ACTUAL STACK GAS FLOW RATE (ACFM): 15601.9783 

STANDARD STACK GAS FLOW RATE (SCFH): 495113.041 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF): 0.0091 

PARTICULATE CONCENTRATION (LBS/SCF): 1.30E•06 

PARTICULATE EMISSION (LBS/HR): 0.6456 

BACK HALF 

PARTICULATE CONCENTRATION (GR./SCF): 0.0079 

PARTICULATE CONCENTRATION (LBS/SCF): 1.13E•06 

PARTICULATE EMISSION (LBS/HR): 0.5610 

ISOKINETIC RATIO (%): 98.9024 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 484 1.10 1.048809 1.60 35 34 

2 488 1.20 1.095445 1.70 40 35 

3 487 1.20 1.095445 1.70 41 36 

4 487 1.20 1.095445 1.70 41 36 

5 488 1.10 1.048809 1.60 42 37 

6 475 0.90 0.948683 1.30 42 37 

7 485 0.95 0.974679 1.40 41 38 

8 486 1.20 1.095445 1.70 42 38 

9 488 1.20 1.095445 1.70 43 38 

10 488 1.20 1.095445 1.70 44 39 

11 485 1.20 1.095445 1.70 44 40 

12 479 0.86 0.927362 1.20 45 40 

485 1.0514 1.5833 41.6667 37.3333 39.5000 

~ r 

.7 ., 
ENlISSION TEST SUMNtARY 

PLANT : Daltile. Muskogee, OK 

DATE : 8•Dec•05 

PLACE : Trim Kiln Exhaust 

RUN# : 2 p o 

TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 60.5 

NOZZLE DIAMETER (INCH.) : 0.2507 PARTICULATE WEIGHT (Front half mg) : 29.31 

METER COEFFICIENT (Y) : 1.005 PARTICULATE WEIGHT (Back half mg) : 24.41 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : •0.38 

GAS METER VOL.(Cu.Ft.) : 47.047 PERCENT CO2 2.5 

BAROMETRIC PRESSURE 30 PERCENT 02 17 

PERCENT CO 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 24.5 STACK LENGTH(inches) : 

STACK AREA (Sq.Ft.) : 3.273856 STACK WIDTH(inches) : 

NOZZLE AREA (feet): 0.000343 STACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 3.273856 

FLowS 

SAMPLED VOLUME (STD. CU .FT.): 49.8598 

VOLUME OF WATER VAPOR (STD. CU .FT.): 2.8477 

FRACTIONAL MOISTURE CONTENT (%): 0.0540 

DRY BASE: 80.5000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.0800 

MOLECULAR WT. OF STACK GAS (WET BASE): 28.4814 

STACK PRESSURE (inch Hg): 29.9721 

STACK GAS VELOCITY (ft/sec.): 77.9556 

ACTUAL STACK GAS FLOW RATE (ACFM): 15312.9267 

STANDARD STACK GAS FLOW RATE (SCFH): 485857.065 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF): 0.0091 

PARTICULATE CONCENTRATION (LBS/SCF): 1.30E•06 

PAR T ICULATE EMISSION (LBS/HR): 0.6298 

BACK HALF 

PARTICULATE CONCENTRATION (GR./SCF): 0.0076 

PARTICULATE CONCENTRATION (LBS/SCF): 1.08E•06 

PARTICULATE EMISSION (LBS/HR): 0.5245 

ISOKINETIC RATlO (%): 98.0689 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 487 1.00 1 1.45 40 40 

2 487 1.20 1.095445 1.70 45 40 

3 488 1.20 1.095445 1.70 46 41 

4 489 1.20 1.095445 1.70 45 41 

5 489 1,00 1 1.45 45 42 

6 475 0.79 0.888819 1.10 45 42 

7 487 1.00 1 1.40 45 43 

8 488 1.20 1.095445 1.70 45 43 

9 489 1.20 1.095445 1.70 47 43 

10 489 1.20 1.095445 1.70 46 43 

11 491 0.98 0.989949 1.40 47 44 

12 475 0.85 0.921954 1.20 47 44 

486.16667 1.0311 1.5167 45.2500 42.1667 43.7083 

`q ~ 
EMISSION TEST SUMMARY 

PLANT : Daltile. Muskogee, OK 

DATE : 8•Dec•0 15 

PLACE : Trim Ki{n Exhaust 

RUN# : 3 p/Yl 

TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 79.7 

NOZZLE DIAMETER (INCH.) : 0.2507 PARTICULATE WEIGHT (Front half mg) : 31.01 

METER COEFFICIENT (Y) : 1.005 PARTICULATE WEIGHT (Back half mg) : 20.19 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : •0.36 

GAS METER VOL.(Cu.Ft.) : 47.487 PERCENT CO2 2.5 

BAROMETRIC PRESSURE 30 PERCENT 02 17 

PERCENT CO 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 24.5 STACK LENGTH(inchs) : 

STACK AREA (Sq.Ft.) : 3.273856 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0.000343 STACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 3.273856 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 50.0569 

VOLUME OF WATER VAPOR (STD. CU .FT.): 3.7515 

FRACTIONAL MOISTURE CONTENT (%): 0.0697 

DRY BASE: 80.5000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.0800 

MOLECULAR WT. OF STACK GAS (WET BASE): 28.3075 

STACK PRESSURE (inch Hg): 29.9735 

STACK GAS VELOCITY (ft/sec.): 79.0460 

ACTUAL STACK GAS FLOW RATE (ACFM): 15527.1052 

STANDARD STACK GAS FLOW RATE (SCFH): 484334.457 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF): 0.0096 

PARTICULATE CONCENTRATION (LBS/SCF): 1.37E•06 

PARTICULATE EMISSION (LBS/HR): 0.6616 

BACK HALF 

PARTICULATE:CONCENTRATION (GR./SCF): 0.0062 

PARTICULATE CONCENTRATION (LBS/SCF): 8.89E•07 

PARTICULATE EMISSION (LBS/HR): 0.4308 

ISOKINETIC RATIO (%): 98.7665 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 487 1.05 1.024695 1.50 43 43 

2 489 1.20 1.095445 1.70 48 44 

3 491 1.20 1.095445 1.70 51 44 

4 491 1.20 1.095445 1.70 51 45 

5 488 1.00 1 1.40 51 45 

6 479 0.85 0.921954 1.20 51 45 

7 480 1.00 1 1.40 48 44 

8 490 1.20 1.095445 1.70 50 44 

9 488 1.20 1.095445 1.70 49 44 

10 490 1.20 1.095445 1.70 48 44 

11 485 1.10 1.048809 1.60 48 44 

12 480 0.88 0.938083 1.30 47 44 

486.5 1.0422 1.5500 48.7500 44.1667 46.4583 

q4 
, 
Surnmary of Suifur Dio.xide A natyzer Calibrations and Bias 

Plant: Daftile, Mus#cogee 

Source: Kitn Scrubber Exhaust 

Date: 12/7I2005 

Anafyzer Caiibratrivn Data 

Cylinder AnaEyzer Absofute °10 Span 

Value Response Difference 

Zero Gas 0 0 0 0 

Mid Range 50.1 49.03 -1.07 -0.97273 

High Range 101 100.25 -0.75 -0.68182 

Run #1 

Systern Cafibration Bias and Driffi Data 

Analyzer fnitial Values Finai Values Drift 

Cafibration .System Systern System System 

Response Calibration Calibration Calibration Calibration 

Response Bias Response Bias 

Zero Gas 0 -0.15 -0.13636- -0.15 -0.13636 0 

Upsca4e 100.25 96.75 -3.18182 96.45 -3.45455 -0.27273 

Average 

Calibration 

Values 

-0.15 

96.6 

Run #2 

Run #3 

Average S42 Concentration: -0.08 

Corrected S02 Concentration: 0.073075 

(Equation 6C-1) 

Zero Gas 0 -0.15 -0.13636 

Upscale 100.25 96.45 -3.45455 

Average S02 Concentration: 0,1 

Con-ected S02 Concentration: 0.224874 

(Equation 6C-1) 

Zero Gas 0 -0.08 -0.07273 

Upscale 100.25 96.45 -3.45455 

-0.08 -0.07273 0.063636 

96.45 -3.45455 0 

0.58 0.527273 0.6 

96.75 -3.181 82 0.272727 

-0.115 

96.45 

0.25 

96.6 

Average S02 Concentration: 0.71 

Corrected S42 Concentration: 0.4822 

(Equation 6C-1) 

760 
Sumrnary of NGx AnaEyzer Caiibrations and Bias 

Piant: Daftiie, Muskogee 

Source: Kiln Scrubber Exhaust 

Date: 12/7/2005 

Ana{yzer Calibratrion Data 

Cylinder Anaiyzer Absolute % Span 

Value P.esponse Difference 

Zero Gas 0 0.08 0.08 0.133333 

Mid Range 25.5 24.7 -0.8 -1.33333 

High Range 51 50.78 -0.22 -0.36667 

System Cafibration B{as and Drift Data 

Analyzer Initial Vafues Final Values Drift Average 

Ca(ibration System System System Systern Calibration 

Response Calibration Calibration Calibration Calibration Vafues 

Response Bias Response Bias 

Run #1 Zero Gas 0.08 0-0.13333 0.3 0.366667 0.5 0.15 

UpscaSe 24.7 22.8 -3.16667 23.5 -2 1.166667 23.15 

Average NOx Concentration: 29.93 

Corrected NOx Concentration: 33.01696 

(Equation 6C-1) 

Run #2 Zero Gas 0.08 0.3 0.366667 0.4 0.533333 0.166667 0.35 

Upscale 24.7 23.5 -2 23.63 -1.78333 0.216667 23.565 

Average NOx Concentration: 30.6 

Corrected NOx Concentration: 33.22744 

(Equation 60-1) 

Run #3 Zero Gas 0.08 0.4 0.533333 0.55 0.783333 0.25 0.475 

Upsca{e 24.7 23.63 -1.78333 23.03 -2.78333 -1 23.33 

Average NOx Concentration: 30.11 

Corrected NOx Concentration: 33.06465 

(Equation 6C-1) 

69 
Summary of CO Anafyzer Catibrations and gias 

Pfant: Daltiie, Mus{%ogee 

Source: Kitn Scrubber Exhaust 

Date: 12/7/2005 

Anatyzer Cafibratrion Data 

Cyfinder Analyzer Absolute % Span 

Value Response Difference 

Zero Gas 0 2.25 2.25 0.45 

Mid Range 200 200.3 0.3 0.06 

High Range 494 488.25 -5.75 -1.15 

System Caiibration Bias and Drift Data 

Analyzer Initial Values Final Va(ues Drift 

Calibration System System Systern System 

Response Calibration Cafibration Calibration Ca(ibration 

Response Bias Response Bias 

Zero Gas 2.25 2.1 -0.03 0.4 -0.37 

Upscale 200.3 188.88 -2.284 179.73 -4.114 

Average CO Concentration: 215.86 

Corrected CO Concentration: 234.476 

(Equation 6C-1) 

Zero Gas 2.25 0.4 -0.37 -0.3 -0.51 

Upscale 200.3 179.73 -4.114 178.78 -4.304 

Average CO Concentration: 206.7 

Corrected CO Concentration: 230.6297 

(Equation 6C-1) 

Zero Gas 2.25 -0.3 -0.51 2 -0.05 

Upsca{e 200.3 178.78- -4.304 180.35- -3.99 

Average CO Concentration: 212.2 

Corrected CO Concentration: 236.5218 

(Equation 6C-1) 

Run #1 

Run #2 

P.un #3 

Average 

Calibration 

Values 

-0.34 1.25 

-1.83 184.305 

-0.14 0.05 

-0.19 179.255 

0.46 0.85 

0.314 179.565 

70 
~ 

(.

;

1.--E 5 c f-,.; k-,b ~ r 

,~ 

!~.' 0 4 ~ 

~ 

G+ , ,. J C, 

 :4.e. r. C~~ C:'. - "r 

DateCFime NOx 

mm/dd/yy hh:mm:ss 1om 

'12/06/05 16:53:03 0.0259$9 Zero PIOx 

72i0610516:54:03 0.061213 

12/0610516:55:03 39.63673 

'12106105 16:56:03 60.6123 51 ppm NOx 

12/06/05 16:57:03 17:0874 

12/06105 16:58:43 34.40918 Siart Convsrter Check 

12/0610516:59:03 34.50684 

12/06/0517:00:03 34.48629 

1210610517:01:03 34.48731 

1210610517:02:03 34.47071 

12/06/0517:03:03 34.4463 

12/06/0517:04:03 34.42872 

12/06l0517:05:03 34.43556 

12/06/0517:06:03 34.39357 

12106/0517:07:03 34.39845 

12/0610517:08:03 34.39064 

1210610517:09:03 34.38478 

12/0610517:10:03 34.39748 

12106/0517:11:03 34.37209 

12/06/0517:12:03 34.36525 

12106/0517:13:03 34.37306 

12106/0517:14:03 34.35842 

1210610517:15:03 34.34768 

1210610517:16:03 34.32424 

1210610517:17:03 34.32912 

1210610517:18:03 34.27444 

12/0610517:19:03 34.27444 

1214610517:20:03 34.29397 

12106l0517:21:03 34.29592 

1210610517:22:03 34.24221 

1210610517:23:03 34.27737 

12l0610517:24:03 34.22659 

12/06/0517:25:03 34.24905 

1 2/06105 1 7:26:03 34.22757 

12/0610517:27:03 34.22754 

12/06/05 17:28:03 34.21094 5top Converler Check 

12l06/0517:29:03 8.681396 

12106/0517:30:03 0.060755 

71 
12/7105 Calibrations 

Date(Time VOC CO NOx S02 

mm/dd/yy hh:mm:ss ppm ppm ppm p )III 

12/07/05 08:51:16 0.1 0.3 0.1 3.1 

12107/05 08:51:26 0.0 0.3 0.1 3.0 

12J07105 08:51:36 0.0 0.3 0.1 3.2 

12107/05 08:51:46 0.0 0.3 0.1 3.2 

12107/05 08:51:56 0.0 0.3 0.0 3.2 

12/07/05 08:52:06 0.3 0.3 0.1 3.2 

12107/05 08:52:16 0.3 0.2 0.0 3.1 

12/07/05 08:52:26 0.3 0.1 27.3 3.2 

12/07/05 08:52:36 0.4 0.2 40.1 3.2 

12107/05 08:52:46 0.4 0.3 40.3 3.3 

12107/05 08:52:56 0.4 0.3 40.4 3.3 

12107/05 08:53:06 0.4 0.3 49.8 3.3 

12/07/05 08:53:16 0.4 0.3 50.8 3.3 

12107/05 08:53:26 0.4 0.3 51.2 3.2 

12/07/05 08:53:36 0.4 0.4 51.5 3.3 

12/07/05 08:53:46 0.4 0.3 51.1 3.3 

12/07105 08:53:56 0.4 0.3 50.8 3.2 

12107/05 08:54:06 0.4 0.3 50.8 3.2 

12/07105 08:54:16 0.4 0.2 50.7 3.2 

12/07/05 08:54:26 0.4 0.2 50.8 3.2 

12/07/05 08:54:36 0.4 0.2 50.8 3.4 

12107/05 08:54:46 0.4 0.2 47.1 3.4 

12/07/05 08:54:56 0.3 0.3 0.5 3.3 

12/07/05 08:55:06 0.1 0.3 0.2 3.2 

12/07105 08:55:16 0.0 0.2 0.1 3.3 

12/07105 08:55:26 0.1 0.2 0.1 3.3 

12/07105 08:55:36 0.3 0.1 0.0 3.2 

12/07105 08:55:46 0.3 0.1 2.0 3.1 

12/07/05 08:55:56 0.3 -0.2 24.2 3.3 

12/07/05 08:56:06 0.3 -0.1 24:5 3.2 

12/07/05 08:56:16 0.3 -0.1 24.7 3.2 

12/07/05 08:56:26 0.3 -0.1 24.6 3.3 

12/07/05 08:56:36 0.3 -0.1 24.7 3.2 

12107/05 08:56:46 0.4 -0.1 24.8 3.2 

12107/05 08:56:56 0.4 -0.1 24.7 3.1 

12107/05 08:57:06 0.3 0.2 10.2 3.1 

12/07/05 08:57:16 0.4 0.2 0.2 3.1 

12107/05 08:57:26 0.1 0.1 0.1 3.1 

12107105 08:57:36 0.0 0.1 0.1 3.1 

12107105 08:57:46 0.0 0.1 0.1 3.1 

12107/05 08:57:56 0.0 0.2 0.1 3.2 

12/07/05 08:58:06 0.0 0.1 0.1 3.1 

12/07105 08:58:16 0.0 0.0 0.1 3.1 

12J07/05 08:58:26 0.2 0.1 0.1 3.1 

12/07/05 08:58:36 0.3 1.2 0.1 3.1 

12/07/05 08:58:46 0.3 2.2 0.1 3.0 

12107/05 08:58:56 0.3 2.1 0.1 3.0 

12107/05 08:59:06 0.3 2.4 0.1 3.1 

12/07106 08:59:16 0.3 2.4 0.1 3.0 

12/07/05 08:59:26 0.3 2.4 0.0 3.1 

12/07/05 08:59:36 0.3 86.9 0.1 3.0 

12/07/05 08:59:46 0.3 191.4 0.0 3.1 

12/07/05 08:59:56 0.3 193.3 0.0 3.1 

12/07/05 09:00:06 0.3 193.5 0.0 3.1 

12107/05 09:00:16 0.3 196.3 0.0 3.0 

12107105 09:00:26 0.3 197.2 0.0 1.2 

12107/05 09:00:36 0.3 197.1 0.0 -0.1 

12/07/05 09:00:46 0.3 198.7 0.0 0.0 

12/07105 09:00:56 0.3 198.1 0.0 0.0 

12/07/05 09:01:06 0.3 199.3 0.0 0.0 

12/07/05 09:01:16 0.3 200.1 0.0 0.0 

12107/05 09:01:26 0.3 200.2 0.0 0.0 

12/07105 09:01:36 0.3 200.5 0.0 0.0 

12107/05 09:01:46 0.3 200.2 -0.1 0.0 

12/07105 09:01:56 0.3 200.3 0.0 -0.1 

12/07/05 09:02:06 0.3 103.2 0.0 -0.1 

12/07/05 09:02:16 0.2 4.4 0.1 -0.1 

12/07/05 09:02:26 0.0 2.7 0.0 0.0 

12/07/05 09:02:36 0.0 2.3 0.0 0.0 

51 ppm NOx 

25.5 ppm NOx 

200 ppm CO 

Zero S02 

! 4. 

