## Cover Letter

Jim Alwood, (202) 564-8974 The following is our PMN submittal for {LOREX X-14-2 - Siloxanes and Silicones, 3-[(2-aminoethyl)amino)propyl Me, di-Me, reaction products with cadmium zinc selenide sulfide, lauric acid and oleylamine Per 10-7-14 Discussion Summary of LoRex Testing Follow-up for X-14-0001 /0002 (Originally Items 1-5) Revised follow-up testing plan as follows: 1) Transmission electron microscopy for size, shape analysis and size distribution of the nanoparticles. Provide images. 2) X-ray diffraction of the nanoparticles for presence of crystalline phases. 3) Surface chemistry, including elemental composition, by XPS. Attachment 15 contains the results for 1-3 4) Weathering test for final product encapsulated in silicone polymer per separate discussion/sample set. Note: We have provided additional testing data per our conversation on 10/20 and includes 3M test data as well as the methodologies used. Attachment 12-18 contain current weathering data on the 3M Film sent out for testing by 3M and by Nanosys. We also added to the Nanosys test results how the sample was prepared. Attachment 16-18 also have the method to prepare the 3M Film before testing to meet regulatory requirements per test method. Attachment 19-26 contain the methodologies referenced in the weathering data reports: Attachment 12-18. We do not have the full copy of the aquatic test method, but did provide the report as a separate file (Attachment 16) and method as described in California Code of Regulation (Attachment 20) Attachments Attachment		General Description			File Name					Pages	Section Reference Attachment 1	Process Flow 			QD Ligand Exchange Process 20140520 CBI Rev 1.pdf 	4	Pt.2, Sec.A, 1d. Attachment 2	Worker Activity Steps 			X-12-0005 QD in Aminosilicone Steps Page 9 (EPA Submittal-	3	Pt.2, Sec.A, End Attachment 3	Customer Process 			QDEF - Customer - QD Ligand Exchange Process 20140520 	1	Pt.2, Sec.B, 1a. Attachment 4	IES Order Results 			IES Order Results 380884-CBI.pdf 			2	Pt.I, Sec.B, 1c. Attachment 5	QD in Aminosilicone SDS 			GEN II - QD Concentrate in Aminosilicone Greater Than 1 	13 Attachment 6	Client Worker Exposure 			GEN II Aminosilione OYA Client Worker Exposure CBI.pdf 	1	Pt.2, Sec.B, End Attachment 7	Adsorbtion Data 			Appendix A Absorption.doc 			1	Worksheet: Adsorption / Coefficient Attachment 8	Thermogravimetric Analysis Data 		Appendix B TGA Data.doc 				1	Worksheet: Other Property (Thermogravimetric Analysis ) Attachment 9	TEM Images 				TEM Images.pdf 				20	Worksheet: Particle size distribution Attachment 10	Chemical Structure Diagram 		Chemical Structure Diagram -Gen II QD Aminosilicone 	1	Pt.I, Sec.B, 1e. Attachment 11	QDEF Film Consturction 			2014-10-20, QDEF Film Construction for PMN 		4

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### Attachment 12	3M TCLP Test Results 			E12-0117 Final Report QDEF 			19

Attachment 13	3M QDEF Surface Wipe Sample Lab Results 	E13-0646 Final Report Attachment B - SGS Report.pdf 0 Attachment 14	3M Wipe Sampling Preparation Results 		E13-0646 Final Report.pdf 			15 Attachment 15	LOREX Requested Test Results 		PMN Testing Followup_Updated-			5 Attachment 16	Nanosys Aquatic Testing Results 		Aquatic Screening -QDEF Test DATA CBI Rev 2.pdf 		6 Attachment 17	Nanosys QDEF Test Data 			QDEF Test DATA CBI.pdf 				19 Attachment 18	Nanosys Additional Metals QDEF Test 		1306127 OTIS Inst Rev 3 -CBI.pdf 			23 Attachment 19	TTLC and STLC Test Method 		22 CCR Appendix II Appendix II 			4 Attachment 20	CA DTSC Toxicity 			Acute Aquatic Test General Description.pdf 		1 Attachment 21	METHOD 1311 TOXICITY CHARACTERISTIC 	1311.pdf 					35 Attachment 22	METHOD 3010A ACID DIGESTION OF AQUEOUS SAMPLES AND EXTRACTS FOR 		3010a.pdf 		5 Attachment 23	METHOD 3520C CONTINUOUS LIQUID-LIQUID EXTRACTION 			3520c.pdf		8 Attachment 24	METHOD 7470A MERCURY IN LIQUID WASTE (MANUAL COLD-VAPOR TECHNIQUE)	7470a.pdf 6 Attachment 25	METHOD 8260B VOLATILE ORGANIC COMPOUNDS BY GAS CHROMATOGRAPHY/ 	8260b.pdf 86 Attachment 26	METHOD 8270D SEMIVOLATILE ORGANIC COMPOUNDS BY GAS 			8270d.pdf 		72 After you have had time to review we would like to set up a conference call to review the weathering documents, so that we are all on the same page. Thanks, Troy Troy Christensen, PE Otis Institute, Inc. 415-734-0186

