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# OAR Box 

# 1672 Prepped by Charmelle Mathews



## Document

Number: 

# {# 55 5 ll-C-2 6
Docket Number: 

# A-98-1 3

Printed 9/30/2008 11:01:00 AM Sheet 55 of 132P. 2 

## A 9 8 1 3 II-C-Z 6

yT *3> . o 

### UNITE D STATE S ENVIRONMENTA L PROTECTIO N AGENC Y | ^MK^ t * Offic e o f Ai rQualit y Plannin g an d Standard s I ±\if-L? Researc h Triangl e Park

, Nort h Carolin a 2771 1 \ / 

## AP R 13 199 

## 8 Mr

. Pete r Gueri n Plain s Termina

l an d Transfer Corporatio n Route 1 , Box 59 5 Cushing , Oklahom

a7402 3
Dea r Mr

. Guerin : Thi s letter i s t o reques t

avisi t by th e U.S

. Environmenta l Protectio n Agenc

y (EPA ) and it s representative s t o th e Plain s Termina l an d Transfe r Corporatio n facilit

y i n Cushing , Oklahom ao n Apri l 21 , 1998

. Visitor s wil l includ e Mr

. Stephen Shed

d o f th e EPA , an

d Mr

. Gre g LaFlaman d Mr

. Bern d Hanek e of Pacifi c Environmenta

l Services , Inc

. (PES)

. Mr

. LaFla

mo f PE S discusse d thi s visi t

wit h yo u in atelephon e conversatio n o n Apri l 9 , 1998

. W e anticipate arrivin g a

t th e facilit y a t 1:0 0 p.m . A s you are aware , th e EPA i s developing nationa l emissio n standard s fo

r hazardou s ai r pollutant s (NESHAP) fo

r organi c liquid s distributio n (non-gasoline ) facilities

. Th e mai n emissio n source s o

f interes t are a s follows : 1 ) storag e tanks ; 2 ) loadin g and unloadin g operations ; 3 ) equipmen

t leaks ; 4 ) wast

e an d wastewate

r treatment an d disposa l operations ; an d 5 ) mixin g an d blendin g operations

. T o assis t i n th e developmen

t o f thi s NESHAP , th e EP A i s collectin g informatio n o n emission s o f hazardou s air

pollutant s (HAP ) fromthes e emissio n source s an

d o n th e type s o

f emissio n control s use d o n eac h o f th e sources . Durin g th e visi t

to your facility , w e wis h to : 1 ) discus s th e facilit y an d emissio n contro l operations ; and 2 ) observ e th e storag e tanks , wastewate r systems , organi c liqui d transfe r operations , and an

y associate d emissio n contro l an d emissio n monitorin g equipment

. Enclosure 1 identifie s th e typ e of informatio n tha

t w e would lik

e t o obtai n durin g our

visit , and als o contain s alistin g of th e material s considere d t o b e HA P b y th e EPA

. Fee l free t o provid e an

y additiona

l informatio n tha

t you believ e i s critical t o ou r understandin g of

thes e processes , thei r

HA P emissions , o r

th e emissio n controls

. Collectio n an d organizatio n o

f th e informatio n identifie d i n Enclosure 1 prio r t o ou r visi t wil l greatl y facilitat

e informatio n exchang e durin g th e visit

. Th e authorit

y fo r the EPA' s information gatherin g i s include d i n sectio n 11 4 o f th e Clea n Ai r Ac t (4 2 U.S.C

. 7414)

. Enclosur e 2 contain s asummar

y of thi s authority

. I

f you believ e tha

t disclosure of

th e informatio n w

e reques t would revea

l atrad e secret , you shoul d clearl y identif

y such informatio n a s discusse d in the enclosure

. An y informatio n subsequently determine d t o constitut

e atrad e secre t

wil l b e protecte d under

1 8 U.S. C 1905

. I

f n o clai mo

f confidentialit

y accompanie s th e informatio n whe n i t i s receive d b y th e EPA , i t ma y b e madeP. 3



## availabl e t o th e publi c b y th e EP

A without furthe r notic e (4 0 CF

RPart 2.203 , Septembe

r 1 , 1976)

