# Instructions for filling the Emission Test Template

This Information Collection Request (ICR) spreadsheet is intended to collect information about emission data from fossil fuel burning power plants and which test methods were used to do so for cases where the test methods are not currently supported by the Electronic Reporting Tool (ERT). This spreadsheet should only be used if the method is not in the ERT or if you do not have access to a lab which performs methods that are in the ERT. Constituents of concern are: Carbon Monoxide, Formaldehyde, Methane, Speciated Volatile Hazardous Air Pollutants (HAPs), Speciated Semi HAPs, Sulfer Dioxide, Oxygen, Carbon Dioxide, Hydrogen Cyanide, Nitrogen Oxides, Total Dissolved Solids (TDS), and Total Suspended Solids (TSS). You must complete 3 separate sampling events for each of the requested constituents. spreadsheet is intended to be used for one boiler of one facility. Data for multiple boilers should be handled by using separate copies of this spreadsheet. Fields shaded in yellow are required. All cells that are shaded in light green are populated using drop

-down lists. You do not need to populate cells shaded in gray, as they are automatically populated from the Boiler Information worksheet. Please Do Not modify the structure of this spreadsheet by adding or subtracting
rows, columns, cells. Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_EmisTestMethods.xls (example: 8100_Unit_2_EmisTestMethods.xls).

Please refer to the following steps when using these spreadsheets.

Boiler Information Worksheet

1. Please enter the the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the control device configuration.

Emission Data Worksheets

The emission data worksheets are provided for each constituent or constituent family requred for this analysis. On each spreadsheet, you must enter boiler operating information during sampling, fuel input information, and emission test results. There are generally 1 to 3 emission test results records to be entered depending on the constiuent or constituent family. For example, CO only requires 1 record with 3 sample events, while Mercury requires that you enter both Hg Hg+2

# , or if the Ontario

- Hydro Method was used, you would need to enter Hg0

# , Hg P

# , and Hg Specieated Volatile Organic HAP and Speciated Semi

-Volatile Organic HAP worksheets allow you to use a drop provided in the Constituent field to define as many records as needed to record each HAP that you have results for. General instructions follow for these worksheets:

Boiler Operation Information

1. Please determine which units of measure (acfm or dscfm) were used for Exhaust Flow Rate and which units of measure (deg C or deg F) were used for Exhaust Temperature. Fill these units of measure into the Units of Measure field. 2. Please provide the values of all requested parameters for each of the 3 sample testing periods in the Sample 1, Sample 2, and Sample 3 fields

. 3. Please provide any other supporting information or comments in the Other Supporting Information field.

Fuel Information

1. Please enter what types of fuel are being used in your boiler using the drop

-downs in the Fuel Type Selection field. You may enter up to 4 fuel types. Then, enter the input rate of each fuel in the Sample 1, Sample 2, and Sample 3 fields. If you are not burning one or more of the fuel types entered in one or more samples, then enter an input rate of zero.

# If you are not burning one or more of the fuel types entered in one or more samples, then enter an input rate of zero. 2. Please enter the unit of measure using the drop down provided. 3. Please enter the test method used to determine the fuel input rate. 4. Please provide any other information that you feel may be important in the Other Supporting Information field.

Emission Data

1. Some constituents ask for the emission rate results of each of the 3 samples in two different units of measure, while others do not. If emission rate results are requested in two different units of measure (ex. lb/MMBtu (Pounds per million BTU) and ppmvd @ 7% O 2 

# (parts per million by volume dry basis at 7 percent oxygen)), you are required to provide both. 2. Please provide the test method used. This may or may not match the example given in the Test Method Used field. Please ensure that the name includes the owning organization of the test method (ex. U.S. EPA Method 0010). 3. Please provide any other information that you feel may be important in the Other Supporting Information field. 4. If data sheets and QA/QC documentation tables are provided for the test method you are entering data for please also enter these data.

# This Information Collection Request (ICR) spreadsheet is intended to collect information about emission data from fossil fuel burning power plants and which test methods were used to do so for cases where the test methods are not currently supported by the Electronic Reporting Tool (ERT). This spreadsheet should only be used if the method is not in the ERT or if you do not have access to a lab which performs methods that are in the ERT. Constituents of concern are: Carbon Monoxide, Formaldehyde, Methane, Speciated Volatile Hazardous Air Pollutants (HAPs), Speciated Semi

-Volatile Organic HAPs, Sulfer Dioxide, Oxygen, Carbon Dioxide, Hydrogen Cyanide, Nitrogen Oxides, Total Dissolved Solids (TDS), and Total Suspended Solids (TSS). You must complete 3 separate sampling events for each of the requested constituents. This spreadsheet is intended to be used for one boiler of one facility. Data for multiple boilers should be handled by using Fields shaded in yellow are required. All cells that are shaded in light green are down lists. You do not need to populate cells shaded in gray, as they are automatically populated

Please Do Not modify the structure of this spreadsheet by adding or subtracting Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_EmisTestMethods.xls (example: 8100_Unit_2_EmisTestMethods.xls).

1. Please enter the the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

The emission data worksheets are provided for each constituent or constituent family requred for this analysis. On each spreadsheet, you must enter boiler operating information during sampling, fuel input information, and emission test results. There are generally 1 to 3 emission test results records to be entered depending on the constiuent or constituent family. For example, CO only requires 1 record with 3 sample events, while Mercury requires that you enter both Hg0 

# and , and Hg+2 

# . However, both the Volatile Organic HAP worksheets allow you to use a drop

-down provided in the Constituent field to define as many records as needed to record each HAP that you have results for.

1. Please determine which units of measure (acfm or dscfm) were used for Exhaust Flow Rate and which units of measure (deg C or deg F) were used for Exhaust Temperature. Fill these units of measure into the Units of Measure field. 2. Please provide the values of all requested parameters for each of the 3 sample testing periods in the Sample 1, Sample

3. Please provide any other supporting information or comments in the Other Supporting Information field.

downs in the Fuel Type Selection field. You may enter up to 4 fuel types. Then, enter the input rate of each fuel in the Sample 1, Sample 2, and Sample 3 fields. If you are not burning one or more of the fuel types entered in one or more samples, then enter an input rate of zero.

# If you are not burning one or more of the fuel types entered in one or more samples, then enter an input rate of zero.

4. Please provide any other information that you feel may be important in the Other Supporting Information field.

1. Some constituents ask for the emission rate results of each of the 3 samples in two different units of measure, while others do not. If emission rate results are requested in two different units of measure (ex. lb/MMBtu (Pounds per million (parts per million by volume dry basis at 7 percent oxygen)), you are required to provide both. 2. Please provide the test method used. This may or may not match the example given in the Test Method Used field. Please ensure that the name includes the owning organization of the test method (ex. U.S. EPA Method 0010). Please provide any other information that you feel may be important in the Other Supporting Information field. 4. If data sheets and QA/QC documentation tables are provided for the test method you are entering data for please also

# EIA

Facility Code Facility Name Boiler ID Control Device Configuraton

6043 Martin PMR2 Listed (by boiler) in Question 16 (page 17) of the questionnaire

EPA-HQ-OAR-2009-0234-DRAFT-1858.xls Boiler Information

### EIA

Facility Code Facility Name Boiler ID 6043 Martin PMR2

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure Other Supporting Information Date of Testing 4/13/2010 4/13/2010 4/13/2010 Steam Output (1000 lb/hr) 5191 5173 5184 1000 lb/hr Total Heat Input (MMBtu/hr) 7183.9 7186.5 7244.5 MMBtu/hr Basis (Wet/Dry) Dry Dry Dry N/A Exhaust Steam % Moisture 9.590379358 9.590379358 9.590379358 % Exhaust Flow Rate (acfm or dscfm) 1375744.499 1363830.505 1372591.485 dscfm Exhaust Temperature (deg C or deg F) 324 324 324 deg F

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate

Sample 2 Fuel Input Rate

Sample 3 Unit of Measure Fuel Flow Measurement Method Other Supporting

Information No.6 Fuel Oil (residual or bunker C) 950 950 958 gallon/minute gas fuel meter

Emission Test Results Formaldehyde Emission Rate Sample 1 (lb/MMBtu) Formaldehyde Emission Rate Sample 1 (ppmvd @ 7%O2) Formaldehyde Emission Rate Sample 2 (lb/MMBtu) Formaldehyde Emission Rate Sample 2 (ppmvd @ 7%O2) Formaldehyde Emission Rate Sample 3 (lb/MMBtu) Formaldehyde Emission Rate Sample 3 (ppmvd @ 7%O2) Test Method Used (ex. U.S. EPA Method 320) Other Supporting Information 0.000156086 0.14 8.73951E-05 0.08 0.000196927 0.18 U.S. EPA Method 320 #VALUE!

EPA-HQ-OAR-2009-0234-DRAFT-1858.xls Formaldehyde Emission DataEIA

Facility Code Facility Name Boiler ID 6043 Martin PMR2

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure Other Supporting Information Date of Testing 4/13/2010 4/13/2010 4/13/2010 Steam Output (1000 lb/hr) 5191 5173 5184 1000 lb/hr Total Heat Input (MMBtu/hr) 7183.9 7186.5 7244.5 MMBtu/hr Basis (W et/Dry) Dry Dry Dry N/A Exhaust Steam % Moisture 9.590379358 9.590379358 9.590379358 % Exhaust Flow Rate (acfm or dscfm) 1375744.499 1363830.505 1372591.485 dscfm Exhaust Temperature (deg C or deg F) 324 324 324 deg F

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate Sample 2 Fuel Input Rate Sample 3 Unit of Measure Fuel FlowMeasurement Method Other Supporting Information No.6 Fuel Oil (residual or bunker C) 950 950 958 gallon/minute gas fuel meter

Emission Test Results Methane Emission Rate Sample 1 (lb/MMBtu) Methane Emission Rate Sample 1 (ppmvd @ 7% O2) Methane Emission Rate Sample 2 (lb/MMBtu) Methane Emission Rate Sample 2 (ppmvd @ 7% O2) Methane Emission Rate Sample 3 (lb/MMBtu) Methane Emission Rate Sample 3 (ppmvd @ 7% O2) Test Method Used (ex. U.S. EPA Method 18) Other Supporting Information 0.000355328 0.62 0.000338393 0.59 0.000289089 0.50 U.S. EPA Method 320 #VALUE!

