Client U.S. Steel 

Location Line 4 Waste Gas Stack (SV118) 

Date 7/12/2005 

Operator T. Kuchinski 

City, State Mt. Iron, Minnesota 

Calibration Input 

Analyzer 
Project U.S. Steel 

Sample Loc. 

Date 

Operators 

Line 4 Waste Gas Stack (SV118) 

711212005 

T. Kuchinski 

Analyzer Make I Mod. I SN 100AH 

Analyzer Range (span), PPM: 100 

Stripchart Speed (units): 20 cm/hr 

ANALYZER CALIBRATION DATA 

Note: Difference must be less than +1- 2 percent of span 

Cylinder 

Test Runs : Test 4 R1 Value, 

PPM 

Zero Gas 0 

Mid-range 51.2 

High-range: 93.1 

SYSTEM CALIBRATION BIAS AND DRIFT DATA: 

EPA METHOD 6C - 502 

ANALYZER CALIBRATION 

Cylinder 

Serial No. 

Zero Gas Nitrogen 

Mid-range CC63443 

High-range CC121446 

Analyzer Absolute Difference, 

Calibration Difference Percent of 

Response, PPM PPM Span 

0.0 0.0 0.00% 

51.2 0.0 0.00% 

93.0 0.1 0.10% 

Note: System Cal bias cannot exceed +1- 5 percent of span. Drift cannot exceed +/- 3 percent of span 

Initial Values Final Values 

Analyzer Cal System Cal System Cal System Cal System Cal 

Response Response, Response, Cal. Bias Response, Cal. Bias 

TEST RUN 1 Time (sec) PPM PPM %of Span PPM %of Span 

Zero Gas - 0 1.3 1.30% 2.2 2.20% 

Upscale Gas - 51 49 -2.20% 49.0 -2.20% 

TEST RUN 2 

Zero Gas - 0 2 2.20% 2.6 2.60% 

Upscale Gas - 51 49.0 -2.20% 50.0 -1.20% 

TEST RUN 3 

Zero Gas - 0 2.6 2.60% 3.30 3.30% 

Upscale Gas - 51.2 50.0 -1.20% 51.10 -0.10% 

System Calibration Bias =[(System Cal. Response- Analyzer Cal. Response) I Span] x 100 

Drift= [(Final System Cal. Response -Initial System Cal Response)/ Span] x 100 

Cert. PPM 

0 

51.2 

93.1 

Drift, 

Percent of 

span 

0.90% 

0.00% 

0.40% 

1.00% 

0.70% 

1.10% 
Project U.S. Steel 

Sample Loc. 

Date 

Operators 

Line 4 Waste Gas Stack (SV118) 

711212005 

T. Kuchinski 

Analyzer Make I Mod. I SN Teco48 

Analyzer Range (span), PPM: =-1-"0:-'0'---

Stripchart Speed (units): 20 cmlhr 

ANALYZER CALIBRATION DATA 

Note: Difference must be less than +1- 2 percent of span 

Cylinder 

Test Runs: Test 4 R1 Value, 

PPM 

Zero Gas 0 

Mid-range 34.1 

High-range: 60.4 

SYSTEM CALIBRATION BIAS AND DRIFT DATA: 

EPA METHOD 10· CO 

ANALYZER CALIBRATION 

Cylinder 

Serial No. 

Zero Gas Nitrogen 

Mid-ran_lle CC78171 

High-range CC12600 

Analyzer Absolute Difference, 

Calibration Difference Percent of 

Response, PPM PPM Span 

0.4 0.4 0.40% 

33.7 0.4 0.40% 

60.1 0.3 0.30% 

Note: System Cal bias cannot exceed +I- 5 percent of span. Drift cannot exceed +I- 3 percent of span 

Initial Values Final Values 

Analyzer Cal System Cal System Cal System Cal System Cal 

Response Response, Response, Cal. Bias Response, Cal. Bias 

TEST RUN 1 Time (sec)_ PPM PPM %of Span PPM %of Span 

Zero Gas 0 0.6 0.20% 0.4 0.00% 

L!!Jscale Gas 33.7 33.7 ·o.OO% 33.2 -0.50% 

TEST RUN 2 

Zero Gas 0 0.4 0.00% 0.3 -0.10% 

Upscale Gas 33.7 33.2 -0.50% 32.3 -1.40% 

TEST RUN 3 

Zero Gas 0.4 0.3 -0.10% 0.3 -0.10% 

Upscale Gas 33.7 32.3 -1.40% 32.7 -1.00% 

System Calibration B1as - [(System Cal. Response - Analyzer Cal. Response) I Span] x 100 

Drift= [(Final System Cal. Response- Initial System Cal Response) I Span] x 100 

Cert. PPM 

0 

34.1 

60.4 

Drift, 

Percent of 

span 

-0.20% 

-0.50% 

-0.10% 

-0.90% 

0.00% 

0.40% 
EPA METHOD 25A-THC as methane 

ANALYZER CALIBRATION 

Project 

Sample Loc. 

Date 

Operators 

U.S. Steel 

Line 4 Waste Gas Stack (SV118) 

711212005 

T. Kuchinski 

Analyzer Make I Mod. I SN Ratfisch Rs 55 CA 

Analyzer Range (span), PPM: 110 methane 

Stripchart Speed (units): 20 cmlhr 

Linearity Demonstration 

Zero Gas 

Low-range 

·Mid-range 

High-range 

Note: Response must be less than +/- 5 percent of actual calibibration gas values. 

Cert. PPM System Response Percent Diff 

Zero Gas 0 0.3 0.3 

Low-range 30.2 30.4 0.66 

Mid-range 46.5 47.3 1.72 

High-range 90.4 90 0.44 

SYSTEM CALIBRATION AND DRIFT DATA: 

(;ylinder 

Serial No. 

Air cylinder 

SG9165492BAL 

CC2937 

CC47777 

Cert. PPM 

0 

30.2 

46.5 

90.4 

Note: System Calibration cannot exceed +/- 5 percent of span gas value. Drift cannot exceed +/- 3 percent of span 

Initial Values Final Values 

System Cal System Cal Drift, 

Response Response, Response, Percent of 

TEST RUN 1 Time (sec) PPM PPM span 

Zero Gas 0.3 2.0 1.55% 

Upscale Gas 30.4 29.2 -1.09% 

TEST RUN 2 

Zero Gas 2.0 2.1 0.09% 

Upscale Gas 29.2 28.3 -0.82% 

TEST RUN 3 

Zero Gas 2.1 1.7 -0.36% 

Upscale Gas 28.3 29.5 1.09% 
Project U.S. Steel 

Sample Location 

Date 

Line 4 Wasre Gas Stack (SV118) 

7112/2005 

Operators T. Kuchinski 

Analyzer Make I Model/ SN 

Analyzer 0 2 Range (span),%: 

CaL Anal. Model 200 

25 

Analyzer C02 Range (span),%: 10 

Stripchart Speed (units): 20 cm/hr 

ANALYZER CALIBRATION DATA 

Note: Difference must be less than +f. 2 percent of span 

o, Cylinder 

Test Runs: Test 1 R1 Value, 

% 

Zero Gas 0.0 

Midwrange: 9.1 

HiQhwranQe: 20.0 

co, Cylinder 

Test Runs: Test 1 R1 Value, 

% 

Zero Gas 0.0 

Midwra_t:lge: 5.0 

High-range: 9.1 

SYSTEM CALIBRATION BIAS AND DRIFT DATA: 

EPA METHOD 3A 

ANALYZER CALIBRATION 

Analyzer Absolute 

Calibration Difference 

Response,% % 

0.0 0.0 

9.0 0.1 

20.0 0.0 

Analyzer Absolute 

Calibration Difference 

Response,% % 

o.o 0.0 

5.0 0.0 

9.0 0.1 

Difference, 

Percent of 

Span 

0.00% 

0.28% 

0.00% 

Difference, 

Percent of 

Span 

0.00% 

0.00% 

0.50% 

Note: System Cal bias cannot exceed+/- 5 percent of span. Drift cannot exceed +1- 3 percent of span 

