Dolan Chemical Laboratory 4001 Bixby Road Groveport, OH 43125 T: 614-836-4221, Audinet 210-4221 F: 614-836-4168, Audinet 210-4168 http://aepenv/labs 

### Water Analysis Form REP-703 Rev. 0, 4/2012



### Location: Mountaineer Plant **Reissued**ReportDate:9/9/2013

Sample Number:132703-001Date Collected:07/02/2013Date Received:7/2/2013 

### CPS Influent

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 30.1 0.050 DPC EPA 200.8 0.010 07/08/2013 14:45 ug/L Arsenic, As 123 0.10 DPC EPA 200.8 0.030 07/08/2013 14:45 ug/L Barium, Ba 208 0.10 DPC EPA 200.8 0.020 07/08/2013 14:45 ug/L Beryllium, Be < 0.30 1.0 DAM EPA 200.7 0.30 07/12/2013 09:38 U ug/L Cadmium, Cd 214 0.050 DPC EPA 200.8 0.010 07/08/2013 14:45 ug/L Chromium, Cr 752 0.20 DPC EPA 200.8 0.040 07/08/2013 14:45 ug/L Cobalt, Co 201 0.020 DPC EPA 200.8 0.0040 07/08/2013 14:45 ug/L Copper, Cu 460 0.050 DPC EPA 200.8 0.010 07/08/2013 14:45 ug/L Lead, Pb 234 0.010 DPC EPA 200.8 0.0020 07/08/2013 14:45 ng/L Mercury, Hg 256000 5000 TLT EPA 1631E 2000 07/12/2013 ug/L Molybdenum, Mo 613 0.050 DPC EPA 200.8 0.010 07/08/2013 14:45 ug/L Nickel, Ni 1610 0.20 DPC EPA 200.8 0.050 07/08/2013 14:45 ug/L Selenium, Se 1200 0.50 DPC EPA 200.8 0.20 07/08/2013 14:45 ug/L Silver, Ag 0.480 0.010 DPC EPA 200.8 0.0020 07/08/2013 14:45 ug/L Thallium, Tl 10.7 0.050 DPC EPA 200.8 0.0020 07/08/2013 14:45 ug/L Tin, Sn < 3.0 10 DAM EPA 200.7 3.0 07/12/2013 09:38 U ug/L Titanium, Ti 217 2.0 DAM EPA 200.7 0.30 07/12/2013 09:38 ug/L Zinc, Zn 3400 0.50 DPC EPA 200.8 0.10 07/08/2013 14:45 mg/L Aluminum, Al 20.6 0.0010DPC EPA 200.8 0.0003 07/08/2013 14:45 mg/L Boron, B 461 0.020 DAM EPA 200.7 0.0040 07/12/2013 09:38 mg/L Calcium, Ca 1800 0.020DAM EPA 200.7 0.0040 07/12/2013 09:38 mg/L Iron, Fe 174 0.050 DAM EPA 200.7 0.010 07/12/2013 09:38 mg/L Magnesium, Mg 4180 0.010 DAM EPA 200.7 0.0020 07/12/2013 09:38 mg/L Manganese, Mn 36.4 0.0005DAM EPA 200.7 0.0001 07/12/2013 09:38 mg/L Potassium, K 75.3 0.050 DAM EPA 200.7 0.0070 07/12/2013 09:37 mg/L Sodium, Na 375 0.030 DAM EPA 200.7 0.0080 07/12/2013 09:37 mg/L Strontium, Sr 15.4 0.0010DAM EPA 200.7 0.0003 07/12/2013 09:37 mg/L Ammonia, NH3, as N 2.26 0.050DMM EPA 350.1 0.020 07/03/2013 mg/L Total Kjeldahl Nitrogen, TKN as N4.49 0.50 DMM EPA 351.2 0.10 07/09/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N68.1 0.10 DMM SM20 4500NO3 H 0.020 07/03/2013 mg/L Total Nitrogen, N 72.6 0.50 DMM Calculation 0.10 07/10/2013 mg/L Total Organic Nitrogen, TON2.2 0.50 DMM Calculation 0.10 07/10/2013

Mountaineer Plant, 132703 Page 1 of 11

### Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number:132703-001ADate Collected:07/02/2013Date Received:7/2/2013 