EPA-HQ-OAR-2009-0234-DRAFT-1858.xls CH4 Emission DataEIA

Facility Code Facility Name Boiler ID 6043 Martin PMR2

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure Other Supporting Information Date of Testing 8/3/2010 8/3/2010 8/3/2010 Steam Output (1000 lb/hr) 5185 5205 5194 1000 lb/hr Total Heat Input (MMBtu/hr) 7269.8 7284.9 7297.6 MMBtu/hr Basis (W et/Dry) Dry Dry Dry N/A Exhaust Steam % Moisture 5 4.8 5.1 % Exhaust Flow Rate (acfm or dscfm) 0 0 0 dscfm Exhaust Temperature (deg C or deg F) 346 352 355 deg F

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate Sample 2 Fuel Input Rate Sample 3 Unit of Measure Fuel Flow Measurement Method Other Supporting

Information No.6 Fuel Oil (residual or bunker C) 391500 392300 393000 lb/hour gas fuel meter

Emission Test Results Total Vapor Phase Mercury Emission Rate Sample 1 (lb/MMBtu) Total Vapor Phase

Mercury Emission Rate Sample 2 (lb/MMBtu) Total Vapor Phase

Mercury Emission Rate Sample 3 (lb/MMBtu) Test Method Used (ex. U.S. EPA Method 30B) Other Supporting

Information 1.52E-07 1.40E-07 1.79E-07 U.S. EPA Method 30B ADL



### Data Sheets and QA

/QC Documentation

Total Mass (ng) trap ID Section 1 Section 2 Sections 1+2 (ng) (ug)
fpl-10-pmr.fl-icr#1-Hg30B-PMR2-1-1-Train A OL 59060 15.61 0.75 16.36 0.00 16.36 0.01636
fpl-10-pmr.fl-icr#1-Hg30B-PMR2-1-1-Train B OL 74721 36.75 0.9 37.65 20.00 17.65 0.01765
fpl-10-pmr.fl-icr#1-Hg30B-PMR2-1-2-Train A OL 59048 15.68 1.07 16.75 0.00 16.75 0.01675
fpl-10-pmr.fl-icr#1-Hg30B-PMR2-1-2-Train B OL 73904 34.51 0.4 34.91 20.00 14.91 0.01491
fpl-10-pmr.fl-icr#1-Hg30B-PMR2-1-3-Train A OL 59060 18.08 0.94 19.02 0.00 19.02 0.019020000
fpl-10-pmr.fl-icr#1-Hg30B-PMR2-1-3-Train B OL 74721 40.09 0.74 40.83 20.00 20.83 0.02083

Start Stop per tube per run per tube per run per tube per run fpl-10-pmr.fl-icr#1-Hg30B-PMR2-1-1-Train A 8/3/2010 8:48 10:48 0.145415123 1.45E-01 0.001057139 1.06E-03 0.004630268 4.63E-03
fpl-10-pmr.fl-icr#1-Hg30B-PMR2-1-1-Train B 8/3/2010 8:48 10:48 0.158952747 1.59E-01 0.001155555 1.16E-03 0.005061329 5.06E-03
fpl-10-pmr.fl-icr#1-Hg30B-PMR2-1-2-Train A 8/3/2010 11:22 13:22 0.146939185 1.47E-01 0.001070437 1.07E-03 0.004688515 4.69E-03
fpl-10-pmr.fl-icr#1-Hg30B-PMR2-1-2-Train B 8/3/2010 11:22 13:22 0.132722146 1.33E-01 0.000966868 9.67E-04 0.00423488 4.23E-03
fpl-10-pmr.fl-icr#1-Hg30B-PMR2-1-3-Train A 8/3/2010 16:30 18:30 0.169264261 1.69E-01 0.001235223 1.24E-03 0.005410276 5.41E-03
fpl-10-pmr.fl-icr#1-Hg30B-PMR2-1-3-Train B 8/3/2010 16:30 18:30 0.188276159 1.88E-01 0.001373964 1.37E-03 0.006017963 6.02E-03 Averages 0.15692827 0.001143198 0.005007205

Average R Vol. diff (%) Limit Abs. diff. (μg/dscm) % Limit
fpl-10-pmr.fl-icr#1-Hg30B-PMR2-1-1-Train A 0.085
fpl-10-pmr.fl-icr#1-Hg30B-PMR2-1-1-Train B 0.084 1.303227809
fpl-10-pmr.fl-icr#1-Hg30B-PMR2-1-2-Train A 0.085
fpl-10-pmr.fl-icr#1-Hg30B-PMR2-1-2-Train B 0.084 1.449901357
fpl-10-pmr.fl-icr#1-Hg30B-PMR2-1-3-Train A 0.085
fpl-10-pmr.fl-icr#1-Hg30B-PMR2-1-3-Train B 0.084 1.542524108

% Limit C rec R (%) by Run R (%) by program Limit

fpl-10-pmr.fl-icr#1-Hg30B-PMR2-1-1-Train A 4.804612428
fpl-10-pmr.fl-icr#1-Hg30B-PMR2-1-1-Train B 5.373134328
fpl-10-pmr.fl-icr#1-Hg30B-PMR2-1-2-Train A 6.823979592
fpl-10-pmr.fl-icr#1-Hg30B-PMR2-1-2-Train B 2.756719504
fpl-10-pmr.fl-icr#1-Hg30B-PMR2-1-3-Train A 5.199115044
fpl-10-pmr.fl-icr#1-Hg30B-PMR2-1-3-Train B 3.683424589 0.26325749 110.5169404 0.019011898 5.317412143

Run ID Sorbent Trap Breakthrough (B) Measured Spike Recovery ( R )

≤10% of Section 1 Hg mass for Hg conc. >1
μg/dscm: or ≤20% of Section 1 for Hg conc. ≤1 μg/dscm 0.256792568 107.5160403
103.3490911 Average Recovery, between 85 and 115% 0.21995592 92.01429239 ≤20% of field recovery

test 0.013537623 4.447783306 ≤ 10 % RD mass for Hg conc. >1 μg/dscm: or ≤20% RD or ≤ 0.2 μg/dscm abs.diff. for Hg conc.
≤1μg/dscm 0.014217039 5.083662756 Hg Emissions(lb/Tbtu) Hg Emissions (lb/hr)

Paired Trap Agreement (RD) Summary

of M30B Quality

A ssurance Checks
Run ID Volume Sampled (dscm) Hg Emissions (lb/yr)* Summary

of Hg Collected on Sorbent Traps via Method 30B

Run ID Appartioned Mass (ng) Initial Spike (ng) Total Non-spike

Individual Sorbent Tube Emission Summary, Method 30B
Run ID Test Date Run Time

EPA-HQ-OAR-2009-0234-DRAFT-1858.xls Hg Emission Data-30BEIA

Facility Code Facility Name Boiler ID 6043 Martin PMR2

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure Other Supporting Information Date of Testing 4/12/2010 4/12/2010 4/13/2010 Steam Output (1000 lb/hr) 5156 5142 5176 1000 lb/hr Total Heat Input (MMBtu/hr) 7124.8 7132.9 7201.8 MMBtu/hr Basis (W et/Dry) Wet Wet Wet N/A Exhaust Steam % Moisture 4.04 4.04 4.04 % Exhaust Flow Rate (acfm or dscfm) 1305376.206 1410918.477 1557569.494 dscfm Exhaust Temperature (deg C or deg F) 313.00 313.00 320.00 deg F

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate Sample 2 Fuel Input Rate Sample 3 Unit of Measure Fuel Flow Measurement Method Other Supporting

Information No.6 Fuel Oil (residual or bunker C) 386000 386400 390200 lb/hour gas fuel meter

