Dolan Chemical Laboratory

4001 Bixby Road

Groveport, OH 43125

T: 614-836-4221, Audinet 210-4221

F: 614-836-4168, Audinet 210-4168

http://aepenv/labs

Water Analysis

Form REP-703

Rev. 0, 4/2012

Location: Mountaineer Plant Reissued Report Date: 9/9/2013

Sample Number: 132703-001 Date Collected: 07/02/2013 Date Received: 7/2/2013

CPS Influent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 30.1 ug/L 0.050 0.010 DPC 07/08/2013 14:45 EPA 200.8

Arsenic, As 123 ug/L 0.10 0.030 DPC 07/08/2013 14:45 EPA 200.8

Barium, Ba 208 ug/L 0.10 0.020 DPC 07/08/2013 14:45 EPA 200.8

Beryllium, Be < 0.30 ug/L U 1.0 0.30 DAM 07/12/2013 09:38 EPA 200.7

Cadmium, Cd 214 ug/L 0.050 0.010 DPC 07/08/2013 14:45 EPA 200.8

Chromium, Cr 752 ug/L 0.20 0.040 DPC 07/08/2013 14:45 EPA 200.8

Cobalt, Co 201 ug/L 0.020 0.0040 DPC 07/08/2013 14:45 EPA 200.8

Copper, Cu 460 ug/L 0.050 0.010 DPC 07/08/2013 14:45 EPA 200.8

Lead, Pb 234 ug/L 0.010 0.0020 DPC 07/08/2013 14:45 EPA 200.8

Mercury, Hg 256000 ng/L 5000 2000 TLT 07/12/2013 EPA 1631E

Molybdenum, Mo 613 ug/L 0.050 0.010 DPC 07/08/2013 14:45 EPA 200.8

Nickel, Ni 1610 ug/L 0.20 0.050 DPC 07/08/2013 14:45 EPA 200.8

Selenium, Se 1200 ug/L 0.50 0.20 DPC 07/08/2013 14:45 EPA 200.8

Silver, Ag 0.480 ug/L 0.010 0.0020 DPC 07/08/2013 14:45 EPA 200.8

Thallium, Tl 10.7 ug/L 0.050 0.0020 DPC 07/08/2013 14:45 EPA 200.8

Tin, Sn < 3.0 ug/L U 10 3.0 DAM 07/12/2013 09:38 EPA 200.7

Titanium, Ti 217 ug/L 2.0 0.30 DAM 07/12/2013 09:38 EPA 200.7

Zinc, Zn 3400 ug/L 0.50 0.10 DPC 07/08/2013 14:45 EPA 200.8

Aluminum, Al 20.6 mg/L 0.0010 0.0003 DPC 07/08/2013 14:45 EPA 200.8

Boron, B 461 mg/L 0.020 0.0040 DAM 07/12/2013 09:38 EPA 200.7

Calcium, Ca 1800 mg/L 0.020 0.0040 DAM 07/12/2013 09:38 EPA 200.7

Iron, Fe 174 mg/L 0.050 0.010 DAM 07/12/2013 09:38 EPA 200.7

Magnesium, Mg 4180 mg/L 0.010 0.0020 DAM 07/12/2013 09:38 EPA 200.7

Manganese, Mn 36.4 mg/L 0.0005 0.0001 DAM 07/12/2013 09:38 EPA 200.7

Potassium, K 75.3 mg/L 0.050 0.0070 DAM 07/12/2013 09:37 EPA 200.7

Sodium, Na 375 mg/L 0.030 0.0080 DAM 07/12/2013 09:37 EPA 200.7

Strontium, Sr 15.4 mg/L 0.0010 0.0003 DAM 07/12/2013 09:37 EPA 200.7

Ammonia, NH3, as N 2.26 mg/L 0.050 0.020 DMM 07/03/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 4.49 mg/L 0.50 0.10 DMM 07/09/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 68.1 mg/L 0.10 0.020 DMM 07/03/2013 SM20 4500NO3 H

Total Nitrogen, N 72.6 mg/L 0.50 0.10 DMM 07/10/2013 Calculation

Total Organic Nitrogen, TON 2.2 mg/L 0.50 0.10 DMM 07/10/2013 Calculation

Mountaineer Plant, 132703 Page 1 of 11
Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number: 132703-001A Date Collected: 07/02/2013 Date Received: 7/2/2013

CPS Influent Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 3.53 ug/L 0.050 0.010 DPC 07/08/2013 14:50 EPA 200.8

