# VES 004901.pdf

# . ' 

# ATTACHMENT 2

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VES 004901

# VES 004902 . pdf

# UNIT2

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# Ma
A.tt e ntlon: Jeff 

### Gorman ENS R**lntw~atio nal**  

### SO l S 

### Campuswood D r . S u

i te 1 04 SyriiCilde, NY 

### USA 13057-4232 Your Project #: 1002-022 

### Site: Veoila

Report Date: 2008 / 12/02 

### CERTIFICATE OF ANALYSIS MAXXAM J O B#: A889378, A89 1648 & 

### A 8Al964 R - i ved: 

### Sample Macr i x; soild # 

### Samples lleee ived: 9 Analyses ¥oisturc Determination 

## Date Quantity E xtracted 9 

### N/A 

### Date Analyzed 11/20/2008 

### Labo ra tory 

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### #: 1002.022

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## Job rumber 

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# .. M.i>:xxAM ANAL Y'TlCS INC : Total cover pages: 

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## ?.00**to(t~** 

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## t>ate: 2008.00.25 10 : 19:15 .0 4 '00' ThiS documerll k 

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# . . ENSR lntemafiooat , Ole nt Pro ject II:**100 2~22**  Project nama : VEOLIA ELeMENTS BY**~TO MIC**  SPECT!l_OSOOPV (CHEMIC AL MAT ERIAL)

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# ·. 2D08.'1WI6 0.53 105 Total 

## aw.mu. fC<I 2COU)9/16 Cl.53 105 T

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# -~· 0.53 105**Tolai~"'(C<) ~**  0.52 103 Total Lead (R>) 200MJ9/16 <152 103**Total -~)**  2008109116 Nil . ROI.=O.OI

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otalller)4ium (Be)**:aioe.~** 

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## o.sz 104 l<idEn-Codoium(Cd) 2IXI6I09I22 

## o...a· 98**~odd-** Clwonium (C<) . 

### 2008109122 OA9 1111**Add~** t.eod (l'b)**~** D.<8 1111 .lrrdd Ext:! 1 " Ntedtc(M ) 20ClMl9l22 O.a4 95 hJdEd**1'*'~(01** alOOI09I22 f).29 811

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## VE S 0 04 940

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### t: A8A2964 .

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## VES 004941

### 50 1 5 Cemp uswood Or Suite 104 • 

### East Syracuse, NY • U SA 13057-4232

Semple 

### Matti x: LIQUID 

### # Sample• Rocelvod: 9

Semple**Mat~x:** 

### SOi . 

### #**S~los** 

### Received: 3 .
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### t.totruc: Willer II Semplos RoceMocl: 3



### MAXXAMANAL YTICS Your Project#: 1 002..022 Slte:V EOUA .



### Report 

### D'"o : 20081 1 1/1' This roportsupemedos al l 

### previous reporis ,.;(h the samo Maxxam 

### job number 

### CERTIFICATE OF ANA L YSIS

9 0 CAMSO P -63 2008/0enG 2008108120 CM1 SOP.Q0408



### T

OC81 oowr pag6S: 

### 1 E PA 7 470 EP

A 60 1 0C



## VES 004942t.Aa>OIM1 Job II: A89164& 

### Report Dolt! 

### :i008/11/1' e,IS R f-iona l 

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### 1 002-022 f'T<Ijecl 

### name: VEOLIA RESULTS O F ANALYSES OF L I QU I D 

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### Dell : 200811111 4 Clienl Prof ect #; 1 

### 002.o22 Project 

### namo: VEOUA ELEMENTS BY ATOMIC SPECTROSCO PY (LIQUID) 

# : %

# ~**·** 01111-(M) mgll 12 11 17 0.6 0.5 0.1 1!59 1m

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....**~(Cd)** mgll • N D 

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## c-.. (Cr) mgll 0.12 

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### ND(O 15 ' 0 . 1 4 1 

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### ft. A89164S Report 

### Dolt: 200811 11 1 4



## • ENSR lntel'llOlionol Client Plt;ject 

### t: 1 002.Q22 Proj<!cl 

### name: VEOI.IA ELEMENTS BY ATOMIC SPECTROSCOPY -(LIQUID)


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### #: 1002-022 Project name: 

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## VES 004946ENSR In t ernational C li ent Pr ojec t #: 1002-022 

### Project n ame: VEOUA Maxxam 

### Job #: A891648 

### Report D 21B : 2008/11/14 

### This 

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### number RESU L TS OF AN ALYSES OF C HEM IC AL MA TERIAL



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### = Qua li ty 

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# ,.