Compound (use drop dow n to define for as many

rows as needed) Volatile Organic HAP Emission Rate Sample

1 (lb/MMBtu) Volatile Organic HAP

Emission Rate Sample

1 (μg @ 7% O2) Volatile Organic

HAP Emission Rate Sample 2 (lb/MMBtu) Volatile Organic

HAP Emission Rate Sample 2 (μg @ 7% O2) Volatile Organic

HAP Emission Rate Sample 3 (lb/MMBtu) Volatile Organic

HAP Emission Rate Sample 3 (μg @ 7% O2) Test Method Used Other Supporting Information Dichlorodifluoromethane [<1.53E-06] [<1.78] [<2.37E-06] [<2.75] [<3.46E-06] [<4.01] U.S. EPA Method 0031 with SW -846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+0.02; plus 1/4 condensate (ug): [<1.0] - Average of 4 Trials, Run 2 (ug): [<0.02]+0.03; [<0.02]+0.03; [<0.02]+0.09; [<0.02]+0.03; plus 1/4 condensate (ug): [<1.0] - Average of 4 Trials, Run 3 (ug): [<0.02]+0.03; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+0.24; plus 1/4 condensate (ug): [<1.0] Chloromethane [<1.51E-06] [<1.75] [<1.5E-06] [<1.74] [<6.86E-06] [<7.95] U.S. EPA Method 0031 with SW -846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<1.0] - Average of 4 Trials, Run 2 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<1.0] - Average of 4 Trials, Run 3 (ug): 0.09+0.14; [<0.02]+0.17; 0.02+0.15; [<0.02]+0.17; plus 1/4 condensate (ug): [<1.0] Vinyl Chloride [<1.46E-06] [<1.7] [<1.46E-06] [<1.69] [<1.42E-06] [<1.65] U.S. EPA Method 0031 with SW -846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<0.50] Bromomethane [<1.72E-06] [<2] [<1.51E-06] [<1.75] [<4.21E-06] [<4.88] U.S. EPA Method 0031 with SW -846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): 0.03+0.03; [<0.02]+0.02; [<0.02]+[<0.02]; [<0.02]+0.03; plus 1/4 condensate (ug): 1.1 - Average of 4 Trials, Run 2 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): 1.1 - Average of 4 Trials, Run 3 (ug): [<0.02]+0.07; [<0.02]+0.09; 0.04+0.12; 0.03+0.08; plus 1/4 condensate (ug): 1.1 Chloroethane [<1.51E-06] [<1.75] [<1.5E-06] [<1.74] [<2.24E-05] [<25.96] U.S. EPA Method 0031 with SW -846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<1.0] - Average of 4 Trials, Run 2 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<1.0] - Average of 4 Trials, Run 3 (ug): 0.1+0.23; 0.32+0.55; 0.36+0.38; [<0.02]+0.61; plus 1/4 condensate (ug): [<1.0] Trichlorofluoromethane [<1.51E-06] [<1.75] [<1.5E-06] [<1.74] [<1.59E-06] [<1.84] U.S. EPA Method 0031 with SW -846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<1.0] - Average of 4 Trials, Run 2 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<1.0] - Average of 4 Trials, Run 3 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+0.03; plus 1/4 condensate (ug): [<1.0] Carbon Disulfide [<7.74E-07] [<0.9] [<9.63E-07] [<1.12] [<9.55E-07] [<1.11] U.S. EPA Method 0031 with SW -846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; 0.01+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; 0.01+[<0.01]; [<0.01]+[<0.01]; [<0.01]+0.03; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+0.04; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Acetone [<1.03E-05] [<11.96] 3.8E-05 44.03 [<6.18E-05] [<71.6] U.S. EPA Method 0031 with SW -846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): 0.07+0.33; [<0.05]+0.24; 0.08+0.08; [<0.05]+0.07; plus 1/4 condensate (ug): [<20] - Average of 4 Trials, Run 2 (ug): 0.88+0.07; 0.16+0.09; 0.07+0.09; 0.15+0.39; plus 1/4 condensate (ug): 240 - Average of 4 Trials, Run 3 (ug): 0.76+0.69; 0.57+1.99; 0.96+1.13; 0.25+0.62; plus 1/4 condensate (ug): [<20] 1,1-Dichloroethene [<1.05E-06] [<1.22] [<1.12E-06] [<1.3] [<7.33E-07] [<0.85] U.S. EPA Method 0031 with SW -846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+0.04; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): 0.01+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.050]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Iodomethane [<1.05E-06] [<1.22] [<1.12E-06] [<1.3] [<7.33E-07] [<0.85] U.S. EPA Method 0031 with SW -846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+0.04; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): 0.01+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.050]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Methylene Chloride [<1.99E-05] [<23.11] [<1.56E-05] [<18.12] [<4.63E-06] [<5.36] U.S. EPA Method 0031 with SW -846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): 0.02+1.12; 0.02+0.72; 0.02+0.06; 0.02+0.3; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): 0.95+0.05; 0.04+0.08; 0.04+0.06; 0.33+0.2; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): 0.04+0.06; 0.05+0.05; 0.05+0.05; 0.13+0.1; plus 1/4 condensate (ug): [<0.50] trans,1,2-Dichloroethene [<7.54E-07] [<0.87] [<7.52E-07] [<0.87] [<7.33E-07] [<0.85] U.S. EPA Method 0031 with SW -846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Vinyl Acetate [<1.05E-06] [<1.22] [<1.12E-06] [<1.3] [<7.33E-07] [<0.85] U.S. EPA Method 0031 with SW -846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+0.04; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): 0.01+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.050]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,1-Dichloroethane [<7.54E-07] [<0.87] [<7.52E-07] [<0.87] [<7.33E-07] [<0.85] U.S. EPA Method 0031 with SW -846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 2-Butanone [<2.48E-06] [<2.88] [<2.48E-06] [<2.87] [<1.91E-05] [<22.08] U.S. EPA Method 0031 with SW -846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<20] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<20] - Average of 4 Trials, Run 3 (ug): [<0.24]+[<0.14]; [<0.37]+[<0.33]; [<0.53]+[<0.18]; [<0.21]+[<0.01]; plus 1/4 condensate (ug): [<20] cis,1,2-Dichloroethene [<7.54E-07] [<0.87] [<7.52E-07] [<0.87] [<7.33E-07] [<0.85] U.S. EPA Method 0031 with SW -846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Chloroform [<7.54E-07] [<0.87] [<7.52E-07] [<0.87] [<7.33E-07] [<0.85] U.S. EPA Method 0031 with SW -846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,1,1-Trichloroethane [<7.54E-07] [<0.87] [<7.52E-07] [<0.87] [<7.33E-07] [<0.85] U.S. EPA Method 0031 with SW -846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Carbon Tetrachloride [<7.54E-07] [<0.87] [<7.52E-07] [<0.87] [<7.33E-07] [<0.85] U.S. EPA Method 0031 with SW -846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,2-Dichloroethane [<7.54E-07] [<0.87] [<7.52E-07] [<0.87] [<7.33E-07] [<0.85] U.S. EPA Method 0031 with SW -846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Benzene [<7.81E-06] [<9.05] [<1.25E-06] [<1.45] [<7.25E-05] [<84.04] U.S. EPA Method 0031 with SW -846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): 0.02+0.02; 0.02+0.02; 0.03+0.02; 0.73+0.02; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): 0.02+[<0.01]; 0.03+0.02; 0.02+0.01; [<0.01]+0.01; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): 0.97+0.51; 1.33+0.95; 1.66+0.97; 1.22+0.77; plus 1/4 condensate (ug): [<0.50] Trichloroethene [<7.54E-07] [<0.87] [<7.52E-07] [<0.87] [<7.33E-07] [<0.85] U.S. EPA Method 0031 with SW -846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,2-Dichloropropane [<7.54E-07] [<0.87] [<7.52E-07] [<0.87] [<7.33E-07] [<0.85] U.S. EPA Method 0031 with SW -846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Dibromomethane [<8.52E-07] [<0.99] [<1.69E-06] [<1.96] [<2.21E-06] [<2.56] U.S. EPA Method 0031 with SW -846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): 1.61 - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): 11.1 - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): 17.6 Bromodichloromethane [<7.54E-07] [<0.87] [<7.52E-07] [<0.87] [<7.33E-07] [<0.85] U.S. EPA Method 0031 with SW -846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] cis,1,3-Dichloropropene [<7.54E-07] [<0.87] [<7.52E-07] [<0.87] [<7.33E-07] [<0.85] U.S. EPA Method 0031 with SW -846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] trans,1,3-Dichloropropene [<7.54E-07] [<0.87] [<7.52E-07] [<0.87] [<7.33E-07] [<0.85] U.S. EPA Method 0031 with SW -846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 4-Methyl-2-Pentanone [<2.48E-06] [<2.88] [<2.48E-06] [<2.87] [<2.42E-06] [<2.8] U.S. EPA Method 0031 with SW -846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<20] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<20] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<20] 1,1,2-Trichloroethane [<7.54E-07] [<0.87] [<7.52E-07] [<0.87] [<7.33E-07] [<0.85] U.S. EPA Method 0031 with SW -846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Chlorodibromomethane [<7.54E-07] [<0.87] [<7.52E-07] [<0.87] [<7.33E-07] [<0.85] U.S. EPA Method 0031 with SW -846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 2-Hexanone [<2.48E-06] [<2.88] [<2.48E-06] [<2.87] [<8.26E-06] [<9.57] U.S. EPA Method 0031 with SW -846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<20] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<20] - Average of 4 Trials, Run 3 (ug): 0.15+[<0.01]; 0.16+0.04; 0.25+0.01; 0.12+[<0.01]; plus 1/4 condensate (ug): [<20] Toluene [<1.14E-06] [<1.32] [<1.34E-06] [<1.56] [<3.21E-06] [<3.72] U.S. EPA Method 0031 with SW -846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): 0.01+0.02; 0.02+0.02; 0.02+[<0.01]; 0.02+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): 0.02+0.03; 0.02+0.01; 0.02+0.01; 0.03+0.01; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): 0.04+0.01; 0.06+0.02; 0.1+0.02; 0.1+[<0.01]; plus 1/4 condensate (ug): [<0.50] Tetrachloroethene [<7.54E-07] [<0.87] [<7.52E-07] [<0.87] [<7.33E-07] [<0.85] U.S. EPA Method 0031 with SW -846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Ethylene Dibromide [<7.54E-07] [<0.87] [<7.52E-07] [<0.87] [<7.33E-07] [<0.85] U.S. EPA Method 0031 with SW -846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Chlorobenzene [<7.54E-07] [<0.87] [<7.52E-07] [<0.87] [<7.33E-07] [<0.85] U.S. EPA Method 0031 with SW -846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,1,1,2-Tetrachloroethane [<7.54E-07] [<0.87] [<7.52E-07] [<0.87] [<7.33E-07] [<0.85] U.S. EPA Method 0031 with SW -846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Ethylbenzene [<7.54E-07] [<0.87] [<7.52E-07] [<0.87] [<1.42E-06] [<1.65] U.S. EPA Method 0031 with SW -846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): 0.02+[<0.01]; 0.03+[<0.01]; 0.04+[<0.01]; 0.03+[<0.01]; plus 1/4 condensate (ug): [<0.50] M&P-Xylene [<2.22E-06] [<2.57] [<2.21E-06] [<2.56] [<2.16E-06] [<2.5] U.S. EPA Method 0031 with SW -846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.03]+[<0.03]; [<0.03]+[<0.03]; [<0.03]+[<0.03]; [<0.03]+[<0.03]; plus 1/4 condensate (ug): [<1.0] - Average of 4 Trials, Run 2 (ug): [<0.03]+[<0.03]; [<0.03]+[<0.03]; [<0.03]+[<0.03]; [<0.03]+[<0.03]; plus 1/4 condensate (ug): [<1.0] - Average of 4 Trials, Run 3 (ug): [<0.03]+[<0.03]; [<0.03]+[<0.03]; [<0.03]+[<0.03]; [<0.03]+[<0.03]; plus 1/4 condensate (ug): [<1.0] O-Xylene [<7.54E-07] [<0.87] [<7.61E-07] [<0.88] [<7.37E-07] [<0.85] U.S. EPA Method 0031 with SW -846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+0.01; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; 0.01+[<0.01]; plus 1/4 condensate (ug): [<0.50] Styrene [<7.9E-07] [<0.92] [<8.3E-07] [<0.96] [<6.8E-06] [<7.88] U.S. EPA Method 0031 with SW -846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+0.01; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+0.02; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): 0.09+[<0.01]; 0.15+0.03; 0.26+0.01; 0.21+[<0.01]; plus 1/4 condensate (ug): [<0.50] Bromoform [<7.54E-07] [<0.87] [<7.52E-07] [<0.87] [<7.33E-07] [<0.85] U.S. EPA Method 0031 with SW -846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,1,2,2-Tetrachloroethane [<7.54E-07] [<0.87] [<7.52E-07] [<0.87] [<7.33E-07] [<0.85] U.S. EPA Method 0031 with SW -846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,2,3-Trichloropropane [<8.26E-07] [<0.96] [<7.52E-07] [<0.87] [<7.33E-07] [<0.85] U.S. EPA Method 0031 with SW -846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; 0.02+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] - Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Run 1 Comments: Speciated Volatile Organic HAP Emission Data Note: Acetone and methylene chloride were observed in the laboratory blank. Laboratory

notes indicate the elevated acetone, methylene chloride, and toluene levels may be due to contamination in the field.