. Sinc e sectio n 114(c ) of th e Clea n Air Ac t exempt s emissio n datafromclaim s of confidentiality , th e emissio n dat ayo u provid e ma

y b e mad e availabl e to th e public

. A clarificatio n of

wha t th e EP A consider s to b e emissio n datai s containe d i n Enclosure 3

. A s note d i n Enclosur

e 4 , th e EP

A ha s designate d PE S as a n authorize d representativ e o f th e Agency

. Therefore , PE S ha s th e right s discusse d above and i n Enclosure 4

. A s an authorize d representativ e o f th e EPA , PE S i s subjec t

t o th e provision s o

f 4 2 U.S.C

. 7414(c ) respectin g confidentialit

y o f method s o r

processe s entitle d t

o protectio n a s trad e secrets

. Th e PE S contrac t

wit h th e EP A i s No

. 68-D60013

. Enclosure 5 summarize s th e EP A policie s an

d procedure s fo

r handlin g privilege d informatio n an d describe s th e EP A contracto r

commitment s an

d procedure s fo r

us e o f confidentia

l materials

. I t

i s th e EPA' s polic y tha

t complianc e by a

n authorize d representativ e wit h th e requirement s detaile d i n Enclosur e 5 provide s sufficien

t protectio n of

th e right s of thos e submittin g privilege d information

. Th e followin g policie s concernin g liabilit y shoul d als o b e o

f interes t t o you : 1

. If aFederal employe e i s injure d i n th e cours e o f hi s employment , h e ha s compensatio n coverag e fromth e Governmen t unde r th e Federa

l Employee s Compensatio n Ac t ( 5 U.S. C 810 8 e t

seq.) ; and
2

. If , du e t o th e employee' s negligence , propert y damag e o r

personal injur

y t o third partie s occurs , th e Federal Tor t Clai mAc t

(2 8 U.S.C

. 1346) provide s amean s of fixin g an y liabilit y upo n th e Federal Government

. Th e Offic e of

Genera l Counsel ha s informe d th e Agenc y tha t afirmma

y no t conditio n th e EPA' s "righ t

o f entry " upo n consen

t t o awaiver

of liabilit y and ha s instructe d employee s no t to sig n suc h waivers

. I

f you hav e an

y question s regardin g thi s refusal , pleas e contac t th e EPA' s Genera

l and Informatio n La

w Divisio n a

t (202 ) 260-0020

.



# 2 -P. 4



## Than k yo u fo r your cooperation

. I f

yo u hav e an y questions , pleas e contac t

Mr

. Stev e Shed d o f m y staf f a t (919 ) 541-5397 , o r

Mr

. Gre g LaFla

mo f PE S a t (919 ) 941-0333

. Sincerely ,

Ken t C

. Hustvedt , Leade

r Wast e an d Chemica l Processe s Grou

p Emission Standard s Divisio n 5 Enclosure s

cc : Bil l Luthans , EP A Regio n V I (w/ o Enclosure s 2-5 ) David Dyke , State o f

Oklahom a(w/ o Enclosure s 2-5 ) bcc : Stev e Shed

d (EPA/OAQPS/ESD/WCPG) (w/ o Enclosure s 2-5 ) Gre g LaFla

m(PES ) (w/o Enclosure s 2-5 ) Bernd Hanek

e (PES ) (w/o Enclosure s 2-5 )
PREPARE

D BY : OAQPS/WCPG:SShedd:MD-13:RTP,NC:(919)541-539 7

(PES/GLaFlam/(919)941-0333:4-02-98 ) (ES D Projec t

No

. 96/05 )P. 5

* *

. « ». * a



## Enclosure 1

SUMMAR

Y OF ORGANIC LIQUID S DISTRIBUTION INFORMATIO N O F INTERES T

T o assis t i n th e collectio n of

informatio n durin g th e requeste d site visit , asummar y of th e informatio n t o b e collecte d i s provide d below

. At thi s time , thi s informatio n pertain s specifically t o eac h o f

th e emissio n source s o

f interest : 1 ) storag e tanks ; 2 ) loadin g an d unloadin g operations ; 3 ) equipmen t leaks ; and 4 ) wast

e and wastewate

r treatmen t and disposal activities

. A s w e learn mor e durin g th e visit , additiona l HA P source s coul d b e adde d t o ou r scope . 

## 1

.

2

.
3

.
4

.
5

.
6

.

