# Exhaust Emissions Sampling Dal Italia, LLC., Muskogee, OK Spray Dryer, Kiln Scrubber, and Trim Kiln Exhausts

. December 6 - 8, 2005 Arrnstrong Environmental, Inc. Project W-2485-05

Report Prepared For: Bob Hurt Daltile 7834 C. F. Hawn Freeway Dallas, TX 75217

Report Prepared December 21, 2005 By: Armstrong Environmental, Inc. 

# 7715 Sovereign Row Dallas, Texas 75247 (214) 631-0021

# TABLE OF CONTENTS

I. Introduction
U. Summary

III. Procedures
I'V. Appendices



# A. Calculation Summaries

B. Continuous Emissions Monitor Summaries

C. Analytical Summaries

D. Field Data Sheets

E. Equipment Calibrations

F. Standard Gas Certifications



# G. S02 Interfernce Summaries Page

1



# 2-9

10- 16

17 -.34

35 - 129

130 - 217

218 -238

~ 

# 239 - 252

253 - 264

265 - 323

## SUMMARY OF EMISSIONS TEST DATA

Table 

# : 4 Plant 

# : Daltile, Muskogee, OK Location 

# : Kiln Scrubber Exhaust Operator 

# : D. Barrera Test Date 

# : 7•Dec•05 Repetition 

# : 1 2 3

STACK GAS Temperature, F 138.3 138.4 138.2 Velocity, fps 29.06 29.06 29.67 Volume Flow, acfm 33664.7 33669.9 34368.6

scfm 22612.7 22453.4 22833.2 scfh 1356762 1347206 1369993 Moisture, 

# % 23.80% 24.33% 24.40% CO2, 

# % 3.00 3.00 3.00 02, 

# % 16.00 16.00 16.00

SAMPLE Start Time, hrs:min 10:10 AM 12:22 PM 2:05 PM Finish Time, hrs:rnin 11:17 AM 1:26 PM 3:10 PM Sample Volume, scf 39.247 38.933 36.583 Isokinetic Ratio, 

# % 104.802 104.7015 96.745


## CARBON MONOXIDE Concentration, ppm 234.48 230.63 Emissions, Ibs/hr 23.12497 22.58507



## NITROGEN OXIDE AS 

## NO2 Concentration, ppm 33.02 33.23 Emissions, Ibs/hr 5.34998 5.346085



## VOC AS 

## C31-18 Concentration, ppm as C3H8, WET 47.17 45.70 Concentration, ppm as C3H8, WET 61.9013 60.39667 Emissions, Ibs/hr as C3H8 9.593337 9.294228 Emissions, Ibs/hr as C 7.849094 7.604368



## SULFUR DIOXIDE Concentration, ppm 0.073 0.225 Emissions, Ibs/hr 0.016456 0.050363



## HYDROGEN FLUORIDE Sample Weight, mg 0.22 0.72 0.24 Concentration, ppm 0.235891 0.789733 0.280929 Emissions, Ibs/hr 0.016617 0.055241 0.019983

CHLORINE Sample Weight, mg 0.00 0.00 0.00 Concentration, ppm 0 0 0 Emissions, Ibs/hr 0 0 0

HYDROGEN CHLORIDE Sample Weight, mg 0.87 0.70 0.64 Concentration, ppm 0.515243 0.415995 0.40519 Emissions, Ibs/hr 

# - 0.06624 0.053104 0.0526



# -n

## SUMMARY OF EMISSIONS TEST DATA

138.4 29.24 33881.2 22583.6 1355016 24.37% 3.00 16.00 1

10:10 AM 11:17 AM 39.193 105.0612

66.74 0.026275 . 5.087779

4.48 0.001764 0.341523

5.429302 Table : 3 Plant : Daltile, Muskogee, OK Location : Kiln Scrubber Exhausi Operator : R. Taylor Test Date : 7•Dec•05 Repetition :

STACK GAS Temperature, F Velocity, fps Volume Flow, acfm

scfm scfh Moisture, % CO2, % 02, %

SAMPLE Start Time, hrs:min Finish Time, hrs:min Sample Volume, scf Isokinetic Ratio, %

PARTICVLATE "ront Half amp e Weight, mg Concentration, gr/scf Emissions, Ibs/hr

Back Half Sample Weight, mg Concentration, gr/scf Emissions, Ibs/hr

Total Particulate, Ibs/hr

CARBON MONOXIDE Concentration, ppm Emissions, Ibs/hr

NITROGEN OXIDE AS NO2 Concentration, ppm Emissions, Ibs/hr



## VOC AS 

## C31-18 Concentration, ppm as C31-18, WET Concentration, ppm as C3H8, WET Emissions, Ibs/hr as C3H8 Emissions, Ibs/hr as C

SULFUR DIOXIDE Concentration, ppm Emissions, Ibs/hr 3

137.0 30.38 35191.8 23764.2 1425855 23.31% 3.00 16.00

2:05 PM 3:10 PM 40.964 104.3513

52.80 0.019888 4.052464

8.20 0.003089 0.62936

4.681824

236.52 24.51404

33.07 5.630942

46.13 60.15022 9.79668 8.015465

0.482 0.114187 2

137.1 28.73 33283.3 22204.8 1332289 24.47% 3.00 16.00

12:22 PM 1:26 PM 38.815 105.821

55.37 0.022011 4.190704

13.38 0.005319 1.012671

5.203375

7

## SUMMARY OF EMISSIONS TEST DATA

Table 

# : 5 Plant 

# : Daltile, Muskogee, OK Location 

# : Trim Kiln Exhaust Operator 

# : R. Taylor Test Date 

# : 8•Dec•05 Repetition 

# : 1 2 3

STACK GAS Temperature, F 485.0 486,2 486.5 Velocity, fps 79.43 77.96 79.05 Volume Flow, acfm 15602.0 15312.9 15527.1

scfm 8251.9 8097.6 8072.2 

# " scfh 495113 485857 484334 Moisture, 

# % 5.50% 5.40% 6.97% CO2, 

# % 2.50 2.50 2.50 02, 

# % 17.50 17.00 17.00

SAMPLE Start Time, hrs:min 11:20 AM 12:50 PM 2:20 PM Finish Time, hrs:min 11:24 AM 1:53 PM 3:22 PM Sample Volume, scf 51.241 49.860 50.057 Isokinetic Ratio, 

# % 98.90241 98.06889 98.76648

PARTICULATE Front Half Sample Weight, mg 30.30 29.31 31.01 Concentration, gr/scf 0.009124 0.009071 0.009559 Emissions, Ibs/hr 0,645556 0.629771 0.661595

Back Half Sample Weight, mg 26.33 24.41 20.19 Concentration, gr/scf 0.007929 0.007554 0.006224 Emissions, Ibs/hr 0.560973 0.524487 0.430751
Total Particulate, Ibs/hr 1.20653 1.154258 1.092346



## CARBON MONOXIDE Concentration, ppm 165.54 171.36 Emissions, Ibs/hr 5.957706 6.032906



## NITROGEN OXIDE AS 

## NO2 Concentration, ppm 30.29 30.92 Emissions, Ibs/hr 1.790916 1.788366



## VOC AS 

## C31-18 Concentration, ppm as C3H8, WET 138.61 128.32 Concentration, ppm as C3H8, DRY 146.6825 137.9369 Emissions, Ibs/hr as C3H8 8.295623 7.631187 Emissions, Ibs/hr as C 6.787328 6.243698

SULFUR DIOXIDE Concentration, ppm 85.25 77.13 Emissions, Ibs/hr 7.012816 6.206723



# :

## 2

485.1 78.24 15369.3 8160.6 489636 5.13°J o 2.50 17.00

12:50 PM 1:53 PM 49.488 97.36155

168.04 5.980783

29.59 1.730175

122.48 129.0969 7.220312 5.907528

71.45 5.812588

65.60 56.29141 1.431065 3

487.0. 78.26 15372.5 8053.7 483223 6.20% 2.50 17.00

2:20 PM 3:22 PM 49.298 98.27505

66.29 57.10798 1.43281

0.89 0.35 0.215143 0.083962 0.019417 0.007478 SUMMARY OF EMISSIONS TEST DATA

Table : 6 Plant : Daltile, Muskogee, OK Location : Trim Kiln Exhaust Operator : D. Barrera Test Date : 8•Dec•05 Repetition

STACK GAS Temperature, F Velocity, fps Volume Flow, acfm

scfm scfh Moisture, % CO2, o' f o 02, %

SAMPLE Start Time, hrs:min 11:20 AM Finish Time, hrs:min 11:24 AM Sample Volume, scf 49.306 I soki netic Ratio, % 96.81248

CARBON MONOXIDE Concentration, ppm Emissions, Ibs/hr 1

484.3 78.48 15415.3 8176.6 490598 5.30% 2.50 17.00

NITROGEN OXIDE AS NO2 Concentration, ppm Emissions, Ibs/hr

VOC AS C31-18 Concentration, ppm as C3H8, WET Concentration, ppm as C31-18, DRY Emissions, Ibs/hr as C3118 Emissions, Ibs/hr as C

SULFUR DIOXIDE Concentration, ppm Emissions, lbs/hr

HYDROGEN FLUORIDE Sample Weight, mg Concentration, ppm Emissions, Ibs/hr

CHLORINE Sample Weight, mg Concentration, ppm Emissions, Ibs/hr 73.10 62.96225 1.603799

0.48 0.115733 0.010465

HYDROGEN CHLORIDE Sample Weight, mg 92.77 92.97 85.60 Concentration, ppm 43.78239 43.71502 40.40418 Emissions, Ibs/hr 2.035316 2.028201 1.850039



# 2

# III. PROCEDURES

The procedure for emissions sampling followed USEPA test methods as detailed in Title 40: Code of Federal Regulations. The following methods were used:

Method Title 1 Sample and Velocity Traverses for Stationary Sources



# 2 Determination of Stack Gas Velocity and Volumetric Flow Rate (Type S

Pitot Tube)

3 Gas Analysis for CO2, 02, Excess Air and Dry Molecular Weight

5 Determination of Particulate Emissions from Stationary Sources

6C Determination of Sulfur Dioxide Emissions from Stationary Sources

(Instrumental Analyzer Procedure)

7E Determination of Nitrogen Oxides Emissions from Stationary Sources

(Instrumental Analyzer Procedure)

10 Determination of Carbon Monoxide Emissions from Stationary Sources

25A Determination of Total Gaseous Organic Concentration using a Flame

Ionization Analyzer

26A Determination of Hydrogen Halides and Halogens Emissions from

Stationary Sources

202 Determination of Condensible Particulate Bmissions from Stationary

Sources
02 and CO2 were determined using FyRite Analyzers.
Velocity and volumetric flow rates were determined at each locations as follows:

~ '^



### ~ , ~ F~~~Y~~~~ ~~ ~~~~ • a~~~e~'~fiA~'o~ ~ 

# s'> ~~N ~ ~ ~ 

# : ,. . t: " ~N~~~n~~u~ 

# ess ..

~ 

# r RQ

~ 

# iR Spray Dryer 24 12 per traverse 2.5 Kil.n Scrubber 20 10 per traverse 3.0 Trim Kiln 12 6 per traverse 5.0
HF, HCI, and Chlorine sampling was performed for a duration of 60 minutes. The sampling train was configured as follows:

0

# Glass Sampling Nozzle Heated Glass Lined Probe Heated teflon filter Impinger #1 - 100 mis 0.1 N H2SO4 Impinger #2 - 100 mis 0.1 N H2SO4 Impinger #3 

# - 100 mis 0.1 N NaOH 

# Impinger #4 - 100 rnls 0.1 N NaOH Impinger #5 - 200 grams silica Gel
Analysis for HF and HCl analysis was performed on the solution from the 1 st and 2nd impinger. Analysis for C12 was performed on the solution from the 3rd and 4th impingers. Analysis was performed using a Dionex LC20 IC/HPLC.
PM sampling was performed for a duration of 60 minutes. The sampling train was configured as follows:
Stainless Steel Sampling Nozzle Heated Glass Lined Probe Heated Glass Fiber Filter (Teflon Filter for Trim Kiln) Impinger # 1- 100 mis H20 Impinger #2 - 100 mis H20 Impinger #3 - 100 mis H20 Impinger #4 - Empty Impinger #5 200 grams silica gel
"Front-Half 'particulate analysis was performed on the probe wash, prefilter glassware, and the filter. "Back-half' particulate anaiysis was performed on the impinger solutions and related glassware by Methylene Chloride extractions of the impinger solutions (evaporated at room temperature) and total solids in the impinger solutions (evaporated at 105 degrees C).


# Continuous emissions were monitored for the Spray Dryer as follows:

r

~ " ✓ '?:y ' —P'

~ ~ i
, ~ c `
. •~ {, r .yi



### _ .~ 1 r. 

### ~ ?e.4i 

### ~ Y.1i 

### ~~ p2..
- ' jT
, i y ^ ~ ~ ~+'~ - •~ •-•
~ ;7 ,~ ,. , ~ y..si
`r 

### ~ '-'. k 

### ~~ .`.y,ia

- 

# a ~~ '.fi'y 

### ~ '1. 

### ~ ::;. 

### ~t~; 4,

~ i..tx ~^~ ;i7 

### ~ iLYfili' 

### ~~~ y f ` " y ~ ~ Y

.q ,

+~ b~-~~ A . I,

_ 

# Fuji 3300 CO a.nalyzer 0- 100 49.9 ppm, 99.1 ppm CO in N2 EPA Protocol 1 EcoPhysics 70S Nox Analyzer 0-60 25.5 ppm, 51.0 ppm Nox in N2 EPA Protocol 1 Western Research 721-AT S02 0- 110 50.1 ppm, 101 pprn S02 in N2

Anal zer EPA Protocol 1- ThermoEnvironmental 51 FID 0- 100 28.8 ppm, 48.8 ppm, and 89.2

analyzer ppm C3H8 in Air EPA Protocol 1



# Continuous emissions were monitored for the Kiln Scrubber as follows:

11,+fT ~~ YV .'{ 7 ~

~^ w ' d ';: ~.r. .`'f.M ~~ { ~ Y,i l . 1 - I

.



## , , - ~ I. 't .- t Ais

- Y N L • .1
, _.



## ~

~ ~ •t"' o - ?:*S :t` e, f

~ >..,1 [ i. 1 a i 

# Fuji 3300 CO analyzer 0- 500 200 ppm, 494 ppm CO in N2 EPA Protocol 1 EcoPhysics 70S Nox Analyzer 0-60 25.5 ppm, 51.0 ppm Nox in N2 EPA Protocol 1 Western Research 721-AT S02 0- 110 50.1 ppm, 101 ppm S02 in N2

Analyzer EPA Protocol 1 ThenmoEnvironmenta151 FID 0- 100 28.8 ppm, 48.8 ppm, and 89.2

analyzer ppm C3H8 in Air EPA Protocol 1



# Continuous emissions were monitored for the Trim Kiln as follows:

;{•f F y'ik'

~~ .1 k .7.

~ '^f a 4 , k- . y•,. - ~'~"'~ X ii `t [ ~ i -

~ w.1. ~ ~a y' Q, 

# Fuji 3300 CO analyzer 0- 500 200 ppm, 494 ppm CO in N2 EPA Protocol 1 EcoPhysics 70S Nox Analyzer 0-60 25.5 ppm, 51.0 ppm Nox in N2 EPA Protocol 1 Westem Research 721-AT S02 0- 110 50.1 ppm, 101 ppm S02 in N2

Analyzer EPA Protocol 1 ThermoEnvironmental 51 FID 0- 250 48.8 ppm, 89.2 ppm, and 200

analyzer ppm C3H8 in Air EPA Protocol I


# Sampling nozzles were measured with a microcaliper onsite prior to sampling.
The CO analyzer was operated following procedures in Method 6C. No ascai

- ite or silica gel was using inline of the sample.
The NOx converter was checked prior to sampling on the Spray Dryer and is documented in Appendix B. The trailer was then moved, and another converter check performed for both the Kiln Scrubber and Trim Kiln, since the analyzer was not turned off between tests.


# Schematics of the sampling locations are shown in Figures 1- 3. The schematic of the continuous emission monitor configuration is shown in Figure 4.

12

# Figure 2 - Kiln Scrubber Zxhaust

St-ick Diameter - 59.5 inches Point #1 -1.5 inches Point #2 - 4.9 inches. Point #3 - 8.7 inches Point #4 - 13.4 inches Point #5 - 20.3 inches Point #6 - 39.1 inciies 

## Point #7 - 46.1 inches Point #8 - 50.8 inches Point #9 - 54.6 incties Point #10 - 58 inches r-►

~

# Figure 3- Trim Kiin Exhaust

so1=



## 1801
,

1-1 

## Ln Stack Diameter - 24.5 Inches Po'mt #1 -1.1 inches Poin# #2 - 3.6 inches Poirk #3 - 7.25 inches Point #4 -1725 inches Poirtt #5 - 20.9 inches Point #6 - 23,4 irtches

# Figure 4 - CEM Configuration

Instack Filter, Heated Probe CO Anafyzer

Heated Sampfe Line

FID Analyaer 

# I NOx Anafyzer

S02 Anafyaer Heated Manifold 

# I Sample 

# I I
To interfernce Train Processor Calibration Poird Pump

1-." (31 

### Bias Calibration Span l.ine \,-,/ Sample processor consists of two short stem impirrgers followed by a 0.3 puynp micron filter

## EMISSION TEST SUMMARY

PLANT : Dal;ile, MuskoAee, OK DATE : 7-Dec•05 PLACE : Kiin Scrubber ExN,aust RUN# : 1 i4 j

~ 

### "
TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 26^.4 NOZZLE DIAMETER (INCH.) : 0.3127 PARTICULATE WEIGHT (Front half mg) : 0 METER COEFFICIENT (Y) : 0.989 PARTICULATE WEIGHT (Back half mg) : 0 PITOT COEFFICIENT (Cp) : 0.84- STATIC PRESSURE (in. H20) : .0.2 GAS METER VOL.(Cu.Ft.) : 37.828 PERCENT CO2 3 BAROMETRIC PRESSURE 29.9 PERCENT 02 16 PERCENT CO 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 59.5 STACK LENGTH(inchs) : STACK AREA (Sq.Ft.) : 19.30907 STACK WIDTH(inchs) : NOZZLE AREA (feet): 0.000533 STACK AREA (Sq.Ft.) : 0

ENTER THE STACK AREA SHOWN ABOVE: 19.30907



## FLOWS SAMPLED VOLUME (STD. CU .FT.): 39.2473 VOLUME OF WATER VAPOR (STD. CU .FT.): 12.2570 FRACTIONAL MOISTURE CONTENT {aJ o ): 

### 0.2380 DRY BASE: 81.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1200 MOLECULAR WT. OF STACK GAS (WET BASE): 26.4737
STACK PRESSURE (inch Hg): 29.8853 STACK GAS VELOCITY (ft/sec.): 29.0578 ACTUAL STACK GAS FLOW RATE (ACFM): 33664.7445 STANDARD STACK GAS FLOW RATE (SCFH): 1356761.65

ISOKINETIC RATIO (%): 104.8020

POINTS STACK T. DEL T A P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 137 0.12 0.34641 0.50 38 37 2 138 0.15 0.387298 0.70 44 38 3 138 0.17 0.412311 0.80 46 38 4 138 0.18 0.424264 0.80 47 39 5 139 0.18 0.424264 0.80 47 39 6 139 0.19 0.43589 0.90 47 40 7 139 0.21 0.458258 1.00 47 40 8 139 0.24 0.489898 1.10 47 40 9 139 0.28 0.52915 1.30 47 41 10 138 0.30 0.547723 1.40 48 41 11 137 0.24 0.489898 1. i 0 44 4 i 12 139 0.30 0.547723 1.40 46 42 13 138 0.30 0.547723 1.40 48 42 14 138 0.29 0.538516 1.30 48 42 15 138 0.21 0.458258 1.00 48 42 16 139 0.19 0.43589 0.90 49 413 17 138 0.20 0.447214 0.90 49 43 18 138 0.21 0.458258 1.00 51 44 19 138 0.22 0.469042 1.00 50 ' 4 20 139 0.21 0.458258 1.00 50 44

138.3 0.4653 1.0150 47.0500 41.0000 44.0250


# P3

## EMISSION TEST SUMMARY

PLANT : Daltile, Iviuskogee, CP, DATE : 7•Dec•05 PLACE : Kiln ScrubbEr Exhaust RUN# : 2 t4 F 

### TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mts) : 26

~ 

## NOZZLE DIAMETER (INCH.) : 0.3127 PARTICULATE WElGHT (Front half mg) : '} METER COEFFIClENT (Y) : 0.989 PARTICULATE WEIGHT (Back half mg) PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : •C.?_ GAS METER VOL.(Cu.Ft.) : 37.411 PERCENT CO2

. 3 BAROMETRIC PRESSURE 29.9 PERCENT 02 lo PERCENT CO 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 59.5 STACK LENGTH(inches) : STACK AREA (Sq.Ft.) : 19.30907 STACK WIDTH(inches) : NOZZLE AREA (feet): 0.000533 STACK AREA (Sq.Ft.) : 0

ENTER THE STACK AREA SHOWN ABOVE: 19.30907


## FLOWS SAMPLED VOLUME (STD. CU .FT.): 38.9335 VOLUME OF WATER VAPOR (STD. CU .FT.): 12.5206 FRACTIONAL MOISTURE CONTENT (%): 0.2433

DRY BASE: 81.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1200 MOLECULAR WT. OF STACK GAS (WET BASE): 26.4141 STACK PRESSURE (inch Hg): 29.8853 STACK GAS VELOCITY (ft/sec.): 29.0622 ACTUAL STACK GAS FLOW RATE (ACFM): 33669.8511 

## STANDARD STACK GAS FLOW RATE (SCFH): 1347205.83

ISOKINETIC RAT10 (%): 104.7015

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 138 0.25 0.5 1.20 41 41 2 138 0.27 0.519615 1.20 44 40 3 139 0.29 0.538516 1.30 45 40 4 139 0.28 0.52915 1.30 45 40 5 139 0.25 0.5 1.20 45 40 6 139 0.20 0.447214 0.96 45 40 7 139 0.19 0.43589 0.91 45 40 8 139 0.19 0.43589 0.91 45 40 9 139 0:21 0.458258 1.00 45 40 10 138 0.22 0.469042 1.00 4•6 40 11 137 0.14 0.374166 0.67 43 40 12 138 0.16 0.4 0.77 44 40 13 138 0.19 0.43589 0.90 46 40 14 138 0.20 0.447214 0.96 46 40 15 139 0.18 0.424264 0.86 46 40 16 139 0.19 0.43589 0.91 45 /_0 17 138 0.20 0.447214 0.96 45 40 18 138 0.22 0.469042 1.00 46 40 19 138 0.25 0.5 1.20 46 40 20 138 0.28 0.52915 1.30 46 40

138.4 0.4648 1.0255 44.9500 40.0500 42.5000 

# ?4

## EMISSION TEST SUMMARY

PLANT : Daltile, Miuskogee, OK DATE : 7•Dec•05 PLACE : Kiln Scrubber Exhaust RUN# : 3 

# ~ F
TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 250.8 

## NOZZLE DIAMETER (INCH.) : 0.3127 PARTICULATE WEIGHT (Front half mg) : 0 METER COEFFICIENT (Y) : 0.989 PARTICULATE WEIGHT (Back half mg) : ;? PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : J.2 GAS METER VOL.(Cu.Ft.) : 34.996 PERCENT CO2 3 BAROMETRIC PRESSURE 29.8 PERCENT 02 16 PERCENT CO 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

## STACK DIAMETER (inch): 59.5 STACK LENGTH(inchs) : STACK AREA (Sq.Ft.) : 19.30907 STACK WIDTH(inchs) : NOZZLE AREA (feet): 0.000533 STACK AREA (Sq.Ft.) : 0

ENTER THE STACK AREA SHOWN ABOVE: 19.30907


# F'LOWS SAMPLED VOLUME (STD. CU .FT.): 36.5833 VOLUME OF WATER VAPOR (STD. CU .FT.): 11.8052 FRACTIONAL MOISTURE CONTENT (%): 0.2440

DRY BASE: 81 .0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1200 MOLECULAR WT. OF STACK GAS (WET BASE): 26.4071 STACK PRESSURE (inch Hg): 29.7853 STACK GAS VELOCITY (ft/sec.): 29.6653 

## ACTUAL STACK GAS FLOW RATE (ACFM): 34368.6052 STANDARD STACK GAS FLOW RATE (SCFH): 1369993.29

ISOKINETIC RATIO (aJ

o ): 96.7450

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 135 0.15 0.387298 0.72 40 38 2 138 0.18 0.424264 0.86 42 38 3 138 0.18 0.424264 0.86 42 38 4 139 0.20 0.447214 0.96 43 38 5 138 0.21 0.458258 1.00 43 38 6 138 0.21 0.458258 1.00 43 37 7 138 0.22 0.469042 1.00 42 37 8 139 0.25 0.5 1.20 42 37 9 139 0.27 0.519615 1.20 42 37 10 138 0.30 0.547723 1.40 41 37 11 138 0.24 0.489898 1.20 39 36 12 138 0.28 0.52915 1.40 40 36 13 138 0.30 0.547723 1.40 40 36 14 138 0.29 0.538516

- 

### 1.30 40 36 15 138 0.26 0.509902 1.20 40 36 16 139 0.20 0.447214 0.96 39 36 17 139 0.18 0.424264 0.86 39 36 18 139 0.18 0.424264 0.86 38 36 19 138 0.21 0.458258 1.00 38 36 20 138 0.22 0.469042 1.10 38 36

138.15 0.4737 1.0740 40.5500 36.7500 38.6500



# ?5

### EMISSION TEST SUMMARY

PLANT : 

### Daltile, Muskogee, OK DATE : 

### 7-Dec•05 PLACE
: 

### Kiln Scrubl

- ,er Exhaust RUN# : 

### 1 

# ?m
TEST DURATION (MINUTES)
: 

### 60 LiQUID COLLECTED (mis) : 

### 268.3 NOZZLE DIAMETER (lNCH.)
: 

### 0.3123 PARTICULATE WEIGHT (Front half mg) : 

### 66.74 METER COEFFICIENT (Y)
: 

### 1.005 PARTICULATE WEIGHT (Back hatf mg) : 

### 4.48 PITOT COEFFICIENT (Cp)
: 

### 0.84 STATIC PRESSURE (in. H20)
: 

### •0.2 GAS METER VOL.(Cu.Ft.)
: 

### 37.326 PERCENT CO2 3 BAROMETRiC PRESSURE 29.9 PERCENT 02 16 PERCENT CO 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 59.5 STACK LENGTH(inchs)
: 

### STACK AREA (Sq.Ft.)
: 

### 19.30907 STACK WIDTH(inchs) : 

### NOZZLE AREA (teet): 0.000532 STACK AREA (Sq.Ft.)
: 

### 0

ENTER THE STACK AREA SHOWN ABOVE: 19.30907



### FLOWS SAMPLED VOLUME (STD. CU .FT.): 39.1932 VOLUME OF WATER VAPOR (STD. CU .FT,): 12.6289 FRACTIONAL MOISTURE CONTENT 

## (V: 0.2437

DRY BASE: 81.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1200 MOLECULAR WT. OF STACK GAS (WET BASE): 26.4101 STACK PRESSURE (inch Hg): 29.8853 STACK GAS VELOCITY (tt/sec.): 29.2447 ACTUAL STACK GAS FLOW RATE (ACFM): 33881.2229 STANDARD STACK GAS FLOW RATE (SCFH): 1355016.48

PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0263 PARTICULATE CONCENTRATION (LBS/SCF): 3.75E.06 PARTICULATE EMISSION (LBS/HR): 5.0878

BACK HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0018 PARTICULATE CONCENTRATION (LBS/SCF): 2.52E•07 PARTICULATE EMISSION (LBS/HR): 0.3415
ISOKINETIC RATIO (gb): 105.0612

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 138 0.21 0.458258 0.92 42 40 2 139 0.20 0.447214 0.88 47 40 3 138 0.20 0.447214 0.88 47 41 4 139 0.18 0.424264 0.79 48 41 5 139 0.17 0.412311 0.75 48 41 6 139 0.22 0.469042 0.97 48 41 7 138 0.26 0.509902 1.15 48 42 8 138 0.28 0.52915 1.20 49 43 9 139 0.28 0.52915 1.20 49 43 10 138 0.25 0.5 1.20 49 43 11 138 0.31 0.556776 1.40 44 43 12 138 0.29 0.538516 1.30 49 43 13 139 0.26 0.509902 1.10 50 43 14 139 0.22 0.469042 0.97 51 44 15 139 0.20 0.447214 0.88 51 44 16 138 0.19 0.43589 0.84 51 44 17 138 0.19 0.43589 0.84 52 45 18 138 0.19 0.43589 0.84 53 45 19 138 0.18 0.424264 0.79 54 45 20 138 0.14 0.374166 0.62 54 46

138.4 0.4677 0.9710 49.2000 42.8500 46.0250



# Me

### EMISSION TEST SUMMARY

PLANT 

# : Daltile. Muskogee, OK DATE 

# : 7•Dec•05 PLACE 

# : Kiln Scrubber =xhiust RUN3i 

# : 2 

# p ft)

TEST DURATION (MINUTES) 

# : 60 LIQUID COLLECTED (mis) 

# : NOZZLE DIAMETER (INCH.) 

# : 0.3123 PARTICULATE WEIGHT (Front half mg) 

# : METER COEFFICiENT (Y) 

# : 1.005 PARTICULATE WEIGHT (Back half mg) 

# : PITOT COEFFICIENT (Cp) 

# : 0.84 STATIC PRESSURE (in. H20) 

# : GAS METER VOL.(Cu.Ft.) 

# : 36.702 PERCENT CO2 BAROMETRIC PRESSURE 29.9 PERCENT 02 PERCENT CO

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 59.5 STACK LENGTH(inches) 

# : STACK AREA (Sq.Ft.) 

# : 19.30907 STACK WIDTH(inches) 

# : NOZZLE AREA (feet): 0.000532 STACK AREA (Sq.Ft.) 

# :

ENTER THE STACK AREA SHOWN ABOVE: 19.30907



### FLOwS SAMPLED VOLUME (STD. CU .FT.): 38.8145 VOLUME OF WATER VAPOR (STD. CU .FT.): 12.5771 FRACTIONAL MOISTURE CONTENT 0.2447

DRY BASE: 81.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1200 MOLECULAR WT. OF STACK GAS (WET BASE): 26.3986
STACK PRESSURE (inch Hg): 29.8853 STACK GAS VELOCITY (ft/sec.): 28.7285 ACTUAL STACK GAS FLOW RATE (ACFM): 33283.2664 STANDARD STACK GAS FLOW RA T E(SCFH): 1332288.54

PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0220 PARTICULATE CONCENTRATION (LBS/SCF): 3.15E•06 PARTICULATE EMISSION (LBS/HR): 4.1907

BACK HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0053 PARTICULATE CONCENTRATION (LBS/SCF): 7.60E.07 PARTICULATE EMISSION (LBS/HR): 1.0127

ISOKINETIC RATIO 

### (%): 105.8210

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 137 0.29 0.538516 1.30 42 41 2 137 0.28 0.52915 1.20 46 41 3 137 0.25 0.5 1.10 45 41 4 1.37 0.20 0.447214 0.88 45 41 5 137 0.18 0.424264 0.79 45 41 6 137 0.17 0.412311 0.74 45 40 7 138 0.18 0.424264 0.79 45 40 8 137 0.18 0.424264 0.79 45 40 9 137 0.17 0.412311 0.75 46 40 10 136 0.15 0.387298 0.66 45 40 11 138 0.22 0.469042 0.98 41 40 12 138 0.21 0.458258 0.92 45 40 13 137 0.19 0.43589 0.83 45 40 14 137 0.17 0.412311 0.75 44 40 15 138 0.18 0.424264 0.79 44 40 16 137 0.22 0.469042 0.97 45 39 17 137 0.25 0.5 1.10 44 40 18 137 0.26 0.509902 1.10 44 40 19 137 0.28 0,52915 1.20 45 40 20 135 0.24 0.489898 1.05 45 40

137.05 0.4599 0.9345 44.5500 40.2000 42.3750 267.2 55.37 13.38 •0.2 3 16 0



# n



# p 7

## EMISSION TEST SUMMARY

PLANT : Daltile. Muskogee. OK DATE : 7•Dec•05 PLACE : Kiln Scrubber Exhaus'. RUNit : 3

r



### y~~~ TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 264.5 

### NOZZLE DIAMETER (INCH.) : 0.3123 PARTICULATE WEIGHT (Front half mg) : 52.8 METER COEFFICIENT (Y) : 1.005 PARTICULATE WEIGHT (Back half mg) : 8.2 PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : •0.2 GAS METER VOL.(Cu.Ft.) : 38.588 PERCENT CO2 3 BAROMETRIC PRESSURE 29.8 PERCENT 02 16 PERCENT CO 0



### FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 59.5 STACK LENGTH(inchs) : 

### STACK AREA (Sq.Ft.) : 19.30907 - STACK WIDTH(inchs) : NOZZLE AREA (feet): 0.000532 STACK AREA (Sq.Ft.) : 0

ENTER THE STACK AREA SHOWN ABOVE: 19.30907


## FLOWS SAMPLED VOLUME (STD. CU .FT.): 40.9636 VOLUME OF WATER VAPOR (STD. CU .FT.): 12.4500 FRACTIONAL MOISTURE CONTENT (gi;): 0.2331

DRY BASE: 81.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1200 MOLECULAR WT. OF STACK GAS (WET BASE): 26.5281 STACK PRESSURE (inch Hg): 29.7853 STACK GAS VELOCITY (ft/sec.): 30.3759 

### ACTUAL STACK GAS FLOW RATE (ACFM): 35191.8041 STANDARD STACK GAS FLOW RATE (SCFH): 1425854.86

PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0199 

### PARTICULATE CONCENTRATION (LBS/SCF): 2.84E•06 PARTICULATE EMISSION (LBS/HR): 4.0525


### BACK HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0031 PARTICULATE CONCENTRATION (LBS/SCF): 4.41E•07 PARTICULATE EMISSION (LBS/HR): 0.6294
ISOKINETIC RATIO (%): 104.3513

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 137 0.23 0.479583 1.00 39 37 2 137 0.22 0.469042 0.97 41 38 3 137 0.21 0.458258 0.92 42 37 4 137 0.19 0.43589 0.83 42 38 5 137 0.18 0.424264 0.79 42 37 6 137 0.24 0.489898 0.84 42 37 7 137 0.27 0.519615 1.20 42 37 8 137 0.29 0.538516 1.30 42 37 9 137 0.28 0.52915 1.20 42 37 10 136 0.25 0.5 1.10 42 37 11 137 0.30 0.547723 1.30 39 36 12 137 0.31 0.556776 1.30 40 37 13 137 0.30 0.547723 1.30 41 37 14 137 0.25 0.5 1.10 41 36 15 137 0.23 0.479583 1.00 41 36 16 137 0.22 0.469042 0.96 41 36 17 137 0.21 0.458258 0.91 41 36 18 137 0.21 0.458258 0.91 41 36 19 137 0.20 0.447214 0.86 41 36 20 137 0.18 0.424264 0.78 41 36

136.95 0.4867 1.0285 41.1500 36.7000 38.9250

•

# EMISSION TEST SUMMARY

PLANT : Daltile, Muskogee, nK DATE : 8-Dec-05 PLACE : Trim Kiln Exhaust RUN# : 1 

# IK 0 I'"
TEST DURATION (MINUTES) : NOZZLE DIAMETER (INCH.) : METER COEFFICIENT (Y) : PITOT COEFFICIENT (Cp) : GAS METER VOL.(Cu.Ft.) : BAROMETRIC PRESSURE 60 LIQUID COLLECTED (mis)

: 

## 0.2497 PARTICULATE 1NEIGHT (Front half mg)

: 

## 0.989 PARTICULATE WEIGHT (Back half mg)

: 

## 0.84 STATIC PRESSURE (in. H20)

: 

## 47.101 PERCENT CO2

. 

## 30 PERCENT 02

: 

## PERCENT CO 58.6 0 0 0.38 2.5 17 0

0 FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 24.5 STACK LENGTH(inchs)

: 

## STACK AREA (Sq.Ft.)

: 

## 3.273856 STACK WIDTH(inchs)
; 

## NOZZLE AREA (feet): 0.00034 STACK AREA (Sq.Ft.)

:


## ENTER THE STACK AREA SHOWN ABOVE: 3.273856



# FLOWS SAMPLED VOLUME (STD. CU .FT.): 49.3056 VOLUME OF WATER VAPOR (STD. CU .FT.): 2.7583 FRACTIONAL MOISTURE CONTENT (¢J o 

# }: 0.0530 DRY BASE: 80.5000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.0800 MOLECULAR WT. OF STACK GAS (WET BASE): 28.4930
STACK PRESSURE (inch Hg): 29.9721 STACK GAS VELOCITY (ft/sec.): 78.4767 ACTUAL STACK GAS FLOW RATE (ACFM): 15415.2827 STANDARD STACK GAS FL01N RATE (SCFH): 490598.094

ISOKINETIC RATIO 

# (%): 96.8125

POINTS STACK T. DELTA P SQUAR D.P DELTA H , 

## METER T. 'METER T. deg F INLET OUTLET

1 481 0.87 0.932738 1.30 39 38 2 486 1.00 1 1.50 44 38 3 486 1.20 1.095445 1.80 45 39 4 485 1.20 1.095445 1.80 44 39 5 486 1.20 1.095445 1.80 44 39 6 484 1.00 1 1.50 44 40 7 480 0.84 0.916515 1.20 42 40 8 485 1.00 1 1.50 45 40 9 487 1.20 1.095445 1.80 46 40 10 486 1.20 1.095445 1.80 46 41 11 485 1.20 1.095445 1.80 46 41 12 481 1.10 1.048809 1.60 46 41

484.33333 1.0392 1.6167 44.2500 39.6667 41.9583


# P9

# EMISSION TEST SUMMARY

PLANT : Daltile, tViuskogee, OK DATE : 8-Dec-05 PLACE : Trim Kiln Exhaust RUN# : 2 

# #0 14r

TEST DURATION (MINUTES) : NOZZLE DIAMETER (INCH.) : METER COEFFICIENT (Y) : PITOT COEFFICIENT (Cp) : GAS METER VOL.(Cu.Ft.) : BAROMETRIC PRESSURE . 60 LIQUID COLLECTED (mis)

: 

## 0.2497 PARTICULATE WEIGHT (Front half mg) 0.989 PARTICULATE WEIGHT (Back half mg)

: 

## 0.84 STATIC PRESSURE (in. H20)

: 

## 47.601 PERCENT CO2

. 

## 30 PERCENT 02 PERCENT CO : 56.8 0 0 -0.38 2.5 17 0

0 FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 24.5 STACK LENGTH(inches)

: 

## STACK AREA (Sq.Ft.)

: 

## 3.273856 STACK WIDTH(inches)

: 

## NOZZLE AREA (feet): 0.00034 STACK AREA (Sq.Ft.)

:


## ENTER THE STACK AREA SHOWN ABOVE: 3.273856



# FLOWS SAMPLED VOLUME (STD. CU .FT.): 49.4880 VOLUME 

## OF WATER VAPOR (STD. 

## CU .FT.): 2.6736 FRACTIONAL MOISTURE CONTENT 

# (%): 0.0513

DRY BASE: 80.5000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.0800 MOLECULAR WT. OF STACK GAS (WET BASE): 28.5121
STACK PRESSURE (inch Hg): 29.9721 STACK GAS VELOCITY (ft/sec.): 78.2426 ACTUAL STACK GAS FLOW RATE (ACFM): 15369.309 STANDARD STACK GAS FLOW RATE (SCFH): 489636.299

ISOKINETIC RATIO 

# (%): 97.3615

PQINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 470 0.86 0.927362 1.30 43 43 2 487 1.00 1 1.50 46 43 3 488 1.20 1.095445 1.80 46 44 4 488 1.20 1.095445 1.80 46 44 5 487 1.20 1.095445 1.80 46 45 6 481 1.00 1 1.50 46 45 7 484 0.87 0.932738 1.30 45 45 8 487 1.00 1 1.50 45 45 9 488 1.20 1.095445 1.80 46 45 10 488 1.20 1.095445 1.80 48 46 11 487 1.20 1.095445 1.80 48 46 12 486 1.00 1 1.50 48 46

485.08333 1.0361 1.6167 46.0833 44.7500 45.4167


# 30

# EMISSION TEST SUMiVIARY

PLANT : Daltile, Muskogee, OK DATE : 8•Dec-05 PLACE : Trim Kiln Exhaust RUN#: 3 ~ 1 

## 4-
TEST DURATION (MINUTES) : NOZZLE DIAMETER (INCH.) : M ETER COEFFICI ENT (Y) ; PITOT COEFFICIENT (Cp) : GAS METER VOL.(Cu.Ft.) ; BAROMETRIC PRESSURE . 60 LIQUID COLLECTED (mis) : 

# 0.2497 PARTICULATE WEIGHT (Front half mg) : 0.989 PARTICULATE WEIGHT (Back half mg) : 0.84 STATIC PRESSURE (in. H20) : 47.556 PERCENT CO2

. 30 PERCENT 02

. PERCENT CO : 69.2 0 0 0.38 

# 2.5 17
0

~~, J 

## FOR CIRCU LAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 24.5 STACK LENGTH(inchs) : 

# STACK AREA (Sq.Ft.) : 3.273856 STACK WIDTH(inchs) : NOZZLE AREA (feet): 0.00034 STACK AREA (Sq.Ft.) :

ENTER THE STACK AREA SHOWN ABOVE: 3.273856


# FLOWS SAMPLED VOLUME (STD. CU .FT.): 49.2980 VOLUME OF WATER VAPOR (STD. CU .FT.): 3.2572 FRACTIONAL MOISTURE CONTENT 0.0620

DRY BASE: 80.5000 

# MOLECULAR WT. OF STACK GAS (DRY BASE): 29.0800 MOLECU LAR WT. OF STACK GAS (WET BASE): 28.3933
STACK PRESSURE (inch Hg): 29.9721 STACK GAS VELOCITY (ft/sec.): 78.2589 

# ACTUAL STACK GAS FLOW RATE (ACFM): 15372.5021 STANDARD STACK GAS FL01N RATE (SCFH): 483223.42.5

ISOKINETIC RATIO (~J o ): 

## 98.2751

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 478 0.88 0.938083 1.30 45 4-6 2 488 1.00 1 1.50 49 46 3 489 1.20 1.095445 1.80 50 46 4 488 1.20 1.095445 1.80 50 46 5 489 1.10 1.048809 1.70 49 46 6 486 1.00 1 1.50 48 47 7 481 0.87 0.932738 1.30 47 47 8 489 1.00 1 1. 50 - 48 46 9 489 1.20 1.095445 1.80 47 48 10 490 1.20 1.095445 1.80 46 46 11 489 1.20 1.095445 1.80 46 45 12 488 1.00 1 1.50 46 45

487 1.0331 1.6083 47.5833 46.1667 46.8750



# 3, 1

## EMISSION TEST SUMMARY

PLANT : Daltile, Muskogee, OK DATE : 8-Dec-05 PLACE : Trim Kiln Exhaust 

### RUN# : 1 1

(J/11
TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 63.4 NOZZLE DIAMETER (INCH.) : 0.2507 PARTICULATE WEIGHT (Front half mg) : 30.3 METER*COEFFICIENT (Y) : 1.005 PARTICULATE WEIGHT (Back half mg) : 26.33 PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : •0.38 

### GAS METER VOL.(Cu.Ft.) : 47.939 PERCENT CO2

. 2.5 BAROMETRIC PRESSURE

. 30 PERCENT 02 17.5 PERCENT CO

. 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 24.5 STACK LENGTH(inchs) : STACK AREA (Sq.Ft.) : 3.273856 STACK WIDTH(inchs) : NOZZLE AREA (feet): 0.000343 STACK AREA (Sq.Ft.) : 0

ENTER THE STACK AREA SHOWN ABOVE: 3.273856


# FLOwS SAMPLED VOLUME (STD. CU .FT.): 51.2415 VOLUME OF WATER VAPOR (STD. CU .FT.): 2.9842 FRACTIONAL MOISTURE CONTENT (%): 0.0550

DRY BASE: 80.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1000 MOLECULAR WT. OF STACK GAS (WET BASE): 28.4891
STACK PRESSURE (inch Hg): 29,9721 STACK GAS VELOCITY (ft/sec.): 79.4271 ACTUAL STACK GAS FLOW RATE (ACFM): 15601.9783 STANDARD STACK GAS FLOW RATE (SCFH): 495113.041

PARTICULATE FRONT HALF 

## PARTICULATE CONCENTRATION (GR./SCF): 0.0091 PARTICULATE CONCENTRATION (LBS/SCF): 1.30E•06 PARTICULATE EMISSION (LBS/HR): 0.6456

BACK HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0079 PARTICULATE CONCENTRATION (LBS/SCF): 1.13E•06 PARTICULATE EMISSION (LBS/HR): 0.5610
ISOKINETIC RATIO (%): 98.9024

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 484 1.10 1.048809 1.60 35 34 2 488 1.20 1.095445 1.70 40 35 3 487 1.20 1.095445 1.70 41 36 4 487 1.20 1.095445 1.70 41 36 5 488 1.10 1.048809 1.60 42 37 6 475 0.90 0.948683 1.30 42 37 7 485 0.95 0.974679 1.40 41 38 8 486 1.20 1.095445 1.70 42 38 9 488 1.20 1.095445 1.70 43 38 10 488 1.20 1.095445 1.70 44 39 11 485 1.20 1.095445 1.70 44 40 12 479 0.86 0.927362 1.20 45 40

485 1.0514 1.5833 41.6667 37.3333 39.5000

~ 

### r .7 .,

# ENlISSION TEST SUMNtARY

PLANT : Daltile. Muskogee, OK DATE : 8•Dec•05 

### PLACE : Trim Kiln Exhaust RUN# : 2 p o TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 60.5 NOZZLE DIAMETER (INCH.) : 0.2507 PARTICULATE WEIGHT (Front half mg) : 29.31 METER COEFFICIENT (Y) : 1.005 PARTICULATE WEIGHT (Back half mg) : 24.41 

### PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : •0.38 GAS METER VOL.(Cu.Ft.) : 47.047 PERCENT CO2 2.5 BAROMETRIC PRESSURE 30 PERCENT 02 17 PERCENT CO 0



## FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 24.5 STACK LENGTH(inches) : STACK AREA (Sq.Ft.) : 3.273856 STACK WIDTH(inches) : NOZZLE AREA (feet): 0.000343 STACK AREA (Sq.Ft.) : 0

ENTER THE STACK AREA SHOWN ABOVE: 3.273856


# FLowS SAMPLED VOLUME (STD. CU .FT.): 49.8598 VOLUME OF WATER VAPOR (STD. CU .FT.): 2.8477 FRACTIONAL MOISTURE CONTENT (%): 0.0540

DRY BASE: 80.5000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.0800 MOLECULAR WT. OF STACK GAS (WET BASE): 28.4814
STACK PRESSURE (inch Hg): 29.9721 STACK GAS VELOCITY (ft/sec.): 77.9556 ACTUAL STACK GAS FLOW RATE (ACFM): 15312.9267 

## STANDARD STACK GAS FLOW RATE (SCFH): 485857.065

PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0091 PARTICULATE CONCENTRATION (LBS/SCF): 1.30E•06 PAR T ICULATE EMISSION (LBS/HR): 0.6298



## BACK HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0076 PARTICULATE CONCENTRATION (LBS/SCF): 1.08E•06 PARTICULATE EMISSION (LBS/HR): 0.5245
ISOKINETIC RATlO (%): 98.0689

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.



## deg F INLET OUTLET

1 487 1.00 1 1.45 40 40 2 487 1.20 1.095445 1.70 45 40 3 488 1.20 1.095445 1.70 46 41 4 489 1.20 1.095445 1.70 45 41 5 489 1,00 1 1.45 45 42 6 475 0.79 0.888819 1.10 45 42 7 487 1.00 1 1.40 45 43 8 488 1.20 1.095445 1.70 45 43 9 489 1.20 1.095445 1.70 47 43 10 489 1.20 1.095445 1.70 46 43 11 491 0.98 0.989949 1.40 47 44 12 475 0.85 0.921954 1.20 47 44

486.16667 1.0311 1.5167 45.2500 42.1667 43.7083

` 

# q ~

## EMISSION TEST SUMMARY

PLANT : Daltile. Muskogee, OK DATE : 8•Dec•0 1

5 PLACE : Trim Ki{n Exhaust RUN# : 3 p/Yl
TEST DURATION (MINUTES)

: 

### 60 LIQUID COLLECTED (mis)

: 

### 79.7 NOZZLE DIAMETER (INCH.)

: 

### 0.2507 PARTICULATE WEIGHT (Front half mg)
: 

### 31.01 METER COEFFICIENT (Y)
: 

### 1.005 PARTICULATE WEIGHT (Back half mg)
: 

### 20.19 PITOT COEFFICIENT (Cp)
: 

### 0.84 STATIC PRESSURE (in. 

### H20)
: 

### •0.36 GAS METER VOL.(Cu.Ft.)

: 

### 47.487 PERCENT CO2 2.5 BAROMETRIC PRESSURE 30 PERCENT 02 17 PERCENT CO 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 24.5 STACK LENGTH(inchs)

: 

### STACK AREA (Sq.Ft.)
: 

### 3.273856 STACK WIDTH(inchs)

: 

### NOZZLE AREA (feet): 0.000343 STACK AREA (Sq.Ft.)

: 

### 0

ENTER THE STACK AREA SHOWN ABOVE: 3.273856


## FLOWS SAMPLED VOLUME (STD. CU .FT.): 50.0569 VOLUME OF WATER VAPOR (STD. CU .FT.): 3.7515 FRACTIONAL MOISTURE CONTENT (%): 0.0697

DRY BASE: 80.5000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.0800 MOLECULAR WT. OF STACK GAS (WET BASE): 28.3075 STACK PRESSURE (inch Hg): 29.9735 STACK GAS VELOCITY (ft/sec.): 79.0460 ACTUAL STACK GAS FLOW RATE (ACFM): 15527.1052 STANDARD STACK GAS FLOW RATE (SCFH): 484334.457



### PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0096 PARTICULATE CONCENTRATION (LBS/SCF): 1.37E•06 PARTICULATE EMISSION (LBS/HR): 0.6616

BACK HALF PARTICULATE:CONCENTRATION (GR./SCF): 0.0062 PARTICULATE CONCENTRATION (LBS/SCF): 8.89E•07 PARTICULATE EMISSION (LBS/HR): 0.4308
ISOKINETIC RATIO (%): 98.7665

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 487 1.05 1.024695 1.50 43 43 2 489 1.20 1.095445 1.70 48 44 3 491 1.20 1.095445 1.70 51 44 4 491 1.20 1.095445 1.70 51 45 5 488 1.00 1 1.40 51 45 6 479 0.85 0.921954 1.20 51 45 7 480 1.00 1 1.40 48 44 8 490 1.20 1.095445 1.70 50 44 9 488 1.20 1.095445 1.70 49 44 10 490 1.20 1.095445 1.70 48 44 11 485 1.10 1.048809 1.60 48 44 12 480 0.88 0.938083 1.30 47 44

486.5 1.0422 1.5500 48.7500 44.1667 46.4583 

# q4,

# Surnmary of Suifur Dio.xide A natyzer Calibrations and Bias

Plant: Daftile, Mus#cogee Source: Kitn Scrubber Exhaust Date: 12/7I2005

Anafyzer Caiibratrivn Data

Cylinder AnaEyzer Absofute °10 

# Span Value Response Difference Zero Gas 0 0 0 0 Mid Range 50.1 49.03 -1.07 -0.97273 High Range 101 100.25 -0.75 -0.68182

Run #1 Systern Cafibration 

# Bias and Driffi 

# Data

Analyzer fnitial Values Finai Values Drift Cafibration .System Systern System System Response Calibration Calibration Calibration Calibration

Response Bias Response Bias

Zero Gas 0 -0.15 -0.13636- -0.15 -0.13636 0 Upsca4e 100.25 96.75 -3.18182 96.45 -3.45455 -0.27273 Average Calibration Values

-0.15 96.6

Run #2

Run #3 Average S42 Concentration: -0.08

Corrected S02 Concentration: 0.073075 (Equation 6C-1)

Zero Gas 0 -0.15 -0.13636 Upscale 100.25 96.45 -3.45455
Average S02 Concentration: 0,1 Con

- ected S02 Concentration: 0.224874 (Equation 6C-1)

Zero Gas 0 -0.08 -0.07273 Upscale 100.25 96.45 -3.45455 -0.08 -0.07273 0.063636 96.45 -3.45455 0

0.58 0.527273 0.6 96.75 -3.181 82 0.272727 -0.115 96.45

0.25 96.6
Average S02 Concentration: 0.71 Corrected S42 Concentration: 0.4822 (Equation 6C-1)

760

# Sumrnary of NGx AnaEyzer Caiibrations and Bias

Piant: Daftiie, Muskogee Source: Kiln Scrubber Exhaust Date: 12/7/2005

Ana{yzer Calibratrion Data

Cylinder Anaiyzer Absolute % Span Value P.esponse Difference Zero Gas 0 0.08 0.08 0.133333 Mid Range 25.5 24.7 -0.8 -1.33333 High Range 51 50.78 -0.22 -0.36667

System Cafibration B{as 

# and Drift Data

Analyzer Initial Vafues Final Values Drift Average Ca(ibration System System System Systern Calibration Response Calibration Calibration Calibration Calibration Vafues

Response Bias Response Bias

Run #1 Zero Gas 0.08 0-0.13333 0.3 0.366667 0.5 0.15

UpscaSe 24.7 22.8 -3.16667 23.5 -2 1.166667 23.15
Average NOx Concentration: 29.93 Corrected NOx 

# Concentration: 33.01696 (Equation 6C-1)

Run #2 Zero Gas 0.08 0.3 0.366667 0.4 0.533333 0.166667 0.35

Upscale 24.7 23.5 -2 23.63 -1.78333 0.216667 23.565
Average NOx Concentration: 30.6 Corrected NOx Concentration: 33.22744 (Equation 60-1)

Run #3 Zero Gas 0.08 0.4 0.533333 0.55 0.783333 0.25 0.475

Upsca{e 24.7 23.63 -1.78333 23.03 -2.78333 -1 23.33
Average NOx Concentration: 30.11 Corrected NOx Concentration: 33.06465 (Equation 6C-1)



# 69

# Summary of CO Anafyzer Catibrations and gias

Pfant: Daltiie, Mus{%ogee Source: Kitn Scrubber Exhaust Date: 12/7/2005

Anatyzer 

# Cafibratrion Data
Cyfinder Analyzer Absolute % 

# Span Value Response Difference Zero Gas 0 2.25 2.25 0.45 Mid Range 200 200.3 0.3 0.06 High Range 494 488.25 -5.75 -1.15

System Caiibration Bias and 

# Drift Data

Analyzer Initial Values Final Va(ues Drift Calibration System System Systern System Response Calibration Cafibration Calibration Ca(ibration

Response Bias Response Bias

Zero Gas 2.25 2.1 -0.03 0.4 -0.37 Upscale 200.3 188.88 -2.284 179.73 -4.114
Average CO Concentration: 215.86 Corrected CO Concentration: 234.476 (Equation 6C-1)

Zero Gas 2.25 0.4 -0.37 -0.3 -0.51 Upscale 200.3 179.73 -4.114 178.78 -4.304
Average CO Concentration: 206.7 Corrected CO Concentration: 230.6297 (Equation 6C-1)

Zero Gas 2.25 -0.3 -0.51 2 -0.05 Upsca{e 200.3 178.78 - -4.304 180.35 - -3.99
Average CO Concentration: 212.2 Corrected CO Concentration: 236.5218 (Equation 6C-1) Run #1

Run #2

P.un #3 Average Calibration Values

-0.34 1.25 -1.83 184.305

-0.14 0.05 -0.19 179.255

0.46 0.85 0.314 179.565



# 70~
(

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# 5

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# r ,~ 

### !~.' 0 4 ~

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### G + , , . J C
, :4.e. r. C



### ~~ C:'. - "r



### DateCFime NOx mm/dd/yy hh:mm:ss 1om '12/06/05 16:53:03 0.0259$9 Zero PIOx 72i0610516:54:03 0.061213 12/0610516:55:03 39.63673 '12106105 16:56:03 60.6123 51 ppm NOx 12/06/05 16:57:03 17:0874 12/06105 16:58:43 34.40918 Siart Convsrter Check 12/0610516:59:03 34.50684 12/06/0517:00:03 34.48629 1210610517:01:03 34.48731 1210610517:02:03 34.47071 12/06/0517:03:03 34.4463 12/06/0517:04:03 34.42872 12/06l0517:05:03 34.43556 12/06/0517:06:03 34.39357 12106/0517:07:03 34.39845 12/0610517:08:03 34.39064 1210610517:09:03 34.38478 12/0610517:10:03 34.39748 12106/0517:11:03 34.37209 12/06/0517:12:03 34.36525 12106/0517:13:03 34.37306 12106/0517:14:03 34.35842 1210610517:15:03 34.34768 1210610517:16:03 34.32424 1210610517:17:03 34.32912 1210610517:18:03 34.27444 12/0610517:19:03 34.27444 1214610517:20:03 34.29397 12106l0517:21:03 34.29592 1210610517:22:03 34.24221 1210610517:23:03 34.27737 12l0610517:24:03 34.22659 12/06/0517:25:03 34.24905 1 2/06105 1 7:26:03 34.22757 12/0610517:27:03 34.22754 12/06/05 17:28:03 34.21094 5top Converler Check 12l06/0517:29:03 8.681396 12106/0517:30:03 0.060755



# 7112/7105 Calibrations

Date(Time VOC CO NOx S02 mm/dd/yy hh:mm:ss ppm ppm ppm 

### p )III 12/07/05 08:51:16 0.1 0.3 0.1 3.1 12107/05 08:51:26 0.0 0.3 

### 0.1 3.0 12J07105 08:51:36 0.0 0.3 

### 0.1 3.2 12107/05 08:51:46 0.0 0.3 

### 0.1 3.2 12107/05 08:51:56 0.0 0.3 

### 0.0 3.2 12/07/05 08:52:06 0.3 0.3 0.1 3.2 12107/05 08:52:16 0.3 0.2 0.0 3.1 12/07/05 08:52:26 0.3 0.1 27.3 3.2 12/07/05 08:52:36 0.4 0.2 40.1 3.2 12107/05 08:52:46 0.4 0.3 40.3 3.3 12107/05 08:52:56 0.4 0.3 40.4 3.3 12107/05 08:53:06 0.4 0.3 49.8 3.3 12/07/05 08:53:16 0.4 0.3 50.8 3.3 12107/05 08:53:26 0.4 0.3 51.2 3.2 12/07/05 08:53:36 

### 0.4 0.4 51.5 3.3 12/07/05 08:53:46 

### 0.4 0.3 51.1 3.3 12/07105 08:53:56 0.4 0.3 

### 50.8 3.2 12107/05 08:54:06 0.4 0.3 

### 50.8 3.2 12/07105 08:54:16 0.4 0.2 

### 50.7 3.2 12/07/05 08:54:26 0.4 0.2 

### 50.8 3.2 12/07/05 08:54:36 0.4 0.2 50.8 3.4 12107/05 08:54:46 

### 0.4 0.2 47.1 3.4 12/07/05 08:54:56 0.3 0.3 0.5 3.3 12/07/05 08:55:06 0.1 0.3 0.2 

### 3.2 12/07105 08:55:16 0.0 0.2 0.1 3.3 12/07105 08:55:26 0.1 0.2 0.1 3.3 12/07105 08:55:36 0.3 0.1 0.0 3.2 12/07105 08:55:46 0.3 0.1 2.0 3.1 12/07/05 08:55:56 0.3 

### -0.2 24.2 3.3 12/07/05 08:56:06 0.3 -0.1 

### 24:5 3.2 12/07/05 08:56:16 0.3 -0.1 

### 24.7 3.2 12/07/05 08:56:26 0.3 -0.1 

### 24.6 3.3 12/07/05 08:56:36 0.3 -0.1 

### 24.7 3.2 12107/05 08:56:46 0.4 -0.1 

### 24.8 3.2 12107/05 08:56:56 0.4 -0.1 24.7 3.1 12107/05 08:57:06 0.3 0.2 10.2 3.1 12/07/05 08:57:16 0.4 0.2 0.2 3.1 12107/05 08:57:26 0.1 0.1 0.1 3.1 12107105 08:57:36 0.0 0.1 0.1 3.1 12107105 08:57:46 0.0 0.1 0.1 3.1 12107/05 08:57:56 0.0 0.2 0.1 3.2 12/07/05 08:58:06 0.0 0.1 0.1 3.1 12/07105 08:58:16 0.0 0.0 0.1 3.1 12J07/05 08:58:26 0.2 0.1 0.1 3.1 12/07/05 08:58:36 0.3 1.2 0.1 3.1 12/07/05 08:58:46 0.3 2.2 0.1 3.0 12107/05 08:58:56 0.3 2.1 0.1 3.0 12107/05 08:59:06 0.3 2.4 0.1 3.1 12/07106 08:59:16 0.3 2.4 0.1 3.0 12/07/05 08:59:26 0.3 

### 2.4 0.0 3.1 12/07/05 08:59:36 0.3 86.9 0.1 3.0 12/07/05 08:59:46 0.3 191.4 0.0 3.1 12/07/05 08:59:56 0.3 193.3 0.0 3.1 12/07/05 09:00:06 0.3 193.5 0.0 3.1 12107/05 09:00:16 0.3 196.3 0.0 3.0 12107105 09:00:26 0.3 197.2 0.0 1.2 12107/05 09:00:36 0.3 197.1 0.0 -0.1 12/07/05 09:00:46 0.3 198.7 0.0 0.0 12/07105 09:00:56 0.3 198.1 0.0 0.0 12/07/05 09:01:06 