Page 1 
1217/05 Calibrations 

12/07105 09:02:46 0.2 2.3 0.0 0.0 

12/07/05 09:02:56 0.3 2.4 0.0 -0.1 

12/07/05 09:03:06 0.3 2.2 0.0 -0.1 

12107/05 09:03:16 0.3 123.6 0.1 -0.1 

12/07105 09:03:26 0.4 470.1 0.0 -0.1 

12/07/05 09:03:36 0.4 486.2 0.0 -0.1 

12107/05 09:03:46 0.3 486.8 0.0 -0.1 

12/07/05 09:03:56 0.3 487.0 0.0 -0.1 

12/07/05 09:04:06 0.3 487.3 0.0 -0.1 

12/07/05 09:04:16 0.3 488.1 0.0 -0.1 

12107/05 09:04:26 0.3 488.2 0.0 -0.1 

12107105 09:04:36 0.3 488.2 0.0 -0.1 494 ppm CO 

12/07/05 09:04:46 0.3 488.2 0.0 -0.1 

12/07/05 09:04:56 0.3 488.4 0.0 -0.1 

12/07/05 09:05:06 0.4 336.9 0.0 -0.1 

12107/05 09:05:16 0.3 14.7 0.0 -0.1 

12/07/05 09:05:26 0.1 3.7 0.1 -0.1 

12107/05 09:05:36 0.0 3.3 0.1 0.0 

12107105 09:05:46 0.0 3.2 0.1 -0.1 

12/07/05 09:05:56 0.0 3.3 0.1 -0.1 

12/07/05 09:06:06 0.0 3.3 0.0 0.0 

12107105 09:06:16 0.0 3.2 0.1 0.0 

12/07105 09:06:26 0.0 3.1 0.1 -0.1 

12J07/05 09:06:36 0.0 3.0 0.1 -0.1 

12/07/05 09:06:46 0.0 3.0 0.1 0.0 

12/07/05 09:06:56 0.1 2.9 0.1 -0.1 

12/07/05 09:07:06 0.2 2.8 0.1 -0.1 

12107/05 09:07:16 0.3 2.4 0.1 -0.1 

12/07/05 09:07:26 0.3 2.4 0.1 -0.1 

12J07/05 09:07:36 0.4 2.0 0.1 4.8 

12/07/05 09:07:46 0.4 1.9 0.4 27.0 

12/07/06 09:07:56 0.3 2.0 0.4 42.4 

12/07/05 09:08:06 0.3 2.1 0.4 47.7 

12/07/05 09:08:16 0.4 2.6 0.3 49.4 

12107/05 09:08:26 0.4 2.6 0.3 49.9 

12/07/05 09:08:36 0.4 2.7 0.4 50.0 

12/07/05 09:08:46 0.4 2.6 0.4 50.1 

12107/05 09:08:56 0.3 2.6 0.3 50.2 

12107/05 09:09:06 0.3 2.7 0.4 50.2 

12/07/05 09:09:16 0.5 2.5 0.3 50.2 

12/07/05 09:09:26 0.6 2.4 0.3 50.3 

12/07/05 09:09:36 0.6 2.2 0.3 50.3 

12/07/05 09:09:46 0.6 2.0 0.3 50.4 

12/07/05 09:09:56 0.6 1.9 0.3 49.8 

12/07106 09:10:06 0.6 2.1 0.3 49.0 

12/07/05 09:10:16 0.5 2.1 0.3 49.0 50.1 ppm S02 

12/07/05 09:10:26 0.5 2.4 0.3 49.0 Zero CO 

12107/05 09:10:36 0.6 2.4 0.4 49.1 

12/07/05 09:10:46 0.5 2.3 0.3 49.2 

12/07105 09:10:56 0.5 2.6 0.3 46.0 

12/07/05 09:11:06 0.5 2.6 0.0 25.6 

12/07/05 09:11:16 0.0 2.6 0.1 9.0 

12/07/05 09:11:26 0.1 2.6 0.1 3.0 

12107/05 09:11:38 0.0 2.8 0.1 1.1 

12107105 09:11:46 0.4 2.6 0.1 0.4 

12/07/05 09:11:56 0.5 2.5 0.1 0.2 

12/07/05 09:12:06 0.6 2.5 0.1 1.1 

12/07/06 09:12:16 0.6 2.1 0.0 29.7 

12/07/05 09:12:26 0.6 2.3 0.0 71,8 

12/07/05 09:12:36 0.6 2.2 0.0 91.8 

12/07/05 09:12:46 0.6 2.2 0.0 97.6 

12/07/05 09:12:56 0.7 2.2 0.0 99.0 

12107/05 09:13:06 0.7 2.2 0.0 99.5 

12/07/05 09:13:16 0.6 2.4 0.0 99.7 

12/07/05 09:13:26 0.6 2.4 0.0 99.9 

12/07/05 09:13:36 0.6 2.3 0.0 99.9 

12/07/05 09:13:46 0.6 2.5 0.0 100.0 

12/07/05 09:13:56 0.6 2.4 0.0 100.1 

12/07/05 09:14:06 0.6 2.5 0.0 100.0 

12/07/05 09:14:16 0.6 2.6 0.0 100.1 

12/07105 09:14:26 0.6 2.8 0.0 100.2 

12/07/05 09:14:36 0.6 2.8 0.0 100.3 101 ppm S02 

7 .3 

Page 2 
1217/05 Calibrations 

12/07/05 09:14:46 0.6 2.5 0.0 100.3 

12/07/05 09:14:56 0.7 2.6 0.0 100.2 

12/07105 09:15:06 0.7 2.6 0.0 100.2 

12107/05 09:15:16 0.6 3.1 0.0 94.1 

12/07/05 09:15:26 0.6 3.3 0.0 53.8 

12107/05 09:1 b:36 0.6 3.1 0.1 19.4 

12/07/05 09:15:46 0.6 3.1 0.0 6.1 

12/07/05 09:15:56 0.6 3.0 0.0 2.2 

12/07/05 09:16:06 0.6 3.0 0.0 1.1 

12/07/05 09:16:16 0.6 2.8 0.1 0.7 

12/07/05 09:16:26 0.6 2.9 0.0 0.4 

12/07/05 09:16:36 0.6 2.9 0.0 0.2 

12107105 09:16:46 0.6 2.9 0.0 0.2 

12/07/05 09:16:56 0.6 3.0 0.0 0.1 

12/07/05 09:17:06 0.6 2.8 0.0 0.0 

12/07/05 09:17:16 0.6 2.8 0.1 0.0 

12107/05 09:17:26 0.6 2.7 0.1 0.0 

12107/05 09:17:36 0.7 2.6 0.1 0.0 

12/07/05 09:17:46 0.7 2.6 0.1 0.0 

12107/05 09:17:56 0.7 2.6 0.1 0.0 

12/07/05 09:18:06 0.6 2.6 0.1 -0.1 

12107/05 09:18:16 0.6 2.4 0.1 -0.2 

12/07/05 09:18:26 0.6 2.3 0.1 -0.2 

12107/05 09:18:36 0.6 2.2 0.1 -0.1 

12107/05 09:18:46 0.6 2.5 0.1 -0.1 

12107105 09:18:56 0.6 2.6 0.1 '-0.2 

12/07105 09:19:06 0.6 2.6 0.1 -0.2 

12/07105 09:19:16 0.6 2.8 0.1 -0.1 

12/07/05 09:19:26 0.2 2.5 0.0 -0.1 

12/07105 09:19:36 0.0 2.5 0.1 -0.1 

12/07105 09:19:46 0.0 2.2 0.3 0.0 

12107/05 09:19:56 0.0 2.1 4.5 0.3 

12/07/05 09:20:06 0.0 2.0 9.1 0.5 

12/07/05 09:20:16 0.0 2.0 13.3 0.5 

12/07/05 09:20:26 0.0 2.1 16.2 0.3 

12/07/05 09:20:36 0.0 2.0 17.9 0.1 

12107105 09:20:46 0.0 2.1 19.0 0.0 

12107/05 09:20:56 0.0 2.2 19.5 -0.1 

12/07/05 09:21:06 0.0 2.3 19.8 -0.1 

12/07/05 09:21:16 0.0 2.2 19.9 -0.2 

12/07/05 09:21:26 0.1 2.4 20.0 -0.2 

12107/05 09:21:36 0.0 2.3 20.0 -0.3 

12107105 09:21:46 0.0 2.3 20.4 -0.3 

12107/05 09:21:56 0.0 2.2 21.2 -0.3 

12107/05 09:22:06 0.0 2.2 21.8 -0.2 

12/07/05 09:22:16 0.0 2.1 22.3 -0.2 

12107/05 09:22:26 0.1 2.1 22.5 -0.2 

12/07/05 09:22:36 0.1 2.1 22.6 -0.2 

12l07105 09:22:46 0.1 2.2 22.7 -0.2 

12/07/05 09:22:56 0.1 2.3 22.7 -0.2 

12/07/05 09:23:08 0.1 2.3 22.7 -0.2 

12/07/05 09:23:16 0.1 2.2 22.8 -0.2 

12107/05 09:23:26 0.0 2.2 22.8 -0.2 25.5 ppm NOx bias 

12107/05 09:23:36 0.0 2.0 22.8 -0.1 Zero CO. S02 Bias 

12/07/05 09:23:46 0.0 2.1 22.8 -0.1 

12/07/05 09:23:56 0.1 2.2 22.7 -0.1 

12/07/05 09:24:06 0.5 2.1 22.5 -0.2 

12/07/05 09:24:16 0.6 2.0 22.2 -0.1 

12107/05 09:24:26 0.6 1.9 20.7 -0.1 

12107105 09:24:36 0.4 2.0 16.7 -0.1 

12/07/05 09:24:46 0.0 1.8 9.2 -0.1 

12/07/05 09:24:56 0.0 2.0 4.2 0.1 

12107/05 09:25:06 0.0 1.8 1.8 6.5 

12/07/05 09:25:16 0.1 1.6 1.0 22.4 

12107105 09:25:26 0.0 1.6 0.6 40.1 

12/07/05 09:25:36 1.4 1.3 0.4 55.3 

12/07/05 09:25:46 0.1 1.5 0.2 66.9 

12/07/05 09:25:56 0.0 1.8 0.1 75.8 

12/07105 09:26:06 0.0 1.8 0.0 81.9 

12107/05 09:26:16 0.0 2.3 0.0 86.0 

12/07/05 09:26:26 0.0 2.4 0.0 88.5 

12/07/05 09:26:36 0.0 2.6 0.0 90.0 

12107/05 09:26:46 0.0 2.7 0.0 91.1 

74 

Page 3 
1217105 Cafibrations 

12J07/05 09:26:56 0.0 2.6 0.0 92.1 

12107/05 09:27:06 0.0 2.1 0.0 92.7 

12/07/05 09:27:16 0.0 2.1 0.0 93.0 

12107105 09:27:26 0.0 2.1 0.0 93.3 

12/07/05 09:27:36 0.0 2.1 0.0 93.6 

12107105 09:27:46 0.0 2.1 0.0 94.0 

12/07105 09:27:56 0,0 2.2 0.0 94.4 

12107/05 09:28:06 0.0 2.6 0.0 94.6 

12/07/05 09:28:16 0.0 2.5 0.0 95.3 

12/07/05 09:28:26 0.0 2.5 0.0 96.4 

12/07/05 09:28:36 0.0 2.5 0.0 96.6 

12/07/05 09:28:46 0.0 2.6 0.0 96.7 

12107l05 09:28:56 0.0 2.6 0.0 96.7 

12/07/05 09:29:06 0.0 2.4 0.0 96.8 

12/07/05 09:29:16 0.0 2.1 0.0 96.8 

12/07105 09:29:26 0.6 1.8 0.0 95.8 

12107/05 09:29:36 0.9 1.9 0.0 94.2 

12/07/05 09:29:46 1.0 2.0 0.0 92.5 

12107/05 09:29:56 1.1 2.1 0.0 86.7 

12/07/05 09:30:06 1.1 2.3 0.0 71.9 

12107/05 09:30:16 0.6 2.2 0.1 51.8 

12107105 09:30:26 0.2 2.7 0.1 34.0 

12107105 09:30:36 0.1 24.5 0.1 22.6 

12/07/05 09:30:46 0.1 73.3 0.1 15.4 

12107l06 09:30:56 0.0 110.9 0.0 11.0 

12/07105 09:31:06 0.0 135.8 0.0 8.0 

12/07105 09:31:16 0.1 152.9 0.0 6.1 

12/07/05 09:31:26 0.0 166.4 0.0 4.6 

12107/05 09:31:36 0.0 175.2 0.0 3.6 

12107/05 09:31:46 0.0 180.2 0.0 2.8 

12/07/05 09:31:56 0.1 182.8 0.0 2.3 

12/07/05 09:32:06 0.0 184.6 0.0 1.8 

12/07105 09:32:16 0.0 185.9 0.0 1.4 

12/07/05 09:32:26 0.1 187.0 0.0 1.3 

12/07/05 09:32:36 0.0 187.8 0.0 1.2 

12/07/05 09:32:46 0.0 188.2 0.0 1.0 

12l07105 09:32:56 0.0 188.7 0.0 0.8 

12/07/05 09:33:06 0.0 188.8 0.0 0.8 

12107/05 09:33:16 0.0 188.7 0.0 0.8 

12107105 09:33:26 0.0 188.9 0.0 0.7 

12/07/05 09:33:36 0.1 189.1 0.0 0.6 

12107105 09:33:46 0.2 187.4 0.0 0.6 

12/07/05 09:33:56 0.8 185.3 0.0 0.6 

12/07/05 09:34:06 1.0 181.2 0.0 0.5 

12107/05 09:34:16 1.1 168.8 0.0 0.5 

12J07105 09:34:26 13.6 133.9 0.0 0.4 

12107/05 09:34:36 46.5 80.1 0.0 0.6 

12/07/05 09:34:46 47.0 42.1 0.1 1.2 

12/07105 09:34:56 47.0 21.3 0.1 1.6 

12/07/05 09:35:06 47.0 13.6 0.0 1.6 

12/07105 09:35:16 48.2 9.1 0.0 1.3 

12/07/05 09:35:26 48.7 6.3 0.0 1.0 

12/07/05 09:35:36 48.7 5.1 0.0 0.8 

12/07/05 09:35:46 48.8 4.2 0.0 0.5 

12/07/05 09:35:56 48.8 3.8 0.0 0.4 

12/07/05 09:36:06 48.8 3.7 0.0 0.3 

12107/05 09:36:16 47.1 3.0 0.0 0.1 

12107/05 09:36:26 9.4 2.6 0.0 0.0 

12/07/05 09:36:36 1.2 2.3 0.0 0.0 

12107/05 09:36:46 1.2 2.4 0.0 0.0 

12107/05 09:36:56 2.1 2.4 0.0 0.0 

12107/05 09:37:06 26.6 2.3 0.0 0.1 

12/07/05 09:37:16 28.7 2.3 0.0 0.3 

12107/05 09:37:26 28.6 2.3 0.1 0.6 

12/07/05 09:37:36 28.7 2.4 0.0 0.7 

12/07/05 09:37:46 28.7 2.6 0.0 0.7 

12107/05 09:37:56 28.5 2.5 0.0 0.5 

12/07105 09:38:06 27.9 2.5 0.0 0.2 

12107/05 09:38:16 8.7 2.6 0.0 0.1 

12/07/05 09:38:26 1.2 2.5 0.0 0.1 

12/07/05 09:38:36 1.2 2.3 0.0 0.0 

101 ppm S02 Bias 

Zero NOx Bias 

200 ppm CO Bias 

Zero VOC 

48.8 ppm C31-18 

28.8 ppm C3H8 

75 

Page 4 
1217/05 CaliSratfons 

12/07105 09:38;46 1.2 2.4 0.0 0.0 

12/07/05 09:38:56 27.9 2.4 0.0 0.0 

12/07/05 09:39:06 89.5 2.5 0.1 0.1 

12107105 09:39:16 90.3 2.4 0:1 0.3 

12107/05 09:39:26 90.4 2.5 0.1 0.5 

12107l05 09:39:36 90.7 2.6 0.1 0.4 

12/07/05 09:39:46 90.8 2.4 0.1 0.4 

12107/05 09:39:56 90.7 2.2 0.1 0.3 

12/07105 09;40:06 90.9 2.4 0.1 0.2 

12/07/05 09:40:16 90.9 2.0 0.1 0.0 

12/07/05 09:40:26 90.0 1.7. 0.1 0.0 

12/07105 09:40:36 39.3 1.7 0.0 -0.1 

12J07/05 09:40:46 1:5 1.8 0.0 -0.1 

12/07/05 09:40:56 1.3 1.6 0.0 -0.1 

89.2 ppm C3H8 

• 76 

Page 5 
12/7/05 Run #1 

Date/Time VOC CO NOx S02 

mm/dd/yy hh:mm:ss ppm ppm ppm ppm 

12/07/0510:09:47 54.6 219.9 29.3 0.4 

12/07/0510:09:57 53.7 220.9 29.3 0.3 

Start Run #1 

12/07/0510:10:07 53.5 221.9 29.2 0.2 

12107/0510:10:17 53.7 223.0 29.3 0.3 

12/07/0510:10:27 52.9 223.8 29.3 0.2 

12/07/0510:10:37 53.3 223.9 29.3 0.1 

12107/0510:10:47 52.8 224.1 29.4 0.1 

12107/0510:10:57 52.5 224.4 29.4 0.2 

1210710510:11:07 52.5 224.5 29.2 0,2 

12/07/0510:11:17 52.7 223.8 . 29.2 0.2 

12/07/0510:11:27 52.3 223.8 29.3 0.2 

12107/0510:11:37 51.2 223.6 29.3 0.2 

12107/0510:11:47 50.8 223.3 29.1 0.2 

12/07/0510:11:57 51.7 222.7 29.0 0.2 

12107/0510:12:07 52.6 222.2 28.9 0.2 

12/0710510:12:17 52.4 222.2 28.7 0.2 

12/07/0510:12:27 52.1 222.0 28.6 0.1 

1210710510:12:37 52.3 221.9 28.6 0.2 

1210710510:12:47 52.2 221.8 . 28.6 0.1 

12/0710510:12:57 53.0 222.1 28.6 0.1 

12/07/06 10:13:07 52.7 222.6 28.5 0,1 

12/07/0510:13:17 51.8 223.6 28.5 0.0 

12/0710510:13:27 52.4 224.6 28.6 0.0 

12107/0510:13:37 51.6 225.3 28.5 0.1 

12107/0510:13:47 52.0 225.3 28.4 0.1 

12107/0510:13:57 51.1 225.3 28.3 0.1 

120710510:14:07 51.3 225.1 28.2 0.1 

1210710510:14:17 51.5 225.0 28.3 0.1 

12/07/0510:14:27 51.0 224.7 28.6 0.1 

12/0710510:14:37 50.9 224.6 28.6 0.1 

1210710510:14:47 50.4 225.1 28.8 0.1 

12/07/0510:14:57 50.9 225.3 29.0 0.2 

12107/0510:15:07 50.1 225.8 29.1 0,2 

12107/0510:15:17 50.1 226.1 29.1 0.1 

12107/0510:15:27 50.2 226.6 29.1 0.1 

1 2107105 1 0:15:37 50.5 227.1 29.0 0.1 

1210710510:15:47 50.0 227.1 29.0 0.1 

12107/0510:15:57 50.8 227.1 29.0 0.1 

12/07/0510:16:07 49.9 227.1 29.1 0.1 

1210710510:16:17 49.5 226.7 29.1 0.1 

12/07/0510:16:27 49.9 226.5 29.1 0.1 

12107/0510:16:37 49.3 225.9 29.2 0.1 

1210710510:16:47 49.2 225.7 29.3 0.1 

1210710510:16:57 49.5 225.3 29.4 0.1 

12/0710510:17:07 49.3 224.8 29.5 0.1 

12107/0510:17:17 48.5 224.1 29.5 0.1 

12107/0510:17:27 48.1 223.6 29.3 0.1 

12107/0510:17:37 47.9 223.4 29.3 0.0 

12/07/0510:17:47 48.1 223.6 29.1 0.0 

1210710510:17:57 47.4 223.4 29.0 0.0 

12/07/0510:18:07 47.6 223.0 28.8 0.0 

12/07/0510:18:17 47.9 222.3 28.7 0.0 

12/07/0510:18:27 48.1 221.4 28.6 0.0 

12107/0510:18:37 48.0 221.0 28.5 0.1 

1210710510:18:47 47.9 221.0 28.8 0.1 

12/07/0510:18:57 48.4 221.2 28.8 0.1 

12/0710510:19:07 48.3 221.7 29.1 0.1 

12/0710510:19:17 48.4 222.3 29.2 0.1 

1 2107/05 1 0:19:27 48.3 223.3 29.2 0.2 

12/07/0510:19:37 47.9 224.4 29.3 0.1 

12/07/0510:19:41 48.5 224.8 29.3 0.1 

12/07/0510:19:57 48.3 224.8 29.3 0.1 

12/07/0510:20:07 48.4 224.8 29.3 0.1 

1210710510:20:17 48.6 224.8 29.3 0.1 

12107/0510:20:27 48.2 224.7 29.4 0.1 

12107/0510:20:37 48.3 224.5 29.5 0.1 

12/0710510:20:47 48.3 224.3 29.6 0.1 

12107/0510:20:57 48.5 224.2 29.7 0.1 

1 2107/05 1 0:21:07 48.9 223.9 29.7 0,1 

12107/0510:21:17 49.1 224.0 29.8 0.1 

7 • ~ 

7 

Page 1 
1217/05 Run #1 

12/0710510:21:27 49.1 224.1 29.8 0.1 

12/07/0510:21:37 49.0 224.9 29.8 0.1 

12/07/0510:21:47 48.8 224.9 29.9 0.0 

12/07/0510:21:57 49.6 224.9 29.9 0.0 

1210710510:22:07 49.2 224.6 29.9 0.0 

12107/0510:22:17 49.1 224.2 29.9 0.1 

12107/0510:22:27 49.8 223.8 30.0 0.1 

12/0710510:22:37 50.0 223.2 30.0 0.1 

12/07/0510:2247 50.4 223.2 30.0 0.1 

12/07/0510:22:57 50.7 222.8 29.9 0.1 

12107/0510:23:07 51.4 222.8 29.8 0.1 

12/07/0510:23:17 52.1 222.8 29.7 0.1 

12/0710510:23:27 52.5 223.3 29.5 0.0 

12/0710510:23:37 53.1 224.1 29.4 010 

12/07/0510:23:47 52.9 224.5 29.0 0.0 

12/07/0510:23:57 53.0 225.2 28.7 0.0 

12/07/0510:24:07 53.4 225.9 28.5 0.0 

12107/0510:24:17 54.1 226.7 28.4 0.0 

12/07/0510:24:27 53.2 227.3 28.3 0.0 

12/07/0510:24:37 53.3 227.5 28.2 0.0 

1210710510:24:47 53.4 227.8 28.3 0.0 

1210710510:24:57 53.1 228.0 28.3 0.0 

12/0710510:25:07 52.5 228.4 28.6 -0.1 

12/07/0510:25:17 52.1 228.6 28.8 -0.1 

1210710510:25:27 51.7 229.3 29.0 -0.1 

1210710510:25:37 50.8 229.5 29.2 -0.1 

12107/0510:25:47 49.9 229.4 29.2 -0.1 

12107/0510:25:57 48.7 229.2 29.1 -0.1 

12/07/0510:26:07 48.2 228.9 29.1 -0.2 

12107/0510:26:17 48.4 228.0 29.1 -0.2 

12107/0510:26:27 47.1 226.9 29.2 -0.1 

12/07/0510:26:37 47.3 226.5 29.3 -0.1 

1210710510:26:47 46.8 225.7 29.4 -0.2 

1210710510:26:57 46.6 225.3 29.6 -0.1 

1210710510:27:07 46.5 224.7 29.7 -0.1 

1210710510:27:17 46.7 224.1 29.7 -0.1 

1210710510:27:27 46.8 223.8 29.8 -0.1 

1210710510:27:37 47.1 224.0 29.9 -0.1 

12/0710510:27:47 46.9 223.9 29.9 0.0 

1210710510:27:57 46.2 223.4 30.1 0.0 

12/0710510:28:07 46.2 222.8 30.2 0.0 

12/0710510:28:17 46.2 221.7 30.1 0.0 

12/0710510:28:27 46.4 220.6 30.0 -0.1 

12/0710510:28:37 46.1 220.0 30.1 -0.1 

12/0710510:28:47 46.3 219.4 30.1 -0.1 

12107/0510:28:57 48.4 218.8 30.1 -0.2 

12/0710510:29:07 46.7 218.4 30.1 -0.2 

12/0710510:29:17 47.0 217.9 30.1 -0.2 

12/07/0510:29:27 47.0 217.6 30.2 -0.2 

12107/0510:29:37 47.4 217.6 30.3 -0.1 

12/07/0510:29:47 47.1 217.3 30.2 -0.1 

12107/0510:29:57 46.5 217.4 30.2 -0.2 

12/07/0510:30:07 46.6 217.5 30.2 -0.2 

12107/0510:30:17 47.1 217.3 30.2 -0.2 

12/07/0510:30:27 47.5 217.0 30.2 -0.2 

12/07/0510:30:37 47.7 216.9 30.1 -0.3 

12/07/0510:30:47 48.0 216.6 30.3 -0.2 

12/07/0510:30:57 47.9 216.4 30.3 -0.2 

12/07/0510:31:07 47.7 216.2 30.3 -0.2 

12107/0510:31:17 47.6 216.0 30.3 -0.2 

12/07/0510:31:27 47.2 215.6 30.3 -0.2 

12/0710510:31:37 47.1 215.1 30.4 -0.2 

12107/0510:31:47 46.8 .215.0 30.3 -0.1 

1210710510:31:57 46.9 215.0 30.3 -0.2 

1210710510:32:07 46.7 214.9 30.3 -0.3 

12/07/0510:32:17 46.9 214.9 30.2 -0.3 

12107/0510:32:27 46.6 214.5 30.2 -0.2 

1 2107/05 1 0:32:37 47.0 214.2 30.2 -0.3 

12107/0510:32:47 46.6 214.3 30.1 -0.2 

12/07/0510:32:57 46.8 214.9 30.1 -0.2 

12/0710510:33:07 46.7 215.6 30.1 -0.3 

12/07/0510:33:17 46.5 215.9 30.1 -0.3 

12/07/0510:33:27 46.4 216.4 30.1 -0.3 

12/07/0510:33:37 46.4 216.4 30.1 -0.3 

Page 2 78 
12/7/05 Run #1 

12/07/0510:33:47 46.6 216.2 30.1 -0.2 

12/07/0510:33:57 46.9 215.9 30.1 -0.3 

12/07/0510:34:07 46.9 216.6 30.0 -0.4 

12/07/0510:34:17 46.3 215.4 30.1 -0.3 

12/07/0510:34:27 46.3 215.3 30.1 -0.4 

12/0710510:34:37 46.1 215.3 30.2 -0.4 

12J07/0510:34:47 46.1 215.4 30.1 -0.3 

12/07/0510:34:57 45.5 215.7 30.1 -0.3 

12/07/0510:35:07 45.5 216.3 30.2 -0.3 

12/07/0510:35:17 45.8 216.5 30.2 -0.3 

12/07/0510:35:27 45.8 217.0 30.2 -0.2 

1210710510:35:37 46.3 217.4 30.3 -0.3 

12107/0510:35:47 45.7 217.6 30.3 -0.3 

12107/0510:35:57 45.9 217.6 30.3 -0.3 

12/07/0510:36:07 45.2 217.6 30.2 -0.3 

1210710510:36:17 45.7 218.0 30.1 -0.3 

12/07/0510:36:27 45.9 217.7 30.1 -0.3 

12107/0510:36:37 45.6 217.6 29.9 -0.4 

12107/0510:36:47 45.6 217.9 29.9 0.0 

12107/0510:36:57 45.6 217.8 29.8 0.0 

12/0710510:37:07 45.7 218.1 29.8 0.0 

12/0710510:37:17 45.5 218.2 29.9 -0.1 

12/07/0510:37:27 45.1 218.3 29.8 -0.1 

12107/0510:37:37 461 217.8 29.8 -0.1 

12/07/0510:37:47 45.7 217.7 30.0 -0.1 

12/07/0510:37:57 45.7 217.2 29.9 -0.1 

12/0710510:38:07 46.0 216.9 29.9 -0.1 

12/0710510:38:17 46.3 216.3 30.0 -0.1 

12/07/0510:38:27 46.2 215.7 30.0 -0.2 

12/07/0510:38:37 46.7 216.3 29.9 -0.1 

12/07/0510:38:47 46.8 214.6 29.9 -0.1 

12/07/0510:38:57 46.4 213.8 29.8 -0.1 

12107/0510:39:07 46.6 213.5 29.8 -0.1 

12/07/0510:39:17 46.5 213.3 29.8 -0.2 

12/07l0510:39:27 46.6 213.3 29.8 -0.1 

12/07/0510:39:37 46.5 212.9 29.9 -0.1 

12/07/0510:39:47 46.3 212.5 30.0 -0.1 

12/07/0510:39:57 46.5 212.4 30.0 -0.2 

12/07/0510:40:07 46.3 212.5 30.2 -0.2 

1210710510:40:17 46.6 212.5 30.1 -0.1 

12/07/0510:40:27 46.6 212.7 30.1 -0.1 

12/07/0510:40:37 46.5 212.8 30.0 -0.1 

12/07/0510:40:47 46.3 212.9 29.9 -0.1 

12/07/0510:40:57 46.1 213.3 29.9 0.0 

12/0710510:41:07 45.7 213.4 29.9 0.0 

12107/0510:41:17 46.2 213.1 29.8 0.0 

12J0710510:41:27 45.9 213.0 29.9 0.0 

12/0710510:41:37 45.8 213.1 29.9 -0.1 

12/0710510:41:47 45.4 212.7 29.9 -0.1 

12/07/0510:41:57 45.5 212.4 29.8 -0.2 

12/07/0510:42:07 45.7 212.2 29.8 -0.2 

1 2107/05 1 0:42:17 45.5 211.9 29.9 -0.2 

12/07/0510:42:27 45.7 211.9 29.9 -0.2 

12/0710510:42:37 45.9 212.0 29.9 -0.1 

12107/0510:4247 46.2 211.8 29.7 -0.1 

12/07/0610:42:57 46.1 211.7 29.7 -0.2 

12/07/0510:43:07 46.1 211.9 29.7 -0.2 

12107/0510:43:17 45.9 211.9 29.7 -0.2 

12107/0510:43:27 45.5 212.1 29.7 -0.1 

12/07/0510:43:37 45.6 212.0 29.7 -0.2 

12/07/0510:43:47 45.9 211.6 29.8 -0.2 

12/07/0510:43:57 46.6 211.5 29.8 -0.3 

12/07/0510:44:07 46.5 211.8 29.9 -0.3 

12/07/0510:44:17 46.1 212.1 30.1 -0.2 

12107/0510:44:27 46.4 212.6 30.1 -0.2 

1210710510:44:37 46.6 212.9 30.1 -0.2 

12/07/0510:44:47 46.1 213.1 30.0 -0.2 

12107/0510:44:57 46.9 212.9 29.9 -0.1 

12/07/0510:45:07 47.1 213.1 29.8 0.0 

12/07/0510:45:17 46.9 213.3 29.8 0.0 

12/07/0510:45:27 47.1 213.7 29.8 0.0 

12/07/0510:45:37 47.8 213.6 29.8 0.0 

12107/0510:45:47 47.2 213.6 29.8 0.0 

12/07/0510:45:67 47.2 213.3 29.9 0.0 

Page 3 

79 
1217105 Run il1 

12107/0510:46:07 46.9 213.1 31.0 -0.1 

12/07/05 10:46:17 46.7 213.3 3(~ () -0.1 

1210710510:46:27 46.5 213.3 30.0 -0.1 

12107/0510:46:37 46.8 213.4 30.1 -0.1 

1210710510:46:47 46.8 213.3 30.0 -0.1 

12/07/0510:46:57 46.5 213.1 29.9 -0.1 

12/07/0510:47:07 47.2 213.0 29.8 -0.1 

12/07/0510:47:17 47.3 212.9 29.7 -0.1 

1210710510:47:27 47.1 213.1 29.7 -0.1 

12107/0510:47:37 46.5 213.0 29.7 -0.1 

1210710510:47:47 46.0 212.8 29.7 0.0 

1210710510:47:57 46.7 212.9 29.8 -0.1 

12/0710510:48:07 47.2 212.6 29.9 0.0 

12/0710510:48:17 46.8 212.5 30.0 0.0 

1210710510:48:27 46.6 212.8 30.2 -0.1 

12107/0510:48:37 46.9 212.9 30.2 -0.1 

12107/0510:48:47 46.5 212.9 30.1 -0.1 

12107/0510:48:57 46.6 212.9 30.1 -0.1 

12/07/0510:49:07 46.8 213.2 30.0 -0.1 

12107/0510:49:17 46.4 213.4 29.9 -0.1 

1210710510:49:27 45.7 213.5 29.8 -0.1 

12/07/05 10:49:37 46.5 213.5 29.8 -0.1 

12/07/0510:49:47 46.2 214.0 29.7 -0.1 

12/07/0510:49:57 45.9 214.6 29.7 -0.1 

12/07/0510:50:07 45.5 214.8 29.7 -0.1 

12107/0510:50:17 45.3 214.9 30.0 -0.1 

12/07/0510:50:27 45.5 214.9 30.0 -0.1 

12/07/0510:50:37 45.1 215.9 30.2 -0.1 

12107/0510:50:47 45.6 215.9 30.3 -0.1 

12/0710510:50:57 45.5 215.3 30.3 -0.1 

12107/0510:51:07 44.7 215.0 30.2 0.0 

12/0710510:51:17 44.6 214.8 30.0 -0.1 

12107/0510:51:27 45.0 214.2 30.0 -0.1 

12107/0510:51:37 45.1 213.1 30.0 -0.1 

1210710510:51:47 44.9 212.5 30.0 -0.1 

12/07/0510:61:57 44.2 212.0 30.0 -0.3 

12/07/0510:52:07 44.2 211.3 30.2 -0.3 

12/0710510:52:17 44.0 210.9 30.3 -0.2 

12107/0510:52:27 43.9 210.6 30.3 -0.1 

12107/0510:52:37 44.3 210.2 30.3 -0.2 

1210710510:52:47 44.3 209.8 30.2 -0.3 

12/07/0510:52:57 44.3 209.5 30.3 -0.3 

12107/0510:53:07 44'.4 209.3 30.2 -0.3 

12/07/0510:53:17 44.3 209.3 30.2 -0.3 

12/07/0510:53:27 44.9 209.5 30.2 -0.2 

12107/0510:53:37 44.6 209.6 30.1 0.0 

12/07/0510:53:47 44.9 209.9 30.1 0.0 

12107/0510:53:57 45.5 210.1 30.3 0.0 

12107/0510:54:07 45.2 141.2 30.1 -1.1 

12107/0510:54:17 46.1 209.6 30.5 0.1 

12107/0510:54:27 45.9 210.1 30.6 0.1 

12/07/0510:54:37 45.9 210.4 30.5 0.1 

1210710510:54:47 46.0 210.6 30.5 0.1 

12/07/0510:54:57 45.5 210.9 30.5 0.1 

12/07/0510:55:07 46.1 211.0 30.4 0.1 

12107/0510:55:17 46.4 210.9 30.3 0.0 

12J07/0510:55:27 46.9 211.0 30.3 0.1 

1210710510:55:37 46.9 211.2 30.4 0.1 

1210710510:55:47 46.5 211.2 30.5 0.0 

1210710510:55:57 46.6 211.2 30.5 -0.1 

12107/0510:56:07 46.7 211.2 30.5 0.0 

12107/0510:56:17 46.9 211.1 30.6 0.0 

12/07/05 10:56:27 47.0 211.1 30.6 0.0 

1 2107/05 1 0:56:37 47.0 21•1.3 30.5 0.1 

12/0710510:56:47 47.2 187.1 30.2 -1.1 

1210710510:56:57 47.2 195.7 30.5 0.1 

12107/0510:57:07 46.8 211.8 30.3 0.0 

12107/0510:57:17 46.7 211.9 30.4 0.0 

12107/0510:57:27 46.7 211.9 30.4 0.0 

12107/0510:57:37 46.7 211.7 30.4 0.0 

12/07/0510:57:47 46.1 211.3 30.5 0.0 

12107/0510:57:57 46.6 210.9 30.4 0.0 

12I07/05 10:58:07 46.4 210.9 30.5 0.0 

12/07/0510:58:17 45.9 210.8 30.6 -0.1 

Page 4 To*-* 
1217/05 Run #1 

12107/0510:58:27 46.2 210.7 30.5 -0.1 

12107/0510:58:37 48.9 210.8 30.5 -0.1 

1210710510:58:47 46.6 211.1 30.6 -0.1 

1210710510:58:57 46.4 211.3 30.6 -0.1 

12107/0510:59:07 46.4 211.7 30.7 0.0 

12J07/0510:59:17 45.3 211.8 30.7 0.0 

12107/0510:59:27 45.7 211.6 30.7 0.0 

12/07/0510:59:37 45.7 211.6 30.7 0.0 

12/07/0510:59:47 45.0 211.5 30.8 0.0 

12/07/0510:59:57 45.5 211.4 30.9 -0.1 

12/07/0511:00:07 45.8 211.5 30.9 -0.1 

1210710511:00:17 45.2 211.6 31.0 0.0 

12/07/0611:00:27 44.8 211.7 30.9 0.0 

1210710511:00:37 44.6 211.5 30.8 0.0 

1 2107/05 1 1:00:47 44.9 211.4 30.8 0.0 

12f07/0511:00:57 44.8 211.2 30,7 0.0 

1 2107/05 1 1:01:07 44.5 211.2 30.6 -0.1 

12l07/0511:01:17 44.9 211.3 30.6 -0.2 

12107/0511:01:27 44.3 211.2 30.5 -0.2 

12107/0511:01:37 44.2 210.9 30.5 -0.2 

1 2107/05 1 1:01:47 44.6 210.5 30.5 -0.1 

12/07/0511:01:57 44.1 210.6 30.5 -0.1 

12107/0511:02:07 44.6 210.5 30.4 -0.2 

12107/0511:02:17 44.8 210.9 30,4 -0.1 

12107105 1 1:02:27 45.6 211.2 30.4 -0.1 

1210710511:02:37 45.3 211.7 30.4 -0.1 

12/0710511:02:47 45.0 212.0 30.3 -0.1 

12107/0511:0257 45.1 212.0 30.4 -0.1 

12/07/0511:03:07 45.2 212.3 30.4 -0.1 

12/07/0511:03:17 45.6 212.1 30.5 -0.1 

12/07/0511:0327 45.6 212.0 30.6 -0.1 

12/0710511:03:37 45.5 211.7 30.6 -0.1 

12/07/0511:03:47 45.4 211.5 30.7 -0.1 

12107/0511:03:57 45.9 211.6 30.8 -0.1 

1 2107/05 1 1:04:07 48.0 211.4 30.9 -0.1 

12/07/0511:04:17 46.0 211.5 30.9 -0.1 

12/07/0511:04:27 46.5 211.7 30.8 -0.2 

12107/0511:04:37 46.8 211.6 30.8 -0.1 

1 2/07105 1 1:04:47 47.0 211.7 30.7 -0.1 

1210710511:04:57 47.0 211.8 30.5 -0.1 

12/0710511:05:07 46.7 211.7 30.4 -0.1 

12/07/0511:05:17 47.4 211.7 30.3 -0.1 

12/07/0511:05:27 46.9 212.0 30.3 -0.1 

12/07/0511:05:37 46.8 212.3 30.3 -0.1 

12107/0511:05:47 47.3 212.6 30.3 -0.1 

12/07/0511:05:57 47.4 212.8 30.3 -0.1 

12107/0511:06:07 47.3 213.1 30.4 0.0 

12107/0511:06:17 47.4 213.2 30.4 0.0 

12/07/0511:06:27 47.4 213.1 30.4 0.0 

12107/0511:06:37 47.2 213.1 30.3 . 0.0 

12107/0511:06:47 47.3 213.1 30.2 0.0 

12107/0511:06:57 47.3 212.8 30.1 0.0 

12/07/0511:07:07 47.3 212.9 30.0 -0.1 

12/07/0511:07:17 46.7 213.2 30.0 0.0 

12107/0511:07:27 46.2 213.7 29.9 0.0 

12/07/0511:07:37 46.1 214.3 30.0 -0.1 

12107/0511:07:47 46.3 214.5 30.1 -0.1 

12/0710511:07:57 45.9 215.0 30.2 -0.1 

12/0710511:08:07 46.2 215.0 30.4 -0.1 

12/0710511:08:17 45.7 214.8 30.5 -0.1 

12/07/0511:08:27 45.5 214.6 30.6 -0.1 

12/0710511:08:37 45.8 214.5 30.6 -0.1 

12/0710511:08:47 45.7 213.6 30.6 -0.2 

12/07/0511:08:57 45.4 213.2 30.6 -0.1 

12/07/0511:09:07 45.6 212.9 30.5 0.0 

12/0710511:09:17 45.3 213.0 30.5 -0.1 

12/07/0511:09:27 45.2 213.1 30.4 -0.1 

12/07/0511:09:37 44.8 212.6 30.6 -0.1 

12/07/0611:09:47 45.1 212.0 30.6 -0.1 

1 2107/05 1 1:09:57 45.3 211.5 30.6 -0.1 

12107/0511:10:07 45.5 211.3 30.5 0.0 

12/07/0511:10:17 45.2 211.4 30.5 -0.1 

12/0710511:10:27 45.2 211.4 30.5 -0.1 

12/07/05 11:10:37 45.1 211.3 30.4 ' 0.0 

Page 5 ol 
1217105 Run #1 

12107/0511:10:47 45.1 211.5 30.4 0.0 

12/07/0511:10:57 45.0 211.8 30.3 -0.1 

12/07/0511:11:07 45.7 212.2 30.2 -0.1 

1 2107/05 1 1:11:17 46.0 212.3 30.2 -0.1 

12107/0511:11:27 45.4 212.7 30.1 -0.1 

12J07/0511:11:37 45.3 213.1 30.1 -0.1 

12107/0511:11:47 45.0 213.5 30.1 -0.2 

12/0710511:11:57 45.4 214.0 30.2 -0.2 

12/07/0511:12:07 45.5 214.5 30.3 -0.2 

12/0710511:12:17 45.5 214.6 30.3 -0.3 

1210710511:12:27 45.5 214.8 30.2 -0.2 

12/0710511:12:37 45.2 214.8 30.1 -0.2 

1210710511:12:47 45.9 214.6 30.0 -0.1 

12/0710511:12:57 45.7 214.5 30.1 0.0 

1210710511:13:07 45.7 214.6 30.1 0.0 

12/0710511:13:17 45.4 214.8 30.2 0.0 

12/0710511:13:27 45.6 215.0 30.2 0.0 

1 2/07105 1 1:13:37 45.8 213.9 30.4 -0.1 

1 2/07105 1 1:13:47 45.3 157.5 30.2 -1.2 

12/0710511:13:57 44.5 139.2 30.0 -3.2 

12/07/0511:14:07 45.5 215.5 30.5 0.0 

12107/0511:14:17 45.8 215.4 30.5 -0.1 

12107/0511:14:27 45.9 215.5 30.4 -0.1 

12/07/0511:14:37 45.9 215.5 30.4 0.0 

12/07/0511:14:47 46.3 215.5 30.4 0.0 

12/07/0511:14:57 45.6 214.9 30.4 -0.1 

12/07/0511:15:07 45.6 214.2 30.3 0.0 

12/07/0511:15:17 46.2 213.6 30.3 0.0 

12/07/0511:15:27 46.5 212.6 30.3 0.0 

1 2107/05 1 1:15:37 46.8 212.3 30.3 0.1 

12/0710511:15:47 46.4 211.8 30.4 0.0 

1 2107/05 1 1:15:57 46.6 211.9 30.4 0.0 

1210710511:16:07 46.6 211.8 30.4 0.0 

1210710511:16:17 46.7 211.9 30.4 0.0 

1210710511:16:27 47.2 212.1 30.3 -0.1 

1210710511:16:37 47.1 212.3 30.3 -0.1 

12107/0511:16:47 47.0 212.4 30.2 0.0 

12/07/0511:16:57 47.1 212.3 30.1 0.0 

Stop Run #1 47.17 215.86 29.93 -0.08 

12/07/0511:17:07 46.9 212.3 30.1 -0.1 

1 2107/05 1 1:17:17 46.6 212.3 30.1 0.0 

12107/0511:17:27 46.8 212.3 30.1 . -0.1 

12107/0511:17:37 46.9 212.2 30.2 -0.1 

12107/0511:17:47 46.6 212.0 30.2 0.0 

12/07/0511:17:57 46.4 211.8 30.2 0.0 

12107/0511:18:07 46.2 92.4 30.2 -0.3 

12107/0511:18:17 43.4 211.5 30.5 0.0 

12/07/0511:18:27 3.5 208.9 30.3 0.0 

12107/05 11:18:37 1.6 196.1 29:1 0.0 

12107/0511:18:47 1.6 147.0 25.3 -0.1 

12/07/0511:18:57 1.5 100.0 18.9 -0.2 

12107/0511:19:07 1.5 65.7 14.2 -0.2 

12/07/0511:19:17 0.8 43.2 11.1 -0.4 

12/0710511:19:27 0.7 29.1 9.2 -0.5 

12/07/0511:19:37 0.7 19.1 11.3 -0.6 

12107/0511:19:47 0.6 13.9 16.2 -0.5 

12107/0511:19:57 0.6 10.3 19.7 -0.4 

12/07/0511:20:07 0.5 7.8 22.2 -0.2 

12107/0511:20:17 0.4 6.5 23.6 -0.1 

12107/0511:20:27 0.4 5.7 23.6 -0.2 

12107/0511:20:37 0.4 5.4 23.6 -0.1 

12/07/0511:20:47 0.4 5.0 23.7 -0.1 

12/07/0511:20:57 0.7 4.8 23.5 -0.2 

12/07/0511:21:07 1.5 4.7 23.5 -0.3 

12/07/0511:21:17 1.5 6.3 23.0 -0.3 

12/0710511:21:27 1.5 9.2 19.7 -0.3 

12/07/0511:21:37 1.5 9.3 14.5 -0.3 

12/07/0511:21:47 1.4 7.8 10.5 -0.4 

12/07/0511:21:57 1.4 6.3 8.2 -0.4 

12J0710511:22:07 1.2 4.9 6.7 -0.3 

12/07/0511:22:17 0.2 3.8 5.7 -0.3 

25.5 ppm NOx 

Zero S02 

Page 6 
1217/05 Run #1 

12/07/0511:22:27 0.2 2.4 4.9 -0.2 

12/07/0511:22:37 0.3 1.3 4.2 -0.1 

12107/0511:22:47 0.2 0.7 3.8 0.6 

12/07/0511:22:57 0.2 0.4 3.7 3.1 

12/0710511:23:07 0.2 0.5 3.7 7.1 

12/0710511:23:17 0.2 0.5 3.7 12.9 

12107/0511:23:27 0.3 0.4 3.7 20.3 

12/07/0511:23:37 0.3 0.5 3.7 28.3 

12/07/0511:23:47 0.2 0.6 3.5 36.0 

12/07/0511:23:57 0.2 0.5 3.4 43.3 

12/07/0511:24:07 0.2 0.4 3.3 49.8 

12/07/0511:24:17 0.2 0.3 3.2 55.1 

12J07/0511:24:27 0.2 0.3 3.0 59.4 

12107/0511:24:37 0.3 0.4 2.9 62.9 

1 2107/05 1 1:24:47 0.2 0.4 2.7 66.0 

12/07/0511:24:57 0.2 0.5 2.5 68.7 

1 2107/05 1 1:25:07 0.2 0.5 2.4 70.6 

12107/0511:25:17 0.2 0.4 2.2 72.4 

12107/0511:25:27 0.2 0.5 2.1 73.8 

12/07/0511:25:37 0.3 0.4 2.0 75.1 

12107/0511:25:47 0.2 0.3 1.9 76.1 

12107/0511:25:57 0.2 0.3 1.8 76.9 

12/07/0511:26:07 0.2 0.3 1.7 77.5 

12/07/0511:26:17 0.3 0.4 1.6 78.3 

12/07/0511:26:27 0.2 0.3 1.6 79.3 

12107/0511:26:37 0.2 0.4 1.6 80.1 

12/07/0511:26:47 0.2 0.3 1.5 80.9 

12107/0511:26:57 0.2 0.3 1.4 81.4 

12/07/0511:27:07 0.2 0.3 1.3 82.4 

12/07/0511:27:17 0.2 0.4 1.3 83.3 

12/07/0511:27:27 0.2 0.3 1.2 84.2 

12/07/0511:27:37 0.3 0.3 1.1 85.1 

12107/0511:27:47 0.3 0.3 1.1 85.6 

12/07/0511:27:57 0.2 0.3 1.0 86.1 

12/07/0511:28:07 0.2 0.4 1.0 86.7 

12/0710511:28:17 0.2 0.3 1.0 87.1 

12/0710511:28:27 0.2 0.3 0.9 87.4 

12/0710511:28:37 0.2 0.3 0.9 87.7 

12107/0511:28:47 0.2 0.3 0.8 89.0 

12/07J0511:28:57 0.2 0.3 0.8 90.6 

12/07/0511:29:07 0.2 0.4 0.7 90.8 

12/07/0511:29:17 0.3 0.4 0.7 91.2 

12/07/0511:29:27 0.3 0.5 0.7 91.6 

12/07/0511:29:37 0.3 0.4 0.7 93.2 

12/07/0511:29:47 0.2 0.3 0.7 94.3 

12/07/0511:29:57 0.3 0.3 0.6 94.5 

12107/0511:30:07 0.3 0.3 0.6 94.8 

12107/0511:30:17 0.2 0.3 0.6 95.1 

12107/0511:30:27 0.3 0.4 0.5 95.1 

12/07/0511:30:37 0.3 0.6 0.5 96.0 

12/07/0511:30:47 0.3 0.5 0.5 96.2 

12107/0511:30:57 0.3 0.4 0.5 96.2 

12107/05 11:31:07 0.2 0.4 0.4 96.4 101 ppm S02 

12107/05 11:31:17 0.2 0.4 0.5 96.5 Zero CO 

12/07/0511:31:27 0.2 0.4 0.5 96.7 

12/0710511:31:37 0.2 0.4 0.4 96.3 

12/0710511:31:47 0.7 0.4 0.4 94.5 

12/07/0511:31:57 0.2 0.4 0.4 93.8 

12107/0511:32:07 0.2 13.8 0.4 93.3 

12107/0511:32:17 0.2 66.1 0.4 89.9 

12107/0511:32:27 0.2 103.3 0.4 82.9 

12/07/0511:32:37 0.2 126.9 0.5 74.8 

1210710511:32:47 0.2 142.8 0.4 66.3 

12107/0511:32:57 0.2 153.6 0.4 58.0 

12/07/0511:33:07 0.2 160.1 0.3 50.2 

12/07/0511:33:17 0.2 163.9 0.3 43.2 

12/07/0511:33:27 0.3 167.2 0.3 37.3 

12/07/0511:33:37 0.2 169.8 0.3 32.5 

12/07/0511:33:47 0.3 172.5 0.4 28.7 

12/07/0511:33:57 0.3 174.8 0.4 25.3 

12/07/0511:34:07 0.3 176.1 0.3 22.3 

12/07/0511:34:17 0.3 176.9 0.4 19.6 

12/07/0511:34:27 0.4 177.5 0.3 17.5 

83 

Page 7 
1217105 Run #1 

12/07l0511:34:37 0.3 177.6 0.3 15.5 

1210710511:34:47 0.3 178.5 0.3 13.8 

1 2107105 1 1:34:57 0,3 178.8 0.3 12.5 

1 P10710511:35:07 0.2 179.4 0.3 11.4 

1210710511:35:17 0.3 179.4 0.3 10.3 

12/0710511:35:27 0.3 179.5 0.3 9.3 

1 2107105 1 1:35:37 0.3 179.7 0.3 8.3 200 ppm CO 

12/07105 11:35:47 0.3 179.7 0.3 7.7 Zero VOC, tVOx 

12/07/0511:35:57 0.3 180.0 0.3 7.1 

12107/0511:36:07 0.2 179.3 0.2 6.6 

12/07/05 1 1:36:17 - 7.6 176.7 0.3 6.0 

12/07l0511:36:27 46.3 175.3 0.3 5.5 

12J07l0511:36:37 47.2 165.9 0.3 5.1 

12/0710511:36:47 47.6 ' 125.4 0.3 4.7 

12/0710511:36:57 47.8 77.1 0.3 4.4 

12107/0511:37:07 47.8 45.4 0.3 4.1 48.8 ppm C3H8 

1 2/07105 1 1:37:17 47.8 28.9 0.3 3.9 

12107/0511:37:27 47.8 18.8 0.3 3.8 

12J0710511:37:37 45.9 12.9 0.3 3.6 

12/0710511:37:47 9.8 8.6 0.2 3.4 

84 

Page 8 
1217/05 Run #2 

Date/Time VOC CO NOx S02 

mm/dd/yy hh:mm:ss ppm ppm ppm ppm 

1210710512:14:40 60.7 186.4 23.4 0.1 

12107105 1 2:14:50 59.0 195.3 25.1 0.2 

Start Run #2 

12/07/0512:15:00 58.1 201.1 26.0 0.1 

12/07/0512:15:10 56.9 204.8 26.5 0.2 

12/0710512:15:20 55.6 206.8 27.0 0.2 

12/07/0512:15:30 53.9 207.9 27.3 0.3 

12/0710512:15:40 50.6 208.5 27.3 0.3 

12/07/0512:15:50 48.8 209.2 27.5 0.2 

12107/0512:16:00 46.9 209.7 27.6 0.2 

12107/0512:16:10 48.7 210.0 27.6 0.3 

12/07/0512:16:20 47.8 210.4 27.7 0.3 

12/07/0512:16:30 47.2 210.8 27.6 0.2 

12/0710512:16:40 47.2 211.0 27.6 0.2 

12/07/0512:16:50 46.7 210.9 27.6 0.3 

12/07/0512:17:00 47.0 210.9 27.7 0.2 

12/07/0512:17:10 46.7 210.8 27.7 0.3 

12/07/0512:17:20 46.7 210.9 27.8 0.4 

12/07/0512:17:30 45.3 210.8 27.9 0.4 

12/07/0512:17:40 45.6 211.0 28.0 0.4 

12/07/05 12:17:50 45.8 211.0 28.0 0.4 

12/07/0512:18:00 45.7 210.6 28.0 0.3 

12/07/0512:18:10 45.7 209.9 28.1 0.2 

12107/0512:18:20 45.9 208.4 28.1 0.3 

12/07/0512:18:30 45.9 206.3 28.1 0.2 

12107/0512:18:40 45.6 204.2 28.1 0.2 

12107/0512:18:50 46.1 202.1 28.2 0.3 

12/07/0512:19:00 45.5 200.3 28.3 0.4 

1210710512:19:10 45.5 199.3 28.4 0.3 

1210710512:19:20 45.5 198.9 28.5 0.3 

12/0710512:19:30 46.3 199.5 28.6 0.3 

12/07/0512:19:40 45.7 200.1 28.7 0.4 

12/07/0512:19:50 45.8 201.0 28.8 0.4 

12107/0512:20:00 46.1 202.4 28.9 0.3 

12107/0512:20:10 44.9 203.3 29.0 0.2 

12/07/0512:20:20 44.9 203.8 29.0 0.3 

12/07/0512:20:30 45.5 203.9 29.0 0.2 

12/0710512:20:40 45.4 204.6 29.2 0.2 

12/07/0512:20:50 45.0 204.8 29.2 0.3 

12/07/0512:21:00 45.8 205.0 29.4 0.3 

1210710512:21:10 46.1 205.5 29.4 0.3 

12107/0512:21:20 45.5 205.7 29.6 0.3 

12107/0512:21:30 44.6 191.1 28.5 -0.9 

1210710512:21:40 45.6 188.4 29.5 0.2 

12/07/0512:21:50 45.8 125.7 29.7 0.1 

12/07/0512:22:00 46.2 206.8 29.7 0.4 

12/07/0512:22:10 46.3 206.9 29.8 0.4 

1210710512:22:20 46.0 207.3 29.8 0.5 

12107/0512:22:30 46.4 207.3 29.9 0.4 

12/07/0512:22:40 46.0 207.3 29.9 0.4 

12/07/0512:22:50 45.3 167.4 28.8 -4.4 

12/07/0512:23:00 46.1 206.4 29.8 0.2 

1 2107/05 1 2:23:10 46.0 207.0 30.1 0.4 

1210710512:23:20 46.8 206.8 30.1 0.3 

12/07/0512:23:30 46.1 206.5 30.1 0.2 

12107/0512:23:40 45.9 207.0 30.1 0.2 

12/07/0512:23:50 46.2 207.4 30.2 0.2 

12107/0512:24:00 46.8 207.4 30.1 0.3 

12107/0512:24:10 46.6 208.0 30.0 0.3 

12107/0512:24:20 47.1 208.5 30.1 0.2 

1 2107/05 1 2:24:30 46.5 208.9 30.1 0.3 

12/07/0512:24:40 46.8 209.3 30.1 0.4 

12/07/0512:24:50 46.4 209.5 30.2 0.6 

12/07/0512:25:00 46.7 209.7 30.3 0.6 

12/07/0512:25:10 46.5 210.0 30.3 0.5 

12/07/0512:25:20 46.4 210.4 30.4 0.4 

12/07/0512:25:30 45.8 210.5 30.4 0.4 

12/0710512:25:40 45.7 210.4 30.7 0.3 

12107/0512:25:50 45.9 210.3 30.8 0.3 

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Page 1 
1217/05 Run tl2 

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Page 2 
12rIl05 Run #2 

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R{ 

Page 3 
12R/05 Run #2 

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o • • 

PBge 4 
1217105 Run #2 

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Page 5 
12/7105 Run #2 

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12107/0513:23:20 44.5 208.3 30.6 0.1 

12107/0513:23:30 44.8 208.6 30.6 0.0 

12/07/0513:23:40 44.5 208.6 30.7 0.1 

1210710513:23:50 44.5 208.5 30.8 0.0 

12107/0513:24:00 45.0 208.2 31.2 0.0 

12107/0513:24:10 45.0 207.9 31.3 0.0 

12107/0513:24:20 44.5 207.8 31.4 0.0 

12/07/0613:24:30 44.7 207.2 31.4 0.1 

12/07/0613:24:40 44.8 206.9 31.3 0.1 

12/07/0513:24:50 43.0 206.8 31.1 0.1 

12/07/0513:25:00 43.5 207.1 31.0 0.1 

12/07/0513:25:10 43.8 207.1 30.8 0.1 

12107/0513:25:20 44.9 207.3 30.7 0.0 

12107/0513:25:30 44.3 207.9 30.7 0.0 

12/07/0513:25:40 44.0 208.7 30.6 0.0 

12/0710513:25:50 45.1 209.0 30.6 0.0 

12/0710513:26:00 44.5 208.8 30.6 0.0 

12/07/0513:26:10 44.3 208.8 30.8 0.0 

12/07/0513:26:20 44.0 208.7 31.0 0.0 

12/0710513:26:30 44.7 208.6 31.3 0.0 

12/0710513:26:40 45.2 208.5 31.2 -0.1 

12107/0513:26:50 44.5 208.1 31.4 -0.1 

StOp Run #2 45.7 206.7 30.6 0.1 

12/0710513:27:00 45.3 208.1 31.4 0.0 

12/0710513:27:10 46.0 207.7 31.5 -0.1 

12/0710513:27:20 46.4 207.7 31.5 -0.1 

s. 

LWAIWJ 

Page 6 
12R/05 Run #2 

12J07/0513:27:30 46.0 207.7 31.4 0.1 

12107/0513:27:40 45.6 207.9 31.3 0.1 

12/07/0513:27:50 45.1 208.4 31.2 0.1 

12/07/0513:28:00 44.8 207.9 31.0 0.0 

12/0710513:28:10 45.3 207.6 30.9 0.0 

12/07/0513:28:20 45.3 207.8 30.8 0.0 

12/07/0513:28:30 30.7 164.7 30.3 0.0 

12/07/0513:28:40 2.1 203.0 29.7 0.0 

12/0710513:28:50 1.7 188.1 29.2 0.0 

12/0710513:29:00 1.3 133.9 24.7 0.1 

12/0710513:29:10 1.1 83.7 17.6 0.1 

12/07/0513:29:20 1.0 49.7 14.2 0.0 

12/0710513:29:30 0.9 29.6 16.7 -0.3 

1 2/07105 1 3:29:40 0.6 19.0 19.6 -0.4 

1210710513:29:50 0.7 12.7 21.7 -0.4 

12/0710513:30:00 0.7 8.7 22.9 -0.5 

12/07/0513:30:10 0.6 6.8 23.4 -0.3 

12/07/0513:30:20 0.6 5.5 23.6 -0.1 

12/07/0513:30:30 0.6 4.8 23.6 -0.1 

1210710513:30:40 0.6 4.0 23.7 -0.1 

12/07/0513:30:50 0.5 3.1 23.6 0.0 

12/07/0513:31:00 0.5 2.3 23.6 -0.1 

12107/0513:31:10 0.4 2.0 23.4 -0.2 

12/07/0513:31:20 1.3 1.6 23.2 -0.2 

12/07/0513:31:30 1.5 1.3 22.9 -0.2 

1 2107/05 1 3:31:40 1.4 1.5 21.3 -0.1 

12107/0513:31:50 1.5 1.9 16.2 -0.1 

12/07/0513:32:00 1.0 1.7 11.2 -0.1 

12/07/0513:32:10 0.3 1.1 7.9 -0.1 

12/07/0513:32:20 0.2 0.7 6.2 -0.1 

12/0710513:32:30 0.3 0.2 5.0 0.1 

12/07/0513:32:40 0.3 -0.1 4.4 1.4 

12/07/0513:32:50 0.3 -0.2 4.0 4.6 

12J0710513:33:00 0.3 -0.3 3.8 9.9 

1 2/07105 1 3:33:10 0.3 -0.4 3.7 17.1 

12/0710513:33:20 0.3 -0.6 3.5 25.1 

12/07/0513:33:30 0.3 -0.5 3.4 32.6 

12107/0513:33:40 0.3 -0.6 3.3 40.3 

12/07/0513:33:50 0.3 -0.7 3.2 47.2 

12/0710513:34:00 0.3 -0.5 3.1 52.7 

1210710513:34:10 0.3 -0.6 3.0 57.4 

12/0710513:34:20 0.2 -0.5 2.9 61.3 

12/07/0513:34:30 0.2 -0.6 2.8 64.7 

12107/0513:34:40 0.2 -0.8 2.7 67.6 

12/07/0513:34:50 0.2 -0.7 2.6 70.0 

12/07/0513:35:00 0.2 -0.5 2.4 72.0 

12/07/0513:35:10 0.2 -0.4 2.4 73.8 

12/07l0513:35:20 0.2 -0.3 2.3 75.5 

12/0710513:35:30 0.3 -0.1 2.1 77.0 

12/07/0513:35:40 0.2 -0.1 2.0 78.1 

; 2107/05 13:35:50 0.2 -0.2 1.9 79.3 

12/0710513:36:00 0.2 -0.2 1.9 80.4 

12107/0513:36:10 0.3 -0.2 1.7 81.2 

12107/0513:36:20 0.3 -0.1 1.7 81.8 

12/07/0513:36:30 0.3 -0.2 1.7 82.3 

12/07/0513:36:40 0.2 -0.2 1.6 82.9 

12/07/0513:36:50 0.2 -0.3 1.5 83.6 

1210710513:37:00 0.2 -0.4 1.5 84.1 

12107/0513:37:10 0.2 -0.5 1.5 85.6 

12/07/0513:37:20 0.2 -0.4 1.4 86.8 

12107/0513:37:30 0.2 -0.5 1.4 87.4 

12/07/0513:37:40 0.2 -0.5 1.3 87.8 

12/07/0513:37:60 0.2 -0.4 1.3 88.1 

12/0710513:38:00 0.2 -0.3 1.2 89.9 

12/0710513:38:10 0.2 -0.3 1.2 90.9 

12/07/0513:38:20 0.3 -0.4 1.2 91.1 

12/07/0513:38:30 0.2 -0.4 1.1 91.4 

12107/0513:38:40 0.3 -0.3 1.1 91.8 

12/07/0513:38:50 0.3 -0.3 1.1 92.4 

12/0710513:39:00 0.3 -0.2 1.0 92.8 

12/07/0513:39:10 0.3 -0.3 0.9 92.9 

12107/0513:39:20 0.3 -0.4 0.9 93.1 

12/07/0513:39:30 0.3 -0.3 1.0 93.2 

25.5 ppm NOx 

Zero S02 

91 

Page 7 
1217/05 Run #2 

12/0710513:39:40 0.3 -0.4 0.9 93.5 

12107/0513:39:50 0.3 -0.5 0.8 93.8 

1210710513:40:00 0.3 -0.4 0.9 93.9 

1210710513:40:10 0.3 -0.4 0.8 93.8 

1210710513:40:20 0.3 -0.3 0.8 94.6 

12/07/0513:40:30 0.3 -0.5 0.8 95.1 

12107/0513:40:40 0.2 -0.5 0.7 95.5 

1210710513:40:50 0.2 -0.4 0.7 95.7 

12107/0513:41:00 0.2 -0.5 0.7 95.9 

12/07/0513:41:10 0.2 -0.5 0.7 96.2 

12/07/05 13:41:20 0.2 -0.3 0.7 96.4 101 ppm S02 

12107105 13:41:30 0.2 -0.2 0.7 96.6 Zero CO 

12J07l0513:41:40 0.3 -0.2 0.6 96.6 

12/07l0513:41:50 0.9 -0.1 0.7 95.7 

12107/0513:42:00 0.4 -0.2 0.6 95.2 

12/0710513:42:10 0.4 0.9 0.6 95.2 

12107/0513:42:20 0.3 38.4 0.6 93.1 

1210710513:42:30 0.3 94.7 0.6 86.9 

12107J0513:42:40 0.3 126.1 0.6 78.2 

1210710513:42:50 0.3 143.2 0.5 69.0 

1210710513:43:00 0.3 154.9 0.6 60.6 

12/07l0513:43:10 0.3 160.3 0.5 52.7 

12/0710513:43:20 0.3 163.3 0.5 45.3 

1210710513:43:30 0.3 164.6 0.5 39.0 

12/07/0513:43:40 0.4 165.4 0.5 33.7 

12/0710513:43:50 0.4 166.4 0.5 29.4 

12/0710513:44:00 0.4 167.1 0.5 25.9 

12107/0513:44:10 0.3 168.1 0.5 22.7 

12107/0513:44:20 0.3 169.8 0.5 20.0 

1210710513:44:30 0.3 171.9 0.5 17.9 

12J0710513:44:40 0.3 173.5 0.5 16.0 

1210710513:44:50 0.2 174.3 0.5 14.5 

1210710513:45:00 0.2 174.7 0.4 13.0 

1 2107105 1 3:45:10 0.3 174.9 0.5 11.8 

1210710513:45:20 0.3 175.3 0.4 10.7 

1 2107105 1 3:45:30 0.3 174.5 0.5 9.5 

1210710513:45:40 0.3 177.3 0.4 8.7 

1210710513:45:50 0.3 178.4 0.4 8.0 

12/07105 13:46:00 0.3 179.8 0.4 7.4 200 ppm CO 

12/07105 13:46:10 0.3 178.6 0.4 6.8 Zero VOC, NOx 

1210710513:46:20 0.3 178.3 0.4 6.4 

12/0710513:46:30 0.3 178.1 0.4 5.9 

12/07/0513:46:40 0.2 177.9 0.4 5.4 

12/07/0513:46:50 0.2 176.9 0.4 4.9 

12/07l0513:47:00 1.2 175.1 0.4 4.5 

12/0710513:47:10 41.0 176.2 0.4 4.2 

1210710513:47:20 45.8 167.3 0.4 4.0 

12J0710513:47:30 47.1 127.1 0.5 3.9 

1210710513:47:40 47.2 68.4 0.5 3.7 

12107105 13:47:50 47.3 35.0 0.4 3.6 48.8 ppm C3H8 

12J0710513:48:00 47.3 20.7 0.4 3.6 

1210710513:48:10 47.2 11.9 0.4 3.4 

12/0710513:48:20 47.2 6.3 0.4 3.2 

12/0710513:48:30 32.3 3.4 0.4 3.0. 

wo 

Page 8 
12l7/05 Run #3 

Date/Time VOC CO NOx S02 

mm/ddtyy hh:mm:ss ppm ppm ppm ppm 

12J07/0514:04:50 49.2 207.4 27.6 0.7 

Start Run 43 

1210710514:05:00 49.4 207.5 27.6 0.6 

12/0710514:05:10 49.4 207.7 27.8 0.6 

12l07/0514:05:20 48.9 208.6 27.9 0.7 

12/07/0514:05:30 49.0 209.9 26.0 0.6 

1210710514:05:40 48.8 210.5 26.1 0.5 

1210710514:05:60 49.5 210.6 28.4 0.5 

1210710514:06:00 49.2 210.4 28.6 0.5 

12107/0514:06:10 49.5 210.4 28.8 0.5 

1210710514:06:20 49.9 210.4 26.9 0.6 

12107/0514:06:30 49.4 210.3 28.9 0.5 

12107/0514:06:40 48.9 210.6 29.0 0.5 

1210710514:06:50 49.2 211.0 29.0 0.4 

12107l0514:07:00 48.4 211.1 29.0 0.4 

1210710514:07:10 49.0 211.0 28.8 0.6 

12/0710514:07:20 48.6 211.0 28.7 0.5 

1210710514:07:30 48.9 211.0 28.8 0.5 

1210710514:07:40 48.3 211.0 28.8 0.5 

12/0710514:07:50 49.0 211.3 29.0 0.5 

12/07/0514:08:00 48.8 211.2 29.1 0.6 

12/07/0514:08:10 48.9 211.0 29.2 0.5 

12/07/0514:08:20 48.0 210.9 29.5 0.6 

12107/0514:08:30 47.5 210.8 29.7 0.5 

1 2107/05 1 4:08:40 46.9 210.8 29.9 0.6 

12107/0514:08:50 46.9 211.0 30.1 0.5 

12107/0514:09:00 46.7 210.8 30.2 0.5 

12107/0514:09:10 46.5 210.8 30.3 0.4 

12107/0514:09:20 46.5 211.0 30.4 0.4 

12107/0514:09:30 47.1 211.2 30.3 0.4 

1210710514:09:40 47.3 211.2 30.1 0.4 

12107/0514:09:50 46.7 211.7 29.9 0.5 

12107/0514:10:00 46.0 212.4 29.8 0.5 

12107/0514:10:10 47.0 213.1 29.7 0.5 

1210710514:10:20 46.8 213.5 29.7 0.5 

12107/0514:10:30 46.2 213.9 29.7 0.5 

1210710514:10:40 46.8 214.5 29.6 0.5 

12107/0514:10:50 46.6 215.1 29.7 0.5 

12J07l0514:11:00 47.1 215.2 29.8 0.5 

1210710514:11:10 46.1 214.6 29.8 0.4 

12107/0514:11:20 46.7 213.4 30.0 0.4 

1210710514:11:30 46.1 212.6 30.4 0.4 

1 2107105 1 4:11:40 46.3 212.1 30.5 0.4 

12/07/0514:11:50 46.3 211.8 30.7 0.4 

12/07/0514:12:00 47.0 211.7 30.8 0.3 

12J07/0514:12:10 47.0 211.6 30.7 0.4 

12J07/0514:12:20 47.4 211.8 30.5 0.4 

12107/0514:12:30 47.4 211.9 30.2 0.4 

12/07/0614:12:40 47.0 212.5 30.2 0.5 

12/07/0514:12:50 46.9 213.3 30.1 0.5 

12/0710514:13:00 46.7 212.6 30.0 0.6 

1210710514:13:10 47.5 211.9 29.9 0.5 

12J0710514:13:20 46.9 211.6 29.9 0.4 

12107/0514:13:30 47.0 211.4 30.0 0.4 

12107/0514:13:40 46.6 211.6 30.2 0.4 

12107/0514:13:50 46.8 211.4 30.3 0.4 

12107/0514:14:00 46.6 211.5 30.4 0.5 

1 2107/05 1 4:14:10 46.2 211.5 30.6 0.4 

12107/0514:14:20 45.8 211.9 30.8 0.5 

12/07/0514:14:30 45.6 212.1 31.0 0.4 

12107/0514:14:40 46.0 212.5 31.0 0.4 

12107/0514:14:50 46.4 212.7 31.0 0.4 

12/07/0514:15:00 45.8 213.4 30.9 0.3 

12/0710514:15:10 45.6 213.6 30.8 0.4 

12/07/0514:15:20 45.8 213.2 30.7 0.5 

12/07/0514:15:30 46.1 213.9 30.5 0.4 

12/07/0514:15:40 46.7 214.5 30.3 0.5 

12/07/0514:15:50 45.4 216.8 30.2 0.6 

12/07/0514:16:00 45.0 217.1 30.2 0.7 

12/07/0514:16:10 45.0 217.6 30.2 0.5 

12/0710514:16:20 46.2 218.3 30.1 0.4 

Page 1 

4 ~. 
1217/05 Run tt3 

12107/0514:16:30 45.2 219.2 30.2 0.4 

1 2107106 1 4:16:40 45.2 220.2 30.4 0.5 

1210710514:16:50 45.8 220.6 30.7 0.5 

1210710514:17:00 45.8 220.8 30.8 0.3 

1210710514:17:10 45.2 221.2 30.8 0.4 

1210710514:17:20 46.2 222.2 30.9 0.4 

12107/0514:17:30 46.0 222.7 30.9 0.4 

12107/0514:17:40 46.1 223.1 30.9 0.4 

1210710514:17:50 46.1 222.3 30.9 0.4 

12107/0514:18:00 46.4 221.4 30.7 0.4 

12107/0514:18:10 46.6 221.3 30.5 0.4 

12/07/0514:18:20 46.6 221.4 30.3 0.4 

1210710514:18:30 46.0 221.4 30.1 0.5 

12/0710514:18:40 46.0 221.5 30.0 0.5 

12J0710514:18:50 47.1 221.0 29.9 0.5 

1210710514:19:00 46.2 220.8 29.8 0.5 

12107/0514:19:10 46.3 ' 220.7 29.8 0.5 

12107/0514:19:20 47.1 220.9 29.9 0.5 

12f07/0514:19:30 46.1 221.6 30.0 0.4 

1210710514:19:40 46.5 221.8 30.1 0.4 

12107/0514:19:50 47.0 221.9 30.3 0.4 

12107/0514:20:00 47.4 222.4 30.4 0.5 

12107/0514:20:10 47.4 222.7 30.6 0.5 

12107/0514:20:20 47.6 222.9 30.6 0.4. 

12/07/0514:20:30 47.2 223.0 30.5 0.6 

1210710514:20:40 47.3 223.5 30.4 0.6 

12107/0514:20:50 48.0 223.9 30.2 0.5 

12/0710514:21:00 47.9 223.9 30.1 0.5 

12/0710514:21:10 47.4 224.0 29.9 0.5 

1210710514:21:20 47.3 224.5 29.8 0.5 

12107/0514:21:30 47.6 225.4 29.8 0.4 

12107/0514:21:40 47.2 225.8 29.8 0.3 

12107/0514:21:50 47.5 225.0 29.8 0.4 

12/07/0514:22:00 47.1 224.4 29.8 0.4 

12/0710514:22:10 46.2 224.2 30.0 0.4 

12/0710514:22:20 46.9 224.2 30.1 0.5 

12/07/0514:22:30 46.8 224.2 30.3 0.6 

12/0710514:22:40 46.4 224.0 30.3 0.5 

12107l0514:22:50 46.8 223.7 30.4 0.5 

12107l0514:23:00 46.6 223.1 30.5 0.5 

12107/0514:23:10 46.6 222.5 30.3 0.5 

12107/0614:23:20 45.8 222.0 30.3 0.4 

12107/0514:23:30 46.0 221.6 30.2 0.4 

12/07/0514:23:40 45.6 220.0 30.0 0.4 

12107/0514:23:50 45.7 218.9 30.0 0.5 

12/07/0514:24:00 44.3 218.2 29.9 0.6 

12107/0514:24:10 45.2 ' 217.6 29.8 0.5 

12/0710614:24:20 44.8 216.9 29.8 0.5 

12/0710514:24:30 44.1 215.8 29.8 0.5 

12107/0514:24:40 44.4 215.2 29.9 0.4 

12107/0514:24:50 43.9 214.6 30.2 0.3 

12/07/0514:25:00 43.6 213.7 30.4 0.4 

1 2107/05 1 4:25:10 44.7 213.2 30.6 0.4 

1210710514:25:20 44.1 212.9 30.8 0.3 

12/07/0514:25:30 44.1 212.2 30.8 0.4 

12107/0514:25:40 44.5 211.2 30.8 0.5 

12J07/0514:25:50 44.9 210.8 30.6 0.5 

12107/0514:26:00 44.9 210.7 30.4 0.5 

1 2107105 1 4:26:10 44.5 210.7 30.2 0.5 

12107105 14:26:20 45.1 210.8 30.0 0.4 

12J0710514:26:30 45.9 211.0 30.0 0.5 

1210710514:26:40 45.4 211.2 29.9 0.6 

12J0710514:26:50 46.0 211.4 30.0 0.5 

12/0710514:27:00 45.7 211.7 30.0 0.5 

12107/0514:27:10 46.2 211.7 30.1 0.6 

12/07/0514:27:20 45.4 211.8 30.2 0.7 

12/07/0514:27:30 45.7 211.2 30.3 0.6 

12/0710514:27:40 46.3 211.1 30.4 0.6 

12/0710514:27:50 45.8 210.9 30.6 0.5 

12/07/0514:28:00 45.9 210.4 30.7 0.5 

1 2107/05 1 4:28:10 47.5 210.2 30.7 0.5 

1210710614:28:20 46.4 210.0 30.7 0.5 

1210710514:28:30 45.6 210.2 30.5 0.4 

1210710514:28:40 46.0 210.0 30.6 0.4 

Page 2 q~ 
1217/05 Run #3 

12/07/0514:28:50 46.0 209.7 30.3 0.4 

12/0710514:29:00 45.9 209.4 30.2 0.5 

12/07/0514:29:10 46.5 209.1 30.0 0.5 

12/0710514:29:20 46.8 208.8 30.0 0.6 

12107/0514:29:30 45.4 209.1 30.0 0.6 

12/07/0514:29:40 45.2 209.6 30.0 0.6 

12/07/0514:29:50 45.8 210.1 30.0 0.5 

12107/0514:30:00 46.6 210.5 30.1 0.4 

12/0710514:30:10 46.5 210.8 30.2 0.6 

12107/0514:30:20 46.7 210.9 30.5 0.6 

12107/0514:30:30 45.6 210.7 30.5 0.6 

12107J0514:30:40 45.8 210.6 30.6 0.5 

1210710514:30:50 46.1 210.9 30.7 0.5 

12/07J0514:31:00 46.6 211.2 30.8 0.5 

1210710514:31:10 45.7 211.2 30.7 0.6 

1210710514:31:20 46.2 211.1 30.5 0.6 

12/0710514:31:30 45.5 211.4 30.3 .0.6 

12/0710514:31:40 45.0 211.2 30.2 0.6 

12107/0514:31:50 45.8 210.9 30.1 0.7 

1210710514:32:00 45.6 210.6 30.0 0.8 

12/07/0514:32:10 45.5 210.6 29.9 0.7 

12l07/0514:32:20 45.4 210.4 29.9 0.7 

12/07/0514:32:30 45.5 210.4 29.9 0.7 

12107/0514:32:40 45.0 210.6 29.9 0.8 

12/0710614:32:60 44.9 210.7 29.9 0.7 

12107/0514:33:00 45.3 210.8 30.1 0.7 

1210710514:33:10 45.5 210.9 30.3 0.6 

12107/0514:33:20 45.4 210.5 30.5 0.5 

12/0710514:33:30 45.8 210.4 30.5 0.6 

12/0710514:33:40 45.8 210.3 30.5 0.7 

12/0710514:33:50 47.0 210.1 30.4 0.7 

12107/0514:34:00 46.2 209.6 30.3 0.7 

12/07/0514:34:10 46.0 209.5 30.1 0.6 

12/07/0514:34:20 46.0 209.1 30.0 0.6 

12/0710514:34:30 46.8 208.8 30.0 0.7 

12/07/0614:34:40 46.8 208.7 29.8 0.7 

12/07/0514:34:50 46.3 208.7 29.8 0.6 

12/07/0514:35:00 46.4 208.3 29.8 0.6 

12107/0514:35:10 46.3 208.0 29.9 0.6 

12/07/0514:35:20 46.0 207.3 30.0 0.7 

12107/0514:35:30 46.1 206.4 30.2 0.6 

12/07/0514:35:40 46.6 205.6 30.3 0.6 

1210710514:35:50 46.3 205.1 30.5 0.5 

12107/0514:36:00 44.9 204.8 30.6 0.5 

12/07/0514:36:10 46.1 204.5 30.7 0.6 

12/0710514:36:20 46.2 204.6 30.7 0.6 

12107/0514:36:30 46.0 205.1 30.5 0.6 

12107/0514:36:40 46.2 205.6 30.4 0.6 

1210710514:36:50 45.5 205.8 30.3 0.6 

12/07/0514:37:00 45.4 206.1 30.2 0.6 

12J07/0514:37:10 46.1 206.1 30.0 0.6 

12/07/0514:37:20 45.1 206.1 30.0 0.7 

12/07/0514:37:30 46.2 205.7 29.9 0.6 

12/07/0514:37:40 45.9 205.8 29.9 0.6 

12107/0514:37:50 45.6 206.4 29.9 0.6 

12/07/0614:38:00 45.7 207.1 30.0 0.5 

12/07/0514:38:10 45.3 207.5 30.0 0.5 

12107/0514:38:20 45.4 207.8 30.1 0.5 

12!07/0514:38:30 45.2 208.5 30.2 0.6 

12/07/05 14:38:40 44.4 208.9 30.3 0.6 

12107J0514:38:50 44.2 209.3 30.6 0.6 

12/0710514:39:00 44.1 209.3 30.6 0.6 

1210710514:39:10 44.7 208.9 30.7 0.6 

12/0710514:39:20 44.0 208.7 30.6 0.6 

12/0710514:39:30 44.6 208.3 30.4 0.7 

12/07/0514:39:40 45.8 207.9 30.3 0.7 

12/07/0514:39:50 46.2 207.5 30.1 0.7 

12/07/0514:40:00 46.2 207.1 30.0 0.6 

12107/0514:40:10 46.1 207.4 29.9 0.7 

12107/0514:40:20 46.1 207.8 29.9 0.8 

12107/0514:40:30 46.5 208.0 29.9 0.8 

12/07/0514:40:40 46.5 207.9 29.9 0.8 

12/0710514:40:50 45.9 208.0 29.9 0.8 

12107/0514:41:00 47.8 208.4 30.0 0.7 

q 5 e

Page 3 
12/7/05 Run #3 

12107/0514:41:10 47.6 208.5 30.1 0.7 

12107/0514:41:20 48.7 208.6 30.3 0.7 

12/07/0614:41:30 47.8 209.0 30.4 0.6 

12/0710514:41:40 48.5 209.8 30.6 0.6 

12/0710514:41:50 47.9 210.4 30.6 0.7 

12107/0514:42:00 46.9 210.9 30.5 0.7 

12107/0514:42:10 47.8 211.2 30.3 0.7 

12107/0514:42:20 46.4 211.5 30.2 0.8 

12/07/0514:42:30 46.3 211.4 30.2 0.8 

12107/0514:42:40 47.7 211.4 30.1 0.7 

12J0710514:42:50 47.0 2113 30.1 0.7 

1210710514:43:00 46.8 211.4 30.1 0.6 

12/07/0514:43:10 46.4 211.6 30.0 0.7 

12107/0514:43:20 46.3 211.9 30.0 0.8 

1210710514:43:30 46.0 211.9 30.1 0.7 

1210710514:43:40 45.9 211.7 30.3 0.7 

12/0710514:43:50 47.0 211.7 30.4 0.6 

12/0710514:44:00 47.4 211.7 30.5 0.6 

12/07/0514:44:10 47.0 211.6 30.6 0.7 

12/07/0514:44:20 46.0 211.8 30.7 0.7 

12107/0514:44:30 45.6 211.9 30.6 0.8 

12/07/0514:44:40 45.0 120.7 30.3 0.3 

1210710514:44:50 43.8 118.0 29.5 -1.3 

1210710514:45:00 43.3 66.0 29.5 -0.8 

12107/0514:45:10 45.2 210.6 30.0 0.9 

12107/0514:45:20 44.8 210.9 29.8 0.8 

12/07/0514:45:30 44.8 211.0 29.8 0.7 

12107/0514:45:40 45.1 210.9 29.7 0.7 

12107/0514:45:50 44.5 210.9 29.7 0.8 

12107/0514:46:00 44.2 211.0 29.7 0.8 

1210710514:46:10 44.5 211.1 29.7 0.7 

12/07/0514:46:20 44.5 211.4 29.7 0.7 

12/07/0514:46:30 44.3 211.7 29.8 0.7 

12107/0514:46:40 44.7 212.0 30.0 0.7 

12107/0514:46:50 44.6 212.3. 30.2 0.8 

12107/0514:47:00 44.0 212.3 30.4 0.8 

1210710514:47:10 44.1 212.2 30.5 0.8 

1210710514:47:20 44.5 212.2 30.6 0.7 

12/0710514:47:30 44.1 211.8 30.4 0.8 

1210710514:47:40 44.1 211.9 30.3 0.8 

12/07/0514:47:50 44.6 211.8 30.1 0.9 

12107/0514:48:00 44.0 211.9 29.9 0.8 

12/0710514:48:10 44.7 212.0 29.9 0.7 

12/07/0514:48:20 44.5 211.8 29.8 0.8 

12/07/0514:48:30 45.4 212.1 29.8 0.9 

12/07/0514:48:40 45.2 212.2 29.8 0.8 

12107/0514:48:50 45.1 212.7 29.8 0.8 

12107/0514:49:00 45.4 212.9 30.0 1.0 

12/07/0514:49:10 45.5 213.1 30.2 0.8 

12/07/0514:49:20 45.8 212.9 30.3 0.8 

12/0710514:49:30 46.4 213.1 30.5 0.8 

12/07/0514:49:40 45.8 212.8 30.7 0.8 

12/07/0514:49:50 45.8 212.5 30.7 0.8 

12/07/0514:50:00 46.1 211.8 30.9 0.8 

12/07/0514:50:10 46.2 211.5 30.9 0.8 

12107J0514:50:20 46.6 211.3 30.7 0.8 

12/07/0514:50:30 47.0 211.0 30.5 0.8 

1210710514:50:40 46.3 210.6 30.2 0.8 

12107/0514:50:50 48.0 210.0 30.0 0.8 

12/07/0514:51:00 47.3 209.7 29.8 0.9 

12/0710514:51:10 47.2 209.3 29.7 0.9 

12/07/0514:51:20 47.7 208.9 29.6 0.9 

12/07/0514:51:30 47.9 208.8 29.6 0.9 

12107/0514:51:40 47.0 209.0 29.7 0.9 

12107/0514:51:50 47.1 209.3 29.7 0.8 

12107/0514:52:00 47.3 210.2 29.7 0.8 

12107/0514:52:10 47.4 210.6 30.0 1.0 

1210710514:52:20 46.9 210.7 30.2 1.0 

1210710514:52:30 46.8 210.9 30.3 0.9 

12/07/0514:52:40 46.9 210.6 30.3 1.0 

12/07/0514:52:50 47.0 210.4 30.2 0.9 

12107/0514:53:00 47.0 210.6 30.1 0.9 

12107/0514:53:10 47.3 210.8 30.0 0.9 

12/07/0514:53:20 46.4 211.0 29.9 1.0 

raim 

f 

Page 4 
12/7/05 Run #3 

12/0710514:53:30 46.6 211.2 29.9 0.9 

12/0710514:53:40 46.0 211.3 29.9 0.8 

12107/0514:53:50 47.0 211.2 29.9 0.8 

12/0710514:54:00 46.7 211.1 29.8 0.9 

12/07/0514:54:10 46.2 211.2 29.8 0.9 

12107/0514:54:20 46.2 211.1 29.8 0.9 

12107/0514:54:30 46.0 211.1 29.9 1.0 

12107/0514:54:40 46.1 211.3 30.0 1.0 

12/07/0514:54:50 45.7 211.1 30.3 1.1 

12107/0514:55:00 46.2 211.1 30.5 1.1 

12/07/0514:55:10 45.4 211.2 30.6 1.1 

1210710514:55:20 45.2 211.3 30.8 1.1 

1210710514:55:30 45.3 211.7 30.7 1,0 

12107/0514:55:40 45.1 211.9 30.6 1,0 

1210710514:55:50 45.6 212.2 30.4 0.8 

12/0710514:56:00 45.3 212.2 30.3 0.9 

12/0710514:56:10 44.7 213.0 30.2 0.9 

1210710514:56:20 45.0 213.1 30.1 0.9 

12/07/0514:56:30 45.2 213.0 29.9 0.9 

12107/0514:56:40 45.3 212.7 29.9 1.0 

12/07/0514:56:50 44.8 212.2 29.8 1.0 

12107/0514:57:00 45.3 212.0 29.7 1.1 

12/07/0514:57:10 45.7 212.0 29.8 1.0 

1210710514:57:20 45.2 212.0 29.8 0.9 

12/07/0514:57:30 45.0 211.9 29.9 1.0 

1210710514:57:40 46.2 211.7 30.0 0.9 

12107/0514:57:50 45.1 211.8 30.2 0.9 

12107/0514:58:00 45.5 212.4 30.4 1.0 

12/07/0514:58:10 45.6 212.7 30.5 1.0 

12/07/0514:58:20 45.3 213.0 30.5 0.9 

12/07/0514:58:30 45.9 213.6 30.6 0.9 

12107/0514:58:40 45.9 213.7 30.6 1.0 

12/07/0514:58:50 45.6 213.6 30.4 1.1 

12/07/0514:59:00 45.8 213.4 30.2 1.1 

12107/0514:59:10 46.0 213.9 30.0 1.1 

12107/0514:59:20 45.5 214.5 29.9 1.1 

1210710514:59:30 45.9 214.7 29.8 1.1 

1210710514:59:40 45.6 214.8 29.8 1.1 

12/0710514:59:50 46.0 214.9 29.8 1.1 

1210710515:00:00 45.7 215.2 29.8 1.0 

12/07/0515:00:10 46.2 215.3 29.8 0.9 

12107/0515:00:20 45.9 215.5 29.9 0.9 

12107/0515:00:30 45.2 215.8 30.0 1.0 

12/07/0515:00:40 46.9 215.8 30.2 1.1 

12/07/0515:00:50 45.8 215.3 30.3 1.0 

12/07/0515:01:00 45.1 216.0 30.5 1.1 

12107/0515:01:10 46.0 214.6 30.7 1.1 

12J07/0515:01:20 45.5 214.2 30.8 1.0 

1210710515:01:30 45.1 213.4 30.8 1.0 

12/0710515:01:40 45.7 213.6 30.7 1.0 

12/0710515:01:50 45.2 213.3 30.6 1.0 

12107/0515:02:00 45.1 213.7 30.3 1.0 

12107/0515:02:10 45.0 213.8 30.1 1.0 

12107/0515:02:20 45.4 214.2 30.1 1.0 

12/07/0515:02:30 45.1 214.2 30.0 1.0 

12107/0515:02:40 45.4 214.0 29.9 1.0 

12/07/0515:02:50 45.5 213.5 29.8 0.9 

12/07/0515:03:00 45.2 213.1 29.8 1.0 

12107/0515:03:10 45.2 212.8 29.9 1.0 

12J0710515:03:20 45.7 212.8 30.0 1.1 

1210710515:03:30 45.5 213.1 30.1 1.1 

1210710515:03:40 45.1 212.8 30.3 1.2 

12107/0515:03:50 45.2 212.8 30.4 1.3 

12107/0515:04:00 46.4 212.8 30.5 1.3 

1 2/07105 1 5:04:10 46.5 212.4 30.6 1.3 

12/0710515:04:20 46.0 212.4 30.7 1.2 

12/07/0515:04:30 46.7 212.6 30.7 1.1 

12J07/0515:04:40 46.4 212.7 30.6 1.1 

12107/0515:04:50 46.2 212.9 30.4 1.1 

12/07/0615:05:00 46.7 213.7 30.2 1.1 

12/07/0515:05:10 46.5 213.8 30.1 1.1 

12107/0515:05:20 46.3 213.4 30.0 1.2 

1210710515:05:30 46.0 213.0 30.0 1.2 

12/0710515:05:40 47.0 213.1 29.9 1.1 

n N~ 

Page 5 
1217/05 Run #3 

12107/0515:05:50 47.0 212.8 29:8 1.1 

1210710515:06:00 47.1 212.6 29.8 1.1 

1210710515:06:10 46.7 213.1 29.8 1.1 

12107/0515:06:20 47.0 213.7 29.8 1.0 

12/07/0515:06:30 46.0 214.7 29.8 1.1 

1210710515:06:40 44.5 215.6 30.0 1.2 

12/0710515:06:50 45.7 216.4 30.0 1.2 

12/07/0515:07:00 45.5 216.5 30.2 1.1 

12107/0515:07:10 45.9 217.4 30.2 1.0 

12/07/0515:07:20 46.7 217.8 30.4 1.1 

12/0710515:07:30 45.5 217.9 30.5 1.1 

12107/0515:07:40 45.1 218.0 30.5 1.2 

12107/0515:07:50 45.7 218.1 30.3 1.2 

12/07/0515:08:00 45.7 218.6 30.2 1.3 

12/07/0515:08:10 45.7 219.0 30.0 1.4 

12/07/0515:08:20 45.5 219.0 29.9 1.3 

12/07/0515:08:30 46.3 218.5 29.8 1.1 

12107/0515:08:40 46.4 218.6 29.7 1.1 

12/07/0515;08:50 45.9 218.7 29.7 1.1 

12/07/0515:09:00 46.0 219.0 29.7 1.0 

12/07/0515:09:10 46.8 218.7 29.7 1.1 

12/07/0515:09:20 46.7 218.6 29.7 1.3 

12/07/0515:09:30 45.7 219.1 29.8 1.3 

12107/0515:09:40 45.0 219.4 29.9 1.2 

12/07/0515:09:50 45.0 218.4 30.0 1.3 

12/07/0515:10:00 45.5 217.8 30.1 1.2 

12/07/0515:10:10 45.7 217.4 30.3 1.2 

120710515:10:20 45.7 217.2 30.4 1.1 

12/07/0515:10:30 46.4 217.0 30.5 1.2 

12/07/0515:10:40 45.9 217.2 30.5 1.2 

12107/0515:10:50 46.0 217.3 30.4 1.2 

Stop Run #3 46.13 212.20 30.11 0.71 

12/0710515:11:00 45.9 217.0 30.2 1.3 

12107/0515:11:10 46.5 216.8 30.0 1.2 

12/07/0515:11:20 46.0 216.5 29.9 1.2 

12107/0515:11:30 46.3 216.7 29.8 1.3 

1210710515:11:40 46.1 217.0 29.8 1.2 

1210710515:11:60 46.6 216.9 29.7 1.3 

1210710515:12:00 46.7 216.9 29.6 1.3 

12/0710515:12:10 46.0 216.6 29.7 1.2 

12107/0515:12:20 35.7 163.5 29.6 1.3 

12/07/0515:12:30 4.0 210.6 28.9 1.3 

12/0710515:12:40 1.5 200.4 28.6 1.3 

1210710515:12:50 1.5 148.6 24.8 1.2 

12107/0515:13:00 1.5 96.1 17.9 1.1 

12107/0515:13:10 1.5 60.4 12.9 1.0 

12107/0515:13:20 1.4 38.0 9.7 0.9 

12J07/0515:13:30 1.3 24.6 7.9 0.7 

12107/0515:13:40 0.7 17.7 6.8 0.7 

12107/0515:13:50 0.7 14.7 6.3 0.6 

12/07/0515:14:00 0.6 12.5 9.2 0.5 

12107/0515:14:10 0.6 9.8 14.4 0.7 

12l07/0515:14:20 0.6 7.3 18.3 0.6 

12/07/0515:14:30 0.6 6.2 20.8 0.8 

12107/0515:14:40 0.6 5.9 22.0 0.8 

12107/0515:14:50 0.6 5.8 22.6 0.7 

12107/0515:15:00 0.5 5.7 22.9 0.6 

12107/0515:15:10 0.4 5.5 23.0 0.6 

12107/0515:15:20 0.4 5.4 23.0 0.6 

12/0710515:15:30 0.4 4.9 23.0 0.5 

12107/0515:15:40 0.4 4.7 23.0 0.6 

12107/0515:15:50 0.3 4.4 23.1 0.6 

12/07/0515:16:00 0.4 4.1 23.0 0.6 

1007/0515:16:10 0.4 3.9 23.0 0.5 

12/07/0515:16:20 0.3 3.7 22.9 0.7 

12107/0515:16:30 1.2 3.8 22.6 0.6 

12107/0515:16:40 1.4 3.7 22.6 0.5 

12107/0515:16:50 1.4 4.6 21.5 0.5 

12107/0515:17:00 1.4 5.5 18.8 0.5 

12107/05 15:17:10 0.7 6.2 10.8 0.6 

12/0710515:17:20 0.2 6.6 7.4 0.6 

25.5 ppm NOx 

Zero S02 

ml 

Page 6 
12/7105 Run #3 

12107/0515:17:30 0.2 5.4 5.5 0.6 

12J0710515:17:40 0.2 4.1 4.6 0.7 

12/07/0515:17:50 0.2 3.1 3.9 1.9 

12/07/0515:18:00 0.2 2.6 3.6 4.5 

12/07/0515:18:10 0.2 2.2 3.4 8.9 

12/0710515:18:20 0.2 2.3 3.4 14.9 

12/07/0515:18:30 0.3 2.1 3.3 22.0 

12/0710515:18:40 0.3 2.0 3.2 291 

12/0710515:18:50 0.3 1.7 3.2 36.1 

12107/0515:19:00 0.2 1.7 3.0 43.0 

12107/0515:19:10 0.2 1.7 3.0 49.1 

12107/0515:19:20 0.2 1.8 2.9 54.6 

12/0710515:19:30 0.2 1.6 2.7 59.4 

12/07/0515:19:40 0.2 1.6 2.6 63.6 

12/07/0515:19:50 0.2 1.7 2.6 67.2 

12/07/0515:20:00 0.2 1.7 2.5 70.4 

12107/0515:20:10 0.2 1.8 2.4 73.3 

12/07/0515:20:20 0.2 1.6 2.3 75.8 

1 2107/05 1 5:20:30 0.1 1.7 2.2 77.9 

12/07/0515:20:40 0.2 1.8 2.1 79.9 

12107/0515:20:50 0.1 1.7 2.0 81.6 

12/07/0515:21:00 0.1 2.0 2.0 83.3 

12/0710515:21:10 0.1 2.1 1.9 84.7 

12/0710515:21:20 0.1 2.0 1.8 86.8 

12/07/0515:21:30 0.2 1.8 1.8 86.9 

12/07/0515:21:40 0.2 1.8 1.7 87.8 

12/07/0515:21:50 0.2 1.6 1.6 88.7 

12107/0515:22:00 0.1 1.8 1.6 89.4 

12107/0515:22:10 0.2 1.5 1.6 90.2 

12/07/0515:22:20 0.1 1.5 1.5 90.9 

12/07/0515:22:30 0.1 1.6 1.5 91.5 

12/07/0515:22:40 0.1 1.5 1.4 91.9 

12107/0515:22:50 0.2 1.6 1.4 92.4 

1210710515:23:00 0.2 1.4 1.4 92.7 

1 2/07105 1 5:23:10 0.2 1.4 1.3 92.9 

12/07/0515:23:20 0.2 1.5 1.3 93.1 

12/07/0515:23:30 0.2 1.8 1.2 93.5 

12/07/0515:23:40 0.2 1.9 1.2 93.7 

12/07/0515:23:50 0.2 1.7 1.1 93.9 

1210710515:24:00 0.2 1.8 1.1 94.0 

1210710515:24:10 0.2 1.8 1.0 94.3 

1210710515:24:20 0.2 1.7 1.0 94.7 

12/0710515:24:30 0.1 1.7 1.0 95.1 

1 2107/05 1 5:24:40 0.2 1.9 1.0 95.3 

12/07/0515:24:50 0.2 2.2 1.0 95.6 

12/0710515:25:00 0.2 2.1 0.9 95.9 

12/0710515:25:10 0.2 2.1 0.9 96.3 

12/0710615:25:20 0.2 2.0 0.9 96.5 

12/07/0515:25:30 0.2 2.1 0.8 96.6 

12/07/05 15:25:40 0.1 2.1 0.8 96.7 101 ppm S02 

12/07/05 15:25:50 0.2 2.0 0.8 96.8 Zero CO 

12/0710515:26:00 0.2 1.8 0.8 96.9 

1210710515:26:10 0.6 1.5 0.8 95.9 

12/0710515:26:20 0.2 1.3 0.7 96.0 

12/07/0515:26:30 0.3 11.3 0.8 96.4 

12/07/0515:26:40 0.3 64.2 0.7 93.9 

12/0710515:26:50 0.2 110.3 0.7 87.6 

12107/0515:27:00 0.3 137.8 0.7 79.5 

12/07/0515:27:10 0.3 154.7 0.6 71.1 

12/07/0515:27:20 0.3 164.1 0.7 62.9 

12/0710515:27:30 0.2 170.4 0.6 55.6 

12/0710515:27:40 0.2 174.2 0.6 49.1 

12/07/0515:27:50 0.2 176.0 0.6 43.5 

12/07/0515:28:00 0.2 177.3 0.6 38.6 

12/0710515:28:10 0.2 178.3 0.6 34.4 

12/07/0515:28:20 0.2 178.7 0.5 30.6 

12107/0515:28:30 0.2 179.0 0.5 27.4 

1210710515:28:40 0.2 179.3 0.5 24.5 

12/07/0515:28:50 0.2 179.7 0.6 22.1 

1210710515:29:00 0.2 179.9 0.5 19.9 

1210710515:29:10 0.2 180.0 0.5 18.1 

12107/0515:29:20 0.2 180.1 0.5 16.3 

12/07/05 15:29:30 0.2 180.3 0.6 15.0 200 ppm CO 

a 

~' 