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### Pay.gov Tracking ID: 25HTFKQP - Agency Tracking ID: 74689549038 NANO141022466853487 NAN001

X

X X

X

X

X
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### X



## X

Page 4 SANITIZED SUBMISSIONTony Soriano Director, Equipment Engineering & Facilities NANOSYS 233 S Hillview Drive Milpitas CA 95035 tsoriano@nanosysinc.com Troy Christensen Managing Principal Otis Institute, Inc. 185 Berry Street #5509 San Francisco CA 94107 troy@otisinstitute.com 415-734-0186

Bob Dubrow Director of Chemistry Nanosys, Inc 233 S Hillview Drive Milpitas CA 95035 bdubrow@nanosysinc.com 408-240-6711



## X X
X
X

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## X

XXX 

## X

XXX 

## X 380884 CAS_Page Intentionally Blank.pdf 

### unspecified
See Attachment 010 (Chemical Structure Diagram - Blank.pdf)

Chemical Structure Diagram - Blank.pdf

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XXX

XXX 

## X

X

X

Page 7 SANITIZED SUBMISSIONPage 8 SANITIZED SUBMISSIONPage 9 SANITIZED SUBMISSIONQuantum Dot in Aminosilicone

Quantum Dot in Aminosilicone

Cadmium selenide zinc sulfide dodecanoic acid and amine in Amino Functional Silicone Fluid

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### XXX XXX 

## X

X See continuation page. id: <P7SC2bC1> Component in an optical down converter 100 50 XXX XXX XXX XXX 

### X

Page 11 SANITIZED SUBMISSIONP7SC2bC1 Part I, Section C, 2.b. Generic use description

The Quantum Dot Matrix material is composed of high efficiency quantum dot phosphors. Larger than a water molecule, but smaller than a virus, these tiny phosphors convert blue light from a standard gallium nitride light-emitting diode into different wavelengths based upon their size. Larger dots emit longer wavelengths (red), while smaller dots emit shorter wavelengths (green). Blending together a mix of dot colors allows Nanosys to engineer a new spectrum of light. This allows liquid crystal display manufacturers to accurately match their light-emitting diode backlight to their light crystal display color filters to achieve the best possible color and efficiency performance. The result is professional photo and cinema level color performance in handheld devices, monitors, televisions, etc.

Page 12 SANITIZED SUBMISSION

## X

40 6 1250 

## 1

XXX 

## X Nanosys, Inc 233 S Hillview Dr Milpitas Santa Clara CA 95035

Page 13 SANITIZED SUBMISSIONSee Attachment 001 (QD Ligand Exchange Process 20140520 Sanitized Rev 1.pdf)

QD Ligand Exchange Process 20140520 Sanitized Rev 1.pdf

Page 14 SANITIZED SUBMISSIONX-12-0005 QD in Aminosilicone Steps Page 9 (EPA Submittal-Santizied).pdf

XXX XXX XXX 3 3 255 

### X X
See continuation page. id: <P9SA2(1)C1R2> XXX XXX 1 1 255 

### X
See continuation page. id: <P9SA2(1)C1R3> See continuation page. id: <P9SA2(3)C1R3> See continuation page. id: <P9SA2(5)C 3 1 255
See continuation page. id: <P9SA2(1)C1R4> See continuation page. id: <P9SA2(3)C1R4> See continuation page. id: <P9SA2(5)C 3 1 255