Initial Values Final Values 

Analyzer Cal System Cal System Cal System Cal System Cal 

Response Response, Response, Cal. Bias Response, Cal. Bias 

TEST RUN 1 Time (sec) % % %of Span % %of Span 

Zero Gas 0 2 0.0 0.1 0.40% 0.00 0.00% 

Upscale Gas 0 2 20.0 20.0 0.00% 19.90 -0.40% 

Zero Gas C02 0.0 0.0 0.00% 0.1 0.50% 

Upscale Gas C~ 5.0 5.0 0.00% 5.0 0.00% 

TEST RUN 2 

Zero Gas 0 2 0.0 o.oo 0.00% 0.1 0.40% 

Upscale Gas 0 2 20.0 19.90 -0.40% 20.0 0.00% 

Zero Gas C02 0.0 0.05 0.50% 0.1 1.00% 

Upscale Gas C02 5.0 5.00 0.00% 5.0 0.00% 

TEST RUN3 

Zero Gas~ 0.0 0.1 0.40% 0.1 0.40% 

Upscale Gas 0 2 9.07 9.00 -0.28% 9.13 0.24% 

Zero Gas C02 0.0 0.1 1.00% 0.0 0.00% 

Upscale Gas C02 9.05 9.0 -0.50% 9.05 0.00% 

Fluorides Test Run 4 

Zero Gas 0 2 0.0 0.1 0.40% 0.0 0.00% 

Upscale Gas 0:l 9.1 9.1 0.24"/ .. 9.0 -0.12% 

Zero Gas C02 0.0 0.0 0.00% 0.0 0.00% 

Upscale Gas CO:z 9.05 9.05 0.00% 9.08 0.30% 

Particulate Test Run 4 

Zero Gas 0 2 0.0 0.0 0.00% 0.1 0.40% 

Upscale Gas 0 2 9.1 9.0 -0.12% 9.1 -0.08% 

Zero Gas C02 0.0 0.0 0.00% 0.1 0.50% 

Upscale Gas C02 9.05 9.08 0.30% 9.0 -0.10% 

nnft- UFtnal Svstem Cal. Response -lmtlal System Cal Response) I Span] x 100 

Drift, 

Percent of 

span 

0.40% 

0.40% 

-0.50% 

0.00% 

-0.40% 

-0.40% 

-0.50% 

0.00% 

0.00% 

-0.52% 

1.00% 

-0.50% 

0.40% 

0.36% 

0.00% 

-0.30% 

-0.40% 

-0.04% 

-0.50% 

0.40% 
Control Module C-2 Barometric Pressure 29.2 

Project: Routine Leak checks Previous Y --- 0.9969 

Date: 6/25/2005 Negative-· ok >5W.C. Previous Delta H -- 1.8844 

Technician: NRS Positive- ok > in.Hg 

Orifice Dry Gas Wet Test Dry Gas Meter WetTest Elapsed Meter Orifice 

Diff Volume Volume, Temp, F Meter Time of Coefficient Coefficient 

Presure H Cubic Feet Cubic Feet Inlet Outlet Temp, F Cal. Point y dH@ 

1Nomma1 t-mal ,final Final t-1nal Final Minutes SEC 

0.500 673.635 3940.50 76.0 73.0 71.5 17 44.03 

!Actual Initial Initial Initial Initial Initial Minutes 

666.680 3933.50 73.0 72.0 71.0 

0.50 Total Total Average Average Average 

6.955 7.00 74.5 72.5 71.3 17.73 1.0095 1.8464 

73.5 

Nominal Final Final Final Final Final Minutes SEC 

1.000 707.320 3974.00 78.0 75.0 73.0 8.0 57.81 

!Actual Initial Initial ln~ial Initial Initial Minutes 

702.290 3969.00 75.0 74.0 73.0 

1.00 Total Total Average Average Average 

5.030 5.00 76.5 74.5 73.0 8.96 0.9962 1.8544 

75.5 Tm 

Nominal Fmal Final Final Final Final Minutes SEC 

2.000 687.110 3954.00 83.0 75.0 71.5 8.0 58.94 

Actual Initial ln~ial Initial Initial Initial Minutes 

680.085 3947.00 80.0 74.0 71.5 

2".00 Total Total Average Average Average 

7.025 7.00 81.5 74.5 71.5 8.98 1.0036 1.8895 

78.0 Tm 

Nominal Final Final Final Final Final Minutes SEC 

3.000 693.190 3960.00 84.0 76.0 71.5 5.0 15.64 

!Actual Initial Initial Initial Initial Initial Minutes 

688.125 3955.00 83.0 75.0 71.5 

3.00 Total Total Average Average Average 

5.065 5.00 83.5 75.5 71.5 5.26 0.9945 1.9019 

79.5 Tm 

Nominal Final Final Final Final Final Minutes SEC 

4.000 699.275 3966.00 86.0 76.0 71.5 4.0 33.88 

Actual Initial Initial Initial Initial Initial Minutes 

694.210 3961.00 84.0 76.0 71.5 

4.00 Total Total Average Average Average 

5.065 5.00 85.0 76.0 71.5 4.56 0.9939 1.9075 

80.5 Tm Average 0.9995 1.8799 
Routine 

Dry Gas Meter Calibration 

Control Module Number: C-"2--

Date: (o-25' -osTechnician: -lfiVL/t"'S.,__ _____ _ 

Dry gas WetTest 

Leak Checks Barometric Press.: "2. c1. '2-

Positive _ _.:::o..ck:__at 5 in.H20 Previous Y: 

Negative 0 1<-- at 15 in.Hg Previous t,.H: --'"-'--

WetTest Elapsed 

Time of 

Meter Orifice 
Project Name: USS Minntac 

Module Number: ..::C:...-;:.2 ~:--::-:­

Date: 6-Aug-05 

Tecb:..:..N:o;R;::_S __ _ 

EPA MS POST TEST METER CALIBRATION 

Nominal sample conditions 

Delta H: 2 W.C. 

Vacuum: ----'9'--_in. Hg 

Project No.: 23/69-927-

Barometric Pressure: --::-::-::2':9':;."'12::. 

Previous Y: 0.9995 

Previous Delta H: -~1:::.8::7~9_:e9_ 

Pre cal +5% 

Pre cal~ 5% 

Within 5% YIN 

1.0495 

0.9495 

YES 

1.9739 

1.7859 

YES 
EPA M5 POST TEST METER CALIBRATION 

Prqj ect Name: uss M:."hc Project No.: 23/&'1-'12..lModule Number: C/2.. Nominal sample conditions Barometric Pressure: 2'1.1? 

Date: Y-(p-os- DeltaH: z..o w.c. Previous Y: . 7"'195"" 

Tech: NR.."> Vacuum: q in. Hg Previous Delta H : /.8792 

Equip Cal Data Sheets1 
Control Module C-5 Barometric Pressure 29.14 

Project Routine Leak checks Previous Y -- 0.9961 

Date: 71912005 Negaf1ve -· ok >SW.C. Previous Delta H -- 1.9659 

Technician: NRS Positive-- ok > in.Hg 

M5APR.WQ1 
Routine 

Dry Gas Meter Calibration 

Control Module Number: C./'i 

Date: 7 1'7 I o<:; 

Technici~n! ---"N"-'12.."'-"S'---------

Leak Checks 

Positive ok 

Negative o kOrifice Dry gas WetTest WetTest 

Barometric Press.: Z. '1. I'-! 

at 5 in. H20 Previous Y: 

at 15 in.Hg Previous ~H: 

Elapsed 

• 9 "t(.,( 

/. "Hos-4' 

Meter Orifice 
Project Name: USS Minntac 

Module Number: _,C'--"-5-::-:--::--:-

Date: 6-Aug-05 

Tech: -"NRS='---

EPA MS POST TEST METER CALIBRATION 

Nominal sample conditions 

Delta H: 0.92 W.C. 

Vacuum: 18 in. Hg 

Project No.: 23/69-927-

Barometric Pressure: --,:-;c;:2C;9'c'.~l2::.. 

Previous Y : 0.9946 

Previous Delta H : --:l-:.9,.:6:;:9::;-2-

Pre cal +5% 

Pre cal- 5% 

Within 5% YIN 

!.0443 

0.9449 

YES 

2.0677 

!.8707 

YES 
EPA MS POST TEST METER CALffiRATION 

BARR 

Project Name: u :;,s M ~. nh c 

Module Number: _...:C...=-----=:5:._ __ _ 

Date: __,8:.,_-....::(p:._-....::Cf5=---

Tech: ---'-N=R:o::S:.__ __ _ 

Equip Cal Data Sheets1 

Nominal sample conditions 

DeltaH: o.9'L W.C. 

Vacuum: \ 'i' in. Hg 

ProjectNo.: 2:C,/!ocr-92lBarometric Pressure: 2 'l.l )> 

Previous Y : .....:..· 'l,__'l:.._'-l:...:!a:___ 

Previous Delta H : (.9<.'1'2... 
ANEROID BAROMETER 

CALl BRA TION 

Barometer LD. Number: i3 A- OS"" 

Barometer Reference: f 12..J:.AJC.u 

Pretest Calibration: 

Before Adjustment 

After Adjustment 

Posttest Check: 

Notes: 

Barr Engineering Co. 

4700 W. 77th St 

Minneapolis, MN 55437 

(952) 832-2600 

Reference ("Hg) 

2'1 0'-/ 

Reference ("Hg) 

Project Name:----------

Project Number: ---------

Barometer ("Hg) Date Technician 

2c;.oo 7/2'-1/D.,. NR5 

Barometer ("Hg) Date Technician 
ANEROID BAROMETER 

CALIBRATION 

Barometer I. D. Number: 'J? A ...osBarometer Reference: f r ; A.. c <-> 

Pretest Calibration: 

Before Adjustment 

After Adjustment 

Pastiest Check: 

Notes: 

Barr Engineering Co. 

4700 W. 77th St 

Minneapolis, MN 55437 

(952) 832·2600 

Reference ("Hg) 

2'7. 2....( 

2..4. (.C:. -

Reference ("Hg) 

Project Name: \ [ S" s ""'--1·~ .., -/<-,._ \ 

Project Number: 2.. > G, 9 "7 Z 7 

/ (-'> 0 

~ C v s \L >D 

- vse .. e[c. of<!~ I 1 

Barometer ("Hg) Date Technician 

2-{. z... D 7 /{1 I <>::> /V1-Lr 

2 c;' { :;,~ 7/111.;;-- 7'+ / c 

Barometer ("Hg) Date Technician 
BARR 

Engineering Company 

PitotTubeNumber: ~ 7-1 

\ 

length: 

Function: M-5 Probe I Free 

1. Are face openings perpendicuiar" to tube axis? 

~ES (gotoZ) 0 NO (go to 1a) / 

""""'~ ' I 

·-~~~~----

' 

l---~----{ - ' . . 

2.. Are face openings paraDel to longitudinal axis? 

~ES(goto3) 0 NO(gotoZa) 

~ J ._.....,. t --_, 

3. Are legs of equal length? 

~ES(goto4) 0 NO (go to 3a) 

k----~~~~-~-----

4. Are center-1i~es of legs coincident? 

9J--:(ES ( go to 5) 0 NO (go to 4a) 

5. Does this pilot tube pass afi of the above criteria? 

Technician Signab.Jre: 

S-Type Pitot Tube 

Geometry Check 

Inspection Date: 

Technician: . ' N' ""-

1a. If NO, is an9Ie less fhan-10"1 

0 YES (gotoZ) 0 NO (discontinue use) 

,.., ' !L __t; . --£3Ei----· -~~--- . ' . I . I . I 

2a. If NO, is angle le_ss than So? _ 

0 YES (goto3) 

I· -17 

'" ~-~ 

0 NO (discontinue Use) 

~· -'D 

,, es: 

..._ 

3a. If NO, is difference less than 1/8 inch? 