EPA-HQ-OAR-2009-0234-DRAFT-1858.xls Spec Volit Org HAP Emis DataEIA

Facility Code Facility Name Boiler ID 6043 Martin PMR2

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure Other Supporting Information Date of Testing 4/12/2010 4/12/2010 4/13/2010 Steam Output (1000 lb/hr) 5156 5142 5176 1000 lb/hr Total Heat Input (MMBtu/hr) 7124.8 7132.9 7201.8 MMBtu/hr Basis (W et/Dry) Wet Wet Wet N/A Exhaust Steam % Moisture 4.04 4.04 4.04 % Exhaust Flow Rate (acfm or dscfm) 1305376.206 1410918.477 1557569.494 dscfm Exhaust Temperature (deg C or deg F) 313.00 313.00 320.00 deg F

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate Sample 2 Fuel Input Rate Sample 3 Unit of Measure Fuel Flow Measurement Method Other Supporting

Information No.6 Fuel Oil (residual or bunker C) 386000 386400 390200 lb/hour gas fuel meter

Compound (use drop dow n to define for as many

rows as needed) Volatile Organic HAP Emission Rate Sample

1 (lb/MMBtu) Volatile Organic HAP

Emission Rate Sample

1 (μg @ 7% O2) Volatile Organic

HAP Emission Rate Sample 2 (lb/MMBtu) Volatile Organic

HAP Emission Rate Sample 2 (μg @ 7% O2) Volatile Organic

HAP Emission Rate Sample 3 (lb/MMBtu) Volatile Organic

HAP Emission Rate Sample 3 (μg @ 7% O2) Test Method Used Other Supporting Information Speciated Volatile Organic HAP Emission Data Note: Acetone and methylene chloride were observed in the laboratory blank. Laboratory

notes indicate the elevated acetone, methylene chloride, and toluene levels may be due to contamination in the field.

Dichlorodifluoromethane Average of 4 Trials, Run 1 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+0.02; plus 1/4 condensate (ug): [<1.0] Chloromethane Average of 4 Trials, Run 1 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<1.0] Vinyl Chloride Average of 4 Trials, Run 1 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<0.50] Bromomethane Average of 4 Trials, Run 1 (ug): 0.03+0.03; [<0.02]+0.02; [<0.02]+[<0.02]; [<0.02]+0.03; plus 1/4 condensate (ug): 1.1 Chloroethane Average of 4 Trials, Run 1 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<1.0] Trichlorofluoromethane Average of 4 Trials, Run 1 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<1.0] Carbon Disulfide Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; 0.01+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Acetone Average of 4 Trials, Run 1 (ug): 0.07+0.33; [<0.05]+0.24; 0.08+0.08; [<0.05]+0.07; plus 1/4 condensate (ug): [<20] 1,1-Dichloroethene Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+0.04; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Iodomethane Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+0.04; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Methylene Chloride Average of 4 Trials, Run 1 (ug): 0.02+1.12; 0.02+0.72; 0.02+0.06; 0.02+0.3; plus 1/4 condensate (ug): [<0.50] trans,1,2-Dichloroethene Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Vinyl Acetate Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+0.04; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,1-Dichloroethane Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 2-Butanone Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<20] cis,1,2-Dichloroethene Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Chloroform Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,1,1-Trichloroethane Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Carbon Tetrachloride Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,2-Dichloroethane Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Benzene Average of 4 Trials, Run 1 (ug): 0.02+0.02; 0.02+0.02; 0.03+0.02; 0.73+0.02; plus 1/4 condensate (ug): [<0.50] Trichloroethene Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,2-Dichloropropane Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Dibromomethane Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): 1.61 Bromodichloromethane Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] cis,1,3-Dichloropropene Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] trans,1,3-Dichloropropene Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 4-Methyl-2-Pentanone Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<20] 1,1,2-Trichloroethane Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Chlorodibromomethane Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 2-Hexanone Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<20] Toluene Average of 4 Trials, Run 1 (ug): 0.01+0.02; 0.02+0.02; 0.02+[<0.01]; 0.02+[<0.01]; plus 1/4 condensate (ug): [<0.50] Tetrachloroethene Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Ethylene Dibromide Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Chlorobenzene Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,1,1,2-Tetrachloroethane Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Ethylbenzene Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] M&P-Xylene Average of 4 Trials, Run 1 (ug): [<0.03]+[<0.03]; [<0.03]+[<0.03]; [<0.03]+[<0.03]; [<0.03]+[<0.03]; plus 1/4 condensate (ug): [<1.0] O-Xylene Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Styrene Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+0.01; plus 1/4 condensate (ug): [<0.50] Bromoform Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,1,2,2-Tetrachloroethane Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,2,3-Trichloropropane Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; 0.02+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Run 2 Comments: Dichlorodifluoromethane Average of 4 Trials, Run 2 (ug): [<0.02]+0.03; [<0.02]+0.03; [<0.02]+0.09; [<0.02]+0.03; plus 1/4 condensate (ug): [<1.0] EPA-HQ-OAR-2009-0234-DRAFT-1858.xls Spec Volit Org HAP Emis DataEIA

Facility Code Facility Name Boiler ID 6043 Martin PMR2

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure Other Supporting Information Date of Testing 4/12/2010 4/12/2010 4/13/2010 Steam Output (1000 lb/hr) 5156 5142 5176 1000 lb/hr Total Heat Input (MMBtu/hr) 7124.8 7132.9 7201.8 MMBtu/hr Basis (W et/Dry) Wet Wet Wet N/A Exhaust Steam % Moisture 4.04 4.04 4.04 % Exhaust Flow Rate (acfm or dscfm) 1305376.206 1410918.477 1557569.494 dscfm Exhaust Temperature (deg C or deg F) 313.00 313.00 320.00 deg F

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate Sample 2 Fuel Input Rate Sample 3 Unit of Measure Fuel Flow Measurement Method Other Supporting

Information No.6 Fuel Oil (residual or bunker C) 386000 386400 390200 lb/hour gas fuel meter

Compound (use drop dow n to define for as many

rows as needed) Volatile Organic HAP Emission Rate Sample

1 (lb/MMBtu) Volatile Organic HAP

Emission Rate Sample

1 (μg @ 7% O2) Volatile Organic

HAP Emission Rate Sample 2 (lb/MMBtu) Volatile Organic

HAP Emission Rate Sample 2 (μg @ 7% O2) Volatile Organic

HAP Emission Rate Sample 3 (lb/MMBtu) Volatile Organic

HAP Emission Rate Sample 3 (μg @ 7% O2) Test Method Used Other Supporting Information Speciated Volatile Organic HAP Emission Data Note: Acetone and methylene chloride were observed in the laboratory blank. Laboratory

notes indicate the elevated acetone, methylene chloride, and toluene levels may be due to contamination in the field.

Chloromethane Average of 4 Trials, Run 2 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<1.0] Vinyl Chloride Average of 4 Trials, Run 2 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<0.50] Bromomethane Average of 4 Trials, Run 2 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): 1.1 Chloroethane Average of 4 Trials, Run 2 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<1.0] Trichlorofluoromethane Average of 4 Trials, Run 2 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<1.0] Carbon Disulfide Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; 0.01+[<0.01]; [<0.01]+[<0.01]; [<0.01]+0.03; plus 1/4 condensate (ug): [<0.50] Acetone Average of 4 Trials, Run 2 (ug): 0.88+0.07; 0.16+0.09; 0.07+0.09; 0.15+0.39; plus 1/4 condensate (ug): 240 1,1-Dichloroethene Average of 4 Trials, Run 2 (ug): 0.01+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.050]; plus 1/4 condensate (ug): [<0.50] Iodomethane Average of 4 Trials, Run 2 (ug): 0.01+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.050]; plus 1/4 condensate (ug): [<0.50] Methylene Chloride Average of 4 Trials, Run 2 (ug): 0.95+0.05; 0.04+0.08; 0.04+0.06; 0.33+0.2; plus 1/4 condensate (ug): [<0.50] trans,1,2-Dichloroethene Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Vinyl Acetate Average of 4 Trials, Run 2 (ug): 0.01+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.050]; plus 1/4 condensate (ug): [<0.50] 1,1-Dichloroethane Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 2-Butanone Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<20] cis,1,2-Dichloroethene Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Chloroform Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,1,1-Trichloroethane Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Carbon Tetrachloride Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,2-Dichloroethane Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Benzene Average of 4 Trials, Run 2 (ug): 0.02+[<0.01]; 0.03+0.02; 0.02+0.01; [<0.01]+0.01; plus 1/4 condensate (ug): [<0.50] Trichloroethene Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,2-Dichloropropane Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Dibromomethane Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): 11.1 Bromodichloromethane Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] cis,1,3-Dichloropropene Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] trans,1,3-Dichloropropene Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 4-Methyl-2-Pentanone Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<20] 1,1,2-Trichloroethane Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Chlorodibromomethane Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 2-Hexanone Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<20] Toluene Average of 4 Trials, Run 2 (ug): 0.02+0.03; 0.02+0.01; 0.02+0.01; 0.03+0.01; plus 1/4 condensate (ug): [<0.50] Tetrachloroethene Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Ethylene Dibromide Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Chlorobenzene Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,1,1,2-Tetrachloroethane Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Ethylbenzene Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] M&P-Xylene Average of 4 Trials, Run 2 (ug): [<0.03]+[<0.03]; [<0.03]+[<0.03]; [<0.03]+[<0.03]; [<0.03]+[<0.03]; plus 1/4 condensate (ug): [<1.0] O-Xylene Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+0.01; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Styrene Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+0.02; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Bromoform Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,1,2,2-Tetrachloroethane Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,2,3-Trichloropropane Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Run 3 Comments: Dichlorodifluoromethane Average of 4 Trials, Run 3 (ug): [<0.02]+0.03; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+0.24; plus 1/4 condensate (ug): [<1.0] Chloromethane Average of 4 Trials, Run 3 (ug): 0.09+0.14; [<0.02]+0.17; 0.02+0.15; [<0.02]+0.17; plus 1/4 condensate (ug): [<1.0] EPA-HQ-OAR-2009-0234-DRAFT-1858.xls Spec Volit Org HAP Emis DataEIA

Facility Code Facility Name Boiler ID 6043 Martin PMR2

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure Other Supporting Information Date of Testing 4/12/2010 4/12/2010 4/13/2010 Steam Output (1000 lb/hr) 5156 5142 5176 1000 lb/hr Total Heat Input (MMBtu/hr) 7124.8 7132.9 7201.8 MMBtu/hr Basis (W et/Dry) Wet Wet Wet N/A Exhaust Steam % Moisture 4.04 4.04 4.04 % Exhaust Flow Rate (acfm or dscfm) 1305376.206 1410918.477 1557569.494 dscfm Exhaust Temperature (deg C or deg F) 313.00 313.00 320.00 deg F

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate Sample 2 Fuel Input Rate Sample 3 Unit of Measure Fuel Flow Measurement Method Other Supporting

Information No.6 Fuel Oil (residual or bunker C) 386000 386400 390200 lb/hour gas fuel meter

Compound (use drop dow n to define for as many

rows as needed) Volatile Organic HAP Emission Rate Sample

1 (lb/MMBtu) Volatile Organic HAP

Emission Rate Sample

1 (μg @ 7% O2) Volatile Organic

HAP Emission Rate Sample 2 (lb/MMBtu) Volatile Organic

HAP Emission Rate Sample 2 (μg @ 7% O2) Volatile Organic

HAP Emission Rate Sample 3 (lb/MMBtu) Volatile Organic

HAP Emission Rate Sample 3 (μg @ 7% O2) Test Method Used Other Supporting Information Speciated Volatile Organic HAP Emission Data Note: Acetone and methylene chloride were observed in the laboratory blank. Laboratory

notes indicate the elevated acetone, methylene chloride, and toluene levels may be due to contamination in the field.