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### Job II: A89 1 648 Report Dale: 2008/111 1 4**~** 

## ' 

# . . ENSR i n t emotional C l ient Project 

### #: 1 002-022 P r o j ect name :**VEO~IA**

· ELEME N TS BY ATOMIC SPECTROSCOPY (WAT ER)

• Rep¢1'13bte Dete<:tion Umlt 

## !!""" • Quafty Cot<rol Batdl



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## VES 004949

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Mmca m 10 AF7338**.o~. ~pie**  10 LBTU -tll·R3 MatrrX UOUIO

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Maxxam 1 0 AF7342 Somple 1 0 CS-U2-I\1

- S<lil Toat Summary



# ., ENSR 

### lnlemOiioroi Clent f'l1ljed 

### #: 1()02-022 Project 

### name: VEOLIA •
Colloolod 2008W13 Ship .... Recetwd 2008108114

Coll-d 20oaJoai 1 2

Sl>..,..d .**~eeMd 20~4** 



## VES 004950MBJOCam Job 

### 1: AS91648**Ropo~** O.lo: 2008fl1114

M.axx am 1 0 AF7342 Oup

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### Client 

### PYo!ect II: 

### 1002-02:2 Projeol nMle : VEOL I A

Co lfcde: d 200810811$ $hl p pod Rouivc<l 200MlS/14



## VES 00495 1ENSR lrumafional



### . Moxxam Jot> 

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# . . • ..._Job H..-r. OA89 1 &43 oalo 

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## · as 2008100121 99. RllloO.OS 99 2008IOen1 0.008. ROLoO.OOS



### . 2008101!121 0.5 T oisiA< -(Ao;) 20 0 8108120 0.0**0~ )**  

# .. .**:~** • . · . Tolsl 8Wy'lbn {llo) 2008/08120 OM 

# . ;**~** 2008108120 0.45 ' 

# .. T otal CO<! .... (Cd)

. T OI.ol Ctvo .....**(C~** 2008108120 0. 43 85

Tolal Lud (Pb) . 2008J08120 0.44 87 SpU<o<tBI""" · . TotaJAisonlo(As) 2008108120 0.49 lfl



# . TotaJ Oetyl'..., (8e) 2008108/20 0.51**~** 101 TotaJ Cadmium (Cd) 2008'08120 . 0.51. · 101 T ..., Clltomlum (Cr)· 2008/08120 0110 99 TOIJ I**L~od** { Pb) 21106108120 0.49 98 .


### . .

Md>od Bllinl< T olal Menlo (As) 200e/08I20 NO; RDL=O .ot . Tolslll«yy liiJm (Do)**~** 

### 110 • . ROL.O . ooos Total Codmlum (Cd) . 2008108120 . NO, ROL"!)-002 T otal Ctlfomium ( Cr) 2008108120 · N O, ROL-o.oDS . T ooa

ll

. ... (l't> 

### l 2006108120 .NO. ROL<0.01 RPO T OI.ol- (As) . • 2006108120 NC Tolali3efyllkttn (Be) :2.0060)8/20 NC Toto! Cadobn (Cd) 2008.'06120 NC TOIOI Chroml\m**(~** 2Q08I08I2Il**~c** Tolslload(Pb) 2008106120 

### N (! : 15$2290 . KCO ft.!ATI\t)< S.PI<E**-~-( Ao)**  2008108121 0.44 88

- EJdrattolllo &o<yllum (8e) 2006108/21 0.41 82

- E><lnldollle CodmkJm (Od) 2008108/21 OAO . 80

· Add Em><Aa ble Ch........, (Cr)' 2.<l06.'Jtl/21 0-43 85 

### u ..... % 

# " % 

# -.: "

mgll .**~** .,giL mgiL <ngiL mg/1.. mg/1.. 

### mgll mgiL mg/1. . mgiL mg/1.. mg/L mg/L mgll.

% % % . % 

# " ugtg uglg uglg ug/g --Leod(Pb) 2.00eioel21 HC . .• NC (II ug/g QC STANOARO . Add El<1n 1< :18blo A<senlc ("') 

# . . 2008J08/21 . 0.77 88 

### Ul>'9 Add El<lnldsblo**~** (C<) 2008108121 0 .30 91 Oglg ; Add El<lnldsblo L ead (l'b) 

### 20081081'2i · 1 .2 

# .. uglg**~Blank -~-(As)**  2006/08121 NO, RDL=1 ugtg Acid Ex1ractabOo Bcrylk.m (Be) 2008108121 NO, RDL=0-5 · uglg · Add Ertadable 

### CO<t miuia (Cd} 2.008.<)8121 NO, ROL=0.3 ug/g

AddExndableC-{C<) 200810812 1 NO. RDL=0.5 Oglg Add EXI<odablo Loed (PI>) . 2008Al612 1 NO. RQI.o 1 uglg RPO. Add """lldoblo Lood {l't>) 2008Al6121 23.6 . % 15 9<2563 SUK · MATRIX SPIKE >lc«>My (Hg) 

### . 

# . 200810e12 1 0.0230 92 

### mWL Splkod . Blank •""'"Y {Hg) 2008/08121 0.0263 

### lOS mgiL Me!llo<I.B- -(Hg) 2008108121 NO, ROLo O.Q001 . mg/1.. ' ljPO MercuiY (Hg) 2008/08121 · NC % 1592587 NC MATRIX SPIKE Add -bio "'"""'"' (llg) 2000108121 0.570 114 tog/g -QC S T ANDARD**AddEl<OodableMo""''Y~** 2CI<lMl8/21 0.305 109 

### uufg

# ~-**~** 

# :"'"""ble Me ouy (Hg) 2008oll8/21 ND. RDloO.OS

# ~ Exltlldllblo M NC**Hotdotec<ad ~~**  • tfon.calculabttl

### ~t**-=-** Retat i ve Peroeot Difference

. S!andsrd • 0\.laMy Control Standen:!