### CPS Influent Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 3.53 0.050 DPC EPA 200.8 0.010 07/08/2013 14:50 ug/L Arsenic, As 2.73 0.10 DPC EPA 200.8 0.030 07/08/2013 14:50 ug/L Barium, Ba 90.1 0.10 DPC EPA 200.8 0.020 07/08/2013 14:50 ug/L Beryllium, Be < 0.30 1.0 DAM EPA 200.7 0.30 07/12/2013 10:25 U ug/L Cadmium, Cd 148 0.050 DPC EPA 200.8 0.010 07/08/2013 14:50 ug/L Chromium, Cr 1.1 0.20 DPC EPA 200.8 0.040 07/08/2013 14:50 ug/L Cobalt, Co 133 0.020 DPC EPA 200.8 0.0040 07/08/2013 14:50 ug/L Copper, Cu 6.44 0.050 DPC EPA 200.8 0.010 07/08/2013 14:50 ug/L Lead, Pb 0.315 0.010 DPC EPA 200.8 0.0020 07/08/2013 14:50 ug/L Molybdenum, Mo 463 0.050 DPC EPA 200.8 0.010 07/08/2013 14:50 ug/L Nickel, Ni 1170 0.20 DPC EPA 200.8 0.050 07/08/2013 14:50 ug/L Selenium, Se 738 0.50 DPC EPA 200.8 0.20 07/08/2013 14:50 ug/L Selenite, Se+4 (Hydride) 183 20 TLT AEP Method 4.0 07/15/2013 ug/L Silver, Ag 0.0080 0.010 DPC EPA 200.8 0.0020 07/08/2013 14:50 J ug/L Thallium, Tl 7.83 0.050 DPC EPA 200.8 0.0020 07/08/2013 14:50 ug/L Tin, Sn < 3.0 10 DAM EPA 200.7 3.0 07/12/2013 10:25 U ug/L Titanium, Ti < 0.30 2.0 DAM EPA 200.7 0.30 07/12/2013 10:25 U ug/L Zinc, Zn 614 0.50 DPC EPA 200.8 0.10 07/08/2013 14:50 mg/L Aluminum, Al 0.0561 0.0010DPC EPA 200.8 0.0003 07/08/2013 14:50 mg/L Boron, B 460 0.020 DAM EPA 200.7 0.0040 07/12/2013 10:25 mg/L Calcium, Ca 855 0.020 DAM EPA 200.7 0.0040 07/12/2013 10:25 mg/L Iron, Fe < 0.010 0.050 DAM EPA 200.7 0.010 07/12/2013 10:25 U mg/L Magnesium, Mg 3860 0.010 DAM EPA 200.7 0.0020 07/12/2013 10:25 mg/L Manganese, Mn 31.4 0.0005DAM EPA 200.7 0.0001 07/12/2013 10:25 mg/L Potassium, K 70.3 0.050 DAM EPA 200.7 0.0070 07/12/2013 10:23 mg/L Sodium, Na 372 0.030DAM EPA 200.7 0.0080 07/12/2013 10:23 mg/L Strontium, Sr 12.3 0.0010DAM EPA 200.7 0.0003 07/12/2013 10:23 mg/L Bromide, Br 42.3 1.0 TJK EPA 300.1 0.20 07/05/2013



### Sample Number:132703-002Date Collected:07/02/2013Date Received:7/2/2013 

### CPS Primary Clarifier Effluent

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ng/L Mercury, Hg 664 50 TLT EPA 1631E 20 07/12/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N49.0 0.10 DMM SM20 4500NO3 H 0.020 07/03/2013

Mountaineer Plant, 132703 Page 2 of 11

### Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number:132703-003Date Collected:07/02/2013Date Received:7/2/2013 