Arsenic, As 2.73 ug/L 0.10 0.030 DPC 07/08/2013 14:50 EPA 200.8

Barium, Ba 90.1 ug/L 0.10 0.020 DPC 07/08/2013 14:50 EPA 200.8

Beryllium, Be < 0.30 ug/L U 1.0 0.30 DAM 07/12/2013 10:25 EPA 200.7

Cadmium, Cd 148 ug/L 0.050 0.010 DPC 07/08/2013 14:50 EPA 200.8

Chromium, Cr 1.1 ug/L 0.20 0.040 DPC 07/08/2013 14:50 EPA 200.8

Cobalt, Co 133 ug/L 0.020 0.0040 DPC 07/08/2013 14:50 EPA 200.8

Copper, Cu 6.44 ug/L 0.050 0.010 DPC 07/08/2013 14:50 EPA 200.8

Lead, Pb 0.315 ug/L 0.010 0.0020 DPC 07/08/2013 14:50 EPA 200.8

Molybdenum, Mo 463 ug/L 0.050 0.010 DPC 07/08/2013 14:50 EPA 200.8

Nickel, Ni 1170 ug/L 0.20 0.050 DPC 07/08/2013 14:50 EPA 200.8

Selenium, Se 738 ug/L 0.50 0.20 DPC 07/08/2013 14:50 EPA 200.8

Selenite, Se+4 (Hydride) 183 ug/L 20 4.0 TLT 07/15/2013 AEP Method

Silver, Ag 0.0080 ug/L J 0.010 0.0020 DPC 07/08/2013 14:50 EPA 200.8

Thallium, Tl 7.83 ug/L 0.050 0.0020 DPC 07/08/2013 14:50 EPA 200.8

Tin, Sn < 3.0 ug/L U 10 3.0 DAM 07/12/2013 10:25 EPA 200.7

Titanium, Ti < 0.30 ug/L U 2.0 0.30 DAM 07/12/2013 10:25 EPA 200.7

Zinc, Zn 614 ug/L 0.50 0.10 DPC 07/08/2013 14:50 EPA 200.8

Aluminum, Al 0.0561 mg/L 0.0010 0.0003 DPC 07/08/2013 14:50 EPA 200.8

Boron, B 460 mg/L 0.020 0.0040 DAM 07/12/2013 10:25 EPA 200.7

Calcium, Ca 855 mg/L 0.020 0.0040 DAM 07/12/2013 10:25 EPA 200.7

Iron, Fe < 0.010 mg/L U 0.050 0.010 DAM 07/12/2013 10:25 EPA 200.7

Magnesium, Mg 3860 mg/L 0.010 0.0020 DAM 07/12/2013 10:25 EPA 200.7

Manganese, Mn 31.4 mg/L 0.0005 0.0001 DAM 07/12/2013 10:25 EPA 200.7

Potassium, K 70.3 mg/L 0.050 0.0070 DAM 07/12/2013 10:23 EPA 200.7

Sodium, Na 372 mg/L 0.030 0.0080 DAM 07/12/2013 10:23 EPA 200.7

Strontium, Sr 12.3 mg/L 0.0010 0.0003 DAM 07/12/2013 10:23 EPA 200.7

Bromide, Br 42.3 mg/L 1.0 0.20 TJK 07/05/2013 EPA 300.1

Sample Number: 132703-002 Date Collected: 07/02/2013 Date Received: 7/2/2013

 CPS Primary Clarifier Effluent

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Mercury, Hg 664 ng/L 50 20 TLT 07/12/2013 EPA 1631E

Nitrate-Nitrite, NO3-NO2, as N 49.0 mg/L 0.10 0.020 DMM 07/03/2013 SM20 4500NO3 H

Mountaineer Plant, 132703 Page 2 of 11
Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number: 132703-003 Date Collected: 07/02/2013 Date Received: 7/2/2013

CPS Effluent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.86 ug/L 0.050 0.010 DPC 07/08/2013 14:55 EPA 200.8