SPI!<E • Falllled 

### nmpe · 

# ..

1 ) The fei:XNCfy W&$ belOw the**~** control knit This may represent a low**~** in torno NIOt.IRs for thle: eped6c: analy($ . . 2 ) The**~** 

### tn the msb1x spike was not calcdated (J.IC) . Beca u se ol l19 hlgh conctOntion o f this sll3lyte in tho parehl sample , thG QCLNI

A 80 - 120



## .. , 

# .. . 20 75 ; 125 7 5- 125 75-125 75-125 75-125 

## so · . 125 76. t19 75:117

. 75-125

78 - 119
25 25 ' 25 25 25 ' 75·125 75-125 75- 1 25 75 - 125 75- . 125 75 · 125 · 7 5. ·125 7S -125
35 ' 75 - 125 . 84 - 113 25 7& ·125 • 75-125 35



## VES 00495 3

# ' ENSR**lntcrna~lonal** 

### Altl!nllon: Jeff Gorman 0""'1 Project 

### II: t002A ) 22 P.O. II: Pro j ect name: vEOL I A 

### Qua i Ry Assuranoe Report 

### (Continued) ·**M•~m** Job NurnbM: GA09 1 648



# ,. ).



# · .



# .. . !-



## VES 004954

### Validation Signature Page M

annm 

### J ob 1t. 

### A 891648
Tho onal)'1lctl data and 

### all 

### QC contained in 

### this 

### repon wcro rcviowtd aDd valida...S by the 

### fullowine indiviclual(s) .



### . ,· 

# - .
. 

# . . .

. ·

•'



## VES 004955

### . · .

I . : · Attentioni J eff Gonnan 

### ENSR Interna tional 

### ; 5015 CampuswoOd 

### Dr ' Suite 104 .



### East Syra<:uso, NY 

### USA 13057-4232 Y our Project#: 100 2.022 Sile:VEOLIA

· · R Oliort.Da t e: 2008111/14 This 

### report "'!P•rsedes . 811 

### preVIouS · reports 

### With lhe 

### same 

## Maxx8ni jo b 

### numbe r ' 

## Sampie !,latrix: 

### Chemical Material · 

### # SemplesRecelvGd: · 12 

### CERTIF ICATE OF ANA LY S IS 1 ' .

( I) Ma>oorn """"""' dOOa nolhl>ld - lion

## lor~ ofme lal a

## -~uslng ... ICP Aldol 

# met ._. : · · ' ' 

# .. '



# · .

. ·



# .

T olal 

### cover P'!QOS ! 

### 1



## VES 004956

### Maxxam Job 

### 8: A8A2964 Report Dll .. :**~11114** ENSR lntemallonal Client Projoct 

### IF.**1002~22**

. P r oject name: VEOLIA RESULTS OF ANAL Y SES O F CHEMICAL MATERIAL

D= Not -0<1**-~·** l • Rt()Ot1ablt 0etocUon Lim it



### - • quol1ty Coolro l llaleh 1 6 1 31519

16138 1 9

;· .**l**



## VES 004957Maxxam 

### Job #; A8A2964 Report 

### Date: 2008/ 1 1/ 14 ENSR ln<emationa l C l

ienl Pro(ed 

### #: 1002-022 Projecr name: VEOL I A ELEMENTS BY ATOMIC SPECTROSCOPY (CHEMICAL MATERIAL)

# ~ Olal Arunlc (As) mg/L 160 1 60 240 0.()6 . 0.01 """ 8olyillwn (Be) mgiL NO 

### NO NO NO 0 .0005**ooai~ (Cd** **)** mg/1. 0 .1 0 0 . 11 0.16 0.000 0.002 otol Ctiom i tan (Cf) mgiL 1,.. ' 1400 . 6SO 0 . 006 0.005 oblllead (Pb) mgiL 

### O.M 0.72 2. 1 ' 0.03 0.01 N

D =Notdote<Oed 

### ; ,1 ROL • Reportllble Oefedion . Uni 

## c Bo.loch • Quality . Coflb'of Batch

T CO>I A,..nK ,-(As) mgiL 0.04 . 0.0< NO 0.91 0.01 .

.... Bel)lbn (Be) mgiL NO 

### NO NO NO .ooo5**ctat~(Cd .**  mg/1. 0.004 . 0.005 

### o.ooe NO 0.002 . Olal ctwmlum (C<) mgiL 

## .. NO · NO ND 1>.33 0.006 . TOOI I**~** (Pb) . mgiL 0 . 03 0.03 

### .o-03 NO . O.Ot 

### =NcC doiadod

= 

# _...Doloctlon Umil**BatCh ~**  Cor.trcl Bak:b 

## ·• 161-49 08 1614908 16149Q8 16,14808 16 1 4906

1614901l 161 4 908 1614908 1.614908**1614~**



## V ES 004958

### ENSR lntem aliol1al

. CHent Project#: 

