## DEPARTMENT OF THE NAVY COMMANDER NAW REGION HAWAII 850 TICONDEROGA ST STE 110 PEARL HARBOR, HAWAII96880.5101 

# li MAR 1 9 100& 0 

# \1

5090 Ser N45/00057 March 14, 2008
CERTIFIBD N]1IL NO. 7006 0100 0007 2053 6072
Mr. Richard Takaba Underground Storage Tank Section Solid & Hazardous Waste Branch Environmental Management Division State of Hawaii Department of Health 919 Ala Moana Boulevard Room 212 Honolulu HI 96814
Dear Mr. Takaba:

SUBJECT: RED HILL TANK COMPLEX

JANUARY 2008 GROUNDWATER MONITORING RESULTSI FACILITY I. D. N0. 9-102271 / RELEASE I.D. NO. 99051, 010011 AND 020028 The Environmental Company (TEC), Inc. collected groundwater samples from four wells on January 15, 2008. The groundwater samples were analyzed for petroleum constituents. We are submitting the Quarterly Groundwater Monitoring Report in Enclosure 1. If there are any questions regarding this matter, or if more information is needed, please contact Ms. Raelynn Della Sala at (808) 471-1171, extension 337.
in rel

R. . WAKUMOTO Division Head, Compliance Regional Environmental Department By direction of the Commander Enclosure: 1. Quarterly Groundwater Monitoring Report, Red Hill Fuel

Storage Facility, Pearl Harbor, Oahu, Hawaii of March 2008

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# Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility Pearl Harbor, Oahu, Hawaii Latitude: 21 0 22'15" N Longitude: 157 0 53'33" W
DOH Facility ID No. 9-102271 DOH Release I D No. 99051, 010011; 020028

March 2008

Prepared 

# by:
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Commander Navy Region Hawaii Environmental Department, Code N45 

# 850 Ticonderoga Street, Suite 110 Pearl Harbor, Hawaii 

# 96860-5101

### 0 

## Quarterly Groundwater Monitoring Report

~ 

## Red Hill Fuel Storage Faciliry March 2008


# Table of Contents
Tableof Contents ............................................................................................................................. i ExecutiveSumrttary ......................................................................................................................... 1 

# 1.0 Introduction ......................................................................................................................... 2 1.1 Project Objective ............................................................................................................. 2 

## 1.2 Previous Reports .............. :.............................................................................................. 2 1.3 Background .....................................................................................................................3 1.3.1 Site Description ....................................................................................................... 3 

# 1.3.2 Facilfty Information ................................................................................................ 3 1.3.3 UST Information ..................................................................................................... 3 1.4 Previous Environmental Investigations .......................................................................... 3 

# 2.0 Sample Collection and Analyses ......................................................................................... 5 2 .1 Monitoring Well Purging ................................................................................................ 5 2.2 Groundwater Sample Collection ..................................................................................... 5 2.3 Groundwater Sample Analyses ....................................................................................... 6 

# 3.0 Groundwater Sample Analytical Results ............................................................................ 6 3.1 January 2008 Sample Analytical Results ........................................................................ 6 3.2 February 2008 Sample Analytical Results ...................................................................... 8 3.3 Groundwater Contaniinant Trend ................................................................................... 8 

# 4.0 Summary and Conclusions .................................................................................................. 8 5.0 References .........................................................................................................................11
Table 1 Analytical Results for Quarterly Groundwater Sampling Release Response Report ....7 Figure 1 TPH Trends in Groundwater, Round 10 (January 15, 2008) .........................................9 Figure 2 PAH Trends in Groundwater, Round 10 (January 15, 2008) ......................................10 Appendix A— Laboratory Analytical Reports

## Quarterly Groundwater MonEtorfng Report

LRed Hill Fuel Storage FacllEty March 2008


# Executive Summary There are 18 active and 2 inactive, 12.5 million gallon, field-constructed underground storage tanks (USTs) located at the Red Hill Fuel Storage Facility. Previous environmental site investigations indicated a release had occurred and contaminated the groundwater underlying the Facility. The Navy implemented a groundwater monitoring program, which includes collecting groundwater samples quarterly from U.S. Navy we112254-01 (RHMW2254-01) and three wells installed in the Facility lower access tunnel (RHMWOl, RHMW02, RHMW03). The U.S. Navy well 2254-01 is located approximately 3,000 

# feet downgradient from the Red Hill Fuel Storage Facility and provides approximately 24 percent of the potable water to the Pearl Harbor Water System. The groundwater samples are analyzed for petroleum constituents and compared against State of Hawaii Department of Health (DOH) Drinking Water Environmental Action Levels (EALs) (DOH, 2005a). This groundwater monitoring report presents the analytical results and comparisons against DOH Drinking Water EALs for samples collected in January 2008. Concentration trends for chemicals that exceeded DOH Drinking Water EALs are also provided in this report. Laboratory analytical results indicate total petroleum hydrocarbons (TPH) as diesel range organics (TPH-DRO) and polynuclear aromatic hydrocarbons (PAHs) are present 

## in the groundwater beneath the Red Hill Fuel Storage Facility at concentrations that exceed DOH Drinking Watsr EALs. TPH-DRO was detected at 574 micrograms per liter (μg/L) in RHMW01,3230 μg/I. in RHMW02, and 242 μg/L in RHMW03. The DOH Drinking Water EAL for TPHDRO is 100 μg/L. Three PAHs 

# were detected in RHMW02 at concentrations above the DOH Drinking Water EALs: naphthalene at 195 μg/L (DOH EAL is 6.2 μg/I.), 1-methylnaphthalene at 73.2 μg/L (DOH EAL is 10 μg/L), and 2-methylnaphthalene at 27.6 μg/L (DOH EAL is 10 μg/L). Concentrations of TPH-DRO at RHMWOl have been above the DOH Drinking Water EAL during groundwater sampling 

# events since September 2005 and had shown a decreasing trend until the January 2008 sampling event. Concentrations of TPH-DRO at RHMW03 had alsoshown a decreasing trend until the January 2008 sampling event. The concentration of TPHDRO has remained relatively stable at RHMW02 at concentrations ranging from 2,250 to 3,180 μg/L, which are well above the DOH Drinking Water EAL of 100 μg/L. Concentrations of PAHs at RHMW02 remain above the DOH Drinking Water EALs, but have shown a decreasing trend over the past two years. The ongoing quarterly collection and analysis of groundwater samples will continue to monitor the quality of the groundwater located beneath the Red Hill Fuel Storage Facility. The analytical results from the groundwater monitoring program will determine whether contamination presents a risk to consumers of the water within the Red Hill sub-basin. 1

## Quarterly Groundwater Monitoring Report

Red Hill Fuel Storage Facflity March 2008 ~



# 1.0 Introduction This report presents the results of the tenth groundwater sampling and analysis event conducted in January 2008 at the Red Hill Fuel Storage Facility, Oahu, Hawaii (hereafter referred to as "the Facility"). The Facility consists of 18 active and 2 inactive underground storage tanks (USTs) operated by the Fleet Industrial and Supply Center (FISC) Pearl Harbor. The groundwater sampling and analysis event is part of a groundwater monitoring program for the underground storage tank site in response to past UST releases, previous enviromnental investigations, and reconunendations from the State of Hawau Department of Health (DOH). 

# 1.1 Project Objective This groundwater sampling and analysis was perfotmed to evaluate the presence of cheniicals of potential concem in groundwater underlying the Facility. The groundwater sampling and analysis was conducted to ensure the Navy remains in compliance with DOH UST release response requirements as described in Hawaii Administrative Rules (HAR) 11-281 Subchapter 7, Release Response Action. The groundwater sampling and analysis procedures generally followed the procedures described in 

# Red Hill Bulk Fuel Storage Facility 

# Groundwater Protection Plan (The Environmental Company, Inc. [TEC], 2008). This groundwater sampling and analysis event was conducted by TEC, Inc. under Air Force Center for Engineering and the Environment (AFCEE) Contract Number F41624-03-D-8618, Task Order 021. 

# 1.2 Previous Reports The following groundwater monitoring reports were submitted to the DOH:

1. Groundwater Sampling Report, First Quarter 2005 (submitted Apri12005) 2. Groundwater Sampfing Report, Second Quarter 2005 (submitted August 2005) Groundwater Sampling Report, Third Quarter 2005 (submitted November 2005) 4. Groundwater Sampling Report, Fourth Quarter 2005 (submitted February 2006) 5. Groundwater Monitoring Results, July 2006 (submitted September 2006) 6. Groundwater Monitoring Results, December 2006 (submitted January 2007) 7. Groundwater Monitoring Results, March 2007 (submitted May 2007) 8. Groundwater Monitoring Results, June 2007 (submitted August 2007)

, 9. Groundwater Monitoring Results, September 2007 (submitted October 2007)

`A

## Quarterly Groundwater Monitorfng Reporr

~ 

## Red Hill Fuel Storage Facllity March 2008


# 1.3 Background The following sections provide a description of the site and information on the Facility and USTs. 1.3.1 Sfte Descrtption 

## The Facility is located in Halawa Heights on Oahu, Hawaii. Land adjacent to the north of the Facility is occupied by Halawa Correctional Facility and private businesses. Land to the south and west of the Facility includes the Coast Guard Reservation. Moanalua Valley is located east of the Facility (Dawson, 2006). The Navy Public Works DepatUnent operates a potable water infiltration tunnel approximately 1,550 feet hydraulically downgradient from the Facility (Dawson, 2006). The U.S. Navy well 2254-01 is located approximately 3,000 feet downgradient (west) of the Facility and provides approximately 24 percent of the potable water to the Pearl Harbor Water System, which serves approximately 52,200 military consumers (TEC, 2008). 

# 1.3.2 Facilfry Information The Facility consists of 18 active and 2 inactive USTs operated by Navy FISC Pearl Harbor. Each UST has a capacity of 12.5 million gallons. The Facility is located approximately 100 feet above the basal aquifer (Dawson, 2006). 

# 1.3.3 UST Information The USTs were constructed in the early 1940s. The tanks were constructed of steel and currently contain Jet Propulsion fuel 5(JP-5) and Diesel Fuel Marine. Previously, several tanks stored Navy Special Fuel Oil, Navy Distillate, aviation gasoline, and motor gasdline. Each tank measures approximately 245 feet in height and 100 feet in diameter. The upper domes of the tanks lie at depths varying between approximately 100 feet and 200 feet below the existing ground surface (TEC, 2006). 

# 1.4 Previous Environmental Investigations 1998 to 2001: From 1998 to 2001, the Navy conducted an investigation at the Facility to assess potential releases from the fuel storage Facility. In February 2001, the Navy installed a one-inch diameter sentinel well (MW-V 1D) to monitor for contamination of the basal aquifer underlying the Facility. The well was installed and completed at approximately 100 feet below grade. At the time of well completion, depth to water in MW-V 1D was measured at 86 feet below grade (Dawson, 2006). In February 2001, groundwater samples collected from sentinel well MW-V 1D contained total petroleum hydrocarbons (TPH) concentrations ranging from 0.883 milligrams per liter (mg/L) to 1.05 mg/L and total lead ranging from 0.0104 mg/L to 0.015 mg/L. The maximum total lead concentration in the samples was equal to the primary drinking water standard of 0.015 mg/L for lead and exceeded the DOH Tier 1 groundwater action level of 0.0056 mg/L (Dawson, 2006). 2005 — Groundwater Sampling: The Navy began quarterly groundwater sampling at existing mottitoring wells in 2005. Dawson Group, Inc. collected groundwater samples from the lower

## Quarterly Groundwater Morsitoriag Report

Red Hill Fuel Storage Facflity March 2008,


## access tunnel well that was installed in 2001 (MW-V 1D) and the Red Hill Navy Pump Station (U.S. Navy we112254-01) in February, June, September, and December 2005. Samples collected in February and June 2005 were not filtered in the field prior to analysis for lead. Analytical results for samples collected from RHMWOl indicated concentrations of total lead were above the DOH Tier 1 action level of 0.0056 mg/L. The results were not considered appropriate for risk assessment since the sample had not been filtered. In addition, lead was not a component of fuels from the tanks near RHMWOl. Lead may have been part of the UST construction material (TEC, 2007). Samples were filtered in September and December 2005, and dissolved lead concentrations were below the DOH Tier 1 action level. Concentrations of all other contaminants of potential concem were below DOH Tier 1 action levels. 

# 2005 — Site Investigation: As part of a site investigation, TEC, Inc. installed three groundwater monitoring wells at the Facility between June and September 2005. Well RHMW02 was installed in the lower access tunnel near Tanks 5 and 6. Well RH3M03 was installed in the lower access tunnel near Tanks 13 and 14. Well RHMW04 was installed hydraulically upgradient of the USTs to provide geochemistry for water moving through the basal aquifer beneath the Facility. Wells RHMW02 and RHMW03 were completed to depths of approximately 125 feet below the tunnel floor, and well RHMW04 was completed to a depth of approximately 300 feet below ground surface outside the tunnel. Groundwater samples were collected from the three newly installed wells and two existing wells (MW-V 1D [renamed RHMWOI] and U.S. Navy well 2254-01) in September 2005. Naphthalene and trichloroethylene were detected in samples collected from RHIvIW02 at concentrations greater than the DOH Tier 1 action levels. Lead was detected in the sample collected from RHMWOI at a concentration greater than the DOH Tier 1 action level; however, the sample was not filtered in the field prior to anaiysis. Analytical results for filtered samples obtained by Dawson during the same period indicated concentrations of dissolved lead were below the DOH Tier 1 action level.


# 2006 — 

# Site Investigation: Dedicated sampling pumps were installed in five wells (RHMWOI, RHMW02, RHMW03, RHMW04, and U.S. Navy we112254-01). TEC, Inc. collected groundwater samples from the wells in July 2006. The groundwater samples were analyzed for petroleum constituents. Naphthalene was detected in samples collected from R14MW02 at concentrations above the DOH Tier 1 action level. In September 2005, with concurrence from the DOH, the Navy decided to use the newer DOH Environmental Action Levels (EALs) for the Red Hill Site Investigation and Risk Assessment project. The EALs are cuaent and provide action levels for more chemicals, and are much more useful for conducting screening risk assessments. Since the DOH June 2005 Policy Letter stated that the two sets of action levels should not be mixed, the Tier 1 screening levels presented in HAR Section 11-281-78 would no longer be used to evaluate environmental impact at the Facility.

4

### Quarterly Groundwater Monftoring Report

''Red Hill Fuel Storage Facility March 2008


## 2006 — Groundwater Sampl7ng: Groundwater samples were collected in December 2006. Analytical results indicated the following: • No chemicals were detected in groundwater from U.S. Navy we112254-01 or RHMW03; • TPH as diesel range organics (TPH-DRO) was detected in groundwater above the DOH Driniting Water EALs in RHMWOl; • TPH as gasoline range organics ('IPH-GRO), TPH-DRO, and naphthalene were detected in groundwater above the DOH Drinking Water EALs in RHMW02.
2007 — Groundwater Sampling: Groundwater samples were collected in March, June, and September 2007. Analytical results indicated the following: • No chemicals were detected above DOH Drinlcing Water EALs at U.S. Navy well 2254-01; • TPH-DRO exceeded DOH Drinking Water EALs at RHMWOI during all three sampling events; • TPH-GRO exceeded DOH Drinking Water EALs at RHMW02 in March; • TPH-DRO and naphthalene exceeded DOH Drinking Water EALs at RHMW02 during all three sampling events; • 1-methylnaphthalene and 2-methylnaphthalene exceeded DOH Drinking Water EAL for taste and odor at RHMW02 during all three sampling events; • TPH-DRO exceeded DOH Drinking Water EALs at RHMW03 in June.



# 2.0 

# Sample Collection and Analyses Field activities relating to groundwater sample collection were conducted on January 15, 2008. Groundwater samples were collected from three monitorring wells located inside the Facility lower access tunnel and one monitoring well located at the Red Hill Navy Pump Station. Sampling and analysis were conducted according to Red Hfll Bulk Fuel Storage Facility Groundwater Protection Plan (TEC, 2008). 

# 2.1 Monitoring Well Purging T'he groundwater monitoring wells were purged and sampled using a dedicated pump system. Well purging was considered complete when no less than three successive water quality parameter measurements had stabilized within approximately 10 percent. Field parameters were measured at regular intervals during well purging and included pH, temperature, specific conductivity, dissolved oxygen, and turbidity. Purge water was disposed in the Facility oil/water separator system. 

# 2.2 Groundwater Sample Collection Each monitoring well was sampled immediately following purging. All wells were sampled directly from the dedicated bladder pump system. Samples were placed into sampling containers with appropriate preservatives (i.e., hydrochloric acid [HCl) for volatile organic analysis, nitric acid [HNO3] for dissolved lead). Dissolved lead samples were filtered in the field and placed in preserved bottles. Sample containers were labeled with the date, sample identification number,

## Quarterly Groundwater Monitoring Report

Red Hill Fuel Storage Faciliry March 2008 0 

## type of analysis, and sampler's name. The containers were placed on ice in sample coolers and transported under chain-of-custody procedures to the certified laboratory for analysis. 

# 2.3 Groundwater Sample Analyses Groundwater samples were analyzed by SGS Enviromnental Service, Inc. in Anchorage, Alaska for TPH-DRO and TPH-GRO by EPA Method 8015B, volatile organic compounds (VOCs) by EPA Method 826013, polynuclear aromatic hydrocarbons (PAHs) by EPA Method 8270C SIMS, and dissolved lead by EPA Method 6020. An estimated TPH-DRO concentration of 102 micrograms per liter (μg/L) was detected at U.S. Navy we112254-01. Since the analytical result was above the DOH Drinking Water EAL of 100 μg/L, additional groundwater samples were collected on February 6, 2008 for reanalysis. One groundwater sample was sent to SGS Environmental Services, Inc. in Anchorage, Alaskaand one groundwater sample was sent to Accutest Laboratories in Orlando, Florida for TPHDRO analysis by EPA Method 8015B.



# 3.0 

# Groundwater Sample Analytical Results This section provides a summary of analytical results for groundwater samples collected from three monitoring wells located in the lower access tunnel of the Facility and one monitoring well located at the Red Hill Navy Pump Station. A summary of groundwater analytical results is included in Table 1. Complete analytical laboratory reports are provided in Appendix A. 

# 3.1 January 2008 Sample Analytical Results All groundwater samples were analyzed for TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved lead. The prelintinary TPH-DRO result for U.S. Navy we112254-01 (also referred to as RHMW2254-01) was considered unusable due to laboratory contamination that was observed in the associated laboratory blank. The TPH-DRO result for RHMW2254-01 was qualified with an "R", as rejected, during data review. No other chemicals of potential concern were detected at or above the method detection limits at RHMW2254-01. TPH-DRO was detected at RHMWOI at 574 μg/L, which is above the DOH Drinking Water EAL of 100 μg/L. All other chemicals of potential concern were below DOH Drinking Water EALs at RHMWOI. TPH-DRO was detected at RHMW02 at 2,310 and 3230 μg/L, which is above the DOH Drinking Water EAL of 100 μg/L. Naphthalene was detected at 195 and 194 μg/L, which is above the toxicity-based DOH Drinking Water EAL of 6.2 μg/L. The concentrations of 1-methylnaphthalene and 2-methylnapthalene were above the DOH Drinking Water EALs for taste and odor. TPH-DRO was detected at RHMW03 at 242 μg/L, which is above the DOH Drinking Water EAL of 100 μg/L. All other chemicals of potential concem were below DOH Drinking Water EALs at RHMWOl.