Page 7 
1217105 Run #3 

12107105 15:29:40 0.2 180.5 0.6 13.8 Zero VOC, NOx 

1210710515:29:50 0.2 180.5 0.5 12.6 

1?10710615:30:00 0.2 179.7 0.5 11.6 

12107/0515:30:10 4.0 178.9 0.5 10.7 

1210710515:30:20 45.8 179.6 0.6 9.9 

1210710515:30:30 47.9 164.2 0.6 9.3 

12/07/0515:30:40 47.8 118.0 0.6 8.7 48.8 ppm C3H8 

12/07/0515:30:50 47.8 69.4 0.6 8.1 

12107/0515:31:00 47.7 39.8 0.5 7.7 

12/0710515:31:10 47.7 24.1 0.6 7.3 

1210710515:31:20 46.5 15.6 0.5 6.8 

12I07105 15:31:30 13.1 10.5 0.5 6.3 

12/07105 9 5:31:40 1.5 7.5 0.5 6.1 

Page 8 t o o 
Zero Gas 0 0.5 0.833333 

Upscale 24.8 24 -1.33333 

Average NOx Concentration: 26.86 

Corrected NOx Concentration: 29.59163 

(Equation 6C-1) 

Zero Gas 0 0.28 0.466667 

Upscaie 24.8 22.4 -4 

Average NOx Concentration: 26.87 

Corrected NOx Concentration: 30.92281 

(Equation 6C-1) 

Run #2 

Ru n #3 

0.28 0.466667 -0.36667 0.39 

22.4 -4 -2.66667 23.2 

0.2 0.333333 -0.13333 0.24 

22 -4.66667 -0.66667 22.2 

Sheet1 

Summary of NOx Analyzer Calibrations and Bias 

Plant: Daltile, Muskogee 

Source: Trim Kiln 

Date: 12/8/05 

Analyzer Calibratrion Data 

Cyiinder Analyzer Absolute % Span 

Value Response Difference 

Zero Gas 0 0 0 0 

Mid Range 25.5 24.8 -0.7 -1.16667 

High Range 51 50.88 -0.12 -0.2 

Run #1 

System Calibration Bias and Drift Data 

Analyzer Initial Values Final Values Drift 

Calibration System System System System 

Response Calibration Calibration Calibration Calibration 

Response Bias Response Bias 

Zero Gas 0 0.4 0.666667 0.5 0.833333 0.166667 

Upscale 24.8 22.55 -3.75 24 -1.33333 2.416667 

Average NOx Concentration: 27.56 

Corrected NOx Concentration: 30.28719 

(Equation 6C-1) 

Average 

Calibration 

Values 

0.45 

23.275 

Page 1 1. ;J 1 
Sheet1 

Summary of CO Analyzer Calibrations and Bias 

Plant: Daltile, Muskogee 

Source: Kiln Scrubber Exhaust 

Date: 12/7105 

Analyzer Calibratrion Data 

Cylinder Analyzer Absolute % Span 

Value Response Difference 

Zero Gas 0 1.7 1.7 0.34 

Mid Range 200 203.1 3.1 0.62 

High Range 494 492.65 -1.35 -0.27 

System Calibration Bias and Drift Data 

Analyzer Initial Values Final Values Drift Average 

Calibration System System System System Calibration 

Response Calibration Calibration Calibration Calibration Values 

Response Bias Response Bias 

Run #1 Zero Gas 1.7 0.98 -0.144 0.28 -0.284 -0.14 0.63 

Upscale 203.1 190.1 -2.6 184.68 -3.684 -1.084 187.39 

Average CO Concentration: 155.21 

Corrected CO Concentration: 165.5387 

(Equation 6C-1) 

Run #2 Zero Gas 1.7 0.28 -0.284 0.28 -0.284 0 0.28 

Upscale 203.1 184.68 -3.684 184.68 -3.684 0 184.68 

Average CO Concentration: 155.21 

Corrected CO Concentration: 168.0369 

(Equation 6C-1) 

Run #3 Zero Gas 1.7 0.28 -0.284 -1.22 -0.584 -0.3 -0.47 

Upscale 203.1 184.68 -3.684 182.08 -4.204 -0.52 183.38 

Average CO Concentration: 157.05 

Corrected CO Concentration: 171.3571 

(Equation 6C-1) 

Page 1 

1. ~ ~ 
Sheet1 

Summary of Suifur Dioxide ^, riaiyzer Caiibrations and Bias 

Plant: Daltile, Muskogee 

Source: Trim Kiln 

Date: 12/8/05 

Analyzer Calibratrion Data 

Cylinder Analyzer Absolute % Span 

Value Response Difference 

Zero Gas 0 -0.08 -0.08 -0.07273 

Mid Range 50.1 50 -0.1 -0.09091 

High Range 101 102.8 1.8 1.636364 

System Calibration Bias and Drift Data 

Anaiyzer Initial Values Final Values Drift Average 

Calibration System System System System Calibration 

Response Calibration Calibration Calibration Calibration Values 

Response Bias Response Bias 

Run #1 Zero Gas -0.08 -0.13 -0.04545 0.28 0.327273 0.372727 0.075 

Upscale 102.8 99.65 -2.86364 98.48 -3.92727 -1.06364 99.065 

Average S02 Concentration: 83.63 

Corrected S02 Concentration: 85.25159 

(Equation 6C-1 ) 

Run #2 Zero Gas -0.08 0.28 0.327273 0.2 0.254545 -0.07273 0.24 

Upscale 102.8 98.48 -3.92727 98.6 -3.81818 0.109091 98.54 

Average S02 Concentration: 69.78 

Corrected S02 Concentration: 71.45005 

(Equation 6C-1 ) 

Run #3 Zero Gas -0.08 0.2 0.254545 -0.4 -0.29091 -0.54545 -0.1 

Upscale 102.8 98.6 -3.81818 98.33 -4.06364 -0.24545 98.465 

Average S02 Concentration: 75.17 

Corrected S02 Concentration: 77.12951 

(Equation 6C-1 ) 

Pa9 e1 1.03 
12/8J05 Calibrations 

OatelTime VOC CO NOx S02 

mm/dd/yy hh:mm:ss ppm ppm ppm ppm 

12/08/05 09:23:04 1.8 8.2 0.0 5.8 

12/08/05 09:23:14 1.7 8.2 0.0 5.8 

12/08/05 09:23:24 1.9 8.1 0.0 5.8 

12/08/08 09:23:34 1.9 8.2 0.0 5.8 

12/08105 09:23:44 2.6 3.7 0.0 6.0 

12108105 09:23:54 2.9 2.5 0.0 5.9 

12/08J05 09:24:04 2.2 2.6 0.0 5.9 

12/08105 09:24:14 2.3 2.4 0.0 5.8 

12/08105 09:24:24 2.4 2.5 0.0 5.8 

12/08105 09:24:34 2.5 2.4 0.0 5.8 

12108105 09:24:44 3.4 2.0 42.5 5.9 

12108105 09:24:54 3.2 2.1 51.9 5.9 

12/06105 09:25:04 2.7 2.2 52.1 6.8 

12108J05 09:25:14 3.1 2.2 52.2 5.9 

12/08/05 09:25:24 2.8 2.2 52.2 5.9 

12/08/05 09:25:34 2.7 2.2 51.4 5.8 

12108/05 09:25:44 2.7 2.2 50.4 4.9 

12108J05 09:25:54 2.7 2.2 47.5 0.8 

12l08105 09:26:04 3.2 1.3 50.8 5.6 

12108105 09:26:14 2.5 1.9 50.9 5.6 

12108/05 09:26:24 2.5 1.8 50.9 5.6 

12/08/05 09:26:34 2.6 1.8 50.9 5.5 

12/08/05 09:26:44 2.7 1.8 50.9 5.5 

12108/05 09:26:64 2.2 2.1 28.3 5.4 

12/08/05 09:27:04 1.8 2.4 0.3 5.4 

12/08/05 09:27:14 2.4 2.3 0.1 5.4 

12/08/05 09:27:24 1.9 2.2 0.1 5.5 

12/08/05 09:27:34 1.1 2.1 0.1 5.5 

12/08105 09:27:44 0.8 2.3 0.0 5.6 

12J08l05 09:27:54 0.9 2.0 0.1 5.5 

12108/05 09:28:04 1.1 1.9 0.1 5.5 

12/08/06 09:28:14 1.1 1.8 0.0 5.7 

12108/05 09:28:24 1.0 1.6 0.1 5.6 

12108/05 09:28:34 0.9 1.8 0.1 5.5 

12/08/05 09:28:44 1.0 1.6 0.1 5.5 

12/08/05 09:28:54 1.2 1.7 0.1 5.5 

12/08/05 09:29:04 1.5 1.5 0.0 5.5 

12108/05 09:29:14 1.5 1.6 0.0 5.5 

12108105 09:29:24 2.0 1.5 0.0 5.5 

12108105 09:29:34 2.0 1.5 0.0 5.6 

12/08l05 09:29:44 2.6 2.0 0.0 5.7 

12J08/05 09:29:54 2.3 2.0 2.9 5.6 

12/08/05 09:30:04 2.8 1.6 24.2 5.7 

12/08105 09:30:14 2.3 1.7 24.6 5.7 

12/08/05 09:30:24 2.1 1.8 24.6 5.6 

12/08/05 09:30:34 2.2 1.9 24.7 5.6 

12/08105 09:30:44 2.4 2.0 24.8 5.7 

12/08/05 09:30:54 1.9 2.1 24.8 5.8 

12l08105 09:31:04 1.9 2.3 24.8 5.8 

12/08/05 09:31:14 2.9 2.3 24.8 5.8 

12108/05 09:31:24 2.0 2.2 24.8 4.1 

12/08/05 09:31:34 2.4 2.3 24.8 -0.1 

12/08105 09:31:44 1.8 2.2 11.5 -0.3 

12/08J05 09:31:54 1.7 2.3 0.2 -0.2 

12108105 09:32:04 1.4 2.3 0.0 -0.2 

12108105 09:32:14 1.3 2.4 0.0 -0.3 

12/08105 09:32:24 1.0 2.4 0.0 -0.3 

12108l05 09:32:34 1.0 2.4 0.0 -0.2 

12/08/05 09:32:44 1.4 2.6 0.1 -0.1 

12/08/05 09:32:54 1.2 2.6 0.0 -0.1 

12108l05 09:33:04 1.3 2.7 0.1 -0.1 

12108J05 09:33:14 2.2 2.6 0.1 -0.1 

1 210 810 5 0 9:33:24 2.1 2.6 0.1 -0.1 

12108J05 09:33:34 2.0 10.2 0.0 -0.1 

12108/05 09:33:44 1.9 164.1 0.0 0.0 

12/08/05 09:33:54 2.2 202.1 0.0 0.0 

12/08/05 09:34:04 2.0 202.6 0.0 -0.1 

12108/05 09:34:14 2.1 202.6 0.0 -0.1 

12/08/05 09:34:24 3.2 202.9 0.0 -0.1 

12/08/05 09:34:34 2.1 202.8 0.0 -0.1 

51 ppm NOx 

Zero CO 

25.5 ppm NOx 

1.04 

Page 1 
1218105 Calibrations 

12/08/05 09:34:44 2.0 203.3 0.0 -0.1 200 ppm CO 

12108/05 09:34:54 2.1 203.2 0.0 -0.1 Zero S02 

12108/05 09:35:04 2.0 203.1 0.0 0.0 

12108/05 09:35:14 2.2 114.9 0.0 0.0 

12108/05 09:35:24 2.2 4.4 0.0 -0.1 

12/08/05 09:35:34 2.2 2.7 0.0 -0.1 

12/08/05 09:35:44 2.5 2.5 0.1 -0.1 

12l08/05 09:35:54 1.9 2.3 0.1 -0.1 

12108/05 09:36:04 1.4 2.1 0.0 0.0 

12108/05 09:36:14 1.3 1.9 0.1 0.0 

12108/05 09:36:24 1.0 1.6 0.0 -0.1 

12/08105 09:36:34 11 1.8 0.0 -0.1 

12/08/05 09:36:44 1.5 1.9 0.1 -0,1 

12/08/05 09:36:54 1.7 1.8 0.1 -0.1 

12/08/05 09:37:04 1.7 3.8 0.1 -0.1 

12/08/05 09:37:14 2.8 332.8 0.1 -0.1 

12/08/05 09:37:24 2.7 491.1 0.0 -0.1 

12/08105 09:37:34 2.7 492.3 0.0 0.0 

12/08/05 09:37:44 2.3 492.4 0.0 -0.2 

12/08/05 09:37:54 2.7 492.6 0.0 -0.2 494 ppm CO 

12/08/05 09:38:04 2.8 492.8 0.0 -0.2 

12/08/05 09:38:14 2.5 492.8 0.0 -0.2 

12/08/05 09:38:24 2.2 492.2 0.0 -0.3 

12/08/05 09:38:34 2.3 166.3 0.0 -0.2 

12/08105 09:38:44 2.0 3.4 0.0 -0.3 

12108/05 09:38:54 2.2 2.2 0.0 -0.2 

12/08/05 09:39:04 1.8 2.1 0.0 -0.3 

12/08/05 09:39:14 1.3 2.1 0.0 -0.3 

12/08/05 09:39:24 0.9 1.8 0.0 -0.2 

12/08105 09:39:34 0.8 1.8 0.0 -0.2 

12/08105 09:39:44 1.1 1.9 0.1 0.0 

12/08/05 09:39:54 1.4 2.1 0.1 0.2 

12/08/05 09:40:04 1.4 2.3 0.0 24.3 

12/08/05 09:40:14 1.7 2.4 0.0 79.6 

12/08/05 09:40:24 1.9 2.5 0.0 106.8 

12/08/05 09:40:34 1.7 2.5 0.0 115.3 

12/08/05 09:40:44 2.0 2.3 0.0 117.5 

12/08/05 09:40:54 2.1 2.3 0.0 118.3 

12/08105 09:41:04 2.3 2.5 0.0 118.4 

12/08/05 09:41:14 2.2 2.4 0.0 118.6 

12108/05 09:41:24 2.4 2.4 0.0 118.9 

12/08/05 09:41:34 2.0 2.6 0.0 118.9 

12/08/05 09:41:44 2.4 3.1 0.0 119.1 

12/08/05 09:41:54 2.3 3.1 0.0 119.2 

12/08/05 09:42:04 1.8 3.2 0.0 111.1 

12108105 09:42:14 2.2 3.1 0.0 103.1 

12108/05 09:42:24 1.8 3.1 0.0 103.2 

12/08105 09:42:34 2.0 3.2 0.1 101.3 

12/08/05 09:42:44 1.7 2.9 0.0 102.2 

12108/05 09:42:54 1.7 3.1 0.0 102.1 101 ppm S02 

12/08/05 09:43:04 1.5 3.2 0.0 102.0 

12/08/05 09:43:14 1.5 2.9 0.0 102.0 

12/08/05 09:43:24 1.4 2.9 0.0 101.9 

12/08l05 09:43:34 1.6 3.0 0.0 98.2 

12/08105 09:43:44 1.5 3.0 0.0 56.1 

12/08105 09:43:54 1.6 3.2 0.0 19.9 

12/08/06 09:44:04 1.8 3.0 0.0 5.9 

12/08/06 09:44:14 1.1 2.7 0.0 2.0 

12/08/05 09:44:24 1.1 2.7 0.0 0.8 

12/08/05 09:44:34 1.8 2.4 0.0 0.4 

12/08105 09:44:44 1.8 2.3 0.0 0.2 

12/08/05 09:44:54 1.2 2.3 0.0 0.6 

12/08/05 09:45:04 1.1 1.9 0.1 43.8 

12/08105 09:45:14 1.2 1.9 0.2 43.4 

12108/05 09:45:24 1.9 2.1 0.2 48.2 

12/08/05 09:45:34 1.6 2.0 0.3 49.8 

12/06105 09:45:44 1.8 1.9 0.2 50.0 

12/08l05 09:45:54 1.7 2.0 0.3 50.0 

12/08105 09:46:04 1.7 2.0 0.2 50.0 

12/08/05 09:46:14 1.9 2.0 0.3 50.0 

12/08/05 09:46:24 1.8 2.1 0.2 50.0 50.1 ppm S02 

12108/05 09:46:34 2.0 2.1 0.2 50.0 

Page 2 1.05 
12/8105 Calibrations 

12l08/05 09:46:44 1.7 2.1 0.2 50.0 

12J08105 09:46:54 1.8 2.0 0.2 50.0 

12/08/05 09:47:04 1.8 2,4 0.1 49,0 

12108105 09:47:14 1.5 2,3 0.1 47.0 

12108105 08:47:24 1.6 2.0 0.1 20.8 

12J08/05 09:47:34 1.6 1.9 0.1 6.9 

12108/05 09:47:44 1.8 1,5 0.1 2.8 

12108/05 09:47:54 1.8 1.5 0.1 1.4 

12I08/05 09:48:04 1.9 1.6 0.0 1.0 

12108l05 09:48:14 1.9 1.5 0.0 0.8 

1,06 

Page 3 
12/8/05 Bias Calibrations 

DatelTime VOC CO NOx S02 

mmlddlyy hh:mm:ss ppm ppm ppm ppm 

12108/0510:15:04 2.0 1.4 2.6 0.0 

12/08/0510:15:14 2.3 1.6 1.8 0.1 

12108/0510:15:24 1.7 1.9 1.4 0.1 

1 2108/05 1 0:15:34 0.9 2.1 1.1 0.1 

1210810510:15:44 0.7 2.0 0.8 0.3 

12108/05 10:15:54 0.7 1.7 1.4 0.3 

1210810510:16:04 0.7 1.3 7.3 0.2 

12J0810510:16:14 0.7 1.0 14.0 0.1 

12108105 1 0:16:24 0.7 0.9 17.5 0.0 

12/08/0510:16:34 0.6 0.9 18.8 0.0 

12108/0510:16:44 0.8 1.0 20.2 0.1 

12/08/0510:16:54 0.8 1.0 21.1 0.1 

12108/0510:17:04 1.0 1.0 21.7 0.0 

12108/0510:1714 0.8 1.1 22.0 0.0 

12/08/0510:17:24 0.8 1.0 22.2 •0.1 

12/08/0510:17:34 0.6 1.0 22.3 -0.1 

12108/0510:17:44 0.8 1.1 22.4 -0.1 

12/08/0510:17:54 0.9 0.9 22.4 0.0 

12/08/0510:18:04 0.9 1.0 22.4 0.0 

12108/0510:18:14 0.9 1.0 22.5 -0.1 

12108/0510:18:24 0.8 1.1 22.5 -0.1 

1 2108/05 1 0:18:34 0.9 1.1 22.6 -0.1 

1210810510:18:44 0.8 0.7 22.6 -0.2 

12/08/0510:18:54 0.8 0.8 22.6 -0.2 

12108/0510:19:04 0.8 0.8 21.7 -0.2 

12/08/0510:19:14 1.5 0.8 21.1 -0.3 

12108/0510:19:24 1.8 0.9 21.0 -0.3 

12108/0510:19:34 2.4 0.9 20.7 -0.2 

12/0810510;19:44 2.3 1.5 19.4 0.0 

12/0810510:19:54 1.4 2.1 17.8 0.0 

1 2108/05 1 0:20:04 0.5 2.5 12.6 0.0 

1 2108/05 1 0:20:14 0.1 2.1 6.0 1.9 

12108/0510:20:24 0.1 1.9 2.7 23.3 

12/08/0510:20:34 0.2 1.9 1.6 61.8 

12/0810510:20:44 0.3 0.9 1.3 71.1 

12/08/0510:20:54 0.4 1.0 0.9 82.2 

1 2108/05 1 0:21:04 0.4 1.0 0.7 86.5 

12/08/0510:21:14 0.4 1.0 0.6 92.5 

12/08/0510:21:24 0.3 0.9 0.5 94.9 

1 2/08105 1 0:21:34 0.3 0.9 0.5 96.9 

12108/0510:21:44 0.3 0.9 0.4 97.4 

12/08/0510:21:54 0.3 0.9 0.4 98.3 

12/08/0510:22:04 0.2 0.7 0.4 99.5 

12/08/0510:22:14 0.1 0.8 0.4 99.7 

12/08/0510:22:24 0.1 1.0 0.4 99.1 

12/08/0510:22:34 0.1 0.8 0.4 99.9 

12/08/0510:22:44 0.1 0.8 0.4 99.8 

12/08/0510:22:54 0.2 0.9 0.4 99.8 

12/08/0510:23:04 0.3 1.1 0.4 99.5 

12108/0610:23:14 0.0 1.1 0.4 97.2 

12/08/0510:23:24 0.3 1.3 0.4 94.5 

12/08/0510:23:34 1.1 1.2 0.4 89.4 

12/08/0510:23:44 1.0 1.5 0.4 88.5 

12/0810510:23:54 0.8 1.8 0.4 87.5 

12108/0510:24:04 0.7 11.5 0.5 78.6 

12/08/0510:24:14 0.5 72.8 0.4 50.5 

12/08/0510:24:24 0.7 116.4 0.3 35.5 

12l08/0510:24:34 0.6 136.5 0.2 22.8 

12108/0510:24:44 0.8 148.4 0.2 18.5 

12/08/0510:24:54 0.9 157.1 0.2 9.2 

12108/0510:25:04 0.7 162.2 0.2 9.9 

12108/0510:25:14 0.7 165.4 0.2 8.6 

12/08/0510:25:24 0.7 167.6 0.1 8.9 

12/08/0510:25:34 0.8 168.5 0.1 5.6 

12/08/0510:25:44 0.7 169.2 0.1 4.9 

12108/0510:25:54 0.7 170.2 0.1 4.8 

12/08/0510:26:04 0.8 171.1 0.1 4.2 

12108/0510:26:14 0.9 171.3 0.1 4.4 

12/08/0510:26:24 0.5 172.3 0.1 4.5 

12/0810510:26:34 0.4 174.3 0.1 6.6 

12/08/0510:26:44 0.5 176.6 0.1 5.9 

25.5 ppm NOx Bias 

Zero CO. S02 Bias 

101 ppm S02 Bias 

Zero NOx Bias 

Page 1 

1.() Y 
12/8/05 Blas Calibrations 

12/08/0510:26:54 0.3 178.8 0.1 5.4 

12108/0510:27:04 0.5 180.5 0.1 4.8 

12108/0510:27:14 0.8 182.7 0.1 4.2 

12/08/0510:27:24 0.2 185.6 0.1 3.7 

12/0810510:27:34 0.3 187.3 0.1 3.4 

12108/0510:27:44 0.6 188.6 0.1 3.0 

12108/0510:27:54 0.4 189.4 0.1 2.7 

12108/0510:28:04 0.4 189.9 0.1 2.5 

12108/0510:28:14 0.3 189.8 0.0 2.3 

12/08/05 10:28:24 0.1 190.1 0.1 2.0 200 ppm CO Bias 

12108105 10:28:34 0.1 190.3 0.0 1.9 Zero VOC 

1210810510:28:44 0.2 190.2 0.0 1.7 

12108/0510:28:54 0.2 187.7 0.0 1.5 

1210810510:29:04 0.1 186.2 0.0 1.4 

1210810510:29:14 0.5 185.5 0.1 1.4 

12108/0510:29:24 1.1 182.9 0.1 1.4 

1210810510:29:34 1.1 170.7 0.1 1.4 

12108/0510:29:44 1.5 146.4 0.1 1.5 

1210810510:29:54 34.2 115.1 0.1 1.8 

12/08/0510:30:04 82.2 71.1 0.1 2.2 

12/08/0510:30:14 87.6 41.1 0.2 2.7 

12108/0510:30:24 88.8 23.9 0.2 3.1 

12108/0510:30:34 90.1 16:1 0.1 3.0 

12/08/0510:30:44 90.0 11.7 0.1 2.8 

12/08/0510:30:54 90.1 9.2 0.1 2.3 

12108/05 10:31:04 89.4 7.1 0.1 2.1 

12108/0510:31:14 88.8 5.6 0.1 1.8 

12/08/05 10:31:24 88.9 4.6 0.1 1.6 89.2 ppm C3hl8 

12/08/0510:31:34 88.7 3.8 0.1 1.2 

12/08/0510:31:44 88.4 3.0 0.0 0.9 

12108/0510:31:54 88.5 2.4 0.0 0.9 

12108/0510:32:04 88.1 2.3 0.0 0.9 

12108/0510:32:14 86.6 2.0 0.1 0.7 

12108/0510:32:24 77.8 1.5 0.0 0.6 

1210810510:32:34 55.3 1.5 0.1 0.5 

12/0810510:32:44 33.7 1.3 0.1 0.4 

12/0810510:32:54 2.8 1.4 0.0 0.4 

1210810610:33:04 7.7 1.5 0.1 0.4 

1210810610:33:14 44.7 1.6 0.1 0.4 

12/0810510:33:24 46.8 1.7 0.1 0.4 

1210810510:33:34 47.7 1.9 0.1 0.5 

12/0810510:33:44 47.6 1.6 0.1 0.5 

12/08/05 10:33:54 47.7 1.5 0.1 0.5 48.8 ppm C31-18 

12J08105 10:34:04 47.8 1.3 0.1 0.4 

12108/0510:34:14 47.7 1.1 0.1 0.4 

12/0810510:34:24 45.3 1.2 0.1 0.3 

12/08/0510:34:34 38.3 1.3 0.1 0.3 

12108/0510:34:44 29.4 1.0 0.1 0.3 

12/08/0510:34:54 12.3 1.2 0.1 0.2 

1210810510:35:04 2.3 1.2 0.0 0.1 

1 2108/05 1 0:35:14 74.2 1.3 0.1 0.2 

12108/05 10:35:24 192.8 1.5 0.1 0.2 

12J08/0510:35:34 194.8 1.6 0.1 0.3 

12108/0510:35:44 195.2 1.5 0.1 0.4 

12J08/0510:35:54 195.5 1.2 0.1 0.4 

12/08/0510:36:04 199.6 1.2 0.1 0.4 

12108/0510:36:14 201.8 1.2 0.1 0.3 

12/08/0510:36:24 201.7 1.2 0.1 0.2 

12/08/05 10:36:34 201.8 1.3 0.1 0.2 200 ppm C31

-18 

12/08/0510:36:44 201.6 1.2 0.1 0.1 

12108/0510:36:54 201.6 1.2 0.1 0.1 

1 2108/05 1 0:37:04 200.2 1.2 0.1 0.1 

12108/0510:37:14 192.6 1.2 0.0 0.1 

12108/0510:37:24 139.4 1.2 0.1 0.0 

12108/05 10:37:34 112.8 1.3 0.1 01 

12/08/0510:37:44 8.7 1.1 0.1 0.0 

12108/0510:37:54 3.0 1.3 0.1 0.1 

1 ZJ08/05 10:38:04 2.8 1.6 0.1 0.1 

j. nB 

Page 2 
12/8105 Run #1 

DatelTime VOC CO NOx S02 

mm/ddlyyhh:mm:ss ppm ppm ppm ppm 

1 2108105 1 1:19:28 129.0 148.3 26.3 83.3 

1210810511:19:38 129.4 148.3 26.3 84.0 

1210810511:19:48 129.7 148.2 26.3 84.6 

12108/05 11:19:58 129.9 148.0 26.4 84.9 

Start Run #1 

12/08/0511:20:08 128.9 148.3 26.5 85.0 

1 2108105 1 1:20:18 130.2 147.9 26.5 85.0 

12/0810511:20:28 130.7 147.8 26.5 85.1 

12108l0511:20:38 130.1 147.7 26.5 85.5 

12108105 1 1:20:48 130.9 147.7 26.5 86.2 

1 2108105 1 1:20:58 130.8 147.6 26.5 86.5 

12/0810511:21:08 131.1 147.7 26.4 86.4 

1 2108105 1 1:21:18 129.9 148.2 26.4 86.2 

12/08J0511:21:28 130.8 148.4 26.4 86.0 

1 2108105 1 1:21:38 130.4 148.6 26.4 86.0 

1 2/08105 1 1:21:48 129.9 148.7 26.4 86.4 

12108/0511:21:58 130.7 148.7 26.5 86.7 

12/08/05 11:22:08 130.7 149.1 26.5 86.7 

12108/0511:22:18 130.6 149.1 26.4 86.4 

1210810511:22:28 129.7 149.3 26.3 86.3 

12/08/0511:22:38 129.5 149.5 26.4 85.9 

12108/0511:22:48 129.4 149.5 26.4 85.3 

12108/05 11:22:58 130.3 149.8 26.5 84.3 

12108/0511:23:08 129.8 150.1 26.5 83.0 

1 2/08105 1 1:23:18 129.3 150.3 26.5 81.8 

1 2108/05 1 1:23:28 129.6 150.3 26.6 81.2 

12/08/0511:23:38 128.5 150.5 26.6 81.1 

1210810511:23:48 129.6 150.5 26.7 81.0 

1 2/08105 1 1:23:58 129.5 150.6 26.7 81.0 

1 2108/05 1 1:24:08 129.4 150.6 26.7 80.8 

1 2108105 1 1:24:18 130.0 150.8 26.6 80.8 

1 2108/05 1 1:24:28 128.6 150.9 26.5 80.6 

12/08/0511:24:38 129.9 151.1 26.5 80.4 

12108/0511:24:48 129.6 151.5 26.5 80.3 

12108/0511:24:58 130.2 151.7 26.7 80.1 

1 2108/05 1 1:25:08 129.2 151.5 26.7 80.2 

12/0810511:25:18 129.3 151.2 26.7 80.1 

12108J0511:25:28 129.6 151.2 26.7 80.1 

12/0810511:25:38 127.8 150.6 26.8 80.0 

12/0810511:25:48 128.2 150.1 26.7 80.2 

12108J0511:25:58 128.2 149.8 26.7 80.3 

1 2108/05 1 1:26:08 126.4 149.6 26.7 80.3 

1 2108105 1 1:26:48 126.2 149.9 26.7 80.5 

1210810511:26:58 126.6 150.0 26.6 80.5 

12108/0511:27:08 126.0 149.7 26.6 80.6 

12/08/0511:27:18 125.8 149.6 26.6 80.6 

1210810511:27:28 125.9 149.7 26.6 80.7 

12108/0511:27:38 126.8 149.6 26.6 80.7 

1210810511:27:48 127.7 149.6 26.6 80.6 

12108/0511:27:58 128.2 149.7 26.6 80.4 

12108/0511:28:08 128.0 149.7 26.6 80.2 

1 2108105 1 1:28:18 127.5 149.8 26.7 79.9 

1210810511:28:28 127.9 149.9 26.7 79.6 

1210810511:28:38 127.1 149.7 26.7 79.6 

12108/0511:28:48 128.4 149.6 26.8 80.1 

12/0810511:28:58 128.4 149.6 26.8 80.8 

12108/0511:29:08 128.5 149.5 26.8 81.5 

12108/0511:29:18 129.2 149.4 26.8 82.3 

1210810511:29:28 128.8 149.2 26.8 83.1 

1210810511:29:38 130.2 148.9 26.8 83.7 

1210810511:29:48 130.0 148.6 26.9 84.2 

1 2/08105 1 1:29:58 131.9 148.3 26.8 84.6 

1 2108105 1 1:30:08 131.8 148.0 26.8 84.9 

12108/0511:30:18 133.7 147.7 26.8 85.0 

12108/0511:30:28 133.5 147.5 26.9 85.3 

1210810511:30:38 135.0 147.4 26.9 85.5 

1210810511:30:48 135.3 147.4 26.9 85.9 

1210810511:30:58 136.3 147.4 27.0 86.2 

1 2108105 1 1:31:08 135.8 147.6 27.1 86.4 

1210810511:31:18 135.0 147.5 27.2 86.7 

1210810511:31:28 135.5 147.4 27.2 86.6 

jn9 

Page 1 
1218105 Run #1 

1 2108105 1 1:31:38 137.1 147.5 27.2 86.5 

12/0810511:31:48 137.6 147.5 27.3 86.4 

1210810511:31:58 137.1 147.7 27.2 86.4 

1 2/08105 1 1:32:08 139.0 147.8 27.2 86.5 

12l0810511:32:18 139.3 147.7 27.3 86.3 

1 2/08105 1 1:32:28 141.0 147.7 27.4 86.2 

1210810511:32:38 141.0 147.8 27.5 86.0 

1 2/08106 1 1:32:48 141.7 148.5 27.6 86.0 

12l0810511:32:58 142.5 149.0 27.7 86.1 

12l0810511:33:08 142.8 149.4 27.7 86.3 

1210810511:33:18 142.9 150.1 27.7 86.8 

1 2108/05 1 1:33:28 144.1 150.9 27.7 86.9 

1 2108/05 1 1:33:38 144.9 151.6 27.8 87.1 

1210810511:33:48 145.4 152.3 27.7 87.2 

12108/0511:33:58 147.9 153.5 27.9 87.4 

12108/0511:34:08 149.1 154.5 27.9 87.7 

1210810511:34:18 149.0 155.2 28.0 87.8 

1 2108105 1 1:34:28 156.3 158.0 28.4 88.0 

1 2108105 1 1:34:38 161.2 159.9 29.2 89.3 

1270810511:34:48 161.8 160.0 29.4 91.0 

1210810511:34:58 165.6 159.6 29.2 91.0 

12108105 1 1:35:08 166.2 159.3 29.1 90.1 

1210810511:35:18 165.4 158.8 28.9 89.1 

1 2/08105 1 1:35:28 '164.3 158.3 28.7 88.3 

1210810511:35:38 163.3 158.3 28.6 88.1 

12/0810511:35:48 163.6 158.4 28.6 88.0 

12108/0511:35:58 162.5 158.1 28.6 88.1 

12108/0511:36:08 162.2 157.8 28.7 88.1 

12108/0511:36:18 163.1 157.4 28.6 88.0 

12/08l0511:36:28 162.2 157.4 28.5 87.9 

12/0810511:36:38 162.1 157.6 28.4 87.8 

1210810511:36:48 161.6 157.5 28.2 87.7 

12/0810511:36:58 162.3 157.7 28.2 87.5 

12/08l0511:37:08 161.5 157.6 28.1 87.4 

12/0810511:37:18 160.4 157.4 28.1 87.3 

12108105-11:37:28 162.8 157.3 28.1 87.3 

12/08/0511:37:38 160.1 157.2 28.2 87.3 

12108/0511:37:48 161.2 157.2 28.2 87.4 

12/0810511:37:58 158.5 157.2 28.1 87.6 

12/0810511:38:08 158.8 156.8 28.1 87.5 

12108/0511:38:18 159.0 156.3 28.1 87.5 

12108/0511:38:28 160.6 156.0 28.1 87.6 

12108/0511:38:38 160.6 155.3 28.0 87.7 

12108/0511:38:48 160.6 155.0 28.1 87.7 

12108/0511:38:58 159.1 154.7 28.1 87.8 

12108/0511:39:08 159.7 154.8 28.1 87.9 

1 2108/05 1 1:39:18 160.9 155.0 28.0 88.0 

12/08/0511:39:28 160.1 155.0 28.0 88.1 

12/08/0511:39:38 160.4 155.3 28.0 88.0 

12J08/0511:39:48 157.4 155.4 28.1 86.0 

12/08/0511:39:58 157.6 155.4 28.0 88.0 

12l0810511:40:08 158.0 155.5 28.0 88.0 

12108/0511:40:18 157.8 155.8 28.0 88.0 

12/0810511:40:28 157.6 156.2 28.0 88.1 

12/0810511:40:38 156.4 156.1 27.9 88.1 

12/0810511:40:48 157.3 156.1 28.0 88.1 

1 2108/05 1 1:40:58 158.1 156.3 28.0 88.2 

12108/0511:41:08 158.5 156.8 28.1 88.2 

12/0810511:41:18 157.8 157.4 28.2 87.9 

1 2/08105 1 1:41:28 157.8 158.1 28.1 87.8 

12/0810511:41:38 157.1 158.6 28.1 87.9 

12108/05 11:41:48 171.4 159.1 28.1 88.1 

12108J0511:41:58 174.3 159.2 28.2 88.5 

12/08105 11:42:08 194.0 159.4 28.2 88.8 

1210810511:42:18 174.7 159.5 28.3 88.9 

12108105 1 1:42:28 171.3 159.3 28.3 88.7 

1210810511:42:38 169.7 159.3 28.2 88,6 

1210810511:42:48 168.8 159.2 28.1 88.6 

1 2108105 1 1:42:58 168.8 159.3 28.1 88.7 

1 2/08105 1 1:43:08 168.8 159.6 28.0 89.1 

12108105 11:43:18 168.8 160.1 28.0 89.2 

1210810511:43:28 187.5 160.3 28.0 89.2 

1210810511:43:38 183.2 160.4 28.0 89.1 

1 2108105 1 1:43:48 179.8 160.4 28.0 89.1 

1.10 

Page 2 
12/8/05 Run #1 

1210810511:43:58 178.6 160.0 28.0 89.1 

12108/0511:44:08 177.7 159.7 28.0 89.0 

12/08/0511:44:18 176.2 159.5 28.0 88.9 

1210810511:44:28 176.4 159.4 27.9 88.8 

1 2/08105 1 1:44:38 174.5 159.0 27.9 88.6 

1 2/08105 1 1:44:48 171.1 72.0 27.3 86.9 

12/08J0511:44:58 171.9 136.8 27.7 88.5 

12/08/0511:45:08 170.2 158.6 27.9 88.4 

1 2108/05 1 1:45:18 168.9 158.8 27.9 88.3 

12/08/05 11:45:28 169.6 159.3 27.9 88.3 

12/08/05 11:45:38 166.7 ' 159.5 27.9 88.3 

1 2108/05 1 1:45:48 166.3 160.3 27.8 88.1 

12/0810511:45:58 166.1 160.7 27.8 88.2 

12108/0511:46:08 166.2 161.1 27.7 88.2 

12/08/0511:46:18 165.3 161.9 27.7 88.3 

12108/0511:46:28 164.8 162.8 27.7 88.4 

1 2108/05 1 1:46:38 164.7 163.8 27.7 88.5 

12/08/0511:46:48 164.7 164.5 27.7 88.4 

1 2108/05 1 1:46:58 163.6 165.2 27.8 88.3 

12/08/0511:47:08 164.7 165.4 27.9 88.2 

12/08/0511:47:18 166.7 165.6 27.9 88.0 

1210810511:47:28 165.6 165.8 27.9 88.0 

12/0810511:47:38 164.7 165.6 27.9 87.8 

12108/0511:47:48 167.7 165.8 27.8 87.7 

12108/0511:47:58 164.4 167.1 28.0 87.9 

1210810511:48:08 164.7 167.7 28.1 88.2 

12108/0511:48:18 164.7 167.8 28.0 88.1 

1210810511:48:28 166.7 167.4 28.0 87.8 

12/08/0511:48:38 165.6 167.3 28.0 87.6 

1210810511:48:48 164.7 166.5 28.0 87.5 

12/08/0511:48:58 167.7 166.3 28.0 87.6 

12/08/0511:49:08 164.4 165.9 27.9 87.6 

12/08/0511:49:18 164.7 . 165.6 27.9 87.6 

12/08/0511:49:28 166.7 165.1 27.9 87.5 

12108/0511:49:38 165.6 164.8 27.9 87.4 

12/08/0511:49:48 164.7 164.2 28.0 87.4 

12108/0511:49:58 167.7 163.1 28.0 87.4 

1 2108/05 1 1:50:08 164.4 162.5 28.0 87.3 

12/08/0511:50:18 164.7 162.5 28.0 87.1 

12108/0511:50:28 166.7 161.9 27.9 87.1 

12108/0511:50:38 165.6 161.6 28.0 87.1 

12/08/0511:50:48 164.7 161.2 28.0 87.0 

12/0810511:50:58 167.7 161.0 28.0 87.1 

1 2108/05 1 1:51:08 164.4 160.8 27.9 87.2 

12/0810511:51:18 164.7 160.8 27.9 87.1 

12/08/0511:51:28 164.7 161.0 27.9 87.1 

12108/0511:51:38 164.7 161.1 27.9 87.0 

1 2108/05 1 1:51:48 175.2 160.7 27.7 86.7 

12108l0511:51:58 130.6 160.8 27.6 86.4 

1 2108/05 1 1:52:08 121.2 161.3 27.5 86.2 

12/08/0511:52:18 122.1 161.8 27.6 86.1 

12108/0511:52:28 122.6 162.0 27.6 86.1 

1 2108/05 1 1:52:38 121.2 162.1 27.8 86.3 

12/08/0511:52:48 123.1 162.1 27.9 86.5 

12/08/0511:5258 122.9 162.1 27.9 86.5 

1 2108/05 1 1:53:08 122.2 162.0 27.9 86.8 

12108/0511:53:18 122.2 161.6 27.8 87.1 

12/08/0511:53:28 122.8 160.9 27.8 87.4 

1 2108/05 1 1:53:38 123.1 160.1 27.8 87.5 

12108/0511:53:48 123.0 159.8 27.8 87.6 

1 2108/05 1 1:53:58 122.1 159.5 27.7 87.5 

12108/0511:54:08 122.5 159.2 27.8 87.4 

12/08/0511:54:18 122.8 158.9 27.8 87.4 

12/0810511:54:28 122.6 158.7 27.7 87.4 

12108/0511:54:38 122.4 158.3 27.6 87.2 

12/08/0511:54:48 122.4 157.9 27.6 86.8 

12/08/0511:54:58 122.1 157.7 27.6 86.5 

12/08/0511:55:08 121.4 157.6 27.6 86.2 

12108/0511:55:18 122.3 157.0 27.7 86.1 

12108/0511:55:28 122.0 156.1 27.6 86.0 

12/08/0511:55:38 123.0 155.2 27.6 85.8 

12108/0511:55:48 123.2 154.6 27.6 85.7 

12/0810511:55:58 123.2 154.2 27.6 85.6 

12/08/0511:56:08 122.6 154.1 27.6 85.4 

1ti 

Page 3 
1218105 Run #1 

12/08/0511:56:18 122.9 153.5 27.5 85.5 

12108/0511:56:28 122.6 153.6 27.4 85.3 

1210810511:56:38 123.3 153.6 27.4 85.2 

12108/0511:56:48 122.2 153.4 27.4 85.2 

12/08/0511:56:58 123.4 153.3 27.5 85.3 

12/08/05 11:57:08 121.8 153.2 27.5 85.4 

12/08/0511:57:18 122.9 153.1 27.5 85.6 

12/08/0511:57:28 121.8 152.7 27.5 85.7 

12/08/0511:57:38 122.6 152.8 27.5 85:6 

12108/0511:57:48 122.5 152.7 27.2 85.5 

12/0810511:57:58 122.1 152.4 27.1 85.4 

12/08/0511:58:08 121.5 152.3 27.1 85.2 

1210810511:58:18 122.5 152.2 27.1 84.9 

12/08/0511:58:28 122.7 152.0 27.1 84.9 

12/0810511:58:38 122.5 151.9 27.2 84.9 

12/0810511:58:48 122.0 152.6 27.3 85.0 

12/0810511:58:58 122.3 152.9 27.4 85.2 

12108/0511:59:08 124.6 153.5 27.5 85.4 

12/08/0511:59:18 125.3 154.1 27.5 85.5 

12/08/0511:59:28 126.5 154.4 27.6 85.6 

12/08/0511:59:38 126.8 154.6 27.6 85.7 

1 2108/05 1 1:59:48 127.2 154.3 27.5 85.7 

12108/0511:59:58 126.9 154.3 27.4 85.3 

12/0810512:00:08 126.5 154.2 27.4 85.1 

1210810512:00:18 126.2 153.7 27.4 85.0 

12/0810512:00:28 128.1 153.4 27.5 84.4 

12/08/0512:00:38 128.9 153.2 27.6 83.7 

12108/0512:00:48 126.8 153.5 27.9 82.9 

12/08/05 12:00:58 127.3 153.7 27.9 82.3 

12108/0512:01:08 126.1 153.7 27.9 81.6 

12/08/0512:01:18 127.3 154.0 27.8 80.8 

12/08/0512:01:28 127.3 154.3 27.7 80.3 

12108/0512:01:38 127.3 154.6 27.7 79.9 

12/08/0512:01:48 126.3 155.0 27.6 79.8 

12108/0512:01:58 127.4 155.5 27.5 79.7 

12108/0512:02:08 127.0 156.2 27.5 79.8 

12/08/0512:02:18 126.3 156.7 27.4 79.8 

1210810512:02:28 126.9 157.2 27.5 80.1 

12108/0512:02:38 126.2 157.2 27.4 80.0 

12108/0512:02:48 125.9 157.4 27.5 80.2 

12108/0512:02:58 127.2 157.4 27.6 80.4 

12108/0512:03:08 126.7 157.4 27.6 80.5 

12/08/0512:03:18 126.7 157.6 27.6 80.8 

12108/0512:03:28 123.1 69.1 26.8 79.2 

12/08/0512:03:38 127.5 157.5 27.6 80.3 

12108/0512:03:48 128.8 157.4 27.5 80.4 

12/08/0512:03:58 128.0 157.2 27.5 80.4 

12/08/0512:04:08 128.4 157.4 27.6 80.3 

12108/0512:04:18 129.1 156.9 27.5 80.3 

12/08105 12:04:28 128.7 156.4 27.6 80.3 

12/0810512:04:38 129.0 156.3 27.6 80.1 

12/0810512:04:48 128.9 156.0 27.6 80.0 

12/08/0512:04:58 129.0 155.8 27.6 79.7 

12/08/0512:05:08 127.6 155.6 27.6 79.4 

12/08/05 12:05:18 127.5 155.5 27.5 79.3 

12108/05 12:05:28 127.2 155.0 27.5 79.2 

12108/0512:05:38 127.8 154.4 27.5 79.1 

12/0810512:05:48 128.1 154.0 27.7 78.9 

1210810512:05:58 127.3 153.6 27.8 78.6 

12108/0512:06:08 128.3 153.0 27.8 78.2 

1210810512:06:18 127.8 153.0 27.8 77.4 

12108/0512:06:28 127.9 152.8 27.8 76.9 

12108/0512:06:38 127.2 153.2 27.8 76.4 

12/08/0512:06:48 128.6 154.0 27.8 76.2 

12/08/0512:06:58 127.6 154.7 27.8 76.0 

12/08/0512:07:08 129.2 155.5 27.8 76.0 

12/08/0512:07:18 128.1 156.2 27.7 76.0 

12/08/0512:07:28 127.4 156.6 27.6 76.1 

12/08/0512:07:38 128.5 156.8 27.5 76.5 

12/08/0512:07:48 128.6 157.0 27.5 76.8 

12/0810512:07:58 128.1 157.2 27.5 77.1 

12/08/0512:08:08 128.5 157.5 27.5 77.6 

12/0810512:08:18 128.3 157.6 27.4 77.7 

12108/0512:08:28 128.5 157.6 27.4 77.7 

1. 1. 2 

Page 4 
1218105 Run #1 

12/08/0512:08:38 128.2 157.7 27.4 77.8 

12108/0512:08:48 129.0 157.7 27.4 77.9 

12/08/0512:08:58 128.6 157.7 27.4 78.0 

12/08/0512:09:08 128.3 157.7 27.5 78.1 

12108/0512:09:18 128.8 157.9 27.6 78.5 

12/08/0512:09:28 128.4 158.1 27.6 78.6 

12/08/0512:09:38 128.0 158.1 27.6 78.7 

12/08/0512:09:48 129.0 158.1 27.6 78.6 

12108/0512:09:58 129.5 157.7 27.6 78.6 

12108/0512:10:08 129.1 157.5 27.6 78.6 

12/08/0512:10:18 129.2 187.5 27.6 78.5 

1210810512:10:28 129.7 157.7 27.4 78.6 

12108/0512:10:38 129.5 157.8 27.5 78.6 

12108/05 121 0:48 129.9 157.8 27.5 78.7 

1 2108105 1 2:10:58 129.2 158.0 27.6 78.8 

12/08/05 12:11 :08 129.3 158.0 27.5 79.0 

1210810512:11:18 129.3 158.0 27.6 79.0 

12/08/0612:11:28 128.8 157.4 27.6 79.1 

12108/0512:11:38 129.8 156.6 27.7 79.1 

1210810512:11:48 128.7 156.1 27.7 79.1 

12/08/0512:11:58 129.2 156.0 27.7 79.1 

1210810512:12:08 128.9 155.8 27.8 79.0 

12/08/0512:12:18 129.1 155.7 27.7 79.0 

1210810512:12:28 129.6 155.9 27.7 78.9 

12/08/0512:12:38 129.5 155.9 27.7 79.1 

12108/0512:12:48 129.1 155.9 27.7 79.3 

12108/0512:12:58 129.4 156.1 27.6 79.3 

1 2108/05 1 2:13:08 129.3 156.4 27.5 79.4 

12/08/0512:13:18 129.1 156.6 27.5 79.3 

12108/0512:13:28 128.7 156.8 27.6 79.1 

12/08/0512:13:38 128.1 157.3 27.6 78.8 

12108/0512:13:48 128.2 157.7 27.6 78.6 

12/08/0512:13:58 129.4 158.0 27.5 78.2 

12108/0512:14:08 128.4 158.0 27.5 77.7 

12108/0512:14:18 128.3 158.3 27.4 77.4 

12/08105 1214:28 128.2 158.5 27.2 77.2 

12108/0512:14:38 128.3 158.6 27.3 76.9 

12108/0512:14:48 127.4 158.7 27.3 76.7 

12108/0512:14:58 127.9 158.8 27.3 76.5 

1210810512:15:08 128.1 158.4 27.2 76.4 

1 2108/05 1 2:15:18 127.3 158.1 27.2 76.2 

1210810512:15:28 127.9 157.6 27.2 75.9 

12/08/0512:15:38 126.8 157.3 27.3 75.8 

12/0810512:15:48 127.5 156.8 27.2 75.8 

12108/0512:15:58 127.6 156.3 27.2 75.7 

12/08/0512:16:08 127.5 156.2 27.2 75.6 

12/08/0512:16:18 127.3 156.2 27.2 75.8 

1 2108/05 1 2:1 fi:28 127.4 156.2 27.2 76.2 

12108/0512:16:38 125.9 156.1 27.2 76.6 

12108/0512:16:48 125.6 156.1 27.2 76.8 

12108/0512:16:58 126.5 156.5 27.3 76.9 

12108/0512:17:08 125.5 156.8 27.3 77.1 

1 2108/05 1 2:17:18 126.3 157.1 27.4 77.3 

12108/0512:17:28 125.6 157.5 27.4 77.6 

12108/0512:17:38 126.0 157.8 27.4 77.7 

12/0810512:17:48 125.6 157.5 27.4 78.1 

12/0810512:17:58 125.6 157.0 27.5 78.7 

12108/0512:18:08 125.0 156.5 27.4 79.0 

12/0810512:18:18 125.2 156.1 27.5 79.4 

12/0810512:18:28 125.6 155.7 27.5 79.6 

12/0810512:18:38 126.1 155.4 27.6 80.0 

12/0810512:18:48 126.8 154.8 27.6 80.4 

1210810512:18:56 125.3 154.7 27.6 80.7 

12/0810512:19:06 126.9 154.6 27.6 81.0 

12/0810512:19:18 127.9 154.6 27.7 81.5 

12/0810512:19:28 127.5 154.9 27.7 82.0 

1 2/08105 1 2:19:38 127.8 155.4 27.9 82.4 

12/08/0512:19:48 128.2 155.6 27.9 82.9 

12/08/0512:19:58 128.4 155.8 28.0 83.2 

12108l0512:20:08 128.1 156.1 28.0 83.4 

1210810512:20:18 128.5 156.4 28.0 83.5 

12108/0512:20:28 129.1 156.5 27.9 83.6 

12108105 1 2:20:38 128.9 156.5 27.9 83.7 

12108/0512:20:48 129.1 156.4 27.9 83.9 

1.~.3 

Page 5 
1218105 Run #1 

12/08/0512:20:58 128.8 156.7 27.9 84.1 

12/08/0512:21:08 129.0 156.7 27.9 84.2 

12108/0512:21:18 129.3 156.8 27.9 84.4 

12/08/0512:21:28 129.0 156.9 27.9 84.3 

12108/0512:21:38 129.0 156.9 27.9 84.0 

12108/0512:21:48 129.3 156.8 27.9 83.7 

12/0810512:21:58 128.8 156.4 27.9 83.4 

12108J0512:22:08 128.7 156.3 27.8 82.9 

12/0810512:22:18 129.2 156.4 27.8 82.7 

12/08/0512:22:28 128.1 156.6 27.8 82.4 

1 2108105 1 2:22:38 128.0 156.7 27.7 82.1 

12/08105 12:22:48 128.2 156.5 27.7 81.8 

12/0810512:22:58 128.8 156.1 27.6 81.6 

1210810512:23:08 129.0 156.0 27.7 81.1 

12108l0512:23:18 128.5 155.7 27.8 80.8 

12J0810512:23:28 128.3 155.8 27.7 80.6 

12J0810512:23:38 128.3 155.7 27.7 80.5 

12/08l0512:23:48 127.7 155.6 27.7 80.4 

12108/0512:23:58 125.0 111.4 27.4 79.4 

Stop Run #1 138.61 155.21 27.55 83.63 

12/08/0512:24:08 126.6 142.8 27.6 80.3 

12/08/0512:24:18 126.6 155.7 27.6 80.0 

12108/0512:24:28 122.9 148.9 27.0 79.3 

12/08/0512:24:38 125.5 148.5 27.4 79.7 

12/08/0512:24:48 125.6 154.3 27.5 79.4 

1210810512:24:58 122.0 153.0 27.4 79.1 

12/0810512:25:08 31.6 150.2 26.5 78.0 

12/0810512:25:18 5.3 110.2 26.0 75.3 

1 2/08105 1 2:25:28 6.0 122.4 24.2 74.7 

1210810512:25:38 5.1 87.1 18.2 70.0 

12/0810512:25:48 5.0 60.7 13.3 61.9 

1210810512:25:58 4.9 41.0 9.6 52.8 

12108/0512:26:08 4.4 28.4 7.1 44.1 

1210810512:26:18 4.6 20.1 5.4 36.5 

12/0810512:26:28 4.6 15.6 4.3 30.2 

12/08/0512:26:38 4.3 12.6 3.5 25.1 

12108/0512:26:48 4.5 11.6 3.2 20.8 

12108/0512:26:58 4.0 10.7 3.1 17.9 

1 2108/06 1 2:27:08 3.5 9.1 2.8 15.7 

12108/0512:27:18 3.1 6.4 4.4 13.2 

12/0810512:27:28 2.8 4.8 9.8 11.1 

12108/0512:27:38 3.0 3.8 14.4 9.4 

12/0810512:27:48 3.2 3.5 17.2 8.5 

12/0810512:27:58 2.9 3.0 18.9 7.7 

12/08/0512:28:08 2.8 2.7 20.1 8.9 

12/08/0512:28:18 3.3 1.7 21.0 6.2 

12/08/0512:28:28 2.8 1.3 21.5 5.4 

1210810512:28:38 2.8 1.2 21.7 4.8 

12108/0512:28:48 2.8 1.4 21.8 4.3 

12/08/0512:28:58 3.0 1.1 21.8 3.8 

12/08/0512:29:08 2.8 0.9 21.8 3.4 

12/08/0512:29:18 2.8 1.1 21.7 3.0 

12108/0512:29:28 3.3 1.0 21.8 2.7 

12/0810512:29:38 2.8 0.9 21.9 2.4 

12J0810512:29:48 2.9 0.9 21.9 2.0 

12/0810512:29:58 3.1 0.8 22.2 1.9 

100810512:30:08 3.2 0.8 22.5 1.7 

12/0810512:30:18 3.4 0.6 22.6 1.3 

12/0810512:30:28 3.0 0.7 22.7 1.1 

12108105 1 2:30:38 3.4 0.5 23.1 0.9 

1210810512:30:48 3.4 0.4 23.6 0.8 

12/08l0512:30:58 3.4 0.3 23.8 0.6 

12/08/0512:31:08 3.2 0.3 24.0 0.4 

1210810512:31:18 3.3 0.2 24.0 0.3 25.5 ppm IVOx 

12/08J0512:31:28 3.9 0.3 24.0 0.2 

1 2108/05 1 2:31:38 3.3 0.3 24.0 0.2 

12/08/0512:31:48 3.5 0.3 24.0 0.4 

12/08/0512:31:58 3.8 0.3 23.7 0.3 

12/08/0512:32:08 3.9 0.2 23.0 0.4 

12/08/0512:32:18 3.4 0.3 22.4 0.3 

12108/0512:32:28 3.7 0.2 22.2 0.3 

1.~ .4 

Page 6 
12/8/05 Run #1 

12/0810512:32:38 4.7 0.2 21.7 0.3 

12108/0512:32:48 5.1 0.3 19.6 0.4 

1210810512:32:58 4.9 0.9 17.0 0.6 

12108/0612:33:08 4.5 1.2 12.1 0.9 

12/08/0512:33:18 4.4 0.8 7.0 1.9 

12/08/0512:33:28 4.6 0.3 3.9 6.8 

12108/0512:33:38 4.6 0.2 2.9 15.6 

12108/0512:33:48 4.6 0.1 2.0 26.9 

12/08/0512:33:58 4.7 0.0 1.5 39.1 

12/08/0512:34:08 4.9 0.1 1.2 48.9 

12108/0512:34:18 4.4 0.2 0.9 58.5 

12J0810512:34:28 4.4 0.1 0.8 66.7 

12/0810512:34:38 5.1 0.1 0.7 72.4 

12J0810512:34:48 4.4 0.1 0.7 76.9 

12/0810512:34:58 4.6 0.1 0.6 80.1 

1210810512:35:08 4.4 0.1 0.6 82.9 

1210810512:35:18 4.3 0.1 0.6 85.4 

12/0810512:35:28 4.9 0.1 0.6 87.5 

1210810512:35:38 4.6 0.1 0.5 89.0 

12/08/0512:35:48 4.6 0.1 0.5 90.6 

12/0810512:35:58 4.5 0.1 0.5 92.3 

12/0810512:36:08 4.3 0.1 0.5 93.7 

1210810512:36:18 4.3 0.2 0.5 94.9 

1210810512:36:28 4.3 0.2 0.5 95.8 

12J0810512:36:38 4.4 0.1 0.5 96,4 

1210810512:36:48 4.3 0.1 0.5 96.7 

12/0810512:36:58 4.4 -0.1 0.5 97.0 

12108/0512:37:08 4.5 0.1 0.5 97.4 

12/0810512:37:18 4.3 0.1 0.5 97.9 

12/0810512:37:28 4.3 -0.1 0.5 98.2 

12108/0512:37:38 4.5 -0.1 0.5 98.3 

12108/0512:37:48 4.5 -0.1 0.5 98.4 

12/0810512:37:58 4.3 -0.2 0.5 98.4 

1210810512:38:08 4.4 -0.2 0.5 98.4 

12/0810512:38:18 3.9 -0.2 0.5 98..5 

12/0810512:38:28 3.6 -0.3 0.4 98.4 

12/08105 12:38:38 4.1 -0.4 0.4 97.1 ' 

