VES 004901.pdf 
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ATTACHMENT 2 

I 

VES 004901 
VES 004902.pdf 
UNIT2 

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VES 004902 
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Waste··Feed Results 

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VES 004903 
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.Week o~ August 11, 2008 

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VES 004904 
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Ma 

A.ttentlon: Jeff Gorman 

ENSR lntw~ational 

SOl S Campuswood Dr. 

Suite 104 

SyriiCilde, NY 

USA 13057-4232 

Your Project #: 1002-022 

Site: Veoila 

Report Date: 2008/12/02 

CERTIFICATE OF ANALYSIS 

MAXXAM J OB#: A889378, A891648 & A8Al964 

R- ived: 

Sample Macrix; soild 

# Samples lleeeived: 9 

Analyses 

¥oisturc Determination 

Date 

Quantity Extracted 

9 N/A 

Date 

Analyzed 

11/20/2008 

Laboratory 

Method 

• RPD'l cakulatcd usinc 13W data. The roundin& of fioal mults may result in the apparent diffcm>ee. 

• r.Ac~~J .""r _ ,....- ,_. ... -<-< 

. 

Mike Challis 

Customer Service Manager 

Maxxam Analytics Inc. 

Burlington 

Method 

Reference 

VES 004905 
CooidonU.t Marum An•lyllca lnwnallol\lll Page 1 ol1 

VES 004906 
i . . . , .. .. . ·: .. . . :. .. ~. 

: 

. ·~ . ====-~_;_•' :.;_ · --· • r· • 

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. '·'" - .. '7'' ·. . . : .· . · 

. ie68So~Dr.Hslf.,;,Pt. ... 

(lef)21~ (flll()1t5-82i1293 . Certliicate of A.rialy.tlca·l Res ttl is ' : . 

. , 

.. · 

~ 

"..i) 

· .CLI.ENl\ l'tfAmm Aa.at)'tkal. Secvica. 

5555 N•r<h S..Vl« Rd ' •· 

8UtflA(t~, Q.~ L7L SH1 

ROIOSOOSI 

A8916-48 

ll.esolt , l'QL ·Colts 

AF733J-01R\ ffiri:n-!1~Rl . . · 

Lib l_ll: .. · R~f.OIA . 

oi<S.ai.J!~ · 08/l11)008 Q:OO 

ASH, OU. 

.... ~ 

: 

'IIEATlHO VAJ,.UE BTIJJLB 

••at~noVotue · .. ., . '(,310 00 

AF733~~01R\ H]ii:U-02-RZ · .' ·Lob (D: : ' ·. · R0801005142~· 

:·i1ate St•pled: ; ·Oa/1212008 0:00 

ASII;o._. 

..... . ' 

A¥733~1R\ mrro-Ul-RJ ·. 

oiie a.C.~;.~:· oali6noos 

'7.00 ·• 0.01 

• 2,1$0 so 

Lob ID: · · R().8il&oo'st.o:u, . 

. Oate s..-plah OStt.JI'l.OOl o:OO . Date Rttd•ed: 01/261200& 

ASH,Oil ' 

.. ~ 

" 

'.'. Alh . 6.... ~·· " 

~· .... 

·. 

,. 

HEATlHG VALUE BMB 

'· HnSn""Moe 

< ~icca less thao the litnil of qUoolitatioo 

Wd iac~. 

00 

. D•le: 29-J(ug.j)8 

Oa'le Aulyrt · 

1\bufx: A..QUEOUS 

. (XU 

oz.Co · 3C·. 

'. 

":(atrix: "'QO~OUS .. 

VJO 

sc, 

VJO 

lo£3 

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.· '• 

VES 004907 
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) 

. . ,· . .. 

I!!!!JI!I-- . llliiiiiiil ~(F.-,. $ bi). u.c ...... 

2e61l S.n<ISI"" 0<. ttUdd P<. I 3( 40 

(IIQI1S.Im-8095 (lfo<)215-6l2-ll93 Certifoeate of Ao.olytieal Results 

LabOrd..-: 

Pro]ed; 

Mauam Aa.a.l.y.tieal St:n'ic.os 

ssss 11..-do s .... ~ Rd B<ri"""'. O.....ri. Ln. SH7 

R080S005 l 

AS9164$ · 

AF73~lR LBTU-J&Ri 

LabiD: R080SOOSI-04A 

ll-'< . PQL Oak< 

·~ . .. . .. . ·:: .' ! ... : ... 

...... -· . . . ... ..t. ...... :. 

.. ••' :. ·.·.-·;·~· .... ., ...... . . -:. ·.·. :' .. . ·.• . ..... . .· 

Date: 29-Aug-08 • 

Dati •Aulyst 

O•te. Samplid: 01/111200$ 0:00 Date lleceivod: 0112612008 MalrU: AQUEOUS 

ASH. CU.. 

""' 0.110 0.01 

. HEATING VALUE BTUJUI.• 

uo"*.1no VGluo IGO 50 

~!':1:337..() ~R\ !J!TU-Ul-!!1 

LablD: R030800Sl-05A 

Do_tc Sam.pted: 08/ ~ 0:00 Dale Recdvod: O&f2612008 

ASH, OIL 

' A\h • 0,0300 flO I 

HEATING VALUE 81\JA.S 

~·- <50,000 so 

AF7333..()l R\ LBUJ-02-RJ 

Lab lD: R080800S I-06A 

Dote Solllpled: 0111312008 0:00 DateRecdvod: 0312612008 

ASH. Oil. 

Alii o.oooo· 0.01 

HEATIHG VALUE BTUJUI 

HeotlngVAIJe 2.000 so 

< tadie.~CS less th>n the 6mitof'!""'litation 

KoWt~~ 

" 0482 ~~ VJO 

·- 02~ 28-1\UQ..,. sc · 

Motri<: AQUEOUS 

... 0482 2e-Aug-oo v.a 

- 02"1 28-"''I-GG sc 

&latril:: AQUEOUS 

" 0<&2 . 26-AJ.IQ.o8 VJO 

o .... 02~ 2&-Aug.oe 8C 

Paao l oO . 

VES 004908 
- -Qo;- ·. . ' --u.c . 

. ,• . 

'la6as~M'""'Or ...... ·~ ~oi)21Hl2.a995 (IO>Qil~ •m Certificate or Anal)'llo>l·Results 

CLlEN"I't Mu:XIft:l Aaai;Ytiea( Services 

5~5N rl!>.s..-....R4 

krlio"""' o..w~o L7.L sm 

1\08080051 

A&9l64S 

AJ:!73J?-41R\ SF -UZ,..Rl 

t..b tD: I\0&0$00Sl-l}1A 

.. 

· · O.te'Saaplod: Wtinoos 0:00 D•t.ll~d .. d: osll612001 · 

ASH,Oll 

""' 

HEATING VALUE BT1JII.B 

H••tlngVa!Uo. 

' AF734!-41R\ SF-Ul-IU 

~b ID: • ROS080051..Q3A 

Do1eSoapled: 081~ . 

ASK, Oil . ,... 

AF734l-41R\ SF-U2-R3 

Lab tD: ROSOSOOSl~A 

Dale Sutpled: 0811312008 0:00 

ASI<, 01. 

""' 

HEATING VALUE BTUILB 

Heattag Va.lue 

4.00 0.01 

Dale !I<Wved: 0812612008 

SA I);Ot 

Date~ed: 08/WlOOI 

1.05 M1 

< so.ooo 50 

< lad'IO.leSiess tha4 ~ limii of ~taboo 

lfoW'ttiN~ 

Date: 29-Au~B 

Date 

Matric AQUEOI!l> 

-

Matric AQUEOUS 

% ~2 z~.oa 

- 02<0 26-AIIg.Q8 

.• 

VJO 

sc 

VJO 

sc 

VJO 

sc 

PocoJ oO 

.. ,.:;. 4418 POTTSIII.l£ PIKE,~· PENNSVI.VAI<IA 19605 GIQ-$21-4833 FAX 610-921-9007 

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... 

.· 

VES004909 
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l!!f!!II!!S 

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2oro~llr -Pe.t9<40 

~d)21S.ez!.eggs(tox)21s.4ll.t29l Certificate or Analytical RJ:s11lts 

CUl\NT: Mat.nc.u A•u.lytical St..rvices 

S.SSS NOC"di. Servitec Rd 

B«rliqtO<l, OacuiO t.1L SU7 

lAb Ordtr: R0$080052 

: PHJ<>et: A891648 

A.aol.)'su A.s-edBosls 

< nd~ less lhao die limit o( quantib.lioo 

H • ltokl fkM ac:c:dl.oc;e. 

Dry Ba>.io o.ru Medto4 

.. 

; 

I) ate: 

1>11< 

~ 

.. 

19-.tug-08 

Aoa'\YII 

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I'~&< l on 

4418 POlTSVILLE Pl<.e. R~NC, PENHSY\.VANCA 196M Gt0..92.1-383-l FAX6t0:.92t-8607 

VES 004910 
•.. .-

.. ~ .·· .. . ·.-

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--~ .-:: . .. 

"'~·.,:.. . ' 2eat&tdi!O'Ia~ HitW1Po.'19Wl 

C)d)216~2!.-(f<I>QZ1 s.a22.1'l.93- C.rtlfieato oC_Analytical Results . . -

, 

,~' t ~ .... 

· CU ENT: 

. . . 

Lab Onltr: 

Pro jed: 

· A.ut,.... 

~u ll\ An (ytic l sUvic:es 

SSSS N..-6 Se:n -. Qlf. 

~urilllg<'!"• O•tari<o .:;;L ~H7 

. : ROiot0052 . 

A.391648 

. AFJ3 R\ CS-Ul-R3 · Lo.b ID: . · . RDSOSOOS2.03A 

OmS- plod: Ollllf2oo8 Oa .. l!«<in<l: ~' 

PERCENT MOIStuRE 

Mou,ue, Totll 

ASH, COli.L 

Alb 

HEATIN<O VALUE, COAL 

l'loi.urOO V ... e 

. · 

! 

, 77JJ 

< lndicalcs ~ !lwl tbe limit of q~ 

H-KoU r .. ~ 

u.a . 

G,OO . 

OnUs 

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.()3174 

.()5MS 

·. 

.. . ~·-:- ~ 

··l 

t .: .. -. ·<: 

-· ·· . .. .. 

Date': 29·Aug·08 . 

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'2-· sc . .. 

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... 

Pose 2 ofl 

VES 004911 
... . . " . ·. 

YOur Proj6(1. #: 1002.022 . Slte:VEOLIA . · . 

At!•nllon: J eff Gorman 

ENSR International 

so 15 callipusw<iQd or. Sullo 104 · 

East Syraoose, NY . ' USA . 13057-42:12 

M,r,)Q(,UI JOB I: 1'>891648 

Reecivo4: !.008108/14, 12;00 

Sample Malri>c: Ll01J10 

tf~s Reoctved: 9 

Sample Manx: Water 

tt Sampl~s Roooivad: 3 

. .. 

. . RePort Ooto! 2008108125 

lhlt report supersedes nil p<evious reports With lhe oamo·Maxxam Job rumber 

CeBnFJCATE Of·ANALYSIS . · 

s 

3 

,· 

200MI8/21 200Mle/2f CAW SQP.Q045l 

al0Ml6/21 :l!13()M)8121 a..t SOP·OCin 

.· 

EPA 7470 

EPA 0010C 

(I) Thlltoii.,.~O<ffonru!dt>y f;,ux>m~ -~ . · (2) Malatlm """'V'fcs'does not Mid-tlt anor,.ls ol..-ln-samptoc using lll&ICP Axjol,..-y. 

.. 

M.i>:xxAM ANAL Y'TlCS INC: Total cover pages: 1 

?.00 to(t~ 

Digitally 

signed by Mike 

· o/. ~""::...;... · -- Chains · t>ate: 

2008.00.25 

10:19:15 .04'00' 

ThiS documerll k k! cHcltOOlc totmM. harv3 CC~py rs ·~ on reqCJe$l 

,655S NMh&eMe9Ro.4.9~~c.n.d• l.7\.liU7 T.t: .(906,)U2-8788 TatHo•: tvoQ)ecJ8.00tO Fwe(UC,$)3~i.J160 

'• 

. .. 

VES 004912 
· .. . • 

·. 

. . . . . 

.. ' . . ·. 

-\-Moiooim Job i: A8$1t~a .' . ·) Rot~Q<t Date: 2Jl0610~5 · 

.. . . 

. .. . . 

•.· g"' I• I " " . . . ·~OIIeclonl.i"r« 

. ·- . ~Caolrol oiltd> . .. . .· .• .· . 

.. 

. . · ... 

) . . ·. Not- _ _. .... -.OJ-, C<>nO>oteaoit. 

. . . 

.-.. 

. EHSR I~Umalio<lat . •. 

Client Piujec( II: 1002-oll 

PfOjed name: VEOLIA ." · . . 

o.s t5910cn 

· .. 

... 

.· 

: 

~6y~~f'.s~ • ..••.•• 

www..lll~••~YU-oGs eo• , I 

: : l' 

.. : 

. 

. . 

... 

· . 

Paso 2 ot ,. 

' . SSSS~~R~ Onblrio,c-&2 L7l.6H7 T.t: ~) 3SM7"90 , Toriw.: (800) 868-0S3B · F'cc (90S) 33:2.4tS9 •• ;· 

. · . ... 

VES 004913 
•' 

· .. . ' . :-

• 0 

._, .. 

• 0 

. . . . . . ' . . ... · .. :' ""'; . . -·· .. •'"'" 

~ ttzs-wcc -.d~ : ... ·.: ..,...,., ..... JCl"l.ttl. ... ~- . : " " 

ENSR lotemational. Client Project II: 1002.022 

Project nome: vEOUA 

ELEMENTS BY ATOMIC SPECTROSCOPY (UQUID) 

.......,_le(At) m~ 12 1l 1'7 0.5 0.5 0.1 15111152 

- Be<,6.m !Bcol mgt\. NO NO NO 0.03 NO o.oos 15911m. 