0Table 1. Malytical Results for Quarterty Groundwater Sampling Release Response Report

January 15, 2008 Red HIII Fuel Storage Faclliry, Hawall
MDOHDrinkbq RHMW01 RHM 02 RHMW02D RHMW03 RHMW2254-01 RHMW2254-01 RHMW2259-01 Mathod Chamlcal HDOHRaaldanNel Walerfsllln9 Unlb UGIL UWL UGIL UGe. UWL UWL UWL DnnMiq Watar EALs' EALd January 15, 2008 January 1e, 2008 January 15, 2008 January 15, 2008 January 15, 200B February 6, 2008 Fabruary 6, 2008 UG/L UWL Result Q MDL RL RecuK Q MDL RL Reault Q MDL RL Result Q MDL RL Reeult Q MDL RL Result 0 MDL RL Result O MDL RL SWS015B TPH-0IESELRANGEORGANICS 100 100 UWL 574 842 421 2310 851 426 3230 87 435 242 F 87 435 102 R 825 412 ND U 1 100 Z80 ND I U I 103 1 515 SWg015B TPH-GASOLINERIINGEORGANICS 100 100 UGIL ND U 10 100 643 F 10 100 662 F 10 100 ND U 10 100 ND U 10 ' 100 SWa260 1,1,1,2-TETRACHLOROETHMIE 043 50DD0 UG/L ND U 015 05 ND U 015 05 ND U 015 05 ND U 015 05 ND U 015 05 1,1,1-TRICHLOROEHIANE 200 970 UG/L ND U 031 1 ND U 031 1 ND U 031 1 ND U 031 1 ND U 031 1 1,1,2,2-TETRACHLOROETHANE 0056 500 UGrL ND U 015 05 ND U 015 05 ND U 015 05 ND U 015 OS ND U 015 05 1,1,2-TRICHLOROETHANE 5 50000 UG/L ND U 031 1 ND U 031 1 ND U 031 1 ND U 031 1 ND U 031 1 1,2A-TRICHLOROBENZPNE 70 3000 UWL ND U 031 1 ND U 031 1 ND U 031 1 ND U 031 1 ND U 031 1 1,2-DIBROMO-3-0HLOROPROPANE(DBCP) 004 10 UG/L ND U 062 2 ND U 062 2 ND U 062 2 ND U 062 2 ND U 062 2 1,24DICHLOROPROPANE 5 10 UG/L ND U 031 1 ND U 031 1 ND U 031 1 ND U 031 1 ND U 031 1 1,3-0ICHLOROBENZENE 180 50000 UG/L ND U 031 1 ND U 031 1 ND U 0.31 1 ND U 031 1 ND U 031 1 1,3-DICHLOROPROPANE 04 50DD0 UG/L ND U 012 04 ND U 012 04 ND U 012 04 ND U 012 04 ND U 012 04 1,4-01CHLOROBENZENE 75 5 UG/L ND U 015 05 ND U 015 05 ND U 015 05 ND U 015 05 ND U 015 05 BENZENE 5 170 UG/L ND U 012 04 017 F 012 04 017 F 012 04 ND U 012 04 ND U 012 04 BROMODICHLOROMETHANE 018 50000 UCVL ND U 015 05 ND U 015 05 ND U 015 05 ND U 015 OS ND U 015 05 BROMOFORM 100 510 UGiL ND U 05 1 ND U 05 1 ND U 05 1 ND U 05 1 ND U 05 1 BROMOMETHANE 85 50000 UWL ND U 094 3 ND U 094 3 ND U 094 3 ND U 094 3 ND U 094 3 CARBONTETRACHLORIDE 5 520 UG/L ND U 031 1 ND U 031 1 ND U 031 1 ND U 031 1 ND U 031 1 CHLOROBENZENE 100 50 UWL ND U 015 05 ND U 015 05 ND U 0.15 05 ND U 015 05 ND U 015 05 CHLOROETHANE 39 18 UWL ND U 031 1 ND U 031 1 ND U 0.31 1 ND U 031 1 NO U 031 1 CHLOROFORM 100 2400 UWL ND U 031 1 ND U 031 1 ND U 031 1 ND U 031 1 ND U 031 1 CHLOROMETHANE 160 500D0 UGIL ND U 031 1 NO U 031 1 ND U 031 1 ND U 031 1 ND U 031 1 cle-1,2-DICHLOROETHYLENE 70 50DD0 UG/L ND U 031 1 ND U 031 1 ND U 031 1 ND U 031 1 ND U 031 1 DIBROMOMETHANE 00056 50000 UGfL ND U 031 1 ND U 031 1 ND U 031 1 ND U 031 1 ND U 031 1 ETHYLBENZENE 700 30 UG/L ND U 031 1 ND U 031 1 035 F 031 1 ND U 031 1 ND U 031 1 HE7(ACHLOROBUTADIENE 006 6 UGrL ND U 0.16 06 ND U 011t 06 ND U 018 06 ND U 018 06 ND U O18 06 M,P-%YLENE(SUMOFISOMERS) 10000 20 UImL ND U 062 2 ND U 062 2 ND U 062 2 ND U 062 2 ND U 062 2 METHYL ETHYL KETONE (243UTANONE) 7000 8400 UG4 ND U 31 10 ND U 31 10 ND U 31 10 ND U 31 10 ND U 31 10 METHYL ISOBUM KETONE (4-METHYL4-PENTANONE) 2000 1300 UG/L ND U 31 10 ND U 31 10 ND U 31 10 ND U 31 10 ND U 31 10 METHYLENECHLORIDE 43 9100 UWL ND U 031 1 ND__

_ U 031 1 __ND _ U 031 1 ND U 031 1 ND U 031 1 NAPHfHALENE 62 21 UG/L 598 062 1 _19b 062 1 1W

_ 062 1 ND U 062 1 ND U 062 1 STYRENE 100 10 UWL ND U 031 1 ND U 031 1 - N'D U 031 1 ND U 031 1 ND U 031 1 METNYLTERTBU7YLETHER(M[BE) 11 5 UG/L ND U 15 5 ND U 15 5 ND U 15 5 ND U 15 5 ND U 15 5 TETRACHLOROETHYLENE(PCE) 5 170 UWL ND U 031 1 ND U 031 1 ND U 031 1 ND U 031 1 ND U 031 1 TOLUENE 1000 40 UG/L ND U 031 1 ND U 031 1 ND U 031 1 ND U 031 1 ND U 031 1 trans-1,24OICHLOROETHENE 100 260 UGY ND U 031 1 ND U 031 1 ND U 031 1 ND U 031 1 ND U 031 1 TRICHLOROETHYLENE(TCE) 5 310 UG/L ND U 0.31 1 ND U 031 1 ND U 0.31 1 ND U 031 1 ND U 031 1 V INYLCHLORIDE 2 3400 UWL ND U 031 1 ND U 1 037 1 1 1 ND U 031 1 ND U 031 1 ND U 031 1 SW8270SIM 1-METHYLNAPHrHALENE 240 10 UG/L 0064 00158 00526 67 0789 283 73.2 0773 258 ND U 00156 00521 ND U 0015 005 2-METHYLNAPHTRALENE 240 10 UG/L 00478 F 00158 00526 218

_ _ 0789 263 27.0

_ _ 0 303 0773 258 ND U 00156 00521 ND U 0015 005 ACENAPIRHENE 370 20 UG/L 0 031 F 00158 00526 0 308 00158 00526 00155 00515 ND U 0 0156 0 0521 ND U 0 015 005 ACENAPHTHYLENE 240 2000 UG4 ND U 00158 00526 ND U 00158 00526 ND U 00155 0.0515 ND U 00156 00521 ND U 0015 005 ANTHRACENE 1800 22 UG2 ND U 00158 00526 ND U 00158 00526 ND U 00155 00515 ND U 00156 00521 ND U 0015 005 BENZO(a)ANTHRACENE 0092 5 UWL ND U 00158 00526 ND U 00158 00526 ND U 00155 00515 ND U 00156 00521 NO U 0015 005 BENZO(a)PYRENE 02 19 UG/L ND U 00158 00528 ND U 0015B 00526 ND U 00155 00515 ND U 00156 00521 ND U 0015 005 BENZO(b)FLUORANTHENE 0092 7 UG/L ND U 00158 00526 ND U 00158 00526 ND U 00155 00515 ND U 00156 00521 ND U 0015 005 BENZO(g,h,i)PERYLENE 1500 013 UGIL ND U 00158 00526 ND U 00168 00528 ND U 00155 00515 ND U 00156 00521 ND U 0015 005 BENZO(k)FLUORANTHENE 092 04 UG/L ND U 00158 00526 ND U 00158 00526 ND U 00155 00515 ND U 00156 g0521 ND U 0015 005 CHRYSENE 92 08 UG4 ND U 00158 00526 ND U 00158 00526 ND U 00155 0.0515 ND U 00158 00521 ND U 0015 005 DIBENZ(a,h)ANTHRACENE 00092 025 UWL ND U 00158 00526 ND U 00158 00526 ND U 00155 00515 ND U 00156 00521 ND U 0015 005 PLUORANTHENE 1500 130 UG/L ND U 00158 00526 ND U 00158 00526 ND U 00155 00515 ND U 00158 00521 NO U 0015 005 FLUORENE 240 950 UG/L 00371 F 00158 00526 0161 0 01 5B 00528 0161 00155 00515 ND U 00156 00521 ND U 0015 005 INDENO(1,2,3c,tl)PYRENE 0092 027 UGfL ND U 00158 00526 ND

_ U 00158 00526 ND

_ U 00155 0.0515 ND U 00156 00521 ND U 0015 005 NAPHTHALENE 62 21 UG/L 021 00326 0105

~ 9J.6

_ _ 163 528 f02 16 515 ND U 00323 0104 ND U 0031 01 PHENANTHRENE 240 410 UWL ND U 00158 00526 ND U 00158 00526 ND U 00155 00515 ND U 00156 00521 ND U 0015 005 PYRENE 180 68 UG

~ L ND U 00158 00526 ND U 00158 00526 ND U 00155 00515 ND U 00156 00521 ND U 0015 005 SW6020 LEAD 15 50000 UG/L ND U 031 1 ND U 031 1 ND U 031 1 ND U 031 1 ND U 031 1

UG/L- microgramsperLiter Q - date queldier U- Indwales that the oompound was arelyzed for but not detecled at orabove the melhod datedion limit F- Indicates the resull was greater than the methcd detecbon limit bul lesa lhan the reponing Ilmit R- Indiwtes the resull wes uneceepleble tlue to data quelity conwms and shoNd not be fuMer evaluated MDL - method detec0on hmit RL- reporbng limit TPH - Tolel Petroleum Hydrocarbons ND - non tleted ,20U'- Result exceeds ona or both HDOH EAL's

- ~ Toxlcily-based enwronmemal acbon levels, Table D-2, Screemrrg fror Enwmnmental ConwmsAtSifesWRhContammafedSodandGnwndwater, HDOH,2005
2 Taste, odor and solublliry threshdds, Table G-1, Soreenmg For Envsonmenta! Concems At Shes Wdh Confermnated SOd arrd Groundwafer, HDOH, 2005 ` RHMW2254-01 was resampled on Februery 6, 2008 beceuse blank contaminabon in the Diesel Componenl alrelysis caused Jenuary 15, 2008 dela to be relected This eliquot wes enalyeed by qcddeat Laboretones ` RHMW2254-01 was resampled on February 6, 2008 because Nank conlammebon In g1e Diesel Componem analysts caused Janualy 15, 2008 deta to be rejeded This ahquot was analyzed by SGS Emimnmental Semces

Page 1 of 1

## Quarterly Groundwater Monitoring Report

' Red Hill Fuel Storage Facility March 2008



# 3.2 February 2008 Sample Analytical Results Additional groundwater samples were collected from RHMW2254-01 on February 6, 2008 for TPH-DRO analysis. One groundwater sample was sent to SGS Environmental Services, Inc. in Anchorage, Alaska and one groundwater sample was sent to Accutest Laboratories in Orlando, Florida. Analytical results from both laboratories showed no TPH-DRO above the respective method detection limits of the laboratories, which were equal to or less than the DOH Drinlcing Water EAL of 100 μg/L.. 

# 3.3 Groundwater Contaminant Trend Groundwater samples have been collected and analyzed by TEC, Inc. since September 2005. Figure 1 shows TPH trends in groundwater at the Facility. Figure 2 shows PAH trends in groundwater at the Facility.
TPH-GRO has not been detected at or above the method detection limit in RHMWOl. The values shown in Figure 1 represent the method detection limits of TPH-GRO. Concentrations of TPH-DRO at RHMWOI have been above the DOH Drinking Water EAL of 100 μg/1, during all groundwater sampling events and had shown a decreasing trend until the January 2008 sampling event. During the seven sampling events shown in Figure 1, concentrations of TPH-GRO at RHMW02 exceeded the DOH Drinking Water EAL three times. The maximum concentration detected was 148 μg/L, which is slightly above the EAL of 100 μg/1.. The concentration of TPH-DRO has remained relatively stable at RHMW02 at concentrations ranging from 2,250 to 3,180 μg/L, which are well above the DOH Drinking Water EAL of 100 μg/L. Although concentrations of PAHs at RF-IMW02 remain above the DOH Drinking Water EALs, they have shown a decreasing trend over the past two years.
TPH-GRO has not been detected at or above the method detection limit in RHMW03. The values shown in Figure 1 represent the method detection limits of TPH-GRO. Concentrations of TPH-DRO at RHMW03 had shown a decreasing trend until the January 2008 sampling event. 

# 4.0 

# Summary and Conclusions TPH-DRO and PAHs are present in the groundwater beneath the Facility at concentrations that exceed DOH Drinking Water EALs. The quarterly collection and analysis of groundwater samples will continue to monitor the quality of the groundwater located beneath the Facility. Groundwater monitoring reports will be submitted to the DOH upon receipt and evaluation of laboratory analytical results.

F3

# I Legend 

## I • Project Wells Red Hill UST Parcel
40-foot Interval Contour Line Unpaved Road
Road
Stream Red Hill Navy Installation Boundary
Red Hill Tunnels 2254-01 Infiltration Gallery Halawa Correctional Facility Boundary 