Arsenic, As 2.09 ug/L 0.10 0.030 DPC 07/08/2013 14:55 EPA 200.8

Barium, Ba 76.0 ug/L 0.10 0.020 DPC 07/08/2013 14:55 EPA 200.8

Beryllium, Be < 0.30 ug/L U 1.0 0.30 DAM 07/12/2013 09:42 EPA 200.7

Cadmium, Cd 0.18 ug/L 0.050 0.010 DPC 07/08/2013 14:55 EPA 200.8

Chromium, Cr 4.4 ug/L 0.20 0.040 DPC 07/08/2013 14:55 EPA 200.8

Cobalt, Co 0.761 ug/L 0.020 0.0040 DPC 07/08/2013 14:55 EPA 200.8

Copper, Cu 0.88 ug/L 0.050 0.010 DPC 07/08/2013 14:55 EPA 200.8

Lead, Pb 0.132 ug/L 0.010 0.0020 DPC 07/08/2013 14:55 EPA 200.8

Mercury, Hg 107 ng/L 50 20 TLT 07/12/2013 EPA 1631E

Molybdenum, Mo 326 ug/L 0.050 0.010 DPC 07/08/2013 14:55 EPA 200.8

Nickel, Ni 27.5 ug/L 0.20 0.050 DPC 07/08/2013 14:55 EPA 200.8

Selenium, Se 404 ug/L 0.50 0.20 DPC 07/08/2013 14:55 EPA 200.8

Silver, Ag 0.0020 ug/L J 0.010 0.0020 DPC 07/08/2013 14:55 EPA 200.8

Thallium, Tl 0.62 ug/L 0.050 0.0020 DPC 07/08/2013 14:55 EPA 200.8

Tin, Sn < 3.0 ug/L U 10 3.0 DAM 07/12/2013 09:42 EPA 200.7

Titanium, Ti < 0.30 ug/L U 2.0 0.30 DAM 07/12/2013 09:42 EPA 200.7

Zinc, Zn 3.8 ug/L 0.50 0.10 DPC 07/08/2013 14:55 EPA 200.8

Aluminum, Al 0.107 mg/L 0.0010 0.0003 DPC 07/08/2013 14:55 EPA 200.8

Boron, B 240 mg/L 0.020 0.0040 DAM 07/12/2013 09:42 EPA 200.7

Calcium, Ca 647 mg/L 0.020 0.0040 DAM 07/12/2013 09:42 EPA 200.7

Iron, Fe 0.931 mg/L 0.050 0.010 DAM 07/12/2013 09:42 EPA 200.7

Magnesium, Mg 2000 mg/L 0.010 0.0020 DAM 07/12/2013 09:42 EPA 200.7

Manganese, Mn 11.1 mg/L 0.0005 0.0001 DAM 07/12/2013 09:42 EPA 200.7

Potassium, K 38.2 mg/L 0.050 0.0070 DAM 07/12/2013 09:40 EPA 200.7

Sodium, Na 210 mg/L 0.030 0.0080 DAM 07/12/2013 09:40 EPA 200.7

Strontium, Sr 6.73 mg/L 0.0010 0.0003 DAM 07/12/2013 09:40 EPA 200.7

Ammonia, NH3, as N 1.16 mg/L 0.050 0.020 DMM 07/03/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 3.79 mg/L 0.50 0.10 DMM 07/09/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 37.9 mg/L 0.10 0.020 DMM 07/03/2013 SM20 4500NO3 H

Total Nitrogen, N 41.7 mg/L 0.50 0.10 DMM 07/10/2013 Calculation

Total Organic Nitrogen, TON 2.6 mg/L 0.50 0.10 DMM 07/10/2013 Calculation

Mountaineer Plant, 132703 Page 3 of 11
Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number: 132703-003A Date Collected: 07/02/2013 Date Received: 7/2/2013

CPS Effluent Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.75 ug/L 0.050 0.010 DPC 07/08/2013 15:14 EPA 200.8

