### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### EIA

Facility Code Facility Name Boiler ID Fuel Type 1

3159 Cromby 2 

## No.6 Fuel Oil (residual or bunker C)

### Fuel Type 2 Fuel Type 3 Other Fuel Description 

## No.6 Fuel Oil (residual or bunker C)

### EIA

Facility Code Facility Name Boiler ID Basis An alyte



## 3159 Cromby 2 As Received Higher Heating Value 

## 3159 Cromby 2 As Received % Moisture 

## 3159 Cromby 2 As Received % Ash 

## 3159 Cromby 2 As Received % Sulfur 

## 3159 Cromby 2 Dry basis Higher Heating Value 

## 3159 Cromby 2 Dry basis % Ash 

## 3159 Cromby 2 Dry basis % Sulfur 

## 3159 Cromby 2 Dry basis Antim ony 

## 3159 Cromby 2 Dry basis Arsenic 

## 3159 Cromby 2 Dry basis Bery llium 

## 3159 Cromby 2 Dry basis Cadmium 

## 3159 Cromby 2 Dry basis Chlorine 

## 3159 Cromby 2 Dry basis Chromium 

## 3159 Cromby 2 Dry basis Cobalt 

## 3159 Cromby 2 Dry basis Fluorine 

## 3159 Cromby 2 Dry basis Lead 

## 3159 Cromby 2 Dry basis Manganese 

## 3159 Cromby 2 Dry basis Mercury 

## 3159 Cromby 2 Dry basis Nickel 

## 3159 Cromby 2 Dry basis Selenium

### An alysis M ethod for each A nalyte

(example: ASTM D5865-04) 

## ASTM D 240

ASTM D 482 ASTM D 1552 ASTM D 240 ASTM D 482 ASTM D 1552 SW6010B SW6010B SW6010B SW6010B ASTM E776/9253 SW6010B SW6010B ASTM D 3761 SW6010B SW6010B ASTM D 3684/SW7471 SW6010B SW6010BEIA

Facility Code Facility

Name Boiler ID 

### HA Ps Test Group 

## 3159 Cromby 2 Dioxin/furan HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) 

### 0022A 

## 7/13/2010 7/13/2010 18180.00 Btu/lb 0.03 0.98 0030A 7/14/2010 7/14/2010 18350.00 Btu/lb 0.04 0.9 0036A 7/15/2010 7/15/2010 18320.00 Btu/lb 0.03 0.94 Fuel Testing ResultsHHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis)Arsenic

Units Bery llium

(Dry Basis) Bery llium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h Fixed Carbon 

## 0.03 0.04 0.03 Proximate Analy

ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen



## 86.8 10.7 0.46 0.98 1.03 87.2 10.8 0.46 0.9 0.61 87 10.7 0.43 0.94 1.2 Ultimate Analy

ses, % by

wtEIA

Facility Code Facility

Name Boiler ID 

### HA Ps Test Group 

## 3159 Cromby 2 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 

### 0023A 

## 7/13/2010 7/13/2010 18240.00 Btu/lb 0026A 7/13/2010 7/13/2010 18340.00 Btu/lb 0027A 7/13/2010 7/13/2010 18380.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

## 0.03 0.89 0.05 0.97 0.05 0.95Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis) 

## 0.03 % 0.01 % 0.04 %Bery llium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 

## 16 mg/Kg 13 mg/Kg 11 mg/Kg

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 

## 0.03 86.9 10.8 0.48 0.89 0.05 87.4 10.8 0.45 0.97 0.05 86.9 10.7 0.35 0.95 Proximate A naly

ses, % by

wt Ultimate Analy ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 

## 0.87 0.32 1.01EIA

Facility Code Facility

Name Boiler ID 

### HA Ps Test Group 

## 3159 Cromby 2 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### 0041A 

## 7/15/2010 7/15/2010 18260.00 Btu/lb 0043A 7/16/2010 7/16/2010 18220.00 Btu/lb 0045A 7/16/2010 7/16/2010 18320.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

## 0.02 0.95 0.05 0.82 0.03 0.99Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis)Bery llium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy

ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen



## 0.02 87.1 10.5 0.5 0.95 0.93 0.05 87 10.6 0.45 0.82 1.08 0.03 87 10.7 0.46 0.99 0.82 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID 

### HA Ps Test Group 

## 3159 Cromby 2 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### 0031A 

## 7/14/2010 7/14/2010 18340.00 Btu/lb 0034A 7/14/2010 7/14/2010 18340.00 Btu/lb 0038A 7/15/2010 7/15/2010 18250.00 Btu/lb Fuel Testing Results

## Mercury and non-mercury metalic HAPs

% Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

## 0.04 0.9 0.04 0.94 0.03 0.92Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis) 

## <.1 mg/Kg <1.5 mg/Kg <1 mg/Kg <.5 <.1 mg/Kg <1.5 mg/Kg <1 mg/Kg <.5 <.1 mg/Kg <1.5 mg/Kg <1 mg/Kg <.5Bery llium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

## mg/Kg <.5 mg/Kg <.5 mg/Kg <.5 mg/Kg 0.55 mg/Kg mg/Kg <.5 mg/Kg <.5 mg/Kg <.5 mg/Kg <.5 mg/Kg mg/Kg <.5 mg/Kg <.5 mg/Kg <.5 mg/Kg <.5 mg/KgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

## 3.34 mg/Kg <1 mg/Kg 0.118 mg/Kg 2.85 mg/Kg <1 mg/Kg 0.12 mg/Kg 2.35 mg/Kg <1 mg/Kg 0.0915 mg/Kg Proximate Analy ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen



## 0.04 87 10.6 0.48 0.9 0.98 0.04 87.6 10.3 0.48 0.94 0.64 0.03 86.8 10.4 0.41 0.92 1.44 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wt

### Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals sy nfuel mg /g petroleum coke μg/g other mg /Kg

### Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orange hightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm mg /Kg