# EI Coast Guard
LM Reservation Emd r ~( ~•~"

~~~ ~~- ~ ~

, ). ~. ~,_ ~ ~t r240

L V

1000 ✓

100 

# 100 

# r , ~

,,

10 $ -05 -os - -0 -0 -0 1)ew6 3 p SePA6 2 9
Time (Date) 

## r Time(Date)
—TPHEAL ­1111-TPH-DRO -9-TPH-GRO A TPH-GRO-01 

# I _TPHEAL --W-TPk1-DR0 --fi-TIPH-GROMIDIL 

## Z

/j TPH at RHIVIW01 Quarterly Monitoring Results 

# r—J " a 

# nl yv a L sout

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### Navy Firing 

## 2253-03 R



## _J_' Range
Hala a 

# FV M

" Correctio 

## I

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160 

### OW 

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### DFMWI 2254-01



## ~I ~ 

# ' ' / '

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### Reservat ion.--,
16D 

## I 

## Boundary of Red Hill N

- aval Reservation 0 

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1000

I 

# IM

el 100

10 

### i-aciiiiy

4 

## 0 A


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RHMW02

' 44 

## RHM 

## 01 %%'a e" 

## 'to \ 

## e\

f 

## -~ __~// `.

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# * A

ip 

# N

A

Meters 

## 0 180 360

0 335 670 

# 1,340

Feet 

# Figure 

# 1 TPH Trends in Groundwater Round 

# 10 (January 

# 15, 2008) Red Hill Fuel Storage Facility Oahu, Hawaii~ {~ ;

560 

### Legend

• Project Wells

~ Red Hill UST

~ Parcel
40-foot Interval Contour Line Unpaved Road
Road
Stream

_. _. Red Hill Navy Installation Boundary

~ Red Hill Tunnels 

### 2254-01 Infiltration Gallery



# ~ Halawa Correctional Facility Boundary



# ~ Coast Guard Reservation



## N

Meters 0 180 360

0 335 670 1,340



## Feet

- 

## Figure 2 

# PAH Trends in Groundwater Round 10 (January 15, 2008) Red Hill Fuel Storage Facility Oahu, Hawaii r I

J '•~



## f I ~

~ --~--~ -~~°° n~

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• '' . 2 

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o

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## ',' f
~ r

..

~ I • ~ r ~j~ ~ r 

### ~ l ` ~ J r ~ ! ~ i~.(~ i • r 

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~ 

### Red Hill Oily Waste - fl ` Disposal Facility,

00I

~

o -- Stream Box Culvert
r ~ •. 00 `~ •
-

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## OWDFMW2 -
co 

## 2 ; _

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### ~ 

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### , = NalaWa •

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### ~• , r•~~

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## _ - y

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## - . ® .

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## t it

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## `;i,

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## y

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i ~ ~ 

### H YYa 

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~ o

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### _ 

## RHMW03

_ ~ --~-~ ----- • ~•'~ '~..~ \~~ ~ ~~~I~~ 1 !J(

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, 

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2254-01 ~~ PAHs at RHMW02 Quarterly Monitoring Results

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~ Time (Date) ' ~~ !~ r _' ~.~~.~..~•~ r-
—*-Naphthalene 1-Methylnaphthalene ---2-Methylnaphthalene Naphthalene EAL Methylnaphthalenes EAL

~ 9



### Boundary of Red Hill

~ 

### --- Naval Reservation

## Quarterly Groundwater Monitoring Report

'Red Hill Fuel Storage Facility March 2008


# 5.0 References Dawson Group, Inc. 2006. Fourth Quarter 2005 Groundwater Sampling Report, Red Hill Fuel Storage Facility, Hawaii. February. Hawaii Administrative RuIes, Title 11, Chapter 281, Subchapter 7. State of Hawaii Depattment of Health. 2005a. Screening for Environmental Concerns at Sites with Contaminated Soil and Groundwater, Volume 1: Summary Tier I Lookup Tables. Interim Final. May. State of Hawaii Department of Health. 2005b. Use of 

## May 2005 Environmental Actfon Levels ("EALs") at Leaking Underground Storage Tank Sites. Memo. 15 July. The Environmental Company, Inc. and AMEC Earth & Environmental, Inc. 2005. Red Hill Bulk Fuel Storage Facility Work Plan, Pearl Flarbor, Hawafi. June. The Environmental Company, Inc. 2006. Red Hill Bulk Fuel Storage Facility, Final — Addendum Planning Documents, Pearl Harbor, Hawaii. May. The Environmental Company, Inc. 2007. Red Hill Bulk Fuel Storage Facilfty, Final Technical Report, Pearl Harbor, Hawaii. August. The Environtnental Company, Inc. 2008. Red Hill Bulk Fuel Storage Facility, Final Groundwater Protectfon Plan, Pearl Harbor, Hawafi. January.

11

# Appendix A

Laboratory Analytical Reports

# SGS Environmental Services Alaska Division Level II Laboratory Data Report

, Project: 9121-003 Red Hill BFSF

Client: The Environmental Company, Inc. (TEC) SGS Work Order: 1080224

Released by:

~



### Barbara Hager Alaska Division Project Manager

ConteMe: CoverPage Cese Nanabve Finel Report Pages Qualay Conbol Summary Fonns Chain of Custady/Sample Recelpt Fonns 

# Barbara Hager

2008.02.05 12:12:30 -09'00'

Note: Unless othervnse noted, all qualrt/ essu'ancefquagty control cdleria is in oomphanoe with the standards set forth by the pmper mgulatory authonty, the SGS Quality Assurance Pragram Plan, and the Nabonal Environmental Accreditabon Conference.I 

# CuSIGt

~ 

# S 

# I

:Ilent Name: The Environmental Company, Inc. (TEC) 'ro)ect Name: 9121-003 Red HIII BFSF Norkorder No.: 1080224 

## CASE NARRATIVE Print Date: 215/2008



## Sample Comments
Refer to the Sample reoelpt fonn for information on sample condition.
Lab Samole ID Samole Tvce Client Samole ID 1080224001 PS RHMW2254-WG10

DRO 8015B: The reported resuH is estimated because it is 4 times below the reporting Ilmh. The associated method blank has a estlmated DRO ooncentratlon of 0.096 mg/I. There is no indication of fuel hydrocarbon peaks on the insbument chromatograms. 1080224002 BMS RHMW2254-WG10 MS

8260B - Matnx spike (MS) recovery for 2-chlorotoluene does not meet QC goals (biased high). Refer to LCS for accuracy.
1080224003 BMSD RHMW2254-WG10 MSD

8260B - Matrix spike duplicate (MSD) reoovery for 1,2,4-tnchlorobenzene does not meet QC goals (biased low). Refer to LCS for aocuracy. 

### 1080224005 PS RHMW02-WG10

8015B - Unknown hydrGcarbon with several peaks Is present. 8260B - Continuing calibration verification (CCV) result for n-propylbenzene dld not meet QC goals (biased high). The result for thls analyte is estimated. 8260B - Naph0lalene resu8 Is above the Ilnear range of 70 uglL at 195.48 uglL. Result is esomated. 

### 1080224006 PS RHMWA01-WG10

8015B - Unknown hydrocarbon with several peaks Is presenl. 8260B - ConOnuing calibratron verification (CCV) resuR for n-propylbenzene dld not meet QC goals (biased hlgh). The resutt for thls analyte is es6mated. 8260B - Naphthalene resuh is above the linear range of 70 ug/L at 194.23 uglL. ResuR is estlmated. 

### 1080224007 PS RHMW01-WG10

8015B - Unknown hydrocarbon with severel peaks is present. 8260B - Naphthalene resuR of 5.98 ug/L maybe due to eany over from prevlous sample (1080224-06) which was detected at 194.23 ug/L naphtlialene.
814440 LCS LCS for HBN 196691 [VXX/17866]

AK101 - LCS recovery for GRO does not meet QC goals (biased high). The associated samples were not deteded above the POL for thls analyte.
815216 CCV CCV for HBN 196846 [VMS/9632]

8260B - Con6nuing calibretion veri6oa8on (CCV) resuh for n-propylbenzene, 2chlorotoluene and 1-ohlorohexane did not meet QC goals (blased high). 2-ohlorotoluene and 1-chlorohexane were not detected in the assoclated samples. Resulte for n-propylbenzene may be biased high.

SGS Envlronmentel Sarvreee Inc. 

# ~ Alaeke orvlslon 200 Weet Poltar Drrve Anchorege Alaeka 99518 r ran]I SaJ D3G3 I!A7\ 5e1.53n1 w.ngw enm Member of SGS Group (Soci616 G6n6rala de Surva,llanae)

# Laboratory Analytical Report

Client: ihe Envlronmental Company, Inc.

1001 Bishop Street Ste 1400 ASB Tower Honolulu, HI 96813 Attn: JeH Hart T: (808)528-1445 F:(808)528-0768 tshart@teanc.com Projed: 

### 9121-003 Red HIII BFSF
Workorder Ho.: 

### 1080224

CeNfication: I oertify tltat this data package is in comphance with the tenns and conditions of the contract, both technically and for completeness, other than the oonditions noted on the sample data sheet(s) andlor the case narrative. This eertficaoon applies only to the tested parameters and the specfic sample(s) recetved at the laboratory 

# i Barbara Hager

Barbara Hager 

# 2008.02.05 12:12:44 -
Alaska Division ProjectManager 

# 09'00'

If you have any questlons regarding this report, or d we can be of further assistanoe, please contact your SGS Project Manager.
Mark Abe mark.abe@sgs.00m Project Manager

SGS EnvlronmentelSerWCec Ine IUaske Gnlaion 200 W ast PoUar Odve Rnchorape Alaeka 99518 t IB0'!1 552 2343 f 19071 581 5301 www.us.Ban.com MemDer ol SGS Group

# ~

Pnnt Date: 2/5/2008
EnGosed are the analy8cal results assoclated with thls workorder As required by the state of Alaska and the USEPA, a formal Qualay Assurance/Quality Control Program is maintalned by SGS. A copy of our Qualily Assurance Plan (QAP), whlch outllnes this program is avallable at your request. The laboratory oertification numbers are AK971-05 (DW), UST-005 (CS) and AK00971 (Micro) for ADEC and 001582 for NELAP (RCRA methods: 1010/1020, 1311, 6000l1000, 9040/9045, 9056, 9060, 9065, 80158, 8021B, 8081A/8082, 8260B, 8270C). Exlrept as speclrically noted, all statements and data In thls report are in conformanoe to the provisions set forth by the SGS QAP, the Natlonal Environmental Laboratory Accreditation Program and, when appllcable, other regulatory authorities. If you have 

### any questions regarding thls report or d we can be of any assistanoe, please contact your SGS Project Manager at 907-562-2343.

The following descnptots may be found on your report which wtll serve to further qualdy the data.

MDL Method Deteohon Limit PQL Pracbcal Quantitatlon Limlt (reporting limlt). CL Control Limit u Indicates the analyte was analyzed for but not detected. F Indlcates value thal Is greater than or equal to the MDL. J The quantitation is an estimation. ND Indloates the analyte Is not deteoted B Indicates the analyte is found in a blank associated vnth the sample. ' The analyte has exreeded allowable regulatory or oontrol hmlts. GT GreaterThan LT Less Than Q QC parameter out of aoceptance renge. M A matnx effect was present. E The analyte resuR Is above the callbrated range DF Analytical Dilutlon Factor JL The analyte was posaively Identified, but the quantitation is a low estimation. <Surn Surrogate QC spiked standard
Note: Soil samples are reported on a dry weight basis unless otherwise specified

SGS Env,ronmental Sarvices Inc I Alaeke D,v,e A_ '1,on 200 W est Potter Drive Anchorege Alaeka 99518

~ 10I,>15

~~

7'Id'! r rY^>\ <Ni C1n1 e see nnin Member of SGS Group

### SAMPLE SUMMARY Print Date: 21512008 :Ilent Name: The Environmental Company, Ine. (TEC)

2 rojeot Name: 8121-003 Red Hlll BFSF Norkorder No.: 1080224 

## 4nalytical Methods

dethod Descriotion Analvtical Method 3270 PAH SIM Semi-Vol GC/MS LiqlLlq ext. 8270C SIMS 1FCEE 3.18260 (W) SW8260B )issolved Metals by ICP-MS SW6020 )RO by 8015B (W) SW8015B 3R0 (W) SW8015B 

## Sample ID Cross Reference

Lab SamDle ID Cllent SamDle ID 1080224001 RHMW2254-WG10 1080224002 RHMW2254-WG10 MS 1080224003 RHMW2254-WG10 MSD 1 D80224004 RHMW03-WG10 1080224005 RHMW02-WG10 1080224006 RHMWA01-WG10 1080224007 RHMW01-WG10 

### 1080224008 TB01-WG10

SGS Envlronmentel Sarvicea Inc I Aleaka Drviaion 100 W eat Vottar Drhe Anchorege Aleska 9 B518 ~RpT 5R _~91d9 uRn71 5R1 53 ~ rl1 r rga rnn. MemDar o13G3 Group (Sou6t6 G6n6rele de Suryeillenee)The Environmental Company, Ino. (TEC) Pnnt Date: 215/2008
Cllent Sample ID: RHMW2254-WG70 AII Dateslrimes are Alaska Local Tlme SGS Ref. #: 1080224001 Collectlon DateRme: 01115108 11:30 Pro)ect ID: 9121-003 Red Hill BFSF Receipt DateRme: 01/17108 14:45 Mamx: Water (Surface, EO., Ground)

Dissolved Metals Analvtleal Prop Paramater R eauR PCIUCL MDL Unns DF Batoh Befeh Qualifism

Lead ND 1.00 0.310 ug/L 5 MMS5294 MXX19964
Batoh Informatlon Analytical Batch: MMS5294 Prep Batch: MXX19964 Inkial Prep Wt.Nol.: 50 mL Analytical Method: SW6020 Prep Method: SW3010A Prep Ectract Vol.: 50 mL Analysls DateTme: 01/28/08 12:22 Prep DateTme: 01/24/08 16:35 Container ID:1080224001-G D llutlon Factor. 5 Analyst: TK

SGS Envlronmentel Sarvlcee Ine 

# I Aleeke Divlelon 200 W eat Potter Drive Anehara9e Aleeke 99518 tI90i158223d3 rfl107156t.5301 v 1 Memher ol SGS Group (SOC191B G6n0rela Ee Survelllanee)

# m

A

The Environmental Company, Inc. (TEC) Print Date: 215/2008
Client Sample ID: RHMW2254-WG10 AII DatesrTmes are Alaska Local Tlme SGS Ref. #: 108D224001 Collection DateTme: 01115108 11:30 Pro)ect ID: 9121-003 Red HIII BFSF Receipt DateTme: 01/17/OS 14:45 Matnx: Water (Surface, EB., Ground)

Volatile Fuels Department

Parametar
Gasollne Range Olganics 4-Bromofluorobenzene <sum
Batchlnfonna0on Analytica l Prec Resuk PQLICL MDL Unk s DF Batch Batch

ND 100 10.0 ug/L 1 VFC8836 VXX17866 102 50-150 % 1 VFC8836 VXX17866 uall6ers

AnalyBcal Batch: VFC8836 Prep Batch: VXX17866 Initial Prep W[Nol.: 5 mL Analytical Method: SW8015B Prep Method: SW5030B Prep Extract Vol.: 5 mL Analysis DateTme: 01/23/08 10:47 Prep Datelrlme: 01/23/08 08:00 Contalner ID:1080224001-A D ilution Factor: 1 Analyst: HM

SGS Envlronmanlel8ervlcee Ine 

# I Aleake Divlclun 200 W ee1 Potter Drive Anchorape Aleeke 99515 l ! f9011 583 4i<9 r 19011 581 i5301 r MemEar of SGS Group (Socl9td G6nArale Ee Survelllence)

# ~ ~

.

The Environmental Company, Inc. (TEC) Print Date: 215/2008

Client Sample ID: RHMW2254-WG10 SGS Ref. #: 1080224001 Project ID: 9121-003 Retl Hill BFSF Matrix: Water (Surface, Eff., Ground)

Semlvolatlle Organio Fuels Department

Parameter Result

Diesel Range Organlcs 0.102 J 5a Androstane <surrn 82.5
Batoh Informatlon AII DatesTmes are Alaska Local Time Collection Datelrfine: 01/15108 11:30 Recelpt DateTme: 01l17108 14:45



### EOP!7M9i?L EM PQLJCL MDL Units DF Batch Batch

0.412 0.0825 mglL 1 XFC7831 XXX19058 

### 50-150 % 1 XFC7831 XXX19058 ualMlers

Analyllcal Batch: XFC7831 Prep Batch: XXX19058 Initlal Prep Wt.Nol.: 970 mL Analytical Method: SW8015B Prep Method: SW3520C Prep Extract Vol.: 1 mL Analysis Date/Time: 01130/08 12:35 Prep DateTme: 01/22/08 08:30 Container ID:1080224001-H Dilution Factor: 1 Analyst: BME

SGS Envlronmental Servlces Inc I Alaeka Dlvlslon 200 W eel Putter Drlre Anchorage Aleska 99513 l [190)I58?

~ 933 rl90115d15301 r MamCer of SGS Group (Socl6t4 G6nArala de Survalllence)

# ~

The Environmental Company, Inc. (TEC) Print Date: 2/5/2008

Cllent Sample ID: RHMW2254-WG70 SGS Ref. #: 1080224001 Project ID: 9121-003 Red HIII BFSF Matrlx: Water (Surfaoe, Eff., Ground)

Volatile Gas Chromatography/Mass Spectroscopy

Parameter Resul AII Dates?mes are Alaska Local Time Collection Date/Tme: 01115/08 11:30 Receipt DateTme: 01/17/08 14:45

AnaMleal PreD PQUCL MDL Units DF Batch Batch QualMiecs

Benzene ND 0.400 0.120 ug/L 1 VMS9632 VXX17871 Toluene ND 1.00 0.310 uglL 1 VMS9632 VXX17871 Ethylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS9832 VXX17871 1,2-Dlchloroethane ° ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Chlorobenzene ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS9832 VXX17871 cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 4-IsopropyMoluene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Styrene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Dibromomethane ND 1.00 0.310 ug/L 1 VMS9832 VXX17871 trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1,2,2-Tetrrachloroethane ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS9632 VXX17871 Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS9632 VXX17871 Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS9632 VXX17871 1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Carbontetrachlonde ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 Chloroform ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Bromobenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Chloromethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2,3-Tnchloropropane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Bromomethane ND 3.00 0.940 ug/L 1 VMS9632 VXX17871 Bromoldtloromethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Vinyl chlonde ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Chlorcethane ND 1.00 0.310 ug/L 1 VMS9832 VXX17871