XXX XXX XXX 1 .25 255 

### X X

XXX XXX XXX 1 .25 255 

### X X

XXX XXX XXX 1 0.25 255 

### X X

See continuation page. id: <P9SA2(1)C1R8> XXX XXX 1 .25 255 

### X
P-3	Final product is then transferred to the final packaging 1L bottle, 5L bottle or 20L Keg. XXX XXX 1 3 255 

### X
See continuation page. id: <P9SA2(1)C1R10> XXX XXX 2 2 255 

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X

Page 15 SANITIZED SUBMISSION

## (1)

See continuation page. id: <P9SA2(1)C1R11> XXX XXX 1 .1 255 

### X

GEN II-L4	All tanks and lines are cleaned with a clean in place system using Toluene at 50 C. See continuation page. id: <P9SA2(3)C1R12> 0.01% of residual quantum dots 1 .25 255
See continuation page. id: <P9SA2(1)C1R13> See continuation page. id: <P9SA2(3)C1R13> 0.01% of residual quantum dots 1 1 255
See continuation page. id: <P9SA2(1)C1R14> XXX XXX 2 2 255 

### X

XXX XXX XXX 2 2 255 

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See continuation page. id: <P9SA2(1)C1R16> XXX XXX 2 2 255 

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Page 16 SANITIZED SUBMISSIONP9SA2(1)C1R2 Part II, Section A, 2.(1) Worker Activity, Row 2

LS-L3	Stir at 30C for 18 hours while pulling vacuum to remove toluene. After toluene removal material is poured from flask into storage containers.

Page 17 SANITIZED SUBMISSIONP9SA2(1)C1R3 Part II, Section A, 2.(1) Worker Activity, Row 3

LS-L4	Laboratory glassware is placed into a 30% Potassium Hydroxide (KOH) / 70% Isopropyl Alcohol (IPA) base bath for a minimum of thirty minutes.

Page 18 SANITIZED SUBMISSIONP9SA2(3)C1R3 Part II, Section A, 2.(3) Prot. Equipment, etc., Row 3

Splash protection including gloves (PVC/Butyl/Neoprene outer gloves in combination with inner nitrile gloves), safety glasses, splash shield, lab coat and splash apron.

Page 19 SANITIZED SUBMISSIONP9SA2(5)C1R3 Part II, Section A, 2.(5) Physical Forms / % new substance, Row 3

0.05% of residual QD in Aminosilicone

Page 20 SANITIZED SUBMISSIONP9SA2(1)C1R4 Part II, Section A, 2.(1) Worker Activity, Row 4

LS-L5	Retrieve glassware and pour off any residual base bath and gently submerge into sodium bicarbonate rinse bath to neutralize the 30% Potassium Hydroxide (KOH) / 70% Isopropyl Alcohol (IPA).

Page 21 SANITIZED SUBMISSIONP9SA2(3)C1R4 Part II, Section A, 2.(3) Prot. Equipment, etc., Row 4

Splash protection including gloves (PVC/Butyl/Neoprene outer gloves in combination with inner nitrile gloves), safety glasses, splash shield, lab coat and splash apron.

Page 22 SANITIZED SUBMISSIONP9SA2(5)C1R4 Part II, Section A, 2.(5) Physical Forms / % new substance, Row 4

0.05% of residual QD in Aminosilicone

Page 23 SANITIZED SUBMISSIONP9SA2(1)C1R8 Part II, Section A, 2.(1) Worker Activity, Row 8

P-2	Collect a sample from vessel. Then QC for OD, , , FWHM, QY, GC, 10C storage, and pair it with a counterpart color concentrate for film casting. If QC results pass, continue to keg filling.

Page 24 SANITIZED SUBMISSIONP9SA2(1)C1R10 Part II, Section A, 2.(1) Worker Activity, Row 10

P-4	Prepare container for shipping. Use a Mylar bag to bag the container for shipment. Add O2 indicator tablets and O2 absorbent tablet. Seal Mylar bag with heat sealer.