1210810512:38:48 3.7 -0.4 0.4 96.6 

12/08J0512:38:58 4.0 -0.2 0.5 97.2 

12/0810512:39:08 3.8 21.5 0.5 96.2 

1210810512:39:18 3.8 86.9 0.5 89.3 

12108/0512:39:28 3.9 128.0 0.4 76.5 

12/08/0512:39:38 3.9 152.4 0.4 62.7 

12/08/0512:39:48 3.9 168.1 0.4 49.8 

12108/0512:39:58 3.9 176.4 0.3 39.6 

1210810512:40:08 4.0 181.9 0.3 31.6 

12108J0512:40:18 3.9 184.9 0.3 25.5 

1210810512:40:28 3.8 184.7 0.3 21.1 

12/0810512:40:38 3.7 184.5 0.3 17.7 

12/0810512:40:48 3.8 184.6 0.3 15.4 

12/0810512:40:58 3.7 181.2 0.3 13.2 

12/08J0512:41:08 3.5 178.2 0.3 11.5 

12/0810512:41:18 3.4 176.0 0.3 10.2 

12108/0512:41:28 3.9 177.2 0.3 9.0 

12/08/0512:41:38 77.8 177.6 0.3 8.5 

12/08/0512:41:48 93.9 168.0 0.3 8.2 

12/08/0512:41:58 92.9 137.7 0.3 7.9 

12/08/0512:42:08 92.9 90.0 0.3 7.6 

12/08/0512:42:18 93.0 52.8 0.3 7.3 

12108J0512:42:28 92.9 34.4 0.3 7,0 

1210810512:42:38 92.9 24.1 0.3 6.6 

1210810512:42:48 93.0 17.2 0.2 6.1 

101 ppm S02 

200 ppm CO 

Zero VOC 

Page 7 ~. ~ ~ 
12/8/05 Run #2 

Date/7'ime VOC CO fVOx S02 

mmldd/yy hh:mm:ss ppm ppm ppm ppm 

12/08/0512:49:28 129.7 150.1 27.9 84.9 

1210810512:49:38 128.6 149.9 28.0 86.8 

12/08/0512:49:48 128.8 150.4 28.0 88.0 

12/08/0512:49:58 128.9 151.1 27.9 8B.9 

Start Run #2 

12/08/0512:50:08 128.6 151.7 27.9 89.7 

12/0810512:50:18 128.9 152.1 27.9 90.1 

12108/0512:50:28 129.1 152.2 27.8 90.4 

12/08/0512:50:38 128.9 152.2 27.7 90.4 

1210810512:50:48 130.2 152.6 27.6 90.4 

1210810512:50:58 129.5 152.9 27.6 90.4 

1210810512:51:08 129.8 153.1 27.6 90.4 

12/0810512:51:18 129.9 153.4 27.6 90.3 

12/0810512:51:28 130.0 153.4 27.5 89.9 

12l0810512:51:38 130.0 153.4 27.6 89.5 

12108/0512:51:48 129.6 153.4 27.5 89.2 

1210810512:51:58 129.9 153.5 27.5 88.9 

12108/0512:52:08 129.2 153.3 27.5 88.6 

12/08/0512:52:18 129.7 153.0 27.5 88.4 

12/08/0512:52:28 129.3 153.1 27.4 88.3 

12/08/0512:52:38 129.2 153.3 27.3 88.0 

12108/0512:52:48 130.0 153.3 27.3 87.7 

12/0810512:52:58 130.0 153.2 27.3 87.3 

12J0810512:53:08 129.8 153.4 27.3 87.0 

1210810512:53:18 128.8 153.3 27.3 86.6 

12/08/0512:53:28 127.9 153.3 27.3 86.0 

12/0810612:53:38 128.7 153.3 27.2 65.4 

1210810512:53:48 127.8 153.0 27.3 84.7 

12/08/0512:53:58 127.7 152.9 27.2 84.0 

12/08/0512:54:08 127.4 152.9 27.0 83.4 

1210810512:54:18 128.1 152.5 27.1 82.9 

12/08/0512:54:28 127.5 152.3 27.1 82.5 

12/08/0512:54:38 126.7 152.3 27.1 82.0 

12108/0512:54:48 126.7 152.5 27.1 81.2 

12108/0512:54:58 127.4 152.8 27.1 80.0 

12108/0512:55:08 126.6 153.2 27.1 78.9 

12/08/0512:55:18 124.1 147.8 26.7 76.7 

1210810512:55:28 124.7 143.6 27.0 76.4 

12/0810512:55:38 123.9 153.6 26.9 75.4 

12/08/0512:55:48 124.5 153.4 26.9 74.6 

12/08/0512:55:58 124.2 153.5 26.8 74.1 

12108105 1 2:56:08 125.0 153.7 26.9 73.5 

12/08/0512:56:18 125.2 153.6 26.8 72.9 

12/0810512:56:28 123.9 153.8 26.7 72.7 

1210810512:56:38 126.0 154.4 26.7 72.6 

12/08/0512:56:48 123.6 154.7 26.6 72.7 

12108/0512:56:58 124.5 154.9 26.7 73.1 

12/0810512:57:08 124.3 155.3 26.7 73.6 

1210810512:57:18 123.6 154.9 26.7 73.9 

12/0810512:57:28 123.9 154.8 26.7 74.0 

12/0810512:57:38 123.2 154.9 26.7 74.0 

12/0810512:57:48 122.8 154.9 26.7 74.1 

1 2108/05 1 2:57:58 123.2 154.9 26.7 73.9 

12108/0512:58:08 123.6 154.9 26.7 74.0 

1 ZJ08/05 12:58:18 121.4 154.7 26.6 74.0 

12108/0512:58:28 122.7 154.1 26.6 74.0 

12/08/0512:58:38 124.6 153.9 26.6 74.0 

12J08/0512:58:48 123.1 153.8 26.5 74.0 

12108/0512:58:58 123.3 153.9 26.5 74.0 

12108/0512:59:08 123.8 154.4 26.5 73.9 

12108/0512:59:18 124.1 154.6 26.5 73.8 

12108/0512:59:28 125.6 154.6 26.6 73.7 

12/08/0512:59:38 123.7 154.6 26.6 73.6 

12108/0512:59:48 124.4 154.4 26.6 73.6 

1210810512:59:58 125.8 153.9 26.6 73.8 

1210810513:00:08 125.1 153.6 26.6 73.9 

1210810513:00:18 125.6 153.7 26.6 74.2 

1210810513:00:28 125.9 153.9 26.6 74.5 

1210810513:00:38 124.6 154.2 26.6 74.7 

12108/06 13:00:48 125.2 154.0 26.5 75.0 

12108/0513:00:58 126.0 164.0 26.6 75.1 

1.16 

Page 1 
12/8105 Run #2 

12/08/0513:01:08 125.2 154.1 26.6 75.3 

12108/0513:01:18 125.2 154.3 26.6 75.4 

1 2108/05 1 3:01:28 125.1 154.4 26.5 75.6 

12/0810513:01:38 124.5 154.6 26.5 75.4 

1210810513:01:48 125.5 154.9 26.5 75.2 

12108/0513:01:58 124.0 155.0 26.6 75.0 

12/08/0513:02:08 122.8 155.0 26.7 74.3 

12/08/0513:02:18 121.8 155.0 27.0 73.0 

12108/0513:02:28 121.9 155.4 27.5 71.2 

12/0810513:02:38 115.2 155.7 27.6 69.3 

12/0810513:02:48 111.7 156.0 27.5 66.9 

1210810513:02:58 111.7 155.7 27.6 64.6 

1210810513:03:08 118.3 153.3 27.6 62.6 

12108/0513:03:18 122.4 150.6 27.3 61.3 

1210810513:03:28 124.3 149.2 27.2 60.3 

1 2108105 1 3:03:38 125.8 149.0 27.1 59.5 

1 2108105 1 3:03:48 126.2 149.5 27.0 58.9 

1 2108105 1 3:03:58 122.9 151.0 27.0 58.8 

1210810513:04:08 122.5 152.4 27.0 58.8 

12108/0513:04:18 121.6 153.7 27.0 59.0 

1210810513:04:28 119.9 154.3 27.1 59.4 

1 2108/05 1 3:04:38 120.4 154.4 27.1 60.0 

1 2108/05 1 3:04:48 119.3 154.7 27.0 60.6 

12l08/0513:04:58 113.0 43.6 26.2 58.3 

12108/0513:05:08 118.0 154.4 27.0 61.7 

12108/0513:05:18 117.6 154.3 27.0 62.1 

12/08/0513:05:28 117.5 154.3 26.9 62.6 

12/08/0513:05:38 117.4 154.4 27.0 63.1 

12/08/0513:05:48 116.7 154.9 26.9 63.4 

12108/0513:05:58 117.3 155.0 27.0 63.8 

12/08/0513:06:08 116.2 155.3 26.9 64.1 

12108/0513:06:18 117.6 155.5 26.9 64.5 

12108/0513:06:28 117.5 155.6 26.9 65.0 

12108/0513:06:38 116.3 155.6 26.9 65.4 

12J08/0513:06:48 117.7 155.6 26.9 66.0 

12108/0513:06:58 118.2 155.6 26.9 66.6 

12/08/0513:07:08 119.4 155.4 27.0 67.1 

1210810513:07:18 119.8 155.3 27.0 67.5 

1 2/08105 1 3:07:28 121.0 155.3 27.0 . 67.8 

12/0810513:07:38 121.9 155.2 27.0 68.0 

12/0810513:07:48 121.6 155.1 27.0 68.4 

12/08/0513:07:58 122.5 154.7 27.1 68.6 

12/0810513:08:08 122.3 155.0 27.0 68.8 

12/08/0513:08:18 122.2 155.4 27.1 69.1 

12/0810513:08:28 122.5 155.5 27.0 69.3 

12108/0513:08:38 122.9 155.6 27.1 69.5 

1210810513:08:48 122.5 155.8 27.1 69.6 

12/08/0513:08:58 122.6 156.0 27.2 69.8 

12/08/0513:09:08 122.2 156.1 27.2 70.0 

12/08/0513:09:18 122.5 156.3 27.2 70.1 

12/08/0513:09:28 123.8 156.7 27.2 70.3 

12/08/0513:09:38 124.1 157.1 27.3 70.3 

12/08/0513:09:48 122.4 157.1 27.3 70.3 

12/08/0513:09:58 123.8 156.7 27.3 70.4 

12/08/0513:10:08 123.8 156.4 27.2 70.4 

12108/0513:10:18 123.3 156.3 27.2 70.5 

1210810513:10:28 122.8 156.4 27.2 70.4 

12/08/0513:10:38 122.6 156.5 27.2 70.3 

12/08/0513:10:48 123.6 156.6 27.2 70.4 

12/08/0513:10:58 123.7 156.3 27.3 70.4 

1 2108105 1 3:11:08 123.5 156.1 27.3 70.5 

12/08/0513:11:18 122.7 155.6 27.2 70.5 

12/08/0513:11:28 123.7 155.3 27.2 70.7 

12/08/0513:11:38 123.4 155.1 27.3 70.7 

12/08/0513:11:48 123.1 155.0 27.3 70.8 

12/08/0513:11:58 123.0 155.0 27.4 70.8 

12/0810513:12:08 122.6 155.1 27.4 70.9 

12/0810513:12:18 121.8 155.2 27.3 71.2 

1210810513:12:28 123.3 155.4 27.3 71.1 

12/08/0513:12:38 123.3 155.5 27.4 71.1 

12/08/0513:12:48 122.2 155.5 27.3 71.1 

12l0810513:12:58 122.7 155.6 27.1 71.1 

12/08/0513:13:08 122.2 156.0 27.2 71.1 

1210810513:13:18 121.6 156.3 27.2 71.4 

1. ! "1 

Page 2 
12/8/05 Run #2 

12I08/0513:13:28 121.9 156.6 27.2 71.5 

1 2108105 1 3:13:38 121.2 156.7 27.2 71.6 

12108105 1 3:13:48 121.4 156.7 27.1 71.6 

12/08/0513:13:58 121.9 156.6 27.2 71.7 

1210810513:14:08 120.4 156.3 27.2 71.8 

12108/0513:14:18 121.2 156.1 27.1 71.7 

12/08/0513:14:28 121.6 155.6 27.1 71.8 

12/08/0513:14:38 121.6 155.3 27.1 72.0 

12/08/0513:14:48 121.6 154.7 27.0 71.7 

12/08/0513:14:58 120.7 154.0 27.0 71.5 

12/08f0513:15:08 119.9 153.6 27.0 71.5 

12/0810513:15:18 120.4 153.0 27.1 71.5 

1210810513:15:28 120.1 152.3 27.0 71.4 

12108/0513:15:38 121.5 151.9 27.0 71.2 

1210810513:15:48 122.3 151.9 26.9 71.2 

12/0810513:15:56 121.4 151.9 26.8 71.3 

1210810513:16:08 122.9 152.1 26.8 71.3 

12108/0513:16:18 123.4 152.5 26.9 71.4 

12108/0513:16:28 123.7 152.5 26.9 71.4 

12/08/0513:16:38 122.9 152.4 26.9 71.6 

12108/0513:16:48 122.8 152.4 27.1 71.7 

12108/0513:16:58 122.4 152.3 27.1 7'1.8 

1 2108/05 1 3:17:08 122.7 152.7 27.1 72.0 

12108/0513:17:18 122.8 152.9 26.9 72.0 

1 2/08105 1 3:17:28 122.0 152.7 26.9 72.0 

1210810513:17:38 122.4 152.6 26.7 71.9 

12/08/0513:17:48 122.8 152.7 26.7 71.9 

12108J0513:17:58 122.9 152.8 26.7 71.9 

12/08/0513:18:08 122.7 152.8 26.7 71.8 

12108/0513:18:18 122.7 152.7 26.7 71.7 

12/08/0513:18:28 122.9 152.9 26.8 71.6 

12/08/0513:18:38 122.5 152.6 26.9 71.6 

12/0810513:18:48 122.7 152.4 26.9 71.6 

12/08/0513:18:58 122.7 152.3 26.8 71.4 

12/08/0513:19:08 121.3 152.5 26.9 71.4 

12/0810513:19:18 122.0 152.7 26.8 71.6 

12/0810513:19:28 122.3 152.7 26.8 71.8 

12108/0513:19:38 123.2 152.4 26.8 72.0 

12l08/0513:19:48 122.4 152.7 26.7 72.2 

12108/0513:19:58 122.7 152.7 26.7 72.3 

12/08/0513:20:08 123.6 153.0 26.6 72.6 

12108/0513:20:18 124.3 153.3 26.7 72.8 

12/08/0513:20:28 123.4 153.9 26.6 73.1 

1210810513:20:38 123.7 154.2 26.6 73.5 

12/08/0513:20:48 123.1 153.9 26.6 73.9 

1210810513:20:58 123.7 153.6 26.6 74.3 

12/08/0513:21:08 123.4 153.1 26.6 74.9 

12108/0513:21:18 123.4 152.7 26.5 75.4 

12/08/0513:21:28 123.6 152.0 26.6 75.8 

12108/0513:21:38 121.7 152.1 26.6 76.3 

12/0810513:21:48 121.3 151.9 26.7 76.7 

12/08/0513:21:58 . 121.5 151.5 26.6 77.1 

12/08/0513:22:08 121.2 151.4 26.5 77.6 

12/08/0513:22:18 121.3 151.5 26.6 78.0 

12J08/0513:22:28 121.1 151.8 26.5 78.3 

12/08/0513:22:38 121.4 151.9 26.5 78.3 

12108/0513:22:48 121.6 152.0 26.5 78.5 

12108/0513:22:58 121.3 151.8 26.5 78.8 

12/0810513:23:08 121.3 152.1 26.6 78.9 

12/08/0513:23:18 121.6 152.4 26.7 79.1 

12/0810513:23:28 122.3 152.5 26.8 79.4 

12108f0513:23:38 122.3 152.4 26.8 79.5 

12/0810513:23:48 123.3 152.1 26.8 79.7 

12/0810513:23:58 122.5 151.8 26.7 79.8 

1210810513:24:08 123.5 151.6 26.8 79.9 

12/08/0513:24:18 124.3 151.5 26.8 80.1 

12108/0513:24:28 123.8 151.8 26.9 80.1 

12/08/0513:24:38 123.5 152.1 26.8 80.0 

12/08/0513:24:48 122.7 152.0 26.8 80.0 

1210810513:24:58 122.6 151.6 26.8 79.9 

1210810513:25:08 123.4 151.6 26.8 79.7 

1210810513:25:18 123.7 161.5 26.8 79.6 

12/08/0513:25:28 122.7 151.4 26.9 79.4 

1 2108105 1 3:25:38 123.5 151.4 27.0 79.1 

1.18 

Page 3 
12/8/05 Run #2 

12/08/0513:25:48 122.4 151.8 26.8 78.5 

12/0810513:25:58 122.4 152.5 26.7 77.2 

12/08/0513:26:08 121.4 152.6 26.7 75.8 

12/08/0513:26:18 122.5 152.7 26.8 74.3 

12/08/0513:26:28 122.1 152.9 27.1 72.9 

12/08/0513:26:38 120.4 152.7 27.2 71.3 

12/08/0513:26:48 121.7 152.3 27.2 70.0 

12/08/0513:26:58 121.1 152.0 27.1 68.4 

12108/0513:27:08 120.7 152.2 26.9 66.8 

12/08/0513:27:18 121.3 152.4 26.9 65.5 

12108/0513:27:28 122.1 152.7 26.9 64.3 

12/08/0513:27:38 121.2 152.6 28.8 63.6 

12108/0513:27:48 122.2 153.0 26.8 62.8 

12108/0513:27:58 119.7 153.1 26.8 62.5 

12108/0513:28:08 121.2 153.2 26.8 62.3 

12108/0513:28:18 119.9 153.5 26.8 62.1 

12108/0513:28:28 120.5 153.7 26.8 62.1 

12/08/0513:28:38 119.7 153.6 26.8 62.1 

12/08/0513:28:48 119.1 153.5 26.8 62.0 

12108/0513:28:58 117.7 153.5 26.7 62.0 

12108/0513:29:08 119.2 153.7 26.6 61.9 

12108/0513:29:18 119.7 153.9 26.6 61.8 

12108/0513:29:28 119.5 153.4 26.7 61.7 

12/08/0513:29:38 120.5 153.4 26.7 62.0 

12108/0513:29:48 120.5 153.3 26.7 62.3 

1210810513:29:58 120.2 153.4 26.8 62.7 

12108/0513:30:08 119.0 153.0 26.8 63.0 

1210810513:30:18 120.4 152.7 26.9 63.3 

12108/0513:30:28 119.6 152.4 27.0 63.8 

12/08/0513:30:38 119.7 152.1 27.0 64.4 

12/0810513:30:48 118.7 152.1 26.9 65.0 

1210810513:30:58 120.2 152.4 26.8 65.3 

12/08/0513:31:08 119.3 152.5 26.9 65.6 

12J0810513:31:18 119.8 152.9 26.8 65.9 

12/0810513:31:28 120.9 153.0 26.8 66.3 

12/0810513:31:38 120.5 153.4 26.8 66.5 

12/0810513:31:48 121.0 153.9 26.8 66.8 

12108/0513:31:58 120.5 154.4 26.8 67.0 

12/0810513:32:08 120.7 154.8 26.8 67.2 

12/08/0513:32:18 120.5 155.1 26.8 67.4 

1210810513:32:28 119.7 155.2 26.8 67.7 

12/0810513:32:38 120.6 155.0 26.7 67.7 

12/08/0513:32:48 119.7 155.1 26.6 67.4 

12/08/0513:32:58 120.5 154.9 26.5 66.9 

12/08/0513:33:08 121.3 154.6 26.6 66.5 

12/08/0513:33:18 121.3 154.9 26.6 66.1 

12108/0513:33:28 121.6 155.2 26.6 65.9 

12108/0513:33:38 121.0 155.3 26.7 65.7 

12108/0513:33:48 120.7 155.4 26.7 65.6 

12108/0513:33:58 121.7 155.4 26.7 65.5 

12/08/0513:34:08 120.8 155.4 26.8 65.3 

12/0810513:34:18 121.8 155.4 26.7 65.0 

12/0810513:34:28 121.7 155.1 26.7 64.6 

1210810513:34:38 121.1 155.0 26.7 64.4 

12/08/0513:34:48 120.9 155.0 26.8 64.3 

12/08/0513:34:58 121.5 154.8 26.8 64.1 

12108/0513:35:08 121.9 154.7 26.7 64.0 

1210810513:35:18 122.4 154.4 26.7 63.7 

1210810513:35:28 121.6 154.4 26.8 63.8 

1210810513:35:38 122.7 154.5 26.8 63.8 

12l0810513:35:48 121.3 154.0 26.9 63.7 

12/0810513:35:58 121.6 153.5 27.0 63.6 

12/0810513:36:08 121.8 153.6 27.0 63.4 

12/0810513:36:18 121.3 153.5 26.9 63.3 

12/08/0513:36:28 122.2 153.1 26.9 63.2 

12/08/0513:36:38 121.6 152.7 26.9 63.1 

12/08/0513:36:48 121.6 152.6 27.0 62.9 

12108/0513:36:58 121.8 152.4 27.0 62.7 

12/08/0513:37:08 121.6 151.9 27.0 62.6 

12J0810513:37:18 121.8 151.7 27.0 62.4 

12/08/05 13:37:28 121.6 151.9 26.9 62.2 

12108/0513:37:38 122.0 152.1 26.9 62.0 

12J08/0513:37:48 120.8 152.1 26.8 62.0 

12108/0513:37:58 120.6 152.1 26.8 61.8 

Page 4 

~_ 1 g 
12/8/05 Run sF2 

12108/0513:38:08 120.7 152.1 26.8 61.8 

12/08/0513:38:18 118.9 152.2 26.8 61.8 

12108/0513:38:28 119.9 152.6 26.8 61.7 

1 2108/06 1 3:38:38 120.0 153.0 26.8 61.7 

1210810513:38:48 120.0 153.1 26.9 61.8 

12108/0513:38:58 119.8 153.6 26.7 61.9 

12108/0513:39:08 120.1 154.6 26.7 62.0 

12/08/0513:39:18 119.5 155.1 26.8 62.1 

12108/0513:39:28 120.2 155.0 26.8 62.3 

12108/0513:39:38 119.5 154.8 26.7 62.6 

12/0810513:39:48 119.7 154.8 26.6 62.5 

12/08/0513:39:58 120.4 154.7 26.6 62.4 

12108/0513:40:08 119.6 154.2 26.5 62.5 

1210810513:40:18 120.4 153.9 26.6 62.5 

12/0810513:40:28 120.7 153.9 26.7 62.4 

12108/0513:40:38 119.8 153.9 26.7 62.4 

12108/0513:40:48 121.1 163.8 26.6 62.3 

12/0810513:40:58 120.4 153.6 28.6 62.3 

12108i0513:41:08 121.8 153.6 26.6 62.3 

12/08/0513:41:18 122.2 153.9 26.6 62.4 

12/08/0513:41:28 121.8 153.9 26.6 62.5 

12/08/0513:41:38 121.8 153.6 26.7 62.5 

12/08/0513:41:48 122.7 153.6 26.7 62.7 

12/0810513:41:58 123.3 153.6 26.7 62.9 

12/0810513:42:08 123.5 153.5 26.6 63.1 

12108/0513:42:18 122.1 153.3 26.7 63.2 

12108/0513:42:28 123.1 153.2 26.6 63.2 

12/08/0513:42:38 123.7 152.8 26.7 63.3 

12/08/0513:42:48 122.5 152.9 26.7 63.4 

12/08/0513:42:58 122.9 153.0 26.6 63.5 

12/08/0513:43:08 122.6 153.2 26.6 63.6 

12/08/0513:43:18 123.0 153.3 26.6 63.7 

12/0810513:43:28 122.8 153.3 26.6 63.6 

12/0810513:43:38 122.8 153.6 26.6 63.7 

12108105 1 3:43:48 123.2 153.8 26.6 63.9 

12/08/0513:43:58 123.0 153.8 26.6 64.1 

12/08/0513:44:08 123.6 153.6 26.6 64.2 

12108/0513:44:18 123.0 163.7 26.7 64.2 

12108/0613:44:28 122.6 153.6 26.7 64.1 

12108/0513:44:38 122.9 153.5 26.7 64.1 

12/0810513:44:48 123.1 153.6 26.7 64.0 

1210810513:44:58 122.7 153.6 26.7 64.1 

12108/0513:45:08 123.5 153.8 26.7 64.1 

12/08/0513:45:18 122.2 154.1 26.7 64.1 

12108/0513:45:28 124.0 154.2 26.7 64.2 

12108/0513:45:38 123.9 154.3 26.8 64.3 

12/08/0513:45:48 123.5 154.5 26.8 64.4 

12/08/0513:45:58 124.6 154.7 26.8 64.5 

12108/0513:46:08 122.4 154.9 26.8 64.8 

12/08/0513:46:18 122.5 154.8 26.8 64.9 

12108/0513:46:28 122.1 155.0 26.8 65.2 

12/08/0513:46:38 122.8 154.7 26.8 65.3 

12108/0513:46:48 122.2 154.8 26.8 65.3 

12/08/0513:46:58 121.5 155.0 26.8 65.3 

12108/0513:47:08 121.6 155.0 26.8 65.5 

12/08/0513:47:18 121.5 154.7 26.9 65.6 

12/0810513:47:28 121.7 154.3 26.9 65.5 

12/08/0513:47:38 121.6 154.0 26.9 65.6 

12108/0513:47:48 120.7 153.6 26.8 65.4 

12/08/0513:47:58 121.7 153.3 26.8 65.4 

12108/0613:48:08 120.8 153.5 26.7 65.3 

12/08/0513:48:18 121.0 153.7 26.6 65.1 

12108/0513:48:28 120.8 153.9 26.6 65.1 

12/0810513:48:38 121.1 153.9 26.7 65.0 

12/08/0513:48:48 121.4 153.9 26.6 65.1 

12108/0513:48:58 120.6 154.1 26.6 65.3 

12108/0513:49:08 121.0 153.9 26.6 65.2 

12108/0513:49:18 121.1 153.7 26.6 65.3 

12108/0513:49:28 120.6 153.5 26.6 65.2 

1 2108/05 1 3:49:38 121.2 153.6 26.5 64.9 

12108/0513:49:48 122.4 153.6 26.6 64.8 

1 2108/05 1 3:49:58 123.2 154.0 26.6 64.7 

12108/0513:50:08 123.0 154.5 26.6 64.5 

12/08/0513:50:18 123.6 154.9 26.6 64.6 

Page 5 1_2V 
1218105 Run #2 

12/0810513:50:28 124.0 155.1 26.6 64.3 

12/08/0513:50:38 123.2 155.1 26.4 64.1 

1210810513:50:48 123.4 155.5 26.4 64.0 

12108/0513:50:58 123.1 155.9 26.3 64.0 

12/0810513:51:08 122.5 155.6 26.4 64.0 

12/08/0513:51:18 123.6 155.2 26.4 64.0 

12108/0513:51:28 122.7 155.1 26.5 64.2 

12/0810513:51:38 123.1 154.8 26.6 64.2 

12/08/0513:51:48 123.5 154.6 26.6 64.2 

12/0810513:51:58 122.4 154.6 26.6 64.1 

12/0810513:52:08 122.3 154.4 26.6 64.0 

1210810513:52:18 122.9 154.4 26.5 64.0 

12/0810513:52:28 122.6 154.3 26.6 63.9 

12/0810513:52:38 123.0 154.3 26.6 63.8 

12/0810513:52:48 122.3 154.3 26.5 63.7 

12/0810513:52:58 122.1 154.1 26.5 63.6 

Stop Run If2 122.48 153.47 26.86 69.78 

12108/0513:53:08 122.9 154.2 26.6 63.4 

12/0810513:53:18 121.9 154.1 26.6 63.5 

12/0810513:53:28 122.5 154.1 26.5 63.4 

12/08l0513:53:38 117.7 127.9 25.5 60.9 

1210BI0513:53:48 120.6 152.9 26.4 63.2 

12108/0513:53:58 36.4 149.4 25.8 62.3 

12108/0513:54:08 6.1 147.5 25.4 61.2 

12/08/0513:54:18 6.4 131.3 24.5 60.5 

12108/0513:54:28 5.3 91.8 19.5 57.9 

12l08/0513:54:38 5.3 60.9 13.1 52.1 

12108/0513:54:48 5.2 41.2 10.2 45.4 

1210810513:54:58 4.4 25.7 7.9 38.9 

12108/0513:55:08 4.5 16.8 6.1 32.0 

12J08l0513:55:18 3.9 10.1 6.4 25.6 

12l08/0513:55:28 3.1 6.0 11.6 20.0 

12/08/0513:55:38 2.9 4.2 15.7 16.3 

12l08/0513:55:48 3.0 3.1 19.0 12.8 

12/08/0513:55:58 2.9 2.5 21.0 10.0 

12108l0513:56:08 2.8 2.0 22.0 8.2 

12/0810513:56:18 2.8 2.0 22.3 6.5 

12108/0513:56:28 3.0 1.6 22.4 5.1 

12/08/0513:56:38 3.6 0.9 22.5 3.9 

12108/0513:56:48 4.4 0.6 22.5 3.0 

12/08/0513:56:58 7.0 0.7 22.4 2.3 

1210810513:57:08 7.3 0.6 22.4 1.8 

12/0810513:57:18 7.3 0.4 22.4 1.5 

12/0810513:57:28 7.9 0.3 22.4 1.1 

12/08l0513:57:38 7.0 0.3 22.3 0.9 

1210810513:57:48 6.2 0.3 22.3 0.7 

1210810513:57:58 7.0 0.4 21.8 0.4 

1210810513:58:08 4.8 0.4 21.2 0.2 

1 2108/05 1 3:58:18 3.7 0.6 21.2 0.1 

1210810513:58:28 4.1 0.8 20.8 0.2 

12/08/0513:58:38 4.9 1.3 18.5 0.2 

12/08/0513:58:48 5.3 1.8 16.0 0.3 

12108/0513:58:58 8.6 2.6 11.3 0.7 

12108/0513:59:08 10.6 3.1 7.0 1.1 

12/0810513:59:18 8.9 1.2 4.3 2.4 

.12108l051159:28 10.7 0.3 2.7 6.8 

12108/05 13:59:38 11.3 0.1 1.8 14.2 

12/0810513:59:48 10.1 -0.1 1.4 23.9 

12/0810513:59:58 9.9 -0.2 1.2 34.6 

12/08/0514:00:08 10.3 -0.2 1.0 44.9 

12108/0514:00:18 10.6 -0.2 0.8 53.9 

12/08/0514:00:28 11.0 -0.3 0.8 60.7 

12/08/0514:00:38 9.8 -0.4 0.8 65.5 

12/08/0514:00:48 9.9 -0.5 0.7 69.6 

12/08/0514:00:58 9.0 -0.4 0.7 72.9 

12/08/0514:01:08 8.7 -0.4 0.7 76.1 

 12/08/0514:01:18 9.0 -0.4 0.6 78.9 

12/08/0514:01:28 8.3 -0.7 0.6 81.1 

12/08/0514:01:38 8.3 -0.8 0.6 82.9 

12/08l0514:01:48 8.8 -1.2 0.6 84.6 

12/0810514:01:58 8.3 -1.0 0.6 85.9 

25.5 ppm NOx 

Zero S02 

Page 6 

I +w ~ 
12/8105 Run #2 

12/08/0514:02:08 8.3 -1.1 0.5 87.0 

12/08/0514:02:18 8.1 -0.9 0.6 88.0 

12/0810514:02:28 7.8 -0.7 0.6 88.7 

1210810514:02:38 7.4 -0.7 0.5 89.6 

12/08/0514:02:48 7.2 -0.7 0.5 90.5 

12/08/0514:02:58 7.3 -0.8 0.5 91.4 

12/08/05 14:03:08 6.6 -1.1 0.4 92.1 

12J08J0514:03:18 6.2 -1.0 0.5 92.7 

12108/0514:03:28 5.4 -1.0 0.5 93.1 

12108/0514:03:38 5.0 -0.8 0.4 93.4 

12108/0514:03:48 4.2 -0.6 0.4 93.7 

12/08/0514:03:58 3.5 -0.6 0.4 94.1 

12/08/0514:04:08 2.9 -0.7 0.4 94.9 

12108/0514:04:18 2.9 -0.8 0.4 95.4 

12108/0614:04:28 2.9 -0.8 0.4 95.9 

12/0810514:04:38 2.9 -1.0 0.3 96.3 

12108/0514:04:48 2.8 -1.1 0.3 96.6 

12108/0514:04:58 2.8 -1.5 0.3 96.9 

1210810514:05:08 3.0 -1.2 0.3 97.3 

12/0810514:05:18 2.8 -1.1 0.3 97.6 

12/08/0514:05:28 2.2 -1.2 0.3 97.9 

12/08/0514:05:38 2.3 -1.2 0.3 98.3 

12/08/0514:05:48 2.1 -1.0 0.2 98.4 

12/08/05 14:05:58 2.2 -0.9 0.3 98.6 101 ppm S02 

12108/05 14:06:08 2.3 -0.7 0.3 98.7 Zero CO3 NOx 

12108/0514:06:18 2.4 -0.7 0.3 98.7 

12108/0514:06:28 2.6 -0.5 0.2 98.0 

12/08/0514:06:38 3.0 -0.5 0.2 96.0 

1210810514:06:48 2.8 -0.4 0.2 95.2 

1210810514:06:58 2.9 -0.2 0.3 95.7 

12/08/0514:07:08 3.0 18.3 0.3 94.2 

12/08/0514:07:18 3.0 75.3 0.3 87.7 

12/08/0514:07:28 2.9 116.2 0.3 76.1 

12/08/0514:07:38 2.6 139.3 0.3 62.8 

12/08/0514:07:48 2.3 151.9 0.3 50.7 

12/08/0514:07:58 2.2 160.7 0.2 40.6 

12/0810514:08:08 2.4 164.7 0.2 32.1 

12/0810514:08:18 2.2 167.3 0.2 25.9 

12108/0514:08:28 2.2 168.6 0.2 21.2 

12/08/0514:08:38 2.3 169.8 0.2 17.8 

1210810514:08:48 2.3 171.0 0.2 15.2 

12108/0514:08:58 2.2 172.3 0.2 12.9 

12/08/0514:09:08 2.3 173.2 0.2 10.9 

12108/0514:09:18 2.3 174.0 0.2 9.4 

12108/0514:09:28 2.2 175.4 0.2 8.7 

12/08/0514:09:38 1.9 177.4 0.2 7.8 

12108/0514:09:48 1.8 179.8 0.2 6.7 

1210810514:09:58 2.1 181.3 0.2 6.7 

12108/0514:10:08 2.2 182.8 0.2 4.9 

12/0810514:10:18 1.9 183.4 0.2 4.2 

12/08/0514:10:28 1.9 183.8 0.2 3.7 

12/08/0514:10:38 1.9 184.3 0.2 3.3 

12108/0514:10:48 2.0 184.7 0.2 2.8 

12108/05 14:10:58 1.7 184.9 0.2 2.3 200 ppm CO 

12/08/05 14:11:08 1.6 184.9 0.2 1.9 Zero vOC 

12/08/0514:11:18 1.7 185.2 0.2 1.8 

12/08/0514:11:28 1.9 182.4 0.1 1.3 

12/08/0514:11:38 2.1 182.4 0.1 0.9 

1210810514:11:48 49.7 184.1 0.1 0.6 

1210810514:11:58 89.7 178.5 0.1 0.7 

12/08/0514:12:08 90.5 152.9 0.2 1.0 

12/08J0514:12:18 90.7 103.7 0.2 1.3 

12/08/05 14:12:28 90.7 62.0 0.2 1.4 89.2 ppm C3H8 

1210810514:12:38 90.7 38.5 0.2 1.2 

12/0810514:12:48 90.5 26.9 0.2 1.0 

12/08/0514:12:58 90.3 18.5 0.2 0.6 

12/08/0514:13:08 90.2 13.1 0.2 0.4 

1.72 

Page 7 
1218/05 Run #3 

DatefTime VOC CO NOx S02 

mmrddlyy hh:mm:ss ppm ppm ppm ppm 

12108/0514:19:48 127.9 153.2 26.4 78.0 

12108/0514:19:58 128.1 153.4 26.3 77.3 

Start Run #3 

12/0810514:20:08 128.1 153.6 26.3 76.5 

12/0810514:20:18 128.0 153.8 26.3 75.8 

12/08I0514:20:28 128.4 154.1 26.3 75.2 

1210810514:20:38 125.7 154.8 26.2 74.6 

12108/0514:20:48 126.7 154.9 26.3 74.2 

12108/0514:20:58 127.4 155.0 26.3 74.0 

1210810514:21:08 127.0 154.9 26.2 73.8 

12108/0514:21:18 127.9 154.9 26.2 73.7 

12/08/0514:21:28 127.3 155.2 26.2 73.7 

12108/0514:21:38 127.0 155.3 26.1 73.8 

12108/0514:21:48 125.1 155.3 26.2 74.0 

12/08/0514:21:58 124.8 155.2 26.3 74.2 

12/0810514:22:08 124.4 155.0 26.3 74.3 

1210810514:22:18 124.7 154.8 26.3 74.3 

1210810514:22:28 124.6 154.8 26.3 74.3 

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1.?3 

Page 1 
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Page 2 I?.. ~ 
1218105 Run #3 

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12 V 

Page 3 
12/8105 Run #3 

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Pags 4 
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12108105 1 5:20:18 112.7 152.6 25.9 82.3 

12108/0515:20:28 111.7 153.1 .26.0 82.6 

12108/0515:20:38 112.0 163.3 25.9 82.6 

1. ~ 

Page 5 
1218/05 Run #3 

12108/0515:20:48 110.8 153.6 26.0 82.6 

12108/0515:20:58 111.1 153.8 26.0 82.6 

12i08/0515:21:08 109.7 153.9 25.9 82.6 

12/08/0515:21:18 109.0 153.5 26.0 82.5 

12/08/0515:21:28 108.2 153.1 25.9 82.6 

12108/0515:21:38 110.1 152.6 26.0 82.5 

12108/0515:21:48 109.6 151.4 26.0 82.4 

12/08/0515:21:58 109.8 150.0 26.1 82.2 

Stop Run #3 128.32 157.05 26.87 75.17 

1210810515:22:08 109.7 148.7 26.1 82.2 

12/08/0515:22:18 109.7 147.2 26.1 82.3 

12/0810515:22:28 109.7 145.7 26.1 82.3 

12J0810515:22:38 97.6 144.1 26.1 82.2 

12/08/0515:22:48 10.4 140.0 25.2 81.4 

12/08/0515:22:58 5.4 136.1 24.5 79.4 

12/08/0515:23:08 5.3 114.6 23.0 77.3 

12J08/0515:23:18 4.6 80.6 17.3 71.3 

12/08/0515:23:28 4.4 51.4 11.6 61.4 

1210810515:23:38 4.1 31.5 7.7 50.1 

12108/0515:23:48 3.1 19.6 5.4 39.8 

1210810515:23:58 2.3 13.8 4.1 31.2 

12108/0515:24:08 2.2 9.6 3.7 24.0 

12/08/0515:24:18 1.7 6.9 7.0 18.2 

12/08/0515:24:28 1.7 5.2 11.2 14.0 

12108/0515:24:38 1.7 3.8 14.7 10.7 

12108/0515:24:48 1.2 2.7 16.8 8.3 

12108/0515:24:58 1.2 2.0 17.7 6.3 

12/08105 15:25:08 1.2 1.6 18.3 4.5 

12/0810515:25:18 1.3 1.0 18.5 3.0 

12/08/0515:25:28 1.3 0.5 18.7 1.8 

12/08/05 15:25:38 1.3 0.6 19.1 1.0 

1210810515:25:48 1.4 0.6 19.2 0.5 

12108/0515:25:58 1.5 0.5 19.4 0.2 

12/08/0515:26:08 1.4 0.3 19.7 0.0 

12108/0515:26:18 0.9 0.3 20.5 -0.4 

12108/0515:26:28 0.9 0.3 21.1 -0.7 

12/08/0515:26:38 1.0 0.3 21.5 -1.0 

12/08/0515:26:48 0.9 0.2 21.7 -1.4 

12/08/0515:26:58 1.0 0.1 21.8 -1.6 

12/08/0515:27:08 0.8 0.1 21.9 -0.8 

12/08/0515:27:18 0.8 0.1 22.0 -0.2 

12/08/05 15:27:28 0.9 0.1 22.0 -0.4 25.5 ppm NOx 

12/08/05 15:27:38 0.7 0.1 22.0 -0.5 Zero S02 

12/08/0515:27:48 0.8 0.0 22.0 -0.5 

12/0810515:27:58 0.8 0.0 21.9 -0.2 

12/08/0515:28:08 0.8 0.0 21.9 -0.3 

12108/0515:28:18 1.0 0.0 21.1 -0.4 

12/08/0515:28:28 1.7 -0.1 20.9 -0.4 

1210810515:28:38 2.6 -0.1 20.9 -0.4 

12/0810515:28:48 2.8 0.0 20.5 -0.5 

1210810515:28:58 3.3 0.1 18.5 -0.4 

12108/0515:29:08 1.1 0.6 15.4 -0.2 

1210810515:29:18 0.2 1.1 9.6 0.1 

1 2108105 1 5:29:28 0.2 0.7 5.4 1.6 

12/0810515:29:38 0.2 0.1 3.4 8.0 

12/08/0515:29:48 0.2 -0.1 2.3 19.3 

12108/0515:29:58 0.1 -0.4 1.5 32.8 

12J0810515:30:08 0.2 -0.5 1.1 45.3 

1 2108/05 1 5:30:18 0.3 -0.6 0.9 55.7 

1210810515:30:28 0.4 -0.5 0.7 63.8 

12/08/0515:30:38 0.1 -0.5 0.6 69.9 

12/08/0515:30:48 0.1 -0.7 0.6 74.4 

12108/0515:30:58 0.1 -0.5 0.5 77.7 

12/08/0515:31:08 0.2 -0.6 0.5 79.9 

1210810515:31:18 0.2 -0.8 0.5 82.0 

1 2108/05 1 5:31:28 0.2 -1.0 0.5 83.8 

12/08/0515:31:38 0.2 -1.3 0.4 85.2 

1210810515:31:48 0.3 -1.4 0.5 86.5 

12108/0515:31:58 0.2 -1.3 0.4 87.5 

12/08/0515:32:08 0.3 -1.3 0.4 87.9 

12/08/0515:32:18 0.2 -1.4 0.4 88.3 

1?V 

Page 6 
1218105 Run #3 

1210810515:32:28 0.2 -1.8 0.4 88.7 

1210810515:32:38 0.1 -1.9 0.3 90.4 

12108/0515:32:48 0.1 -2.0 0.3 92.0 

12/0810515:32:58 0.1 -2.0 0.3 93.4 

12/08/0515:33:08 0.0 -1.9 0.3 94.7 

12/0810515:33:18 0.1 -1.9 0.3 95.1 

12/08/0515:33:28 0.4 -1.4 0.2 95.5 

12108/0515:33:38 0.4 -1.2 0.3 95.8 

12108/0515:33:48 0.3 -1.1 0.3 96.1 

12/08/0515:33:58 0.3 -1.2 0.3 96.6 

12108f0515:34:08 0.1 -1.2 0.2 97.2 

12108/0515:34:18 0.2 -1.2 0.2 98.3 

12108/05 15:34:28 0.0 -1.4 0.2 98.3 101 ppm S02 

12/08/05 15:34:38 0.0 -1.2 0.2 98.5 Zero CO, NOx 

12/0810515:34:48 0.1 -1.1 0.2 98.2 

1210810515:34:58 0.5 -1.2 0.1 97.5 

12/08/0515:35:08 0.5 -1.0 0.2 92.2 

12/0810515:35:18 0.2 -0.8 0.2 89.8 

12/0810515:35:28 0.3 14.7 0.2 88.0 

12108/0515:35:36 0.4 74.1 0.2 81.0 

12108/0515:35:48 0.8 118.7 0.2 68.3 

12108/0515:35:58 0.3 142.1 0.2 54.3 

12/0810515:36:08 0.4 154.6 0.2 41.5 

12/0810515:36:18 0.3 160.3 0.2 31.4 

12/08/0515:36:28 0.2 164.7 0.2 24.2 

12/0810515:36:38 0.3 167.2 0.2 18.8 

1210810515:36:48 0.2 169.1 0.1 15.2 

12/0810515:36:58 0.2 170.4 0.1 12.2 

12/0810515:37:08 0.1 171.5 0.2 9.9 

12/0810515:37:18 0.0 172.3 0.1 8.5 

1210810515:37:28 0.1 172.7 0.1 7.1 

1210810518:37:38 0.2 173.4 0.1 6.1 

12/0810515:37:48 0.2 174.4 0.1 5.2 

12/0810515:37:58 0.3 174.7 0.1 4.5 

12/0810515:38:08 0.3 175.0 0.1 3.8 

12108l0515:38:18 0.4 175.6 0.1 3.2 

1 2108/05 1 5:38:28 0.2 178.3 0.1 2.9 

12108/0515:38:38 0.2 176.7 0.1 2.5 

1 2108/05 1 5:38:48 0.2 176.9 0.1 2.1 

1 2108105 1 5:38:58 0.2 177.1 0.1 1.8 

1210810515:39:08 0.2 177.7 0.1 1.5 

12108/0516:39:18 0.2 178.4 0.1 1.2 

12108/0515:39:28 0.2 178.4 0.1 1.2 

1 2/08105 1 5:39:38 0.2 178.8 0.1 0.9 

12/0810515:39:48 0.2 180.0 0.1 0.6 

1 2108/05 1 5:39:58 0.3 181.0 0.1 0.3 

12/0810515:40:08 0.4 181.5 0.1 0.2 

12108/0515:40:18 0.3 181.8 0.1 0.2 

12108/0515:40:28 0.0 182.2 0.0 0.2 200 ppm CO 

12108/05 15:40:38 0.0 182.3 0.1 0.1 Zero VOC 

12/0810515:40:48 0.0 182.0 0.0 0.1 

1210810515:40:58 0.0 181.8 0.0 0.1 

12/08/0515:41:08 0.0 178.9 0.0 0.0 

12108105 1 5:41:18 6.2 179.1 0.0 -0.1 

12108/0515:41:28 80.1 179.4 0.1 -0.2 

1 2/08105 1 5:41:38 87.5 175.0 0.1 -0.2 

12l0810515:41:48 90.6 146.6 0.1 -0.1 

12108/0515:41:58 91.0 94.3 0.1 -0.1 

12108105 15:42:08 90.8 55.6 0.1 -0.1 89.2 ppm C3H8 

12/08/0515:42:18 90.8 34.7 0.1 -0.1 

12108l0515:42:28 91.1 22.5 0.1 -0.1 

12108/0515:42:38 91.5 15.6 0.0 -0.2 

Page 7 

j_ ? ~ 
Appendix C 
PARTICULATE ANALYTICAL DATA FORM 

Company: Daltile, Muskogee, OK 

Date: 12/7/05 

Location: Kiln Scrubber Exhaust 

Run 1 Run 2 Run 3 

Density (Pa) 

Blank Concentration (Ca) 0 d t ~ -2 's"; :0 IV6: 

Rinse Volume (Vaw) 

Residue in Rinse (Wa) = Ca*Vaw*Pa 0.0009 0.0009. 0.0009 

Date of Weighing .05;: 

Time 

Gross Weight A*$ 

Date of Weighing bt 

Time 

Gross Weight 0-1; 8:~ 9*. 

Date of Weighing V2l 05'. 

Time 'A 

Beaker Tare Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Average Gross Weight 101.8792 99.7192 114.6258 

Less Blank Residue (Wa) 0.0009 0.0009 0.0009 

Average Beaker Tare Weight 101.8554 99.7016 114.6105 

Weight of Particulate in Rinse (mg) 22.94 16.67 14.40 

ACETONE BLANK ANALYTICAL DATA FORM 

Blank Volume (Va) 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time i!; 

Gross Weight 

Average Gross Weight 106,3603 

Date of Weighing VV 

Time 

Tare Weight 

Date of Weighing 

Time 

Tare Weight 1. 0 

Average Tare Weight 106.3589 

Weight of Blank (Ma) 0.00140 

Ca= Ma/(Va*Pa) = mg/g 0.00713 

Note: In no case should a blank residue greater than 0.01 mglg or 0.001% of the blank 

lweight be subtracted from the sample weight. 

13 2 
1:00-0 6 

V. 04: 

0.4104 

.00 

A. 

I T 

0.4015 0.4180 

-:0 

3 2 0:A M:. 

Date of Weighing 

Time 

Gross Filter Wt. 

Date of Weighing 

Time 

Gross Filter Wt. 

Ave. Gross Filter Wt. 

Date of Weighing 

Time 

Filter Tare Wt. 

Date of Weighing 

Time 

Filter Tare Wt. 

FII-7ER ANALITICAL DATA 

Company: Dalt'le, ~vliusL.ogee, OK 

Date: .1200105 

Location: Kiln Scrubber Exhaust 

Run 4 

Filter ID Number 5.M:. 

Run 5 Run 6 

Ave. Filter Tare Wt. 0.3666 

VVt. OT t-IVI On riiier tgrams) U.V4.50 

Total Weight of Particulate (mg) 43.8 

0.3628 0.3797 

0.0387 0.0384 

38.7 38.4 

1.3 
PARTICULATE ANALYTICAL DATA FORM 

Company: Daltile, Muskogee, OK 

Date: 12/8/05 

Location: Trim Kiln Exhaust 

Run 1 Run 2 Run 3 

Density (Pa) 1 7$5 

Blank Concentration (Ca) .1 j i.0.1 b. 07 ( 

Rinse Volume (Vaw) ... ......... . 

Residue in Rinse (Wa) = Ca*Vaw*Pa 0.0009 0.0009 0.0010 

Date of Weighing 6. i. il V 

Time -2: :AM** 

Gross Weight 14 9-1 5.7 4. '6 4 

Date of Weighing :: A-V.9v 

Time M: 31 P M: 

Gross Weight 

Date of Weighing 

Time i 7-,0 i A- W 

Beaker Tare Weight 

Date of Weighing 

Time 

Beaker Tare Weight 7 6 .5 .1'87 

Average Gross Weight 102,5745 98.6548 . 103.1606 

Less Blank Residue (Wa) 0.0009 0.0009 . 0.0010 

Average Beaker Tare Weight 102.5648 98.6449 103.1486 

Weight of Particulate in Rinse (mg) 8.80 8.91 10.91 

ACETONE BLANK ANALYTICAL DATA FORM 

Blank Volume (Va) 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 20 i~ 0'5* 

Time 

Gross Weight 0: 

Average Gross Weight 106.3603 

Date of Weighing 

Time A-- 

Tare Weight 

Date of Weighing 

Time 

Tare Weight :::::::!00; 80 

Average Tare Weight 106.3589 

Weight of Blank (Ma) 0.00140 

Ca= Ma/(Va*Pa) = mg/g 0.00713 

Note: In no case should a blank residue greater than 0.01 mg/g or 0.001% of the blank 

lweight be subtracted from the sample weight. 1~4 
FILTER ANALITICAL DATA 

Company: Daltile, Muskogee, OK 

Date: 12/8/05 

Location: Trim Kiln Exhaust 

Run I Run 2 Run 3 

Filter ID Number ti T : 

Date of Weighing AW 

Time .... 2O AM 

Gross Filter Wt. 0.:3 

Date of Weighing 

Time .:::; 0A6;: M, 

Gross Filter Wt. 

Ave. Gross Filter Wt. 0.3999 0.3933 0.3946 

Date of Weighing 0 42 0 0 i. Ofw. : 

Time 

Filter Tare Wt. 

Date of Weighing 02V -1 

Time OR .4 2' K 

Filter Tare Wt. 0 V-.20 4 .3 

Ave. Filter Tare Wt. 0.3784 0.3729 0.3746 

Wt. of PM on Filter (grams) 0.0215 0.0204 0.0201 

Total Weight of Particulate (mg) 21.5 20.4 20.1 
PARTICULATE ANALYTICAL DATA FORM 

Company: Daltile, Muskogee, OK 

Date: 12/7/05 

Location: Kiln Scrubber Exhaust, lmpinger Solution 

Run -1 Run 2 Run 3 

Density(Pa) 

Blank Concentration (Ca) 

Rinse Volume (Vaw) i ii". iliii.- ~ ! 

Residue in Rinse (Wa) = Ca*Vaw*Pa 0.0012 0.0012 0.0012 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 06! 

Time 

Gross Weight 

Date of Weighing 1 0 .0 

Time 1: AM 

Beaker Tare Weight 

Date of Weighing 

Time 

Beaker Tare Weight O's .9 96 2.: 7=lwl-w 

Average Gross Weight 112.7740 106.0108 103-1696 

Less Blank Residue (Wa) 0.0012 0.0012 0.0012 

Average Beaker Tare Weight 112.7694 105.9964 103.1620 

Weight of Particulate in Rinse (mg) 3.40 13.25 6.45 

H20 BLANK ANALYTICAL DATA FORM 

Blank Volume (Va) 

Date of Weighing 

Time i i .2-4- i A" NA. 

Gross Weight 

Date of Weighing 

Time 2a 

Gross Weight :77': .18 12- 7,61: 

Average Gross Weight 127.1877 

Date of Weighing 

Time 

Tare Weight 

Date of Weighing 

Time 

Tare Weight 

Average Tare Weight 127.1867 

Weight of Blank (Ma) 0.001 

Ca= Ma/(Va*Pa) = g/g 4E.06 

Note: In no case should a blank residue greater than 0.01 mg/g or 0.001% of the blank 

lweight be subtracted from the sample weight. 1 ~ 8 
PARTICULATE ANALYTICAL DATA FORM 

Company: Daltile, Muskogee, OK 

Date: 12/7/05 

Location: Kiln Scrubber Exhaust MeCL Rinse 

Run 1 Run 2 Run 3 

Density (Pa) 

Blank Concentration (Ca) 5. 4 

Rinse Volume (Vaw) 

Residue in Rinse (Wa) = Ca*Vaw*Pa 0.0007 . 