SGS Envlronmenlal5ervlcee Inc I Aleeke Divlelun l(8071582.2343 200 W asl Potter Driva /190115815301 Anchurage Alaeke 99 51 8
r Membar of SGS Group (SocIAtA G9n9rale tleaSurvelllence)

# EHEI

The Envlronmental Company, Inc. (TEC) Print Date: 2/5/2008

Client Sample ID: 

### RHMW2254-WG70 AII Dataslflmes are Alaska Local Tlme SGS Ref. #: 1080224001 Collection Datefrime: 01/15108 11:30 Project ID: 9121-003 Red HIII BFSF Recelpt Data/Tlme: 01/17/08 14:45 MaVix: Water (Surface, Eff., Ground)



### Volatile Gas Chromatography/Mass Spectroscopy Analvtical Preo Parameter Rgsult POUCL 

### MDL Units 

### OF Batch 

### Bateh Qualiflem sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 1,1-Dlchloroethene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS9632 VXX17871 Methylene chlonde ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Tnchlorofluoromethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 P 8 M-Xylene ND 2.00 0.620 ug/L 1 VMS9632 VXX17871 Naphthalene ND 1.00 0.620 ug/L 1 VMS9632 VXX17871 o-Xylene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Bromoform ND 1.00 0.500 ug/L 1 VMS9632 VXX17871 1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1,1-Tdchloroethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS9632 VXX77871 Tdchloroethene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 trans-1,2-Dlchloroethene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2-Dichlorobenzene ND 1.00 0310 ug/L 1 VMS9632 VXX17871 2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Hexachlorobutadlene ND 0.800 0.180 ug/L 1 VMS9632 VXX17871 Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2,3-Tnchlorobenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2-Dlchloroethane-D4 <surr> 105 73-120 

### % 1 VMS9632 VXX17871 Toluene-08 <sum 104 80-120 

### % 1 VMS9632 VXX17871 4-Bromofluorobenzene <surr> 107 76-120 

### % 1 VMS9632 VXX17871

Batch Informatlon Analytical Batch: VMS9632 Prep Batch: VXX17871 Initlal Prep Wt.Nol.: 5 mL Analytical Method: SW8260B Prep Method: SW5030B Prep Extract Vol.: 5 mL Analysls Datelrlme: 01129/08 20:37 Prep Date/Tlme: 01/29/08 14:08 Container ID:1080224001-D Dilutlon Factor. 1 Analyst: DSH

SGS Enrlronmental Servicee Inc 

## I Aleeka Dlvlelen 2gg W eal Poller Drlve Anehorage Aleske 98518 I.1190]I582 23C3 /l90]1581.5301 ww, v sge ca
T MemGer of SGS Group (SoclOt6 G9n9rale tla Survelllance)

# ~

The Environmental Company, Inc. (TEC) Pdnt Dale: 2/5/2008
Clienl Sample ID: RHMW2254-WG10 AII DateslTmes are Alaska Local Time SGS Ref. #: 1080224001 Collection DateRme: 01115/08 11:30 Projecl ID: 9121-003 Red Hill BFSF Receipt Date/Time: 01117/08 14:45 MaVix: Water (Surface, Eff., Ground)

Polynuclear Aromatics GC/MS Analvtical Preo Parameter Result P GLICL MDL Units DF Bateh Batch Qualiflem
Acenaphthylene ND 0.0500 0.0150 ug/L 1 XMS4385 XXX19059 Acenaphthene ND 0.0500 0.0150 ug/L 1 XMS4385 XXX19059 Fluorene ND 0.0500 0.0150 ug/L 1 XMS4385 XXX19059 Phenanthrene ND 0.0500 0.0150 ug/L 1 XMS4385 XXX19059 Anthracene ND 0.0500 0.0150 ug/L 1 XMS4385 XXX19059 Fluoranlhene ND 0.0500 0.0150 ug/L 1 XMS4385 XXX19059 Pyrene ND 0.0500 0.0150 ug/L 1 XMS4385 XXX19059 Benzo(a)Anthracene ND 0.0500 0.0150 uglL 1 XMS4385 XXX19059 Chrysene ND 0.0500 0.0150 uglL 1 XMS4385 XXX19059 Benzo[b]Fluoranthene ND 0.0500 0.0150 ug/L 1 XMS4385 XXX19059 Benzo[k]Ouoranthene ND 0.0500 0.0150 uglL 1 XMS4385 XXX19059 Benzo[a]pyrene ND 0.0500 0.0150 uglL 1 XMS4385 XXX19059 Indeno[1,2,3-c,d] pyrene ND 0.0500 0.0150 uglL 1 XMS4385 XXX19059 Dlbenzo[a,h]anthmcene ND 0.0500 0.0150 ug/L 1 XMS4385 XXX19059 Benzo[g,h,i]perylene ND 0.0500 0.0150 uglL 1 XMS4385 XXX19059 Naphthalene ND 0.100 0.0310 uglL 1 XMS4385 XXX19059 1-Methylnaphthalene ND 0.0500 0.0150 uglL 1 XMS4385 XXX19059 2-Methylnaphthalene ND 0.0500 0.0150 ug/L 1 XMS4385 XXX19059 Terphenyl-014 <sum 81 50-135 % 1 XMS4385 XXX19059
Batch Informatlon Analylical Batch: XMS4385 Prep Batch: XXX19059 Initlal Prep Wt.Nol.: 1000 mL Analybcal Method: 8270C SIMS Prep Method: SW3520C Prep Exbact Vol.: 1 mL Analysis Datelfime: 01128/08 13:31 Prep Dalelfime: 01/22108 08:50 Contalner ID:1080224001-J D llution Factor: 1 Analyst: WAA

SGS Environmenlal Sarvlcaa Inc Alaeka Divlelon 0 W eat Potter Drlve AneOnrage Aleske 99518 r(t071582 23<3 f ]0 IN0>1581.5101 v xsQe cem MemberofSGS Group (Socl6l6 G6n6rele Ge Surveillence). .•

The Environmental Company, Ine. (TEC) Pnnt Date: 21512008

Client Sample ID: RHMW03-WG10 SGS Ref. #: 1080224004 Project ID: 9121-003 Red Hill BFSF Matnx: Water (Surface, Eff., Ground)

Dlssolved Metals

Parameter Resuk

Lead ND


### Batchlnformatlon AII Dates/Times are Alaska Local Tlme Collection Date/Time: 0111510813:15 Receipt DateTme: 01117/08 14:45

Analvkeal PreD PQLICL MDL Unks DF Batch Batch

1.00 0.310 ug/L 5 MMS5294 MXX19964 

### ualkiars

Analytical Batch: MMS5294 Prep Batch: MXX19964 Initial Prep Wt.Nol.: 50 mL Analytical Method ,

SW6020 Prep Method: SW3010A Prep Extract Vol.: 50 mL Analysis DateRme: 01128/08 13:39 Prep Date/Time: 01124/08 16:35 Contalner ID:1080224004-G D ilutlon Factor. 5 Analyst: TK

SGS Envlronmenlal Servlces Inc 

# ~ Aleeka Dlvlslon 700 W eat Potter Drlve Anchorage Aleeka 98518 t(9n11 552 23<3 f 190)1 551 5301 www.ua.ana

~ n MemOer of SGS Group (Soc1916 G9n9rale Ee Survelllanee)

# EEI

The Environmental Company, Ino. (TEC) Pdnt Date: 2!512008

Client Sample ID: RHMW03-WG10 SGS Ref. #: 10802240D4 Project ID: 9121-003 Red HIII BFSF Matnx: Water (Surface, Eff., Ground)

Volatile Fuels Department

Parameter AII Dates/Times are Alaska Local Tlme Colledlon DatelTime: 01115108 13:15 Rewlpt DatelTlme: 01117/08 14:45

Analvtleal Preo Reau PQLIC MDL Unhs DF Batch Bateh Quali6ers

Gasoline Range Organics ND 100 10.0 ug1L 1 VFC8836 VXX17866 4-Bromofluorobenzene <surr> 105 50-150 % 1 VFC8836 VXX17866
Batch IMorrnatlon Analyhcal Batch: VFC8836 Prep Batch: VXX17868 Initial Prep Wt.Nol.: 5 mL Analytical Method: SW8015B Prep Method: SW5030B Prep ExVact Vol.: 5 mL Analysis DateTme: 01/23108 11:42 Prep Datefrime: 01/23/08 08:00 Container ID:1080224004-A Dllution Factor: 1 Analysl: HM

SGS Envlronmentel5ervlcee Inc 

# I
Alecke Divlelon 200 W aet Potter Drive Anchore9e Alacka 99518 1l98]I582 23A3 I(98]1561.530t ur u ue eae com MemCer of SGS Group (Socl6t6 G9n9mle tle Survalllenca)

# Em

The Environmental Company, Inc. (TEC) Print Date: 2/512008

Client Sample ID: RHMW03-WG10 SGS Ref. #: 1080224004 Project ID: 9121-003 Red Hill BFSF Maoix , Water (Surface, Eff., Ground)

Semivolatlle Organic Fuels DepartmeM

Parameter
Dlesel Range Organics 5a Androstane <sum
Batch Infonnadon AII DateslTlmes are Alaska Local Time Collection DateTme: 01115/08 13:15 Recelpt Date/Tfine: 01117/08 14:45

Analvtiwl Pren Result PQUCL MDL UnRs DF Batch Batch

0.242 J 0.435 0.0870 mg/L 1 XFC7831 XXX19058 87 50-150 % 1 XFC7831 XXX19058 uallflers

Analytical Batch: XFC7831 Prep Batch: XXX19058 Initial Prep WtJVoI.: 920 mL AnalyYlcal Method: SW8015B Prep Method: SW3520C Prep ExVact Vol.: 1 mL Analysls DatelTme: 01/30/08 13:04 Prep Date/Tlme: 01/22/08 0890 Contalner ID:1080224004-H D ilution Factor. 1 Analyst: BME

SG8 Environmental 8ervicee Inc 

# I
Aleaka Divlalon 0 eat Potter Drlve Anchera9e Aleske 99518 r(90]55B449[3 20 (lP0 W 1)581.5vn1 v a.eae.nom MemDer of SGS Group (Sec14t! G9n9rale ae Survelllance)The Environmental Company, Inc. (TEC) Print Date: 2/5/2008

Cllent Sample ID: RHMW03-WG70 SGS Ref. #: 1080224004 Project ID: 9121-003 Red HIII BFSF Matrix: Water (Surface, Eff., Ground)

Volatlle Gae Chromatography/Mass Spectroscopy

Parameter Resutt AII DatesTmes are Alaska Local Time Collection Date/Tlme: 01/15/08 13:15 Recelpt Datelrlme: 01/1710814:45

Analvtical PreD POL/C MDL Unite DF Bateh Batch QuallBera

Benzene ND 0.400 0.120 ug/L 1 VMS9632 VXX17871 Toluene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Ethylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1.4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 1,2-Dlchloroethane ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Chlorobenzene ND 0.500 0.150 ugfL 1 VMS9632 VXX17871 4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 uglL 1 VMS9632 VXX17871 cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 4-Isopropyttoluene ND 1.00 0.310 uglL 1 VMS9632 VXX17871 cls-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Styrene ND 1.00 0.310 ug1L 1 VM89632 VXX17871 Dlbromomethane ND 1.00 0.310 ug/L 1 VMS9632 VXX77871 trans-1,3-Dlohloropropene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2,4-Trichlorobenzene ND 1.00 0.310 ug1L 1 VMS9632 VXX77871 1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug1L 1 VMS9632 VXX17871 1,2-Dlbromo-3chloropropane ND 2.00 0.620 ug1L 1 VMS9632 VXX17871 Methyl-t-butyl ether ND 5.00 1.50 ug1L 1 VMS9632 VXX17871 Tetrachloroethene ND 1.00 0.310 ug1L 1 VMS9632 VXX17871 Dlbromochloromethane ND 0.500 0.150 uglL 1 VMS9632 VXX77871 1,3-Dichloropropane ND 0.400 0.120 ug1L 1 VMS9632 VXX17871 1,2-Dibromoethane ND 1.00 0.310 ug1L 1 VMS9632 VXX17871 Carbon tetrachloride ND 1.00 0.310 ug/L 1 VM89632 VXX17871 1,1,1,2-TetrachlorGethane ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 Chlorofonn ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Bromobenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Chloromethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2,3-Tnchloropropane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Bromomethane ND 3.00 0.940 ug/L 1 VMS9632 VXX17871 Bromochloromethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Vlnyl chlodde ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Dichlorod10uoromethane ND 1.D0 0.310 ug/L 1 VMS9632 VXX17871 Chloroethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871

SGSEnvlronmenlalServleeslnc Al9skeDlvislon 98]1582 23d3 200WeetPollerDrlveAnckara9eAleska9951a

f(99]I 581.5381 w MemGer of sGS Group (SociAtA GAnArele tle Surva,llanca)

# ~ . .



### The Envlronmental Company, Inc. (TEC) Print Date: 2/512008

Client Sample ID: RHMW03-WG70 AII DatesTmes are Alaska Local Time SGS Ref. #: 1080224004 Collectfon DateTme: 01/15/08 13:15 Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 01/17/08 14:45 Matnx: Water (Surface, Eff., Ground)

Volatlle Gas ChromatographyfMass Spectroscopy AnaMlwl Preo Parameter Reault POLICL MDL Units DF Batch Batch Qualiflem sec-Butylbenzene ND 1.00 0.310 uglL 1 VMS9632 VXX17871 Bromodichloromethane ND 0.500 0.150 uglL 1 VMS9632 VXX17871 1,1-Dichloroethene ND 1.00 0.310 uglL 1 VMS9632 VXX17871 2-Butanone (MEK) ND 10.0 3.10 uglL 1 VMS9632 VXX17871 Methylene chlonde ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 P 8 M-Xylene ND 2.00 0.620 ug/L 1 VMS9632 VXX17871 Naphthalene ND 1.00 0.620 ug/L 1 VMS9632 VXX17871 o-Xylene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Bromofonn ND 1.00 0.500 uglL 1 VMS9632 VXX17871 1-Chlorohexane ND 1.00 0.310 uglL 1 VMS9632 VXX17871 1,2,4-Tnmethylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1,1-Tnchloroethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1-Dlchloroethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Trichloroethene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 trans-1,2-Dlchloroethene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2-Dlchlorobenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 2,2-Dichloropropane ND ' 1.00 0.310 ug/L 1 VM89632 VXX17871 Hexachlorobutadlene ND 0.600 0.180 ug1L 1 VMS9632 VXX17871 Isopropylbenzene (Cumene) ND 7.00 0.310 ug/L 1 VMS9632 VXX17871 1,2-Dlchloropropane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,3-Dlchlorobenzene ND 1.00 0.310 uglL 1 VMS9632 VXX17871 1,2,3-Tnchlorobenzene ND 1.00 0.310 uglL 1 VMS9632 VXX17871 1,2-Dlchloroethane-D4 <surrn 102 73-120 % 1 VMS9632 VXX17871 Toluene-d8 <sum 103 80-120 % 1 VMS9632 VXX17871 4-Bromofluorobenzene <sum 105 76-120 % 1 VMS9632 VXX17871
Batch Informetlon Analytical Batch: VMS9632 Prep Batch: VXX17871 Inibal Prep Wt.Nol.: 5 mL Analytical Method: SW8260B Prep Method: SW5030B Prep Ectract Vol.: 5 mL Analysls Date/Tlme: 01/29/08 21:08 Prep Datelfime: 01/29/08 14:08 Container ID:1080224004-D Dilufion Factor. 1 Analyst: DSH

SGS Environmenlel Servlcas InG I Alaske Dlvlslon 200 W ael Potler Drlve Anchorege Aleeka 99518

~ tI90j158243<3 /19n)1561.5301 vw.vgw.com Member of SGS Group (BocIAtA mletl Gdn9a Survaillenee)

# E

The Environmenta[ Company, Inc. (TEC) Pnnt Date: 2/5/2008

Client Sample ID: RHMW03-WGf 0 AII DatesTmes are Alaska Local Tlme SGS Ref. #: 1080224004 Collection DateRme: 01/15/08 13:15 ' Projed ID: 9121-003 Red Hill BFSF Receipt DateTme: 01/17/08 14:45 Matriz: Water (Surtaoe, Eff., Ground)

Polynuelear Aromatics GC/MS Anelvticel ) areo Parameter Raauh PQLICL MDL Units DF Batoh Batoh Qualiftem

Acenaphthylene ND 0.0521 0.0156 uglL 1 XMS4385 XXX19059 Aoenaphthene ND 0.0521 00156 ug/L 1 XMS4385 XXX19059 Fluorene ND 0.0521 0.0156 uglL 1 XMS4385 XXX19059 Phenanthrene ND 0.0521 0.0156 uglL 1 XMS4385 XXX19059 Anthracene ND 0.0521 0.0156 uglL 1 XMS4385 XXX79059 Fluoranthene ND 0.0521 0.0156 ug/L 1 XMS4385 XXX19059 Pyrene ND 0.0521 0.0156 uglL 1 XMS4385 XXX19059 Benzo(a)Anthracene ND 0.0521 0.0166 uglL 1 XMS4385 XXX19059 Chrysene ND 0.0521 0.0156 uglL 1 XMS4385 XXX19059 Benzo[b]Fluoranthene ND 0.0521 0.0156 uglL 1 XM94385 XXX19059 Benzo[k]fluoranthene ND 0.0521 0.0156 ug/L 1 XMS4385 XXX19059 Benzo[a]pyrene ND 0.0521 0.0156 uglL 1 XMS4385 XXX19059 Indeno[1,2,3-c,d] pyrene ND 0.0521 0.0156 uglL 1 XMS4385 XXX19059 Dibenzo[a,h]anthraoene ND 0.0521 0.0156 uglL 1 XMS4385 XXX19059 Benzo[g,h,l]perylene ND D.0521 0.0156 uglL 1 XMS4385 XXX19059 Naphthalene ND 0.104 0.0323 uglL 1 XMS4385 XXX19059 1-Methylnaphthalene ND 0.0521 0.0156 ug1L 1 XMS4385 XXX19059 2-Methylnaphthalene ND 0.0521 0.0156 uglL 1 XMS4385 XXX19059 Telphenyl-d14 <surrn 90.8 5D-135 % 1 XMS4385 XXX19059
Batch Infonnaffon Analytical Batch: XMS4385 Prep Batch: XXX19059 Initlal Prep Wt.Nol.: 960 mL Analytical Method: 8270C SIMS Prep Method: SW3520C Prep Extract Vol.: 1 mL Analysis Date/Tme: 01/28108 15:10 Prep Date/Time: 01122/08 08:50 Container ID:1080224004-J Dilution Factor. 1 ' Analyst: WAA

SGS Envlronmental Sarvlcea Inc 

# I Aleaka Divlalon 200 W ast Potter Drlve AncboraBe Alaeka 99515 l Il90]1583 23A3 Il9011581 5301 r Member uf SGS Group (Soc14tA GAnArele de Survelllenea). n

The Environmental Company, Inc. (TEC) Print Date: 215l2008
ClientSamplelD: RHMW02-WG10 SGS Ref. #: 1080224005 ProJect ID: 8121-003 Red Hill BFSF Matnx: Water (SurFaoe, Eft., Ground)

Dissolved Metals

Parameter

Lead
Batch Iniormaaon Analylical Batch: MMS5294 Analyfical Method: SW8020 Analysis Date/Time: 01/28108 13:45 Dllution Factor. 5 AII Datesmmes are Alaska Local Tlme Collechon DateTme:01/15/08 14:45 Receipt Date/Tlme: 01/17108 14:45

Analvtical Pmp Rasult P LICL MDL Units DF Batch I;atoh Qualiflem

ND 1.00 0.310 ug/L 5 MMS5284 MXX19984

Prep Batch: MXX19964 Initlal Prep Wt.Nol.: 50 mL Prep Method: SW3010A Prep Extract Vol.: 50 mL Prep Date/Tlme: 01/2410816:35 Container ID:1080224005-G Analvst: TK

SGS Environmental Servlcee Inc 

# I Aleske Divla 5e24lon 200 W est Patter Drlve Ancborape Ala9ka 99515 l 1 f99]13l3 / f9911581.5301 v Member ul SGS Grcup (SoelAlA G6n9rele Ga Survelllance)

# ~

The Environmental Company, Inc. (TEC) Print Date , 21512008
Client Sample ID: RHMW02-WG10 SGS Ref. #: 1080224005 ProJect ID: 9121-003 Red Hill BFSF Matnx: Water (Surfaoe, Eff., Ground)

Volatlle Fuels Department

Parameter AII Dates/Tlmes are Alaska Local Time Collection Date/Tlme: 01/15/08 14:45 Recelpt Dalefrlme: 01117/08 14:45

Analvticat Pfeo Resu POLICL MDL Units DF Bateh Bateh QuallBen
Gasoline Range Organlcs 64.3 J 100 10.0 uglL 1 VFC8836 VXX17866 4-Bromofluorobenzene <sum 