0 YES (goto4) · 0 NO (discontinue use) 

4a. If NO, are center-lines of face openings less than 1/32 inch? 

0 YES (goto5) 0 NO (discontinue use) 

tzlYES ONO -~ 

·. 
BARR 

Engineering Company 

Pilot Tube Number: 

i 

Length: ] = 

Function: ~ Free 

1. Are face openings perpendicular to tube axis? 

0 NO (go to 1a) 

2. Are face openings parallel to longitudinal axis? 

)~?~s {go to 3) _ 0 NO (go to 2a) 

3. Are legs of equal length? 

---, 

~YES{goto4) 0 NO (go to 3a) 

f-- -~~~---={--)-----

4. Are center-lines of legs coincident? 

R._ YES (go to 5) 0 NO (go to 4a) 

~- --~~--=<--?-----

5. Does this pitot tube pass all o~ tlle af:love criteria? 

Tectinidan Signature: 

S-Type Pitot Tube 

Geometry Check 

Inspection Date: 

Technician: M""' ~~~----------

1a. If NO, is ang"le less than· 10°? 

0 YES (goto2) 0 NO (discontinue use) 

""' . rL .. _ __t; --£3E3----· 1 I 

-~~~-- I I . . . . 

2a. If NO, is angle I~ than 5"? _ 

0 YES (go to 3) . 0 NO (discontinue use) 

3a. If NO, is difference Jess than 1/8 inch? 

0 YES (goto4) · 0 NO (discontinue use) 

4a.. If_ NO, are center-lines of face openings less than 1/32 inch? 

0 YES (go to 5) 0 NO (discontinue use) 

0NO 
REFERENCE STANDARDS 

Hart Scientific 91 03-A s/n A 1 8289 

Hart Scientific 9140 sin A18086 

Temperature Calibraion Points 

Reference Deg F (To) 

Probe Temp (deg F) 

Reference Temp (deg R) deg F + 460 

Probe Temp (deg R), deg F + 460 

Difference (degrees) 

% DiffAbs. T 

Is difference less than 1 .5% at all 

measured points? 

1700 

1600 

1500 

~ 1400 

.:: 

~ 1300 

" 

~ 1200 w 

g; 1100 w 

:;; 1000 

K 8 900 

lil 800 

~ 700 

600 

500 

400 

THERMOCOUPLE CALIBRATION 

THERMOCOUPLE ID C-2-1 

Cal Date: 4/15/2005 Meter In or Out 

CALIBRATION TECHNICIAN: JMM 

TRACEABILITY 

Report No. A180718 

Report No. A1 82024 

32 

32 

32 

492 

492 

0 

0.0% 

YES 

212 

212 

210 

672 

670 

2 

0.3% 

DATE 

12/11/2003 

12/11/2003 

400 

400 

392 

860 

852 

8 

0.9% 

LABORATORY 

Hart Scientific 

Hart Scientific 

650 

650 

645 

1110 

1105 

5 

0.5% 

70 

70 

68 

530 

528 

2 

0.4% 

400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 

REFERENCE TEMPERATURE, deg.R 

Are extrapolated lim its less than 1.5%? YES 

If not acceptable, describe corrective action: 

FAHRENHEIT 

CALIBRATION RANGE 

-20 1200 
BARR 

Engineering Company 

~ ...... -r Thermocouple Number: -l.L-· -_,<?<:::__dd:==-

Media 

Std Used 

Reference Deg F (To) 

Reference Corr Temp (deg R) deg F + 460 

Probe Temp ( deq F) 

Probe Temp (del!_ R), deg_F + 460 

Difference (degrees) 

% Diff Abs. T (Renkin) 

Olff_ less than 1.5% at all points 

Graph Attached 

Extrapolated Range with Diff. <= 1.5% 

Description of the thermocouple's function: 

32 

~~ 

3;i.... 

If not acceptable, describe corrective procedures undertaken: 

212 

.;2t~ 

J.tO 

THERMOCOUPLE 

CALIBRATION 

400 

"ictJ 

-y,qd--

(Yes/No) 

(Yes/No) 

Date: L( ~ i S - 0 S: 

Technician: ,_,, )_.f'A-'-'":...r ____ _ 

650 Ambient 

&70 70 

{pL.( 'j &_'{ 

to 
BARR 

REFERENCE STANDARDS 

Hart Scientific 9103-A sin A1B289 

Hart Scientific 9140 s/n A1B086 

Temperature Calibraion Points 

Reference Deg F (To) 

Probe Temp (deg F) 

Reference Temp (deg R) deg F + 460 

Probe Temp (deg R), deg F + 460 

Difference (degrees) 

% DiffAbs. T 

Is difference less than 1.5% at all 

measured points? 

1700 

1600 

1500 

~ 1400 

; 

::! 1300 

" 

~ 1200 w 

!l; 1100 

~ i 1000 

8 900 

~ 800 rr 

w i: 700 

600 

500 

400 

THERMOCOUPLE CALIBRATION 

THERMOCOUPLE ID C-2-0 

Cal Date: 4/15/2005 Meter In or Out 

CALIBRATION TECHNICIAN: JMM 

TRACEABILITY 

Report No. A1B0718 

Report No. A1B2024 

32 212 

32 212 

32 211 

492 672 

492 671 

0 1 

0.0% 0.1% 

YES 

DATE 

12/11/2003 

12/11/2003 

400 

400 

394 

860 

854 

6 

0.7% 

LABORATORY 

Hart Scientific 

Hart Scientific 

650 70 

650 70 

645 69 

1110 530 

1105 529 

5 1 

0.5% 0.2% 

400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 

REFERENCE TEMPERATURE, deg.R 

Are extrapolated limits less than 1 .5%? YES 

If not acceptable, describe corrective action: 

FAHRENHEIT 

CALIBRATION RANGE 

-20 1200 
BARR 

Engineering Company 

Thermocouple Number: C - ~ CJ 

Media 

Std Used 

Reference Deg F (To) 

Reference CorrTem_IJ_(deg R) deg F + 460 

Probe Temp (deg F) 

Probe Temp (deg R), deg F +460 

Difference (degrees) 

% Oiff Abs. T (Renkin} 

Dift less than 1.5% at all points 

Graph Attached 

ExtrapOlated Range with Oiff. <= 1.5% 

Description of the thermocouple's function; 

32 

<,:1 

3~ 

If not acceptable, describe corrective procedures undertaken: 

212 

J £)._ 

J Ll 

THERMOCOUPLE 

. CAL! BRA TION 

400 

'-(tJO 

s <7 "1 

(Yes/No) 

(Yes/No) 

Date: '-j ~ I 5"- ~ 0 5' 

Technician: 0 f"V"'. 

650 Ambient 

&s-o {0 

& '-i.s c,c; 

to 
THERMOCOUPLE CAll BRA TION 

BARR 

THERMOCOUPLE ID C-5-0 

Cai;Date: 12/27/2004 Meter In or Out 

CALIBRATION TECHNICIAN: NRS 

REFERENCE STANDARDS TRACEABILITY DATE LABORATORY 

Hart Scientific 91 03-A s/n A 1 B289 Report No. A1B0718 12/11/2003 Hart Scientific 

Hart Scientific 9140 s/n A18086 Report No. A182024 12/11/2003 Hart Scientific 

Temperature Calibraion Points 20 70 150 

Reference Deg F (To) "20 70 150 

Probe Temp (deg F) 19 69 149 

Reference Temp (deg R) deg F + 460 480 530 610 

Probe Temp (deg R). deg F + 460 479 529 609 

Difference (degrees) 1 1 1 

% DiffAbs. T 0.2% 0.2% 0.2% 

Is difference less than 1.5% at all 

measured points? YES 

THERMOCOUPLE CALIBRATION 

1700 

1600 

~500 

~400 <( ffi' 300 

~200 

~14itlO 

w"' n:t®o 

6900 

0 

0 800 

2 

0:: 700 

llJ F: 600 

500 

400 

400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 

REFERENCE TEMPERATURE, deg.R 

Are extrapolated limits less than 1.5%? YES 

If not acceptable, describe corrective action: 

FAHRENHEIT 

CALIBRATION RANGE 

-20 1200 
BARR 

Engineering Company 

Thermocouple Number: T~ GS'"-o 

Media 

Std Used D-& 

Reference Deg F (To) 

Reference GorrTemp (deq R) deq F + 460 

Probe Temp {deq F) 

Probe Temfl (deg R), deg F +460 

Difference (degrees) 

% Diff Abs. T (Renkin) 

Oiff. less than 1.5% at all points 

Graph Attached 

Extrapolated Range with Oiff. <= 1.5% 

Description of _the thermocouple"'s.function: 

20 

z_o 

'-/ S'O 

19 

W-'7 

-1 

0 ·2-

70 

+o 

$30 

(9"\ 

S<.."'i 

-I 

0 .<._ 

THERMOCOUPLE 

CALl BRA TION 

Date~ \. ~-!..-7-Ct-{ 

T echnician: __,N=' ,2-,;S:._ __ _ 

150 

!s-D 

(,>\0 

l';i"f 

(,09 

-r 

0-"Z.. 

to 

C.M1-.-ol MoJ~\._ s ts~K oo:f-le.f tl...u...,c_o.,.'i'k 

If not acceptable, descnbe corrective procedures undertaken: 
THERMOCOUPLE CALIBRATION 

BARR 

THERMOCOUPLE ID C-5-1 

Cal; Date: 12/27/2004 Meter In or Out 

CALIBRATION TECHNICIAN: NRS 

REFERENCE STANDARDS TRACEABILITY DATE LABORATORY 

Hart Scientific 9103-A s/n A1B289 Report No. A180718 12/11/2003 Hart Scientific 

Hart Scientific 9140 s/n A18086 Report No. A1B2024 12/11/2003 Hart Scientific 

Temperature Calibraion Points 20 70 150 

Reference Deg F (To) 20 70 150 

Probe Temp (deg F) 20 69 148 

Reference Temp (deg R) deg F.,. 460 480 530 610 

Probe Temp (deg R), deg F.,. 460 480 529 608 

Difference (degrees) 0 1 2 

% DiffAbs. T 0.0% 0.2% 0.3% 

Is difference less than 1.5% at all 

measured points? YES 

THERMOCOUPLE CALIBRATION 

1700 

1600 

~500 

p400 

fE1300 

~200 

~1llt>O wO> 

([1®0 

6 900 

(.) 