0.0006 0.0007 

Date of Weighing 0 dd 

Time X- AM 

Gross Weight 

Date of Weighing T Ydi 

Time 01 P. 

Gross Weight .5 

Date of Weighing 

Time AM 

Beaker Tare Weight .1. W'; -3 0.4 0 

Date of Weighing 0 5: 

Time '3i.0 741 '': 

Beaker Tare Weight 74 

Average Gross Weight 109.4593 109.3047 105.5283 

Less Blank Residue (Wa) 0.0007 0.0006 0.0007 

Average Beaker Tare Weight 109.4576 109.3039 105.5259 

Weight of Particulate in Rinse (mg) 1.08 0.13 1.75 

METHYLENE CHLORIDE BLANK ANALYTICAL DATA FORM 

Blank Volume (Va) 

Date of Weighing 

Time 

Gross Weight -7 1! 

Date of Weighing 

Time 

Gross Weight 

Average Gross Weight 109.08705 

Date of Weighing 

Time 7 A 

Tare Weight ---- -- ------- 

Date of Weighing 

Time 3 2. 5 F.. M: 

Tare Weight 

Average Tare Weight 109.08625 

Weight of Blank (Ma) 0.0008 

Ca= Ma/(Va*Pa) = g/g 2.353E•06 

Note: In no case should a blank residue greater than 0.01 mg/g or 0.001% of the blank 

[weight be subtracted from the sample weight. 

I ~ 'q 
PARTICULATE ANALYTICAL DATA FORM 

Company: Daltile, Muskogee, OK 

Date: 12/8/05 

Location: Trim Kiln Exhaust, lmpinger Solution 

Run 1 Run 2 Run 3 

Density (Pa) 

Blank Concentration (Ca) 05 

Rinse Volume (Vaw) 

Residue in Rinse (Wa) = Ca*Vaw*Pa 0.0012 0.0012 0.0012 

Date of Weighing 0 --- --- ---- - 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 2. 

Time j 

Beaker Tare Weight 1 (Y Zia a 0 

Date of Weighing .5: 

Time 

Beaker Tare Weight .1 26:00 8 a; 

Average Gross Weight 130.2595 127.3868 126.8213 

Less Blank Residue (Wa) 0.0012 0.0012 0.0012 

Average Beaker Tare Weight 130.2334 127.3624 126.8004 

Weight of Particulate in Rinse (mg) 24.85 23.20 19.70 

H20 BLANK ANALYTICAL DATA FORM 

Blank Volume (Va) 

Date of Weighing 

Time :7i.MNANA ~ Gross Weight 1 2 7; .18 .7 1; 8:: 

Date of Weighing 

Time 

Gross Weight 

Average Gross Weight 127.1877 

Date of Weighing 

Time 

Tare Weight 

Date of Weighing 

Time ...... 2;5 

Tare Weight 

Average Tare Weight 127.1867 

Weight of Blank (Ma) 0.001 

Ca= Ma/(Va*Pa) = g/g 4E•06 

Note: In no case should a blank residue greater than 0.01 mg/g or 0.001% of the blank 

l weight be subtracted from the sample weight. 

I 

140 
PARTICULATE ANALYTICAL DATA FORM 

Company: Daltile, Muskogee, OK 

Date: 12/8/05 

Location: Trim Kiln Exhaust MeCL Rinse 

Run 1 Run 2 Run 3 

Density (Pa) ji ji. -.3 

Blank Concentration (Ca) 

Rinse Volume (Vaw) ...... m s7 ....... 

Residue in Rinse (Wa) = Ca*Vaw*Pa 0.0006 0.0007 0,0008 

Date of Weighing 

Time A .7~or: AM! 

Gross Weight 

Date of Weighing . 4D' 

Time 

Gross Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Average Gross Weight 98.4930 106.2810 96.2500 

Less Blank Residue (Wa) 0.0006 0.0007 0.0008 

Average Beaker Tare Weight 98.4909 106.2791 96.2488 

Weight of Particulate in Rinse (mg) 1.48 1.21 0.49 

METHYLENE CHLORIDE BLANK ANALYTICAL DATA FORM 

Blank Volume (Va) 

Date of Weighing 

Time t A 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Average Gross Weight 109.08705 

Date of Weighing 

Time .2 A 

Tare Weight 

Date of Weighing 

Time 

Tare Weight 

Average Tare Weight 109.08625 

Weight of Blank (Ma) 0.0008 

Ca= Ma/(Va*Pa) = g/g 2.353E•06 

Note: In no case should a blank residue greater than 0.01 mg/g or 0.001% of the blank 

lweight be subtracted from the sample weight. 

141 
Sheetl 

Summary of HF, HCI, and Cl- Analysis 

Plant: Daltile, Muskogee, OK 

-Location: ITrim Kiln Exhaust 

Dar te: - 12/8/051 

R6'n- Imp # IVolume Milution I FI-, ug/mi HF, mg I 

1 1 & 2 300: 20 11.721 74.04696 15.17;93.56856 

1 1 & 2 1 300 201 11.421 72.15156 14.911 91.96488 

Average --j L 73.09926 ; 

211 &2 1 --300-i 10' 20.151 63.653851 28.961 31264 89.

211 1 & 2 300 i 10 , 21.381 67.53942' 31.331 96.62172 

Average 1 65.59664 92.96718 

~

 300 __10 21.14! 66.781261 26.63 

 3001 io 20.83 65.8019728.88 

1 Average 66.29162 L 

82.12692 

89.06592 

85-59642 

-ku,-n, # jImp# Volume Dilution Cl-, ugimi C12, mg 

113 & 4 3001 1, 1.59 0.477 

113 & 4 300 j v 1 1.59 0.477 1 

0.4771 

213 & 4 300 1 2.951 

2'3 & 4 300 1 0.894 

895 

313 & 4 30 .11 

1 

1.11! 0.333 

-~ 4 300 1.21 

0.3465 

142 

Page 1 
Sheetl 

Summary of HF, HCI, and Cl- Analysis 

Plant: iDaltile, Muskogee, OK 

Loca—Uon: Kiln Scrubber Exhaust 

ba te '- -- --:- 12/7/05 1,' 

Run # Lrpp luDilution ~Fl-, u /ml HF, mg 9 ug/mi 'HCI, mg 

1 ~ 1 &2 5001 1 0.43 Lq.2~636~ 1.69 0.86 6 '&6 

111 &2 500 1 0.4 0.2106 1 1.69 0.86866 

Average 4 0.218498 1 0.86866 r. 

2'1 & 2 500 1 0.70551 

0.742365 

1 0.7239381 

1.34 0.68876 

0.69647 

1 . 34 

2 1 &2 5001 1 ; 1.411 

Average 

3'11 &2 500 0.44 0.23166~___ J.28 ~ 0.65792 

311 &2 500 1 0.481 0.252721 1. 2 -1 ---0.6168 

Average 0.242191 0.63736 

Run # Imp# Volume Dilution iCl-, ug/mi ~ C12, mg 

113 & 4 250! 1 0 ; 

1 F3—&- 4— 250 F 1 0 0' 

0! 

2 3 & 4 —.-...--.-250 1 0 1 oi 

2 3& 4 250 1 O 

3j3&4 250 11 01 

3i3&4 j 250 11 0 

oi 

1.44 

Page 1 
Sheetl 

Summary of HF, HCI, and Cl- Analysis -- 

F~I-a n"t-: Daltil , Muskogee, OK 

Location: ITrim Kiln Exhaust 

ba-*t-e--:'-.----1 12/8/0§1-.-- 

Run # Imp# Volume 11311utlon I HF, mg cl im 9 

1 1 &2 1 3001 -f T- 11.72! 3 15.17 46.78428 

11 &2 3001 -11.42; 36.075781 14.91 j 45.98244 1 -0- L 

lAverage 36.54963' 46.38336 

211 & 2 300 10 20.15 63.65385 28.96 89.31264 

211 &2 

00 

10~ 21.38 67.539-4-2 31 33 96.62172 

Average 65.59664 92.96718 

31 -11 & 2 1 21.141_ 66.78126 26.63 82.12692 

311& 2 3001 10 20.831 65.80197' -2-8.88 

Average 6~6.29162 85,5964~ 

Run # Amp # Volume Dilution ;CI-, ug/mi C12, mg 

113 & 4 3001 1 1.59 0.477 

1'3 & 4 3001 1.59 0.477 

& 4 300 

213 & 4 300 1 

1 

1 

0-477 

2.95 1 0.885! 

O'NA, 

0.8895 

313 & 4 - 300 

313 & 4 ;j 300 

1 1.111 0.333 1 

1 1.2' 0.36L 

0.3465; 

I 

Page 1 
Conditions : 4_96 ug/ml F1- in H2SC34 

= 4 _ 93 ug/ml. Ci- i n H2SO4 

Date : 12/09/'2005 

Time : 10-46=34 

-102 . 4OOmV 1024 .000mV 

Component Retention Area External 

F1- 1. 

C1-- 1. 

412.24 N 4.6! 

287.24 H 4.3{ 

Component 

FlC1- 

N 

. ► 

Number Retention Area External Units 

1 1.033 412.26 M 4.65 ug/ml 

2 1.650 287.20 M 4.39 ug/m l 

699.40 9.04 

.14~ 
Cond'tioiis = 4.96 ug/ml Fl- in H2SO4 

4.93 ug/ml Cl- in H2SO4 

Date = 12/09/2005 

Time = 11:06:28 

—102.4OOmV 

uomponent Retent 

Fl- 1. 

ci- 1.6 3 

1024.00OmV 

0 

........... ....... ... ....... .......... ............. ............ ....... ........... ... ....................... ................. . ... ......... ................ .......... 

31 

21 

3i 

6 

......... . . .......... ................ .... . .... .................. ...... ... .......................... 

Area EXteTna I 

426,10 4.8, 

277.35 H 4.2! 

compondnt Number Retention Area External Units 

Fl— 1 1.016 426.10 4.82 ug/ml 

Cl.— 2 1.633 277.35 M 4.25 tig/ml 

VA 703-45 9.07 

14'7 
102.4 .00OmV 

F1- 

Ci10.07 

8.58 

-102.400mV 

Component REten`' Rrea Er,terna] 

855.80 M 

586 ..44 hl 

Conditions = 9.92 ug/ml F1- in H2SO4 

= 9.86 ug/ml Cl- in H2SO4 

Date : 12/09/2005 

Time : 11=16-04 

CQmponent Number Retention Area External Units 

Fl - 1 1.016 855.80 N) 10.07 u g/m 1 

C1- 2 1.650* 586.44 M 8.58 ug/ml 

2 1442.24 18.65 

• 
Conditions = 9.92 ug/ml Fl- in H2SO4 

9.86 ug/ml Cl- in F12SO4 

Date = 12/09/2005 

Time 11:37:13 

-1.02..4OOmV 

Component Retenti 

Fl- 1. 

ci- 1.66 

1024.00OmV 

0 ...................... .............. .......... .................. ........... ........... ......................... ......................... ......................................... ..... .................... .. ....... 

6 

2[ 

3I. »... I 

4 

6 

Area ExteM 

891.30 N 10.5 

578.30 M 8.4* 

Component 

Flc i__ 

K 

Number Reten't."Lon 

1 1.033 

2 1.666 

Area External Units 

891.30 m 10-50 ug/ml 

578.30 111 8 .47 ug/rnl 

1469.60 18.97 

149 
Conditions : 19.84 ug/ml Fl- in H2SO4 

: 19-72 ug/ml Cl- in H2SO4 

Date : 12/09/2005 

Time : 11:58:43 

Fl- 1. 

ci- 1.68 

1024.00OmV 

on 

!, ». 

.«... ...«...... 

............................. 

................... 

21 ........ 

3 

4[— : . 

6 

–102.4OOmV 

Component Retenti ATea ExteTna 

2015.60 M 22.9 

1295.24 H 18.9 

. Component 

Fl– 

ci– 

K 

Number Retention Area External Units 

1 1.050 2015.60 M 22.96 ug/ml 

2 1.683 .1295.24 M 18.94 ug/m1 

3310.84 41.90 

1. 5`0 
F1- 

ci1. 22.2: 

18.6; 

1952.35 N 

1275.15 H 

—102 .400mV 

uomponent Reten ' 

1024 .00OmV 

Area Externa 

Condltions : 19.84 ug/ml F1— in H2SO4 

= 19.72 ug/ml C].-- in H2SO4 

Date : 12/09/2005 

Time : ?2-08:11 

Component Number Retention Area External Un.i.ts 

F1— 1 1.050 1952,35 M 22.26 ug/ml 

Ca.— 2 1.fa66 1275.15 M 18.62 ug/m.l. 

2 3227.50 40.88 

151 
1024.00OmV 

mi uo LAt'01 "a 

Conditions : 39-68 ug/ml Fl- in H2SO• 

: 39.44 ug/ml Cl- in H2SO4 

Date : 12/09/2005 

Time : 12:17:36 

-102.400m%/ 

Component Retent ion . . . . ...... ........... 

~' . 

....... . .............. 

..................... 

50 .......... 

.................. ..... 

2 

4 

6 

3757.50 M 42.27 

2706.60 H 41.2E 

Fl- 1. 

ci- 1.7 

Component Number Retention Area External Units 

Fl- 1 1.066 3757.50 111 42.27 ug/ml 

ci- 2 1.750 2706.60 Ivi 41 .28 tjg/ml 

2 6464.10 83.55 

152 
Conditions : 39.68 ug/ml Fl- in H2SO4 

z 39.44 ug/ml Cl- in H2SO4 

Date z 12/09/2005 

Time : 12:26:54 

-102.4OOmV 

uomponeEt Retenti 

Fl- I . 

ci - 1.75 

1024.00OmV 

on 

............ ...... i ............................... ....... ............... ...................................... . ..... . ........................

. 

. 1 

Ii ~~: . ........... __ ~ 

. . ...... . ........... 

.......... ............... 

.. ........... 

.................. ........ .. 

......................... 

0 ............. ............ 

2 1 

4 

5(........ " ; ~ 

6 

. ................ . ..................... . ..... 

ATea EXteTRa.. ~ 

3763.40 M 42.31t 

2698.10 h 41.11, 

Component Number Retention Area External' Units 

Fl- 1 1.066 3763.40 M 42.33 ug/ml 

ci- 2 1.750 2698.10 11 41.15 u'q/M1 

2 6461.50 .83.48. 
AMOUPIT IPt3ECTED 

AREA 0.000 

0.000 

3760.450 

39.680 

i 

2 

3 

4 

5 

Calibrat.ion filp = F1-.ca]. 

Avg slope of cur ;ia ,. 94.40 

Y-axis intercapt: 0.00 

Coef f of 1i n regr = 0.84 

No . Ar ea. Amou nt CF 

0: 0.000 0.000 0.000 

1 : 419.200 4.960 84.516 

2: 873.550 9.920 88.059 

3: 1983.975 19.840 99.999 

4"- 37b0 .450 39.680 94.769 

~ V-5 4 
AMOUNT IhI.IECTED 

AREA 0.000 

0.000 

2702.350 

39.4-4n 

1 

2 

3 

m ou 

5 

Calibration file ~ Cl--.cal 

Avo slope of curve : 65.32 

Y-ax i s i ntercept z 0 . QO - 

Caeff of l i n regr : 0.91 

1\1o . Area P.mount CF 

0 : 0.000 0.000 4 K.00U 

1 . 282.275 4.930 57 w257 

2= 582.370 9.860 59.064 

3 = 1285.195 19.720 65 . 172 

4 = 2702.350 39.440 68 . 51.8 

, 

. ~ ,r-,~ 5 
Conditions : Daltile Muskogsae 

: Scrub Exhaust 

Ru n It ". I nips 1 'o-c 2 

--eta 500mle Dilution 1/1 

Date 21/100/2005 

Time 4 " .,7 44 

-102.4OOmV 

component Retention - 

1024.00OmV 

Area Externa 

Fl- 1. 

ci- 1.75 

.. .................. .......... ........ . .......... ........................ . . ..... ........ .... .......... . ................. .............................................. ........ .......... .... ................. 

21........ .~ ~ 

4 

..................... ............ .. ............ ... ....... . .................................................... . .............................. . .......................................................... ........................................................ ... ....... ..... 

36.40 H 0.4 

96.60 N IS 

Component Number Retention 

Fl- 1 1.066 

ci- 2 1.750 

2 

Area External Units 

36.40 M 0.43 ug/ml 

96.60 M 1 .69 ug/ml 

133.00 2.12 

1.82 
Conditions : Daltile Muskogee 

: Scrub Exhaust 

: Run #1 Imps 1 & 2 

: Volume 500m1s Dilution 1/1 

Date : 12/09/2005 

Time z 14:27:02 

-102.400mV 

component Retent 

Fl- 1. 

ci- 1.7 

1024.00OmV 

10 . . ..................... . .... . ............ . ..... 

50 

3 

4 ........ 

. ............................................................................. 

• Area Externa 

33.64 H 0.4 

96,54 1.6. 

Component Number FZetention Area . External Units 

Fl- 1 1.066 33.60 (vi 0.40 tlg/ml 

ci- 2 1.750 96.50 1 .69 tig/ml 

2 130.10 2.08 

1 R3 
—102.400mV 

Component Reten . 

1024.00OmV 

fI/P 

1.34 

1.37 

.0 , 

1, 

1. 

( unknown•) 

F1-- 

C1- 

Area External 

32.80 

113.35 

78.31 H 

Conc#itions = Dait=le Musl<ogee 

= Scrubber Exhaust 

= Run #2 Imps 3. & 2 

= Volume 500m1s Dilution 1/1 

Date : 12,/09/2005 

Time = 15=02=34 

Component Number Retention -Area External Units 

Fl-w :L 1.216 113.35 x.34• ug/rni 

CJ.-- 2 1.733 78.3:1 M 1.37 ug/ml 

2 191.66 2.71 

164 
Conditions = Daltile Muskogee 

Scrubber Exhaust 

Run #2 Imps 1 & 2 

Volume 500m1s Dilution 1/1 

Date = 12/09/2005 

Time = 15:12:27 

-102.4OOmV 

Component Reten 

(unknown) 0. 

Fl1024.00OmV 

Lion 

.. .......... .......... 

................. ... ......................... ....... ....... .......... ............ ............................ ........... ............. ... .. ..... ...... ............ .. ........ ............ 

216 

733 

3t 

4 

61 

............ .......... .......... ........ . ......... ........ .................... . .. ....... ....... ......... ................................... .......... ................ .......... ....... .. ....... . .............. ....... . ....... . .................. 

Area Externa.' 

30.40 NIA 

119.50 1.41 

76.90 H 1.31 

Component 

Fl- clK 

Number Retention Area External Units 

1 1.216 119.50 1.41 ug/m1 

2 1.733 76.90 M 1.34 ug/rnl 

196.40 2.76 

165 
cond (12 'k , itions : Blan 

Date : 12/09/2005 

Time : 15:22:07 

-102.4OOmV 

Component. Retent 

(unknown) 2. 

1024.00OmV 

0 

t " I 

2 

3 ........ 

Area External 

65.15 m N/A 

61 

Component Number Retention Area External Units 

Ee 0.00 0.00 

1. ~ s 
F1- 

cl- 

--102.40omv 1024 .00OmV 

CompanAnt Reten . 

1. 

I. 

Area Ext'erna l 

379.44 E1 4.25 

318.46 M 4,82 

Conditions = 4.96 ug/m]. F~ — ~.n H2SO4 

=4.93 ug/m 1 C-- i n H2504 

Date = 12/10/2005 

Time = 09=31-29 

Component 

~ 

~

l_ C i -- 

KA 

Number Retention 

1 1.050 

2 1.700 

Area External Units 

379.44 M 4.25 ug/ml 

318.06 m 4.82 Ug/m]. 

697.50 5.07 

167 
Conditions = 4.96' ug/ml F1-- in H2SO4 

= 4.93 uglml C 1-- i n H2504 

Date = 12/10/2005 

Time = 09-40-30 

— 102 . 400mV 

Component Retenti 0 R.._ .. _.. .. ~.... 

1024 . C~ OOmV 

Area Externa' 

F1' 1. 

Cl- 1.6 

j s». 

83 ~ j.... 

398.44 Ef 4.4( 

288.25 M 4.4( 

31 ...... : i 

. . ~ 4I........ ; . ~ 

5 

Gomponent Number Retention Area External Units 

F]. — 1 - 1. 050 398.40 M 4.48 ug/m l 

C1— 2 1.683 288.25 M 4.40 ug/m.l. 

2 686.65 8_ 88 

168 
Conditions : 9.92 ugg/ml Fl— Jin H25O4 

: 9.86 ug/ml Cl— in H2SO4 

Date ".12/10/2005 

T i me : 09:49:26 

102.4OOmV. 

COMPOwt Retenti 

F I - 1. 

ci - 1.68 

(unknowO 2. 

1024.00OmV 

on ............ 

............................. ............ . . ............................................................................ . ................................... ...................... ................ ~ ................. 

..

...................... ......... 

3 

2

1 

~ `~ ~ 

; . ~ 

.......... 

~ ....... : i 4 

6 

........... .............. . ...................................................................... ............. ... .... ........... . . ............. .............. .. . ........ . . . . . ......... . ................ .. . .......... . ........... ....................... .. 

A,r ea ExteTnal 

898.75 M 10 59 

617.26 Pi 9.01 

72.30 H N/A 

Component Number Retention 

Fl- 1 1.050 

ci- 2 1.683 

2 

-compo nqRndje~A" ............. ot g;e 

cl3 ...... 

.............. ........... : .......................................................................... . ............... 

F-1- Component Number Retention 

1 1.050 

2 1.683 

I 

Area External. Units 

898.75 11 10.59 ug/m 

617.26 M 9.01 ug/mi 'L 

1516-01- 1.9.60 

.H2504...... .......... 

...... ...... ......... .......... 

T02,4 :0-0-um., 

Area External Units 

886.40 M 3-0.44 Llg/Ml 

6 21.5 1. M 9 .07 ug/rnl 

1507-91 19.51 

89b?40 N ExtjOV4 

6 21. 51 N 9.( 

169 
Conditions : 9.92 ug/ml Fl- in H2SO4 

: 9.86 ug/ml Cl- in H2SO4 

Date : 12/10/2005 

Time - 10:03':01 

-102- .4OOmV 

Lomponent meEenti on 

1024.00OmV 

Area External 

Flci- 1.68 

............ . ... 

21 

....... 

3 

4 ....... 

......................... .............. . ...... .............. ................ ......... .. ..................... ............ ............ ............................. 4 i .......... I ...... ...... .................... ... 

886.40 M 10.44 

621.51 M 9.07 

Component Number Retention Area External Units 

Fl- 1 1.050 886.40 11 10.44 ug/ml 

ci- 2 1.683 621.51 11 9.07 ug/m1 

2 1507.91 19.51 

170 
Conditions 

Date 

Time 

Coraponent Reter 

= 19.84 ug/ml Fl— %n H2SO4 

= 14.72 ug/ml C1— in H2SO4 

: 12/10/2005 

= 10:16=09 

102 . 400mV 

. "1- 1. 

C1- 

(unknown) 2. 

1024 .00OmV 

Area External 

1940.75 M 22.13 

1351.41 19.92 

112.44 N/A 

Component 

Fl— 

r- 1_ 

K 

Number Retention Area External Units 

:l 1.050 1940.75 M 22.13 ug/ml 

2 1.700 1357.07 19.92 ug/m]. 

3297.82 42.05 

171 
Oondi,tions : 19 .S4 ug/ml F1— in H2SO4 

: 19.72 ug/ml Cl-- in H2SO4 

Date = 12/10/2005 

Time : 10:27:12 

--102 . 4o0mV 1024 . ooC7mV 

Componept Retent' ~o~..:...._...__ ~ ..._..,....M. _...._.. ......._......_..,w.....M....._.._..........._..w...._.._..._..._.__..M. ................ ............. r. 

 ......... ! ~ ~ 

._.......__w ...' 

1 ~.....w i :.. ......._..... ......................... ~:,~~~„• . F1- 1. 

I ~+, , ..... ~....... 

! 1 6 '_ ........ ~:... ...._..: ~.:~ f C1- 1.71 

2

........ 

~ 

{ 3 ........ 

4 

5 _ : 

6 

 ...... ; 

..................... ............. ..... .__.._................................. _.. ... .............. .......................................................... ...._...._....................................._.._........_M..._ ~ 

Cornponent Number Retention Area External Units 

Fl— 1 1.066 1951.05 M 22.25 ug/m:l 

Cl— 2 1.716 1327.70 M 1.9 .46 ug/m l 

2 3278.75 41.70 

Area External 

1951.05 M 22.25 

, 

1327,14 M 19.46 

1'.~ 2 
Area External 

3961.65 H 44.53 

2792.20 M 42.64 

124.22 M N/A 

Conditions : 39.68 ug/ml Fl- in H2SO4 

: 39.44 ug/ml Cl- in H2SO4 

Date : 12/10/2005 

Time : 10:52.`46 

-102.4OOmV 

uomponenL xetOn'Ll 

Fl- 1.08 

Cl- 1.78 

(unknown) 2. 

1024.00OmV 

............................. . ......... .. ........... 

3 ........................ .. ................. ................ ........ 

................... 

3 ............. .......... ......... 

21 ,_~: 

31 ....... 

4 

61 .......... 

......................................................................... ... ...... .. .............. . ........... . ........................................... ............... ....... ......... ............ ....... ....... . . ..................... 

Component 

F I — 

ci2 

Number Retention Area External Units 

1 1.083 3961.65 M 44.53 ug/ml 

2 1.783 2792.20 M 42-64 ug/ml 

6753.85 87-16 

173 
Conditions = 39.68 ug/ml Fl- in H2SO4 

39.44. ug/ml C.'l- in F[2SO4 

Date 12/1012005 

Time 11:01:39 

-102.4OOmV 1024.00OmV 

uOMPOnent KeLent ion 

~ ,..I•w ~ i 

. ............... 

so 

2 . ..».. 

.ii . 

4 

3 

4 ........ 

61 

... .... ........................ ..... . .. . ..................................................................... ...... ................................ .... . ...................................................................... . .............................................. 

Component -Number Retention Area External Units 

Fl-- 1 1.066 3890-85 M 4.'-

'j

~ .74 ug /I  m 

 1 

ci— 2 1.750 2737-50 M 41.77 ug/ml 

2 6628.35 85-51 

Fl- 1. 

ci- 1.7 

Area External 

3890.85 m 43.71, 

2737.50 M 41.77 

1.74 
AM4UNT INJECTEU 

AREA 0.000 

0.000 

3926.250 

39.680 

i 

2 

3 

4 

~ 

Calibration file = Fl-_oal 

Avg s1oFe of curve = 96.24 

Y-ax is i nteroept : 0.00 

roeff of l i n regr : 0.90 

No . Area Amount CF 

0: 0.000 0.000 • 0. 000 

1 ~ 388.920 4.960 78.411 

2: 882.575 9.920 88.969 

3: 1945 .9(30 19.840 98.080 

4 = a926 .250 39.680 98.948 

175, 
AI"iQUNT INJECTED 

AREA 0.000 

0.000 

2764.850 

39.440 

1 

2 

3 

4 

5 

Calibration file : Cl-.cal 

Avg slope of curve '- 67.77 

Y-ax i s i ntercept : 0.00 

Coeff of l i n regr x 0.92 

hlo . Area Amount CF 

0: 0.000 0.000 0.000 

1 : 303.155 4.930 61.492 

2: 619.385 9.860 62 ~ 818 

3: 1342.385 19.720 68 . 07 2 

4 = 2764 .850 39.440 70.103 

176 
Conditions = Daltile Muskogee 

Scrubber Exhaust 

Run #3 Imps 1 & 2 

Volume 5001s Dilution 1/1 

Date 12/10/2005 

Time = 11:54:46 

-102.4OOmV 

uomponenli, Retent 

Number Retent-ion 

1 1.233 

2 1.730 

Fl- 1.2 

ci- 1.7 

ComponentFlciVA 

1024.00OmV 

Area Extel-'nal Units 

34.20 11 0.44 ug/ml 

78.85 1 .28 tig/ml 

113-05 1.72 

~ on ... .... . . ............................ .............. .......... ............... . ................ . ............ . .......... 

33 

so 

2 

3 

4

..... 

5 

6 

... . ..... . .... . .... . ........... . ... . .......................... 

Area External 

34.24 N 0.44 

78.85 1.2E 

i77 
Conditions : Daltile Muskogee 

: Scrubber Exhaust 

: Run #3 Imps I & 2 

z VOlLtMe 5001s Dilution 1/1 

Date : 12/10/2005 

Time : 12:04:26 

—102.4OOmV 

UOMPOnent i(etent 

Fl- 1.1 

ci - 1.71 

1024.00OmV 

.... . ............................. ...... . ........................ ..... . ..... ............................. .......................... ........................... . .......... 

i3l 

6 

2 

 . ..». i 

~ 

AT ea External 

38.04 H 0.4E 

73.95 N 1.2( 

61 . . ..... 

; 

~ 

............... ......... ....... ....... .......................... . ........ .. ... .......... ....... ........... ... ............ . 

Component 

Fl— 

ci— 

rA 

Number Reten"E-Aon 

2 1,716 

Area Exi--ernal Unfts 

38.00 M 0.48 ug/ml 

73.95 M 1 .20 ug/rnl 

111.95 1.69 

:111WK-W, LKI W, 
Conditions : Daltile Muskogee 

: Trim Kiln 

: Run #1 Imps I & 2 

: Volume 3001e Dilution 1910 1/20 

Date : 12/10/2005 

Time : 13:07:37 

-102.400mV 

COmponeflt vetenti 

Flci- 1.73 

1024.00OmV 

0 

...... ...... 

... . ... ..... 

............. . 

....................... 

.......... . ................ . 

32 ...... : f,. ... _......... ~ 

1t 

3 

4 

6 

.. . ............ ............... . ........... ............................................................................ ........ .. 

Area External 

1074.99 M 

1008.63 M 

. 

11.72 

15.1; 

Component 

ci2 

Number Retention Area External Units 

1 1.066 1074.99 M 11.72 ug/ml 

2 1.733 1008,63 M 15.17 ug/m1 

2083.62 26.88 

179 
Conditions : Daltile - Muskogee 

: Trim Kiln 

: Run #1 Imps 1 & 2 

: Volume 3001s Dilution 12W IAO Date : 12/10/2005 

Time : 13:29:29 

—102.4OOmV 

ComponeSt Retenti-on 

.. 

1024.00OmV 

ATea External 

Fl- 1. 

ci- 1.71 

................ 

I ........ 

. ........... . .. .................... . ...... .......... 

. I; 

6 

21 

3 1 ....... 

4 

................ *-............-...............-....-...-............-.-..................-........I .......... . .. . . . . . ...... .. ........... ................. ................... 

1043.40 M .11.42 

989.80 m 14.91 

Component 

FI -. 

ci2 

Number Retention "Area External Units 

1 1.050 1043.40*M 11.42 ug/ml 

2 1.716 989.80 m 14.91 ug/ml 

2033-20 26.33 
Conditions = Daitile Muskogee 

= Trim Kiln 

= Run #2 Imps 1 & 2 

= Volume 3001s Di1ut -iQn 1/10 

Date = 12110l2005 

Ti.me = 13=38=33 

--102 .400mV 1024.00OmV 

Component Retention Area Ezternal 

F1- 

Ci1.08 1.78 

1976.90 H 20.1E 

2008.60 M 28.4E 

Riumber Retent.i-on Area External Units 

1 1.083 1976.90 11 20.15 ug/rn1 

2 1.783 2008.60 M .28 . 96 ugrm l 

3985.50 49.11 

Component 

F J. -- 

C .l. 

K 

181 
Conditions z Daltile Muskogee 

: Trim Kiln 

: Run #2 Imps 1 & 2 

: Volume 3001s Dilution 1/10 

Date z 12*110/2005 

Time : 13:47:22 

-102.400mV 1024.00OmV 

Componept Retenti on........ . ........ ........... ...... ........ .................. . ..... . . ... .... .. ..... .. .. .... ................ ......... ....... ............................. ....... . ......... .................. . 

Fl- 1.10 0 ....... . ...... ....... 

ci- 1.81 '6..... .................. 

2 

4 

' : . 

61 

........ ................. ............. ...... .. .............. .. ......... ................. .......... ...... ..... . ....... ........ . ...... 

Component Number Retention Area External Units 

Fl- 1 1.100 2099.50 M 21.38 ug/ml 

cl- 2 1,-816 2.180.08 M 31.33 ug/ml 

2 4279.58 52 .71 

ATea Externa 

2099.50 M 21.3 

2180.08 H 31.3 
Conditions : Daltile Muskosee 

= Trim Kiln 

: Run #3 Tmps 1 & 2 

= Volume 3001s Dilution 1/10 

Date = 12/10/2005 

Time = 13=57:56 

-102 .400mV 1024,OOOmV 

Component Retenti4n Rrea Externa 

F'1- 

C1- 

2076.05 M 21.1 

1840.85 M 26.6 

Component 

rl-- C1- 

Number Retention 

1 1.083 

2 1.783 

Area External Units 

2076.05 M 21.14 ug/m 1 

1840.85 M 26.63 ug/ml 

2 3916.90 47.77 

IR3 
Conditions : Daltile Nluskagee 

: Trim Kiln 

: Run #3 Imps 1 & 2 

: Volume 3001s Dilution 1/10 

Date = 12/10/2005 

Time = 14:06:57 

—102.400mV 1024 .040mV 

Component Retent' i o n ................. »....«............,.«...».......................».w.«...w.....w....._.....w.......«._..«..».......».....w..w.w.....«.....»....,» .................. .......w ....... .w.w ....w..w............w...w w......w.w.»w... 

, 

5 0 ~ .w ,» 

~ f •w 

».w ....N.......b...Mi w.»..q..ny.w.p..w.......wr.w...n. . 

~ .. w.». r..........=w ........................«.=...w.w.»..w,.... 

z

. ..... 

~ ,.. 

,~M • 

.« 

................. 

.....ww.».».w.w .«. » w. ~n=n= ~=nnununnmu=m=xnnu=n=a _ 

3~».w. : 

• ' E 

4 . .... 

5 

 ..... 

: 

~ ; 

i • 6 . w.... ; 

' i 

Component Number petention Area External Units 

F 1-- 1 1.066 2044.55 M 20.83 ug/m l 

2 1.750 2002.81 h1 28.88 ug/m3. 

2 4047 _ 36 49.70 

F1- 1. 

ci- 1.7 

Area Externa 

2444=55 Ef 20.8 

2002.81 M 28.8 

184 
Fl- 1. 

Cl- 1.68 

Conditions : 19.84 ug/ml Fl— in H2SO4 

: 19.72 ug/ml Cl— in H2SO4 

Date : 12/10/2005 

Time : 14:16:03 

—102.4OOmV 

Component Retenti . ....... . ..... ..... ......... . ....................... .......... . ........... 

............................ 

............. ............... ...... 

21 ...... 

~,~.. 

3 

4 

6 

1024.00OmV 

2080.40 M 21.11 

1291.73 h 19.0 , 

Area ExterRa 

Component Number Retention Area Exteriial Units 

Fl— 1 1.050 2080.40 M 21.19 ug/ml 

ci- 2- 1.683 1291.73 11 19.03 ug/ml 

2 3372-13 40.22 

195 
Conditions : Blank 

Date : 12/10/2005 

Time - 14:32:12 

—102.400mV 1024.00OmV 

component Ratept ion 

.............. ....... 

Area ExteTna 

2 ...... 

(unknown) 2.3 50 146.95 N NIA 

4 

6! 

. ... . ......... ............ ............ .... 

Component Number Retention Area External Units 

0 . 0.00 0.-00 

. Z ~ s 
Conditions =4.93 ug/ml Ci— in hlaON 

Da.te = 12719/2005 

Time -- 07=56=14 

—~ 3 .200mV 

Component Retention 

(unknown) 0. 

ci51.2 .00Omt! 

Area Externa; 

1374.55 li NIA 

245.90 Pf 4.51 

Component Number Retention Area External Units 

C1 — 2 .1 . 86b 295 .90 fvl 4.51 ug/ml 

1 295.90 4.51. , 
Area f-txterna 

1130.00 N/A 

272,00 M Cii 

126.06 M N/A 

cl - 1. 

(unknowR) 2. 

Conditions : 4.93 uo/nil Cl— in NaOl-i 

Date : 12/19/2005 

Time : 07:59:45 

—51.200mV 

Component Retent-lon 

Unknown 

.......... .......................... .. ......... ............... . .. ........ ................................................................................... 

. ........... . .. 

8501 ..... ....... .. .......... ......... 

.. .................... 

$66 ................ 

2 

3 

4 

61 

............... 

51.2.00OmV 

Component Number Retention Area External Units 

Cl— 2 1.866 272.00 M 4.18 ug/ml 

I 272.00 4.18 

~ WE, 
Conciitions = 9.86 ug/ml CI.— in hlaOH 

Date = 12/19/2005 

T i. me - 08 : 03 = 09 

—5.1 .200mV 

Oomponent Retention 

(unknown) 0.8t 

Cl- 1.86 

512.C700m`I 

Area Ex'Lernal 

1223.35 N/A 

575.40 M 8.79 

Component hiumber Retention Area Exter nal Units 

Cl•- 2 1.866 575.40 M 8.79 ug/ml 

1 575.40 8.79 • 

189 
? a6a.00 N/A 

564.40 M 8.6 , 

I00.17 H N/A 

(unknown) a, 

Cl- I . 

(unknown) 2. 

Co ndit ions : 9.86 Ug/ml Cl-- in NaQH 

Date : 1 2!1 9l2005 

Time = 08 - 05 = 54 

—51 .200mV 

Componen ~ Re ~ ention 

512 .QOC7mW 

Area Eaternc, 

Component. Number Retention Area External Units 

C1— 2 1.866 564.40 M 8.64 ug/mi 

i 564.40 8.64 

190 
Conditions = 14 .79 uglrnl Cl-- i n NaOH 

Date = 12f 1972005 

Time = 08 = C39 = 33 

—51 . 200mV 5 1 2 . (3C}qmV 

ComponQnt Retention 

(unknowl') 0. 

ciArea Externa 

1140.80 rdIA 

937.40 M 15.0 

Component Number Retention Area External Units 

Clμ- 2 1.866 937,f0 iu1 15.07 ug/ml 

1 937.40 15*. 07 

.. 1.91 
(unknorin) O.K. 

C1- 1.86 

1077.50 N/A 

958.00 h1 15.3t 

Conditi.ons = 14.79 ug/ml Cl- in NaOH 

Date 12/19/2005 

Time = 08=12=20 

—51 .200mV 

ComponenT Retention 

512 .00OmV 

Area Externa 

Component hlumber Retention Area External Units 

Cl-- 2 1.866 958.00 fh 15.36 ug/ml 

1 958.00 15.36 

1.92 
Conditions ' 19.78 ug/ml C].-- in NaOH 

Qate : :i? /1.9/2005 

Time = 08-16=00 

--5 :L . 200 rn'J 

Compoaent Retention 

(unknown) Q.8E 

ci- 1.86 

51.2 . OOOmV 

Area Ezterna'. 

659.10 hl/A 

1246,65 M 16,6e, 

Component Number Retention Area External Units 

C1-- 2 1.883 124•6 . b5 m 18 . 69 ug/m]. 

1 1246 _ 55 18.69 

193 
Conditions = 19.78 ug/ml C].— in MaOH 

Date = 12/19/2005 

Time - 08:21=30 

—51.200mV 

Component Retention 

; unknotiin } 0. 

C1- 1, 

512 .00OmV 

Area Externa': 

844.80 N/A 

1272.70 hf 19.03 

Component Number Retention Area External Units 

C1-- 2 1.883 1272.70 M 19.03 ug/ml 

1 1272.70 19,03 

P4 
AMOUNT ZNJECTEa 

AREA 0. 000 

0.00C 

1259.675 

19.720 

1 

2 

3 

4 

5 

Calibration file = C1-- .cal 

Avg slope of curve : 63.88 

Y--ax:~ s a. ntercept = 0.00 

Coeff of .L a, n r egr : 0.83 

No . Area Amount CF 

0: 0.000 0.000 0.000 

1: 283.950 4.930 57,596 

2: 5601.900 9.860 57.799 

3 - 947.700 14.790 64.077 

4= 1 259 . 6 75 19.720 63.878 

, 

~ Iq~ 
Condi'tions : Da.lti le , Muskogee , OK Ki 1 n 5crubber 

= Run #1 ImRs 3 & 4 

: Volume 250'Dilution 1/1 

Date = 12/19/2005 

Time : 10=15:29 

.~- 5". .2a'OmV 512.040mV 

Campanent Retentian 

(unknown) 0.8 

Area External 

682.20 N/A 

( unknoain ) 2. 

~.. ~ ........_.....~~_...... ............. ............ .................. ~.~ ....._..._........_.._..... ~ ..._.~ ........_............. _._. ~................. .............................................._.............. ~ 

50 """•••• «mn..unun• 1 ...... . ~ . 

. . ... ................ 

,!I • 

, e •~ 

2 

 . ...... ; ~ ,..:a,• 

3 . ..... : ~ 

4

~ 

5 ; 

1 

6 . ..... ; . 

. .................................... .........................,..................... ... ........ ......... .........,............ . ..... ................... ....................... .._.... .................... .......... ......... ... ....,...........,....................,.... ~ 

231.74 NlA 

ComRonent hlumber Retention Area External Units 

, 0.00 0.00 

2n2 
Conditions : Daltile, Muskogee, OK Kiln' Scrubber 

= Run #1 Imps 3 & 4 

= Volume 250 Dilution 1/1 

Date = 12/19/2005 

Time = 10:25:59 

-.51 .200mV 

CoMDonent 2etention 

(unknawn) 0. 

~

unknown ~ 2. 

unknown 2. 

53.2.000mV 

Area fxternal 

523.05 h/A 

257.00 NIA 

362.30 N/A 

Component Number Retention Area External Units 

\ I • •• •wi •J 

203 
Conditions Daltile, Muskogee, t1K Kiln Scrubber 

= Run #2 Imps 3 & 4 

~ Volume 250 Dilution 1l1 

Date 1211912005 

Time = 10:29:55 

--51 , 20QmV 

Comaonent Retention 

512.40amV 

Area Externa: 

(unknown) 4. 

(unknown) 1. 

(unknotan) 2. 

463.45 N!A 

233.54 NIA 

372.60 NlA 

Component Number Retention Area External Units 

F 0.00 0.00 

P4 
Conditions = Daltile, Muskogee, OK Kiln Scrubber 

= Ru n#2 Z rnps 3& 4 

= Volume 250 Dilution 1/1 

Date = 12/19/2005 

Time = 10=34:01 

--51 .20QmV 512.000mV 

Component Retention 

(unknown} U. 

( unknown ) 1. 

(unknown) 2.' 

Component Number Retention Area External Units 

101 C0 •• • •• 

Area Externa] 

470.20 N/A 

234.55 NlA 

379.14 NIA 

2n5 
Conditions = Daltile, Muskogee, OK Kiln Scrubber 

= Run #3 Imps 3 & 4 

: Vo3.ume 250 Dil.ution 1/1 

Date : 12/19/2005 

Time - 10=42=35 

–51 .2.00m`J 512.00Om`J 

component Retention 

{unknown} 0.8 

Area Externa 

486.90 NlA 

(unknown) 1.95 

(unknouxn) 2, 

~ __._._.«...... . ~I, ..._._..« ._.__«.«.«.__«..........._. .... .... ... ........ ~._._..._...... _.« ...«....... «........_.«..««..«.«....................«.«• ......................._...««....._........._. _ ._ .. ~ 

50...... .....«... ......: • ....,.,,... i : ~3 ~~ • 

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0 ~ 2 

: ~ f 

3 — : 9 . ~ 

•i : , 1 

~ . ~ . 

44...__ : 

I . ~ . , 

~_.- --- ... ------ .~...._._.. ~ 

254.60 NIA 

338.85 N/A 

Component Number Retention Area External Units 

or, 0.00 0.00 

• 2n6 
Conditions : Daltile,, Muskogee, OK Kiln Scrubber 

: Run #3 Imps 3 & • 

: Volume 250 Diluti.on 1/1 

Date : 12/19/2005 

Time : 10:46:29 

--51.200MV 

Component Retent 101 

.. ............ 

(unknown) 0. 8 so 

~

unknown) 1.9 

unknown) 2. 

so 

2 

3 

6 

............. 

Area External 

507.05 N/A 

243.50 N/A 

328.90 NIA 

51.2.00OmV 

Component Number Retention Area External Units 

x 0 - 00 0.00 

207 
Concfitions : Daltile, Muskogee sok: Trim Kiln 

: Run #1 Imps 3 & 4 

= Volume 300 Dilution 1r1 

Date : 12/19/2005 

Time : 10:55:10 

—51 .200m41 

Component Retenti 

(unknown) 0.8 

Cl ~- 1.783 

(unknown) 2. 

512. 0OJmEr 

o~ ....~M........ ,~... ._.. ......_......._.._... _ _....... . ... _. ................. ...... .. ._.~.,......_._..._ .~._....._.._.........._..._.............. _._ .~~....__....._............_.___ ~ 

50 ~~. ...... ~ 

2. 

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b........ : 

I ; . 

~............ ........................._ ................. ..........._.............. ..... ....... ....... ..... .................. _ ...................... .. ......................... .......... ....._................................ ............. ............. ..... ........ ~ . 

Area EYterna: 

611.40 N/A 

91,60 M 1.5C, 

424.90 N/A 

Component Mumber Retention Area - External Units 

C 1-- 2 1.783 91.60 M 1.59 ug/ml 

0 91.60 1.59 

208 
Conditions : Dalti 1e , Mus kogee , 04G Tr im Ki 1 n 

: Run #1 Imps 3 & 4 

= volume -300 Dilution 1f1 

Date = 12/19I2005 

Time = 10 - 59 : 0Z 

—51 w?_O0mV 

Conponent Reten" 

(unknown) 0, 

C1- 1. 

(unknown) 2. 

512 .00OmV 

Area External 

609.10 NrA 

91.60 N 1'.5i 

361.34 N/A 

Cojmponent Number Retention Area External Units 

Ci-- 2 1.783 .91 . 50 M 1.59 ug/m]. 

1 91.60 1.59 

209 
Area Externa 

038.24 N/A 

169.95 2,9: 

515.20 NlA 

91.50 N/A 

Condit ion s: Daltile , Muskogee , OK Trim Ki ln 

: Run #2 Imps 3 & 4 

: Volume •300 D•ilution 1/1 

Date : 12/19/2005 

Time = 11:08-12 

—51 .200mV 

Component Retent' 

(unknown) 4.8 

C1- 1.6 

~

unknown ~ 2. 

unkno ~an 2.3 

512 _400mV 

ion ~ __.__.._...., j_ .......................... ..._..._._................. ~...~_.. __...,_. ._._ _.__..._._._..._._.M..._......._._ _ ......._....... ........__..___ ... .._....... 

54 ~~•-..__._. , :,•:~nt~. 1 

~ ~. 

83 . :....:. =:~~~• . 2 ....~ir 

16 

3 4 . 

.... : 

; . . . 

4 ..... ; ' . 

5 M..... . 

6 

Cornponent Number Retention Area 

C]. -- 2 1.683 169.95 

1 169 .95 

External Units 

2.95 ug/ml 

2.95 

210 
Conditions : Daltile, Muskogee, OK Trim Kiln 

: Run #2 Imps 3 & 4 

: Volume 300 Dilution 1/1 

Date : 12/19/2005 

Time-- 11:12:00 

Component Retention 

t 

512. OOOmV 

Area Externa 

(unknowp) 0. 

ci- 1.70 

(unknown) 2. 

635.60 N/A 

171.50 2.9E 

522.20 NIA 

0 

21 

. i 

~ . -. : 

~ 

5 --- 

.... . ........... ... 

Component Number Retention Area, External Units 

ci- 2 1.700 171.50 2.98 ug/ml 

171.50 2.98 

211 
Concfitions = Daltile, Muskogee, OK Trim tGiln 

"- Run #3 Imps 3 & 4 

= Volume 300 Qilution 1/1 

Date = 12/19/2005 

Time = 11=21=11 

--5 1 . 200mv 

Component Reter'' 

(unknown) b. 

(unknoain) 2. 

5 9. 2. OOOm'•J 

Area Externa 

555,95 H/A 

64.10 1.1 1 

607.00 N/A 

Component Number Retention Area External Units 

Cl- 2 1.700 b 4 .10 1.11 u g/ m], 

1 64.10 1.11 

2 ~. 2 
camponent Keter 

(unknaEFD) 0. 

F'l- I. 

Cl - 1. 

( un(tnown ) 2. 

Area Externa. 

449,86 N!A 

152,55 1.31 

69.20 M 1.2( 

621.30 N/A 

ConcLiti.ons = Daltile, Musl ~ ogee, OK Trim Kilrz 

~ Run #3 Imps .3 & 4 

= Volume 300 Dilution 1/1 

Date = 12/19/2005 

Time = 11=25=02 

—51 .2QOmU 512 .00OmV 

ComRonent hlumber Retenfi.ion 

1 1.133 

2 a. . 683 

Area External Units 

FlC1— 

152.55 1.32 ug/m 1 

69.20 M 1.20 ug/m 1 

2 221 .75 2.52 

213 
CQnditions = Daltile, Muskogee x OK Trim Kiln 

= NaoH Blank 

Date = 12/19/2005 

Time = 11 = 34 . 34 

---51 , 200mV 

Component Reten'' 

{unknown} 0. 

51.2 .00Omv 

Area Ezterna 

1189.15 N/A 

Component Number Retention Area External Units 

.0 0.00 . 0 .00 

214 
512.000m.V 

Conditions : Daltile, Musko:gee, OK Trim Kiln 

: 4.93 ug/ml Cl- in NaOH 

Date : 12/19/2005 

Time z 11:37:37 

-51..'200mv 

Component. Retention 

....... . ..... ...... 

(unknown) 0.8 50 

Y : cl- 1.8 50 

2 

Ai•ea ExteTne 

1204.20 N NIA 

304.90 H 5.2 

4 

5 ...... 

6~`. . . I 

-- -- ....... ...... --~ 

Component Number Retention Area External Units 

ci- 2 1.850 304.90 M 5.29 ug/ml 

1 304.90 5.29 

1 

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~ t ^~• 1 ~. a y . ~ ,~ '~ ~ _ - . tt; :'!? 

j 

_ __ ~ .L` - 1, ( - •1. J a 

- •S ~ . •'' r _ l 

...~ ; ! 4. ;✓ t . ~t ~~ 

• r+. 

. . `~ ; i - ~ - ' ~ r , ~~ '. ~♦ - , - ~ 

!,' ~ t`\ 1 lt ~r, r •~' + - 

Fluoride,Sta ~ndard ' 1 „ 

. > ,' --} : '• 

. ~ ' 

~ •j ~ . Comnonent Concentratlon 

~ . ~ .. ~ • - ~ ~?ng/I1) `. - 

. _ . 

Fluonde 992 t .4 

• . 

• 

' r . ~ <::. + ' 

~ ~ : • ~ ~ . . ~ . 

: • : 

• ' . ~ 

The concentration ~~ alue is._based , on proven-,reliab7e : ~ nietbods of analysis ` The ~ estimafed 

uncertainties are two standard deviations of tbe:concentration Nialues. The concentration ~~ alue is 

ti;tairanted to be stable for three,months from''the.date of shiprnent. 

The preparation and analyses of the Fluoride Standard was performed urit.h eatreme care by 

DIO'NTEX Corrporation Consurnables Manufact•uring Department. 

Dc-cu:nentNo. 034183-18 13-Dec-02 

Oionex Cor aration P Olonex U.S. Regional Otlices Oionex Intetnational Subsidiarics diane~; i ~~• .•- •!' I ~~ ' •. O ,t~:•.;i•::: 1228 Ti1gnVPay sunnyvale, Ck (408)737-8522 AusUla.(01) 6165125 Garnanj•(06126) 991•0 

.0. Box 3603 

~lnnyvalc. CA 

tYCStmonl, IL 

Narston, TX 

(630) 785-3660 

(?Bl ) 847•SG52 

beoum (03) 353 42 94 

Cartrda (905) 844-9650 atapsn (06) 6BB5•1213 

Naly(O6) 66 5150 52 

ot<rNa was 

~ ~ ~ ~•.~ .•..— „ 

4085-3503 J.11adt GA (770) 431-8700 C!>d:nt(852) 2d2E 3282 Kwm (2) 2653-2580 li'N 03131E-031DM 3104 

; r06) 737-0700 !.wic , t1J (E56) 595-0600 De~ (45) 36 35 90 90 Tne !0—1,'eHds (0161) 43 43 C3 -Z 2054 Dof>:x CarpDn+an 

Saq trir Ctiy, UT (801) 972-9292 Fiance (01) 39 30 01 10 Sf~;nd(OG2)2C5 E~ 66 
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, 

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h'Gtb+ ~~~μ.~4 ~, v ~•_ 

~ :~ ~ T'li~:~sui `1e=xon~stanc~ard ~was=' re" are~;'b`~~.the d>ssd~utLO~ of~:IiZ h- un' =;sa1 ~:=in:~ $:~~r~e~o~hm~'~ ~~~~{ ~ ,.. ' 

~ ~-::: :~ , _.g, ' ~ y -.K. :•~ p,~ :~?' . .u, :tY.._:~.. ~ . ~»~., ..--',,•.. ~. :P . ~r ~ a: -, ~ - ~ ..:~,~. . ~,~~ ~~

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_ l'_ ^ . 'r ~ .. 

•:z:: n: '^.. -?. ~ '. 

~ [r~ y' c ta `ts:~ i ,fi'e ;: o.tt~ le ~;1a ~ ~tstates -1he ~~ ~.:.~, . : r ~ , , deion~zed;: ~vater ;wwbuchti~va~ =tested b_ > I ~..;for iouic'; o,n minan ;T _ ~ ~ ~ . J ~ ~r c 

•.1. '. ~ N . ♦ I.~ . N. • -'Y 1yr, :•i . t :t•' ~{r• . :

.ti ~71'n y4'...; .'P . ~k.. . ti .\ ~t'~:1':.. W' +q , 4 ! , S a -;,'; \.. ! !'- ' t. S-' r' ^.'3~ ~a:~ . Li :1 ]

11 .~ t ..'i ~~t _ k„ . ~'~ 1• t •'i ••.:sn,. . t .-. . F i,. - ~ t'~ -. ~. ~ - t'..•. ~ , ..•-C. ,t •t.:~ . .1 : ,. .:y ~.~: ..\p-. ~~ i.,.l J r t.J.ti ~.~ ..-t. ~ ~Y::~1.~ •_l.c :!- ~ -::tir.,• ~ :+.i ♦ ' 1 r t ~ `ti 

- 

~ 7 

~ ,,~:~ ~~~ norniiaal concentrati.on' ` ~ v 1 ~a ue' ~ t~ of h " e°°ronic com onent p ~ _ ~ :for uiformataonai:'". u osES' onl" ..The , ~, _ ~ion t: ~ ~~_ 

, `t , P rP Y, , ~r 

i r `• - ~.~ ' 

:•4 ti+~ ^ a r ~~ ~ ~ t .~ t~ t'~ , + \ . ~ 

t~ _ :)...: . } ~ corlcentration value wa`s: deterrn[iried b" Ion<Chromato° a h .The; s.stem was s andar z >L :dl ed`11 siiit , : t r ~'; -., g?r1. P,,. Y .Y y,. g 

r ;~ _ ,• : ~ .. + :1. 

t ~ ; t~ie ~I tion Ins a al. t7tiite of= Stand'a_rds 8 ~>~Teehriolo ST Standard Reference ~ =lVlatenal ~SRlV1 ~ v._- ~ ~ 

. gY ~ )~ ~ _ .>- - ~ ~ . 1 l - _ ' _ t • .. 

. ~ - t:~-;~ : t - . - _ 'Z - 31$2 Chlonde, Staridard Sol ho ) u n.:Tlie:actual:concen , ~ ~ratlon::value-deterniined' ~o'r the'sm "le 2on g 

t~ r~.~ •~ +.- : ~ ,, r ~ i. _t.. t.. ,i .i...r2r i { ~ .`Y 1'~ :t .c. ~ ."; ) ~ r .5 t ~ -i 7 ~ rl '\ t- i. 5i v t 

~ is 1>lsted below. t ~ ~ \ _ , ti . , ;. ~ r > • : 

s ; ~ . , , , L t ; ; :E ~ ' 

_ ) . r t 

., 1 ~ ~ ,, • _.,~ . ' ~ ' • `, 

iw ' 1 L .{ ~•~ .•1rt .. . r .. , ' y ~ ' P. . ,j ~ t . - 

.t '~~ s~ 7~ Y \ T ~~~ ~ r 17'.. 

~ -_`. Yv i rt ~`~~ ~+ ~ ~ Y t ) ~ 1, . 