### 0.3 199.3 0.0 0.0 12/07/05 09:01:16 0.3 

### 200.1 0.0 

### 0.0 12107/05 09:01:26 0.3 

### 200.2 0.0 

### 0.0 12/07105 09:01:36 0.3 

### 200.5 0.0 0.0 12107/05 09:01:46 0.3 

### 200.2 -0.1 0.0 12/07105 09:01:56 0.3 200.3 0.0 -0.1 12/07/05 09:02:06 0.3 103.2 0.0 -0.1 12/07/05 09:02:16 0.2 4.4 0.1 -0.1 12/07/05 09:02:26 0.0 2.7 0.0 0.0 12/07/05 09:02:36 0.0 

### 2.3 0.0 0.0 51 ppm NOx

25.5 ppm NOx

200 ppm CO Zero S02

! 4. Page 1

### 1217/05 Calibrations

12/07105 09:02:46 0.2 2.3 0.0 0.0 12/07/05 09:02:56 0.3 2.4 0.0 -0.1 12/07/05 09:03:06 0.3 2.2 0.0 -0.1 12107/05 09:03:16 0.3 123.6 0.1 -0.1 12/07105 09:03:26 0.4 470.1 0.0 -0.1 12/07/05 09:03:36 0.4 486.2 0.0 -0.1 12107/05 09:03:46 0.3 486.8 0.0 -0.1 12/07/05 09:03:56 0.3 487.0 0.0 -0.1 12/07/05 09:04:06 0.3 487.3 0.0 -0.1 12/07/05 09:04:16 0.3 488.1 0.0 -0.1 12107/05 09:04:26 0.3 

### 488.2 0.0 -0.1 12107105 09:04:36 0.3 

### 488.2 0.0 -0.1 494 ppm CO 12/07/05 09:04:46 0.3 

### 488.2 0.0 -0.1 12/07/05 09:04:56 0.3 

### 488.4 0.0 -0.1 12/07/05 09:05:06 0.4 

### 336.9 0.0 -0.1 12107/05 09:05:16 0.3 14.7 0.0 -0.1 12/07/05 09:05:26 0.1 3.7 0.1 -0.1 12107/05 09:05:36 0.0 3.3 0.1 0.0 12107105 09:05:46 0.0 3.2 0.1 -0.1 12/07/05 09:05:56 0.0 3.3 0.1 -0.1 12/07/05 09:06:06 0.0 3.3 0.0 0.0 12107105 09:06:16 0.0 3.2 0.1 0.0 12/07105 09:06:26 0.0 3.1 0.1 -0.1 12J07/05 09:06:36 0.0 3.0 0.1 -0.1 12/07/05 09:06:46 0.0 3.0 0.1 0.0 12/07/05 09:06:56 0.1 2.9 0.1 -0.1 12/07/05 09:07:06 0.2 2.8 0.1 -0.1 12107/05 09:07:16 0.3 2.4 0.1 -0.1 12/07/05 09:07:26 0.3 2.4 0.1 -0.1 12J07/05 09:07:36 0.4 2.0 0.1 4.8 12/07/05 09:07:46 0.4 1.9 0.4 27.0 

### 12/07/06 09:07:56 0.3 2.0 0.4 42.4 12/07/05 09:08:06 0.3 2.1 0.4 

### 47.7 12/07/05 09:08:16 0.4 2.6 0.3 49.4 12107/05 09:08:26 0.4 2.6 0.3 49.9 12/07/05 09:08:36 0.4 2.7 0.4 50.0 12/07/05 09:08:46 0.4 2.6 0.4 50.1 12107/05 09:08:56 0.3 2.6 0.3 50.2 12107/05 09:09:06 0.3 2.7 0.4 50.2 12/07/05 09:09:16 0.5 2.5 

### 0.3 50.2 12/07/05 09:09:26 0.6 2.4 

### 0.3 50.3 12/07/05 09:09:36 0.6 2.2 0.3 50.3 12/07/05 09:09:46 0.6 2.0 0.3 50.4 12/07/05 09:09:56 0.6 1.9 0.3 49.8 12/07106 09:10:06 0.6 

### 2.1 0.3 49.0 12/07/05 09:10:16 0.5 

### 2.1 0.3 

### 49.0 50.1 ppm S02 12/07/05 09:10:26 0.5 

### 2.4 0.3 

### 49.0 Zero CO 12107/05 09:10:36 0.6 

### 2.4 0.4 49.1 12/07/05 09:10:46 0.5 2.3 0.3 49.2 12/07105 09:10:56 0.5 2.6 0.3 46.0 12/07/05 09:11:06 0.5 2.6 0.0 25.6 12/07/05 09:11:16 0.0 2.6 0.1 9.0 12/07/05 09:11:26 0.1 2.6 0.1 3.0 12107/05 09:11:38 0.0 2.8 0.1 1.1 12107105 09:11:46 0.4 2.6 0.1 0.4 12/07/05 09:11:56 0.5 2.5 0.1 0.2 12/07/05 09:12:06 0.6 2.5 0.1 1.1 12/07/06 09:12:16 0.6 2.1 0.0 29.7 12/07/05 09:12:26 0.6 2.3 0.0 71,8 12/07/05 09:12:36 0.6 2.2 0.0 91.8 12/07/05 09:12:46 0.6 2.2 0.0 97.6 12/07/05 09:12:56 0.7 2.2 0.0 99.0 12107/05 09:13:06 0.7 2.2 

### 0.0 99.5 12/07/05 09:13:16 0.6 2.4 0.0 99.7 12/07/05 09:13:26 0.6 2.4 0.0 99.9 12/07/05 09:13:36 0.6 2.3 0.0 99.9 12/07/05 09:13:46 0.6 2.5 0.0 100.0 12/07/05 09:13:56 0.6 2.4 0.0 100.1 12/07/05 09:14:06 0.6 2.5 0.0 100.0 12/07/05 09:14:16 0.6 2.6 0.0 100.1 12/07105 09:14:26 0.6 2.8 0.0 

### 100.2 12/07/05 09:14:36 0.6 2.8 0.0 

### 100.3 101 ppm S02 

# 7 .3

Page 21217/05 Calibrations

12/07/05 09:14:46 0.6 2.5 0.0 

## 100.3 12/07/05 09:14:56 0.7 2.6 0.0 100.2 12/07105 09:15:06 0.7 2.6 0.0 100.2 12107/05 09:15:16 0.6 3.1 0.0 94.1 12/07/05 09:15:26 0.6 3.3 0.0 53.8 12107/05 09:1 b:36 0.6 3.1 0.1 19.4 12/07/05 09:15:46 0.6 3.1 0.0 6.1 12/07/05 09:15:56 0.6 3.0 0.0 2.2 12/07/05 09:16:06 0.6 3.0 0.0 1.1 12/07/05 09:16:16 0.6 2.8 0.1 0.7 12/07/05 09:16:26 0.6 2.9 0.0 0.4 12/07/05 09:16:36 0.6 2.9 0.0 0.2 12107105 09:16:46 0.6 2.9 0.0 0.2 12/07/05 09:16:56 0.6 3.0 0.0 0.1 12/07/05 09:17:06 0.6 2.8 0.0 0.0 12/07/05 09:17:16 0.6 2.8 0.1 0.0 12107/05 09:17:26 0.6 2.7 0.1 0.0 12107/05 09:17:36 0.7 2.6 0.1 0.0 12/07/05 09:17:46 0.7 2.6 0.1 0.0 12107/05 09:17:56 0.7 2.6 0.1 0.0 12/07/05 09:18:06 0.6 2.6 0.1 -0.1 12107/05 09:18:16 0.6 2.4 0.1 -0.2 12/07/05 09:18:26 0.6 2.3 0.1 -0.2 12107/05 09:18:36 0.6 2.2 0.1 -0.1 12107/05 09:18:46 0.6 2.5 0.1 -0.1 12107105 09:18:56 0.6 2.6 0.1 '-0.2 12/07105 09:19:06 0.6 2.6 0.1 -0.2 12/07105 09:19:16 0.6 2.8 0.1 -0.1 12/07/05 09:19:26 0.2 2.5 0.0 -0.1 12/07105 09:19:36 0.0 2.5 0.1 -0.1 12/07105 09:19:46 0.0 2.2 0.3 0.0 12107/05 09:19:56 0.0 2.1 4.5 0.3 12/07/05 09:20:06 0.0 2.0 9.1 0.5 12/07/05 09:20:16 0.0 2.0 13.3 0.5 12/07/05 09:20:26 0.0 2.1 16.2 0.3 12/07/05 09:20:36 0.0 2.0 17.9 0.1 12107105 09:20:46 0.0 2.1 19.0 0.0 12107/05 09:20:56 0.0 2.2 19.5 -0.1 12/07/05 09:21:06 0.0 2.3 19.8 -0.1 12/07/05 09:21:16 0.0 2.2 19.9 -0.2 12/07/05 09:21:26 0.1 2.4 20.0 -0.2 12107/05 09:21:36 0.0 2.3 20.0 -0.3 12107105 09:21:46 0.0 2.3 20.4 -0.3 12107/05 09:21:56 0.0 2.2 21.2 -0.3 12107/05 09:22:06 0.0 2.2 21.8 -0.2 12/07/05 09:22:16 0.0 2.1 22.3 -0.2 12107/05 09:22:26 0.1 2.1 22.5 -0.2 12/07/05 09:22:36 0.1 2.1 22.6 -0.2 12l07105 09:22:46 0.1 2.2 22.7 -0.2 12/07/05 09:22:56 0.1 2.3 22.7 -0.2 12/07/05 09:23:08 0.1 2.3 22.7 -0.2 12/07/05 09:23:16 0.1 

## 2.2 22.8 -0.2
12107/05 09:23:26 0.0 

## 2.2 22.8 -0.2 25.5 ppm NOx bias 12107/05 09:23:36 0.0 

## 2.0 22.8 -0.1 Zero CO. S02 Bias 12/07/05 09:23:46 0.0 

### 2.1 22.8 -0.1 12/07/05 09:23:56 0.1 2.2 22.7 -0.1 12/07/05 09:24:06 0.5 2.1 22.5 -0.2 12/07/05 09:24:16 0.6 2.0 22.2 -0.1 12107/05 09:24:26 0.6 1.9 20.7 -0.1 12107105 09:24:36 0.4 2.0 16.7 -0.1 12/07/05 09:24:46 0.0 1.8 9.2 -0.1 12/07/05 09:24:56 0.0 2.0 4.2 0.1 12107/05 09:25:06 0.0 1.8 1.8 6.5 12/07/05 09:25:16 0.1 1.6 1.0 22.4 12107105 09:25:26 0.0 1.6 0.6 40.1 12/07/05 09:25:36 1.4 1.3 0.4 55.3 12/07/05 09:25:46 0.1 1.5 0.2 66.9 12/07/05 09:25:56 0.0 1.8 0.1 75.8 12/07105 09:26:06 0.0 1.8 0.0 81.9 12107/05 09:26:16 0.0 2.3 0.0 86.0 12/07/05 09:26:26 0.0 2.4 0.0 88.5 12/07/05 09:26:36 0.0 2.6 0.0 90.0 12107/05 09:26:46 0.0 2.7 0.0 91.1 

# 74

Page 31217105 Cafibrations

12J07/05 09:26:56 0.0 2.6 0.0 92.1 12107/05 09:27:06 0.0 2.1 0.0 92.7 12/07/05 09:27:16 0.0 2.1 0.0 93.0 12107105 09:27:26 0.0 2.1 0.0 93.3 12/07/05 09:27:36 0.0 2.1 0.0 93.6 12107105 09:27:46 0.0 2.1 0.0 94.0 12/07105 09:27:56 0,0 2.2 0.0 94.4 12107/05 09:28:06 0.0 2.6 0.0 94.6 12/07/05 09:28:16 0.0 2.5 0.0 95.3 12/07/05 09:28:26 0.0 2.5 0.0 96.4 12/07/05 09:28:36 0.0 2.5 0.0 96.6 12/07/05 09:28:46 0.0 2.6 

### 0.0 96.7
12107l05 09:28:56 0.0 2.6 

### 0.0 96.7
12/07/05 09:29:06 0.0 2.4 

### 0.0 96.8
12/07/05 09:29:16 0.0 2.1 

### 0.0 96.8 12/07105 09:29:26 0.6 1.8 0.0 95.8 12107/05 09:29:36 0.9 1.9 0.0 94.2 12/07/05 09:29:46 1.0 2.0 0.0 92.5 12107/05 09:29:56 1.1 2.1 0.0 86.7 12/07/05 09:30:06 1.1 2.3 0.0 71.9 12107/05 09:30:16 0.6 2.2 0.1 51.8 12107105 09:30:26 0.2 2.7 0.1 34.0 12107105 09:30:36 0.1 24.5 0.1 22.6 12/07/05 09:30:46 0.1 73.3 0.1 15.4 12107l06 09:30:56 0.0 110.9 0.0 11.0 12/07105 09:31:06 0.0 135.8 0.0 8.0 12/07105 09:31:16 0.1 152.9 0.0 6.1 12/07/05 09:31:26 0.0 166.4 0.0 4.6 12107/05 09:31:36 0.0 175.2 0.0 3.6 12107/05 09:31:46 0.0 180.2 0.0 2.8 12/07/05 09:31:56 0.1 182.8 0.0 2.3 12/07/05 09:32:06 0.0 184.6 0.0 1.8 12/07105 09:32:16 0.0 185.9 0.0 1.4 12/07/05 09:32:26 0.1 187.0 0.0 1.3 12/07/05 09:32:36 0.0 187.8 0.0 1.2 12/07/05 09:32:46 0.0 188.2 0.0 1.0 12l07105 09:32:56 0.0 188.7 0.0 0.8 12/07/05 09:33:06 

### 0.0 188.8 0.0 0.8 12107/05 09:33:16 

### 0.0 188.7 0.0 0.8
12107105 09:33:26 

### 0.0 188.9 0.0 0.7 12/07/05 09:33:36 

### 0.1 189.1 0.0 0.6 12107105 09:33:46 0.2 187.4 0.0 0.6 12/07/05 09:33:56 0.8 185.3 0.0 0.6 12/07/05 09:34:06 1.0 181.2 0.0 0.5 12107/05 09:34:16 1.1 168.8 0.0 0.5 12J07105 09:34:26 13.6 133.9 0.0 0.4 12107/05 09:34:36 46.5 80.1 0.0 0.6 12/07/05 09:34:46 47.0 42.1 0.1 1.2 12/07105 09:34:56 47.0 21.3 0.1 1.6 12/07/05 09:35:06 47.0 13.6 0.0 1.6 12/07105 09:35:16 48.2 9.1 0.0 1.3 12/07/05 09:35:26 48.7 6.3 0.0 1.0 12/07/05 09:35:36 

### 48.7 5.1 0.0 0.8 12/07/05 09:35:46 

### 48.8 4.2 0.0 0.5 12/07/05 09:35:56 

### 48.8 3.8 0.0 0.4 12/07/05 09:36:06 

### 48.8 3.7 0.0 0.3 12107/05 09:36:16 47.1 3.0 0.0 0.1 12107/05 09:36:26 9.4 2.6 0.0 0.0 12/07/05 09:36:36 1.2 2.3 0.0 0.0 12107/05 09:36:46 1.2 2.4 0.0 0.0 12107/05 09:36:56 2.1 2.4 0.0 0.0 12107/05 09:37:06 26.6 2.3 0.0 0.1 12/07/05 09:37:16 

### 28.7 2.3 0.0 0.3 12107/05 09:37:26 

### 28.6 2.3 0.1 0.6 12/07/05 09:37:36 

### 28.7 2.4 0.0 0.7 12/07/05 09:37:46 

### 28.7 2.6 0.0 0.7 12107/05 09:37:56 28.5 2.5 0.0 0.5 12/07105 09:38:06 27.9 2.5 0.0 0.2 12107/05 09:38:16 8.7 2.6 0.0 0.1 12/07/05 09:38:26 1.2 2.5 0.0 0.1 12/07/05 09:38:36 1.2 2.3 0.0 0.0 101 ppm S02 Bias Zero NOx Bias

200 ppm CO Bias Zero VOC

48.8 ppm C31-18

28.8 ppm C3H8



# 75
Page 41217/05 CaliSratfons

12/07105 09:38;46 1.2 2.4 0.0 0.0 12/07/05 09:38:56 27.9 2.4 0.0 0.0 12/07/05 09:39:06 89.5 2.5 0.1 0.1 12107105 09:39:16 90.3 2.4 0:1 0.3 12107/05 09:39:26 90.4 2.5 0.1 0.5 12107l05 09:39:36 90.7 2.6 0.1 0.4 12/07/05 09:39:46 

### 90.8 2.4 0.1 0.4 12107/05 09:39:56 

### 90.7 2.2 0.1 0.3 12/07105 09;40:06 90.9 2.4 0.1 0.2 12/07/05 09:40:16 90.9 2.0 0.1 0.0 12/07/05 09:40:26 90.0 1.7. 0.1 0.0 12/07105 09:40:36 39.3 1.7 0.0 -0.1 12J07/05 09:40:46 1:5 1.8 0.0 -0.1 12/07/05 09:40:56 1.3 1.6 0.0 -0.1 

### 89.2 ppm C3H8



# • 76
Page 512/7/05 Run #1



### Date/Time VOC CO NOx S02 mm/dd/yy hh:mm:ss ppm ppm ppm ppm 12/07/0510:09:47 54.6 219.9 29.3 0.4 12/07/0510:09:57 53.7 220.9 29.3 0.3

Start Run #1 12/07/0510:10:07 53.5 221.9 29.2 0.2 12107/0510:10:17 53.7 223.0 29.3 0.3 12/07/0510:10:27 52.9 223.8 29.3 0.2 12/07/0510:10:37 53.3 223.9 29.3 0.1 12107/0510:10:47 52.8 224.1 29.4 0.1 12107/0510:10:57 52.5 224.4 29.4 0.2 1210710510:11:07 52.5 224.5 29.2 0,2 12/07/0510:11:17 52.7 223.8

. 29.2 0.2 12/07/0510:11:27 52.3 223.8 29.3 0.2 12107/0510:11:37 51.2 223.6 29.3 0.2 12107/0510:11:47 50.8 223.3 29.1 0.2 12/07/0510:11:57 51.7 222.7 29.0 0.2 12107/0510:12:07 52.6 222.2 28.9 0.2 12/0710510:12:17 52.4 222.2 28.7 0.2 12/07/0510:12:27 52.1 222.0 28.6 0.1 1210710510:12:37 52.3 221.9 28.6 0.2 1210710510:12:47 52.2 221.8

. 28.6 0.1 12/0710510:12:57 53.0 222.1 28.6 0.1 12/07/06 10:13:07 52.7 222.6 28.5 0,1 12/07/0510:13:17 51.8 223.6 28.5 0.0 12/0710510:13:27 52.4 224.6 28.6 0.0 12107/0510:13:37 51.6 225.3 28.5 0.1 12107/0510:13:47 52.0 225.3 28.4 0.1 12107/0510:13:57 51.1 225.3 28.3 0.1 120710510:14:07 51.3 225.1 28.2 0.1 1210710510:14:17 51.5 225.0 28.3 0.1 12/07/0510:14:27 51.0 224.7 28.6 0.1 12/0710510:14:37 50.9 224.6 28.6 0.1 1210710510:14:47 50.4 225.1 28.8 0.1 12/07/0510:14:57 50.9 225.3 29.0 0.2 12107/0510:15:07 50.1 225.8 29.1 0,2 12107/0510:15:17 50.1 226.1 29.1 0.1 12107/0510:15:27 50.2 226.6 29.1 0.1 1 2107105 1 0:15:37 50.5 227.1 29.0 0.1 1210710510:15:47 50.0 227.1 29.0 0.1 12107/0510:15:57 50.8 227.1 29.0 0.1 12/07/0510:16:07 49.9 227.1 29.1 0.1 1210710510:16:17 49.5 226.7 29.1 0.1 12/07/0510:16:27 49.9 226.5 29.1 0.1 12107/0510:16:37 49.3 225.9 29.2 0.1 1210710510:16:47 49.2 225.7 29.3 0.1 1210710510:16:57 49.5 225.3 29.4 0.1 12/0710510:17:07 49.3 224.8 29.5 0.1 12107/0510:17:17 48.5 224.1 29.5 0.1 12107/0510:17:27 48.1 223.6 29.3 0.1 12107/0510:17:37 47.9 223.4 29.3 0.0 12/07/0510:17:47 48.1 223.6 29.1 0.0 1210710510:17:57 47.4 223.4 29.0 0.0 12/07/0510:18:07 47.6 223.0 28.8 0.0 12/07/0510:18:17 47.9 222.3 28.7 0.0 12/07/0510:18:27 48.1 221.4 28.6 0.0 12107/0510:18:37 48.0 221.0 28.5 0.1 1210710510:18:47 47.9 221.0 28.8 0.1 12/07/0510:18:57 48.4 221.2 28.8 0.1 12/0710510:19:07 48.3 221.7 29.1 0.1 12/0710510:19:17 48.4 222.3 29.2 0.1 1 2107/05 1 0:19:27 48.3 223.3 29.2 0.2 12/07/0510:19:37 47.9 224.4 29.3 0.1 12/07/0510:19:41 48.5 224.8 29.3 0.1 12/07/0510:19:57 48.3 224.8 29.3 0.1 12/07/0510:20:07 48.4 224.8 29.3 0.1 1210710510:20:17 48.6 224.8 29.3 0.1 12107/0510:20:27 48.2 224.7 29.4 0.1 12107/0510:20:37 48.3 224.5 29.5 0.1 12/0710510:20:47 48.3 224.3 29.6 0.1 12107/0510:20:57 48.5 224.2 29.7 0.1 1 2107/05 1 0:21:07 48.9 223.9 29.7 0,1 12107/0510:21:17 49.1 224.0 29.8 0.1

7 •

~

7 Page 11217/05 Run #1

12/0710510:21:27 49.1 224.1 29.8 0.1 12/07/0510:21:37 49.0 224.9 29.8 0.1 12/07/0510:21:47 48.8 224.9 29.9 0.0 12/07/0510:21:57 49.6 224.9 29.9 0.0 1210710510:22:07 49.2 224.6 29.9 0.0 12107/0510:22:17 49.1 224.2 29.9 0.1 12107/0510:22:27 49.8 223.8 30.0 0.1 12/0710510:22:37 50.0 223.2 30.0 0.1 12/07/0510:2247 50.4 223.2 30.0 0.1 12/07/0510:22:57 50.7 222.8 29.9 0.1 12107/0510:23:07 51.4 222.8 29.8 0.1 12/07/0510:23:17 52.1 222.8 29.7 0.1 12/0710510:23:27 52.5 223.3 29.5 0.0 12/0710510:23:37 53.1 224.1 29.4 010 12/07/0510:23:47 52.9 224.5 29.0 0.0 12/07/0510:23:57 53.0 225.2 28.7 0.0 12/07/0510:24:07 53.4 225.9 28.5 0.0 12107/0510:24:17 54.1 226.7 28.4 0.0 12/07/0510:24:27 53.2 227.3 28.3 0.0 12/07/0510:24:37 53.3 227.5 28.2 0.0 1210710510:24:47 53.4 227.8 28.3 0.0 1210710510:24:57 53.1 228.0 28.3 0.0 12/0710510:25:07 52.5 228.4 28.6 -0.1 12/07/0510:25:17 52.1 228.6 28.8 -0.1 1210710510:25:27 51.7 229.3 29.0 -0.1 1210710510:25:37 50.8 229.5 29.2 -0.1 12107/0510:25:47 49.9 229.4 29.2 -0.1 12107/0510:25:57 48.7 229.2 29.1 -0.1 12/07/0510:26:07 48.2 228.9 29.1 -0.2 12107/0510:26:17 48.4 228.0 29.1 -0.2 12107/0510:26:27 47.1 226.9 29.2 -0.1 12/07/0510:26:37 47.3 226.5 29.3 -0.1 1210710510:26:47 46.8 225.7 29.4 -0.2 1210710510:26:57 46.6 225.3 29.6 -0.1 1210710510:27:07 46.5 224.7 29.7 -0.1 1210710510:27:17 46.7 224.1 29.7 -0.1 1210710510:27:27 46.8 223.8 29.8 -0.1 1210710510:27:37 47.1 224.0 29.9 -0.1 12/0710510:27:47 46.9 223.9 29.9 0.0 1210710510:27:57 46.2 223.4 30.1 0.0 12/0710510:28:07 46.2 222.8 30.2 0.0 12/0710510:28:17 46.2 221.7 30.1 0.0 12/0710510:28:27 46.4 220.6 30.0 -0.1 12/0710510:28:37 46.1 220.0 30.1 -0.1 12/0710510:28:47 46.3 219.4 30.1 -0.1 12107/0510:28:57 48.4 218.8 30.1 -0.2 12/0710510:29:07 46.7 218.4 30.1 -0.2 12/0710510:29:17 47.0 217.9 30.1 -0.2 12/07/0510:29:27 47.0 217.6 30.2 -0.2 12107/0510:29:37 47.4 217.6 30.3 -0.1 12/07/0510:29:47 47.1 217.3 30.2 -0.1 12107/0510:29:57 46.5 217.4 30.2 -0.2 12/07/0510:30:07 46.6 217.5 30.2 -0.2 12107/0510:30:17 47.1 217.3 30.2 -0.2 12/07/0510:30:27 47.5 217.0 30.2 -0.2 12/07/0510:30:37 47.7 216.9 30.1 -0.3 12/07/0510:30:47 48.0 216.6 30.3 -0.2 12/07/0510:30:57 47.9 216.4 30.3 -0.2 12/07/0510:31:07 47.7 216.2 30.3 -0.2 12107/0510:31:17 47.6 216.0 30.3 -0.2 12/07/0510:31:27 47.2 215.6 30.3 -0.2 12/0710510:31:37 47.1 215.1 30.4 -0.2 12107/0510:31:47 46.8 .215.0 30.3 -0.1 1210710510:31:57 46.9 215.0 30.3 -0.2 1210710510:32:07 46.7 214.9 30.3 -0.3 12/07/0510:32:17 46.9 214.9 30.2 -0.3 12107/0510:32:27 46.6 214.5 30.2 -0.2 1 2107/05 1 0:32:37 47.0 214.2 30.2 -0.3 12107/0510:32:47 46.6 214.3 30.1 -0.2 12/07/0510:32:57 46.8 214.9 30.1 -0.2 12/0710510:33:07 46.7 215.6 30.1 -0.3 12/07/0510:33:17 46.5 215.9 30.1 -0.3 12/07/0510:33:27 46.4 216.4 30.1 -0.3 12/07/0510:33:37 46.4 216.4 30.1 -0.3

Page 2 

# 7812/7/05 Run #1

12/07/0510:33:47 46.6 216.2 30.1 -0.2 12/07/0510:33:57 46.9 215.9 30.1 -0.3 12/07/0510:34:07 46.9 216.6 30.0 -0.4 12/07/0510:34:17 46.3 215.4 30.1 -0.3 12/07/0510:34:27 46.3 215.3 30.1 -0.4 12/0710510:34:37 46.1 215.3 30.2 -0.4 12J07/0510:34:47 46.1 215.4 30.1 -0.3 12/07/0510:34:57 45.5 215.7 30.1 -0.3 12/07/0510:35:07 45.5 216.3 30.2 -0.3 12/07/0510:35:17 45.8 216.5 30.2 -0.3 12/07/0510:35:27 45.8 217.0 30.2 -0.2 1210710510:35:37 46.3 217.4 30.3 -0.3 12107/0510:35:47 45.7 217.6 30.3 -0.3 12107/0510:35:57 45.9 217.6 30.3 -0.3 12/07/0510:36:07 45.2 217.6 30.2 -0.3 1210710510:36:17 45.7 218.0 30.1 -0.3 12/07/0510:36:27 45.9 217.7 30.1 -0.3 12107/0510:36:37 45.6 217.6 29.9 -0.4 12107/0510:36:47 45.6 217.9 29.9 0.0 12107/0510:36:57 45.6 217.8 29.8 0.0 12/0710510:37:07 45.7 218.1 29.8 0.0 12/0710510:37:17 45.5 218.2 29.9 -0.1 12/07/0510:37:27 45.1 218.3 29.8 -0.1 12107/0510:37:37 461 217.8 29.8 -0.1 12/07/0510:37:47 45.7 217.7 30.0 -0.1 12/07/0510:37:57 45.7 217.2 29.9 -0.1 12/0710510:38:07 46.0 216.9 29.9 -0.1 12/0710510:38:17 46.3 216.3 30.0 -0.1 12/07/0510:38:27 46.2 215.7 30.0 -0.2 12/07/0510:38:37 46.7 216.3 29.9 -0.1 12/07/0510:38:47 46.8 214.6 29.9 -0.1 12/07/0510:38:57 46.4 213.8 29.8 -0.1 12107/0510:39:07 46.6 213.5 29.8 -0.1 12/07/0510:39:17 46.5 213.3 29.8 -0.2 12/07l0510:39:27 46.6 213.3 29.8 -0.1 12/07/0510:39:37 46.5 212.9 29.9 -0.1 12/07/0510:39:47 46.3 212.5 30.0 -0.1 12/07/0510:39:57 46.5 212.4 30.0 -0.2 12/07/0510:40:07 46.3 212.5 30.2 -0.2 1210710510:40:17 46.6 212.5 30.1 -0.1 12/07/0510:40:27 46.6 212.7 30.1 -0.1 12/07/0510:40:37 46.5 212.8 30.0 -0.1 12/07/0510:40:47 46.3 212.9 29.9 -0.1 12/07/0510:40:57 46.1 213.3 29.9 0.0 12/0710510:41:07 45.7 213.4 29.9 0.0 12107/0510:41:17 46.2 213.1 29.8 0.0 12J0710510:41:27 45.9 213.0 29.9 0.0 12/0710510:41:37 45.8 213.1 29.9 -0.1 12/0710510:41:47 45.4 212.7 29.9 -0.1 12/07/0510:41:57 45.5 212.4 29.8 -0.2 12/07/0510:42:07 45.7 212.2 29.8 -0.2 1 2107/05 1 0:42:17 45.5 211.9 29.9 -0.2 12/07/0510:42:27 45.7 211.9 29.9 -0.2 12/0710510:42:37 45.9 212.0 29.9 -0.1 12107/0510:4247 46.2 211.8 29.7 -0.1 12/07/0610:42:57 46.1 211.7 29.7 -0.2 12/07/0510:43:07 46.1 211.9 29.7 -0.2 12107/0510:43:17 45.9 211.9 29.7 -0.2 12107/0510:43:27 45.5 212.1 29.7 -0.1 12/07/0510:43:37 45.6 212.0 29.7 -0.2 12/07/0510:43:47 45.9 211.6 29.8 -0.2 12/07/0510:43:57 46.6 211.5 29.8 -0.3 12/07/0510:44:07 46.5 211.8 29.9 -0.3 12/07/0510:44:17 46.1 212.1 30.1 -0.2 12107/0510:44:27 46.4 212.6 30.1 -0.2 1210710510:44:37 46.6 212.9 30.1 -0.2 12/07/0510:44:47 46.1 213.1 30.0 -0.2 12107/0510:44:57 46.9 212.9 29.9 -0.1 12/07/0510:45:07 47.1 213.1 29.8 0.0 12/07/0510:45:17 46.9 213.3 29.8 0.0 12/07/0510:45:27 47.1 213.7 29.8 0.0 12/07/0510:45:37 47.8 213.6 29.8 0.0 12107/0510:45:47 47.2 213.6 29.8 0.0 12/07/0510:45:67 47.2 213.3 29.9 0.0

Page 3 

# 791217105 Run il1

12107/0510:46:07 46.9 213.1 31.0 -0.1 12/07/05 10:46:17 46.7 213.3 3(

~ () -0.1 1210710510:46:27 46.5 213.3 30.0 -0.1 12107/0510:46:37 46.8 213.4 30.1 -0.1 1210710510:46:47 46.8 213.3 30.0 -0.1 12/07/0510:46:57 46.5 213.1 29.9 -0.1 12/07/0510:47:07 47.2 213.0 29.8 -0.1 12/07/0510:47:17 47.3 212.9 29.7 -0.1 1210710510:47:27 47.1 213.1 29.7 -0.1 12107/0510:47:37 46.5 213.0 29.7 -0.1 1210710510:47:47 46.0 212.8 29.7 0.0 1210710510:47:57 46.7 212.9 29.8 -0.1 12/0710510:48:07 47.2 212.6 29.9 0.0 12/0710510:48:17 46.8 212.5 30.0 0.0 1210710510:48:27 46.6 212.8 30.2 -0.1 12107/0510:48:37 46.9 212.9 30.2 -0.1 12107/0510:48:47 46.5 212.9 30.1 -0.1 12107/0510:48:57 46.6 212.9 30.1 -0.1 12/07/0510:49:07 46.8 213.2 30.0 -0.1 12107/0510:49:17 46.4 213.4 29.9 -0.1 1210710510:49:27 45.7 213.5 29.8 -0.1 12/07/05 10:49:37 46.5 213.5 29.8 -0.1 12/07/0510:49:47 46.2 214.0 29.7 -0.1 12/07/0510:49:57 45.9 214.6 29.7 -0.1 12/07/0510:50:07 45.5 214.8 29.7 -0.1 12107/0510:50:17 45.3 214.9 30.0 -0.1 12/07/0510:50:27 45.5 214.9 30.0 -0.1 12/07/0510:50:37 45.1 215.9 30.2 -0.1 12107/0510:50:47 45.6 215.9 30.3 -0.1 12/0710510:50:57 45.5 215.3 30.3 -0.1 12107/0510:51:07 44.7 215.0 30.2 0.0 12/0710510:51:17 44.6 214.8 30.0 -0.1 12107/0510:51:27 45.0 214.2 30.0 -0.1 12107/0510:51:37 45.1 213.1 30.0 -0.1 1210710510:51:47 44.9 212.5 30.0 -0.1 12/07/0510:61:57 44.2 212.0 30.0 -0.3 12/07/0510:52:07 44.2 211.3 30.2 -0.3 12/0710510:52:17 44.0 210.9 30.3 -0.2 12107/0510:52:27 43.9 210.6 30.3 -0.1 12107/0510:52:37 44.3 210.2 30.3 -0.2 1210710510:52:47 44.3 209.8 30.2 -0.3 12/07/0510:52:57 44.3 209.5 30.3 -0.3 12107/0510:53:07 44'.4 209.3 30.2 -0.3 12/07/0510:53:17 44.3 209.3 30.2 -0.3 12/07/0510:53:27 44.9 209.5 30.2 -0.2 12107/0510:53:37 44.6 209.6 30.1 0.0 12/07/0510:53:47 44.9 209.9 30.1 0.0 12107/0510:53:57 45.5 210.1 30.3 0.0 12107/0510:54:07 45.2 141.2 30.1 -1.1 12107/0510:54:17 46.1 209.6 30.5 0.1 12107/0510:54:27 45.9 210.1 30.6 0.1 12/07/0510:54:37 45.9 210.4 30.5 0.1 1210710510:54:47 46.0 210.6 30.5 0.1 12/07/0510:54:57 45.5 210.9 30.5 0.1 12/07/0510:55:07 46.1 211.0 30.4 0.1 12107/0510:55:17 46.4 210.9 30.3 0.0 12J07/0510:55:27 46.9 211.0 30.3 0.1 1210710510:55:37 46.9 211.2 30.4 0.1 1210710510:55:47 46.5 211.2 30.5 0.0 1210710510:55:57 46.6 211.2 30.5 -0.1 12107/0510:56:07 46.7 211.2 30.5 0.0 12107/0510:56:17 46.9 211.1 30.6 0.0 12/07/05 10:56:27 47.0 211.1 30.6 0.0 1 2107/05 1 0:56:37 47.0 21•1.3 30.5 0.1 12/0710510:56:47 47.2 187.1 30.2 -1.1 1210710510:56:57 47.2 195.7 30.5 0.1 12107/0510:57:07 46.8 211.8 30.3 0.0 12107/0510:57:17 46.7 211.9 30.4 0.0 12107/0510:57:27 46.7 211.9 30.4 0.0 12107/0510:57:37 46.7 211.7 30.4 0.0 12/07/0510:57:47 46.1 211.3 30.5 0.0 12107/0510:57:57 46.6 210.9 30.4 0.0 12I07/05 10:58:07 46.4 210.9 30.5 0.0 12/07/0510:58:17 45.9 210.8 30.6 -0.1



### Page 4 

# To * -*1217/05 Run #1

12107/0510:58:27 46.2 210.7 30.5 -0.1 12107/0510:58:37 48.9 210.8 30.5 -0.1 1210710510:58:47 46.6 211.1 30.6 -0.1 1210710510:58:57 46.4 211.3 30.6 -0.1 12107/0510:59:07 46.4 211.7 30.7 0.0 12J07/0510:59:17 45.3 211.8 30.7 0.0 12107/0510:59:27 45.7 211.6 30.7 0.0 12/07/0510:59:37 45.7 211.6 30.7 0.0 12/07/0510:59:47 45.0 211.5 30.8 0.0 12/07/0510:59:57 45.5 211.4 30.9 -0.1 12/07/0511:00:07 45.8 211.5 30.9 -0.1 1210710511:00:17 45.2 211.6 31.0 0.0 12/07/0611:00:27 44.8 211.7 30.9 0.0 1210710511:00:37 44.6 211.5 30.8 0.0 1 2107/05 1 1:00:47 44.9 211.4 30.8 0.0 12f07/0511:00:57 44.8 211.2 30,7 0.0 1 2107/05 1 1:01:07 44.5 211.2 30.6 -0.1 12l07/0511:01:17 44.9 211.3 30.6 -0.2 12107/0511:01:27 44.3 211.2 30.5 -0.2 12107/0511:01:37 44.2 210.9 30.5 -0.2 1 2107/05 1 1:01:47 44.6 210.5 30.5 -0.1 12/07/0511:01:57 44.1 210.6 30.5 -0.1 12107/0511:02:07 44.6 210.5 30.4 -0.2 12107/0511:02:17 44.8 210.9 30,4 -0.1 12107105 1 1:02:27 45.6 211.2 30.4 -0.1 1210710511:02:37 45.3 211.7 30.4 -0.1 12/0710511:02:47 45.0 212.0 30.3 -0.1 12107/0511:0257 45.1 212.0 30.4 -0.1 12/07/0511:03:07 45.2 212.3 30.4 -0.1 12/07/0511:03:17 45.6 212.1 30.5 -0.1 12/07/0511:0327 45.6 212.0 30.6 -0.1 12/0710511:03:37 45.5 211.7 30.6 -0.1 12/07/0511:03:47 45.4 211.5 30.7 -0.1 12107/0511:03:57 45.9 211.6 30.8 -0.1 1 2107/05 1 1:04:07 48.0 211.4 30.9 -0.1 12/07/0511:04:17 46.0 211.5 30.9 -0.1 12/07/0511:04:27 46.5 211.7 30.8 -0.2 12107/0511:04:37 46.8 211.6 30.8 -0.1 1 2/07105 1 1:04:47 47.0 211.7 30.7 -0.1 1210710511:04:57 47.0 211.8 30.5 -0.1 12/0710511:05:07 46.7 211.7 30.4 -0.1 12/07/0511:05:17 47.4 211.7 30.3 -0.1 12/07/0511:05:27 46.9 212.0 30.3 -0.1 12/07/0511:05:37 46.8 212.3 30.3 -0.1 12107/0511:05:47 47.3 212.6 30.3 -0.1 12/07/0511:05:57 47.4 212.8 30.3 -0.1 12107/0511:06:07 47.3 213.1 30.4 0.0 12107/0511:06:17 47.4 213.2 30.4 0.0 12/07/0511:06:27 47.4 213.1 30.4 0.0 12107/0511:06:37 47.2 213.1 30.3

. 0.0 12107/0511:06:47 47.3 213.1 30.2 0.0 12107/0511:06:57 47.3 212.8 30.1 0.0 12/07/0511:07:07 47.3 212.9 30.0 -0.1 12/07/0511:07:17 46.7 213.2 30.0 0.0 12107/0511:07:27 46.2 213.7 29.9 0.0 12/07/0511:07:37 46.1 214.3 30.0 -0.1 12107/0511:07:47 46.3 214.5 30.1 -0.1 12/0710511:07:57 45.9 215.0 30.2 -0.1 12/0710511:08:07 46.2 215.0 30.4 -0.1 12/0710511:08:17 45.7 214.8 30.5 -0.1 12/07/0511:08:27 45.5 214.6 30.6 -0.1 12/0710511:08:37 45.8 214.5 30.6 -0.1 12/0710511:08:47 45.7 213.6 30.6 -0.2 12/07/0511:08:57 45.4 213.2 30.6 -0.1 12/07/0511:09:07 45.6 212.9 30.5 0.0 12/0710511:09:17 45.3 213.0 30.5 -0.1 12/07/0511:09:27 45.2 213.1 30.4 -0.1 12/07/0511:09:37 44.8 212.6 30.6 -0.1 12/07/0611:09:47 45.1 212.0 30.6 -0.1 1 2107/05 1 1:09:57 45.3 211.5 30.6 -0.1 12107/0511:10:07 45.5 211.3 30.5 0.0 12/07/0511:10:17 45.2 211.4 30.5 -0.1 12/0710511:10:27 45.2 211.4 30.5 -0.1 12/07/05 11:10:37 45.1 211.3 30.4 ' 0.0

Page 5 

# ol1217105 Run #1

12107/0511:10:47 45.1 211.5 30.4 0.0 12/07/0511:10:57 45.0 211.8 30.3 -0.1 12/07/0511:11:07 45.7 212.2 30.2 -0.1 1 2107/05 1 1:11:17 46.0 212.3 30.2 -0.1 12107/0511:11:27 45.4 212.7 30.1 -0.1 12J07/0511:11:37 45.3 213.1 30.1 -0.1 12107/0511:11:47 45.0 213.5 30.1 -0.2 12/0710511:11:57 45.4 214.0 30.2 -0.2 12/07/0511:12:07 45.5 214.5 30.3 -0.2 12/0710511:12:17 45.5 214.6 30.3 -0.3 1210710511:12:27 45.5 214.8 30.2 -0.2 12/0710511:12:37 45.2 214.8 30.1 -0.2 1210710511:12:47 45.9 214.6 30.0 -0.1 12/0710511:12:57 45.7 214.5 30.1 0.0 1210710511:13:07 45.7 214.6 30.1 0.0 12/0710511:13:17 45.4 214.8 30.2 0.0 12/0710511:13:27 45.6 215.0 30.2 0.0 1 2/07105 1 1:13:37 45.8 213.9 30.4 -0.1 1 2/07105 1 1:13:47 45.3 157.5 30.2 -1.2 12/0710511:13:57 44.5 139.2 30.0 -3.2 12/07/0511:14:07 45.5 215.5 30.5 0.0 12107/0511:14:17 45.8 215.4 30.5 -0.1 12107/0511:14:27 45.9 215.5 30.4 -0.1 12/07/0511:14:37 45.9 215.5 30.4 0.0 12/07/0511:14:47 46.3 215.5 30.4 0.0 12/07/0511:14:57 45.6 214.9 30.4 -0.1 12/07/0511:15:07 45.6 214.2 30.3 0.0 12/07/0511:15:17 46.2 213.6 30.3 0.0 12/07/0511:15:27 46.5 212.6 30.3 0.0 1 2107/05 1 1:15:37 46.8 212.3 30.3 0.1 12/0710511:15:47 46.4 211.8 30.4 0.0 1 2107/05 1 1:15:57 46.6 211.9 30.4 0.0 1210710511:16:07 46.6 211.8 30.4 0.0 1210710511:16:17 46.7 211.9 30.4 0.0 1210710511:16:27 47.2 212.1 30.3 -0.1 1210710511:16:37 47.1 212.3 30.3 -0.1 12107/0511:16:47 47.0 212.4 30.2 0.0 12/07/0511:16:57 47.1 212.3 30.1 0.0

Stop Run #1 47.17 215.86 29.93 -0.08

12/07/0511:17:07 46.9 212.3 30.1 -0.1 1 2107/05 1 1:17:17 46.6 212.3 30.1 0.0 12107/0511:17:27 46.8 212.3 30.1

. -0.1 12107/0511:17:37 46.9 212.2 30.2 -0.1 12107/0511:17:47 46.6 212.0 30.2 0.0 12/07/0511:17:57 46.4 211.8 30.2 0.0 12107/0511:18:07 46.2 92.4 30.2 -0.3 12107/0511:18:17 43.4 211.5 30.5 0.0 12/07/0511:18:27 3.5 208.9 30.3 0.0 12107/05 11:18:37 1.6 196.1 29:1 0.0 12107/0511:18:47 1.6 147.0 25.3 -0.1 12/07/0511:18:57 1.5 100.0 18.9 -0.2 12107/0511:19:07 1.5 65.7 14.2 -0.2 12/07/0511:19:17 0.8 43.2 11.1 -0.4 12/0710511:19:27 0.7 29.1 9.2 -0.5 12/07/0511:19:37 0.7 19.1 11.3 -0.6 12107/0511:19:47 0.6 13.9 16.2 -0.5 12107/0511:19:57 0.6 10.3 19.7 -0.4 12/07/0511:20:07 0.5 7.8 22.2 -0.2 12107/0511:20:17 0.4 6.5 23.6 -0.1 12107/0511:20:27 0.4 5.7 

## 23.6 -0.2
12107/0511:20:37 0.4 5.4 

## 23.6 -0.1
12/07/0511:20:47 0.4 5.0 

## 23.7 -0.1
12/07/0511:20:57 0.7 4.8 

## 23.5 -0.2 12/07/0511:21:07 1.5 4.7 23.5 -0.3 12/07/0511:21:17 1.5 6.3 23.0 -0.3 12/0710511:21:27 1.5 9.2 19.7 -0.3 12/07/0511:21:37 1.5 9.3 14.5 -0.3 12/07/0511:21:47 1.4 7.8 10.5 -0.4 12/07/0511:21:57 1.4 6.3 8.2 -0.4 12J0710511:22:07 1.2 4.9 6.7 -0.3 12/07/0511:22:17 0.2 3.8 5.7 -0.3 25.5 ppm NOx Zero S02



## Page 61217/05 Run #1

12/07/0511:22:27 0.2 2.4 4.9 -0.2 12/07/0511:22:37 0.3 1.3 4.2 -0.1 12107/0511:22:47 0.2 0.7 3.8 0.6 12/07/0511:22:57 0.2 0.4 3.7 3.1 12/0710511:23:07 0.2 0.5 3.7 7.1 12/0710511:23:17 0.2 0.5 3.7 12.9 12107/0511:23:27 0.3 0.4 3.7 20.3 12/07/0511:23:37 0.3 0.5 3.7 28.3 12/07/0511:23:47 0.2 0.6 3.5 36.0 12/07/0511:23:57 0.2 0.5 3.4 43.3 12/07/0511:24:07 0.2 0.4 3.3 49.8 12/07/0511:24:17 0.2 0.3 3.2 55.1 12J07/0511:24:27 0.2 0.3 3.0 59.4 12107/0511:24:37 0.3 0.4 2.9 62.9 1 2107/05 1 1:24:47 0.2 0.4 2.7 66.0 12/07/0511:24:57 0.2 0.5 2.5 68.7 1 2107/05 1 1:25:07 0.2 0.5 2.4 70.6 12107/0511:25:17 0.2 0.4 2.2 72.4 12107/0511:25:27 0.2 0.5 2.1 73.8 12/07/0511:25:37 0.3 0.4 2.0 75.1 12107/0511:25:47 0.2 0.3 1.9 76.1 12107/0511:25:57 0.2 0.3 1.8 76.9 12/07/0511:26:07 0.2 0.3 1.7 77.5 12/07/0511:26:17 0.3 0.4 1.6 78.3 12/07/0511:26:27 0.2 0.3 1.6 79.3 12107/0511:26:37 0.2 0.4 1.6 80.1 12/07/0511:26:47 0.2 0.3 1.5 80.9 12107/0511:26:57 0.2 0.3 1.4 81.4 12/07/0511:27:07 0.2 0.3 1.3 82.4 12/07/0511:27:17 0.2 0.4 1.3 83.3 12/07/0511:27:27 0.2 0.3 1.2 84.2 12/07/0511:27:37 0.3 0.3 1.1 85.1 12107/0511:27:47 0.3 0.3 1.1 85.6 12/07/0511:27:57 0.2 0.3 1.0 86.1 12/07/0511:28:07 0.2 0.4 1.0 86.7 12/0710511:28:17 0.2 0.3 1.0 87.1 12/0710511:28:27 0.2 0.3 0.9 87.4 12/0710511:28:37 0.2 0.3 0.9 87.7 12107/0511:28:47 0.2 0.3 0.8 89.0 12/07J0511:28:57 0.2 0.3 0.8 90.6 12/07/0511:29:07 0.2 0.4 0.7 90.8 12/07/0511:29:17 0.3 0.4 0.7 91.2 12/07/0511:29:27 0.3 0.5 0.7 91.6 12/07/0511:29:37 0.3 0.4 0.7 93.2 12/07/0511:29:47 0.2 0.3 0.7 94.3 12/07/0511:29:57 0.3 0.3 0.6 94.5 12107/0511:30:07 0.3 0.3 0.6 94.8 12107/0511:30:17 0.2 0.3 0.6 95.1 12107/0511:30:27 0.3 0.4 0.5 95.1 12/07/0511:30:37 0.3 0.6 0.5 96.0 12/07/0511:30:47 0.3 0.5 0.5 96.2 12107/0511:30:57 0.3 

### 0.4 0.5 

### 96.2
12107/05 11:31:07 0.2 

### 0.4 0.4 

### 96.4 101 ppm S02 12107/05 11:31:17 0.2 

### 0.4 0.5 

### 96.5 Zero CO
12/07/0511:31:27 0.2 

### 0.4 0.5 

### 96.7 12/0710511:31:37 0.2 0.4 0.4 96.3 12/0710511:31:47 0.7 0.4 0.4 94.5 12/07/0511:31:57 0.2 0.4 0.4 93.8 12107/0511:32:07 0.2 13.8 0.4 93.3 12107/0511:32:17 0.2 66.1 0.4 89.9 12107/0511:32:27 0.2 103.3 0.4 82.9 12/07/0511:32:37 0.2 126.9 0.5 74.8 1210710511:32:47 0.2 142.8 0.4 66.3 12107/0511:32:57 0.2 153.6 0.4 58.0 12/07/0511:33:07 0.2 160.1 0.3 50.2 12/07/0511:33:17 0.2 163.9 0.3 43.2 12/07/0511:33:27 0.3 167.2 0.3 37.3 12/07/0511:33:37 0.2 169.8 0.3 32.5 12/07/0511:33:47 0.3 172.5 0.4 28.7 12/07/0511:33:57 0.3 174.8 0.4 25.3 12/07/0511:34:07 0.3 176.1 0.3 22.3 12/07/0511:34:17 0.3 176.9 0.4 19.6 12/07/0511:34:27 0.4 177.5 0.3 17.5


# 83
Page 7

### 1217105 Run #1

12/07l0511:34:37 0.3 177.6 0.3 15.5 1210710511:34:47 0.3 178.5 0.3 13.8 1 2107105 1 1:34:57 0,3 178.8 0.3 12.5 1 P10710511:35:07 0.2 179.4 0.3 11.4 1210710511:35:17 0.3 179.4 0.3 10.3 12/0710511:35:27 

### 0.3 179.5 0.3 9.3 1 2107105 1 1:35:37 

### 0.3 179.7 0.3 8.3 200 ppm CO 12/07105 11:35:47 

### 0.3 179.7 0.3 7.7 Zero VOC, tVOx 12/07/0511:35:57 0.3 

### 180.0 0.3 7.1 12107/0511:36:07 0.2 179.3 0.2 6.6 12/07/05 1 1:36:17

- 

### 7.6 176.7 0.3 6.0 12/07l0511:36:27 46.3 175.3 0.3 5.5 12J07l0511:36:37 47.2 165.9 0.3 5.1 12/0710511:36:47 47.6 ' 

### 125.4 0.3 4.7 12/0710511:36:57 

### 47.8 77.1 0.3 4.4 12107/0511:37:07 

### 47.8 45.4 0.3 4.1 48.8 ppm C3H8 1 2/07105 1 1:37:17 

### 47.8 28.9 0.3 3.9 12107/0511:37:27 

### 47.8 18.8 0.3 3.8 12J0710511:37:37 45.9 12.9 0.3 3.6 12/0710511:37:47 9.8 8.6 0.2 3.4



# 84 Page 81217/05 Run #2

Date/Time VOC CO NOx S02 

### mm/dd/yy hh:mm:ss ppm ppm ppm ppm 1210710512:14:40 60.7 186.4 23.4 0.1 12107105 1 2:14:50 59.0 195.3 25.1 0.2

Start Run #2 12/07/0512:15:00 58.1 201.1 26.0 0.1 12/07/0512:15:10 56.9 204.8 26.5 0.2 12/0710512:15:20 55.6 206.8 27.0 0.2 12/07/0512:15:30 53.9 207.9 27.3 0.3 12/0710512:15:40 50.6 208.5 27.3 0.3 12/07/0512:15:50 48.8 209.2 27.5 0.2 12107/0512:16:00 46.9 209.7 27.6 0.2 12107/0512:16:10 48.7 210.0 27.6 0.3 12/07/0512:16:20 47.8 210.4 27.7 0.3 12/07/0512:16:30 47.2 210.8 27.6 0.2 12/0710512:16:40 47.2 211.0 27.6 0.2 12/07/0512:16:50 46.7 210.9 27.6 0.3 12/07/0512:17:00 47.0 210.9 27.7 0.2 12/07/0512:17:10 46.7 210.8 27.7 0.3 12/07/0512:17:20 46.7 210.9 27.8 0.4 12/07/0512:17:30 45.3 210.8 27.9 0.4 12/07/0512:17:40 45.6 211.0 28.0 0.4 12/07/05 12:17:50 45.8 211.0 28.0 0.4 12/07/0512:18:00 45.7 210.6 28.0 0.3 12/07/0512:18:10 45.7 209.9 28.1 0.2 12107/0512:18:20 45.9 208.4 28.1 0.3 12/07/0512:18:30 45.9 206.3 28.1 0.2 12107/0512:18:40 45.6 204.2 28.1 0.2 12107/0512:18:50 46.1 202.1 28.2 0.3 12/07/0512:19:00 45.5 200.3 28.3 0.4 1210710512:19:10 45.5 199.3 28.4 0.3 1210710512:19:20 45.5 198.9 28.5 0.3 12/0710512:19:30 46.3 199.5 28.6 0.3 12/07/0512:19:40 45.7 200.1 28.7 0.4 12/07/0512:19:50 45.8 201.0 28.8 0.4 12107/0512:20:00 46.1 202.4 28.9 0.3 12107/0512:20:10 44.9 203.3 29.0 0.2 12/07/0512:20:20 44.9 203.8 29.0 0.3 12/07/0512:20:30 45.5 203.9 29.0 0.2 12/0710512:20:40 45.4 204.6 29.2 0.2 12/07/0512:20:50 45.0 204.8 29.2 0.3 12/07/0512:21:00 45.8 205.0 29.4 0.3 1210710512:21:10 46.1 205.5 29.4 0.3 12107/0512:21:20 45.5 205.7 29.6 0.3 12107/0512:21:30 44.6 191.1 28.5 -0.9 1210710512:21:40 45.6 188.4 29.5 0.2 12/07/0512:21:50 45.8 125.7 29.7 0.1 12/07/0512:22:00 46.2 206.8 29.7 0.4 12/07/0512:22:10 46.3 206.9 29.8 0.4 1210710512:22:20 46.0 207.3 29.8 0.5 12107/0512:22:30 46.4 207.3 29.9 0.4 12/07/0512:22:40 46.0 207.3 29.9 0.4 12/07/0512:22:50 45.3 167.4 28.8 -4.4 12/07/0512:23:00 46.1 206.4 29.8 0.2 1 2107/05 1 2:23:10 46.0 207.0 30.1 0.4 1210710512:23:20 46.8 206.8 30.1 0.3 12/07/0512:23:30 46.1 206.5 30.1 0.2 12107/0512:23:40 45.9 207.0 30.1 0.2 12/07/0512:23:50 46.2 207.4 30.2 0.2 12107/0512:24:00 46.8 207.4 30.1 0.3 12107/0512:24:10 46.6 208.0 30.0 0.3 12107/0512:24:20 47.1 208.5 30.1 0.2 1 2107/05 1 2:24:30 46.5 208.9 30.1 0.3 12/07/0512:24:40 46.8 209.3 30.1 0.4 12/07/0512:24:50 46.4 209.5 30.2 0.6 12/07/0512:25:00 46.7 209.7 30.3 0.6 12/07/0512:25:10 46.5 210.0 30.3 0.5 12/07/0512:25:20 46.4 210.4 30.4 0.4 12/07/0512:25:30 45.8 210.5 30.4 0.4 12/0710512:25:40 45.7 210.4 30.7 0.3 12107/0512:25:50 45.9 210.3 30.8 0.3 12/07/0512:26:00 45.8 210.2 31.0 0.3 12/07/0512:26:10 45.6 210.1 30.9 0.3 

# R:5

Page 11217/05 Run tl2

12/07/0512:26:20 46.2 210.4 30.8 0.2 12/07/0512:26:30 45.9 210.6 30.7 0.3 12/07/0512:26:40 46.2 210.5 30.6 0.2 12/07/0512:26:50 45.7 210.8 30.6 0.3 12/0710512:27:00 46.3 210.9 30.6 0.3 12107/0512:27:10 46.5 210.9 30.6 0.4 12i07/0512:27:20 45.3 95.4 29.1 0.2 12107/0512:27:30 46.7 211.2 30.7 0.3 12107/0512:27:40 46.9 211.3 30.7 0.4 12107/0512:27:50 46.3 211.6 30.9 0.4 12/07/0512:28:00 45.8 192.0 29.8 0.0 12107/0512:28:10 46.7 212.1 31.0 0.3 12/07/0512:28:20 47.1 212.0 31.0 0.2 12/0710512:28:30 47.1 212.0 30.8 0.3 1210710512:28:40 47.2 211.8 30.8 0.4 12107/0512:28:50 47.0 212.0 30.7 0.4 1210710512:29:00 46.3 212.0 30.7 0.4 12107/0512:29:10 46.2 212.0 30.7 0.4 12/07/0512:29:20 48.3 212.0 30.8 0.4 12/07/0512:29:30 46.5 211.9 30.9 0.4 12/07/0512:29:40 46.6 211.8 31.0 0.4 12/07/0512:29:50 46.9 211.7 31.2 0.3 12/07/0512:30:00 45.9 211.7 31.2 0.2 12/07/0512:30:10 46.3 211.4 31.4 0.2 12107/0512:30:20 46.6 211.1 31.4 0.2 12/07/0512:30:30 46.9 210.9 31.3 0.2 12/07/0512:30:40 46.4 210.8 31.1 0.2 12107/0512:30:50 46.4 210.9 31.0 0.3 12/07/0512:31:00 46.2 210.9 31.0 0.3 12/0710512:31:10 46.1 210.9 30.9 0.3 12/0710512:31:20 46.0 210.6 30.9 0.3 1210710512:31:30 46.5 210.6 30.9 0.3 12/07/0512:31:40 46.4 210.6 30.9 0.2 1210710512:31:50 46.2 210.6 31.0 0.2 12J0710512:32:00 45.8 210.5 31.1 0.2 12/0710512:32:10 46.0 210.4 31.0 0.2 12/0710512:32:20 45.9 210.5 31.0 0.2 12/07/0512:32:30 45.8 210.4 30.9 0.2 12/07/0512:32:40 45.4 210.3 30.8 0.2 12107/0512:32:50 45.9 210.4 30.7 0.2 12107/0512:33:00 45.8 210.3 30.8 0.3 12/07/0512:33:10 44.7 210.3 30.8 0.4 12107J0512:33:20 44.9 210.1 30.8 0.3 12/07/0512:33:30 45.2 209.9 30.9 0.4 12/07/0512:33:40 44.8 209.8 31.0 0.3 12/07/0512:33:50 44.5 209.7 31.2 0.3 12/07/0512:34:00 45.3 209.5 31.4 0.2 12/0710512:34:10 45.1 209.6 31.4 0.3 12/07/0512:34:20 45.0 209.3 31.4 0.2 12/07/0512:34:30 45.0 209.4 31.4 0.2 12107/0512:34:40 44.3 209.6 31.4 0.2 12/07/0512:34:50 44.5 209.7 31.3 0.2 12107/0512:35:00 43.8 209.5 31.3 0.2 12/07/0512:35:10 44.5 209.7 31.4 0.3 1 2107/05 1 2:35:20 45.3 209.2 31.4 0.2 12107/0512:35:30 44.4 209.0 31.5 0.2 12/07/0512:35:40 44.9 208.5 31.5 0.2 12/07/0512:35:50 45.5 208.1 31.5 0.2 1210710512:36:00 45.8 207.9 31.5 0.2 12/0710512:36:10 45.7 208.2 31.3 0.2 1210710512:36:20 45.9 208.0 31.3 0.2 12/07/0512:36:30 47.0 207.9 31.1 0.1 12/07/0512:36:40 46.9 207.6 31.0 0.2 12/07/0512:36:50 46.6 208.0 30.8 0.1 12/07/0512:37:00 46.9 207.9 30.9 0.1 12/0710512:37:10 46.9 208.4 30.9 0.1 12/07/0512:37:20 46.8 209.2 31.1 0.2 12/07/0512:37:30 46.4 209.6 31.1 0.2 12/07/0512:37:40 46.8 210.0 31.2 0.2 12/0710512:37:50 47.6 210.1 31.3 0.2 12107/0512:38:00 47.4 209.9 31.3 0.2 12/07/0512:38:10 47.4 209.6 31.3 0.2 12/07/0512:38:20 46.7 209.7 31.3 0.2 12/07/0512:38:30 46.4 209.3 31.2 0.2