7

.
8

.
9

. Produc t

throughput s (e.g. , bbl

. yea r of eac h organi c liquid) , and proces s technica l description , wit

h simplifie d schematic s and aplo t plan o f th e entir e facility

. Types/concentration s of

hazardou s ai r

pollutant s (HAP ) i n tanks/wastewate r stream s (or

annualize d mas s emissio n rates ) prio r to emissio n contro l device

. Type s of emissio n reductio n measure s o r contro l device s associate d wit h eac h of th e emissio n sources , i f

any . Contro l devic e efficiency o r concentratio n o f

HAP i n ai r

stream s (o r

annualize d mas s emissio n rates ) subsequent t o th e emissio n contro l device(s) , i f applicable

. Capital and operatin g cost s associate d wit h th e emissio n contro l device(s) , i f applicable

. Operatin g an

d maintenanc e experienc e associate d wit h th e emissio n contro l device(s ) (i.e. , identif

y ke y operatin g parameter s fo r efficien t control , parameter s tha

t indicat e poo r control , o r

problem s associate d wit

h aspecifi c emissio n source/contro l devic e combination)

. Type s of emissio n monitorin g device s use d t o monito r emission s o r

contro l devic e performance , a s applicable

. Rational e fo

r selectin g an

y emissio n contro l device s currentl y installe d o n th e operations

. Regulator y histor y and curren t

regulator y requirement s associate d wit h emission s fromth e operations

.



# 4
-bttp3!A»ww«pMOvAi«/0-qps/_iito_yiUpoUi_ a P. 6

SE C 11 2 HAZARDOU

S AIRPOLLUTANTS-7/«» 6 updat e "Thi s draf tlis tinclude

s curren tEP A staf f recommendation

s fo r technica

l correction

s an d clarification

s o f the hazardou

s ai r pollutant

s (HAP ) lis ti a Section 112(bX 0 o f the Clea n Ai r Ac tThi s draf tha s bee n distribute

d t o appris

e intereste d partie s o f potentia l futur e change s I n th e HA P lis tan d i s informationa

l only . Th

e recommende

d revisions o f

th e curren

tHA P lis t whic h ar e include d i n this draf

td o no tthemselve

s chang e th e lis ta s adopte

d by Congress an

d hav e n o lega l effec tEP

A intend s t o propose specifi c revision s o f di e HA P list , includin

g an y technica l correction s o r clarification

s o f th e list , only throug h notice an

d commen

trulemaking. " CA S No . Pollutan

t 75-07- 0 Acetaldehyd

e 60-35- 5 Acetamide 75-05- 8 Acetonitrile 9846- 2 Acctophenon

e 53-96- 3 2-Aeetylaminofluoren e 10742 4 Acrolein 7946- 1 Aoylamid e 79-10- 7 Acryli c ad d 107-13- 1 Acrylonitrile 107-05- 1 Atty

l chlorid e 92-67- 1 4Mminoblpheny i 62-53- 3 Aniline 9044 4 o-Anisidine 1332-21 4 Asbestos 71-43- 2 Benzen

e (including benzen

e ftora gasoline ) 92-87- 5 Benzidin

e 9847- 7 Bcnzotrichlorid e 100-44- 7 Benzy

l chlorid e 92-52- 4 Bipheny

l 117-81- 7 Bis(2-ethylhcxy0phthalate(DEHP ) 542-88- 1 Bisfchloramethyl ) ethe r 75-25- 2 Bromofor