. _ ~ -T ~ 1 - .,, 

~ ~ •, .,_• 

-t,. :e t ` i y ~ t 1 

Chloride ~ Standard ' t , 

, ) -[ . , ~ 1 ,;i , ♦ 

, r , t , .,r t.X K t.rt ~ ' r • , . ~ V:• ++ . . " -Compunent Coricentration V - 

{i?°(g/L) 

Chlonde: - 986 ~ 4 : 

The concentration value is based :on piroven reliable. methods. ~ of analy.sis. ~ . The 'estimated - 

uncertainties are two standard deviations of the concentrat'ion ~alues:: ' The concentration value is ~ •. I.

warranted. •to be stable for -tlir'ee months from the date of shipment : ; 

The preparation and analyses of the Chloride Standard was performed with extreme -care by the ' 

DIONEX Corporation Consumables Manufacturing Department. ~~ ' - 

Documcnt No. 034184-25 20 May 1998 

nex Corporatton Oionex U.S. Repional offieet 

b -1 i:an tva,v S:mny+zic, CA (408) 737-8522 

9or, 3603 μh:slmont, i: (630) 769•3650 

'vale, CR Houston,lX (281)017-5652 

:-25G3 Ptlana • CtR (7701432'8100 

7 37-0100 Martton, NJ (B.i 59r0600 

Sa 31 Lake CAt', U7 (801)972-9292 

Ofonex tntemalionat Sabsidiaries 

Rusfiia (01) 616 5125 Gevgmy (03126) 991-0 

BelDn7m (03) 353 42 94 Nely(06) 66 515052 

Canada(905)844•9650 Japwr(06)6885-1213 

CAi73 f8:2) 2428 3282 Xaea(2) 2653-2580 

D--murk (45) 36 36 90 90 The lk!lff&nds (0161) 43 4303 

Fra.x't (01) 39 30 01 10 SWte&7d (O62) 2M 99 66 

sm 

`\.a10~t'~f 

;~ `~,! == ' ~ Di 

~ t~ J ~ ~C.7~ .:.~." ;`;::1, ~ 

~ 11 ON •TN! W!• 

lPN 031316-0310M 3M 

tD 7(vu. rlirrvm ('nrnnruirn 

FIELD DATA 

PLANT: 

DATE: /L 

REPETITION: ( 

LOCATION (SOURCE #): 

~~. ± ~j 

I1~I1'INGERS 

OPERA.TOR:s~ l ~ ~ Iiiitial rinal 

SAMPLE TR.AIN r: ! ( ~ ~ 41 ( Lij z ~ 

METBR BOX #:/v i ~ #2 16V io ~ 

BAROMETRIC PRESSURE: Z_'~I. ~ ~~ #3 1 Q`J L, 

AMBIENT TEMPERATURE: .3 U 

ASSUMED MOTS'TTi-RE: Za E 

#4~ 

~ #~~ 

PROBE LENGTH: ~ ~ 3 , NOZZLE DIAMETER; .QjI zj t 3~ / ~ cY~`S ~- #G ~ ~ ~ • ~ 

STACK DIAMETER: 

METER H: /, `~~ ~ CO2 02 

C FACTOR . ~`~ r 

METER CO-EFF ICIENT: l G~ S 

I 

~ ~ 

FILTER TARE: - 3 ~6~~3~ ~_ 3 

PRE-TEST LEAK CHECK, POST-TEST LEAK CHECK 

Meter: 6 `{cu.ft. 1~" in. HG ~ Meter: d,~ cu.ft. I a 

/ 

in. HG 

Pitots: . ~G na : ~ in. H20 Pitots: ~ ~• L in. H20 

'' • •t 

'. , ~ 

o~i"~' ., 

.. ~ 

' ' 

~,~'~ ~Z ~jo ' ~o ~ 

z 

47Z.zf3 Y ~- L/ 1 ~- 

6 7 Ll.o. f- 1-J I z61 14 

Z~ 

1.4 r 

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~ G ~ I ~ / ~ ~ 1 ~ V ► /. ~ ~ ~ . 

'7 1 s '6 -7 ~ 

Y . k); 

6?31 L y 3 q 

r c/~ g 

a~,4~ Z 

~ Y ~7, L/ y y 3 ~" ~~ ► 

~ 1 c-!3 

13 -7 _Z~& 

gy 617- .~- — tll / 1;, 6 q .s~ ~- 

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g ) ) %.3 ~ ~ ~ ' • , 9 ~. ~' ~`y ~.~ i~l ~-s" ''~- 

l V n 1~ Z Y. y =y 6 7,6' z -d ~ 
FIELD D.A T'A 

PLANT: D,-/~

!t ieuY~~ ~M 

~ DATE: /2/ 7 Q S 

REPETITION: ~ 

LOCATION (SOURCE n): SG 

OPERATOR: 

SAMPLE TR.AIN ~: / 2 

MBTER BOX ~: ,e v 

sAROIYIETRIC PRESSURE: 

AIvIBIENT TBMPERATURE.3 ~ 

ASSUlvtED MOISTURE: 

PROBE LENGTH: 

NOZZLE DIAMETER:a3)Z 3 

STACK DIAMETEO

R: 

METER H: ~ ~~` 

C RACTOR: e 7t' 

NiETER CO-EFF'ICIENT:/. 

FILTER TARE: . 36'1_$i ;1;1_3 7 PRE-TEST LEAK CHEC 

Meter: 6060cu.ft. a(~! in. HG 

~

/ ' Pitots: A H20 

IMPINGERS 

Initial 

41 !crD 

#2 I

~ ~ 

#3 l ~d 

#4 

#5 Z ~~/ 

#6 

r inal 

~ 

l

C 

 c~ f ~ v 

Z 

ZIOr2, 

26 7- Z 

CO2 02 

1,4 

~ 

POST-TES-1 LEAK CHECK 

Meter: 6~c1"~' cu.ft. @ ~~ in. HG 

Pitots: ~ (u~ ~ :,~in. H20 

 =3' ~ ~~. ~ ...- 

mommmm~~~~~ 

~~~~~~~ ~~[~ 
~ Rd? IN,GERS 

ial ial 

t I 

~I~ ~ 

~ 

r2 

u 

4 

 ~ 

O ~ S r5 

#6 Zl~'-~ •, ~ 

CO2 ~ 

~ 

POST-TEST T~EA.K CHECK 

Meter: °'' e 5cu.ft. @ ~ G in. HG 

P1tO1S: ✓ nQ, ~3, I lll. H20 

FIELD D ATA i 

PLANT: 05 a ) _J~ 

DATE: 

REPETITION: ~ 

i.00ATION {SOU~tCE 

OPERATOR: ~UI 

S Aiv4'LE TRAIN ra~ 

METER B OX r : 

BA.ROMETRxC PRESSY7RE: 

AMBIENT T.EIAQERATURG: NC 

ASSUlffiD MOISTU~tE: ~ 

PROBE LEN GTHP 

NOZZLE DIAMETER: 

STACK DIAMETER:3_'7,~ 

I1xETER H: 

C FACTOR: 

MLTER CO-EF'FICIENT. r 

FILTER TARE: 

PRE-TEST I.EA.~FC CHE 

Meter: !S U cu. ftit in. HG 

~n_. H20 

~ - 

~ 

- ime r }=in°Y"" 

 ovtfc fi~,~ea 

1 y~s' t y ?P4 e7~,& 3 I 

t, • , ~ - l Z. 3 a : 

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: 

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'~ Z . . ✓1 7'. r * ~ ! ~~ ~ ~ ~ ~ ~~ ,5,~ 

o .~ L 3. ~ , ,~S_ • 1, 1 ~~ . ::~ ~ `f ~ 3 ~- ~ ~~ r `! ~ 

9 6%., ~ 

~ 

( ', Llo ~' , 3 113 . ldf, ~ q(* 3 31 As 6 1 

~ q3 qo p lgq y~ ~ 

~• • ~~ f ~ ~ , ~ ~ 3 ~ ~/, ,~ `~_ ~- :~ ~ 

7 I f' ~ ~~ • t✓ ' 'f r ~ '"rr C ~ , ~ Z !`C y 

23 , C~ ~ ~~-- S~ 1 7 

x `~r. Y 1'r-I 

17L s-~ I I Ifcl( I ~Z. ~ t~f ~ ` s~~ 

jj ~ j 1 o ~ 

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11 1. cj:; ~ I 

! 

I ! • ~s,r~ 'I I I • . 

i297 
F'rELD DATA , 

PLANTZ% /1-4f tle 

DATE: ~ - 7 d 5 

REPETITI N: 

LOCATION (SOURCE Y): 

OPERATOR: 

SA]ViPLE TRAIN r: 

METER BOX T: / 

BAROMETRIC PRESSURE: 

AtvBIBNT TEMPfiR,ATURE: 3 <o 

ASSUIv1ED MOISTU'RE: 7-;Z,- 

PROBE LENGTH: 

NOZZLE DTAMETER: 

STACK DIAMETER:;y~~~~~ % 7 !1/r,~~~~ 

METER H: ~ ~{ ,~ 3 

C FACTOR Fif

METER CO-EFF CIENT: 

FILTER TARE: 

PRE-TEST I.EAK CHEC{ 

FMPINGEF.S 

Initial r:nal 

, 

7 ~~~ - ~ r3 /G1) I U S 

r.

~

4 tllffl 

45 I '~ Sc2- 

Za Irv, . y 

~~'6 

Uo . L( 

CO2 02 

POST-TEST LE.4K CHECK 
IIti'fPmTGERS 

r,,I 

Initia] 

~ ~~ .~ p~ 

42 

F;nal 

~ !~, JG ~3-0v 

.U.f 

f -7 1 ~ 

r-r3 

r~ 5 ) 'T'D ; ~ ~ • ~j cq . 'O 

46 

CO2 2 

POST-TEST LEAK CHECK 

Meter: CJ-s cu.ft. &97in. HG 

Pitntc• ~' n V~ in_ H20 Y.. 

~ ~rELD DATA 

PLAI~'T: ~•~7 r ~ 

DATE: 

2EPETITIO23: 

LOCATION (SOE'RCE :E): 

OP.ERATOR: 

SAM'LB TRA.INr: 

AETER BOK r: I I 

BAROMETRIC PRESSURE: ~G•~j' 

AMBIENT T'EMPi✓RATCItZE: 

ASSV-IvIED MOIST ~ tE: 

PROBE LENGTH. ~ NOZZLE DIAMETER: % 3! ~ 

STA.CK DIAII2ETER: S ~ 5~ ~ 

1l2ETER H: -7 3 

C FACTO R: "~ ~f • 

METER CO-EFFICLENT: 6,9 f~ 

FILTER TARE: 

PRE-TEST LEAK CHECK 

Meter. D-Da h cu.ft @f in. HG 

,D;+„*... v n - Y-. _ ;,, u-)r.n 

!n ` 

c6 q6 3 

L(`-1 Y© q- ~ ~/ © 3 

3 =19 f.3 /-3 lIbI L -L( a ~ 

~ : 31 l3 ..~ I - ( a (3. ~ S ~~0 ~ ~ ~{ ~ ~ 

~ 3`( . • ~ zs • Ca ~ • ~~5.' • ":~~ `~5~ E ~ ~ 

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d j? 4( r 4. ~ 

! 3 tYc~ L0 3 J~ 5..5'` 

K6 

3536 

~ I ; ( ( IF. , I ~ 4 3 ~-,)G4 ~( o 1 ~54 qo I' 

© 25 ~0 I 

, a(6 3 s ~~ 

3.. 

~ • ~ ias I ~ 3 .•~ . ~d ~a ~,. ~~ .~ a.~ 3 

 . ~ , b ~ ~' ~ 

 ~j ~ 2S 

l t 

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I 3 J/D Y-0 12--5—Y 1 uq 1 ~ 

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ra• ~ i :; ~_ ~~ ~ ~ ~ I ~. 3 b'~ 3 ~` ~ ~' 

 • • 

. ~ I 

1 1 

1 . T71 ~~'i'', . ~ I2 ~ (~ 

r ~ 
I-IN'IPINGERS 

Iiutial : inai 

T~ 1 l "V ~ 

,~ , ' ~1 j •: ~': '71"~~ . F~ 

//~~ 

•.. , ,~ 

42 ' 1 V 

~•, ~'''~ /~~ `~,~ ' r ~ J U 

rr4 

-U - r. ~1 C.t ~1 ~ 

#6 

g 

CO2 02 

3 ~ 3 .• C 

POST TEST LEA.K CHECK 

Meter:CS -64 Qcu.ft @ 5 in. HG 

p;t~,~ • v~- n _ ~~„ u)n 

,FIELD D A T A 

~ PLANT: 7 4-, ~C 

DATE: t /c) S 

/ REPETITION: `3 

LOCATIOlNT (SO URCE 1): -SC'f'rf,~~~'~ ~ 

OPER_ATOR:•~) 

~ SANPLE TRA.IN r: S" 

METER B0X #: I r~ 

BAROMETRIC.:PRESSURE: 

AMBTENi TEMPERAT'JRE: 

ASSUM' cD MOISTURE: 

PROBE LENGTH: U ' 

NOZZLE DIAMETE{R: : . i ' ~~-~ r ►r • ~ 'r 

STACK DIA.METER: ~ ~~ ~ ~ ra ~ •. r. ~ 

METER H: tr• ~,-'~~ a► 

C FACTOR; 

METE R CO-EFFICIENT: 6 :q 5'? 

FILTER TARE: ....:- 

PRE-TEST LEAK CHECK 

Meter::V-AB 4n cu.ft e`~~ in. HG 

Pitots: ~: ~ ~''~in_ H2n 

=1 0 

 •Ime , "rt~` 

r.ess;~ _ 

" I 1 1 ~ 

 "` 

Ct~. ~ 

~,pt'7+ 

et ,o t!c 

~ A 

, em ~cnt' u►, 

I' 6Ko /35 ,lS 

~ ~f0 c3F ` 

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~ ~r~ z ~3 ~~ r ~.~ 6 3. ~~2s y z 

, 

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~ l'q;3Z 38 6 t. ~~ 2~~ ~f Lq 

~ 3 

Z, 1 u: q2 

.3 

qlF V -9 R .r . . 7 . 6 l(d 1 36 ~5 ~ 
FLOW DATA 

~~~~~~ 

~~~~~ 

~~~~~~ 

~~~~~~ 

~~~~~s~ 

~~~~~~ 

o~~~~~ 

~~~~~~ 

~s~~~~l 

o~~~~~ 

o~~~~~ 

~~~~~~ 

a~~~~~ 

s~~~~ea~ 

os_~s~~ 

o~~~e~~ 

~~~~~~ 

~~~~~~ 

~~~~~~ 

e~~~~~ 

~~~~~~ 

o, 

• 

PLANT: 

DATE: 

RUNT #: ?- AIf , 

LOCATION (SOURCE u): rt -, 

OPERATOR: Y, -9 ~~ 

AMBIENT TEMPERATURE: 

]BAROMETRIC PRESSURE: CO2 

ASSUMED MOISTURE: 

STACK DIAMETER: 

C FACTOR: 

COMMENTS: 

02 

231 
31 o 

. ~

LD DATA I. 

PLAIvT:~u 

I~ ATE~ 1 z ~ o S ~ ,~,~ , V o ~,~ 

REPETITION: t f~-~~ ~ ~ C~~' ' r ,z 

LOCATION (SOURCE '):'Fr,~; LA. A. IMPIlNGERS 

OPER..ATOR: K~ Iiutial ~Yinai 

SAZviPLE TR AIN r: n 1/!~ I 3 ~ 

METER B0X n: ~ y , ~2 

BAR.OMETRIC PRESSURE:30. O 1-0 0 

AMBIE2rTT TEMPER.ATtJRE: ~o ~ ~ ~~•-~ ' ~ 

ASSU-1viED MOISTURE:~ ~ / ~ ~ 1 S" ~ r

5 

PROBE LENG'TH: ✓ .S~ .• r6 

NOZZLE DIAMETER: ,ZSv . Z5~/ ;: ~~"~ ~~' ~ ~ 6 3• / 

STACK DIAMETER• Z% 

METERH: Ir y~' ~ Y . CO2 42 

C FACTOR: 

MET'ER CO-EFFICIENT: 

. ~, ' • z - S , . ~.~ 1^ 

FILTER TARE: 

PRE=T'EST LEAK CHEC,'K POST-TEST LEA CHECK - 

Meter; b~~ cu.ft. @ ~ in. HG ., ~:: Meter. ~, avocu.ft.. !`~ in. HG 

Pltots. ~ Z d n ~Y in.• H2O. , } .., ',,'~~;, Pitots: in. H20 

dsa a 

es , Bad 

`;A~- ~~~• 'Q. • •~4 •a .I:~ 

'Q .... "l: 

:

~ •,/~~'~✓.ti/ ` - (/ _ ~~• 

10"n 

~ 

••,'.~ 

, Yz>. 4X_ -_,, ~~ ~~•.•~• ~:~ J`~ •-" •/ ~~ ' 

1 

40, 

' :! F' ^~

.. . f• 1 1 /`.. * . , ~ . '.)~..' • ~~ •._ 

 • i • • ll ~ ~ ~' ; (.-yl. 

 `• •, lt ~ 

•. ~~ 

., . l'. . , . . . . '. ft`1 - , t 

 , t . ..y0r -r~ l -J.:.. '• =U~ ,. ~ • ~~'- ~~ 

1! Vff~. 

/ ` •, ~ 4. 

, -. . ' ' .. . • ~. .~: , `. F' . 

34 

Z ~ `!•t~k'j .. . ~ fJ~ ~,+~ • ij f ~. y' ~' t v' _ ~~ ~ ~ 

<g zi, ~ ~} 3 ~ y ~r 

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•~ ~ ~ ~ ~ ~ ~ ~ 

I LI.~. I I I ! I I I ~ 2ii 
Tit'IPIlNGERS 

. Initial 

-?UrI /UV 

#2 IdD 

#3 / db 

9'T --' 

#s 

#6 

rinal 

~ 3 

2.. 

FFELD .DATA 

- 

PLANT: 

DATE: 

REPETITION: 21 

LOCATION (SOURCE Y): 

OPERATOR: ~7'"- 

SAIvLPLE TRATN 

NIETER BOX #: f o 

BAROMETRIC PRESSURE: 36. o 

AMBIENT TEMPERATURE:36 

ASSUMBD MOISTLRE T 

PROBE LENGTH: 35- 

NOZZLE DIA.METER: -. 

STACK DIAMETER: ZA/, ~ 

1YIETER H: 

C FACTOR: 

METER CO-EFFTCIENT: 

FILTER TARE: , 3 ?Z 5 - 

PRE-TEST LEAK CHE

Meter:v_oaacu.ft. @ n. HG Zi. 

Aitnte• i i. n ~ NIM 

CO2 ' 02 : 

POST-TEST LEAK CHECK 

Meter.o-cc~~cu.ft. @ I~ in. HG 

Pitnt,.- . yr , (a~, d4' m_ H20 

~~ - ~~~:~, . M ~~~~. 

~~~~~~~~~~~ • 

~~ 
FI.ELD BATA 

PLANT: 

DATE: 

REPETITION: .:1 • 

LOCATION (SOURCE 

OPERATOR: 

SAIviPLE TR.AIN #. 

METER BOX #: J o 

BAROMETRIC PRESSURE:jCw-0 4~ 

AMBIENT TEMPERATURE: 3 

ASSU'NMD MOISTURE: ~ 

PROBE LENGTH: > ~_ - 

NO22ZLE DIAMETER: 

STACK DIANIXTER: ?.- 1 . 5" 

METER H: ~. ~ 60 

C FACTOR: _ s e-f 

METER CO-EI'FICIENT: °° r 

FII.TER TARE:. S"7 y 

PRE-TEST LEAK CHECK 

Meter: Q • Ua'cu.ft. @ ~ 'in.' HG 

n T-T7(1 

IMPIINGERS 

Initial Fiiial 

~ 

#2 GP p o 

n3 

• #a 

~j 7 vu~ S~r 

. ~6 7~' 7 n 

CO2• 02 

, POST-TEST LEAK CHECK 

~ 

Meter: O- cIcO cu.ft. @ G d in. HG 

Di+.,+r• rnl V7r1 

M~'~~,. ~ ..'. ~~;~F~i~~:~~.. 

mmmmm 

mwt~=mm~~"~mlwm 
FIELD DATA 

PLANT- ~/.~.~f ~`~ 

DATE.: ' 

R,Epr--TITION: 

LOC"'ATION, (S0LJRCE_-."):rtr/,,q *;b,7 

opERAToR: 

NISTER BOX 

BAROMETRIC PRESSURE:- 3 0, 

Alvf BMNT T ENPERATU`] 

AS STJ-NffiD MOISTURE: 

PROBE LENGTH: 50 `r 

NOZZLE DIAMETER: 

STACK DIAMETER: )-14, . 5 X;T, 3 , 

METER H: 1, 

C FACTOR:r 

METER CO-EFFICIENT: 

FILTER TARE: 

PRE-TEST LEAK CHECK 

B,fPINTGERS 

Initial Final 

:R1 

1? ~~~' *10 2, 

fr4 t*, .:-7 I 

77 

-.5 

#6 

CO2 0.2 

2 

POST-TEST LEAK CHECK 
' 

PLA.NT: Q ~~~ ~~ 

FIELf) jDATA. 

DATE:,~- t~ ~°Aa 

5 

REPETITI I~~: 

LOCATIO~T (SOLRCE 4): ~~'~rap ~ ~ DZPP~ GERS 

OPERATOR: f3 Iititial rii3al 

SAN''LE TRAII~t r: ~ 

METER BOX ~: 

r 1 l p B~~S` 

~~ 

BAROMETRIC PRESSURE. t3 -jd. C) 

r2 ! ~ D 

r3 ° ~`..

r=~ ~ r~ ~~~,~ ~ 6 

r ~ l O ~ • 

ANiBIENT TEMPERATURE: 3 ~ 

,~~ .. . _ ~ a 6 

ASSV~~ D MorSTURE:• 

PROBE LENGTH: ,5ir ' 

rs 

rG ~ 

NOZZLE DIAMETER: 

STACK DIA.METER: Z'Sl.s ; 

METER H: ~ .L~l~. 3 CO2 02 

 METER CO-EEF'CIENT: t'~ .c? ~ 

C FACTOR. ~~ 

FILTER TARE: 

PRE-TEST LEA.K:' CHECK POST-TEST LEAK CHECK 

Meter:p_p d® cu.ft. @ t•Sin. HG Meter: O,Qpb cu.ft. @ in. HG 

Pitots:. ✓ in:'H2O. Pitots: "n. H20 

 0_401 

 ~ o ~ F Y c ~ a ,uflc eni 

~ 

in uw 

~ ... } ::a 4 43.. 

~ . • ~~/ • ~ L r> ~ 

d: 

~~ 

' »-:: 

~S ~ 

. ~ 

. 

.~: ~ 3 `os • `-~~~ •~c~ ~ r ~ ~ s ~6° ; ~6 ~ ~ ~ ~ 

`~ ,

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:/3 ; ~ .5 

1 

: 4.3 .~~ ~ 

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51 i a 

~ 13;3V 1 qrf t~ 1. / VJ6.. I ks" .2s s~ 6 

: 3 

~ 13 :4fi5/ l- F7 

l'k .2_ , 4 q zs~" 

I ~t~~~ r I • 

F,7 1 .12 rl 6 
FIE•LD DATA 

P L.A N T: 

DAT ✓- /I 

P,EPETITION: ~-' r 

LOCATION (SOL7RCE *1 

OPERATOR: 

SANPLE TRAIN 0: 

NSMR BOX #: 

B-A.ROMETRIC PRESSURE: 

,A2vfBIE\,7T TEMPERATURE: 

ASSLTMED MOISTURE: 

PROBE LENGTH. 

NOZZLE DL4,MEtER: 

STACKDIAM)ETER: A~ 

METER H: ~9 

C FACTOR. 

METER CO-EM.,CIENT: 

FILTER TARE: 

PRE-TEST LEAK CHECK 

Meter: - cu 6 A @V'~ in. HG 

0. Ylf-in, H20• 

IMPINGERS 

Iiiitial —tinal 

42 

:93 

74 r 1r). b6 

r. 6 205, 2, 

bi, 2, 

CO2 02 

Iz 5 1 5L 

POST-TEST- LEAK CHic 

Meter 0-.V 01!6ft @c 4. in. HG 

Pitots: t.~r' (cb, _' ~in. H20 

~ IF ~ 

L7 L 

~~~ ' ®~IF~I~'S~~!~ v . ~:~~~ ' ~ ~~ '~ 

'~— . .~e • ~ ~ ~ ~® . ~ _ / ~~~ 

r omm P. 4 am-Am 

® wjolf ~®~ ° ~ ~~~ ~ 

:.~ . .i%,~' ® ~ p ~~~~i ~~~~~ 

~ , ® ~ . 1/i'~~~. w / p ~~~~~ 

~ ~~~ _ ~ ~~~_ 

so MR 

~ ~ i ~~~ ' ~'' ®~ 

®(l~~1~~®' d~%'~• ~~ , 

, • ~ ~~~~~ 

~_ ~ ~_~ _~® ~ _- ~ 

~~~_~~ _ - 

__ 

-~~~ 

~ _ .... I I I I I I I I I 12? 7 
_ e 

,. , 

~~s~~~ 

,, 

o~~~~~ 

s~~~a~~~ 

0~~~~~ 

~~~~~~ 

o~~~~r~ 

~~~~~~ 

o~~~~~ 

o~~~~~ 

~~~~~~ 

~~~~~0 

o~~~~

~~~~~~ 

WH*= 

~~~~~~ 

~~~~~~ 

~~~~~~ 

~~~~~~ 

~~~~~~ 

~~~~~~ 

~~~~~~ 

~~~~~~ 

~~~~~~ 

~~~~~~. 

~~~~~ 

Zs.`( 

l , f~ 

1 l 

FLOW DATA 

PLANT: 

DATE: j, 

RUN 

.

4-. ~ L~GY' ~ L Clir~C~I~ 

, ~~ 

LOCATION (SOURCE 

OPERATOR: GL1 

AMBIENT TEMPERATURJE.- I-Tec> 

BAROMETRIC PRESSURE. 

ASSUMED MOISTURE: 7 

STACK DIAMETER: ?,V. S ~~/~ ~=~ j~ l~ 

C FACTOR: - 8 

COMMENTS: 

CO2 02 

Armstrong Environmental Inc. CONVERSION FACTORS 

EPA Method 5 

522 Series Meter Box Callbration 1 mm Hg : 0.13330 kPa 

Pre-Test Orifice Method 1 cm = 0.39370 inch 

English Meter Box Units, English IC Factor 1 mm = 0.03937 inch 

1 cu ft = 28.32 liters 

!r Box x 11 Date: ------------------> 10l11/05 

rl #: 73 Barometric Pressure: -------»-> 29.75 (in. Hg) 

Theoretical Critical Vacuum: --> 14.03 (in. Hg) 

11 

)RTAt% For valid tesl resulls, the Aclual Vacuurn should be 1 to 2 in. Hg greater than ttre Theoretical Critical Vacuum shown above. 

)RTAA The,Critical Oririce Coefficienl, IC, must be entered in English units, (fl)"3'(deg R)"0.5/((in.Hg)"(min)). 

11 

DRY GAS METER READINGS - ------- -CRITICAL ORIFICE READINGS- 

- Average Temperatures - 

Volume Volume Volume Initial Temps. Final Temps. Oririce IC Oririce Acival - Ambient Temperature - DGM DGM Ambient 

IH Time Initiai Final Total Inlel Outlat lnlet Outlet Serlal# Coefficient Vacuum Initial Final Average Outlet Overall Temp 

20) (min) (cu ti) (cu fl) (cu (l) (deg F) (deg F) (deg F) (deg F) (numbar) (see above) (in Hg) (deg F) (deg F) (deg F) (deg R) (deg R) (deg R) 

0.26 6.00 482.900 484.824 1.924 75.0 74.0 75.0 74.0 40 0.242 23.5 74.0 73.0 73.5 534.0 534.5 533.5 

0.53 5.00 486.500 488.797 2.297 75.0 74.0 75.0 75.0 48 0.344 22.0 74.0 74.0 74.0 534.5 534.8 534.0 

0.96 6.50 490.297 494.308 4.011 75.0• 75.0 76.0 75.0 55 0.464 20.0 74.0 74.0 74.0 535.0 535.3 534.0 

1.55 6.50 494.700 499.812 5.112 76.0 75.0 77.0 75.0 63 0.593 18.0 74.0 74.0 74.0 535.0 535.8 534.0 

3.00 10.00 500.400 511.137 10.737 77.0 75.0 79.0 75.0 73 0.824 14.5 75.0 75.0 75.0 535.0 536.5 535.0 

............................................. RESUi.TS ................... . ...... ..,..................... . 

W GAS METER --- -------- ORIFICE ---- - DRY GAS METER - ORIFICE 

JME VOLUME 

RECT CORRECTED 

n(sld) Vm(sld) 

(cu fl) (litors) 

1.890 0.1 

2.257 0.1 

3.942 0.2 

5.027 0.2 

0.581 0.4 

VOLUME VOLUME VOLUME 

CORRECT CORRECT NOMINAL 

Vcr(std) Vcr(sld) Vcr 

(cu fl) (liters) (cu fl) 

1.873 0.1 1.904 

2.216 0.1 2.255 

3.882 02 3.950 

4.966 0.2 5.053 

10.596 0.4 10.802 

CALIBRATION FACTOR 

Y 

Value Variation 

(number) (number) 

0.991 0.001 

0.982 -0.007 

0.985 -0.005 

0.988 -0.001 

1.001 0.012 

CALIBRATION FACTOR 

dH@ 

Value Variation 

(in H20) (in H20) 

1.448 -0.0251 

1.490 0.017 

1.486 0.013 

1.466 -0.007 

1.475 0.002 

Average Y -------> 0.989 1.473 <------- Average dH@ 

For Calibration Faclor Y, the ratio of the reading of the calibration meter to the dry gas meter, 

cceptable tolerance oi individual values from lhe average is +-0.02. 

or Orifice Calibration Factor dH@, ilra orifice differential pressure in inches of H20 ithat equates to 0.75 cfm of air 

168 F and 29.92 inch ~f~g, acce able tolerance of individual us from the average is +-0.2. 

SIGNED: Date: f~ / ~ •~f 

~ 

.~ 

.~ 
Temperature Nieter Caiibrations 

fJeter Box #: 11 

Date: 10/11105 

Calibrated By: RT. 

Emtech Thermo 

Degrees F Checker Probe Stack Oven Exit Auxiilary 

Point 1 32 30 30 30 31 30 

Point 2 212 211 212 211 212 211 

Point 3 752 751 751 751 751 751 

Emtech Thermo 

Degrees R Checker Probe Stack Oven Exit Auxiliary 

Point 1 492 490 490 490 491 490 

Point 2 672 671 672 671 672 671 

Point 3 1212 1211 1211 1211 1211 1211 

Percent Difference 

Probe Stack Oven Exit Auxiliary 

Point 1 0.406504 0.406504 0.406504 0.203252 0.406504 

Point 2 0.14881 0 0.14881 0 0.14881 

Point 3 0.082508 0.082508 0.082508 0.082508 0.082508 

i t 
Armstrong Environmenta! Inc. CONVERSION FACTORS 

EPA Meihod 5 

522 Series Meter Box Calibration 1 mm Hg : 0.13330 kPa 

Pro-Test Oririce Method 1 cm 0.39370 inch 

English Meter Box Units, English IC Faclor 1 mm = 0.03937 inch 

1 cu fi = 28.32 liters 

Box >; 11 1}ale: --------- -----> 12119/05 

#: 40312 Baromelric Pressure: ------ ----> 30.25 (in. Hg) 

Theoretical Critical Vacuum:---> 14.27 (in. Hg) 

I 

RTAI` For valid tesl resuits, lhe Actual Vacuum should be 1 to 2 in. Hg greater than the Theoretical Critical Vacuum shown above. 

RTA!\The Critical Oririce Coefficient, IC, musl be entered in English units, (ft)^3 0 (deg R)"0.5/((in.Hg)•(min)). 

I 

---- DRY GAS METER READINGS - -CRITICAL ORIFICE READINGS- 

- Average Temperatures -- 

Volume Volume Volume Initial Temps. Final Temps. Otiflce IC Orifice Actual - Ambient Temperalure - DGM DGM Ambient 

1 Time Initial Final Total Iniet Oullet Iniet Oullet Serialfl Coefficient Vacuum Initial Final Average Outlet Overall Temp 

O) (min) (cu ft) (cu fi) (cu ti) (deg F) (deg F) (deg F) (deg F) (number) (see above) (in Hg) (deg F) (deg F) (deg F) (deg R) (deg R) (deg R) 

0.25 11.50 438.400 442.075 3.675 56.0 56.0 57.0 57.0 40 0.242 24.0 56.0 56.0 56.0 516.5 516.5 516.0 

0.51 10.50 442.300 446.997 4.697 57.0 57.0 58.0 57.0 48 0.344 22.0 57.0 57.0 57.0 517.0 517.3 517.0 

0.94 7..00 447.500 451.878 4.378 75.0 75.0 76.0 75.0 55 0.464 20.5 57.0 57.0 57.0 535.0 535.3 517.0 

1.60 6.50 452.400 457.635 5.235 76.0 75.0 77.0 75.0 63 0.593 19.0 57.0 57.0 57.0 535.0 535.8 517.0 

3.00 9.00 458.800 468.862 10.062 77.0 75.0 79.0 75.0 73 0.824 16.0 57.0 57.0 57.0 535.0 536.5 517.0 

............................................ RESULTS .... .................. ...... ..,................,,,. 

Y GAS METER --- 

ME VOLUME 

tECT CORRECTED 

(sid) Vm(std) 

;u fl) (liters) 

.799 0.1 

.852 0.2 

.375 0.2 

.234 0.2 

.081 0.4 

ORIFICE 

VOLUME VOLUME VOLUME 

CORRECT CORRECT NOMlNAL 

Vcr(std) Vcr(sld) Vcr 

(cu n) (liters) (cu ft) 

3.711 0.1 3.588 

4.810 0.2 4.660 

4.320 0.2 4.186 

5.131 0.2 4.972 

9.864 0.4 9.557 

- DRY GAS METER -- 

CALIBRATION FACTOR 

Y 

Value Variation 

(number) (number) 

0.977 -0.006 

0.991 0.008 

0.988 0.005 

0.980 -0.003 

0.978 -0.004 

ORiFICE --------- 

CALIBRATION FACTOR 

dH@ 

Value Varialion 

(in H20) (in H20) 

1.398 -0.0111 

1.412 0.005 

1.385 -0.022 

1.441 0.034 

1.402 -0.005 

Average Y -------> 0.983 1.407 <------- Ave rag e d H@ 

For Calibration Faclor Y, the ratio of the reading of lhe caiibration meter to the dry gas meter, 

x;eptable tolerance of individual values from the average is +-0.02. 

+r Orifice Calibration Factor dH@, lhe orifice differenliai pr sure in inches of H20 lhat equates lo 0.75 cfm of air 

68 F and 29.92 inche Hg, a ept tolerance o' vidual values from the average is +-0.2. 

SIGNED: ' ~ , Dale: 

✓ 

TND 

t"'a 
Temperature Meter Calibrations 

Meter Box #: 11 

Date: 12/19/05 

Calibrated By: RT 

Emtech 42312 

Degrees F Calibrator Probe Stack Oven Exit Auxillary 

Point 1 32 32 32 32 32 32 

Point 2 100 100 100 100 100 100 

Point 3 250 251 251 251 252 251 

Emtech 42312 

Degrees R Calibrator Probe Stack Oven Exit Auxillary 

Point 1 492 492 492 492 492 492 

Point 2 560 560 560 560 560 560 

Point 3 710 711 711 711 712 711 

Percent Difference 

Probe Stack Oven Exit Auxillary 

Point 1 0 0 0 0 0 

Point 2 0 0 0 0 0 

Point 3 0.140647 0.140647 0.140647 0.280899 0.140647 

242 
APE. Armstrong Environmental (nc. CONVERSION FACTORS 

EPA Method 5 

522 Series Meter Box Calibration 1 mm Hg * 0.13330 kPa 

Pre-Test Orif'rce Method 1 cm = 0.39370 inch 

Engtish Meter Box Uni1s, English IC Factor 1 mm = 0.03937 inch 

1 cu f1= 28.32 liters 

)r Box x 10 Date: ------------»»_---> 10/10/05 

al #: 30272 Barometric Pressure: ---------> 29.75 (in. Hg) 

Theoretical Critical Vacuum: --- > 14.03 (in. Hg) 

!11 

)RTAf\ For valid lest results, lhe Actuai Vacuum stiould be 1 to 2 in. Hg greater than the Theoretical Critical Vacuum shown above. 

)RTAf%The 

II 

Critical Orifice Coefficient, K', must be entered in English units, (it)"3'(deg R)"0.5/((in.Hg)'(min)). 

------------ DRY GAS METER READINGS ---------- -CRITICAL ORIFICE READINGSt -- Average Temperatures - 

Volume Volume Volume Initial Temps. Final Temps. Orifice IC Orifice Actual -- Ambfent Temperature - DGM DGM Ambient 

IH Time Initial Final Total Inlet Ouilet Inlet Outlet Serial# Coefficient Vacuum Initial Final Average Outiet Overali Temp 

20) (mih) (cu ft) (cu ft) (cu ft) (deg F) (deg F) (deg F) (deg F) (number) (see above) ttn Hg) (deg F) (deg F) (deg F) (dag R) (deg R) (deg R) 

0.24 6.00 508.200 510.089 1.889 76.0 76.0 77.0 76.0 40 0.242 24.0 75.0 76.0 75.5 536.0 536.3 535.5 

0.50 6.00 510.400 513.118 2.718 77.0 76.0 77.0 76.0 48 0.344 22.0 76.0 76.0 76.0 536.0 536.5 536.0 

0.91 6.00 513.400 517.046 3.646 77.0 76.0 77.0 76.0 55 0.464 20.5 76.0 76.0 76.0 536.0 538.5 536.0 

1.50 5.00 517.400 521.271 3.871 77.0 76.0 78.0 77.0 63 0.593 18.0 77.0 75.0 76.0 536.5 537.0 536.0 

2.85 6.00 521.800 528.204 6.404 78.0 77.0 80.0 77.0 73 0.824 16.0 76.0 75.0 75.5 537.0 538.0 535.5 

.N........N....I..N....NN ............... RESULTS ........N.... 

 ..... 

...............N...N.......... 

2Y GAS METER --- --------- ORIFICE ----- -- DRY GAS METER -- ------- ORIFICE ---- 

1ME VOLUME VOLUME VOLUME VOLUME CALIBRATION FACTOR CALIBRATION FACTOR 

3ECT CORRECTED CORRECT CORRECT NOMINAL Y dHO 

i(sid) Vm(std) Vcr(std) Vcr(sld) Vcr Value Variation Value Variation 

cu ft) (iiters) (cu fi) (liters) (cu fl) (number) (number) (in H20) (in H20) 

1.850 0.1 1.869 0.1 1.907 1.010 0.006 1.363 -0.0369 

2.662 0.1 2.655 0.1 2.711 0.997 -0.007 1.407 0.008 

3.574 0.1 3.577 0.1 3.653 1.001 -0.004 1.411 ' 0.011 

3.797 0.1 3.813 0.2 3.894 1.004 ' -0.000 1.420 0.020 

i.291 0.2 6.354 0.3 6.484 1.010 0.006 1.397 -0.002 

Average Y ------- > 1.005 1.400 <------- Average dH@ 

For Calibration Factor Y. the ratio of ttie reading of the calibration meter lo the dry gas meter, 

xeplable tolerance of individual values from the average is +-0.02. 

x Orifice Calibration Factor dH@, the oririce differential pressure in inches of H20 that equates to 0.75 cfm of air 

68 F and 29.92 ' ches-of-klg, acce tabl ol rance of individu

71~1/

esfrom the average is +-0.2. 

SIGNED: ../~~_ ~'" Date: ' r ~ 

; V 

'Ph 

w 
Temperature Meter Calibrations 

Meter Box #: 10 

Date: 10/10/05 

Calibrated By: RT 

Emtech Thermo 

Degrees F Checker Probe Stack Oven Exit Auxiliary 

Point 1 32 31 31 31 31 31 

Point 2 212 210 211 210 210 211 

Point 3 752 750 750 750 750 751 

Emtech Thermo 

Degrees R Checker Probe Stack Oven Exit Auxillary 

Point 1 492 491 491 491 491 491 

Point 2 672 670 671 670 670 671 

Point 3 1212 1210 1210 1210 1210 1211 

Percent Difference 

Probe Stack Oven Exit Auxillary 

Point 1 0.203252 0.203252 0.203252 0.203252 0.203252 

Point 2 0.297619 0.14881 0.297619 0.297619 0.14881 

Point 3 0.165017 0.165017 0.165017 0.165017 0.082508 

244 
APE Armslrong Environmental Inc. CONVERSION FACTORS 

EPA Method 5 

522 Series Meter Box Calibration 1 mm Hg = 0.13330 kPa 

Pre-Test Oririce Melhod 1 cm = 0.39370 Inch 

English Meter Box Units, English I<' Factor 1 mm = 0.03937 inch 

1 cu tl = 28.32 (iters 

Box t 10 Dale: ------------ 12/19105 

#: 30272 Barometric Pressure: ----------> 30.25 (in. Hg) 

Theoretical Critical Vacuum: --- > 14.27 (in. Hg) 

RTAf` For valid tesl results, the Actual Vacuum should be 1 to 2 in. Hg greater than the Theoretical Critica) Vacuum shown above. 

:RTAN The Critical Oririce Coefficient, W. musl be entered in English units, (f!)^3"(deg R)^0.5/((in.Hg)"(min)). 

---------------- DRY GAS METER READINGS --------------- -CRITICAL ORIFICE READINGS- 

- Average Temperatures - 

Volume Volume Volume Initial Temps. Final Temps. Orifice IC Oririce Actual -- Ambient Temperature -- DGM DGM Ambient 

1 Time Initial Final Total Inlet Oullet Inlet Outlel Seriallt Coofficient Vacuum Initial Final Average Outlet Overall Temp 

O) (min) (cu ft) (cu ft) (cu ft) (deg F) (deg F) (deg F) (deg F) (number) (see above) (in Hg) (deg F) (deg F) (deg F) (deg R) (deg R) (deg R) 

0.25 21.00 229.800 236.307 6.507 54.0 54.0 57.0 57.0 40 0.242 23.0 54.0 57.0 55.5 515.5 515.5 515.5 

0.51 13.50 236.600 242.583 5.983 57.0 57.0 59.0 58.0 48 0.344 21.0 57.0 58.0 57.5 517.5 517.8 517.5 

0.92 11.00 256.200 262.767 6.567 61.0 59.0 61.0 59.0 55 0.464 19:5 58.0 59.0 58.5 519.0 520.0 518.5 

1.50 8.50 249.100 255.604 6.504 60.0 62.0 58.0 59.0 63 0.593 18.0 58.0 59.0 58.5 520.5 519.8 518.5 

2.90 6.00 266.000 272.323 6.323 61.0 59.0 64.0 59.0 73 0.824 16.0 59.0 60.0 59.5 519.0. 520.8 519.5 

. ........................................... RESULTS .....................................,............. 

Y GAS METER --- ------- ORIFICE -------- - DRY GAS M>=TER - ORIFICE 

VIE VOLUME 

:ECT CORRECTED 

(std) Vm(sld) 

:u ft) (liters) 

.740 0.3 

.174 0.2 

.754 0.3 

.702 0.3 

.525 0.3 

VOLUME VOLUME VOLUME 

CORRECT CORRECT NOMiNAL 

Vcr(std) Vcr(std) Vcr 

(cu ft) (liters) (cu fi) 

6.779 0.3 6.549 

6.181 0.2 5.994 

6.779 0.3 6.587 

6.701 0.3 6.511 

6.560 0.3 6.387 

Average Y -------> 

CALIBRATION FACTOR 

Y 

Value Variation 

(number) (number) 

1.006 0.003 

1.001 -0.002 

1.004 0.001 

1.000 -0.003 

1.005 0.002 

1.003 

CALISRATION FACTOR 

dHQ 

Value Variation 

(in H20) (in H20) 

1.397 -0.0040 

1.412 0.010 

1.401 0.000 

1.392 -0.009 

1.404 0.002 

1.401 < ------- Average dH a~ 

For Calibration Factor Y, the ratio of the reading of the calibration meter to the dry gas meter, 

ceptable tolerance of individual values (rom the average is +-0.02. 

ir Oririce Calibration Factor dH@, the orifice differential pressure in in s of H20 that equates lo 0.75 cfm of air 

68 F and 29.92,.inches of'FiDi~i accepi ble toler~nce of ind el v s from lhe average is +-0.2. _f: 

~ "` ~ c~ ~. 

SIGNED: ~'L^-/~7'" - ~ Date: ~t.. - • f ~ ~° ~ 

. , 

~ 

,.~ 

C.1 
Temperature Meter Calibrations 

Meter Box #: 10 

Date: 12/19/05 

Calibrated By: RT 

Emtech 42312 

Degrees F Calibrator Probe Stack Oven Exit Auxillary 

Point 1 32 32 32 32 32 32 

Point 2 100 101 102 101 101 101 

Point 3 250 252 252 252 252 251 

Emtech 42312 

Degrees R Ca(ibrator Probe Stack Oven Exit Auxilfary 

Point 1 492 492 492 492 492 492 

Point 2 560 561 562 561 561 561 

Point 3 710 712 712 712 712 711 

Percent Difference 

Probe Stack Oven Exit Auxillary 

Point 1 0. 0 0 0 0 

Point 2 0.178253 0.355872 0.178253 0.178253 0.178253 

Point 3 0.280899 0.280899 0.280899 0.280899 0.140647 

246 
: PI T OT TUBEE INSPECTI ON DATA SHEET 

, p r

01Tlpc'ly N3tle: ~i.~'I Ie _ ~~~ ~,~- r1'e—Sc~m~~ 

~ 

l° 

• ~ 

~ ~ v 

~ 

, ~ ai.e J ~/ i ~ z 

rr PWc:~ n.t i 

? os ~ Sar:ol e 

Da te ! 2- 1 S' 

/ ~ 1 evel ? 

obstructi ons? /U 

-o damaged? ~ U 

~ 

~ -10 0< a l< + 100 !~ 

1 

~ -10 0 < G 2< -100 ~ 

j f -50 < 3 1 < +5 a 

~ \ Q ~ L72C + ~ 'J 

~ f 

~ Y ~ ~ ~ O 

; - 

' r~ q 

Li 1.05 Dt < P a < 1.5 Dt , ,~~~ 

1 .05 Dt < Pb < 1 .5 Di. 

~ • ~ ( 

~ 

ri . 3 16< D,< 3 /

8

1

; / t •..~ ~S I 

•- Of D A tan Y < 0.125" 

~ A tan 6 < 0.03125" C) 

I Pa = Pb T 0.063" 

II 

, t 

Sa~~:txc xC::Lt 

~ 

:► rr S I'i: SL1I ~ ~ I 

Txi IM.rt;t ►RESSVtf OPr%1%c rlA%t or TIK rtTDT Tuit ` I 

SXALL i!I tr(u L•;ik OR lsOYC rn[ NOZ2L! (KTRY rjAtlt. 

I 1 

1 ., 

« « 

___.. 

• I• 

tl:s;t I ~ DtCiTIK LLYrt ~DilTlOr 

r0i CSTj ~ nittir4 T, :%jM :SLCVl1TlML Z. DCLREr iralCaTIK LfYCI 

rOStnow rDa DCTtRmlrl%t: o 

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r — 

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~ 

. •— — • •,:•-- _J t l 

DCCtijt ,IKOtCATI%G LEYCL 0011710• 

10, OfTr nIwlr0 3, ...d t,t 

.. uomments. 

- Pi tot tube/probe number ~ meets or exceeds all specifications 

criteria and/or appl icabl e design F eatures* and is hereby assigr.ed a 

pi io t. tutie c ai i bra t: i on -F actor o -F 0.84 

S i gna ~

_ 

.ure 

. o. ~ 'Spe 4-00 C ,:Q, ~ ~Jol. 42, No. loQ, hie ~. hod 2. Ver t~:y the minimu ~ n Q 

2 inch se.back o: the ther:nocoupie znd the mi;tinum 3/4 inch 

separation betueen the pitot .ube and the nczzle as shown a: 

:he Zop of tnis page. 

247 
~ >r 

Kput 1101a1106 lr•n ns1ri« 

rw I[)tbqi ~ 1. tru tiLtwlIIK L , Miitr 1. ~ c1t ~~C LtKt 

. mitiss w ILtu.1441S 6 

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Y 

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M111K l" K2tM1s1es . 

. ' • ` 

_. . _ ._. .._..._. 

Kcut .19"u•ruK ltrll Mltl" 

a Ktt.~•.ni r, .r ~► 

Comments: 

. .• 

P I T ~T TU4E INSPEi.TION DA i A Si ~ EE T 

CornpQny Name: J .e/j Pre-sam,ple 

~ Date 1,17,~ 

Post Sama 

Date 

. 

level? 

obstructions? 

.. . • 

damaged? 

-100 < ci 1 < +100 

-100 < a* 2 < 

< ~ i < 

< < 

' . Y 

8 

A 

1.05 Dt < P a < 1 5 D . t 

1.05 Dt < Pb '< 1.5 Dt 

3/1611 .< Dt.< 3/$ 11 

A tan Y< 0.125t 

A tan 9 <. 03 25" 0 1 

-

P a - Pb ± fl.06 3" -- 

~ 

Iv0 

~. 1 

. 3'  i 

~ 

~ 

• ` 

1 

1 

- ~7~ 

, 

rJ ;'S' ~f_j. 

- b 

. 

f - — i 

Pitot tube/probe number meets or. exceeds all specifications 

criteria and/or appl icab e design features* and is -hereby assigned,.a 

pi tot tube cal jbrati on f actor of 0.8411 

_ S i g na tu re 

` 

~~.~--'---,

~,~~= . ._ 

D a te . 

' ee 40 CFRo, Yo . 2, Ho. 160, Me:hod 2. Yerify the niniri,w l' ~ '' • ~ ~ 

2 inch setback of tna thermcouplt and the ninim= 3/4 inctt ~ 

seRtrition betrreen tha pi tat tube end tht noZ:le :s shown et 

the top of this paQe. 

2A8 
PI i Gi i U ~~ INSrEC i ION Or.Tr, S„HE i 

~ ✓ le. ~ ~'' 'C - ~ - .,

~~•G / d J,^ ~ _cc•- .. . ~ i ~' ''OS ~ SciTo 1? 

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s..tt tt tttt ca. o= t.o.t t.t loi:a Irt:r ryt. . 

: 

-10° < cz < ~ 

t / f ~ 

< 5 2 < +5° ~ l~ ---~! 

K:atL IrotClflrC C:YfL ~ t'StTlO. ~ ' 

oi tt:i ~ rir. T. ~.tr taa-.+i.::tK :. K:.,[[ tor[srt.0 ttKt ~ 

. ~ ITIOr !O. iCT[int.t.t • /. 

A 

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. 

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4 

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-- -•r- I~ ~ I fit..a na<0.03120- u ~ f 

. ~ t~-• ~, 

I . 

_ ;~; .. . _.. ~1 ~ ~ ~ '~ ' Pb = 0. 063 

K✓[f ; wutt.0 ,tRt ~rtt.e. ~ 

rw 

Coribll?n s : 

~ 1 to L ~~ be,/Jroo ~ nUm~_r ~~ rle~ ~ s or ~xcoG~ s a11 s ~ ec 1 i1c' ~ lor,s 

cri ~ e ria a n d/or ap.l icab e d es i gn i e3 ~ u r e s - and ~s n~r~by assi ~n~~a 

~~t.:~ e cal ~~ ra ~~ ort i ac ior o,' 0.3 ~' c 

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Q L U r?~~C- ✓` r -'~ 'i` ' , ,~ 

~ SV. .i .^..0 

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;e:a-t:;on ~ ez.+pea :ne

. 

 ~ it.: c,,e anc :`e n.c ~~ : as shorn t: 

the to^, ci ::^.is paqe. 

2,49 
PiTJi iU3E iNSP --CiION DATA SHEE, i 

r•, ~ ~ C~ 

11,11.16

~aeG ~^ p

~mJcT? f . Y ~ 3Tle : / . r~ . e-5c1~1~1_

~ 

, 

P o s t SGmc3 e 

D z ~~ 12- ,7 d I' 

:K•-xrnt 

................. 

~..~~ 

!' ~ I yr

•IrG rC::IL 

P

•--•~~~~

.~.~ 

Tii :rL't rtt:7W[ Q"rIK rLMC LT TfK •ITCT T•MC 

1►.tL IC f ~(~ ~:1~ 6t .60~ C twl iO::IL LMttT I, wt. 

~ 

► I 

.~ 

~ ~-----~ ~ 

~ s / (~p • 

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qfttltl~ IOa i(TCanrrrwC • 

~ 

--~ —•—• ~ , y -- ^ . _~— _ ~- ~ - --T+-"--° 

Y 

• 1 

'Q~ 

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, 

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ro. X'I>^ ~ rtK L, .••1{, 

Comn?nis: 

1 pvel ? ( ~-, 

r '~' 

N o obs ttruo t- i ons? LxLlzb) 

damageri -? 

-10 0 < < -10 ° I ~ 

q --- -10 0 < a2 < 100 I 3 

~ •• - ---- ~ ° < ~ 1< ~ 5° I .__ ~ 

~ -50 < 6 2< 

~ Y ~ 

f a f l 

, 41, 3 ~/- ) 

1.050-6<Pa< 1.5 

A 

D-,..3 ~ i 

1 

.3 1 ~ I1.05Jt<Pb<1.5 

3/10' (, .< D 

 3/8 rt 

D~ 

, 

67 ~✓ A tan Y< 0.125" 

A 'tan 8< 0.03125" 

Pa = Pb _ 0. 063" 

1 1:L7 i1'SL ( t ~ 

r 

I 

(0), 1!1 ta. 

~ o -LL ~ ;;be/probe n ~~mCer ~~ mepts or exceeds ai 1 speci f icaiions 

cri `eria and/or appl icabl e design ~ eaturps* anr~ is herehy assigne a 

pi :ot. LuSe cal ibration -F actor of 0.84. " 

o ~ ~ ~,~ ~• 

S i gna ture r,~~' ~~; _t.n •YY 

. _ 

~ a e 

'cee 40 C- ~ oG, Vcl. =2, Nc. icC. !•!^_.hoG 2. Yeri`y :ha r.inimun 

2 incn se.tack ot :Ne - `: e :-toc : uc'e ar.d :he rini-um 3/ 4 ;nch 

se ~ 2fd:ion ~ !Lr+e°_:1 'x'. e ` 1- + -.. _uvt 2:1e :hO d5 :hoti•: L: 

.he to, o` :his page. 

250 
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~ : fJl ~ll~~iv~~:.~~ , J ,.-! 

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` 

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_ I,VT t:~.0 ( ! 

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~ 

~~ 1 •• t 1~ :l:T j ~ ; 

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t_-r' ~ ~I ► . 

'J 1 

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obs truc t- i ons? 

ltlb 

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J —5.0 ~ 

1 

< ~ < _

- -O 

< ~ ? < ~

P*° 

Y ' I 

I , ~ • J~0 ~ I 

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.

.5 o-.-, 

1.05ot<?b<1.50.6 

. 1 

Z~~I 

? lo l,.< ~_~ 3 / ~11 _I / _ 

~f~ f 

~ A i~ .~ - n Y < 0.1 Z ~ " . U' 7 

 

~ A. 4. ;j

:, < o. 03; 25" 

I 

I Pa ' Pb = 0.053" '\ ~C J 

~tj `') 

Na 

~ 

~ 

v 

S 

1 

.1 

~ J I 

~ .0 

, . 1 S" 

r L 

~ ~

i? 

0 .6*( Z, 

<fs 

Con„i en Ls . 

• ~ 7i,C ~ i,;; ~°~ ,t7r0 ~~ nU;~~~r ,~ ..5 6t2°i.5 Cr ?XCp°Js c! l s ~ 2t7 i 1Cc~ tiCrS 

Crli.°?"lZ cnd/Cr 3p}:i 1Ca0lGEs10Ti i°ctt llres *an(i ?s ziarQ',i, c' 

~~:~ . ~~_~~ ca 1 i b ra t ; or, ~ ?c tor o f 

SiGna L ,, ;-a-~ 

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~~ !: .y_.., c ~ , 5.. -., li.. to ~ , t!... a ~ C ~ Y 

L 1nC;. S2:GiCX Uf :f+E: ~ i.'~":0• . • D~~ LTUi :!te :/i .:Ch 

3L%2.'LsJC[1 Dt«QL:. :T.? y^lwi dTt: :h! •',:i.:It LS S!1C-r- 2: 

:ae io^ os pa^y !. 

2 ',5 1- 

Appendix F: 
AP 3106 Pasadena Freeway 

Pasadena, Texas 77503 

(713) 534-8217 Fax(713) 534-8133 

Specialty Gas Products 

Date: 6/27/2005 

Customer: Matheson - Trigas Project: 16015 

Description: NO in N2 - EPA Protocol Exp. Date: 6/27/2007 

Cylinder No: EB0001164 Cylinder Pressure: 1900psig 

Requested Certified 

Component Concentration Concentration Accuracy 

Nitric Oxide 50 ppm 50.4 ppm 1% 

Nitrogen, Balance 

NOx: 51 ppm 

Reference Standard 

Description Expiration date Cylinder Number Concentration 

GMIS 11/22/2006 ND22557 99.8 PPM no 

Instrumentation 

Description Model # Date Last Clibrated Principle 

Horiba Process Analyzer CLA-510-NO 6/16/2005 CHEMI 

Anaylsis Results: Z= zero gas, S= standard gas, X= sample gas 

First Triad - NO Second Triad - NO 

Z1= -1.20 S1= 994.80 X1= 498.30 Z1= -1.10 S1= 998.50 X1= 502.80 

S2= 994.10 Z2= -1.30 X2= 498.40 S2= 998.20 Z2= -0.70 X2= 502.40 

Z3= -1.10 X3= 499.80 S3= 997.40 Z3= -0.80 X3= 500.80 S3= 994.20 

Average = 50.3ppm Average = 50.53ppm 

Curve: Y = 0.33645 + 0.099857*X 

Analyst: 

% 

TFIIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

2,93 
~

•. 

Specialty Gas Products 

3106 Pasadena Freeway 

Pasadena, Texas 77503 

(713) 534-8217 Fax(713) 534-8133 

Date: 6/27/2005 

Customer: Matheson - Trigas Project: 16014 

Description: NO in N2 - EPA Protocol Exp. Date: 6127l2007 

Cy(inder No: EB0001156 Cylinder Pressure: 1900psig 

Requested Certified 

Component Concentration Concentration Accuracy 

Nitric Oxide 25 ppm 25.0 ppm 1% 

Nitrogen, Balance 

Reference Standard 

NOx: 25.5 ppm 

Description Expiration date Cylinder Number Concentration 

GMIS 11/22/2006 ND22557 99.8 PPM no 

Instrumentation 

Description Model # Date Last Clibrated Principle 

Horiba Process Analyzer CLA-510-NO 6/16/2005 CHEMI 

Anayisis Results: Z= zero gas, S= standard gas, X= sample gas 

First Triad - NO 

Z1= -1.20 S1= 994.80 

S2= 994.10 Z2= -1.30 

Z3= -1.10 X3= 246.10 

Average = 24.90ppm 

Curve: Y = 0.33645 + 0.099857*X 

Second Triad - NO 

X1= 244.50 Z1= -1.10 S1= 998.50 X1= 247.10 

X2= 244.80 S2= 998.20 Z2= -0.70 X2= 247.00 

S3= 997.40 Z3= -0.80 X3= 246.40 S3= 994.20 

Average = 25.00ppm 

Analys : . -----'— 

,.. 

THIS STANX

.