ToO>I GadLrivm (Cd) mgi\. 0.1 0.1 . 0. 1 0.1 0:0. 0.02 ' 1591852 

•"9'\. 5.1 4.7 *·I 0.3 0.39 o.os m tB52 

"""" t:.t 1.3 ,1.1 o.s NO 0.1 111411652 

~ 0.0180 (1) o.o425 ro o.o4ooro .0015 O.llOGS~ .0015 1592563 

=l<ol-

·= Ropotlob40 -IW 

Baldi• OuallyCooO!d - . • 

1 ) ""'"""-...-..-~-~ ......... ...., .... """", 

2 """"' ) -tigl\_, -------,---aliquot.-- __ .,-

~ ~ ~ ~ 

........... (At) mgt\.. 0.2 0.2 .8. 1 NO 0.1 . 15411a"..Z 

rol!' ller)OIIum (llo) mg/1. . NO NO o.oos NO OJ)()$ 1591152 

otllc.d-(Cd) mg/1. NO NO . Q.02 NO 0-02' 1591152 

.... a.-lorA IC<I mg/1. 0.12 o.os o.cs NO o.os 1ft11SZ 

.... lAid~) mo)4. ,.., NO 0.1 NO 0.1 t5918S2 

~~) mg/1. 0.0016t'f) NO (I) O.oo1s 0.14-:t p.023 ~-

>10 " Not-'"' . flOL • ~Ootedlon Umll oo:SIIlch • Ouoll!y Control Bald> . 

1 ) Sao\ill6 boUio-.. _ oedlmenl. s.. .... wu-to- '"""' ........ ~ ... 

\0 0 

,•', . 

VES 004914 
'· ... •'. , • ; "'~ ;·.: ' ' ' ·'-' ... :· 

' ; .. 

~- iy; ~ a . !: !----:--------~-.....:,;__ :....._!.··:.....:..... -:~=·=:=: ... :::;;:t.,..:::<:::·:::..?. _~·:= ....... r.:;:r:;;:~::-:= ENSR-. 

· d 

' 

·• . . 

Clenl PIOjec11: 1002-022 

Ptojec:t name: VEOUA 

ELEMENT-S BY ATOMIC_ SPECTROSCOPY (LIQUID) 

~--~~~ !!3 I RD~ pea••~ .... ~(As) m!1L NO NO .., 0.1, i591852 

Oflll Be<)41um tilt) m!1L NO NO NO o.oos 1591852 

.... ~(Cdj """' NO NO tiO 0.02 1591852 

~r ... ~(Q) mgll. o.n 0.11 0.11 ().1)$ 1591852 

... I.Bad (PI>) • mgiL NO NO NO O.t 1591852 

~~ mgll. OJ)OOO o.otm. H/A • IJ.oo1S 15112563 

. Not"""'*" ..... ~ .. .._..... Deloldon !..hit .. pc:·Boldo • OUslity COnltot- '-.· ...... 

J 

' · ,,, Paoe 4 or 14 

VES 004915 
-=)· . Maxxam Jol> lt. ASSII\143 

(:-·. : Repoi\Dato:'zooB/0812.5' . . . . 

. 0 . ~ .~J 

·. 

... -· , - :;. 

EHSR 1nte<nalional 

Oieol1'rojed 11.: 1002-()22 

Project name: \IEOl.lA 

· RESUL ~S OF AtiAL V$£5 OF SOIL 

• 

Pago5d 14 

.... · 

... .. . ~ .... 

. ' 

.. 

VES 004916 
: ·.::· ~·1'"~.: .·. -~ .• ·• 

• • I .. -,~ ' • ' "' 

';! ... . . •• 

. .. ... . ; 

' . . :.1\ll a_/(; a rn _,---- -~· ...:._ ,• -:----'-:-------= J><:;;;'f:;;-;•vr;;;S;;;G ;;W;;:"""~-::;-;;- .::.'.:::. . r-~ .. ,. .. .., .... 4 . • ..........,..,...;::;,.,... •.•• ~~ ~ .. ~ . . • . . ENSRI~ ·· · 

-~ Ma.ocatn JobJI: A891G43 ClontProjecU: 1002-o2Z·· 

:·::· j R41p0n Dato: 200Ml8125 Projed n;une: VEOLI!\ : • · 

·~· ' • . ... 

Eli;MEI'flS BY. ATOt.itl(. sp'eeTR:OSCOPY. (S.Oil) 

;,') .. 

'. 

; 

.. 

Pogo6ofl4 

VES 004917 
. . . 

D. ~.~-..;. Job ftM.I1lWI ·: .. Report DalAl: 2008108125 

--~ 

.... 

'• . . ·· . ' 

:. 

a.sll. lnCOmolional 

Cloooll'rojeci 11;.1002-022 

PIOject name: VEOUA 

.. ELEMENTS BY·ATOMIC SPEClli.OSCOPY (WATER_) 

., 

.. 

. . 

. · 

. . 

Pogo 7 ol14 

&S5S,_ ......... ,.cod. ..._~ . .,._.·l7lfili7 . . . 

"": .·. ... . . 

. •:,· 

~~.;,.~·· WWW ......... III!..._~-. ·-·· •- ... · .. 

.. -· ·· .. · 

· .. 

VES 004918 
. · . 

. · 

·, -J· M!xxam J«> _,Ail91048 • • R01>9<1 O.te: 200010812S 

\ ' . . .. . . 

.. 

'. 

' . 

.• ') 

. · .. · 

·. 

.. 

Maaam·IO -10 ~ Hlll\J.UMI 

• MMri>< ,LIOOIO 

. \ -10 

-0 ~ 

AF7S34 

. M.lltrix. ~~ 

' -10 Al7335 . 

-· Ma<rix 10 HeTU-02-Itl LIQUIO 

......_Ill _ $ooljlle ID Ull\J.u2-41 i 

~ 

............ AF1337 

~- ID IB11J.U:!~ . llni>< UQ\.00 

' 

l:~st Summary 

.·· 

Pago 8ol 14 

. - : .. '•C • ,• ·~ •' :~. ,' ...... 

• . ' .. :. 

... ~ ... ... .. . .. · ._ 

ENSR~nal 

.... ~ lzS'~ .. ;:;~ ,· .. 

~'!"'·= -~- .·-";'\ -

' Client Pro~ •: 1002-o22 . . ~ .. , • .;.., VEOtiA 

.. ·, 

·. 

·' 

VES 004919 
t.eoxum Job II< AS9164l! 

·J ROI>Ofl oafo: 2008106ns. 

Uu.x.an\ 10 · AF'7338 

Sa .. •10 · LB1'Uom-R3 f<Mrlx UQUIO ' 

fib~ 10 AF7340 

Satoplo ID SF~2-41:1 

Matrix' lJQUI) 

........, 10 AF13<1 0..0 

- 10 SF.ul.fl:l IUtrix LIQUID 

ftaXUd lO Af-n42 

S;unpiciO CS-U2·R1 

• Mattix Soi1 

Tttst Summaoy 

.·· .. ··:: ....... . 

. . . .. 

...... , .... 40 

·'" ... ~ 

-· 

VES 004920 
' ' . ' ·: '-.' 

. . ::·. . ~. . .. ... --

. 

1\11.' a ~~~ ... /'J !.T-! . --'-'--- _;__:. __________ _; __ -'- -~"~.,$...,..~~ =.;:~-~~ ... [:;.?..~~;:..._~~-~;:;-:;. 

ENSR lmma6onal 

·:: 

· . 

No"""" 1!J IF7342 Oup 

Sample 10 CS.U2-R1 

~Sol 

........... -I) -

CS4J2.fU 

. 

-Sol 

Ma.xxam 10 .. AF7344 

$aqllle ll CS-U2.fU 

lo1alrix Sof 

lrkloc;;mlD AF7347 

S ...... 10 MS.U2.fl3 

Matril( W1ter · 

.· Teet Summary 

. • ,. Pogo 10 of 14 

Cf,ent Ptojoct #: 1002-022 

Projecl name: VEOLJA. 

CoU..o.d 2()()M)8113 

Shipped . R-.i 2008100114 · 

V...S-5 NMh .$111Mce Road,~~. c.t.da l7L 5H7 Tel: (90S) $$2>8r88 Tol Freo; (000) &6t.QG39 P.c (VOti)'3.S2...8tGII 

VES 004921 
· .. ;· .~ 

~ Maxx:am Job IJ. ~ItU8 

'c) Ro\>ort Date: XlG8108/2S 

- ·. 

ENSR lntematioOal 

CliontProjec< l o 1002.()22 

Pt<>jo<:! name:·VEOltA 

'."'\ 

') 

GENERAL COMMENTS 

~~ Afl3:13.01: t.4CI31$ AM~: Ouo .,.,i,e .. fT4llo mollt>c, ..,,.,.. ~<~q\linl<l ~ i..J,, wore adjus<od ..;.,.oong~y. 

Sample "-"1:»4.01 : Motola ·Maly<is: Ouelo 11\e - malllx, IMl(llo-".""~ dijuliO<L Odedjon imns _, a<fu...., ~!JII<. 

Soll ... o llf733S.OI: UeWs -: Due"· lhe .. ..,.. malrix. ....... noqWed dluliOn. O«odlon Gi.wo; _.. ..-~y. 

- AR33$.01: ....... Malyois: D!>e ........... - ...,.,.._....,_ Oolocion --· ..., .. .., -~~y. 

- AR331-o1: -IW>tftls: Due" lhe ...... ......._.....,.. ,....--. Detodion lnib ~ odjutOod OOOO<doVI· 

Samjllo AR:»&.ol:,__ o..e.,.,._......._ """lPPI~dllulkin.~---~VY· 

• 

$o"''* Af733&.QI II«aas~ Due ........... ""'*-~-~--..- 10 ilio>ll. - Afl3«)<)1:--o... ........... ,_, ___ Ooaaion ____ . 

Sample ~14 :-..,_ Oue"lhasamplo""!IAA. --d"""""'-OoO>cion--. adjuslad IICOOOdioiCjy. 

to lhe items. tested. 

. . 

·. 

P&go 11 ottc 

\ -. . . . 

VES 004922 
.. · . . . 

. .f\.11 a '?<5" · . am .. ', ~~·~ .. ···· 

DrtN#t ~sirvk .., ~ ... •t-: 

.. .. """""'--~~CII. Ul. 

E.NSR lntematiooal 

Attention: Jeff Gomlan 

Ctiont P!Oje<t 11< 1002.022 · ""':\ : .·!, .... 

....... ) :. \' ' .. 

·-

', 

• 

\ .. 

QMlC 

tlatdl 

"""'hi OCT""' 

1591002 u.e OC ,ST-'HOAIW 

'S4>1ked Qlao1< 

MeCtlOd 8$ank; 

RPO 

1591~52 K<D MATRIX SPIKE 

(AF73-11) 

~-

~~8C$11C 

'. : 

RPO 

.· 

t&S2280KCO &lATRIX SPf<E 

O.~': , , 

PIOje!:t name: VE.'OUA 

. Quaflly Ass•nanoc Report 

.........Jab -.qoagt648 

Dole 

'. -yuo6 

Oltoltdo 

CNall<lo(Q) 

(Q) 2006108121 ~· Q>lootclo 

~(CO 

(CI) 

~· 2008100121 

T--(As) 2008108120 

-~(Be} . >008Ili8i2o T""'~(C4) 

, T .... a...iium·(Cr) 

-

2001108120 

T""'Leodl"b) 200tiiOei20 

TOCII-(As) 2001108120 , T...,11«)41Lm (Be) 

T-~(C4) ::::: 

T-Chori<m (Cr) 21101108120 

T-Load (AI)' 200tiiOei20 

TOCII "fC*'olC (As) , lll08I08I<O' 

"""" 8o!yttlurtl (Be) 

200&<l6I20 

TCICIII 

filial 

a..mlum 

Cedoium-(Cd) 

(Cr) 2006108/20 

~ 

T GQIII.oad (Pb) 200Mll!/20 

Tot~~~Moolo(~J 2008108120 

TOIIII~(Be) 2008108120 

T-Codnoluin (Cd) 200Ml8/20 

TGCII a-... (Cr). 

lddedt_..,......(As) 

TGCII~(Pb) 

-

20081011121 

~ 

h:tl 06 '4'e Beq£un (Be) 20081011121 

Add e.. t }' Cacbium (Cd) 20QISIIl8/21 

2008101112 I 

' v.u 0..00, RDl.illl0.01 95 

99, ROL=O.OS 99 

o.ooa, RDt.-o oo~ 

<U 

0.0 0~) 

··~ 87 

0,(5 .. 0.<3 as 

OM 17 ' 

0.(9 07 

O.SI 101 

. 051 101 

G,Sl) ' .. 0<9 ee 

HO, RDt.oOJl l 

NO, R1JI.o0.000S 

1<0, RfX..o0.002 

NO, RDL<O,cios 

NO, RDLoO,Qt 

NC 

NC 

NC 

NC 

NC 

' 0.4-4 'as, OAt 82 

0,(0 80 

ii.C3 as 

,.....; 

" % 

" " 

nog~~._ 

mQIL 

nvt. 

~'!. 

• 

~ 

• oo\. 

~ 

"""-

"""-

~ •v'l 

mgo\. 

nog/L 

"' ,,. 

% 

· % 

"' tq'g 

-.tv 

tq'g 

-~·~(Cr) oglg 

-edt-t.oad-(1'1>) lOOtWeal NC NC(l) oglg 

QCSTANOARD .odd&lractlbte-(A.s) 200&'08JZI o.n 88 ~ 

.odd-Cl1t<lioom (Crl 20Qe/011/21 0.30 •• o4'll . .odd~Leod(Pb) :<008100121 1.2 84 ~ 

Mel-oo Blanl<: N:ld~-(As) ' ' :1.0061011121 NO, RfX• ( ug/g : 

lvJJ ~· flCo)Gum (Be) 2000100121 ' NO, ROLOO,l! oglg 

lldd ~bie Cadmium (Cd) :20Ciel00fl1 NO, ROL•~I.3 ' uglg 

--Cl>n>riUn (Cr) 

20081011/21 HO, ROLoO.S ug/g 

--•!Md(Pb) 2006/lJII/21 ND;ROtJof tlglg 

:fmixsp;i<£ Add&ndabielead{AJ) 2008108121 .23.5 ... t S!I2SGl sue ....-...y(Hg) 200&Q8121 ' 0,0230 02 IIQI( . 