0 800 

:::;; 

0:: 700 

w 

~ 600 

500 

400 

400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 

REFERENCE TEMPERATURE, deg.R 

Are extrapolated limits less than 1 .5%? YES 

If not acceptable, describe corrective action: 

FAHRENHEIT 

CALIBRATION RANGE 

-20 1200 
BARR 

Engineering Company 

Thermocouple Number: TC- c.:-s-- 1:..-

Media 

Std Used D-'it 

Reference Deg F (To) 

Reference Carr Temp ( deg R) deq F + 460 

Probe Temp {deg F) 

Probe Temp (deq R), deq F + 460 

Difference (deqree~) 

% Diff Abs. T (Renkin) 

Diff. less than 1.5% at all points 

Graph Attached 

Extrapolated Range with Diff. <= 1.5% 

Description of the thennocouple .. s. function: 

20 

2.0 

4~0 

20 

'-j >'O 

0 

0-0 

70 

+o 

S$0 

(.; c\ 

SZ.9 

- \ 

o:z. 

THERMOCOUPLE 

CALIBRATION 

150 

l <;:"0 

~{0 

1'-1:<6 

C.Cl? 

-"Z. 

0-3 

@I No) 

@No) 

Date' I'Qi (L-2't--C'{ 

Technician: "-'i'Li 

to 

C..~-1--r-.l 1-\cel~\.__ S"' b bM :c-~ 1 .. 1- +t-,.._..""-"<•-f' 1<-

If not acceptable, describe corrective procedures undertaken: 
BARR 

PYROMETER 

CALIBRATION 

Pyrometer Number: (" '"'' - :t 

Pyrometer Reference: C L 5rJiJ 1L-(Pte• tF Technician: 

Reference (°F) Reference rc) Pyrometer L__) 

1000 538 (003 

950 510 cr,;--1 

900 482 CfD'i 

850 454 ~s?> 

800 427 g-o_> 

750 399 75> 

700 371 7D'I 

650 343 (c.>~ 

600 316 t,;c vj 

550 288 553 

500 260 so :f.-

450 232 '--i~> I 

400 204 t.{oJ.... 

350 177 ss-J300 149 _5c'-l 

250 121 ;;! :,-'I 

200 93 :/63 

150 67 iS~ 

100 38 iO) 

50 10 !?)-, 

0 -18 3 

-50 -46 - '1 )-

Notes: 
BARR 

PYROMETER 

CALIBRATION 

Pyrometer Number: {_-5' 

Pyrometer Reference: {1_ -J uC/ -locc+ 

Reference CFJ Reference (

0

C} 

1000 538 

950 510 

900 482 

850 454 

800 427 

750 399 

700 371 

650 343 

600 316 

550 288 

500 260 

450 232 

400 204 

350 177 

-:-

300 149 

250 121 

200 93 

150 67 

100 38 - 50 10 

0 -18 

-50 -46 

· Notes: 

Date: 1 }_-). 9 -o<f 

Technician: ~S;._ 

Pyrometer C_l 

f001 

'15o 

cz 60 

"?)So 

gvo 

/)1 

po 

(;;50 

s '7 i 

')in 

LJ 1/ 

41/c 

sn 

]er_; 

2_ 'l 'i 

z<t"' 

11Y 

i'i~ 

']6 

41 

-1 

-5')_ 
BARR 

REFERENCE STANDARDS 

Hart Scientific 9103-A s/n A1B289 

Hart Scientific 9140 sin A 18086 

Temperature Calibraion Points 

Reference Deg F (To) 

Probe Temp ( deg F) 

Reference Temp (deg R) deg F + 460 

Probe Temp (deg R), deg F + 460 

Difference (degrees) 

% Diff Abs. T 

Is difference less than 1.5% at all 

measured points? 

1700 

1600 

1500 

'; 1400 ., • 

~ 1300 

" 

~ 1200 

~ 1100 w 

:;; 1000 .... 

.. 

" 900 § 

~ 800 w 

j: 700 

600 

500 

400 

THERMOCOUPLE CALIBRATION 

THERMOCOUPLE ID TC 7-1 

Cal;Date: 1/3/2005 

CALIBRATION TECHNICIAN: 

M-5 Probe 

JMM 

TRACEABILITY 

Report No. A1B0718 

Report No. A1B2024 

32 212 

32 212 

32 209 

492 672 

492 669 

0 3 

0.0% 0.4% 

YES 

DATE LABORATORY 

12/11/2003 Hart Scientific 

12/11/2003 Hart Scientific 

400 650 Ambient 

400 650 70 

395 642 70 

860 1110 530 

855 1102 530 

5 8 0 

0.6% 0.7% 0.0% 

400 500 600 700 800 900 1 000 11 00 1200 1300 1400 1500 1600 1700 

REFERENCE TEMPERATURE, deg.R 

Are extrapolated limits less than 1.5%? YES 

If not acceptable, describe corrective action: 

FAHRENHEIT 

CALIBRATION RANGE 

950 -20 490 
BARR 

Engineering Company 

,-c_ 

Thermocouple Number:_,·'--' _·--'------

Media 

Std Used 

Reference Deg F (To) 

Reference Carr Temp (deq Rl deo F + 460 

Probe Temp (deg l'l 

Probe Temp (deg R), deg F + 460 

Difference (degrees) 

%Dill Abs. T (Renkin) 

Dlff. less than 1.5% at all points 

Graph Attached 

Extrapolated Range with Dill. <= 1.5% 

Description of the thermocouple's function: 

. j'A,l{,,j .5: 1/v~~ 

32 

3J4'1 "2. 

s}-

49<-

0 

o.o 

If not acceptable, describe corrective procedures undertaken: 

70 

76 

<;;"30 

/0 

5"30 

C) 

o.o 

THERMOCOUPLE 

CALIBRATION 

212 

;:n:l. , 

(o 7Z. 

;;>a"' 

"' lo"t 

-;, 

O·Lj 

(~No) 

(~/No) 

Date: I-$ -asTechnician: 1 1 ~ 

400 650 

L-/b() (o.>() 

'i;C.O 1110 

5 "l'f G"i :L 

2s-s- I I 07_ 

-r -'51 

"'·"' o.j 

to 
REFERENCE STANDARDS 

Hart Scientific 9103-A s/n A1B289 

Hart Scientific 9140 s/n A1 8086 

Temperature Calibraion Points 

Reference Deg F (To) 

Probe Temp (deg F) 

Reference Temp (deg R) deg F + 460 

Probe Temp (deg R), deg F + 460 

Difference (degrees) 

% DiffAbs. T 

Is difference less than 1.5% at all 

measured points? 

1700 

1600 

1500 

~ 1400 ~ • 

ili 1300 

s " 1200 

~ 1100 w 

:;; 1000 

o! 

" 900 

: 

~ 800 w i= 700 

600 

500 

400 

THERMOCOUPLE CALIBRATION 

THERMOCOUPLE ID TC7-4 

Cai;Date: 1/3/2005 

CALIBRATION TECHNICIAN: 

M-5 Probe 

JMM 

TRACEABILITY 

Report No. A1 B0718 

Report No. A1B2024 

32 

32 

32 

492 

492 

0 

0.0% 

YES 

212 

212 

211 

672 

671 

1 

0.1% 

DATE 

12/11/2003 

12/11/2003 

400 

400 

399 

860 

859 

1 

0.1% 

LABORATORY 

Hart Scientific 

Hart Scientific 

650 

650 

650 

1110 

1110 

0 

0.0% 

Ambient 

70 

70 

530 

530 

0 

0.0% 

400 500 600 700 800 900 1000 11 00 1200 1300 1400 1500 1600 1700 

REFERENCE TEMPERATURE, deg.R 

Are extrapolated limits less than 1.5%? YES 

If not acceptable, describe corrective action: 

FAHRENHEIT 

CALIBRATION RANGE 

-20 1200 
BARR 

Engineering Company 

~--- '-'( Thermocouple Number:---,</'--·---'----

Media 

Std Used D-'6 

Reference Deo F (To)_ 

Reference Carr Temp (deg R) deg F + 460 

Probe Temp (deg F) 

Probe Temp (deQ R), deo F + 460 

Difference {decrees) 

% Diff Abs. T (Renkin) 

Diff. less than 1.5% at all points 

Graph Attached 

Extrapolated Range with Diff. <::;;: 1.5% 

32 

$.).__ 

492. 

.? 1 

'-1'1-z0 

0-0 

If not acceptable, describe corrective procedures undertaken: 

70 

7d 

5"30 

70 

5"30 

'0 

o.o 

THERMOCOUPLE 

CALIBRATION 

Date: /- 3 - C! '{" 

Technician: j~ 

212 400 650 

:JD- _Lj_!}/) ~so 

c, I '2._ Sc.o lifO 

,y I ) ] 1"'7 G)O 

&>/.( l?s; { 1{0 

-I -r 0 

6-f 0.( O.D 

to 
N 

§ 

f 

0 "' 

2 

a: • 

~ 

• 

~ • 

_;; ~ 

~ r 

1- -" 

-" !<' 

E 

m " "' 

§!I 

a: • t 

• . £ ;,; 

:t ~ 0 f5 "- c 

~ 

~ ~ .1: ~ c 

"' 0 :I 0:: 

= 

• c 0 0 z a: 0 

B: 

il 

1- ~ 

z 

rJ 

0 

~ " 

~ 

=> 

z " 

1" "' {; . 