Page 25 SANITIZED SUBMISSIONP9SA2(1)C1R11 Part II, Section A, 2.(1) Worker Activity, Row 11

P-5	Clean bag with IPA wipes and setup box for shipping container(s). Included are MSDS and CofA

Page 26 SANITIZED SUBMISSIONP9SA2(3)C1R12 Part II, Section A, 2.(3) Prot. Equipment, etc., Row 12

This is a closed system and personnel where lab coat, gloves, safety glasses, and face shield with connecting and discounting lines

Page 27 SANITIZED SUBMISSIONP9SA2(1)C1R13 Part II, Section A, 2.(1) Worker Activity, Row 13

GEN II-L5	All Transfer tanks and flexible lines are taking to the stationary pumped cleaning system using Toluene.

Page 28 SANITIZED SUBMISSIONP9SA2(3)C1R13 Part II, Section A, 2.(3) Prot. Equipment, etc., Row 13

This is a closed system and personnel where lab coat, gloves, safety glasses, and face shield with connecting and discounting lines

Page 29 SANITIZED SUBMISSIONP9SA2(1)C1R14 Part II, Section A, 2.(1) Worker Activity, Row 14

QAQC-1	Quality Control --Dilute 20μL of this solution in 4 mL of hexane. Filter and determine the optical density using the UV/vis spectrometer. Material is placed into cuvette in preparation for removal from glove box. Once analysis is complete liquid is discarded into solvent waste.

Page 30 SANITIZED SUBMISSIONP9SA2(1)C1R16 Part II, Section A, 2.(1) Worker Activity, Row 16

QAQC-3	Pour the 20g sample into the smaller well of a 50mL cartridge. Pour Epoxy Part A into the larger well of the 50mL cartridge to about the same level and close both wells. Dispense cartridge into a thinky cup to level the two sides and to remove the air from the cartridge. Dispense about 4g of mixed material into a thinky cup and wait the required aging time for the sample. Dispense aged sample onto film and wait an additional aging time. Coat film using the roller apparatus.

Page 31 SANITIZED SUBMISSIONX-12-0005 QD in Aminosilicone Steps Page 9 (EPA Submittal-Santizied).pdf

LS-L4 0 0.005 kg/batch Off-site Incineration See continuation page. id: <P9ASA3(5a)C1R1> 0
LS-L5 0 0.005 kg/batch Off-site Incineration See continuation page. id: <P9ASA3(5a)C1R2> 0

P-1 0 .01 kg/batch Off-site Incineration See continuation page. id: <P9ASA3(5a)C1R3> 0

P-2 0 0.005 kg/batch Off-site Incineration See continuation page. id: <P9ASA3(5a)C1R4> 0

P-5 0 0.005 kg/batch Off-site Incineration See continuation page. id: <P9ASA3(5a)C1R5> 0

GEN IIL4 0 0.1 kg/batch Off-site Incineration See continuation page. id: <P9ASA3(5a)C1R6> 0

GEN IIL5 0 0.01 kg/batch Off-site Incineration See continuation page. id: <P9ASA3(5a)C1R7> 0
QAQC1 0 0.005 kg/batch Off-site Incineration See continuation page. id: <P9ASA3(5a)C1R8> 0

Page 32 SANITIZED SUBMISSIONP9ASA3(5a)C1R1 Part II, Section A, B.(5a) Control Technology & Efficiency, Row 1

QD with aminosilicone containated solvent and wipes are sent to a permited HW incinerator for disposal.

Page 33 SANITIZED SUBMISSIONP9ASA3(5a)C1R2 Part II, Section A, B.(5a) Control Technology & Efficiency, Row 2

QD with aminosilicone containated solvent and wipes are sent to a permited HW incinerator for disposal.

Page 34 SANITIZED SUBMISSIONP9ASA3(5a)C1R3 Part II, Section A, B.(5a) Control Technology & Efficiency, Row 3

QD with aminosilicone containated filter and wipes are sent to a permited HW incinerator for disposal.

Page 35 SANITIZED SUBMISSIONP9ASA3(5a)C1R4 Part II, Section A, B.(5a) Control Technology & Efficiency, Row 4

QD with aminosilicone sample disposal and wipes are sent to a permited HW incinerator for disposal.