# ~ Page 2

### 12rIl05 Run #2

12107/0512:38:40 46.5 208.6 31.2 0.2 12107/0512:38:50 47.4 207.7 31.3 0.3 12107/0512:39:00 47.3 206.8 31.4 0.2 12107/0512:39:10 46.5 206.1 31.4 0.3 12107/0512:39:20 46.9 205.3 31.5 0.3 12107/0512:39:30 46.4 204.5 31.5 0.2 12107/0512:39:40 45.8 204.0 31.7 0.1 12l07/0512:39:50 45.6 203.8 31.8 0.2 1210710512:40:00 45.4 204.0 31.9 0.2 12/0710512:40:10 45.4 204.0 31.7 0.2 12J0710512:40:20 44.9 204.7 31.6 0.1 12/0710512:40:30 45.3 204.9 31.5 0.1 12/0710512:40:40 45.3 204.9 31.3 0.1 12/0710512:40:50 45.0 205.5 31.1 0.2 12/0710512:41:00 45.2 206.7 31.1 0.1 12/0710512:41:10 44.9 207.9 30.9 0.2 1210710512:41:20 45.2 209.0 30.8 0.2 12/0710512:41:30 45.3 210.1 30.7 0.2 12/0710512:41:40 44.6 210.9 30.7 0.2 12/0710512:41:50 45.3 211.3 30.7 0.2 1210710512:42:00 45.3 211.6 30.8 0.1 12/0710512:42:10 45.4 211.9 30.8 0.1 12/0710512:42:20 45.3 211.9 31.0 0.2 12107/0512:42:30 45.3 211.5 31.1 0.2 12107/0512:42:40 45.2 211.5 31.1 0.2 12107/0512:42:50 44.4 211.4 31.1 0.1 1210710512:43:00 44.6 211.1 30.9 0.1 12l0710512:43:10 45.1 211.1 30.8 0.1 1210710512:43:20 44.9 211.0 30.7 0.1 1210710512:43:30 45.0 211.1 30.8 0.2 12/0710512:43:40 45.3 211.0 30.8 0.1 12107/0512:43:50 45.4 210.9 30.9 0.1 1210710512:44:00 45.6 210.9 31.0 0.2 12/0710512:44:10 45.1 210.8 31.0 0.1 12/0710512:44:20 45.7 210.8 30.9 0.1 12/0710512:44:30 45.4 210.5 30.9 0.1 1210710512:44:40 44.8 210.5 30.8 0.2 12/0710512:44:60 45.6 210.5 30.8 0.1 1210710512:45:00 46.0 210.2 30.7 0.1 12/0710512:45:10 45.5 209.9 30.7 0.1 12/0710512:45:20 46.3 209.8 30.6 0.1 1210710512:45:30 46.3 209.8 30.6 0.1 12/0710512:45:40 45.6 209.6 30.5 0.1 1210710512:45:50 45.6 209.4 30.6 0.2 1210710512:46:00 46.0 209.5 30.7 0.1 12/0710512:46:10 46.2 209.0 30.8 0.1 12/07/0512:46:20 45.8 208.3 31.0 0.2 1210710512:46:30 46.1 208.4 31.0 0.1 12J0710512:46:40 45.9 208.1 31.0 0.1 12/0710512:46:50 46.6 207.9 31.0 0.1 12/0710512:47:00 46.3 207.8 31.0 0.2 12/0710512:47:10 46.6 207.6 30.9 0.1 12/0710512:47:20 46.6 207.2 30.8 0.1 1210710512:47:30 46.4 206.7 30.8 0.1 12/0710512:47:40 46.3 206.3 30.9 0.1 12107J0512:47:50 46.6 205.6 31.0 0.2 1210710512:48:00 46.4 205.1 31.1 0.2 12/0710512:48:10 46.0 204.3 31.2 0.1 12/07J0512:48:20 46.0 203.6 31.2 0.1 1210710512:48:30 45.6 202.9 31.2 0.1 1210710512:48:40 46.0 202.2 31.2 0.1 12/0710512:48:50 45.6 201.7 31.1 0.1 12/07/0512:49:00 45.7 201.6 31.1 0.1 12l07/05 12:49:10 45.8 201,3 31.0 0.1 1210710512:49:20 45.3 201.5 30.8 0.1 12l0710512:49:30 45.0 201.7 30.8 0.1 12107/0512:49:40 44.9 201.7 30.8 0.2 1 2107105 1 2:49:50 44.7 201.8 30.8 0.1 12107l0512:50:00 45.2 202.0 30.9 0.1 1 2107/05 1 2:50:10 45.3 202.6 30.9 0.1 12107/0512:50:20 45.2 203.4 31.0 0.1 12l07/0512:50:30 45.4 203.8 31.1 0.1 12107/0512:50:40 45.4 204.1 31.0 0.1 12107/0512:50:50 44.9 204.7 31.0 0.0 

# R{

Page 312R/05 Run #2

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# o • 

# •
PBge 41217105 Run #2

12/07/0513:03:20 44.9 210.1 30.7 0.1 12/07/0513:03:30 44.7 210.0 30.7 0.1 12/07/05 13:03:40 44.7 209.6 30.8 01

- 12/07/0513:03:50 44.9 209.4 30.8 0.1 12107/0513:04:00 44.6 209.5 30.8 0.1 12107/0513:04:10 45.0 209.6 30.9 0.1 12/0710513:04:20 45.8 209.5 30.8 0.1 12/07/0513:04:30 45.3 209.4 30.8 0.2 1210710513:04:40 45.5 209.4 30.6 0.2 12/07/0513:04:50 45.5 210.0 30.6 0.1 1210710513:05:00 45.5 210.6 30.5 0.1 12l0710513:05:10 44.9 210.9 30.5 0.1 1210710513:05:20 45.0 211.4 30.5 0.1 1210710513:05:30 45.8 211.8 30,6 0.1 12107/0513:05:40 45.5 212.6 30.7 0.1 12107l0513:05:50 45.8 213.4 30.8 0.1 12107/0513:06:00 46.2 214.1 30.9 0.1 12107/0513:06:10 45.7 214.4 30.9 0.1 12107/0513:06:20 45.9 214.5 31.0 0.1 12/07/0513:06:30 45.8 214.6 31.0 0.1 12/07/0513:06:40 46.5 214.7 30.9 0.1 1210710513:06:50 46.5 214.6 30.8 0.1 12/07/0513:07:00 46.7 214.5 30.7 0.1 12107/0513:07:10 46.8 214.6 30.7 0.1 12/07l0513:07:20 46.5 214.7 30.7 0.1 12/07J0513:07:30 46.5 214.1 30.7 0.0 12/07/0513:07:40 46.7 214.2 30.7 0.0 12107/0513:07:50 46.8 213.9 30.7 -0.1 12/07/0513:08:00 46.6 213.5 30.8 0.0 12107/0513:08:10 46.2 213.3 30.8 0.0 12/07/0513:08:20 46.2 213.1 30.9 0.0 12107/0513:08:30 46.7 213.1 31.0 0.1 12/0710513:08:40 46.5 213.2 31.0 0.1 1210710513:08:50 46.8 213.1 31.0 0.1 12/0710513:09:00 46.9 212.7 31.0 0.1 12/0710513:09:10 46.6 212.6 30.9 0.1 1210710513:09:20 45.7 212.8 30.8 0.1 12/0710513:09:30 45.5 213.0 30.7 0.1 12/0710513:09:40 45.9 212.5 30.7 0.1 1210710513:09:50 45.9 212.2 30.7 0.2 12107/0513:10:00 46.3 212.3 30.6 0.1 12107/0513:10:10 45.8 212.6 30.7 0.1 12/07/0513:10:20 45.7 212.7 30.8 0.1 1210710513:10:30 45.3 212.4 30.9 0.1 12/07l0513:10:40 45.5 211.9 31.0 0.1 1210710513:10:50 45.3 211.2 31.2 0.1 1 2107/05 1 3:11:00 45.7 210.6 31.3 0.1 1210710513:11:10 45.5 210.1 31.4 0.1 1 2107/05 1 3:11:20 45.8 209.4 31.5 0.1 12/0710513:11:30 45.0 208.0 31.4 0.1 12J0710513:11:40 45.4 206.7 31.3 0.1 1210710513:11:50 44.9 177.1 30.6 -1.2 12107/0513:12:00 42.6 161.8 29.8 -1.2 12/07/0513:12:10 43.8 183.8 30.3 -0.2 12107/0513:12:20 44.7 203.2 30.9 0.1 1210710513:12:30 44.5 202.8 30.9 0.1 1210710513:12:40 43.8 201.8 30.9 0.1 12/07/0513:12:50 44.2 200.9 30.9 0.0 12/0710513:13:00 43.7 200.3 31.1 0.0 12/0710513:13:10 43.8 199.9 31.3 0.0 12/0710513:13:20 44.4 199.7 31.3 0.0 1210710513:13:30 44.8 199.4 31.3 0.1 12/0710513:13:40 44.6 199.3 31.1 0.1 1 2/07105 1 3:13:50 44.9 199.3 31.0 0.0 12107l0513:14:00 44.8 199.2 31.0 0.0 12107/0513:14:10 43.8 199.4 31.0 0.1 12107/0513:14:20 44.0 198.4 30.7 -0.2 1210710513:14:30 44.2 200.9 30.9 0.3 1210710513:14:40 44.9 200.7 30.8 0.3 12/0710513:14:50 45.0 201.4 30.9 0.3 12/0710513:15:00 44.3 201.4 31.1 0.4 12/0710513:15:10 44.6 201.6 31.3 0.4 1 2107105 1 3:15:20 45.0 201.6 31.5 0.4 12I0710513:15:30 44.9 199.6 31,4 0.0 

# 89
Page 512/7105 Run #2

12/07/0513:15:40 44.8 199.7 31.4 0.0 12/0710513:15:50 44.1 200.1 31.3 0.0 1210710513:16:00 45.3 200.5 31.1 0.0 12/07/0513:16:10 44.9 201.0 31.0 0.0 12107/0513:16:20 45.4 201.4 30.8 0.1 12/07/0513:16:30 45.1 201.3 30.9 0.1 12/07/0513:16:40 44.7 201.4 30.8 0.1 12/07/0513:16:50 44.7 201.3 30.7 0.1 12/07/0513:17:00 45.1 201.0 30.8 0.0 12/0710513:17:10 44.8 200.7 30.9 0.0 12107/0813:17:20 44.3 200.8 31.0 0.0 1210710513:17:30 44.9 200.9 31.0 -0.1 12/07/0513:17:40 44.5 201.2 31.0 -0.1 1210710513:17:50 44.6 201.8 30.9 0.0 12/07/0513:18:00 44.8 202.0 30.6 -0.1 12/07/0513:18:10 45.0 202.7 30.6 -0.1 12107/0513:18:20 44.2 203.1 30.6 0.0 12107/0513:18:30 44.6 203.5 30.5 0.1 12/07/0513:18:40 45.1 203.7 30.6 0.1 12/07/0513:18:50 44.6 203.9 30.6 0.1 12107/0513:19:00 45.0 203.8 30.8 0.1 12/0710513:19:10 45.1 203.6 30.8 0.1 12/07/0513:19:20 45.6 203.7 30.9 0.1 12107/0513:19:30 44.8 204.0 31.1 0.1 12107/0513:19:40 45.8 204.3 31.1 0.1 12/07/0513:19:60 45.5 205.0 31.0 0.1 12107/0513:20:00 45.6 205.2 31.0 0.0 12107/0513:20:10 45.5 205.4 30.9 0.0 12107/0513:20:20 45.4 205.4 30.8 0.0 12107/0513:20:30 45.5 204.9 30.7 0.0 12107/0513:20:40 46.1 205.2 30.7 0.0 1210710513:20:50 46.1 205.3 30.7 0.0 12107/0513:21:00 45.7 206.0 30.7 0.0 12107/0513:21:10 45.5 206.9 30.8 0.0 1 2107105 1 3:21:20 45.5 207.2 31.0 0.0 1210710513:21:30 46.2 207.4 31.2 0.1 1210710513:21:40 48.0 207.6 31.3 0.1 1210710513:21:50 45.8 207.9 31.2 0.1 1210710513:22:00 46.0 208.3 31.1 0.1 12/0710513:22:10 45.8 207.9 31.1 0.0 12/07/0513:22:20 46.4 207.8 31.0 0.1 12/07/0513:22:30 45.7 207.7 30.9 0.1 12/07/0513:22:40 45.4 208.3 30.7 0.1 12/07/0513:22:50 45.4 208.6 30.6 0.0 12/07/0513:23:00 45.0 208.6 30.5 0.0 12/07/0513:23:10 45.5 208.5 30.6 0.1 12107/0513:23:20 44.5 208.3 30.6 0.1 12107/0513:23:30 44.8 208.6 30.6 0.0 12/07/0513:23:40 44.5 208.6 30.7 0.1 1210710513:23:50 44.5 208.5 30.8 0.0 12107/0513:24:00 45.0 208.2 31.2 0.0 12107/0513:24:10 45.0 207.9 31.3 0.0 12107/0513:24:20 44.5 207.8 31.4 0.0 12/07/0613:24:30 44.7 207.2 31.4 0.1 12/07/0613:24:40 44.8 206.9 31.3 0.1 12/07/0513:24:50 43.0 206.8 31.1 0.1 12/07/0513:25:00 43.5 207.1 31.0 0.1 12/07/0513:25:10 43.8 207.1 30.8 0.1 12107/0513:25:20 44.9 207.3 30.7 0.0 12107/0513:25:30 44.3 207.9 30.7 0.0 12/07/0513:25:40 44.0 208.7 30.6 0.0 12/0710513:25:50 45.1 209.0 30.6 0.0 12/0710513:26:00 44.5 208.8 30.6 0.0 12/07/0513:26:10 44.3 208.8 30.8 0.0 12/07/0513:26:20 44.0 208.7 31.0 0.0 12/0710513:26:30 44.7 208.6 31.3 0.0 12/0710513:26:40 45.2 208.5 31.2 -0.1 12107/0513:26:50 44.5 208.1 31.4 -0.1

StOp Run #2 45.7 206.7 30.6 0.1

12/0710513:27:00 45.3 208.1 31.4 0.0 12/0710513:27:10 46.0 207.7 31.5 -0.1 12/0710513:27:20 46.4 207.7 31.5 -0.1



# s. LWA IW 

### J
Page 612R/05 Run #2

12J07/0513:27:30 46.0 207.7 31.4 0.1 12107/0513:27:40 45.6 207.9 31.3 0.1 12/07/0513:27:50 45.1 208.4 31.2 0.1 12/07/0513:28:00 44.8 207.9 31.0 0.0 12/0710513:28:10 45.3 207.6 30.9 0.0 12/07/0513:28:20 45.3 207.8 30.8 0.0 12/07/0513:28:30 30.7 164.7 30.3 0.0 12/07/0513:28:40 2.1 203.0 29.7 0.0 12/0710513:28:50 1.7 188.1 29.2 0.0 12/0710513:29:00 1.3 133.9 24.7 0.1 12/0710513:29:10 1.1 83.7 17.6 0.1 12/07/0513:29:20 1.0 49.7 14.2 0.0 12/0710513:29:30 0.9 29.6 16.7 -0.3 1 2/07105 1 3:29:40 0.6 19.0 19.6 -0.4 1210710513:29:50 0.7 12.7 21.7 -0.4 12/0710513:30:00 0.7 8.7 22.9 -0.5 12/07/0513:30:10 0.6 6.8 23.4 -0.3 12/07/0513:30:20 0.6 5.5 23.6 -0.1 12/07/0513:30:30 0.6 4.8 

## 23.6 -0.1
1210710513:30:40 0.6 4.0 

### 23.7 

## -0.1 12/07/0513:30:50 0.5 3.1 

## 23.6 0.0 12/07/0513:31:00 0.5 2.3 

## 23.6 -0.1 12107/0513:31:10 0.4 2.0 23.4 -0.2 12/07/0513:31:20 1.3 1.6 23.2 -0.2 12/07/0513:31:30 1.5 1.3 22.9 -0.2 1 2107/05 1 3:31:40 1.4 1.5 21.3 -0.1 12107/0513:31:50 1.5 1.9 16.2 -0.1 12/07/0513:32:00 1.0 1.7 11.2 -0.1 12/07/0513:32:10 0.3 1.1 7.9 -0.1 12/07/0513:32:20 0.2 0.7 6.2 -0.1 12/0710513:32:30 0.3 0.2 5.0 0.1 12/07/0513:32:40 0.3 -0.1 4.4 1.4 12/07/0513:32:50 0.3 -0.2 4.0 4.6 12J0710513:33:00 0.3 -0.3 3.8 9.9 1 2/07105 1 3:33:10 0.3 -0.4 3.7 17.1 12/0710513:33:20 0.3 -0.6 3.5 25.1 12/07/0513:33:30 0.3 -0.5 3.4 32.6 12107/0513:33:40 0.3 -0.6 3.3 40.3 12/07/0513:33:50 0.3 -0.7 3.2 47.2 12/0710513:34:00 0.3 -0.5 3.1 52.7 1210710513:34:10 0.3 -0.6 3.0 57.4 12/0710513:34:20 0.2 -0.5 2.9 61.3 12/07/0513:34:30 0.2 -0.6 2.8 64.7 12107/0513:34:40 0.2 -0.8 2.7 67.6 12/07/0513:34:50 0.2 -0.7 2.6 70.0 12/07/0513:35:00 0.2 -0.5 2.4 72.0 12/07/0513:35:10 0.2 -0.4 2.4 73.8 12/07l0513:35:20 0.2 -0.3 2.3 75.5 12/0710513:35:30 0.3 -0.1 2.1 77.0 12/07/0513:35:40 0.2 -0.1 2.0 78.1

; 2107/05 13:35:50 0.2 -0.2 1.9 79.3 12/0710513:36:00 0.2 -0.2 1.9 80.4 12107/0513:36:10 0.3 -0.2 1.7 81.2 12107/0513:36:20 0.3 -0.1 1.7 81.8 12/07/0513:36:30 0.3 -0.2 1.7 82.3 12/07/0513:36:40 0.2 -0.2 1.6 82.9 12/07/0513:36:50 0.2 -0.3 1.5 83.6 1210710513:37:00 0.2 -0.4 1.5 84.1 12107/0513:37:10 0.2 -0.5 1.5 85.6 12/07/0513:37:20 0.2 -0.4 1.4 86.8 12107/0513:37:30 0.2 -0.5 1.4 87.4 12/07/0513:37:40 0.2 -0.5 1.3 87.8 12/07/0513:37:60 0.2 -0.4 1.3 88.1 12/0710513:38:00 0.2 -0.3 1.2 89.9 12/0710513:38:10 0.2 -0.3 1.2 90.9 12/07/0513:38:20 0.3 -0.4 1.2 91.1 12/07/0513:38:30 0.2 -0.4 1.1 91.4 12107/0513:38:40 0.3 -0.3 1.1 91.8 12/07/0513:38:50 0.3 -0.3 1.1 92.4 12/0710513:39:00 0.3 -0.2 1.0 92.8 12/07/0513:39:10 0.3 -0.3 0.9 92.9 12107/0513:39:20 0.3 -0.4 0.9 93.1 12/07/0513:39:30 0.3 -0.3 1.0 93.2 25.5 ppm NOx Zero S02



# 91
Page 71217/05 Run #2

12/0710513:39:40 0.3 -0.4 0.9 93.5 12107/0513:39:50 0.3 -0.5 0.8 93.8 1210710513:40:00 0.3 -0.4 0.9 93.9 1210710513:40:10 0.3 -0.4 0.8 93.8 1210710513:40:20 0.3 -0.3 0.8 94.6 12/07/0513:40:30 0.3 -0.5 0.8 95.1 12107/0513:40:40 0.2 -0.5 0.7 95.5 1210710513:40:50 0.2 -0.4 0.7 95.7 12107/0513:41:00 0.2 -0.5 0.7 95.9 12/07/0513:41:10 0.2 

### -0.5 0.7 

### 96.2 12/07/05 13:41:20 0.2 

### -0.3 0.7 

### 96.4 101 ppm S02 12107105 13:41:30 0.2 

### -0.2 0.7 

### 96.6 Zero CO
12J07l0513:41:40 0.3 

### -0.2 0.6 

### 96.6 12/07l0513:41:50 0.9 -0.1 0.7 95.7 12107/0513:42:00 

### 0.4 -0.2 0.6 95.2 12/0710513:42:10 0.4 0.9 0.6 95.2 12107/0513:42:20 0.3 38.4 0.6 93.1 1210710513:42:30 0.3 94.7 0.6 86.9 12107J0513:42:40 0.3 126.1 0.6 78.2 1210710513:42:50 0.3 143.2 0.5 69.0 1210710513:43:00 0.3 154.9 0.6 60.6 12/07l0513:43:10 0.3 160.3 0.5 52.7 12/0710513:43:20 0.3 163.3 0.5 45.3 1210710513:43:30 0.3 164.6 0.5 39.0 12/07/0513:43:40 0.4 165.4 0.5 33.7 12/0710513:43:50 0.4 166.4 0.5 29.4 12/0710513:44:00 0.4 167.1 0.5 25.9 12107/0513:44:10 0.3 168.1 0.5 

### 22.7 12107/0513:44:20 0.3 169.8 0.5 20.0 1210710513:44:30 0.3 171.9 0.5 17.9 12J0710513:44:40 0.3 173.5 0.5 16.0 1210710513:44:50 0.2 174.3 0.5 14.5 1210710513:45:00 0.2 174.7 0.4 13.0 1 2107105 1 3:45:10 0.3 174.9 0.5 11.8 1210710513:45:20 0.3 175.3 0.4 10.7 1 2107105 1 3:45:30 0.3 174.5 0.5 9.5 1210710513:45:40 0.3 177.3 0.4 8.7 1210710513:45:50 

### 0.3 178.4 0.4 8.0 12/07105 13:46:00 

### 0.3 179.8 0.4 7.4 200 ppm CO 12/07105 13:46:10 

### 0.3 178.6 0.4 6.8 Zero VOC, NOx 1210710513:46:20 

### 0.3 178.3 0.4 6.4 12/0710513:46:30 0.3 178.1 0.4 5.9 12/07/0513:46:40 0.2 177.9 0.4 5.4 12/07/0513:46:50 0.2 176.9 0.4 4.9 12/07l0513:47:00 1.2 175.1 0.4 4.5 12/0710513:47:10 41.0 176.2 0.4 

### 4.2 1210710513:47:20 45.8 167.3 0.4 4.0 12J0710513:47:30 47.1 127.1 0.5 3.9 1210710513:47:40 

### 47.2 68.4 0.5 3.7 12107105 13:47:50 

### 47.3 35.0 0.4 3.6 48.8 ppm C3H8 12J0710513:48:00 

### 47.3 20.7 0.4 3.6 1210710513:48:10 

### 47.2 11.9 0.4 3.4 12/0710513:48:20 47.2 6.3 0.4 3.2 12/0710513:48:30 32.3 3.4 0.4 3.0.



# wo
Page 812l7/05 Run #3

Date/Time VOC CO NOx S02 

### mm/ddtyy hh:mm:ss ppm ppm ppm ppm 12J07/0514:04:50 49.2 207.4 27.6 0.7



### Start Run 43 1210710514:05:00 49.4 207.5 27.6 0.6 12/0710514:05:10 49.4 207.7 27.8 0.6 12l07/0514:05:20 48.9 208.6 27.9 0.7 12/07/0514:05:30 49.0 209.9 26.0 0.6 1210710514:05:40 48.8 210.5 26.1 0.5 1210710514:05:60 49.5 210.6 28.4 0.5 1210710514:06:00 49.2 210.4 28.6 0.5 12107/0514:06:10 49.5 210.4 28.8 0.5 1210710514:06:20 49.9 210.4 26.9 0.6 12107/0514:06:30 49.4 210.3 28.9 0.5 12107/0514:06:40 48.9 210.6 29.0 0.5 1210710514:06:50 49.2 211.0 29.0 0.4 12107l0514:07:00 48.4 211.1 29.0 0.4 1210710514:07:10 49.0 211.0 28.8 0.6 12/0710514:07:20 48.6 211.0 28.7 0.5 1210710514:07:30 48.9 211.0 28.8 0.5 1210710514:07:40 48.3 211.0 28.8 0.5 12/0710514:07:50 49.0 211.3 29.0 0.5 12/07/0514:08:00 48.8 211.2 29.1 0.6 12/07/0514:08:10 48.9 211.0 29.2 0.5 12/07/0514:08:20 48.0 210.9 29.5 0.6 12107/0514:08:30 47.5 210.8 29.7 0.5 1 2107/05 1 4:08:40 46.9 210.8 29.9 0.6 12107/0514:08:50 46.9 211.0 30.1 0.5 12107/0514:09:00 46.7 210.8 30.2 0.5 12107/0514:09:10 46.5 210.8 30.3 0.4 12107/0514:09:20 46.5 211.0 30.4 0.4 12107/0514:09:30 47.1 211.2 30.3 0.4 1210710514:09:40 47.3 211.2 30.1 0.4 12107/0514:09:50 46.7 211.7 29.9 0.5 12107/0514:10:00 46.0 212.4 29.8 0.5 12107/0514:10:10 47.0 213.1 29.7 0.5 1210710514:10:20 46.8 213.5 29.7 0.5 12107/0514:10:30 46.2 213.9 29.7 0.5 1210710514:10:40 46.8 214.5 29.6 0.5 12107/0514:10:50 46.6 215.1 29.7 0.5 12J07l0514:11:00 47.1 215.2 29.8 0.5 1210710514:11:10 46.1 214.6 29.8 0.4 12107/0514:11:20 46.7 213.4 30.0 0.4 1210710514:11:30 46.1 212.6 30.4 0.4 1 2107105 1 4:11:40 46.3 212.1 30.5 0.4 12/07/0514:11:50 46.3 211.8 30.7 0.4 12/07/0514:12:00 47.0 211.7 30.8 0.3 12J07/0514:12:10 47.0 211.6 30.7 0.4 12J07/0514:12:20 47.4 211.8 30.5 0.4 12107/0514:12:30 47.4 211.9 30.2 0.4 12/07/0614:12:40 47.0 212.5 30.2 0.5 12/07/0514:12:50 46.9 213.3 30.1 0.5 12/0710514:13:00 46.7 212.6 30.0 0.6 1210710514:13:10 47.5 211.9 29.9 0.5 12J0710514:13:20 46.9 211.6 29.9 0.4 12107/0514:13:30 47.0 211.4 30.0 0.4 12107/0514:13:40 46.6 211.6 30.2 0.4 12107/0514:13:50 46.8 211.4 30.3 0.4 12107/0514:14:00 46.6 211.5 30.4 0.5 1 2107/05 1 4:14:10 46.2 211.5 30.6 0.4 12107/0514:14:20 45.8 211.9 30.8 0.5 12/07/0514:14:30 45.6 212.1 31.0 0.4 12107/0514:14:40 46.0 212.5 31.0 0.4 12107/0514:14:50 46.4 212.7 31.0 0.4 12/07/0514:15:00 45.8 213.4 30.9 0.3 12/0710514:15:10 45.6 213.6 30.8 0.4 12/07/0514:15:20 45.8 213.2 30.7 0.5 12/07/0514:15:30 46.1 213.9 30.5 0.4 12/07/0514:15:40 46.7 214.5 30.3 0.5 12/07/0514:15:50 45.4 216.8 30.2 0.6 12/07/0514:16:00 45.0 217.1 30.2 0.7 12/07/0514:16:10 45.0 217.6 30.2 0.5 12/0710514:16:20 46.2 218.3 30.1 0.4



### Page 1 

# 4 ~

.1217/05 Run tt3

12107/0514:16:30 45.2 219.2 30.2 0.4 1 2107106 1 4:16:40 45.2 220.2 30.4 0.5 1210710514:16:50 45.8 220.6 30.7 0.5 1210710514:17:00 45.8 220.8 30.8 0.3 1210710514:17:10 45.2 221.2 30.8 0.4 1210710514:17:20 46.2 222.2 30.9 0.4 12107/0514:17:30 46.0 222.7 30.9 0.4 12107/0514:17:40 46.1 223.1 30.9 0.4 1210710514:17:50 46.1 222.3 30.9 0.4 12107/0514:18:00 46.4 221.4 30.7 0.4 12107/0514:18:10 46.6 221.3 30.5 0.4 12/07/0514:18:20 46.6 221.4 30.3 0.4 1210710514:18:30 46.0 221.4 30.1 0.5 12/0710514:18:40 46.0 221.5 30.0 0.5 12J0710514:18:50 47.1 221.0 29.9 0.5 1210710514:19:00 46.2 220.8 29.8 0.5 12107/0514:19:10 46.3 ' 220.7 29.8 0.5 12107/0514:19:20 47.1 220.9 29.9 0.5 12f07/0514:19:30 46.1 221.6 30.0 0.4 1210710514:19:40 46.5 221.8 30.1 0.4 12107/0514:19:50 47.0 221.9 30.3 0.4 12107/0514:20:00 47.4 222.4 30.4 0.5 12107/0514:20:10 47.4 222.7 30.6 0.5 12107/0514:20:20 47.6 222.9 30.6 0.4. 12/07/0514:20:30 47.2 223.0 30.5 0.6 1210710514:20:40 47.3 223.5 30.4 0.6 12107/0514:20:50 48.0 223.9 30.2 0.5 12/0710514:21:00 47.9 223.9 30.1 0.5 12/0710514:21:10 47.4 224.0 29.9 0.5 1210710514:21:20 47.3 224.5 29.8 0.5 12107/0514:21:30 47.6 225.4 29.8 0.4 12107/0514:21:40 47.2 225.8 29.8 0.3 12107/0514:21:50 47.5 225.0 29.8 0.4 12/07/0514:22:00 47.1 224.4 29.8 0.4 12/0710514:22:10 46.2 224.2 30.0 0.4 12/0710514:22:20 46.9 224.2 30.1 0.5 12/07/0514:22:30 46.8 224.2 30.3 0.6 12/0710514:22:40 46.4 224.0 30.3 0.5 12107l0514:22:50 46.8 223.7 30.4 0.5 12107l0514:23:00 46.6 223.1 30.5 0.5 12107/0514:23:10 46.6 222.5 30.3 0.5 12107/0614:23:20 45.8 222.0 30.3 0.4 12107/0514:23:30 46.0 221.6 30.2 0.4 12/07/0514:23:40 45.6 220.0 30.0 0.4 12107/0514:23:50 45.7 218.9 30.0 0.5 12/07/0514:24:00 44.3 218.2 29.9 0.6 12107/0514:24:10 45.2 ' 217.6 29.8 0.5 12/0710614:24:20 44.8 216.9 29.8 0.5 12/0710514:24:30 44.1 215.8 29.8 0.5 12107/0514:24:40 44.4 215.2 29.9 0.4 12107/0514:24:50 43.9 214.6 30.2 0.3 12/07/0514:25:00 43.6 213.7 30.4 0.4 1 2107/05 1 4:25:10 44.7 213.2 30.6 0.4 1210710514:25:20 44.1 212.9 30.8 0.3 12/07/0514:25:30 44.1 212.2 30.8 0.4 12107/0514:25:40 44.5 211.2 30.8 0.5 12J07/0514:25:50 44.9 210.8 30.6 0.5 12107/0514:26:00 44.9 210.7 30.4 0.5 1 2107105 1 4:26:10 44.5 210.7 30.2 0.5 12107105 14:26:20 45.1 210.8 30.0 0.4 12J0710514:26:30 45.9 211.0 30.0 0.5 1210710514:26:40 45.4 211.2 29.9 0.6 12J0710514:26:50 46.0 211.4 30.0 0.5 12/0710514:27:00 45.7 211.7 30.0 0.5 12107/0514:27:10 46.2 211.7 30.1 0.6 12/07/0514:27:20 45.4 211.8 30.2 0.7 12/07/0514:27:30 45.7 211.2 30.3 0.6 12/0710514:27:40 46.3 211.1 30.4 0.6 12/0710514:27:50 45.8 210.9 30.6 0.5 12/07/0514:28:00 45.9 210.4 30.7 0.5 1 2107/05 1 4:28:10 47.5 210.2 30.7 0.5 1210710614:28:20 46.4 210.0 30.7 0.5 1210710514:28:30 45.6 210.2 30.5 0.4 1210710514:28:40 46.0 210.0 30.6 0.4



### Page 2 

# q~1217/05 Run #3

12/07/0514:28:50 46.0 209.7 30.3 0.4 12/0710514:29:00 45.9 209.4 30.2 0.5 12/07/0514:29:10 46.5 209.1 30.0 0.5 12/0710514:29:20 46.8 208.8 30.0 0.6 12107/0514:29:30 45.4 209.1 30.0 0.6 12/07/0514:29:40 45.2 209.6 30.0 0.6 12/07/0514:29:50 45.8 210.1 30.0 0.5 12107/0514:30:00 46.6 210.5 30.1 0.4 12/0710514:30:10 46.5 210.8 30.2 0.6 12107/0514:30:20 46.7 210.9 30.5 0.6 12107/0514:30:30 45.6 210.7 30.5 0.6 12107J0514:30:40 45.8 210.6 30.6 0.5 1210710514:30:50 46.1 210.9 30.7 0.5 12/07J0514:31:00 46.6 211.2 30.8 0.5 1210710514:31:10 45.7 211.2 30.7 0.6 1210710514:31:20 46.2 211.1 30.5 0.6 12/0710514:31:30 45.5 211.4 30.3 .0.6 12/0710514:31:40 45.0 211.2 30.2 0.6 12107/0514:31:50 45.8 210.9 30.1 0.7 1210710514:32:00 45.6 210.6 30.0 0.8 12/07/0514:32:10 45.5 210.6 29.9 0.7 12l07/0514:32:20 45.4 210.4 29.9 0.7 12/07/0514:32:30 45.5 210.4 29.9 0.7 12107/0514:32:40 45.0 210.6 29.9 0.8 12/0710614:32:60 44.9 210.7 29.9 0.7 12107/0514:33:00 45.3 210.8 30.1 0.7 1210710514:33:10 45.5 210.9 30.3 0.6 12107/0514:33:20 45.4 210.5 30.5 0.5 12/0710514:33:30 45.8 210.4 30.5 0.6 12/0710514:33:40 45.8 210.3 30.5 0.7 12/0710514:33:50 47.0 210.1 30.4 0.7 12107/0514:34:00 46.2 209.6 30.3 0.7 12/07/0514:34:10 46.0 209.5 30.1 0.6 12/07/0514:34:20 46.0 209.1 30.0 0.6 12/0710514:34:30 46.8 208.8 30.0 0.7 12/07/0614:34:40 46.8 208.7 29.8 0.7 12/07/0514:34:50 46.3 208.7 29.8 0.6 12/07/0514:35:00 46.4 208.3 29.8 0.6 12107/0514:35:10 46.3 208.0 29.9 0.6 12/07/0514:35:20 46.0 207.3 30.0 0.7 12107/0514:35:30 46.1 206.4 30.2 0.6 12/07/0514:35:40 46.6 205.6 30.3 0.6 1210710514:35:50 46.3 205.1 30.5 0.5 12107/0514:36:00 44.9 204.8 30.6 0.5 12/07/0514:36:10 46.1 204.5 30.7 0.6 12/0710514:36:20 46.2 204.6 30.7 0.6 12107/0514:36:30 46.0 205.1 30.5 0.6 12107/0514:36:40 46.2 205.6 30.4 0.6 1210710514:36:50 45.5 205.8 30.3 0.6 12/07/0514:37:00 45.4 206.1 30.2 0.6 12J07/0514:37:10 46.1 206.1 30.0 0.6 12/07/0514:37:20 45.1 206.1 30.0 0.7 12/07/0514:37:30 46.2 205.7 29.9 0.6 12/07/0514:37:40 45.9 205.8 29.9 0.6 12107/0514:37:50 45.6 206.4 29.9 0.6 12/07/0614:38:00 45.7 207.1 30.0 0.5 12/07/0514:38:10 45.3 207.5 30.0 0.5 12107/0514:38:20 45.4 207.8 30.1 0.5 12!07/0514:38:30 45.2 208.5 30.2 0.6 12/07/05 14:38:40 44.4 208.9 30.3 0.6 12107J0514:38:50 44.2 209.3 30.6 0.6 12/0710514:39:00 44.1 209.3 30.6 0.6 1210710514:39:10 44.7 208.9 30.7 0.6 12/0710514:39:20 44.0 208.7 30.6 0.6 12/0710514:39:30 44.6 208.3 30.4 0.7 12/07/0514:39:40 45.8 207.9 30.3 0.7 12/07/0514:39:50 46.2 207.5 30.1 0.7 12/07/0514:40:00 46.2 207.1 30.0 0.6 12107/0514:40:10 46.1 207.4 29.9 0.7 12107/0514:40:20 46.1 207.8 29.9 0.8 12107/0514:40:30 46.5 208.0 29.9 0.8 12/07/0514:40:40 46.5 207.9 29.9 0.8 12/0710514:40:50 45.9 208.0 29.9 0.8 12107/0514:41:00 47.8 208.4 30.0 0.7

e 

# q 5 Page 312/7/05 Run #3

12107/0514:41:10 47.6 208.5 30.1 0.7 12107/0514:41:20 48.7 208.6 30.3 0.7 12/07/0614:41:30 47.8 209.0 30.4 0.6 12/0710514:41:40 48.5 209.8 30.6 0.6 12/0710514:41:50 47.9 210.4 30.6 0.7 12107/0514:42:00 46.9 210.9 30.5 0.7 12107/0514:42:10 47.8 211.2 30.3 0.7 12107/0514:42:20 46.4 211.5 30.2 0.8 12/07/0514:42:30 46.3 211.4 30.2 0.8 12107/0514:42:40 47.7 211.4 30.1 0.7 12J0710514:42:50 47.0 2113 30.1 0.7 1210710514:43:00 46.8 211.4 30.1 0.6 12/07/0514:43:10 46.4 211.6 30.0 0.7 12107/0514:43:20 46.3 211.9 30.0 0.8 1210710514:43:30 46.0 211.9 30.1 0.7 1210710514:43:40 45.9 211.7 30.3 0.7 12/0710514:43:50 47.0 211.7 30.4 0.6 12/0710514:44:00 47.4 211.7 30.5 0.6 12/07/0514:44:10 47.0 211.6 30.6 0.7 12/07/0514:44:20 46.0 211.8 30.7 0.7 12107/0514:44:30 45.6 211.9 30.6 0.8 12/07/0514:44:40 45.0 120.7 30.3 0.3 1210710514:44:50 43.8 118.0 29.5 -1.3 1210710514:45:00 43.3 66.0 29.5 -0.8 12107/0514:45:10 45.2 210.6 30.0 0.9 12107/0514:45:20 44.8 210.9 29.8 0.8 12/07/0514:45:30 44.8 211.0 29.8 0.7 12107/0514:45:40 45.1 210.9 29.7 0.7 12107/0514:45:50 44.5 210.9 29.7 0.8 12107/0514:46:00 44.2 211.0 29.7 0.8 1210710514:46:10 44.5 211.1 29.7 0.7 12/07/0514:46:20 44.5 211.4 29.7 0.7 12/07/0514:46:30 44.3 211.7 29.8 0.7 12107/0514:46:40 44.7 212.0 30.0 0.7 12107/0514:46:50 44.6 212.3. 30.2 0.8 12107/0514:47:00 44.0 212.3 30.4 0.8 1210710514:47:10 44.1 212.2 30.5 0.8 1210710514:47:20 44.5 212.2 30.6 0.7 12/0710514:47:30 44.1 211.8 30.4 0.8 1210710514:47:40 44.1 211.9 30.3 0.8 12/07/0514:47:50 44.6 211.8 30.1 0.9 12107/0514:48:00 44.0 211.9 29.9 0.8 12/0710514:48:10 44.7 212.0 29.9 0.7 12/07/0514:48:20 44.5 211.8 29.8 0.8 12/07/0514:48:30 45.4 212.1 29.8 0.9 12/07/0514:48:40 45.2 212.2 29.8 0.8 12107/0514:48:50 45.1 212.7 29.8 0.8 12107/0514:49:00 45.4 212.9 30.0 1.0 12/07/0514:49:10 45.5 213.1 30.2 0.8 12/07/0514:49:20 45.8 212.9 30.3 0.8 12/0710514:49:30 46.4 213.1 30.5 0.8 12/07/0514:49:40 45.8 212.8 30.7 0.8 12/07/0514:49:50 45.8 212.5 30.7 0.8 12/07/0514:50:00 46.1 211.8 30.9 0.8 12/07/0514:50:10 46.2 211.5 30.9 0.8 12107J0514:50:20 46.6 211.3 30.7 0.8 12/07/0514:50:30 47.0 211.0 30.5 0.8 1210710514:50:40 46.3 210.6 30.2 0.8 12107/0514:50:50 48.0 210.0 30.0 0.8 12/07/0514:51:00 47.3 209.7 29.8 0.9 12/0710514:51:10 47.2 209.3 29.7 0.9 12/07/0514:51:20 47.7 208.9 29.6 0.9 12/07/0514:51:30 47.9 208.8 29.6 0.9 12107/0514:51:40 47.0 209.0 29.7 0.9 12107/0514:51:50 47.1 209.3 29.7 0.8 12107/0514:52:00 47.3 210.2 29.7 0.8 12107/0514:52:10 47.4 210.6 30.0 1.0 1210710514:52:20 46.9 210.7 30.2 1.0 1210710514:52:30 46.8 210.9 30.3 0.9 12/07/0514:52:40 46.9 210.6 30.3 1.0 12/07/0514:52:50 47.0 210.4 30.2 0.9 12107/0514:53:00 47.0 210.6 30.1 0.9 12107/0514:53:10 47.3 210.8 30.0 0.9 12/07/0514:53:20 46.4 211.0 29.9 1.0



## raim f 

### Page 412/7/05 Run #3

12/0710514:53:30 46.6 211.2 29.9 0.9 12/0710514:53:40 46.0 211.3 29.9 0.8 12107/0514:53:50 47.0 211.2 29.9 0.8 12/0710514:54:00 46.7 211.1 29.8 0.9 12/07/0514:54:10 46.2 211.2 29.8 0.9 12107/0514:54:20 46.2 211.1 29.8 0.9 12107/0514:54:30 46.0 211.1 29.9 1.0 12107/0514:54:40 46.1 211.3 30.0 1.0 12/07/0514:54:50 45.7 211.1 30.3 1.1 12107/0514:55:00 46.2 211.1 30.5 1.1 12/07/0514:55:10 45.4 211.2 30.6 1.1 1210710514:55:20 45.2 211.3 30.8 1.1 1210710514:55:30 45.3 211.7 30.7 1,0 12107/0514:55:40 45.1 211.9 30.6 1,0 1210710514:55:50 45.6 212.2 30.4 0.8 12/0710514:56:00 45.3 212.2 30.3 0.9 12/0710514:56:10 44.7 213.0 30.2 0.9 1210710514:56:20 45.0 213.1 30.1 0.9 12/07/0514:56:30 45.2 213.0 29.9 0.9 12107/0514:56:40 45.3 212.7 29.9 1.0 12/07/0514:56:50 44.8 212.2 29.8 1.0 12107/0514:57:00 45.3 212.0 29.7 1.1 12/07/0514:57:10 45.7 212.0 29.8 1.0 1210710514:57:20 45.2 212.0 29.8 0.9 12/07/0514:57:30 45.0 211.9 29.9 1.0 1210710514:57:40 46.2 211.7 30.0 0.9 12107/0514:57:50 45.1 211.8 30.2 0.9 12107/0514:58:00 45.5 212.4 30.4 1.0 12/07/0514:58:10 45.6 212.7 30.5 1.0 12/07/0514:58:20 45.3 213.0 30.5 0.9 12/07/0514:58:30 45.9 213.6 30.6 0.9 12107/0514:58:40 45.9 213.7 30.6 1.0 12/07/0514:58:50 45.6 213.6 30.4 1.1 12/07/0514:59:00 45.8 213.4 30.2 1.1 12107/0514:59:10 46.0 213.9 30.0 1.1 12107/0514:59:20 45.5 214.5 29.9 1.1 1210710514:59:30 45.9 214.7 29.8 1.1 1210710514:59:40 45.6 214.8 29.8 1.1 12/0710514:59:50 46.0 214.9 29.8 1.1 1210710515:00:00 45.7 215.2 29.8 1.0 12/07/0515:00:10 46.2 215.3 29.8 0.9 12107/0515:00:20 45.9 215.5 29.9 0.9 12107/0515:00:30 45.2 215.8 30.0 1.0 12/07/0515:00:40 46.9 215.8 30.2 1.1 12/07/0515:00:50 45.8 215.3 30.3 1.0 12/07/0515:01:00 45.1 216.0 30.5 1.1 12107/0515:01:10 46.0 214.6 30.7 1.1 12J07/0515:01:20 45.5 214.2 30.8 1.0 1210710515:01:30 45.1 213.4 30.8 1.0 12/0710515:01:40 45.7 213.6 30.7 1.0 12/0710515:01:50 45.2 213.3 30.6 1.0 12107/0515:02:00 45.1 213.7 30.3 1.0 12107/0515:02:10 45.0 213.8 30.1 1.0 12107/0515:02:20 45.4 214.2 30.1 1.0 12/07/0515:02:30 45.1 214.2 30.0 1.0 12107/0515:02:40 45.4 214.0 29.9 1.0 12/07/0515:02:50 45.5 213.5 29.8 0.9 12/07/0515:03:00 45.2 213.1 29.8 1.0 12107/0515:03:10 45.2 212.8 29.9 1.0 12J0710515:03:20 45.7 212.8 30.0 1.1 1210710515:03:30 45.5 213.1 30.1 1.1 1210710515:03:40 45.1 212.8 30.3 1.2 12107/0515:03:50 45.2 212.8 30.4 1.3 12107/0515:04:00 46.4 212.8 30.5 1.3 1 2/07105 1 5:04:10 46.5 212.4 30.6 1.3 12/0710515:04:20 46.0 212.4 30.7 1.2 12/07/0515:04:30 46.7 212.6 30.7 1.1 12J07/0515:04:40 46.4 212.7 30.6 1.1 12107/0515:04:50 46.2 212.9 30.4 1.1 12/07/0615:05:00 46.7 213.7 30.2 1.1 12/07/0515:05:10 46.5 213.8 30.1 1.1 12107/0515:05:20 46.3 213.4 30.0 1.2 1210710515:05:30 46.0 213.0 30.0 1.2 12/0710515:05:40 47.0 213.1 29.9 1.1



# n N~ Page 51217/05 Run #3

12107/0515:05:50 47.0 212.8 29:8 1.1 1210710515:06:00 47.1 212.6 29.8 1.1 1210710515:06:10 46.7 213.1 29.8 1.1 12107/0515:06:20 47.0 213.7 29.8 1.0 12/07/0515:06:30 46.0 214.7 29.8 1.1 1210710515:06:40 44.5 215.6 30.0 1.2 12/0710515:06:50 45.7 216.4 30.0 1.2 12/07/0515:07:00 45.5 216.5 30.2 1.1 12107/0515:07:10 45.9 

### 217.4 30.2 1.0 12/07/0515:07:20 46.7 217.8 30.4 1.1 12/0710515:07:30 45.5 217.9 30.5 1.1 12107/0515:07:40 45.1 218.0 30.5 1.2 12107/0515:07:50 45.7 218.1 30.3 1.2 12/07/0515:08:00 45.7 218.6 30.2 1.3 12/07/0515:08:10 45.7 219.0 30.0 1.4 12/07/0515:08:20 45.5 219.0 29.9 1.3 12/07/0515:08:30 46.3 218.5 29.8 1.1 12107/0515:08:40 

### 46.4 218.6 29.7 1.1 12/07/0515;08:50 45.9 218.7 29.7 1.1 12/07/0515:09:00 46.0 219.0 29.7 1.0 12/07/0515:09:10 46.8 218.7 29.7 1.1 12/07/0515:09:20 

### 46.7 218.6 29.7 1.3 12/07/0515:09:30 45.7 219.1 29.8 1.3 12107/0515:09:40 45.0 219.4 29.9 1.2 12/07/0515:09:50 45.0 218.4 30.0 1.3 12/07/0515:10:00 45.5 217.8 30.1 1.2 12/07/0515:10:10 45.7 

### 217.4 30.3 1.2 120710515:10:20 45.7 217.2 30.4 1.1 12/07/0515:10:30 

### 46.4 217.0 30.5 1.2 12/07/0515:10:40 45.9 

### 217.2 30.5 1.2 12107/0515:10:50 46.0 217.3 30.4 1.2
Stop Run #3 46.13 212.20 30.11 0.71

12/0710515:11:00 45.9 217.0 30.2 1.3 12107/0515:11:10 46.5 216.8 30.0 1.2 12/07/0515:11:20 46.0 216.5 29.9 1.2 12107/0515:11:30 46.3 216.7 29.8 1.3 1210710515:11:40 46.1 217.0 29.8 1.2 1210710515:11:60 46.6 216.9 29.7 1.3 1210710515:12:00 46.7 216.9 29.6 1.3 12/0710515:12:10 46.0 216.6 29.7 1.2 12107/0515:12:20 35.7 163.5 29.6 1.3 12/07/0515:12:30 4.0 210.6 28.9 1.3 12/0710515:12:40 1.5 200.4 28.6 1.3 1210710515:12:50 1.5 148.6 24.8 1.2 12107/0515:13:00 1.5 96.1 17.9 1.1 12107/0515:13:10 1.5 60.4 12.9 1.0 12107/0515:13:20 1.4 38.0 9.7 0.9 12J07/0515:13:30 1.3 24.6 7.9 0.7 12107/0515:13:40 0.7 17.7 6.8 0.7 12107/0515:13:50 0.7 14.7 6.3 0.6 12/07/0515:14:00 0.6 12.5 9.2 0.5 12107/0515:14:10 0.6 9.8 

### 14.4 0.7 12l07/0515:14:20 0.6 7.3 18.3 0.6 12/07/0515:14:30 0.6 6.2 20.8 0.8 12107/0515:14:40 0.6 5.9 22.0 0.8 12107/0515:14:50 0.6 5.8 22.6 0.7 12107/0515:15:00 0.5 5.7 22.9 0.6 12107/0515:15:10 0.4 5.5 23.0 0.6 12107/0515:15:20 0.4 5.4 23.0 0.6 12/0710515:15:30 0.4 4.9 23.0 0.5 12107/0515:15:40 0.4 4.7 

## 23.0 0.6 12107/0515:15:50 0.3 4.4 

## 23.1 0.6 12/07/0515:16:00 0.4 4.1 

## 23.0 0.6 1007/0515:16:10 

### 0.4 3.9 

## 23.0 0.5 12/07/0515:16:20 0.3 3.7 22.9 0.7 12107/0515:16:30 1.2 3.8 22.6 0.6 12107/0515:16:40 1.4 3.7 22.6 0.5 12107/0515:16:50 1.4 4.6 21.5 0.5 12107/0515:17:00 1.4 5.5 18.8 0.5 12107/05 15:17:10 0.7 6.2 10.8 0.6 12/0710515:17:20 0.2 6.6 7.4 0.6 25.5 ppm NOx Zero S02



# m

l

Page 612/7105 Run #3

12107/0515:17:30 0.2 5.4 5.5 0.6 12J0710515:17:40 0.2 4.1 4.6 0.7 12/07/0515:17:50 0.2 3.1 3.9 1.9 12/07/0515:18:00 0.2 2.6 3.6 4.5 12/07/0515:18:10 0.2 2.2 3.4 8.9 12/0710515:18:20 0.2 2.3 3.4 14.9 12/07/0515:18:30 0.3 2.1 3.3 22.0 12/0710515:18:40 0.3 2.0 3.2 291 12/0710515:18:50 0.3 1.7 3.2 36.1 12107/0515:19:00 0.2 1.7 3.0 43.0 12107/0515:19:10 0.2 1.7 3.0 49.1 12107/0515:19:20 0.2 1.8 2.9 54.6 12/0710515:19:30 0.2 1.6 2.7 59.4 12/07/0515:19:40 0.2 1.6 2.6 63.6 12/07/0515:19:50 0.2 1.7 2.6 67.2 12/07/0515:20:00 0.2 1.7 2.5 70.4 12107/0515:20:10 0.2 1.8 2.4 73.3 12/07/0515:20:20 0.2 1.6 2.3 75.8 1 2107/05 1 5:20:30 0.1 1.7 2.2 77.9 12/07/0515:20:40 0.2 1.8 2.1 79.9 12107/0515:20:50 0.1 1.7 2.0 81.6 12/07/0515:21:00 0.1 2.0 2.0 83.3 12/0710515:21:10 0.1 2.1 1.9 84.7 12/0710515:21:20 0.1 2.0 1.8 86.8 12/07/0515:21:30 0.2 1.8 1.8 86.9 12/07/0515:21:40 0.2 1.8 1.7 87.8 12/07/0515:21:50 0.2 1.6 1.6 88.7 12107/0515:22:00 0.1 1.8 1.6 89.4 12107/0515:22:10 0.2 1.5 1.6 90.2 12/07/0515:22:20 0.1 1.5 1.5 90.9 12/07/0515:22:30 0.1 1.6 1.5 91.5 12/07/0515:22:40 0.1 1.5 1.4 91.9 12107/0515:22:50 0.2 1.6 1.4 92.4 1210710515:23:00 0.2 1.4 1.4 92.7 1 2/07105 1 5:23:10 0.2 1.4 1.3 92.9 12/07/0515:23:20 0.2 1.5 1.3 93.1 12/07/0515:23:30 0.2 1.8 1.2 93.5 12/07/0515:23:40 0.2 1.9 1.2 93.7 12/07/0515:23:50 0.2 1.7 1.1 93.9 1210710515:24:00 0.2 1.8 1.1 94.0 1210710515:24:10 0.2 1.8 1.0 94.3 1210710515:24:20 0.2 1.7 1.0 94.7 12/0710515:24:30 0.1 1.7 1.0 95.1 1 2107/05 1 5:24:40 0.2 1.9 1.0 95.3 12/07/0515:24:50 0.2 2.2 1.0 95.6 12/0710515:25:00 0.2 2.1 0.9 95.9 12/0710515:25:10 0.2 2.1 0.9 96.3 12/0710615:25:20 0.2 2.0 0.9 96.5 12/07/0515:25:30 0.2 2.1 0.8 96.6 12/07/05 15:25:40 0.1 2.1 0.8 96.7 101 ppm S02 12/07/05 15:25:50 0.2 2.0 0.8 

### 96 .8 Zero CO 12/0710515:26:00 0.2 1.8 0.8 96.9 1210710515:26:10 0.6 1.5 0.8 95.9 12/0710515:26:20 0.2 1.3 0.7 96.0 12/07/0515:26:30 0.3 11.3 0.8 96.4 12/07/0515:26:40 0.3 64.2 0.7 93.9 12/0710515:26:50 0.2 110.3 0.7 87.6 12107/0515:27:00 0.3 137.8 0.7 79.5 12/07/0515:27:10 0.3 154.7 0.6 71.1 12/07/0515:27:20 0.3 164.1 0.7 62.9 12/0710515:27:30 0.2 170.4 0.6 55.6 12/0710515:27:40 0.2 174.2 0.6 49.1 12/07/0515:27:50 0.2 176.0 0.6 43.5 12/07/0515:28:00 0.2 177.3 0.6 38.6 12/0710515:28:10 0.2 178.3 0.6 34.4 12/07/0515:28:20 0.2 178.7 0.5 30.6 12107/0515:28:30 0.2 179.0 0.5 27.4 1210710515:28:40 0.2 179.3 0.5 24.5 12/07/0515:28:50 0.2 179.7 0.6 22.1 1210710515:29:00 0.2 179.9 0.5 19.9 1210710515:29:10 0.2 180.0 0.5 18.1 12107/0515:29:20 0.2 180.1 0.5 16.3 12/07/05 15:29:30 0.2 180.3 0.6 15.0 200 ppm CO



# a ~ 

# '
Page 71217105 Run #3

12107105 15:29:40 

### 0.2 180.5 0.6 13.8 Zero VOC, NOx 1210710515:29:50 

### 0.2 180.5 0.5 12.6 1?10710615:30:00 0.2 179.7 0.5 11.6 12107/0515:30:10 4.0 178.9 0.5 10.7 1210710515:30:20 45.8 179.6 0.6 9.9 1210710515:30:30 

### 47.9 164.2 0.6 9.3 12/07/0515:30:40 

### 47.8 118.0 0.6 8.7 48.8 ppm C3H8 12/07/0515:30:50 

### 47.8 69.4 0.6 8.1 12107/0515:31:00 

### 47.7 39.8 0.5 7.7 12/0710515:31:10 47.7 24.1 0.6 7.3 1210710515:31:20 46.5 15.6 0.5 6.8 12I07105 15:31:30 13.1 10.5 0.5 6.3 12/07105 9 5:31:40 1.5 7.5 0.5 6.1

Page 8 

# t 

# o o

# Zero Gas 0 0.5 0.833333

Upscale 24.8 24 -1.33333
Average NOx Concentration: 26.86 Corrected NOx 

# Concentration: 29.59163 (Equation 6C-1)

Zero Gas 0 0.28 0.466667 Upscaie 24.8 22.4 -4
Average NOx Concentration: 26.87 Corrected NOx Concentration: 30.92281 (Equation 6C-1) Run #2

Ru n #3 0.28 0.466667 -0.36667 0.39 22.4 -4 -2.66667 23.2

0.2 0.333333 -0.13333 0.24 22 -4.66667 -0.66667 22.2 Sheet1

Summary of NOx Analyzer Calibrations and Bias



# Plant: Daltile, Muskogee Source: 

# Trim Kiln Date: 

# 12/8/05

Analyzer Calibratrion Data


# Cyiinder Analyzer Absolute % Span Value Response Difference Zero Gas 0 0 0 0 Mid Range 25.5 24.8 -0.7 -1.16667 High Range 51 50.88 -0.12 -0.2

Run #1 System Calibration Bias and Drift Data



# Analyzer Initial Values Final Values Drift Calibration System System System System Response Calibration Calibration Calibration Calibration

Response Bias Response Bias

Zero Gas 0 0.4 0.666667 0.5 0.833333 0.166667 Upscale 24.8 22.55 -3.75 24 -1.33333 2.416667
Average NOx Concentration: 27.56 Corrected NOx Concentration: 30.28719 (Equation 6C-1) Average Calibration Values

0.45 23.275

Page 1 1 . ;J 

# 1

# Sheet1

Summary of CO Analyzer Calibrations and Bias

Plant: Daltile, Muskogee Source: Kiln Scrubber Exhaust Date: 12/7105

Analyzer Calibratrion Data
Cylinder Analyzer Absolute % Span Value Response Difference Zero Gas 0 1.7 1.7 0.34 Mid Range 200 203.1 3.1 0.62 High Range 494 492.65 -1.35 -0.27

System Calibration Bias and Drift Data

Analyzer Initial Values Final Values Drift Average Calibration System System System System Calibration Response Calibration Calibration Calibration Calibration Values

Response Bias Response Bias

Run #1 Zero Gas 1.7 0.98 -0.144 0.28 -0.284 -0.14 0.63

Upscale 203.1 190.1 -2.6 184.68 -3.684 -1.084 187.39
Average CO Concentration: 155.21 Corrected CO Concentration: 165.5387 (Equation 6C-1)

Run #2 Zero Gas 1.7 0.28 -0.284 0.28 -0.284 0 0.28

Upscale 203.1 184.68 -3.684 184.68 -3.684 0 184.68
Average CO Concentration: 155.21 Corrected CO Concentration: 168.0369 (Equation 6C-1)

Run #3 Zero Gas 1.7 0.28 -0.284 -1.22 -0.584 -0.3 -0.47

Upscale 203.1 184.68 -3.684 182.08 -4.204 -0.52 183.38
Average CO Concentration: 157.05 Corrected CO Concentration: 171.3571 (Equation 6C-1)

Page 1 1. 