: . Splk<d'Diw "'""-ili$1 _,..,_ 

200Ml!ll21 G.0263 105 ~ 

~(llg) 20QISIIl8/21 NO. RDLoO.QDOf ft'Qil 

Rf'D """""Y~ . ~~ NC ... 15925871AC W.lRIX SPii<.E ---ili$) 200Ml8121 • 0.570 114 ug.';l 

OC SJANDAAD ---(tiQ) 2ooMlll/21 0.306 100 

r.teChod 8131'!k -~~('!~ :zoottAJeht NO. RDL<O.OS '" ~ 

Rf'D .Add H . 1 NC % 

' ' 

~~ "' Not deaacted NC•~ 

~ • R&h PllnlO<IIOi,.._, 

Slandald• Quar.yCo:M>OS1Mdl•d 

SP.c:E • Fortied ~e · · · · I ) The ~f'l,t)Yel'f was~ the lower OlfCrollimil.. nit~ ~eot 110W bias In ~ ~ts lot llis apeoc:i&c fiNfVM·· 

. '2) Tho ~«11he ---.lot_,.. (NC). llecouso olt1elll1>_...1bn olthiS _,..in lho po10N-tho 

Pogel2ol14 

QCu.iS 

WA 

8o · 120 

. 20 

75 1~ 

75 ·1~ 

75· 125 

7S · 12S 

75 . 125 . . 80 • 120 

78. 1tt 

t$ · 111 

75-- 12S 7~ . t,l9 

25 

25 

25 

· :.cs 

25 

75 •I:.CS 

' 75 · 125 

7S-12S 

7S·1l5 

· YS · 125 

·75 - 125 

75. 125 

75 ·125 

:15 

15. t25 

84 ·113 

25 

7S · 125 

75. 125 

35 

This ~is in eledronic ~ tlaod OOP'J k ·~ (1('1 teqlJ8St. 

&s66NorthSGMce R.o.cl. ~ ~ Cenid• l7t ..' 5l-t7 T.t (005) ~..t?68 Tol F~ (WOO) Gfi.OII» FC.C (9Q5) S324ti69 . . . . . 

,' 

,• 

VES 004923 
( 

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. ·~ 

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ENSR lnteniafional 

Allenlion Jol! Go<mari 

C1iool P,]e<:t it.: 1002.CZ2 

P.O. II: , 

P~l name: VEOLIA . 

·. 

Quallty·Assuranco . Report.( Continued) . McuotMm Job Numi.Mir. GNl91648 

.. ac u...11s 

· .

. ·. 

I . 

.. 

,. 

VES 004924 
.. ' : 

.. . 

. ~·.· .. .. ,, . .· . . . .. . . ... ~ .. ...... · 

· . 

:. rvi a -AI .,;;~ __ __:. · _. _____ ,_...;··__:. __ --" .."'". ______ .l!rlwr~~ · ;: .. !!:. ==-= .. =·~-i3;;;"': .. :::-::":- ,.... '"' '"''c • , .. c ..,...,.....-..:ICIII*~ 

~ . (') 

.: -:' 

., 

. . . . . 

Ma.xxam Job f:·AS91G48 .· 

FilANK. MO. 8.Sc, ~& 4b. M.aoage< 

; 

. · 

· .. ··· 

. \. 

Validation Signature Page , . 

.· 

' . 

.• 

... . · 

.. 

' \ 

'· ·.·.·? 

·. 

·.· 

.-

. .. 

VES 004925 
;?\ 

.. ) 

~ 

7\ 

.0 

. . :.,· 

... ·.' .. ... . .. - . :, ;.. . ...... ; 

......... -...... 

·Week of September 8, 2008 

. · .

VES 004926 
·. 

' 

,-\ . , I . 

····' 

) · . 

·' • ·. J 

·. " - ·. . .. 

. .. . :· 

~=~~ 2oe9~t>".-Pt.194<0 

(ioQllsm891SC"-'l21$422-lllD ·Certifi.,.te of Anolytic;al Res11Lts 

I.A.b Order : 

· frojec.t: 

Mus.-,o..,.lytl<al s.mc.s 

llSS N•t1b Suvlco R4 

l•riiiiC'f-.Oabri• l.1LSH7 

RJ)l090041 

A8.'..2964 

AI. Received. Basi.$ Ory 6as.b UoJcs 

AL3449.:G!R \ CS-Ul-Rl 

Lab ID: · Rll30900Cl~ I A 

~Saaop oj., 0910112001 0~_. ... , 0911812008 

ERCEKr~E 

-...r.w 31.9 "' 

ASH, COAL 

""' 63.< 93.1 "' . ~TING VALUE. COAL 

~"'- 1&0 260 B•lllb 

AL34!n.:a I R \ S~12.-Rl 

lAbiD: ROI0900«.01A 

01k8• 11111(Jlo4: 

· n...- 0911&12001 

PERCEln IKXSTURE 

Mob:t~.n . Tc\ill 30.& " · .O.SH, COAt:. 

Al.h oo.a · B7.G "' 

ltEA Tli<G VALUE., COAL 

HeatJrt Vabe 32.0 <60 8-

Date: 11-&p.()IJ 

M•thod. 

't•btrlc SOLIQ 

02%1$ ~~ VJO 

03174 ta.S.p-04 VJO 

OSss$ . t&.seo:Oe MRIP . 

Matrix: SOUO 

02216 

·~· VJO . 

03174 1&-seo-46 Vio . 

0 5$6$ ,._ ... . MRW 

Por;elof2 

· . 

.. 

VES 004927 
.· 

.. ,-) 

. · 

. ·, 

ie6s-Or,tot11e0jl't. IS440 

l!e1)21 S-822-81195 OroOlfS-822• m Certificaie o£ A'na.lytital RC.uits 

CU lt.I'O': 

tab On!or: 

Pr_o)oct: 

M axu .. All> l ytic• I ~rylui 

SSSS N~m. s.n... IU 

8.rlloc<oo, Oa<ario L7L 5117 

R03090048 

A8A2964 • 

. ,.AI\.345l-4 iR \ 'cs-U:t-R3 

. Lab W: ROS09004UlA 

o ... ~ · 09/IOOOOS 

~Rcerr· uoisruf\E 

Oak R«dnd: 09/l lflOOI 

MoiP..n. T<Ql 

ASH, COAl. 

.... 

HEATING VALUE, COAL 

Ku VIII~ 

·: 

.... 

61.5 

< Indicates lu• 1han tbe limit of.qoantiution 

twdT4.M~ 

370 

' 

.. 

Uolu 

p,(stru; souo 

.. 0Zl16 $-S~ VIO 

.. 03174 ,_,..,. VJO 

05865 

.. 

hf!C l of2 

« 18 POTTSVlLLE PIKE.R£A91NG. PENNSYlVANIA 19005 610.921-6833 FAXG10-921.e667 

. .•... 

: ~· .. 

VES 004928 

.. 

.· 

. , .. 

.· .. .. 

·. 

1!!11!!!!!1 ..... •. . . .. .... ..,_Vv_>OR)llt . 

~-Oo- Holliti1Pe.f9«0 . , . (ld)21$.821,6995(fax)2fs.<f~ CectU(tate ot Aulfiicol R .. ults 

CtlENT: ' . . . Max~m ~alyflc:.Jt Stt'\li<:cs 

SSSS Norll. S....i« RAr 

Uudl~. Oo<sllo (.7L ~ll7 

ROSQ99<!47 

ASA296C. 

ltcsull rQt. Uaits · M ... od · Date· 

Al,J«l-01R \ LBTU-Ul-Rl 

t.ab _m, Rll8090CM7.0V. 

Dalo SaAple<l: 091081200! 0:00 . Dolo a.c<lvoct: 09flll'2001 

.. ASitOil .. .. 

Ach · O.MO i).Ot 

HEATING VALUE BTUJLB 

. tte .. u,.~a~ut 

t.J.34#-01R \ LB'I'U-U:t-IU 

Lab lD: RllS090047~SA 

....... so 

Dote S•lll•led: 

'. ~SH.,otL . 

.o91091200i 0:00 · Date a.-ivod: 09it&f2008 

..... .· 0.01 

1.780 50 

AW44S:01R \ LBTU-UMO 

Lab ll>: 

Dale Sa"'!' led: o91101200S 0:00 Ostc lt<uived: 09/1112001 

ASH.OL 

~ 

liEATING VALUE Bl\JJ\.8 

0.0100 • O.Of 

Maliu: AQUEOUS 

' . 

02<0 

Matrix: AQlJE9US .• 

. .. 

.. 

Aaaly• 

VJO . 

VJO 

VJO 

t\&atu,G,vatuo · . 0240 t9;.5.cp.OII 

< lnd~ less 1ban 1llo ljmitof quanliwioo 

HoWl\Mec~ 

.. · 

Pr.aeloO 

.-· ~ . . • · . . 

·. -. 

·. 

VES 004930 
.. . 

7\ "j 

-· I 

... .··.' .. ·· .. . . . ~ ..... . : - ·. ' .. .... .. 

•. 

.. · 

.. .. . 

e&rtifu:ate of _ylics tw lts 

~~: .· llliauaA .. IJ(I<>IS<rVtces.· 

m51'1-5.mc. ~ 

8wli-cM'Iof0&b.rif 1..71.. SH1 

Lab Ord.cc: ·• 

· Protett. 

Rj)8090047 

....SA2964 . 

ll.esutt rQL . !)oito· 

AL3446=91 R \ SF-01-Rl -, (p: . • RDS090047~7A 

. o•~c ~' 0910112008 o:oo 

·ASH;OL 

. 

·. Hii,A -

T[NG VI.LUE BTUJi.,o ... , .. ....,v.... . 

· At..34§7dl1R.\ im-ui.iu·· 

DOte-~ 09/IIIZOOI · 

12.5 1).01 

.800 60 

. ,:· Lab m; · RDil690047.:08A 

Daoe.S~ 09miloo8 o:oo. -Dat• lti:c<ivc:d: As({. OCL . • • 09/(~ : 

• A,j, . 

IlEA TIHG VALUE BlUILB 

" 

... 

·.lluliq!V- 170 ..... Al;!448-tl~ \ SF-U:t-Rl . La.b W:. RD8090047~9A 

· Date Sal.llPk<l: 09/IM.OO& O:Oo . Dat•ll.<ce!vcd: 09/11/2008 

AS!i, QIL 

' AJ;i- .• 

EAl'lto~G vALue stuiLB 

HMti'Q ~:I!Ue 

< tn<licales ~essthat> ~~ Unut·of quantitotioo 

«·Hold ~~ 

1l.4 t O.Ot· ~ 

2<0 50 

Metlood Oatfl An(y$t · · 

Milrilc: AQUEOUS· · 

,.., .n-s.<>a VJO 

ln<O 

M11rilc: [I.QUEOI!S 

IX8>.. ~.00 . VJO 

02<0 11-s.p.ol. """" 

Malrru AQUEOU~ . 

VJO 

Page J of.J 

·. 

·" .., 

' . ' 

.. 

.; 

.· 

... 

VES 004931 
.... .. 

.· 

.· M a ('~,. /'(j a 

. ... 

~-~,c:· --,- -------- -- ----Drl=-=•!.!:.:s..~~-~!!!~~"""""'""'"'"'­ . . 

' 5015 Cllmp<Jswood Or · 

Suite 104 ~ 

East syracuse, NY 

USA 13057-4232 

Your Project#: 1002~ 

Site:VEOLIA 

Report Oat'!: 2008109/23 

fiG\XXAu JOB f : ABA2964 RecMvod 200~1 12>00 

. Spmptc Ma1tbc: 'Cllll<ni<:al Material 

'# Samplos Received: 12' 

··y 

Total Uotnlo lo'Sofl 0 

ToloiiAWI~ lol Soli by A>Ool ICP./IES 0 

TO(altM...,_ydobyMa11CP~ 

T'!"" 1Ao1ob -yolo by MaliCP t0 

CERllACAJe OF 1\HALYSIS 

.o ... Dale 

2QOM)9/18 2006109122 OntOO'<l072 

200BIOOI'22 200Ml9122 Ont SOP<l072 

· 2008109116 ' 2:0otw9ft6 CAM SOP-00406 

200Ml9116 200ei09117 CW. SOP-<10400 

(1) Thll..,.-.,...,..,... by -mMal,... Mismoauga · 

(2)-~ . dooOnothcldaa;r-br....,y.aolmOI* . . ln-wnpleousing . ... ICP--· 

MAXXAioiAMALYTICS . • Digitally 

signed by 

,,.,; Mike Challis 

~~Da e: 

:::_: .91· · 200&.09.23 

10:33:26 

·04'00' 

T ota1 COYe< pages: 1 

P.a9!J1 d tO 

'ltisdoo.mont loin"""""""'""-....,~ I$ ....aat>le on c-. 

EPI\ S~-6010C 

EP.\ 6010C 

EP~GOIOC 

VES 004932 
.'! : 

· M a .. Aj a rri --~------- ---- --------'-2!!;-~!:l .. ~s~-~. ~~'"·~~~sa-o;·!:!'!!~ •. . ("ftn•'•"•• 

,~ IAalOQim Job 1: A8A2964 · · • RAlpatt Oaio: 2lOS/09123 . . . ·:... . 

ENSR ln1ematlonal · 

Client P.rojecll: 1002.()22 . 

Project name: VEOLIA ' 

,RESULTS OF ANALYSES OF CHEMICAL MATERIAL 

. '· 

.. 

•''\ 

·· ··)' 

' 

·Not- .~ Oclodloo u .... 83td\ • Ql..lallity COnft?' 8atd\ 

..... _ • ReporUtAe Ooledion Uml 

- • (Milly C4o'<rol 0-

1813819 

p,g.2d10 . 

VES 004933 
. M -/0 . IM- !y~-..1 · . {'~.<;~., -- -"- "----- -- """"'=~=7="'== 

) 

Mwcicom Job It:: A8A2964 

• Report Oato: l0081()9123 

~ . . 

ENSR lntemafiooat , 

Olent Project II: 1002~22 

Project nama: VEOLIA 

ELeMENTS BY ~TOMIC SPECT!l_OSOOPV (CHEMICAL MATERIAL) 

~ ') 

J 

--(.'.&) nV\. . 160 . 1110 240 

- Bor,1lh.n (Oe) ~ No NO NO 

- cactmiom (C4) or¢. 0.10 0.11 0.16 

OCa1 Cl1o-omum (C<I I1'Q'I. 1600 1400 630 

-~lf'bl mgll 0.58 0.72 2.1 

0 • Not detel:;tad 01. ·---·Uml eao:n • boolly c:or..!-

. 