" _..; ~~ 

0 

~ 

. "" .. • 

• 0 

" > 

w " 

• 1-

J . 

~ N 

§ § • <r a: g 

w -" rr E m ;u * 

i'- .£ u.. .E = = 0 ~ 

0 

I! I 0 -

0~ 0 .8 . - ~ o9- .'!! • ' c • ~ "- w 0 0 

> 
lect 

pi Lac 

• 

srator 

s.k,d 

Lt vG 

7·1L·o5 

lAc k.L 

>ample I Sample ll Meter 

Point 

Test No, 

CM 

)._ Runs 1. 2 

s d 

TEST RUN 1 

Train 

EPA METHOD 13B· FLUORIDES 

FIELD DATA SHEET 

Metery • "]'i 1( Bar. Pres Z S. 3 In Hg 

AH@ I. •1<1 J. Stat. Pres -6. J:JJ In H20 

cpC>.?5'l Probe Lngth 2 ft 

p Liner Type; OS.S. OOther 

!L 

Sa

Run1 

Pretest () 

Posttest 

Pilot (3 ln.) Pos. 

Nu-z 

z Je C21 I; b,<-t.f;o"' 

......

7 



Sill I 

BARROl 

SCOTT-MARRIN, INC. 

6531 BOX SPRINGS BLVD. • RIVERSIDE, CA 92507 

TELEPHONE (909) 653-6780 • FAX (909) 653-2430 

REPORT OF ANALYSIS 

EPA PROTOCOL GAS MIXTURES 

TO: Sam Foss DATE: July 13 2004 

Barr Engineering Co 

7390 OHMS Lane 

Edina MN 55439-2330 

CUSTOMER ORDER NUMBER: Vbl/S FOSS 

COMPONENT CONCENTRATION(v/v) REFERENCE 

±EPA UNCERTAINTY STANDARD 

CYLINDER NO: CC121446 

Sulfur Dioxide 93.1 ± 0.9 ppm GMIS 

CYLINDER#: 

Nitrogen Balance CC12025 

CYLINDER PRESSURE: 1150 psig @ 111.8 ppm 

ppm = pmole/mole % = mole-% 

ANALVZER EXPIRATION REPLICATE 

MAKE, MODEL. SIN, DETECTION DATE ANALYSIS DATA 

BOVAR MODEL 922M 07/12/04 

S/N VD922B4844 07/12/06 93.1 ppm 

CONTINUOUS 93.1 ppm 

UV PHOTOMETRY 93.3 ppm 

LAST CAL DATE: 06/14/04 MEAN: 93.2 ppm 

The above analyses were performed in accordance with Procedure G1 of the EPA Trac ility Protocol, Report Number 

EPA-600/R97/121, dated September 1997. 

This cyiinder should not be used if the pressure is less than 150 psig. 

ANALYST:}~ M.J.MONSON 

The only liability of this company for gas which falls to comply with this analysis shall be replacement r reanalysis thereof by the company without extra cost. 

STANDARD CALIBRATION GASES IN ALUMINUM CYLINDERS 
I SCOTT -MARRIN, INC. 

CHRONOLOGICAL RECORD OF CERTIFIED CONCENTRATIONS 

CUSTOMER: Barr Engineering co 

PURCHASE ORDER: Vbl/S Foss 

CYLINDER NUMBER: CC121446 

COMPONENT 502 

DATE 

07/10/02 

07/17/02 

07/12/04 

AVERAGE 

NOTES: 

93.0 ppm 

93.0 ppm 

93.2 ppm 

93.1 ppm 

S,._UTECH\CHRONOl.OOC 6!9fi 

CUSTOMER CODE: BARROl 

DATE: 07 I 13/04 
51111 

BJ\RROl 

SCOTT-MARRIN, INC. 

653 1 BOX SPRINGS BLVD. • RIVERSIDE, CA 92507 

TELEPHONE(9St) 653-6780 • FAX (951) 653-2430 

REPORT OF ANALYSIS 

EPA PROTOCOL GAS MIXTURES 

·o: Jason McCann DATE: June 28 2005 

Barr Engineering Co 

4700 W 77th St 

Minneapolis, MN 55435-4803 

USTOMER ORDER NUMBER: 20050516A 

--------~---~--------------------------------------------------- ----------------------~----------------------------------------- COMPONENT CONCENTRATION(v/V) REFERENCE ANALVZER EXPIRATION REPLICATE 

±EPA UNCERTAINTY STANDARD MAKE, MODEL, &JN, DETECTION DATE ANALYSIS DATA 

CYLINDER NO: CC63443 

BOVAR MODEL 922M 06/15/05 06/23/05 

.lfur Dioxide 51.0 ± 0.6 ppm GMIS S/N VD922U844 06/23/07 51.0 ppm 50.9 ppm 

CYLINDER#: CONTINUOUS 50.9 ppm 50.9 ppm 

fitrogen Balance CC12172 UV PHOTOMETRY 51.0 ppm 51.0 ppm 

;YLINDER PRESSURE: 2000 psig @53.9ppm LAST CAL DATE: 06/07/05 MEAN: 51.0 ppm 50.9 ppm 

m • !lftlOle/mole \ = mole-\ 

The above analyses were performed in accordance with Procedure G1 of the EPA Tra eability Protocol, Report Number 0 "A·600/R97/121, dated September 1997. 

lis cylinder should not be used if the pressure is less than 150 psig. 

I>.NALYST: ~ ~ ?P- APPROVED: -.flA~r.lL:::~----------

The only liability of this company lor gas which fails to comply with this analysis shall be replacement or reanalysis thereof by the company without extra cost. 

STANDARD CAURRATION AAR.F~ IN AlliUINII~lr:VIINn5=R.C:.. 
Sill I 

BARROl 

SCOTT-MARRIN, INC. 