### 115 50-150 % 1 VFC8836 VXX17866
Batch Informauon AnalyBcal Batch: VFC8836 Prep Batch: VXX17866 InfBal Prep Wt.Nol.: 5 mL AnalyBeal Method: SW8015B Prep Method: SW5030B Prep Extract Vol.: 5 mL Analysls Date/Tlme: 01123/08 12:00 Prep Date/Tlme: 01/23/08 08:00 Contalner ID:1080224005-A D llutlon Factor: 1 Analyst: HM

SGS Envlrenmental Servlcee Ine I Aleeke Divlelon 200 W esl Potter Drive Anchura9e Alaska 99519 1190]158F 23A3 I(9071561 5301 v Member of SGS Group (Soclbt6 G6n6rale Ee Surveillance)

# ~

The Environmental Company, Inc. (TEC) Print Date: 2/512008

Chent Sample ID: RHMW02-WG10 AII Dates/Tlmes are Alaska Local Time SGS Ref. #: 1080224005 Collection DateRme: 01/15/08 14:45 Project ID: 9121-003 Red Hill BFSF Reoeipt Date/Time: 01/17108 14:45 Matnx: Water (Surface, Eff., Ground)

Semivolatile Organic Fuels Department

Parameter Result
Dlesel Range Organics 2.31 5a Androstane <sum 84.6
BaMh Informa6on AnalyBcal Batch: XFC7831 AnalyBcal Method: SW80158 Analysis Date/Tlme: 01/30/0813 , 14 Dilution Factor 1 Analvtical Preo P UCL MDL Units DF Ba ch Batch Qualifters

0.426 0.0851 mg/L 1 XFC7831 XXX19058 

### 50-150 % 1 XFC7831 XXX19058

Prep Batch: XXX19058 Inibal Prep Wt Nol.: 940 mL Prep Method: SW3520C Prep Extract Vol.: 1 mL Prep Date/Tlme: 01122108 08:30 Container ID:1080224005-H

SGS Environmentel Servlces Inc I Aleaka Divlelan 0 eat Potter Drive Anchorepe Aleaka 99518 t190)1 5e293A3 20 f190 W )1581.5001 w 1 Member af SGS Group (SacIAtB GAnBrele tle Survelllance)

# F

- MA

The Environmental Company, Inc. (TEC) Pnnt Date: 2/512008

Chent Sample ID: RHMW02-WG10 SGS Ref. #: 1080224005 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Volatile Gas Chromatography/Mass Spectroscopy

Parameter Resuk AII Dates/Tmes are Alaska Local Time Collection Date/Tme: 01115/08 14:45 Receipt DateRme: 01/17/08 14•45

Anatvtical Pro8 PQLJC MDL Unhs DF Batch Batch QuallOere

Benzene 0.170 J 0.400 0.120 ug/L 1 VMS9632 VXX17871 Toluene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Ethylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 n-Butylbenzene 8.75 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,4-Dlchlorobenzene ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 1,2-Dlchloroethane ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Chlorobenzene ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS9632 VXX17871 cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 44sopropyltoluene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 cls-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 n-Propylbenzene 12.8 1.00 0.310 ug/L 1 VMS9632 VXX17871 Styrene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Dibromomethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 trrans-1,3-Dlchloropropene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2,4-Tnchlorobenzene ND 1.00 0.310

, ug/L 1 VMS9632 VXX17871 1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 1,2-Dlbromo-3chloropropane ND 2.00 0.620 uglL 1 VMS9632 VXX17871 Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS9632 VXX17871 Te6rachloroethene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS9832 VXX17871 1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Carbon tetrachlonde ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1,12-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 Chloroform ND 1.00 0.310 ug/L 1 VM89632 VXX17871 Bromobenzene ND 1.00 0.310 uglL 1 VMS9632 VXX17871 Chloromethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Bromomethane ND 3.00 0.940 ug/L 1 VM89632 VXX17871 Bromochloromethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Vlnyl chloride ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Dtchlorodi6uoromethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Chloroethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871

SGS Envlronmenlal Sarvlcae Inc 

# I
Aleake Givlelnn 1(98]) 582.23<3 29U W eel Potter Drive Ancaorage Aleeke 99518 !(Q81) 581 5381 w

, MemEer of SGS Group (Socl6t6 G6n6rale tle Survelllance)I

The Environmental Company, Inc. (TEC) Pnnt Date: 215/2008
Cllent Sample ID: RHMW02-WG10 AII Dates/Times are Alaska Local Tlme SGS Ref. #: 1080224005 Colledlon Date/Time: 01115/08 14:45 Project ID: 9121-003 Red Hill BFSF Receipt Date(rime: 01/17/08 14:45 Matnx: Water (Surfaoe, Eff., Ground)

Volatile Gas Chromatography/Mass Spectroscopy 

### AnaMlcal 

### EM Parameter , Result PQUCL MDL Units DF Batah Batoh Quallflem seo-Butylbenzene 7.38 1.00 0.310 ug/L 1 VMS9632 VXX17871 Bromodlchloromethane ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS9632 VXX17871 Methylene chloride ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Trichloro0uoromethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 P& M-Xylene ND 2.00 0.620 ug/L 1 VMS9632 VXX17871 Naphthalene 195 1.00 0.620 ug/L 1 VM89632 VXX17871 o-Xylene 1.06 1.00 0.310 ug/L 1 VMS9632 VXX17871 Bromoform ND 1.00 0.500 ug/L 1 VMS9632 VXX17871 1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2,4-Tdmethylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 tert-Butylbenzene 1.15 1.00 0.310 ug/L i VMS9632 VXX17871 1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1-Dlchloroethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 2-Chlorololuene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Tdchloroethene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Hexachlorobutadlene ND 0.600 0.180 ug/L 1 VMS9632 VXX17871 Isopropylbenzene (Cumene) 5.33 1.00 0.310 ug/L 1 VMS9832 VXX17871 1,2-Dlchloropropane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1-Dlchloropropene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2,3-Tnchlorobenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2-Dlchloroethane-04 <surr> 103 73-120 % 1 VMS9632 VXX17871 Toluene-d8 <sum 94.4 80-120 % 1 VMS9632 VXX17871 4-Bromofluorobenzene <surrn 106 76-120 % 1 VMS9632 VXX17871
Batch Informaticn Analytical Batch• VMS9632 Prep Balch: VXX17871 In18al Prep WtJVoI.: 5 mL AnalytlGal Method: SW8260B Prep Method: SW50308 Prep Exfract Vol.: 5 mL Analysis DatelTlme: 01/29108 21:39 Prep Datelrlme: 01/29108 14:08 Container ID:1080224005-D D flutlon Factor: 1 Analyst: DSH

SGSEnvlronmentalServicealnc I AleskeDlvlslon 200WestPotlerDrlveAnchoregeAleeke99518

~ t 190)f 584?4<3 1(997) 551.5301 v a a0w.com Member of SGS Group (SocIAIA Gbn9rale Ee Survelllsnee)

# ~

,

The Environmental Company, Inc. (TEC) Pnnt Date: 21512008

Client Sample ID: RHMW024VG10 AII Dates?mes are Alaska Local Time SGS Ref. #: 1080224005 Collecfion DateTme• 01/15/08 14:45 Project ID: 9121-003 Red Hill BFSF Recelpt DateRme: 01/17/08 14:45 Matrix: Water (Surface, Eff., Ground)

Polynuclear Aromatics GCIMS 

### Analvtical 

### plgg Parameter Result PQUCL MDL Unha DF Bateh Bateh Quallaers

Acenaphthylene ND 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Acenaphthene 0.308 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Fluorene 0.161 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Phenanthrene ND ' 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Anthracene ND 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Fluoranthene ND 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Fyrene ND 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Benzo(a)lnthracene ND 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Chrysene ND 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Benz.o[b]Fluoranthene ND 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Benzo[k)fluorenthene ND 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Benzo[a]pyrene ND 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Indeno[1,2,3-c,d] pyrene ND 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Dibenzo[a,h]anOvacene ND 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Benzo[g,h,l]perylene ND 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Naphthalene 93.6 5.26 1.63 ug/L 50 XMS4386 XXX19059 1-Methylnaphthalene 67.0 2.63 0.789 ug/L 50 XMS4386 XXX19059 2-Methylnaphthalene 23.8 2.63 0.789 ug/L 50 XMS4386 XXX19059 Terphenyl-d14 <surr> 88.4 50-135 % 1 XMS4385 XXX19059
Bateh Informa0on Analytical Batch: XMS4385 Prep Batch: XXX79059 Initial Prep Wt.Nol.: 950 mL Analybcal Method: 8270C SIMS Prep Method: SW3520C Prep Exlract Vol.: 1 mL Analysis Date(flme: 01/28/08 15:42 Prep Datefrime: 01122108 08:50 Container 10:1080224005-J Ddubon Faotor: 1 Analyst: WAA Analybcal Batch: XMS4386 Prep Batch: XXX19059 Initial Prep Wt.Nol.: 950 mL Analy6cal Method: 8270C SIMS Prep Method: SW3520C Prep Exlract Vol.: 1 mL Analysis Datelrime: 01/28/08 21:20 Prep Date/Tlme: 01122108 08:50 Contalner ID: Ddution Factor: 50 Analyst: WAA

SGS Envlronmental Servlcae Inc I AlaekeDivlelon 200 W est pattar Drlva Anchorage Alaeke 99518 l t 190)1 584

~ 3d3 r r9811 581.5301 v MemberafSGS Group (Snc1619 G9n9rale tle Survelllence)The Environmental Company, Inc. (TEC) Print Date: 2I5/2008

Cllent Sample ID: RHMWA01-WG70 SGS Ref. #: 1080224006 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, ER., Ground)

Dissolved Metals

Parameter

Lead

Batch Informatlon Analytieal Batch: MMS5294 Analytical Method: SW6020 Analysis Date/Tlme: 01/28/08 13:54 Dilution Factor: 5 AII Dates(rlmes are Alaska Local Time Collection DatelTme:01/15/08 13:05 Receipt Date/Time: 01/17/08 14:45

Analytical Pmp Resul t PLILICL MDL UnMs DF Batch Batch Qualiflers

ND 1.00 0.310 ug/L 5 MMS5294 MXX19964

Prep Batch: MXX79964 Inrttal Prep Wt.Nol.:50 mL Prep Method: SW3010A ' Prep 6ctrad Vol.: 50 mL Prep Datelflme: 01/24/08 16.35 Container ID:1080224006-G Analyst: TK

SGS Environmentel Servlcea Inc 

# I Alaeke Dlvlslun 200 W esl Putter Drive Anehora9e Alaska 99513 11a0)15842369 r190115815301 www.us.aes.cam Member ol SGS Group (Soc191A G6n6rele Ee Survalllance)

# ~

The Environmental Company, Inc. (TEC) Pnnt Date: 2/512008
Cllent Sample ID: RHMWA01-WG10 AII Dates/Tlmes are Alaska Local T1me 

### SGS Ref. #: 1080224006 Collection DatelTlme: 01115/08 13:05 Project ID: 9121-003 Red HIII BFSF Receipt Datelrlme: 01/17/08 14:45 Matr1x: Water (Surface, Eff., Ground)

VolaUle Fuels DepaRment

Paramatar
Gasollne Range Organice 4-BromoOuorobenzene <surr>
Batch IMormarlon AnalyBcal Batch: VFC8836 AnalyOcal Method: SW8015B Analysis DateTme: 01/2310812:18 Dllutlon Factor: 1 AnalvOcal Prop Result PQVCL MDL Units DF Batch Ba ch Quallfiers

66 2 J 100 10.0 ug/L 1 VFC8836 VXX17866 

### 117 50-150 % 1 VFC8836 VXX17866

Prep Batch: VXX17866 Initial Prep WtNol.: 5 mL Prep Method: SW5030B Prep Extract Vol.: 5 mL Prep Datelrime: 01123/08 08:00 Container ID:1080224006-A Analvst: HM

SGS Envlranmental Sarvlcea Inc I Aleeke Divlelun 200 W esl Potter Drive Anchurage Alaeke 99518 l 1 f90>1 RR2R3e3 f 1907I5615301 v aaQn cem MemDer of SGS Grnup (SncIRtR G4n9rale tle Survelllence)

# M 6 

# GES mi . ,.

The Environmental Company, Inc. (TEC) Pnnt Date: 2/5/2008
Cllent Sample ID: RHMWA01-WG10 SGS Ref. #: 1080224006 Project ID: 9121-003 Red Hill BFSF Matnx: Water (Surface, Eff., Ground)

Semivolatlle Organic Fuels Department

Parameter
Dlesel Range Organics 5a Androstane <sum
Batch Informatlon AII DatesRlmes are Alaska Local Time Collectlon Date/rime: 01/15/08 13:05 Reoeipt Dale/ilme: 01/17108 14:45

Analvtical Pmp ResuB PQUCL MOL Units DF Bateh Batch

3.23 0.435 0.0870 mg/L 1 XFC7831 XXX19058 102 50-150 % 1 XFC7631 XXX19058 uall0era

Analytical Batch: XFC7831 Prep Batch: XXX19058 Initial Prep Wl.Nol.: 920 mL Analytical Method: SW8015B Prep Method SW3520C Prep Extracl Vol.: 1 mL Analysis Date/Tlme: 01/30108 13:23 Prep Date/Tlme: 01/22/08 08:30 Contalner ID:1080224006-H D ilutlon Factor: 1 Analyst: BME

SGS Envlronmentel servicea Inc 

# I Alecka Diviclun 0 eat Potter Drive Ancllurege Alaake 99518 t 19911 564 23<3 Y0 1190 W 71 561 5301 w s cem 1 MemOer of SGS GrouD (SocIAIA GAnArale oe Survelllence)

# ~

The Environmental Company, Inc. (TEC) Pnnt Dale: 2/5/2008

ClientSamplelD: RHMWA01-WG70 SGS Ref. #: 1080224006 Project ID: 9121-003 Red Hill BFSF Matnx: Water (Surface, Eff., Ground)

Volatile Gas Chrometography/Mass Spectroscopy

Parameter 

### Resul AII DatesTmes are Alaska Local Time Collection Date>Tme: 01/15/0813:05 Recelpt Date/Time: 01/17108 14:45

Analvtical Prao PE
~ L C L MDL Units DF Bateh Bateh Qualiflem

Benzene 0.170 J 0.400 0.120 ug/L 1 VMS9632 VXX17871 Toluene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Ethylbenzene 0.350 J 1.00 0.310 ug/L 1 VMS9632 VXX17871 n-Butylbenzene 8.94 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,4-Dlchlorobenzene ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 1,2-Dlchloroethane ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Chlorobenzene ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS9632 VXX17871 cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VM89632 VXX17871 4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 cls-1,3-Dlchloropropene ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 n-Propylbenzene 12.7 1.00 0.310 ug/L 1 VMS9632 VXX17871 Styrene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Dlbromomethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2,4-Trichlorobenzene ND 1.00 0.310 uglL 1 VMS9632 VXX17871 1,1,2,2-Tetrrachloroethane ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 1,2-Dibromo3chloropropane ND 2.00 0.620 ug/L 1 VMS9632 VXX17871 Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VM89632 VXX17871 Tetrachloroethene ND 1.00 0.310 uglL 1 VMS9632 VXX17871 Dibromochloromethane ND 0.500 0.150 uglL 1 VMS9632 VXX17871 1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS9632 VXX17871 1,2-Dibromoethane ND 1.00 0.310 ug1L 1 VMS9632 VXX17871 Calbon tetrachlonde ND 1.00 0.310 uglL 1 VMS9632 VXX17871 1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug1L 1 VMS9632 VXX17871 Chlorofonn ND 1.00 0.310 uglL 1 VMS9632 VXX17871 Bromobenzene ND 1.00 0.310 uglL 1 VMS9632 VXX17871 Chloromethane ND 1.00 0.310 ug1L 1 VMS9632 VXX17871 1,2,3-Trichloropropane ND 1.00 0.310 uglL 1 VMS9632 VXX17871 Bromomethane ND 3.00 0.940 uglL 1 VMS9632 VXX17871 Bromochloromethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Vinyl chlonde ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Chloroethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871

SGS Environmental Servicee Inc I Aleaka Division 1l99]f 582 23A3 200 W ael PotlerOrlve Il9971581 5391 Anckorage Alacka 99513
www us aoc com 1 MemCar o15Ga GrouD (SOel0l6 G6n9rale Ee Survalllence)The Environmental Company, lnc. (TEC) Pnnt Date: 2/5/2008
Cllent Sample ID: RHMWA01-WG10 AII Dates>Tmes are Alaska Local Tlme SGS Re(. #: 1080224006 Collecbon Date/Tme: 01115/08 13:05 Project ID: 9121-003 Red Hill BFSF Recelpt Datefrlme: 01/17/08 14:45 Matrix: Water (Surfaoe, EB., Ground)

Volatile Gas Chromatography/Mass Spectroscopy Analyti cal Preo Parameter Result PGUCL MDL Unhs DF Batoh Batch Qualifiers seo-Butylbenzene 7.50 1.00 0.310 ug/L 1 VMS9632 VXX17871 Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS9632 VXX17871 Methylene chloride ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 P& M-Xylene ND 2.00 0.620 ug/L 1 VMS9632 VXX17871 Naphthalene 194 1.00 0.620 ug/L 1 VMS9632 VXX17871 o-Xylene 1.10 1.00 0.310 ug/L 1 VMS9632 VXX17871 Bromofonn ND 1.00 0.500 ug/L 1 VMS9632 VXX17871 1-Chiorohexane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2,4-Trimethylbenzene ND 100 0.310 ug/L 1 VMS9632 VXX17871 tert-Butylbenzene 1.20 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1,1-Tnchlorcethane ND 1.00 0.310 ug/L 1 VM89632 VXX17871 1.1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Tnchloroethene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 trans-1,2-Dlchloroethene ND 1.00 0.310 ug/L 1 VMS9632 VXX77871 1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Hexachlorobutadiene ND 0.600 0.180 ug/L 1 VMS9632 VXX17871 Isopropylbenzene (Cumene) 5.63 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2-Dlchloropropane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1-Dlchloropropene ND - 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1,2-Tnchloroethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2,3-Tnchlorobenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2-Dichlorcethane-D4 <surr> 102 73-120 % 1 VMS9632 VXX17871 Toluene-d8 <surr> 98.6 80-120 % 1 VMS9632 VXX17871 4-Bromofluorobenzene <surrn 105 76-120 % 1 VMS9632 VXX17871