~ ~·~ '• --(.'.&) mgll 0.04 0.04 NO 

- 6efytllum (Bo) ' NO NO NO 

-· c8dt.lu,. (Cd) mgll O.o04 0.005 0.006 

.,.;, QvooNn (CI) mgll NO NO NO 

-lad(Pb) 

- O.G3. om 0.03 

~;-~ .. -· -- Uml pc ·- • o..lly Criol8""" 

,. 

P>Qo3cfl0 

. . ~ """"S..:.... RoO<!. - ""*"'• c-da L1L 5KT . 

o..o6 0.01 

NO 0006' 

0.003 0.002 

0.000 0.005 

0.03 0.01 

~ RD~ 

1l.OI· 0.0 1 

NO 0011(1 

NO 0.002 

,<).33 o.oos ~ 0 .01 

\814901 

1414!1!)8 

1614900 

181 .. 908 ' 

IG14908 

": ~.., 

1~14906 

!014008 

16141108 

16149Q8 '· 1614900 

.. ~ 

VES 004934 
·.: : .. ·.· ··. . . : . .. . · .... 

. · .·:M a~ft~~.~! -: ------------ ---"---~~--'"'~•~-~,..,.~ .... ~·""!!!~-!!!!!~$!:!"'!!!!!""!!<.. ENSR lnlemallonal 

~ . ;~./ 

Mald:am Jill t: ~ . 

Rt!>ott Dlto; 2008/0!!123 

Cient PrO!«:t 1: 1002.()22 

Project name: VEOl.l#. . . ' . 

ELEMENTS BY ATOMIC·SPECTROSCOPY (CHEMICi'.l MATeRIAl) 

. . · ~Dote . 

Totai-(As) 

~ 

~ 

~ ·0 .03 NO ·tvA • . "'" · o.OI 

. jr .... Bcl)l1ll.w1o (Be) . ongil. NO NO NIA WA .boo$ 

T..,. Cadm.Jum <ci!l ~ NO • 0.002 . )'1/A NIA O.G02 

T .... aw.mo.o (01 rg'L 0.12 0~7 NJA · WA o.oos 

T .... Lud(Pb) mgl\. NO NO NIA . ""' 0.0 1, 

f'doi~-(Ao) ~ NIA NIA $< 90 I 

-~-(Be) oW NIA NIA NO >«> o.s 

--~(Cd) """' ..... ·. NIA.- 200 160 G.3 

-~a-,o,m{Crl """' ·WA "'" 1200 910 0.5 

-eo· · w load <i't>> "fig . NIA NJA ~ ~ I 

H) N4(~. 

NIA No<~e 

~a:~c::v=e':t: 

. .. . .. 

~ lldit ~-(As) uglg 9<\ I 

. /ldd--- ... ·(8e) uglg NO . . 0.5 ' .

·~ • 620332 

. Ell><• .... c:.:tri.om iOlrl uglg 170. 11.3 ,_ . e.s-=-~<Ct! "'IIII 1000 o.s 162C332 

;;a.,'""- Lad (Po) uglg :MO 1 1620332 

·rc ·!l«"--

~-t.mlt ~ ·..:-.. Quai(y ,_ e.cn 

.. 

.. _: .. · "-Gt4ol 10 

. . 5SHotOS-. ~ -Oriorio,~ l7li!K7 

101-4908 

16 ~9011 

1814908 

141<1808 

IGt<IIOi 

jQI)32 

-,z 

11211332 

I&Zn32 

18= 

' 

. . 

VES 004935 
,· 

' 

.. 

.. · . 

. a~a m Drl"*''i~~~ . . -:: . ()?.:-" •• ,., .... ~----:----~--...:'----'----==-===:::,::;:==:. 

; 

.. , 

.. 

·. 

Test S~m ry 

......... 10 1\1.3<36· 

._ 10 HO'ru.U -RI 

Maid:IC CMMk;at MaCirf~ 

-10 AU<$7 

10 HBTU-IJ2.R2 

- a..--

c ......... 

_,..

10 H.3433 

., HOTU-u2-rel 

·- ~·" ·~ 

~ 

. I 

. ENSR l""""'lional 

· Client Ptofed fl: I 002:0ZZ 

Project name: VEOUA 

. Collo<Ud 2Q<leiO!ll(ie 

Shipped . 

Received' 20()&109((1 ... 

COieetod 

,...,.,... 

Re<><iWd -· 

Cd!OC\Od l!008o'l9/10 

......... - -·· 

..... . ' 

.. 

c 

) u.ua.to Al..34<3 Col!oclod 20oMwoe .. $Onoplo 10 l9TU-U2-RI ~ 

......... Chordai.....W •R..o.lv.cl 2001109iu 

. . ....... 

-10 -'1.3«5 

Sample .. I.B'IU.U2-R3 

Mmx Chemical MaiOOat 

Pas,- Sof tO 

Collected 2006/00110 

std""'d 

Reed..., 200810011 I 

VES 004936 
... ·· ., ·' 

. . t0t a C)lft~tr:.-J --'-'-- ;-- ---------=--'- - -"'----"' .... "~=m="'"'-"'='"'= .... =·=""'"='"" 

::-~ .... ; . . · 

.· 

') '•' 

\, ..... 

Test Summary 

Tes.' 

. - 10 . Al.344S.Ilup 

tit)n """"-. 

~:=~ .. · 

-10 AL3447 

~ 10 SF-U:!-& ' 

11atrta Cherioat Ma_... 

- ID AI.34C8 

~ 10 .sf'.U2-4U 

- 0--lal 

~ _., AL3U9 

........ 10 cs.w~· 

-~-

i:: 

-10 111..3449 llup 

Sanopi<IO ~~I 

·MabiJC 

Ctlomool """•""' 

'utruml!l(d.aUtlo" 

IC 

- --R .... -C><odo,"- L7L5H7 

., 

lltdcl\ 

16!3819 

"-go6ott0 

EHSRl.......,_ 

Clio<>! Ptoje<;t t; 1002.()22 

Project name: vaJU\ 

~ 2008109/tO 

Shlppe< 

~d 200e10911 1 

Colledod ~lO 

Shipped 

Rooe!v<>d 3108109NI 

Colkdod 

..._. ~ 

R~ ~ 

~ .. 20fl811)Q.<l8 

Sl!l-" 

Received 2008109111 

E•- 2006/09115 

~ 

VES 004937 
' . 

.... f •• '• 

M a 'fJ.l.:;;J,T. ___ _: __ ....:..._....:.... ___ _ _;__....:...__....:...__:_ _ _: _ _,.,.!!!~'l-:!~·!l•:.:s.~-~.!:0-~ .. !:!'~·~ 

.· 

lolw<amiO 111.3450 

-10 CS.U2·R2 

Matrix ~ Ml'tortal 

Test Summaty 

P11!107otl0 

EHSRil1!ema!lonal 

CGonl Pn>ject f; 1002.o22 

P.mject name; VEOUA 

.,.,.,_ 200Ml!IIIO 

--· 

-

·. 

'• 

. 

' 

VES 004938 
... 

· .. M ct ..r<i ·····...::... ·' .:.._ ·· · --~-......:~-~-_.:.------.....!!.-!;-~ ... !Z..:!:-==--~ · ~.,~w~~~ · :, ~ ... ,Y"tlcoa-

. . : . ~ . .... : ·.· . ;''. 

., R ............ orolyrto fNU•""te"..j· 

. ··-:-, 

; .J ...... 

.. 

.; ... ·· 

GENERAL COMII£HfS 

'· 

~ 

Pago8ol10 

EtlSR~ 

Cten1 Proji>c;t 1: 1002422 

Pro)ec:t name: VEOI..IA 

VES 004939 
.. .. !) . ,, 

.. ' 

·. 

') 

te1cgoe KCO 

S!>I*!Blri 

--

RPO' 

111203321(0) MA'!'fliX'SPI<E 

. oc &fAJ<l)AAJ) 

--

• Not delld&d 

• Non.cot.Jiablt 

• Relatile Perooot OW ..-.nee 

ENSR_,.tlonal 

Allllnbl: Je•'f Go<mon 

Clent Project*: 1002.()22 

P.O.#: 

Pnljecl name: VEOI..IA 

Quali'Y A:lsuro.nCA! Report. -Job -0 GA8A2964' 

2CICIM)Qit6 

20081ll?f16 

T--{o'$} :200810!1116 0.53 . 108 

T .... _(Bo) 2008109116 G..54 108 

ToOai~(Cd) ·. 2D08.'1WI6 0.53 105 

Total aw.mu. fC<I 2COU)9/16 Cl.53 105 

T .... lsad(Pb) 2001i/oo11G O.SI un T""'-~l 20081011116 0.51 102 

T .... ~('llo) -· 0.53 100 

ToOl! Ood<NIM:n (Cd) 

-~· 0.53 105 

Tolai~"'(C<) ~ 0.52 103 

Total Lead (R>) 200MJ9/16 <152 103 

Total -~) 2008109116 Nil. ROI.=O.OI 

. T otalller)4ium (Be) :aioe.~ .• NO. ROI.<0.0005 

Total Cadmkom (Cd) ~~· NO, ROL.0..002 

T-Ct1<om1um (C<) 2008109116 NO. Rlll.-<1.005 

T .... J.,ood~l 2000/o9116 NO. Rll~-<1 01 

Totol........,(l\s) 200Ml911G NC 

Totallle<\4llum (Be) 2ll08109116 we 

Total m (Cdl 2008100/JG NC 

T-CM>ri ... (C<) 2001110WI6 'NC 

·Total tad (l'b) 2008109/IG .NC 

Jodd - AioMic(M) ~ 0.50 100 

- - Bo!)ll""' (Bo) 200Ml9t22 o.sz 104 

l<idEn-Codoium(Cd) 2IXI6I09I22 o...a· 98 

~odd-Clwonium (C<) . 2008109122 OA9 1111 

Add~ t.eod (l'b) ~ D.<8 1111 

.lrrdd Ext:! 1 " Ntedtc(M) 20ClMl9l22 O.a4 95 

hJdEd 1'*'~(01 alOOI09I22 f).29 811 

- E>ol-lsad (l'b} -..m 1.3 . 95 ----!"") 2IXIli09l22 II>. ROI.q ---('llo} 2QOS•m II>. ROI.oO.S 

· Add Exo-~(Cd) 200&09t22 NO, Rlll<jj.3 --a...nu. (()') ~ tO. ROl:.aO.S 

Add-LNd lOOei09I22 RJ)Uoc1 

eo.-Slru)daro 

san-e>~• 

Pago9oll0 

This ~ Is In eledfonlc format, hW COpy i$ ava~ 01'\ ~eat. 

2j) 

~ 76·12S 

~ 7S-12S 

"'D\. 75.125 

"'0\. 75- 1.25 

mglt. 75 - 125 

·~ eo-t26 

~ 78 · 119 

~ 75 .. ·111 

mgll 75· 

mgll 76-1 ' . If¢ 

mgn... 

"''l"-

"''l"-

': mg/L 

% 2S 

'14 25 

'14 2S 

'14 25 

" 2S 

ug(g 75 ·125 

uglg 15 . i2S 

uotv 75· 125 

75-1.25 

75· 125 

T$ - 12:S 

75 . 125 

75- 125 

6665-S..W.R .... ._Ontorio,""-'>. l7l6117 Tol: (005)3.SN788 oll .-.-:(800)~39 Fox:(liOS)332.0160 

VES 004940 
: 

: 

) Validation Signature Page 

l\laxxani Job t: A8A2964. 

·· ·· .. . . .. 

PI!A.NK MO, a .Sc., lOOQIUlic ~- Maoascc 

Pago 10 ot IG 

VES 004941 
5015 Cempuswood Or 

Suite 104 • 

East Syracuse, NY • 

USA 13057-4232 

Semple Mattix: LIQUID 

# Sample• Rocelvod: 9 

Semple Mat~x: SOi. 

# S~los Received: 3 . 

Sample t.totruc: Willer 

II Semplos RoceMocl: 3 

MAXXAMANAL YTICS 

Your Project#: 1002..022 

Slte:VEOUA . 

Report D'"o: 2008111/1' 

This roportsupemedos all previous reporis ,.;(h the samo Maxxam job number 

CERTIFICATE OF ANALYSIS 

9 

0 

CAMSOP-63 

2008/0enG 2008108120 CM1 SOP.Q0408 

TOC81 oowr pag6S: 1 

EPA 7470 

EPA 6010C 

VES 004942 
t.Aa>OIM1 Job II: A89164& 

Report Dolt! :i008/11/1' 

e,ISR f-ional 

al..,t Project lt. 1 002-022 

f'T<Ijecl name: VEOLIA 

RESULTS OF ANALYSES OF LIQUID 

=:<Cil . I." I ... , .... 

c NoC detec:t.d 

~0-fonUm .. 

BM<~> • ~ c.nno 11o1c:1> 

.01 1591002 

. ' 

. . 

VES 004943 
EHSR lntemotional 

M""""m J>b II: A891848 

Report Dell : 2008111114 

Clienl Profect #; 1 002.o22 

Project namo: VEOUA 

ELEMENTS BY ATOMIC SPECTROSCOPY (LIQUID) 

: % ~ · 01111-(M) mgll 12 11 17 0.6 0.5 0.1 1!591m 

.... Bo<yllum (Bo) mgll NO NO NO 0.03 NO O.ll05 11!01852 

O'.aiC-!Cd) mgll 0.1 0.1 0.1 0.1 0.1)4 '0.<12 11581852 

..., CMlmlum (c.j ....... ••• . .1 4.1 0.3 0.39 0.115 15111852 

...,IAaci(Pb) mgll 1.4 1.3 1.1 0.5 .., 0.1 19Gies2 

!Hol ' mgll o.oflio 111 o'A43(1) o.ooooro p .OOIS o.aoee ~ b.oo~s 1-

~ • Not dolecOOd 

~:~Pe!e<Dcn t.ml ~~Belch • CluiallY Conlrol Ba.m 

I) Duelo""'-- oomplon>q'*-ddG-.. DolodiOni.,. __ -~· 2 ). ~ boflfe~cd Ytebo ~ s.,... ..._. lll'lll*tn to ob4• repre$et1l36Ve aliquot. RaaAta m~~y bol>l- hlghduoiO __ .. _ . . . 