### CPS Effluent

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 1.86 0.050 DPC EPA 200.8 0.010 07/08/2013 14:55 ug/L Arsenic, As 2.09 0.10 DPC EPA 200.8 0.030 07/08/2013 14:55 ug/L Barium, Ba 76.0 0.10 DPC EPA 200.8 0.020 07/08/2013 14:55 ug/L Beryllium, Be < 0.30 1.0 DAM EPA 200.7 0.30 07/12/2013 09:42 U ug/L Cadmium, Cd 0.18 0.050 DPC EPA 200.8 0.010 07/08/2013 14:55 ug/L Chromium, Cr 4.4 0.20 DPC EPA 200.8 0.040 07/08/2013 14:55 ug/L Cobalt, Co 0.761 0.020 DPC EPA 200.8 0.0040 07/08/2013 14:55 ug/L Copper, Cu 0.88 0.050 DPC EPA 200.8 0.010 07/08/2013 14:55 ug/L Lead, Pb 0.132 0.010 DPC EPA 200.8 0.0020 07/08/2013 14:55 ng/L Mercury, Hg 107 50 TLT EPA 1631E 20 07/12/2013 ug/L Molybdenum, Mo 326 0.050 DPC EPA 200.8 0.010 07/08/2013 14:55 ug/L Nickel, Ni 27.5 0.20 DPC EPA 200.8 0.050 07/08/2013 14:55 ug/L Selenium, Se 404 0.50 DPC EPA 200.8 0.20 07/08/2013 14:55 ug/L Silver, Ag 0.0020 0.010 DPC EPA 200.8 0.0020 07/08/2013 14:55 J ug/L Thallium, Tl 0.62 0.050 DPC EPA 200.8 0.0020 07/08/2013 14:55 ug/L Tin, Sn < 3.0 10 DAM EPA 200.7 3.0 07/12/2013 09:42 U ug/L Titanium, Ti < 0.30 2.0 DAM EPA 200.7 0.30 07/12/2013 09:42 U ug/L Zinc, Zn 3.8 0.50 DPC EPA 200.8 0.10 07/08/2013 14:55 mg/L Aluminum, Al 0.107 0.0010DPC EPA 200.8 0.0003 07/08/2013 14:55 mg/L Boron, B 240 0.020 DAM EPA 200.7 0.0040 07/12/2013 09:42 mg/L Calcium, Ca 647 0.020 DAM EPA 200.7 0.0040 07/12/2013 09:42 mg/L Iron, Fe 0.931 0.050 DAM EPA 200.7 0.010 07/12/2013 09:42 mg/L Magnesium, Mg 2000 0.010 DAM EPA 200.7 0.0020 07/12/2013 09:42 mg/L Manganese, Mn 11.1 0.0005DAM EPA 200.7 0.0001 07/12/2013 09:42 mg/L Potassium, K 38.2 0.050 DAM EPA 200.7 0.0070 07/12/2013 09:40 mg/L Sodium, Na 210 0.030DAM EPA 200.7 0.0080 07/12/2013 09:40 mg/L Strontium, Sr 6.73 0.0010DAM EPA 200.7 0.0003 07/12/2013 09:40 mg/L Ammonia, NH3, as N 1.16 0.050DMM EPA 350.1 0.020 07/03/2013 mg/L Total Kjeldahl Nitrogen, TKN as N3.79 0.50 DMM EPA 351.2 0.10 07/09/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N37.9 0.10 DMM SM20 4500NO3 H 0.020 07/03/2013 mg/L Total Nitrogen, N 41.7 0.50 DMM Calculation 0.10 07/10/2013 mg/L Total Organic Nitrogen, TON2.6 0.50 DMM Calculation 0.10 07/10/2013

Mountaineer Plant, 132703 Page 3 of 11

### Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number:132703-003ADate Collected:07/02/2013Date Received:7/2/2013 

### CPS Effluent Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 1.75 0.050 DPC EPA 200.8 0.010 07/08/2013 15:14 ug/L Arsenic, As 1.83 0.10 DPC EPA 200.8 0.030 07/08/2013 15:14 ug/L Barium, Ba 70.2 0.10 DPC EPA 200.8 0.020 07/08/2013 15:14 ug/L Beryllium, Be < 0.30 1.0 DAM EPA 200.7 0.30 07/12/2013 10:29 U ug/L Cadmium, Cd 0.10 0.050 DPC EPA 200.8 0.010 07/08/2013 15:14 ug/L Chromium, Cr 3.3 0.20 DPC EPA 200.8 0.040 07/08/2013 15:14 ug/L Cobalt, Co 0.247 0.020 DPC EPA 200.8 0.0040 07/08/2013 15:14 ug/L Copper, Cu 0.24 0.050 DPC EPA 200.8 0.010 07/08/2013 15:14 ug/L Lead, Pb 0.042 0.010 DPC EPA 200.8 0.0020 07/08/2013 15:14 ug/L Molybdenum, Mo 310 0.050 DPC EPA 200.8 0.010 07/08/2013 15:14 ug/L Nickel, Ni 12.9 0.20 DPC EPA 200.8 0.050 07/08/2013 15:14 ug/L Selenium, Se 379 0.50 DPC EPA 200.8 0.20 07/08/2013 15:14 ug/L Selenite, Se+4 (Hydride) 145 20 TLT AEP Method 4.0 07/15/2013 ug/L Silver, Ag 0.0030 0.010 DPC EPA 200.8 0.0020 07/08/2013 15:14 J ug/L Thallium, Tl 0.40 0.050 DPC EPA 200.8 0.0020 07/08/2013 15:14 ug/L Tin, Sn < 3.0 10 DAM EPA 200.7 3.0 07/12/2013 10:29 U ug/L Titanium, Ti < 0.30 2.0 DAM EPA 200.7 0.30 07/12/2013 10:29 U ug/L Zinc, Zn 1.3 0.50 DPC EPA 200.8 0.10 07/08/2013 15:14 mg/L Aluminum, Al 0.0187 0.0010DPC EPA 200.8 0.0003 07/08/2013 15:14 mg/L Boron, B 239 0.020 DAM EPA 200.7 0.0040 07/12/2013 10:29 mg/L Calcium, Ca 646 0.020 DAM EPA 200.7 0.0040 07/12/2013 10:29 mg/L Iron, Fe < 0.010 0.050 DAM EPA 200.7 0.010 07/12/2013 10:29 U mg/L Magnesium, Mg 2000 0.010 DAM EPA 200.7 0.0020 07/12/2013 10:29 mg/L Manganese, Mn 10.9 0.0005DAM EPA 200.7 0.0001 07/12/2013 10:29 mg/L Potassium, K 37.9 0.050 DAM EPA 200.7 0.0070 07/12/2013 10:27 mg/L Sodium, Na 209 0.030DAM EPA 200.7 0.0080 07/12/2013 10:27 mg/L Strontium, Sr 6.73 0.0010DAM EPA 200.7 0.0003 07/12/2013 10:27 mg/L Bromide, Br 24.7 1.0 TJK EPA 300.1 0.20 07/05/2013