### 1002-022



### Projec t name: VEOUA Maxxam Job # : 

### A8A2964 Re port Date: 2008111/ 1 4 

### Th i s roponsupersedes all prev1ous reports wilh 

### !he :.arne Maxxamj ob • nunt>e< ELf MENTS BY ATOMIC SPEC T ROSCOPY (CHE MICAL MATERIAL) ;-



### Maloalm 10 AL3436 AL3437 AL3438 AL3443 AL3444 AL3445 AL3445 

### Sarno! i na Da te . 0910312008 ' 09m9/2008 09/1012008 0910812008 0910912008 09/1012008 0 9/ 1 012008 Units HBTU·U2-R1 HBTU-U2-R2 HBTU-U2 - R3 LBTU-U2-R1 LBTU-U2-R2 LBTU-U2-R3 LBTU-U2·R3 Lab-Oup I To ta l At<enic lAs ) maiL 160 160 240 . 0 .00 0.04 · 0 .04 NO 

### T

o t al Be rv iUuniTB e mQ NO NO NO' N O N O N O NO 

### To te i Co d m i u m (Cd moL · 0.10 0 .1 1 0.16 0 .003 · · 0. 00 4 0.005 0. 0 08 

### Tota l C h ro mium (Cr . mg L 1500 . 14 00 630 0.006 N O . N D · NO 

### Tota l 

### Lead (Pb) rng/l. 0.58 _ 0 . 72 2.1 O.O

_ L • .**Q.O~** 

### 0.03 0 . 03

# ~**~** 

# !ACid N O m 

### Not de t ected 

### NIA • Not Applicable

### ~ 

### !!!._

### ~ 

# I= I:
RDL " Reportable Detection limit . L ab-Oup " Laborato<y 

### lnltlated Dupl i cate QC Batch a 

### Qual ity 

### Control Batch N/A N/A N/A 

### N/A**~** 

### N/A · N/A

· NJA 

## NiA

N/A



### . N/A N/A 

### lA N/A 

# • / A 

# ;;: ' A 'A



## VES 00 4959

### ENSR 

### International alent Project# : 1002.c.22 Project 

## neme : VEOUA Maxxam Job 

### ft. A8A2964 Report Date: 

### 2008/1 1 / 14 

### This re port supersedes 

### au previous reports with 

### t he same M exxam job num ber 

### ELEMENTS BY A TO MIC SPECTROSCOPY (CHEMICAL MAT!RIAL) 

# '

Maxxam 1 0 AL3446 Al3447 AL3448 Al3449 Al3450 AL3451 

### Samp li n g Date 09/08/2008 0 9/09 12008 09/10/2008 09/0812008 09/0912008 09/1012008 · · Units SF-U2-R1 SF.U2-R2 SF-U2-R3 CS.U2-R1 CS.U2·R2 CS.U2 . -R3 ROL QC 

### Batch To ta l 

### Arsonic 

### !Asl . mQ/L 

### 0 .0 1 0.03 NO N/A 

### NIA N/A 0.01 

### 1614908 To:al**~llum** 

### {Be mg/1. 

### NO NO 

### NO NIA NfA NIA 0.0005 161 4908 Tota l cadmium (Cd mg/L NO 

### NO 

### 0.002 N/A NIA NIA 

### 0 . 002 1614908 Totlll Chromium 

### CCr I mQil · 0.33 · 

### 0.12 0.37 NIA NfA 'NIA 0.005 

### 1614908 Total Lead (Pb) I 

## tW1- NO NO NO · NIA 

### N/A N/A 0.01 1614908 Acid 

### Extraclable Arsenic 

### lAs! ' 11!1 

### N/A N / A NfA 32.6 28 . 3 31 . 1 1 1620332 Acid 

### Extractable BeiVIUum !Be ua N/A N /A · NfA NO NO NO 0.2 162 0332 Acid Exlractable Cedmium 

### (Cd ug'g N/A NfA N/A 69 .4 50.2 58.7 0.3 1620332 Acid 

### Extractable ChromiLm 

### CCrl**~·g** 

### N/A N /A ' N/A 416 305 345 0.5 1620 332 Acid 

### Extractab l e LeadjPb) lll!Q 

### N/A . N/A NIA 

### 1tl . · 7 5A 8l.8 1 1620332



## VES 004960

## ' 

# . Maxxam Job 

### 1: A8A2964 Flepo<t O.:a: 200S/1 1 /14

Maxx amiO SampleiO Mattix 

### AIM36

# ~=**:: etia** **t** T • .

st Summary

M8xkemlri AU43 7 SanwleiO H8TlJ.U2 -R 2 : . • N.atrlx Cheri:al**Ma l** 

-10 AL3438 SamoleiD H 91\!·U2-R3 . Natr1x ChcM'cal**Mato ~** 

l.lalocam 10 AL3443 Sample lD . LB T U-U2 -R 1 .

. lrlattlx Chemical**Ma~ la** **l**

MaxiumiO . Al.3#1**~pie** 

### tp l.BTI:J.V2-R2

- Cllomica! Malorl .. 