Arsenic, As 1.83 ug/L 0.10 0.030 DPC 07/08/2013 15:14 EPA 200.8

Barium, Ba 70.2 ug/L 0.10 0.020 DPC 07/08/2013 15:14 EPA 200.8

Beryllium, Be < 0.30 ug/L U 1.0 0.30 DAM 07/12/2013 10:29 EPA 200.7

Cadmium, Cd 0.10 ug/L 0.050 0.010 DPC 07/08/2013 15:14 EPA 200.8

Chromium, Cr 3.3 ug/L 0.20 0.040 DPC 07/08/2013 15:14 EPA 200.8

Cobalt, Co 0.247 ug/L 0.020 0.0040 DPC 07/08/2013 15:14 EPA 200.8

Copper, Cu 0.24 ug/L 0.050 0.010 DPC 07/08/2013 15:14 EPA 200.8

Lead, Pb 0.042 ug/L 0.010 0.0020 DPC 07/08/2013 15:14 EPA 200.8

Molybdenum, Mo 310 ug/L 0.050 0.010 DPC 07/08/2013 15:14 EPA 200.8

Nickel, Ni 12.9 ug/L 0.20 0.050 DPC 07/08/2013 15:14 EPA 200.8

Selenium, Se 379 ug/L 0.50 0.20 DPC 07/08/2013 15:14 EPA 200.8

Selenite, Se+4 (Hydride) 145 ug/L 20 4.0 TLT 07/15/2013 AEP Method

Silver, Ag 0.0030 ug/L J 0.010 0.0020 DPC 07/08/2013 15:14 EPA 200.8

Thallium, Tl 0.40 ug/L 0.050 0.0020 DPC 07/08/2013 15:14 EPA 200.8

Tin, Sn < 3.0 ug/L U 10 3.0 DAM 07/12/2013 10:29 EPA 200.7

Titanium, Ti < 0.30 ug/L U 2.0 0.30 DAM 07/12/2013 10:29 EPA 200.7

Zinc, Zn 1.3 ug/L 0.50 0.10 DPC 07/08/2013 15:14 EPA 200.8

Aluminum, Al 0.0187 mg/L 0.0010 0.0003 DPC 07/08/2013 15:14 EPA 200.8

Boron, B 239 mg/L 0.020 0.0040 DAM 07/12/2013 10:29 EPA 200.7

Calcium, Ca 646 mg/L 0.020 0.0040 DAM 07/12/2013 10:29 EPA 200.7

Iron, Fe < 0.010 mg/L U 0.050 0.010 DAM 07/12/2013 10:29 EPA 200.7

Magnesium, Mg 2000 mg/L 0.010 0.0020 DAM 07/12/2013 10:29 EPA 200.7

Manganese, Mn 10.9 mg/L 0.0005 0.0001 DAM 07/12/2013 10:29 EPA 200.7

Potassium, K 37.9 mg/L 0.050 0.0070 DAM 07/12/2013 10:27 EPA 200.7

Sodium, Na 209 mg/L 0.030 0.0080 DAM 07/12/2013 10:27 EPA 200.7

Strontium, Sr 6.73 mg/L 0.0010 0.0003 DAM 07/12/2013 10:27 EPA 200.7

Bromide, Br 24.7 mg/L 1.0 0.20 TJK 07/05/2013 EPA 300.1

Mountaineer Plant, 132703 Page 4 of 11
Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number: 132703-004 Date Collected: 07/02/2013 Date Received: 7/2/2013

 Landfill Leachate Effluent

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 10.6 ug/L 0.050 0.010 DPC 07/08/2013 15:19 EPA 200.8

Arsenic, As 37.1 ug/L 0.10 0.030 DPC 07/08/2013 15:19 EPA 200.8

Barium, Ba 29.7 ug/L 0.10 0.020 DPC 07/08/2013 15:19 EPA 200.8

Beryllium, Be < 0.30 ug/L U 1.0 0.30 DAM 07/12/2013 09:50 EPA 200.7

Cadmium, Cd 1.64 ug/L 0.050 0.010 DPC 07/08/2013 15:19 EPA 200.8

Chromium, Cr 2.5 ug/L 0.20 0.040 DPC 07/08/2013 15:19 EPA 200.8

Cobalt, Co 3.15 ug/L 0.020 0.0040 DPC 07/08/2013 15:19 EPA 200.8

Copper, Cu 0.60 ug/L 0.050 0.010 DPC 07/08/2013 15:19 EPA 200.8

Lead, Pb 0.072 ug/L 0.010 0.0020 DPC 07/08/2013 15:19 EPA 200.8

Mercury, Hg 82.3 ng/L 50 20 TLT 07/12/2013 EPA 1631E

Molybdenum, Mo 6470 ug/L 0.050 0.010 DPC 07/08/2013 15:19 EPA 200.8

Nickel, Ni 23.7 ug/L 0.20 0.050 DPC 07/08/2013 15:19 EPA 200.8

Selenium, Se 228 ug/L 0.50 0.20 DPC 07/08/2013 15:19 EPA 200.8

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 07/08/2013 15:19 EPA 200.8

Thallium, Tl 2.80 ug/L 0.050 0.0020 DPC 07/08/2013 15:19 EPA 200.8

Tin, Sn < 3.0 ug/L U 10 3.0 DAM 07/12/2013 09:51 EPA 200.7

Titanium, Ti < 0.30 ug/L U 2.0 0.30 DAM 07/12/2013 09:50 EPA 200.7

Zinc, Zn 2.4 ug/L 0.50 0.10 DPC 07/08/2013 15:19 EPA 200.8

Aluminum, Al 0.0360 mg/L 0.0010 0.0003 DPC 07/08/2013 15:19 EPA 200.8

Boron, B 60.7 mg/L 0.020 0.0040 DAM 07/12/2013 09:50 EPA 200.7

Calcium, Ca 419 mg/L 0.020 0.0040 DAM 07/12/2013 09:50 EPA 200.7

Iron, Fe 0.090 mg/L 0.050 0.010 DAM 07/12/2013 09:51 EPA 200.7

Magnesium, Mg 459 mg/L 0.010 0.0020 DAM 07/12/2013 09:50 EPA 200.7

Manganese, Mn 1.79 mg/L 0.0005 0.0001 DAM 07/12/2013 09:50 EPA 200.7

Potassium, K 94.3 mg/L 0.050 0.0070 DAM 07/12/2013 09:49 EPA 200.7

Sodium, Na 1590 mg/L 0.030 0.0080 DAM 07/12/2013 09:49 EPA 200.7

Strontium, Sr 5.34 mg/L 0.0010 0.0003 DAM 07/12/2013 09:49 EPA 200.7

Ammonia, NH3, as N 1.48 mg/L 0.050 0.020 DMM 07/03/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 2.44 mg/L 0.50 0.10 DMM 07/09/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 6.54 mg/L 0.10 0.020 DMM 07/03/2013 SM20 4500NO3 H

Total Nitrogen, N 8.98 mg/L 0.50 0.10 DMM 07/10/2013 Calculation

Total Organic Nitrogen, TON 1.0 mg/L 0.50 0.10 DMM 07/10/2013 Calculation

Mountaineer Plant, 132703 Page 5 of 11
Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number: 132703-004A Date Collected: 07/02/2013 Date Received: 7/2/2013