Batch Informa0on Analybcal Batch: VMS9632 Prep Batch: VXX17871 Initial Prep Wt.Nol.: 5 mL Analytical Method: SW8260B Prep Method: SW5030B Prep Extrad Vol.: 5 mL Analysls Date/Time: 01129/08 22:10 Prep Date/Time: 01/29108 14:08 Container ID:1080224006-D Dilution Factor: i Analyst: DSH

SGS Envlronmental Servlces Inc 

# ~ Aleeke Dlvlclon 200 W esl Poner Drlve Ancbore9e Alaske 9951 8 I IAn11582 23<9 119071 s81 53n1 www ux caa eem Membar cl SGS Group (Socl9t9 G6n6rele Ce Surveillence)

# ~

The Environmental Company, Inc. (TEC) Pnnt Date• 215/2008

Cllent Sample ID: RNMWA01-WG10 AII DatesRmes are Alaska Local Tlme SGS Ref. #: 1080224006 Collection DateRme: 01115/08 13:05 Project ID: 9121-003 Red HIII BFSF Receipt DatelTme: 01/17/08 14:45 Matnx: Water (Surface, Eff., Ground)

Polynuclear Aromatias GC/MS 

### E9el1dl.a[ Pre8 Parametar Result PQUCL MDL Unha DF Balch Batch
Acenaphthylene ND 0.0515 0.0155 ug/L 1 XMS4385 XXX19059 Acenaphthene 0.303 0.0515 0.0155 ug/L 1 XMS4385 XXX19059 Fluorene 0.161 0.0515 0.0155 ug/L 1 XMS4385 XXX19059 Phenanthrene ND 0.0515 0.0155 ug/L 1 XMS4385 XXX19059 Anthraoene ND 00515 0.0155 ug/L 1 XMS4385 XXX19059 Fluoranthene ND 0.0515 0.0155 ug/L 1 XMS4385 XXX19059 Fyrene ND 0.0515 0.0155 ug/L 1 XMS4385 XXX19059 Benzo(a)Artthracene ND 0.0515 0.0155 ug/L 1 XM84385 XXX19059 Chrysene ND 0.0515 0.0155 ug/L 1 XMS4385 XXX19059 Benzo[b]Fluoranthene ND 0.0515 0.0155 ug/L 1 XMS4385 XXX19059 Benzo[k]fiuoranthene ND 0.0515 0.0155 ug/L 1 XMS4385 XXX19059 Benzo[a]pyrene ND 0.0515 0.0155 ug/L 1 XMS4385 XXX19059 Indeno[1,2,3-e,d] pyrene ND 0.0515 0.0155 ug/L 1 XMS4385 XXX19059 Dlbenzo[a,h]anthracene ND 0.0515 0.0155 ug/L 1 XMS4385 XXX19059 Benzo[g,h,]perylene ND 0.0515 0.0155 ug/L 1 XMS4385 XXX19059 Naphthalene 102 5.15 1.60 ug/L 50 XMS4386 XXX19059 1-Methylnaphthalene 73.2 2.58 0.773 ug/L 50 XMS4386 XXX19059 2-Methylnaphthalene 27.6 2.58 0.773 ug/L 50 XMS4386 XXX19059 Telphenyl-d14 <surr> 88.5 50-135 °h 1 XMS4385 XXX19059
Batch Informatlon uallflers

AnalyBcal Batch: XMS4385 Prep Batch: XXX19059 InlBal Prep Wt.Nol.: 970 mL Analyhcal Method: 8270C SIMS Prep Method: SW3520C Prep Extracl Vol.: 1 mL Analysis Date/Tlme: 01/28/08 16:15 Prep Date/Tlme: 01122I08 08:50 Container ID:1080224006-J D llution Factor: 1 Analyst: WAA AnalyGcal Batch: XMS4386 Prep Batch: XXX19059 Initial Prep Wt./Vol.: 970 mL Analytical Method: 8270C SIMS Prep Method: SW3520C Prep Extracl Vol.: 1 mL Analysis pate/Tlme: 01/28/08 21:52 Prep Datefflme: 01/22108 08:50 Contalner ID: Dllubon Factor: 50 Analyst: WAA

SGe Envlronmenlal Sarvlcee Ine I Aleska Divlelon 0 W esl Potter Drive Anckora9e Alaeka 99519 l I/p0'(15B> 234a_ 1 Z0 (9p)1591 5101 www.nnsea enm MemDer ol SGS Group (Socl9t9 G9n9rele de Survelllence)

# ~

The Environmental Company, lne. (TEC) Print Date: 2/5I2008

Client Sample ID: RHMW01-WG10 AII DatesTmes are Alaska Local Time SGS Ref. #: 1080224007 Collection Datelrlme: 01/15108 16:15 Project ID: 9121-003 Red Hill BFSF Receipt DateTme: 01/17/08 14:45 Matrix: Water (Surface, ER., Ground)

Dissolved Metals Analvtleal Preo Parameter Rasult POLICL MDL Unha DF Batch Batch Qualiflers

Lead ND 1.00 0.310 ug/L 5 MMS5294 MXX79964
Batoh Information Anaiylical Batch: MMS5294 Prep Batch: MXX19964 Initlal Prep Wt.Nol.: 50 mL Analyhcal Method: SW6020 Prep Method: SW3010A Prep Extract Vol. , 50 mL Analysls Date/Tlme: 01/28108 14:00 Prep DatelTlme: 01/24108 16 , 35 Contalner ID:1080224007-G Ddutlon Factor: 5 Analyst: TK

SGS Envlronmenfel Servlcea Inc I Aleska Divielon 200 W esl Pelter Drive Anehorape Alaeka 99515 l 1 f90]15R22L3 f f9071561_5301 m c.aQe.com Member of SGS Grnup (SncIR1R GAn9rele Ee Survelllence)

# B I MA

The Environmental Company, Inc. (TEC) Print Date: 2/512008

ClientSamplelD: RHMW01-WG10 SGS Ref.#:1080224007 Projeet ID: 9121-003 Red Hill BFSF Matdx: Water (Surface, Eff., Ground)

Volatile Fuels Department

Pammebr
Gasohne Range Organlca 4-Bromofluorobenzene <surrn

Batoh Infonnation AII Dates/Tlmes are Alaska Local Tlme Colledlon DateTme: 01115108 16:15 Reoeipt Date/Time: 01/17/08 14:45

Analvtiwl Pmp ResuR PQLICL MDL UnOs DF Bateh Batch

ND 100 10.0 ug/L 1 VFC8836 VXX17866 104 50-150 % 1 VFC8836 VXX17866 uali6ers

Analytical Batch: VFC8836 Prep Batch: VXX17866 InBial Prep Wt.Nol.: 5 mL Analytical Method: SW8015B Prep Method , SW50308 Prep Ectract Vol.: 5 mL Analysis DateTme: 01/23/08 13:13 Prep DateTme: 01/23108 08:00 Container ID:1080224007-A D ilu6on Factor. 1 Analyst HM

SGS Envlranmentel Sarvlcee Inc 

## I Aleake Divlslon 200 W eet Potter Drive Anc0ora9e Alaeke 99518 1(„(P071 5922343 1(9071 591 5301 rr fl sQa [nm
r MamUer of SGS Group (Sociht9 GAnArele Ee Survelllence)Anal eal Preo Resuk PUUCL MDL Units DF Batch Batch Qualiflem

0.574 0.421 0.0842 mg/L 1 XFC7831 XXX19058 97.6 50-150 % 1 XFC7631 XXX19058 Semivolatile OrOanlc Fuels Department

Parameter
Diesel Range Organics 5a Androstane <sum The Envlronmental Company, Inc. (TEC) Pnnt Date: 215/2008
Cllent Sample ID: RHMW07-WG10 AII DatesRmes are Alaska Local Tlme SGS Ref. #: 1080224007 Collectlon DateTme:01/15/O8 16:15 Project ID: 9121-003 Red HIII BFSF Recelpt Date/Tlme: 01/17/08 14:45 Matnx: Water (Surface, Eff., Ground)

Batchln(orma0on AnalyGOal Batch: XFC7831 Analyqcal Method: SW8015B Analysis Date/Time: 01/30108 13•33 Dilutlon Factor: 1 Prep Batch: XXX19058 Prep Method' SW3520C Prep Date/Tlme: 01122/08 08:30 Initlal Prep Wt.Nol.: 950 mL Prep Extract Vol.: 1 mL Container ID:1080224007-H Analvst: BME

SGS Envlronmentel Servlces Inc 

# I
Aleska DNlslon O W eat Potter Drlre Anehorage Aleaka 99518 t(9D715fi2.2]<] T

YD f9n>I581.530t w w ue eua.eem
MemUer ol SGS Group (SocIA19 G4n9rale Ee Sunalllance)

# ~

The Environmental Company, Inc. (TEC) Pnnt Date: 215/2008

Client Sample ID: RHMW01-WG70 SGS Ref. #: 1080224007 Project ID: 9121-003 Red Hill BFSF Matnx: Water (Surface, Eff., Ground)

Volatile Gas Chromatography/Mass Spectrosoopy

Parameter 

### Resuh AII DatesRlmes are Alaska Local Tlme Collectlon Date/Tlme: 01/15108 16:15 Receipt Date/Time: 01117/08 14:45

Analvtical Pree PQLJC MDL Unhs DF Batch Batch Qualinem

Benzene ND 0.400 0.120 ug/L 1 VM89632 VXX77871 Toluene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Ethylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 n-Butylbenzene 0.450 J 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,4Dlchlorobenzene ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 1,3,5-Tdmethylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Chlorobenzene ND 0.500 0.150 uglL 1 VMS9632 VXX17871 4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS9632 VXX17871 cls-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 cls-1,3-Dlchloropropene ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Styrene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Dibromomethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 trans-1,3-Dlchloropropene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2,4-Tnchlorobenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 1,2-Dibromo-3cirloropropane ND 2.00 0.620 ug/L 1 VMS9632 VXX17871 Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS9632 VXX17871 TetrachlorGethene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Dlbromochloromethane ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS9632 VXX17871 1.2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Carbon tetrechlonde ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1,1,2-Tetrachloroethane ND 0500 0.150 ug/L 1 VMS9632 VXX17871 Chlorofonn ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Bromotrenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Chloromethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Bromomethane ND 3.00 0.940 ug/L 1 VMS9632 VXX17871 Bromochloromethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Vinyl chloride ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Dichlorodf6uoromethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 C111orcethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871

SGS Environmentel Servlcee Inc I Alaeke Divlslon t 19911 582.2343 20U W est Poller Drlve f (9911 551.5391 Aneborege Aleeka 99518 w w ucsoc en Member of SGS Graup (Sacl9t9 G9n6rale de Survelllance).0 .,



### The Environmental Company, Inc. (TEC) Print Date: 215/2008

Client Sample ID: 

### RHMW01-WG70 All Dates/Tlmes are Alaska Local Time SGS Ref. #: 1080224007 Collection Date/Tlme: 01/15/08 16:15 Projed ID: 9121-003 Red Hill BFSF Recelpt DateRme: 01117108 14:45 Matnx: Water (Surface, Eff., Ground)



### Volatile Gas Chromatography/Mass Spectrosoopy Analytical Preo Parameter Result PQL/CL 

### MDL Unhs DF Batoh Batch QualHiers sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Bromotlichloromethane ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 1,1-Dlchloroethene ND 1.00 0.310 uglL 1 VMS9632 VXX17871 2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS9632 VXX17871 Methylene chloride ND 1.00 0.310 uglL 1 VMS9632 VXX17871 Tdchlorofluoromethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 P& M-Xylene ND 2.00 0.620 ug/L 1 VMS9632 VXX17871 Naphthalene 5.98 1.00 0.620 ug/L 1 VMS9632 VXX17871 o-Xylene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Bromoform ND 1.00 0.500 ug/L 1 VMS9632 VXX17871 1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 tert-Butylbenzene 0.440 J 1.00 0.310 ug/L 1 VMS9632 VXX17871 1, 1,1 -Trichloroethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1-Dlchloroethane ND 1.00 0.310 uglL 1 VMS9632 VXX17871 2-Chlorotoluene ND 1.00 0.310 uglL 1 VMS9632 VXX17871 Trichloroethene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2-Dlchlorobenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 2,2-Dlchloropropane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Hexachlorobutadlene ND 0.600 0.180 ug/L 1 VMS9632 VXX17871 Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2-Dlchloropropane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1-Dlchloropropene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1,2-Tnchloroethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,3-Dlchlorobenzene ND 

### - 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2,3-TnchlDrobenzene ND 1.00 0.310 uglL 1 VMS9632 VXX17871 1,2-Dichloroethane-D4 <sum 99.6 73-120 

### % 1 VMS9632 VXX17871 Toluene-d8 <surr> 104 80-120 

### % } VMS9632 VXX17871 4-BromGfluorobenzene<sum 101 76-120 

### % 1 VMS9632 VXX17871
Batch Informatlon Analybcal Batch: VMS9632 Prep Batch: VXX17871 Indlal Prep Wt.Nol.: 5 mL Analytloal Method: SW8260B Prep Method: SW5030B Prep Extract Vol.: 5 mL Analysis DatelTme: 01/29/08 22:41 Prep Datelrime: 01/2910814:08 Container ID:1080224007-D DIIuSon Factor: 1 Analyst: DSH

SGS Environmenlal servlcee Inc 

# I Alaaka Divislon 200 W eel Poller Driva Anehorepe Alaeka 99515 l 1 f907,5

89 J_

C? f(,QQII 561.53n1 r s.aQe enm MemEero/SGS Gruup (Soc1916 G6n4rale Ga Survelllance)

### The Environmental Company, Inc. (TEC) Pnnt Date: 215/2008

ClientSamplelD: RHMW01-WG70 SGS Ref. #: 1080224007 Pro]ed ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)



### Polynuclear Aromatice GC/MS

Parameter AII Dates/Tlmes are Alaska Local Time Collection Date/Tlme. 01/15108 16:15 Receipt DateRme: 01/17/08 14:45

Analvtleal Preo 

### Result PaUCL MDL Units DF Batch Batch Qualiflem

Acenaphthylene ND 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Acenaphthene 0.0310 J 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Fluorene 0.0371 J 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Phenanthrene ND 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Anthraoene ND 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Fluoranthene ND 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Pyrene ND 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Benzo(a)4nthracene ND 0.0526 0.0158 ug/L 

### i XMS4385 XXX19059 Chrysene ND 0.0526 0.0158 uglL 1 XMS4385 XXX19059 Benzo[b]Fluoranthen® ND 0.0526 0.0158 ug/L 1 XMS43t15 XXX19059 Benzo[k]8uoranthene ND 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Benzo[a]pyrene ND 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Indeno[1,2,3c,d] pyrene ND 

### ' 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Dibenzo[a,h]anthracene ND 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Benzo[g,h,i]perylene ND 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Naphthalene 0.210 0.105 0.0326 ug/L 1. XMS4385 XXX19059 1-Methylnaphthalene 0.0640 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 2-Methylnaphthalene 0.0478 J 0.0526 0.0158 ug/L 1 XMS4385 XXX19059 Terphenyl-d14 <surr> 83.2 50-135 

### % 1 

### XMS4385 XXX19059


### Batah Informa0on Analytical Batch: XM34385 Prep Batch: XXX19059 Initlal Prep Wt.Nol.: 950 mL Analyllcal Method: 8270C SIMS Prep Method: SW3520C Prep Extract Vol.: 1 mL Analysis DataTme: 01/28108 16:48 Prep Date/Tlme: 01/22/08 08:50 Contalner ID:1080224007-J Dilution Factor: 1 Analysl: WAA

SGS Environmentel Ssrvices Ine 

## I Alaeka Dlvlclun 300 W eet Potter Drive Anchore9e Alcske 99518



# +[ 190]1584 2363 1l9071591.5301 w MemEer oi SGS Graup (Sacl9t9 G4n4rale tle Survelllance)

# m i

The Environmental Company, Inc. (TEC) Print Date. 21512008

Client Sample ID: TB01-WG10 SGS Ref. #: 1080224008 Pro/ect ID. 9121-003 Red Hill BFSF Matnx: Water (Surfaoe, Eff., Ground)



### VolaUle Gas Chromatography/Mass Spectroscopy

Parameter Resuh AII Dates/Tmes are Alaska Local Time Collection Datelrime: 01115108 09:05 Receipt Date/Time: 01/17/08 14:45

Analvtleal Preo PGLICL MDL 

### Unita DF Bateh Batch Qualiflers

Benzene ND 0.400 0.120 uglL 1 VMS9632 VXX17871 Toluene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Ethylbenzene ND 1.00 0.310 uglL 1 VMS9632 VXX17871 n-Butylbenzene ND 1.00 0.310 uglL 1 VMS9632 VXX17871 1,4-Dlchlorobenzene ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 1,2-Dlchloroethane ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 1,3,5-Tnmethylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 4-Chlorotoluene ND 1.00 0.310 uglL 1 VMS9632 VXX17871 Chlorobenzene ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 uglL 1 VMS9632 VXX17871 cls-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 4-Isopropyholuene ND

. 1.00 0.310 ug/L 1 VMS9632 VXX17871 cls-1,3-Dlchloropropene ND 0.500 0.150 ug/L 1 VM89632 VXX17871 n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Styrene ND 1.00 0.310 uglL 1 VMS9632 VXX17871 Dibromomethane ND 1.00 0.310 uglL 1 VMS9632 VXX17871 trans-1,3-Diohloropropene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 1,2-Dlbromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS9632 VXX17871 Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS9632 VXX17871 Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 1,3-Dlchloropropane ND 0.400 0.120 uglL 1 VMS9632 VXX17871 1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Carbon tetrachloride ND 1.00 0.310 uglL 1 VMS9632 VXX17871 1,1,12-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 Chloroform ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Bromobenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Chloromethane ND 1.00 0.310 uglL 1 VMS9632 VXX17871 1,2,3-Tnchloropropane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Bromomethane ND 3.00 0.940 uglL 1 VMS9632 VXX17871 Bromochloromethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Vlnyl chlonde ND 1.00 0.310 uglL 1 VMS9632 VXX17871 Dlchlorodi8uoromethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Chloroethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871

SGS Environmental Servlcea Inc 

# I Aleske Dlvlslon 200 W est Polter Drlve Ancaura9e Alaske 99518 t f99]f 56] 23<3 r f9011 551.5301 w l MemEer ol SGS Group (SOCIAU 136n9rala tle Survalllance)

# FTM N

A



### The Environmental Company, Inc. (TEC) Print Date: 215/2008

Cllent Sample ID: TB01-WG10 AII Datea/Times are Alaska Local Time SGS Ref. #: 1080224008 Collection Date/Tlme: O1H5/08 09:05 Project ID: 9121-003 Red HIII BFSF Recelpt Date/Time: 01/17/08 14:45 Matrix: Water (Surface, Eff., Ground)