Mountaineer Plant, 132703 Page 4 of 11

### Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number:132703-004Date Collected:07/02/2013Date Received:7/2/2013 

### Landfill Leachate Effluent

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 10.6 0.050 DPC EPA 200.8 0.010 07/08/2013 15:19 ug/L Arsenic, As 37.1 0.10 DPC EPA 200.8 0.030 07/08/2013 15:19 ug/L Barium, Ba 29.7 0.10 DPC EPA 200.8 0.020 07/08/2013 15:19 ug/L Beryllium, Be < 0.30 1.0 DAM EPA 200.7 0.30 07/12/2013 09:50 U ug/L Cadmium, Cd 1.64 0.050 DPC EPA 200.8 0.010 07/08/2013 15:19 ug/L Chromium, Cr 2.5 0.20 DPC EPA 200.8 0.040 07/08/2013 15:19 ug/L Cobalt, Co 3.15 0.020 DPC EPA 200.8 0.0040 07/08/2013 15:19 ug/L Copper, Cu 0.60 0.050 DPC EPA 200.8 0.010 07/08/2013 15:19 ug/L Lead, Pb 0.072 0.010 DPC EPA 200.8 0.0020 07/08/2013 15:19 ng/L Mercury, Hg 82.3 50 TLT EPA 1631E 20 07/12/2013 ug/L Molybdenum, Mo 6470 0.050 DPC EPA 200.8 0.010 07/08/2013 15:19 ug/L Nickel, Ni 23.7 0.20 DPC EPA 200.8 0.050 07/08/2013 15:19 ug/L Selenium, Se 228 0.50 DPC EPA 200.8 0.20 07/08/2013 15:19 ug/L Silver, Ag < 0.0020 0.010 DPC EPA 200.8 0.0020 07/08/2013 15:19 U ug/L Thallium, Tl 2.80 0.050 DPC EPA 200.8 0.0020 07/08/2013 15:19 ug/L Tin, Sn < 3.0 10 DAM EPA 200.7 3.0 07/12/2013 09:51 U ug/L Titanium, Ti < 0.30 2.0 DAM EPA 200.7 0.30 07/12/2013 09:50 U ug/L Zinc, Zn 2.4 0.50 DPC EPA 200.8 0.10 07/08/2013 15:19 mg/L Aluminum, Al 0.0360 0.0010DPC EPA 200.8 0.0003 07/08/2013 15:19 mg/L Boron, B 60.7 0.020 DAM EPA 200.7 0.0040 07/12/2013 09:50 mg/L Calcium, Ca 419 0.020 DAM EPA 200.7 0.0040 07/12/2013 09:50 mg/L Iron, Fe 0.090 0.050 DAM EPA 200.7 0.010 07/12/2013 09:51 mg/L Magnesium, Mg 459 0.010 DAM EPA 200.7 0.0020 07/12/2013 09:50 mg/L Manganese, Mn 1.79 0.0005DAM EPA 200.7 0.0001 07/12/2013 09:50 mg/L Potassium, K 94.3 0.050 DAM EPA 200.7 0.0070 07/12/2013 09:49 mg/L Sodium, Na 1590 0.030DAM EPA 200.7 0.0080 07/12/2013 09:49 mg/L Strontium, Sr 5.34 0.0010DAM EPA 200.7 0.0003 07/12/2013 09:49 mg/L Ammonia, NH3, as N 1.48 0.050DMM EPA 350.1 0.020 07/03/2013 mg/L Total Kjeldahl Nitrogen, TKN as N2.44 0.50 DMM EPA 351.2 0.10 07/09/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N6.54 0.10 DMM SM20 4500NO3 H 0.020 07/03/2013 mg/L Total Nitrogen, N 8.98 0.50 DMM Calculation 0.10 07/10/2013 mg/L Total Organic Nitrogen, TON1.0 0.50 DMM Calculation 0.10 07/10/2013

Mountaineer Plant, 132703 Page 5 of 11

### Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number:132703-004ADate Collected:07/02/2013Date Received:7/2/2013 