 Landfill Leachate Effluent Dissolved

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 9.57 ug/L 0.050 0.010 DPC 07/08/2013 15:23 EPA 200.8

Arsenic, As 30.9 ug/L 0.10 0.030 DPC 07/08/2013 15:23 EPA 200.8

Barium, Ba 26.6 ug/L 0.10 0.020 DPC 07/08/2013 15:23 EPA 200.8

Beryllium, Be < 0.30 ug/L U 1.0 0.30 DAM 07/12/2013 10:37 EPA 200.7

Cadmium, Cd 1.31 ug/L 0.050 0.010 DPC 07/08/2013 15:23 EPA 200.8

Chromium, Cr 1.6 ug/L 0.20 0.040 DPC 07/08/2013 15:23 EPA 200.8

Cobalt, Co 2.52 ug/L 0.020 0.0040 DPC 07/08/2013 15:23 EPA 200.8

Copper, Cu 0.38 ug/L 0.050 0.010 DPC 07/08/2013 15:23 EPA 200.8

Lead, Pb 0.029 ug/L 0.010 0.0020 DPC 07/08/2013 15:23 EPA 200.8

Molybdenum, Mo 5820 ug/L 0.050 0.010 DPC 07/08/2013 15:23 EPA 200.8

Nickel, Ni 21.1 ug/L 0.20 0.050 DPC 07/08/2013 15:23 EPA 200.8

Selenium, Se 180 ug/L 0.50 0.20 DPC 07/08/2013 15:23 EPA 200.8

Selenite, Se+4 (Hydride) 86.6 ug/L 20 4.0 TLT 07/15/2013 AEP Method

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 07/08/2013 15:23 EPA 200.8

Thallium, Tl 2.38 ug/L 0.050 0.0020 DPC 07/08/2013 15:23 EPA 200.8

Tin, Sn < 3.0 ug/L U 10 3.0 DAM 07/12/2013 10:38 EPA 200.7

Titanium, Ti < 0.30 ug/L U 2.0 0.30 DAM 07/12/2013 10:37 EPA 200.7

Zinc, Zn 2.7 ug/L 0.50 0.10 DPC 07/08/2013 15:23 EPA 200.8

Aluminum, Al 0.0295 mg/L 0.0010 0.0003 DPC 07/08/2013 15:23 EPA 200.8

Boron, B 60.7 mg/L 0.020 0.0040 DAM 07/12/2013 10:37 EPA 200.7

Calcium, Ca 419 mg/L 0.020 0.0040 DAM 07/12/2013 10:37 EPA 200.7

Iron, Fe < 0.010 mg/L U 0.050 0.010 DAM 07/12/2013 10:38 EPA 200.7

Magnesium, Mg 457 mg/L 0.010 0.0020 DAM 07/12/2013 10:37 EPA 200.7

Manganese, Mn 1.72 mg/L 0.0005 0.0001 DAM 07/12/2013 10:37 EPA 200.7

Potassium, K 94.2 mg/L 0.050 0.0070 DAM 07/12/2013 10:36 EPA 200.7

Sodium, Na 1590 mg/L 0.030 0.0080 DAM 07/12/2013 10:36 EPA 200.7

Strontium, Sr 5.29 mg/L 0.0010 0.0003 DAM 07/12/2013 10:36 EPA 200.7

Bromide, Br 11.3 mg/L 1.0 0.20 TJK 07/05/2013 EPA 300.1

Mountaineer Plant, 132703 Page 6 of 11
Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number: 132703-005 Date Collected: 07/02/2013 Date Received: 7/2/2013

1st Stage Feed 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 6.01 ug/L 0.050 0.010 DPC 07/08/2013 15:28 EPA 200.8