Vinyl Chloride Average of 4 Trials, Run 3 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<0.50] Bromomethane Average of 4 Trials, Run 3 (ug): [<0.02]+0.07; [<0.02]+0.09; 0.04+0.12; 0.03+0.08; plus 1/4 condensate (ug): 1.1 Chloroethane Average of 4 Trials, Run 3 (ug): 0.1+0.23; 0.32+0.55; 0.36+0.38; [<0.02]+0.61; plus 1/4 condensate (ug): [<1.0] Trichlorofluoromethane Average of 4 Trials, Run 3 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+0.03; plus 1/4 condensate (ug): [<1.0] Carbon Disulfide Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+0.04; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Acetone Average of 4 Trials, Run 3 (ug): 0.76+0.69; 0.57+1.99; 0.96+1.13; 0.25+0.62; plus 1/4 condensate (ug): [<20] 1,1-Dichloroethene Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Iodomethane Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Methylene Chloride Average of 4 Trials, Run 3 (ug): 0.04+0.06; 0.05+0.05; 0.05+0.05; 0.13+0.1; plus 1/4 condensate (ug): [<0.50] trans,1,2-Dichloroethene Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Vinyl Acetate Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,1-Dichloroethane Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 2-Butanone Average of 4 Trials, Run 3 (ug): [<0.24]+[<0.14]; [<0.37]+[<0.33]; [<0.53]+[<0.18]; [<0.21]+[<0.01]; plus 1/4 condensate (ug): [<20] cis,1,2-Dichloroethene Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Chloroform Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,1,1-Trichloroethane Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Carbon Tetrachloride Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,2-Dichloroethane Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Benzene Average of 4 Trials, Run 3 (ug): 0.97+0.51; 1.33+0.95; 1.66+0.97; 1.22+0.77; plus 1/4 condensate (ug): [<0.50] Trichloroethene Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,2-Dichloropropane Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Dibromomethane Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): 17.6 Bromodichloromethane Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] cis,1,3-Dichloropropene Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] trans,1,3-Dichloropropene Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 4-Methyl-2-Pentanone Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<20] 1,1,2-Trichloroethane Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Chlorodibromomethane Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 2-Hexanone Average of 4 Trials, Run 3 (ug): 0.15+[<0.01]; 0.16+0.04; 0.25+0.01; 0.12+[<0.01]; plus 1/4 condensate (ug): [<20] Toluene Average of 4 Trials, Run 3 (ug): 0.04+0.01; 0.06+0.02; 0.1+0.02; 0.1+[<0.01]; plus 1/4 condensate (ug): [<0.50] Tetrachloroethene Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Ethylene Dibromide Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Chlorobenzene Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,1,1,2-Tetrachloroethane Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] Ethylbenzene Average of 4 Trials, Run 3 (ug): 0.02+[<0.01]; 0.03+[<0.01]; 0.04+[<0.01]; 0.03+[<0.01]; plus 1/4 condensate (ug): [<0.50] M&P-Xylene Average of 4 Trials, Run 3 (ug): [<0.03]+[<0.03]; [<0.03]+[<0.03]; [<0.03]+[<0.03]; [<0.03]+[<0.03]; plus 1/4 condensate (ug): [<1.0] O-Xylene Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; 0.01+[<0.01]; plus 1/4 condensate (ug): [<0.50] Styrene Average of 4 Trials, Run 3 (ug): 0.09+[<0.01]; 0.15+0.03; 0.26+0.01; 0.21+[<0.01]; plus 1/4 condensate (ug): [<0.50] Bromoform Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,1,2,2-Tetrachloroethane Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50] 1,2,3-Trichloropropane Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

EPA-HQ-OAR-2009-0234-DRAFT-1858.xls Spec Volit Org HAP Emis DataEIA Facility Code Facility Name Boiler ID 6043 Martin PMR2

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure Other Supporting Information Date of Testing 4/12/2010 4/12/2010 4/13/2010 Steam Output (1000 lb/hr) 5158 5147 5180 1000 lb/hr Total Heat Input (MMBtu/hr) 7110.5 7132.6 7197.8 MMBtu/hr Basis (W et/Dry) Wet Wet Wet N/A Exhaust Steam % Moisture 9.90 8.86 9.94 % Exhaust Flow Rate (acfm or dscfm) 1,305,376 1,410,918 1,557,569 dscfm Exhaust Temperature (deg C or deg F) 313.67 313.88 326.96 deg F

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate Sample 2 Fuel Input Rate Sample 3 Unit of Measure Fuel Flow Measurement Method Other Supporting Information No.6 Fuel Oil (residual or bunker C) 385200 386400 390000 lb/hour gas fuel meter