### Landfill Leachate Effluent Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 9.57 0.050 DPC EPA 200.8 0.010 07/08/2013 15:23 ug/L Arsenic, As 30.9 0.10 DPC EPA 200.8 0.030 07/08/2013 15:23 ug/L Barium, Ba 26.6 0.10 DPC EPA 200.8 0.020 07/08/2013 15:23 ug/L Beryllium, Be < 0.30 1.0 DAM EPA 200.7 0.30 07/12/2013 10:37 U ug/L Cadmium, Cd 1.31 0.050 DPC EPA 200.8 0.010 07/08/2013 15:23 ug/L Chromium, Cr 1.6 0.20 DPC EPA 200.8 0.040 07/08/2013 15:23 ug/L Cobalt, Co 2.52 0.020 DPC EPA 200.8 0.0040 07/08/2013 15:23 ug/L Copper, Cu 0.38 0.050 DPC EPA 200.8 0.010 07/08/2013 15:23 ug/L Lead, Pb 0.029 0.010 DPC EPA 200.8 0.0020 07/08/2013 15:23 ug/L Molybdenum, Mo 5820 0.050 DPC EPA 200.8 0.010 07/08/2013 15:23 ug/L Nickel, Ni 21.1 0.20 DPC EPA 200.8 0.050 07/08/2013 15:23 ug/L Selenium, Se 180 0.50 DPC EPA 200.8 0.20 07/08/2013 15:23 ug/L Selenite, Se+4 (Hydride) 86.6 20 TLT AEP Method 4.0 07/15/2013 ug/L Silver, Ag < 0.0020 0.010 DPC EPA 200.8 0.0020 07/08/2013 15:23 U ug/L Thallium, Tl 2.38 0.050 DPC EPA 200.8 0.0020 07/08/2013 15:23 ug/L Tin, Sn < 3.0 10 DAM EPA 200.7 3.0 07/12/2013 10:38 U ug/L Titanium, Ti < 0.30 2.0 DAM EPA 200.7 0.30 07/12/2013 10:37 U ug/L Zinc, Zn 2.7 0.50 DPC EPA 200.8 0.10 07/08/2013 15:23 mg/L Aluminum, Al 0.0295 0.0010DPC EPA 200.8 0.0003 07/08/2013 15:23 mg/L Boron, B 60.7 0.020 DAM EPA 200.7 0.0040 07/12/2013 10:37 mg/L Calcium, Ca 419 0.020 DAM EPA 200.7 0.0040 07/12/2013 10:37 mg/L Iron, Fe < 0.010 0.050 DAM EPA 200.7 0.010 07/12/2013 10:38 U mg/L Magnesium, Mg 457 0.010 DAM EPA 200.7 0.0020 07/12/2013 10:37 mg/L Manganese, Mn 1.72 0.0005DAM EPA 200.7 0.0001 07/12/2013 10:37 mg/L Potassium, K 94.2 0.050 DAM EPA 200.7 0.0070 07/12/2013 10:36 mg/L Sodium, Na 1590 0.030DAM EPA 200.7 0.0080 07/12/2013 10:36 mg/L Strontium, Sr 5.29 0.0010DAM EPA 200.7 0.0003 07/12/2013 10:36 mg/L Bromide, Br 11.3 1.0 TJK EPA 300.1 0.20 07/05/2013

Mountaineer Plant, 132703 Page 6 of 11

### Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number:132703-005Date Collected:07/02/2013Date Received:7/2/2013 