# ...,.....,0 AL3-«6 . Sampi• 1D i.lmJ.u2-R3 Nn1»e Chcwrieol**M~ ie.!**  

### Ei'ISR International Clenl 

### Project#: 1002-022 Projed namo:**VEO~ IA** 
Collected 

### "'!!pped 

# .........

• l Cofloded 2008J09I109 · Sh i pped Recei'Vod 2008109111

collected 2008.109110 Shlppod ' Reodvul 2008.09111

COI'-c: l e d 20(l6.()9fOg



# ·-d ReuiV'td 2008109111 .
CoUoe\Od 2C108!109110 ShipP ed R4W;elved 2008J09,'1 1



## VES 004961

### Maxxwn .btl 

### II: 

### A8A2964 Report O.>t : 

### 2008/11114

hlaxxamiD N.3445 0Up Samp1o 10 LBTU .If2 · R3 Matrix Cb!"*:t. l I MtoMI

- · 10 Al.3440 S..plo ll**SF-U2~1** Test**Sum~ry**

## -~- 

# ....
lblrxam ID Al.34.C7 -10**SF-U2~ o.c**  

## .......... ... ,

Maxxam I D Al.34-48 

# '**semp~.** ID SF-U2-R3 M &trt.**~C'Imlc:al** Matetl tl

Muxam JO Al3449 Salnpe.IO CS.U2·R I . Mdr'bl OMmlcll J. \a1etlll .

Mmcut 0 At.34C9 Oup 5ampt6P**CS.O~fU** M allb : ctMtnical Material ENSRinlema:lonal Clenl Project 

### II: 1002-()22 • PO'CjeCI name: IIEOLLA

Collected 2008J09110 Shipped**~cckred** 2006109111



# eo•- 2000/0WIO 

### Sh il>pod Re«lwd 20CitlJ0Qi1 ; 

# . · .

VES 004962_. Job , , 

### A8A2964 

### R.o!>o<t 

## o• : 2008/11/14
Ma1001 m fO AL3450 S>onpje ID C$-U2·fl2 Matrix Cbemlcal**M~turi al** 

Ma:ltan't " ttt ALM51 SUoplelD CS.U2-& 

### Tost Summe ry



# ..

. - Clwrieal 

# M -

. . 

# . . . 

# · ·· "' ENSR lntemalional Cfi e nl Project#: 1002.022 Project 

### name: IIEOI.IA

Cob..::ted 2008109t\l9

Shlpp • d Reeelved 21108109/11

Colec:ted 200!W!V10 

# _. 

# - -1 , ·



## VES 004963M axxam .bb 

### H: A8A2964 Report Dale: 21108/1 1 /14 

# I

# uu**~ntawonWfo~-·~·•** GENJtRAL COMJIEtlTS

, ;



### . 

# .. ENSR l ntemoUorial C lien t PfOjecl #: 1002.022 Project 

### name: VEOliA



### . . .



## VES 0049641&1<4908 KCO

, Spll<od BionicMelhodRPD
1620332 'KCO**IM !UX~KE** **.** 

### QCST;ANOAAo MShod Blank 

### ENSR l ntomational Attention; 

### Jell GO<man 

### Cilcfll P roject lt. 

### 1 002.022 

### P.O.II: Pro j ect name: 

### VEOUA Qua!i1y Assurance RepOrt Maxxam Job Number. GA8A2964
200Ml9/!6 99. 99 2008100116 ti!D, RDL-0.005 2008/09116 4. 1 . • TOiaiAIHnlc(As) 2008109/15 0.53 106**TOOai ~-(** **Be)** 2008/09116 ' 0. 54 '105

. TOial CoOmlum (Cd ) . 2008109/16 0.53 105 To<ol Chl1lmium**(C~** 200tW9/ 1 6 0.53 1 05 T ota l Lcod (1'0) 200MMII16 0. 51 102 Total Afl¢ftic (As) 2000109116 0.61 1 02**Totai (Be)'**  200&.109118 0 . 63 106 Totalc-(Cd) 20061091 1 6 0.53 105 Tolll Ckon'ium (Cr) 2006/()g/18 0.62 103 TQUilead (Pb) 20081091 1 6 0 .5;2 1 03 To<al"'""" c (As) 200el09118 NO, RD LuO.ot T obl Bet)11um (S.) . 2008109116 NO, RDLoll.OOOS · T «a1 C.a dn'l ium (C d) 

# -· · ND, Rtll.u0.002 . Total Clllom'""' (Cr) 2008/09118 NO, RDLo0.005 Tolal Load (l't> ) 20011109/16 NO , RDL • 0.01 TotoiAroenlc(/\o) 2006/09118 • NC Total Be!l'lliom (8e) 2006/091 1 6 • NC TotaiCootrlun (C<I) 200610!l116 

### He T0181 Cluomltrn (Cr) 2(1()W()9J16 NC To<al Leed (Pb) 2008109/16 NC .tdd**Ell.~** Arsenic (M ) . . 2.008100122 0 .50 100 Add Eld- ll«y Uiti m (S a ) 200e/Oaf22 0.52 104

- Eld- Cadmium (C<I) 20011109122 0.48 96 lod6**~Cilrom um(~** 

# ~ OA9 98 ·

. Acid E!draclable leod (PbY 

### OA8 

### 96 Add £xtt8!ctabie A f'S.Iri: (A!) 2006109122 0.84. 95 Acid &b'sctab l e etwun iu m (C r ). 

### 2006I09J22 0.29 89 · . Acid**ble** l oad (Fb) 2008100/22 1 .3 96 

# Add"""'-- (As) . 2<100109122 NO, RlJI.o1**Add~ BG~y** **ll iu** **m** (Ber 2008109122 NO, RDlcO.S Add Exlnl<l- CadmiUn (C d ) 