# ~ ~

# Sheet1

Summary of Suifur Dioxide 

# ^ , riaiyzer Caiibrations and 

## Bias

Plant: 

# Daltile, Muskogee Source: Trim Kiln Date: 

# 12/8/05

Analyzer Calibratrion Data


# Cylinder Analyzer Absolute 

# % Span Value Response Difference Zero Gas 0 -0.08 -0.08 -0.07273 Mid Range 50.1 50 -0.1 -0.09091 High Range 101 102.8 1.8 1.636364

System Calibration Bias 

# and Drift Data

Anaiyzer Initial Values Final Values Drift Average Calibration System System System System Calibration Response Calibration Calibration Calibration Calibration Values

Response Bias Response Bias

Run #1 Zero Gas -0.08 -0.13 -0.04545 0.28 0.327273 0.372727 0.075

Upscale 102.8 99.65 -2.86364 98.48 -3.92727 -1.06364 99.065
Average S02 Concentration: 83.63 Corrected S02 Concentration: 85.25159 (Equation 6C-1 

# )

Run #2 Zero Gas -0.08 0.28 0.327273 0.2 0.254545 -0.07273 0.24

Upscale 102.8 98.48 -3.92727 98.6 -3.81818 0.109091 98.54
Average S02 Concentration: 69.78 Corrected S02 Concentration: 71.45005 (Equation 6C-1 

# )

Run #3 Zero Gas -0.08 0.2 0.254545 -0.4 -0.29091 -0.54545 -0.1

Upscale 102.8 98.6 -3.81818 98.33 -4.06364 -0.24545 98.465
Average S02 Concentration: 75.17 Corrected S02 Concentration: 77.12951 (Equation 6C-1 

# )

Pa9 e1 

# 1.0312/8J05 Calibrations

OatelTime VOC CO NOx S02 mm/dd/yy hh:mm:ss ppm ppm ppm ppm 12/08/05 09:23:04 1.8 8.2 0.0 5.8 12/08/05 09:23:14 1.7 8.2 0.0 5.8 12/08/05 09:23:24 1.9 8.1 0.0 5.8 12/08/08 09:23:34 1.9 8.2 0.0 5.8 12/08105 09:23:44 2.6 3.7 0.0 6.0 12108105 09:23:54 2.9 2.5 0.0 5.9 12/08J05 09:24:04 2.2 2.6 0.0 5.9 12/08105 09:24:14 2.3 2.4 0.0 5.8 12/08105 09:24:24 2.4 2.5 0.0 5.8 12/08105 09:24:34 2.5 2.4 0.0 5.8 12108105 09:24:44 3.4 2.0 42.5 5.9 12108105 09:24:54 3.2 2.1 51.9 5.9 12/06105 09:25:04 2.7 2.2 52.1 6.8 12108J05 09:25:14 3.1 2.2 52.2 5.9 12/08/05 09:25:24 2.8 2.2 52.2 5.9 12/08/05 09:25:34 2.7 2.2 51.4 5.8 12108/05 09:25:44 2.7 2.2 50.4 4.9 12108J05 09:25:54 2.7 2.2 47.5 0.8 12l08105 09:26:04 3.2 

## 1.3 50.8 5.6
12108105 09:26:14 2.5 

## 1.9 50.9 5.6 12108/05 09:26:24 2.5 

## 1.8 50.9 5.6 12/08/05 09:26:34 2.6 

## 1.8 50.9 5.5 12/08/05 09:26:44 2.7 1.8 50.9 5.5 12108/05 09:26:64 2.2 2.1 28.3 5.4 12/08/05 09:27:04 1.8 2.4 0.3 5.4 12/08/05 09:27:14 2.4 2.3 0.1 5.4 12/08/05 09:27:24 1.9 2.2 0.1 5.5 12/08/05 09:27:34 1.1 2.1 0.1 5.5 12/08105 09:27:44 0.8 2.3 0.0 5.6 12J08l05 09:27:54 0.9 2.0 0.1 5.5 12108/05 09:28:04 1.1 1.9 0.1 5.5 12/08/06 09:28:14 1.1 1.8 0.0 5.7 12108/05 09:28:24 1.0 1.6 0.1 5.6 12108/05 09:28:34 0.9 1.8 0.1 5.5 12/08/05 09:28:44 1.0 1.6 0.1 5.5 12/08/05 09:28:54 1.2 1.7 0.1 5.5 12/08/05 09:29:04 1.5 1.5 0.0 5.5 12108/05 09:29:14 1.5 1.6 0.0 5.5 12108105 09:29:24 2.0 1.5 0.0 5.5 12108105 09:29:34 2.0 1.5 0.0 5.6 12/08l05 09:29:44 2.6 2.0 0.0 5.7 12J08/05 09:29:54 2.3 2.0 2.9 5.6 12/08/05 09:30:04 2.8 1.6 24.2 5.7 12/08105 09:30:14 2.3 1.7 24.6 5.7 12/08/05 09:30:24 2.1 1.8 24.6 5.6 12/08/05 09:30:34 2.2 1.9 24.7 5.6 12/08105 09:30:44 2.4 2.0 

## 24.8 5.7 12/08/05 09:30:54 1.9 2.1 

## 24.8 5.8 12l08105 09:31:04 1.9 2.3 

## 24.8 5.8 12/08/05 09:31:14 2.9 2.3 

## 24.8 5.8 12108/05 09:31:24 2.0 2.2 24.8 4.1 12/08/05 09:31:34 2.4 2.3 24.8 -0.1 12/08105 09:31:44 1.8 2.2 11.5 -0.3 12/08J05 09:31:54 1.7 2.3 0.2 -0.2 12108105 09:32:04 1.4 2.3 0.0 -0.2 12108105 09:32:14 1.3 2.4 0.0 -0.3 12/08105 09:32:24 1.0 2.4 0.0 -0.3 12108l05 09:32:34 1.0 2.4 0.0 -0.2 12/08/05 09:32:44 1.4 2.6 0.1 -0.1 12/08/05 09:32:54 1.2 2.6 0.0 -0.1 12108l05 09:33:04 1.3 2.7 0.1 -0.1 12108J05 09:33:14 2.2 2.6 0.1 -0.1 1 210 810 5 0 9:33:24 2.1 2.6 0.1 -0.1 12108J05 09:33:34 2.0 10.2 0.0 -0.1 12108/05 09:33:44 1.9 164.1 0.0 0.0 12/08/05 09:33:54 2.2 202.1 0.0 0.0 12/08/05 09:34:04 2.0 202.6 0.0 -0.1 12108/05 09:34:14 2.1 202.6 0.0 -0.1 12/08/05 09:34:24 3.2 202.9 0.0 -0.1 12/08/05 09:34:34 2.1 

### 202.8 

## 0.0 -0.1 51 ppm NOx Zero CO

25.5 ppm NOx



# 1.04

Page 1

### 1218105 Calibrations

12/08/05 09:34:44 2.0 

### 203.3 0.0 -0.1 200 ppm CO 12108/05 09:34:54 2.1 

### 203.2 0.0 -0.1 Zero S02 12108/05 09:35:04 2.0 

### 203.1 0.0 0.0 12108/05 09:35:14 2.2 114.9 0.0 0.0 12108/05 09:35:24 2.2 4.4 0.0 -0.1 12/08/05 09:35:34 2.2 2.7 0.0 -0.1 12/08/05 09:35:44 2.5 2.5 0.1 -0.1 12l08/05 09:35:54 1.9 2.3 0.1 -0.1 12108/05 09:36:04 1.4 2.1 0.0 0.0 12108/05 09:36:14 1.3 1.9 0.1 0.0 12108/05 09:36:24 1.0 1.6 0.0 -0.1 12/08105 09:36:34 11 1.8 0.0 -0.1 12/08/05 09:36:44 1.5 1.9 0.1 -0,1 12/08/05 09:36:54 1.7 1.8 0.1 -0.1 12/08/05 09:37:04 1.7 3.8 0.1 -0.1 12/08/05 09:37:14 2.8 332.8 0.1 -0.1 12/08/05 09:37:24 2.7 491.1 0.0 -0.1 12/08105 09:37:34 2.7 492.3 0.0 0.0 12/08/05 09:37:44 2.3 

### 492.4 0.0 -0.2 12/08/05 09:37:54 2.7 

### 492.6 0.0 -0.2 494 ppm CO 12/08/05 09:38:04 2.8 

### 492.8 0.0 -0.2 12/08/05 09:38:14 2.5 

### 492.8 0.0 -0.2 12/08/05 09:38:24 2.2 492.2 0.0 -0.3 12/08/05 09:38:34 2.3 166.3 0.0 -0.2 12/08105 09:38:44 2.0 3.4 0.0 -0.3 12108/05 09:38:54 2.2 2.2 0.0 -0.2 12/08/05 09:39:04 1.8 2.1 0.0 -0.3 12/08/05 09:39:14 1.3 2.1 0.0 -0.3 12/08/05 09:39:24 0.9 1.8 0.0 -0.2 12/08105 09:39:34 0.8 1.8 0.0 -0.2 12/08105 09:39:44 1.1 1.9 0.1 0.0 12/08/05 09:39:54 1.4 2.1 0.1 0.2 12/08/05 09:40:04 1.4 2.3 0.0 24.3 12/08/05 09:40:14 1.7 2.4 0.0 79.6 12/08/05 09:40:24 1.9 2.5 0.0 106.8 12/08/05 09:40:34 1.7 2.5 0.0 115.3 12/08/05 09:40:44 2.0 2.3 0.0 117.5 12/08/05 09:40:54 2.1 2.3 0.0 118.3 12/08105 09:41:04 2.3 2.5 0.0 118.4 12/08/05 09:41:14 2.2 2.4 0.0 118.6 12108/05 09:41:24 2.4 2.4 0.0 118.9 12/08/05 09:41:34 2.0 2.6 0.0 118.9 12/08/05 09:41:44 2.4 3.1 0.0 119.1 12/08/05 09:41:54 2.3 3.1 0.0 119.2 12/08/05 09:42:04 1.8 3.2 0.0 111.1 12108105 09:42:14 2.2 3.1 0.0 103.1 12108/05 09:42:24 1.8 3.1 0.0 103.2 12/08105 09:42:34 2.0 3.2 0.1 101.3 12/08/05 09:42:44 1.7 2.9 0.0 

### 102.2 12108/05 09:42:54 1.7 3.1 0.0 

### 102.1 101 ppm S02 12/08/05 09:43:04 1.5 3.2 0.0 

### 102.0 12/08/05 09:43:14 1.5 2.9 0.0 

### 102.0 12/08/05 09:43:24 1.4 2.9 0.0 101.9 12/08l05 09:43:34 1.6 3.0 0.0 98.2 12/08105 09:43:44 1.5 3.0 0.0 56.1 12/08105 09:43:54 1.6 3.2 0.0 19.9 12/08/06 09:44:04 1.8 3.0 0.0 5.9 12/08/06 09:44:14 1.1 2.7 0.0 2.0 12/08/05 09:44:24 1.1 2.7 0.0 0.8 12/08/05 09:44:34 1.8 2.4 0.0 0.4 12/08105 09:44:44 1.8 2.3 0.0 0.2 12/08/05 09:44:54 1.2 2.3 0.0 0.6 12/08/05 09:45:04 1.1 1.9 0.1 43.8 12/08105 09:45:14 1.2 1.9 0.2 43.4 12108/05 09:45:24 1.9 2.1 0.2 48.2 12/08/05 09:45:34 1.6 2.0 0.3 49.8 12/06105 09:45:44 1.8 1.9 0.2 50.0 12/08l05 09:45:54 1.7 2.0 0.3 50.0 12/08105 09:46:04 1.7 2.0 0.2 50.0 12/08/05 09:46:14 1.9 2.0 0.3 50.0 12/08/05 09:46:24 1.8 2.1 0.2 50.0 50.1 ppm S02 12108/05 09:46:34 2.0 2.1 0.2 50.0

Page 2 

# 1.05

### 12/8105 Calibrations

12l08/05 09:46:44 1.7 2.1 0.2 50.0 12J08105 09:46:54 1.8 2.0 0.2 50.0 12/08/05 09:47:04 1.8 2,4 0.1 49,0 12108105 09:47:14 1.5 2,3 0.1 47.0 12108105 08:47:24 1.6 2.0 0.1 20.8 12J08/05 09:47:34 1.6 1.9 0.1 6.9 12108/05 09:47:44 1.8 1,5 0.1 2.8 12108/05 09:47:54 1.8 1.5 0.1 1.4 12I08/05 09:48:04 1.9 1.6 0.0 1.0 12108l05 09:48:14 1.9 1.5 0.0 0.8



# 1,06 Page 312/8/05 Bias Calibrations

DatelTime VOC CO NOx S02 

### mmlddlyy hh:mm:ss ppm ppm ppm ppm 12108/0510:15:04 2.0 1.4 2.6 0.0 12/08/0510:15:14 2.3 1.6 1.8 0.1 12108/0510:15:24 1.7 1.9 1.4 0.1 1 2108/05 1 0:15:34 0.9 2.1 1.1 0.1 1210810510:15:44 0.7 2.0 0.8 0.3 12108/05 10:15:54 0.7 1.7 1.4 0.3 1210810510:16:04 0.7 1.3 7.3 0.2 12J0810510:16:14 0.7 1.0 14.0 0.1 12108105 1 0:16:24 0.7 0.9 17.5 0.0 12/08/0510:16:34 0.6 0.9 18.8 0.0 12108/0510:16:44 0.8 1.0 20.2 0.1 12/08/0510:16:54 0.8 1.0 21.1 0.1 12108/0510:17:04 1.0 1.0 21.7 0.0 12108/0510:1714 0.8 1.1 22.0 0.0 12/08/0510:17:24 0.8 1.0 22.2 •0.1 12/08/0510:17:34 0.6 1.0 22.3 -0.1 12108/0510:17:44 0.8 1.1 22.4 -0.1 12/08/0510:17:54 0.9 0.9 22.4 0.0 12/08/0510:18:04 0.9 1.0 22.4 0.0 12108/0510:18:14 0.9 

## 1.0 22.5 -0.1
12108/0510:18:24 0.8 

## 1.1 22.5 -0.1
1 2108/05 1 0:18:34 0.9 

## 1.1 22.6 -0.1
1210810510:18:44 0.8 

### 0.7 

## 22.6 -0.2 12/08/0510:18:54 0.8 0.8 22.6 -0.2 12108/0510:19:04 0.8 0.8 21.7 -0.2 12/08/0510:19:14 1.5 0.8 21.1 -0.3 12108/0510:19:24 1.8 0.9 21.0 -0.3 12108/0510:19:34 2.4 0.9 20.7 -0.2 12/0810510;19:44 2.3 1.5 19.4 0.0 12/0810510:19:54 1.4 2.1 17.8 0.0 1 2108/05 1 0:20:04 0.5 2.5 12.6 0.0 1 2108/05 1 0:20:14 0.1 2.1 6.0 1.9 12108/0510:20:24 0.1 1.9 2.7 23.3 12/08/0510:20:34 0.2 1.9 1.6 61.8 12/0810510:20:44 0.3 0.9 1.3 71.1 12/08/0510:20:54 0.4 1.0 0.9 82.2 1 2108/05 1 0:21:04 0.4 1.0 0.7 86.5 12/08/0510:21:14 0.4 1.0 0.6 92.5 12/08/0510:21:24 0.3 0.9 0.5 94.9 1 2/08105 1 0:21:34 0.3 0.9 0.5 96.9 12108/0510:21:44 0.3 0.9 0.4 97.4 12/08/0510:21:54 0.3 0.9 0.4 98.3 12/08/0510:22:04 0.2 0.7 0.4 99.5 12/08/0510:22:14 0.1 0.8 0.4 99.7 12/08/0510:22:24 0.1 1.0 

## 0.4 99.1
12/08/0510:22:34 0.1 0.8 

## 0.4 99.9
12/08/0510:22:44 0.1 0.8 

## 0.4 99.8
12/08/0510:22:54 0.2 0.9 

## 0.4 99.8 12/08/0510:23:04 0.3 1.1 0.4 99.5 12108/0610:23:14 0.0 1.1 0.4 97.2 12/08/0510:23:24 0.3 1.3 0.4 94.5 12/08/0510:23:34 1.1 1.2 0.4 89.4 12/08/0510:23:44 1.0 1.5 0.4 88.5 12/0810510:23:54 0.8 1.8 0.4 87.5 12108/0510:24:04 0.7 11.5 0.5 78.6 12/08/0510:24:14 0.5 72.8 0.4 50.5 12/08/0510:24:24 0.7 116.4 0.3 35.5 12l08/0510:24:34 0.6 136.5 0.2 22.8 12108/0510:24:44 0.8 148.4 0.2 18.5 12/08/0510:24:54 0.9 157.1 0.2 9.2 12108/0510:25:04 0.7 162.2 0.2 9.9 12108/0510:25:14 0.7 165.4 0.2 8.6 12/08/0510:25:24 0.7 167.6 0.1 8.9 12/08/0510:25:34 0.8 168.5 0.1 5.6 12/08/0510:25:44 0.7 169.2 0.1 4.9 12108/0510:25:54 0.7 170.2 0.1 4.8 12/08/0510:26:04 0.8 171.1 0.1 4.2 12108/0510:26:14 0.9 171.3 0.1 4.4 12/08/0510:26:24 0.5 172.3 0.1 4.5 12/0810510:26:34 0.4 174.3 0.1 6.6 12/08/0510:26:44 0.5 176.6 0.1 5.9 25.5 ppm NOx Bias Zero CO. S02 Bias

101 ppm S02 Bias Zero NOx Bias

Page 1 

# 1.() 

# Y12/8/05 Blas Calibrations

12/08/0510:26:54 0.3 178.8 0.1 5.4 12108/0510:27:04 0.5 180.5 0.1 4.8 12108/0510:27:14 0.8 182.7 0.1 4.2 12/08/0510:27:24 0.2 185.6 0.1 3.7 12/0810510:27:34 0.3 187.3 0.1 3.4 12108/0510:27:44 0.6 188.6 0.1 3.0 12108/0510:27:54 0.4 189.4 0.1 2.7 12108/0510:28:04 0.4 189.9 0.1 2.5 12108/0510:28:14 

### 0.3 189.8 0.0 2.3 12/08/05 10:28:24 

### 0.1 190.1 0.1 2.0 200 ppm CO Bias 12108105 10:28:34 

### 0.1 190.3 0.0 1.9 Zero VOC 1210810510:28:44 

### 0.2 190.2 0.0 1.7 12108/0510:28:54 0.2 187.7 0.0 1.5 1210810510:29:04 0.1 186.2 0.0 1.4 1210810510:29:14 0.5 185.5 0.1 1.4 12108/0510:29:24 1.1 182.9 0.1 1.4 1210810510:29:34 1.1 170.7 0.1 1.4 12108/0510:29:44 1.5 146.4 0.1 1.5 1210810510:29:54 34.2 115.1 0.1 1.8 12/08/0510:30:04 82.2 71.1 0.1 2.2 12/08/0510:30:14 87.6 41.1 0.2 2.7 12108/0510:30:24 88.8 23.9 0.2 3.1 12108/0510:30:34 90.1 16:1 0.1 3.0 12/08/0510:30:44 90.0 11.7 0.1 2.8 12/08/0510:30:54 90.1 9.2 0.1 2.3 12108/05 10:31:04 89.4 7.1 0.1 2.1 12108/0510:31:14 

### 88.8 5.6 0.1 1.8 12/08/05 10:31:24 

### 88.9 4.6 0.1 1.6 89.2 ppm C3hl8 12/08/0510:31:34 

### 88.7 3.8 0.1 1.2 12/08/0510:31:44 

### 88.4 3.0 0.0 0.9 12108/0510:31:54 88.5 2.4 0.0 0.9 12108/0510:32:04 88.1 2.3 0.0 0.9 12108/0510:32:14 86.6 2.0 0.1 0.7 12108/0510:32:24 77.8 1.5 0.0 0.6 1210810510:32:34 55.3 1.5 0.1 0.5 12/0810510:32:44 33.7 1.3 0.1 0.4 12/0810510:32:54 2.8 1.4 0.0 0.4 1210810610:33:04 7.7 1.5 0.1 0.4 1210810610:33:14 44.7 1.6 0.1 0.4 12/0810510:33:24 46.8 1.7 0.1 0.4 1210810510:33:34 47.7 1.9 0.1 0.5 12/0810510:33:44 

### 47.6 1.6 0.1 0.5 12/08/05 10:33:54 

### 47.7 1.5 0.1 0.5 48.8 ppm C31-18
12J08105 10:34:04 

### 47.8 1.3 0.1 0.4 12108/0510:34:14 

### 47.7 1.1 0.1 0.4 12/0810510:34:24 45.3 1.2 0.1 0.3 12/08/0510:34:34 38.3 1.3 0.1 0.3 12108/0510:34:44 29.4 1.0 0.1 0.3 12/08/0510:34:54 12.3 1.2 0.1 0.2 1210810510:35:04 2.3 1.2 0.0 0.1 1 2108/05 1 0:35:14 74.2 1.3 0.1 0.2 12108/05 10:35:24 192.8 1.5 0.1 0.2 12J08/0510:35:34 194.8 1.6 0.1 0.3 12108/0510:35:44 195.2 1.5 0.1 0.4 12J08/0510:35:54 195.5 1.2 0.1 0.4 12/08/0510:36:04 199.6 1.2 0.1 0.4 12108/0510:36:14 201.8 1.2 0.1 0.3 12/08/0510:36:24 

### 201.7 1.2 0.1 0.2 12/08/05 10:36:34 

### 201.8 1.3 0.1 0.2 200 ppm C31

- 18 12/08/0510:36:44 

### 201.6 1.2 0.1 0.1 12108/0510:36:54 

### 201.6 1.2 0.1 0.1 1 2108/05 1 0:37:04 200.2 1.2 0.1 0.1 12108/0510:37:14 192.6 1.2 0.0 0.1 12108/0510:37:24 139.4 1.2 0.1 0.0 12108/05 10:37:34 112.8 1.3 0.1 01 12/08/0510:37:44 8.7 1.1 0.1 0.0 12108/0510:37:54 3.0 1.3 0.1 0.1 1 ZJ08/05 10:38:04 2.8 1.6 0.1 0.1


# j

. nB

Page 212/8105 Run #1



### DatelTime VOC CO NOx S02 mm/ddlyyhh:mm:ss ppm ppm ppm ppm 1 2108105 1 1:19:28 129.0 148.3 26.3 83.3 1210810511:19:38 129.4 148.3 26.3 84.0 1210810511:19:48 129.7 148.2 26.3 84.6 12108/05 11:19:58 129.9 148.0 26.4 84.9

Start Run #1 12/08/0511:20:08 128.9 148.3 26.5 85.0 1 2108105 1 1:20:18 130.2 147.9 26.5 85.0 12/0810511:20:28 130.7 147.8 26.5 85.1 12108l0511:20:38 130.1 147.7 26.5 85.5 12108105 1 1:20:48 130.9 147.7 26.5 86.2 1 2108105 1 1:20:58 130.8 147.6 26.5 86.5 12/0810511:21:08 131.1 147.7 26.4 86.4 1 2108105 1 1:21:18 129.9 148.2 26.4 86.2 12/08J0511:21:28 130.8 148.4 26.4 86.0 1 2108105 1 1:21:38 130.4 148.6 26.4 86.0 1 2/08105 1 1:21:48 129.9 148.7 26.4 86.4 12108/0511:21:58 130.7 148.7 26.5 86.7 12/08/05 11:22:08 130.7 149.1 26.5 86.7 12108/0511:22:18 130.6 149.1 26.4 86.4 1210810511:22:28 129.7 149.3 26.3 86.3 12/08/0511:22:38 129.5 149.5 26.4 85.9 12108/0511:22:48 129.4 149.5 26.4 85.3 12108/05 11:22:58 130.3 149.8 26.5 84.3 12108/0511:23:08 129.8 150.1 26.5 83.0 1 2/08105 1 1:23:18 129.3 150.3 26.5 81.8 1 2108/05 1 1:23:28 129.6 150.3 26.6 81.2 12/08/0511:23:38 128.5 150.5 26.6 81.1 1210810511:23:48 129.6 150.5 26.7 81.0 1 2/08105 1 1:23:58 129.5 150.6 26.7 81.0 1 2108/05 1 1:24:08 129.4 150.6 26.7 80.8 1 2108105 1 1:24:18 130.0 150.8 26.6 80.8 1 2108/05 1 1:24:28 128.6 150.9 26.5 80.6 12/08/0511:24:38 129.9 151.1 26.5 80.4 12108/0511:24:48 129.6 151.5 26.5 80.3 12108/0511:24:58 130.2 151.7 26.7 80.1 1 2108/05 1 1:25:08 129.2 151.5 26.7 80.2 12/0810511:25:18 129.3 151.2 26.7 80.1 12108J0511:25:28 129.6 151.2 26.7 80.1 12/0810511:25:38 127.8 150.6 26.8 80.0 12/0810511:25:48 128.2 150.1 26.7 80.2 12108J0511:25:58 128.2 149.8 26.7 80.3 1 2108/05 1 1:26:08 126.4 149.6 26.7 80.3 1 2108105 1 1:26:48 126.2 149.9 26.7 80.5 1210810511:26:58 126.6 150.0 26.6 80.5 12108/0511:27:08 126.0 149.7 26.6 80.6 12/08/0511:27:18 125.8 149.6 26.6 80.6 1210810511:27:28 125.9 149.7 26.6 80.7 12108/0511:27:38 126.8 149.6 26.6 80.7 1210810511:27:48 127.7 149.6 26.6 80.6 12108/0511:27:58 128.2 149.7 26.6 80.4 12108/0511:28:08 128.0 149.7 26.6 80.2 1 2108105 1 1:28:18 127.5 149.8 26.7 79.9 1210810511:28:28 127.9 149.9 26.7 79.6 1210810511:28:38 127.1 149.7 26.7 79.6 12108/0511:28:48 128.4 149.6 26.8 80.1 12/0810511:28:58 128.4 149.6 26.8 80.8 12108/0511:29:08 128.5 149.5 26.8 81.5 12108/0511:29:18 129.2 149.4 26.8 82.3 1210810511:29:28 128.8 149.2 26.8 83.1 1210810511:29:38 130.2 148.9 26.8 83.7 1210810511:29:48 130.0 148.6 26.9 84.2 1 2/08105 1 1:29:58 131.9 148.3 26.8 84.6 1 2108105 1 1:30:08 131.8 148.0 26.8 84.9 12108/0511:30:18 133.7 147.7 26.8 85.0 12108/0511:30:28 133.5 147.5 26.9 85.3 1210810511:30:38 135.0 147.4 26.9 85.5 1210810511:30:48 135.3 147.4 26.9 85.9 1210810511:30:58 136.3 147.4 27.0 86.2 1 2108105 1 1:31:08 135.8 147.6 27.1 86.4 1210810511:31:18 135.0 147.5 27.2 86.7 1210810511:31:28 135.5 147.4 27.2 86.6 

# jn9
Page 1

### 1218105 Run #1

1 2108105 1 1:31:38 137.1 147.5 27.2 86.5 12/0810511:31:48 137.6 147.5 27.3 86.4 1210810511:31:58 137.1 147.7 27.2 86.4 1 2/08105 1 1:32:08 139.0 147.8 27.2 86.5 12l0810511:32:18 139.3 147.7 27.3 86.3 1 2/08105 1 1:32:28 141.0 147.7 27.4 86.2 1210810511:32:38 141.0 147.8 27.5 86.0 1 2/08106 1 1:32:48 141.7 148.5 27.6 86.0 12l0810511:32:58 142.5 149.0 27.7 86.1 12l0810511:33:08 142.8 149.4 27.7 86.3 1210810511:33:18 142.9 150.1 27.7 86.8 1 2108/05 1 1:33:28 144.1 150.9 27.7 86.9 1 2108/05 1 1:33:38 144.9 151.6 27.8 87.1 1210810511:33:48 145.4 152.3 27.7 87.2 12108/0511:33:58 147.9 153.5 27.9 87.4 12108/0511:34:08 149.1 154.5 27.9 87.7 1210810511:34:18 149.0 155.2 28.0 87.8 1 2108105 1 1:34:28 156.3 158.0 28.4 88.0 1 2108105 1 1:34:38 161.2 159.9 29.2 89.3 1270810511:34:48 161.8 160.0 29.4 91.0 1210810511:34:58 165.6 159.6 29.2 91.0 12108105 1 1:35:08 166.2 159.3 29.1 90.1 1210810511:35:18 165.4 158.8 28.9 89.1 1 2/08105 1 1:35:28 '164.3 158.3 28.7 88.3 1210810511:35:38 163.3 158.3 28.6 88.1 12/0810511:35:48 163.6 158.4 28.6 88.0 12108/0511:35:58 162.5 158.1 28.6 88.1 12108/0511:36:08 162.2 157.8 28.7 88.1 12108/0511:36:18 163.1 157.4 28.6 88.0 12/08l0511:36:28 162.2 157.4 28.5 87.9 12/0810511:36:38 162.1 157.6 28.4 87.8 1210810511:36:48 161.6 157.5 28.2 87.7 12/0810511:36:58 162.3 157.7 28.2 87.5 12/08l0511:37:08 161.5 157.6 28.1 87.4 12/0810511:37:18 160.4 157.4 28.1 87.3 12108105-11:37:28 162.8 157.3 28.1 87.3 12/08/0511:37:38 160.1 157.2 28.2 87.3 12108/0511:37:48 161.2 157.2 28.2 87.4 12/0810511:37:58 158.5 157.2 28.1 87.6 12/0810511:38:08 158.8 156.8 28.1 87.5 12108/0511:38:18 159.0 156.3 28.1 87.5 12108/0511:38:28 160.6 156.0 28.1 87.6 12108/0511:38:38 160.6 155.3 28.0 87.7 12108/0511:38:48 160.6 155.0 28.1 87.7 12108/0511:38:58 159.1 154.7 28.1 87.8 12108/0511:39:08 159.7 154.8 28.1 87.9 1 2108/05 1 1:39:18 160.9 155.0 28.0 88.0 12/08/0511:39:28 160.1 155.0 28.0 88.1 12/08/0511:39:38 160.4 155.3 28.0 88.0 12J08/0511:39:48 157.4 155.4 28.1 86.0 12/08/0511:39:58 157.6 155.4 28.0 88.0 12l0810511:40:08 158.0 155.5 28.0 88.0 12108/0511:40:18 157.8 155.8 28.0 88.0 12/0810511:40:28 157.6 156.2 28.0 88.1 12/0810511:40:38 156.4 156.1 27.9 88.1 12/0810511:40:48 157.3 156.1 28.0 88.1 1 2108/05 1 1:40:58 158.1 156.3 28.0 88.2 12108/0511:41:08 158.5 156.8 28.1 88.2 12/0810511:41:18 157.8 157.4 28.2 87.9 1 2/08105 1 1:41:28 157.8 158.1 28.1 87.8 12/0810511:41:38 157.1 158.6 28.1 87.9 12108/05 11:41:48 171.4 159.1 28.1 88.1 12108J0511:41:58 174.3 159.2 28.2 88.5 12/08105 11:42:08 194.0 159.4 28.2 88.8 1210810511:42:18 174.7 159.5 28.3 88.9 12108105 1 1:42:28 171.3 159.3 28.3 88.7 1210810511:42:38 169.7 159.3 28.2 88,6 1210810511:42:48 168.8 159.2 28.1 88.6 1 2108105 1 1:42:58 168.8 159.3 28.1 88.7 1 2/08105 1 1:43:08 168.8 159.6 28.0 89.1 12108105 11:43:18 168.8 160.1 28.0 89.2 1210810511:43:28 187.5 160.3 28.0 89.2 1210810511:43:38 183.2 160.4 28.0 89.1 1 2108105 1 1:43:48 179.8 160.4 28.0 89.1 

# 1.10
Page 212/8/05 Run #1

1210810511:43:58 178.6 160.0 28.0 89.1 12108/0511:44:08 177.7 159.7 28.0 89.0 12/08/0511:44:18 176.2 159.5 28.0 88.9 1210810511:44:28 176.4 159.4 27.9 88.8 1 2/08105 1 1:44:38 174.5 159.0 27.9 88.6 1 2/08105 1 1:44:48 171.1 72.0 27.3 86.9 12/08J0511:44:58 171.9 136.8 27.7 88.5 12/08/0511:45:08 170.2 158.6 27.9 88.4 1 2108/05 1 1:45:18 168.9 158.8 27.9 88.3 12/08/05 11:45:28 169.6 159.3 27.9 88.3 12/08/05 11:45:38 166.7 ' 159.5 27.9 88.3 1 2108/05 1 1:45:48 166.3 160.3 27.8 88.1 12/0810511:45:58 166.1 160.7 27.8 88.2 12108/0511:46:08 166.2 161.1 27.7 88.2 12/08/0511:46:18 165.3 161.9 27.7 88.3 12108/0511:46:28 164.8 162.8 27.7 88.4 1 2108/05 1 1:46:38 164.7 163.8 27.7 88.5 12/08/0511:46:48 164.7 164.5 27.7 88.4 1 2108/05 1 1:46:58 163.6 165.2 27.8 88.3 12/08/0511:47:08 164.7 165.4 27.9 88.2 12/08/0511:47:18 166.7 165.6 27.9 88.0 1210810511:47:28 165.6 165.8 27.9 88.0 12/0810511:47:38 164.7 165.6 27.9 87.8 12108/0511:47:48 167.7 165.8 27.8 87.7 12108/0511:47:58 164.4 167.1 28.0 87.9 1210810511:48:08 164.7 167.7 28.1 88.2 12108/0511:48:18 164.7 167.8 28.0 88.1 1210810511:48:28 166.7 167.4 28.0 87.8 12/08/0511:48:38 165.6 167.3 28.0 87.6 1210810511:48:48 164.7 166.5 28.0 87.5 12/08/0511:48:58 167.7 166.3 28.0 87.6 12/08/0511:49:08 164.4 165.9 27.9 87.6 12/08/0511:49:18 164.7

. 165.6 27.9 87.6 12/08/0511:49:28 166.7 165.1 27.9 87.5 12108/0511:49:38 165.6 164.8 27.9 87.4 12/08/0511:49:48 164.7 164.2 28.0 87.4 12108/0511:49:58 167.7 163.1 28.0 87.4 1 2108/05 1 1:50:08 164.4 162.5 28.0 87.3 12/08/0511:50:18 164.7 162.5 28.0 87.1 12108/0511:50:28 166.7 161.9 27.9 87.1 12108/0511:50:38 165.6 161.6 28.0 87.1 12/08/0511:50:48 164.7 161.2 28.0 87.0 12/0810511:50:58 167.7 161.0 28.0 87.1 1 2108/05 1 1:51:08 164.4 160.8 27.9 87.2 12/0810511:51:18 164.7 160.8 27.9 87.1 12/08/0511:51:28 164.7 161.0 27.9 87.1 12108/0511:51:38 164.7 161.1 27.9 87.0 1 2108/05 1 1:51:48 175.2 160.7 27.7 86.7 12108l0511:51:58 130.6 160.8 27.6 86.4 1 2108/05 1 1:52:08 121.2 161.3 27.5 86.2 12/08/0511:52:18 122.1 161.8 27.6 86.1 12108/0511:52:28 122.6 162.0 27.6 86.1 1 2108/05 1 1:52:38 121.2 162.1 27.8 86.3 12/08/0511:52:48 123.1 162.1 27.9 86.5 12/08/0511:5258 122.9 162.1 27.9 86.5 1 2108/05 1 1:53:08 122.2 162.0 27.9 86.8 12108/0511:53:18 122.2 161.6 27.8 87.1 12/08/0511:53:28 122.8 160.9 27.8 87.4 1 2108/05 1 1:53:38 123.1 160.1 27.8 87.5 12108/0511:53:48 123.0 159.8 27.8 87.6 1 2108/05 1 1:53:58 122.1 159.5 27.7 87.5 12108/0511:54:08 122.5 159.2 27.8 87.4 12/08/0511:54:18 122.8 158.9 27.8 87.4 12/0810511:54:28 122.6 158.7 27.7 87.4 12108/0511:54:38 122.4 158.3 27.6 87.2 12/08/0511:54:48 122.4 157.9 27.6 86.8 12/08/0511:54:58 122.1 157.7 27.6 86.5 12/08/0511:55:08 121.4 157.6 27.6 86.2 12108/0511:55:18 122.3 157.0 27.7 86.1 12108/0511:55:28 122.0 156.1 27.6 86.0 12/08/0511:55:38 123.0 155.2 27.6 85.8 12108/0511:55:48 123.2 154.6 27.6 85.7 12/0810511:55:58 123.2 154.2 27.6 85.6 12/08/0511:56:08 122.6 154.1 27.6 85.4 

# 1ti Page 31218105 Run #1

12/08/0511:56:18 122.9 153.5 27.5 85.5 12108/0511:56:28 122.6 153.6 27.4 85.3 1210810511:56:38 123.3 153.6 27.4 85.2 12108/0511:56:48 122.2 153.4 27.4 85.2 12/08/0511:56:58 123.4 153.3 27.5 85.3 12/08/05 11:57:08 121.8 153.2 27.5 85.4 12/08/0511:57:18 122.9 153.1 27.5 85.6 12/08/0511:57:28 121.8 152.7 27.5 85.7 12/08/0511:57:38 122.6 152.8 27.5 85:6 12108/0511:57:48 122.5 152.7 27.2 85.5 12/0810511:57:58 122.1 152.4 27.1 85.4 12/08/0511:58:08 121.5 152.3 27.1 85.2 1210810511:58:18 122.5 152.2 27.1 84.9 12/08/0511:58:28 122.7 152.0 27.1 84.9 12/0810511:58:38 122.5 151.9 27.2 84.9 12/0810511:58:48 122.0 152.6 27.3 85.0 12/0810511:58:58 122.3 152.9 27.4 85.2 12108/0511:59:08 124.6 153.5 27.5 85.4 12/08/0511:59:18 125.3 154.1 27.5 85.5 12/08/0511:59:28 126.5 154.4 27.6 85.6 12/08/0511:59:38 126.8 154.6 27.6 85.7 1 2108/05 1 1:59:48 127.2 154.3 27.5 85.7 12108/0511:59:58 126.9 154.3 27.4 85.3 12/0810512:00:08 126.5 154.2 27.4 85.1 1210810512:00:18 126.2 153.7 27.4 85.0 12/0810512:00:28 128.1 153.4 27.5 84.4 12/08/0512:00:38 128.9 153.2 27.6 83.7 12108/0512:00:48 126.8 153.5 27.9 82.9 12/08/05 12:00:58 127.3 153.7 27.9 82.3 12108/0512:01:08 126.1 153.7 27.9 81.6 12/08/0512:01:18 127.3 154.0 27.8 80.8 12/08/0512:01:28 127.3 154.3 27.7 80.3 12108/0512:01:38 127.3 154.6 27.7 79.9 12/08/0512:01:48 126.3 155.0 27.6 79.8 12108/0512:01:58 127.4 155.5 27.5 79.7 12108/0512:02:08 127.0 156.2 27.5 79.8 12/08/0512:02:18 126.3 156.7 27.4 79.8 1210810512:02:28 126.9 157.2 27.5 80.1 12108/0512:02:38 126.2 157.2 27.4 80.0 12108/0512:02:48 125.9 157.4 27.5 80.2 12108/0512:02:58 127.2 157.4 27.6 80.4 12108/0512:03:08 126.7 157.4 27.6 80.5 12/08/0512:03:18 126.7 157.6 27.6 80.8 12108/0512:03:28 123.1 69.1 26.8 79.2 12/08/0512:03:38 127.5 157.5 27.6 80.3 12108/0512:03:48 128.8 157.4 27.5 80.4 12/08/0512:03:58 128.0 157.2 27.5 80.4 12/08/0512:04:08 128.4 157.4 27.6 80.3 12108/0512:04:18 129.1 156.9 27.5 80.3 12/08105 12:04:28 128.7 156.4 27.6 80.3 12/0810512:04:38 129.0 156.3 27.6 80.1 12/0810512:04:48 128.9 156.0 27.6 80.0 12/08/0512:04:58 129.0 155.8 27.6 79.7 12/08/0512:05:08 127.6 155.6 27.6 79.4 12/08/05 12:05:18 127.5 155.5 27.5 79.3 12108/05 12:05:28 127.2 155.0 27.5 79.2 12108/0512:05:38 127.8 154.4 27.5 79.1 12/0810512:05:48 128.1 154.0 27.7 78.9 1210810512:05:58 127.3 153.6 27.8 78.6 12108/0512:06:08 128.3 153.0 27.8 78.2 1210810512:06:18 127.8 153.0 27.8 77.4 12108/0512:06:28 127.9 152.8 27.8 76.9 12108/0512:06:38 127.2 153.2 27.8 76.4 12/08/0512:06:48 128.6 154.0 27.8 76.2 12/08/0512:06:58 127.6 154.7 27.8 76.0 12/08/0512:07:08 129.2 155.5 27.8 76.0 12/08/0512:07:18 128.1 156.2 27.7 76.0 12/08/0512:07:28 127.4 156.6 27.6 76.1 12/08/0512:07:38 128.5 156.8 27.5 76.5 12/08/0512:07:48 128.6 157.0 27.5 76.8 12/0810512:07:58 128.1 157.2 27.5 77.1 12/08/0512:08:08 128.5 157.5 27.5 77.6 12/0810512:08:18 128.3 157.6 27.4 77.7 12108/0512:08:28 128.5 157.6 27.4 77.7 

# 1. 1. 2

Page 41218105 Run #1

12/08/0512:08:38 128.2 157.7 27.4 77.8 12108/0512:08:48 129.0 157.7 27.4 77.9 12/08/0512:08:58 128.6 157.7 27.4 78.0 12/08/0512:09:08 128.3 157.7 27.5 78.1 12108/0512:09:18 128.8 157.9 27.6 78.5 12/08/0512:09:28 128.4 158.1 27.6 78.6 12/08/0512:09:38 128.0 158.1 27.6 78.7 12/08/0512:09:48 129.0 158.1 27.6 78.6 12108/0512:09:58 129.5 157.7 27.6 78.6 12108/0512:10:08 129.1 157.5 27.6 78.6 12/08/0512:10:18 129.2 187.5 27.6 78.5 1210810512:10:28 129.7 157.7 27.4 78.6 12108/0512:10:38 129.5 157.8 27.5 78.6 12108/05 121 0:48 129.9 157.8 27.5 78.7 1 2108105 1 2:10:58 129.2 158.0 27.6 78.8 12/08/05 12:11 :08 129.3 158.0 27.5 79.0 1210810512:11:18 129.3 158.0 27.6 79.0 12/08/0612:11:28 128.8 157.4 27.6 79.1 12108/0512:11:38 129.8 156.6 27.7 79.1 1210810512:11:48 128.7 156.1 27.7 79.1 12/08/0512:11:58 129.2 156.0 27.7 79.1 1210810512:12:08 128.9 155.8 27.8 79.0 12/08/0512:12:18 129.1 155.7 27.7 79.0 1210810512:12:28 129.6 155.9 27.7 78.9 12/08/0512:12:38 129.5 155.9 27.7 79.1 12108/0512:12:48 129.1 155.9 27.7 79.3 12108/0512:12:58 129.4 156.1 27.6 79.3 1 2108/05 1 2:13:08 129.3 156.4 27.5 79.4 12/08/0512:13:18 129.1 156.6 27.5 79.3 12108/0512:13:28 128.7 156.8 27.6 79.1 12/08/0512:13:38 128.1 157.3 27.6 78.8 12108/0512:13:48 128.2 157.7 27.6 78.6 12/08/0512:13:58 129.4 158.0 27.5 78.2 12108/0512:14:08 128.4 158.0 27.5 77.7 12108/0512:14:18 128.3 158.3 27.4 77.4 12/08105 1214:28 128.2 158.5 27.2 77.2 12108/0512:14:38 128.3 158.6 27.3 76.9 12108/0512:14:48 127.4 158.7 27.3 76.7 12108/0512:14:58 127.9 158.8 27.3 76.5 1210810512:15:08 128.1 158.4 27.2 76.4 1 2108/05 1 2:15:18 127.3 158.1 27.2 76.2 1210810512:15:28 127.9 157.6 27.2 75.9 12/08/0512:15:38 126.8 157.3 27.3 75.8 12/0810512:15:48 127.5 156.8 27.2 75.8 12108/0512:15:58 127.6 156.3 27.2 75.7 12/08/0512:16:08 127.5 156.2 27.2 75.6 12/08/0512:16:18 127.3 156.2 27.2 75.8 1 2108/05 1 2:1 fi:28 127.4 156.2 27.2 76.2 12108/0512:16:38 125.9 156.1 27.2 76.6 12108/0512:16:48 125.6 156.1 27.2 76.8 12108/0512:16:58 126.5 156.5 27.3 76.9 12108/0512:17:08 125.5 156.8 27.3 77.1 1 2108/05 1 2:17:18 126.3 157.1 27.4 77.3 12108/0512:17:28 125.6 157.5 27.4 77.6 12108/0512:17:38 126.0 157.8 27.4 77.7 12/0810512:17:48 125.6 157.5 27.4 78.1 12/0810512:17:58 125.6 157.0 27.5 78.7 12108/0512:18:08 125.0 156.5 27.4 79.0 12/0810512:18:18 125.2 156.1 27.5 79.4 12/0810512:18:28 125.6 155.7 27.5 79.6 12/0810512:18:38 126.1 155.4 27.6 80.0 12/0810512:18:48 126.8 154.8 27.6 80.4 1210810512:18:56 125.3 154.7 27.6 80.7 12/0810512:19:06 126.9 154.6 27.6 81.0 12/0810512:19:18 127.9 154.6 27.7 81.5 12/0810512:19:28 127.5 154.9 27.7 82.0 1 2/08105 1 2:19:38 127.8 155.4 27.9 82.4 12/08/0512:19:48 128.2 155.6 27.9 82.9 12/08/0512:19:58 128.4 155.8 28.0 83.2 12108l0512:20:08 128.1 156.1 28.0 83.4 1210810512:20:18 128.5 156.4 28.0 83.5 12108/0512:20:28 129.1 156.5 27.9 83.6 12108105 1 2:20:38 128.9 156.5 27.9 83.7 12108/0512:20:48 129.1 156.4 27.9 83.9 

# 1.

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# .3

Page 51218105 Run #1

12/08/0512:20:58 128.8 156.7 27.9 84.1 12/08/0512:21:08 129.0 156.7 27.9 84.2 12108/0512:21:18 129.3 156.8 27.9 84.4 12/08/0512:21:28 129.0 156.9 27.9 84.3 12108/0512:21:38 129.0 156.9 27.9 84.0 12108/0512:21:48 129.3 156.8 27.9 83.7 12/0810512:21:58 128.8 156.4 27.9 83.4 12108J0512:22:08 128.7 156.3 27.8 82.9 12/0810512:22:18 129.2 156.4 27.8 82.7 12/08/0512:22:28 128.1 156.6 27.8 82.4 1 2108105 1 2:22:38 128.0 156.7 27.7 82.1 12/08105 12:22:48 128.2 156.5 27.7 81.8 12/0810512:22:58 128.8 156.1 27.6 81.6 1210810512:23:08 129.0 156.0 27.7 81.1 12108l0512:23:18 128.5 155.7 27.8 80.8 12J0810512:23:28 128.3 155.8 27.7 80.6 12J0810512:23:38 128.3 155.7 27.7 80.5 12/08l0512:23:48 127.7 155.6 27.7 80.4 12108/0512:23:58 125.0 111.4 27.4 79.4

Stop Run #1 138.61 155.21 27.55 83.63

12/08/0512:24:08 126.6 142.8 27.6 80.3 12/08/0512:24:18 126.6 155.7 27.6 80.0 12108/0512:24:28 122.9 148.9 27.0 79.3 12/08/0512:24:38 125.5 148.5 27.4 79.7 12/08/0512:24:48 125.6 154.3 27.5 79.4 1210810512:24:58 122.0 153.0 27.4 79.1 12/0810512:25:08 31.6 150.2 26.5 78.0 12/0810512:25:18 5.3 110.2 26.0 75.3 1 2/08105 1 2:25:28 6.0 122.4 24.2 74.7 1210810512:25:38 5.1 87.1 18.2 70.0 12/0810512:25:48 5.0 60.7 13.3 61.9 1210810512:25:58 4.9 41.0 9.6 52.8 12108/0512:26:08 4.4 28.4 7.1 44.1 1210810512:26:18 4.6 20.1 5.4 36.5 12/0810512:26:28 4.6 15.6 4.3 30.2 12/08/0512:26:38 4.3 12.6 3.5 25.1 12108/0512:26:48 4.5 11.6 3.2 20.8 12108/0512:26:58 4.0 10.7 3.1 17.9 1 2108/06 1 2:27:08 3.5 9.1 2.8 15.7 12108/0512:27:18 3.1 6.4 4.4 13.2 12/0810512:27:28 2.8 4.8 9.8 11.1 12108/0512:27:38 3.0 3.8 14.4 9.4 12/0810512:27:48 3.2 3.5 17.2 8.5 12/0810512:27:58 2.9 3.0 18.9 7.7 12/08/0512:28:08 2.8 2.7 20.1 8.9 12/08/0512:28:18 3.3 1.7 21.0 6.2 12/08/0512:28:28 2.8 1.3 21.5 5.4 1210810512:28:38 2.8 1.2 21.7 4.8 12108/0512:28:48 2.8 1.4 21.8 4.3 12/08/0512:28:58 3.0 1.1 21.8 3.8 12/08/0512:29:08 2.8 0.9 21.8 3.4 12/08/0512:29:18 2.8 1.1 21.7 3.0 12108/0512:29:28 3.3 1.0 21.8 2.7 12/0810512:29:38 2.8 0.9 21.9 2.4 12J0810512:29:48 2.9 0.9 21.9 2.0 12/0810512:29:58 3.1 0.8 22.2 1.9 100810512:30:08 3.2 0.8 22.5 1.7 12/0810512:30:18 3.4 0.6 22.6 1.3 12/0810512:30:28 3.0 0.7 22.7 1.1 12108105 1 2:30:38 3.4 0.5 23.1 0.9 1210810512:30:48 3.4 0.4 23.6 0.8 12/08l0512:30:58 3.4 0.3 23.8 0.6 12/08/0512:31:08 

### 3.2 0.3 24.0 0.4
1210810512:31:18 3.3 0.2 24.0 0.3 25.5 ppm IVOx 12/08J0512:31:28 3.9 0.3 24.0 0.2 1 2108/05 1 2:31:38 3.3 0.3 24.0 0.2 12/08/0512:31:48 3.5 0.3 24.0 0.4 12/08/0512:31:58 3.8 0.3 23.7 0.3 12/08/0512:32:08 3.9 0.2 23.0 0.4 12/08/0512:32:18 3.4 0.3 22.4 0.3 12108/0512:32:28 3.7 0.2 22.2 0.3 

# 1.

~ 

# .4
Page 612/8/05 Run #1

12/0810512:32:38 4.7 0.2 21.7 0.3 12108/0512:32:48 5.1 0.3 19.6 0.4 1210810512:32:58 4.9 0.9 17.0 0.6 12108/0612:33:08 4.5 1.2 12.1 0.9 12/08/0512:33:18 4.4 0.8 7.0 1.9 12/08/0512:33:28 4.6 0.3 3.9 6.8 12108/0512:33:38 4.6 0.2 2.9 15.6 12108/0512:33:48 4.6 0.1 2.0 26.9 12/08/0512:33:58 4.7 0.0 1.5 39.1 12/08/0512:34:08 4.9 0.1 1.2 48.9 12108/0512:34:18 4.4 0.2 0.9 58.5 12J0810512:34:28 4.4 0.1 0.8 66.7 12/0810512:34:38 5.1 0.1 0.7 72.4 12J0810512:34:48 4.4 0.1 0.7 76.9 12/0810512:34:58 4.6 0.1 0.6 80.1 1210810512:35:08 4.4 0.1 0.6 82.9 1210810512:35:18 4.3 0.1 0.6 85.4 12/0810512:35:28 4.9 0.1 0.6 87.5 1210810512:35:38 4.6 0.1 0.5 89.0 12/08/0512:35:48 4.6 0.1 0.5 90.6 12/0810512:35:58 4.5 0.1 0.5 92.3 12/0810512:36:08 4.3 0.1 0.5 93.7 1210810512:36:18 4.3 0.2 0.5 94.9 1210810512:36:28 4.3 0.2 0.5 95.8 12J0810512:36:38 4.4 0.1 0.5 96,4 1210810512:36:48 4.3 0.1 0.5 96.7 12/0810512:36:58 4.4 -0.1 0.5 97.0 12108/0512:37:08 4.5 0.1 0.5 97.4 12/0810512:37:18 4.3 0.1 0.5 97.9 12/0810512:37:28 4.3 -0.1 0.5 98.2 12108/0512:37:38 4.5 -0.1 0.5 98.3 12108/0512:37:48 4.5 -0.1 0.5 98.4 12/0810512:37:58 4.3 -0.2 0.5 98.4
1210810512:38:08 4.4 -0.2 0.5 98.4 12/0810512:38:18 3.9 -0.2 0. 

## 5 98..5 12/0810512:38:28 3.6 -0.3 0.4 98.4 12/08105 12:38:38 4.1 -0.4 0.4 97.1 ' 1210810512:38:48 3.7 -0.4 0.4 96.6 12/08J0512:38:58 4.0 -0.2 0.5 97.2 12/0810512:39:08 3.8 21.5 0.5 96.2 1210810512:39:18 3.8 86.9 0.5 89.3 12108/0512:39:28 3.9 128.0 0.4 76.5 12/08/0512:39:38 3.9 152.4 0.4 62.7 12/08/0512:39:48 3.9 168.1 0.4 49.8 12108/0512:39:58 3.9 176.4 0.3 39.6 1210810512:40:08 4.0 181.9 0.3 31.6 12108J0512:40:18 3.9 184.9 0.3 25.5 1210810512:40:28 3. 

## 8 184 .7 0.3 21.1 12/0810512:40:38 3.7 184.5 0.3 17.7 12/0810512:40:48 3. 

### 8 184 .6 0.3 15.4 12/0810512:40:58 3.7 181.2 0.3 13.2 12/08J0512:41:08 3.5 178.2 0.3 11.5 12/0810512:41:18 3.4 176.0 0.3 10.2 12108/0512:41:28 3.9 177.2 0.3 9.0 12/08/0512:41:38 77.8 177.6 0.3 8.5 12/08/0512:41:48 93.9 168.0 0.3 8.2 12/08/0512:41:58 92.9 137.7 0.3 7.9 12/08/0512:42:08 92.9 90.0 0.3 7.6 12/08/0512:42:18 

### 93 .0 52.8 0.3 7.3 12108J0512:42:28 92.9 34.4 0.3 7,0 1210810512:42:38 92.9 24.1 0.3 6.6 1210810512:42:48 93.0 17.2 0.2 6.1 101 ppm S02

200 ppm CO Zero VOC



## Page 7 

# ~. ~ ~12/8/05 Run #2

Date/7'ime VOC CO fVOx S02 mmldd/yy hh:mm:ss ppm ppm ppm ppm 12/08/0512:49:28 129.7 150.1 27.9 84.9 1210810512:49:38 128.6 149.9 28.0 86.8 12/08/0512:49:48 128.8 150.4 28.0 88.0 12/08/0512:49:58 128.9 151.1 27.9 8B.9

Start Run #2 12/08/0512:50:08 128.6 151.7 27.9 89.7 12/0810512:50:18 128.9 152.1 27.9 90.1 12108/0512:50:28 129.1 152.2 27.8 90.4 12/08/0512:50:38 128.9 152.2 27.7 90.4 1210810512:50:48 130.2 152.6 27.6 90.4 1210810512:50:58 129.5 152.9 27.6 90.4 1210810512:51:08 129.8 153.1 27.6 90.4 12/0810512:51:18 129.9 153.4 27.6 90.3 12/0810512:51:28 130.0 153.4 27.5 89.9 12l0810512:51:38 130.0 153.4 27.6 89.5 12108/0512:51:48 129.6 153.4 27.5 89.2 1210810512:51:58 129.9 153.5 27.5 88.9 12108/0512:52:08 129.2 153.3 27.5 88.6 12/08/0512:52:18 129.7 153.0 27.5 88.4 12/08/0512:52:28 129.3 153.1 27.4 88.3 12/08/0512:52:38 129.2 153.3 27.3 88.0 12108/0512:52:48 130.0 153.3 27.3 87.7 12/0810512:52:58 130.0 153.2 27.3 87.3 12J0810512:53:08 129.8 153.4 27.3 87.0 1210810512:53:18 128.8 153.3 27.3 86.6 12/08/0512:53:28 127.9 153.3 27.3 86.0 12/0810612:53:38 128.7 153.3 27.2 65.4 1210810512:53:48 127.8 153.0 27.3 84.7 12/08/0512:53:58 127.7 152.9 27.2 84.0 12/08/0512:54:08 127.4 152.9 27.0 83.4 1210810512:54:18 128.1 152.5 27.1 82.9 12/08/0512:54:28 127.5 152.3 27.1 82.5 12/08/0512:54:38 126.7 152.3 27.1 82.0 12108/0512:54:48 126.7 152.5 27.1 81.2 12108/0512:54:58 127.4 152.8 27.1 80.0 12108/0512:55:08 126.6 153.2 27.1 78.9 12/08/0512:55:18 124.1 147.8 26.7 76.7 1210810512:55:28 124.7 143.6 27.0 76.4 12/0810512:55:38 123.9 153.6 26.9 75.4 12/08/0512:55:48 124.5 153.4 26.9 74.6 12/08/0512:55:58 124.2 153.5 26.8 74.1 12108105 1 2:56:08 125.0 153.7 26.9 73.5 12/08/0512:56:18 125.2 153.6 26.8 72.9 12/0810512:56:28 123.9 153.8 26.7 72.7 1210810512:56:38 126.0 154.4 26.7 72.6 12/08/0512:56:48 123.6 154.7 26.6 72.7 12108/0512:56:58 124.5 154.9 26.7 73.1 12/0810512:57:08 124.3 155.3 26.7 73.6 1210810512:57:18 123.6 154.9 26.7 73.9 12/0810512:57:28 123.9 154.8 26.7 74.0 12/0810512:57:38 123.2 154.9 26.7 74.0 12/0810512:57:48 122.8 154.9 26.7 74.1 1 2108/05 1 2:57:58 123.2 154.9 26.7 73.9 12108/0512:58:08 123.6 154.9 26.7 74.0 1 ZJ08/05 12:58:18 121.4 154.7 26.6 74.0 12108/0512:58:28 122.7 154.1 26.6 74.0 12/08/0512:58:38 124.6 153.9 26.6 74.0 12J08/0512:58:48 123.1 153.8 26.5 74.0 12108/0512:58:58 123.3 153.9 26.5 74.0 12108/0512:59:08 123.8 154.4 26.5 73.9 12108/0512:59:18 124.1 154.6 26.5 73.8 12108/0512:59:28 125.6 154.6 26.6 73.7 12/08/0512:59:38 123.7 154.6 26.6 73.6 12108/0512:59:48 124.4 154.4 26.6 73.6 1210810512:59:58 125.8 153.9 26.6 73.8 1210810513:00:08 125.1 153.6 26.6 73.9 1210810513:00:18 125.6 153.7 26.6 74.2 1210810513:00:28 125.9 153.9 26.6 74.5 1210810513:00:38 124.6 154.2 26.6 74.7 12108/06 13:00:48 125.2 154.0 26.5 75.0 12108/0513:00:58 126.0 164.0 26.6 75.1 

# 1.16

Page 112/8105 Run #2

12/08/0513:01:08 125.2 154.1 26.6 75.3 12108/0513:01:18 125.2 154.3 26.6 75.4 1 2108/05 1 3:01:28 125.1 154.4 26.5 75.6 12/0810513:01:38 124.5 154.6 26.5 75.4 1210810513:01:48 125.5 154.9 26.5 75.2 12108/0513:01:58 124.0 155.0 26.6 75.0 12/08/0513:02:08 122.8 155.0 26.7 74.3 12/08/0513:02:18 121.8 155.0 27.0 73.0 12108/0513:02:28 121.9 155.4 27.5 71.2 12/0810513:02:38 115.2 155.7 27.6 69.3 12/0810513:02:48 111.7 156.0 27.5 66.9 1210810513:02:58 111.7 155.7 27.6 64.6 1210810513:03:08 118.3 153.3 27.6 62.6 12108/0513:03:18 122.4 150.6 27.3 61.3 1210810513:03:28 124.3 149.2 27.2 60.3 1 2108105 1 3:03:38 125.8 149.0 27.1 59.5 1 2108105 1 3:03:48 126.2 149.5 27.0 58.9 1 2108105 1 3:03:58 122.9 151.0 27.0 58.8 1210810513:04:08 122.5 152.4 27.0 58.8 12108/0513:04:18 121.6 153.7 27.0 59.0 1210810513:04:28 119.9 154.3 27.1 59.4 1 2108/05 1 3:04:38 120.4 154.4 27.1 60.0 1 2108/05 1 3:04:48 119.3 154.7 27.0 60.6 12l08/0513:04:58 113.0 43.6 26.2 58.3 12108/0513:05:08 118.0 154.4 27.0 61.7 12108/0513:05:18 117.6 154.3 27.0 62.1 12/08/0513:05:28 117.5 154.3 26.9 62.6 12/08/0513:05:38 117.4 154.4 27.0 63.1 12/08/0513:05:48 116.7 154.9 26.9 63.4 12108/0513:05:58 117.3 155.0 27.0 63.8 12/08/0513:06:08 116.2 155.3 26.9 64.1 12108/0513:06:18 117.6 155.5 26.9 64.5 12108/0513:06:28 117.5 155.6 26.9 65.0 12108/0513:06:38 116.3 155.6 26.9 65.4 12J08/0513:06:48 117.7 155.6 26.9 66.0 12108/0513:06:58 118.2 155.6 26.9 66.6 12/08/0513:07:08 119.4 155.4 27.0 67.1 1210810513:07:18 119.8 155.3 27.0 67.5 1 2/08105 1 3:07:28 121.0 155.3 27.0

. 67.8 12/0810513:07:38 121.9 155.2 27.0 68.0 12/0810513:07:48 121.6 155.1 27.0 68.4 12/08/0513:07:58 122.5 154.7 27.1 68.6 12/0810513:08:08 122.3 155.0 27.0 68.8 12/08/0513:08:18 122.2 155.4 27.1 69.1 12/0810513:08:28 122.5 155.5 27.0 69.3 12108/0513:08:38 122.9 155.6 27.1 69.5 1210810513:08:48 122.5 155.8 27.1 69.6 12/08/0513:08:58 122.6 156.0 27.2 69.8 12/08/0513:09:08 122.2 156.1 27.2 70.0 12/08/0513:09:18 122.5 156.3 27.2 70.1 12/08/0513:09:28 123.8 156.7 27.2 70.3 12/08/0513:09:38 124.1 157.1 27.3 70.3 12/08/0513:09:48 122.4 157.1 27.3 70.3 12/08/0513:09:58 123.8 156.7 27.3 70.4 12/08/0513:10:08 123.8 156.4 27.2 70.4 12108/0513:10:18 123.3 156.3 27.2 70.5 1210810513:10:28 122.8 156.4 27.2 70.4 12/08/0513:10:38 122.6 156.5 27.2 70.3 12/08/0513:10:48 123.6 156.6 27.2 70.4 12/08/0513:10:58 123.7 156.3 27.3 70.4 1 2108105 1 3:11:08 123.5 156.1 27.3 70.5 12/08/0513:11:18 122.7 155.6 27.2 70.5 12/08/0513:11:28 123.7 155.3 27.2 70.7 12/08/0513:11:38 123.4 155.1 27.3 70.7 12/08/0513:11:48 123.1 155.0 27.3 70.8 12/08/0513:11:58 123.0 155.0 27.4 70.8 12/0810513:12:08 122.6 155.1 27.4 70.9 12/0810513:12:18 121.8 155.2 27.3 71.2 1210810513:12:28 123.3 155.4 27.3 71.1 12/08/0513:12:38 123.3 155.5 27.4 71.1 12/08/0513:12:48 122.2 155.5 27.3 71.1 12l0810513:12:58 122.7 155.6 27.1 71.1 12/08/0513:13:08 122.2 156.0 27.2 71.1 1210810513:13:18 121.6 156.3 27.2 71.4 