6531 BOX SPRINGS BLVD. • RIVERSIDE, CA 92507 

TELEPHONE (909) 653-6780 o FAX (909) 653-2430 

REPORT OF ANALYSIS 

EPA PROTOCOL GAS MIXTURES 

TO: John Stock DATE: June 26 2003 

Barr Engineering Co 

7390 OHMS Lane 

Edina MN 55439-2330 

CUSTOMER ORDER NUMBER: 20030619A 

~~~-----------------~--------------------------------------------~~ ----------------------------------------------------------------~·· 

COMPONENT CONCENTRATION(v/v) REFERENCE ANALVZER EXPIRATION REPLICATE 

±EPA UNCERTAINTY STANDARD MAKE, MODEL, S/N, DETECTION DATE ANALYSIS DATA 

CYLINDER NO: CC12600 

CARLE INST MODEL 8000 01/18/01 06/25/03 

Carbon Monoxide 60.4 ± 0.6 ppm GMIS SIN 8249 06/25/06 60.5 ppm 60.2 ppm 

CYLINDER#: METHANATION/FID 60.5 ppm 60.2 ppm 

Nitrogen Balance CC85729 GAS CHROJ.iATOGRAPHY 60.7 ppm 60.1 ppm 

CYLINDER PRESSURE: 2000 psig @ 55.4 ppm LAST CAL DATE: 06/24/03 MEAN: 60.6 ppm 60.2 ppm 

ppm = 1-UJlOle/mole \ "" mole-% 

The above analyses were performed in accordance with Procedure G1 of the EPA Traceabil(ly Protocol, Report Number 

EPA-600/RS?/121, dated September 1997. / 

This cylinder should not be used if the pressure is less than 150 psig. I 

ANALYST: __ ~~----~~~~~==~~, _________ APPROVED: ____ ~~~----------------------- M.J.MONSON 

The only llabHity of this company for gas which fails to comply With this analysis shall be replacement or reana ysis thereof by the company without extra cost. 

STANDARD CALIBRATION GASES IN ALUMINUM CYLINDERS 
Ellll 

BARROl 

SCOTT-MARRIN, INC. 

6531 BOX SPRINGS BLVD. • RIVERSIDE, CA 92507 

TELEPHONE (951) 653-6780 • FAX (951) 653-2430 

REPORT OF ANALYSIS 

EPA PROTOCOL GAS MIXTURES 

TO: Nicholas Shreve 

Barr Engineering Co 

7390 OHMS Lane 

DATE: December 22 2004 

Edina MN 55439-2330 

CUSTOMER ORDER NUMBER: 20041123ANRS 

COMPONENT CONCENTRATION(v/v) REFERENCE ANALYZER EXPIRATION REPLICATE 

"'EPA UNCERTAINTY STANDARD MAKE, MODEL, S/N, DETECTION DATE ANALYSIS DATA 

CYLINDER NO: CC78171 

CARLE IHST MODEL 8000 12/14/04 12/21/04 

Carbon Monoxide 34. 1 :t 0.3 ppm GMIS S/N 8249 12/21/07 34.0 ppm 34.2 ppm 

CYLIIIDER #: METHANATION/FID 34.0 ppm 34.1 ppm 

Nitrogen Balance CA03684 GAS CHROMATOGRAPHY 34.1 ppm 34.1 ppm 

CYLIIIDER PRESSURE: 2000 ps ig @54.5 ppm LAST CAL DATE: 12/13/04 MEAII: 34.0 ppm 34.1 ppm 

ppm = IJiti.Ole/mole % = mole-\ 

The above analyses were performed in accordance with Procedure G1 of the EPA Trace bility Protocol, Report Number 

EPA-600/R97/121, dated September 1997. 

This cylinder should not be used if the pressure is less than 150 psig. 

ANALYST:--~~-'-~"'-":...:...;""--'....:..:'--.=::.....;·:;_··--- APPROVED: 

M.J.MONSON 

The only liability of this company tor gas which fails 10 comply with this analysis shall be replacement or eana\ysls thereof by the company without extra cost. 

STANDARD CALIBRATION GASES IN ALUMIIIUM CYLINDERS 
NATIONAL SPECIALTY GASES 

630 UNITED DRIVE 

DURHAM, NC 27713 

CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS MIXTURE 

Customer: Twin City Oxygen Reference# 88-89053 

NSGPO# 4271165 Certification Date: 02/19/04 

Customer PO# 42921 Expiration Date: 02/19/07 

Cylinder# cC47n7 . Pressure, psig* 2000 

ANALYTICAL INFORMATION 

METHOD: This standard was analyzed according to EPA Traceability Protocol for A={ and Certification of Ga:se<l\lS Callbration standards: 

Procedure G1 (September 1997) 

ANAL Y2ED CYLINDER 

Components 

Methane 

Balance - Air 

REFERENCE STANDARD 

Type/SRM Sample# 

GMIS (Traceable to SRM # 2751 ) 

INSTRUMENTATION 

Instrument/Model/Serial# 

Rosemount 400A THC 00335 

Certified Concentratjon 

90.4 ppm 

Cylinder# 

CC36118 

Last Date Calibrated 

01/23/04 

AnaMical Accuracy** 

+/-1% 

Concentration 

100.3 ppm CH4/AIR 

Analytical Method 

Flame Ionization Detector 

Analyst: -------,-----J::.;e:::.r.::;em=y.:..K:;:e:::.nw:.:.o:::rt:::.h,..y_ 

This report states accurately the results of the investigation made upon the material submitted to the analytical 

laboratory. Every effort has been made to determine objectively the information requested. However, in 

connection with this report, National Specialty Gases shall have no liability in excess of established charge for 

this service. Assayed at National Specialty Gases, 630 United Drive, Durham, NC 2n13 (919) 544-3772 

•oo not use this standard When cylinder pressure is below 150 pslg. 

-Analytical accuracy includes typical known error sources which. at least, include precision of the analytical instUmenl NSG020149L 
NATIONAL SPECIALTY GASES 

630 UNITED DRIVE 

DURHAM, NC 27713 

CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS MIXTURE 

Customer: 

NSG PO# 

Customer PO# 

Twin City Oxygen 

3558412 

39278 

Cylinder# CC2937 

ANALYTICAL INFORMATION 

Reference# 88-78516 

Certification Date: 08/01/02 

Expiration Date: 08/01/05 

-Pressure, psig* 2000 

METHOD: This standard was analyzed according to EPA Traceability Prctocol for Assay and certification of Gaseous Calibration 

Standards: Procedure G-1: September 1997. 

ANALVZED CYLINDER 

Components 

Methane 

Balance - Air 

REFERENCE STANDARD 

Type/SRM Sample# 

GMIS (Traceable to SRM # 2751 ) 

INSTRUMENTATION 

Instrument/Model/Serial # 

Rosemount 400A THC 00335 

Certified Concentration 

46.5 PPM 

Cylinder# 

CC36118 

Last Date Calibrated 

07/16/02 

Analytical Accuracy** 

+/-1% 

Concentration 

100.3 ppm CH4/AIR 

Analytical Method 

Flame Ionization Detector 

Analyst: ------------'-Am=y'-J"-''-'P-'r"'ok'-"oOJ:p'-"o"'w"'ic:::z:_ 

This report states accurately the results of the investigation made upon the material submitted to the analytical 

laboratory. Every effort has been made to determine objectively the information requested. However, in 

connection with this report, National Specialty Gases shall have no liability in excess of established charge for 

this service. Assayed at National Specialty Gases, 630 United Drive, Durham, NC 27713 (919) 544-3772 

*oo not use this standard when cylinder pressure is below 150 psig. 

**Analytical accuracy includes typical known error sources which, at least, include precision of the analytical instrument NSG 020149L 
CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS MIXTURE 

Customer: Twin City Oxygen Reference# 88-91148 

NSGPO# 4424096 Certification Date: 06/15/04 

Customer PO# 43778 Expiration Date: 06/15/07 

Cylinder# SG9165492BAL Pressure, psig* 2000 

ANALYTICAL INFORMATION 

METHOD: This standard was analyzed according to EPA Traceabirrty Protocol for Assay and Certification of Gaseous calibration Standards: 

Procedure G1 (September 1997) 

ANALYZED CYLINDER 

Components 

Methane 

Balance - Air 

REFERENCE STANDARD 

Type/SRM Sample# 

GMIS ( Traceable to SRM # 2750 ) 

INSTRUMENTATION 

I nstrument/Modei/Serial # 

Rosemount 400A THC 00335 

Certified Concentration 

30.2 ppm 

Cylinder# 

CC16937 

Last Date Calibrated 

06/08/04 

Analytical Accuracy•• 

+/-1% 

Concentration 

51.57 ppm CH4/AIR 

Analytical Method 

Flame Ionization Detector 

Analyst: -----------'-'R"'ic:..::ha::.rd:::...::S£yk.::e::::s_ 

This report states accurately the results of the investigation made upon the material submitted to the analytical 

laboratory. Every effort has been made to determine objectively the information requested. However, in 

connection with this report, National Specialty Gases shall have no liability in excess of established charge for 

this service. Assayed at National Specialty Gases, 630 United Drive, Durham, NC 27713 (919) 544-3772 

"'Do not use this standard when cylinder pressure is below 150 psig. 

**Analytical accuracy Includes typical known error sources which, at least, include precision of the analytical instrument. NSG 020149L 
.. 1111 

BARROl 

SCOTT-MARRIN, INC . 6531 BOX SPRINGS BLVD. • RIVERSIDE. CA 92507 

TELEPHONE (909) 653·6780 • FAX (909) 653-2430 

REPORT OF ANALYSIS 

EPA PROTOCOL GAS MIXTURES 

TO: Sam Foss DATE: August 13 2004 

Barr Engineering Co 

7390 OHMS Lane 

Edina MN 55439-2330 

CUSTOMER ORDER NUMBER: VBL/S Foss 

-..-.~.~- ~~_,...,.,_,..,...,.,v.- .... _.,_. __ , ... ...... -... ,~------"""---,._,. ............ _..,.......__.....,_..,._ ------~--·-- ____ _, _______ .. -~------~·--·---·- _.. _ _,_. ..... ...,._.......,....,...,._...,..._.....,.-------------·--·---·-·--'··-- ...... ·---·-----------.-.~-'""•'~' ~---- ...... ~---···-·· ..... -·-. .,., ....... --.... -~ 

COMPONENT CONCENTRATION(v/V) REFERENCE ANALVZER EXPIRATION REPLICATE 

"EPA UNCERTAINTY STANDARD MAKE, MODEL, S/N, DETECTION DATE ANALYSIS DATA 

CYLINDER NO: CC12009 

VARIAN MODEL 1860 TCD 08/10/04 

Carbon Dioxide 5.01 :t. 0.05% GMIS S/N NONE OB/10/07 5.00% 

CYLINDER#: THERMAL CONDUCTIVITY 5.01%-

CC42814 GAS CHROMATOGRAPHY 5.03% 

@B.OB LAST CAL DATE: 07/2B/04 MEAN: 5.01% 

VARIAN MODEL 1860 TCD 08/12/04 

Oxygen 19.97 " 0.20% GMIS 5/N NONE 08/12/01 19.98% 

CYLINDER#: THERMAL CONDUCTIVITY 19.97% 

Nitrogen Balance CA03201 GAS CHROMATOGRAPH~ 19.96% 

CYLINDER PRESSURE: 2000 psig @ 24.B2% LAST CAL DATE: 07/23/04 MEAN: 19.97% 

ppm = ~ole/mole % =mole-% 

The above analyses were performed in accordance wtth Procedure G1 of the EPA Trac ability Protocol, Report Number 

EPA·600/R97/121, dated Sep ember 1997. 

This cylinder sh uld o e d if the pressure is less than 150 psig. 

The only liability of this company for gas which fails to comply with lhis analysis shall be replacement or reanalysis thereof by the company without extra cost. 