### 2008109122 NO, RDL.o0.3 · Add -Chr-(Cr) ' 

### . 2008109122 RDUo05

. - E><lrad- . RDL • 1 . % 80 · 120 % ' % 

# ,. 20 mg.\. 75·125 mgll • 7.5 ·1125 mg.\. 7 5 -.125 mg.\. 75· 125 mgll 75 - 125 mgll . 80 · 126 mgll 76 ·119 mg/1. , ' 76 ·1 17 mgll. 75 .. 1 25 mgll 76 . 1 19 II¢ II¢ mgll mgll mgll

% 25 % 25 % 26 % 25 % 2S 75·125 75·126 7 5· 'i2S 7S· 1 26

. 75-125

75·125 75-125 ' 76·125



## V E S 00 4 96 5

### Validation Signa t u r e P a ge Maxxam J ob 

### 1 : A8A2964


### The aoalyticlli 

### data and 

### all QC 

### OODIOined in 

### Ibis rcpott WC<C 

### reviewed and valida t ed by 

### tire fuiJowing iodivi d uai(S).



# . .**'.J~**



### . ": · 

### Scientific SpeCialist



### ' .**Mf)UM)haa~bip ~topar4~i,.opor** **u.e 0rtho** **dedronk~N!4hvod»ftlqUi«d ••ip6~,upar~** **s.t0.2ot**
. J sOil&C 1'7025:2tflS(S).**·~~** tbert9.0fU.. SCCMd CALA havc-f41Pt0Yed**~** ptOCC8S .nd**~-report** fbmut. 

### ., 

# . 

# . .

. .. :



## V ES 004966

# VES 004967 . pdf

# UNIT3

VES 004967

## W as t e F e ed Re s ults

' 

# - '



# ...

. 

# . · .

VES 004968

# M . . a . .

am
At tentio n : Jeff Gormad ENSR International 

### 5015 

### CampuswoOd Dr .

. Suite 1 04 

### Syracude, NY . USA 

### 13057-4232 Your Project#: 1002-022**~ite:** 

### Veoi.la



### Report Dale: 2008/12102 

## CER TIFIC ATE O F ANALYS IS MAXXAM ' JOB #: A889378, A891648 & 

### A8A2964 Received: 

### Saiuple Matrix: soild # 

### Samples Received: 9 

## Analyses Moisture Dctenftinatlon 

## Date Quantity Extrileted 9 N/A 

### Date Analyzed 

# ttnonoos LabOratory Method

• RPD's calcu la te<! using raw dala. The 

### roundins of final =ulrs may 

### resu lt in the 

### appml difference.

# ·~4r:....-.**'** 

# ' · __,., . .,..... ' ....,...., . ,;;**Ji~~** . ..


### . 

# . . Mike Challis Customer Service Manager 

### MlllOOm Analytics Inc. · Burlington Method 

## Reference

VES 004969Confldem i N: M IXXam AnaJyb &nttmatfonat Page 1 or1 

## VES 004970**~** 

## }



# ( ) 1!!!!!!1 -- 

# . : llliiliiiil tyste!M

### ~~). 

### u.c ifleg-... Ot . HO.fleld ... 

## '?'«) (1d)21 S82U99<S ((c,)21 5-822-1 'lJJ3 

### Certifieate of Anal ytical Resul ts CLrEtiT: M aiu m Aaalytlial Servi«S



## . ·ssss No..,.·S<Mc<ll.d



## florliacto,;_ O otoJio · L 7L SK7 Lab 0.-dcr. R080 1 0020



### · P ro jt« : A889371



### · AO&l)'S<S As R e«ivedlluis D ry B asis 

### Ual.ts 

## W3l3-4 l !!, \**~'i-U3-I.Y.** Lab iD: M1080020'-0IA Date**Sa~** 08/0SI2008 

## o . .. tue<l ..

d : · 08114/lOOI PERCENT M OISTURE

Moisture , T otaJ 75.1 

# .. . A

S H. CO A L 

# """ • 8.52**~u** 

# .. fleA11NG V.AL\IE; COAL

tk»ting Value · 15«1 6.2-70 · 

# ....... , .

### AE0!4-0l!!~Q.!**Y3-~** 

### . IAbiD : ROI080020-02A 

## o ...**s~:** 0810712008 

### Date ltcc.c::i¥e4..:**01!114120~8** PE f<CE NT MOISTURE.**o;s.~.** Total 71.5

. ASH, COAL



# ..... 9.80

. -

HEATIN G VALUE. COAL

-Value 

### 161!0



### < 

### l a<jicates less dw\ tho 

### (imitofquaAtitation R - H.o14 t:uae cx.c.e&ulee 

# .. - 3 ·

U 

# " 5,890 

# - Date : 18 - Aug-08 .

Metllod Date A.llalyst 

### [llatrlc SOUD OU18 

### 1 4-IIIJ9.()8 VJO 03174- 

# . ......... VJO**sass** • 15-Aug.oa OAS

. I •
. Matrix: $0[..10 •

02216**~** VJO 03t74

# ·~ VJO • 0$865 

# ..**~** OAS

P&&c I o ( 2

. . ":"14 POTTSVILlE P t tq:. RE.A()(NG . PENNSYLVANIA 19005

### 610-92.1~33 FAX 610.921-0667


## VES 004971

## j

•,. 