Page 36 SANITIZED SUBMISSIONP9ASA3(5a)C1R5 Part II, Section A, B.(5a) Control Technology & Efficiency, Row 5

QD with aminosilicone contaminated wipes are sent to a permited HW incinerator for disposal.

Page 37 SANITIZED SUBMISSIONP9ASA3(5a)C1R6 Part II, Section A, B.(5a) Control Technology & Efficiency, Row 6

Solvent from CIP contamined with QD in Aminosilicone and wipes are sent to a permited HW incinerator for disposal.

Page 38 SANITIZED SUBMISSIONP9ASA3(5a)C1R7 Part II, Section A, B.(5a) Control Technology & Efficiency, Row 7

Solvent from transfer tank/hose cleaning contamined with QD in Aminosilicone and wipes are sent to a permited HW incinerator for disposal.

Page 39 SANITIZED SUBMISSIONP9ASA3(5a)C1R8 Part II, Section A, B.(5a) Control Technology & Efficiency, Row 8

Waste samples contamined with QD in Aminosilicone and wipes are sent to a permited HW incinerator for disposal.

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### XXX 

## X

See Attachment 003 (QDEF - Customer - QD Ligand Exchange Process 20140520 CBI Rev 1.pdf)

QDEF - Customer - QD Ligand Exchange Process 20140520 CBI Rev 1.pdf QD Matrix with Aminosilicone is applied using a dispensing system that mixes the QD Matrix with Aminosilicone with Epoxy Part A and Part B. The mixture is dispensed in-between two plastic films and allowed to cure. The resulting product is a QD Efficiency Film (QDEF).

Page 41 SANITIZED SUBMISSIONP10SB1(a)(4)1 Part II, Section B, 1(a)(4). Operation Site Locations

XXX

Page 42 SANITIZED SUBMISSIONGEN II Aminosilione OYA Client Worker Exposure Sanitized.pdf

C1 2 2 255 XXX XXX XXX

1 0 0.002 QD with aminosilicone containated solvent and wipes are sent to a permited HW incinerator for disposal. 

### X

Page 43 SANITIZED SUBMISSIONPage 44 SANITIZED SUBMISSION001 Sanitized Process Flow QD Ligand Exchange Process 20140520 Sanitized Rev 1.pdf Pt.2, Sec.A, 1d. 4
002 Worker Activity Steps - Sanitized X-12-0005 QD in AminosiliconeSteps Page 9 (EPA SubmittalPt.2, Sec.A, End 3 003 Customer Process QDEF - Customer - QD Ligand Exchange Process 20140520 Pt.2, Sec.B, 1a. 1
004 Santizied IES Order Results CAS_Page Intentionally Blank.pdf Pt.I, Sec.B, 1c. 2 005 Sanitized SDS GEN II - QD Concentrate in Aminosilicone Greater Than 1 13 006 Santized Client Worker Exposure GEN II Aminosilione OYA Client Worker Exposure Sanitized.pdf Pt.2, Sec.B, End 1 007 Adsorbtion Data Appendix A Absorption.doc 1 008 Thermogravimetric Analysis Data Appendix B TGA Data.doc Worksheet: Other Property (Thermogravimetric Analysis ) 1 009 TEM Images TEM Images.pdf Worksheet: Particle size distribution 20 010 Sanitized Chemical Sturcure Diagram Chemical Structure Diagram - Blank.pdf Pt.I, Sec.B, 1e. 1 011 QDEF Film Consturction 2014-10-20, QDEF Film Construction for PMN 4
012 3M TCLP Test Results E12-0117 Final Report QDEF 19 013 3M QDEF Surface Wipe Sample Lab Results E13-0646 Final Report Attachment B - SGS Report.pdf 0 014 3M Wipe Sampling Preparation Results E13-0646 Final Report.pdf 15
015 Nanosys LOREX Request Test Results PMN Testing Followup_Updated- 5 016 Sanitized Aquatic Testing Results Aquatic Screening - QDEF Test DATA Sanitized.pdf 6 017 Sanitized Nanosys QDEF Data QDEF Test DATA Sanitized.pdf 19 018 Sanitized Nanosys Additional Metals QDEF Test 1306127 OTIS Inst Rev 2 - Sanitized.pdf 23 019 TTLC and STLC Test Method 22 CCR Appendix II Appendix II 4 020 CA DTSC Toxicity Acute Aquatic Test General Description.pdf 1 021 METHOD 1311 TOXICITY CHARACTERISTIC 1311.pdf 35 