RD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

2. 15 4 
Specialty G>~s ~'roducts 

3106 Pasadena Freeway 

Pasadena,Texas 77503 

(713) 534-8217 Fax(713) 534-8133 

Date: 617/2004 

Custorner: Trigas Project: 9210-01 

Description: Propane in Air - EPA Protocol Exp. Date: 6/7l2007 

Cylinder No: SX41680 Cyfinder Pressure: 1900psig 

Requested Certified 

Component Concentration Concentration Accuracy 

Propane 30 ppm 28.8 ppm 1% 

Air, Balance 

Reference Standard 

Description Expiration date Cylinder Number Concentration 

NTRM 712/2004 SG9183302 103.6 ppm Propane 

Instrumentation 

Description Model n Date Last Clibrated Principle 

Horiba Process Analyzer FIA-510 5/24/2004 FIA 

Anayisis Results: Z= zero gas, S= standard gas, X= sample gas 

First Triad - Prooane 

Z1= 0.60 S1= 207.90 X1= 57.60 

S2= 207.70 Z2= 0.60 X2= 57.50 

Z3= 0.60 X3= 57.40 S3= 208.00 

Curve: Y=-0.05085+0.501149*X 

Average = 28.77pm 

~ 

Analys~-~ 

r•' 

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

2.'~ 5 
Specialty Gas. ~''rc~ c.~c.~•cts 

3106 Pasadena Freeway 

Pasadena, Texas 77503 

(713) 534-8217 Fax(713) 534-8133 

Date: 6/7/2004 

Customer: Trigas Project: 9211-01 

Description: Propane in Air - EPA Protocol Exp. Date: 6/7/2007 

Cyiinder No: CC177391 Cylinder Pressure: 1900psig 

Requested Certified 

Component Concentration Concentration Accuracy 

Propane 50 ppm 48.8 ppm 1% 

Air, Balance 

Reference Standard 

Description Expiration date Cylinder Number Concentration 

NTRiVi 7/2/2004 SG9183302 103.6 ppm Propane 

Instrumentation 

Description Niod'el # Date Last Ctibrated Principle 

Horiba Process Analyzer FIA-510 5/24/2004 FIA 

Anayisis Resuits: Z= zero gas, S= standard gas, X= sampie gas 

First Triad - Pronane 

Z1= 0.60 S1= 207.90 X1= 97.60 

S2= 207.70 Z2= 0.60 X2= 97.20 

Z3= 0.60 -X3= 97.50 S3= 208.00 

Curve: Y=-0.05085+0.501149"X 

Average = 48.78pm 

•r• ,. 

Analyst: 

.~' 

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

2 156 
Speci'alty Gas Prod~ c~-s 

3106 Pasadena Freeway 

Pasadena, Texas 77503 

(713) 534-8217 Fax(713) 534-8133 

Date: 8l312005 

Custorner: Trigas Project: 17092 

Description: Propane in Air - EPA Protocol Exp. Date: 813l2008 

Cylinder No: CC112437 Cylinder Pressure: 1950psig 

Requested Certified 

Component Concentration Concentration Accuracy 

Propane 90 ppm 89.2 ppm 1% 

Air, Balance 

Reference Standard 

Description Exairation date Cylinder Number Concentration 

SRM 12l112009 XF004033B 488 ppm Propane 

Instrumentation 

Description Model # Date Last Clibrated Principle 

Horiba Process Analyzer FIA-510 813l2005 FIA 

Anaylsis Results: Z= zero gas, S= standard gas, X= sampie gas 

First Triad - Prooane 

Z1= -0.10 S1= 975.30 X1= 176.50 

S2= 975.10 Z2= -0.10 X2= 175.40 

Z3= -0.10 X3= 176.20 S3= 975.20 

C urve: Y=1.0614+0.500676'X 

Average = 89.21 pm 

Irr 

J 

Analyst:,%~~ - 

THIS ST,9NDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

2,57 
Specialty ~~ Pr ~s oducts

3106 Pasadena Freeway 

Pasadena, Texas 77503 

(713) 534-8217 Fax(713) 534-8133 

Date: 8/3/2005 

Customer: Trigas Project: 17093 

Description: Propane in Air - EPA Protocol Exp. Date: 813I2008 

Cyiinder No: SX28250 Cylinder Pressure: 1950psig 

Requested Certified 

Component Concentration Concentration Accuracy 

Propane 200 ppm 200 ppm 1% 

Air, Balance 

Reference Standard 

Description Expiration date Cylinder Number Concentration 

SRM 12l1/2009 XF004033B 488 ppm Propane 

Instrumentation 

Description Model # Date Last Clibrated Principle 

Horiba Process Anaiyzer FIA-510 8/3/2005 FIA 

Anaylsis Resuits: Z= zero gas, S= standard gas, X= sample gas 

First Triad - Prooane 

Z1= -0.10 S1= 975.30 X1= 398.10 

S2= 975.10 Z2= -0.10 X2= 398.00 

Z3= -0.10 X3= 397.80 S3= 975.20 

Curve: Y=1.0614+0.500676*X 

Average = 200.3 ppm 

Analyst: 

~- 

THIS STANDARD`IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT US`r= THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

2...58 
Specialty Gas Products 

3106 Pasadena Freeway 

• Pasadena, Texas 77503 

(713) 534-8217 Fax(713) 534-8133 

Date: 7/13/2004 

Customer: Matheson-Trigas Project No: 9970 

Description: S02 in N2 - EPA Protocol Exp. Date: 7113/2006 

Cylinder No: . CC88735 Cylinder Pressure: 1900psig 

Requested Certified 

Component e Concentration Concentration Accuracy 

Sulfur Dioxide 100ppm 101 pprn 1% 

Nitrogen, Ba!ance 

Reference Standard 

Description Expiration date Cylinder Number Concentration 

GMIS 1l19/2006 CC177157 793.8pprn S02 

* GMIS CC1771 57 Tracebility 

Description Expiration date Cylinder Number Concentration 

NTRM 6/1/2006 SG9199568 1997ppm S02 

lnstrumentation 

Description Model # Date Last Clibrated Princiale 

Horiba Process Analyzer VIA-510-S02 6/15/2004 NDIR 

Anayisis Results: Z= zero gas, S= standard gas, X= sample gas 

First Triad - S02 Second Triad - S02 

Z1= -0.90 S1= 791.9 X1= 98.7 Z1= -0.90 S1= 794 X1= 99.0 

S2= 794.0 Z2= -0.70 X2= 99.0 S2= 793.2 Z2= -0.60 X2= 99.2 

Z3= -0.90 X3= 99.2 S3= 792.6 Z3= -0.60 X3= 99.30 S3= 793.4 

Cu rve: Y=1. 971 +0. 999869'`X 

Average = 100.6ppm Average =100.9ppm 

^ /~ ----- Analyst : ' --_- 

~ Ling WeFr-"- ~ 

THIS STAN-Y~RD IS NlST TRACEABLE. IT WAS CERTIFIED P.CCORD!NG TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

2,59 
Specialty Gas ~'rc~ ducts 

3106 Pasadena Freeway 

Pasadena, Texas 77503 

(713) 534-8217 Fax(713) 534-8133 

Date: 7113/2004 

Customer: Matheson-Trigas Project No: 9969 

Description: S02 in N2 - EPA Protocol Exp. Date: 7/13/2006 

Cylinder No: CC177434 Cylinder Pressure: 1900psig 

Requested Certified 

Component Concentration Concentration Accuracy 

Sulfur Dioxide 50ppm 50.1 pprn 1% 

Nitrogen, Balance 

Reference Standard 

Description Expiration date Cylinder Number Concentration 

NTRM 6/1/2006 Sg9135833 99.8ppm S02 

Instrumentation 

DescriQtion Model # Date Last Clibrated Principle 

Horiba Process Analyzer VIA-510-S02 717/2004 NDIR 

Anayisis Resuits: Z= zero gas, S= standard gas, X= sample gas 

First Triad - S02 Second -Triad - S02 

Z1= -1.30 S1= 999.90 X1= 502.60 Z1= -0.80 S1= 997.90 X1= 500.30 

S2= 999.90 Z2= -0.70 X2= 503.60 S2= 998.70 Z2= -0.10 X2= 500.30 

Z3= 0.00 X3= 503.60 S3= 999.90 Z3= -0.20 X3= 501.60 S3= 999.30 

Curve: Y=0.0064+0.09986'`X 

Average = 50.15ppm Average =49.98ppm 

. ...~ 

Analyst: - 

~ 

Ling,Wen 

THIS STANDARD IS NIST TRACEABLE. (T WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

r.~ 
s pecialty Gas Products 

3106 Pasadena Freeway 

Pasadena, Texas 77503 

(713) 534-8217 Fax(713) 534-8133 

Date: 6/27/2005 

Customer: Trigas Project: 16017 

Description: CO in N2 - EPA Protocof Exp. Date: 6/27/2008 

Cyfinder No: EB0000701 Cylinder Pressure: 1900psig 

Requested Certified 

Component Concentration Concentration Accuracy 

Carbon Monoxide 50 ppm 49.9 ppm 1% 

Nitrogen, Balance 

Reference Standard 

Description Expiration date Cyiinder Number Concentration 

NTRM 5/29/2006 SX19190 994.2 ppm CO 

Instrumentation 

Descriation Modei # Date Last Ciibrated Princigie 

Horiba Process Analyzer VIA-510-CO 6/10/2005 NDIR 

Anaylsis Results: Z= zero gas, S= standard gas, X= sampie gas 

First Triad - CO Second Triad - CO 

Z1= -0.90 S1= 204.90 X1= 198.70 Z1= -0.40 S1= 513.30 X1= 497.10 

S2= 204.80 Z2= -0.80 X2= 198.60 S2= 513.20 Z2= -0.40 X2= 497.10 

Z3= -0.80 X3= 198.60 S3= 204.90 Z3= -0.40 X3= 496.90 S3= 513.20 

Y=0.28607+0.250309'"X Y=0.031031 +0.100163*X 

Average = 49.94ppm Average = 49.82ppm 

~ - 

analyst: ' 

~ 

THIS STANDARD IS NIST TRACEABLE. iT VUAS CERTIFIED ACCOP,DING TO THE EPA PriO T OCOL PROCEDURES. 

)0 NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

261 
SpecidIty G~s ' Proc~I~..,{c ~-s 

 3106,Pasadena Freeway 

Pasadena, Texas 77503 

(713) 534-8217 i=ax(713) 534-8133 

Date: 6/27/2005 

Customer: Trigas Project: 16018 

Description: CO in N2 - EPA Protocol Exp. Date: 6/27/2008 

Cylinder No: EB0000761 Cylinder Pressure: 1900psig 

Requested Certified 

ComQonent Concentration Concentration Accuracy 

Carbon Monoxide 100 ppm 991 ppm 1% 

Nitrogen, Bafance 

Reference Standard 

Description Expiration date Cyiinder Number Concentration 

NTRM 5129J2006 SX19190 994.2 ppm CO 

Instrumentation 

Description Niodel # Date Last Clibrated Princinie 

Horiba Process Analyzer VIA-510-CO 6/1012005 NDIR 

Anayisis Results: Z= tero gas, S= standard gas, X= sampie gas 

First Triad - CO Second Triad - CO 

Z1= -0.90 S1= 204.90 X1= 396.60 Z1= -0.40 S1= 513.30 X1= 985.70 

S2= 204.80 Z2= -0.80 X2= 396.60 S2= 513.20 Z2= -0.40 X2= 985.40 

Z3= -0.80 X3= 396.50 S3= 204.90 Z3= -0.40 X3= 985.20 S3= 513.20 

Y=0.28607+0.250309*X Y=0.031031 +0.100163"`X 

Average = 99.45ppm Average = 98.74ppm 

. ._._.~ 

Analyst: 

TH1S STANDARD IS NlST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSlG 

2 62 
Specialty Gas ~'rod~..~c~-.~ 

3106 Pasadena Freeway 

Pasadena, Texas 77503 

(713) 534-8217 Fax(713) 534-8133 

Date: 8/1612004 

Customer: Nlatheson - T rigas Project: 10548 

Description: CO, 02 in N2 - EPA Protocol Exp. Date: 8/162007 

Cylinder No: CC187154 Cylinder Pressure: 1900psig 

Requested Certified 

Comaonent Concentration Concentration 

Carbon Monoxide 200ppm 200ppm 

Nitrogen, Balance 

Reference Standard 

Description Expiration date Cylinder Number 

G M I S 4!6!2006 CC 177636 

Instrumentation 

Description Model # Date Last Clibrated 

Horiba Process Analyzer VIA-510-CO 8/6/2004 

Anayisis Results: Z= zero gas, S= standard gas, X= sample gas 

First Triad - CO Second Triad - CO 

Z1= -0.3 S1= 993.5 X1= 199.9 Z1= -0.4 S1= 995.5 

S2= 993.20 Z2= -0.30 X2= 200.00 S2= 995.80 Z2= -0.30 

Z3= -0.30 X3= 199.90 S3= 993.00 Z3= -0.30 X3= 200.60 

Curve: Y=-0.6893+1.001139X 

Average =199.6ppm Average = 199.8ppm 

Accuracy 

1% 

Concentration 

994.2 ppm CO 

Principle ' 

NDIR 

X 1= 200.6 

X2= 200.60 

S3= 995.60 

Analyst: 

Ling 1iJen 

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

2.. R 3 
Cylinder Number Concentration 

CC177636 994.2 ppm CO 

Date Last Clibrated Principle 

8/6/2004 ND I R 

Second Triad - CO 

Z1= -0.4 S1= 995.5 X1= 495.4 

S2= 995.80 Z2= -0.30 X2= 495.60 

Z3= -0.30 X3= 495.50 S3= 995.60 

Average = 494.4ppm 

Specialty Gas P 

3106 Pasadena Freeway 

Pasadena, Texas 77503 

(713) 534-8217 Fax(713) 534-8133 

Date: 811612004 

Customer: Matheson - Trigas 

Description: CO, 02 in N2 - EPA Protocol 

Cylinder No: CC176507 

Requested 

Component Concentration 

Carbon Monoxide 500ppm 

Nitrogen, Balance 

Reference Standard 

Description Expiration date 

G M I S 4/6l2006 

instrumentation 

Description Modei # 

Horiba Process Analyzer VIA-510-CO 

Anayisis Results: Z= zero gas, S= standard gas, X= sample gas 

First Triad - CO 

Z1= -0.3 S'f= 993.5 X1= 494.2 

S2= 993.20 Z2= -0.30 X2= 494.00 

Z3= -0.30 X3= 493.90 S3= 993.00 

Curve: Y=-0.6893+1.001139X 

Average =494.1ppm 

P roject: 10549 

Exp. Date: 8/162007 

Cylinder Pressure: 1900psig 

Certified 

Concentration Accuracv 

494ppm 1% 

Analyst: 

Ling W6ri 

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

2 9-4 
Appendix G 
Sheetl 

Summary 

,ant: 

I nterfern ce An 

Daltile, Muskogee, OK 

Location: Trim Kiln Exhaust 

Date: 1218/051 

Anal)Lzer: lWestem Research 721-AT 

Run # Method 6 Method 6C Difference, % 

1 86.36 83.63 103.2644 

72.24 69.78 103.52541 1 

31 79.02, 75-171 105.12171 

Page 1 273 
EMISSION TEST SUMMARY 

PLANT : Deltile, Muskogee, OK 

DATE : 6-Dec-05 

PLACE : Trim Kiln Exhaust, S02 Interference Train 

RUN# : 1 

TEST DURATION (MINUTES) : 64 LIQUID COLLECTED (mis) : 

NOZZLE DIAMETER (INCH.) : 0 Sulfur Dioxide Weight, mg : 

METER COEFFICIENT (Y) : 0.944 

PITOT COEFFICIENT (Cp) : 0 STATIC PRESSURE (in. H20) : 

GAS METER VOL.(Cu.Ft.) : 2.316 PERCENT CO2 . 

BAROMETRIC PRESSURE . 30 PERCENT 02 . 

PERCENT CO . 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 0 STACK LENGTH(inchs) : 

STACK AREA (Sq.Ft.) : 0 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0 STACK AREA (Sq.Ft.) : 

ENTER THE STACK AREA SHOWN ABOVE: 0 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 2.2267 

Sulfur Dioxide, ppm : 86.3631 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. 

deg F I N LET 

1 0 0.01 59.62 

0 0.0000 0.0100 59.6200 

0 

14.49 

0 

0 

0 

0 

0 

C 

METER T. 

OUTLET 

59.62 

59.6200 59.6200 

274 
EMISSION TEST SUMMARY 

PLANT : Daltile, Muskogee, OK 

DATE : 6-Dec-05 

PLACE : Trim Kiln Exhaust, S02 Interference Trein 

RUN# : 2 

TEST DURATION (MINUTES) : 62 LIQUID COLLECTED (mis) : 0 

NOZZLE DIAMETER (INCH.) : 0 Sulfur Dioxide Weight, mg : 10.93 

METER COEFFICIENT (Y) : 0.944 0 

PITOT COEFFICIENT (Cp) : 0 STATIC PRESSURE (in. H20) : 0 

GAS METER VOL.(Cu.Ft.) : 2.091 PERCENT CO2 . 0 

BAROMETRIC PRESSURE . 30 PERCENT 02 : 0 

PERCENT CO : 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 0 STACK LENGTH(inchs) : 

STACK AREA (Sq.Ft.) : 0 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0 STACK AREA (Sq. Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 0 

FL01NS 

SAMPLED VOLUME (STD. CU .FT.): 2.0078 

Sulfur Dioxide, ppm : 72.2463 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 0 0.01 60.28 60.28 

0 0.0000 0.0100 60.2800 60.2800 60.2800 

275 
ENIISSION TEST SUNINIARY 

PLANT : Daltile, Muskogee, OK 

DATE : 6•Dec•05 

PLACE : Trim Kiln Exhaust, S02 Interference Train 

RUN# : 3 

TEST DURATION (MINUTES) : 62 LIQUID COLLECTED (mis) : 0 

NOZZLE DIAMETER (INCH.) : 0 Sulfur Dioxide Weight, mg : 11.72 

METER COEFFICIENT (Y) : 0.944 0 

PITOT COEFFICIENT (Cp) : 0 STATIC PRESSURE (in. H20) : 0 

GAS METER VOL.(Cu.Ft.) : 2.052 PERCENT CO2 : 0 

BAROMETRIC PRESSURE . 30 PERCENT 02 : 0 

PERCENT CO . 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 0 STACK LENGTH(inchs) : 

STACK AREA (Sq.Ft.) : 0 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0 STACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 0 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 1.9684 

Sulfur Dioxide, ppm : 79.0194 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 0 0.01 60.8 60.8 

0 0.0000 0.0100 60.8000 60.8000 60.8000 

J 

276 
Sulfur Dioxide Barium-Thorin Analysis 

Plant: Daltile, Muskogee, OK 

Location: Trim Kiln Exhaust, S02 Interference 

Date: 8•Dec•05 

Standardization Ba (C102)4 

Titration (mis) Avg. Titration (mis) 

9.833333 

Blank Titration (mis) Avg. Blank (mis) 

0 

Volume of Standard Sulfuric Acid (mis) 

Normality of Standard Sulfuric Acid 

Normality: 0.010169 

Aliquot Average 

Run # Location Volume Dilution Volume Titration Titration 

(mis) (mis) (mis) (mis) (mis) 

1 I m P 1•2 

~:;:,:,;::::,:,; :::::: .:..::::::::::::::::::::... . 

18 •~: :~ ~:~~~i~~~~ ~l~, ~~~ '5: E?:= ~~~~' :~~$;~ 5 .5666667 

2 I m p 1•2 

:$. Q'• :i~ : 4.2 

3 I m P 1•2 . Q: ~'`~~~'~~~:~ ::::::: ~:~ : :: ~:~~~~~~:~:;:~~ ::;:;::::;: ' 

: ~ $ .. ~ .::: ~ ::::::: ~~~:~:::~:)~~ :`:: ~::~~::~ :::::4i ~:~::~~ :::::: ~'~ :::. .. .5...... . .4t ~~'~'.:~~:~:: 4.5 

Run # Location Total Grams Total Mg 

1 Imp 1& 2 S02 0.014492 14.49 

2 Imp 1& 2 S02 0.010934 10.93 

3 Imp 1& 2 S02 0.011715 11.72 

2.7'7 
PEF-LD DATA 

PLAN'f: ~~ i F t ~, 

DATE: 

REPETITION: 

LOCAi—ION (SOURCE,,): 

OPERATOR: ~AT 

SANDLE TRAIN 'Tr: 

NETER BOX 'Tr: 

BAROMEnuc PREssuRE: 3 

AMBIENT TENTERATURE: 

ASSTj'NED MOISTURE: 

PROBE LENGTH: ' 

NOZZLE PLAMETER: 

STACK DIAM:ETER: 

METE R H: 

C FACTOR: 

METER CO-EFECIENT: Iqq 

FU,TER TARE: 

PRE-TEST LEAK CHECK 

Meter: S - 0100cu.ft. @ in. HG 

Pitntc• (n) in '910 

EMPLNITGERS 

Initial Finai 

#1 3; 0 

., 1 3 "ev 3 4& .U-) 30 30 

'4 

96 

CO2 02 

POST-TEST LEAK CHECK 

Meter: 40 -c-0 o cuft @ in. HG 

pitovq- e- (a. in- R20 

Time 4:1 Tk_ 

r Ft: 

Tt 

oudev-;' - 

Ory 

~-T emp;* T 

7- 1 57 IS 

3 30 ~ ,! G?, t ~ r~`" 

Y .71. r l ~ ~~ 

1yo lb Ir 

YgT 1- 16 

co RVI / ir i~ ! 

Sf If -o 

~o ;oS o3•Z C6 ~~ ( 

. 

z~ I 

! c s.~ t ~ s 

( ~~.63 ~s. I ~ 

i I i ! 

I i i 

! I 

I_.. .. ~ _ .. 

. ! ~ . `_ ' I ' i ' 

 _y ; ~ ; ~ _-- ~ _ __. -.f : .. 

I 

Ave. 
! r le ti ~~ - PLANT: ~~,t'r 

DATE: 

REPETITION: 

LOCATION (SOURCET.-)11 -- ~ 

OPEPLATOR: 

SAN4PLE TR.AJN 

NMTER BOX rr. 

BAROMETRIC PRESSURE: 

AMBM'NT TENTERATURE: 

ASSLTIvIED MOISTURE: 

PROBE LENGTH: 

NOZZLE DIAMETER: 

STACK DIAAIETER: 

METER H: 

C FACTOR: 

METER CO-EFFICEENT: (5 

FILTF-R TARE: 

PRE-TEST LEAK CHECK 

Meter 0, eVO cu.fL @ in. HG 

Pitots: . A) in. H20 

FIELD DATA 

FWDiGERS 

Initial Final 

-ul 50 2p 

-Tur 2 

.U.-W tr.) 

-Ulf rr-t 

rrD .0 - 

#6 

CO2 02 

POST-TEST LEAK CHECK 

LMeter: 0 .000 mfL @ in. HG 

Pitots: a, in. H20 

PLW Mme. _~ .'sltmd~. t ~~PcIU Vi T lz 

lniets 

Im .,.. 

p1 - - T 

S-D 723. 1,6 IS" 

:5,~- -_ 21. -7 16 r.S'- 

11.06 11 .33.'? 

1. vs- 1 38•7 

't Y, o e(p /so" 

X2 %W e ~ 

tv 3 

to (09. C( 

7%f - C& 16 

cp ti 

L17 

7 

( I . 

2 7. 
FIELD DATA 

PLAN'.r: 

DATE* t , 06, 

REPETITION: 

LOCATION (SOURCF,4): 

OPER.~kTOR: 'F'4 

SAI,,,IPLE TRAliN 41: 

LvETER BOX rlr: 

BA.ROMETRIC PRESSURE: 3 E) 

AMBIENT TENDERATURE: 

AS SUIvIED MOISTTi-RE: 

PROBE LENGTH: 

NOZZLE DL41METER: 

STACK DLAAIEETER: 

LMETER El: 

C FACTOR: 

METER CO-EFMCIENT: 

FILTER TARE: 

PRE-TEST LEAK CHECK 

Meter: 0 ,00 cuft @ in. HG 

Pitot-q. (a- ln_ T-T20 

""rmPINGERS 

Initial Final 

r'r'3 

~ 

CO2 02 

POST-TEST LEAK CHECK 

Meter: ig -, c- , Ovcu.ft. @ in. HG 

pitots. (a. in. H20 

"T 

i _14 

Ahe 

Delta -Tm V.: T 

o 

c 

iii.HME." 

l~~ a3.~ ~ ~~ 

b~ : ~o ~~3• ~` ~!b ~ f 

TOT_ 

3q.y (4. 

I cG 4 

! f .~g~~~~ ~~ ~~ 

~ ~ ~e . 

I f ! ~ ~__ ! 

f ~ ~ 

Ave, 128011 
A1tr sirottci Etivirormrenial Itrc. 

EI'A Melhoci 0 

Oririce MeIIioJ 

Liiglish tvleler Box Units, English IC Factor 

cI Dry Gas Meter Oiile: --- ----------- --------- > July 11, 2003 

3909 t3arorrnellic f'ressure: ---- - ---- > 29.70. 

'i"hr.uretical Crilical Vacuuun:----• 13.91 (ilt. 1-1g) 

CONVL=RSION FAt;1 Vi:S 

I ttutti Hg = 0.13330 N.Pa 

1 cin = 0.39370 iiicit 

1 nrrn - 0.03937 iricil 

I cu tl = >13.:32 19ters 

%h For•valici lesl resulls, tiie Acltial Vacuum stwuld be I to 2 iii. I-ig greater Ihati lhe Theorelical Ctilicai Vacuum shuwn above. 

%n 1 -I,e Critical Oifi'ice Coet('iciei,t, W. musl be etilered in Eriglisll utiils, (fl)^3 4 (deg 

---------------- Dftl' GAS ML"i'ER ftEADINGS --------- ------- -CRITICAL ORIFICE READINGSTheurelical Criticat Vacuwrr:---> 14.05 (in. 1 -Ig) 

Voli,me Volun,e Volun,e Iniiiat Temps. Final Tetnps. Otifice IC Orifice Aclual - Anibient Tempetature -- OGM DGM /ltttbicni 

Tiiiie Inilial Fitial Tolal Inlel ' Ottllel hilel Oullel Serialit Coelficient Vacuum Inilial Final Average Outlel t)verall Temp 

(nth). (cu tt) (cu tl) (cu tl) (deg F) (deg F) (deg F) (deg F) (nurttber) (see above) (lii lig) (deg F) (deg F) (deg F) (deg R) ((leg R) (dt:y 

) 5.00 I6.716 16.917 0.20*1 87.0 07.0 07.0 87.0 10907 0.029 23.0 07.0 87,0 07.0 547.0 547.0 547.0 

l 5,00 16.917 17.110 0.201 07.0 07.0 87.0 07.0 - 16907 0.029 23.0 07.0 07.0 07.0 547.0 547.0 547.0 

l 5.00 17.118 11.320 0.202 07:0 07.0 87.0 87.0 16907 0.029 19.5 07.0 07.0 07.0 547.0 547.0 7.0 

.~ ......... •...... •..................... I(t_.SUt_TS .............. r•••••..................... www.....ww 

AS MLTER --- --------- ORI1=10E --------- - - DIZY GAS METER -- -------- OIIIFICE --------- 

VOLUMI.=. VOLUMI= VOLUMC VOLUME CALIBRATIOIJ FACTOR CALIERAI•ION FACTOIZ 

T CORRECI'ED GORRECT C012REC1' NOMINAL Y dHQ 

) Vm(slcl) vc,(stcl) Vcr(sld) Vcr Value Varialioti Value Vatialion 

i (tilers) (cu (t) (liters) (cu Il) (tiuttiber) (nuttiber) (in 1-120) (in I-120) 

1 0.0 0.102 0.0 0.190 0.94G 0.002 0.000 0.0000 

t 0.0 0.1821. 0.0 0.190 0.945 0.002 0.000 0.000 

i 0.0 0.1 Li2 0.0 0.190 0.941 -0.003 0.000 U.000 

Avet age Y ------- > 0.944 0.000 <------- Average dl-IQ 

...,,:alioti Faclor Y. lhe ralio o( the teaditig o( lhe caiibtalioii nteler lu Ilte dry gas titeter, 

laufe.loieratice of itidividual values frotti Ihe average is +-0.02. 

ririce•Calibralion Fhctor-dl-tL, tlie wi(ice dillerenljal pre su i e in inc,l i es o( 1120 lhal equales lo 0 .75 c(m o( air 

F artid 29.92 incties o( I ly, accelJla~ile-idle ange~o( ir ividual v lues itom Ilie average is +-0.2. , 

SIGN_f=D: '-" ~~f, t. .r` ~ Date: 

. 

---~ 

; 

T\D 

Q0 

~ 
l APEX (NSTRUMENTS VUA ORIFICE ADAPTEIt C/11,I8RATIOfd ^^_ 

Cattlirallott CorfUtltons 

oale rlme 07/10103 16:3U 

03rotrtelric Pressure 749.0 rum 119 

Thcorellcal Critical Vacuuni 353.5 1 n>tn 119 

Calibtatton Tecltniclan RM 

Fa clor slConvc rslons 

5tJ Tentp 293 1< 

SIJ t'ress 760.00 mrn I Iq _ 

K t 0.306 K/r om I ly 

Calihra{Ivrt lnio+nntlort 

WT1.1 M(tlel rlu,npar A1.11 

~

WIM Scriil Nymbcr I6807 

WI M Gan,ma ~^._ ___ I.OUOl1U 

''Ihe Critical Urillce Co¢ilieiertl, K', Irr L•nUlish vrtits, 

'll+cCri0cal Orilicc Coclticicrtt, 1(', i4 Metrlc vnits, (L'1(I!(Inmllg'nur,). 1tOTE: VULUME Ill UIEttS 

Callbra0on Data 

Wet Tesl fActer 

Rvn // Vrilice ltun Ttme Voltrnto Voltnne Voluttta 7emperaluro 

5cria111 Clap.ed brilial FMaf Tolal Irritial 

NM) N.J 

f. _ L L IC 

1 1 74-14-03 G 306.025 312.500 6.475 30 

2 F

K4 -fe•03 312.500 310.960 6.4 60 30 

3 K•t - 14 -03 G 310.960 325.d2U 6.460 30 

Rasulis 

VUA Atiopler 

Tempt,raluto 

Fhlal 

/lrnb Tentir 

Inslhl 

Atttb Tentp 

Flltal 

Actual 

Vacuuin 

Coetticlent 

Melrlc Urdts • 

(+.,r) (1 -4E) 8—'(4 K, 

't; 'C 'C nnn I Ip sac above 

30 29 29 597 0.0239 

30~— 29 29 610 0.0230 

30 29 30 O I U 0.023 

(:0alllcionl % Variallort 

ngllsh Units troin_AvU 

Cf!Q a I 

2.071E-02 ~0.17 

2.063t=-02 —~ 

~ 

0.{ 1 

_ 2.004C-02 -O.UG 

2.066[-02 ^' ~ 

I eertily 11ls,t O, ilicc scl rnrntbar/L' wns tesleci in nccorJanctr wilh Ilto US EPA MelltoJ 5 stanJartis. 

Sec.11te C•o(;o ol Fctferi ,10111.1t1a ns, liUe 4 0, I>att 60;nppa+u ix A, MElttoJ"5, ilem 7.2. 

---- -- 

~

Cquatlon lo Calcutale.SlanJardized Flowrate I 

(Given /1nlbient Eiaruinetric'Pressure and Absoiule 

Temperature Condiliolls: Pb, r & Ta,nn(ab:)): 

1/Z 

Qcr(slJ)-K

, 

 * Pbar/Tamb(abs) 

~ 

00 

N)l 
Li 

~ 

4 1 1 1 

LL 
Sheetl 

.S-YMTary of S02 lnterfernce Check 

Plant 4 Scrubber 

Monitor: 'Western Researcf ~ 721--AT 

21 3 

Monitor S02, ppm 01 ol 10 

Modified Method 6 §—Of'! L ol 01 0 

% Difference 1 01 i 0! 0 

284 

Page 1 
Sulfur Dioxide Barium-Thorin Analysis 

Plant: Daltile. Dallas, TX 

Location: Plant #4 ScrubSer 

Date: 10•Jul•03 

Standardization Ba (C102)4 

Titration (mis) Avg. Titration (mis) 

10.5 

Blank Titration (mis) Avg. Bfank (mis) 

0.1 

Vofume of Standard Sulfuric Acid (mis) 

Normality of Standard Sulfuric Acid b:1: 

Normality, 0.009524 

Aliquot' Average 

Run # Location Volume Dilution Volume Titration Titration 

(m!s) (rnls) (mis) (mIs) (mis) 

1 I m ..~~,~, 

P 1•2 ~~ : : ~ ~:: 

_~ :~ 0.1 

2 Iml' I 2 0.1 

..:~ ; 3 Im a 1•2 ~~ ~~: :~ ~~; ~a:~:~ ~~ :x: ~ `:v:: ~: 0 1 

Run n l.ocation Total Grams Total IYlg 

1 Imp2&3 S02 0 0.00 

2 I m p 2& 3 S02 0 0.00 

3 Imp 2& 3 S02 0 0.00 

2R5 
' + i r ..' I _ ' : 

' t_.~ , ;. : '- ~~ .. . ~_ .k..... 1.. . ~ f ~ . 1 • ( I +~ _ . ~ _.' _. ~. .; ~ ~ ~ ! '. 

. ....... . 

E ~ I~ ~ i i__ ' 1! _ ~__.... ~ ._..! .. . : .- ~ _.._ .~ . _~__..~ ~ —~`_..~

.h.. 

_I_....-_..:~ ._ i .~._.._+ ._.~._ ...' ' 1 .l.._.. i ; ~ I i _ 

; :~ 1 c_?' fr<i r:'~:~~'c,` r I .._!_ I.- : . ~ _.-i_. ~ ~ r_.`~f 

_ ~ ._. L_.. _._. ~ _ .~" : v~- 11 

I L 

AI Lb ~i__' _ ~~ _ ~C-~ ~ _ ~ r ~ ! ~ _ 

SIR- • J, 9 

_~ _.L ! _ _.»E_._ 1 ~ •— -- —•— ~ --- —• _ _. _ . 

loj 

...~_ _L—.1.. ~ — -- ~ __~ _. .~ • L. ~L.~. .~».~._. 

1-2 

.L.~1~_~....~.._ -.~ ._ ~ _ _ _ _.__~ ._.... ~_ __ _..L._ _ _ .! ~1_..~.~_I _ _~ i ~ ~ -i _ 

LL _ ._~ 

; -•--!-.•- r .~._~_ - !• _~ F 4 

~ ' i~ .l_~~~. + i . _ I -- -.._~_ _ ~~ . i- _~ , ... .. -i _!_ i ___. _.L» _ i_i __~_..~. 

__%_._.!. .. . - -~,__. -. j _»-_,-._ _»._L___ _. ll _ ._ » .~..-_._ ..l_._ ~~___~~_I..__•~..~ _(~...~i~_» i___. _ •~ __i_._...~.~ ' .L..__i_._.i ._ 

I ~._L_ 

I L 

Li ! ~ ~ i fi 1 I j ! r ~ c :. 

. i _~ _-..~ ._.. _ 1 _ 

-.1 L 

I —J 

_.'• 

L--.-" L 

.. ~.._....~ .._.. ' .. ~ . .. ~ .... ..~ .... .1__... ~ .» _ ~-_.....j......i_._.... r . .. ~ ,.._..~ ..._...!_........ ~ ....__.L.... » ~ .«._l...__. E . ».L._.. ~ ...__i_.__..;_..._1_.._ €..». ! --- { ~ - ~ »- ~ - _ _-- ~ -•--1 •rf--- ~-- 

1 

LL 
EIViI5SiON TEST SUIViMARY 

PLANT : Daitil ~ , Dallzs, TX 

DATE : 9•Jui-03 

PLACE : Plant 4 Scrubber 

RUN# : 1 

TEST DURATION (NIINUTES) : 60 L1QU(D COLLEC T ED (mis) : 0 

NOZZLE DIAMETER (INCH.) : 0 S02 Sample 1Neight, mg: 0 

METER COEFFICIENT (Y) : 0.944 0 

PITOT COEFFICIENT (Cp) : 0 STATIC PRESSURE (in. H20) : 0 

GAS METER VOL.(Cu.Ft.) : 1.818 PERCENT CO2 : 0 

BAROMETRIC PRESSURE ; 29.5 PERCENT 02 0 

PERCENT CO : 0 

FLowS 

SAMPLED VOLUME (S T D. CU.FT.): 1.6737 

S02, ppm: 0.0000 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 0 0.00 72 72 

2 0 72 72 

3 0 72 72 

4 0 73 73 

5 0 73 73 

6 0 73 73 

7 0 73 73 

8 0 74 74 

9 0 75 75 

10 0 75 75 

11 0 75 75 

12 0 76 76 

#DIV/0! 0.0000 0.0000 73.5833 73.5833 73.5833 

2R7. 
EMISSlON TEST SUMMARY 

?LANT : Da ~~ iie, Da'las, TX 

DATE : 9-Ju1-03 

PLACE : Plan ~ 4 Sct•ubber 

RUNn : 2 

TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 0 

NOZZLE DIAMETER (INCH.) : 0 S02 Sam'ple Weight, mg: 0 

METER COEFFICIEN T(Y) : 0.944 0 

P1TOT COEFFIC(ENT (Cp) : 0 STATIC PRESSURE (in. H20) : 0 

GAS METER VOL.(Cu.Ft.) : 1.843 PERCENT CO2 : 0 

3AROMETRIC PRESSURE : 29.5 PERCENT 02 : 0 

PERCENT CO 0 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 1.6694 

S02, ppm: 0.0000 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F I N L LET OUTLET 

1 0 0.00 82 82 

2 0 81 81 

3 0 81 81 

4 0 82 82 

6 0 82 82 

6 0 82 82 

7 0 82 82 

8 0 83 83 

9 0 83 83 

10 0 83 83 

11 0 83 83 

12 0 84 84 

#DIV/0! 0.0000 0.0000 82.3333 82.3333 82.3333 

~ 
EMISSION TEST SUMN[ARY 

PLANT : Daitiie, Dailas, TX 

DATE : 9-Ju1-03 

PLACE : Plant 4 Scrubber 

RUN# : 3 

TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 0 

NOZZLE DIAMETER (INCH.) : 0 S02 Sample Vl/eigh#, mg: 0 

METER COEFFICIENT (Y) : 0.944 0 

PITOT COEFFICIENT (Cp) : 0 STATIC PRESSURE (in. H20) : 0 

GAS METER VOL.(Cu.Ft.) : 1.857 PERCENT CO2 : 0 

BAROMETRIC PRES'SURE : 29.5 PERCENT 02 : 0 

PERCENT CO : 0 

FL01NS 

SAMPLED VOLUME (STD. CU .FT.): 1.6818 

S02, ppm: 0.0000 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 0 0.00' 86 86 

2 0 8-3 83 

3 0 82 82 

4 0 82 82 

5 0 82 82 

6 0 82 82 

7 0 82 82 

8 0 82 82 

9 0 82 82 

10 0 82 82 

11 0 82 82 

12 0 82 82 

#DIV/0! 0.0000 0.0000 82.4167 82.4167 82.4167 

28.9 
} ' FIELD D ATA 

PL ANT: 

DAi.: -•_ 1' ~ . ._ ~ ~~ ~ ~~ 

REFETITION: 

LOCATION (aOURCE r): ~~1~,~~~- r~ 

~ 

~,~,f ~J ~~ ~f ~~ INEPIsti GERS 

OPERATOR: ~'~~ ~T'r' ~.. ~ Initial Final 

SANPLE TrZAIN ~: ~~; j }~,.~.~ F r :q1 

METER BOX r: -'-~ J i~2 

B AROMET2IC'PRESSURE: '~= ~

) c 

AMBIENT TEMPERA i iJRE:. ',72.— ~ _ I ~ 01'4 

ASSUINIED MOIS'ru-RE: - -u 5 

PROBE LENGTH: —": o Z — 1 -7 =b 

NOZZLE DL4h'IETER: ~ 

STACK D~TER: 

ME•TER~ H: ~ . . ;. .. 

CO2 02 

, 

C S'ACTOR: 

METER CO-EF'FICIEN'I': 

FILTER TARE: ' 

PRE-TEST LE.4K CHECK POST-TEST LEA,B'. CHECh'.. 

Ivieter: cu.ft. @ in. HG 

, Meter: Q. © cu.ft. @ in. HG 

~;rn+ n . ;,, TJ7n•: Fitntv (Q~. 'in. x20 

,~st~ii~'"~' 

3 ~~ zes ~ ~-~ _ ~e`i

. 

3~ 

~c'" _ie. :y 

t ' ~ -"' ~. _. 

,. ~t 

. ~ 

`Fi~. '~' 

a, ~ux•~~'~~~~ 

• 

. u ~'et .~~. 

,~ ~ 

u c ' ~cm. 

m 

Txsno " 

~• 

a 

.t .~ ~ ~ ~ • . . ~ . ! ~~~ ~ . ~~ • ~ ~. i . 

f I 

~ ,, I 

J 

! 

' 7 z 

?~h' ~ o' ~ ~3.. i 

f

:..~ 

t~ ► ~;.:~ 

-~~:~.,~,~ . . , i ~ 

Z 

~ 

~~ 

~ 

r ~~ . ° u ~~~~n. I r~~~ • ~ 3. ~~ : I ~ ~ ! I 

/. i 

.)!1' ;; ~ F ✓~ ~~ i 16 Lr i Y ~ ! • I 

. ~~ 

,. M:1~~ ; c~~ • ~3~ o •, ~ i 

17 (!' n 

, 

~ s 10 :~ , '. . ! , l 

1 

✓ ~ Y `7 

~ !•~ . f ~ ~• i ~ i G l ~ ~ ~ ' ! ~ I 

1 i i I 1 i l i I 

I ~ ! ! I • i 

' I I I I I 1 ! . I•• 1 i 1 I 

j~ I I i ' I I i ~ I.► 

~ I i I I i ! I l I• I I 

290 _ 
, FIELD DATa 

PLANT: 

, 

DATi: 

REPETITION: vLOCATION (SOURCE =): 5;0-Z 

OPERA?'OR: ( r'~ 

S Q.MPLE TR.AIN r: — 

Iv~TF,R BOX ;~ : --- ~ 

B AR0METRIC PRESSURE:2--~7 ✓5 

AIvIB1~'T TEiVL'ERAn-RE: 

ASSUMED MOISTt3RE: 

PROBE LENGTH: 

NOZZLE DL3..METER: 

STACK DL~..~VIETER: 

METER H: 

C FACTOR: 

METER CO-EFFICIENT: 

FILTER T.4RE: 

PRE-TEST LEAK CHECK 

Meter: cu.ft. @ in. HG 

Pitots: A in. H20 

nfFRi GERS 

I7utial Fir.al =I 

~ 

~

r. 4 

s2) 

:-6 

CO2 02 

POST-TEST LEAK CHECK 

Meter: cu.ft. @ in. HG 

Pit.ots: A in. 17D0 

~

~t.+; S"'.rty_.:~ 

?'.1 ~:,~~=~`~~ 

'CvlC~ , ~.~i •n~ .~-..a. 

~.+w+~•'Kiy~'•'~r~:~5~ ` ~lI'~.

.~ i ', i+°~ itl:'..f`(%y~ t•.N_~`.~ "1.

C~' `a^` 

t7.i'~~~~~ 

~'_ D .:vkr ~ ~ '"'''. ~''- ~~x 11~•~..'..' ••~"I..P p~~ 

'^•i + ~h~.•~ `.Ai..~

-•'

. . ' ..4 

~

" ..~"t~~~,", 

f ~~~? ~'.~i.~lsi:K,,. 

~ 1 Yl+"c.'.•,~'".. 

,,~t~ rs y~vr 

~T i~ 

.3b' 

: ~ 

.3~U \~` ..>~Iei±i:.F 

~ fi~: ~~ 

.~'

~ .e _'~ii .• 

_ '.ti'. 

, ~-. \~ 

r o ~ 'SnZ.=;^_"' 

~ ra,1'~?~~'~~~] 

r~N . ~y-•! 