### 1st Stage Feed

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 6.01 0.050 DPC EPA 200.8 0.010 07/08/2013 15:28 ug/L Arsenic, As 19.0 0.10 DPC EPA 200.8 0.030 07/08/2013 15:28 ug/L Barium, Ba 52.5 0.10 DPC EPA 200.8 0.020 07/08/2013 15:28 ug/L Beryllium, Be < 0.30 1.0 DAM EPA 200.7 0.30 07/12/2013 09:54 U ug/L Cadmium, Cd 1.03 0.050 DPC EPA 200.8 0.010 07/08/2013 15:28 ug/L Chromium, Cr 3.8 0.20 DPC EPA 200.8 0.040 07/08/2013 15:28 ug/L Cobalt, Co 2.02 0.020 DPC EPA 200.8 0.0040 07/08/2013 15:28 ug/L Copper, Cu 0.83 0.050 DPC EPA 200.8 0.010 07/08/2013 15:28 ug/L Lead, Pb 0.129 0.010 DPC EPA 200.8 0.0020 07/08/2013 15:28 ng/L Mercury, Hg 140 250 TLT EPA 1631E 100 07/12/2013 J ug/L Molybdenum, Mo 3110 0.050 DPC EPA 200.8 0.010 07/08/2013 15:28 ug/L Nickel, Ni 28.6 0.20 DPC EPA 200.8 0.050 07/08/2013 15:28 ug/L Selenium, Se 342 0.50 DPC EPA 200.8 0.20 07/08/2013 15:28 ug/L Silver, Ag 0.0030 0.010 DPC EPA 200.8 0.0020 07/08/2013 15:28 J ug/L Thallium, Tl 1.45 0.050 DPC EPA 200.8 0.0020 07/08/2013 15:28 ug/L Tin, Sn < 3.0 10 DAM EPA 200.7 3.0 07/12/2013 09:54 U ug/L Titanium, Ti < 0.30 2.0 DAM EPA 200.7 0.30 07/12/2013 09:54 U ug/L Zinc, Zn 3.7 0.50 DPC EPA 200.8 0.10 07/08/2013 15:28 mg/L Aluminum, Al 0.0686 0.0010DPC EPA 200.8 0.0003 07/08/2013 15:28 mg/L Boron, B 157 0.020 DAM EPA 200.7 0.0040 07/12/2013 09:54 mg/L Calcium, Ca 528 0.020 DAM EPA 200.7 0.0040 07/12/2013 09:54 mg/L Iron, Fe 0.564 0.050 DAM EPA 200.7 0.010 07/12/2013 09:54 mg/L Magnesium, Mg 1260 0.010 DAM EPA 200.7 0.0020 07/12/2013 09:54 mg/L Manganese, Mn 6.70 0.0005DAM EPA 200.7 0.0001 07/12/2013 09:54 mg/L Potassium, K 64.2 0.050 DAM EPA 200.7 0.0070 07/12/2013 09:52 mg/L Sodium, Na 835 0.030DAM EPA 200.7 0.0080 07/12/2013 09:52 mg/L Strontium, Sr 6.07 0.0010DAM EPA 200.7 0.0003 07/12/2013 09:52 mg/L Ammonia, NH3, as N 1.30 0.050DMM EPA 350.1 0.020 07/03/2013 mg/L Total Kjeldahl Nitrogen, TKN as N2.68 0.50 DMM EPA 351.2 0.10 07/09/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N22.4 0.10 DMM SM20 4500NO3 H 0.020 07/03/2013 mg/L Total Nitrogen, N 25.1 0.50 DMM Calculation 0.10 07/10/2013 mg/L Total Organic Nitrogen, TON1.4 0.50 DMM Calculation 0.10 07/10/2013

Mountaineer Plant, 132703 Page 7 of 11

### Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number:132703-005ADate Collected:07/02/2013Date Received:7/2/2013 

### 1st Stage Feed Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 6.00 0.050 DPC EPA 200.8 0.010 07/08/2013 15:33 ug/L Arsenic, As 17.0 0.10 DPC EPA 200.8 0.030 07/08/2013 15:33 ug/L Barium, Ba 52.5 0.10 DPC EPA 200.8 0.020 07/08/2013 15:33 ug/L Beryllium, Be < 0.30 1.0 DAM EPA 200.7 0.30 07/12/2013 10:52 U ug/L Cadmium, Cd 0.83 0.050 DPC EPA 200.8 0.010 07/08/2013 15:33 ug/L Chromium, Cr 3.1 0.20 DPC EPA 200.8 0.040 07/08/2013 15:33 ug/L Cobalt, Co 1.38 0.020 DPC EPA 200.8 0.0040 07/08/2013 15:33 ug/L Copper, Cu 0.57 0.050 DPC EPA 200.8 0.010 07/08/2013 15:33 ug/L Lead, Pb 0.073 0.010 DPC EPA 200.8 0.0020 07/08/2013 15:33 ug/L Molybdenum, Mo 3090 0.050 DPC EPA 200.8 0.010 07/08/2013 15:33 ug/L Nickel, Ni 20.3 0.20 DPC EPA 200.8 0.050 07/08/2013 15:33 ug/L Selenium, Se 342 0.50 DPC EPA 200.8 0.20 07/08/2013 15:33 ug/L Selenite, Se+4 (Hydride) 134 20 TLT AEP Method 4.0 07/15/2013 ug/L Silver, Ag 0.0050 0.010 DPC EPA 200.8 0.0020 07/08/2013 15:33 J ug/L Thallium, Tl 1.33 0.050 DPC EPA 200.8 0.0020 07/08/2013 15:33 ug/L Tin, Sn < 3.0 10 DAM EPA 200.7 3.0 07/12/2013 10:52 U ug/L Titanium, Ti < 0.30 2.0 DAM EPA 200.7 0.30 07/12/2013 10:52 U ug/L Zinc, Zn 3.0 0.50 DPC EPA 200.8 0.10 07/08/2013 15:33 mg/L Aluminum, Al 0.0335 0.0010DPC EPA 200.8 0.0003 07/08/2013 15:33 mg/L Boron, B 156 0.020 DAM EPA 200.7 0.0040 07/12/2013 10:52 mg/L Calcium, Ca 528 0.020 DAM EPA 200.7 0.0040 07/12/2013 10:52 mg/L Iron, Fe 0.030 0.050 DAM EPA 200.7 0.010 07/12/2013 10:52 J mg/L Magnesium, Mg 1250 0.010 DAM EPA 200.7 0.0020 07/12/2013 10:52 mg/L Manganese, Mn 6.71 0.0005DAM EPA 200.7 0.0001 07/12/2013 10:52 mg/L Potassium, K 64.1 0.050 DAM EPA 200.7 0.0070 07/12/2013 10:50 mg/L Sodium, Na 835 0.030DAM EPA 200.7 0.0080 07/12/2013 10:50 mg/L Strontium, Sr 6.04 0.0010DAM EPA 200.7 0.0003 07/12/2013 10:50 mg/L Bromide, Br 19.9 1.0 TJK EPA 300.1 0.20 07/05/2013