Arsenic, As 19.0 ug/L 0.10 0.030 DPC 07/08/2013 15:28 EPA 200.8

Barium, Ba 52.5 ug/L 0.10 0.020 DPC 07/08/2013 15:28 EPA 200.8

Beryllium, Be < 0.30 ug/L U 1.0 0.30 DAM 07/12/2013 09:54 EPA 200.7

Cadmium, Cd 1.03 ug/L 0.050 0.010 DPC 07/08/2013 15:28 EPA 200.8

Chromium, Cr 3.8 ug/L 0.20 0.040 DPC 07/08/2013 15:28 EPA 200.8

Cobalt, Co 2.02 ug/L 0.020 0.0040 DPC 07/08/2013 15:28 EPA 200.8

Copper, Cu 0.83 ug/L 0.050 0.010 DPC 07/08/2013 15:28 EPA 200.8

Lead, Pb 0.129 ug/L 0.010 0.0020 DPC 07/08/2013 15:28 EPA 200.8

Mercury, Hg 140 ng/L J 250 100 TLT 07/12/2013 EPA 1631E

Molybdenum, Mo 3110 ug/L 0.050 0.010 DPC 07/08/2013 15:28 EPA 200.8

Nickel, Ni 28.6 ug/L 0.20 0.050 DPC 07/08/2013 15:28 EPA 200.8

Selenium, Se 342 ug/L 0.50 0.20 DPC 07/08/2013 15:28 EPA 200.8

Silver, Ag 0.0030 ug/L J 0.010 0.0020 DPC 07/08/2013 15:28 EPA 200.8

Thallium, Tl 1.45 ug/L 0.050 0.0020 DPC 07/08/2013 15:28 EPA 200.8

Tin, Sn < 3.0 ug/L U 10 3.0 DAM 07/12/2013 09:54 EPA 200.7

Titanium, Ti < 0.30 ug/L U 2.0 0.30 DAM 07/12/2013 09:54 EPA 200.7

Zinc, Zn 3.7 ug/L 0.50 0.10 DPC 07/08/2013 15:28 EPA 200.8

Aluminum, Al 0.0686 mg/L 0.0010 0.0003 DPC 07/08/2013 15:28 EPA 200.8

Boron, B 157 mg/L 0.020 0.0040 DAM 07/12/2013 09:54 EPA 200.7

Calcium, Ca 528 mg/L 0.020 0.0040 DAM 07/12/2013 09:54 EPA 200.7

Iron, Fe 0.564 mg/L 0.050 0.010 DAM 07/12/2013 09:54 EPA 200.7

Magnesium, Mg 1260 mg/L 0.010 0.0020 DAM 07/12/2013 09:54 EPA 200.7

Manganese, Mn 6.70 mg/L 0.0005 0.0001 DAM 07/12/2013 09:54 EPA 200.7

Potassium, K 64.2 mg/L 0.050 0.0070 DAM 07/12/2013 09:52 EPA 200.7

Sodium, Na 835 mg/L 0.030 0.0080 DAM 07/12/2013 09:52 EPA 200.7

Strontium, Sr 6.07 mg/L 0.0010 0.0003 DAM 07/12/2013 09:52 EPA 200.7

Ammonia, NH3, as N 1.30 mg/L 0.050 0.020 DMM 07/03/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 2.68 mg/L 0.50 0.10 DMM 07/09/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 22.4 mg/L 0.10 0.020 DMM 07/03/2013 SM20 4500NO3 H

Total Nitrogen, N 25.1 mg/L 0.50 0.10 DMM 07/10/2013 Calculation

Total Organic Nitrogen, TON 1.4 mg/L 0.50 0.10 DMM 07/10/2013 Calculation

Mountaineer Plant, 132703 Page 7 of 11
Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number: 132703-005A Date Collected: 07/02/2013 Date Received: 7/2/2013

1st Stage Feed Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 6.00 ug/L 0.050 0.010 DPC 07/08/2013 15:33 EPA 200.8