m 10649 4 U-Butadien e 156-62- 7 Caldu

m cyanamid

e 105-60- 2 Caprolacta

m (Remove

d 6/18/96 . 61FR30816) 13346- 2 Capta

n 63-25- 2 Carbary

l 75-15 4 Carbo

n disulfide 56-23- 5 Carbo

n tetrachlorid

e 463-58- 1 Carbony

l sulfid e 120-80 4 Catecho

l 13340- 4 Chlorambe

n 57-74 4 Chlordan

e 7782-50- 5 Chlorin

e 79-11- 8 CMoroaceti

c aci d 532-27 4 2-Chloroacetophenon e 10840- 7 Chlorobenzen

e 510-15 4 Chlorobenzilat e 67-66- 3 Chlorofor

m 107-30- 2 Chloromethy

l methy l ethe r 12649- 8 Chloropren

e 1319-77- 3 Cresol/Crcsyli

c acid (mixed isomers) 95-48- 7 o-Crcso

l 108-39 4 m-Creso

l 10644- 5 p-Cceso

l 98-82- 8 Cumen

e N/ A 2,4- D (2,4-Dichlorophenoxyacetic Add ) (indudin g salt

s an d esters ) 72-55 4 DDE(l.l-dichloro-2,2-bi s

(p-chlorophenyi

) ethylene) 334-88- 3 Diazontcthan e 132-64- 9 Dibenzofura n CA S No . Pollutan

t 96-12- 8 l^-Dibromo-3<hloropropane 84-74- 2 Dibuty

l phthalat e 10646- 7 1,4-DIdilorobenzen e 9144- 1 34'-Dlchlorobetaidin e 11144 4 Dichloroetby

l ethe r (Bb{2-chloroethyl]ether

) 542-75- 6 1.3-Dichloropropcu e 62-73- 7 Dichlorvos 11142- 2 Diethanolamin

e 6447- 5 Diethy

l sulfat e 11940 4 3,3M5i_Mthoxybenzldin e 12149- 7 NJM>fanethylanaiii e 11943- 7 3J'-Dlmethylben_idine 7944- 7 Dlmetbylcarbamoy l chlorid e 68-12- 2 KN-Dimethylfimnainlde 57-14- 7 1,1-Dlmetbylhydtazin e 131-11- 3 Dimethy

l phthalat e 77-78- 1 Dimethy

l sulfat e N/ A 4,6-Dlnitio-o-trcso l (indudin g salts) 51-28- 5 2,4-D__ltropheno i 121-14- 2 2,4-Dlnitrotoluen e 12341- 1 l,4-Dloxane(l,4-Diethyleneoxide ) 12246- 7 U-Diphenylhydrazine 106-89 4 Epichtaohydri a 10648- 7 1,2-Epoxybutan

e 14048- 5 Ethy

l acrylat e 10041 4 Ethylbcnzen

e 51-79 4 Ethy

l carbamat

e (Urethane

) 7540- 3 Ethy

l chloride (Chloroethane

) 10643 4 Ethylen

e dibromid

e (Dibromoethane

) 10746- 2 Ethylen

e dichloride (U-Dichloroethane ) 107-21- 1 Ethylen

e glyco l 151-56 4 Ethyleneimine(Aziridine) 75-21 4 Ethylen

e oxid e 9645- 7 Ethylen

e thioure a 75-34- 3 Ethyllden

e dichlorid

e (l.l-Dfchloroethane ) 5040 4 Formaldehyd

e 7644 4 Heptachio

r 118-74- 1 Hexachiorobenzen e 8748- 3 Hexachlorobutadlen e N/ A 1,2^.4,5.6-Hexachlorocyclyhexan e (all stereo isomers , includin g lindane ) 7747 4 Hexachlorocydopentadien e 67-72- 1 Hexachloroethan e 82246 4 Hexamethylen

e diisocyanat

e 680-31 4 Hexamethylphosphoramid e 110-54-3 Hexan

e 30241- 2 Hydrazin

e 7647414HydrochIori c aci

d (Hydroge

n chlorid e [ga s only] ) 7664-39-3Hydroge

n fluoride (Hydrofluori

c add ) 123-31 4 Hydroquinon

e 78-59- 1 Isophoron

e 108-31 4 Mild c anhydrid

e 67-56- 1 Methano

l 7243- 5 Methoxychlo

r 7443 4 Methy

l bromid e (Bromomethane

) 7447- 3 Methy

l chlorid e (Chioromethane

) 71-55 4 Methy

l chlorofor m (l.l.l-Trichlorocthane ) 7843- 3 Methy

l ethy l keton e (2-Butanone

) 60-34 4 Methylhydraztn

e 7448 4 Methy

l iodide (lodomethane

) 108-10- 1 Methy

l isobuty l keton e (Hexone ) CAS No . 62443 4 8042 4 163444 4 101-14 4 7549- 2 10148 4 101-77 4 91-20- 3 9845- 3 9243- 3 10042- 7 7946 4 68443- 5 62-75 4 5949- 2 56-38- 2 8248 4 8746- 5 10845- 2 106-50- 3 7544- 5 7803-51- 2 N/ A 8544 4 1336-36- 3 1120-71 4 57-57 4 123-38 4 114-26- 1 7847- 5 75-56 4 75-55 4 91-22- 5 106-51 4 10042- 5 9649- 3