## X
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## (1)

022 METHOD 3010A ACID DIGESTION OF AQUEOUS SAMPLES AND EXTRACTS FOR 3010a.pdf 5 023 METHOD 3520C CONTINUOUS LIQUIDLIQUID EXTRACTION 3520c.pdf 8 024 METHOD 7470A MERCURY IN LIQUID WASTE (MANUAL COLD-VAPOR TECHNIQUE) 7470a.pdf 6
025 METHOD 8260B VOLATILE ORGANIC COMPOUNDS BY GAS CHROMATOGRAPHY/ 8260b.pdf 86 026 METHOD 8270D SEMIVOLATILE ORGANIC COMPOUNDS BY GAS 8270d.pdf 72

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## X Measured

0.996-0.897 Measured

999 Measured 20 Hexane <1 Measured 20

Estimate

XXX XXX 

## X X 009 2.75-9 Measured 200 - 1000 cSt Measured Viscosity

Page 47 SANITIZED SUBMISSIONTypical Concentration "Cd 9100 ppm Se 1700ppm Zn 14500 ppm S not reported" Measured Thermogravimetric Analysis 

## X 008 85-95 % Voliatle at 600 C Measured Solulbility Ethanol 20C 999 g/l Measured

Page 48 SANITIZED SUBMISSION

## ATTACHMENT HEADER SHEET

Attachment Number 001 Attachment Name Sanitized Process Flow 

## Associated PMN Section Number

Pt.2, Sec.A, 1d.
Does not contain CBI 

## Report Number NANO141022466853487

## ATTACHMENT HEADER SHEET

Attachment Number 002 Attachment Name Worker Activity Steps - Sanitized 

## Associated PMN Section Number

Pt.2, Sec.A, End
Does not contain CBI 

## Report Number NANO141022466853487

## ATTACHMENT HEADER SHEET

Attachment Number 003 Attachment Name Customer Process 

## Associated PMN Section Number

Pt.2, Sec.B, 1a.
Does not contain CBI 

## Report Number NANO141022466853487

## ATTACHMENT HEADER SHEET

Attachment Number 004 Attachment Name Santizied IES Order Results 

## Associated PMN Section Number

Pt.I, Sec.B, 1c.
Does not contain CBI 

## Report Number NANO141022466853487

## ATTACHMENT HEADER SHEET

Attachment Number 005 Attachment Name Sanitized SDS 

## Associated PMN Section Number

N/A
Does not contain CBI 

## Report Number NANO141022466853487

## ATTACHMENT HEADER SHEET

Attachment Number 006 Attachment Name Santized Client Worker Exposure 

## Associated PMN Section Number

Pt.2, Sec.B, End
Does not contain CBI 

## Report Number NANO141022466853487

## ATTACHMENT HEADER SHEET

Attachment Number 007 Attachment Name Adsorbtion Data 

## Associated PMN Section Number

N/A
Does not contain CBI 

## Report Number NANO141022466853487

## ATTACHMENT HEADER SHEET

Attachment Number 008 Attachment Name Thermogravimetric Analysis Data 

## Associated PMN Section Number Worksheet: Other Property (Thermogravimetric Analysis )

Does not contain CBI 

## Report Number NANO141022466853487

## ATTACHMENT HEADER SHEET

Attachment Number 009 Attachment Name TEM Images 

## Associated PMN Section Number Worksheet: Particle size distribution
Does not contain CBI 

## Report Number NANO141022466853487

## ATTACHMENT HEADER SHEET

Attachment Number 010 Attachment Name Sanitized Chemical Sturcure Diagram 

## Associated PMN Section Number

Pt.I, Sec.B, 1e.
Does not contain CBI 

## Report Number NANO141022466853487

## ATTACHMENT HEADER SHEET

Attachment Number 011 Attachment Name QDEF Film Consturction 

## Associated PMN Section Number

N/A
Does not contain CBI 

## Report Number NANO141022466853487

## ATTACHMENT HEADER SHEET

Attachment Number 012 Attachment Name 3M TCLP Test Results 