Arsenic, As 17.0 ug/L 0.10 0.030 DPC 07/08/2013 15:33 EPA 200.8

Barium, Ba 52.5 ug/L 0.10 0.020 DPC 07/08/2013 15:33 EPA 200.8

Beryllium, Be < 0.30 ug/L U 1.0 0.30 DAM 07/12/2013 10:52 EPA 200.7

Cadmium, Cd 0.83 ug/L 0.050 0.010 DPC 07/08/2013 15:33 EPA 200.8

Chromium, Cr 3.1 ug/L 0.20 0.040 DPC 07/08/2013 15:33 EPA 200.8

Cobalt, Co 1.38 ug/L 0.020 0.0040 DPC 07/08/2013 15:33 EPA 200.8

Copper, Cu 0.57 ug/L 0.050 0.010 DPC 07/08/2013 15:33 EPA 200.8

Lead, Pb 0.073 ug/L 0.010 0.0020 DPC 07/08/2013 15:33 EPA 200.8

Molybdenum, Mo 3090 ug/L 0.050 0.010 DPC 07/08/2013 15:33 EPA 200.8

Nickel, Ni 20.3 ug/L 0.20 0.050 DPC 07/08/2013 15:33 EPA 200.8

Selenium, Se 342 ug/L 0.50 0.20 DPC 07/08/2013 15:33 EPA 200.8

Selenite, Se+4 (Hydride) 134 ug/L 20 4.0 TLT 07/15/2013 AEP Method

Silver, Ag 0.0050 ug/L J 0.010 0.0020 DPC 07/08/2013 15:33 EPA 200.8

Thallium, Tl 1.33 ug/L 0.050 0.0020 DPC 07/08/2013 15:33 EPA 200.8

Tin, Sn < 3.0 ug/L U 10 3.0 DAM 07/12/2013 10:52 EPA 200.7

Titanium, Ti < 0.30 ug/L U 2.0 0.30 DAM 07/12/2013 10:52 EPA 200.7

Zinc, Zn 3.0 ug/L 0.50 0.10 DPC 07/08/2013 15:33 EPA 200.8

Aluminum, Al 0.0335 mg/L 0.0010 0.0003 DPC 07/08/2013 15:33 EPA 200.8

Boron, B 156 mg/L 0.020 0.0040 DAM 07/12/2013 10:52 EPA 200.7

Calcium, Ca 528 mg/L 0.020 0.0040 DAM 07/12/2013 10:52 EPA 200.7

Iron, Fe 0.030 mg/L J 0.050 0.010 DAM 07/12/2013 10:52 EPA 200.7

Magnesium, Mg 1250 mg/L 0.010 0.0020 DAM 07/12/2013 10:52 EPA 200.7

Manganese, Mn 6.71 mg/L 0.0005 0.0001 DAM 07/12/2013 10:52 EPA 200.7

Potassium, K 64.1 mg/L 0.050 0.0070 DAM 07/12/2013 10:50 EPA 200.7

Sodium, Na 835 mg/L 0.030 0.0080 DAM 07/12/2013 10:50 EPA 200.7

Strontium, Sr 6.04 mg/L 0.0010 0.0003 DAM 07/12/2013 10:50 EPA 200.7

Bromide, Br 19.9 mg/L 1.0 0.20 TJK 07/05/2013 EPA 300.1

Mountaineer Plant, 132703 Page 8 of 11
Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number: 132703-006 Date Collected: 07/02/2013 Date Received: 7/2/2013

Bioreactor Effluent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 0.47 ug/L 0.050 0.010 DPC 07/08/2013 15:38 EPA 200.8

Arsenic, As 1.50 ug/L 0.10 0.030 DPC 07/08/2013 15:38 EPA 200.8

Barium, Ba 51.3 ug/L 0.10 0.020 DPC 07/08/2013 15:38 EPA 200.8

Beryllium, Be < 0.30 ug/L U 1.0 0.30 DAM 07/12/2013 10:21 EPA 200.7

Cadmium, Cd 0.10 ug/L 0.050 0.010 DPC 07/08/2013 15:38 EPA 200.8

Chromium, Cr 7.0 ug/L 0.20 0.040 DPC 07/08/2013 15:38 EPA 200.8

Cobalt, Co 0.129 ug/L 0.020 0.0040 DPC 07/08/2013 15:38 EPA 200.8

Copper, Cu 0.97 ug/L 0.050 0.010 DPC 07/08/2013 15:38 EPA 200.8

Lead, Pb 0.113 ug/L 0.010 0.0020 DPC 07/08/2013 15:38 EPA 200.8

Mercury, Hg 39.0 ng/L 1.0 0.40 TLT 07/12/2013 EPA 1631E

Molybdenum, Mo 13.1 ug/L 0.050 0.010 DPC 07/08/2013 15:38 EPA 200.8

Nickel, Ni 2.14 ug/L 0.20 0.050 DPC 07/08/2013 15:38 EPA 200.8

Selenium, Se 3.9 ug/L 0.50 0.20 DPC 07/08/2013 15:38 EPA 200.8

Silver, Ag 0.0020 ug/L J 0.010 0.0020 DPC 07/08/2013 15:38 EPA 200.8

Thallium, Tl 0.06 ug/L 0.050 0.0020 DPC 07/08/2013 15:38 EPA 200.8

Tin, Sn < 3.0 ug/L U 10 3.0 DAM 07/12/2013 10:22 EPA 200.7

Titanium, Ti < 0.30 ug/L U 2.0 0.30 DAM 07/12/2013 10:21 EPA 200.7

Zinc, Zn 1.9 ug/L 0.50 0.10 DPC 07/08/2013 15:38 EPA 200.8

Aluminum, Al 2.89 mg/L 0.0010 0.0003 DPC 07/08/2013 15:38 EPA 200.8

Boron, B 180 mg/L 0.020 0.0040 DAM 07/12/2013 10:21 EPA 200.7

Calcium, Ca 532 mg/L 0.020 0.0040 DAM 07/12/2013 10:21 EPA 200.7

Iron, Fe 0.692 mg/L 0.050 0.010 DAM 07/12/2013 10:21 EPA 200.7

Magnesium, Mg 1340 mg/L 0.010 0.0020 DAM 07/12/2013 10:21 EPA 200.7

Manganese, Mn 5.37 mg/L 0.0005 0.0001 DAM 07/12/2013 10:21 EPA 200.7

Potassium, K 72.2 mg/L 0.050 0.0070 DAM 07/12/2013 10:20 EPA 200.7

Sodium, Na 826 mg/L 0.030 0.0080 DAM 07/12/2013 10:20 EPA 200.7

Strontium, Sr 6.00 mg/L 0.0010 0.0003 DAM 07/12/2013 10:20 EPA 200.7

Ammonia, NH3, as N 9.30 mg/L 0.050 0.020 DMM 07/03/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 11.2 mg/L 0.50 0.10 DMM 07/09/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 1.54 mg/L 0.10 0.020 DMM 07/03/2013 SM20 4500NO3 H