### Volatlle Gas Chromatography/Mass Spectroscopy Analytical Preo Parameter 

### Resu PaLfCL MDL 

### UnHs DF Batch Batch Qualiflers seo-Butylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS9632 VXX17871 11-Dichloroethene ND 1.00 0.310 uglL 1 VMS9632 VXX17871 2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS9632 VXX17871 Methylene chlonde ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 P& M-Xylene ND 2.00 0.620 ug/L 1 VMS9632 VXX17871 Naphthalene ND 1.00 0.620 ug/L 1 VMS9632 VXX17871 o-Xylene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Bromoform ND 1.00 0.500 ug/L 1 VMS9632 VXX17871 1-Chiorohexane ND 

### , 100 0.310 ug/L 1 VMS9632 VXX17871 1,2,4-Tnmethylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX77871 tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Trichloroethene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 trans-1,2-Dichloroeth®ne ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 Hexachlorobutadiene 0.330 J 0.600 0.180 ug/L 1 VMS9632 VXX17871 Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1-Dlchloropropene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS9632 VXX17871 1,2-Dichloroethane-D4 <sum 104 73-120 

### % 1 VMS9632 VXX17871 Toluene-d8 <surr> 104 80-120 

### % 1 VMS9632 VXX77871 4-Bromofluorobenzene <sum 104 76-120 

### % 1 VMS9632 VXX17871
Batch InfonnaUon Analytical Batch: VMS9632 Prep Batch: VXX17871 Initlal Prep Wt.Nol.: 5 mL Analytical Method: SW8260B Prep Method: SW5030B Prep Extract Vol.: 5 mL Analysis DateRme , 01/29108 20:06 Prep DafeTme: 01129/08 14:08 Container ID:1080224008-A Dilution Fador: 1 Analyst: DSH

SGS Environmentel Servlcee Inc 

# I Alaska Divlelon 0 W eet Potter Grlve Anchorega Alaska 99518 l I I90115BP 2343 f 20 19071561.5301 w Member of SGS Group (SucIAIA G9nArale Ee Survalllence)

# 1111P771

SGS Ret# 814184 Method Blank Printed DatefPime 02/05/2008 12:09 CBent Name The Environmentsl Company, Inc. (TEC) Prep Batc6 XXJC19058 

### Project NnmeJ# 9121-003 Red Hill BFSF Methad SW3520C M atrix Water (Surface, Eff., Ground) Date 01/2212008 

### QC rcsults affect the following produclion semples: 1080224001,1080224004,1080224005,1080224006,1080224007 Repnning/Contml Anellss Petenleter ResuLLa t

~ ,,,,, MDL Unns Dete



### Semivolalile Oraanic Elsels Denartment
Diesel Range Organics 0.0962 J 0.400 0.0800 mg/L 01/30/08


### Surrogates
5a Androstane <surr> 88.5 60-120 s/ 01/30/08 

### Beteh XFC7831 Methad SW8015B Instrument HP 5890 Sones 11 FID SV D R

# ~

SCS Ref.# 814188 Method Blank Printed DateITlme 02/05/2008 12:09 

### Cllent Name The Environmental Company, lnc. (TEC) Prep Batch XXX 19059 Project Name/N 9121-003 Red Hill BFSF Method SW3520C Metriz Water (Surface, Eff., Ground) Date 01/22/2008 QC n;sults affce[ Ihc following production samplcs: 1080224001,1080224004,1080224005,1080224006,1080224007
Reponmg/Control Analysis Parametcr Rcsul ts MDL Unrts Daic



### PolrLn uclea 

### r_Ar oma 

### ticn GC/MS
Acenaphthylene ND 0.0500 0.0150 ug/L 01128/08 Acenaphthene ND 0.0500 0.0150 ug/L 01/28/08 Fluorene ND 0.0500 0.0150 ug/L 01/28/08 Phenanthrene ND 0.0500 0.0150 ugtt. 01/28/08 

### Anthracene ND 0.0500 0.0150 upJL 

### 01/28/08 Fluoranthene ND 0.0500 0.0150 ug/L 01/28/08 Pyrene ND 0.0500 0.0150 ug/L 01/28/08 Benzo(a)Anthracene ND 0.0500 0.0150 ug/L 01/28/08 Chrysene ND 0.0500 0.0150 ug/L 01/28/08 Benzo[b]Fluorenthene ND 0.0500 0.0150 ug/L 01/28/08 

### Benzo(k]Fluoranthene ND 0.0500 0.0150 ug/L 01128/08 Benzo[a]pyrene ND 0.0500 0.0150 ug/L 01/28/08 

### Indcno[1,2,3-c,d]pyrene ND 0.0500 0.0150 ug/[. 01/28/08 Dibenzo[a,h]anthcacene ND 0.0500 0.0150 ug/L 01128/08 Benw[g,h,i]perylene ND 0.0500 0.0150 ug/L 01/28/08 Naphthalene ND 0.100 0.0310 ug/L 01128/08 

### 1-Methylnaphthalene ND 0.0500 0.0150 ug/L 01128/08 2-Methylnaphthalene ND 0.0500 0.0150 ug/L 01128/08 Surrogates Terphenyl-d14 <surf> 96.1 50-135 r/ o 01/28108 Batch XMS4385 

### Method 8270C SIMS Instruroeot HP 689015973 MS SVOA

# Ir e $ `

J

~

SCS ReL# 814439 Method Blank Printed Date/Ptme 02/05/2008 12:09 

### COent Name The Envlronmental Company, Inc. (TEC) Prep Batch VXX 17866 ProJectName/# 9121-003RedHi11BFSF Methad SW5030B Matria Water (Surface, Eff., Ground) Date 01/23/2008QC msults affect fhe following production semples

### 1080224001,1080224004,1080224005,1080224006,1080224007
Reponing/Conlrol Analys's Pardm¢tcr Raulta MDL U mn Dalc


### Vola.tilB Fwe18 Dapartment Gasoline Range Organics 

### iJi:
Surrogetes

4-BromoFluorobenzene <surr> 102 

### Baah VFC8836 Method SW8015B Insvumenl HP 5990 Serics 11 PID+HECD VBA 

### ]0o 10.0 ug/L 01/23/08

50-150 % 01123/08`



### SGS ReL# 814679 Method Blank Printed Date/Pime 02/05/2008 12:09 Client Name The Environmental Company, Inc. (TEC) Prep Batch MXX 19964 Projeet Name/# 9121-003 Red Hill BFSF Method SW3010A Matrix Water (Surface, EfF., Ground) Date 01/24/2008
QC results aftect thc following productlon samples: 1080224001,1080224004,1080224005,1080224006,1080224007 Reponing/Control Analysis vo.a.nM— Rcsuhs .___ MDL Unns n,n ~ 

### lSetals by ICP/NS
Lead 

### f:G] 1.00 0.310 ug/l. 01/28/08
Betch MMS5294 Method SW6020 Instrumeot Perkin Elmcr Scicx ICP-MS P3

# SGS

SGS Ret# 815213 Method Blank Printed DateJrime 02/05/2008 12:09 Client Name The Envtronmental Company, Inc. (TEC) Prep Batch VXX17871 Project Name/# 9121-003 Red Hill BFSF Method SW5030B Matri= Water (Surface, Eff., Ground) Date 01/29/2008 

### QC results affect the following production samples: 1080224001,1080224004,1080224005,1080224006,1080224007,1080224008 Reporting/Control Malyats Parameter Results t

, m „ MDL Unns Date



### Volatile Gae Chroasatography/!lasa Spectroacopy

# ~

SGS Re[# 815213 Method Blank Printed Date/Time 02/05/2008 12:09 

### Clieot Name The Environmental Company, Inc. (TEC) Prep Batch VXX17871 ProjeetName!# 9121-003 Red Hill BFSF Method SW5030B Matdx Water (Surface, Eff., Ground) Date 01/29/2008
R<poning/Cunaol Analysa m Paracter Rcsults

~ ,,,,, r MDL Units Dwc

VOlat:lle Ga9 ChLOIDStOylaphy/M8B8 3pBCti09C0



### Benune ND 0.400 0.120 ug/L 01/29/08 

### Toluene ND 1.00 0.310 ug/L 01/29108 Ethylbenzene ND 1.00 0.310 u81I. 01/29108 n-Butylbenzene ND 1.00 0.310 ug/L 01l29/08 

### 1,4-Dichlorobenzene ND 0.500 0.150 ug/L 01/29108 1,2-Dichloroethane ND 0.500 0.150 ug/L 01/29108 

### 1,3,5-Trlmethylbenzene ND 1.00 0.310 ug/L 01/29/O8 4-Chlorotoluene ND lA0 0.310 upJL 01/29/08 Chlorobenune ND 0.500 0.150 up/L 01/29/08 4-Methyl-2-pentanone(MIBK) ND 10.0 3.10 ug/1. 01129/08 cls-1,2-Dichloroethene ND 1.00 0.310 ug/L 01129/08 4-lsopropyltoluene ND 1.00 0.310 ug/L 01/29/08 cis-1,3-Dichloropropene ND 0.500 0.150 ug/L ' 01/29/08 n-Propylbenzene ND 1.00 0.310 ug/L 01/29/08 Styrene ND 1.00 0.310 ug/L 01129/08
Dibromomethane ND 1.00 0.310 uH/l. 01/29/08 

### hatts-1,3-Dichloropropene ND 1.00 0.310 ug/L 01/29/08 1,2,4-Trichlorobenzene ND 1.00 0.310 ug/t. 01/29/05 

### 1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 01/29/09 1,2-Dibromo-3-chloropropane ND 2.00 0.620 

### upJ[. 01/29108 

### Methyl-t-butyl ether ND 5.00 1.50 

### uPJ[. 01/29108 Tetrachlorcethene ND 1.00 0.310 uP/L 01/29/08
Dibromochloromethane ND 0.500 0.150 u81L 01/29/08 

### I,3-Dichloropropane ND 0.400 0.120 ug/t. 01/29/08 1,2-Dibromoethane ND 1.00 0.310 ug/[. 01/29/08
Carbon tetr•achloride ND 1.00 0.310 uH/L 01/29/08 1, 1, 1,2-Tetrachloroethane ND 0.500 0.150 ug/l. 01/29/08 Chloroform ND 1.00 0.310 ug/L 01/29/08 

### Bromobenzene ND 1.00 0.310 ug/L 01/29/08 Chloromethane ND 1.00 0.310 ug/L 01/29/08 

### 1,2,3-Tnchloropropane ND 1.00 0.310 ug/L 01/29/08 Bromomethane ND 3.00 0940 ug/L 01/29/08 

### Bromochloromethane ND 1.00 0.310 ug/L 01/29/08 Vinyl chlorlde ND 1.00 0.310 ug/l. 01/29/08 Dichlorodifluoromethane ND 1.00 0.310 ug/L 01/29108 

### Chloroethane 1 ND 1.00 0.310 ugn. 01/29108 sec-Butylbenzene ND 1.00 0.310 ug/l. 01/29108
Bromodichloromethane ND 0.500 0.150 ug/L 01/29108 I,]-Dichloroethene ND 1.00 0.310 ug/L 01/29/08. .,

SGS Ref.# 815213 Method Blank Pduted Date/Ptme 02/05/2008 I2:09 Client Name The Environmental Company, Inc. (TEC) Prep Batch VXX 17871 Projeet Name/# 9121-003 Red Hill BFSF Methud SW5030B Matrix Water (Surface, Eff., Ground) Date 01/29/2008
Repurting/Conmol Analysis Pammeter Results i

,,,, d MDL Units Date


### Volatile Gae Chromatography/lfass Spectroaco
2-Butanone (MEK) ND 10.0 3.10 ug/I. 01129/08 Methylene chloode ND 1.00 0.310 ug/L 01/29108
Trichlorofluoromethane ND 1.00 0.310 ugn. 01/29108 P& M-Xylene ND 2.00 0.620 ug/I. 01/29/08 Naphthalene ND 1.00 0.620 ug/l. 01/29108 o-Xylene ND 1.00 0.310 ug/l. 01/29/08
Bromofonn ND 1.00 0.500 ug/L 01/29/08
1-Chlorohexane ND 1.00 0.310 ug/L 01/29/08 1,2,4-Tnmethylbenune ND 1.00 0.310 ugil. 01/29/08 tert-Butylbenzene ND 1.00 0.310 ug/L 01129/08 1,1,1-Trichloroethane ND 1.00 0.310 ug/L 01/29/08 ],l-Dichlorcethane ND 1.00 0.310 ug/l. 01/29/08
2-Chlorotoluene ND 1.00 0.310 ug/L 01/29108
Tnchloroethene ND 1.00 0.310 ug/L 01/29/08 trans-1,2-Dtchloroethene ND 1.00 0.310 ug/L 01/29108 1,2-Dtchlorobenzene ND 1.00 0.310 ug/L 01/29/08 2,2-Dichloropropane ND 1.00 0.310 ug/L 01/29108
Hexachlorobutadiene ND 0.600 0.180 ug/L 0I/29/08 lsopropylbenzene (Cumene) ND 1.00 0.310 ug/L 01/29/08 1,2-Dichloropropane ND 1.00 0.310 ug/L 01/29108 1,1-Dichloropropene ND 1.00 0.310 ug/L 0I/29108 1,1,2-Trlchloroethane ND 1.00 0.310 ug/L 01129108 1,3-Dichlorobenune ND 1.00 0.310 ug/L 0I/29108 1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 0I/29/08
Surrogatea
1,2-Dichloroethane-D4<surr> 100 73-120 

### % 01129108
Toluene-08<surr> 102 80-120 c/, 01/29/08
4-Bromofluorobenzene <surr> 

### ] 10 76-120 y, 01/29108
Batch VMS9632 Method SW8260B Inrtrumeot HP 5890 Scrics 11 MS3 VNA

# NJ

SGS Ref# 814185 Lab Control Sample Printed Datelrlme 0210512008 12:09 Prep Batch XXX19058 Ctient Name The Environmental Company, Inc. (TEC) Method SW3520C ProjectName/# 9121-003 Red Hill BFSF Date 01/22/2008 Matrix Water (Surface, Eff., Ground) QC results affect the following production samples: 

### 1080224001,1080224004,1080224005,1080224006,1080224007

QC Ptt LCS/LCSD RPD Sptkcd Analysts Patmnctcr Rrsuhs Recov Ltmin PPD Ltmtts Amount Detc


### Semivolatile Organic Eltela Department
Diesel Range Organics LCS 1.02

Surrogates
5a Androstane <surr> LCS

Batch XFC7831 Method SW8015B Instrument HP 5890 Series 11 FID SV D R 102 ( 75-125 ) 1 mg/L 01/30/2008

86 ( 60-120 ) 01/30/2008

# ~

SCS Ref.# 814189 Lab Control Sample Printed DatelPime 02/05/2008 12:09 Prep Batch XXX19059 

### Client Name The Environmental Company, Inc. (TEC) Method SW3520C ProJect Name!# 9121-003 Red Hill BFSF Date 01122/2008 Matrix Water (Surface, Eff., Ground) QC rcsults affcct thc following productton samples: " 1080224001,1080224004,1080224005,1080224006,1080224007

QC Pct LCS/LCSD RPD Spikcd Malysrs Parameter ResuUs Raov Limrts RPD Lim,l4 Amount Dale


### Bolynuclear Aromatice GC/M3

# ~ 0



### SCS ReG# 814189 Lab Control Sample Printed Date/Time 02/05/2008 12:09 Prep eatch XXX19059 

### Cuent Name The Environmental Company, Inc. (TEC) Method SW3520C Project NamH# 9121-003 Red Hill BFSF Date 01/22/2008 Matri: Water (Surface, Eff., Ground)

QC Pa LCS/[.CSD RPD Sptked Analysts Pazarnctor Reaulis Recov Ltmrts RPD Limes Amount Datc


### Bolynuclear Aromatica GC/MS Acenaphthylene LCS 0.300 60 ( 50-105 ) 0.5 ug/L Ol /28/2008
Acenaphffiene LCS 0.303 61 ( 45-110 ) 0.5 ug/L 01/28/2008

Fluorene LCS 0.310 62 ( 50-110 ) 0.5 ug/L 01/28/2008



### Phenanthrene LCS 0.319 64 ( 50-115 ) 0.5 ug/L 01/28/2008

Anthtacene LCS 0.311 62 ( 50-110 ) 0.5 ug/L 01/28/2008



### Fluorenthene LCS 0.373 75 ( 55-115 ) 0.5 ug/L 01/28/2008
Pyrene LCS 0.384 77 ( 50-126 ) 0.5 ug/L 01/28/2008


### Benzo(a)Anthracene LCS 0.363 73 ( 55-I10 ) 0.5 ug/L 01/28/2008
Chtysene LCS 0.381 76 ( 55-110 ) 0.5 ug/L 01/28/2008
Benzo[b]Fluonmthene LCS 0.369 74 ( 45-120 ) 0.5 ug/L 01/28/2008
Benzo[k]Buoranthene LCS 0.364 73 (49-125) 0.5 ug/L 01/28/2008


### Benzo[a]pyrene LCS 0.356 71 ( 55-110 ) 0.5 ug/L 01/28/2008
lndeno[I,2,3-c,d] pyrene LCS 0.335 67 ( 45-125 ) 0.5 ug/L 01/28/2008
Dibenw[a,h]anthracene LCS 0.325 65 ( 40.125 ) 0.5 ug/L 01/28/2008


### Benzo[g,h,i]perylene LCS 0.352 70 (40-125) 0.5 ug/L 01/28/2008
Naphthalene LCS 0.264 53 (40-115) 0.5 ug/L 01/28/2008
1-Methylnaphthalene LCS 0.293 59 ( 35-121 ) 0.5 ug/L 01/28/2008
2-Methylnaphthalene LCS 0.266 53 ( 45-]05 ) 0.5 ug/L 01/28/2008

Surrogates 

### Terphenyl-dl4 <surr> LCS 79 ( 50-135 ) 01/28/2008

# FFM

SGS ReLq 814189 Lab Conttol Sample Printed Date/rime 02105/2008 12:09 Prep Batch XXX19059 CBent Name The Environmental Company, Inc. (TEC) Method SW3520C Project Name/q 9121-003 Red Htll BFSF Date 01/22/2008 Matri: Water (Surface, Eff., Ground)
QC Pct LCS/LCSD RPD Spiked Anelysts Patamctcr Resuitl Rccov Ltmrts RPD Ltmns Amount Dare


### Polynucleas Aromatica GC/!1S

Bateh XMS4385 Method 8270C SIMS Instrument HP 6890/5973 MS SVOA

# ~

Printed DatelTime 02/05/2008 12:09 

### Prep Betch VXX17866

Metbad SW5030B Date 01/23/2008 SCS Ref.# 814440 Lab Control Sample

Client Neme The Environmental Company, Inc. (TEC) ProjeetNamel# 9121-003 Red Hill BFSF Matrix Water (SurFace, Eff:, Ground)
QC results affect the following production samplcs. 1080224001,1080224004,1080224005,1080224006,1080224007

QC Pct LCS/I.CSD RPD Spikcd Analysis 

### parsrneter Resvin Rocov Limin RPD Limm Amount Date


### Volatile Fuels Departme[nt
Gasoline Range Organics LCS 228 114 f ( 79-108 ) 200 ug/L 01/23/2008

Surrogates
4-Bromofluorobenzene <surt> LCS 99 ( 50-150 ) 01/23/2008



### Batch VFC8836 Method SW8015B 

### Instrument HP 5890 Senes II PID+HECD VBA

# eivitils

SGS Ref.# 814680 Lab Control Sample Printed DateITime 02/05R008 12:09 Prep Batch MXX19964 Cllent Name The Environmental Company, Inc. (TEC) Method SW3010A Project Name/# 9121-003 Red Hill BFSF Date 01/24/2008 Matri: Water (Surface, Eff., Ground) QC rcsults affect thc following productton samplcs: 1080224001,1080224004,1080224005,1080224006,1080224007
QC P<t LCS/LCSD RPD Spiked Amlysis Paremctcr Rpultr Recov Limiu RPD Ltmtts Amount Datc
Mat.aln by ICP/NS

Lead LCS 971 97 ( 80-120 ) 1000 ug/L 01/2812008

Batch MMS5294 Method SW6020 Instrument Perkin Elmer Sciex ICP-MS P3

# 979F

q■

SGS Ref.# 815214 Lab Control Sample Printed Date/Time 02/05/2008 12:09 Prep Batch VXX17871 Client Name The Environmental Company,.lnc. (TEC) Method SW5030B ProjectName/# 9121-003RedHiI1BPSF Date 01129/2008 Matrix Water ($urface, Eff., Ground) QC n:sults affecl the following produclton samples. 1080224001,1080224004,1080224005,1080224006,1080224007,1080224008

QC Po LCS/LCSD RPD Spikod Amlysis Pammeter Rewns Rccov Limm RPD Limns Amoum Delc


### Volatile Gas Chromatography/Elasa Spectroecopy

# ~

SGS Ref.# 815214 Lab Control Sample Pdnted DatelPime 02/05/2008 12:09 

### Prep Betch VXX17871 Clieat Name The Environmental Company, Inc. (TEC) Method SW5030B Pro)ect Neme/# 9121-003 Red Htll BFSF Date 01129/2008 Metrix Water (Surface, Eff:, Ground)
QC Pct LCS/LCSD RPD Sptked Anelysis Parameter Resulta Recov Ltmrts RPD Limiu Amount Dem


### Volatile Gas Chromatography/llass Speotrosaopy
Benzene LCS 30.7 102 ( 80-120 ) 30 ug/L 01/29/2008

Toluene LCS 31.3 104 ( 77-I20 ) 30 ug/L 01/2912008
Ethylbenzene LCS 32.2 107 ( 80-I20 ) 30 ug/l. 01129/2008
n-Butylbenzene LCS 33.7 112 ( 80-124 ) 30 ug/L 01/29/2008


### 1,4-Dtchlorobenzene LCS 33.5 112 ( 80-120 ) 30 ug/L 01/2912008
1,2-Dichloroethane LCS 30.5 102 ( 80-129 ) 30 ug/L 01/29/2008


### 1,3,5-Trimcthylbenune LCS 33.3 111 ( 80-I28 ) 30 ug/L 01/29/2008

4-Chlorotoluene LCS 35.8 119 ( 79-128 ) 30 ug/L 01/29/2008

Chlorobenzene LCS 32.1 107 ( 80-120 ) 30 ug/l. 01/29/2008
4-Methyl-2-pentanone (MIBK) LCS 73.6 82 ( 69-134 ) 90 ug/L. 01/29/2008
cts-1,2-Dichlorcethene LCS 28.5 95 ( 80-125 ) 30 ug/L 01/29/2008


### 4-Isopropyltoluene LCS 32.8 109 ( 80-125 ) 30 ug/L 01/29/2008
cts-1,3-Dichloropropene LCS 24.8 83 ( 80-I20 ) 30 ug/L. 01/29/2008


### n-Propylbenzene LCS 37.7 126 ( 80-129 ) 30 ug/L 01/29/2008
Styrene LCS 31.6 105 ( 80-120 ) 30 ug/L 01/29/2008



### Dibromomethane LCS 26.0 87 ( 80-120 ) 30 ug/L 01/29/2008
trans-1,3-Dtchloropropene LCS 31.8 106 ( 80-124 ) 30 ug/L 01/29/2008

1,2,4-Tnchlorobenzene LCS 25.9 86 (80-120) 30ug/L 01/29/2008

1,1,2,2-Tetrachloroethane LCS 30.5 102 ( 76-123 ) 30 ug/L 01/29/2008


### 1,2-Dibromo-3chloropropane LCS 31.8 106 (73-130) 30 ug/[. 01/29/2008
Methyl-t-butyl ether LCS 42.8 95 ( 80-120 ) 45 ug/L 01/2912008