. 174641 4 79-34- 5 127-18 4 755045 4 10848- 3 9540- 7 58444 4 95-53 4 8001-35- 2 12042- 1 7940- 5 7941 4 9545 4 8846- 2 12144 4 158249 4 54044- 1 10845 4 59340- 2 7541 4 75-35 4 1330-20- 7 9547 4 108-38-3 10642- 3 Pollutan

t. Methy l isocyanat

e Methy l methacrylat

e Methy l ten-buty l ethe r 4,4'-Methylenebis(2-chloroaniline ) Methylen e chlorid e (Dicblorometfaane

) 4.4'-Methytenedlpheny

l diisocyanat

e (MDI ) 4,4'-Metfrylenedianilin

e Naphthalen

e Nitrobenzen

e 4-NUrobiphcny

l 4-Ntaopheno

l 2-Nltroprepan

e N-Nltroso-N-methylure

a N-Nltrosodimethylamin

e N-Nltrosomorpholin

e Parathio n Pentachloronhrobenzen

e (Qubitobenzene

) Pentachloropheno

l Pheno l p-Phenylenediamin

e Phosgen e Phosphin e Phosphoru

s Compound

s Phthali c anhydrid

e Polychlorinate

d biphenyl

s (Arodors ) 1 J-Propane sulton

e beta-Propiolacton

e Prapionaldehyd

e Propoxur(Baygon

) Propylen e dichlorid e (1,2-Dichloropropane

) Propylen e oxid e 1,2-Propylenimin

e (2-Methyiaziridine

) Quinolin e Quinon e (p-Benzoquinone

) Styren e Styren e oxid e 2J,7,8-Tetrachlorodibenzo •p-dioxi n 1.1 A2-Tetrachloroethan

e Teuachloroethylen

e (Perchloroethylene

) Titaniu m tetrachlorid

e Toluen e Toluene-2,44iamin e 2,4-ToIuen

e diisocyanat

e o-Toluidin

e Toxaphen e (chlorinate

d camphene

) 1,2,4-Trichlorobenzen

e 1,1,2-Trichloroethan

e Tricbloroethylen

e 2,4,5-Trichloropheno

l 2,4,6-Trichloropheno

l Triethylamin

e Triflunli n 2J,4-Trimethylpcntan

e Viny l acetat e Viny l bromid e Viny l chlorid e Vlnyliden e chlorid e (1,1-Dichloroethylene

) Xylenes (mixe

d isomers ) o-Xylene m-Xylen e p-Xylen e 

# % 5P. 7

hnp5<faw^jepa.go»w_n1»igrt_rtox/lg8pol_ i ta t Antimon y Compound s "Include s mono - an d dl
- ether s o f ethylen e Arseni c Compound s glycol , diethyien e (inorgani c indudin g assine ) glycol , an d triethylen e glyco l R-(0CH2CH2) n Berylliu m Compound s -OR'wher e Cadmiu m Compound s n>l,2,or 3 Chromiu m Compound s R* alky l o raryl group s Cobal tCompound s R'-R.H . o rgroup s which , whe n removed , Cok e Ove n Emission s yid d glyco l Cyanid e Compound s 1 ether s wit h th e structure : R-(OCH2CH2)n-OH . Glyco l ethers 2 Polymer s are exdude d Lea d Compound s from th e glyco l category . Manganes e Compound s Mercury Compound s 3 (Unde rReview ) Fin e mineral fiberU Nldc d Compound s 4 (Unde rReview ) Porycydi c Organi c Mattert Radionuclide * (includin g iadon) S 5 A typ e o f ato m whk h spontaneousl y Srirnhi m Compound s undergoe s radioactiv e decay . NOTE : Fo ral l listing s abov e whic h contai n th e wor d "compound s an d for glyco l edten , th e following applies : Unles s otherwis e spedfied , thes e listing s ar

e define d a s including an y uniqu e chemica l substanc e thatcontain s di e name d chemica l (Le ^ antimony , arsenic , ete. ) ss par

to f thatchemical' s infrastructure . 1X"C N wher e X • I f

o rany othe rgrou p wher e a formal dissociatio n ma y occur . Fo rexample . KC N o rCa(CN)2 . 2 (Unde rreview) Glyco l Ethe rdefinitio n draf