Total Nitrogen, N 12.7 mg/L 0.50 0.10 DMM 07/10/2013 Calculation

Total Organic Nitrogen, TON 1.9 mg/L 0.50 0.10 DMM 07/10/2013 Calculation

Mountaineer Plant, 132703 Page 9 of 11
Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number: 132703-006A Date Collected: 07/02/2013 Date Received: 7/2/2013

Bioreactor Effluent Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 0.44 ug/L 0.050 0.010 DPC 07/08/2013 15:43 EPA 200.8

Arsenic, As 1.50 ug/L 0.10 0.030 DPC 07/08/2013 15:43 EPA 200.8

Barium, Ba 49.2 ug/L 0.10 0.020 DPC 07/08/2013 15:43 EPA 200.8

Beryllium, Be < 0.30 ug/L U 1.0 0.30 DAM 07/12/2013 10:55 EPA 200.7

Cadmium, Cd 0.023 ug/L J 0.050 0.010 DPC 07/08/2013 15:43 EPA 200.8

Chromium, Cr 6.2 ug/L 0.20 0.040 DPC 07/08/2013 15:43 EPA 200.8

Cobalt, Co 0.102 ug/L 0.020 0.0040 DPC 07/08/2013 15:43 EPA 200.8

Copper, Cu 0.31 ug/L 0.050 0.010 DPC 07/08/2013 15:43 EPA 200.8

Lead, Pb 0.030 ug/L 0.010 0.0020 DPC 07/08/2013 15:43 EPA 200.8

Molybdenum, Mo 10.9 ug/L 0.050 0.010 DPC 07/08/2013 15:43 EPA 200.8

Nickel, Ni 1.96 ug/L 0.20 0.050 DPC 07/08/2013 15:43 EPA 200.8

Selenium, Se 2.8 ug/L 0.50 0.20 DPC 07/08/2013 15:43 EPA 200.8

Selenite, Se+4 (Hydride) < 0.080 ug/L U 0.40 0.080 TLT 07/15/2013 AEP Method

Silver, Ag 0.0020 ug/L J 0.010 0.0020 DPC 07/08/2013 15:43 EPA 200.8

Thallium, Tl 0.037 ug/L J 0.050 0.0020 DPC 07/08/2013 15:43 EPA 200.8

Tin, Sn < 3.0 ug/L U 10 3.0 DAM 07/12/2013 10:56 EPA 200.7

Titanium, Ti 0.81 ug/L J 2.0 0.30 DAM 07/12/2013 10:55 EPA 200.7

Zinc, Zn 1.3 ug/L 0.50 0.10 DPC 07/08/2013 15:43 EPA 200.8

Aluminum, Al 2.88 mg/L 0.0010 0.0003 DPC 07/08/2013 15:43 EPA 200.8

Boron, B 177 mg/L 0.020 0.0040 DAM 07/12/2013 10:55 EPA 200.7

Calcium, Ca 532 mg/L 0.020 0.0040 DAM 07/12/2013 10:55 EPA 200.7

Iron, Fe 0.614 mg/L 0.050 0.010 DAM 07/12/2013 10:55 EPA 200.7

Magnesium, Mg 1330 mg/L 0.010 0.0020 DAM 07/12/2013 10:55 EPA 200.7

Manganese, Mn 5.34 mg/L 0.0005 0.0001 DAM 07/12/2013 10:55 EPA 200.7

Potassium, K 70.4 mg/L 0.050 0.0070 DAM 07/12/2013 10:54 EPA 200.7

Sodium, Na 804 mg/L 0.030 0.0080 DAM 07/12/2013 10:54 EPA 200.7

Strontium, Sr 5.89 mg/L 0.0010 0.0003 DAM 07/12/2013 10:54 EPA 200.7

Bromide, Br 19.0 mg/L 1.0 0.20 TJK 07/05/2013 EPA 300.1

Sample Number: 132703-007 Date Collected: 07/02/2013 Date Received: 7/2/2013

Field Blank 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Mercury, Hg < 0.20 ng/L U 0.50 0.20 TLT 07/12/2013 EPA 1631E

Mountaineer Plant, 132703 Page 10 of 11
Location: Mountaineer Plant Report Date: 9/9/2013

THIS TEST REPORT RELATES ONLY TO THE ITEMS TESTED AND SHALL NOT BE REPRODUCED EXCEPT IN FULL WITHOUT WRITTEN 

APPROVAL OF THE LABORATORY. ALL TEST RESULTS MEET ALL OF THE REQUIREMENTS OF THE ACCREDITING AUTHORITY, 

UNLESS OTHERWISE NOTED.

U: Analyte was analyzed and not detected at or above adjusted Method Detection Limit

J: Analyte was positively identified, though the quantitation was below Reporting Limit.

This report has been reissued with a corrected bromide result for the Bioreactor Effluent. The original result had a 

dilution factor of 10 that was not applied.

Brian Snyder, Chemist II

Email bssnyder@aep.com Tel. 614-836-4224

Fax 614-836-4168 Audinet 210-4224

Mountaineer Plant, 132703 Page 11 of 11