Compound (use drop down to define for as many rows as needed) Semi-Volatile Organic HAP Emission Rate Sample 1 (lb/MMBtu) Semi-Volatile Organic HAP Emission Rate Sample 1 (μg @ 7% O2) Semi-Volatile Organic HAP Emission Rate Sample 2 (lb/MMBtu) Semi-Volatile Organic HAP Emission Rate Sample 2 (μg @ 7% O2) Semi-Volatile Organic HAP Emission Rate Sample 3 (lb/MMBtu) Semi-Volatile Organic HAP Emission Rate Sample 3 (μg @ 7% O2) Test Method Used Other Supporting Information N-nitrosomethylethylamine [<9.58E-06] [<11.1] [<9.58E-06] [<11.1] [<9.58E-06] [<11.1] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<9.45]+[<9.45]+[<9.45] - Run 2 (ug): [<9.45]+[<9.45]+[<9.45] - Run 3 (ug): [<9.45]+[<9.45]+[<9.45] Methyl methanesulfonate [<2.08E-06] [<2.41] [<2.08E-06] [<2.41] [<2.08E-06] [<2.41] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.05]+[<2.05]+[<2.05] - Run 2 (ug): [<2.05]+[<2.05]+[<2.05] - Run 3 (ug): [<2.05]+[<2.05]+[<2.05] N-Nitrosodiethylamine [<2.23E-06] [<2.59] [<2.23E-06] [<2.59] [<2.23E-06] [<2.59] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.2]+[<2.2]+[<2.2] - Run 2 (ug): [<2.2]+[<2.2]+[<2.2] - Run 3 (ug): [<2.2]+[<2.2]+[<2.2] Ethyl methanesulfonate [<2.23E-06] [<2.59] [<2.23E-06] [<2.59] [<2.23E-06] [<2.59] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.2]+[<2.2]+[<2.2] - Run 2 (ug): [<2.2]+[<2.2]+[<2.2] - Run 3 (ug): [<2.2]+[<2.2]+[<2.2] Aniline [<1.88E-06] [<2.17] [<1.88E-06] [<2.17] [<1.88E-06] [<2.17] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.85]+[<1.85]+[<1.85] - Run 2 (ug): [<1.85]+[<1.85]+[<1.85] - Run 3 (ug): [<1.85]+[<1.85]+[<1.85] Phenol [<4.14E-06] [<4.8] [<1.98E-06] [<2.29] [<1.98E-06] [<2.29] U.S. EPA Method 0010 with SW-846 Method 8270D DLL: Run 1 (ug): [<1.95]+4.75+5.55 - Run 2 (ug): [<1.95]+[<1.95]+[<1.95] - Run 3 (ug): [<1.95]+[<1.95]+[<1.95] Pentachloroethane [<2.74E-06] [<3.17] [<2.74E-06] [<3.17] [<2.74E-06] [<3.17] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.7]+[<2.7]+[<2.7] - Run 2 (ug): [<2.7]+[<2.7]+[<2.7] - Run 3 (ug): [<2.7]+[<2.7]+[<2.7] Bis(2-chloroethyl)ether [<1.93E-06] [<2.23] [<1.93E-06] [<2.23] [<1.93E-06] [<2.23] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.9]+[<1.9]+[<1.9] - Run 2 (ug): [<1.9]+[<1.9]+[<1.9] - Run 3 (ug): [<1.9]+[<1.9]+[<1.9] 2-Chlorophenol [<1.88E-06] [<2.17] [<1.88E-06] [<2.17] [<1.88E-06] [<2.17] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.85]+[<1.85]+[<1.85] - Run 2 (ug): [<1.85]+[<1.85]+[<1.85] - Run 3 (ug): [<1.85]+[<1.85]+[<1.85] 1,3-Dichlorobenzene [<2.43E-06] [<2.82] [<2.43E-06] [<2.82] [<2.43E-06] [<2.82] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.4]+[<2.4]+[<2.4] - Run 2 (ug): [<2.4]+[<2.4]+[<2.4] - Run 3 (ug): [<2.4]+[<2.4]+[<2.4] 1,4-Dichlorobenzene [<5.95E-06] [<6.89] [<4E-06] [<4.64] [<1.81E-05] [<20.96] U.S. EPA Method 0010 with SW-846 Method 8270D DLL: Run 1 (ug): 8.6+6.2+[<2.8] - Run 2 (ug): 4.2+4.85+[<2.8] - Run 3 (ug): 33.3+17.4+[<2.8] 1,2-Dichlorobenzene [<2.08E-06] [<2.41] [<2.08E-06] [<2.41] [<2.08E-06] [<2.41] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.05]+[<2.05]+[<2.05] - Run 2 (ug): [<2.05]+[<2.05]+[<2.05] - Run 3 (ug): [<2.05]+[<2.05]+[<2.05] Benzyl alcohol [<5.81E-06] [<6.74] [<8.77E-06] [<10.16] [<9.17E-06] [<10.63] U.S. EPA Method 0010 with SW-846 Method 8270D DLL: Run 1 (ug): [<3.55]+10.1+[<3.55] - Run 2 (ug): 9.7+12.7+[<3.55] - Run 3 (ug): 7.6+16+[<3.55] Bis(2-chloroisopropyl)ether [<2.03E-06] [<2.35] [<2.03E-06] [<2.35] [<2.03E-06] [<2.35] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2]+[<2]+[<2] - Run 2 (ug): [<2]+[<2]+[<2] - Run 3 (ug): [<2]+[<2]+[<2] Hexachloroethane [<2.23E-06] [<2.59] [<2.23E-06] [<2.59] [<2.23E-06] [<2.59] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.2]+[<2.2]+[<2.2] - Run 2 (ug): [<2.2]+[<2.2]+[<2.2] - Run 3 (ug): [<2.2]+[<2.2]+[<2.2] N-Nitrosodi-n-propylamine [<1.93E-06] [<2.23] [<1.93E-06] [<2.23] [<1.93E-06] [<2.23] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.9]+[<1.9]+[<1.9] - Run 2 (ug): [<1.9]+[<1.9]+[<1.9] - Run 3 (ug): [<1.9]+[<1.9]+[<1.9] 2-Methylphenol [<2.13E-06] [<2.47] [<2.13E-06] [<2.47] [<2.13E-06] [<2.47] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.1]+[<2.1]+[<2.1] - Run 2 (ug): [<2.1]+[<2.1]+[<2.1] - Run 3 (ug): [<2.1]+[<2.1]+[<2.1] 4-Methylphenol&3-Methylphenol [<5.73E-06] [<6.64] [<5.73E-06] [<6.64] [<5.73E-06] [<6.64] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<5.65]+[<5.65]+[<5.65] - Run 2 (ug): [<5.65]+[<5.65]+[<5.65] - Run 3 (ug): [<5.65]+[<5.65]+[<5.65] Acetophenone [<2.89E-06] [<3.35] [<2.7E-06] [<3.13] [<2.69E-06] [<3.11] U.S. EPA Method 0010 with SW-846 Method 8270D DLL: Run 1 (ug): [<1.8]+4.95+[<1.8] - Run 2 (ug): [<1.8]+4.4+[<1.8] - Run 3 (ug): [<1.8]+4.35+[<1.8] N-nitrosomorpholine [<2.08E-06] [<2.41] [<2.08E-06] [<2.41] [<2.08E-06] [<2.41] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.05]+[<2.05]+[<2.05] - Run 2 (ug): [<2.05]+[<2.05]+[<2.05] - Run 3 (ug): [<2.05]+[<2.05]+[<2.05] o-Toluidine [<5.07E-06] [<5.88] [<5.07E-06] [<5.88] [<5.07E-06] [<5.88] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<5]+[<5]+[<5] - Run 2 (ug): [<5]+[<5]+[<5] - Run 3 (ug): [<5]+[<5]+[<5] N-nitrosopyrrolidine [<1.52E-06] [<1.76] [<1.52E-06] [<1.76] [<1.52E-06] [<1.76] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.5]+[<1.5]+[<1.5] - Run 2 (ug): [<1.5]+[<1.5]+[<1.5] - Run 3 (ug): [<1.5]+[<1.5]+[<1.5] N-nitrosopiperidine [<8.51E-06] [<9.87] [<8.51E-06] [<9.87] [<8.51E-06] [<9.87] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<8.4]+[<8.4]+[<8.4] - Run 2 (ug): [<8.4]+[<8.4]+[<8.4] - Run 3 (ug): [<8.4]+[<8.4]+[<8.4] Nitrobenzene [<1.98E-06] [<2.29] [<1.98E-06] [<2.29] [<1.98E-06] [<2.29] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.95]+[<1.95]+[<1.95] - Run 2 (ug): [<1.95]+[<1.95]+[<1.95] - Run 3 (ug): [<1.95]+[<1.95]+[<1.95] Isophorone [<3.34E-05] [<38.7] [<2.28E-06] [<2.64] [<8.8E-06] [<10.2] U.S. EPA Method 0010 with SW-846 Method 8270D DLL: Run 1 (ug): 94.3+[<2.25]+[<2.25] - Run 2 (ug): [<2.25]+[<2.25]+[<2.25] - Run 3 (ug): 8.4+15.4+[<2.25] 2-Nitrophenol [<2.03E-06] [<2.35] [<2.03E-06] [<2.35] [<2.03E-06] [<2.35] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2]+[<2]+[<2] - Run 2 (ug): [<2]+[<2]+[<2] - Run 3 (ug): [<2]+[<2]+[<2] 2,4-Dimethylphenol [<2.64E-06] [<3.06] [<2.64E-06] [<3.06] [<2.64E-06] [<3.06] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.6]+[<2.6]+[<2.6] - Run 2 (ug): [<2.6]+[<2.6]+[<2.6] - Run 3 (ug): [<2.6]+[<2.6]+[<2.6] Bis(2-chloroethoxy)methane [<2.13E-06] [<2.47] [<2.13E-06] [<2.47] [<2.13E-06] [<2.47] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.1]+[<2.1]+[<2.1] - Run 2 (ug): [<2.1]+[<2.1]+[<2.1] - Run 3 (ug): [<2.1]+[<2.1]+[<2.1] 2,4-Dichlorophenol [<2.03E-06] [<2.35] [<2.03E-06] [<2.35] [<2.03E-06] [<2.35] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2]+[<2]+[<2] - Run 2 (ug): [<2]+[<2]+[<2] - Run 3 (ug): [<2]+[<2]+[<2] 1,2,4-Trichlorobenzene [<1.57E-06] [<1.82] [<1.57E-06] [<1.82] [<1.57E-06] [<1.82] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.55]+[<1.55]+[<1.55] - Run 2 (ug): [<1.55]+[<1.55]+[<1.55] - Run 3 (ug): [<1.55]+[<1.55]+[<1.55] Naphthalene [<1.93E-06] [<2.23] [<1.93E-06] [<2.23] [<1.93E-06] [<2.23] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.9]+[<1.9]+[<1.9] - Run 2 (ug): [<1.9]+[<1.9]+[<1.9] - Run 3 (ug): [<1.9]+[<1.9]+[<1.9] 4-Chloroaniline [<5.07E-06] [<5.88] [<5.07E-06] [<5.88] [<5.07E-06] [<5.88] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<5]+[<5]+[<5] - Run 2 (ug): [<5]+[<5]+[<5] - Run 3 (ug): [<5]+[<5]+[<5] 2-Chloronaphthalene [<2.69E-06] [<3.11] [<2.69E-06] [<3.11] [<2.69E-06] [<3.11] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.65]+[<2.65]+[<2.65] - Run 2 (ug): [<2.65]+[<2.65]+[<2.65] - Run 3 (ug): [<2.65]+[<2.65]+[<2.65] 2,6-Dichlorophenol [<2.69E-06] [<3.11] [<2.69E-06] [<3.11] [<2.69E-06] [<3.11] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.65]+[<2.65]+[<2.65] - Run 2 (ug): [<2.65]+[<2.65]+[<2.65] - Run 3 (ug): [<2.65]+[<2.65]+[<2.65] Hexachloropropene [<1.62E-06] [<1.88] [<1.62E-06] [<1.88] [<1.62E-06] [<1.88] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.6]+[<1.6]+[<1.6] - Run 2 (ug): [<1.6]+[<1.6]+[<1.6] - Run 3 (ug): [<1.6]+[<1.6]+[<1.6] Hexachlorobutadiene [<1.72E-06] [<2] [<1.72E-06] [<2] [<1.72E-06] [<2] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.7]+[<1.7]+[<1.7] - Run 2 (ug): [<1.7]+[<1.7]+[<1.7] - Run 3 (ug): [<1.7]+[<1.7]+[<1.7] N-Nitrosodi-n-butylamine [<2.03E-06] [<2.35] [<2.03E-06] [<2.35] [<2.03E-06] [<2.35] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2]+[<2]+[<2] - Run 2 (ug): [<2]+[<2]+[<2] - Run 3 (ug): [<2]+[<2]+[<2] 4-Chloro-3-methylphenol [<2.94E-06] [<3.41] [<2.94E-06] [<3.41] [<2.94E-06] [<3.41] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.9]+[<2.9]+[<2.9] - Run 2 (ug): [<2.9]+[<2.9]+[<2.9] - Run 3 (ug): [<2.9]+[<2.9]+[<2.9] 2-Methylnaphthalene [<2.23E-06] [<2.59] [<2.23E-06] [<2.59] [<2.23E-06] [<2.59] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.2]+[<2.2]+[<2.2] - Run 2 (ug): [<2.2]+[<2.2]+[<2.2] - Run 3 (ug): [<2.2]+[<2.2]+[<2.2] Isosafrole [<2.23E-06] [<2.59] [<2.23E-06] [<2.59] [<2.23E-06] [<2.59] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.2]+[<2.2]+[<2.2] - Run 