# .·
iii69 . Sal,'dolcr.et> : - Po.

## i~**~·** f-«12:8195 ( 1 ..

)21

5-822 - l 293 

### C..rtiOq t e o( Analytical Res•la C LUNl' : . · M iu::am Aa a lyti e al St:nices SSSS Korth Servici Rd

### (hu**i~CM.** Oatart. L7L S H

7 

### l .a.b**Ordc•· ~**  

## Roaosa o zo · · :fro J oc:t**~8&93 78**  

## Aao.tr- Asll«eiYedBull 

### Dry B ull 

### A)t,3J.5..GlR \ C$-!13=R3 

## Lob 

# ro : 'Rosoaoo1(l.(iJA Da<cS....,I<.t : O!lf17f2!!03 · 0... R.<tt<Y ..t : 

### OtJ1412001 PERCEHT MO ISTURE

, M<*CW.:T.cll1 ASH , · COAL



# ... HEATiNG V-'i.UE. COAL

t1 oltiog 

### vaeUe 7G . S , 8.o9 .• 

## zu 15()0**o.~** 

### • ba te: 18-A•g · 08

,. Uai.ts • Met lood**·** 

### Autj,t . 

## -M.? tr!£ 

## SOLID 1<0 022 16

# · VXJ 

# " 031 7 .. ..**15~** VJ O ,



### . llli>'l b ' o;a65**1S-IWQ-o ~**  DAS


# . .

·**----~=---...:..-- -_;,_.,----'**  

# _ _._,.--:- ____ -:-- _ __;_,....--:.

# · ..



# .... . •,



### < 

### l.odi<otes I..,**.dian~** 

### limit**ofquaod~Uoo** 

### ff-1l oWr ..**~** 

# .·



# .. , 

# .**~.** 

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## " Alt cn!loni Jeff Gorman 

### ENSR Internationa l 5015 Campuswood Dr 

### Su i to104 

### East Syracuse, 

### NY USA 

### 13057-4232

MAXxAMJOB 

### II; A889378 Received:**~oa/00/08 ,**  

### 0:00 

### Sample Matrix: UQUID 

### # Samples Reoelved: 9
Sample Matrix: Soil · 

### # Sa'!'ples**~eceived:** 

### 3 

### ·' · Ndons I n Ctlem l iil M a tedal -inSollbyCVM · . To«aa M 01all in Soi.by 

### AldOl I CP.AES 

### Sample Matrix: Water 

### H

Samples 

### ReceM>d: 3 

### Your Project 11-: 

### 1002-022 Site:VEOUA



### . Report Dat e: 2008111/14 This repo(l supersedes all pre\liQus repotls wilh lho 

### SOIM Maxxam job number 

### CERTIFICAT E O F ANALYSIS

9 9 2006/oe/15 2008108/18 CAM SOP.Q0453 2008J0811S 2008108118 CAM SOP-00408

. 3 . 2008108115 .

3 . 200810l!115 200810811 5**CAMSOP·00~5:f** 3 . 2008108(1 5 2008/0&'17 0nt SOP.0072 . EPA 7470 EP

A 6010C

ePA 7470**EPASW~IOC.**

( t ) tAruoc.am AnatyUc:s; does not**hold~** b analysis of metals In water samples**u~** lle IC P A)ljal mothodotogy.


### MAXXAMANAL YTICs 

### Tota l coverpages:1



## VES 004990

### Maxxa rn Job 

### lt. 11889378 R

eport Oslo: 2008/ 1 1/ 14 ENSR lnlemalionsl 

### C l

ie nt Projo c llt. 1002.022 Pro j oct name: VEO LI A RESU L TS O F ANA L YS E S O F U QU I O

. 05 1687 , 595

» O

S 1 557595

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. Projecl 

### r .ame : VEOI.IA E LEMENTS BY AT OMIC SPEC TROSCOPY (LIQUID)

# ~%

.... _(As) mg/1. 11 12" 11 0.5 0.3 0.1 15 87400

.... e..,o.m(Bo) mgll ND NO NO 0.03 Nil 0 . 005 1587 400 ota!C-(Cd) mgll. 

### NO ND NO 0 .1 NO O.D2 158 1400 ota

l Clvorium**(C~** mgll. 3 .9 . .•. $ , .4.5 0.3 0.'18 0.05 1 587400 

### otat Load (Pb) mgll. 0.6 1 . 2 1. 3 0.5 NO · 0.1**1S87~00** ry(Hg) mgiL**o.oo:~9** 

# ro 0.0 . !_58 (1)**0.~100** (1) .0015 0 .0019 (1) .0015 1581 438 • N:oC do lOdod RDL =**~· De** **-Um lt**  QC 8ald> • O""'IIY Comrol 8ol<lh · · . .