STANDARD CALIBRATION GASES IN ALUMINUM CYLINDERS 
51111 

BARROl 

SCOTT-MARRIN, INC. 

6531 BOX SPRINGS BLVD. • RIVERSIDE, CA 92507 

TELEPHONE (909l 653-67BO o FAX (909) 653-2430 

REPORT OF ANALYSIS 

EPA PROTOCOL GAS MIXTURES 

TO: Sam Foss DATE: April 16 2004 

Barr Engineering Co 

7390 OHMS Lane 

Edina MN 55439-2330 

CUSTOMER ORDER NUMBER: 200402l0ASMF2 

COMPONENT CONCENTRATION(v/V) REFERENCE 

+EPA UNCERTAINTY STANDARD 

CYLINDER NO: CC12898 

Carbon Dioxide 9.05 ± 0. 03% GMIS 

CYLINDER#: 

CC51172 

@ 17.98% 

Oxygen 9.07 ± 0.05% GMIS 

CYLINDER#: 

Nitrogen Balance CC81204 

CYLINDER PRESSURE: 2000 psig @ 9. 88% 

ppm = JUYIOle/mole % = mole-% 

ANALVZER EXPIRATION REPLICATE 

MAKE, MODEL., SlN, DETECTION DATE ANALYSIS DATA 

VARIAN MODEL 1860 TCD 04/12/04 

SIN NONE 04/12/07 9.06% 

THERMAL CONDUCTIVITY 9.05% 

GAS CHROMATOGRAPHY 9.05% 

LAST CAL DATE: 03/29/04 MEAN: 9.05% 

VARIAN MODEL 1860 TCD 04/15/04 

S/N NONE 04/15/07 9.08% 

THERMAL CONDUCTIVITY 9.08% 

GAS CHROMATOGRAPHY 9.05% 

LAST CAL DATE: 03/25/04 MEAN: 9.07% 

The above analyses were performed in accordance with Procedure G1 of the EPA Traceability Protocol, Report Number 

EPA-600/R97/121, dated Se mber 1997. 

This cylinder shou d if the pressure is less than 150 psig. 

The only liability of1his company for gas wh·rch fails to comply with this analysis shall be replacement or reanalysis thereof by the company without extra cost. 

STANDARD CALIBRATION GASES IN ALUMINUM CYLINDERS 


, .. -:: 

VISIBLE EMISSIONS 

EVALUATOR 

This is to certify' that 

met)he specifications of Federal Reference Method 9 

ond.qualified OS 0 visible emissions evoluqtor. 

Maxienum deviation on white and block smoke did not 

exceed7;5% opacity and no single error exceeding 

15%ppocity was incurred during the certification test 

conducted by Eastern Technical Associates of Raleigh, 

North Carolina. This certificate is valid for six months 

rrdm'date of issue. -... ' . 

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OPI:<.._'-'Ci.._ING ...,..ceo..-..-.. FQ.._,..._ .._,._.JCE&"' .;;,vJRCL"' 

Juoe-99 

Test Date(s): 711212005 Process Equipment Numba/ Identification: Line 4 Waste Gas stack (SV118) 

Company Name: U.S. Minnesota Ore Operations- (Minntac) 

Equipment & Operating Data 

1. Process Equipment Description: Ste 11 A lomerator- Line 4 Waste Gas Stack PM/Fiuorides/S02, CO, VOC 

2. Were the process and control equipment operated consistent with normal operating procedure? YES NO 

3. Include copy of production records or instruments which indicates rate of production or operation of the equipment, i.e. units per 

hour, pounds per hour, pressure, air flow, etc. 

4. Date(s) and procedure(s) of last maintenance/cleaning within 6 months Remains unchanged from Test Plan 

Line 4 down for annal major repair from May 31 through June 21- see attached R.Potts e-mail 

5. Process rate (amount of raw material or finished product per hour, wet or dry basis) while com busting (list fuel type(s) and 

ratios as app<::r:.o.t:p:.:ria:ot:.:e'-) ---------------------------------

Process Parameter: list type and units Run 1 Run2 Run3 

Green ball feed rate, long tons per hour (L TPH) 588 584 595 

Fired Qroduction rate, (L TPH) 465 463 472 

Heat Input (1 06 British thermal units/hour) Wood 90.61 85.83 94.91 Heat Input (106 British thermal units/hour) Gas 123.88 98.29 111.38 

Heat Input (106 British thermal units/hour) Total 151.29 126.38 142.19 

6. Summarize control equipment operating data documented during testing. Values reported should reflect maximum, minimum, 

averages, or as approved in the test plan. (See test plan and aPProval letter) 

Examples of APC equipment and parameters generally monitored Monitor as specified in the test plan approval letter. 

• Scrubb& (list type of scrubb&}: AP (in. w.c.) and feed rate • Baghouse, Cyclone, and Multi-clone: AP (in. w.c.) 

(!WTil and vsig_) 

• and Thermal • Nmnber and identity of operating electrostatic precipitator field(s) 

Incinaator: eF t=po,ru.J 

APC equipment and parameter monitore Run 1 Run2 Run3 

Wet Scrubber, dP (in. w.c.)-average 11.09 11.20 11.21 

Wet Scrubber, feed rate (gpm)- average 2985 2991 2985 

List pollutant & averaging basi!i-Sbould reflect permit Run 1 Run2 Run3 

Continuous Opacity Monitor (list hourly average) NA 

NA Monitor (list averaging basis): NA 

NA Monitor (list averaging basis): NA 

AbbreviatioDs: APC-air pollution control 

lbs.-pounds 

gpm.-gallons pa minute 

psig-pressure per square inch gauge 

in. w.c.-inches of water column 

M- pressure drop 

NOTE: This form provides only a:;ummary of the operating CJJnditions during the performance tesL Additional and more detailed records are 

required to meet the requirements of Minn. R. 7017.2035. This form is to be submitted tiS part oftfJe performance test report to: North, Metro, 

or South District, Performance Test Coordinator, MN Pollution Control Agency, 520 Lafayette Rd., St. Paul, MN 

PMR

594 58

471 46

93.96 95.

102.09 95.

128.92 146

F-Run4 PMR

11.23 11.

2985 298

Run3 Run
Run Date 

DATA COLLECTED DURING STACK TESTING 

Line 4 July 12, 2005 

Acid Pellet Production 

Feed Rates L TPH Prod. Fuel Data 

Pollutant Start End Green 1· Rate Wood I Gas MBTUH I Total 

Tested for Time Time ball To Grate LTPH MBTUH I Grate I Kiln I MBTUH 

Waste Gas Stack Line 4 

1 7/12/2005 PM- Qases 10:00 11:09 588.39 522.22 464.78 90.61 0.00 123.88 214.49 

2 7/12/2005 PM- gases 11:55 13:06 584.25 520.22 463.00 85.83 0.00 98.29 184.12 

3 7/12/2005 PM- gases 16:00 17:16 595.29 530.52 472.16 94.91 0.00 111.38 206.29 

4 7/12/2005 PM 19:25 20:21 587.65 520.40 463.16 93.36 0.00 102.09 195.45 

4 7/12/2005 Fluoride 

---

17:55 19:05 594.35 528.66 470.51 95.22 0.00 95.76 190.98 

AVG 589.99 524.40 466.64 90.45 0.00 106.28 201.64 

Based on 1 0-minute averages that approximately align with the test times. 

Note: Gas meter was in error- read 17.67% low. Corrected values are shown 
Run Date 

Data Collected During Stack Testing 

Line 4 July 12, 2005 

Acid Pellet Production 

Wood Moisture, sulfur and BTU Analyses 

As Received Dry basis 

Start End % % BTU % BTU 

Time Time H20 s per lb s per lb 

Waste Gas Stack Line 4 

1 7/12/2005 10:00 11:09 11.8 0.021 7576.48 0.024 8470.50 

2 7/12/2005 11:55 13:06 9.2 0.050 7140.29 0.055 7797.20 

3 7/12/2005 16:00 17:16 4.6 0.022 7767.11 0.023 8124.40 

4 7/12/2005 19:25 20:21 6 0.031 7615.38 0.033 8072.30 

4 7/12/2005 17:55 19:05 4.6 0.022 7767.11 0.023 8124.40 

AVG 7.24 0.029 7573.27 0.034 8130.70 
Tom Kuchinski 

From: 

Sent: 

To: 

Cc: 

Subject: 

Raymond Potts [RPotts@uss.com] 

Thursday, August 04, 2005 1 :07 PM 

Tom Kuchinski 

Chrissy L Bartovich; Richard Berg 

Re: Line 4 maintenance and repairs 

Line 4 was down for its "scheduled" annual major repair from May 31 through June 21. The 

entire line including the wet scrubber and cooler areas received attention (repairs) 

during this shutdown. 

Ray 

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Tom Kuchinski 

From: 

Sent: 

To: 

Subject: 

Chrissy L Bartovich [clbartovich@uss.com] 

Wednesday, June 29, 2005 10:53 AM 

Richard Berg 

RE: Line 4 Initial Performance Test 

Forwarded by Chrissy L Bartovich/Minntac/USS on 06/29/2005 10:54 AM 

<Clbartovich®uss.corn> 

"Place, Andrew" 

<Andrew.Place®sta 

te.mn.us> 

<Robert.Beresford®state.mn.us> 

To: Chrissy L Bartovich 

cc: 11 Beresford, Robert" 

Subject: RE: Line 4 Initial Performance 

Test 

05/20/2005 02:49 

PM 

Chrissy, that sounds fine. Keep me posted. I would agree that unless there is some major 

modification to the test plan, or, the testing gets postponed for an indefinite amount of 

time, we can communicate via email and avoid redoing the complete testing process. 

Talk to you later and have a good weekend. 

-----Original Message-----

From: Chrissy L Bartovich [mailto:clbartovich®uss.com] 

Sent: Thursday, May 19, 2005 1:34 PM 

To: Place, Andrew 

Cc: Robert.Beresford®state.mn.us; Raymond Potts 

Subject: Line 4 Initial Performance Test 

Hi Andy, 

It looks like we won't be doing the initial performance testing on Line 

4 this week. We are having difficulty operating the line. This line will be going down 

at the end of the month for a 16 day major repair, 

It looks like it would be late June or early July when we would be able to conduct the 

initial performance test. We need to do this test by July 31 as a part of our pending PSD 

permit. 

I'm assuming we can work this the same as the SV054 - an email notification when we are 

able to test rather than going through the entire process again. If you have any 

questions please let me know. 

Thanks, 

Chrissy 

1 
Message Page 1 of 1 

Tom Kuchinski 

From: Tom Kuchinski 

Sent: Thursday, May 12, 2005 9:08AM 

To: Richard Berg 

Subject: FW: Test Plan Approval for 5/16/05 test and 5/31/05 GEMS cert. 

Attachments: CERTIFICATION PAGE.doc; MICROFICHE CD SUBMITTALS.doc; OPERATING DATA 

SUMMARY FOR COMBUSTION SOURCES.doc; OPERATING DATA SUMMARY FOR 

PROCESS SOURCES.doc; USS-Minn, SV1 03, SV118, SV127, 5-05.doc; USS-Minn, 

SV144&151, GEMS RATA, 5-05.doc 

From: Place, Andrew [mailto:Andrew.Piace@state.mn.us] 

Sent: Thursday, May 12, 2005 9:02AM 

To: Chrissy L Bartovich 

Cc: Tom Kuchinski; Beresford, Robert 

Subject: Test Plan Approval for 5/16/05 test and 5/31/05 CEMS cert. 

Chrissy, 

The test plan approval forms associated with the upcoming performance test on Agglomerator Lines 3, 4, and 5 