~ 

TotolArocric(As) mg.\. 0.2 0.2 0.1 NO 0.1 1601052 

dol B..,...., (Bo) mgll NO NO 0.005 NO .005 1501852 

.... ~(Cd) mgll • ND NO ·o.02 NO 0.02 1501~ 

ota1 c-.. (Cr) mgll 0.12 0.05 0.1)6 NO 0.05 159\852 

OOollal!d (l'b). mgll NO NO 0.1 00 0.1 1591652 

!>19) .. mgll 0.0018(1) ND(O 15' 0.141 := 15S256) 

... 

VES 004944 
MalOllll!l Jcb ft. A89164S 

Report Dolt: 200811 1114 

• 

ENSR lntel'llOlionol 

Client Plt;ject t: 1 002.Q22 

Proj<!cl name: VEOI.IA 

ELEMENTS BY ATOMIC SPECTROSCOPY -(LIQUID) 

NO NO NO 0.1 1591852 

NO NO 14) 0.005 15~1852 

Otal Codrrllm {Cd) NO NO "" 0.(12 1601852 

0181 CMxrUn (c.j 0.22 0.11 0.18 O.ll$ 15eles2 

.... Looll F.I>J • 

,_ • NO NO 14) 0.1 159\862 

~ 

- O.OOGO O.OOIIZ HIA 15 1-

·Not~ 

'A•Nct~ 

e ~ Oetedi'onl.tnll 

"""' • Qusllly ()oatr<JI-

. . 

·. 

. , 

.• 

" 1". 

· 

. . 

VES 004945 
·, 

~ ~~~ ~---------------------------------------------------~~~--~~ .. ~~~·~W.~·~--~~$~~~-~~~ ~""'""·· Mo-m .kb II: A89164a 

Report De": 2008111/14 

ENSR lntemalf<>nal 

Client Projecl #: 1002-022 

Project name: VEOUA 

RESULTS OF ANALYSES OF SOIL 

so~O~I.IMR 

B- Qopll!y~-

.· 

~-

VES 004946 
ENSR Int ernational 

Client Project #: 1002-022 

Project name: VEOUA 

Maxxam Job #: A891648 

Report D21B: 2008/11/14 

This report supersed~ ell previous reports with the samo Maxxam job number 

RESULTS OF ANALYSES OF CHEMICAL MATERIAL 

NO= Notdetecled 

ROL c Reporiable Dei!J<'~Ion Limit 

QC Bach = Quality Control Batch 

• '' I 

,. 

VES 004947 
Maxxam Job II: A891648 

Report Dale: 2008/11114 

~ .' . 

ENSR intemotional 

Client Project #: 1 002-022 

Project name: VEO~IA 

·ELEMENTS BY ATOMIC SPECTROSCOPY (WATER) 

• Rep¢1'13bte Dete<:tion Umlt 

!!""" • Quafty Cot<rol Batdl 

.. . 

·.· 

VES 004948 
... 

~ <3 ~~ n• ••"u rYl--------------------------------------------------~ .. ~~~~·~r~=:==~·=·~J~$~~~~~ 

Maxxom JoC> • : A891648 

R090n Dolo: 2008111114 

llaxxam ID AF7333 

Sampi•IO HOW·~·l1t 

Ml'trix LIOU10 

. ........ Ill AF7335 ·. SamP'•ID HDlU..W,.R3 

Matrt~~; UQUIO 

Maxx&Jn iD AF1337 

Sampie ID t.Ol\.HJ2-ft2 

Mwtit I.IOUIO 

Tost Summary 

ENSRinCUent Project#: 1002-022 

Project """"'' VI:OUA 

CoMeot.d 200010811 1 

Shipped 

R,uaiYed 2008108/14 

VES 004949 
M a Aa ~.,,. hl.- .. , c·$ ~-------- ----- --~..........,== .. ....,,...,....,~-'=:!·"'~~

MalaAm Job "A89164ll 

Report Oo.o: 2008111/14 

Mmcam 10 AF7338 

.o~. ~pie 10 LBTU-tll·R3 

MatrrX UOUIO 

. .._.,ID N'n38 

-ID 51412-<t1 

- LIQU1D 

....X...IP AF7340 

s.,.,a. iD SF-U2.R2' 

. MatJfx LIOUlO 

Mlloca• ID AF7U1 

. Sample ID SF-112-R3 _,. UOOID 

Maxxam 10 AF7342 

Somple 10 CS-U2-I\1 

- S<lil 

Toat Summary 

., 

ENSR lnlemOiioroi 

Clent f'l1ljed #: 1()02-022 

Project name: VEOLIA • 

Colloolod 2008W13 

Ship .... Recetwd 2008108114 

Coll-d 20oaJoai12 

Sl>..,..d . 

~eeMd 20~4 

VES 004950 
MBJOCam Job 1: AS91648 

Ropo~ O.lo: 2008fl1114 

M.axxam 10 AF7342 Oup 

.S;ompk 10 S·~1 

U:etrfl( Sol 

~ID AF7343 

-10 CS.W-R2 

- Sol ... 

Manem ro AF7345 

- 10 llS-U2-R1 

""""' -

_,., _ - ID lo&\.I2-R2 --

lllxxamiO N'7347 

Sam,lle 10 . M&-li2-R3 

Matrix Watot 

Teet Summary 

ENSRtntematlonal 

Client PYo!ect II: 1002-02:2 

Projeol nMle: VEOLIA 

Colfcde:d 200810811$ 

$hlppod 

Rouivc<l 200MlS/14 

VES 004951 
ENSR lrumafional 

.Moxxam Jot> #: All91848 

Roport Ooto: 200811 1M4 

CIGnt Pmject #: 1002-o22 

Project name: VEOt.IA 

AFT3a:l-0 ~ Motals Ana!V*: Ooo to ll8 pitt mtJtttlc, a~ttnt a roquimd ditUtlon. Oeied.lon flmM.s we~ tlld,luAed aaoon:llngly. 

Sample AF733~1: Motab. ~ Due to ttte ttmple melrlx. tD!l$1t roq~t:d dlkldon. Detedion Dlllllls were adjustGd 8CX'.ordlngly. 

S.lfllllo Wl331>01: Mdals Anal\'$1s: Duo to,.''"""" molllx. ....... .....,.., dlluilon. ~limb_. adp.!ad aatordlngly. 

9ln'CR Af7338-01: MeW.- Cue to~-·-· --oddLClon.Oe ___ o....,olod"""'ca"'. 

' -.... N'7337-<>1:-.Mol/* 0... to ... """4"0- <ompiO ""f.lbd-.--waroodjullld . 

' • . . . l . • 

AF7338-0I:,__ O...toh---~-Oolocllan--o..--dto,. 

N'733!W1:_A_ l»>tol\oiaqoo __ ..... _Oo-. __ ..........,, '*">· 

8ompo ~=--_, .......... ----0.~--......... .... ,. 

Sorrc:lo A/.'73<41.01: NsOals Analysis: Duo toltle...,.,.. ..-.. ,.... ~wod -· o...-.lniit.,.... ..,_ -lngly. 

to tbelton. tosled. 

. . 

' 

•! 

:b 

VES 004952 
• 

'M a v</~ ~ -- ------------ --~Drl!!a-~.s!.:.·.s~·!!""!!!!!"" '~m~J-2$~"'!!-~-~· i!"'~e.)I~I.C.t 

ONOC 

8-

.;:~ lnll or. ~o 

1591002 UE QCSTANOAAD 

S!>bd 810llk 

--. RPO •. 1591852 ~co MA TRDC SPII<E 

(AI'T341) 

ChlcWide{CI} 

Chlc<ld• {CI) 

Chloride (CO 

Ch1Dl1d• {CI} 

ENSR fntematlonat 

Altenlion: Jeff Gorman 

Client Project II: 1002·022 

P.O. fl.: 

Pnlject name: VEOUA 

Quanty Assurance Report ..• ..._Job H..-r. OA891&43 

oalo .. Analy.ted w.,. ,.....,. ,..;. 

2001!106121 o.oo._~lo0.01 ·as 

2008100121 99. RllloO.OS 99 

2008IOen1 0.008. ROLoO.OOS 

.2008101!121 0.5 

ToisiA<-(Ao;) 2008108120 0.0 0~) 

.. . :~ •. · . Tolsl 8Wy'lbn {llo) 2008/08120 OM . ; ~ 

Total CO<! .... (Cd) 2008108120 0.45 ' .. . TOI.ol Ctvo ..... (C~ 2008108120 0.43 85 

Tolal Lud (Pb) . 2008J08120 0.44 87 

SpU<o<tBI""" · .TotaJAisonlo(As) 2008108120 0.49 lfl . TotaJ Oetyl'..., (8e) 2008108/20 0.51 ~ 101 

TotaJ Cadmium (Cd) 2008'08120 . 0.51. · 101 

T..., Clltomlum (Cr)· 2008/08120 0110 99 

TOIJI L~od {Pb) 21106108120 0.49 98. 

. . Md>od Bllinl< Tolal Menlo (As) 200e/08I20 NO; RDL=O.ot . 

Tolslll«yyliiJm (Do) ~ 110 •. ROL.O.ooos 

Total Codmlum (Cd). 2008108120 . NO, ROL"!)-002 

Total Ctlfomium (Cr) 2008108120 · NO, ROL-o.oDS . 

T ooall .... (l't> l 2006108120 .NO. ROL<0.01 

RPO TOI.ol-(As) . • 2006108120 NC 

Tolali3efyllkttn (Be) :2.0060)8/20 NC 

Toto! Cadobn (Cd) 2008.'06120 NC 

TOIOI Chroml\m (~ 2Q08I08I2Il ~c 

Tolslload(Pb) 2008106120 N(! : 

15$2290 .KCO ft.!ATI\t)< S.PI<E -~-(Ao) 2008108121 0.44 88 

- EJdrattolllo &o<yllum (8e) 2006108/21 0.41 82 

- E><lnldollle CodmkJm (Od) 2008108/21 OAO. 80 

· Add Em><Aable Ch........, (Cr)' 2.<l06.'Jtl/21 0-43 85 

u ..... 

% 

" % 

-.: " 

mgll. 

~ 

.,giL 

mgiL 

<ngiL 

mg/1.. 

mg/1.. 

mgll 

mgiL 

mg/1. . 

mgiL 

mg/1.. 

mg/L 

mg/L 

mgll. 

% 

% 

% . 

% 

" ugtg 

uglg 

uglg 

ug/g 

--Leod(Pb) 2.00eioel21 HC ..• NC (II ug/g 

QC STANOARO . Add El<1n1<:18blo A<senlc ("') . . 2008J08/21 . 0.77 88 Ul>'9 

Add El<lnldsblo ~ (C<) 2008108121 0.30 91 Oglg 

; Add El<lnldsblo Lead (l'b) 20081081'2i ·1.2 .. uglg 

~Blank -~-(As) 2006/08121 NO, RDL=1 ugtg 

Acid Ex1ractabOo Bcrylk.m (Be) 2008108121 NO, RDL=0-5 · uglg 

· Add Ertadable CO<tmiuia (Cd} 2.008.<)8121 NO, ROL=0.3 ug/g 

AddExndableC-{C<) 2008108121 NO. RDL=0.5 Oglg 

Add EXI<odablo Loed (PI>) . 2008Al6121 NO. RQI.o1 uglg 

RPO. Add """lldoblo Lood {l't>) 2008Al6121 23.6 . % 

159<2563 SUK ·MATRIX SPIKE >lc«>My (Hg) . . 200810e121 0.0230 92 mWL 

Splkod. Blank •""'"Y {Hg) 2008/08121 0.0263 lOS mgiL 

Me!llo<I.B- -(Hg) 2008108121 NO, ROLoO.Q001 . mg/1.. 

' ljPO MercuiY (Hg) 2008/08121 · NC % 

1592587 NC MATRIX SPIKE Add -bio "'"""'"' (llg) 2000108121 0.570 114 tog/g 

-QC STANDARD AddEl<OodableMo""''Y~ 2CI<lMl8/21 0.305 109 uufg 

~- ~ :"'"""ble Meouy (Hg) 2008oll8/21 ND. RDloO.OS 

Exltlldllblo M NC ~ 

Hotdotec<ad 

~~ • tfon.calculabttl 

~t-=- Retative Peroeot Difference . S!andsrd • 0\.laMy Control Standen:! 

SPI!<E • Falllled nmpe · 

.. 

1 ) The fei:XNCfy W&$ belOw the ~ control knit This may represent a low ~ in torno NIOt.IRs for thle: eped6c: analy($ .. 2 ) The ~ tn the msb1x spike was not calcdated (J.IC). Because oll19 hlgh conctOntion of this sll3lyte in tho parehl sample, thG 

QCLNIA 

80- 120 

.. , ... 20 

75 ; 125 

75-125 

75-125 

75-125 

75-125 

so·. 125 

76. t19 

75:117 

. 75-125 

78 - 119 

25 

25' 

25 

25 

25 '75·125 

75-125 

75- 125 

75 - 125 

75-.125 

75 · 125· 

75. ·125 

7S -125 

35' 

75 - 125 .

84 - 113 

25 

7& ·125• 

75-125 

35 

VES 004953 
' 

ENSR lntcrna~lonal 

Altl!nllon: Jeff Gorman 

0""'1 Project II: t002A)22 

P.O. II: 

Project name: vEOLIA 

QuaiRy Assuranoe Report (Continued) 

· M•~m Job NurnbM: GA091648 

,. 

). 

· . 

.. . 

!-

VES 004954 
Validation Signature Page 

Mannm J ob 1t. A891648 

Tho onal)'1lctl data and all QC contained in this repon wcro rcviowtd aDd valida...S by the fullowine indiviclual(s) . 

. ,· -. . . . . 

. · 

•' 

VES 004955 
. ·. 

I . : 

·Attentioni Jeff Gonnan 

ENSR International 

; 5015 CampuswoOd Dr 

' Suite 104 . 

