### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell). 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

-
5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell). 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

2364 Merrimack Station 2 bitum inous 3/29/2010 3/30/2010 3/31/2010Fuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte

2364 Merrimack Station 2 As Received Higher Heating Value 2364 Merrimack Station 2 As Received % Moisture 2364 Merrimack Station 2 As Received % Ash 2364 Merrimack Station 2 As Received % Sulfur 2364 Merrimack Station 2 Dry basis Higher Heating Value 2364 Merrimack Station 2 Dry basis % Ash 2364 Merrimack Station 2 Dry basis % Sulfur 2364 Merrimack Station 2 Dry basis Antim ony 2364 Merrimack Station 2 Dry basis Arsenic 2364 Merrimack Station 2 Dry basis Beryllium 2364 Merrimack Station 2 Dry basis Cadmium 2364 Merrimack Station 2 Dry basis Chlorine 2364 Merrimack Station 2 Dry basis Chromium 2364 Merrimack Station 2 Dry basis Cobalt 2364 Merrimack Station 2 Dry basis Fluorine 2364 Merrimack Station 2 Dry basis Lead 2364 Merrimack Station 2 Dry basis Manganese 2364 Merrimack Station 2 Dry basis Mercury 2364 Merrimack Station 2 Dry basis Nickel 2364 Merrimack Station 2 Dry basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04)

ASTM D240 ASTM D482 ASTM D1552 EPA 6010Cm od EPA 6010Cm od EPA 6010Cm od EPA 6010Cm od EPA 6010Cm od EPA 6010Cm od EPA 6010Cm od EPA 6010Cm od EPA 6010Cm od EPA 6010Cm od ASTM D3684-01 EPA 6010Cm od EPA 6010Cm odEIA Facility Code Facility Name Boiler ID 2364 Merrimack Station 2

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) FM9371-01R\MK2-fuel-Run 3/29/2010 3/29/2010 FM9372-01R\MK2-fuel-Run 3/30/2010 3/30/2010 FM9372-01R\MK2-fuel-Run 3/31/2010 3/31/2010 Fuel Testing ResultsHAPs Test Group

Mercury and non-mercury

metalic HAPs

HHV Units % Moisture (as received) % A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) 13920 Btu/lb 13900 Btu/lb 13960 Btu/lb% A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony (Dry Basis) An timony

Units 7.62 1.52 0.062 μg/g <3 mg /Kg 7.7 1.56 0.057 μg/g <3 mg /Kg 7.61 1.49 0.063 μg/g <3 mg /KgArsenic (Dry

Basis) Arsenic Units Beryllium (Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) 3.4 mg/Kg <1 mg/Kg <1 mg /Kg 10.4 mg /Kg 3.26 3.92 mg/Kg <1 mg/Kg <1 mg /Kg 9.53 mg /Kg 3 4.54 mg/Kg <1 mg/Kg <1 mg /Kg 9.94 mg /Kg 3.05Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units mg/Kg 15.3 mg/Kg 6.82 mg /Kg <2 mg /Kg mg/Kg 20.5 mg/Kg 6.11 mg /Kg <2 mg /Kg mg/Kg 11.9 mg/Kg 6.53 mg /Kg <2 mg /KgCobalt (Dry

Basis) Cobalt Units 2.44 mg/Kg 2.35 mg/Kg 2.42 mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg /g petroleum coke μg/g other mg /KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm