### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### EIA

Facility Code Facility Name Boiler ID Fuel Type 1

3161 EDDYSTONE 3&4 

## No.6 Fuel Oil (residual or bunker C)

### Fuel Type 2 Fuel Type 3 Other Fuel Description



## other Natural Gas

### EIA

Facility Code Facility Name Boiler ID Basis An alyte



## 3161 EDDYSTONE 3&4 As Received Higher Heating Value 

## 3161 EDDYSTONE 3&4 As Received % Moisture 

## 3161 EDDYSTONE 3&4 As Received % Ash 

## 3161 EDDYSTONE 3&4 As Received % Sulfur 

## 3161 EDDYSTONE 3&4 Dry basis Higher Heating Value 

## 3161 EDDYSTONE 3&4 Dry basis % Ash 

## 3161 EDDYSTONE 3&4 Dry basis % Sulfur 

## 3161 EDDYSTONE 3&4 Dry basis Antim ony 

## 3161 EDDYSTONE 3&4 Dry basis Arsenic 

## 3161 EDDYSTONE 3&4 Dry basis Bery llium 

## 3161 EDDYSTONE 3&4 Dry basis Cadmium 

## 3161 EDDYSTONE 3&4 Dry basis Chlorine 

## 3161 EDDYSTONE 3&4 Dry basis Chromium 

## 3161 EDDYSTONE 3&4 Dry basis Cobalt 

## 3161 EDDYSTONE 3&4 Dry basis Fluorine 

## 3161 EDDYSTONE 3&4 Dry basis Lead 

## 3161 EDDYSTONE 3&4 Dry basis Manganese 

## 3161 EDDYSTONE 3&4 Dry basis Mercury 

## 3161 EDDYSTONE 3&4 Dry basis Nickel 

## 3161 EDDYSTONE 3&4 Dry basis Selenium

### An alysis M ethod for each A nalyte

(example: ASTM D5865-04) 

## ASTM D 240

ASTM D 482 ASTM D 1552 ASTM D 240 ASTM D 482 ASTM D 1552 SW6010B SW6010B SW6010B SW6010B ASTM E776/9253 SW6010B SW6010B ASTM D 3761 SW6010B SW6010B ASTM D 3684/SW7471 SW6010B SW6010BEIA

Facility Code Facility

Name Boiler ID 

### HA Ps Test Group 

## 3161 EDDYSTONE 3&4 Dioxin/furan HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) 

### 0060A 

## 7/20/2010 7/20/2010 18480.00 Btu/lb 0.03 0.5 0055A 7/21/2010 7/21/2010 18470.00 Btu/lb 0.06 0.5 0065A 7/22/2010 7/22/2010 18420.00 Btu/lb 0.05 0.49 Fuel Testing ResultsHHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis)Arsenic

Units Bery llium

(Dry Basis) Bery llium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h Fixed Carbon 

## 0.03 0.06 0.05 Proximate Analy

ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen



## 87.4 10.8 0.37 0.5 0.9 87.4 10.8 0.38 0.5 0.86 87 10.6 0.37 0.49 1.49 Ultimate Analy

ses, % by

wtEIA

Facility Code Facility

Name Boiler ID 

### HA Ps Test Group 

## 3161 EDDYSTONE 3&4 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 

### 0050A 

## 7/20/2010 7/20/2010 18530.00 Btu/lb 0048A 7/20/2010 7/20/2010 18490.00 Btu/lb 0053A 7/20/2010 7/20/2010 18510.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

## 0.04 0.49 0.04 0.5 0.03 0.5Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis) 

## 0.05 % 0.01 % 0.03 %Bery llium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 

## 14 mg/Kg 10 mg/Kg 10 mg/Kg

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 

## 0.04 87.4 10.8 0.41 0.49 0.04 87.4 10.9 0.35 0.5 0.03 87.5 11 0.36 0.5 Proximate A naly

ses, % by

wt Ultimate Analy ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 

## 0.81 0.8 0.58EIA

Facility Code Facility

Name Boiler ID 

### HA Ps Test Group 

## 3161 EDDYSTONE 3&4 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### 0062A 

## 7/21/2010 7/21/2010 18530.00 Btu/lb 0068A 7/22/2010 7/22/2010 18500.00 Btu/lb 0072A 7/23/2010 7/23/2010 18500.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

## 0.06 0.48 0.05 0.5 0.04 0.45Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis)Bery llium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy

ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen



## 0.06 86.8 11 0.36 0.48 1.3 0.05 87.2 10.8 0.36 0.5 1.09 0.04 87.5 11 0.36 0.45 0.65 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID 

### HA Ps Test Group 

## 3161 EDDYSTONE 3&4 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### 0057A 

## 7/21/2010 7/21/2010 18400.00 Btu/lb 0066A 7/22/2010 7/22/2010 18390.00 Btu/lb 0070A 7/23/2010 7/23/2010 18540.00 Btu/lb Fuel Testing Results

## Mercury and non-mercury metalic HAPs

% Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

## 0.03 0.47 0.04 0.5 0.04 0.49Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis) 

## <.1 mg/Kg <1.5 mg/Kg <1 mg/Kg <.5 <.1 mg/Kg <1.5 mg/Kg <1 mg/Kg <.5 <.1 mg/Kg <1.5 mg/Kg <1 mg/Kg <.5Bery llium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

## mg/Kg <.5 mg/Kg <.5 mg/Kg <.5 mg/Kg 0.928 mg/Kg mg/Kg <.5 mg/Kg 0.596 mg/Kg <.5 mg/Kg 0.863 mg/Kg mg/Kg <.5 mg/Kg <.5 mg/Kg <.5 mg/Kg 1 mg/KgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

## 2.67 mg/Kg <1 mg/Kg 0.239 mg/Kg 2.63 mg/Kg <1 mg/Kg 0.224 mg/Kg 2.98 mg/Kg <1 mg/Kg 0.255 mg/Kg Proximate Analy ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen



## 0.03 87.8 10.3 0.43 0.47 0.97 0.04 87.3 10.6 0.42 0.5 1.14 0.04 87.6 10.9 0.35 0.49 0.62 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wt

### Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals sy nfuel mg /g petroleum coke μg/g other mg /Kg

### Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orange hightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm mg /Kg