2 (ug): [<2.2]+[<2.2]+[<2.2] - Run 3 (ug): [<2.2]+[<2.2]+[<2.2] Hexachlorocyclopentadiene [<2.53E-05] [<29.38] [<2.53E-05] [<29.38] [<2.53E-05] [<29.38] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<25]+[<25]+[<25] - Run 2 (ug): [<25]+[<25]+[<25] - Run 3 (ug): [<25]+[<25]+[<25] 1,2,4,5-Tetrachlorobenzene [<2.18E-06] [<2.53] [<2.18E-06] [<2.53] [<2.18E-06] [<2.53] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.15]+[<2.15]+[<2.15] - Run 2 (ug): [<2.15]+[<2.15]+[<2.15] - Run 3 (ug): [<2.15]+[<2.15]+[<2.15] 2,4,6-Trichlorophenol [<2.38E-06] [<2.76] [<2.38E-06] [<2.76] [<2.38E-06] [<2.76] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.35]+[<2.35]+[<2.35] - Run 2 (ug): [<2.35]+[<2.35]+[<2.35] - Run 3 (ug): [<2.35]+[<2.35]+[<2.35] 2,4,5-Trichlorophenol [<2.28E-06] [<2.64] [<2.28E-06] [<2.64] [<2.28E-06] [<2.64] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.25]+[<2.25]+[<2.25] - Run 2 (ug): [<2.25]+[<2.25]+[<2.25] - Run 3 (ug): [<2.25]+[<2.25]+[<2.25] 2-Nitroaniline [<2.38E-06] [<2.76] [<2.38E-06] [<2.76] [<2.38E-06] [<2.76] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.35]+[<2.35]+[<2.35] - Run 2 (ug): [<2.35]+[<2.35]+[<2.35] - Run 3 (ug): [<2.35]+[<2.35]+[<2.35] Safrole [<1.32E-06] [<1.53] [<1.32E-06] [<1.53] [<1.32E-06] [<1.53] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.3]+[<1.3]+[<1.3] - Run 2 (ug): [<1.3]+[<1.3]+[<1.3] - Run 3 (ug): [<1.3]+[<1.3]+[<1.3] Dimethyl phthalate [<2.23E-06] [<2.59] [<2.23E-06] [<2.59] [<2.23E-06] [<2.59] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.2]+[<2.2]+[<2.2] - Run 2 (ug): [<2.2]+[<2.2]+[<2.2] - Run 3 (ug): [<2.2]+[<2.2]+[<2.2] Acenaphthylene [<2.03E-06] [<2.35] [<2.03E-06] [<2.35] [<2.03E-06] [<2.35] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2]+[<2]+[<2] - Run 2 (ug): [<2]+[<2]+[<2] - Run 3 (ug): [<2]+[<2]+[<2] 2,6-Dinitrotoluene [<2.13E-06] [<2.47] [<2.13E-06] [<2.47] [<2.13E-06] [<2.47] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.1]+[<2.1]+[<2.1] - Run 2 (ug): [<2.1]+[<2.1]+[<2.1] - Run 3 (ug): [<2.1]+[<2.1]+[<2.1] m-dinitrobenzene [<2.33E-06] [<2.7] [<2.33E-06] [<2.7] [<2.33E-06] [<2.7] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.3]+[<2.3]+[<2.3] - Run 2 (ug): [<2.3]+[<2.3]+[<2.3] - Run 3 (ug): [<2.3]+[<2.3]+[<2.3] 3-Nitroaniline [<3.5E-06] [<4.05] [<3.5E-06] [<4.05] [<3.5E-06] [<4.05] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<3.45]+[<3.45]+[<3.45] - Run 2 (ug): [<3.45]+[<3.45]+[<3.45] - Run 3 (ug): [<3.45]+[<3.45]+[<3.45] 2,4-Dinitrotoluene [<2.18E-06] [<2.53] [<2.18E-06] [<2.53] [<2.18E-06] [<2.53] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.15]+[<2.15]+[<2.15] - Run 2 (ug): [<2.15]+[<2.15]+[<2.15] - Run 3 (ug): [<2.15]+[<2.15]+[<2.15] 4-Nitrophenol [<1.93E-06] [<2.23] [<1.93E-06] [<2.23] [<1.93E-06] [<2.23] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.9]+[<1.9]+[<1.9] - Run 2 (ug): [<1.9]+[<1.9]+[<1.9] - Run 3 (ug): [<1.9]+[<1.9]+[<1.9] 2,4-Dinitrophenol [<2.53E-05] [<29.38] [<2.53E-05] [<29.38] [<2.53E-05] [<29.38] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<25]+[<25]+[<25] - Run 2 (ug): [<25]+[<25]+[<25] - Run 3 (ug): [<25]+[<25]+[<25] Acenaphthene [<2.33E-06] [<2.7] [<2.33E-06] [<2.7] [<2.33E-06] [<2.7] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.3]+[<2.3]+[<2.3] - Run 2 (ug): [<2.3]+[<2.3]+[<2.3] - Run 3 (ug): [<2.3]+[<2.3]+[<2.3] Dibenzofuran [<2.33E-06] [<2.7] [<2.33E-06] [<2.7] [<2.33E-06] [<2.7] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.3]+[<2.3]+[<2.3] - Run 2 (ug): [<2.3]+[<2.3]+[<2.3] - Run 3 (ug): [<2.3]+[<2.3]+[<2.3] Pentachlorobenzene [<2.13E-06] [<2.47] [<2.13E-06] [<2.47] [<2.13E-06] [<2.47] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.1]+[<2.1]+[<2.1] - Run 2 (ug): [<2.1]+[<2.1]+[<2.1] - Run 3 (ug): [<2.1]+[<2.1]+[<2.1] 2-Naphthylamine [<5.07E-06] [<5.88] [<5.07E-06] [<5.88] [<5.07E-06] [<5.88] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<5]+[<5]+[<5] - Run 2 (ug): [<5]+[<5]+[<5] - Run 3 (ug): [<5]+[<5]+[<5] 1-Naphthylamine [<5.07E-06] [<5.88] [<5.07E-06] [<5.88] [<5.07E-06] [<5.88] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<5]+[<5]+[<5] - Run 2 (ug): [<5]+[<5]+[<5] - Run 3 (ug): [<5]+[<5]+[<5] 2,3,4,6-Tetrachlorophenol [<2.28E-06] [<2.64] [<2.28E-06] [<2.64] [<2.28E-06] [<2.64] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.25]+[<2.25]+[<2.25] - Run 2 (ug): [<2.25]+[<2.25]+[<2.25] - Run 3 (ug): [<2.25]+[<2.25]+[<2.25] Fluorene [<2.23E-06] [<2.59] [<2.23E-06] [<2.59] [<2.23E-06] [<2.59] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.2]+[<2.2]+[<2.2] - Run 2 (ug): [<2.2]+[<2.2]+[<2.2] - Run 3 (ug): [<2.2]+[<2.2]+[<2.2] Diethyl phthalate [<2.13E-06] [<2.47] [<1.98E-06] [<2.29] [<1.21E-05] [<14.08] U.S. EPA Method 0010 with SW-846 Method 8270D DLL: Run 1 (ug): 2.55+1.9+[<1.85] - Run 2 (ug): [<1.85]+2.15+[<1.85] - Run 3 (ug): 22.3+11.8+[<1.85] 4-Chlorophenyl phenyl ether [<2.28E-06] [<2.64] [<2.28E-06] [<2.64] [<2.28E-06] [<2.64] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.25]+[<2.25]+[<2.25] - Run 2 (ug): [<2.25]+[<2.25]+[<2.25] - Run 3 (ug): [<2.25]+[<2.25]+[<2.25] 4-Nitroaniline [<1.52E-06] [<1.76] [<1.52E-06] [<1.76] [<1.52E-06] [<1.76] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.5]+[<1.5]+[<1.5] - Run 2 (ug): [<1.5]+[<1.5]+[<1.5] - Run 3 (ug): [<1.5]+[<1.5]+[<1.5] Azobenzene [<1.72E-06] [<2] [<1.72E-06] [<2] [<1.72E-06] [<2] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.7]+[<1.7]+[<1.7] - Run 2 (ug): [<1.7]+[<1.7]+[<1.7] - Run 3 (ug): [<1.7]+[<1.7]+[<1.7] 2-Methyl-4,6-dinitrophenol [<2.13E-06] [<2.47] [<2.13E-06] [<2.47] [<2.13E-06] [<2.47] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.1]+[<2.1]+[<2.1] - Run 2 (ug): [<2.1]+[<2.1]+[<2.1] - Run 3 (ug): [<2.1]+[<2.1]+[<2.1] Diphenylamine [<2.89E-06] [<3.35] [<2.89E-06] [<3.35] [<2.89E-06] [<3.35] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.85]+[<2.85]+[<2.85] - Run 2 (ug): [<2.85]+[<2.85]+[<2.85] - Run 3 (ug): [<2.85]+[<2.85]+[<2.85] 4-Bromophenyl phenyl ether [<2.18E-06] [<2.53] [<2.18E-06] [<2.53] [<2.18E-06] [<2.53] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.15]+[<2.15]+[<2.15] - Run 2 (ug): [<2.15]+[<2.15]+[<2.15] - Run 3 (ug): [<2.15]+[<2.15]+[<2.15] Phenacetin [<3.7E-06] [<4.29] [<3.7E-06] [<4.29] [<3.7E-06] [<4.29] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<3.65]+[<3.65]+[<3.65] - Run 2 (ug): [<3.65]+[<3.65]+[<3.65] - Run 3 (ug): [<3.65]+[<3.65]+[<3.65] Hexachlorobenzene [<2.23E-06] [<2.59] [<2.23E-06] [<2.59] [<2.23E-06] [<2.59] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.2]+[<2.2]+[<2.2] - Run 2 (ug): [<2.2]+[<2.2]+[<2.2] - Run 3 (ug): [<2.2]+[<2.2]+[<2.2] 1,3,5-Trinitrobenzene [<1.57E-06] [<1.82] [<1.57E-06] [<1.82] [<1.57E-06] [<1.82] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.55]+[<1.55]+[<1.55] - Run 2 (ug): [<1.55]+[<1.55]+[<1.55] - Run 3 (ug): [<1.55]+[<1.55]+[<1.55] 4-Aminobiphenyl [<2.03E-05] [<23.5] [<2.03E-05] [<23.5] [<2.03E-05] [<23.5] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<20]+[<20]+[<20] - Run 2 (ug): [<20]+[<20]+[<20] - Run 3 (ug): [<20]+[<20]+[<20] Pentachlorophenol [<5.02E-06] [<5.82] [<5.02E-06] [<5.82] [<5.02E-06] [<5.82] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<4.95]+[<4.95]+[<4.95] - Run 2 (ug): [<4.95]+[<4.95]+[<4.95] - Run 3 (ug): [<4.95]+[<4.95]+[<4.95] Phenanthrene [<2.13E-06] [<2.47] [<2.13E-06] [<2.47] [<2.13E-06] [<2.47] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.1]+[<2.1]+[<2.1] - Run 2 (ug): [<2.1]+[<2.1]+[<2.1] - Run 3 (ug): [<2.1]+[<2.1]+[<2.1] Pentachloronitrobenzene [<1.98E-06] [<2.29] [<1.98E-06] [<2.29] [<1.98E-06] [<2.29] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.95]+[<1.95]+[<1.95] - Run 2 (ug): [<1.95]+[<1.95]+[<1.95] - Run 3 (ug): [<1.95]+[<1.95]+[<1.95] Anthracene [<1.82E-06] [<2.12] [<1.82E-06] [<2.12] [<1.82E-06] [<2.12] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.8]+[<1.8]+[<1.8] - Run 2 (ug): [<1.8]+[<1.8]+[<1.8] - Run 3 (ug): [<1.8]+[<1.8]+[<1.8] Dinoseb [<1.72E-06] [<2] [<1.72E-06] [<2] [<1.72E-06] [<2] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.7]+[<1.7]+[<1.7] - Run 2 (ug): [<1.7]+[<1.7]+[<1.7] - Run 3 (ug): [<1.7]+[<1.7]+[<1.7] Di-n-butyl phthalate [<1.93E-06] [<2.23] [<1.82E-06] [<2.12] [<2.21E-06] [<2.57] U.S. EPA Method 0010 with SW-846 Method 8270D DLL: Run 1 (ug): 2.1+[<1.8]+[<1.8] - Run 2 (ug): [<1.8]+[<1.8]+[<1.8] - Run 3 (ug): 2.95+[<1.8]+[<1.8] Fluoranthene [<1.62E-06] [<1.88] [<1.62E-06] [<1.88] [<1.62E-06] [<1.88] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.6]+[<1.6]+[<1.6] - Run 2 (ug): [<1.6]+[<1.6]+[<1.6] - Run 3 (ug): [<1.6]+[<1.6]+[<1.6] Pyrene [<1.77E-06] [<2.06] [<1.77E-06] [<2.06] [<1.77E-06] [<2.06] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.75]+[<1.75]+[<1.75] - Run 2 (ug): [<1.75]+[<1.75]+[<1.75] - Run 3 (ug): [<1.75]+[<1.75]+[<1.75] p-(dimethylamino)azobenzene [<1.01E-06] [<1.18] [<1.01E-06] [<1.18] [<1.01E-06] [<1.18] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1]+[<1]+[<1] - Run 2 (ug): [<1]+[<1]+[<1] - Run 3 (ug): [<1]+[<1]+[<1] Speciated Semi Volatile Organic HAP Emission Data