# 1. ! "1

Page 212/8/05 Run #2

12I08/0513:13:28 121.9 156.6 27.2 71.5 1 2108105 1 3:13:38 121.2 156.7 27.2 71.6 12108105 1 3:13:48 121.4 156.7 27.1 71.6 12/08/0513:13:58 121.9 156.6 27.2 71.7 1210810513:14:08 120.4 156.3 27.2 71.8 12108/0513:14:18 121.2 156.1 27.1 71.7 12/08/0513:14:28 121.6 155.6 27.1 71.8 12/08/0513:14:38 121.6 155.3 27.1 72.0 12/08/0513:14:48 121.6 154.7 27.0 71.7 12/08/0513:14:58 120.7 154.0 27.0 71.5 12/08f0513:15:08 119.9 153.6 27.0 71.5 12/0810513:15:18 120.4 153.0 27.1 71.5 1210810513:15:28 120.1 152.3 27.0 71.4 12108/0513:15:38 121.5 151.9 27.0 71.2 1210810513:15:48 122.3 151.9 26.9 71.2 12/0810513:15:56 121.4 151.9 26.8 71.3 1210810513:16:08 122.9 152.1 26.8 71.3 12108/0513:16:18 123.4 152.5 26.9 71.4 12108/0513:16:28 123.7 152.5 26.9 71.4 12/08/0513:16:38 122.9 152.4 26.9 71.6 12108/0513:16:48 122.8 152.4 27.1 71.7 12108/0513:16:58 122.4 152.3 27.1 7'1.8 1 2108/05 1 3:17:08 122.7 152.7 27.1 72.0 12108/0513:17:18 122.8 152.9 26.9 72.0 1 2/08105 1 3:17:28 122.0 152.7 26.9 72.0 1210810513:17:38 122.4 152.6 26.7 71.9 12/08/0513:17:48 122.8 152.7 26.7 71.9 12108J0513:17:58 122.9 152.8 26.7 71.9 12/08/0513:18:08 122.7 152.8 26.7 71.8 12108/0513:18:18 122.7 152.7 26.7 71.7 12/08/0513:18:28 122.9 152.9 26.8 71.6 12/08/0513:18:38 122.5 152.6 26.9 71.6 12/0810513:18:48 122.7 152.4 26.9 71.6 12/08/0513:18:58 122.7 152.3 26.8 71.4 12/08/0513:19:08 121.3 152.5 26.9 71.4 12/0810513:19:18 122.0 152.7 26.8 71.6 12/0810513:19:28 122.3 152.7 26.8 71.8 12108/0513:19:38 123.2 152.4 26.8 72.0 12l08/0513:19:48 122.4 152.7 26.7 72.2 12108/0513:19:58 122.7 152.7 26.7 72.3 12/08/0513:20:08 123.6 153.0 26.6 72.6 12108/0513:20:18 124.3 153.3 26.7 72.8 12/08/0513:20:28 123.4 153.9 26.6 73.1 1210810513:20:38 123.7 154.2 26.6 73.5 12/08/0513:20:48 123.1 153.9 26.6 73.9 1210810513:20:58 123.7 153.6 26.6 74.3 12/08/0513:21:08 123.4 153.1 26.6 74.9 12108/0513:21:18 123.4 152.7 26.5 75.4 12/08/0513:21:28 123.6 152.0 26.6 75.8 12108/0513:21:38 121.7 152.1 26.6 76.3 12/0810513:21:48 121.3 151.9 26.7 76.7 12/08/0513:21:58

. 121.5 151.5 26.6 77.1 12/08/0513:22:08 121.2 151.4 26.5 77.6 12/08/0513:22:18 121.3 151.5 26.6 78.0 12J08/0513:22:28 121.1 151.8 26.5 78.3 12/08/0513:22:38 121.4 151.9 26.5 78.3 12108/0513:22:48 121.6 152.0 26.5 78.5 12108/0513:22:58 121.3 151.8 26.5 78.8 12/0810513:23:08 121.3 152.1 26.6 78.9 12/08/0513:23:18 121.6 152.4 26.7 79.1 12/0810513:23:28 122.3 152.5 26.8 79.4 12108f0513:23:38 122.3 152.4 26.8 79.5 12/0810513:23:48 123.3 152.1 26.8 79.7 12/0810513:23:58 122.5 151.8 26.7 79.8 1210810513:24:08 123.5 151.6 26.8 79.9 12/08/0513:24:18 124.3 151.5 26.8 80.1 12108/0513:24:28 123.8 151.8 26.9 80.1 12/08/0513:24:38 123.5 152.1 26.8 80.0 12/08/0513:24:48 122.7 152.0 26.8 80.0 1210810513:24:58 122.6 151.6 26.8 79.9 1210810513:25:08 123.4 151.6 26.8 79.7 1210810513:25:18 123.7 161.5 26.8 79.6 12/08/0513:25:28 122.7 151.4 26.9 79.4 1 2108105 1 3:25:38 123.5 151.4 27.0 79.1 

# 1.18

Page 312/8/05 Run #2

12/08/0513:25:48 122.4 151.8 26.8 78.5 12/0810513:25:58 122.4 152.5 26.7 77.2 12/08/0513:26:08 121.4 152.6 26.7 75.8 12/08/0513:26:18 122.5 152.7 26.8 74.3 12/08/0513:26:28 122.1 152.9 27.1 72.9 12/08/0513:26:38 120.4 152.7 27.2 71.3 12/08/0513:26:48 121.7 152.3 27.2 70.0 12/08/0513:26:58 121.1 152.0 27.1 68.4 12108/0513:27:08 120.7 152.2 26.9 66.8 12/08/0513:27:18 121.3 152.4 26.9 65.5 12108/0513:27:28 122.1 152.7 26.9 64.3 12/08/0513:27:38 121.2 152.6 28.8 63.6 12108/0513:27:48 122.2 153.0 26.8 62.8 12108/0513:27:58 119.7 153.1 26.8 62.5 12108/0513:28:08 121.2 153.2 26.8 62.3 12108/0513:28:18 119.9 153.5 26.8 62.1 12108/0513:28:28 120.5 153.7 26.8 62.1 12/08/0513:28:38 119.7 153.6 26.8 62.1 12/08/0513:28:48 119.1 153.5 26.8 62.0 12108/0513:28:58 117.7 153.5 26.7 62.0 12108/0513:29:08 119.2 153.7 26.6 61.9 12108/0513:29:18 119.7 153.9 26.6 61.8 12108/0513:29:28 119.5 153.4 26.7 61.7 12/08/0513:29:38 120.5 153.4 26.7 62.0 12108/0513:29:48 120.5 153.3 26.7 62.3 1210810513:29:58 120.2 153.4 26.8 62.7 12108/0513:30:08 119.0 153.0 26.8 63.0 1210810513:30:18 120.4 152.7 26.9 63.3 12108/0513:30:28 119.6 152.4 27.0 63.8 12/08/0513:30:38 119.7 152.1 27.0 64.4 12/0810513:30:48 118.7 152.1 26.9 65.0 1210810513:30:58 120.2 152.4 26.8 65.3 12/08/0513:31:08 119.3 152.5 26.9 65.6 12J0810513:31:18 119.8 152.9 26.8 65.9 12/0810513:31:28 120.9 153.0 26.8 66.3 12/0810513:31:38 120.5 153.4 26.8 66.5 12/0810513:31:48 121.0 153.9 26.8 66.8 12108/0513:31:58 120.5 154.4 26.8 67.0 12/0810513:32:08 120.7 154.8 26.8 67.2 12/08/0513:32:18 120.5 155.1 26.8 67.4 1210810513:32:28 119.7 155.2 26.8 67.7 12/0810513:32:38 120.6 155.0 26.7 67.7 12/08/0513:32:48 119.7 155.1 26.6 67.4 12/08/0513:32:58 120.5 154.9 26.5 66.9 12/08/0513:33:08 121.3 154.6 26.6 66.5 12/08/0513:33:18 121.3 154.9 26.6 66.1 12108/0513:33:28 121.6 155.2 26.6 65.9 12108/0513:33:38 121.0 155.3 26.7 65.7 12108/0513:33:48 120.7 155.4 26.7 65.6 12108/0513:33:58 121.7 155.4 26.7 65.5 12/08/0513:34:08 120.8 155.4 26.8 65.3 12/0810513:34:18 121.8 155.4 26.7 65.0 12/0810513:34:28 121.7 155.1 26.7 64.6 1210810513:34:38 121.1 155.0 26.7 64.4 12/08/0513:34:48 120.9 155.0 26.8 64.3 12/08/0513:34:58 121.5 154.8 26.8 64.1 12108/0513:35:08 121.9 154.7 26.7 64.0 1210810513:35:18 122.4 154.4 26.7 63.7 1210810513:35:28 121.6 154.4 26.8 63.8 1210810513:35:38 122.7 154.5 26.8 63.8 12l0810513:35:48 121.3 154.0 26.9 63.7 12/0810513:35:58 121.6 153.5 27.0 63.6 12/0810513:36:08 121.8 153.6 27.0 63.4 12/0810513:36:18 121.3 153.5 26.9 63.3 12/08/0513:36:28 122.2 153.1 26.9 63.2 12/08/0513:36:38 121.6 152.7 26.9 63.1 12/08/0513:36:48 121.6 152.6 27.0 62.9 12108/0513:36:58 121.8 152.4 27.0 62.7 12/08/0513:37:08 121.6 151.9 27.0 62.6 12J0810513:37:18 121.8 151.7 27.0 62.4 12/08/05 13:37:28 121.6 151.9 26.9 62.2 12108/0513:37:38 122.0 152.1 26.9 62.0 12J08/0513:37:48 120.8 152.1 26.8 62.0 12108/0513:37:58 120.6 152.1 26.8 61.8

Page 4 

# ~ 

# _ 1 g12/8/05 Run sF2

12108/0513:38:08 120.7 152.1 26.8 61.8 12/08/0513:38:18 118.9 152.2 26.8 61.8 12108/0513:38:28 119.9 152.6 26.8 61.7 1 2108/06 1 3:38:38 120.0 153.0 26.8 61.7 1210810513:38:48 120.0 153.1 26.9 61.8 12108/0513:38:58 119.8 153.6 26.7 61.9 12108/0513:39:08 120.1 154.6 26.7 62.0 12/08/0513:39:18 119.5 155.1 26.8 62.1 12108/0513:39:28 120.2 155.0 26.8 62.3 12108/0513:39:38 119.5 154.8 26.7 62.6 12/0810513:39:48 119.7 154.8 26.6 62.5 12/08/0513:39:58 120.4 154.7 26.6 62.4 12108/0513:40:08 119.6 154.2 26.5 62.5 1210810513:40:18 120.4 153.9 26.6 62.5 12/0810513:40:28 120.7 153.9 26.7 62.4 12108/0513:40:38 119.8 153.9 26.7 62.4 12108/0513:40:48 121.1 163.8 26.6 62.3 12/0810513:40:58 120.4 153.6 28.6 62.3 12108i0513:41:08 121.8 153.6 26.6 62.3 12/08/0513:41:18 122.2 153.9 26.6 62.4 12/08/0513:41:28 121.8 153.9 26.6 62.5 12/08/0513:41:38 121.8 153.6 26.7 62.5 12/08/0513:41:48 122.7 153.6 26.7 62.7 12/0810513:41:58 123.3 153.6 26.7 62.9 12/0810513:42:08 123.5 153.5 26.6 63.1 12108/0513:42:18 122.1 153.3 26.7 63.2 12108/0513:42:28 123.1 153.2 26.6 63.2 12/08/0513:42:38 123.7 152.8 26.7 63.3 12/08/0513:42:48 122.5 152.9 26.7 63.4 12/08/0513:42:58 122.9 153.0 26.6 63.5 12/08/0513:43:08 122.6 153.2 26.6 63.6 12/08/0513:43:18 123.0 153.3 26.6 63.7 12/0810513:43:28 122.8 153.3 26.6 63.6 12/0810513:43:38 122.8 153.6 26.6 63.7 12108105 1 3:43:48 123.2 153.8 26.6 63.9 12/08/0513:43:58 123.0 153.8 26.6 64.1 12/08/0513:44:08 123.6 153.6 26.6 64.2 12108/0513:44:18 123.0 163.7 26.7 64.2 12108/0613:44:28 122.6 153.6 26.7 64.1 12108/0513:44:38 122.9 153.5 26.7 64.1 12/0810513:44:48 123.1 153.6 26.7 64.0 1210810513:44:58 122.7 153.6 26.7 64.1 12108/0513:45:08 123.5 153.8 26.7 64.1 12/08/0513:45:18 122.2 154.1 26.7 64.1 12108/0513:45:28 124.0 154.2 26.7 64.2 12108/0513:45:38 123.9 154.3 26.8 64.3 12/08/0513:45:48 123.5 154.5 26.8 64.4 12/08/0513:45:58 124.6 154.7 26.8 64.5 12108/0513:46:08 122.4 154.9 26.8 64.8 12/08/0513:46:18 122.5 154.8 26.8 64.9 12108/0513:46:28 122.1 155.0 26.8 65.2 12/08/0513:46:38 122.8 154.7 26.8 65.3 12108/0513:46:48 122.2 154.8 26.8 65.3 12/08/0513:46:58 121.5 155.0 26.8 65.3 12108/0513:47:08 121.6 155.0 26.8 65.5 12/08/0513:47:18 121.5 154.7 26.9 65.6 12/0810513:47:28 121.7 154.3 26.9 65.5 12/08/0513:47:38 121.6 154.0 26.9 65.6 12108/0513:47:48 120.7 153.6 26.8 65.4 12/08/0513:47:58 121.7 153.3 26.8 65.4 12108/0613:48:08 120.8 153.5 26.7 65.3 12/08/0513:48:18 121.0 153.7 26.6 65.1 12108/0513:48:28 120.8 153.9 26.6 65.1 12/0810513:48:38 121.1 153.9 26.7 65.0 12/08/0513:48:48 121.4 153.9 26.6 65.1 12108/0513:48:58 120.6 154.1 26.6 65.3 12108/0513:49:08 121.0 153.9 26.6 65.2 12108/0513:49:18 121.1 153.7 26.6 65.3 12108/0513:49:28 120.6 153.5 26.6 65.2 1 2108/05 1 3:49:38 121.2 153.6 26.5 64.9 12108/0513:49:48 122.4 153.6 26.6 64.8 1 2108/05 1 3:49:58 123.2 154.0 26.6 64.7 12108/0513:50:08 123.0 154.5 26.6 64.5 12/08/0513:50:18 123.6 154.9 26.6 64.6

Page 5 

# 1_2V1218105 Run #2

12/0810513:50:28 124.0 155.1 26.6 64.3 12/08/0513:50:38 123.2 155.1 26.4 64.1 1210810513:50:48 123.4 155.5 26.4 64.0 12108/0513:50:58 123.1 155.9 26.3 64.0 12/0810513:51:08 122.5 155.6 26.4 64.0 12/08/0513:51:18 123.6 155.2 26.4 64.0 12108/0513:51:28 122.7 155.1 26.5 64.2 12/0810513:51:38 123.1 154.8 26.6 64.2 12/08/0513:51:48 123.5 154.6 26.6 64.2 12/0810513:51:58 122.4 154.6 26.6 64.1 12/0810513:52:08 122.3 154.4 26.6 64.0 1210810513:52:18 122.9 154.4 26.5 64.0 12/0810513:52:28 122.6 154.3 26.6 63.9 12/0810513:52:38 123.0 154.3 26.6 63.8 12/0810513:52:48 122.3 154.3 26.5 63.7 12/0810513:52:58 122.1 154.1 26.5 63.6

Stop Run If2 122.48 153.47 26.86 69.78

12108/0513:53:08 122.9 154.2 26.6 63.4 12/0810513:53:18 121.9 154.1 26.6 63.5 12/0810513:53:28 122.5 154.1 26.5 63.4 12/08l0513:53:38 117.7 127.9 25.5 60.9 1210BI0513:53:48 120.6 152.9 26.4 63.2 12108/0513:53:58 36.4 149.4 25.8 62.3 12108/0513:54:08 6.1 147.5 25.4 61.2 12/08/0513:54:18 6.4 131.3 24.5 60.5 12108/0513:54:28 5.3 91.8 19.5 57.9 12l08/0513:54:38 5.3 60.9 13.1 52.1 12108/0513:54:48 5.2 41.2 10.2 45.4 1210810513:54:58 4.4 25.7 7.9 38.9 12108/0513:55:08 4.5 16.8 6.1 32.0 12J08l0513:55:18 3.9 10.1 6.4 25.6 12l08/0513:55:28 3.1 6.0 11.6 20.0 12/08/0513:55:38 2.9 4.2 15.7 16.3 12l08/0513:55:48 3.0 3.1 19.0 12.8 12/08/0513:55:58 2.9 2.5 21.0 10.0 12108l0513:56:08 2.8 2.0 22.0 8.2 12/0810513:56:18 2.8 2.0 22.3 6.5 12108/0513:56:28 3.0 1.6 22.4 5.1 12/08/0513:56:38 3.6 0.9 22.5 3.9 12108/0513:56:48 4.4 0.6 22.5 3.0 12/08/0513:56:58 7.0 0.7 22.4 2.3 1210810513:57:08 7.3 0.6 22.4 1.8 12/0810513:57:18 7.3 0.4 22.4 1.5 12/0810513:57:28 7.9 0.3 22.4 1.1 12/08l0513:57:38 7.0 0.3 22.3 0.9 1210810513:57:48 6.2 0.3 22.3 0.7 1210810513:57:58 7.0 0.4 21.8 0.4 1210810513:58:08 4.8 0.4 21.2 0.2 1 2108/05 1 3:58:18 3.7 0.6 21.2 0.1
1210810513:58:28 4.1 0.8 20.8 0.2 12/08/0513:58:38 4.9 1.3 18.5 0.2 12/08/0513:58:48 5.3 1.8 16.0 0.3 12108/0513:58:58 8.6 2.6 11.3 0.7 12108/0513:59:08 10.6 3.1 7.0 1.1 12/0810513:59:18 8.9 1.2 4.3 2.4 .12108l051159:28 10.7 0.3 2.7 6.8 12108/05 13:59:38 11.3 0.1 1.8 14.2 12/0810513:59:48 10.1 -0.1 1.4 23.9 12/0810513:59:58 9.9 -0.2 1.2 34.6 12/08/0514:00:08 10.3 -0.2 1.0 44.9 12108/0514:00:18 10.6 -0.2 0.8 53.9 12/08/0514:00:28 11.0 -0.3 0.8 60.7 12/08/0514:00:38 9.8 -0.4 0.8 65.5 12/08/0514:00:48 9.9 -0.5 0.7 69.6 12/08/0514:00:58 9.0 -0.4 0.7 72.9 12/08/0514:01:08 8.7 -0.4 0.7 76.1 12/08/0514:01:18 9.0 -0.4 0.6 78.9

12/08/0514:01:28 8.3 -0.7 0.6 81.1 12/08/0514:01:38 8.3 -0.8 0.6 82.9 12/08l0514:01:48 8.8 -1.2 0.6 84.6 12/0810514:01:58 8.3 -1.0 0.6 85.9 25.5 ppm NOx

Zero S02

Page 6 

# I +w ~12/8105 Run #2

12/08/0514:02:08 8.3 -1.1 0.5 87.0 12/08/0514:02:18 8.1 -0.9 0.6 88.0 12/0810514:02:28 7.8 -0.7 0.6 88.7 1210810514:02:38 7.4 -0.7 0.5 89.6 12/08/0514:02:48 7.2 -0.7 0.5 90.5 12/08/0514:02:58 7.3 -0.8 0.5 91.4 12/08/05 14:03:08 6.6 -1.1 0.4 92.1 12J08J0514:03:18 6.2 -1.0 0.5 92.7 12108/0514:03:28 5.4 -1.0 0.5 93.1 12108/0514:03:38 5.0 -0.8 0.4 93.4 12108/0514:03:48 4.2 -0.6 0.4 93.7 12/08/0514:03:58 3.5 -0.6 0.4 94.1 12/08/0514:04:08 2.9 -0.7 0.4 94.9 12108/0514:04:18 2.9 -0.8 0.4 95.4 12108/0614:04:28 2.9 -0.8 0.4 95.9 12/0810514:04:38 2.9 -1.0 0.3 96.3 12108/0514:04:48 2.8 -1.1 0.3 96.6 12108/0514:04:58 2.8 -1.5 0.3 96.9 1210810514:05:08 3.0 -1.2 0.3 97.3 12/0810514:05:18 2.8 -1.1 0.3 97.6 12/08/0514:05:28 2.2 -1.2 0.3 97.9 12/08/0514:05:38 2.3 -1.2 0.3 98.3 12/08/0514:05:48 2.1 

### -1.0 0.2 98.4 12/08/05 14:05:58 2.2 

### -0.9 0.3 98.6 101 ppm S02 12108/05 14:06:08 2.3 

### -0.7 0.3 98.7 Zero CO3 NOx 12108/0514:06:18 2.4 

### -0.7 0.3 98.7 12108/0514:06:28 2.6 -0.5 0.2 98.0 12/08/0514:06:38 3.0 -0.5 0.2 96.0 1210810514:06:48 2.8 -0.4 0.2 95.2 1210810514:06:58 2.9 -0.2 0.3 95.7 12/08/0514:07:08 3.0 18.3 0.3 94.2 12/08/0514:07:18 3.0 75.3 0.3 87.7 12/08/0514:07:28 2.9 116.2 0.3 76.1 12/08/0514:07:38 2.6 139.3 0.3 62.8 12/08/0514:07:48 2.3 151.9 0.3 50.7 12/08/0514:07:58 2.2 160.7 0.2 40.6 12/0810514:08:08 2.4 164.7 0.2 32.1 12/0810514:08:18 2.2 167.3 0.2 25.9 12108/0514:08:28 2.2 168.6 0.2 21.2 12/08/0514:08:38 2.3 169.8 0.2 17.8 1210810514:08:48 2.3 171.0 0.2 15.2 12108/0514:08:58 2.2 172.3 0.2 12.9 12/08/0514:09:08 2.3 173.2 0.2 10.9 12108/0514:09:18 2.3 174.0 0.2 9.4 12108/0514:09:28 2.2 175.4 0.2 8.7 12/08/0514:09:38 1.9 177.4 0.2 7.8 12108/0514:09:48 1.8 179.8 0.2 6.7 1210810514:09:58 2.1 181.3 0.2 6.7 12108/0514:10:08 2.2 182.8 0.2 4.9 12/0810514:10:18 1.9 183.4 0.2 4.2 12/08/0514:10:28 1.9 183.8 0.2 3.7 12/08/0514:10:38 1.9 184.3 0.2 3.3 12108/0514:10:48 

### 2.0 184.7 0.2 2.8 12108/05 14:10:58 

### 1.7 184.9 0.2 2.3 200 ppm CO 12/08/05 14:11:08 

### 1.6 184.9 0.2 1.9 Zero vOC 12/08/0514:11:18 

### 1.7 185.2 0.2 1.8 12/08/0514:11:28 1.9 182.4 0.1 1.3 12/08/0514:11:38 2.1 182.4 0.1 0.9 1210810514:11:48 49.7 184.1 0.1 0.6 1210810514:11:58 89.7 178.5 0.1 0.7 12/08/0514:12:08 90.5 152.9 0.2 1.0 12/08J0514:12:18 

### 90.7 103.7 0.2 1.3 12/08/05 14:12:28 

### 90.7 62.0 0.2 1.4 89.2 ppm C3H8 1210810514:12:38 

### 90.7 38.5 0.2 1.2 12/0810514:12:48 

### 90.5 26.9 0.2 1.0 12/08/0514:12:58 90.3 18.5 0.2 0.6 12/08/0514:13:08 90.2 13.1 0.2 0.4



# 1.72

Page 71218/05 Run #3

DatefTime VOC CO NOx S02 mmrddlyy 

### hh:mm:ss ppm ppm ppm ppm 12108/0514:19:48 127.9 153.2 26.4 78.0 12108/0514:19:58 128.1 153.4 26.3 77.3

Start Run #3 12/0810514:20:08 128.1 153.6 26.3 76.5 12/0810514:20:18 128.0 153.8 26.3 75.8 12/08I0514:20:28 128.4 154.1 26.3 75.2 1210810514:20:38 125.7 154.8 26.2 74.6 12108/0514:20:48 126.7 154.9 26.3 74.2 12108/0514:20:58 127.4 155.0 26.3 74.0 1210810514:21:08 127.0 154.9 26.2 73.8 12108/0514:21:18 127.9 154.9 26.2 73.7 12/08/0514:21:28 127.3 155.2 26.2 73.7 12108/0514:21:38 127.0 155.3 26.1 73.8 12108/0514:21:48 125.1 155.3 26.2 74.0 12/08/0514:21:58 124.8 155.2 26.3 74.2 12/0810514:22:08 124.4 155.0 26.3 74.3 1210810514:22:18 124.7 154.8 26.3 74.3 1210810514:22:28 124.6 154.8 26.3 74.3 12108106 1 4:22:38 123.9 154.9 26.3 74.4 1210810514:22:48 124.4 154.7 26.3 74.6 1210810514:22:58 124.8 154.6 26.3 74.8 1 2108/05 1 4:23:08 124.0 154.8 26.4 74.8 12108/0514:23:18 124.5 154.9 26.5 74.7 1210810514:23:28 124.3 155.0 26.7 74.6 1210810514:23:38 124.6 154.7 26.7 73.9 1210810514:23:48 124.4 154.3 26.8 72.6 12108/0514:23:58 123.5 153.8 26.8 71.0 1210810514:24:08 124.0 153.8 26.7 69.5 12108105 14:24:1 8 123.4 153.8 26.7 67.7 1 2108105 1 4:24:28 123.3 153.3 26.8 65.8 12/0810514:24:38 122.4 153.6 26.8 64.3 12108/0514:24:48 123.3 153.3 26.8 63.0 12108l0514:24:58 123.4 153.2 26.8 62.0 1210810514:25:08 122.6 153.0 26.7 61.3 12108/0514:25:18 123.2 153.2 26.6 60.7 12108/0514:25:28 123.0 153.6 26.9 60.3 12108/0514:25:38 122.5 153.9 27.9 59.9 12l0810514:25:48 122.9 154.4 28.4 59.1 12108/0514:25:58 122.7 154.9 28.6 58.2 12108/0514:26:08 123.0 154.8 28.3 57.1 12l0810514:26:18 122.9 155.2 28.0 55.6 12/0810514:26:28 123.3 155.8 27.7 54.1 1210810514:26:38 124.0 156.2 27.4 53.1 1210810514:26:48 124.6 156.3 27.3 52.6 12/0810514:26:58 124.4 156.6 27.1 52.3 12/0810514:27:08 123.9 156.8 27.1 52.2 12108J0514:27:18 124.6 156.7 27.0 52.3 1210810514:27:28 124.5 156.2 27.1 52.6 12/0810514:27:38 125.2 158.2 27.0 52.8 12/08l0514:27:48 125.0 156.0 26.9 53.0 1210810514:27:58 125.2 155.6 26.8 53.3 12/0810514:28:08 123.6 155.0 28.7 53.7 1210810514:28:18 123.7 154.7 26.6 53.9 12/08l0514:28:28 126.0 154.4 26.6 54.1 1210810514:28:38 125.0 153.6 26.5 54.1 12J0810514:28:48 124.5 153.1 26.5 54.2 12/08/0514:28:58 124.5 153.2 26.4 54.2 12108/0514:29:08 125.4 153.1 26.5 54.4 1210810514:29:18 124.8 152.7 26.5 54.6 12108105 14:29:28 124.9 152.5 26.4 54.7 12108/0514:29:38 124.6 152.2 26.4 55.0 1210810514:29:48 125.3 152.4 26.4 55.2 12108/0514:29:58 123.3 152.4 26.4 66.4 12108/0514:30:08 122.8 152.8 26.4 55.7 12108l0514:30:18 122.5 153.3 26.4 55.8 12J08/0514:30:28 121.5 153.7 26.5 55.8 1210810514:30:38 120.9 154.1 26.4 56.1 12108/0514:30:48 121.0 154.6 26.5 56.2 12108/0514:30:58 121.0 155.0 26.8 56.4 12108/0514:31:08 120.6 155.1 26.6 56.8 1210810514:31:18 120.8 155.1 26.7 57.1 

# 1.?3
Page 11218/05 Run #3

12/08/0514:31:28 121.4 154.8 26.6 57.7 1210810514:31:38 121.1 154.3 26.5 58.0 12/08/0514:31:48 120.4 154.0 26.5 58.5 12/08/0514:31:58 120.7 153.9 26.5 58.9 12/08/0514:32:08 125.1 155.2 26.6 59.3 12108/0514:32:18 138.6 158.6 27.6 60.6 12/08/0514:32:28 140.0 158.8 27.6 61.8 12108/0514:32:38 140.0 159.5 27.5 62.2 12108/0514:32:48 140.0 160.3 27.5 63.2 12/08/0514:32:58 138.5 161.1 27.4 65.4 12/0810514:33:08 139.0 161.9 27.4 67.9 12/0810514:33:18 138.8 162.3 27.4 69.7 12/08/0514:33:28 140.0 162.1 27.6 70.8 12108/0514:33:38 140.1 161.8 27.8 71.6 12/08/0514:33:48 125.4 161.5 27.9 72.6 12108/0514:33:58 129.6 160.8 27.9 73.1 12/08/0514:34:08 136.5 160.0 27.9 74.4 12/08/0514:34:18 137.8 159.5 27.8 77.0 1210810514:34:28 136.9 158.8 27.7 78.2 12/08/0514:34:38 136.3 158.6 27.5 77.6 1210810514:34:48 136.6 158.4 27.4 76.2 12/08/0514:34:58 136.2 158.1 27.4 74.9 12/0810514:35:08 137.5 158.0 27.4 73.8 12108/0514:35:18 136.6 158.1 27.3 72.9 1210810514:35:28 138.0 158.5 27.4 72.4 12/0810514:35:38 138.1 158.5 27.4 71.9 12/08/0514:35:48 139.0 158.5 27.4 71.6 12108/0514:35:58 138.4 158.8 27.5 71.3 12/08/0514:36:08 138.6 159.0 27.5 71.2 12/08/0514:36:18 138.3 158.8 27.6 71.2 12/08/0514:36:28 138.8 158.7 27.6 71.4 12/08/0514:36:38 138.4 158.5 27.7 71.7 12108/0514:36:48 137.4 158.1 27.7 71.8 12/0810514:36:58 138.4 157.7 27.6 71.9 12/08/0514:37:08 138.1 157.2 27.6 72.0 1210810514:37:18 138.3 156.9 27.6 72.1 1210810514:37:28 138.8 156.6 27.6 72.2 1210810514:37:38 139.1 156.6 27.4 72.4 12/08/0514:37:48 138.5 157.3 27.4 72.3 1210810514:37:58 138.9 157.7 27.4 72.4 12108/0514:38:08 138.6 158.2 27.4 72.5 12/0810514:38:18 138.3 158.8 27.5 72.5 12/08/0514:38:28 139.1 159.1 27.4 72.5 12108/0514:38:38 139.0 159.6 27.5 72.7 12/08/0514:38:48 138.5 160.2 27.5 72.9 12/08/0514:38:58 138.1 160.5 27.5 73.2 12/08/0514:39:08 139.0 160.7 27.6 73.6 12108/0514:39:18 138.6 160.7 27.6 73.8 1 2108/05 1 4:39:28 137.4 160.4 27.6 74.1 1210810514:39:38 136.0 160.5 27.5 74.3 12/08/0514:39:48 1352 160.7 27.5 74.0 12/08/0514:39:58 136.3 160.6 27.4 73.8 1 2/08105 1 4:40:08 135.9 160.2 27.6 73.5 1210810514:40:18 135.9 160.2 27.5 73.4 12/08/0514:40:28 135.1 160.0 27.5 73.1 12/08/0514:40:38 134.8 159.9 27.5 72.9 12108/0514:40:48 136.6 159.6 27.5 72.7 12108/0514:40:68 136.2 160.0 27.4 72.6 1210810514:41:08 136.2 160.4 27.4 72.6 12108/0514:41:18 136.0 161.1 27.3 72.6 12/0810514:41:28 136.7 161.4 27.4 72.5 12/0810514:41:38 135.8 161.9 27.4 72.5 12/08/0514:41:48 136.4 162.0 27.5 72.6 12/08/0514:41:58 137.0 161.8 27.6 72.6 12/08/0514:42:08 137.6 161.8 27.5 72.5 12/0810514:42:18 137.6 161.5 27.5 72.5 12108/0514:42:28 137.1 161.6 27.6 72.5 12/08/0514:42:38 137.6 161.6 27.5 72.5 12/08/0514:42:48 137.1 161.7 27.6 72.5 12108/0514:42:58 137.2 162.2 27.7 72.6 1210810514:43:08 136.8 162.1 27.6 72.7 12/08/0514:43:18 137.3 162.1 27.7 72.8 12108/0514:43:28 138.0 162.3 27.6 72.9 12/08/0514:43:38 138.6 162.2 27.6 73.0

Page 2 

# I?.. ~1218105 Run #3

12/08/0514:43:48 138.9 162.1 27.6 73.0 12108/0514:43:58 139.2 162.1 27.6 73.1 12/0810514:44:08 138.2 162.0 27.6 73.2 12/0810514:44:18 138.7 161.6 27.7 73.2 12/08/0514:44:28 138.9 161.6 27.8 73.4 12108/0514:44:38 138.4 161.6 27.8 73.4 12/0810514:44:48 138.3 161.7 27.7 73.5 12108/0514:44:58 138.5 161.6 27.7 73.6 1210810514:45:08 138.6 161.5 27.6 73.7 12108/0514:45:18 139.0 161.3 27.6 73.7 12/0810514:45:28 139.0 161.1 27.6 73.8 12/0810514:45:38 139.3 160.3 27.6 73.9 12J0810514:45:48 138.9 160.0 27.6 74.1 12108/0514:45:58 140.1 160.1 27.7 74.2 12/08/0514:46:08 140.6 160.1 27.8 74.3 12J0810514:46:18 139.5 160.0 27.8 74.7 12/08/0514:46:28 138.9 160.2 27.9 75.0 12/08/0514:46:38 138.8 159.3 27.9 75.3 12/0810514:46:48 138.7 158.6 27.9 75.6 12/0810514:46:58 139.2 158.3 27.8 75.7 12/0810514:47:08 139.1 158.2 27.8 75.8 12/08/0514:47:18 139.6 158.0 27.7 75.8 1210810514:47:28 138.6 157.8 27.6 76.0 1210810514:47:38 138.8 157.8 27.5 76.1 12108/0514:47:48 139.9 158.2 27.5 76.3 12108/0514:47:58 140.0 158.5 27.5 76.5 12J08/05 14:48:08 139.7 158.8 27.6 76.8 1210810514:48:18 139.3 159.1 27.6 77.0 12/08/0514:48:28 139.2 159.6 27.7 77.2 1 2108/05 1 4:48:38 139.6 160.0 27.6 77.3 12/08/0514:48:48 137.6 160.2 27.7 77.5 12/0810514:48:58 136.7 160.5 27.6 77.8 12108/0514:49:08 136.7 160.5 27.6 78.0 12/08/0514:49:18 136.9 160.3 27.6 78.2 12/08/0514:49:28 136.3 160.1 27.6 78.2 12/08/0514:49:38 137.0 159.8 27.7 78.4 12/0810514:49:48 137.0 159.7 27.7 78.6 1210810514:49:58 137.0 159.4 27.8 78.7 12108/0514:50:08 137.8 159.2 27.7 78.9 12108/0514:5018 137.4 159.3 27.6 78.9 12108/0514:50:28 136.8 159.7 27.6 78.9 1210810514:50:38 137.3 160.2 27.6 79.0 12108/0514:50:48 137.7 160.7 27.7 79.0 12/0810514:50:58 136.6 160.7 27.7 79.1 12/08/0514:51:08 135.3 161.0 27.7 79.1 12/08/0514:51:18 135.5 161.0 27.6 79.2 12/08/0514:51:28 135.4 160.3 27.6 79.3 12108/0514:51:38 136.4 159.7 27.5 79.2 12/08/0514:51:48 136.8 159.4 27.5 79.2 12/08/0514:51:58 136.0 159.3 27.5 79.1 12/0810514:52:08 136.0 159.1 27.4 79.2 12/0810514:52:18 136.0 159.0 27.4 79.3 12/08/0514:52:28 136.7 159.0 27.4 79.3 1210810514:52:38 137.3 159.0 27.4 79.4 12108/0514:52:48 138.0 159.2 27.5 79.3 12/08/0514:52:58 137.1 158.9 27.5 79.4 12/0810514:53:08 137.3 158.9 27.5 79.4 12/08/0514:53:18 137.5 159.1 27.5 79.4 12/08/0514:53:28 137.7 159.3 27.5 79.5 12/08/0514:53:38 137.6 159.3 27.5 79.6 12/08/0514:53:48 137.8 159.2 27.4 79.7 12/08/0514:53:58 138.5 159.0 27.3 79.6 1210810514:54:08 138.2 158.8 27.3 79.6 12/0810514:54:18 139.0 158.9 27.2 79.6 12/08/0514:54:28 137.9 159.2 27.1 79.6 12108/0514:54:38 138.3 159.6 27.2 79.6 12/08/0514:54:48 139.0 159.9 27.3 79.6 12/0810514:54:58 139.4 159.6 27.2 79.6 12/08/0514:55:08 138.3 160.0 27.3 79.6 12/08/0514:55:18 139.2 160.2 27.3 79.6 12/08/0514:55:28 138.8 160.3 27.3 79.7 12/08/0514:55:38 138.9 160.3 27.3 79.8 12108/0514:55:48 139.0 160.4 27.3 80.1 12/08/0514:55:58 138.9 160.5 27.3 80.1 

# 12 V Page 312/8105 Run #3

12/08/0514:56:08 138.8 160.4 

### 27.3 80.3 12J0810514:56:18 138.8 160.0 27.2 80.2 12108/0514:56:28 138.6 159.7 27.1 80.3 12108/0514:56:38 138.1 159.6 27.1 80.4 12/08/0514:56:48 137.9 159.4 27.1 80.4 12/08/0514:56:58 137.3 158.9 27.2 80.5 12108/0514:57:08 136.8 158.8 27.2 80.5 12/0810514:57:18 136.5 158.7 27.2 80.6 12/08/0514:57:28 136.1 158.6 27.2 80.7 12/08/0514:57:38 137.1 158.7 27.2 80.9 12108/0514:57:48 136.1 158.7 27.3 81.1 12108/0514:57:58 136.0 158.6 27.4 81.3 12/08/0514:58:08 136.1 158.5 27.3 81.3 1210810514:58:18 136.2 158.2 27.3 81.5 12/08/0514:58:28 135.4 158.4 

### 27.2 81.4 1210810614:58:38 137.0 158.4 27.1 81.4 12/08/0514:58:48 137.1 158.3 27.1 81.4 12108/0514:58:58 137.1 158.2 27.1 81.4 1208/0514:59:08 138.7 158.4 27.1 81.4 1210810514:59:18 137.2 168.4 

### 27.2 81.5 12108/0514:59:28 136.9 159.0 

### 27.2 81.4 12108/0514:59:38 137.6 159.6 27.1 81.4 12/08/0514:59:48 138.0 159.8 27.3 81.5 12108/0514:59:58 137.8 160.2 27.3 81.5 12108/0515:00:08 138.9 159.9 27.3 81.6 12/08/0515:00:18 139.4 159.2 27.3 81.5 12l08/0515:00:28 139.5 159.0 27.2 81.5 12108/0515:00:38 140.0 159.0 

### 27.2 81.7 12108/0515:00:48 140.4 169.6 27.3 81.7 12108/0515:00:58 142.1 160.8 27.7 82.1 12l08/0515:01:08 141.2 160.8 27.6 

### 82.7 12/0810515:01:18 142.3 161.2 27.5 82.4 1210810515:01:28 141.3 160.7 27.5 81.9 12108/0515:01:38 141.5 161.4 27.7 82.0 12108/0515:01:48 139.6 159.8 27.5 81.9 12108/0515:01:58 139.9 159.5 27.3 81.0 12108/05 15:02:08 139.3 159.1 27.2 80.6 12/08/0515:02:18 139.1 157.7 27.2 80.4 12/08/0515:02:28 138.4 135.4 23.0 76.3 1210810515:02:38 138.6 132.2 22.1 72.8 1210810515:02:48 151.7 161.5 30.9 72.6 12/08/0515:02:58 137.8 156.8 27.7 80.2 12108/0515:03:08 136.9 157.1 27.6 80.5 12108/0515:03:18 136.9 157.5 27.4 80.8 12J08/0515:03:28 137.3 158.1 27.3 81.2 12108/0515:03:38 136.9 158.6 

### 27.2 81.4 12108/0515:03:48 137.9 158.8 

### 27.3 81.5 1210810515:03:58 137.5 158.7 

### 27.3 81.5 12/08/0515:04:08 135.9 158.7 27.4 81.6 12108/0515:04:18 136.1 158.7 27.2 81.6 12108/0515:04:28 136.2 158.2 27.2 81.5 12/08/0515:04:38 136.4 158.3 27.0 81.4 12/0810515:04:48 136.3 158.3 27.0 81.3 12108/0515:04:58 134.5 158.2 27.0 81.2 12/0810515:05:08 135.8 168.2 26.9 81.2 12/08/0515:05:18 136.5 159.0 26.9 81.2 12108105 1 5:05:28 137.3 159.4 27.4 82.2 12108/0515:05:38 135.9 158.3 26.8 82.3 12/08/0515:05:48 135.9 158.6 26.8 81.6 12108/05 15:05:58 135.3 158.7 26.8 81.4 12/08/0515:06:08 135.7 158.6 26.9 81.6 12/0810515:06:18 114.3 154.1 26.3 81.4 12108/0515:06:28 107.4 154.2 25.4 79.0 12/08/0515:06:38 109.3 154.5 25.7 78.6 12/0810515:06:48 109.9 154.6 25.4 78.9 12/08/0515:06:58 110.9 155.2 25.2 79.1 1210810515:07:08 110.2 155.4 25.5 79.4 12108/0515:07:18 110.7 155.3 25.5 80.2 12108/0515:07:28 110.5 155.3 25.5 81.0 12/08/0515:07:38 111.0 155.1 25.5 81.5 12/0810515:07:48 110.4 154.8 25.4 81.7 12108/0515:07:58 111.3 154.7 25.3 82.0 12/08/0515:08:08 112.0 154.5 25.3 82.1 12/08/0515:08:18 112.0 154.6 25.3 82.3

Pags 41218J05 Run #3

12/0810515:08:28 111.6 154.6 26.2 82.3 12/0810515:08:38 112.0 154.5 25.3 82.2 12108/0515:08:48 112.5 154.5 25.3 82.3 12/0810515:08:58 111.8 154.6 25.4 82.2 12/0810515:09:08 113.4 154.5 25.5 82.2 1210810515:09:18 113.5 154.2 25.5 82.2 1210810515:09:28 113.1 154.3 25.6 82.2 12108/0515:09:38 113.3 154.3 25.6 82.3 12/0810515:09:48 113.3 154.0 25.7 82.4 12/0810515:09:58 112.7 1541 25.6 82.4 12108/0515:10:08 112.6 154.0 26.7 82.3 12108105 15:10:18 112.9 153.5 25.7 82.3 12108/0515:10:28 112.8 153.2 25.7 82.3 12/08/051510:38 112.5 153.1 25.7 82.4 12108/0515:10:48 112.9 153.2 25.7 82.3 12/08/0515:10:58 112.5 153.1 25.8 82.3 1210810515:11:08 113.1 153.3 25.8 82.3 1210810515:11:18 113.2 153.7 25.7 82.3 12/08/0515:11:28 112.6 153.9 25.7 82.2 12108/0515:11:38 111.5 154.2 25.7 82.1 1210810515:11:48 111.5 154.6 25.7 82.1 1210810515:11:58 111.3 155.2 25.7 82,0 12108/0515:12:08 111.0 155.7 25.7 81.9 12/08/0515:12:18 109.9 156.3 25.9 82.0 12/08/0515:12:28 110.3 156.7 26.0 82.1 12108/0515:12:38 109.7 156.5 26.0 82.0 12/08/0515:12:48 110.0 156.3 26.0 82.0 1210810515:12:58 109.8 156.1 25.9 81.9 12/08/0515:13:08 110.2 155.6 25.9 81.7 12108/0515:13:18 108.9 155.7 25.9 81.6 1210810515:13:28 108.8 155.6 26.0 81.5 12/08/0515:13:38 108.8 155.6 25.9 81.4 12108J0515:13:48 109.3 156.1 26.0 81.3 12/08/0515:13:58 109.4 156.3 25.9 81.3 12/0810515:14:08 110.1 156.3 25.9 81.2 12/08/0515:14:18 109.2 156.4 25.9 81.2 12/08/05 15:14:28 109.6 156.5 25.9 81.2 1210810515:14:38 109.1 156.7 25.8 61.1 12/08/0515:14:48 109.1 156.8 25.9 81.1 12/08/0515:14:58 108.4 156.4 26.0 81.2 12/0810515:15:08 109.9 155.9 26.0 81.3 12/0810515:15:18 109.4 155.6 26.0 81.2 12/08/0515:15:28 109.9 155.7 26.0 81.2 12/08/05 1 b:15:38 110.4 155.8 26.0 81.2 12108/0515:15:48 110.1 155.6 26.0 81.2 12/08/05 15:15:58 111.3 155.2 26.0 B i. 2 12/08/0515:16:08 110.9 154.9 26.1 81.3 12108/0515:16:18 109.2 154.5 26.0 81.2 12108/0515:16:28 110.3 154.6 26.1 81.2 1210810515:16:38 110.6 154.1 26.0 81.2 1210810515:16:48 111.5 153.6 26.0 81.1 1210810515:16:58 111.6 153.0 26.0 811 12/0810515:17:08 112.2 152.4 26.1 81.1 1210810515:17:18 111.9 151.9 26.1 81.1 12/08/0515:17:28 112.0 151.4 26.1 81.0 12108/0515:17:38 111.6 151.2 26.1 81.3 12/08/0515:17:48 111.7 151.0 26.0 81.3 12108/0515:17:58 112.2 151.0 26.0 81.3 12/08/0515:18:08 112.7 151.4 26.0 81.2 12108/0515:18:18 112.3 151.6 26.0 81.4 12/0810515:18:28 112.6 151.9 26.0 81.4 12108/0515:18:38 112.6 151.8 26.1 81.3 12/08/0515:18:48 113.9 151.9 26.0 81.5 1210810515:18:58 113.0 152.4 26.0 81.6 12/0810515:19:08 111.8 152.6 26.0 81.8 12/08/0515:19:18 112.4 152.7 25.9 81.8 12/08/0515:19:28 112.7 152.5 25.9 81.8 12/0810515:19:38 112.2 152.1 25.9 82.0 12/0810515:19:48 111.9 151.9 25.9 82.2 12108105 1 5:19:58 113.0 151.9 25.9 82.1 12108/0515:20:08 112.6 152.2 25.9 82.1 12108105 1 5:20:18 112.7 152.6 25.9 82.3 12108/0515:20:28 111.7 153.1 .26.0 82.6 12108/0515:20:38 112.0 163.3 25.9 82.6 

# 1. ~ Page 51218/05 Run #3

12108/0515:20:48 110.8 153.6 26.0 82.6 12108/0515:20:58 111.1 153.8 26.0 82.6 12i08/0515:21:08 109.7 153.9 25.9 82.6 12/08/0515:21:18 109.0 153.5 26.0 82.5 12/08/0515:21:28 108.2 153.1 25.9 82.6 12108/0515:21:38 110.1 152.6 26.0 82.5 12108/0515:21:48 109.6 151.4 26.0 82.4 12/08/0515:21:58 109.8 150.0 26.1 82.2
Stop Run #3 128.32 157.05 26.87 75.17

1210810515:22:08 109.7 148.7 26.1 82.2 12/08/0515:22:18 109.7 147.2 26.1 82.3 12/0810515:22:28 109.7 145.7 26.1 82.3 12J0810515:22:38 97.6 144.1 26.1 82.2 12/08/0515:22:48 10.4 140.0 25.2 81.4 12/08/0515:22:58 5.4 136.1 24.5 79.4 12/08/0515:23:08 5.3 114.6 23.0 77.3 12J08/0515:23:18 

### 4.6 80.6 17.3 71.3 12/08/0515:23:28 4.4 51.4 11.6 61.4 1210810515:23:38 4.1 31.5 7.7 50.1 12108/0515:23:48 3.1 19.6 5.4 39.8 1210810515:23:58 2.3 13.8 4.1 31.2 12108/0515:24:08 2.2 9.6 3.7 24.0 12/08/0515:24:18 1.7 6.9 7.0 18.2 12/08/0515:24:28 1.7 5.2 11.2 14.0 12108/0515:24:38 1.7 3.8 14.7 10.7 12108/0515:24:48 1.2 2.7 16.8 8.3 12108/0515:24:58 1.2 2.0 17.7 6.3 12/08105 15:25:08 1.2 1.6 18.3 4.5 12/0810515:25:18 1.3 1.0 18.5 3.0 12/08/0515:25:28 1.3 0.5 18.7 1.8 12/08/05 15:25:38 1.3 0.6 19.1 1.0 1210810515:25:48 1.4 0.6 19.2 0.5 12108/0515:25:58 1.5 0.5 19.4 0.2 12/08/0515:26:08 1.4 0.3 19.7 0.0 12108/0515:26:18 0.9 0.3 20.5 -0.4 12108/0515:26:28 0.9 0.3 21.1 -0.7 12/08/0515:26:38 1.0 0.3 21.5 -1.0 12/08/0515:26:48 0.9 0.2 21.7 -1.4 12/08/0515:26:58 1.0 0.1 21.8 -1.6 12/08/0515:27:08 0.8 0.1 21.9 -0.8 12/08/0515:27:18 0.8 0.1 

### 22.0 -0.2 12/08/05 15:27:28 0.9 0.1 

### 22.0 -0.4 25.5 ppm NOx 12/08/05 15:27:38 0.7 0.1 

### 22.0 -0.5 Zero S02 12/08/0515:27:48 0.8 0.0 

### 22.0 -0.5 12/0810515:27:58 0.8 0.0 21.9 -0.2 12/08/0515:28:08 0.8 0.0 21.9 -0.3 12108/0515:28:18 1.0 0.0 21.1 -0.4 12/08/0515:28:28 1.7 -0.1 20.9 

### -0.4 1210810515:28:38 2.6 -0.1 20.9 -0.4 12/0810515:28:48 

### 2.8 0.0 20.5 -0.5 1210810515:28:58 3.3 0.1 18.5 -0.4 12108/0515:29:08 1.1 0.6 15.4 -0.2 1210810515:29:18 0.2 1.1 9.6 0.1 1 2108105 1 5:29:28 0.2 0.7 5.4 1.6 12/0810515:29:38 0.2 0.1 

### 3.4 8.0 12/08/0515:29:48 0.2 -0.1 2.3 19.3 12108/0515:29:58 0.1 -0.4 1.5 32.8 12J0810515:30:08 0.2 -0.5 1.1 45.3 1 2108/05 1 5:30:18 0.3 -0.6 0.9 55.7 1210810515:30:28 

### 0.4 -0.5 0.7 63.8 12/08/0515:30:38 0.1 -0.5 0.6 69.9 12/08/0515:30:48 0.1 -0.7 0.6 74.4 12108/0515:30:58 0.1 -0.5 0.5 77.7 12/08/0515:31:08 0.2 -0.6 0.5 79.9 1210810515:31:18 0.2 -0.8 0.5 82.0 1 2108/05 1 5:31:28 0.2 -1.0 0.5 83.8 12/08/0515:31:38 0.2 -1.3 0.4 85.2 1210810515:31:48 0.3 -1.4 0.5 86.5 12108/0515:31:58 0.2 -1.3 0.4 87.5 12/08/0515:32:08 0.3 -1.3 0.4 87.9 12/08/0515:32:18 0.2 -1.4 0.4 88.3



# 1?V Page 61218105 Run #3

1210810515:32:28 0.2 -1.8 0.4 88.7 1210810515:32:38 0.1 -1.9 0.3 90.4 12108/0515:32:48 0.1 -2.0 0.3 92.0 12/0810515:32:58 0.1 -2.0 0.3 93.4 12/08/0515:33:08 0.0 -1.9 0.3 94.7 12/0810515:33:18 0.1 -1.9 0.3 95.1 12/08/0515:33:28 0.4 -1.4 0.2 95.5 12108/0515:33:38 0.4 -1.2 0.3 95.8 12108/0515:33:48 0.3 -1.1 0.3 96.1 12/08/0515:33:58 0.3 -1.2 0.3 96.6 12108f0515:34:08 0.1 -1.2 0.2 97.2 12108/0515:34:18 

### 0.2 -1.2 0.2 98.3 12108/05 15:34:28 0.0 -1.4 0.2 98.3 101 ppm S02 12/08/05 15:34:38 0.0 -1.2 0.2 98.5 Zero CO, NOx 12/0810515:34:48 0.1 -1.1 0.2 98.2 1210810515:34:58 0.5 -1.2 0.1 97.5 12/08/0515:35:08 0.5 -1.0 0.2 92.2 12/0810515:35:18 0.2 -0.8 0.2 89.8 12/0810515:35:28 0.3 14.7 0.2 88.0 12108/0515:35:36 0.4 74.1 0.2 81.0 12108/0515:35:48 0.8 118.7 0.2 68.3 12108/0515:35:58 0.3 142.1 0.2 54.3 12/0810515:36:08 0.4 154.6 0.2 41.5 12/0810515:36:18 0.3 160.3 0.2 31.4 12/08/0515:36:28 0.2 164.7 0.2 24.2 12/0810515:36:38 0.3 167.2 0.2 18.8 1210810515:36:48 0.2 169.1 0.1 15.2 12/0810515:36:58 0.2 170.4 0.1 12.2 12/0810515:37:08 0.1 171.5 0.2 9.9 12/0810515:37:18 0.0 172.3 0.1 8.5 1210810515:37:28 0.1 172.7 0.1 7.1 1210810518:37:38 0.2 173.4 0.1 6.1 12/0810515:37:48 0.2 174.4 0.1 5.2 12/0810515:37:58 0.3 174.7 0.1 4.5 12/0810515:38:08 0.3 175.0 0.1 3.8 12108l0515:38:18 0.4 175.6 0.1 3.2 1 2108/05 1 5:38:28 0.2 178.3 0.1 2.9 12108/0515:38:38 0.2 176.7 0.1 2.5 1 2108/05 1 5:38:48 0.2 176.9 0.1 2.1 1 2108105 1 5:38:58 0.2 177.1 0.1 1.8 1210810515:39:08 0.2 177.7 0.1 1.5 12108/0516:39:18 0.2 178.4 0.1 1.2 12108/0515:39:28 0.2 178.4 0.1 1.2 1 2/08105 1 5:39:38 0.2 178.8 0.1 0.9 12/0810515:39:48 0.2 180.0 0.1 0.6 1 2108/05 1 5:39:58 0.3 181.0 0.1 0.3 12/0810515:40:08 0.4 181.5 0.1 0.2 12108/0515:40:18 

### 0.3 181.8 0.1 0.2 12108/0515:40:28 0.0 182.2 0.0 0.2 200 ppm CO 12108/05 15:40:38 0.0 182.3 0.1 0.1 Zero VOC 12/0810515:40:48 0.0 182.0 0.0 0.1 1210810515:40:58 0.0 181.8 0.0 0.1 12/08/0515:41:08 0.0 178.9 0.0 0.0 12108105 1 5:41:18 6.2 179.1 0.0 -0.1 12108/0515:41:28 80.1 179.4 0.1 -0.2 1 2/08105 1 5:41:38 87.5 175.0 0.1 -0.2 12l0810515:41:48 90.6 146.6 0.1 -0.1 12108/0515:41:58 91.0 94.3 0.1 -0.1 12108105 15:42:08 90.8 55.6 0.1 -0.1 89.2 ppm C3H8 12/08/0515:42:18 90.8 34.7 0.1 -0.1 12108l0515:42:28 91.1 22.5 0.1 -0.1 12108/0515:42:38 91.5 15.6 0.0 -0.2

Page 7 

# j_ ? 

# ~

# Appendix C

# PARTICULATE ANALYTICAL DATA FORM
Company: Daltile, Muskogee, OK Date: 12/7/05 

# Location: Kiln Scrubber Exhaust

Run 1 

# Run 2 Run 3 

# Density (Pa)
Blank Concentration (Ca) 

# 0 d 

# t ~ 

# -2 's"; :0 

# IV6: Rinse Volume (Vaw) Residue in Rinse (Wa) = 

# Ca*Vaw*Pa 0.0009 0.0009

. 0.0009



# Date of Weighing .05;:



# Time Gross Weight A*$


# Date of Weighing bt

Time Gross Weight 0- 1; 8: ~ 9*.



# Date of Weighing V2 

# l 05'.



# Time 

# 'A Beaker Tare Weight
Date of Weighing

Time Beaker Tare Weight
Average Gross Weight 101.8792 99.7192 114.6258 

# Less Blank Residue (Wa) 0.0009 0.0009 0.0009 

# Average Beaker Tare Weight 101.8554 99.7016 114.6105 

# Weight of Particulate in Rinse (mg) 22.94 

# 16.67 14.40



# ACETONE BLANK ANALYTICAL DATA FORM

Blank Volume (Va) Date of Weighing

Time Gross Weight
Date of Weighing

Time i!; 

# Gross Weight
Average Gross Weight 106,3603 

# Date of Weighing VV



# Time Tare Weight
Date of Weighing

Time Tare Weight 1

. 

# 0 

# Average Tare Weight 106.3589


# Weight of Blank (Ma) 0.00140 

# Ca= Ma/(Va*Pa) = 

# mg/g 0.00713 

# Note: In no case should a blank residue greater than 0.01 

# mglg or 0.001% 

# of the blank lweight be subtracted from the sample weight. 

# 13 

# 2

# 1:00-0 6

V. 

# 04:

0.4104



# .00 A.

I 

# T

0.4015 0.4180



# -:0

3 

# 2 0:A 

# M:. Date of Weighing

Time Gross Filter Wt.
Date of Weighing

Time Gross Filter Wt.

Ave. Gross Filter Wt.
Date of Weighing

Time Filter Tare Wt.
Date of Weighing

Time Filter Tare Wt. FII-7ER 

# ANALITICAL DATA

Company: Dalt'le,

~ 

# vliusL.ogee, OK Date: .1200105 

# Location: Kiln Scrubber Exhaust

Run 4

Filter 

# ID Number 

# 5.M:

. Run 5 

# Run 6



# Ave. Filter Tare Wt. 0.3666

VVt. OT t-IVI On 

# riiier tgrams) U.V4.50


# Total Weight of Particulate (mg) 43.8 

# 0.3628 0.3797

0.0387 0.0384



# 38.7 38.4



# 1.3

# PARTICULATE ANALYTICAL DATA FORM

Company: Daltile, Muskogee, OK Date: 

## 12/8/05 Location: Trim Kiln Exhaust Run 

## 1 Run 2 Run 

## 3
Density (Pa) 

# 1 7$5
Blank Concentration (Ca) 

# .1 i.0.1 

# b. 07 j ( Rinse Volume (Vaw)

... 

# . ......... Residue in Rinse (Wa) 

## = Ca*Vaw*Pa 

# 0.0009 0.0009 0.0010

Date of Weighing 

# 6. 

# i. il V Time 

## :AM** -2: Gross Weight 

# 14 9-1 5.7 4. 

# '6 4
Date of Weighing 

## :: A-V.9v

Time 

# M: 31 P M: Gross Weight

Date of Weighing

Time 

## i 

## 7-,0 i 

## A- W Beaker Tare Weight
Date of Weighing

Time Beaker Tare Weight 

# 7 6 .5 .1'87
Average Gross Weight 

# 102,5745 98.6548

. 103.1606 Less Blank Residue (Wa) 

# 0.0009 0.0009

. 0.0010 Average Beaker Tare Weight 

# 102.5648 98.6449 

# 103.1486
Weight of Particulate in Rinse (mg) 

# 8.80 8.91 10.91



# ACETONE BLANK ANALYTICAL DATA FORM

Blank Volume (Va) Date of Weighing

Time Gross Weight
Date of Weighing 

## 20 

# i
~ 

# 0'5* Time Gross Weight 

# 0:
Average Gross Weight 

# 106.3603
Date of Weighing

Time 

# A-- Tare Weight
Date of Weighing

Time Tare Weight 

# :::::::!00; 80
Average Tare Weight 

# 106.3589
Weight of Blank (Ma) 

## 0.00140 Ca= Ma/(Va*Pa) 

## = mg/g 

# 0.00713
Note: In no case should a blank residue greater than 

## 0.01 mg/g or 

## 0.001% of the blank 

## lweight be subtracted from the sample weight. 

# 1~4

# FILTER ANALITICAL DATA

Company: Daltile, Muskogee, OK 

# Date: 12/8/05 

# Location: Trim Kiln Exhaust 

# Run I Run 2 Run 3

Filter ID Number 

# ti T

:



## Date of Weighing 

# AW

Time .... 2 

# O AM Gross Filter Wt. 0.: 

# 3

Date of Weighing

Time .:::; 0A6 ;: M
, Gross Filter Wt.

Ave. Gross Filter Wt. 0.3999 0.3933 0.3946
Date of Weighing 

# 0 42 0 0 

# i. Of w. : Time Filter Tare Wt.
Date of Weighing 02V -1

Time 

# OR 

# .4 2' 

# K Filter Tare Wt. 

# 0 V-.20 4 .3

Ave. Filter Tare Wt. 0.3784 0.3729 0.3746
Wt. of PM on Filter (grams) 0.0215 0.0204 0.0201
Total Weight of Particulate (mg) 21.5 20.4 20.1

# PARTICULATE ANALYTICAL DATA FORM
Company: Daltile, Muskogee, OK Date: 12/7/05 Location: Kiln Scrubber Exhaust, lmpinger Solution

Run -1 Run 2 Run 3
Densit y (Pa)
Blank Concentration (Ca) Rinse Volume (Vaw) i ii". iliii.-

~ 

## ! 

# Residue in Rinse (Wa) = Ca*Vaw*Pa 0.0012 0.0012 0.0012



# Date of Weighing

Time Gross Weight
Date of Weighing 06!