~` 

'i: _ ~~'T~

''•`''

~~~ . ~+~Z'^S 

•_fi~l:4A i~,~ ;'* ry _ 

. ».~ yynj L~ ~ ~{S I _ 

I • I 

~ ~ _~ • 

1 ~ 

I ~ • ~ 

. . ~ I (~ 

_ 

~ 

~ 

/ 
FEELr,D DATA. 

~~ ~~~r I ~ 

Da ~~,: : '' ~ ~ ~~' 

....~... ;. ~. ~ 3 

LOCATiON (SOliRCE =): Ran~ ~ a:~t1` ~ ~✓~~ ~~ 

0?ER.ATOR: Tv 

SA.~v= TRAIlNT 

ME= BOX 

B AROMETRIC PRESSTIRE: 

qMBIENT TEMPER.ATURE: 

ASSU1\4ED MOISTURE: 

PROBE LENGTH: 

NOZZLE DIAMETER: 

STACI{ DL4IYIETER: 

METER H: 

C FACTOR 

METER CO-EFFICIEINT: 

FILTER TARE : 

PRE-TEST LEAK CHECH 

Meter: cu.f:. @ in. HG 

Pitots: na, in. H20 

]MPL~ GERS 

Initial Final 

T~ 

T~ 

^6 

CO2 02 

POST-TEST LEAK CT3ECK 

Meter: cu.ft. @ in. HG 

r itots: na, il-i. H20 

i~r^..J ~F ,,.• 7r ,~ ~ • • , •-: ¢ 

, iN i f ~ »r., ..t• *~ 

 ,~., ~ 

~ s 

•~'~+G~ V~'"i 

.;k. 

k~(~ p-~~~~ 'GWD 

zr•. ~,~ ~y 

Y,Y. L`~•„ 

T' ,[l,.` Y.. •-~~'"~ 

ic .~ 

~~' 

D - ~ ~, ~~ L;••'- 

' 9 i x c.. •S~~ ~`. ~1 w ~ ~°S~iT .s_-:-7``q"`t"~

r"';' 

~')'. ~`. ~ ~~.

R.• ~ S`v „ ~• !f' O ~ .. ~ ~~~ ~ ~ • ;.. 1 ~; ~^ 7a `'w`w-,~ 1~ +.z ~ 

.. 1-. ,• +%~i .~f y," 

 ~ 

b,V" WE

~r'., p.Y••e 

~ 

/ ~_~ ~ • • ~ 

~ - 

_ 

• 4 

• 

~ 

i I 

• 

E21 
------ ORIFICE 

CALIBRATION FACTOR 

dH Q 

Value Variation 

(in H20) (in 1-120) 

0.000 0.0000 

0.000 0.000 

0.000 0.000 

0.000 <------ Average dl -tQ 

Arrnstrong Envirorntnental Inc. 

EPA Melliod G 

OriGce Melhod 

Cnglislt Meler Box Unils, Eriglisli K' Factor 

;ox r Dry Gas Meler Date: -------- ------ ---------- > July 11, 2003 

3909 l3aromeliic Pressure: ----------> 29.78 

flteorelical Critical Vacutan:---> 13.91 (in. (-Ig) 

CONVERSION FAC 1'(}RS 

1 rnnt Hg : 0.13330 kPa 

1 cin = 0.39370 incii 

t mrn ¢ 0.03937 inch 

1 cu 1t - 28.32 liters 

TAP For valid lest resuils, the Actual Vacuum should be 1 lo 2 in. 1-19 greater Itian ltie Theorelical Crilicai Vacuurn sliown above. 

TAf~ The Critical Oritice Coef(icient, K', must be entered in Englislt units, (1t)"3'(deg R)"0.51((in.Hg)'(min)). 

---------------- DRY GAS METER READINGS ---------------- -CRITICAL ORIFICE READINGSTheorelical Crilical Vacuum:---> 14.05 (in. Hg) 

Voluine Volume Volurrne Initial Temps. Flnal Teinps. Orifice IC Orifice Actual -- Ambient Temperalure -- DGM DGM Anibierrt 

Time Initial Final Tolal lniel Oullet Inlet Outlel Serial# Coetficient Vactluttt Initial Final Average Oullet Overall Temp 

) (rnin) (cu (t) (cu 10 (cu fl) (deg F) (deg F) (deg F) (deg F) (number) (see above) (in Hg) (deg F) (deg F) (deg F) (deg R) (deg R) (deg R) 

.00 5.00 16.7161G.917 0.201 87.0 87.0 87.0 87.0 16907 0.029 23.0 87.0 87,0 87.0 547.0 547.0 547.0 

.00 5.00 16.917 17.118 0.201 87.0 87.0 87.0 87.0 - 16907 0.029 23.0 87.0 87.0 87.0 547.0 547.0 547.0 

.00 5.00 17.118 17.320 0.202 87.0 87.0 87.0 87.0 16907 0.029 19.5 87.0 87.0 87.0 547.0 547.0 547.0 

. .......................................... RESULTS uN.w...A...A..AA.A........w......u..uAAA.aw...A 

GAS METER --- --------- ORIFICE --------- - - DRY GAS METER -- 

IF_ VOLUME VOLUME VOLUME VOLUME CALIBRATION FACTOR 

:CT CORRECTED CORRECT CORRECT NOMINAL Y 

:td) Vm(std) Vcr(st(l) Vcr(sld) Vcr Value Variatiorn 

i (t) (lilers) (cu ft) (liters) (cu ft) (number) (nurrnber) 

93 0.0 0.182 0.0 0.190 0.945 0.002 

93 0.0 0.182 0.0 0.190 0.945 0.002 

9d 0.0 0.182 0.0 0.190 0.941 -0.003 

Average Y ----- --> 0.944 

or Calibralion Factor Y. lhe ralio of lhe reading of the calibralion rneler to the dry gas rneter, 

eptable lolerance of individual valties from the average is +-0.02. 

Oririce Catibralion Faclor dHQ, Ihe orifice difJerenl'aI pre sure in inches of H20 that equates to 0.75 cfm of air 

:8 F and 29.92 inches oi Hg, accepla e-tdlerance~f i ividual v'lues frorn lhe average is'+-0.2. , 

SIGNED: ~!~ 

~ ~ 

 1~ t J ~ ~ Dale: ~~ , 11 U ~ 

i ~ 

~ 

W 
C APEX INSTRUMENTS VUA ORIFICE ADAPTER CAI,IBRATION 

C ,librallon Intormalion 

WTM Modet Number At.17 

iWTM Serial rlvnibcr _ 16907 

IIWTM Canrar>:r 1.00000 

Faclors/Converstons 

Sld Temp 293 t~ 

Sld Press 760.00 nun I ig 

t(t 0.306 Klotut tiy 

Callbrallort ConJitlons 

Uale I -rime 07/10/03 16:30 

Baronictric Prassure 749.0 nunt li0 

Tlieorellcal Critical Vacuum' 353.5 mm Fig 

Calibrallon Tecltnlcian RM 

'Thc Crilical Uriflee COciticianl, W. Itt rnglish usiits, (1ta '°R"'jl(irr.Hy'min). 

`The Critical Oritice Coefficient, K', in Metric units, (L9CU(rnrnily'rrtln). HOTE: VOLUME IN LITER$ 

Calibration Oata Results 

_ Wel Test Meler VUAAdaptcr 

Run a Orilice 

Serialq 

Run Tlme 

Elapsed 

Volunm 

4+ilial 

Voiume 

Flrral 

Voiume 

Tolal 

Temperalwo 

Initlal 

Temperature 

Final 

Amb Tomp 

Inival 

Amb Temp 

Finai 

Aclual 

Vaeuum 

Coettictent 

Metric Unils - 

Coefticlarnt 

Englisit Units 

% Varialion 

rroorr Avg 

_ (Ur— (VI+) IVMr) (V.) (1.+) (t.r1 (1 .40 (1-"0) K' IC (<0.51,6) 

min L L L °C 'C 'C 'C mnt IHg see above' see above % 

1 K4-14-03 G 1 306.025 312.500 6.475 30 30 29 29 597 0.0239 2.871E-02 0.17 

2 K4-14-03 G 312.500 316.960 6.460 30 1 30 29 20 610 0.0230 2.063E-02 -0.11 

3 K4-14-03 6 310.960 325.420 6.460 30 30 29 30 610 0.0230 2.064E-02 _0.06 

0.0238 2.066E-02 

IEquation lo Calculate.Standardized Flowrate ^ ~ 

I (Given Ambient Barornetric'Pressure and Absolute 

'rernperalure Conditlons: Pbar & TarntKabs)): 

Qcr(sld)=K-

, * 

Pbar/Tamb(abs) 

ziz 

I cerlily lliat orilice set number /C ~ Z1–•1'<1~'62~fJ ' was tesled in accordance willh Ilte US EPA Melbod 5 standards. 

Sxa tttc Coc:e ol Feclorao,

'

ulititions, litie 40, part 60; Ahpendix A. Meilltod ' 5, Item 7.2. 

Signaturq 

I 

~ 

~ 

_ 1~ 
... .___—....- _ . . .. . .. . . . . . , , . , . , L . : . . . .- . .. ~ ~ _ ; . ..- . . _.. .. . i ,. . ..- _ i- . __ . • _ . 

'~. r . . • . . , i ~ . • i i . ' . ~ . . ~ . . i . . ~ , , ~ . i . 

~. _ .,. 

r ~ ~ ~ + ~ ..~. 

! • I - -- . . .;- -h-•- 

i

~ (- , ; ~'i'~ ;~:~ , - 

----Lr-' r ~ G- ` , -- . _.. _-•-- 

' ~ _ _ ` 

.i _ , 

;... ~ ._ ~ _ . !. ~ _ 

i- -; 

i : . . .!- . ; i 

.....~.... 

- _ 

' .. . _ 

~ y"' ,~ '~'~, 

. I ` . --'t- ;_ .~ ... - --- ! / 

s '_ . 

. _ r . ~ • ;- -;._ 

~I _ _ ~! ._. .' _ -i ~ 

~. . _1 , , ,..__. 

.. .r .._ ~~~_~ _._i. . 

. ., ~~.~ ''~ 

_ . __ ~-• .. ~ .__.~~ i i. 

+ . _ .~_. .~_ . i . . ~ 'E ! - j t ~ _ .__ ..._ ~ _ _,...._~ _. .. ___ ~ -.- - - ~ ,• - =--- =- •~ . ..._.. . 

: -~ -f j , ~'•`'~ ~~1"-~-~:---.: t_ ., 

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Sheet1 

Summary of Sulfur Dioxide Analyzer Calibrations and Bias 

Plant: Daltile 

Source: Plant 4 Scrubber 

Date: 719103 

Analyzer Calibratrion Data 

Cyiinder Analyzer Absolute % Span 

Value Response Difference 

Zero Gas 0 0.15 0.15 0.25 

Mid Range 25.7 25.7 0 0 

High Range 50.7 50.65 -0.05 -0.08333 

System Calibration Bias and Drift Data 

Analyzer Initiai Values Final Values Drift Average 

Caiibration System System System System Calibration 

Response Caiibration Calibration Calibration Calibration Values 

Response Bias Response Bias 

Run #1 Zero Gas 0.15 0.98 0.005 0.23 0.133333 0.083333 0.205 

Upscale 25.7 24.85 -0.14167 23.53 -3.61667 -2.2 24.19 

Average S02 Concentration: 0.17 

Corrected S02 Concentration: -0.0375 

(cquation 6C-1) 

Run 92 Zero Gas 0.15 0.23 0.013333 -0.13 -0.46667 -0.6 0.05 

Upscale 25.7 23.53 -0.36167 23.9 -3 0.616667 23.715 

Average S02 Concentration: -0.13 

Corrected S02 Concentration: -0.19548 

(Equation 6C-1) 

Run #3 Zero Gas 0.15 -0.13 -0.04667 -0.05 -0.33333 0.133333 -0.09 

Upscale 25.7 23.9 -0.3 23.5 -3.66667 -0.66667 23.7 

Average S02 Concentration: -0.1 

Corrected S02 Concentration: -0.0108 

(Equation 6C-1) 

Q Page 1 ~ 26 
7110103 Calii7ratfons 

Datei7irne CO S02 

^tm/ddlyy n~ :mt

~ :ss ppm pprn 

07109103 Oa:33:3: 0.1 0.2 

07109103 03:33:45 0.1 E1.2 Zera IN12 

07109/03 09:33:55 0.0 0.1 

07/09/03 09:34:05 0.1 0.1 

07/09/03 09:34:15 0.1 30.2 

07109/03 09:34•

~5 0.1 35.5 

07/09/03 09:34:35 0.1 43.2 

07109/03 09:34:45 0.0 47.1 

07/09/03 09:34:55 -0.3 47.8 

07/09/03 09:35:05 -0.3 48.3 

07109103 09:35:15 -0.4 48.8 

07/09103 09:35:25 -0.3 49.1 

07/09/03 09:35:35 -0.4 49.4 

07/09/03 093S:45 -0.4 49.6 

07109/03 09:35:55 -0.2 49.7 

07/09/03 09:36:05 -0.3 49.9 

07/09103 09:36:15 -0.2 50.1 

07109/03 09:36:25 -0.2 50.1 

07109103 09:36:35 -0.2 50.1 

07/09/03 09:36:45 -0.2 50.2 

07/09/03 09:36:55 -0.1 50.3 

07/09/03 09:37:05 -0.1 50.5 

07/09/03 09:37:15 -0.1 50.4 

07/09/03 09:37:25 -0.1 50.6 

07/09/03 09:37:35 -0.1 50,6 

07/09103 09:37:45 -0.2 50.6 

07/09/03 09:37:55 -0.3 50.7 50.7 ppm S02 

07/09103 0938:05 -0.2 50.7 

07/09103 09:38:15 -0.3 50.6 

07J09/03 09:38:25 -0.3 50.7 

07109/03 09:38:35 -0.3 50.6 

07109103 09:38:45 -0.1 50.0 

07/09/03 09:38:65 -0.2 47.9 

07/09103 09:39:OS 0.0 43.5 

07/09/03 09:39:15 0.0 37.7 

07/09/03 09:39:25 0.0 31.6 

07/09/03 09:39:35 0.0 26.4 

07/09/03 09:39:45 0.1 22.5 

07/09103 09:39:55 0.1 19.5 

07/09/03 09:40:05 0.1 17.0 

07109/03 09:40:15 -0.1 15.5 

07/09/03 09:40:25 -0.1 15.0 

07/09103 09:40:3S -0.1 15.1 

07/09/03 09:40:45 -0.2 15.7 

07/09103 09:40:55 0.0 16.6 

07/09!03 09:41:05 -0.1 17.5 

07/09/03 09:41:1 5 -0.2 18.4 

07/09/03 09:41:25 -0.1 19.3 

07/09/03 09:41:35 -0.2 20.2 

07/09/03 09:41:45 -0.1 21.0 

07I09/03 09:41:55 -0.3 21.4 

07/09/03 09:42:05 -0.2 22.0 

07/09/03 09:42:15 -0.2 22.6 

07/09/03 09:42:25 -0.2 23.1 

07/09/03 09:42:35 -0.2 23.6 

07/09/03 09:42:45 -0.1 24.0 

07/09/03 09:42:55 0.0 24.3 

07/09/03 09:43:05 0.1 24.5 

07/09/03 09:43:1 5 0.1 24.7 

07109/03 09:43:25 0.1 24.8 

07109/03 09:43:35 0.2 24.9 

07/09/03 09:43:45 0.3 25.0 

07/09/03 09:43 :55 0.2 25.2 

07/09/03 09:44:05 0.0 25.3 

07/09/03 09:44:15 0.1 25.4 

07J09/03 09:44:25 0.2 25.5 

07/09/03 09:44:35 0.4 25:6 

07/na103 09:44:45 0.2 23.7 

07/09/03 09:44:55 0.2 25.7 25.7 pprn S02 

07/09/03 09:45:05 0.2 25.7 

Page1 

~ 

~~ 7 
711 0703 Caf, bsafions 

07/09/03 09:45:15 0.2 25.7 

07/09103 09:45:25 0.3 25.7 

07/09103 09:45:35 0.3 26.5 

07109!03 09:45:45 0.2 25.6 

07/09/03 09:45:55 0.2 25.6 

07109J03 09:46:05 0.2 25.6 

07/09/03 09:46:15 0.2 25.5 

07109/03 09:46:25 0.1 25.5 

07/09103 09:46:35 0.0 25.2 

07/09/03 09:46:45 0.1 24.6 

07/09/03 09:46:55 0.2 23.2 

07109103 09:47:05 0.1 21.3 

07109/03 09:47:15 0.3 19.3 

07109/03 09:47:25 0.3 17.5 

07/09103 09:47:35 0.3 15.8 

07/09/03 09:47:45 0.3 14.3 

07/09103 09:47:55 0.2 12.9 

07/09iO3 09:48:05 0.3 11.5 

07/09/03 09:48:15 0.3 10.5 

07/09/03 09:48:25 0.3 9.6 

07/09/03 09:48:35 0.2 8.7 

07/09/03 09:48:45 0.3 7.8 

07/09/03 09:48:55 0.2 7.2 

07/09/03 09:49:05 0.2 6.8 

07109/03 09:49:15 0.2 6.3 

07/09103 09:49:25 0.2 5.8 

07/09103 09:49:35 0.2 5.3 

07109f03 09:49:45 0.2 4.9 

07/09/03 09:49:55 0.2 4.5 

07/09103 09:50:05 0.1 4.1 

07109/03 09:S0:15 0.1 3.8 

07109J03 09:50:25 0.2 3.6 

07109103 09:50:35 0.0 3.3 

07/09/03 09:50:45 0,0 3.1 

07109/03 09:50:55 0.1 3.0 

07109103 09:51:C5 0.1 2.9 

07109103 09:51:15 0.0 2.8 

07109103 09:51:25 0.2 2.7 

07109103 09:51:35 0.0 2.3 

07/09103 09:51:45 0.1 2.1 

07/09/03 09:51:65 0.1 2:0 

07/09/03 09:52:C5 0.1 1.9 

07/09/03 09:52:15 0.1 1.9 

07109J03 09:52:25 0.1 1.8 

07109103 09:52:35 0.2 1.7 

07/09/Gt3 09:52:45 0.3 1.6 

07/09/03 09:52:55 0.3 1.5 

07r09/03 09:53:05 0.3 1.4 

07/09/03 09:53:15 0.3 1.4 

07/09/03 09:53:25 0.2 1.3 

07/09/03 09:53:35 0.3 1.2 

07109l03 09:53:45 0.2 1.1 

07/09/03 09:53:55 0.2 1.2 

07/09103 09:54:05 0.2 1.2 

07/09/03 09:54:1 5 0.2 1.1 

07109/03 09:64:25 0.1 1.0 

07/09103 09:54:35 0.1 0.9 

07/09/03 09:54:45 0.0 0.5 

07109/03 09:54:65 0.0 0.3 

07109/03 09:55:05 0.0 0.2 

07109103 04:53:15 -0.1 0.2 

07/09/03 09:55:25 0.0 0.2 

07/09/03 09:55_35 0.0 0.1 

07/09103 09:55:45 -0.1 1.8 

07/09103 09:55:55 0.0 3.1 

O~ rrJ9x~ o n0•SS.nc 

1 1 1 vJ V

~ . .V J 

M. 4 

-v 1 4.7 

07/09/03 09:56:15 -0.2 6.7 

07/09/03 09:65:25 -0.1 8•7 

071,,91n3 09:56:35 -0.1 10.7 

07109103 09:56:4 5 -0.1 12.6 

071J9103 09:55:5 5 -0.1 14.2 

07,101o;03 09:57:05 0.0 15.6 

07139103 09:5;' : i S 0.0 15.9 

Zero Bias 

Page 2 

~ P 
7110103 Calib,-atior.s 

07/09103 09:57:25 0.0 18.0 

07/09103 09:57:35 0.1 19.1 

07J09/03 09:57:45 0.0 20.0 

07/09103 09:57:55 0.1 20.7 

07/09/03 09:58:05 0.2 Z1.2 

07/09/03 09:58:15 0.1 21.8 

07/09/03 09:58:25 0.1 22.3 

07/09103 09:58:35 0.0 22.8 

07/09/03 09:58:45 0.1 23.1 

07109103 09:58:55 0.1 23.5 

07/09/03 09:59:05 0.1 23.7 

07/09103 09:59:15 0.0 24.0 

07/09/03 09:59:25 -0.2 24.2 

07/09103 09:59:35 -0.2 24.4 

07/09/03 09:59:45 -0.3 24.5 

07109/03 09:59:55 -0.2 24.5 

07109/0310:00:05 -0.3 24.6 

07/0910310:00:15 -0.2 24.7 

07/09J0310:00:25 -0.1 24.8 

07/0910310:00:35 -0.1 24.8 

07/0910310:00:45 -0.1 24.8 

07/0910310:00:55 -0.2 24.9 

07/09/0310:01:05 -0.3 25.0 

07/0910310:01:15 -0.3 24.8 

07109/0310:09:25 -0.1 24.7 

0710910310:09:35 -0.1 24.7 

07/0910310:01:45 -0.2 24.8 

07109/0310:01:55 -0.2 24.8 

0710910310:02:05 -0.4 24.9 

0710910310:02:15 -0.4 24.9 

0710910310:02:25 -0.2 24.9 

07/09/0310:02:35 -0.1 24.7 

07/0910310:02:45 0.1 23.9 

07/09/0310:02:55 0.2 22.6 

0710910310:03:05 0.1 21.0 

07J0910310:03:15 0.1 18.9 

07/09/0310:03:25 0.1 17.0 

07/0910310:03:35 0.1 15.4 

07/0910310:03:45 0.1 14.2 

07/0910310:03:55 0.0 13.1 

07/0910310:04:05 0.0 12.1 

07/0910310:04:15 0.1 11.2 

07/0910310:04:25 0.0 10.5 

07/09/0310:04:35 0.0 9.7 

07/09/0310:04:45 0.1 9.1 

07/09/0310:04:55 0.1 8.4 

0710910310:05:05 0.0 7.7 

07109/0310:05:15 0.0 7.2 

07/0910310:05:25 0.1 7.0 

07/0910310:05:35 0.0 6.5 

07/09/0310:05:45 0.0 6.1 

07/09/0310:05:55 0.0 5.8 

07/09/0310:06:05 -0.1 5.5 

07109103 10:06:15 0.1 5.1 

07109/0310:06:25 0.0 4.8 

07109/0310:06:35 0.0 4.5 

07/0910310:06:45 0.0 4.3 

07109/0310:06:55 0.0 4.0 

07/09/0310:07:05 0.0 3.8 

07/0910310:07:15 0:0 3.6 

07/0910310:07:25 0.0 3.5 

07109103 10:07 :36 0.1 3.5 

07/09/0310:07:45 0.2 3.3 

07/09/0310:07:55 0.2 3.2 

071091e310:08:05 0.0 3.1 

07/0910310:08:15 0.0 3.0 

0710910310:08:25 -0.1 2.9 

25.7 ppm $02 Bias 

Paae 3 

~ 2g9 
7110/03 Run #1 

Date!?ime CO S02 

mcrsldd'Yp• hh:mm:ss p2m, purn 

07/09/03 10:11:55 0. ; 1.1 

07/0910310:12:05 0.1 1.1 

07109103 10:12: •. 5 0.9 1.0 

07/0910310:12:25 3.7 1.0 

0710910310:12:35 6.8 1.0 

0710910310:12:45 9.2 1.0 

07/09/03 10:12:55 10.8 1.0 

07109/0310:13:05 11.7 0.9 

07/09l03 111: IJ:15 I2.8 V.7 

07/09/0310:13:25 13.7 0.8 

07/09/0310:13:35 14.5 0.8 

07/09/0310:13:45 15.3 0.8 

07109/0310:13:55 16.0 0.8 

07/09/0310:14:05 16.5 0.8 

07/09/0310:14:13 16.5 0.7 

07/0910310:14:25 16.7 0.7 

07/0910310:14:35 17.0 0.7 

07/09/03 10:14:45 17.1 0.7 

07/0910310:14:55 17.2 0.7 

07/09/0310:15:05 17.2 0.7 

Start Run #1 

07/09/0310:15:15 17.0 0.7 

07109103 10:15:25 17.0 0.7 

0 7/09/ 0 3 10 :15: 3 5 17.1 0.6 

07/09/03 10:15:45 17.2 0.5 

07109/0310:15:55 17.5 0.6 

07/09/0310:16:05 17.6 0.7 

07/0910310:16:15 17.5 0.8 

07/09103 10:16:25 17.5 0.6 

07/09/0310:16:35 17.3 0.6 

07109/0310:16:45 17.3 0.6 

07109/03 10:16:55 17.1 0.5 

0710910310:17:05 17.1' 0.5 

07109103 10:17:15 17.3 0.4 

07109103 10:17:25 17.4 0.4 

07/09103 10:17:35 17.5 0.4 

07/0910310:17:45 17.2 0.4 

07/09/0310:17:55 17.1 0.5 

07/09103 10:18:05 17.0 0.5 

07/09/03 10:18:15 17.2 0.6 

07/09/0310:18:25 17.3 0.5 

07109/0310:18:35 17.3 0.5 

07109/0310:18:45 17.6 0.3 

07109/0310:18:S5 17.7 0.3 

07/09/0310:19::5 17.7 0.3 

07109J0310:197'15 18.0 0.4 

07/09103 10:19:25 18.1 0.4 

07/09103 10:19:35 18.1 0.3 

07109/0310:19:45 18.3 0.3 

07109/0310:19:55 18.5 0.2 

07109/0310:20:05 18.4 0.2 

07/09/0310:20:15 18.2 0.2 

07/09/03 10:20:25 18.1 0.2 

07/0910310:20:35 17.9 0.3 

07/0910310:20:45 17.8 0.3 

07/0910310:20:55 17.6 0.4 

07109/0310:21:05 17.5 0.3 

07/0910310:21:15 17.3 0.3 

07/09/0310:21:25 17.3 0.3 

07/09103 10:21:35 17.3 0.3 

07/0910310:21:46 17.4 0.4 

07109/0310:21:55 17.4 0.4 

07/09/0.310:22:05 17.4 0.3 

07109/03 10:22:15 17.4 0.2 

0710910310:22:25 17.6 0.2 

07/0910310:22:35 17.8 0.2 

07/0910310:22:45 17.9 0.3 

07i0910310:22:55 18.2 0.2 

07/09,1 0310:23:05 17.9 0.3 

07/0910310:23:95 18.

11 0.3 

0710910310:23:25 18.2 0.2 

Paae 1 ~ 

300 
7110103 Run t1 

07109/0310:23:35 18.7 0.2 

0710910310:23:45 20.0 0.2 

07J0910310:23:55 20.9 0.2 

07/0310310:24:05 21.6 0.2 

07/09/0310:24:15 21.8 0.2 0~7109103 10:24:25 22.3 0.2 

0710910310:24:35 22.5 0.2 

0710910310:24:45 22.3 0.2 

07/09l0310:24:55 21.8 0:2 

07/0910310:25:05 21.2 0.2 

07/0910310:25:15 20.3 0.1 

07109J0310:25:25 19.3 0.1 

07109/0310:25:35 18.4 0.2 

07J09/0310:25: 45 18.1 0.3 

0710910310:25:55 17.8 0.4' 

07/0910310:26:05 17.7 0.4 

071091031026:15 17.6 0.3 

07/0910310:26:25 17.3 0.2 

07/09103 10:26:35 17.1 0.2 

0710910310:26:45 17.0 0.1 

07/09/0310:26:55 17.0 0.2 

07/09/0310:27:05 17.0 0.2 

0710910310:27:15 17.0 0.2 

07/0910310:27:25 16.7 0.2 

0710910310:27:3S 16.4 0.2 

0710910310:27:45 15.9 0.2 

07109/0310:27:55 15.5 0.2 

07/03/0310:28:05 15.4 0.3 

0710910310:28:15 15.3 0.2 

07/09103 1028:25 15.1 0.2 

0710910310:28:35 15.0 0.3 

07/09J0310:28:45 14.8 0.3 

07/09/0310:28:55 15.0 0.2 

0710910310:29:05 14.9 0.2 

0710910310:29:15 0.2 

07/09/0310:29:25 15.0 02 

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07/09/0310:29:45 14.9 0.2 

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07/09/03 90:30:C5 15.3 0.2 

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07/09/0310:30:25 15.5 0.2 

07/09/0310:30;35 15.5 0.2 

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07/09/0310:31:15 14.8 0.1 

07109/0310:3125 14.7 0.1 

07/09/0310:31:35 14.6 0.1 

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07/0910310:33:05 15.2 0.2 

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07/0910310:33:25 14.8 0.1 

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Page 3 ME c3 () 2 
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07l0910311:45:35 34.8 3.7 

0710910311:45:45 34.6 3.5 

07/09/0311:45:55 34.6 3.4 

07/09/0311:46:05 34.5 3.3 

07/09/0311:46:15 34.6 3.2 

07/09/0311:46:25 34.3 3.0 

07/0910311:4635 34.0 2.9 

07/0910311:46:45 34.0 2.7 

0710910311:46:55 34.1 2.6 

07109/0311:47:05 34.0 2.4 

0710910311:47:15 33.5 2.3 

07/0910311:47:25 33.3 2.1 

07109/0311:47:35 33.4 2.0 

0710910311:47:45 33.7 1.9 

07/0910311:47:55 33.8 1.8 

07/09/03 11:48:05 34.6 1.6 

07/09/0311:48:15 34.9 1.6 

07/09/0311:48:25 35.5 1.5 

07/0910311:48:35 35.6 1.5 

07/09/0311:48:45 35.9 1.4 

07/09/0311:48:85 37.4 1.4 

07/09/0311:49:05 39.9 1.3 

07109/0311:49:15 42.6 1.2 

07/0910311:49:25 44.2 1.0 

07l09/0311:49:35 45.4 1.0 

07109/0311:49:45 46.2 1.0 

07/09/0311:49:55 47.2 0.8 

Start Run 92 

0710910311:50:05 47.B 0.6 

07/0910311:50:15 47.6 0.7 

07/09/0311;50:25 47.0 0.7 

07/09/0311:50:35 45.5 0.6 

07/09/031130:45 42.8 0.5 

07/09/0311:50:55 39.5 0.5 

07/0910311:51:05 36.0 0.4 

07109/0311:51:15 32.5 0.3 

07109/0311:51:25 28.4 0.2 

07/09/0311:51:35 25.2 0.1 

07J09/0311:51:45 23.0 0.1 

07/09/0311:51:55 21.4 0.1 

07109/0311:52:05 20.6 0.0 

07109/0311:52:15 20.0 0.0 

07/09/0311:52:25 19.7 0.0 

07109/0311:52:35 19.7 0.0 

07109/0311:52:45 19.8 0.0 

07/09/03 11:52:55 19.9 0.0 

07/09/0311:53:05 19.9 -0.2 

07/0910311:53:15 19.5 -0.2 

07/0910311:53:25 18.9 -0.2 

07/09!0311:53:35 18.4 -0.2 

0710910311:53:45 18.2 -0.3 

0710910311:53:55 17.8 -0.5 

07/09/0311:54:05 17.7 -0.5 

07/0910311:54:15 17.6 -0.4 

07109/0311:54:25 17.5 -0.5 

07109/0311:54:35 17.4 -0.6 

07/09/03 11:54:45 i 7.4 -0.2 

07/09/0311:54:55 17.3 0.0 

07/0910311:55:05 17.3 -0.1 

07/09/0311:55:15 17.3 -0.1 

07/09/0311:55:25 17.2 -0.1 

0710910311:55:35 17.3 -0.1 

07109/0311:55:45 17.2 -0.1 

07/0910311:55:55 17.1 -0.1 

0710910311:55:05 17.2 -0.1 

07/09103 11:56:15 17.2 -0. i . 

07I09/0311:56;25 17.1 -0.2 

07/09!0311:55:35 17.2 -0.3 

07/09J0311:55:45 17.2 •0.2 

Page 1 

~ 

3 n v 

- 
7110103 Run x2 

0710910311:56:55 17.4 -0.2 

0710910311:57:05 "7.5 -0.3 

07/0910311:57:15 17.1 -0.3 

07/091^311:67:25 17.2 -0.3 

07/0910311:517 :35 17.1 -0.4 

07109/0311:57:45 17.3 -0.4 

07/09/0311:57:55 17.0 -0.4 

07/09/03 11:58:05 17.1 -0.4 ' 

07/09J0311:58:15 17.0 -0.4 

07/0910311:5825 16.9 -0.3 

07/09/0311:5w*:35 16.9 -0.4 

07/09/0311:58:45 17.1 -0.5 

07/0910311:58:55 172 -0.5 

07/09/0311:59:05 17.4 -0.4 

07/0910311:59:15 17.5 -0.4 

07/0910311:59:25 17.7 -0.4 

07/0910311:59:35 17.9 -0.5 

07/0910311:59:45 18.0 -0.5 

07/0910311:59:55 18.1 -0.5 

07/09/0312:00:05 17.9 -0.4 

07/09/0312:00:15 17.8 -0.4 

07/09/0312:00:25 17.7 -0.2 

07/09/0312:00:35 17.7 -0.1 

07/0910312:00:45 17.7 -0.3 

07109/0312:00:55 18.0 -02 

07109/0312:01:05 18.0 -0.1 

07 109/03 12:01:15 18.1 -0.1 

07109/0312:01:25 17.9 -0.1 

07/09/0312:01:35 17.7 -0.1 

07109/0312:01:45 17.5 -0.1 

07109/0312:01:55 17.2 -0.2 

07109/0312:02:05 17.1 -0.2 

07/09/0312:02:15 17.2 -0.2 

07109/0312:02:25 17.2 -0.2 

07/0910312:02:35 17.3 -0.2 

0710910312:02:45 17.1 -0.1 

07/09/0312:02:55 16.8 -0.1 

0710910312:03:05 16.6 -0.1 

07/09/0312:03:15 15.9 -0.1 

07/0910312:03:25 15.6 -0.2 

07/09/0312:03:35 15.3 -0.2 

07109/0312:03:45 15.1 -0.2 

07/09/0312:03:55 15.1 -0.1 

07/09/0312:04:05 15.1 -0.1 

07109/0312:04:15 15.3 -0.1 

07109/0312:04:.25 15.2 -0.1 

07/09/0312:04:35 15.3 -0.1 

07/0910312:04:45 15.3 -0.1 

07/09/0312:04:55 15.4 -0.2 

07/09/0312:05:C5 15.4 -0.2 

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07/09/0312:05:25 15.6 -0.2 

07/09/0312:05:35 15.8 -0.2 

07109/0312:05:45 15.9 -0.2 

07/09/0312:05:55 16.1 -0.1 

07/0910312:06:015 16.1 -0.2 

0710910312:06:15 16.2 -0.2 

07/09/0312:06:25 16.3 -0.1 

07/09/0312:06:35 16.5 -0.1 

07/09/0312:06:45 16.5 -0.1 

07109/0312:06:55 16.7 -0.3 

07109/0312:07:%r.1 5 16.9 -0.3 

07/0910312:07:15 17.1 -0.3 

07/0910312:07:25 17.5 -0.3 

07/09103 112:07:35 17.8 -0.3 

07109/0312:07:45 18.0 -0.2 

07/09/0312:07:5-5 18.1 -0.1 

07109103 12:08:05 18.1 -0 .2 

07/09!0312:08:15 18.1 -0.2 

07/09/0312:08:25 18.2 -0.2 

07/09/0312:08 33-5 18.5 -0.3 

07/09/0312:08:46 18.4 -0.3 

07/0910312:08:55 18.4 -0.2 

0710910312:09:05 18.3 -0.1 

Paae 2 _ ~ 
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07J09103 12:09:15 18.2 -0.2 

07/09103 12:03:25 ' 8.4 -0.2 

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1, 8.4 -0.3 

0 7 /09103 12:08:45 18.5 -0.2 

07/0910312:09:55 18.9 C.0 

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07109/03 12:10:15 18.8 0.0 

07/0910312:1

101 :25 18.5 0.0 

07/0910312:10;35 18.3 0.0 

07/0910312:10:45 18.3 0.0 

07/09/0312:10:55 18.2 -0.1 

07/0910312:11:05 18.3 0.0 

0710910312:11:15 18.3 0.0 

07109/; 3 12:11:25 18.0 0.0 

07/09/03 12:11:35 17.9 0.0 

07/09/0312:11:45 17.7 0.0 

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0710910312:12:05 17.4 -0.1 

07/0910312:12:15 17.5 -0.1 

07/09/0312:12:25 17.6 -0.1 

07/09/0312:12:35 17.8 -0.1 

07/0910312:12:45 17.9 -0.2 

0710910312:12:55 17.8 -0.1 

07/0910312:13:05 17.5 -0.1 

07/09/0312:13:15 17.5 -0.1 

07/0910312:13:25 17.5 -0.2 

07/0910312:13:35 17.8 -0.2 

07/0910312:13:45 18.1 -0.1 

07/09/0312:13:55 18.5 0.0 

07/09/0312:14:05 18.9 -0.1 

07/09/D312:14:15 18.8 -0.1 

07/09/0312:14:25 18.6 -0.1 

07109/03 12:14:35 18.2 -0. i 

07/09/03 12:14:45 18.1 0.0 

07/0910312:14:55 17.8 -0.1 

07/0910312:15:05 17.4 -0.1 

07/09/0312:15:15 17.2 -0.2 

07/0910312:15:25 17.1 -0.1 

07/0910312:16:35 17.1 -0.1 

07/09/03 1215:45 17.1 0.0 

07/09/0312:15:55 17.1 -0.1 

07109/0312:16:05 17.5 0.0 

07/09/03 12:16:15 17.7 0.0 

07/09/03 12:16:25 17.9 0.0 

0710910312,1e;a6 1710 

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07/09/D312:16:55 18.1 -0.1 

07/09J0312:17:05 18.5 -0.1 

07/09/03 12:17:15 19.3 -0.1 

07109/0312:17:25 2C.2 -0.1 

07/09/0312:17:3S 21.4 -0.1 

07/09/0312:17:45 22.8 -0.1 

07109/0312:17:55 24.1 -0.1 

07/0910312:18:05 25.4 -0.1 

07/09/03 12:18:1 S 26.7 -0.1 

07J09/0312:18:2S 27.9 -0.1 

07/09/0312:18:35 28.7 -0.1 

07/09/0312:18:45 29.3 -0.1 

07109/0312:18:55 30.0 -0.1 

07/09/03 i2:19:06 30.8 -0.1 

07/09/03 12:1 9:15 31.5 -0.2 

07109/0312:19:25 32.1 -0.2 

07109/0312:19:35 32.5 -0.1 

07/0910312:19:45 33.0 -0.1 

07/09/0312:19:55 33.0 -0.1 

07/09/031220:05 33.0 -0.1 

07/0910312:20:15 33.3 0.0 

07/09!0312:20:25 33.6 0.0 

0710910312:20:35 33.9 -0.1 

07/09103 12:20:45 34.3 0.0 

07/09/0312:20:55 

3

41.3 -0.1 

07109/0312:21:05 34.4 -0.1 

07/0910312:21:15 34.5 -0.1 

07/09/0312:21:25 34.4 -0.2 

?age 3 

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7110/03 Run tl2 

07l09103 12:21 25 34.6 -0 .2 

07/09/0312:21:45 3 "11 .8 -0.2 

07109/031221:55 34.7 -0.2 

07109!05 12:22:05 34.8 -0.3 

07/09;0312:22:15 34.9 -0.2 

07/09/0312:22:25 35.0 -0.1 

07/0910312:22:35 34.9 -0.1 

07/0910312:22:45 35.1 -0.1 

0710910312:22:55 35.0 -0.1 

0710910312:23:05 35.1 -0.2 

0710910312:23:15 35.0 -0.2 

07/0910312:23:25 35.2 -0.2 

0710910312:23:35 35.2 -0.3 

07/0910312:23:45 35.1 -0.3 

07/09/0312:23:55 34.8 -0.3 

07/09/0312:24:05 34.5 -0.2 

07109/0312:24:15 34.1 -0.1 

07/09/0312:24:25 33.9 -0.1 

0710910312:24:35 34.0 -0.2 

07/09/0312:24:45 33.8 -0.2 

07/0910312:24:55 33.6 -0.2 

07/09/031225:05 33.4 -0.3 

07/09/0312:25:15 32.9 -0.3 

07109/0312:25:25 32.3 -0.2 

07/09/031225:35 32.2 -0.2 

07/0910312:25:45 32.0 -0.2 

07/0910312:25:55 31.9 -0.3 

07/09/0312:26:05 32.1 -0.3 

07/09/0312:26:15 32.3 -0.2 

0710910312:2625 32.4 0.0 

07109/0312:26:35 32.7 0.0 

07/09/0312:26:d5 32.9 -0.1 

07/0910312:26:55 33.2 0.0 

07/0910312:27:05 33.2 0.0 

07/0910312:27:15 33.2 0.0 

07109/0312:27:25 33.1 0.0 

07J09/0312:27:35 32.7 0.0 

0710910312:27:45 32.5 0.0 

07/09/0312:27:55 32.0 -0.1 

0710910312:28:05 31.7 0.0 

07/09/0312:28:15 31.4 0.0 

07/0910312:28:25 31.3 0.0 

07/09/031228:35 31.1 -0.1 

07/09/0312:28:45 30.7 -0.1 

07/09/0312:28:55 30.0 -0.1 

07/09/0312:29:05 29.2 -0.1 

07/09/0312:29:15 28.4 -0.1 

07/0910312:29:25 27.6 -0.2 

07/09/0312:29:35 26.8 -0.2 

07/09/0312:29:45 25.8 -0.1 

07109/0312:29:55 25.1 -0.1 

07/0910312:30:05 24.4 0.0 

07/09/0312:30:15 23.8 0.0 

07109/0312:30:25 23.4 0.0 

07/09/0312:30:35 23.1 -0.1 

07109/0312:30:45 22.6 -0.1 

07/09/0312:30:55 22.4 -0.2 

0710910312:31:05 22.2 -0.1 

0710910312:31:15 22.1 -0.1 

0710910312:31:25 22.1 -0.1 

07/09/0312:31:35 21.9 -0.1 

07/09/0312:31:45 22.2 -0.1 

07109/0312:31:55 22.4 -0.2 

07109/0312:32:05 22.5 -0.2 

07/0910312.32:15 22.6 -^.1 

07/09/0312:32:25 22.9 -0.1 

07/0910312:32:35 22.9 -0.1 

07/09/0312:32:45 23.4 -0.1 

07/09/0312:32:55 24.1 -0.1 

07/0910312:33:05 24.3 -0.2 

v7/09/

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07/09/0312:33:25 25.5 -0.3 

07/09/0312:33:35 26.5 -0.2 

07109/0312:33:45 27.9 -0.2 

Pags 4 ~ 
7.j10103 Run »2 

07/09/0312:33:55 28.7 -0.1 

Q7/09/C312.s4.CIo 29.5 

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07/09/0312:34:15 33.1 -0.1 

07109/0312:34:25 30.6 -0.1 

071091Q3 12:34 :35 30.8 0.0 

07/0910312:34:45 30.7 -0.1 

07109/0312:34:55 30.4 -0.3 

0710910312:35:05 29.9 -0.2 

07/09/03 12:35:15 29.8 -0 .3 

07/0910312:35:25 30.0 -0.2 

07139/0312:35:35 30.4 - ^10.2 

0710910312:35:45 31.1 -0.2 

07J09/0312:35:55 31.4 -0.2 

07/0910312:36:05 32.1 -0.2 

07/0910312:36:15 32.6 -0.1 

07/0910312:36:25 33.1 -0.2 

07/09/0312:36:35 34.1 -0.2 

07/0910312:36:45 34.8 -0.3 

07/09/0312:36:55 35.5 -0.2 

07/09/0312:37:05 36.4 -0.2 

07/09/0312:37:15 37.1 -0.3 

07/0910312:37:25 37.4 -0.2 

07/0910312:37:35 37.4 -0.1 

07109/0312:37:45 37.3 -0.2 

0710910312:37:55 37.3 -0.3 

07/09/.1312:38:05 37.3 -0.3 

07/09/03 12:38:1 5 37.3 -0.3 

07l0910312:38:25 37.1 -0.4 

07109/0312:38:35 36.8 -0.4 

07/0910312:38:45 36.3 -0.3 

07/09/0312:38:55 36.1 -0.3 

0710910312:39:C5 36.0 -0.4 

07/09/0312:39:15 36.1 -0.3 

07/09/0312:39:25 36.3 -0.3 

07l0910312:39:35 35.3 -0.1 

07109/0312:39:45 36.2 -0.1 

07/09/0312:39:55 36.2 0.0 

07/0910312:40:05 36.4 0.0 

07109/0312:40:15 36.3 0.0 

07109/0312:40:25 36.3 0.0 

17109/0312:40:35 36.3 0.0 

07/0910312:40:45 36.2 0.0 

07109/0312:40:55 36.2 0.0 

07/09/0312:41:05 36.3 0.0 

07/09/03 12:41:15 36.3 0.0 

07/09/0312:41:25 35.9 0.0 

07109/0312:41:35 35.7 0.0 

07/0910312:41:45 35.5 -0.1 

07/09/0312:41:55 35.4 -0.1 

07109/0312:42:05 35.4 -0.1 

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07/0910312:42:25 35.2 0.0 

07/09/0312:42:35 35.1 0.0 

0 7 /09J03 12:42:45 34.9 -0.1 

07/09/0312:42:55 34.8 -0.1 

07/09/0312:43:05 34.8 -0.1 

07/09/0312:43:15 34.9 -0.1 

07/09/0312:43:25 34.8 -0.1 

07/09/0312:43:35 34.7 0.0 

07109/0312:43:45 34.4 0.0 

07109/0312:43:55 34.0 -0.1 

07/0910312:44:05 33.S -0.1 

07/09/0312:44:15 33.4 -0.1 

07109/0312:44:25 33.2 -0.1 

07,109/0312:44:35 !3.1 -0.2 

07109/0312:44:45 33.2 -0.2 

07109/0312:44:55 33.4 -0.1 

07/09/0312:45:05 33.9 -0.1 

07/09/0312:45:15 34.1 -0.2 

07109/0312:45:25 34.1 -0.2 

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07/Q9/e1 12:46:05 

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Page 5 
7110103 ??un 42 

07,'09I0312:46:15 36.2 0.0 

0710910312:45:25 37.0 -0.1 

0710910312:45:35 37.5 -0.1 

07/09/0312:46:45 3B.0 0.0 

07/0910312:46:55 38.2 0.0 

07/09/0312:47:05 38.4 0.0 

07/0910312:47:15 38.5 0.0 

0710910312:4725 38.0 0.0 

07/09/0312:4735 37.5 0.0 

07/0910312:47:45 37.5 -0.1 

07/09/0312:47:55 37.7 -0.1 

07/09/0312:48:OS 37.8 -0.1 

07/09/0312:48:15 37.6 -0.1 

07109/0312:48:25 37.5 -0.1 

07109/0312:48:35 37.6 -0.1 

07109/0312:48:45 37.4 -0.1 

0710910312:48:55 37.1 0.0 

07/09/0312:4905 36.4 -0.1 

07/0910312:49:15 36.1 0.0 

07/09/0312:4925 36.0 0.0 

07/0910312:49:35 35.7 0.0 

07/09/0312:49:45 35.3 0.0 

07/0910312:49:55 35.1 -0.1 

Stop Run 93 -0.13 

07/09/0312:50:05 35.3 -0.2 

0710910312:50:15 35.7 -0.2 

07/09/0312:50:25 35.5 -0.2 

07/0910312:50:35 35.4 0.0 

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0710910312:50:55 35.0 -0.1 

0710910312:51:05 34.9 -0.1 

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07/09/0312:51:25 35.0 -0.1 

07/0910312:51:35 34.9 -0.1 

07/0910312:51:45 34.8 -0.1 

07/09/0312:51:55 33.1 -0.1 

07109/0312:52:05 28,9 -0.1 

07/0910312:52:15 23.7 -0.1 

07/09/0312:52:25 19.4 -0.1 

07/0910312:52:35 16.7 -0.2 

07109/0312:52:45 14.1 -0.2 

07/09/0312:52:55 11.8 -0.2 

0710910312:53:05 9.8 -0.1 

07/09/03 12:53:1 5 8.4 0.0 

07109/0312:53:25 7.2 0.0 

07/0910312:53:35 6.1 -0.1 

07/0910312:53:45 5.0 0.0 

07109/0312:53:55 4.1 -0.1 

07/09/0312:54:05 3.4 -0.1 

07/0910312:54:15 2.5 -0.1 

07109/0312:54:25 1.6 -0.2 

07/09/0312:54:35 0.9 -0.1 

07109/0312:54:45 0.4 0.0 

0710910312:54:S5 0.1 0.2 

0710910312:55:05 -0.1 0.6 

07/09/03 12:55:15 1.3 

0710910312:55:25 -0.3 2.2 

07/0910312:55:35 -0.2 3.3 

07/09/0312:55:45 -0.3 4.2 

07109/0312:55:55 -0.3 5.4 

0710910312:56:05 -0.5 6.6 

07/09/0312:56:15 -0.5 7.6 

0710910312:56:25 -0.8 8.6 

07109!0312:55:35 -0.9 9.6 

07/09/03 12:56:45 -1.2 i 0.5 

07109/0312:56:55 -1.5 11.2 

0710910312:57:05 -1.4 11.9 

07/09/0312:57:15 -1.3 12.6 

07/09/0312:57:25 -1.1 13.3 

07109/3312:57 :35 -0.9 13.8 

07/09/0312:57:45 -0.9 14.2 

Zero N2 

Page 6 ~ 

313 
7110103 Run 92 

07109/0312:57:55 -0.6 14.7 

07/09103 12:58:05 -0.8 

07109/03 12:58:15 -0.9 15.4 

0710910312:5S:25 -0.3 115.9 

07109/0312:58:35 -0.8 16.3 

0710910312:58:45 -0.9 16.6 

07/0910312:S8:55 -1.2 16.9 

07109/C3 12 :59:05 -1.0 17.2 

07/0910312:59:15 -1.3 17.5 

07/0910312:59:25 -1.0 17.7 

07109/0312:59:35 -1.1 17.8 

0710910312:59:45 -0.9 18.0 

0710910312:59:55 -0.7 18.2 

07/09/0313:00:05 -0.9 18.4 

07109/0313:00:15 -0.9 18.6 

07109/0313:00:25 -1.3 18.7 

07i0910313:00:35 -1.3 18.9 

07l09/0313:00:4S -1.2 19.0 

07/0910313:00:55 -0.8 19.2 

07/09/0313:01:05 -0.7 19.3 

07/09103 13:01:15 -0.7 19.4 

0710910313:01:25 -1.0 19.5 

07i09103 13:01 :35 -1.0 19.6 

07109/0313:01:4S -0.6 19.8 

07/09/0313:01:5S -0.5 20.1 

07/09/0313:02:05 -0.8 20.3 

07/0910313:02:15 -1.0 20.9 

07/0910313:C2:2S -1.3 21.0 

07/09/0313:02:3S -1.5 21.1 

07/09/0313:02:4S -1.2 21.4 

07109/0313:02:55 -1.5 21.7 

07/09/0313:03:05 -1.3 22.0 

07/09/0313:03:15 -1.3 22.2 

07/09/0313:03:25 -1.4 22.4 

07/09/0313:03:35 -1.5 22.6 

07/0910313:03:45 -1.5 22.9 

07/0910313:0355 -1.6 23.0 

07/09/0313:04:05 -1.7 23.0 

07109/0313:04:15 -1.8 23.2 

07109/0313:04:25 -1.7 23.3 

07/09/0313:04:35 -1.6 23.4 

07/09/0313:04:45 -1.7 23.7 

07/09/0313:04:55 -1.7 23.9 

07/09/0313:05:05 - 1.8 23.9 

07/09103 13:05:9 5 -1.9 23.9 

07/09.'0313:05:25 -2.1 23.9 

07109/0313:05:35 -2.4 23.9 

25.7 ppm S02 

?age 7 ~ 

314 
7/10103 Run R3 

Date/Tims S02 

mmlddlyy hh:rnm:ss pDm 

07/09/0313:11:35 4.3 

07/09/03 1351:45 4.0 

07/09/03 13:11:55 3.8 

07109/0313:12:05 3.6 

07/09/0313:12:15 3.4 

07/09/0313:12:25 3.3 

07109/0313:12:35 3.2 

07/09103 13:12:45 2.9 

07/09/03 13:12:55 2.8 

07/09/0313:13:05 2.5 

07/09103 13:13:15 2.4 

07/0910313:13:26 2.2 

07/09103 13:13:35 2.0 

07/09/03 13:13:45 2.0 

07/09/03 13:13:55 1.8 

07/09/03 13:14:05 1.6 

07/09/03 13:14:15 1.6 

07/09/03 13:14:25 1.4 

07J09/03 13:14:35 1.4 

07/09/03 13:14:45 1.3 

07/09/0313:14:55 1.2 

Start Pun n3 

07/09103 13:15:05 1.1 

07/09/03 13:16:15 1.0 

0710910313:15:25 0.9 

07/09/0313:15:35 0.9 

07/0910313:15:45 0.9 

07109103 13:15:55 0.7 

07l0910313:16:05 0.6 

07109103 13:16:15 0.6 

07J0910313:16:25 0.5 

07/09/0313:16:35 0.4 

07109103 13:16:45 0.3 

07/09/03 13:16:55 0.2 

07109/0313:17:05 0.2 

07/09/03 13:17:15 0.1 

07J09/0313:17:25 0.1 

07J09/D313:17:35 0.1 

07/09/03 13:17:45 0.1 

07/09/0313:17:55 0.0 

07/09/0313:18:05 0.0 

07/09/0313:18:15 0.0 

0710910313:18:25 -0.1 

07109/0313:18:35 -0.2 

07/09/0313:18:45 -0.1 

07/09/0313:18:55 0.0 

07/09/0313:19:05 0.0 

07/09/0313:19:15 -0.1 

07/09/0313:19:25 -0.1 

07/09/0313:19:35 -0.1 

07/09/0313:19:45 -0.2 

07/09/0313:19:55 -0.1 

07/09J0313:20:05 -0.2 

07/09/0313:20:15 -0.3 

07/09/0313:20:25 -0.3 

07109/0313:20:35 -0.3 

07/0910313:20:45 -0.4 

07/09/0313:20:55 -0.4 

07/0910313:21:05 -0.3 

07/0910313:21:15 -0.3 

07/09/0313:21:25 -0.4 

07109/0313:21:35 -0.4 

07/09/0313:21:45 -0.4 

07/0910313.21.55 -0.4 

07/09/0313:22:05 -0.5 

07/09/0313:22:15 -0.3 

07109I0313:22:25 -0.1 

07/09/0313:22:35 0.0 

07/09I0313:22:45 0.0 

07/09/0313:22:55 0.0 

07/09/0313:23:05 -0.2 

. : 

ri 15 

Page 1 
7110103 Rur V3 

07/09103 13:23:1 5 -0.2 

G710910313:23:25 -0.2 

07/09103 1 3:23:35 - C. .1 

0710910313:23:45 C.0 

0710910313:23:55 -0.1 

07/0910313:24:05 -0.2 

07/09/0313:24:15 -0.1 

0710910313:24:25 -0.1 

0710910313:24:35 0.0 

07109/0313:24:45 0.0 

07109/0313:24:55 -0.1 

07/0910313:25:05 -0.1 

0710910313:25:15 -0.1 

07/0910313:25:25 -0.1 

0710910313:25:35 -0.2 

0710910313:25:45 -0.1 

07/09/0313:25:55 -0.1 

07/09/0313:26:05 -0.1 

0710910313:26:15 -0.1 

0710910313:26:25 -0.2 

07/0910313:26:35 -0.3 

07/09/0313:26:45 -0.2 

07/0910313:26:55 -0.1 

07/09/0313:27:05 -0.1 

07/09/0313:27:15 -0.1 

07/09/0313:27:25 -0.1 

07/09/0313:27:35 -0.1 

07/0910313:27:45 -0.2 

07/09/0313:27:55 -0.2 

07/0910313:28:05 -0.2 

07/0910313:28:15 -0.1 

07/0910313:28:25 -0.1 

07/09/0313:28:35 -0.1 

07109/0313:28:45 -0.1 

0710910313:28:55 -0.1 

0710910313:29:05 -0.1 

07/0910313:29:15 -0.2 

0710910313:29:25 -0.3 

07109/0313:29:35 -0.2 

07109/0313:29:45 -0.2 

07109/0313:29:55 -0.2 

07/0910313:30:05 -0.2 

07109/0313:30:15 -0.2 

07109/0313:30:25 -0.2 

07/091031330:35 -0.3 

07/09/0313:30:45 -0.2 

07/09/0313:30:55 -0.2 

07/09/0313:31:05 -0.2 

07/09/0313:31:15 -0.2 

07/09/0313:31:25 -0.3 

07/0910313:31:35 -0.2 

07/09/0313:31:45 -0.2 

0710910313:31:55 -0.3 

0710910313:32:05 -0.3 

07109/03 13:32:15 -0 3 

07/09/0313:32:25 0.0 

0710910313:32:35 0.0 

07109/0313:32:45 -0.1 

07109/0313:32:55 0.0 

0710910313:33:05 0.0 

07/09/03 9 3:33:15 0.0 

07/09/0313:33:25 0.0 

07/0910313:33:35 0.0 

0710910313:33:45 0.0 

07109J0313:33:55 0.0 

07/0910313:34:05 0.0 

0710910313:34:15 -0.1 

0710910313:34:25 -0.1 

07/0910313:34:35 -0.1 ~7109/0.13:34:45 -0.1 

07/09/0313:34:55 -0.1 

07/0910313:35:05 •0.2 

07/09/03 13:35:15 -0.1 

07/0910313:35:25 

-0.1 

316 

Page 2 
7110103 Pun #3 

0710910313:35:35 -0.1 

07/0910313:35:45 -0.1 

0710910313:35:55 -0.2 

07109/0313:36:05 -0.1 

0710910313:36:15 -0.1 

0710910313:36:25 -0.1 

07109/0313:36:35 0.0 

0710910313:36:45 0.0 

0710910313:36:55 0.0 

07109/0313:37:05 0.0 

0710910313:37:15 0.0 

07109/0313:37:25 0.0 

0710910313:37:35 0.0 

07/0910313:37:45 0.0 

07/0910313:37:55 0.0 

0710910313:38:05 0.0 

07109/0313:38:15 0.0 

07109/0313:38:25 0.0 

0710910313:38:35 0.0 

07/0910313:38:45 0.0 

0710910313:38:55 0.0 

0710910313:39:05 0.0 

07/09/03 13:39:15 0.0 

07/0910313:39:25 -0.1 

07/09/0313:39:35 -0.1 

07/0910313:39:45 -0.1 

07/0910313:39:55 0.0 

07109/0313:40:05 0.0 

0710910313:40:15 -0.1 

07/0910313:40:25 -0.1 

07/0910313:40:35 0.0 

07/0910313:40:45 0.0 

0710910313:40:55 -0.1 

07109/0313:41:05 -0.1 

07109I03 13:41:15 -0.1 

07/09103 13:41:25 0.0 

07/0910313:41:35 -0.1 

07109/0313:41:45 -0.1 

07/09/03 13:4 i : 55 -0.1 

07/09/0313:42:05 -0.1 

07/09/03 13:42:15 0.0 

07/09/03 13:42:25 OA 

07/09/0313:42:35 -0.1 

0710910313:42:45 -0.1 

07/09/0313:42:55 -0.1 

0710910313:43:05 -0.1 

07/09/03 13:43:15 0.0 

0710910313:43:25 0.0 

0710910313:43:35 -0.1 

07109/0313:43:45 -0.1 

07109/0313:43:55 -0.1 

07/0910313:44:05 0.0 

07/0910313:44:95 0.0 

07/09/0313:44:25 -0.1 

07/0910313:44:35 -0.1 

07/0910313:44:45 -0.1 

07/09/0313:44:55 -0.1 

07J0910313:45:05 -0.1 

0710910313:45:15 -0.1 

07109103 13:4 5:25 -0.1 

0710910313:45:35 -0.1 

07/0910313:45:45 -0.1 

07/0910313:45:55 -0.1 

07/09/0313:46:05 -0.2 

07/09/0313:45:15 -0.2 

07/0910313:46:25 -0.2 

0710910313:46:35 -0.2 

07/09/0313:46:45 -0.2 

07/0910313:46:55 -0.2 

07109/0313:47:05 -0.1 

07/09/03 13:47:15 -0.1 

0710910313:47:25 -0.1 

07109/0313:47:35 -0.1 

07/0910313:47:45 -0.1 

317 

Page 3 k~~~~ 
71i0103 i2Ur. r3 

07/0910313:47:55 -0.2 

07109/0313:48:05 -0.9 

07/0910313:48:15 -0.1 

07/0910313:48:25 -0.2 

0710910313:48:35 -0.2 

0710910313:48:45 -0.2 

07109/0313:48:55 -0.3 

0710910313:49:05 -0.3 

07/0910313:49:15 -0.3 

07109/0313:49:25 =0.2 

07/09/0313:49:35 -J.2 

07/0910313:49:45 -0.3 

07/0910313:49:55 -0.2 

07109/0313:50:05 -0.2 

07109/0313:50:15 -0.2 

0710910313:50:25 -0.3 

07/0910313:50:35 -0.3 

0710910313:50:45 -0.2 

0710910313:50:55 -0.2 

07/0910313:51:05 -0.1 

07/09103 13:51:15 -0.2 

07109103.13:51:25 0,0 

07109J0313:51:35 -0.1 

0710910313:51:45 -0.1 

07/09/03 13:51:55 0.0 

07/0910313:52:05 0,0 

07/0910313:52:15 0.0 

0710910313:52:25 0.0 

07/09/03 ;3:52:35 0.0 

07/09/0313:52:45 0.0 

07/09/03 13:52: 55 -0. i 

0710910313:53:05 -0.1 

0710910313:53:15 -0.1 

0710910313:53:25 -0.1 

0710910313:53:35 -0.1 

07/0910313:53:45 0.0 

07/09/03 13:53: 55 -0.1 

0710910313:54:05 0.0 

07/0910313:54:15 -0.1 

0710910313:54:25 -0.1 

0710910313:54:35 -0.1 

07/0910313:54:45 -0.1 

0710910313:54:55 -0.1 

0710910313:55:05 -0.1 

07/0910313:55:15 -0.2 

07109/0313:55:25 -0.1 

0710910313:55:35 -0.1 

0710910313:55:45 -0.1 

07/0910313:55:55 -0.2 

07/0910313:56:05 -0.2 

07/09/0313:56:15 -0.3 

07/0910313:56:25 -0.2 

07/0910313:56:35 -0.2 

07109/0313:56:45 -0.3 

07/0910313:56:55 -0.2 

0710910313:57:05 -0.2 

07109/0313:57:15 -0.2 

0710910313:57:25 -0.2 

07109/0313:57:35 -0.2 

07/0910313:57:45 -0.2 

07/0910313:57:55 -0.1 

0710910313:58:05 -0.2 

07/09f0313:58:15 -0.2 

07f09/0313:55:2:. -0.2 

0710910313:58:35 -0.2 

07J09/03 13:58:45 -0,1 

0710910313:58:55 -0. -, 

07/09/03 13:59:03 -0.1 

07109/0313:59:15 -0.1 

07/09/0313:59:25 -0.2 

07/09/0313:59:35 -0.2 

0710910313:59:45 -0.2 

07109/0313:59:55 -0.3 

07/09110314:00

- 05 -0.3 

3 18 

Page 4 

~ 
7110/03 Run 93 

07109103 14:00: 14 5 -0.2 

07/09/C314:00:25 -0.2 

07/09/0314:00:35 -01 

07109/0314:00:45 -0.1 

07109/0314:00:55 0.0 

07/09/0314:01:05 0.0 

07109/03 14:01:15 0.0 

07/09/0314:01:25 -0.1 

07/0910314:01:35 -0.2 

07/09/0314:01:45 -0.2 

07/09/0314:01:55 -0.1 

07/09/0314:02:05 -0.1 

07/09/0314:02:15 -0.2 

07/09/0314:02:25 -0.2 

07/0910314:02:35 -0.1 

07/09/0314:02:45 -0.2 

07109/0314:02:55 -0.2 

07/0910314:03:05 -0.2 

07109/0314:03:15 -0.2 

07/0910314:03:25 -0.1 

07/09/0314:03:35 -0.1 

07/0910314:03:45 -0.2 

07/09/0314:03:55 -0.3 

07/09/0314:04:05 -0.2 

0710910314:04:15 -0.2 

07/09/0314:04:25 -0.2 

07/09/0314:04:35 -0.2 

07/09/0314:04:45 -0.3 

07/09/0314:04:55 -0.3 

07/09f0314:05:05 -0.3 

07109/0314:05:15 -0.2 

0710910314:05:25 -0.2 

07/09/0314:05:35 -0.2 

07/09/0314:05:45 -0.2 

07109/0314:05:55 -0.1 

0710910314:06:05 -0.1 

07/0910314:06:15 -0.1 

07/0910314:05:25 -0.2 

07109/0314:06:35 -0.1 

07109/0314:06:45 -0.2 

07/0910314:06:55 -0.2 

07/09/0314:07:05 -0.1 

07/0910314:07:15 0.0 

07/09/0314:07:25 -0.1 

07/0910314:07:35 0.0 

07/09/0314:07:45 0.0 

07109/0314:07:55 0.0 

07109/0314:08:05 -0.1 

07/09/0314:08:15 -0.2 

07/09/0314:08:25 -0.1 

07/09/0314:08:35 -0.1 

07/09/0314:08:45 -0.1 

07/09/0314:08:55 0.0 

07109/0314:09:05 -0.1 

07/0910314:09:15 -0.1 

07109/0314:09:25 -0.1 

07/09/0314:09:35 -0.1 

07/0910314:09:45 0.0 

07109/0314:09:55 -0.1 

07109/0314:10:05 •0.1 

07/09/03 14:10:15 -0.1 

07/09/0314:10:25 -0.1 

07/09/0314:10:35 -0.1 

07/09/0314:10:45 -0.1 

07/09/0314:10:55 -0.1 

07/0910314:11:05 -0.2 

07109/0314:11:15 -0.2 

07/0910314:11:25 -0.2 

07109/0314:11:35 -0.2 

07109/0314:11:45 -0.2 

07109/0314:11:55 -0.1 

07J09/0314:12:05 -0.1 

07/09/0314:12:15 -0.2 

07/09/0314•12:25 -0.1 

11 ~ 3i9 

Page 5 
7110103 Rur~ rj-'3 

07/0910314:12:35 -0.2 

0710910314'12:45 -0.2 

07109/03 1 4: , 2:55 -0.1 

07i09l0314:13:05- G.0 

07/09103 14:13:15 0.0 

07109/0314:13:25 -0.1 

0710910314:13:35 -0.1 

07/09/03 14:13:45 -0. 1 

07109/0314:13:55 -0.1 

07J0910314:14:05 0.0 

07/09/03 14:14:15 0.0 

07/0910314:14:25 0.0 

0710910314:14:35 -0.1 

07/09J0314:14:45 -0.1 

0710910314:14:55 -0.1 

Stop Run 43 -0.10 

07109/0314:15:05 -0.1 

07/09103 14:1 5:15 -0.1 

07J0910314:15:25 -0.1 

07/09/031415:35 -01 

0710910314:15:45 -0.1 

07/0910314:15:55 -0.1 

07/09/0314:16:05 -0.2 

07/09/03 14:16:15 -0.2 

07l09/0314:16:25 -0.2 

07109/0314:16:35 -0.2 

07J09/0314:16:45 -0.1 

0710910314:16:55 -0.2 

07/091C314:17:05 -0.2 

07/0910314:17:15 -0.2 

0710910314:1 7:25 -0.2 

0710910314:17:35 -0.2 

0710910314:17:45 -0.1 

0710910314:17:55 -0.2 

0710910314:18:05 -0.2 

07109/03 14:18:15 -0.1 

07/09/03 14:18:25 0.0 

0710910314:18:35 -0.1 

07/0910314:18:45 -0.1 

0710910314:18:55 0.0 

0710910314:19:05 -0.1 

07109/03 14:19:15 -0.1 

07/0910314:19:25 -0.1 

07109/0314:19:35 -0.1 

07/09J0314:19:45 0.0 

07/09/03 14:19:55 0.2 

0710910314:20:05 0.6 

07109103 14:20:15 1.3 

07/09/0314:20:25 2.0 

07J09/0314:20:35 2.8 

07/0910314:20:45 3.6 

07/09/0314:20:55 4.4 

07/0910314:21:05 5.4 

0710910314:21:15 6,4 

07/09/03 14:21:25 7.2 

07109/0314;21:35 8.2 

07I09103 14:21:45 9.0 

07/09/03 14:21:55 9.8 

07/09103 14:22:05 10.6 

07/09/03 1 4:22:15 11.3 

07109/03 't 4:22:25 12.0 

07109J03 14: 22:35 12.7 

07/09/03 14:22:45 13.3 

07/09103 14:22:55 13.8 

07/09103 14:23:05 14.2 

07109103 14:23:1 5 14.6 

07109/03 14:23:25 15.1 

07109103 14:23:35 15.6 

07/09/03 14:23:45 15.8 

07/09J03 14 :23:55 16.1 

07/09103 14:24:05 16.5 

Zeto N2 

FE. 320 

Page 6 
7/10103 Run #V3 

0710910314:24:15 16.8 

07109103 14:24:25 17.1 

07/0910314:24:35 17.4 

07/09103 14:24:45 17.5 

07/09103 14 :24:55 17.7 

07/0910314:25:05 17.8 

07109/03 14:25:15 18.0 

07/09/03 14 : 25:25 18.1 

07/09/03 14:25:35 18.2 

07/0910 3 14: 25:4 5 18.4 

07/09/03 14:25:55 18.9 

07/09/03 14:26:05 19.2 

07/0910314:26:15 19.5 

0710910314:26:25 19.9 

07/09/0314:26:35 20.3 

07/09/0314:26:45 20.5 

07/09/0314:26:55 20.9 

07109/0314:27:05 21.2 

07/0910314:27:15 21.6 

07/09/0314:27:25 21:9 

07/09/0314:27:35 22.3 

07/09/0314:27:45 22.6 

07/09/0314:27:55 22.9 

07/0910314:28:05 23.2 

07109/0314:28:15 23.4 

07/09/0314:28:25 23.5 

0710910314:28:35 23.5 25.7 ppm S02 

07/0910314:28:45 23.6 

07/69/0314:28:55 23.6 

Page 7 ~ 

3 2 1 
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Customer: NiATH=SON TRI-GAS - IRVING 

Cylinder Number: SX-321 45 

Cylinder pressure: 2000 

Last Analysis date: 4-17-2003 

Expiration Date: 10/17/03 

Protocol: Reference n Lot # 

G 1 249290 109-35-28491 

REPLICATE RESPONSES 

Date: 4-10-2003 

Cornponent : Sulf ~ur Dioxide w ~-- 25.6 PPM ~ ~ a ~

' r $-•a 

25.5 PPM Certified Conc: 25.7 Y 0.2 PPM~, ~ rf ~ t• 

~ "'- `` 25:5 PPM ~ T f{ 

Date: 4-17-2003 

25.9 PPM 

25.4 PPM 

25..8 PPM 

BALANCE GAS: 

.. ~.~, 

Nitrogen~` ~ 

~tl ~. 

ILV 

P,EFERENCE STANDARDS ;" ~ 

~• Cornaonent: Sulfur Dioxide 

SRM #: SRMr.J693a 

Cylinder CAL=01 ~0596 

Concentration: 49.9 ppm, 

- t -•:~ `'~ 

CER T IFICATION INSTRUMENTS 

Component: Sulfur Dioxide~A 

Make/Modef: Nicolet 550 

Serial Nurnber: ACN-9402192 

Measurement Principle: FTIR ~Y' ~t~ ' "' ' i >. ...^'~ '4 w „• , , 

Last Ca(ibration: 4-3-2003 ° 

Nlotes: 

This certification was performed according to EPA Traceability Protocol ~or Assay & Certification of Gaseous 

Calibration Standards September 1997, using procedure G1 andlor G2. 

-~ a yst U` Date 

~ ~~? 
U_A !j1T LIQUIDE 

CERTf FICaTE of ANALYSIS 

4 -0.12 0.07 0.01 

~ P1~1P._W 00A~'~:~. " ~~ 

50.95 50.44 r 

-0.30 0.09 -0.1

50.62 Component 1 e tE 50.79 51.12 50.87 

1p 

50.45 50.79 50.60 r s Sulfur Dioxide 51.84 51.75 51.60 

e,`~ _. ~ 50.08 50.42 50.23 51.20 51.11 50.96 :.,... . ~ w ,. ~ 

. . 

" ~~ ~« . . 

. ~ 

Analyst: 

. ~ 

Air Lic{uide America Corroralio„ 

11426 Fairmont Parkv+ay, La Porte, Texas 77571-6000 

Pnone: (28 1 ) 474-8400 Fxx: (281) 474-8419 

vw 

32 3