## Associated PMN Section Number

N/A
Does not contain CBI 

## Report Number NANO141022466853487

## ATTACHMENT HEADER SHEET

Attachment Number 013 Attachment Name 3M QDEF Surface Wipe Sample Lab Results 

## Associated PMN Section Number

N/A
Does not contain CBI 

## Report Number NANO141022466853487

## ATTACHMENT HEADER SHEET

Attachment Number 014 Attachment Name 3M Wipe Sampling Preparation Results 

## Associated PMN Section Number

N/A
Does not contain CBI 

## Report Number NANO141022466853487

## ATTACHMENT HEADER SHEET

Attachment Number 015 Attachment Name Nanosys LOREX Request Test Results Sanitized 

## Associated PMN Section Number

N/A
Does not contain CBI 

## Report Number NANO141022466853487

## ATTACHMENT HEADER SHEET

Attachment Number 016 Attachment Name Sanitized Aquatic Testing Results 

## Associated PMN Section Number

N/A
Does not contain CBI 

## Report Number NANO141022466853487

## ATTACHMENT HEADER SHEET

Attachment Number 017 Attachment Name Sanitized Nanosys QDEF Data 

## Associated PMN Section Number

N/A
Does not contain CBI 

## Report Number NANO141022466853487

## ATTACHMENT HEADER SHEET

Attachment Number 018 Attachment Name Sanitized Nanosys Additional Metals QDEF Test 

## Associated PMN Section Number

N/A
Does not contain CBI 

## Report Number NANO141022466853487

## ATTACHMENT HEADER SHEET

Attachment Number 019 Attachment Name TTLC and STLC Test Method 

## Associated PMN Section Number

N/A
Does not contain CBI 

## Report Number NANO141022466853487

## ATTACHMENT HEADER SHEET

Attachment Number 020 Attachment Name CA DTSC Toxicity 

## Associated PMN Section Number

N/A
Does not contain CBI 

## Report Number NANO141022466853487

## ATTACHMENT HEADER SHEET

Attachment Number 021 Attachment Name METHOD 1311 TOXICITY CHARACTERISTIC LEACHING PROCEDURE



## Associated PMN Section Number

N/A
Does not contain CBI 

## Report Number NANO141022466853487

## ATTACHMENT HEADER SHEET

Attachment Number 022 Attachment Name METHOD 3010A ACID DIGESTION OF AQUEOUS SAMPLES AND EXTRACTS FOR TOTAL METALS FOR ANALYSIS BY FLAA OR ICP SPECTROSCOPY 

## Associated PMN Section Number

N/A
Does not contain CBI 

## Report Number NANO141022466853487

## ATTACHMENT HEADER SHEET

Attachment Number 023 Attachment Name METHOD 3520C CONTINUOUS LIQUID-LIQUID EXTRACTION



## Associated PMN Section Number

N/A
Does not contain CBI 

## Report Number NANO141022466853487

## ATTACHMENT HEADER SHEET

Attachment Number 024 Attachment Name METHOD 7470A MERCURY IN LIQUID WASTE (MANUAL COLD-VAPOR TECHNIQUE)



## Associated PMN Section Number

N/A
Does not contain CBI 

## Report Number NANO141022466853487

## ATTACHMENT HEADER SHEET

Attachment Number 025 Attachment Name METHOD 8260B VOLATILE ORGANIC COMPOUNDS BY GAS CHROMATOGRAPHY/ MASS SPECTROMETRY (GC/MS) 

## Associated PMN Section Number

N/A
Does not contain CBI 

## Report Number NANO141022466853487

## ATTACHMENT HEADER SHEET

Attachment Number 026 Attachment Name METHOD 8270D SEMIVOLATILE ORGANIC COMPOUNDS BY GAS CHROMATOGRAPHY/MASS SPECTROMETRY (GC/MS) 

## Associated PMN Section Number

N/A
Does not contain CBI 

## Report Number NANO141022466853487