Time Gross Weight

Date of Weighing 

# 1 0

. 0

Time 1: AM 

# Beaker Tare Weight
Date of Weighing

Time Beaker Tare Weight O's .9 96 2.: 

# 7=lwl-w Average Gross Weight 112.7740 106.0108 103-1696 Less Blank Residue (Wa) 0.0012 0.0012 0.0012 

# Average Beaker Tare Weight 112.7694 105.9964 103.1620
Weight of Particulate in Rinse (mg) 3.40 

# 13.25 6.45



# H20 BLANK ANALYTICAL DATA FORM

Blank Volume (Va) Date of Weighing

Time i i .2-4- i A" NA. Gross Weight
Date of Weighing

Time 

# 2a Gross Weight :77': .18 7
, 6 1: 

# 12- Average Gross Weight 127.1877 Date of Weighing

Time Tare Weight
Date of Weighing

Time Tare Weight 

# Average Tare Weight 127.1867 Weight of Blank (Ma) 0.001 Ca= Ma/(Va*Pa) = g/g 4E.06 

# Note: In no case should a blank residue greater than 0.01 mg/g or 0.001% of the blank lweight be subtracted from the sample weight. 

# 1


# ~ 

# 8

# PARTICULATE ANALYTICAL DATA 

# FORM
Company: Daltile, Muskogee, OK Date: 12/7/05 Location: Kiln Scrubber Exhaust MeCL Rinse

Run 1 Run 2 Run 3
Density (Pa)
Blank Concentration (Ca) 

# 5. 4 Rinse Volume (Vaw) Residue in Rinse (Wa) = Ca*Vaw*Pa 0.0007

. 0.0006 0.0007



# Date of Weighing 

# 0 dd

Time X- AM 

# Gross Weight
Date of Weighing T Ydi Time 01 P. 

# Gross Weight .5



# Date of Weighing

Time AM 

# Beaker Tare Weight .1. W'; -3 0.4 

# 0


# Date of Weighing 0 5:



# Time .0 '3i 

# 7 41 

# '': Beaker Tare Weight 74 

# Average Gross Weight 109.4593 109.3047 105.5283 

# Less Blank Residue (Wa) 0.0007 0.0006 0.0007 

# Average Beaker Tare Weight 109.4576 109.3039 105.5259


# Weight of Particulate in Rinse (mg) 1.08 0.13 1.75



# METHYLENE 

# CHLORIDE BLANK ANALYTICAL DATA 

# FORM

Blank Volume (Va) Date of Weighing

Time Gross Weight 

# -7 1!
Date of Weighing

Time Gross Weight
Average Gross Weight 109.08705 

# Date of Weighing

Time 7 A 

# Tare Weight ---- -- ------- 

# Date of Weighing

Time 3 2. 

# 5 F.. M: 

# Tare Weight
Average Tare Weight 109.08625 

# Weight of Blank (Ma) 0.0008 

# Ca= Ma/(Va*Pa) = g/g 2.353E•06 

# Note: In no case should a blank residue greater than 0.01 mg/g or 0.001% of the blank [weight be subtracted from the sample weight. 

# I 

# ~ 

# 'q

# PARTICULATE ANALYTICAL DATA FORM
Company: Daltile, Muskogee, OK Date: 12/8/05 

# Location: Trim Kiln Exhaust, lmpinger Solution

Run 1 

# Run 2 Run 3 

# Density (Pa)
Blank Concentration (Ca) 

# 05 Rinse Volume (Vaw) Residue in Rinse (Wa) = 

# Ca*Vaw*Pa 0.0012 0.0012 0.0012



# Date of Weighing 0

--- --- ---- -



# Time Gross Weight
Date of Weighing

Time Gross Weight

Date of Weighing 2.



# Time j 

# Beaker Tare Weight 1 (Y Zia 

# a 0 

# Date of Weighing .5:



# Time Beaker Tare Weight 

# 2 6:00 

# a; .1 8


# Average Gross Weight 130.2595 127.3868 126.8213 

# Less Blank Residue (Wa) 0.0012 0.0012 0.0012 

# Average Beaker Tare Weight 130.2334 

# 127.3624 126.8004


# Weight of Particulate in Rinse (mg) 24.85 

# 23.20 19.70



# H20 BLANK ANALYTICAL DATA FORM

Blank Volume (Va) Date of Weighing

Time :7i.MNANA ~ 

# Gross Weight 1 2 7; .18 .7 1; 8:: 

# Date of Weighing

Time Gross Weight
Average Gross Weight 127.1877


# Date of Weighing

Time Tare Weight
Date of Weighing

Time

...... 

# 2;5 

# Tare Weight
Average Tare Weight 127.1867


# Weight of Blank (Ma) 0.001 

# Ca= Ma/(Va*Pa) = g/g 4E•06


# Note: In no case should a blank residue greater than 0.01 

# mg/g or 0.001% 

# of the blank l weight be subtracted from the sample weight. I 

# 140

# PARTICULATE ANALYTICAL DATA FORM

Company: Daltile, Muskogee, OK Date: 

## 12/8/05 Location: Trim Kiln Exhaust MeCL Rinse Run 

## 1 Run 2 Run 

## 3 Density (Pa) 

# ji 

# ji. - .3
Blank Concentration (Ca) Rinse Volume (Vaw)

...... 

# m s7

....... 

## Residue in Rinse (Wa) 

## = Ca*Vaw*Pa 

# 0.0006 0.0007 0,0008

Date of Weighing

Time 

# A 

# .7

~ 

# or: AM! Gross Weight
Date of Weighing

. 

## 4D ' Time Gross Weight

Date of Weighing

Time Beaker Tare Weight
Date of Weighing

Time Beaker Tare Weight
Average Gross Weight 

# 98.4930 106.2810 96.2500 Less Blank Residue (Wa) 

# 0.0006 0.0007 0.0008 Average Beaker Tare Weight 

# 98.4909 106.2791 96.2488 Weight of Particulate in Rinse (mg) 

# 1.48 1.21 0.49



# METHYLENE CHLORIDE BLANK ANALYTICAL DATA FORM

Blank Volume (Va) Date of Weighing

Time 

# t A Gross Weight
Date of Weighing

Time Gross Weight
Average Gross Weight 

# 109.08705
Date of Weighing

Time .2 

## A Tare Weight
Date of Weighing

Time Tare Weight
Average Tare Weight 

# 109.08625
Weight of Blank (Ma) 

# 0.0008 Ca= Ma/(Va*Pa) 

## = g/g 

# 2.353E•06
Note: In no case should a blank residue greater than 

## 0.01 mg/g or 

## 0.001% of the blank 

# lweight be subtracted from the sample weight. 

# 141

# Sheetl



# Summary of HF, HCI, 

# and Cl- 

# Analysis

Plant: Daltile, Muskogee, OK

- 

# Location: ITrim Kiln Exhaust Da r te: - 12/8/051



# R6'n - Imp # 

# IVolume Milution I FI-, ug/mi HF, mg I 1 1 & 

# 2 300: 

# 20 11.721 

# 74.04696 15.17; 93.56856 

# 1 1 & 

# 2 1 300 

# 201 11.421 72.15156 

# 14.911 91.96488 

# Average

-- j L 73.09926 ;



# 211 &2 1



# -- 300 -i 10' 20.151 63.653851 28.961 89. 31264 96.62172 

# 21 1 1 & 

# 2 300 

# i 10 , 

# 21.381 67.53942' 31.331 

# Average 1 

# 65.59664 92.96718



# ~ __ 300 10 

# 21.14! 66.781261 26.63 3001 

# io 20.83 65.80197 28.88

1 

# Average 66.29162 

# L 82.12692 

# 89.06592 85-59642

- 

# ku ,- n , # jImp# Volume Dilution Cl-, 

# ugimi C12, 

# mg 113 & 

# 4 3001 1, 1.59 

# 0.477 113 

# & 

# 4 300 j

v 

# 1 1.59 0.477 1 0.4771

213 & 

# 4 300 1 2.951 

# 2'3 & 

# 4 300 1 

# 0.894 895

313 & 

# 4 30

. 

# 11 1 

# 1.11! 0.333 

# 1.21

- ~ 

# 4 300 

# 0.3465



# 142

Page 1

# Sheetl



# Summary of HF, HCI, and 

# Cl- 

# Analysis

Plant: iDaltile, Muskogee, OK 

# Loca

— Uon: Kiln Scrubber Exhaust 

# ba te '- -- --:- 12/7/05 1

, '



# Run # 

# Lrpp 

# ~ Fl-, u /ml HF, mg 

# ug/mi 'HCI, 

# mg luDilution 

# 9 5001 '&6 1

~ 

# 1 

# &2 1 0.43 

# Lq.2

~ 

# 636 ~ 

# 1.69 0.86 6 111 &2 

# 500 1 0.4 

# 0.2106 1 1.69 0.86866 Average 

# 4 0.218498 

# 1 0.86866 r.


# 2'1 

# & 2 

# 500 1 0.70551 0.742365 1 0.7239381 

# 1.34 0.68876 0.69647 

# 1

. 

# 34 2 

# 1 &2 

# 5001 1 ; 1.411 Average



# 3'11 &2 

# 500 0.44 

# 0.23166

~ 

# ___ J.28 

# ~ 0.65792 311 

# &2 500 1 0.481 

# 0.252721 1. 

# 2

- 1

--- 

# 0.6168 

# Average 0.242191 0.63736

Run 

# # 

# Imp# Volume Dilution iCl-, ug/mi ~ 

# C12, mg 113 & 4 

# 250! 1 0 

# ; 1 F3

— & - 4 — 

# 250 F 

# 1 0 0' 0!



# 2 

# 3 & 4 

# —.-...--.- 250 1 0 1 oi 2 

# 3 & 4 

# 250 

# 1 O

3j3&4 

# 250 11 

# 01 3i3&4 

# j 250 11 0 

# oi



# 1.44 Page 

# 1

# Sheetl



# Summary of HF, HCI, 

# and Cl- 

# Analysis --

F~I

- a 

# n"t

- : Daltil , 

# Muskogee, OK Location: ITrim Kiln Exhaust ba -*t-e--:'-.----1 12/8/0§1-.--



# Run # 

# Imp# 

# Volume 11311utlon I 

# HF, mg cl im 

# 9

- 

# f T - 11.72! 3 1 1 

# &2 1 3001 15.17 46.78428 

# 11 &2 3001 

# 11.42; 36.075781 

# 14.91 j 

# 45.98244

- 1 

# - 0 - L lAverage 36.54963' 46.38336

10 20.15 63.65385 28.96 

# 89.31264 

# 211 & 

# 2 300 

# 211 &2 00 10~ 

# 21.38 67.539
- 4
- 2 31 33 

# 96.62172 

# Average 65.59664 92.96718



# 31 1 

# & 2 -1 66.78126 26.63 82.12692

1 

# 21.141_ 311 & 

# 2 3001 

# 10 20.831 65.80197'
- 2
- 8.88 

# Average 6

~ 

# 6.29162 85,5964 ~



# Run # 

# Amp # 

# Volume Dilution ;CI-, ug/mi C12, 

# mg 113 & 

# 4 3001 1 

# 1.59 0.477 

# 1'3 & 

# 4 3001 1.59 0.477

& 

# 4 300 213 & 

# 4 300 1 1 1 

# 0-477

2.95 1 

# 0.885!

O'NA, 

# 0.8895

313 & 

# 4 - 300 313 & 

# 4 ;

j 300 1 1.111 0.333 1

1 

# 1.2' 0.36L

0.3465;



# I

Page 1

# Conditions : 4_96 ug/ml F1- in H2SC34 

# = 4 _ 93 

# ug/ml. Ci- i n H2SO4 Date : 12/09/'2005 Time : 10-46=34

-102 . 4OOmV 1024 .000mV 

# Component Retention Area External

F1- 

# 1.

C1-- 

# 1. 412.24 N 

# 4.6!

287.24 H 

# 4.3{



# Component


# FlC1-

N .►



# Number Retention Area External Units

1 1.033 412.26 M 4.65 ug/ml 2 1.650 287.20 M 4.39 ug/m l

699.40 9.04

. 

# 14~

# Cond'tioiis = 4.96 ug/ml Fl- in H2SO4 4.93 ug/ml Cl- in H2SO4 Date = 12/09/2005 Time = 11:06:28

—102.4OOmV uomponent Retent

Fl- 1.



# ci- 1.6

3 1024.00OmV
0

........... ....... ... ....... .......... ............. ............ ....... ........... ... ....................... ................. . ... ......... ................ ..........



# 31 

# 21

3i

6

......... . . .......... ................ .... . .... .................. ...... ... .......................... 

## Area EXteTna I



## 426,10 4.8,

277.35 H 4.2!



# compondnt Number 

# Retention Area External Units

Fl— 1 1.016 426.10 4.82 ug/ml 

# Cl.— 2 1.633 277.35 M 4.25 tig/ml

VA 

# 703-45 9.07



# 14'7

# 102.4 .00OmV

F1-

Ci10.07

8.58 

# -102.400mV Component REten`' Rrea Er,terna]

855.80 M

586 ..44 hl 

# Conditions = 9.92 ug/ml F1- in H2SO4

= 9.86 ug/ml Cl- in H2SO4 Date : 12/09/2005 Time : 11=16-04

CQmponent Number Retention Area External Units

Fl - 1 1.016 855.80 N) 10.07 u g/m 1 C1- 2 1.650* 586.44 M 8.58 ug/ml

2 1442.24 18.65



# •

# Conditions = 9.92 ug/ml Fl- in H2SO4 9.86 ug/ml Cl- in F12SO4 Date 

# = 12/09/2005 Time 11:37:13



# -1.02..4OOmV Component Retenti

Fl- 1. 

# ci- 1.66 1024.00OmV
0

...................... .............. .......... .................. ........... ........... ......................... ......................... ......................................... ..... .................... .. .......



## 6 2[


# 3I. »... 

# I

4

6 

# Area ExteM

891.30 N 10.5

578.30 M 8.4*

Component

Fl

# c 

# i__

K Number Reten 't."Lon

1 1.033 2 1.666 Area External Units

891.30 

# m 10-50 ug/ml 

# 578.30 111 8 .47 ug/rnl

1469.60 18.97



# 149

# Conditions : 19.84 ug/ml Fl- in H2SO4 : 19-72 ug/ml Cl- in H2SO4 Date : 12/09/2005 Time : 11:58:43

Fl- 1.


# ci- 1.68 1024.00OmV

on

!, ». .«... ...«......

.............................

................... 

# 21

........



# 3

4[ — :

.

6 –102.4OOmV Component Retenti ATea ExteTna

2015.60 M 22.9

1295.24 H 18.9

. Component

Fl– 

# ci–

K Number Retention Area External Units

1 1.050 2015.60 M 22.96 ug/ml 2 1.683 .1295.24 M 18.94 ug/m1

3310.84 41.90



# 1. 5`0

# F1-



# ci1. 22.2:

18.6; 1952.35 N

1275.15 H —102 .400mV uomponent Reten ' 1024 .00OmV Area Externa Condltions : 19.84 ug/ml F1— in H2SO4



# = 19.72 ug/ml C].-- in H2SO4 Date : 12/09/2005 Time : ?2-08:11

Component Number Retention Area External Un.i.ts

F1— 1 1.050 1952,35 M 22.26 ug/ml Ca.— 2 1.fa66 1275.15 M 18.62 ug/m.l.



# 2 3227.50 40.88



# 151

## 1024.00OmV 

# mi uo LAt'01 "a



## Conditions 

# : 39-68 ug/ml Fl- in H2SO•



# : 39.44 ug/ml 

# Cl- in H2SO4 Date 

# : 12/09/2005 Time 

# : 12:17:36

-102.400m%/ Component Retent ion

. . . . ...... ...........



# ~ ' .

....... . ..............

..................... 

# 50 .......... .................. ..... 

# 2

4

6 3757.50 M 42.27

2706.60 H 41.2E 

# Fl- 1.

ci- 

# 1.7

Component Number Retention Area External Units

Fl- 

# 1 1.066 

# 3757.50 111 42.27 ug/ml 

# ci- 2 1.750 2706.60 Ivi 

# 41 .28 tjg/ml

2 6464.10 

# 83.55



# 152

## Conditions 

# : 39.68 ug/ml Fl- in H2SO4



# z 39.44 ug/ml 

# Cl- in H2SO4 Date 

# z 12/09/2005 Time 

# : 12:26:54

-102.4OOmV uomponeEt Retenti



# Fl- 

# I .

ci - 1.75 1024.00OmV



# on

............ ...... 

# i

............................... ....... ............... ...................................... . ..... . ........................ 

# . . 1

I 

# i ~~:

. ........... 

# __ ~

. . ...... . ...........

.......... ...............

.. ...........

.................. ........ ..

......................... 

# 0 ............. ............ 

# 2 1

4

5(........ " ; ~



# 6

. ................ . ..................... . ..... 

# ATea EXteTRa

. . ~



## 3763.40 M 42.31t



## 2698.10 h 41.11,



## Component Number Retention Area External' Units

Fl- 

# 1 1.066 3763.40 M 42.33 ug/ml 

# ci- 

# 2 1.750 2698.10 11 41.15 u'q/M1

2 

# 6461.50 .83.48.

# AMOUPIT IPt3ECTED

AREA 0.000 0.000



# 3760.450 39.680

i


# 2

3



# 4

5 Calibrat.ion filp = F1-.ca].

Avg slope of cur ;ia ,. 94.40 

# Y-axis intercapt: 0.00 Coef f of 1i n regr = 0.84

No . Ar ea. Amou nt CF

0: 0.000 0.000 0.000 1 : 419.200 4.960 84.516 

# 2: 873.550 9.920 88.059 3: 1983.975 19.840 99.999 4"- 37b0 .450 39.680 94.769

~ 

# V-5 4

# AMOUNT IhI.IECTED

AREA 0.000 0.000

2702.350 39.4-4n

1

2

3

m ou

5 

# Calibration file

~ 

# Cl--.cal

Avo slope of curve : 65.32 Y-ax i s i ntercept z 0 . QO - 

# Caeff of l i n regr : 0.91 1\1o . Area P.mount CF

0 : 0.000 0.000 4 K.00U 1 . 282.275 4.930 57 w257 2= 582.370 9.860 59.064 3 = 1285.195 19.720 65 . 172 4 = 2702.350 39.440 68 . 51.8

,



# . ~ 

# , r- , ~ 

# 5

## Conditions : 

## Daltile Muskogsae

: 

## Scrub Exhaust Ru n 

# It ". I nips 

# 1 'o-c 2 --eta 

## 500mle Dilution 1/1 

## Date 21/100/2005 Time 4 " 

## .,7 

# 44

-102.4OOmV component Retention - 

# 1024.00OmV 

# Area Externa



# Fl- 1.

ci- 1.75 .. .................. .......... ........ . .......... ........................ . . ..... ........ .... .......... . ................. .............................................. ........ .......... .... .................



# 21

........ 

# .~ ~

4

..................... ............ .. ............ ... ....... . .................................................... . .............................. . .......................................................... ........................................................ ... ....... ..... 

# 36.40 H 

# 0.4

96.60 N IS

Component Number Retention

Fl- 

# 1 1.066 ci- 2 

# 1.750



# 2 Area External Units

36.40 M 0.43 ug/ml 

# 96.60 M 1 .69 

# ug/ml

133.00 2.12



# 1.82

# Conditions : Daltile Muskogee : Scrub Exhaust : Run #1 Imps 1 & 2
: Volume 500m1s Dilution 1/1 Date : 12/09/2005 Time z 14:27:02

-102.400mV component Retent

Fl- 1.



# ci- 1.7 1024.00OmV
10



# . .
..................... 

# .
.... 

# .
............ 

# .
.....



# 50

3

........ 4



# .
............................................................................. 

# • Area Externa

33.64 H 0.4

96,54 1.6.

Component Number FZetention Area . External Units

Fl- 1 1.066 33.60 

# (vi 0.40 tlg/ml 

# ci- 2 1.750 96.50 1 .69 tig/ml

2 130.10 2.08



# 1 R3

# —102.400mV

Component Reten . 1024.00OmV

fI/P 1.34
1.37 .0 , 1,

1. ( unknown•) F1--
C1- Area External

32.80 113.35
78.31 H 

# Conc#itions = Dait=le Musl<ogee

= Scrubber Exhaust = Run #2 Imps 3. & 2 = Volume 500m1s Dilution 1/1 Date 

# : 12,/09/2005 Time 

# = 15=02=34



# Component Number Retention

- Area External Units
Fl-w :L 1.216 113.35 x.34• ug/rni CJ.-- 2 1.733 78.3:1 M 1.37 ug/ml

2 191.66 2.71



# 164

## Conditions = Daltile Muskogee Scrubber Exhaust Run #2 Imps 1 & 2 Volume 500m1s Dilution 1/1 Date = 12/09/2005 Time = 15:12:27

-102.4OOmV Component Reten

(unknown) 0.Fl1024.00OmV

Lion

.. .......... .......... ................. ... ......................... ....... ....... .......... ............ ............................ ........... ............. ... .. ..... ...... ............ .. ........ ............



## 216

733

3t

4



# 61

............ .......... .......... ........ . ......... ........ .................... . .. ....... ....... ......... ................................... .......... ................ .......... ....... .. ....... . .............. ....... . ....... . .................. 

## Area Externa.'

30.40 

# NIA 119.50 1.41

76.90 H 1.31

Component

Fl-

# clK Number Retention Area External Units

1 1.216 119.50 1.41 ug/m1 2 1.733 76.90 M 1.34 ug/rnl

196.40 2.76



# 165

# cond 

# (12 'k

, 

# itions 

# : Blan Date 

# : 12/09/2005 Time 

# : 15:22:07

-102.4OOmV Component. Retent



# (unknown) 2. 1024.00OmV 0



# t " I

2

3

........ 

# Area External

65.15 m N/A

61



# Component Number Retention Area External Units

Ee 0.00 0.00



# 1.

~ 

# s

# F1-



# cl- 1024 .00OmV 

# --102.40omv CompanAnt Reten .



# 1.



# I. Area Ext'erna l



# 379.44 E1 4.25

318.46 M 4,82 Conditions = 4.96 ug/m]. F 

# ~ — 

# ~ .n H2SO4



# = 4.93 

# ug/m 1 C-- i n H2504 Date = 12/10/2005 Time = 09=31-29



# Component

~ ~ 

# l 

# _ C i --

KA 

# Number Retention

1 1.050 2 1.700 

# Area External Units

379.44 M 4.25 ug/ml 318.06 m 4.82 Ug/m].



# 697.50 5.07



# 167

# Conditions = 4.96' ug/ml F1-- in H2SO4 = 4.93 uglml C 1-- i n H2504 Date = 12/10/2005 

# Time = 09-40-30

— 102 . 400mV 

# Component Retenti 0



# R.._ .. _.. ..

~ 

# .... 1024 . C

~ 

## OOmV 

# Area Externa'

F1' 1.



# Cl- 1.6 j s».



## 83 ~ 

## j.... 398.44 Ef 4.4(

288.25 M 4.4(

31 ...... : i

. . 

## ~ 

# 4I ........ ;

. 

## ~



# 5



# Gomponent Number 

# Retention Area External Units
F]. — 1 - 1. 050 398.40 M 4.48 ug/m l C1— 2 1.683 288.25 M 4.40 ug/m.l.

2 686.65 8_ 88



# 168

## Conditions 

# : 9.92 ug g /ml Fl— Jin H25O4 

# : 9.86 ug/ml 

# Cl— in H2SO4 Date ".12/10/2005 T i me 

# : 09:49:26

102.4OOmV. COMPOwt 

# Retenti



# F 

# I - 

# 1.

ci - 1.68 (unknowO 2. 1024.00OmV



# on

............ ............................. ............ . . ............................................................................ . ................................... ...................... ................ ................. 

# ~

..

...................... .........



# 3
2 1



# ~ `~ ~

;

. ~



# ..........



# ~ 

# ....... : i 4



# 6

........... .............. . ...................................................................... ............. ... .... ........... . . ............. .............. .. . ........ . . . . . ......... . ................ .. . .......... . ........... ....................... .. 

# A,r ea ExteTnal

898.75 M 

# 10 59

617.26 Pi 

# 9.01
72.30 H N/A

Component Number Retention

Fl- 1 1.050 ci- 2 1.683

2



# n 

# qRndj e

~ 

# A" g ; e -compo ot

.............

# cl3 

# ......

.............. ........... 

# :

.......................................................................... . ...............

F-1- Component Number Retention 1 1.050 2 1.683



# I Area External. Units



# 898.75 11 10.59 ug/m

' L 

# 617.26 M 

# 9.01 ug/mi



# 1516-01- 1.9.60

.H2504



# ...... .......... ...... ...... ......... .......... T02
, 4 

# :0
- 0
- um. ,

Area External Units 886.40 M 

# 3-0.44 

# Llg/Ml 6 21.5 1. M 9 .07 ug/rnl



# 1507-91 19.51 89b?40 

# N ExtjOV4



# 6 21. 

# 51 N 9.(



# 169

# Conditions : 9.92 ug/ml Fl- in H2SO4
: 9.86 

# ug/ml Cl- in H2SO4 Date : 12/10/2005 Time - 10:03':01



# -102

- .4OOmV Lomponent meEenti on 1024.00OmV Area External

Fl

# ci- 1.68 ............ . ...


# 21 .......

3

4 .......

......................... .............. . ...... .............. ................ ......... .. ..................... ............ ............ ............................. 4 i .......... I 

# ...... ...... .................... ... 886.40 M 10.44

621.51 M 9.07

Component Number Retention Area External Units

Fl- 1 1.050 886.40 11 10.44 ug/ml 

# ci- 2 1.683 621.51 11 9.07 ug/m1

2 1507.91 19.51



# 170

## Conditions

Date Time

Coraponent Reter 

# = 19.84 ug/ml Fl— %n H2SO4

= 14.72 ug/ml C1— in H2SO4 : 12/10/2005



# = 10:16=09



# 102 . 400mV

. "1- 1.

C1-

(unknown) 2. 

# 1024 .00OmV Area External

1940.75 M 22.13

1351.41 19.92

112.44 N/A

Component

Fl— 

# r- 1_

K Number Retention Area External Units

:l 1.050 1940.75 M 22.13 ug/ml 2 1.700 1357.07 19.92 ug/m].

3297.82 42.05



# 171

# Oondi,tions : 19 .S4 ug/ml F1— in H2SO4 : 19.72 ug/ml Cl-- in H2SO4 

# Date = 12/10/2005 Time : 10:27:12

--102 . 4o0mV 1024 . ooC7mV 

# Componept Retent'



# ~o~.. : 

# ...._...__ ~ 

# ..._..,....M. _...._.. ......._......_..,w.....M....._.._..........._..w...._.._..._..._.__..M. ................ ............. r.

......... ! ~
~ 

# ._.......__w ...'

1 ~ 

# .....w i :.. ......._.....

......................... ~:,~~~ 

# „• . F1- 1. I ~ +, 

# , ..... ~ 

# .......

! 1 

# 6 '_ ........

~ 

# :... ...._..:

~.:~ f 

# C1- 1.71
2 ........

~ { 

# 3 ........

4 

# 5 _ :

6 

# ...... ;

..................... ............. ..... .__.._................................. _.. ... .............. .......................................................... ...._...._....................................._.._........_M..._

~



# Cornponent Number Retention Area External Units

Fl— 1 1.066 1951.05 M 22.25 ug/m:l Cl— 2 1.716 1327.70 M 1.9 .46 ug/m l

2 3278.75 41.70 

# Area External

1951.05 M 22.25 

# , 1327,14 M 19.46



# 1'.

~ 

# 2

# Area External

3961.65 

# H 44.53

2792.20 M 42.64 124.22 M 

# N/A Conditions 

# : 39.68 ug/ml Fl- in H2SO4



# : 39.44 ug/ml 

# Cl- in H2SO4 Date 

# : 12/10/2005 Time 

# : 10:52.`46

-102.4OOmV 

# uomponenL xetOn'Ll



# Fl- 1.08

Cl- 1.78 

# (unknown) 2. 1024.00OmV

............................. . ......... .. ........... 

## 3

........................ 

# ..

................. ................ ........

................... 

# 3

............. .......... ......... 

# 21 

# ,_

~ :



# 31

.......



# 4

.......... 

# 61

......................................................................... ... ...... .. .............. . ........... . ........................................... ............... ....... ......... ............ ....... ....... . . .....................


# Component


# F I —ci

# 2 Number Retention Area External Units



# 1 1.083 3961.65 M 44.53 ug/ml 2 

# 1.783 2792.20 M 42-64 ug/ml



# 6753.85 87-16



# 173

## Conditions = 39.68 ug/ml Fl- in H2SO4 

# 39.44. ug/ml C.'l- in F[2SO4 Date 12/1012005 Time 11:01:39

-102.4OOmV 1024.00OmV uOMPOnent KeLent 

# ion

~ ,. 

# .I •w ~ i

. ...............



# so 2 . ..».. . ii

.



# 4

3



# 4

........



# 61

... .... ........................ ..... . .. . ..................................................................... ...... ................................ .... . ...................................................................... . ..............................................

Component -Number Retention Area External Units


# Fl-- 1 

# 1.066 3890-85 M 

# 4.'

- 'j ~ 

# .74 ug /I m 1 

# ci— 2 

# 1.750 2737-50 M 

# 41.77 ug/ml

2 

# 6628.35 85-51 

# Fl- 1.

ci- 1.7 

# Area External

3890.85 m 43.71 ,

2737.50 M 41.77



# 1.74

# AM4UNT INJECTEU

AREA 0.000 0.000

3926.250 39.680

i
2

3

4

~ 

# Calibration file = Fl-_oal

Avg s1oFe of curve = 96.24 Y-ax is i nteroept : 0.00 roeff of l i n regr : 0.90

No . Area Amount CF

0: 0.000 0.000 • 0. 000 1

~ 

## 388.920 4.960 78.411 2: 882.575 9.920 88.969 3: 1945 .9(30 19.840 98.080 4 = a926 .250 39.680 98.948



# 175

,

# AI"iQUNT INJECTED

AREA 0.000 0.000



# 2764.850 39.440

1
2

3

4

5 

# Calibration file : Cl-.cal

Avg slope of curve '- 67.77 Y-ax i s i ntercept : 0.00 

# Coeff of l i n regr x 0.92

hlo . Area Amount CF

0: 0.000 0.000 0.000 1 : 303.155 4.930 61.492 2: 619.385 9.860 62

~ 

# 818 3: 1342.385 19.720 68 . 07 2 4 = 2764 .850 39.440 70.103



# 176

# Conditions = Daltile Muskogee Scrubber Exhaust Run #3 

# Imps 1 & 

# 2 Volume 5001s Dilution 1/1 

# Date 12/10/2005 

# Time = 11:54:46

-102.4OOmV uomponenli, Retent



# Number Retent-ion

1 1.233 2 1.730 

# Fl- 1.2



# ci- 1.7

Component
# FlciVA 

## 1024.00OmV



# Area Extel-'nal Units



# 34.20 11 

# 0.44 ug/ml 78.85 1 .28 

# tig/ml

113-05 1.72 ~ 

# on


# ... .... . . ............................ .............. .......... ............... . ................ . ............ . ..........

33

so 

# 2

3

4 .....

5

6

... . ..... . .... . .... . ........... . ... . .......................... Area External



# 34.24 N 

# 0.44

78.85 1.2E



# i77

## Conditions : Daltile Muskogee

: Scrubber Exhaust
: Run #3 Imps I & 2
z VOlLtMe 5001s Dilution 1/1 Date : 12/10/2005 Time : 12:04:26

—102.4OOmV UOMPOnent 

## i(etent



# Fl- 

# 1.1 ci - 1.71 1024.00OmV



# .... .

............................. 

# ...... . ........................ ..... . ..... ............................. .......................... ........................... . ..........

i3l


# 6

2 

# . ..». i


# ~ AT ea External



# 38.04 H 0.4E
73.95 N 1.2(



# 61


# . . ..... ; 

# ~

............... ......... ....... ....... .......................... . ........ .. ... 

# .......... ....... ........... ... ............ .
Component
Fl— 

# ci—

rA Number Reten"E-Aon

2 1,716 

# Area Exi- -ernal Unfts

38.00 M 0.48 ug/ml 

# 73.95 M 

# 1 .20 ug/rnl

111.95 1.69

:111WK
- W, 

# LKI W,

# Conditions : 

# Daltile Muskogee
: 

# Trim Kiln

: 

# Run #1 

# Imps I & 

# 2

: 

# Volume 3001e 

# Dilution 1910 1/20 Date : 

# 12/10/2005 Time : 13:07:37



# -102.400mV COmponeflt vetenti



# Flci- 1.73 1024.00OmV
0

...... ...... ... . ... .....

............. .
.......................

.......... . ................ .



## 3 : 2

...... f 

# ,. ... _......... 

# ~

1 

# t

3



# 4

6

.. . ............ ............... . ........... ............................................................................ ........ .. 

# Area External



# 1074.99 

# M

1008.63 

# M



# . 11.72



# 15.1;

Component



# ci

# 2 Number Retention Area External Units

1 1.066 1074.99 

# M 11.72 

# ug/ml 2 1.733 1008,63 

# M 15.17 

# ug/m1

2083.62 26.88



# 179

# Conditions : Daltile

- Muskogee : Trim Kiln : Run #1 Imps 1 & 2 : Volume 3001s Dilution 12W 

# IAO Date : 12/10/2005 Time : 13:29:29

—102.4OOmV ComponeSt Retenti-on

.. 1024.00OmV ATea External

Fl- 1.


# ci- 1.71 ................



# I

........ 

# .

........... 

# .
.. .................... 

# .

...... ..........



### . I;



# 6
21

3 1

.......



# 4

................ *-............-...............-....-...-............-.-..................-........I .......... 

# .

.. 

# . . . . .

...... .. ........... ................. ................... 

# 1043.40 M .11.42

989.80 

# m 14.91

Component

FI -.

# ci2 Number Retention "Area External Units

1 1.050 1043.40*M 11.42 ug/ml 2 1.716 989.80 

# m 14.91 ug/ml

2033-20 26.33

# Conditions = Daitile Muskogee = Trim Kiln = Run #2 Imps 1 & 2 = Volume 3001s Di1ut

- iQn 1/10 Date = 12110l2005 Ti.me = 13=38=33



# --102 .400mV 1024.00OmV Component Retention Area Ezternal

F1-

Ci1.08

1.78 1976.90 H 20.1E

2008.60 M 28.4E

Riumber Retent.i-on Area External Units

1 1.083 1976.90 11 20.15 ug/rn1 2 1.783 2008.60 M .28



# . 96 ugrm 

# l

3985.50 49.11 Component

F J. -- C .l.

K



# 181

# Conditions z Daltile Muskogee : Trim Kiln : Run #2 Imps 1 & 2 : Volume 3001s Dilution 1/10 Date z 12*110/2005 Time : 13:47:22



# -102.400mV 1024.00OmV Componept Retenti 

# on

........ . ........ ........... ...... ........ .................. . ..... . . ... .... .. ..... .. .. .... ................ ......... ....... ............................. ....... . ......... .................. .



# Fl- 1.10 0

....... . ...... ....... 

# ci- 1.81 '6..... ..................

2

4



# ' :

.


# 61

........ ................. ............. ...... .. .............. .. ......... ................. .......... ...... ..... . ....... ........ . ......



# Component Number Retention Area External Units

Fl- 1 1.100 2099.50 M 21.38 ug/ml 

# cl- 2 1,-816 2.180.08 M 31.33 ug/ml

2 4279.58 52 

# .71 ATea Externa

2099.50 M 21.3

2180.08 H 31.3

# Conditions : Daltile Muskosee = Trim Kiln : Run #3 Tmps 1 & 2 = Volume 3001s Dilution 1/10 Date = 12/10/2005 Time = 13=57:56

-102 .400mV 1024,OOOmV Component Retenti4n Rrea Externa

F'1-

C1- 2076.05 M 21.1

1840.85 M 26.6

Component 

# rl- - C1- Number Retention

1 1.083 2 1.783 Area External Units

2076.05 M 21.14 ug/m 1 1840.85 M 26.63 ug/ml

2 3916.90 47.77



# IR3

# Conditions : Daltile Nluskagee 

# : Trim Kiln : Run #3 Imps 1 & 2 : Volume 3001s Dilution 1/10 Date = 12/10/2005 Time = 14:06:57

—102.400mV 1024 .040mV 

# Component Retent' i o n ................. »....«............,.«...».......................».w.«...w.....w....._.....w.......«._..«..».......».....w..w.w.....«.....»....,» .................. .......w ....... .w.w ....w..w............w...w w......w.w.»w...

,

5 0
~ 

### .w ,» ~ f •w ».w ....N.......b...Mi w.»..q..ny.w.p..w.......wr.w...n.

. ~ 

### .. w.». r..........=w ........................«.=...w.w.»..w,....



# z . ..... 

# ~
,.. , 

# ~ M • 

### .«

................. 

### .....ww.».».w.w .«. » w. ~ 

### n=n=

~ 

### =nnununnmu=m=xnnu=n=a



# _ 3~

».w. :

• ' E


# 4

. ....



### 5

..... :

~ 

## ; i • 

# 6 . w.... ;

' i



# Component Number petention Area External Units

F 1-- 1 1.066 2044.55 M 20.83 ug/m l 2 1.750 2002.81 h1 28.88 ug/m3.

2 4047 _ 36 49.70 

# F1- 1.

ci- 1.7 

# Area Externa

2444=55 Ef 20.8

2002.81 M 28.8



# 184

# Fl- 1.

Cl- 1.68

Conditions 

# : 19.84 ug/ml Fl— in H2SO4



# : 19.72 

# ug/ml Cl— 

# in H2SO4 Date 

# : 12/10/2005 Time 

# : 14:16:03

—102.4OOmV Component Retenti



# . ....... . ..... ..... ......... . ....................... .......... . ...........

............................

............. ............... ...... 

# 21

...... ~,~..



# 3



# 4

6 

# 1024.00OmV

2080.40 M 

# 21.11

1291.73 h 19.0 , 

# Area ExterRa

Component 

# Number Retention Area Exteriial Units

Fl— 

# 1 1.050 

# 2080.40 M 21.19 

# ug/ml ci- 

# 2- 1.683 1291.73 11 19.03 

# ug/ml

2 3372-13 

# 40.22



# 195

## Conditions 

# : Blank Date 

# : 12/10/2005 Time 

# - 14:32:12

—102.400mV 1024.00OmV component Ratept 

# ion

.............. ....... 

## Area ExteTna



# 2



# ...... (unknown) 

# 2.3 50 146.95 

# N 

# NIA

4



# 6!

. ... . ......... ............ ............ ....

Component Number Retention Area External Units



# 0 . 0.00 0.-00



# . Z

~ 

# s

# Conditions =4.93 ug/ml Ci— in hlaON Da.te = 12719/2005 

# Time - - 07=56=14

—~ 

## 3 .200mV 

# Component Retention

(unknown) 0.



# ci51.2 .00Omt! 

# Area Externa;

1374.55 li NIA

245.90 Pf 4.51



# Component 

# Number Retention Area External Units

C1 — 

# 2 .1 . 86b 295 .90 fvl 4.51 ug/ml

1 

# 295.90 4.51.
,

# Area f- 

# txterna

1130.00 N/A

272,00 

# M Cii 126.06 

# M N/A 

# cl

- 

# 1. (unknowR) 2.

Conditions 

# : 4.93 uo/nil 

# Cl— in NaOl-i

Date 

# : 12/19/2005 Time 

# : 07:59:45

—51.200mV Component Retent-lon



# Unknown .......... .......................... .. ......... ............... . .. ........ ...................................................................................

. ........... . ..



# 8501 ..... ....... .. .......... .........

.. ....................

$66 

# ................ 2

3



# 4

61

............... 

# 51.2.00OmV

Component Number Retention Area External Units 

# Cl— 2 

# 1.866 272.00 M 4.18 ug/ml



# I 

# 272.00 4.18



# ~ 

# WE,

## Conciitions = 9.86 ug/ml CI.— in hlaOH Date = 12/19/2005 T i. me - 08 : 03 = 09

—5.1 .200mV Oomponent Retention

(unknown) 0.8t

Cl- 1.86 512.C700m`I Area Ex'Lernal

1223.35 N/A

575.40 M 8.79

Component hiumber Retention Area Exter nal Units

Cl•- 2 1.866 575.40 M 8.79 ug/ml

1 575.40 8.79 •



# 189

# ? a6a.00 N/A



# 564.40 M 8.6 , I00.17 H N/A 

# (unknown) a,

Cl- I . 

# (unknown) 2. Co ndit ions : 9.86 Ug/ml Cl-- in NaQH

Date : 1 2!1 9l2005 

# Time = 08 - 05 = 54

—51 .200mV 

# Componen ~ 

# Re

~ 

# ention 512 .QOC7mW 

# Area Eaternc ,

Component. 

# Number Retention Area External Units

C1— 2 1.866 564.40 M 8.64 ug/mi



# i 564.40 8.64



# 190

# Conditions = 14 .79 uglrnl Cl-- i n NaOH Date = 12f 1972005 Time = 08 = C39 = 33

—51 . 200mV 5 1 2 . (3C}qmV ComponQnt Retention

(unknowl ') 0.



# ciArea Externa

1140.80 rdIA

937.40 M 15.0

Component Number Retention Area External Units Clμ- 2 1.866 937,f0 iu1 15.07 ug/ml

1 937.40 15*. 07

.. 

# 1.91

# (unknorin) O.K.

C1- 1.86 1077.50 N/A

958.00 h1 15.3t Conditi.ons = 14.79 ug/ml Cl- in NaOH Date 12/19/2005 Time = 08=12=20

—51 .200mV ComponenT Retention 512 .00OmV Area Externa

Component hlumber Retention Area External Units
Cl-- 2 1.866 958.00 fh 15.36 ug/ml

1 958.00 15.36



# 1.92

# Conditions ' 19.78 ug/ml C].-- in NaOH Qate : :i? /1.9/2005 Time = 08-16=00

--5 :L . 200 rn'J Compoaent Retention

(unknown) Q.8E



# ci- 1.86 51.2 . OOOmV Area Ezterna'.

659.10 hl/A

1246,65 M 16,6e,



# Component Number Retention Area External Units

C1-- 2 1.883 124•6 . b5 

# m 18 . 69 ug/m].

1 1246 _ 55 18.69



# 193

# Conditions = 19.78 ug/ml C].— in MaOH Date = 12/19/2005 Time - 08:21=30

—51.200mV Component Retention

; unknotiin } 0.

C1- 1, 512 .00OmV Area Externa':

844.80 N/A

1272.70 hf 19.03

Component Number Retention Area External Units

C1-- 2 1.883 1272.70 M 19.03 ug/ml

1 1272.70 19,03



# P4

# AMOUNT ZNJECTEa

AREA 0. 

# 000 0.00C



# 1259.675 19.720

1

2

3

4

5 

# Calibration file = C1-- .cal



# Avg slope of curve : 63.88 Y--ax:

~ 

# s a. ntercept = 0.00 Coeff of .L a, n r egr : 0.83
No . Area Amount CF

0: 0.000 0.000 0.000 

# 1: 283.950 4.930 57,596 2: 56 0

1.900 9.860 57.799 3 - 947.700 14.790 64.077 4= 1 259 . 6 75 19.720 63.878

,



# ~ Iq~

# Condi'tions : Da.lti le , Muskogee , OK Ki 1 n 5crubber = Run #1 ImRs 3 & 4 

# : Volume 250'Dilution 1/1 Date = 12/19/2005 

# Time : 10=15:29

. 

## ~ - 5". .2a'OmV 512.040mV 

# Campanent Retentian

(unknown) 0.8 

# Area External

682.20 N/A



# ( unknoain ) 2. ~ 

# .. ~ 

# ........_..... ~~ 

# _...... ............. ............ .................. ~.~ 

# ....._..._........_.._..... ~ 

# ..._. ~ 

# ........_............. _._. ~ 

# ................. .............................................._.............. ~



## 50 """•••• «mn..unun• 

### 1

...... . ~ 

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## 2 . ...... ; 

# ~ ,..:a,•



## 3 . ..... : 

# ~

4 

# ~

5 ; 1



# 6 . ..... ;

.

. .................................... .........................,..................... ... ........ ......... .........,............ . ..... ................... ....................... .._.... .................... .......... ......... ... ....,...........,....................,.... ~ 

# 231.74 

# NlA



# ComRonent hlumber Retention Area External Units



# , 0.00 0.00



# 2n2

# Conditions : Daltile, Muskogee, OK Kiln' Scrubber 

# = Run #1 Imps 3 & 4 = Volume 250 Dilution 1/1 Date = 12/19/2005 

# Time = 10:25:59

-.51 .200mV 

# CoMDonent 2etention



# (unknawn) 0.



# ~ unknown 

# ~ 2. unknown 2. 53.2.000mV 

# Area fxternal

523.05 h/A



# 257.00 

# NIA 362.30 

# N/A

Component Number Retention Area External Units

\ I 

# • •• 

# •wi •J



# 203

# Conditions Daltile, Muskogee, t1K Kiln Scrubber 

# = Run #2 Imps 3 & 4

~ 

# Volume 250 Dilution 1l1 Date 1211912005 Time = 10:29:55

- 

## -51 , 20QmV 

# Comaonent Retention 512.40amV Area Externa:

(unknown) 4.



# (unknown) 1. 

# (unknotan) 2. 463.45 

# N!A

233.54 

# NIA

372.60 

# NlA



# Component Number Retention Area External Units

F 0.00 0.00



# P4

# Conditions = Daltile, Muskogee, OK Kiln Scrubber = Ru n#2 Z rnps 3& 4 = Volume 250 Dilution 1/1 Date = 12/19/2005 Time = 10=34:01

--51 .20QmV 512.000mV Component Retention

(unknown} U.

( unknown ) 1. (unknown) 2.'

Component Number Retention Area External Units

101 C0 •• 

# • •• Area Externa]

470.20 N/A

234.55 NlA
379.14 NIA



# 2n5

# Conditions = Daltile, Muskogee, OK Kiln Scrubber = Run #3 Imps 3 & 4 : Vo3.ume 250 Dil.ution 1/1 Date : 12/19/2005 

# Time - 10=42=35

–51 .2.00m`J 512.00Om`J 

# component Retention

{unknown} 0.8 

# Area Externa

486.90 NlA



# (unknown) 1.95 

# (unknouxn) 2, ~ 

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# . ,

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# _.- --- ... ------

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# ...._._.. ~ 

# 254.60 NIA 

# 338.85 N/A

Component Number Retention Area External Units

or, 0.00 0.00



# • 2n6

## Conditions : Daltile,, Muskogee, OK Kiln Scrubber

: Run #3 Imps 3 & •
: Volume 250 Diluti.on 1/1 Date : 12/19/2005 Time : 10:46:29

--51.200MV Component Retent 101

.. ............
(unknown) 0. 8 

# so



# ~ unknown) 1.9 unknown) 2. 

# so

2



# 3

6

............. Area External

507.05 

# N/A

243.50 N/A 328.90 

# NIA 51.2.00OmV

Component Number Retention Area External Units

x 0 - 00 

# 0.00



# 207

# Concfitions : Daltile, Muskogee s ok: Trim Kiln 

# : Run #1 Imps 3 & 4 = Volume 300 Dilution 1r1 Date : 12/19/2005 Time : 10:55:10

—51 .200m41 

# Component Retenti

(unknown) 0.8

Cl

~ 

# - 1.7 83 

# (unknown) 2. 512. 0OJmEr

... 

# o~ ....~M........ ,~...
._.. ......_......._.._... _ _....... . _. ................. ...... .. ._.~.,......_._..._ .~._....._.._.........._..._.............. _._ .~~....__....._............_.___ ~

50 ~~. ...... ~

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~............ ........................._ ................. ..........._.............. ..... ....... ....... ..... .................. _ ...................... .. ......................... .......... ....._................................ ............. ............. ..... ........ ~

. Area EYterna:

611.40 N/A



# 91,60 M 1.5C, 424.90 N/A



# Component Mumber Retention 

# Area - External Units

C 1-- 2 1.783 91.60 M 1.59 ug/ml

0 91.60 1.59



# 208

# Conditions : Dalti 1e , Mus kogee , 04G Tr im Ki 1 n : Run #1 Imps 3 & 4 = volume

- 300 Dilution 1f1 Date = 12/19I2005 Time = 10 - 59 : 0Z

—51 w?_O0mV Conponent Reten"

(unknown) 0,

C1- 1. (unknown) 2. 512 .00OmV Area External

609.10 NrA

91.60 N 1'.5i 

# 361.34 N/A

Cojmponent Number Retention Area External Units

Ci-- 2 1.783 .91 . 50 M 

# 1.59 ug/m].

1 91.60 1.59



# 209

# Area Externa

038.24 N/A

169.95 2,9:
515.20 NlA 

# 91.50 N/A Condit ion s: Daltile , Muskogee , OK Trim Ki ln



# : Run #2 Imps 3 & 4 : Volume •300 D•ilution 1/1 Date : 12/19/2005 Time = 11:08-12

—51 .200mV 

# Component Retent'

(unknown) 4.8

C1- 1.6



# ~ unknown 

# ~ 2. 

# unkno

~ 

# an 2.3 

# 512 _400mV

ion


# __.__.._...., ..._..._._................. ~ 

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# 6



# Cornponent Number Retention Area
C]. -- 2 1.683 169.95

1 169 .95 

# External Units
2.95 ug/ml

2.95



# 210

# Conditions 

# : Daltile, Muskogee, OK Trim Kiln


# : Run #2 Imps 

# 3 & 4


# : Volume 

# 300 Dilution 

# 1/1 Date 

# : 12/19/2005 Time-- 11:12:00

Component Retention

t 

# 512. OOOmV 

# Area Externa

(unknowp) 0.



# ci- 1.70 

# (unknown) 2. 635.60 N/A

171.50 

# 2.9E


# 522.20 NIA 

# 0


# 21

. i



# ~

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# ~

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Component Number Retention Area
, External Units


# ci- 2 

# 1.700 171.50 2.98 ug/ml



# 171.50 2.98



# 211

# Concfitions = Daltile, Muskogee, OK Trim tGiln



# " - Run #3 Imps 3 & 4 = Volume 300 Qilution 1/1 Date = 12/19/2005 

# Time = 11=21=11

--5 1 . 200mv 

# Component Reter''

(unknown) b.



# (unknoain) 2. 5 9. 2. OOOm'•J 

# Area Externa

555,95 H/A

64.10 1.1 1
607.00 N/A

Component 

# Number Retention Area External Units
Cl- 2 1.700 b 4 .10 1.11 u g/ m],

1 64.10 1.11



# 2

~ 

# . 2

# camponent Keter

(unknaEFD) 0.
F'l- I.


# Cl

- 

# 1. ( un(tnown ) 2. 

# Area Externa.

449,86 N!A 152,55 1.31
69.20 M 1.2(
621.30 N/A ConcLiti.ons = Daltile, Musl

~ 

# ogee, OK Trim Kilrz

~ 

# Run #3 Imps .3 & 4 = Volume 300 Dilution 1/1 Date = 12/19/2005 Time = 11=25=02

—51 .2QOmU 512 .00OmV



# ComRonent hlumber Retenfi.ion

1 1.133 2 a. . 683 

# Area External Units

FlC1— 152.55 1.32 ug/m 1 69.20 M 1.20 ug/m 1

2 221 .75 2.52



# 213

# CQnditions = Daltile, Muskogee x OK Trim Kiln 

# = NaoH Blank Date = 12/19/2005 Time = 11 = 34 . 34

---51 , 200mV Component Reten''

{unknown} 0. 51.2 .00Omv Area Ezterna

1189.15 N/A

Component Number Retention Area External Units

.0 0.00 . 0 .00



# 214

# 512.000m.V

Conditions 

# : Daltile, Musko:gee, OK Trim Kiln



# : 4.93 ug/ml 

# Cl- in NaOH Date 

# : 12/19/2005 Time 

# z 11:37:37

-51..'200mv 

# Component. Retention



# ....... . ..... ......

(unknown) 0.8 

## 50

Y : cl- 1.8 

## 50



# 2 Ai•ea ExteTne



# 1204.20 

# N NIA



# 304.90 

# H 5.2



# 4

5 ......



# 6 

# ~ 

# . `

. . I

-- -- 

# ....... ...... 

# --~

Component Number Retention Area External Units


# ci- 2 

# 1.850 304.90 M 

# 5.29 ug/ml

1 

# 304.90 

# 5.29

1 

# 215_ y 1

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# Comnonent Concentratlon

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# estimafed uncertainties are two standard deviations of tbe:concentration Nialues. The concentration

~~ 

# alue is ti;tairanted to be stable for three,months from''the.date of shiprnent.
The preparation and analyses of the Fluoride Standard was performed urit.h eatreme care by DIO'NTEX Corrporation Consurnables Manufact•uring Department.

Dc-cu:nentNo. 034183-18 13-Dec-02

Oionex Cor aration

P Olonex U.S. Regional Otlices Oionex Intetnational Subsidiarics 

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~ lnnyvalc. CA tYCStmonl, IL

Narston, TX (630) 785-3660

(?Bl ) 847•SG52 beoum (03) 353 42 94

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# o'r the'sm "le 2on 31$2 Chlonde, Staridard Sol ho )
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,

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# Compunent Coricentration V -

{i?°(g/L) Chlonde: - 986

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The concentration value is based : on piroven reliable. methods.

~ 

# of analy.sis.

~ 

# . The 'estimated - uncertainties are two standard deviations of the concentrat'ion

~ 

# alues:: ' The concentration value is

~ 

# •.

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# warranted. •to be stable for -tlir'ee months from the date of shipment : ; The preparation and analyses of the Chloride Standard was performed with extreme -care by the ' DIONEX Corporation Consumables Manufacturing Department.

~~ 

# ' -

Documcnt No. 034184-25 20 May 1998

nex Corporatton Oionex U.S. Repional offieet b

- 1 i:an tva,v S:mny+zic, CA (408) 737-8522 9or, 3603 μh:slmont, i: (630) 769•3650 'vale, CR Houston,lX (281)017-5652 :-25G3 Ptlana • CtR (7701432'8100

7 37-0100 Martton, NJ (B.i 59r0600

Sa 3 1 Lake CAt', U7 (801)972-9292 Ofonex tntemalionat Sabsidiaries Rusfiia (01) 616 5125 Gevgmy (03126) 991-0 BelDn7m (03) 353 42 94 Nely(06) 66 515052 Canada(905)844•9650 Japwr(06)6885-1213 CAi73 f8:2) 2428 3282 Xaea(2) 2653-2580 D--murk (45) 36 36 90 90 The lk!lff&nds (0161) 43 4303 Fra.x't (01) 39 30 01 10 SWte&7d (O62) 2M 99 66 sm `\.a10 ~t'~f

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### Armstrong Environmental Inc. CONVERSION FACTORS EPA Method 5 522 Series Meter Box Callbration 1 mm Hg : 0.13330 kPa Pre-Test Orifice Method 1 cm = 0.39370 inch English Meter Box Units, English IC Factor 1 mm = 0.03937 inch 1 cu ft = 28.32 liters !r Box x 11 Date: ------------------> 10l11/05 rl #: 73 Barometric Pressure: -------»-> 29.75 (in. Hg) Theoretical Critical Vacuum: --> 14.03 (in. Hg)

11 

### )RTAt% For valid tesl resulls, the Aclual Vacuurn should be 1 to 2 in. Hg greater than ttre Theoretical Critical Vacuum shown above. )RTAA The,Critical Oririce Coefficienl, IC, must be entered in English units, (fl)"3'(deg R)"0.5/((in.Hg)"(min)). 11

DRY GAS METER READINGS - ------- -CRITICAL ORIFICE READINGS-


### - Average Temperatures -

Volume Volume Volume Initial Temps. Final Temps. Oririce IC Oririce Acival - Ambient Temperature - DGM DGM Ambient IH Time Initiai Final Total Inlel Outlat lnlet Outlet Serlal# Coefficient Vacuum Initial Final Average Outlet Overall Temp 20) (min) (cu ti) (cu fl) (cu (l) (deg F) (deg F) (deg F) (deg F) (numbar) (see above) (in Hg) (deg F) (deg F) (deg F) (deg R) (deg R) (deg R) 0.26 6.00 482.900 484.824 1.924 75.0 74.0 75.0 74.0 40 0.242 23.5 74.0 73.0 73.5 534.0 534.5 533.5 0.53 5.00 486.500 488.797 2.297 75.0 74.0 75.0 75.0 48 0.344 22.0 74.0 74.0 74.0 534.5 534.8 534.0 0.96 6.50 490.297 494.308 4.011 75.0• 75.0 76.0 75.0 55 0.464 20.0 74.0 74.0 74.0 535.0 535.3 534.0 1.55 6.50 494.700 499.812 5.112 76.0 75.0 77.0 75.0 63 0.593 18.0 74.0 74.0 74.0 535.0 535.8 534.0 3.00 10.00 500.400 511.137 10.737 77.0 75.0 79.0 75.0 73 0.824 14.5 75.0 75.0 75.0 535.0 536.5 535.0

............................................. RESUi.TS ................... . ......
..,..................... .

W GAS METER --- -------- ORIFICE ---- - DRY GAS METER - 

### ORIFICE



## JME VOLUME RECT CORRECTED n(sld) Vm(sld) (cu fl) (litors) 1.890 0.1 2.257 0.1 3.942 0.2 5.027 0.2 0.581 0.4 

## VOLUME VOLUME VOLUME CORRECT CORRECT NOMINAL Vcr(std) Vcr(sld) Vcr (cu fl) (liters) (cu fl) 1.873 0.1 1.904 2.216 0.1 2.255 3.882 02 3.950 4.966 0.2 5.053 10.596 0.4 10.802 CALIBRATION FACTOR 

## Y Value Variation (number) (number) 0.991 0.001 0.982 -0.007 0.985 -0.005 0.988 -0.001 1.001 0.012 CALIBRATION FACTOR dH@ 

### Value Variation (in H20) (in H20) 1.448 -0.0251 1.490 0.017 1.486 0.013 1.466 -0.007 1.475 0.002 

# Average Y -------> 0.989 

# 1.473 <------- Average dH@

For Calibration Faclor Y, the ratio of the reading of the calibration meter to the dry gas meter, cceptable tolerance oi individual values from lhe average is +-0.02. 

### or Orifice Calibration Factor dH@, ilra orifice differential pressure in inches of H20 ithat equates to 0.75 cfm of air 168 F and 29.92 inch



# ~f~ g, acce able tolerance of individual us from the average is +-0.2.

SIGNED: Date: f~ / ~ •~ f



### ~

.~

.~

# Temperature Nieter Caiibrations

fJeter Box #: 11 

# Date: 10/11105 

# Calibrated By: RT.

Emtech Thermo Degrees F Checker Probe Stack Oven Exit Auxiilary

Point 1 32 30 30 30 31 30

Point 2 212 211 212 211 212 211

Point 3 752 751 751 751 751 751

Emtech Thermo Degrees R Checker Probe Stack Oven Exit Auxiliary

Point 1 492 490 490 490 491 490

Point 2 672 671 672 671 672 671

Point 3 1212 1211 1211 1211 1211 1211

Percent Difference Probe Stack Oven Exit Auxiliary

Point 1 0.406504 0.406504 0.406504 0.203252 0.406504

Point 2 0.14881 0 0.14881 0 0.14881

Point 3 0.082508 0.082508 0.082508 0.082508 0.082508



# i t

### Armstrong Environmenta! Inc. CONVERSION FACTORS EPA Meihod 5 

### 522 Series Meter Box Calibration 1 mm Hg : 0.13330 kPa Pro-Test Oririce Method 1 cm 0.39370 inch English Meter Box Units, English IC Faclor 1 mm = 0.03937 inch 1 cu fi = 28.32 liters Box >; 11 1}ale: --------- -----> 12119/05 #: 40312 Baromelric Pressure: ------ ----> 30.25 (in. Hg) 

### Theoretical Critical Vacuum:---> 14.27 (in. Hg)

I 

### RTAI` For valid tesl resuits, lhe Actual Vacuum should be 1 to 2 in. Hg greater than the Theoretical Critical Vacuum shown above. RTA!\The Critical Oririce Coefficient, IC, musl be entered in English units, (ft)^3 0 (deg R)"0.5/((in.Hg)•(min)). I

---- DRY GAS METER READINGS - -CRITICAL ORIFICE READINGS-
- Average Temperatures --

Volume Volume Volume Initial Temps. Final Temps. Otiflce IC Orifice Actual - Ambient Temperalure - DGM DGM Ambient 

### 1 Time Initial Final Total Iniet Oullet Iniet Oullet Serialfl Coefficient Vacuum Initial Final Average Outlet Overall Temp O) (min) (cu ft) (cu fi) (cu ti) (deg F) (deg F) (deg F) (deg F) (number) (see above) (in Hg) (deg F) (deg F) (deg F) (deg R) (deg R) (deg R) 0.25 11.50 438.400 442.075 3.675 56.0 56.0 57.0 57.0 40 0.242 24.0 56.0 56.0 56.0 516.5 516.5 516.0 0.51 10.50 442.300 446.997 4.697 57.0 57.0 58.0 57.0 48 0.344 22.0 57.0 57.0 57.0 517.0 517.3 517.0 0.94 7..00 447.500 451.878 4.378 75.0 75.0 76.0 75.0 55 0.464 20.5 57.0 57.0 57.0 535.0 535.3 517.0 1.60 6.50 452.400 457.635 5.235 76.0 75.0 77.0 75.0 63 0.593 19.0 57.0 57.0 57.0 535.0 535.8 517.0 3.00 9.00 458.800 468.862 10.062 77.0 75.0 79.0 75.0 73 0.824 16.0 57.0 57.0 57.0 535.0 536.5 517.0



### ............................................ RESULTS .... .................. ......

..,................,,,.