# NJ

SCS ReL# 815214 Lab Control Sample Printed DatelPime 02/05/2008 12:09 Prep Bateh VXXI7871 Client Name The Envtronmental Company, Inc. (TEC) Method SW5030B Project NameNt 9121-003 Red Hdl BFSF Date 01/29/2008 MaMx Water (Surface, Eff., Ground)

QC Pct LCS/LCSD RPD Sptked Anelysis Paremeter Results Rccov Limas RPD Ltmits Amount Datc
Volatil® Gae Chromat:oqraphy/hiasa SpecYros

Telrachloroethene LCS 28.1 94 ( 79-122 ) 30 ug/L 01/29/2008

Dtbromochloromethane LCS 30.6 102 ( 80-120 ) 30 ug/[. 01/29/2008
1,3-Dichloropropane LCS 33.8 113 ( 80-121 ) 30 ug/L 01/29/2008

1,2-Dibromoethane LCS 30.5 102 (80-I20) 30 ug/L 01/29/2008

Carbon tetrachlotide LCS 31.4 105 ( 80-126 ) 30 ug/L 01/29/2008
1,1,1,2-Tetrachloroethane LCS 30.7 102 ( 80-120 ) 30 ug/L 01/29/2008

Chloroform LCS 30.8 103 ( 80-124 ) 30 ug/L 01/29/2008

Bromobenzene LCS 28.8 96 ( 80-120 ) 30 ug/L 01/29/2008

Chloromethane LCS 29.5 98 ( 67-125 ) 30 ug/L 01119/2008
1,2,3-Trfchloropropane LCS 31.0 103 ( 80-120 ) 30 ug/l. 01129/2008

Bromomethane LCS 30.0 100 ( 30-140 ) 30 ug/L 01/29/2008

Bromochloromethane LCS 28.4 95 ( 77-129 ) 30 ug/L 01/29/2008
Vinyl chlotide LCS 30.8 103 ( 72-145 ) 30 ug/L 01/29/2008

DichlorodiBuoromethane LCS 31.3 104 ( 62-153 ) 30 ug/l. 01/29/2008

Chloroethane LCS 29.1 97 ( 67-133 ) 30 ug/L 01/29/2008
sec-Butylbenzene LCS 34.2 114 ( 80-120 ) 30 ug/L 01/29/2008

Bromodichloromethane LCS 28.7 96 ( 80-120 ) 30 ug/L 01/29/2008
1,1-Dichloroethene LCS 29.3 98 ( 76-130 ) 30 ug/L 01/29/2008
2-Butanone (MEK) LCS 96.3 107 ( 66-136 ) 90 ug/C. 01/29/2008
Methylene chloride LCS 28.1 94 ( 63-131 ) 30 ug/L 01/29/2008

# ~

SCS Ret# 815214 l.ab Control Sample Prioted Date/Pime 02/0512008 12:D9 Prep Batch VXX17871 

### Client Name The Environmental Company, Inc. (TEC) Method SW5030B Project Name/# 9121-003 Red Hill BFSF Date 01/29/2008 Matrix Water (Surface, Eff., Ground)

QC Pct LCS/LCSD RPD Spiked A1mlysis Paremetet Rcsulta Rucov Limrt¢ RPD L .mn.r Ammmt Date


### Volatile Gae Chromatoqraphy/Maee Spectroac
TrlchloroHuoromethane LCS 32.6 109 (68-145) 30ug/L 01/29/2008
P& M-Xylene LCS 64.0 107 ( 80-120 ) 60 ug/L 01/29/2008
Naphthalenc LCS 26.8 89 ( 75-120 ) 30 ug/L 0I/29/2008
o-Xylene LCS 30.7 102 ( 80-120 ) 30 ug/I. 01/29/2008

Bromofonn LCS 29.7 99 ( 80-120 ) 30 ug/L 01/29/2008



### 1-Chlorohexane LCS 54.6 121 ( 70-125 ) 45 ug/L 01/29/2008
1,2,4-Tnmethylbenzene LCS 33.2 111 ( 80-125 ) 30 ug/L 01/29/2008
tert-Butylbenune LCS 32.3 108 ( 80-122 ) 30 ug/L 01/29/2008

l,l,l-Tnchloroethane LCS 31.9 106 ( 80-122 ) 30 ug/L 01/29/2008


### l,l-Dichloroethane LCS 31.4 105 ( 80-120 ) 30 ug/L 01/29/2008



### 2-Chlorotoluene LCS 36.5 122 ( 80-125 ) 30 ug/I. 0IR9/2008

Tnchloroethene LCS 26.9 90 ( 80-125 ) 30 ug/l. 01/29/2008

trans-1,2-Dichloroethene LCS 28.9 96 ( 79-132 ) 30 ug/L 01/29/2008


### 1,2-Dichlorobenzene LCS 29.8 99 ( 80-120 ) 30 ug/l. 01/29/2008
2,2-Dichloropropane LCS 32.1 107 ( 80-132 ) 30 ug/L 01/29/2008

Hexachlorobutadiene LCS 26.9 90 ( 77-125 ) 30 ug/L 01/29/2008
Isopropylbenzene (Cumene) LCS 32.0 107 ( 80-121 ) 30 ug/L 01/29/2008
1,2-Dichloropropane LCS 30.6 102 ( 80-121 ) 30 ug/L 01/29/2008


### 1,1-Dichloropropene LCS 31.5 105 (80-122) 30ug/L 0I/29/2008
1,1,2-Tnchloroethane LCS 31.5 105 (77-120) 30 ug/l. 01129/2008
1,3-Dichlorobenzene LCS 33.1 110 (80-120) 30 ug/L 01/29/2008

### _
.
~

SGS Ref.# 815214 Lab Control Sample Printed Datefl7me 02/05/2008 12:09 Prep Batch VXX17871 

### Client Name The Environmental Company, Inc. (TEC) Methoa SW5030B ProjectName/# 9121-003RedHiI1BFSF Date 01/29/2008 Matrix Water (Surface, Eff., Ground)

QC Pct LCS/I.CSD RPD Spiked Analysis Paremeter

~ Reaunc Recov Limm RPD Limus Ammm1 Date


### Volatile Gas Chromatoqraphy/Dlasa Spectroec

1,2,3-Tnchlorobenzene LCS 25.5 85 ( 77-120 ) 30 ug/L 01/29/2008

Surregates 1,2-Dichloroethane-D4 <surr> LCS 102 ( 73-120 ) 01129/2008

Toluene-d8 <surr> LCS 100 ( 80-120 ) 01/29/2008



### 4-Bromofluorobenzene <surr> LCS 104 ( 76-120 ) 01/29/2008

Batch VMS9632 Method SW8260B Instrument HP 5890 Series 11 MS3 VNA

# ~ CHAIN OF CUSTODY RECORD SGS Envxronmental Services 

# 1080224 Locattona Nationwide Alasxa aawaii Maryfend Louiaana New Jaisey West Virginia North Caroliaa us s oi 

# ;LIENT: TEC INC. 0 S~ 

# #: ' `"', ,RePferduce bNTACT:,teff Hart PHONS NO: 808.528.1445 ; Page of


## ,ROJECT: 9121-003 SITE/PWSID#: Red Hill BFSF

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# Q~ 

# I CHATN OF CUSTODY RECORD SGS Environnaental Servicer.T 

# 1080224 Locatlons Nadonwide Alaska liawai; Maryland Louisisna New 7ersey West Vitginia Nrnlh Cnml' n 

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documentsVonnelapprovetl1F016 SGS_ COC_electronk.xls rav.01 011131Z0p6

# SGS Environmental Services Alaslca Division Level II Laboratory Data Report
Project: 9121-003 Red Hill BFSF Client: T6e Environmental Company, Inc. (TEC) SGS Work Order: 1080225

Released by:

~ 

# _SGS_

Barbara Hager Alaska Division Projeet Manager

Contenls: CoverPage Case Nanebve Final Repon Pages Qualdy Conbol Summary Fomis Chain of Custody/Sample Receipt Fomis 

# Barbara Hager 2008.02.08 16:42:10 - 09'00'

NoOe: Unless othervrise noted, all quality assurancelqualily conbol criteria is in compliance with the alandards sel foM by the proper regulatory authonly, are SGS Qualiry Assurance Pragiam Plen, and tAe Nabonal Environmental Acpedeebon Conference.

# ~

:Ilent Name: The Environmental Company, Ine. (TEC)

~ rojeet Name: 9727-009 Red HIII BFSF Norkorder No.: 7080225 

## CASE NARRATIVE ., ,.

Print Date: 2/8/2008



## Sample Comments
Refer to the sample receipt fonn for Informabon on sample condition.
Lab Samole ID Samole TvDe Client Samole ID

There were no analy0cal anomalies assoclated wRh the data reported herein.

SGS Environmental Servlces Inc I Alaeke Dlvlelon 200 W est Potter Drrve Anchora9e Aleske 99518 l I/an11 SR9 91I] 119^]1 aa1 51n1 • aaa mm Member ofSGS GrouP (Soclet6 Generele tle Survaillance)

# A~
Laboratory Analytical Report

Client: The Envlronmental Company, Inc.

1001 Blshop Street Ste 1400 ASB Tower Honolulu, HI 96813 Aftn: Jeft Hart T: (808)528-1445 F:(808)528-0768 

### jshart@teclnc.lbm Project 9121-003 Red Hill BFSF Workorder No.: 1080225

CertiBcagon: I certify that this data package is in compliance wilh the tenns and conditions of tha contract, bolh technically and for completeness, other than the condltlons noted on the sample data

- sheet(s) and/or the case narra0ve. Thls certificabon applies only to the tested parameters and

the specific sample(s) received at the laboratory. 

# do 

# Barbara Hager

~ 

# S(aS'
BarbaTa Hager 

# 2008.02.08 16:42:27 -
Alaska Dlvtsion Project Managa 

# 09'00'

If you have any questlons regarding Iltis report, or if we can be of further assistance, please contact your SGS Project Manager.
Mark Abe mark.abe@sgs.com Project Manager

SGS Envlronmenial Servicee Inc I Aleeke Urvislan 200 Weel paltar Drive Anchorega Alaeka 99518 T tl901156223<3 f f90]15fi1.5301 w ssga.com MemEerofSGS Group

# SG$-

Prinl Date: 2/8/2008
Endosed are the analy0cal results associated wM thls workorder As requlred by the state of Alaska and the USEPA, a fonnal Quallty Assurance/Quality Control Program is maintelned by SGS. A copy of our Quality Assurance Plan (QAP), which outlines mis program is available at your request. The laboratory certifioabon numbers are AK971-05 (DW), UST-005 (CS) and AK00971 (Micro) for ADEC and 001582 for NELAP (RCRA methods: 1010/1020, 1311, 6000/7000, 9040/9045, 9056, 9060, 9065, 8015B, 8021 B, 8001A18082, 8260B, 8270C). Excepl as specifically noted, all statements and data in this report are In conformance to the provlslons set foM by the SGS QAP, the Natlonal Envlronmental Laboratory Accredifation Program and, when appllcable, other regulatory authorities. If you have any quesaons regarding this report or if we can be of any asslstance, please oontaot your SGS Project Manager at 907-562-2343.

The following descriptors may be found on your report whlch wlll serve to further qualify the data.
MDL Method Detection Limft PQL Practical Quantitation Limit (reporting limlt). CL Control Limit U Indicates the analyte was analyzed for but not detected. F Indlcates value tltat is greater than or equal to the MDL. J The quantilation is an estimation. ND Indicates the analyte Is not detected B Indlcates the analyte is found in a blank assoclated wi61 the sample. ' The anatyte has exceeded allowable regulatory or control limlts. GT Greater Than LT LessThan Q QC parameter out of acceptance range. M A mabix etfect was present. E The analyte result Is above the calibrated range. DF Analytical Dilutlon Fador JL The analyte was posltively Identfied, but the quantitatlon Is a low estimation. <Sum Surrogate QC splked standard
Note: Soll samples are reported on a dry weight basis unless othervvlse specrtied

SGS Env,ronmenlel Serv,cee Inc 

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## SAMPLE SUMMARY Pnnt Date: 218l2008 ;Ilent Name: The Envlronmental Company, Ino. (TEC) Iroject Name: 8121-003 Red HIII BFSF Norkorder No.: 1080225 

## 4nalytical Methods

vlethod Descriotlon AnalWcal Methad )RO by 8015B Low Volume (W) SW8015B 

## Sample ID Cross Reference
Lab SamDle ID Cllent Samole ID 1080225001 RHMW2254-01-WG10.1

SGS Envrtonmental Ssrvlcee Inc I Aleeke Dlvlalon 200 W est Potter Drive Anchorege Alaske 58518 T(onv)ssoo

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The Environmental Company, Ino. (TEC) Pdnt Date: 218/2008

CllentSamplelD: RHMW2254-01-WG78.1 AII DatesRmes are Alaska Local Tlme SGS Ref. #: 1080225001 Collectlon Date/71me: 02106/08 09:30 Project ID: 9121-003 Red HIII BFSF Receipt Datalflme: 02/07/08 11:15 Matrix: Water (Surface, Eff., Ground)

Semivoiatiie Organic Fuels Department

Parameter R asuh P L7CL

Diesel Range Organics ND 0.0515 

### 5a Androstane <surr> 90.6 50-150
Batch Informatlon 

### a 3~ 

### Em¢ Units DF Batch Batch uali8ers


### mg/L 1 XFC7835 XXX19093 % 1 XFC7835 XXX19093

Analyhcal Batch: XFC7835 Prep Batch: XXX79093 InlBal Prep Wt.Nol.: 970 mL Analytical Method: SW8015B Prep Method: SW3520C Prep Extract Vol.: 1 mL Analysls DateRme: 02/08/08 10:42 Prep DateTme: 02107/08 11:35 Container ID:1080225001-A D ilution Factor. 1 Analyst: HKG

SGS Environmenlel Servlcee Inc I Aleake Dlvlsion 20D W est Poller Drive Ancftora9e Alaeka 99518 i f 19071 584.R3e3 f f90115B1.5301 v. MemEer of SGS Group (SoeIB16 G4n6rale 0e Survelllence)

# 0

SGS ReG# 815962 Method Blank Printed Date/rime 02/08/2008 16:39 Client Name The Environmental Company, Inc. (TEC) Prep Bateh XXX19093 ProJeet Name/# 9121-003 Red Hill BFSF Method SW3520C Metria Water (Surface, E.ff., Ground) Date 02/07/2008 QC results affect thc follomng produclion samplcs: 1080225001 Reporttng/Contral Anelysis Peratncter Resu lt s MDL Umts Date Diesel Range Organics ND 0.0500 0.0100 mg/[. 07/08/08
Surrogsta

5a Androstane <surr> 98 60-120 % 02/08ro8
Betch XFC7835 Method SW8015B Insnoment HP 5890 Scrics 11 FID SV D R

### SCS Ref.N 815963 Lab Control Sample Printed Date/rime 02/08/2008 16:39 815965 Lab Control Sample Duplicate Prep Batch XXX19093 Client Name The Environmental Company, Inc. (TEC) Method SW3520C , Project Neme/I! 9121-003 Red Hill BFSF Date 02/07/2008 Matrix Water(Surface, EfP., Ground) QC results affcct thc following production samplcs• 1080225001

QC 

### Parameter Results Pct Rccov LCS/LCSD

Lim,ts RPD RPD Sp,ked Limas Amoum A,mlys,s Date


### Semivolati.le Orqanic EVela DeparTment Diesel Range Organics LCS 1.02 102 ( 

### 75-125 ) 

### 1 mg/L 02/08/2008 LCSD 1.06 106 4 (<20) 1 mg/L 02/08/2008
Surrogates 5a Androstane <surr> LCS 94 "( 60-120 ) 02/08/2008 LCSD 101 7 02/08/2008

Batch XFC7835 Method SW8015B Instrument Hp 5890 Series 11 FID SV D R

# ~ CHAIN OF CUSTODY RECORD SGS Environmental Servicr- r,,,,



# 10802.25 IMNNoqmmmummim I.ocations Nationwide 

### Alaska Hawaii Maryland Louisiana 

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## REMARKS

RHMW2264-01-WG70.1 2l612006 Water X

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doaunrentsVotmslapprovedlFOla_SOS coC_eleetroMoxls rev.01 01113120o6

# SAMPLE DELIVERY GROUP CASE NARRATIVE

Client: The Environmental Company Job No: F55567 

### Site: Red Hill Bulk Stomge Facility, HI Report Date: 2/18/2008 5:28:31 PM 1 Sample was collected on 02/06/2008 and was received at Accutest on 02/08/2008 properly preserved, at 1.8 Deg. C and intact. The Sample recetved an Accutest job number of F55567. A listing of the Laboretory Sample ID, Client Sample ID and dates of collection are ptrsented in the Results Summary Section of this mpott 

### Except as noted below, all method specified calibtatlons and qualiry control perfonnance criterla wee met for this job. For more infonnation, please refer to QC summary pages. 

## Extractables by GC by Method SW846 8015 M

Matrix: AQ Batch ID: OP24049 All samples were exttacted within the tecommended method holding time. 

### All samples were analyzed within the tecommended method holding time. All method blanks for this batch meet method specific critetia. Samples F55505-32MSD, F55505-32MS, F55505-32MSD were used as the QC samples indicated. Matrix Spike Recovery for TPH (C I O-C28) is outside control limits. Outside control limits due to high level tn sample relative to spike amount. 

### Samples OP24049-MS, OP24049-MSD have surrogates outside contml limits. Probable cause: due to matrix interference. OP24049-MS, OP24049-MSD for o-Telphenyl: Oucside control limits due to dilution.

Accutest Laboramries Southeast (ALSE) celtifies that this'epolt meets the pmject'equirements for analytical data produced for the samples as received at ALSE and as stated on the COC. ALSE certifies that the data meets the Data Quality Objectives for precision, accutacy and completeness as spectfied in the ALSE Quality Manual except as noted above. This report is to be used in tts entirety. ALSE is not responsible for any assumptions of data quality if pattial data packages are used.
Natmtive pmpared by.

Date: Februarv 18. 2008 

### Ellen Pampel, lnorganic QA (signature on file)

Monday, February 18, 2008



## ®® 4 of 53 0 aoe-l.rr

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### Accutest Laboratories 

# Report of Analysis Page 1 of 1 j
rtSamplelD: RHMW2254-01-WGI0.1 © 

### Sample ID: F55567-1 Date Sampled: 02/06/08 dz: AQ - Ground Water Date Received: 02/08/08 rod: SW846 8015 M SW846 3510C Percent Solids: n/a 

### ect: Red Hill Bulk Storage Facility, HI
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch #1 YY07207.D l 02/I1/08 NY 02/09/08 OP24049 GYY234 #2


### Initial Volume Final Volume Run #1 980 ml 1.0 ml Run #2
CAS No. Compound Result RL MDL Units Q

TPH (C10-C28) ND 0.26 0.10 mg/I


### CAS No. Surrogate Recoveries Run# 1 Run# 2 Limita

84-15-1 o-Terphenyl 91% 42-I14%



### ND = Not detected MDL - Method Detection Limit J= Indicates an estimated value RL = Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N= Indicates presumptive evidence of a compound

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Job Number: F55567 Account: TECHIHON The Environmental Company Project: Red Hill Bulk Storage Facility, HI Sample File ID DF Aualyzed By Prep Date Prep Batch Analytical Batch OP24049-MB YY07206.13 1 02/11/08 NY 02/09/08 OP24049 GYY234



### The QC reported here applies to the following samplea: Method: SW846 8015 M



### F55567-1

CAS No. Compouud Result RL 

### MDL Units Q

TPH (CIO-C28) ND 0.25 0.10 mg/1

CAS No. Surrogate Recoveries Limits 0



### 84-15-1 o-Terphenyl 77%0, 42-114% 

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# Blank Spike Summary Job Number: F55567 Account: TECHIHON The Environmental Company Project: Red Hdl Bulk Storage Factltty, HI Page 1 of 1 ~ 

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### By Prep Date Prep Batch Analytical Batch OP24049-BS YY07205.D 1 02/11/08 NY 02/09/08 OP24049 GYY234



### The QC reported here applies to the following samples: Method: SW846 8015 M

F55567-1 vt 

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# ®

CAS No. Compound



### TPH (CIO-C28)

CAS No. Surrogate Recoveries

84-15-1 o-Tetphenyl 

### Spike BSP BSP mg/1 rog/1 % Limits



### 1 0.839 84 59-114

BSP Limits

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