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.... 8orj!lul!l (Be) mg/l 

### NO NO 

### . I< D NO NO 0.005 . 1561400 

### otat 

### cn.tum (Cd) mgiL · NO 

### N D N O NO NO 0.62 1587 400**OIOICM>mtum(~** mgiL 0.05 NO . NO NO . NO 

## o.os 1587400 otoll.ead (Pb) mgll. NO 

### N O NO . NO**·~ o**  0.1 158 7400 (Hg) mgiL NO (I)**NO~) ·**  NIA 0.0087 (1) 

### N D(I) .00 15 1587438 II Not dotoded A • Not AppliCIIIbf O

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### vms Stlbm i ltcd**an~** b;ottl&.**~** 

### m_ay . be biased 1ow due to lmpropet 

### preserva tfon .



## V E S 004992MOXJCam 

### Job 

### II: A889378 

### Report Date: 2008/ 11/ 14 .



# . ·

. .. ENSR lnlemational Clieni Project II: 1002-022

. Project n ome: 

### VEOLIA ELE MENTS BY ATOMIC SPECTROSCOPY (UQUID) ·

# ~ l

..., At$8flle (As) rogll. NO 0 . 1 1587400 To<al Bor,Cllum {&} 

# ........ NO 0 . 005 1587.00 Olal Cadm i llffi (Cd) mg/1. NO 0 .02 15874 00 otaiC-(c.) mg/l NO 0.05 158l400 otalload (Pb) mgll NO 0.1 15&7@

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### Report Oato: 200S/11/ 14



# .. £*4• 

### ENSR lntomatlooat Client Project#; 

### 1002.022

. Project namo : 1/EOUA RESUL T S OF AN ALYSES OF SOIL



# . . . .

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### ENSR International Cl i ent Pro j ect 

### # : 1 002..022 Project n ame: VEOLIA 

### Maxxam Job 

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### report superse<Jes all previous reports 

### with the 

### same Maxxam job 

### number EL EM ENTs BY AT O MI C S P ECTROSCOPY (S OIL )

N O e Not detected 

### Rf?L 

# = Reportable Detection Umlt QC Batch " Quality Control Batch .



## VES 004995

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SR I <Umatiol'llll a ; ent Projec;lll: 1002-{)22 Project nam e: VEOUA ELEMENTS B Y ATOMIC SPECTROSCOPY (WATER)

•**R~** OOOdon Umil Ba!d1 • Quoily .**Cor*'>~** Baldi



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Mauam 10 A.e6304 Sampl• 10 HBTU -:0 3- Rt Matrix UOt.nD .

Uaxxam 10 AE630S Somplo ID H8TU-l13-lU**~** UQUIO

Maxxem to AaSDG SompleiD HBTU-U34<3

' · Mattix LIQU I D

.........**10~ ~mple**  10 LBTIJ..U3-R 1

· · Matri x UOU I O



### Ma.xnm 10 AE6306 Sama>l$ 10 LBTU-U3-R2.

. · llafltx LIQUID Test Summary ENSR 

### in temattonal Cient Projed #: t002.Q22 P r

ojecl name: VEOUA



## VES 004997

# · ...,o M 

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### Date: 2008/11/14

llaxxamiO AE0009 Sample 10 LB TlJ..U3-R3 Matrix . UQUIO

. llalowoiD A£63090v;>

Sample 

### I!> 1.8'1\J · V3-R3 • · Motllx UQU ID
M

uxaM 10 AE63i0

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- tiQUID

Muxam 10 AE63 1 2 ' .Sampt • 10 SF-o0s.R3 M- UQ V IO

Muxa m to Ae63 t3 Sample ID CS-U3-R1 Matrix SoU 

### Test Summary E.NSR lnt«nalfonal 

### C

lient Project#: 

### 1 002.022 Pro j ocl nome: VEO LI A

• Co11Ki.d · · 2008/0Ml7**·. ·**  

# Sb- .
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### . 20081081<ia

Co l

lei:t od 2008108105 : S-d Reeetvod 2008/08108



## VES 004998' ·**', ;**  

### M""""m Job #: 

### A88937 8 R ep ort 0018: 20081 1 11 14

## ~ Muxam 10 AE6313 OUp Sntplt 10 CS - !J3.R t UaMx 

## so f ·
Mtxxam 

## m AE6314 · Sampte. tO**~2** Matrix Sol

Malo<OmiD Ae6315 

### s ...**p~eto ~R3**  Matrtx Soli

Max!t8m 10 AEB316 Santplell NS.V3 · R1 : Molrii' Wat er

# ~**~ID** AE 631 7 S..nple ID MS.\J3.R2 Malrtx 

# -
'MalOUiillliD · AE63 18 S«Jnppe 10 MS-Ua.R3 MlrtriX Wat lll' Test Summary ENSR In t ernational ell""' Project**#: 002~2**  Project name: VEOLIA
Col l eelcd 2008108105 Shipped Received ' 2008108108 .

. .- . C oh ct.d· 2006100107 SNpped

.**~** Received 20061()8108:**~** ,' '

Coli- 2008108107 Sh i

pped R•c•tv.d 2008108108

Co-d**~** ShlppOd R

- 2008/06106 

# eo-• 20,08mi01'

Slllpped Recolved '

### ~
Collectod 2008108107 ' Sb\J>ped 

### 2,ooeiOaios**~,d** 

## ''

VES 00 4 999