Y GAS METER ---



### ME VOLUME tECT CORRECTED (sid) Vm(std) ;u fl) (liters) .799 0.1 .852 0.2 .375 0.2 .234 0.2 .081 0.4 ORIFICE



### VOLUME VOLUME VOLUME CORRECT CORRECT NOMlNAL Vcr(std) Vcr(sld) Vcr (cu n) (liters) (cu ft) 3.711 0.1 3.588 4.810 0.2 4.660 4.320 0.2 4.186 5.131 0.2 4.972 9.864 0.4 9.557 - DRY GAS METER --

CALIBRATION FACTOR Y Value Variation (number) (number) 0.977 -0.006 0.991 0.008 0.988 0.005 0.980 -0.003 0.978 -0.004 ORiFICE ---------

CALIBRATION FACTOR dH@ Value Varialion (in H20) (in H20) 1.398 -0.0111 1.412 0.005 1.385 -0.022 1.441 0.034 1.402 -0.005 

# Average Y -------> 0.983 

# 1.407 <------- Ave rag e d H@

For Calibration Faclor Y, the ratio of the reading of lhe caiibration meter to the dry gas meter, x;eptable tolerance of individual values from the average is +-0.02.
+r Orifice Calibration Factor dH@, lhe orifice differenliai pr sure in inches of H20 lhat equates lo 0.75 cfm of air 

### 68 F and 29.92 inche Hg, a ept tolerance o' vidual values from the average is +-0.2.

SIGNED: '

~ 

### , Dale:

✓

TND

t"'a

# Temperature Meter Calibrations

Meter Box #: 11 

# Date: 12/19/05 

# Calibrated By: RT

Emtech 42312 Degrees F Calibrator Probe Stack Oven Exit Auxillary

Point 1 32 32 32 32 32 32

Point 2 100 100 100 100 100 100

Point 3 250 251 251 251 252 251

Emtech 42312 Degrees R Calibrator Probe Stack Oven Exit Auxillary

Point 1 492 492 492 492 492 492

Point 2 560 560 560 560 560 560

Point 3 710 711 711 711 712 711

Percent Difference Probe Stack Oven Exit Auxillary

Point 1 0 0 0 0 0

Point 2 0 0 0 0 0

Point 3 0.140647 0.140647 0.140647 0.280899 0.140647



# 242

### APE. Armstrong Environmental (nc. CONVERSION FACTORS EPA Method 5 522 Series Meter Box Calibration 1 mm Hg * 0.13330 kPa Pre-Test Orif'rce Method 1 cm = 0.39370 inch Engtish Meter Box Uni1s, English IC Factor 1 mm = 0.03937 inch 1 cu f1= 28.32 liters )r Box x 10 Date: ------------»»_---> 10/10/05 al #: 30272 Barometric Pressure: ---------> 29.75 (in. Hg) 

### Theoretical Critical Vacuum: --- > 14.03 (in. Hg)

!11 

### )RTAf\ For valid lest results, lhe Actuai Vacuum stiould be 1 to 2 in. Hg greater than the Theoretical Critical Vacuum shown above. )RTAf%The II Critical Orifice Coefficient, K', must be entered in English units, (it)"3'(deg R)"0.5/((in.Hg)'(min)).

DRY GAS METER READINGS ---------- -CRITICAL ORIFICE READINGS------------

t -- Average Temperatures - 

### Volume Volume Volume Initial Temps. Final Temps. Orifice IC Orifice Actual -- Ambfent Temperature - DGM DGM Ambient IH Time Initial Final Total Inlet Ouilet Inlet Outlet Serial# Coefficient Vacuum Initial Final Average Outiet Overali Temp 20) (mih) (cu ft) (cu ft) (cu ft) (deg F) (deg F) (deg F) (deg F) (number) (see above) ttn Hg) (deg F) (deg F) (deg F) (dag R) (deg R) (deg R) 0.24 6.00 508.200 510.089 1.889 76.0 76.0 77.0 76.0 40 0.242 24.0 75.0 76.0 75.5 536.0 536.3 535.5 0.50 6.00 510.400 513.118 2.718 77.0 76.0 77.0 76.0 48 0.344 22.0 76.0 76.0 76.0 536.0 536.5 536.0 0.91 6.00 513.400 517.046 3.646 77.0 76.0 77.0 76.0 55 0.464 20.5 76.0 76.0 76.0 536.0 538.5 536.0 1.50 5.00 517.400 521.271 3.871 77.0 76.0 78.0 77.0 63 0.593 18.0 77.0 75.0 76.0 536.5 537.0 536.0 2.85 6.00 521.800 528.204 6.404 78.0 77.0 80.0 77.0 73 0.824 16.0 76.0 75.0 75.5 537.0 538.0 535.5

.N........N....I..N....NN ............... RESULTS ........N....

..... ...............N...N..........



### 2Y GAS METER --- --------- ORIFICE ----- -- DRY GAS METER -- ------- ORIFICE ----



### 1ME VOLUME VOLUME VOLUME VOLUME CALIBRATION FACTOR CALIBRATION FACTOR 3ECT CORRECTED CORRECT CORRECT NOMINAL Y dHO i(sid) Vm(std) Vcr(std) Vcr(sld) Vcr Value Variation Value Variation cu ft) (iiters) (cu fi) (liters) (cu fl) (number) (number) (in H20) (in H20) 1.850 0.1 1.869 0.1 1.907 1.010 0.006 1.363 -0.0369 2.662 0.1 2.655 0.1 2.711 0.997 -0.007 1.407 0.008 3.574 0.1 3.577 0.1 3.653 1.001 -0.004 1.411 ' 0.011 3.797 0.1 3.813 0.2 3.894 1.004 ' -0.000 1.420 0.020 i.291 0.2 6.354 0.3 6.484 1.010 0.006 1.397 -0.002 

# Average Y ------- > 1.005 1.400 <------- Average dH@

For Calibration Factor Y. the ratio of ttie reading of the calibration meter lo the dry gas meter, 

### xeplable tolerance of individual values from the average is +-0.02.
x Orifice Calibration Factor dH@, the oririce differential pressure in inches of H20 that equates to 0.75 cfm of air 68 F and 29.92 ' ches-of-klg, acce tabl ol rance of individu

7 1~ 1/ es from the average is +-0.2.

SIGNED: ../

~~ 

### _ ~ 

### '" Date: 

# ' r

~



# ; V 'P h

w

# Temperature Meter Calibrations

Meter Box #: 10 

# Date: 10/10/05 

# Calibrated By: RT

Emtech Thermo 

# Degrees F Checker Probe Stack Oven Exit Auxiliary

Point 1 32 31 31 31 31 31

Point 2 212 210 211 210 210 211

Point 3 752 750 750 750 750 751

Emtech Thermo Degrees R Checker Probe Stack Oven Exit Auxillary

Point 1 492 491 491 491 491 491

Point 2 672 670 671 670 670 671

Point 3 1212 1210 1210 1210 1210 1211

Percent Difference Probe Stack Oven Exit Auxillary

Point 1 0.203252 0.203252 0.203252 0.203252 0.203252

Point 2 0.297619 0.14881 0.297619 0.297619 0.14881

Point 3 0.165017 0.165017 0.165017 0.165017 0.082508



# 244

### APE Armslrong Environmental Inc. CONVERSION FACTORS EPA Method 5 522 Series Meter Box Calibration 1 mm Hg = 0.13330 kPa Pre-Test Oririce Melhod 1 cm = 0.39370 Inch 

### English Meter Box Units, English I<' Factor 1 mm = 0.03937 inch 1 cu tl = 28.32 (iters Box t 10 Dale: ------------ 12/19105 

### #: 30272 Barometric Pressure: ----------> 30.25 (in. Hg) Theoretical Critical Vacuum: --- > 14.27 (in. Hg)



### RTAf` For valid tesl results, the Actual Vacuum should be 1 to 2 in. Hg greater than the Theoretical Critica) Vacuum shown above. :RTAN The Critical Oririce Coefficient, W. musl be entered in English units, (f!)^3"(deg R)^0.5/((in.Hg)"(min)).

---------------- DRY GAS METER READINGS --------------- -CRITICAL ORIFICE READINGS-
- Average Temperatures - 

### Volume Volume Volume Initial Temps. Final Temps. Orifice IC Oririce Actual -- Ambient Temperature -- DGM DGM Ambient 1 Time Initial Final Total Inlet Oullet Inlet Outlel Seriallt Coofficient Vacuum Initial Final Average Outlet Overall Temp O) (min) (cu ft) (cu ft) (cu ft) (deg F) (deg F) (deg F) (deg F) (number) (see above) (in Hg) (deg F) (deg F) (deg F) (deg R) (deg R) (deg R) 0.25 21.00 229.800 236.307 6.507 54.0 54.0 57.0 57.0 40 0.242 23.0 54.0 57.0 55.5 515.5 515.5 515.5 0.51 13.50 236.600 242.583 5.983 57.0 57.0 59.0 58.0 48 0.344 21.0 57.0 58.0 57.5 517.5 517.8 517.5 0.92 11.00 256.200 262.767 6.567 61.0 59.0 61.0 59.0 55 0.464 19:5 58.0 59.0 58.5 519.0 520.0 518.5 1.50 8.50 249.100 255.604 6.504 60.0 62.0 58.0 59.0 63 0.593 18.0 58.0 59.0 58.5 520.5 519.8 518.5 2.90 6.00 266.000 272.323 6.323 61.0 59.0 64.0 59.0 73 0.824 16.0 59.0 60.0 59.5 519.0. 520.8 519.5



## . ........................................... RESULTS .....................................,.............

Y GAS METER --- ------- ORIFICE -------- - DRY GAS M>=TER - ORIFICE

VIE VOLUME :ECT CORRECTED (std) Vm(sld) :u ft) (liters) .740 0.3 .174 0.2 .754 0.3 .702 0.3 .525 0.3 

## VOLUME VOLUME VOLUME CORRECT CORRECT NOMiNAL Vcr(std) Vcr(std) Vcr (cu ft) (liters) (cu fi) 6.779 0.3 6.549 6.181 0.2 5.994 6.779 0.3 6.587 6.701 0.3 6.511 6.560 0.3 6.387 

# Average Y -------> CALIBRATION FACTOR Y Value Variation (number) (number) 1.006 0.003 1.001 -0.002 1.004 0.001 1.000 -0.003 1.005 0.002 

# 1.003 CALISRATION FACTOR dHQ 

### Value Variation (in H20) (in H20) 1.397 -0.0040 1.412 0.010 1.401 0.000 1.392 -0.009 1.404 0.002 

# 1.401 < ------- Average dH a ~

For Calibration Factor Y, the ratio of the reading of the calibration meter to the dry gas meter, 

### ceptable tolerance of individual values (rom the average is +-0.02.

ir Oririce Calibration Factor dH@, the orifice differential pressure in in s of H20 that equates lo 0.75 cfm of air 

### 68 F and 29.92,.inches of'FiDi

~ 

### i accepi ble toler

~ 

### nce of ind el v s from lhe average is +-0.2. _f: ~ "` ~ c~ ~. SIGNED: 

### ~ ' L 

### ^

- /~ 7'" - 

### ~ Date: 

# ~ t.. - • f 

# ~ ~° ~

. ,



### ~
,.~ C.1

# Temperature Meter Calibrations

Meter Box #: 10 Date: 12/19/05 Calibrated By: RT

Emtech 42312 Degrees F Calibrator Probe Stack Oven Exit Auxillary

Point 1 32 32 32 32 32 32

Point 2 100 101 102 101 101 101

Point 3 250 252 252 252 252 251

Emtech 42312 Degrees R Ca(ibrator Probe Stack Oven Exit Auxilfary

Point 1 492 492 492 492 492 492

Point 2 560 561 562 561 561 561

Point 3 710 712 712 712 712 711

Percent Difference Probe Stack Oven Exit Auxillary

Point 1 0. 0 0 0 0

Point 2 0.178253 0.355872 0.178253 0.178253 0.178253

Point 3 0.280899 0.280899 0.280899 0.280899 0.140647



# 246

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# 2 ' ,5 1-

# Appendix F:

# AP 3106 Pasadena Freeway Pasadena, Texas 77503 (713) 534-8217 Fax(713) 534-8133 

# Specialty Gas Products

Date: 6/27/2005 Customer: Matheson - Trigas Project: 16015 Description: NO in N2 - EPA Protocol Exp. Date: 6/27/2007 Cylinder No: EB0001164 Cylinder Pressure: 1900psig Requested Certified Component Concentration Concentration Accuracy 

## Nitric Oxide 50 ppm 50.4 ppm 1% Nitrogen, Balance NOx: 51 ppm Reference Standard
Description Expiration date Cylinder Number Concentration 

## GMIS 11/22/2006 ND22557 99.8 PPM no Instrumentation
Description Model 

# # Date Last Clibrated Principle 

## Horiba Process Analyzer CLA-510-NO 6/16/2005 CHEMI Anaylsis Results: Z= zero gas, 

## S= standard gas, X= sample gas

First Triad 

# - NO Second Triad 

# - NO 

## Z1= -1.20 S1= 994.80 X1= 498.30 Z1= -1.10 S1= 998.50 X1= 502.80 S2= 994.10 Z2= -1.30 X2= 498.40 S2= 998.20 Z2= -0.70 X2= 

## 502.40 Z3= -1.10 X3= 499.80 S3= 997.40 Z3= -0.80 X3= 500.80 S3= 994.20 Average = 50.3ppm Average = 50.53ppm Curve: Y = 0.33645 + 0.099857*X

Analyst: 

# % TFIIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG



# 2,93

# ~ 

# •.

Specialty Gas Products 3106 Pasadena Freeway Pasadena, Texas 77503 (713) 534-8217 Fax(713) 534-8133

Date: 6/27/2005 Customer: Matheson - Trigas Project: 16014 Description: NO in N2 - EPA Protocol Exp. Date: 6127l2007 Cy(inder No: EB0001156 Cylinder Pressure: 1900psig Requested Certified Component Concentration Concentration Accuracy 

# Nitric Oxide 25 ppm 25.0 ppm 1% Nitrogen, Balance

Reference Standard NOx: 25.5 ppm

Description Expiration date Cylinder Number Concentration 

# GMIS 11/22/2006 ND22557 99.8 PPM no Instrumentation
Description Model # Date Last Clibrated Principle 

# Horiba Process Analyzer CLA-510-NO 6/16/2005 CHEMI Anayisis Results: Z= zero gas, S= standard gas, X= sample gas

First Triad - NO 

# Z1= -1.20 S1= 994.80 S2= 994.10 Z2= -1.30 Z3= -1.10 X3= 246.10 Average = 24.90ppm Curve: Y = 0.33645 + 0.099857*X Second Triad - NO 

# X1= 244.50 Z1= -1.10 S1= 998.50 X1= 247.10 X2= 244.80 S2= 998.20 Z2= -0.70 X2= 247.00 S3= 997.40 Z3= -0.80 X3= 246.40 S3= 994.20 Average = 25.00ppm

Analys :

. -----'—

,.. THIS STANX . RD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG



# 2. 1 5 4

# Specialty 

# G >~ 

# s ~' 

# roduct s
3106 Pasadena Freeway Pasadena,Texas 77503 

## (713) 534-8217 Fax(713) 534-8133

Date: 617/2004 Custorner: Trigas Project: 9210-01
Description: Propane in Air - EPA Protocol Exp. Date: 6/7l2007 Cylinder No: SX41680 Cyfinder Pressure: 1900psig
Requested Certified 

## Component Concentration Concentration Accuracy 

## Propane 30 ppm 28.8 ppm 1% Air, Balance

Reference Standard
Description Expiration date Cylinder Number Concentration 

## NTRM 712/2004 SG9183302 103.6 ppm Propane 

# Instrumentation Description Model n Date Last Clibrated Principle Horiba Process Analyzer FIA-510 5/24/2004 FIA 

# Anayisis Results: Z= zero gas, S= standard gas, X= sample gas

First Triad - Prooane Z1= 0.60 S1= 207.90 X1= 57.60 S2= 207.70 Z2= 0.60 X2= 57.50 Z3= 0.60 X3= 57.40 S3= 208.00 Curve: Y=-0.05085+0.501149*X Average = 28.77pm



# ~ Analys


# ~ -~
r•' 

## THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG



# 2.'

~ 

# 5

# Specialty 

# Ga s 

# . ~'' 

# r c~ 

# c.
~ 

# c.

~ 

# • 

# ct s
3106 Pasadena Freeway Pasadena, Texas 77503 (713) 534-8217 Fax(713) 534-8133

Date: 6/7/2004 Customer: Trigas Project: 9211-01 Description: Propane in Air - EPA Protocol Exp. Date: 6/7/2007 

# Cyiinder No: CC177391 Cylinder Pressure: 1900psig Requested Certified Component Concentration Concentration Accuracy 

## Propane 50 ppm 48.8 ppm 1% Air, Balance

Reference Standard 

# Description Expiration date Cylinder Number Concentration NTRiVi 7/2/2004 SG9183302 103.6 ppm Propane Instrumentation
Description Niod'el # Date Last Ctibrated Principle 

## Horiba Process Analyzer FIA-510 5/24/2004 FIA 

# Anayisis Resuits: Z= zero gas, S= standard gas, X= sampie gas

First Triad - Pronane Z1= 0.60 S1= 207.90 X1= 97.60 S2= 207.70 Z2= 0.60 X2= 97.20 Z3= 0.60 -X3= 97.50 S3= 208.00 Curve: Y=-0.05085+0.501149"X Average = 48.78pm

•r•
,.


## Analyst:

.~ ' 

## THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG



# 2 1 56

# Speci'alty 

# Ga s P 

# r o 

# d

~ c~
- 

# s

3106 Pasadena Freeway Pasadena, Texas 77503 (713) 534-8217 Fax(713) 534-8133

Date: 8l312005 Custorner: Trigas Project: 17092
Description: Propane in Air - EPA Protocol Exp. Date: 813l2008 Cylinder No: CC112437 Cylinder Pressure: 1950psig Requested Certified Component Concentration Concentration Accuracy 

## Propane 90 ppm 89.2 ppm 1% Air, Balance

Reference Standard
Description Exairation date Cylinder Number Concentration 

## SRM 12l112009 XF004033B 488 ppm Propane Instrumentation
Description Model # Date Last Clibrated Principle 

## Horiba Process Analyzer FIA-510 813l2005 FIA 

# Anaylsis Results: Z= zero gas, S= standard gas, X= sampie gas

First Triad - Prooane Z1= -0.10 S1= 975.30 X1= 176.50 S2= 975.10 Z2= -0.10 X2= 175.40 Z3= -0.10 X3= 176.20 S3= 975.20 C urve: Y=1.0614+0.500676'X Average = 89.21 pm

Ir r

J 

## Analyst: ,%~~ - 

## THIS ST,9NDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG



# 2,57

# Specialty ~~ Pr 

# odu cts

~ 

# s

3106 Pasadena Freeway Pasadena, Texas 77503 (713) 534-8217 Fax(713) 534-8133

Date: 8/3/2005 Customer: Trigas Project: 17093 Description: Propane in Air - EPA Protocol Exp. Date: 813I2008 Cyiinder No: SX28250 Cylinder Pressure: 1950psig Requested Certified Component Concentration Concentration Accuracy 

## Propane 200 ppm 200 ppm 1% Air, Balance



# Reference Standard
Description Expiration date Cylinder Number Concentration 

## SRM 12l1/2009 XF004033B 488 ppm Propane Instrumentation
Description Model # Date Last Clibrated Principle 

## Horiba Process Anaiyzer FIA-510 8/3/2005 FIA Anaylsis Resuits: Z= zero gas, S= standard gas, X= sample gas

First Triad - Prooane Z1= -0.10 S1= 975.30 X1= 398.10 S2= 975.10 Z2= -0.10 X2= 398.00 Z3= -0.10 X3= 397.80 S3= 975.20 Curve: Y=1.0614+0.500676*X Average = 200.3 ppm

Analyst:

~ - 

## THIS STANDARD`IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. DO NOT US`r= THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG



# 2...58

# Specialty 

# Gas Products

3106 Pasadena Freeway
• Pasadena, Texas 77503 (713) 534-8217 Fax(713) 534-8133

Date: 7/13/2004 Customer: Matheson-Trigas Project No: 9970 Description: S02 in N2 - EPA Protocol Exp. Date: 7113/2006 Cylinder No: . CC88735 Cylinder Pressure: 1900psig Requested Certified Component

e Concentration Concentration Accuracy Sulfur Dioxide 100ppm 101 pprn 1% 

# Nitrogen, Ba!ance

Reference Standard Description Expiration date Cylinder Number Concentration GMIS 1l19/2006 CC177157 793.8pprn S02 * GMIS CC1771 57 Tracebility Description Expiration date Cylinder Number Concentration NTRM 6/1/2006 SG9199568 1997ppm S02 lnstrumentation Description Model # Date Last Clibrated Princiale Horiba Process Analyzer VIA-510-S02 6/15/2004 NDIR Anayisis Results: Z= zero gas, S= standard gas, X= sample gas

First Triad - S02 Second Triad - S02 Z1= -0.90 S1= 791.9 X1= 98.7 Z1= -0.90 S1= 794 X1= 99.0 S2= 794.0 Z2= -0.70 X2= 99.0 S2= 793.2 Z2= -0.60 X2= 99.2 Z3= -0.90 X3= 99.2 S3= 792.6 Z3= -0.60 X3= 99.30 S3= 793.4 Cu rve: Y=1. 971 +0. 999869'`X Average = 100.6ppm Average =100.9ppm

^ /

~ 

# ----- Analyst : ' --_-

~ 

# Ling WeFr

- " - ~ 

# THIS STAN-Y



# ~ RD IS NlST TRACEABLE. IT WAS CERTIFIED P.CCORD!NG TO THE EPA PROTOCOL PROCEDURES. DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG


# 2,59

# Specialty 

# G as

~ 

# 'rc

~ 

# du cts

3106 Pasadena Freeway Pasadena, Texas 77503 (713) 534-8217 Fax(713) 534-8133

Date: 7113/2004 Customer: Matheson-Trigas Project No: 9969 Description: S02 in N2 - EPA Protocol Exp. Date: 7/13/2006 Cylinder No: CC177434 Cylinder Pressure: 1900psig Requested Certified Component Concentration Concentration Accuracy 

# Sulfur Dioxide 50ppm 50.1 pprn 1% Nitrogen, Balance

Reference Standard
Description Expiration date Cylinder Number Concentration 

# NTRM 6/1/2006 Sg9135833 99.8ppm S02 Instrumentation

DescriQtion Model # Date Last Clibrated Principle 

# Horiba Process Analyzer VIA-510-S02 717/2004 NDIR Anayisis Resuits: Z= zero gas, S= standard gas, X= sample gas

First Triad - S02 Second -Triad - S02 

# Z1= -1.30 S1= 999.90 X1= 502.60 Z1= -0.80 S1= 997.90 X1= 500.30 S2= 999.90 Z2= -0.70 X2= 503.60 S2= 998.70 Z2= -0.10 X2= 500.30 Z3= 0.00 X3= 503.60 S3= 999.90 Z3= -0.20 X3= 501.60 S3= 999.30 Curve: Y=0.0064+0.09986'`X Average = 50.15ppm Average =49.98ppm

. ... ~ 

# Analyst: -

~



# Ling,Wen THIS STANDARD IS NIST TRACEABLE. (T WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG



# r.~

# s 

# Ga s 

# Products

pecialty

3106 Pasadena Freeway Pasadena, Texas 77503 (713) 534-8217 Fax(713) 534-8133

Date: 6/27/2005 Customer: Trigas Project: 16017 Description: CO in N2 - EPA Protocof Exp. Date: 6/27/2008 Cyfinder No: EB0000701 Cylinder Pressure: 1900psig Requested Certified 

# Component Concentration Concentration Accuracy Carbon Monoxide 50 ppm 49.9 ppm 1% Nitrogen, Balance

Reference Standard
Description Expiration date Cyiinder Number Concentration 

## NTRM 5/29/2006 SX19190 994.2 ppm CO Instrumentation

Descriation Modei # Date Last Ciibrated Princigie 

## Horiba Process Analyzer VIA-510-CO 6/10/2005 NDIR 

# Anaylsis Results: Z= zero gas, S= standard gas, X= sampie gas

First Triad - CO Second Triad - CO 

## Z1= -0.90 S1= 204.90 X1= 198.70 Z1= -0.40 S1= 513.30 X1= 497.10 S2= 204.80 Z2= -0.80 X2= 198.60 S2= 513.20 Z2= -0.40 X2= 497.10 Z3= -0.80 X3= 198.60 S3= 204.90 Z3= -0.40 X3= 496.90 S3= 513.20

Y=0.28607+0.250309'"X Y=0.031031 +0.100163*X Average = 49.94ppm Average = 49.82ppm



# ~

- 

## analyst: '

~ 

# THIS STANDARD IS NIST TRACEABLE. iT VUAS CERTIFIED ACCOP,DING TO THE EPA PriO T OCOL PROCEDURES. )0 NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

# 261

# SpecidIty G

~ 

# s

' 

# Pro c~I~ 

# ..,{c

~ - 

# s
3106,Pasadena Freeway Pasadena, Texas 77503 (713) 534-8217 i=ax(713) 534-8133

Date: 6/27/2005 Customer: Trigas Project: 16018 Description: CO in N2 - EPA Protocol Exp. Date: 6/27/2008 Cylinder No: EB0000761 Cylinder Pressure: 1900psig Requested Certified ComQonent Concentration Concentration Accuracy 

## Carbon Monoxide 100 ppm 991 ppm 1% Nitrogen, Bafance

Reference Standard
Description Expiration date Cyiinder Number Concentration 

## NTRM 5129J2006 SX19190 994.2 ppm CO Instrumentation
Description Niodel # Date Last Clibrated Princinie 

## Horiba Process Analyzer VIA-510-CO 6/1012005 NDIR Anayisis Results: Z= tero gas, S= standard gas, X= sampie gas

First Triad - CO Second Triad - CO 

## Z1= -0.90 S1= 204.90 X1= 396.60 Z1= -0.40 S1= 513.30 X1= 985.70 S2= 204.80 Z2= -0.80 X2= 396.60 S2= 513.20 Z2= -0.40 X2= 985.40 Z3= -0.80 X3= 396.50 S3= 204.90 Z3= -0.40 X3= 985.20 S3= 513.20
Y=0.28607+0.250309*X Y=0.031031 +0.100163"`X Average = 99.45ppm Average = 98.74ppm

. ._._. ~


## Analyst:



# TH1S STANDARD IS NlST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSlG 

# 2 62

# Specialty 

# G as ~' 

# rod ~..~c~ - .~ 3106 Pasadena Freeway Pasadena, Texas 77503 (713) 534-8217 Fax(713) 534-8133



## Date: 8/1612004 Customer: Nlatheson - T rigas Project: 10548 Description: CO, 02 in N2 - EPA Protocol Exp. Date: 8/162007 Cylinder No: CC187154 Cylinder Pressure: 1900psig Requested Certified Comaonent Concentration Concentration


## Carbon Monoxide 200ppm 200ppm Nitrogen, Balance
Reference Standard Description Expiration date Cylinder Number
G M I S 4!6!2006 CC 177636


# Instrumentation Description Model # Date Last Clibrated Horiba Process Analyzer VIA-510-CO 8/6/2004 Anayisis Results: Z= zero gas, S= standard gas, X= sample gas

First Triad - CO Second Triad - CO 

## Z1= -0.3 S1= 993.5 X1= 199.9 Z1= -0.4 S1= 995.5 S2= 993.20 Z2= -0.30 X2= 200.00 S2= 995.80 Z2= -0.30 Z3= -0.30 X3= 199.90 S3= 993.00 Z3= -0.30 X3= 200.60
Curve: Y=-0.6893+1.001139X Average =199.6ppm Average = 199.8ppm Accuracy

1%



## Concentration 994.2 ppm CO



# Principle '

NDIR

X 1= 200.6 X2= 200.60 S3= 995.60

Analyst: Ling 1iJen



## THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

# 2.. R 3

## Cylinder Number Concentration
CC177636 994.2 ppm CO

Date Last Clibrated 

## Principle
8/6/2004 ND I R

Second Triad

- 

## CO 

## Z1= -0.4 S1= 995.5 X1= 495.4 S2= 995.80 Z2= -0.30 X2= 495.60 Z3= -0.30 X3= 

## 495.50 S3= 995.60

Average = 494.4ppm 

# Specialty Gas P

3106 Pasadena Freeway Pasadena, Texas 77503 (713) 534-8217 Fax(713) 534-8133

Date: 811612004 Customer: Matheson - Trigas Description: CO, 02 in N2 - EPA Protocol Cylinder No: CC176507
Requested Component Concentration


## Carbon Monoxide 500ppm Nitrogen, Balance
Reference Standard Description Expiration date


## G M I S 4/6l2006

instrumentation
Description Modei 

## # Horiba Process Analyzer VIA-510-CO Anayisis Results: Z= zero gas, S= standard gas, X= sample gas

First Triad

- 

## CO 

## Z1= -0.3 S'f= 993.5 X1= 494.2 S2= 993.20 Z2= -0.30 X2= 

## 494.00 Z3= -0.30 X3= 493.90 S3= 993.00
Curve: Y=-0.6893+1.001139X Average =494.1ppm P roject: 10549 Exp. Date: 8/162007 Cylinder Pressure: 1900psig
Certified Concentration Accuracv 

## 494ppm 1%

Analyst: Ling W6ri

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

# 2 9-4

# Appendix G

# Sheetl

Summary

,ant: I nterfern ce An
Daltile, Muskogee, OK Location: Trim Kiln Exhaust Date: 1218/051 Anal)Lzer: lWestem Research 721-AT

Run # Method 6 Method 6C Difference, % 1 86.36 83.63 103.2644 103.52541 72.24 69.78 1 31 79.02, 75-171 105.12171

Page 1 

# 273

# EMISSION TEST SUMMARY

PLANT

: 

# Deltile, Muskogee, OK DATE

: 

# 6-Dec-05 PLACE

: 

# Trim Kiln Exhaust, S02 Interference Train RUN#

: 

# 1
TEST DURATION (MINUTES)

: 

# 64 LIQUID COLLECTED (mis)

: 

# NOZZLE DIAMETER (INCH.)

: 

# 0 Sulfur 

# Dioxide Weight, mg

: 

# METER COEFFICIENT (Y)

: 

# 0.944 PITOT COEFFICIENT (Cp)

: 

# 0 STATIC PRESSURE (in. H20)

: 

# GAS METER VOL.(Cu.Ft.)

: 

# 2.316 PERCENT CO2

. 

# BAROMETRIC PRESSURE

. 

# 30 PERCENT 

# 02

. 

# PERCENT CO

.


# FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 0 STACK LENGTH(inchs) : STACK AREA (Sq.Ft.) : 0 STACK WIDTH(inchs) : NOZZLE AREA (feet): 

# 0 STACK AREA (Sq.Ft.) :

ENTER THE STACK AREA SHOWN ABOVE: 0



# FLOWS SAMPLED VOLUME (STD. CU .FT.): 2.2267

Sulfur Dioxide, ppm : 86.3631

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T.

deg F I N LET

1 0 0.01 59.62

0 0.0000 0.0100 59.6200 0 14.49 0 0 0 0 0

C

METER T. OUTLET

59.62

59.6200 59.6200



# 274

# EMISSION TEST SUMMARY

PLANT : Daltile, Muskogee, OK DATE : 6-Dec-05 PLACE : Trim Kiln Exhaust, S02 Interference Trein RUN# : 2
TEST DURATION (MINUTES)

: 

# 62 LIQUID COLLECTED (mis)

: 

# 0 NOZZLE DIAMETER (INCH.)

: 

# 0 Sulfur Dioxide Weight, mg

: 

# 10.93 METER COEFFICIENT (Y)

: 

# 0.944 0 PITOT COEFFICIENT (Cp)

: 

# 0 STATIC PRESSURE (in. H20)

: 

# 0 GAS METER VOL.(Cu.Ft.)

: 

# 2.091 PERCENT CO2

. 

# 0 BAROMETRIC PRESSURE

. 

# 30 PERCENT 02

: 

# 0 PERCENT CO

: 

# 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 0 STACK LENGTH(inchs)

: 

# STACK AREA (Sq.Ft.)

: 

# 0 STACK WIDTH(inchs)

: 

# NOZZLE AREA (feet): 0 STACK AREA (Sq. Ft.)

: 

# 0

ENTER THE STACK AREA SHOWN ABOVE: 0


# FL01NS SAMPLED VOLUME (STD. CU .FT.): 2.0078

Sulfur Dioxide, ppm

: 

# 72.2463

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 0 0.01 60.28 60.28

0 0.0000 0.0100 60.2800 60.2800 60.2800



# 275

# ENIISSION TEST SUNINIARY

PLANT

: 

# Daltile, Muskogee, OK DATE

: 

# 6•Dec•05 PLACE

: 

# Trim Kiln Exhaust, S02 Interference Train RUN#

: 

# 3
TEST DURATION (MINUTES)

: 

# 62 LIQUID COLLECTED (mis)

: 

# 0 NOZZLE DIAMETER (INCH.)

: 

# 0 Sulfur Dioxide Weight, mg

: 

# 11.72 METER COEFFICIENT (Y)

: 

# 0.944 0 PITOT COEFFICIENT (Cp)

: 

# 0 STATIC PRESSURE (in. H20)

: 

# 0 GAS METER VOL.(Cu.Ft.)

: 

# 2.052 PERCENT CO2

: 

# 0 BAROMETRIC PRESSURE

. 

# 30 PERCENT 02

: 

# 0 PERCENT CO

. 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 0 STACK LENGTH(inchs)

: 

# STACK AREA (Sq.Ft.)

: 

# 0 STACK WIDTH(inchs)

: 

# NOZZLE AREA (feet): 0 STACK AREA (Sq.Ft.)

: 

# 0

ENTER THE STACK AREA SHOWN ABOVE: 0


# FLOWS SAMPLED VOLUME (STD. CU .FT.): 1.9684

Sulfur Dioxide, ppm

: 

# 79.0194

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 0 0.01 60.8 60.8

0 0.0000 0.0100 60.8000 60.8000 60.8000

J 

# 276

# Sulfur Dioxide Barium-Thorin Analysis

Plant: Daltile, Muskogee, OK Location: Trim Kiln Exhaust, S02 Interference Date: 8•Dec•05 Standardization Ba (C102)4 Titration (mis) Avg. Titration (mis) 9.833333 Blank Titration (mis) Avg. Blank (mis) 

## 0

Volume of Standard Sulfuric Acid (mis) Normality of Standard Sulfuric Acid Normality: 0.010169
Aliquot Average Run # Location Volume Dilution Volume Titration Titration (mis) (mis) (mis) (mis) (mis)

1 I m P 

# 1•2 ~ 

## :;:,:,;::::,:,; :::::: .:..::::::::::::::::::::... .
•~: :~ ~~~ 

# E?:= ~~~~' 

# 18 '5: ~:~~~i~~~~ ~l~, :~~$;~ 

# 5 .5666667

2 I m p 

# 1•2 :$. Q'• :i

~ 

# : 4.2



# 3 I m 1•2

P

. Q: ~'`~~~'~~~:~ 

## ::::::: ~:~ 

## : :: ~:~~~~~~:~:;:~~ 

## ::;:;::::;: '

:

~ 

## $

.. ~ 

## .:::

~ 

## ::::::: ~~~:~:::~:)~~ 

## :`:: ~::~~::~ 

## :::::4i ~:~::~~ 

## :::::: ~'~ 

## :::.

.. .5......

. .4t ~~'~'.:~~:~:: 

## 4.5

Run # Location Total Grams Total Mg

1 Imp 1& 2 S02 0.014492 14.49

2 Imp 1& 2 S02 0.010934 10.93

3 Imp 1& 2 S02 0.011715 11.72



# 2.7'7

# PEF-LD DATA

PLAN'f: 

# ~~ i F t 

# ~ , 

# DATE: 

# REPETITION: LOCAi

— ION (SOURCE,,): 

# OPERATOR:

~ 

# AT SANDLE 

# TRAIN '

Tr: NETER BOX '

Tr: BAROMEnuc PREssuRE: 3 AMBIENT TENTERATURE: ASSTj'NED MOISTURE: 

# PROBE LENGTH: ' 

# NOZZLE PLAMETER: STACK 

# DIAM:ETER: METE 

# R H: C 

# FACTOR: METER CO-EFECIENT: 

# Iqq FU,TER TARE: PRE-TEST LEAK CHECK Meter: 

# S - 0100cu.ft. @ in. HG

Pitntc• 

## (n) in 

## '910 

# EMPLN ITGERS 

# Initial Finai #1 3; 0 

# ., 1 3 "ev 

# 3 4& .U- ) 30 30



# '4

96

CO2 02

POST-TEST 

# LEAK CHECK 

# Meter: 40 -c-0 o 

# cuft @ 

# in. HG 

# pitovq- 

# e- (a. in- R20

Time 4:1 Tk_ 

## r Ft: Tt 

### oudev-;'

- Ory



### em p;*

~ 

### -T T



# 7- 

# 1 57 

# IS 

# 3 30 ~ 

# ,! G?, t ~ 

# r ~ 

# `"



# Y

. 

# 71. r l ~ ~~ 

# 1yo lb 

# Ir YgT 1- 16


# co RVI / 

# ir i~ ! 

# Sf If -o

~ 

# o ;oS o3•Z C6 ~~ ( .


# z~ I

! c s. ~ 

# t

~ 

# s

(

~~ 

# .63

~ 

# s. I

~ 

# i I i 

# ! I i i 

# ! I

I_..

.. ~ 

# _ ..

. !
~



# . `_ 

# ' I ' 

# i ' _y ; ~ ; 

# ~ _-- ~

_ __. -. 

# f : .. 

# I

Ave.! r 

### le 

## ~~ - ti 

## PLANT: 

# ~ ~ 

## , t'r
DATE: REPETITION:

11 

# -- LOCATION (SOURCET.-) ~ 

## OPEPLATOR: 

# SAN4PLE TR.AJN 

# NMTER BOX rr. BAROMETRIC PRESSURE: AMBM'NT TENTERATURE: ASSLTIvIED MOISTURE: PROBE LENGTH: 

# NOZZLE DIAMETER: STACK 

# DIAAIETER: METER H: C 

# FACTOR: METER CO-EFFICEENT: (5 

# FILTF-R TARE: PRE-TEST LEAK CHECK 

# Meter 0, eVO 

# cu.fL @ 

# in. HG Pitots: . 

# A) in. H20 

# FIELD DATA

FWDiGERS Initial Final
-ul 

# 50 2p 

## -Tur 2

. U .-W tr.) -Ulf rr-t rrD .0 -
#6



# CO2 02



# POST-TEST 

# LEAK CHECK 

# LMeter: 0 .000 

# mfL @ 

# in. HG 

# Pitots: 

# a, in. H20

PLW 

### Mme.



## _

~ .'sltmd 

## ~

. t ~~ 

### PcIU Vi T 

### lz lniets 

### Im .,.. p 

# 1 - - T 

# S
- D 723. 

# 1,6 IS" :5 , ~ 

# - -_ 21. 

# -7 16 

# r.S' -

11 

# 11.06 .33.'?

1. 

# vs - 1 

# 38•7 

# 't Y , o 

# e(p /so"

X2 %W 

# e ~

tv 

# 3 to (09. C( 

# 7%f - C& 

# 16 cp 

# ti L17

7



# ( I

.

2 7.

# FIELD DATA

PLAN'.r: DATE* t , 

# 06 , 

# REPETITION: LOCATION (SOURCF,4): OPER.

~ 

# kTOR: 'F'4 SAI , ,,IPLE 

# TRAliN 41: 

# LvETER BOX rlr: BA.ROMETRIC PRESSURE: 3 E) 

# AMBIENT TENDERATURE: 

# AS SUIvIED MOISTTi

- RE: PROBE LENGTH: 

# NOZZLE DL41METER: STACK 

# DLAAIEETER: LMETER El: C 

# FACTOR: METER CO-EFMCIENT: FILTER TARE: PRE-TEST LEAK CHECK 

# Meter: 0 , 00 

# cuft @ 

# in. HG 

# Pitot-q. (a- ln_ T-T20 " " rmPINGERS Initial Final

r'r'3



### ~



# CO2 02



# POST-TEST LEAK 

# CHECK Meter: 

# ig -, c- , Ovcu.ft. 

# @ in. 

# HG pitots. (a. in. H20

"T i 

# _1 4 Ahe Delta -Tm V. : T
o c iii.HME."



# l~~ a3.~ ~ ~~



# b~ : ~o ~~3• ~` ~!b ~ f



# TO T

_ 3q 

# .y (4

.

I 

# cG 4



# ! f

. ~g~~~~ ~~ ~~

~ ~ ~e

.



# I f !
~ 

# ~_


# _ !
f
~ ~



# 128011 Ave,

### A1tr sirottci Etivirormrenial Itrc. EI'A Melhoci 0

Oririce MeIIioJ 

### Liiglish tvleler Box Units, English IC Factor
cI Dry Gas Meter Oiile: --- ----------- --------- > July 11, 2003 

### 3909 t3arorrnellic f'ressure: ----

- 

### ---- > 29.70. 'i"hr.uretical Crilical Vacuuun:----• 13.91 (ilt. 1

- 1g) 

### CONVL=RSION FAt;1 Vi:S
I ttutti Hg = 0.13330 N.Pa 1 cin = 0.39370 iiicit 1 nrrn - 0.03937 iricil I cu tl = >13.:32 19ters



### %h For•valici lesl resulls, tiie Acltial Vacuum stwuld be I to 2 iii. I-ig greater Ihati lhe Theorelical Ctilicai Vacuum shuwn above. %n 1

- I,e Critical Oifi'ice Coet('iciei,t, W. musl be etilered in Eriglisll utiils, (fl)^3 4 (deg

---------------- Dftl' GAS ML"i'ER ftEADINGS --------- ------- -CRITICAL ORIFICE READINGSTheurelical Criticat Vacuwrr:---> 14.05 (in. 1

- Ig) 

### Voli,me Volun,e Volun,e Iniiiat Temps. Final Tetnps. Otifice IC Orifice Aclual - Anibient Tempetature -- OGM DGM /ltttbicni
Tiiiie Inilial Fitial Tolal Inlel ' Ottllel hilel Oullel Serialit Coelficient Vacuum Inilial Final Average Outlel t)verall Temp (nth)

. (cu tt) (cu tl) (cu tl) (deg F) (deg F) (deg F) (deg F) (nurttber) (see above) (lii lig) (deg F) (deg F) (deg F) (deg R) ((leg R) (dt:y ) 5.00 I6.716 16.917 0.20*1 87.0 07.0 07.0 87.0 10907 0.029 23.0 07.0 87,0 07.0 547.0 547.0 547.0
l 5,00 16.917 17.110 0.201 07.0 07.0 87.0 07.0

- 

### 16907 0.029 23.0 07.0 07.0 07.0 547.0 547.0 547.0
l 5.00 17.118 11.320 0.202 07:0 07.0 87.0 87.0 16907 0.029 19.5 07.0 07.0 07.0 547.0 547.0 7.0

.~ ......... •...... •..................... I(t_.SUt_TS

.............. r•••••..................... www.....ww



### AS MLTER --- --------- ORI1=10E --------- - - DIZY GAS METER -- -------- OIIIFICE ---------



### VOLUMI.=. VOLUMI= VOLUMC VOLUME CALIBRATIOIJ FACTOR CALIERAI•ION FACTOIZ T CORRECI'ED GORRECT C012REC1' NOMINAL Y dHQ ) Vm(slcl) vc,(stcl) Vcr(sld) Vcr Value Varialioti Value Vatialion i (tilers) (cu (t) (liters) (cu Il) (tiuttiber) (nuttiber) (in 1-120) (in I

- 120) 1 0.0 0.102 0.0 0.190 0.94G 0.002 0.000 0.0000 t 0.0 0.1821. 0.0 0.190 0.945 0.002 0.000 0.000 i 0.0 0.1 Li2 0.0 0.190 0.941 -0.003 0.000 U.000

Avet age Y ------- > 0.944 0.000 <------- Average dl-IQ

...,,:alioti Faclor Y. lhe ralio o( the teaditig o( lhe caiibtalioii nteler lu Ilte dry gas titeter, laufe.loieratice of itidividual values frotti Ihe average is +-0.02.


### ririce•Calibralion Fhctor-dl-tL, tlie wi(ice dillerenljal pre su i 

### e in inc,l i 

### es o( 1120 lhal equales lo 0 .75 c(m o( air F artid 29.92 incties o( I ly, accelJla



## ~ ile-idle ange


## ~ o( ir ividual v lues itom Ilie average is +-0.2.
,
SIGN_f=D: '-" 

## ~~ f, t. .r` 

## ~ Date:

. --- 

# ~

;

T\D Q0

~l APEX (NSTRUMENTS VU 

# A OR IFICE ADAPTEIt C/11,I8RATIOfd 

# ^^_

Cattlirallott CorfUtltons

oale rlme 07/10103 16:3U

03rotrtelric Pressure 749.0 rum 119

Thcorellcal Critical Vacuuni 353.5 1 n>tn 119

Calibtatton Tecltniclan RM Fa clor slConvc rslons

5tJ Tentp 293 1 <

SIJ t'ress 760.00 mrn I Iq 

# _

K t 0.306 K/r om I ly Calihra{Ivrt lnio+nntlort

WT1.1 M(tlel rlu,npar A1.11



# ~ WIM Scriil Nymbcr I6807

WI M Gan,ma

~ ^._ ___ I.OUOl1U

''Ihe Critical Urillce Co¢ilieiertl, K', Irr L•nUlish vrtits, 'll+ c Cri0cal O rilicc Coclticicrtt, 1(', i4 Metrlc vnits, (L'1(I!(Inmllg'nur,). 1tOTE: VULUME Ill UIEttS

Callbra0on Data
Wet Tesl fActer Rvn // Vrilice ltun Ttme Voltrnto Voltnne Voluttta 7emperaluro

5cria111 Clap.ed brilial FMaf Tolal Irritial NM) 

### N .J f.



### _ L L I C 1 1 74-14-03 

### G 306.025 312.500 6.475 30 2 

# F

K 4 -fe•03 312.500 310.9 6 0 6. 

### 4 60 

### 30 3 K•t

- 14

- 03 G 310.96 0 325.d2U 6.460 30 Rasulis

VUA A t iopler
Tempt,raluto Fhlal /lrnb Tentir

Inslhl Atttb Tentp

Flltal Actual

Vacuuin Coetticlent

Melrlc Urdts • (+.,r) ( 1 -4E) 8—'(4 K,

't; 'C 'C nnn I Ip sac above
3 0 29 29 597 0.0239
30

~ — 29 29 610 0.0230 

### 30 29 30 O I U 0.023 (:0alllcionl % Variallort ngllsh Units troin_AvU

Cf!Q a I 2.071E-02

~ 0.17
2.06 3t=-02 — ~

~ 0.{ 1
2.004C-02

_ -O.UG 2.066[-02 ^' ~

I eertily 11ls,t O
, ilicc scl rnrntbar /L ' wns tesleci in nccorJanctr wilh Ilto US EPA MelltoJ 5 stanJartis. Sec.11te C•o(;o ol Fctferi ,10111.1t1a ns, liUe 4 0, I>att 60;nppa+u ix A, MElttoJ"5, ilem 7.2.

---- -- 

# ~ Cquatlon lo Calcutale.SlanJardized Flowrate I (Given /1nlbient Eiaruinetric'Pressure and Absoiule Temperature Condiliolls: Pb, r & Ta,nn(ab:)):

1/Z Qcr(slJ)-K ,

* Pbar/Tamb(abs)

~ 00 N)l

### Li

~



# 4 1 1 1

LL

## Sheetl

.S-YMTary of 

# S02 lnterfernce Check

Plant 4 Scrubber Monitor: 'Western Researcf
~ 

# 721-

- AT

21 

# 3

Monitor 

# S02, ppm 

# 01 ol 1 0 Modified Method 

# 6 §

—

Of'! L ol 01 0 % Difference 

# 1 01 i 0! 0



# 284 Page 

# 1

# Sulfur Dioxide Barium-Thorin Analysis

Plant: Daltile. Dallas, TX Location: Plant #4 ScrubSer Date: 10•Jul•03



## Standardization Ba (C102)4 Titration (mis) Avg. Titration (mis) 10.5 

# Blank Titration (mis) Avg. Bfank (mis) 0.1



# Vofume of Standard Sulfuric Acid (mis) Normality of Standard Sulfuric Acid b:1: Normality, 0.009524
Aliquot' Average Run # Location Volume Dilution Volume Titration Titration (m!s) (rnls) (mis) (mIs) (mis)



# 1 I m ..~~,~,



# 1•2 :~ 

## P

~~ 

# : :

~ ~ 

# ::

_ ~ 

# 0.1

2 Im l' 

## 2

I 0.1

..: 

### ~ ; 

# 3 Im a 

# 1•2 ~~ ~~: ~~ 

# ; :x:

~ 

### ~a:~:~ 

# `:v:: ~: :~ ~~ 

## 0 

# 1

Run n l.ocation Total Grams Total IYlg

1 

## Imp2&3 S02 0 0.00

2 I m p 2& 3 S02 0 0.00

3 Imp 2& 3 S02 0 0.00



# 2R5

# ' + i r ..' I

_ ' :

1.. 

# . ' t_. ~ 

## , ;. : '- ~~ 

## .. . ~ 

## _ .k.....

~ 

## f

~ 

## . 1 • ( I +~ 

## _ . ~ 

## _.'
_. ~ 

## . .; ~ ~ ~ 

## ! '.

. ....... .

E 

## ~ I ~ ~ i 

# i__ ' 1!

_ ~ 

# __.... ~ 

# ._..! .. . : .-

~ 

# _.._ . ~ 

# . _ ~ 

# __.. ~ ~ —~ 

# `_..

~ 

# .h.. _I_....-_..:

~ 

# ._ i

. ~ 

# ._.._+ ._. ~ 

# ._ ...' ' 1 .l.._.. i ; ~ 

# I i _
; :

~ 1 

## c_?' fr<i r:'~:~~ ' 

# c,` r I .._!_ I .- : . ~ 

# _.-i_. ~ ~ 

# r_.` ~ 

# f

_ ~ 

# ._. L_.. _._. ~ 

# _ . ~ 

# " : v

~ 

# - 11 

# I L

AI 

# Lb

~ i__' 

# ~~ r ~ !



# _ _ ~C-~ ~ _ ~ ~ _



# 9 SIR- 

# J, •

_~ _.L !

_ _.»E_._ 1 

# ~ •— -- —•— 

# ~ --- —•

_ _. _ . loj

... 

# ~

_ _L—.1.. 

# ~ — -- 

# ~ __~ _. . 

# ~ • L.



# ~ L.



# ~ . . 

# ~ ». 

# ~ ._.

1- 

# 2
.L.~1~_~



# .... ~ 

# .._ -. ~ 

# ._ ~ 

# _ _ _ _.__ ~ 

# ._....

_ ~



# __ _..L._

_ _ .!

~



# 1_.. ~.~ 

# _I _ _ ~ i ~ ~ - i

_



# LL 

# _ ._ ~

; 

# -•--!-.•- r



# . ~ 

# ._ ~ 

# _ - !•

_ ~ 

# F 

# 4

~ 

# ' i ~ 

# .l_

~~ 

# ~. + i

. _ I -- -.._ ~ 

# _ _ ~~ 

# . i -

_ ~ 

# , 

# ... .. - i 

# _!_ i ___. _.L»

_ i_i

__ ~ 

# _.. ~.



# »

. ~ 

# ..-_._ __%_._.!. .. . - - ~ 

# ,__. -. j 

# _»-_,-._ _»._L___
_. ll 

# _ ._ •~ 

# ' 

# ..l_._

~~



# ___ ~~ 

# _I..__• ~..~ _(~...~i~ 

# _» i___.

_ __i_._...

~.~ 

# .L..__i_._.i
._ I



# ~ ._L_

I 

# L 

# L i ! ~ ~ i 

# fi 1 I j 

# ! r 

# ~ c :. 

# . i _ ~ 

# _-.. ~ 

# ._.. _ 1

_

-.1 

# L 

# I —J _.'• L--.-" L



# .. ~ 

# .._.... ~ 

# .._.. '

.. ~ 

# . .. ~ 

# .... .. ~ 

# .... .1__... ~ 

# .» _

~ 

# -_.....j......i_._.... r 

# . .. ~ 

# ,.._.. ~ 

# ..._...!_........

~ 

# ....__.L.... »

~ 

# .«._l...__. E . ».L._.. ~ 

# ...__i_.__..;_..._1_.._ €..». ! --- { ~ - ~ »- ~ 

# - _ _-- ~ 

# -•--1 •rf---

~ 

# -- 

# 1 

# LL

# EIViI5SiON TEST SUIViMARY

PLANT : Daitil

~ 

# , Dallzs, TX DATE : 9•Jui-03 

# PLACE : Plant 4 Scrubber RUN# : 1


# TEST DURATION (NIINUTES) : 60 L1QU(D COLLEC T ED (mis) : 0 

# NOZZLE DIAMETER (INCH.) : 0 S02 Sample 1Neight, mg: 0 METER COEFFICIENT (Y) : 0.944 0 

# PITOT COEFFICIENT (Cp) : 0 STATIC PRESSURE (in. H20) : 0 GAS METER VOL.(Cu.Ft.) : 1.818 PERCENT CO2 : 0 BAROMETRIC PRESSURE ; 29.5 PERCENT 02 0 PERCENT CO : 0



# FLowS SAMPLED VOLUME (S T D. CU.FT.): 1.6737 S02, ppm: 0.0000

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 0 0.00 72 72 

# 2 0 72 72 3 0 72 72 4 0 73 73 5 0 73 73 6 0 73 73 7 0 73 73 8 0 74 74 9 0 75 75 10 0 75 75 11 0 75 75 12 0 76 76

#DIV/0! 0.0000 0.0000 73.5833 73.5833 73.5833



# 2R7.

# EMISSlON TEST SUMMARY

?LANT : Da

~~ 

## iie, Da'las, TX DATE : 9-Ju1-03 PLACE : Plan ~ 

## 4 Sct•ubber 

# RUNn : 2
TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 0 

# NOZZLE DIAMETER (INCH.) : 0 S02 Sam'ple Weight, mg: 0 METER COEFFICIEN T(Y) : 0.944 0 P1TOT COEFFIC(ENT (Cp) : 0 STATIC PRESSURE (in. H20) : 0 GAS METER VOL.(Cu.Ft.) : 1.843 PERCENT CO2 : 0 3AROMETRIC PRESSURE : 29.5 PERCENT 02 : 0 

# PERCENT CO 0



# FLOWS SAMPLED VOLUME (STD. CU .FT.): 1.6694 S02, ppm: 0.0000

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.



# deg F I N L LET OUTLET

1 0 0.00 82 82 

# 2 0 81 81 3 0 81 81 4 0 82 82 6 0 82 82 6 0 82 82 7 0 82 82 8 0 83 83 9 0 83 83 10 0 83 83 11 0 83 83 12 0 84 84

#DIV/0! 0.0000 0.0000 82.3333 82.3333 82.3333



# ~

# EMISSION TEST SUMN[ARY

PLANT : Daitiie, Dailas, TX DATE : 9-Ju1-03 PLACE : Plant 4 Scrubber RUN# : 3
TEST DURATION (MINUTES)

: 

# 60 LIQUID COLLECTED (mis)

: 

# 0 NOZZLE DIAMETER (INCH.)

: 

# 0 S02 Sample Vl/eigh#, mg: 0 METER COEFFICIENT (Y)

: 

# 0.944 0 PITOT COEFFICIENT (Cp)

: 

# 0 STATIC PRESSURE (in. H20)

: 

# 0 GAS METER VOL.(Cu.Ft.)

: 

# 1.857 PERCENT CO2

: 

# 0 BAROMETRIC PRES'SURE

: 

# 29.5 PERCENT 02

: 

# 0 PERCENT CO

: 

# 0

FL01NS SAMPLED VOLUME (STD. CU .FT.): 1.6818 S02, ppm: 0.0000

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 0 0.00' 86 86 2 0 8-3 83 3 0 82 82 4 0 82 82 5 0 82 82 6 0 82 82 7 0 82 82 8 0 82 82 9 0 82 82 10 0 82 82 11 0 82 82 12 0 82 82

#DIV/0! 0.0000 0.0000 82.4167 82.4167 82.4167



# 28.9

# } ' FIELD D ATA

PL ANT: 

# DAi.: -•_ 1' ~ 

# . ._ ~ ~~ ~ ~~ 

# REFETITION: LOCATION (aOURCE r): ~~1~,~~~- r~

~ 

### ~,~, f

~ J ~~ ~ f ~~ 

# INEPIsti GERS OPERATOR: ~'~~ ~ 

# T'r'

~ 

# .. ~ 

# Initial Final 

# SANPLE TrZAIN ~: ~~ 

# ; j } r ~,.~.~ F 

# :q1 METER BOX r: -'- ~ J i~2 

# B AROMET2IC'PRESSURE: ' ~= ~ 

# ) c AMBIENT TEMPERA i

iJRE:. ', 7 2.—

~ 

# _ I ~ 

# 01'4 ASSUINIED MOIS'ru

- RE: - - 

# u 5 PROBE LENGTH: —": o Z — 1 -7 =b NOZZLE DL4h'IETER: ~ 

# STACK D

~ 

# TER: ME•TER ~ 

# H: ~

. . ;.

.. 

# CO2 

# 02

, 

# C S'ACTOR: METER CO-EF'FICIEN'I': FILTER TARE: ' PRE-TEST LE.4K CHECK POST-TEST LEA,B'. CHECh'.. Ivieter: cu.ft. @ in. HG

, 

# Meter: Q. © cu.ft. @ in. HG

~ 

## ;rn+ n

. ;,, TJ7n•: Fitntv (Q

~ 

## . 'in. x20

, ~ 

# st

~ 

# ii

~ 

# '"

~ 

# '

3 ~~ zes ~ ~-~ 

# _ ~e`i . 3~



### ~ c'" _ie. : y t ' ~ 

# -"'

~ 

# . _.

,. ~t . ~ `Fi~. '~'



### a, ~ux•~~'~~~~ •



### . u ~ 'et

. ~~ . ,~ ~



### u c '

~ cm. m 

### Txsno " ~ 

# •

a 

# .t

. ~ 

### ~ ~ ~ •

. . 

### ~ . ! 

### ~~~ ~ . ~~ • ~ ~. i

. 

## f I 

# ~ ,, I J ! 

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### ------ ORIFICE

CALIBRATION FACTOR dH Q Value Variation 

### (in H20) (in 1-120) 0.000 0.0000 0.000 0.000 0.000 0.000



### 0.000 <------ Average dl

- tQ Arrnstrong Envirorntnental Inc.

EPA Melliod G

OriGce Melhod 

### Cnglislt Meler Box Unils, Eriglisli K' Factor
;ox r Dry Gas Meler Date: -------- ------ ---------- > July 11, 2003 3909 l3aromeliic Pressure: ----------> 29.78 flteorelical Critical Vacutan:---> 13.91 (in. (-Ig) CONVERSION FAC 1'(}RS
1 rnnt Hg : 0.13330 kPa 1 cin = 0.39370 incii t mrn ¢ 0.03937 inch 1 cu 1t - 28.32 liters



### TAP For valid lest resuils, the Actual Vacuum should be 1 lo 2 in. 1-19 greater Itian ltie Theorelical Crilicai Vacuurn sliown above. TAf

~ 

### The Critical Oritice Coef(icient, K', must be entered in Englislt units, (1t)"3'(deg R)"0.51((in.Hg)'(min)).

---------------- DRY GAS METER READINGS ---------------- -CRITICAL ORIFICE READINGSTheorelical Crilical Vacuum:---> 14.05 (in. Hg) 

## Voluine Volume Volurrne Initial Temps. Flnal Teinps. Orifice IC Orifice Actual -- Ambient Temperalure -- DGM DGM Anibierrt Time Initial Final Tolal lniel Oullet Inlet Outlel Serial# Coetficient Vactluttt Initial Final Average Oullet Overall Temp ) (rnin) (cu (t) (cu 10 (cu fl) (deg F) (deg F) (deg F) (deg F) (number) (see above) (in Hg) (deg F) (deg F) (deg F) (deg R) (deg R) (deg R) .00 5.00 16.716 1G.917 0.201 87.0 87.0 87.0 87.0 16907 0.029 23.0 87.0 87,0 87.0 547.0 547.0 547.0 .00 5.00 16.917 17.118 0.201 87.0 87.0 87.0 87.0 - 16907 0.029 23.0 87.0 87.0 87.0 547.0 547.0 547.0 .00 5.00 17.118 17.320 0.202 87.0 87.0 87.0 87.0 16907 0.029 19.5 87.0 87.0 87.0 547.0 547.0 547.0

. .......................................... RESULTS uN.w...A...A..AA.A........w......u..uAAA.aw...A



### GAS METER --- --------- ORIFICE --------- - - DRY GAS METER --

IF_ VOLUME VOLUME VOLUME VOLUME CALIBRATION FACTOR :CT CORRECTED CORRECT CORRECT NOMINAL Y :td) Vm(std) Vcr(st(l) Vcr(sld) Vcr Value Variatiorn i (t) (lilers) (cu ft) (liters) (cu ft) (number) (nurrnber) 93 0.0 0.182 0.0 0.190 0.945 0.002 93 0.0 0.182 0.0 0.190 0.945 0.002 9d 0.0 0.182 0.0 0.190 0.941 -0.003
Average Y ----- --> 0.944

or Calibralion Factor Y. lhe ralio of lhe reading of the calibralion rneler to the dry gas rneter, eptable lolerance of individual valties from the average is +-0.02.