East Syra<:uso, NY 

USA 13057-4232 

Your Project#: 1002.022 

Sile:VEOLIA 

· · ROliort.Date: 2008111/14 

This report "'!P•rsedes. 811 preVIouS ·reports With lhe same Maxx8ni job number ' 

Sampie !,latrix: Chemical Material · 

# SemplesRecelvGd:·12 

CERTIFICATE OF ANALYSIS 

1 ' . 

(I) Ma>oorn """"""' dOOa nolhl>ld - lion lor~ ofmelala -~uslng ... ICP Aldol met._.: · · ' ' .. ' 

· . . · . 

T olal cover P'!QOS! 1 

VES 004956 
Maxxam Job 8: A8A2964 

Report Dll .. : ~11114 

ENSR lntemallonal 

Client Projoct IF. 1002~22 

. Project name: VEOLIA 

RESULTS OF ANALYSES OF CHEMICAL MATERIAL 

D= Not-0<1 

-~· 

l • Rt()Ot1ablt 0etocUon Limit 

- • quol1ty Coolrolllaleh 

16131519 

1613819 

;· 

. l 

VES 004957 
Maxxam Job #; A8A2964 

Report Date: 2008/11/14 

ENSR ln<emational 

Clienl Pro(ed #: 1002-022 

Projecr name: VEOLIA 

ELEMENTS BY ATOMIC SPECTROSCOPY (CHEMICAL MATERIAL) 

~ 

Olal Arunlc (As) mg/L 160 160 240 0.()6 . 0.01 

""" 8olyillwn (Be) mgiL NO NO NO NO 0.0005 

ooai~ (Cd) mg/1. 0.10 0. 11 0.16 0.000 0.002 

otol Ctiomitan (Cf) mgiL 1,.. ' 1400 . 6SO 0 .006 0.005 

oblllead (Pb) mgiL O.M 0.72 2.1 ' 0.03 0.01 

ND=Notdote<Oed 

;,1 

ROL • Reportllble Oefedion .Uni 

c Bo.loch • Quality .Coflb'of Batch 

TCO>I A,..nK,-(As) mgiL 0.04 . 0.0< NO 0.91 0.01 . 

.... Bel)lbn (Be) mgiL NO NO NO NO .ooo5 

ctat~(Cd . mg/1. 0.004 . 0.005 o.ooe NO 0.002. 

Olal ctwmlum (C<) mgiL .. NO · NO ND 1>.33 0.006 . 

TOOII ~ (Pb) . mgiL 0 .03 0.03 .o-03 NO . O.Ot 

=NcC doiadod = _...Doloctlon Umil 

BatCh ~ Cor.trcl Bak:b 

·• 

161-4908 

1614908 

16149Q8 

16,14808 

1614906 

1614901l 

1614908 

1614908 

1.614908 

1614~ 

VES 004958 
ENSR lntemaliol1al 

. CHent Project#: 1002-022 

Project name: VEOUA 

Maxxam Job #: A8A2964 

Report Date: 2008111/14 

This roponsupersedes all prev1ous reports wilh !he :.arne Maxxamjob•nunt>e< 

ELfMENTS BY ATOMIC SPECTROSCOPY (CHEMICAL MATERIAL) 

;-

Maloalm 10 AL3436 AL3437 AL3438 AL3443 AL3444 AL3445 AL3445 

Sarno! ina Date . 0910312008 '09m9/2008 09/1012008 0910812008 0910912008 09/1012008 09/1012008 

Units HBTU·U2-R1 HBTU-U2-R2 HBTU-U2-R3 LBTU-U2-R1 LBTU-U2-R2 LBTU-U2-R3 LBTU-U2·R3 Lab-Oup I 

Total At<enic lAs) maiL 160 160 240 . 0.00 0.04 · 0.04 NO 

Total BerviUuniTBe mQ NO NO NO' NO NO NO NO 

Totei Codmium (Cd moL · 0.10 0.1 1 0.16 0.003 · · 0.004 0.005 0.008 

Total Chromium (Cr . mg L 1500 . 1400 630 0.006 NO . ND · NO 

Total Lead (Pb) rng/l. 0.58 _ 0.72 2.1 O.O_L • . Q.O~ 0.03 0.03 

~ ~ 

!ACid 

NO m Not detected 

NIA • Not Applicable 

~ !!!._ 

~ I= 

I: 

RDL " Reportable Detection limit . 

Lab-Oup " Laborato<y lnltlated Duplicate 

QC Batch a Quality Control Batch 

N/A 

N/A 

N/A 

N/A 

~ 

N/A· 

N/A 

· NJA 

NiA 

N/A 

.N/A N/A lA N/A 

• 

/A 

;;: 

'A 

'A 

VES 004959 
ENSR International 

alent Project#: 1002.c.22 

Project neme: VEOUA 

Maxxam Job ft. A8A2964 

Report Date: 2008/11/14 

This report supersedes au previous reports with the same Mexxam job number 

ELEMENTS BY ATOMIC SPECTROSCOPY (CHEMICAL MAT!RIAL) 

' 

Maxxam 10 AL3446 Al3447 AL3448 Al3449 Al3450 AL3451 

Sampling Date 09/08/2008 09/0912008 09/10/2008 09/0812008 09/0912008 09/1012008 · · 

Units SF-U2-R1 SF.U2-R2 SF-U2-R3 CS.U2-R1 CS.U2·R2 CS.U2.-R3 ROL QC Batch 

Total Arsonic !Asl . mQ/L 0.01 0.03 NO N/A NIA N/A 0.01 1614908 

To:al ~llum {Be mg/1. NO NO NO NIA NfA NIA 0.0005 1614908 

Total cadmium (Cd mg/L NO NO 0.002 N/A NIA NIA 0.002 1614908 

Totlll Chromium CCr I mQil · 0.33 · 0.12 0.37 NIA NfA 'NIA 0.005 1614908 

Total Lead (Pb) I tW1- NO NO NO· NIA N/A N/A 0.01 1614908 

Acid Extraclable Arsenic lAs! ' 11!1 N/A N/A NfA 32.6 28.3 31.1 1 1620332 

Acid Extractable BeiVIUum !Be ua N/A N/A · NfA NO NO NO 0.2 1620332 

Acid Exlractable Cedmium (Cd ug'g N/A NfA N/A 69.4 50.2 58.7 0.3 1620332 

Acid Extractable ChromiLm CCrl ~·g N/A N/A 'N/A 416 305 345 0.5 1620332 

Acid Extractable LeadjPb) lll!Q N/A. N/A NIA 1tl . ·75A 8l.8 1 1620332 

VES 004960 
' . 

Maxxam Job 1: A8A2964 

Flepo<t O.:a: 200S/11/14 

MaxxamiO 

SampleiO 

Mattix 

AIM36 

~=::etiat 

T •.st Summary 

M8xkemlri AU437 

SanwleiO H8TlJ.U2-R2 : . • N.atrlx Cheri:al Ma l 

-10 AL3438 

SamoleiD H91\!·U2-R3 . 

Natr1x ChcM'cal Mato~ 

l.lalocam 10 AL3443 

Sample lD .LBTU-U2-R1 . 

. lrlattlx Chemical Ma~lal 

MaxiumiO. Al.3#1 

~pie tp l.BTI:J.V2-R2 

- Cllomica! Malorl .. 

...,.....,0 AL3-«6 . 

Sampi• 1D i.lmJ.u2-R3 

Nn1»e Chcwrieol M~ ie.! 

Ei'ISR International 

Clenl Project#: 1002-022 

Projed namo: VEO~IA 

Collected 

"'!!pped 

......... 

•l 

Cofloded 2008J09I109 · Shipped 

Recei'Vod 2008109111 

collected 2008.109110 

Shlppod ' 

Reodvul 2008.09111 

COI'-c:led 20(l6.()9fOg 

ReuiV'td ·-d2008109111. 

CoUoe\Od 2C108!109110 

ShipPed 

R4W;elved 2008J09,'11 

VES 004961 
Maxxwn .btl II: A8A2964 

Report O.>t: 2008/11114 

hlaxxamiD N.3445 0Up 

Samp1o 10 LBTU.If2·R3 

Matrix Cb!"*:t.l IMtoMI 

- ·10 Al.3440 

S..plo ll SF-U2~1 

Test Sum~ry 

-~-.... 

lblrxam ID Al.34.C7 

-10 SF-U2~ 

o.c ............. , 

Maxxam ID Al.34-48 ' semp~. ID SF-U2-R3 

M&trt. ~C'Imlc:al Matetltl 

MuxamJO Al3449 

Salnpe.IO CS.U2·RI . 

Mdr'bl OMmlcll J.\a1etlll . 

Mmcut 0 At.34C9 Oup 

5ampt6P CS.O~fU 

Mallb: ctMtnical Material 

ENSRinlema:lonal 

Clenl Project II: 1002-()22 

• PO'CjeCI name: IIEOLLA 

Collected 2008J09110 

Shipped 

~cckred 2006109111 

eo•- 2000/0WIO Shil>pod 

Re«lwd 20CitlJ0Qi1 ; 

.·. 

VES 004962 
_. Job , , A8A2964 

R.o!>o<t o•: 2008/11/14 

Ma1001m fO AL3450 

S>onpje ID C$-U2·fl2 

Matrix Cbemlcal M~turial 

Ma:ltan't"ttt ALM51 

SUoplelD CS.U2-& 

Tost Summery 

.. 

. - Clwrieal M-

. . . . . 

···"' 

ENSR lntemalional 

Cfienl Project#: 1002.022 

Project name: IIEOI.IA 

Cob..::ted 2008109t\l9 

Shlpp• d 

Reeelved 21108109/11 

Colec:ted 

_. 

200!W!V10 

- -1 

,· 

VES 004963 
Maxxam .bb H: A8A2964 

Report Dale: 21108/1 1/14 

I uu ~ntawonWfo~-·~·• GENJtRAL COMJIEtlTS 

,; 

. .. 

ENSR lntemoUorial 

Client PfOjecl #: 1002.022 

Project name: VEOliA 

.. . 

VES 004964 
1&1<4908 KCO 

,Spll<od Bionic 

MelhodRPD 

1620332 'KCO IM !UX~KE . 

QCST;ANOAAo 

MShod Blank 

ENSR lntomational 

Attention; Jell GO<man 

Cilcfll Project lt. 1002.022 

P.O.II: 

Project name: VEOUA 

Qua!i1y Assurance RepOrt 

Maxxam Job Number. GA8A2964 

200Ml9/!6 99. 99 

2008100116 ti!D, RDL-0.005 

2008/09116 4.1 . 

• TOiaiAIHnlc(As) 2008109/15 0.53 106 

TOOai ~-(Be) 2008/09116 ' 0.54 '105 

.TOial CoOmlum (Cd) . 2008109/16 0.53 105 

To<ol Chl1lmium (C~ 200tW9/16 0.53 105 

Total Lcod (1'0) 200MMII16 0.51 102 

Total Afl¢ftic (As) 2000109116 0.61 102 

Totai (Be)' 200&.109118 0.63 106 

Totalc-(Cd) 2006109116 0.53 105 

Tolll Ckon'ium (Cr) 2006/()g/18 0.62 103 

TQUilead (Pb) 2008109116 0.5;2 103 

To<al"'"""c (As) 200el09118 NO, RDLuO.ot 

Tobl Bet)11um (S.) . 2008109116 NO, RDLoll.OOOS · 

T «a1 C.adn'lium (Cd) -·· ND, Rtll.u0.002 . 

Total Clllom'""' (Cr) 2008/09118 NO, RDLo0.005 

Tolal Load (l't>) 20011109/16 NO, RDL•0.01 

TotoiAroenlc(/\o) 2006/09118 • NC 

Total Be!l'lliom (8e) 2006/09116 • NC 

TotaiCootrlun (C<I) 200610!l116 He 

T0181 Cluomltrn (Cr) 2(1()W()9J16 NC 

To<al Leed (Pb) 2008109/16 NC 

.tdd Ell.~ Arsenic (M) .. 2.008100122 0.50 100 

Add Eld-ll«yUitim (Sa ) 200e/Oaf22 0.52 104 

- Eld-Cadmium (C<I) 20011109122 0.48 96 

lod6 ~Cilrom um(~ 

~ OA9 98· . Acid E!draclable leod (PbY OA8 96 

Add £xtt8!ctabie Af'S.Iri: (A!) 2006109122 0.84. 95 

Acid &b'sctable etwunium (Cr). 2006I09J22 0.29 89·. 

Acid ble l oad (Fb) 2008100/22 1.3 96 Add"""'--(As) . 2<100109122 NO, RlJI.o1 

Add~ BG~yllium (Ber 2008109122 NO, RDlcO.S 

Add Exlnl<l-CadmiUn (Cd) 2008109122 NO, RDL.o0.3 · 

Add -Chr-(Cr)' . 2008109122 RDUo05 

. - E><lrad- . RDL• 1 

.% 80 · 120 

% ' 

% ,. 20 

mg.\. 75·125 

mgll • 7.5 ·1125 

mg.\. 75 -.125 

mg.\. 75· 125 

mgll 75 - 125 

mgll . 80 · 126 

mgll 76 ·119 

mg/1., '76 ·1 17 

mgll. 75 .. 125 

mgll 76 . 119 

II¢ 

II¢ 

mgll 

mgll 

mgll 

% 25 

% 25 

% 26 

% 25 

% 2S 

75·125 

75·126 

75· 'i2S 

7S· 126 

. 75-125 

75·125 

75-125 ' 

76·125 

VES 004965 
Validation Signature Page 

Maxxam J ob 1: A8A2964 

The aoalyticlli data and all QC OODIOined in Ibis rcpott WC<C reviewed and validated by tire fuiJowing iodividuai(S). 

.. '.J~ 

. ": · 

Scientific SpeCialist 

' . 

Mf)UM)haa~bip~topar4~i,.oporu.e 0rtho dedronk~N!4hvod»ftlqUi«d ••ip6~,upar~s.t0.2ot 

.JsOil&C 1'7025:2tflS(S). ·~~ tbert9.0fU.. SCCMd CALA havc-f41Pt0Yed ~ ptOCC8S .nd ~-report fbmut. ., . 

.. 

. .. 

: 

VES 004966 
VES 004967 .pdf 
UNIT3 

VES 004967 
Waste Feed Results 

' 

-

' 

... 

. . 

·. 