EPA-HQ-OAR-2009-0234-DRAFT-1858.xls Spec SemiVol Org HAP Emis DataEIA Facility Code Facility Name Boiler ID 6043 Martin PMR2

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure Other Supporting Information Date of Testing 4/12/2010 4/12/2010 4/13/2010 Steam Output (1000 lb/hr) 5158 5147 5180 1000 lb/hr Total Heat Input (MMBtu/hr) 7110.5 7132.6 7197.8 MMBtu/hr Basis (W et/Dry) Wet Wet Wet N/A Exhaust Steam % Moisture 9.90 8.86 9.94 % Exhaust Flow Rate (acfm or dscfm) 1,305,376 1,410,918 1,557,569 dscfm Exhaust Temperature (deg C or deg F) 313.67 313.88 326.96 deg F

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate Sample 2 Fuel Input Rate Sample 3 Unit of Measure Fuel Flow Measurement Method Other Supporting Information No.6 Fuel Oil (residual or bunker C) 385200 386400 390000 lb/hour gas fuel meter

Compound (use drop down to define for as many rows as needed) Semi-Volatile Organic HAP Emission Rate Sample 1 (lb/MMBtu) Semi-Volatile Organic HAP Emission Rate Sample 1 (μg @ 7% O2) Semi-Volatile Organic HAP Emission Rate Sample 2 (lb/MMBtu) Semi-Volatile Organic HAP Emission Rate Sample 2 (μg @ 7% O2) Semi-Volatile Organic HAP Emission Rate Sample 3 (lb/MMBtu) Semi-Volatile Organic HAP Emission Rate Sample 3 (μg @ 7% O2) Test Method Used Other Supporting Information Speciated Semi Volatile Organic HAP Emission Data

Benz(a)anthracene [<1.47E-06] [<1.7] [<1.47E-06] [<1.7] [<1.47E-06] [<1.7] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.45]+[<1.45]+[<1.45] - Run 2 (ug): [<1.45]+[<1.45]+[<1.45] - Run 3 (ug): [<1.45]+[<1.45]+[<1.45] Butyl benzyl phthalate [<2.03E-06] [<2.35] [<2.03E-06] [<2.35] [<2.03E-06] [<2.35] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2]+[<2]+[<2] - Run 2 (ug): [<2]+[<2]+[<2] - Run 3 (ug): [<2]+[<2]+[<2] 2-Acetylaminofluorene [<2.43E-06] [<2.82] [<2.43E-06] [<2.82] [<2.43E-06] [<2.82] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.4]+[<2.4]+[<2.4] - Run 2 (ug): [<2.4]+[<2.4]+[<2.4] - Run 3 (ug): [<2.4]+[<2.4]+[<2.4] Chrysene [<1.52E-06] [<1.76] [<1.52E-06] [<1.76] [<1.52E-06] [<1.76] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.5]+[<1.5]+[<1.5] - Run 2 (ug): [<1.5]+[<1.5]+[<1.5] - Run 3 (ug): [<1.5]+[<1.5]+[<1.5] Bis(2-ethylhexyl)phthalate [<2.6E-06] [<3.02] [<2.69E-06] [<3.11] [<4.17E-06] [<4.84] U.S. EPA Method 0010 with SW-846 Method 8270D DLL: Run 1 (ug): 3.2+[<2.25]+[<2.25] - Run 2 (ug): [<2.25]+3.45+[<2.25] - Run 3 (ug): 6.8+3.3+[<2.25] Di-n-octyl phthalate [<2.33E-06] [<2.7] [<2.33E-06] [<2.7] [<2.33E-06] [<2.7] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.3]+[<2.3]+[<2.3] - Run 2 (ug): [<2.3]+[<2.3]+[<2.3] - Run 3 (ug): [<2.3]+[<2.3]+[<2.3] 7,12-Dimethylbenz(a)anthracene [<1.67E-06] [<1.94] [<1.67E-06] [<1.94] [<1.67E-06] [<1.94] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.65]+[<1.65]+[<1.65] - Run 2 (ug): [<1.65]+[<1.65]+[<1.65] - Run 3 (ug): [<1.65]+[<1.65]+[<1.65] 3-Methylcholanthrene [<2.08E-06] [<2.41] [<2.08E-06] [<2.41] [<2.08E-06] [<2.41] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.05]+[<2.05]+[<2.05] - Run 2 (ug): [<2.05]+[<2.05]+[<2.05] - Run 3 (ug): [<2.05]+[<2.05]+[<2.05] Benzo(b)fluoranthene [<1.77E-06] [<2.06] [<1.77E-06] [<2.06] [<1.77E-06] [<2.06] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.75]+[<1.75]+[<1.75] - Run 2 (ug): [<1.75]+[<1.75]+[<1.75] - Run 3 (ug): [<1.75]+[<1.75]+[<1.75] Benzo(k)fluoranthene [<2.08E-06] [<2.41] [<2.08E-06] [<2.41] [<2.08E-06] [<2.41] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.05]+[<2.05]+[<2.05] - Run 2 (ug): [<2.05]+[<2.05]+[<2.05] - Run 3 (ug): [<2.05]+[<2.05]+[<2.05] Benzo(a)pyrene [<1.37E-06] [<1.59] [<1.37E-06] [<1.59] [<1.37E-06] [<1.59] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.35]+[<1.35]+[<1.35] - Run 2 (ug): [<1.35]+[<1.35]+[<1.35] - Run 3 (ug): [<1.35]+[<1.35]+[<1.35] Indeno(1,2,3-cd)pyrene [<1.93E-06] [<2.23] [<1.93E-06] [<2.23] [<1.93E-06] [<2.23] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.9]+[<1.9]+[<1.9] - Run 2 (ug): [<1.9]+[<1.9]+[<1.9] - Run 3 (ug): [<1.9]+[<1.9]+[<1.9] Dibenz(a,h)anthracene [<2.13E-06] [<2.47] [<2.13E-06] [<2.47] [<2.13E-06] [<2.47] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.1]+[<2.1]+[<2.1] - Run 2 (ug): [<2.1]+[<2.1]+[<2.1] - Run 3 (ug): [<2.1]+[<2.1]+[<2.1] Benzo(g,h,i)perylene [<2.03E-06] [<2.35] [<2.03E-06] [<2.35] [<2.03E-06] [<2.35] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2]+[<2]+[<2] - Run 2 (ug): [<2]+[<2]+[<2] - Run 3 (ug): [<2]+[<2]+[<2]

EPA-HQ-OAR-2009-0234-DRAFT-1858.xls Spec SemiVol Org HAP Emis Data

### EIA

Facility Code Facility Name Boiler ID 6043 Martin PMR2

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure Other Supporting Information Date of Testing 4/13/2010 4/13/2010 4/13/2010 Steam Output (1000 lb/hr) 5191 5173 5184 1000 lb/hr Total Heat Input (MMBtu/hr) 7183.9 7186.5 7244.5 MMBtu/hr Basis (Wet/Dry) Dry Dry Dry N/A Exhaust Steam % Moisture 9.590379358 9.590379358 9.590379358 % Exhaust Flow Rate (acfm or dscfm) 1375744.499 1363830.505 1372591.485 dscfm Exhaust Temperature (deg C or deg F) 324 324 324 deg F

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate Sample 2 Fuel Input Rate Sample 3 Unit of Measure Fuel Flow Measurement Method Other Supporting Information No.6 Fuel Oil (residual or bunker C) 950 950 958 gallon/minute gas fuel meter

Emission Test Results Hydrogen Cyanide Emission Rate Sample 1 (lb/MMBtu) Hydrogen Cyanide

Emission Rate Sample 2 (lb/MMBtu) Hydrogen Cyanide

Emission Rate Sample 3 (lb/MMBtu) Test Method Used

(ex. U.S. EPA

Conditional Test Method 033) Other Supporting Information 0.000199327 0.000170677 0.000186602 U.S. EPA Method 320 #VALUE!

EPA-HQ-OAR-2009-0234-DRAFT-1858.xls HCN Em ission Data

### EIA

Facility Code Facility Name Boiler ID 6043 Martin PMR2

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure Other Supporting Information Date of Testing 4/13/2010 4/13/2010 4/13/2010 Steam Output (1000 lb/hr) 5191 5173 5184 1000 lb/hr Total Heat Input (MMBtu/hr) 7183.9 7186.5 7244.5 MMBtu/hr Basis (Wet/Dry) Dry Dry Dry N/A Exhaust Steam % Moisture 9.590379358 9.590379358 9.590379358 % Exhaust Flow Rate (acfm or dscfm) 1375744.499 1363830.505 1372591.485 dscfm Exhaust Temperature (deg C or deg F) 324 324 324 deg F

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate

Sample 2 Fuel Input Rate

Sample 3 Unit of Measure Fuel Flow Measurement Method Other Supporting

Information No.6 Fuel Oil (residual or bunker C) 950 950 958 gallon/minute gas fuel meter

Emission Test Results HCl Emission Rate Sample 1 (lb/MMBtu) HCl Emission Rate Sample 1 (ppmvd @ 7%O2) HCl Emission Rate

Sample 2 (lb/MMBtu) HCl Emission Rate Sample 2 (ppmvd @ 7%O2) HCl Emission Rate

Sample 3 (lb/MMBtu) HCl Emission Rate Sample 3 (ppmvd @ 7%O2) Test Method Used (ex. U.S. EPA Method 320) Other Supporting Information 0.00034016 0.26 0.000506774 0.39 0.000827925 0.63 U.S. EPA Method 320 #VALUE!

EPA-HQ-OAR-2009-0234-DRAFT-1858.xls HCl Emission DataEIA

Facility Code Facility Name Boiler ID 6043 Martin PMR2

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure Other Supporting Information Date of Testing 4/13/2010 4/13/2010 4/13/2010 Steam Output (1000 lb/hr) 5191 5173 5184 1000 lb/hr Total Heat Input (MMBtu/hr) 7183.9 7186.5 7244.5 MMBtu/hr Basis (W et/Dry) Dry Dry Dry N/A Exhaust Steam % Moisture 9.590379358 9.590379358 9.590379358 % Exhaust Flow Rate (acfm or dscfm) 1375744.499 1363830.505 1372591.485 dscfm Exhaust Temperature (deg C or deg F) 324 324 324 deg F

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate Sample 2 Fuel Input Rate Sample 3 Unit of Measure Fuel FlowMeasurement Method Other Supporting Information No.6 Fuel Oil (residual or bunker C) 950 950 958 gallon/minute gas fuel meter

Emission Test Results HF Emission Rate Sample 1 (lb/MMBtu) HF Emission Rate Sample 1 (ppmvd @ 7% O2) HF Emission Rate Sample 2 (lb/MMBtu) HF Emission Rate Sample 2 (ppmvd @ 7% O2) HF Emission Rate Sample 3 (lb/MMBtu) HF Emission Rate Sample 3 (ppmvd @ 7% O2) Test Method Used (ex. U.S. EPA Method 18) Other Supporting Information 7.68697E-05 0.11 8.25525E-05 0.12 0.000127354 0.18 U.S. EPA Method 320 #VALUE!

EPA-HQ-OAR-2009-0234-DRAFT-1858.xls HF Emission Data