### Oririce Catibralion Faclor dHQ, Ihe orifice difJerenl'aI pre sure in inches of H20 that equates to 0.75 cfm of air :8 F and 29.92 inches oi Hg, accepla e-tdlerance 

# ~ f i ividual v'lues frorn lhe average is'+-0.2.
,



### ~ ~ J ~ ~ ~~ , 11 

# U SIGNED:



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# i ~

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# C APEX INSTRUMENTS VUA ORIFICE ADAPTER CAI,IBRATION

C
, librallon In to r malion

WTM Modet Number At.17

i WTM Serial rlvnibcr 16907

_

I IWTM Canrar>:r 1.00000 Faclors/Converstons

Sld Temp 293 t~

Sld Press 760.00 nun I ig

t( t 0.306 Klotut tiy Callbrallort ConJitlons

Uale 

# I
- rime 07/10/03 16:30

Baronictric Prassure 749.0 nunt li0

Tlieorellcal Critical Vacuum' 353.5 mm Fig

Calibrallon Tecltnlcian RM 'Thc Crilical Uriflee COciticianl, W. Itt rnglish usiits, (1t a ' ° R"'jl(irr.Hy'min). `The Critical Oritice Coefficient, K', in Metric units, (L9CU(rnrnily'rrtln). HOTE: VOLUME IN LITER$

Calibration Oata Results

_ Wel Test Meler VUAAdaptcr Run a Orilice

Serialq Run Tlme

Elapsed Volunm

4+ilial Voiume

Flrral Voiume

Tolal Temperalwo

Initlal Temperature

Final Amb Tomp

Inival Amb Temp

Finai Aclual

Vaeuum Coettictent

Metric Unils - Coefticlarnt

Englisit Units % Varialion

rroorr Avg

_ (U r — (VI+) IVMr) (V.) ( 1 .+) (t.r1 ( 1 .40 (1-" 0 ) K' IC (<0.5 1 ,6)
min L L L ° C 'C 'C 'C mnt IHg see above' see above %
1 

### K4-14-03 G 1 306.025 312.500 6.475 30 30 29 

### 29 597 0.0239 2.871E-02 0 

### .17
2 K4-14-03 G 312.500 316.960 6.460 30



# 1 30 29 20 610 0.0230 2.063E-02 -0.11 3 K4-14-03 6 310.960 325.420 6.460 30 30 29 30 610 0.0230 2.064E-02 _0.06 0.0238 2.066E-02



## IEquation lo Calculate.Standardized Flowrate ^

~ I 

### (Given Ambient Barornetric'Pressure and Absolute 'rernperalure Conditlons: Pbar & TarntKabs)):

Qcr(sld)=K- 

## , * Pbar/Tamb(abs) 

## ziz I cerlily lliat orilice set number /C

~ Z 1

– • 1 ' <1~ '6 2

~ fJ ' was tesled in accordance willh Ilte US EPA Melbod 5 standards. Sxa tttc Coc:e ol Feclorao,

' ulititions, litie 40, part 6 0; Ahpendix A. Meilltod

' 5, Item 7.2.
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Summary of Sulfur Dioxide Analyzer Calibrations and Bias

Plant: Daltile Source: Plant 4 Scrubber Date: 719103



# Analyzer Calibratrion Data
Cyiinder Analyzer Absolute % Span Value Response Difference Zero Gas 0 0.15 0.15 0.25 Mid Range 25.7 25.7 0 0 High Range 50.7 50.65 -0.05 -0.08333



# System Calibration Bias and Drift Data

Analyzer Initiai Values Final Values Drift Average Caiibration System System System System Calibration Response Caiibration Calibration Calibration Calibration Values

Response Bias Response Bias

Run #1 Zero Gas 0.15 0.98 0.005 0.23 0.133333 0.083333 0.205

Upscale 25.7 24.85 -0.14167 23.53 -3.61667 -2.2 24.19
Average S02 Concentration: 0.17 Corrected S02 Concentration: -0.0375 (cquation 6C-1)

Run 92 Zero Gas 0.15 0.23 0.013333 -0.13 -0.46667 -0.6 0.05

Upscale 25.7 23.53 -0.36167 23.9 -3 0.616667 23.715
Average S02 Concentration: -0.13 Corrected S02 Concentration: -0.19548 (Equation 6C-1)

Run #3 Zero Gas 0.15 -0.13 -0.04667 -0.05 -0.33333 0.133333 -0.09

Upscale 25.7 23.9 -0.3 23.5 -3.66667 -0.66667 23.7



# Average S02 Concentration: -0.1 Corrected S02 Concentration: -0.0108 (Equation 6C-1)



# Q Page 1 

# ~ 

# 26

### 7110103 Calii7ratfons

Datei7irne CO S02 ^tm/ddlyy n


## ~ :mt 

## ~ :ss ppm pprn 07109103 Oa:33:3: 0.1 0.2
07109103 03:33:45 0.1 E1.2 Zera IN12 07109/03 09:33:55 0.0 0.1 07/09/03 09:34:05 0.1 0.1 07/09/03 09:34:15 0.1 30.2 07109/03 09:34• 

# ~ 5 0.1 35.5 07/09/03 09:34:35 0.1 43.2 07109/03 09:34:45 0.0 47.1 07/09/03 09:34:55 -0.3 47.8 07/09/03 09:35:05 -0.3 48.3 07109103 09:35:15 -0.4 48.8 07/09103 09:35:25 -0.3 49.1 07/09/03 09:35:35 -0.4 49.4 07/09/03 093S:45 -0.4 49.6 07109/03 09:35:55 -0.2 49.7 07/09/03 09:36:05 -0.3 49.9 07/09103 09:36:15 -0.2 50.1 07109/03 09:36:25 -0.2 50.1 07109103 09:36:35 -0.2 50.1 07/09/03 09:36:45 -0.2 50.2 07/09/03 09:36:55 -0.1 50.3 07/09/03 09:37:05 -0.1 50.5 07/09/03 09:37:15 -0.1 50.4 07/09/03 09:37:25 -0.1 50.6 07/09/03 09:37:35 -0.1 50,6 07/09103 09:37:45 -0.2 50.6 07/09/03 09:37:55 -0.3 50.7 50.7 ppm S02 07/09103 0938:05 -0.2 50.7 07/09103 09:38:15 -0.3 50.6 07J09/03 09:38:25 -0.3 50.7 07109/03 09:38:35 -0.3 50.6 07109103 09:38:45 -0.1 50.0 07/09/03 09:38:65 -0.2 47.9 07/09103 09:39:OS 0.0 43.5 07/09/03 09:39:15 0.0 37.7 07/09/03 09:39:25 0.0 31.6 07/09/03 09:39:35 0.0 26.4 07/09/03 09:39:45 0.1 22.5 07/09103 09:39:55 0.1 19.5 07/09/03 09:40:05 0.1 17.0 07109/03 09:40:15 -0.1 15.5 07/09/03 09:40:25 -0.1 15.0 07/09103 09:40:3S -0.1 15.1 07/09/03 09:40:45 -0.2 15.7 07/09103 09:40:55 0.0 16.6 07/09!03 09:41:05 -0.1 17.5 07/09/03 09:41:1 5 -0.2 18.4 07/09/03 09:41:25 -0.1 19.3 07/09/03 09:41:35 -0.2 20.2 07/09/03 09:41:45 -0.1 21.0 07I09/03 09:41:55 -0.3 21.4 07/09/03 09:42:05

- 0.2 22.0 07/09/03 09:42:15 -0.2 22.6 07/09/03 09:42:25 -0.2 23.1 07/09/03 09:42:35 -0.2 23.6 07/09/03 09:42:45 -0.1 24.0 07/09/03 09:42:55 0.0 24.3 07/09/03 09:43:05 0.1 24.5 07/09/03 09:43:1 5 0.1 24.7 07109/03 09:43:25 0.1 24.8 07109/03 09:43:35 0.2 24.9 07/09/03 09:43:45 0.3 25.0 07/09/03 09:43 :55 0.2 25.2 07/09/03 09:44:05 0.0 25.3 07/09/03 09:44:15 0.1 25.4 07J09/03 09:44:25 0.2 25.5 07/09/03 09:44:35 0.4 25:6 07/na103 09:44:45 0.2 23.7 07/09/03 09:44:55 0.2 25.7 25.7 pprn S02 07/09/03 09:45:05 0.2 25.7



### Page1



# ~ ~~ 7

### 711 0703 Caf , bsafions

07/09/03 09:45:15 0.2 25.7 07/09103 09:45:25 0.3 25.7 07/09103 09:45:35 0.3 26.5 07109!03 09:45:45 0.2 25.6 07/09/03 09:45:55 0.2 25.6 07109J03 09:46:05 0.2 25.6 07/09/03 09:46:15 0.2 25.5 07109/03 09:46:25 0.1 25.5 07/09103 09:46:35 0.0 25.2 07/09/03 09:46:45 0.1 24.6 07/09/03 09:46:55 0.2 23.2 07109103 09:47:05 0.1 21.3 07109/03 09:47:15 0.3 19.3 07109/03 09:47:25 0.3 17.5 07/09103 09:47:35 0.3 15.8 07/09/03 09:47:45 0.3 14.3 07/09103 09:47:55 0.2 12.9 07/09iO3 09:48:05 0.3 11.5 07/09/03 09:48:15 0.3 10.5 07/09/03 09:48:25 0.3 9.6 07/09/03 09:48:35 0.2 8.7 07/09/03 09:48:45 0.3 7.8 07/09/03 09:48:55 0.2 7.2 07/09/03 09:49:05 0.2 6.8 07109/03 09:49:15 0.2 6.3 07/09103 09:49:25 0.2 5.8 07/09103 09:49:35 0.2 5.3 07109f03 09:49:45 0.2 4.9 07/09/03 09:49:55 0.2 4.5 07/09103 09:50:05 0.1 4.1 07109/03 09:S0:15 0.1 3.8 07109J03 09:50:25 0.2 3.6 07109103 09:50:35 0.0 3.3 07/09/03 09:50:45 0,0 3.1 07109/03 09:50:55 0.1 3.0 07109103 09:51:C5 0.1 2.9 07109103 09:51:15 0.0 2.8 07109103 09:51:25 0.2 2.7 07109103 09:51:35 0.0 2.3 07/09103 09:51:45 0.1 2.1 07/09/03 09:51:65 0.1 2:0 07/09/03 09:52:C5 0.1 1.9 07/09/03 09:52:15 0.1 1.9 07109J03 09:52:25 0.1 1.8 07109103 09:52:35 0.2 1.7 07/09/Gt3 09:52:45 0.3 1.6 07/09/03 09:52:55 0.3 1.5 07r09/03 09:53:05 0.3 1.4 07/09/03 09:53:15 0.3 1.4 07/09/03 09:53:25 0.2 1.3 07/09/03 09:53:35 0.3 1.2 07109l03 09:53:45 0.2 1.1 07/09/03 09:53:55 0.2 1.2 07/09103 09:54:05 0.2 1.2 07/09/03 09:54:1 5 0.2 1.1 07109/03 09:64:25 0.1 1.0 07/09103 09:54:35 0.1 0.9 07/09/03 09:54:45 0.0 0.5 07109/03 09:54:65 0.0 0.3 07109/03 09:55:05 0.0 0.2
07109103 04:53:15 -0.1 0.2 07/09/03 09:55:25 0.0 0.2 07/09/03 09:55_35 0.0 0.1 07/09103 09:55:45 -0.1 1.8 07/09103 09:55:55 0.0 3.1

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- v 1 4.7 07/09/03 09:56:15 -0.2 6.7 07/09/03 09:65:25 -0.1 8•7 

### 071 ,, 91n3 09:56:35 -0.1 10.7 07109103 09:56:4 5 -0.1 12.6 071J9103 09:55:5 5 -0.1 14.2 07, 1 0 1 o;03 09:57:05 0.0 15.6 07139103 09:5;' : i S 0.0 15.9 

### Zero Bias

Page 2 

# ~ 

# P7110103 Calib,-atior.s

07/09103 09:57:25 0.0 18.0 07/09103 09:57:35 0.1 19.1 07J09/03 09:57:45 0.0 20.0 07/09103 09:57:55 0.1 20.7 07/09/03 09:58:05 0.2 Z1.2 07/09/03 09:58:15 0.1 21.8 07/09/03 09:58:25 0.1 22.3 07/09103 09:58:35 0.0 22.8 07/09/03 09:58:45 0.1 23.1 07109103 09:58:55 0.1 23.5 07/09/03 09:59:05 0.1 23.7 07/09103 09:59:15 0.0 24.0 07/09/03 09:59:25 -0.2 24.2 07/09103 09:59:35 -0.2 24.4 07/09/03 09:59:45 -0.3 24.5 07109/03 09:59:55 -0.2 24.5 07109/0310:00:05 -0.3 24.6 07/0910310:00:15 -0.2 24.7 07/09J0310:00:25 -0.1 24.8 07/0910310:00:35 -0.1 24.8 07/0910310:00:45 -0.1 24.8 07/0910310:00:55 -0.2 24.9 07/09/0310:01:05 -0.3 25.0 07/0910310:01:15 -0.3 24.8 07109/0310:09:25 -0.1 24.7 

### 0710910310:09:35 -0.1 24.7 07/0910310:01:45 -0.2 24.8 07109/0310:01:55 -0.2 24.8 0710910310:02:05 -0.4 24.9 0710910310:02:15 -0.4 24.9 0710910310:02:25 -0.2 24.9 07/09/0310:02:35 -0.1 24.7 07/0910310:02:45 0.1 23.9 07/09/0310:02:55 0.2 22.6 0710910310:03:05 0.1 21.0 07J0910310:03:15 0.1 18.9 07/09/0310:03:25 0.1 17.0 07/0910310:03:35 0.1 15.4 07/0910310:03:45 0.1 14.2 07/0910310:03:55 0.0 13.1 07/0910310:04:05 0.0 12.1 07/0910310:04:15 0.1 11.2 07/0910310:04:25 0.0 10.5 07/09/0310:04:35 0.0 9.7 07/09/0310:04:45 0.1 9.1 07/09/0310:04:55 0.1 8.4 0710910310:05:05 0.0 7.7 07109/0310:05:15 0.0 7.2 07/0910310:05:25 0.1 7.0 07/0910310:05:35 0.0 6.5 07/09/0310:05:45 0.0 6.1 07/09/0310:05:55 0.0 5.8 07/09/0310:06:05 -0.1 5.5 07109103 10:06:15 0.1 5.1 07109/0310:06:25 0.0 4.8 07109/0310:06:35 0.0 4.5 07/0910310:06:45 0.0 4.3 07109/0310:06:55 0.0 4.0 07/09/0310:07:05 0.0 3.8 07/0910310:07:15 0:0 3.6 07/0910310:07:25 0.0 3.5 07109103 10:07 :36 0.1 3.5 07/09/0310:07:45 0.2 3.3 07/09/0310:07:55 0.2 3.2 071091e310:08:05 0.0 3.1 07/0910310:08:15 0.0 3.0 0710910310:08:25 -0.1 2.9 

### 25.7 ppm $02 Bias

Paae 3 

# ~ 2g9

### 7110/03 Run #1

Date!?ime CO S02 

### mcrsldd'Yp• hh:mm:ss p2m, purn 07/09/03 10:11:55 0. ; 1.1 07/0910310:12:05 0.1 1.1 07109103 10:12: •. 5 0.9 1.0 07/0910310:12:25 3.7 1.0 0710910310:12:35 6.8 1.0 0710910310:12:45 9.2 1.0 07/09/03 10:12:55 10.8 1.0 07109/0310:13:05 11.7 0.9 

### 07/09l03 111: IJ:15 I2.8 V.7 07/09/0310:13:25 13.7 0.8 07/09/0310:13:35 14.5 0.8 07/09/0310:13:45 15.3 0.8 07109/0310:13:55 16.0 0.8 07/09/0310:14:05 16.5 0.8 07/09/0310:14:13 16.5 0.7 07/0910310:14:25 16.7 0.7 07/0910310:14:35 17.0 0.7 07/09/03 10:14:45 17.1 0.7 07/0910310:14:55 17.2 0.7 07/09/0310:15:05 17.2 0.7



### Start Run #1 07/09/0310:15:15 17.0 0.7 07109103 10:15:25 17.0 0.7 0 7/09/ 0 3 10 :15: 3 5 17.1 0.6 07/09/03 10:15:45 17.2 0.5 07109/0310:15:55 17.5 0.6 07/09/0310:16:05 17.6 0.7 07/0910310:16:15 17.5 0.8 07/09103 10:16:25 17.5 0.6 07/09/0310:16:35 17.3 0.6 07109/0310:16:45 17.3 0.6 07109/03 10:16:55 17.1 0.5 0710910310:17:05 17.1' 0.5 07109103 10:17:15 17.3 0.4 07109103 10:17:25 17.4 0.4 07/09103 10:17:35 17.5 0.4 07/0910310:17:45 17.2 0.4 07/09/0310:17:55 17.1 0.5 07/09103 10:18:05 17.0 0.5 07/09/03 10:18:15 17.2 0.6 07/09/0310:18:25 17.3 0.5 07109/0310:18:35 17.3 0.5 07109/0310:18:45 17.6 0.3 07109/0310:18:S5 17.7 0.3 07/09/0310:19::5 17.7 0.3 07109J0310:197'15 18.0 0.4 07/09103 10:19:25 18.1 0.4 07/09103 10:19:35 18.1 0.3 07109/0310:19:45 18.3 0.3 07109/0310:19:55 18.5 0.2 07109/0310:20:05 18.4 0.2 07/09/0310:20:15 18.2 0.2 07/09/03 10:20:25 18.1 0.2 07/0910310:20:35 17.9 0.3 07/0910310:20:45 17.8 0.3 07/0910310:20:55 17.6 0.4 07109/0310:21:05 17.5 0.3 07/0910310:21:15 17.3 0.3 07/09/0310:21:25 17.3 0.3 07/09103 10:21:35 17.3 0.3 07/0910310:21:46 17.4 0.4 07109/0310:21:55 17.4 0.4 07/09/ 0 .310:22:05 17.4 0.3 07109/03 10:22:15 17.4 0.2 0710910310:22:25 17.6 0.2 07/0910310:22:35 17.8 0.2 07/0910310:22:45 17.9 0.3 07i0910310:22:55 18.2 0.2 07/09, 1 0310:23:05 17.9 0.3 07/0910310:23:95 18. 1 1 0.3 0710910310:23:25 18.2 0.2

Paae 1 

# ~ 3007110103 Run t1

07109/0310:23:35 18.7 0.2 0710910310:23:45 20.0 0.2 07J0910310:23:55 20.9 0.2 07/0310310:24:05 21.6 0.2 07/09/0310:24:15 21.8 0.2 0

~ 7109103 10:24:25 22.3 0.2 0710910310:24:35 22.5 0.2 0710910310:24:45 22.3 0.2 07/09l0310:24:55 21.8 0:2 07/0910310:25:05 21.2 0.2 07/0910310:25:15 20.3 0.1 07109J0310:25:25 19.3 0.1 07109/0310:25:35 18.4 0.2 07J09/0310:25: 45 18.1 0.3 0710910310:25:55 17.8 0.4' 07/0910310:26:05 17.7 0.4 071091031026:15 17.6 0.3 07/0910310:26:25 17.3 0.2 07/09103 10:26:35 17.1 0.2 0710910310:26:45 17.0 0.1 07/09/0310:26:55 17.0 0.2 07/09/0310:27:05 17.0 0.2 0710910310:27:15 17.0 0.2 07/0910310:27:25 16.7 0.2 0710910310:27:3S 16.4 0.2 0710910310:27:45 15.9 0.2 07109/0310:27:55 15.5 0.2 07/03/0310:28:05 15.4 0.3 0710910310:28:15 15.3 0.2 07/09103 1028:25 15.1 0.2 0710910310:28:35 15.0 0.3 07/09J0310:28:45 14.8 0.3 07/09/0310:28:55 15.0 0.2 0710910310:29:05 14.9 0.2 0710910310:29:15 0.2 07/09/0310:29:25 15.0 02 0710910310:29:35 15.0 0.1 07/09/0310:29:45 14.9 0.2 0710910310:29:55 15.1 0.3 07/09/03 90:30:C5 15.3 0.2 0710910310:30:15 15.3 0.2 07/09/0310:30:25 15.5 0.2 07/09/0310:30;35 15.5 0.2 07/09/0310:30:45 15.3 0.2 07109/0310:30:55 15.2 0.1 0710910310:31:05 14.9 0.2 07/09/0310:31:15 14.8 0.1 07109/0310:3125 14.7 0.1 07/09/0310:31:35 14.6 0.1 07109103 10:31:45 14.7 0.1 07109/03 10:31:55 14.6 0.2 07/09/0310:32:05 14.6 0.2 07; 09/03 10:32:'t 5 ', 4.7 0.2 07/0910310:32:25 14.9 0.1 07/09/03 10:32:35 15.1 0.2 07/09l0310:32:45 15.4 02 07/09J0310:32:55 15.4 0.2 07/0910310:33:05 15.2 0.2 07J0910310:33:15 75.7 0.1 07/0910310:33:25 14.8 0.1 07109/03 10 :33:35 14.8 0.2 07/0910310:33:45 14.8 0.2 07J09/03 10:33:55 14. - r- 0.1 07109/0310.34:05 14.5 0.1 07/09/03 10:34:1 5 14.4 0.1 07109/0310:34:25 14.4 0.2 07109103 1 0:34:35 14.4 0.1 07J09/0310:34:45 14.3 0.1 07109/0310:34:55 14.3 0.1 07109/03 1 D:35:05 14.4 0.1 07/09, 1 03 ; 0:35:15 14.4 0. 4 07109.r0310:35:25 14.5 0.1 07/09/0310:35:35 14.7 0.1 07J09, 1 03 10:35:45 1 ".7 0.1

Page 2 *a 3017! i 0103 Run #1

C7109/0310:35:SS 14.8 0.1 37109/03 10:36:05 i 4 .3 0.1 07/09J03 10:30:' S 14.8 0.1 37/081C310:3$:25 14.9 0.1 07109f03'0:36:35 14.9 0.1 07/09/03 10:36:45 14.7 0.1 07/09/03 10:36:55 14.7 0. ; 07109103 10:37:05 14.5 0.1 07!09.iO310:37:15 14.4 0.1 07/0910310:37:25 14.2 0.2 07/09/0310:37:35 14.0 0.1 07/09/0310:37:45 13.9 0.2 07109/0310:37:55 13.7 0.1 07/0910310:38:05 13.8 0.1 0710910310:38:15 14.0 0.1 07/0910310:38:25 14.1 0.1 C71091C31J:38:35 14,0 0.1 07/0910310:38:45 14.0 0.1 07/09/03 10:38:55 14.1 0.1 07/09/03 1 0:39:05 14.1 0.1 07/09/0310:39:15 14.2 0.1 07/0910310:39:26 14.0 0.1 07109/0310:39:35 14.2 0.1 0710910310:39:45 14.3 0.2 07/09/0310:39:55 14.8 0.2 07/09/0310:40:05 14.9 0.2 07/09/0310:40:15 15.2 0.2 0710910310:40:25 15.4 0.1 07/09/03 10:40:35 15.4 0.1 07109/0310:40:45 15.6 0.1 07/09/0310:40:65 15.4 0.1 07/09/0310:41:C5 15.4 0.1 07/0910310:41:15 15.3 0.1 07/0910310:41:25 1S.4 0.2 07109/0310:41:35 15.5 0.2 07/0910310:41:-05 15.6 0.2 07109/0310:41:65 15.7 0.2 07/09103 1 C:

~ 2:05 15, 0 0 0.2 0710910310:42:15 15.7 0.1 07/0910310:42:25 15.6 0.1 07/09/0310:42:35 15.5 0.2 07/09/03 10:42:45 15.5 02 07/09/0310:42:55 15.6 0.1 07/09/0310:43:05 15.7 0.1 07/09/0310:43:15 15.8 0.1 07/09/0310:43:25 16.0 0.2 07109/C310:43:35 16.3 0.2 07/0910310:43:45 16.3 0.2 07/09/0310:43:55 16.3 0.2 07/09/0310:44:05 16.4 0.2 07/0910310:44:15 16.4 0.1 07/09/0310:44:25 16.3 0.1 0 7109/03 10:44 :35 16.1 0.1 07/09/0310:44:45 16.0 0.1 07/09/0310:44:65 15.9 0.1 07/09/0310:45:C35 15.8 0.1 07/09/0310:45:15 15.9 0.1 07/09/0310:45:25 15.9 0.2 07/09/C310:45:35 16.1 0.1 07109/0310:45:45 15.9 0.1 0710910310:45:55 15.9 0.1 07/09/03 10:46:05 16.0 0.1 07/09103 10:46:15 16.1 0.1 07/09/0310:46:25 16.1 0.1 C 7109/C 3 10:4 6:3 5 16.1 0.1 07109/0310:46:45 15.8 0.1 07/09!03 10:46:55 15.5 0. 1 1 /091031 1 0:47:C5 15.4 C.1 07/09/0310:47:15 15.4 0.1 07/0910310:47:25 15.5 0.1 07/0910310:47:35 15.7 0.1 07/0910310:47:45 15.6 0.1 07/09!0310:47:65 15.9 0.1 07/0910310:48:05 16.0 0.1

Page 3 

# ME c3 () 2

### 7/10103 Zun Z 1

0 7109/0 3 10 : 4 8:15 16.1 0.1 0710910310:48:25 16.2 0.1 07109/03 10:48:35 16.2 0.1 07/0910310:48:45 16.2 0.1 07/09/0310:48:55 16.2 0.1 07/09/03 90:49:05 16.4 0.1 07109/0310:49:15 16.4 0.0 07;09/0314:4925 16.5 0.0 07109/0310:49:35 16.2 0.1 07109/0310:49:45 16.2 0.0 0 7/09/03 10: 4 9: 5 5 16.1 0.0 07109/0310:50:05 16.3 0.1 07/09/0310:50:15 16.4 0.1 07/09/0310:50:25 16.5 0.1 07/0910310:50:35 16.6 0.0 07109/0310:50:45 16.7 0.0 07/0910310:50:55 16.5 0.1 07109/03 10:51:05 16.4 0.1 07109/03 10:51:15 16.0 0.1 07/09/0310:51:25 15.7 0.1 07/09/0310:51:35 15.3 0.1 07/09/0310:51:45 15.3 0.1 0,','0910310;51:55 15. ~ 0.1 07/0910310:52:05 15.0 0.0 07109103 10:52:15 15.1 0.0 07/09103 10:52 :25 15.1 0.0 07/09/03 10:52:35 15.1 0.0 07109/0310:52:45 15.1 0.1 07J09/03 1 D:52:55 14.9 0.1 07/0910310:53:05 14.9 0.0 07/09/03 10:53:15 14.9 0.1 07/0910310:53:25 1" 1 4 .9 0.1 07/09/0310:53:35 14.6 0.1 0710910310:53:45 14.4 0.1 07/09/0310:53:55 14.5 0.0 0710910310:54;05 14.3 0.1 07/09/03 10:54 :15 14.1 0.0 07/09/03 10:5 :25 14.3 0.0 07/09/0310:54:35 14.3 0.1 07/0910310:54:45 14.4 0.0 07109/0310:54:55 14.3 0.1 D7109/0310:55:05 14.6 0.1 07/09/0310:55:15 14.7 0.1 07/09/0310:55:25 14.9 0.0 07/09/0310:55:35 14.8 0.0 07/09/0310:55:45 14.7 0.1 07/09/03 40:55:55 14.5 0.0 07109/0310:56:05 14.5 0.0 07109/0310:56:15 14.6 0.0 07/09/0310:56:25 14.5 0.1 0710910310:56:35 14.8 0.0 07109/0310:56:45 14.9 0.0 07109/03 10:58:55 15.0 0.0 07/09/0310:57:05 15.5 0.0' 0710910310:57:15 15.9 0.0 07/0910310:57:25 16.0 0.0 07/09/0310:57:35 16.2 0.0 07/09/03 1 D:57:4 5 15.9 0.1 C7109/0310:57:55 15.6 0.0 07/09/0310:58:05 15.1 -0.1 07/09/03 10:58:15 15.1 0.0 07/0910310:58:25 14.9 -0.1 07/09103 10:68:35 15.1 0.0 07109/0310:58:45 15.2 0.0 07/0910310:58:55 15.6 0.1 07109/0310:59:05 15.6 0.0 07/09/0310:59:15 15.8 0.0 C710910310:59:25 15.6 0.0 0710910310:59:35 15.7 0.0 07/09/0310:69:45 15.5 0.0 07/0910310:59:55 15.3 0.0 07109/0311:00:05 15.3 0.0 07109103 1 1:00:15 15.4 0.0 07/09103 11:0 1

0 1 :25 15.7 0.0

Page 4 A* 303

..7110103 Run #1

07/09103 11:00:35 16.1 0.0 071091C3 i 1:00:45 i 5.= 'J.0 07/0910311:00:55 '15.7 0.0 07109/03 11:0 i:05 17.0 0.0 07109/0311:01:15 17.1 0.0 07109/03 11:01:25 17.0 0.0 07109/0311:01:35 16.9 0.0 07109/0311:01:45 16.8 0.0 0710910311:01:55 16.9 0.0 0710910311:02:05 16.7 0.0 07/09/03 11:02:15 16.4 0.0 07/09/0311:02:25 16.2 0.0 07/09/03 11:02:35 16.1 0.0 07109/03 1 'f :02 :45 162 0.0 07109/0311:02:55 16.2 0.0 0710910311:03:05 16.3 0.0 07109f03 11:03:15 16.4 0.0 07/0910311:03:25 16.3 0.0 07/0910311:03:35 16.2 -0.1 07/0910311:03:45 16.4 -0.1 07/09/0311:03:55 16.4 0.0 07109/0311:04:05 16.5 0.0 07I09/0311:04:15 16.2 0.0 07/0910311:04:25 16.2 0.0 07/09/03 11:04:35 16.1 0.0 0710910311:04:45 15.9 0.0 07/0910311:04:65 15.3 0.0 07109/0311:OS:06 15.1 -0.1 0710910311:05:15 15.0 -0.1 07/0910311:05:25 14.8 -0.1 07/0910311:05:35 14.8 -0.9 0710910311:05:45 15.1 -0.1 07109/0311:05:35 15.4 0.0 07109/0311:06:05 15.5 0.0 07/09/0311:06:15 15.6 0.0 07/09/0311:06:25 15.5 0.0 07/0910311:06:35 15.9 0.0 07109/0311:06:45 15.9 0.0 07109/0311:06:55 16.0 -0.1 0710910311:07:05 16.2 -0.1 07/0910311:07:15 16.1 -0.1 07/0910311:07:25 16.3 -0.1 07/09/0311:07:35 16.2 -0.1 07109/0311:07:45 16.2 0.0 07/09/0311:07:55 15.9 0,0 07/09/0311:08:05 15.8 0.0 07/0910311:08:15 15.7 0.0 0710910311:08:25 15.6 0.0 07109/0311:08:3S 15.3 0.0 07/0910311:08:45 15.0 0.0 07109J0311:08:55 14.7 0.0 ' 07/09/03 11:09:05 14.4 -0.1

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Stop Run
, "O1 0.17

07/09/0311:15:15 16.9 -0.2 07/0910311:15:25 16.8 -0.2 07/09/0311:15:35 16.7 -0.1 07/0910311:15:45 16.5 -0.1 0710910311:15:55 16.2 -0.2 07/09/0311:16:05 16.0 -0.2 07/0910311:18:15 15.9 0.2 0710910311:16:25 15.7 0.1 07/09/0311:16:35 15.6 0.2 07/0910311:16:45 15.6 0.3 07/0910311:16:55 15.6 0.2 07109/03 11:17 :05 15.5 0.2 07109103 11:17:15 15.5 0.3 07/09/0311:17:25 15.0 0.3 07109/03 11:17:35 15.0 0.2 07/0910311:17:45 14.9 0.2 07/09/0311:17:55 14.7 0.3 07/09/0311:18:05 13.7 0.3 07109/0311:18:15 12.4 0.2 07109/0311:18:25 10.8 0.2 07/09/0311:18:35 9.4 0.3 07/09/0311:18:45 7.8 0.2 07J09/0311:18:55 6.7 0.2 

### 07109/03 11:19:05 5.7 0.2 07/09/0311:19:15 4.8 0.3 07/09/03 11:19:25 4.3 0.3 07109/0311:19:35 3.8 0.3 07109/0311:19:45 3.3 0.4 07/0910311:19:55 2.6 0.4 07109/0311:20:05 2.0 0.2 07/09/03 1 1 20:15 1.4 0.1 07109/0311:20:25 0.7 0.1 0710910311:20:35 0.3 0.1 07/09/0311:20:45 0.3 0.1 0710910311:20:55 0.3 0.1 07/09/0311:21:05 0.3 0.1 07109/0311:21:15 02 0.1 07/09/0311:21:25 0.1 0.1 0710910311:21:35 0.0 0.1 07/0910311:21:45 0.0 0.1 07/09/0311:21:55 0.0 0.1 07/0910311:22:05 0.0 0.1 07109J0311:22:15 0.1 0.0 07/0910311:22:25 0.1 0.1 0710910311:22:35 0.1 0.4 07/09/0311:22:45 0.0 0.9 07/0910311:22:55 0.0 1.5 07/0910311:23:05 0.1 2.3 0710910311:23:15 0.0 3.1 07/09/0311:23:25 -0.1 3.8 07109/0311:23:35 -0.1 4.7 07109/0311:23:45 -0.1 5.6 07/09/0311:23:55 -0.2 6.4 07/09/0311:24:05 -0.2 7.2 07/09/0311:24:15 -0.3 6.1 07/09/0311:24:25 -0.3 8.9



### Page 6

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### Start Run 92 0710910311:50:05 47.B 0.6 07/0910311:50:15 47.6 0.7 07/09/0311;50:25 47.0 0.7 07/09/0311:50:35 45.5 0.6 07/09/031130:45 42.8 0.5 07/09/0311:50:55 39.5 0.5 07/0910311:51:05 36.0 0.4 07109/0311:51:15 32.5 0.3 07109/0311:51:25 28.4 0.2 07/09/0311:51:35 25.2 0.1 07J09/0311:51:45 23.0 0.1 07/09/0311:51:55 21.4 0.1 07109/0311:52:05 20.6 0.0 07109/0311:52:15 20.0 0.0 07/09/0311:52:25 19.7 0.0 07109/0311:52:35 19.7 0.0 07109/0311:52:45 19.8 0.0 07/09/03 11:52:55 19.9 0.0 07/09/0311:53:05 19.9 -0.2 07/0910311:53:15 19.5 -0.2 07/0910311:53:25 18.9 -0.2 07/09!0311:53:35 18.4 -0.2 0710910311:53:45 18.2 -0.3 0710910311:53:55 17.8 -0.5 07/09/0311:54:05 17.7 -0.5 07/0910311:54:15 17.6 -0.4 07109/0311:54:25 17.5 -0.5 07109/0311:54:35 17.4 -0.6 07/09/03 11:54:45 i 7.4 -0.2 07/09/0311:54:55 17.3 0.0 07/0910311:55:05 17.3 -0.1 07/09/0311:55:15 17.3 -0.1 07/09/0311:55:25 17.2 -0.1 0710910311:55:35 17.3 -0.1 07109/0311:55:45 17.2 -0.1 07/0910311:55:55 17.1 -0.1 0710910311:55:05 17.2 -0.1 07/09103 11:56:15 17.2 -0. i . 07I09/0311:56;25 17.1 -0.2 07/09!0311:55:35 17.2 -0.3 07/09J0311:55:45 17.2 •0.2

Page 1 3 n v 

# ~ -7110103 Run x2

0710910311:56:55 17.4 -0.2 0710910311:57:05 "7.5 -0.3 07/0910311:57:15 17.1 -0.3 07/091^311:67:25 17.2 -0.3 07/0910311:51 7 :35 17.1 -0.4 07109/0311:57:45 17.3 -0.4 07/09/0311:57:55 17.0 -0.4 07/09/03 11:58:05 17.1 -0.4 ' 07/09J0311:58:15 17.0 -0.4 07/0910311:5825 16.9 -0.3 07/09/0311:5w*:35 16.9 -0.4 07/09/0311:58:45 17.1 -0.5 07/0910311:58:55 172 -0.5 07/09/0311:59:05 17.4 -0.4 07/0910311:59:15 17.5 -0.4 07/0910311:59:25 17.7 -0.4 07/0910311:59:35 17.9 -0.5 07/0910311:59:45 18.0 -0.5 07/0910311:59:55 18.1 -0.5 07/09/0312:00:05 17.9 -0.4 07/09/0312:00:15 17.8 -0.4 07/09/0312:00:25 17.7 -0.2 07/09/0312:00:35 17.7 -0.1 07/0910312:00:45 17.7 -0.3 07109/0312:00:55 18.0 -02 07109/0312:01:05 18.0 -0.1 07 109/03 12:01:15 18.1 -0.1 07109/0312:01:25 17.9 -0.1 07/09/0312:01:35 17.7 -0.1 07109/0312:01:45 17.5 -0.1 07109/0312:01:55 17.2 -0.2 07109/0312:02:05 17.1 -0.2 07/09/0312:02:15 17.2 -0.2 07109/0312:02:25 17.2 -0.2 07/0910312:02:35 17.3 -0.2 0710910312:02:45 17.1 -0.1 07/09/0312:02:55 16.8 -0.1 0710910312:03:05 16.6 -0.1 07/09/0312:03:15 15.9 -0.1 07/0910312:03:25 15.6 -0.2 07/09/0312:03:35 15.3 -0.2 07109/0312:03:45 15.1 -0.2 07/09/0312:03:55 15.1 -0.1 07/09/0312:04:05 15.1 -0.1 07109/0312:04:15 15.3 -0.1 07109/0312:04:.25 15.2 -0.1 07/09/0312:04:35 15.3 -0.1 07/0910312:04:45 15.3 -0.1 07/09/0312:04:55 15.4 -0.2 07/09/0312:05:C5 15.4 -0.2 07/09/0312:05:15 15.5 -0.2 07/09/0312:05:25 15.6 -0.2 07/09/0312:05:35 15.8 -0.2 07109/0312:05:45 15.9 -0.2 07/09/0312:05:55 16.1 -0.1 07/0910312:06:0

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Paae 2

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### Run #2

07J09103 12:09:15 18.2 -0.2 07/09103 12:03:25 ' 8.4 -0.2 07109103 12:09:3-

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### 0710910312,1e;a6 1710

- 

### 0,9 07/09/D312:16:55 18.1 -0.1 07/09J0312:17:05 18.5 -0.1 07/09/03 12:17:15 19.3 -0.1 07109/0312:17:25 2C.2 -0.1 07/09/0312:17:3S 21.4 -0.1 07/09/0312:17:45 22.8 -0.1 07109/0312:17:55 24.1 -0.1 07/0910312:18:05 25.4 -0.1 07/09/03 12:18:1 S 26.7 -0.1 07J09/0312:18:2S 27.9 -0.1 07/09/0312:18:35 28.7 -0.1 07/09/0312:18:45 29.3 -0.1 07109/0312:18:55 30.0 -0.1 07/09/03 i2:19:06 30.8 -0.1 07/09/03 12:1 9:15 31.5 -0.2 07109/0312:19:25 32.1 -0.2 07109/0312:19:35 32.5 -0.1 07/0910312:19:45 33.0 -0.1 07/09/0312:19:55 33.0 -0.1 07/09/031220:05 33.0 -0.1 07/0910312:20:15 33.3 0.0 07/09!0312:20:25 33.6 0.0 0710910312:20:35 33.9 -0.1 07/09103 12:20:45 34.3 0.0 07/09/0312:20:55 3 4 1.3 -0.1 07109/0312:21:05 34.4 -0.1 07/0910312:21:15 34.5 -0.1 07/09/0312:21:25 34.4 -0.2

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### v7/09/

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### 312:'.3:15 24.9 -0.2 07/09/0312:33:25 25.5 -0.3 07/09/0312:33:35 26.5 -0.2 07109/0312:33:45 27.9 -0.2



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07,'09I0312:46:15 36.2 0.0 0710910312:45:25 37.0 -0.1 0710910312:45:35 37.5 -0.1 07/09/0312:46:45 3B.0 0.0 07/0910312:46:55 38.2 0.0 07/09/0312:47:05 38.4 0.0 07/0910312:47:15 38.5 0.0 0710910312:4725 38.0 0.0 07/09/0312:4735 37.5 0.0 07/0910312:47:45 37.5 -0.1 07/09/0312:47:55 37.7 -0.1 07/09/0312:48:OS 37.8 -0.1 07/09/0312:48:15 37.6 -0.1 07109/0312:48:25 37.5 -0.1 07109/0312:48:35 37.6 -0.1 07109/0312:48:45 37.4 -0.1 0710910312:48:55 37.1 0.0 07/09/0312:4905 36.4 -0.1 07/0910312:49:15 36.1 0.0 07/09/0312:4925 36.0 0.0 07/0910312:49:35 35.7 0.0 07/09/0312:49:45 35.3 0.0 07/0910312:49:55 35.1 -0.1

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### Page 6 

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# 313

### 7110103 Run 92

07109/0312:57:55 -0.6 14.7 07/09103 12:58:05 -0.8 07109/03 12:58:15 -0.9 15.4 0710910312:5S:25 -0.3 1 15.9 07109/0312:58:35 -0.8 16.3 0710910312:58:45 -0.9 16.6 07/0910312:S8:55 -1.2 16.9 07109/C3 12 :59:05 -1.0 17.2 07/0910312:59:15 -1.3 17.5 07/0910312:59:25 -1.0 17.7 07109/0312:59:35 -1.1 17.8 0710910312:59:45 -0.9 18.0 0710910312:59:55 -0.7 18.2 07/09/0313:00:05 -0.9 18.4 07109/0313:00:15 -0.9 18.6 07109/0313:00:25 -1.3 18.7 07i0910313:00:35 -1.3 18.9 07l09/0313:00:4S -1.2 19.0 07/0910313:00:55 -0.8 19.2 07/09/0313:01:05 -0.7 19.3 07/09103 13:01:15 -0.7 19.4 0710910313:01:25 -1.0 19.5 07i09103 13:01 :35 -1.0 19.6 07109/0313:01:4S -0.6 19.8 07/09/0313:01:5S -0.5 20.1 07/09/0313:02:05 -0.8 20.3 07/0910313:02:15 -1.0 20.9 07/0910313:C2:2S -1.3 21.0 07/09/0313:02:3S -1.5 21.1 07/09/0313:02:4S -1.2 21.4 07109/0313:02:55 -1.5 21.7 07/09/0313:03:05 -1.3 22.0 07/09/0313:03:15 -1.3 22.2 07/09/0313:03:25 -1.4 22.4 07/09/0313:03:35 -1.5 22.6 07/0910313:03:45 -1.5 22.9 07/0910313:0355 -1.6 23.0 07/09/0313:04:05 -1.7 23.0 07109/0313:04:15 -1.8 23.2 07109/0313:04:25 -1.7 23.3 07/09/0313:04:35 -1.6 23.4 07/09/0313:04:45 -1.7 23.7 07/09/0313:04:55 -1.7 23.9 07/09/0313:05:05

- 

### 1.8 23.9 07/09103 13:05:9 5 -1.9 23.9 07/09.'0313:05:25 -2.1 23.9 07109/0313:05:35 -2.4 23.9 

### 25.7 ppm S02

?age 7 

# ~ 

# 3147/10103 Run R3



### Date/Tims S02 mmlddlyy 

### hh:rnm:ss pDm 07/09/0313:11:35 4.3 07/09/03 1351:45 4.0 07/09/03 13:11:55 3.8 07109/0313:12:05 3.6 07/09/0313:12:15 3.4 07/09/0313:12:25 3.3 07109/0313:12:35 3.2 07/09103 13:12:45 2.9 07/09/03 13:12:55 2.8 07/09/0313:13:05 2.5 07/09103 13:13:15 2.4 07/0910313:13:26 2.2 07/09103 13:13:35 2.0 07/09/03 13:13:45 2.0 07/09/03 13:13:55 1.8 07/09/03 13:14:05 1.6 07/09/03 13:14:15 1.6 07/09/03 13:14:25 1.4 07J09/03 13:14:35 1.4 07/09/03 13:14:45 1.3 07/09/0313:14:55 1.2

Start Pun n3 07/09103 13:15:05 1.1 07/09/03 13:16:15 1.0 0710910313:15:25 0.9 07/09/0313:15:35 0.9 07/0910313:15:45 0.9 07109103 13:15:55 0.7 07l0910313:16:05 0.6 07109103 13:16:15 0.6 07J0910313:16:25 0.5 07/09/0313:16:35 0.4 07109103 13:16:45 0.3 07/09/03 13:16:55 0.2 07109/0313:17:05 0.2 07/09/03 13:17:15 0.1 07J09/0313:17:25 0.1 07J09/D313:17:35 0.1 07/09/03 13:17:45 0.1 07/09/0313:17:55 0.0 07/09/0313:18:05 0.0 07/09/0313:18:15 0.0 0710910313:18:25 -0.1 07109/0313:18:35 -0.2 07/09/0313:18:45 -0.1 07/09/0313:18:55 0.0 07/09/0313:19:05 0.0 07/09/0313:19:15 -0.1 07/09/0313:19:25 -0.1 07/09/0313:19:35 -0.1 07/09/0313:19:45 -0.2 07/09/0313:19:55 -0.1 07/09J0313:20:05 -0.2 07/09/0313:20:15 -0.3 07/09/0313:20:25 -0.3 07109/0313:20:35 -0.3 07/0910313:20:45 -0.4 07/09/0313:20:55 -0.4 07/0910313:21:05 -0.3 07/0910313:21:15 -0.3 07/09/0313:21:25 -0.4 07109/0313:21:35 -0.4 07/09/0313:21:45 -0.4 07/0910313.21.55 -0.4 07/09/0313:22:05 -0.5 07/09/0313:22:15 -0.3 07109I0313:22:25 -0.1 07/09/0313:22:35 0.0 07/09I0313:22:45 0.0 07/09/0313:22:55 0.0 07/09/0313:23:05 -0.2

. : 

# ri 15

Page 17110103 Rur V3

07/09103 13:23:1 5 -0.2 G710910313:23:25 -0.2 07/09103 1 3:23:35 - C. .1 0710910313:23:45 C.0 0710910313:23:55 -0.1 07/0910313:24:05 -0.2 07/09/0313:24:15 -0.1 0710910313:24:25 -0.1 0710910313:24:35 0.0 07109/0313:24:45 0.0 07109/0313:24:55 -0.1 07/0910313:25:05 -0.1 0710910313:25:15 -0.1 07/0910313:25:25 -0.1 0710910313:25:35 -0.2 0710910313:25:45 -0.1 07/09/0313:25:55 -0.1 07/09/0313:26:05 -0.1 0710910313:26:15 -0.1 0710910313:26:25 -0.2 07/0910313:26:35 -0.3 07/09/0313:26:45 -0.2 07/0910313:26:55 -0.1 07/09/0313:27:05 -0.1 07/09/0313:27:15 -0.1 07/09/0313:27:25 -0.1 07/09/0313:27:35 -0.1 07/0910313:27:45 -0.2 07/09/0313:27:55 -0.2 07/0910313:28:05 -0.2 07/0910313:28:15 -0.1 07/0910313:28:25 -0.1 07/09/0313:28:35 -0.1 07109/0313:28:45 -0.1 0710910313:28:55 -0.1 0710910313:29:05 -0.1 07/0910313:29:15 -0.2 0710910313:29:25 -0.3 07109/0313:29:35 -0.2 07109/0313:29:45 -0.2 07109/0313:29:55 -0.2 07/0910313:30:05 -0.2 07109/0313:30:15 -0.2 07109/0313:30:25 -0.2 07/091031330:35 -0.3 07/09/0313:30:45 -0.2 07/09/0313:30:55 -0.2 07/09/0313:31:05 -0.2 07/09/0313:31:15 -0.2 07/09/0313:31:25 -0.3 07/0910313:31:35 -0.2 07/09/0313:31:45 -0.2 0710910313:31:55 -0.3 0710910313:32:05 -0.3 07109/03 13:32:15 -0 3 07/09/0313:32:25 0.0 0710910313:32:35 0.0 07109/0313:32:45 -0.1 07109/0313:32:55 0.0 0710910313:33:05 0.0 07/09/03 9 3:33:15 0.0 07/09/0313:33:25 0.0 07/0910313:33:35 0.0 0710910313:33:45 0.0 07109J0313:33:55 0.0 07/0910313:34:05 0.0 0710910313:34:15 -0.1 0710910313:34:25 -0.1 07/0910313:34:35 -0.1

~ 7109/0.13:34:45 -0.1 07/09/0313:34:55 -0.1 07/0910313:35:05 •0.2 07/09/03 13:35:15 -0.1 07/0910313:35:25

- 0.1 

# 316
Page 27110103 Pun #3

0710910313:35:35 -0.1 07/0910313:35:45 -0.1 0710910313:35:55 -0.2 07109/0313:36:05 -0.1 0710910313:36:15 -0.1 0710910313:36:25 -0.1 07109/0313:36:35 0.0 0710910313:36:45 0.0 0710910313:36:55 0.0 07109/0313:37:05 0.0 0710910313:37:15 0.0 07109/0313:37:25 0.0 0710910313:37:35 0.0 07/0910313:37:45 0.0 07/0910313:37:55 0.0 0710910313:38:05 0.0 07109/0313:38:15 0.0 07109/0313:38:25 0.0 0710910313:38:35 0.0 07/0910313:38:45 0.0 0710910313:38:55 0.0 0710910313:39:05 0.0 07/09/03 13:39:15 0.0 07/0910313:39:25 -0.1 07/09/0313:39:35 -0.1 07/0910313:39:45 -0.1 07/0910313:39:55 0.0 07109/0313:40:05 0.0 0710910313:40:15 -0.1 07/0910313:40:25 -0.1 07/0910313:40:35 0.0 07/0910313:40:45 0.0 0710910313:40:55 -0.1 07109/0313:41:05 -0.1 07109I03 13:41:15 -0.1 07/09103 13:41:25 0.0 07/0910313:41:35 -0.1 07109/0313:41:45 -0.1 07/09/03 13:4 i : 55 -0.1 07/09/0313:42:05 -0.1 07/09/03 13:42:15 0.0 07/09/03 13:42:25 OA 07/09/0313:42:35 -0.1 0710910313:42:45 -0.1 07/09/0313:42:55 -0.1 0710910313:43:05 -0.1 07/09/03 13:43:15 0.0 0710910313:43:25 0.0 0710910313:43:35 -0.1 07109/0313:43:45 -0.1 07109/0313:43:55 -0.1 07/0910313:44:05 0.0 07/0910313:44:95 0.0 07/09/0313:44:25 -0.1 07/0910313:44:35 -0.1 07/0910313:44:45 -0.1 07/09/0313:44:55 -0.1 07J0910313:45:05 -0.1 0710910313:45:15 -0.1 07109103 13:4 5:25 -0.1 0710910313:45:35 -0.1 07/0910313:45:45 -0.1 07/0910313:45:55 -0.1 07/09/0313:46:05 -0.2 07/09/0313:45:15 -0.2 07/0910313:46:25 -0.2 0710910313:46:35 -0.2 07/09/0313:46:45 -0.2 07/0910313:46:55 -0.2 07109/0313:47:05 -0.1 07/09/03 13:47:15 -0.1 0710910313:47:25 -0.1 07109/0313:47:35 -0.1 07/0910313:47:45 -0.1 

# 317

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# k

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07/0910313:47:55 -0.2 07109/0313:48:05 -0.9 07/0910313:48:15 -0.1 07/0910313:48:25 -0.2 0710910313:48:35 -0.2 0710910313:48:45 -0.2 07109/0313:48:55 -0.3 0710910313:49:05 -0.3 07/0910313:49:15 -0.3 07109/0313:49:25 =0.2 07/09/0313:49:35 -J.2 07/0910313:49:45 -0.3 07/0910313:49:55 -0.2 07109/0313:50:05 -0.2 07109/0313:50:15 -0.2 0710910313:50:25 -0.3 07/0910313:50:35 -0.3 0710910313:50:45 -0.2 0710910313:50:55 -0.2 07/0910313:51:05 -0.1 07/09103 13:51:15 -0.2 07109103.13:51:25 0,0 07109J0313:51:35 -0.1 0710910313:51:45 -0.1 07/09/03 13:51:55 0.0 07/0910313:52:05 0,0 07/0910313:52:15 0.0 0710910313:52:25 0.0 07/09/03 ;3:52:35 0.0 07/09/0313:52:45 0.0 07/09/03 13:52: 55 -0. i 0710910313:53:05 -0.1 0710910313:53:15 -0.1 0710910313:53:25 -0.1 0710910313:53:35 -0.1 07/0910313:53:45 0.0 07/09/03 13:53: 55 -0.1 0710910313:54:05 0.0 07/0910313:54:15 -0.1 0710910313:54:25 -0.1 0710910313:54:35 -0.1 07/0910313:54:45 -0.1 0710910313:54:55 -0.1 0710910313:55:05 -0.1 07/0910313:55:15 -0.2 07109/0313:55:25 -0.1 0710910313:55:35 -0.1 0710910313:55:45 -0.1 07/0910313:55:55 -0.2 07/0910313:56:05 -0.2 07/09/0313:56:15 -0.3 07/0910313:56:25 -0.2 07/0910313:56:35 -0.2 07109/0313:56:45 -0.3 07/0910313:56:55 -0.2 0710910313:57:05 -0.2 07109/0313:57:15 -0.2 0710910313:57:25 -0.2 07109/0313:57:35 -0.2 07/0910313:57:45 -0.2 07/0910313:57:55 -0.1 0710910313:58:05 -0.2 07/09f0313:58:15 -0.2 07f09/0313:55:2:. -0.2 0710910313:58:35 -0.2 07J09/03 13:58:45 -0,1 0710910313:58:55 -0. -, 07/09/03 13:59:03 -0.1 07109/0313:59:15 -0.1 07/09/0313:59:25 -0.2 07/09/0313:59:35 -0.2 0710910313:59:45 -0.2 07109/0313:59:55 -0.3 07/09110314:00

- 05 -0.3 

# 3 18

Page 4 

# ~7110/03 Run 93

07109103 14:00: 1 4 5 -0.2 07/09/C314:00:25 -0.2 07/09/0314:00:35 -01 07109/0314:00:45 -0.1 07109/0314:00:55 0.0 07/09/0314:01:05 0.0 07109/03 14:01:15 0.0 07/09/0314:01:25 -0.1 07/0910314:01:35 -0.2 07/09/0314:01:45 -0.2 07/09/0314:01:55 -0.1 07/09/0314:02:05 -0.1 07/09/0314:02:15 -0.2 07/09/0314:02:25 -0.2 07/0910314:02:35 -0.1 07/09/0314:02:45 -0.2 07109/0314:02:55 -0.2 07/0910314:03:05 -0.2 07109/0314:03:15 -0.2 07/0910314:03:25 -0.1 07/09/0314:03:35 -0.1 07/0910314:03:45 -0.2 07/09/0314:03:55 -0.3 07/09/0314:04:05 -0.2 0710910314:04:15 -0.2 07/09/0314:04:25 -0.2 07/09/0314:04:35 -0.2 07/09/0314:04:45 -0.3 07/09/0314:04:55 -0.3 07/09f0314:05:05 -0.3 07109/0314:05:15 -0.2 0710910314:05:25 -0.2 07/09/0314:05:35 -0.2 07/09/0314:05:45 -0.2 07109/0314:05:55 -0.1 0710910314:06:05 -0.1 07/0910314:06:15 -0.1 07/0910314:05:25 -0.2 07109/0314:06:35 -0.1 07109/0314:06:45 -0.2 07/0910314:06:55 -0.2 07/09/0314:07:05 -0.1 07/0910314:07:15 0.0 07/09/0314:07:25 -0.1 07/0910314:07:35 0.0 07/09/0314:07:45 0.0 07109/0314:07:55 0.0 07109/0314:08:05 -0.1 07/09/0314:08:15 -0.2 07/09/0314:08:25 -0.1 07/09/0314:08:35 -0.1 07/09/0314:08:45 -0.1 07/09/0314:08:55 0.0 07109/0314:09:05 -0.1 07/0910314:09:15 -0.1 07109/0314:09:25 -0.1 07/09/0314:09:35 -0.1 07/0910314:09:45 0.0 07109/0314:09:55 -0.1 07109/0314:10:05 •0.1 07/09/03 14:10:15 -0.1 07/09/0314:10:25 -0.1 07/09/0314:10:35 -0.1 07/09/0314:10:45 -0.1 07/09/0314:10:55 -0.1 07/0910314:11:05 -0.2 07109/0314:11:15 -0.2 07/0910314:11:25 -0.2 07109/0314:11:35 -0.2 07109/0314:11:45 -0.2 07109/0314:11:55 -0.1 07J09/0314:12:05 -0.1 07/09/0314:12:15 -0.2 07/09/0314•12:25 -0.1

1 1 

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07/0910314:12:35 -0.2 0710910314'12:45 -0.2 07109/03 1 4: , 2:55 -0.1 07i09l0314:13:05- G.0 07/09103 14:13:15 0.0 07109/0314:13:25 -0.1 0710910314:13:35 -0.1 07/09/03 14:13:45 -0. 1 07109/0314:13:55 -0.1 07J0910314:14:05 0.0 07/09/03 14:14:15 0.0 07/0910314:14:25 0.0 0710910314:14:35 -0.1 07/09J0314:14:45 -0.1 0710910314:14:55 -0.1

Stop Run 43 -0.10

07109/0314:15:05 -0.1 07/09103 14:1 5:15 -0.1 07J0910314:15:25 -0.1 07/09/031415:35 -01 0710910314:15:45 -0.1 07/0910314:15:55 -0.1 07/09/0314:16:05 -0.2 07/09/03 14:16:15 -0.2 07l09/0314:16:25 -0.2 07109/0314:16:35 -0.2 07J09/0314:16:45 -0.1 0710910314:16:55 -0.2 07/091C314:17:05 -0.2 07/0910314:17:15 -0.2 0710910314:1 7:25 -0.2 0710910314:17:35 -0.2 0710910314:17:45 -0.1 0710910314:17:55 -0.2 0710910314:18:05 -0.2 07109/03 14:18:15 -0.1 07/09/03 14:18:25 0.0 0710910314:18:35 -0.1 07/0910314:18:45 -0.1 0710910314:18:55 0.0 0710910314:19:05 -0.1 07109/03 14:19:15 -0.1 07/0910314:19:25 -0.1 07109/0314:19:35 -0.1 07/09J0314:19:45 0.0 07/09/03 14:19:55 0.2 0710910314:20:05 0.6 07109103 14:20:15 1.3 07/09/0314:20:25 2.0 07J09/0314:20:35 2.8 07/0910314:20:45 3.6 07/09/0314:20:55 4.4 07/0910314:21:05 5.4 0710910314:21:15 6,4 07/09/03 14:21:25 7.2 07109/0314;21:35 8.2 07I09103 14:21:45 9.0 07/09/03 14:21:55 9.8 07/09103 14:22:05 10.6 07/09/03 1 4:22:15 11.3 07109/03 't 4:22:25 12.0 07109J03 14: 22:35 12.7 07/09/03 14:22:45 13.3 07/09103 14:22:55 13.8 07/09103 14:23:05 14.2 07109103 14:23:1 5 14.6 07109/03 14:23:25 15.1 07109103 14:23:35 15.6 07/09/03 14:23:45 15.8 07/09J03 14 :23:55 16.1 07/09103 14:24:05 16.5 

### Zeto N2



# FE

. 320

Page 67/10103 Run #V3

0710910314:24:15 16.8 07109103 14:24:25 17.1 07/0910314:24:35 17.4 07/09103 14:24:45 17.5 07/09103 14 :24:55 17.7 07/0910314:25:05 17.8 07109/03 14:25:15 18.0 07/09/03 14 : 25:25 18.1 07/09/03 14:25:35 18.2 07/0910 3 14: 25:4 5 18.4 07/09/03 14:25:55 18.9 07/09/03 14:26:05 19.2 07/0910314:26:15 19.5 0710910314:26:25 19.9 07/09/0314:26:35 20.3 07/09/0314:26:45 20.5 07/09/0314:26:55 20.9 07109/0314:27:05 21.2 07/0910314:27:15 21.6 07/09/0314:27:25 21:9 07/09/0314:27:35 22.3 07/09/0314:27:45 22.6 07/09/0314:27:55 22.9 07/0910314:28:05 23.2 07109/0314:28:15 23.4 07/09/0314:28:25 23.5 0710910314:28:35 23.5 25.7 ppm S02 07/0910314:28:45 23.6 07/69/0314:28:55 23.6

Page 7 

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## Customer: NiATH=SON TRI-GAS - IRVING Cylinder Number: SX-321 45 Cylinder pressure: 2000 Last Analysis date: 4-17-2003 Expiration Date: 10/17/03 Protocol: Reference n Lot # G 1 249290 109-35-28491

REPLICATE RESPONSES

Date: 4-10-2003 Cornponent : Sulf

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# 25.5 PPM Certified Conc: 25.7 Y 0.2 PPM ~, ~ rf ~ t•

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## Cornaonent: Sulfur Dioxide SRM #: SRMr.J693a Cylinder CAL=01

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## 0596 

# Concentration: 49.9 ppm,

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## CER T IFICATION INSTRUMENTS

Component: Sulfur Dioxide

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## A Make/Modef: Nicolet 550 Serial Nurnber: ACN-9402192 ' Measurement Principle: FTIR i

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## Last Ca(ibration: 4-3-2003 °

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# or Assay & Certification of Gaseous Calibration Standards September 1997, using procedure G1 andlor G2.

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## 50.08 50.42 50.23 51.20 51.11 50.96 :.,...

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### Analyst:



# . ~ Air Lic{uide America Corroralio„ 11426 Fairmont Parkv+ay, La Porte, Texas 77571-6000 Pnone: (28 1 ) 474-8400 Fxx: (281) 474-8419


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