Mountaineer Plant, 132703 Page 8 of 11

### Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number:132703-006Date Collected:07/02/2013Date Received:7/2/2013 

### Bioreactor Effluent

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 0.47 0.050 DPC EPA 200.8 0.010 07/08/2013 15:38 ug/L Arsenic, As 1.50 0.10 DPC EPA 200.8 0.030 07/08/2013 15:38 ug/L Barium, Ba 51.3 0.10 DPC EPA 200.8 0.020 07/08/2013 15:38 ug/L Beryllium, Be < 0.30 1.0 DAM EPA 200.7 0.30 07/12/2013 10:21 U ug/L Cadmium, Cd 0.10 0.050 DPC EPA 200.8 0.010 07/08/2013 15:38 ug/L Chromium, Cr 7.0 0.20 DPC EPA 200.8 0.040 07/08/2013 15:38 ug/L Cobalt, Co 0.129 0.020 DPC EPA 200.8 0.0040 07/08/2013 15:38 ug/L Copper, Cu 0.97 0.050 DPC EPA 200.8 0.010 07/08/2013 15:38 ug/L Lead, Pb 0.113 0.010 DPC EPA 200.8 0.0020 07/08/2013 15:38 ng/L Mercury, Hg 39.0 1.0 TLT EPA 1631E 0.40 07/12/2013 ug/L Molybdenum, Mo 13.1 0.050 DPC EPA 200.8 0.010 07/08/2013 15:38 ug/L Nickel, Ni 2.14 0.20 DPC EPA 200.8 0.050 07/08/2013 15:38 ug/L Selenium, Se 3.9 0.50 DPC EPA 200.8 0.20 07/08/2013 15:38 ug/L Silver, Ag 0.0020 0.010 DPC EPA 200.8 0.0020 07/08/2013 15:38 J ug/L Thallium, Tl 0.06 0.050 DPC EPA 200.8 0.0020 07/08/2013 15:38 ug/L Tin, Sn < 3.0 10 DAM EPA 200.7 3.0 07/12/2013 10:22 U ug/L Titanium, Ti < 0.30 2.0 DAM EPA 200.7 0.30 07/12/2013 10:21 U ug/L Zinc, Zn 1.9 0.50 DPC EPA 200.8 0.10 07/08/2013 15:38 mg/L Aluminum, Al 2.89 0.0010DPC EPA 200.8 0.0003 07/08/2013 15:38 mg/L Boron, B 180 0.020 DAM EPA 200.7 0.0040 07/12/2013 10:21 mg/L Calcium, Ca 532 0.020 DAM EPA 200.7 0.0040 07/12/2013 10:21 mg/L Iron, Fe 0.692 0.050 DAM EPA 200.7 0.010 07/12/2013 10:21 mg/L Magnesium, Mg 1340 0.010 DAM EPA 200.7 0.0020 07/12/2013 10:21 mg/L Manganese, Mn 5.37 0.0005DAM EPA 200.7 0.0001 07/12/2013 10:21 mg/L Potassium, K 72.2 0.050 DAM EPA 200.7 0.0070 07/12/2013 10:20 mg/L Sodium, Na 826 0.030DAM EPA 200.7 0.0080 07/12/2013 10:20 mg/L Strontium, Sr 6.00 0.0010DAM EPA 200.7 0.0003 07/12/2013 10:20 mg/L Ammonia, NH3, as N 9.30 0.050DMM EPA 350.1 0.020 07/03/2013 mg/L Total Kjeldahl Nitrogen, TKN as N11.2 0.50 DMM EPA 351.2 0.10 07/09/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N1.54 0.10 DMM SM20 4500NO3 H 0.020 07/03/2013 mg/L Total Nitrogen, N 12.7 0.50 DMM Calculation 0.10 07/10/2013 mg/L Total Organic Nitrogen, TON1.9 0.50 DMM Calculation 0.10 07/10/2013