VES 004968 
M. . a .. am 

Attention: Jeff Gormad 

ENSR International 

5015 CampuswoOd Dr . 

. Suite 104 

Syracude, NY . 

USA 13057-4232 

Your Project#: 1002-022 

~ite: Veoi.la 

Report Dale: 2008/12102 

CERTIFICATE OF ANALYSIS 

MAXXAM'JOB#: A889378, A891648 & A8A2964 

Received: 

Saiuple Matrix: soild 

# Samples Received: 9 

Analyses 

Moisture Dctenftinatlon 

Date 

Quantity Extrileted 

9 N/A 

Date 

Analyzed 

ttnonoos 

LabOratory 

Method 

• RPD's calculate<! using raw dala. The roundins of final =ulrs may result in the appml difference. 

·~4r:....-.' '· __,.,..,..... ' ....,...., .,;; Ji~~ ... 

. . . 

Mike Challis 

Customer Service Manager 

MlllOOm Analytics Inc. · 

Burlington 

Method 

Reference 

VES 004969 
Confldem

iN: MIXXam AnaJyb &nttmatfonat Page 1 or1 

VES 004970 
~ 

} 

() 

1!!!!!!1-- .:llliiliiiil tyste!M ~~). u.c 

ifleg-... Ot .HO.fleld ... '?'«) 

(1d)21 S82U99<S ((c,)21 5-822-1 'lJJ3 Certifieate of Analytical Results 

CLrEtiT: Maium Aaalytlial Servi«S 

. ·ssss No..,.·S<Mc<ll.d 

florliacto,;_ OotoJio· L7L SK7 

Lab 0.-dcr. R08010020 

·Projt«: A889371 

·AO&l)'S<S As Re«ivedlluis Dry Basis Ual.ts 

W3l3-4l!!, \ ~'i-U3-I.Y. LabiD: M1080020'-0IA 

Date Sa~ 08/0SI2008 o ... tue<l .. d:· 08114/lOOI 

PERCENT MOISTURE 

Moisture, TotaJ 75.1 ... ASH. COAL 

""" •8.52 ~u .. fleA11NG V.AL\IE; COAL 

tk»ting Value· 15«1 6.2-70 · ....... ,. 

AE0!4-0l!!~Q.! Y3-~ . IAbiD: ROI080020-02A 

o ... s~: 0810712008 Date ltcc.c::i¥e4..: 01!114120~8 

PEf<CENT MOISTURE. 

o;s.~. Total 71.5 

.ASH, COAL 

..... 9.80 

. -HEATING VALUE. COAL 

-Value 161!0 

< la<jicates less dw\ tho (imitofquaAtitation 

R -H.o14 t:uae cx.c.e&ulee 

.. -

3·U " 

5,890 

-

Date: 18-Aug-08 . 

Metllod Date A.llalyst 

[llatrlc SOUD 

OU18 14-IIIJ9.()8 VJO 

03174- . ......... VJO 

sass • 15-Aug.oa OAS 

. I • 

. Matrix: $0[..10 • 

02216 ~ VJO 

03t74 

·~ VJO• 

0$865 .. ~ OAS 

P&&c I o( 2 

.. ":"14 POTTSVILlE Pttq:. RE.A()(NG. PENNSYLVANIA 19005 610-92.1~33 FAX 610.921-0667 

VES 004971 
j 

•,. 

.· 

iii69.Sal,'dolcr.et>:- Po. i~ 

~· f-«12:8195 (1 .. )21 5-822-l 293 C..rtiOqte o( Analytical Res•la 

CLUNl': . ·Miu::am Aaalytieal St:nices 

SSSS Korth Servici Rd 

(hu i~CM. Oatart. L7L SH7 

l.a.b Ordc•·~ Roaosaozo · · 

:froJoc:t ~8&9378 

Aao.tr- Asll«eiYedBull Dry Bull 

A)t,3J.5..GlR \ C$-!13=R3 

Lob ro: 'Rosoaoo1(l.(iJA 

Da<cS....,I<.t: O!lf17f2!!03 · 0... R.<tt<Y..t: OtJ1412001 

PERCEHT MOISTURE 

,M<*CW.:T.cll1 

ASH,·COAL 

... 

HEATiNG V-'i.UE. COAL 

t1oltiog vaeUe 

7G.S, 

8.o9 .• zu 

15()0 o.~ 

• bate: 18-A•g·08 

,. 

Uai.ts • Metlood · Autj,t. 

-M.? tr!£ SOLID 

1<0 02216 

· VXJ 

" 0317 .. .. 15~ VJO, 

. llli>'lb' o;a65 1S-IWQ-o~ DAS 

.. · ----~=---...:..-- -_;,_.,----' _ _._,.--:-____ -:--_ __;_,....--:. 

· .. 

.... 

. •, 

< l.odi<otes I.., .dian~ limit ofquaod~Uoo 

ff-1loWr .. ~ 

.· 

.. , . 

~. 

.. 

,. 

VES 004972 
. ·11!!1!!!11 . - ..... - . llliiliiiil -~w: 

• .. . 

) 286aSaroddoneer.·ll!l&..t>o.l9«'1 

~e1)21 ~.11995 (l<x)ll s.822-12Sl Certlficat~ of Analyticol_ Results· 

-. 

.. .. 

~Onler: · 

Project: 

Mau.aOiAct•l:f1ic.s ~e. · 

6'740~a. • .i ' . 

· M;..-.p; (1otari• LSN ZLI 

R0808001? 

. ilsm1s 

A~04-0tR\ BimJ:uw 

LablD: RQ30800t9:0)k 

R .. ~lt PQL On.its 

Doie::;,..,ted: . OS!Osnooa· 0:00 h .. e .RCc.ived: OSti~S 

'ISH, OIL 

- ~ % 

.HEATING VAI,.uE BlUJtB . ~Value ' ·: .. . . .. .' AE!30S-01R \ mn:u-U3-R2 . 

·: 

Lab.[D: . ROSOl!()(\ l9.()2A. . 

·. " 1)a_us. .. pled; oS/Omoos ·o:oo. _ ·n • .; &Cew..t.:· WI~ 

_C) ":~ . 

., -

-liEI.nNG )IAUIE.BTU/l.B 

-tJno·VAE&30(;..il1R \ H)UU-03-ro 

LOb[(): . R0&0800 l9.()3A. ... ·. Dat.-saoopi.d: 0&(07/2008 0.:00 

· 'IS,.; . OIL 

""' 

HEATlNG VALUE Bl:tliLB . · HeaG.;,.votuc ·: · • . . . . 

,, 

< lQdicates less tlwl-tbe I lAW< of quautitalioo · 

it · lfokt :ru.,~ CX;'~ · · · 

6.00 . b.01 % · . 

. 3,290 60 

6.45 0.01 ' ~~o 

1,300 

Dat" /8-Aug'(/8 

. l>a~~ · ·A,Iiatyst 

1\btri<; AQUEOUS 

O.az ~~.()8 VJO . 

~·· 5~a cA.~ 

Matrix: AQOilOUS 

04&2 ;~ VJO 

OZ40' 15-Aug-o3 !)As • 

Matrii: _:\QUilOUS 

'• · · . ........... . VJO . ; . 

., 

4416 POITSVUJ.E PIKE;R.EA.otNri. PENNSYl VAIAA 19605 610~1oo8833 FAXG:I0~2t-9667 . . ' . 

: 

: 

.. 

. -. 

.· . 

: 

VES 004973 
. .. '•. 

. ' 

A '· 

v 

·. 

. .. 

·· .. 

. ·. 

.(j 

~~cote o(· A.a.a\ytical ~ults · . ' . 

. 'CLIItN'T: 

IAI.ont..-: . .. 

. M.alxu. iu.atytiu lo.e. 

. ·""0 c • ..q;.be& bad' 

' f.o,~op. O'Mfrio' UN 1L8 

RO&ll800l9 

ASl9373' 

AAab'lot · '· Raldt !QL UoJu 

'. 

tabiD: 

Date Sam.pled: 

ROI03001.?-04A 

Galll512008 ~:00 Daullo«lvod: 01/IC/lOOI 

ASH,OL · Alh" ·~ . . . .. 

HEAT'ING VALUE BTUILB 

Heatii'IIJ Vtlu& ' . .. ' ·. 

W308..0lR \'LB'J)U-U3-IU 

0..410 .0.01 

ttO 60 .. 

taHD: R08~0019-0SA • . 

Da,tiSaia~: llll07/2008 o:oo 'oat• Rcc<lv..S: ·olli412008 

ASII, 01~ . . . ··. 

..... 

HEATIHO VoUuE BTUILB 

ll!a&IQ v .... 

A.R§io9-6lR \ LBT.U-U3-R3 . 

lM ID: ROSOIOOl~ 

·OaiD s,;...,~eo~: .· 00071200& o:oo 

ASII,.Ofl, 

N:h 

HEA 11NG ~UE !ITIJILB. 

tt......,v~. 

•' 

··. 

< ladlCalcs lOss \l>llllbe limiCofqtlan~n 

. ~-llololn .... .......-

. ' 

OASO 

<50.000 

.. 

·. 

"' 

Me<to.od · lido 

02.<0 

Matrix: AQUI!OUS 

0240 

' ' 

' . 

Aaai}'Jt . 

VJO 

VJO 

.. 

vx) ·. 

·. · 

' . 

' . 

VES 004974 
·.· . .,. 

) 

· 

i::.J . 

() 

' .. ./ 

~Sardsme Dt.Hotftet. P4. 19440 

(le0ll~.e99S(fax)21S-m·l25'3 CertJUcate or Analytical 1\toul~ 

CUE NT: 

Lab.Onlec: 

PrGjec.t: 

Ao.alyses 

Mauam .A.l.~ la.c. 

6749 Ca.u~ Rnd . 

~qo, <Htan. LSN 2!.8 

RO&OS0019 

A889378 

AE63tO.OlR \ Sf-U3-RJ. 

Lab ro: Rosd'loo ~7~ 

Result PQL UlliU M etltod Ott~ 

Dab> Sunpled: · OSIOSI200i 0:00 O.te R«eivtd: 081!412003 

.ASH, 011. 

Matrix: AQ!Jf!OUS .. 

~'tlNG VAWE BT\Jilll 

HMtingV .... 

@it-OlR \ SF-U3•Rl 

Lab Ill: R0&030019.08A 

llale Sampled; 

ASH., OL 

~ 

OS/07/2003 0:00 

HeAliNG VAWE BTUIUI 

AE63U-01R \ SF-U}=iu 

Lab ID: I\Jl3030019-o9A 

. Date Samplod: OS/0712008 0:00 

ASH, OIL 

...,. . 

HEAT!HG VAWE BllJILB 

Heatioo ,.,. 

4.71 0.01 

380 $0 

Date IU<:plved: 081!412008 

3.<(6 0.0~ 

820 50 

Date Received; 0811 ol/200& 

3.21 ...,, 

220 so 

< lllliicatcs leso than lbe limit of qu3atiWion 

s • Hold Tm,.,.""¢...,. 

0482 

0<82 ··~· 

02. 0 1~-ofl 

Matrix: AQUEOUS 

" 04& 14~ 

- 0240 15..-.ug.oo 

A .. IJ'rt . 

VJO 

VJO 

OAS · 

VJO 

OAS 

Pa&e J ofl. 

4418 Pdn SVILl.E Plf<F. READING. PENNSYLVI.NtA. 19605 &10.92148.33 FAX6 o..921~7 

VES 004975 
, ........ 

r 

) 

5015 Campu$wood De ' 

Suite 104 

ea.t Syr.lcuse, NY 

USA · 305!-4~ 

~ ... 

' , 

Sam!*> Malrlx: UOI.!ID 

·. ,#Saroplesf1oceM!d:9 

-loSollb\'CNMt . >:ot.l . ..... "Soil by~ ICP-AES 1 

SamplelA;l!rix: Water 

# Sainples Reoolved: 3 

-"Wo!«b\'0/Mt 

· MAXXAM ANAL Yl!CS INC. 

·. 

., 

'· 

·' 

YOU< Projoct If.: 1002.022. 

Site:VEOLIA 

. , . Report Date: 2001/98121 

This report supen;edOs all pt'GIIious reports will\ the same Max>;mt job I1U<OOer 

CERl!flCAle OF ANALYSIS 

'-

EPA.7470 

DigitaUy signed 

~ . by Mike ChaHis ''7-~ Date: 

· ... a6/!e ·2ooa.os22 · ._.......,.... OS:19:14.()4'0Q" 

oft4 · 

Thi.s~enlts lA ~~heroO)(Yfts ~oct~ 

~5Hodh~l\.O.t.~CJWdo ~ L7L~ Tel: ~332-071!8 ToiFf-.: ~~ Fac 6)..332-Gt69 

'. 

,• 

.. 

VES 004976 
I 

·M a~~~! ..!'-·.-.,...------.:.._.-~----..,-----_.;.-~~.=~.~~:!!':~!.~~~.:.!l!:~~-~~d#!~g;..,;t:_;. J'NSR t.u.m.<lonal 

--. 

·• Ma>aam Job #: A889378 

) • Rop«t Date: 2008/08121 

. ~ Oe6ldlon Uml 

BR:b • QI.Wiy~ Bak:tl ' ' I ' ' 0 0 

'· . ' ,; : . 

I 

' .. 

.. 

.,. 

:. . . .. . 

I· 

: -., 

.. . .. 

Client P<Ojoct f: !002~ 

Pto1oct nomo: IIEOUA 

.... 

. • 

. • .. •

.·. 

. ' 

VES 004977 
.. 

. . 

M a a~~ !D -----:......:..~-------....:. ___ ..:..-~we~ ..... ~-="*"""'~ ..... ~::~!:_;c:.,_~d;;'!....,.,_~ ~-~.,.:- ENSR: iotematl<>nol ....... 

) 

: 

Maicxun Job II: A889378 

Repo<t Date: 2008Al8121 ' 

·. . .. . ··. 

1 . •' • 

. ~· 

.. '. 

(j· .... ,_.,.,. (Cd) . CMldm(C<) 

i . . 

t 

I 

.... 

' • 

tilelll Proioct II; 1002-022 

P<oject """"" VEOUII. 

ELEMENTS BY ATOIIti~ SPECTROSCOP.Y (UQUlPl . 

II 12 :11 · OS 

NO' . .NO ..,: O.o:i ... 

