Dry Scrubber Blue Goose Combustion Data Septem ber 2011 Fyrite

Location : Dry

Scrubber Date 9/27/11 Time:

run O2 CO2

1 18 3 2 18 3 3 18 3
Avg 18 3

Molecular wt

1 29.2 2 29.2 3 29.2

AVG 29.2

diff 0

0 0

All diff must be less that 0.3
Analysts: O'Brien &Gere

Page 1Test ID: 9-27-11-POM-ABF Run#1 

### Value 0

0 0

180.00 110.00 0.0014 0.0000 0.0000 200.00 200.00 0.0014

230.00 150.00 0.0025 0.0025

910.00 1000.00 0.0004 0 0.00040



### Value 2.9000 1.4000 4.3000 Volume of MC Used 3M (ml) 3M W eight of MCEM From Back Glassware Rinses (g) 3M Net of MCEM Adjusted from Blanks (g)



### MCEM Analysis Calculations 1B QC Filter Blank (g) Net MCEM From Filter (g) Volume of Acetone Used 2A (ml) Volume of MC Used 2M (ml) 2M W eight of MCEM From Front Half Glassware Rinses (g) 4A W eight of Acetone Blank (g) 4M W eight of MC Blank (g) Volume of MC Used in Blank (ml) Volume of Acetone Used in Blank (ml)

Total mg of Particulate MCEM **Total mg of MCEM** 

# An **ode Bake Furnace Dry Scrubber Test #1** 

3W B W eight of MCEM From Blank (g) 3WNet of Extracted W ater Adjusted from Blank (g)

Total mg of Gaseous MCEM Volume of Deionized W ater Used 3W(ml) Volume of Deionized W ater Used in Blank (ml) 2M Net MCEM Adjusted from Blank (g)



# 9/27/2011

**MCEM Analysis Data** 1A Filter W eight (g)

3WW eight of Impinger W ater Plus Back Half Rinses Extracted (g). Volume of Acetone Used 3A (ml)Test ID: 9-27-11-POM-ABF Run#1



### Value 0.5664 0.84 18 % O 2 in Anode Bake Furnace Gas Stream 3.0000 %CO 2 in Anode Bake Furnace Gas Stream 29.2 28.638309 0.050150982 533.5 643.4 29 70 1.65 1.021 29 128 0.89 71.956 79.2 28.98 0.25 0.00034088462



### Value 70.6329889 35.80838 61.7 2.90422 17.5 0.825125 0.050151 0.038839 99.7966 I = % Isokinetic variation 

### Air Test Calculations  Hav g= average orifice meter differential Vm = Total sample volume from dry gas meter (dcf) Vlc Volume collected Ps = Absolute stack gas pressure (in Hg)

Vwc (std) = conv erted water v olume Total silica gel catch (ml) Vwsg (std) = conv erted silica gel water v olume Bws = fraction of gas that is moisture Total sampling time required for test (min) Ms = Stack gas (wet) molecular weight (lb/lb-mole) Bws = Stack gas moisture content

Vwc(std) Nozzle diameter (in) Area of Nozzle (ft^2)

Vm (std) = Volume of sample measured by DGM (dscf) Vs = Average stack gas v elocity Total impinger catch (ml) Tm = Absolute average dry gas meter temp (R). Ts = Stack gas absolute av erage temperature (R) Pm = Pressure at orifice meter (in. Hg) Ta = Sampling site ambient temperature, (°F)  H@ = Orifice meter calibration factor, (in. water) Y = Dry gas meter calibration factor Pbar = Barometric pressure, (in. Hg) Md = Stack gas dry molecular weight, (lb/lb-mole) 

# An **ode Bake Furnace Dry Scrubber Test #1**  **9/27/2011**

**Method 5 Parameter** p = Stack gas v elocity pressure (av g. sqrt p - in. water) Cp = Pitot tube calibration coefficient28.98529 0.014706Test ID: 9-27-11-POM-ABF Run#1 LIMS ID#: 2011008909



### Value 2.9000 0.0029 1.4 0.0014 70.63298889

29 38.48 9.45 Green Carbon Baked tons/hr 0.050150982 62418.77575 3745126.5452 82674.39211 Acfm 65714.41835 Scfm 0.0009 Emission Rate of Total MCEM gr/dscf 0.34 8.13 0.1635 3.92 **0.50**

**0.036 Emission Rate of Gaseious MCEM lb/Ton of Green Carbon Baked**  **0.017 Emission Rate of Particulate MCEM lb/Ton of Green Carbon Baked**  **0.053 Emission Rate of Total MCEM lb/Ton of Green Carbon Baked** 

Start time: 9/27/2011 9:05 End time: 9/27/2011 11:23

Total mg of MCEM in Gaseous Sample

Vm(std) Volume of Air Sampled by DGM (dscf) 

# An **ode Bake Furnace Dry Scrubber Test #1**  **9/27/2011**

**Combined Method 5 Parameter and Analytical**
Total g of MCEM in Gaseous Sample

Pbar Barometric Pressure During Test (in Hg) Area of Anode Bake Furnace Stack (ft2)

Bws Moisture in Roof Emissions Qstd Flow of Anode Bake Furnace Emissions (dscf/min) Total mg of MCEM in Particulate Sample Total g of MCEM in Particulate Sample

Qstd Flow of Anode Bake Furnace Emissions (dscf/hr)

Emission Rate of Gaseous MCEM lb/hr Emission Rate of Gaseous MCEM lb/d Emission Rate of Particulate MCEM lb/hr

**Emission Rate of Total MCEM lb/hr** Emission Rate of Particulate MCEM lb/d

## Value 6 0.006 70.63298889

29 38.48 9.45 Green Carbon produced tons/hr 0.050150982 62461.8529 Qstd Flow of Anode Bake Furnace Emissions (dscf/min) 3747711.174 0.0013 Particulate gr/dscf **0.70 Particulate lb/hr** 

**0.074 Particulate Emissions from Anode Bake Furnace lb/Ton of Green Carbon Baked**  Qstd Flow of Anode Bake Furnace Emissions (dscf/hr) 

## Combined Method 5 Parameter and Analy **tical**

Vm(std) Volume of Air Sampled by DGM (dscf) Pbar Barometric Pressure During Test (in Hg) 

# An **ode Bake Furnace Emission Calculations Test #1 9/27/2011** 

Total mg of Particulate Total g of Particulate

Area of Anode Bake Furnace Stack (ft2 )

Bws Moisture in Anode Bake Furnace Emissions