Mountaineer Plant, 132703 Page 9 of 11

### Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number:132703-006ADate Collected:07/02/2013Date Received:7/2/2013 

### Bioreactor Effluent Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 0.44 0.050 DPC EPA 200.8 0.010 07/08/2013 15:43 ug/L Arsenic, As 1.50 0.10 DPC EPA 200.8 0.030 07/08/2013 15:43 ug/L Barium, Ba 49.2 0.10 DPC EPA 200.8 0.020 07/08/2013 15:43 ug/L Beryllium, Be < 0.30 1.0 DAM EPA 200.7 0.30 07/12/2013 10:55 U ug/L Cadmium, Cd 0.023 0.050 DPC EPA 200.8 0.010 07/08/2013 15:43 J ug/L Chromium, Cr 6.2 0.20 DPC EPA 200.8 0.040 07/08/2013 15:43 ug/L Cobalt, Co 0.102 0.020 DPC EPA 200.8 0.0040 07/08/2013 15:43 ug/L Copper, Cu 0.31 0.050 DPC EPA 200.8 0.010 07/08/2013 15:43 ug/L Lead, Pb 0.030 0.010 DPC EPA 200.8 0.0020 07/08/2013 15:43 ug/L Molybdenum, Mo 10.9 0.050 DPC EPA 200.8 0.010 07/08/2013 15:43 ug/L Nickel, Ni 1.96 0.20 DPC EPA 200.8 0.050 07/08/2013 15:43 ug/L Selenium, Se 2.8 0.50 DPC EPA 200.8 0.20 07/08/2013 15:43 ug/L Selenite, Se+4 (Hydride)< 0.080 0.40 TLT AEP Method 0.080 07/15/2013 U ug/L Silver, Ag 0.0020 0.010 DPC EPA 200.8 0.0020 07/08/2013 15:43 J ug/L Thallium, Tl 0.037 0.050 DPC EPA 200.8 0.0020 07/08/2013 15:43 J ug/L Tin, Sn < 3.0 10 DAM EPA 200.7 3.0 07/12/2013 10:56 U ug/L Titanium, Ti 0.81 2.0 DAM EPA 200.7 0.30 07/12/2013 10:55 J ug/L Zinc, Zn 1.3 0.50 DPC EPA 200.8 0.10 07/08/2013 15:43 mg/L Aluminum, Al 2.88 0.0010DPC EPA 200.8 0.0003 07/08/2013 15:43 mg/L Boron, B 177 0.020 DAM EPA 200.7 0.0040 07/12/2013 10:55 mg/L Calcium, Ca 532 0.020 DAM EPA 200.7 0.0040 07/12/2013 10:55 mg/L Iron, Fe 0.614 0.050 DAM EPA 200.7 0.010 07/12/2013 10:55 mg/L Magnesium, Mg 1330 0.010 DAM EPA 200.7 0.0020 07/12/2013 10:55 mg/L Manganese, Mn 5.34 0.0005DAM EPA 200.7 0.0001 07/12/2013 10:55 mg/L Potassium, K 70.4 0.050 DAM EPA 200.7 0.0070 07/12/2013 10:54 mg/L Sodium, Na 804 0.030DAM EPA 200.7 0.0080 07/12/2013 10:54 mg/L Strontium, Sr 5.89 0.0010DAM EPA 200.7 0.0003 07/12/2013 10:54 mg/L Bromide, Br 19.0 1.0 TJK EPA 300.1 0.20 07/05/2013



### Sample Number:132703-007Date Collected:07/02/2013Date Received:7/2/2013 

### Field Blank

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ng/L Mercury, Hg < 0.20 0.50 TLT EPA 1631E 0.20 07/12/2013 U

Mountaineer Plant, 132703 Page 10 of 11

### Location: Mountaineer Plant Report Date: 9/9/2013

THIS TEST REPORT RELATES ONLY TO THE ITEMS TESTED AND SHALL NOT BE REPRODUCED EXCEPT IN FULL WITHOUT WRITTEN APPROVAL OF THE LABORATORY. ALL TEST RESULTS MEET ALL OF THE REQUIREMENTS OF THE ACCREDITING AUTHORITY, UNLESS OTHERWISE NOTED. U: Analyte was analyzed and not detected at or above adjusted Method Detection Limit J: Analyte was positively identified, though the quantitation was below Reporting Limit.

This report has been reissued with a corrected bromide result for the Bioreactor Effluent. The original result had a dilution factor of 10 that was not applied.

Brian Snyder, Chemist II Email bssnyder@aep.comTel. 614-836-4224

Fax 614-836-4168Audinet 210-4224

Mountaineer Plant, 132703 Page 11 of 11