"" NO ·NO 0.1 

· ' s.ac:"" .... . .. ... 0,.18 • o.M. · 1681400, ; " . · 

••• .:1.2 1.3 o:s .· . 0,004ll (\j ,•0,01Sa(Q 6.ot0>.(1) .001.5 

... . ' 

·. 

0\lA. 0,2, ' G.l .G.2. . NO NO o.l • f!IBi<Oi> 

11!01-. NO NO NO' NO'· No· o.oos· 1687..0' 

..... . NO .... . ... .., . "" G.D2 IS07<00 

- o.os .. .NO NO 'NO'• Nil Q.O!I" 1581-!00 .• . .. " . 

- NO 11) .·. NO NO NO .. 1611~ 

mQ!I. NO (I) .• ' ND(Q ·NtA D.008l'(l) f.C;(I) 

,, . . : 

· ... . ·: . 

. . ... 

·· .. . 

Page3d14 

.55Ss~~ R.o.4. ~~~ L7t.SH7 et (806)~ olt~~e~t F~~~'t'e'J 

.. • . 

. 

' 

. .. . ' 

.. . 

.., 

•. 

VES 004978 
• .. 

. . · 

.. ) • Ma>Oam Job It: 1Jl8937e. 

Rec>o<l Oa!a: 200810812 I 

. ' 

.... ......,(A$) ...... NO 0.1 ,_ .... ............... 19<) ...... No 0.1105 .587~ 

~""""'""" (Cd) ...... ·NO O.ot 1~400 .. · ... - ~ -.. ... oc.oa,;;,;....{()) ....... HO O.llli \587 ..... .- . .... leod (1!1>) .,g.. $ 0.1 U$1400 

"""' . ·. NO (0. : 15 tWoe: . . . -- . ·• ,. 

·Nat~ . - ' • R~""""""" l.iml 

8atd). o.tlt Controt ~ . . . . 

... ., .. ... ; 

... ' . 

.. .. :- . ' .. 

· . 

.. .. 

~ .. ' · ' ._ , .. .. ·. . -: . 

: 

; 

.. 

•. 

·' 

.. PoQe4otl< 

$5$Nodh~~~~~ l7t..6H7 

' 

Teo!: (9QS)~.em;a ToJ~ (810<»~ F"c::C)QS)sn-8169 

. . . 

VES 004979 
r0 a a~!1:!------- ---- -...:...-'- --- -:.!-...=: .... ~=.,_~ ........ ~ .. =--"'""";";;; . =·=~ ENSRinlsmational • \ t.lalcxam Job 11:1\689378 

·J Re!>ortl>a!8: 2006/08121 

,, 

.. 

... 

. '· 

.. , . 

J 

) 

Client Pr910d 1: 1()()2.002 · Pl<>jea name:IIEOLIA 

RESULTS OF ANAL VSES OF SOIL 

. .. ~ .. : ' . '. 

,. 

~5oft4 . 

.. 

. ' 

( 

' . . .... . 

VES 004980 
"•) 

·. 

A 

:J 

. . : .... 

. _.v.: a a~.m-."'"· --- --~--------:----7--~~;;::;:;~:;;-;;· --:;..,..:;;;;;; .... :_-;'i..,.__;;i;";;'":;;o.~ ENSR lntemati<>ol'll· 

"""""""' Job II: AS89378 ~aport Oal&: 2008J08/ll 

C1lont Pnl!Oa#: taln~22. 

Pro)ocrnamo: VEOUA 

~TS BY ATOMIC SPECTROs_GOPY (SOII.j 

-.. """"_ on "6.8 .&:1 . 7.-i o.s 15S7443 

--11'1) ogfg ,.. f5 ... -~(Be) on NO" ."NO . NO o.s. 15_1T<St ·~- '"'*-• <>oJonluon (Col). on . f)llil 1200 '""' 0.3 : 158744:2 

~(C<) ..., .,.,. ~ ...,. o.s Ui87Aa2 

-l.eod{Pb) on .t:m . '1400' , ... I 1S81"<8t 

·Ncl- = RepodatM o.don Utra 

. ,OiJt/ll:v Cor*aC 8«d'' 

· . . 

··.· · . . 

~ :• 

.... ') 

....... . : .. :• . : . 

VES 004981 
· 

u i . 

I 

I ·.: 

c J . ._ . \ 

! 

I 

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Maxxam .Job 11': A889378 

Report l)_ate: 2008.06/21 

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VES 004984 
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Naxxam Job #:...A889378 

Re~ort Dale: 2008Alet2t 

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VES 004986 
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VES 004988 
yandation Signature raga 

IAa>oc~<O job #: A68~lT8 . 

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VES004989 
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Altcn!loni Jeff Gorman 

ENSR International 

5015 Campuswood Dr 

Suito104 

East Syracuse, NY 

USA 13057-4232 

MAXxAMJOB II; A889378 

Received: ~oa/00/08, 0:00 

Sample Matrix: UQUID 

# Samples Reoelved: 9 

Sample Matrix: Soil · 

# Sa'!'ples ~eceived: 3 

·'· 

Ndons In Ctlemliil Matedal 

-inSollbyCVM · . To«aa M01all in Soi.by AldOl ICP.AES 

Sample Matrix: Water 

H Samples ReceM>d: 3 

Your Project 11-: 1002-022 

Site:VEOUA 

.Report Date: 2008111/14 

This repo(l supersedes all pre\liQus repotls wilh lho SOIM Maxxam job number 

CERTIFICATE OF ANALYSIS 

9 

9 

2006/oe/15 2008108/18 CAM SOP.Q0453 

2008J0811S 2008108118 CAM SOP-00408 

. 3 . 2008108115 . 

3. 200810l!115 2008108115 CAMSOP·00~5:f 3 . 2008108(15 2008/0&'17 0nt SOP.0072 . 

EPA 7470 

EPA 6010C 

ePA 7470 

EPASW~IOC. 

(t) tAruoc.am AnatyUc:s; does not hold~ b analysis of metals In water samples u~ lle ICP A)ljal mothodotogy. 

MAXXAMANAL YTICs 

Total coverpages:1 

VES 004990 
Maxxarn Job lt. 11889378 

Report Oslo: 2008/11/14 

ENSR lnlemalionsl 

Client Projocllt. 1002.022 

Projoct name: VEOLIA 

RESULTS OF ANALYSES OF UQUIO 

.05 1687,595 

»OS 1557595 

" · 

VES 004991 
M ~ ~.;. 4a. ~l)l'tll r:n c:s ------- -------- --- "'"'"''"'-"'"'!\r""'S"•""""'="'"'""'"··"' .. "'""""'

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MoJO<.am Job #: A869376 

Report Dale: 2008/11/14 

ENSR lntematiooal 

Client Projoct #: 1002-{)22 

. Projecl r.ame: VEOI.IA 

ELEMENTS BY ATOMIC SPECTROSCOPY (LIQUID) 

~% 

.... _(As) mg/1. 11 12" 11 0.5 0.3 0.1 1587400 

.... e..,o.m(Bo) mgll ND NO NO 0.03 Nil 0.005 1587400 

ota!C-(Cd) mgll. NO ND NO 0.1 NO O.D2 1581400 

otal Clvorium (C~ mgll. 3.9 ..•. $ ,.4.5 0.3 0.'18 0.05 1587400 

otat Load (Pb) mgll. 0.6 1.2 1.3 0.5 NO · 0.1 1S87~00 

ry(Hg) mgiL o.oo:~9 ro 0.0!_58 . (1) 0.~100 (1) .0015 0.0019 (1) .0015 1581438 

• N:oC dolOdod 

RDL = ~·De-Umlt 

QC 8ald> • O""'IIY Comrol 8ol<lh · · . . 

1 ) San'P~ w. tsbntlted an \I'IP(eseMd ~ RestJtt ~y be blas:ed low' duie to mpropor preseN on. , 

cCal Atoenle (As) mgll. 0.2 0.1 0.2 NO NO 0.1 ' 1587..00 

.... 8orj!lul!l (Be) mg/l NO NO . I<D NO NO 0.005 . 1561400 

otat cn.tum (Cd) mgiL ·NO ND NO NO NO 0.62 1587400 

OIOICM>mtum(~ mgiL 0.05 NO. NO NO . NO o.os 1587400 

otoll.ead (Pb) mgll. NO NO NO . NO ·~o 0.1 1587400 

(Hg) mgiL NO (I) NO~) · NIA 0.0087 (1) ND(I) .0015 1587438 

II Not dotoded 

A • Not AppliCIIIbfO 

• R~ Oetdon Limit 

SMdl• Quollt)' Cc:lr*ol 83tcfl . 

t ) Sarnpto vms Stlbmiltcd an~ b;ottl&. ~ m_ay .be biased 1ow due to lmpropet preservatfon. 

VES 004992 
MOXJCam Job II: A889378 

Report Date: 2008/11/14 . 

.· ... 

ENSR lnlemational 

Clieni Project II: 1002-022 

. Project nome: VEOLIA 

ELEMENTS BY ATOMIC SPECTROSCOPY (UQUID) · 

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..., At$8flle (As) rogll. NO 0.1 1587400 

To<al Bor,Cllum {&} ........ NO 0.005 1587.00 

Olal Cadmillffi (Cd) mg/1. NO 0.02 1587400 

otaiC-(c.) mg/l NO 0.05 158l400 

otalload (Pb) mgll NO 0.1 15&7@ 

~{iig)' • NO (I) .0015 1587438 

~~· No< deleeled . . L • ~ Doledloo U .... cic - • a""ny c...1ro1 BalCh · 

1) ---.. ~cdboOie.- - bo b-l~duolo lrno<op«.,._allon. 

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VES 004993 
M a CAh v.<1 .a l~o~>in-

~ci: ------- - ------ - -------"'o!!"""=·.,.=s!!: ..... !!-~·~"~·.....,~~-!!;· 

Maxxam Job It A889378 

Report Oato: 200S/11/14 

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£*4• 

ENSR lntomatlooat 

Client Project#; 1002.022 

. Project namo: 1/EOUA 

RESULTS OF ANALYSES OF SOIL 

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·.· . • .. 

,, . 

VES 004994 
ENSR International 

Client Project #: 1002..022 

Project name: VEOLIA 

Maxxam Job it. A889378 

Report Date: 2008/11/14 

This report superse<Jes all previous reports with the same Maxxam job number 

ELEMENTs BY ATOMIC SPECTROSCOPY (SOIL) 

NO e Not detected 

Rf?L = Reportable Detection Umlt 

QC Batch " Quality Control Batch . 

VES 004995 
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Ma>o:orn Job II: A889378 

Repc.rt Date: 2008/11/14 

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ENSR I<Umatiol'llll a ;ent Projec;lll: 1002-{)22 

Project name: VEOUA 

ELEMENTS B Y ATOMIC SPECTROSCOPY (WATER) 

• R~ OOOdon Umil 

Ba!d1 • Quoily. Cor*'>~ Baldi 

. , 

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VES 004996 
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Maxxam Job #: A889378. 

Rop<W'I Oato: 2008111114 

Mauam 10 A.e6304 

Sampl• 10 HBTU-:03-Rt 

Matrix UOt.nD . 

Uaxxam 10 AE630S 

Somplo ID H8TU-l13-lU 

~ UQUIO 

Maxxem to AaSDG 

SompleiD HBTU-U34<3 

'·Mattix LIQUID 

......... 10~ 

~mple 10 LBTIJ..U3-R1 

· · Matrix UOUIO 

Ma.xnm 10 AE6306 

Sama>l$ 10 LBTU-U3-R2. 

. · llafltx LIQUID 

Test Summary 

ENSR intemattonal 

Cient Projed #: t002.Q22 

Projecl name: VEOUA 

VES 004997 
·...,o M ;a ~~i<r;n ---- ------------- -------;!i"""~~!!!!.!&!!!:>-~ :!!:!:.!J'm~ d.:!.._!!l!:!l-:!. 

Maxxam Job II: A889378 

Repcrt Date: 2008/11/14 

llaxxamiO AE0009 

Sample 10 LBTlJ..U3-R3 

Matrix . UQUIO 

.llalowoiD A£63090v;> 

Sample I!> 1.8'1\J·V3-R3 • · Motllx UQUID 

MuxaM 10 AE63i0 . .....,.,. 10 • SF4J3-R1 

· Matttx 'UQUIO 

)lla1o<om 10 AE6311 

S""'P\0 ID SI'·IJ3-R2 

- tiQUID 

Muxam 10 AE6312 

' .Sampt• 10 SF-o0s.R3 

M- UQVIO 

Muxam to Ae63t3 

Sample ID CS-U3-R1 

Matrix SoU 

Test Summary 

E.NSR lnt«nalfonal 

Client Project#: 1002.022 

Projocl nome: VEOLIA 

• Co11Ki.d· · 2008/0Ml7 

·. · Sb- . . Ro<eiV... .20081081<ia 

Collei:tod 2008108105: 

S-d 

Reeetvod 2008/08108 

VES 004998 
' · ', ; 

M""""m Job #: A889378 

Report 0018: 2008111114 

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Muxam 10 AE6313 OUp 

Sntplt 10 CS-!J3.Rt 

UaMx sof · 

Mtxxam m AE6314 

· Sampte. tO ~2 

Matrix Sol 

Malo<OmiD Ae6315 

s ... p~eto ~R3 

Matrtx Soli 

Max!t8m 10 AEB316 

Santplell NS.V3·R1 : 

Molrii' Water 

~ 

~ID AE6317 

S..nple ID MS.\J3.R2 

Malrtx 

-

'MalOUiillliD ·AE6318 

S«Jnppe 10 MS-Ua.R3 

MlrtriX Watlll' 

Test Summary 

ENSR International 

ell""' Project #: 002~2 

Project name: VEOLIA 

Colleelcd 2008108105 

Shipped 

Received ' 2008108108. 

. .-. Cohct.d· 2006100107 

SNpped 

. ~ Received 20061()8108: 

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Coli- 2008108107 

Shipped 

R•c•tv.d 2008108108 

Co-d 

ShlppOd ~ 

R- 2008/06106 

eo-• 20,08mi01' 

Slllpped 

Recolved' ~ 

Collectod 2008108107 ' 

Sb\J>ped 

~,d 2,ooeiOaios 

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VES 004999