toptions : Possibl e Collectio n t o CAA 112(b)(1 ) footnot e dia twoul d b e consisten twid i OPPT S modifie d definition . Ne w OPPT S definitio n as publishe d is : R- (OCH2CH2) n • OR'where : n-1,2 , o r3 R-alky l C 7 o rles s o rR » phenyl o ralky l substitute d pheny l R'-Ho ralky l a o rles s o rOR" " carboxyli c ad d ester , sulfite , phosphate , nitrat

e o r sulfonat e CA A Glyco l ethe rdefinitio n exactl y a s i n th e statut e (error s indudcd) : 'Indude s mono - an d d i ether

s o f ethylen e glycol , diethylen e glycol , an d triethylen e glyco l R> (OCH2CH2)n-OR ' where 

### o-lior- 3 R• allcy l o rary l group s R * • R. H o rgroup s which , whe n removed , yiel d glyco l ether s wit h th e structur e R-(OCH2CH)n-OH . Polymer s ar e exdude d fro m th e glyco l category
. CA A Glyco l ethe rdefinitio n wit h technica l correctio n nu_de.(

A 2 was lef tou to f di e las t formula) 

### % &P. 8
Antimon y Compound s Indudesmono
- an d di
- ethers o f ethylene) Arseni c Compound s glycol , diethylen e (inorgaxd c inductin g aistne ) glycol , an d triethylen e glyco l R-(OCH2CH2) n Berylliu m Compound s -OR'wher e Cactadu m Compound s n-l,2,or 3 Chromiu m Compound s R• alky l o raryl group s Cobal tCompound s R'-R.H , o rgroup s which , whe n removed, Cok e Ove n Emission s yid d glyco l Cyanid e Compounds ! ether s wid i th e structur e R-(OCH2CH2)n-OH . Glyco l ediers 2 Polymer s ar e exdude d Lea d Compound s fro m di e glyco l category . Manganes e Compound s Moon y Compound s 3 (Unde rReview ) Fin e mineral fibers ] Nicke l Compound s 4 (Unde rReview ) Polycycli c Organi c Matte

M Radloimdide t(includin g tadon) 5 5 A typ e ofator a whic h spontaneously Seleniu m Compound s undergoe s radioactiv e decay . NOTE : Fo ral l listing s above whic h contai n di e word "compounds " an d for glyco l edws , the followin g applies : Unles s otherwis e specified , dies e listing s ar

e defined a s indudin g an y uniqu e chemica l substanc e thatcontain s th e name d chemica l (Le , antimony , arsenic , ete. ) a s par to f thatchemical' s inftastructure . IXX2 . wher e X-i f

oranyotfie rgroup wher e a sOfQSfl l QtfSQCtfUQ O ma y occur . Fo rexample , KCN o rCa(CN)2 . 2 (Unde rreview) Glyco l Ethe rdefinitio n draf

toptions : Possibl e Coneedo n t o CAA 1120K O footnot e tha twoul d b e consisten twid i OPPT S modified definition . Ne w OPPT S definitio n as publishe d is : R• (OCH2CH2) n - OR ' where : n-1,2 , o r3 R-alky l C 7 o rles s o rR
- pheny l o ralky l substitute d pheny l R'
- H o ralky l C 7 o rles s o r0R > carboxyli c ad d ester , sulfate , phosphate , nitrat

e o r sulfonate CAA'Glyco l ethe rdefinition exactl y a s i n di e statut e (error s Indudcd) : Indude s mono * and d i cthe n o f ethylen e glycol , diethylen e glycol , an d triethylen e glyco l R• (OCH2CH2)n-OR'wher e n-l^.or. 3 R• alky l o raryl group s R * • R. H o rgroup s which , when removed , yid d glyco l ether s wid i di e structur e R-(0CH2CH)n-0H . Polymers ar e exdude d fro m th e glyco l category . CA A Glyco l ethe rdefinitio n wid i technical correction made_(

A 2 wa s lef tou to f di e las t fonnula ) 

# tf 7P. 9



## Docke t No

. A-98-1 3 Subcategor

y H- C

The enclosure s wit

h thi s documen

t ar e identica l to th e enclosure s wit

h docke t itemH-C- 3



# 4