(SV103, SV118, & SV127) on May 16th, and initial GEMS RATA on Agglomerator Lines 6 and 7 (SV144 and 

SV151) on May 31st, are attached to this message. They include the Test Plan Approvals, Operating Data 

Summarys, Certifications, and Microfiche/CO Submittals. Please use the forms attached as they have recently 

been updated. Also, please print a copy of this email message and include it in the report for each 

test with the approval letter . The email provides authentication for the test plan approvals. 

If you have problems with any of the attachments feel free to contact me. Additional forms are provided at 

.wWWJJr;;a.state.mn.us/air/performan<;<ete.§.l.html 

Sincerely, 

Andy Place 

Performance Test Coordinator 

Minnesota Pollution Control Agency 

520 Lafayette Road 

St. Paul, MN 55155-4194 

(651) 296-7169 

8/5/2005 
Facility Name: US Steel-Minnesota Ore Operations 

Facility Contact: Chrissy Bartovich 

Address: Minntac Plant, P.O. Box 417, 8819 Old Highway 169, Mountaio Iron, MN 55768 

Fax: (218)749-7360 

Emission Unit(s): Agglomerator Lines 3, 4, and 5 (SV103, SV118 and SV127) 

Scheduled For: May 16, 2005, at your Facility located in Mountain Iron, Minnesota. 

AQ#26A 

Your test plan submitted on Aprill8, 2005, and discussed on May 11, 2005, has been approved 

by the Minnesota Pollution Control Agency (MPCA) as follows: 

0 Shortened test notification approved 

0 Test plan approved without modification 

[8J Test plan approved with the following provisions: 

Equipment should be operated at maximum capacity during testiog. Include process 

equipment and control equipment operatiog rates on the Operating Data Summary form. 

Include io the final testreport(s) the full reference method data record (strip chart and/or 

datalogger output) used to calculate emissions. The data record should ioclude calibration 

values for any instrumental analyzer used for emissions compliance testing. 

For SV103, the public notice process has been conducted for Air Emission Permit No. 

13700005-004, which contains an Opacity Standard Adjustment ofless than or equal to 40 % 

opacity as authorized by Minn. R. 7011.0120, subp. 3, for SVJ 03 Lioe 3 Waste Gas Stack 

(Agglomerator Line 3). This Opacity Standard Adjustment will become effective upon 

permit issuance and extend until Startup of the upgraded particulate pollution control 

equipment at SV103. This upgrade is required by the permit no later than October 30, 2006. 

The particulate control equipment upgrade must enable the Permittee to comply with the 0.01 

gr/dscf emission limit for Front-HalfParticulate Matter in Table 1 of 40 CFR 63, Subpart 

RRRRR, and is expected to reduce opacity emissions to below 20%. The MPCA 

understands that to demonstrate compliance with the AO% opacity limit for SV103, the unit, 

at the time of testing, may be out of compliance with the current 20% limit. This exemption 

from current permit conditions applies only for the duration of the upcoming test. 

Attached Forms: 

[8J Operating Data Summary- Combustion 

Sources 

[8J Operating Data Summary- Process Sources 

I:8J Certifications Form 

0 Operating Data Summary- Waste 

Combustors 

0 Operating Data Summary- Asphalt Plants 

[8J Microfiche/CD-ROM Submittal Form 

Note: Forms are also available at: www.pca.state.mn.us/air/performancetest.html 

Approved by: Date: May 12, 2005 
Andrew Place 

Performance Test Coordinator 

Compliance and Enforcement Section 

Industrial Division 

Please contact me at (651) 296-7169 if you have any questions regarding this approval. 

Please be aware that enforcement action will be taken for performance test failures indicating emissions above applicable limits 

(excess actual emissions to the environment). Failures commonly result in assessment of a monetary penalty. Upon the first test 

failure, the Company should take immediate measures to minimize emissions. The measures taken should be documented, as 

they will become part of the record of corrective actions. 

Hard Copy Peiformance Test Reports and Microfiche or CD Copy submittals will be addressed to: Compliance Tracking 

Coordinator, Compliance and Enforcement Unit, Industrial Division, Minnesota Pollution Control Agency, 520 Lafayette Road 

North, St. Paul, Minnesota 55155-4194 

cc: Tom Kuchinski, Barr Engineering, Minneapolis (email) 

Bob Beresford, MPCA, Duluth (email) 

AQ Correspondence File No. 26A 
U. S. Steel Corporation 

Minnesota Ore Operations 

P.O. Box 417 

Mt. Iron, MN 55768 

Aprill5,2005 

Mr. Andrew Place 

North District, Major Facilities 

Minnesota Pollution Control Agency 

520 Lafayette Road 

St. Paul, Minnesota 55155-3898 

RE: USS -Minnesota Ore Operations (Minntac) 

Notification of Testing and Test Plan 

Dear Andrew, 

This document is the Notification of Testing and Test Plan for performance tests to be conducted 

during the week of May 16, 2005. Tests will be performed on the Agglomerator Lines 3, 4 and 5 

waste gas stacks (SV103, SV118 and SV127 respectively). 

TEST PLAN 

Part 1. General Information 

(1) Name and address of the emission facility. 

U.S. Steel- Minnesota Ore Operations 

Minntac Plant 

P.O. Box417 

8819 Old Hwy 169 

Mountain Iron, Minnesota 55768 

(2) Name, title and telephone number of contact person at the emission facility. 

Chrissy Bartovich 

Environmental Control Engineer 

Voice phone 218-749-7364 Fax phone 218-749-7360 

Electronic mail: clbartovich@uss.com 

(3) Permit number or name of other applicable document. 

Pending Air Emissions Permit 13 700005-004 (PSD Permit) 

( 4) Reason for testing. 

Initial performance test per the pending permit. 

- 1-
( 5) Schematic drawing of the stacks and sample ports. 

Enclosed herein. 

a) Location of Plant 

Within the corporate limits of the city of Mountain Iron, MN. 

b) Name, contact person, and telephone number for testing company 

Barr Engineering, Minneapolis, MN. 

Richard Berg (952) 832-2787 

Part 2. Testing Requirements 

(1) List ofpollutsnts to be tested, the emission limit for each po!lutsnt and the applicable rule or 

regulation for the emission limit. 

Group 9 Agglomerator Line 3 & Group 10 Agglomerator Line 4 and Line 5- PM, 

PMw, Opacity, CO, S02, VOC, and Fluoride 

There are no permitted emissions limits for PM10 CO, VOC and Fluoride until the PSD 

permit is in effect. The following emissions limits are in effect. 

Particulate Matter (PM) 

Minn. R 7011.0610 subp. l(A)(l) 

0.30 grains per dry stsndard cubic foot, or the less stringent of either Minn. R 

7011.0730 or Minn. R. 7011.0735 

Opacity - Line 3 only 

Minn. R 7011.0120 subp. 2(B) 

Less than or equal to 40% 

Opacity - Line 4 and Line 5 

Minn. R 7011.0610 subp. l(A)(2) 

Less than or equal to 20% except for one six-minute period per hour of not more 

than 60% opacity. 

(2) Description of procedure for fuel sampling and analysis, where applicable. 

If biomass is used as a fuel during the test, wood will be sampled and analyzed for heat 

and sulfur content. 

Part 3. Operating Conditions 

(1) List the process or operating rate and conditions of the process equipment and the air 

pollution control equipment for the test. 

All tests will be performed while the associated process equipment is operating at maximum 

capacity and all control equipment will be operated normally. 

-2-
Green ball feed rate range is 280 to 350 LTPH on Line 3. 

Green ball feed rate range is 525 to 625 LTPH for Lines 4 and 5. 

Fuel will be either a blend of natural gas and wood or 100% gas during the tests. 

(2) Explanation of why the proposed conditions are considered to be in accordance with Part 

7017.2025, Subpart 2, for required testing conditions. 

The statement about the assumption of worst case conditions in the cited subpart applies. 

(3) List the range of process or operating rates for this emission nnit. 

The minimum process rate is zero. The maximum green ball feed process rate is 

approximately 350 LTPH for Line 3 and 625 LTPH for Lines 4 and 5. 

( 4) Descriptions of how air pollution control and process equipment will be monitored. 

The emission control nnits will be monitored for pressure drop and water flow during all 

tests. 

Part 4. Test Methods 

(1) List of the methods to be used to determine the emission rate of each pollutant. 

Test Port Location 

Determination of velocity and volumetric flow 

Determination of gas molecular weight 

Determination of moisture content 

Determination of PM 

Determination of Condensable PM 

Determination ofPM10 

Determination of CO concentration 

Determination ofVOC concentration 

Determination of SO, concentration 

Determination of Fluoride concentration 

Visual Determination of the Opacity of Emissions 

EPA Method 1 

EPAMethod2 

EPAMethod3A 

EPAMethod4 

EPAMethod5 

EPA Method 202 

EPA Method201A 

EPA Method 10 

EPA Method 25A 

EPA Method 6C 

EPA Method 13B 

EPAMethod9 

Note- both filterable and condensable particulate matter will be measured. PM10 measurements 

(Method 201A) cannot be made at the waste gas staclJ; because of high moisture content in the gas 

stream. PM10 will be determined by adding the inorganic condensible particulates to the dry plus 

organic particulates on Lines 4 & 5. PM10 will be conducted on Line 3 only. 

(2) Number oftest runs, length of the test runs, and sampling rate for each method. 

3 one-hour test runs except for Methods 1, 2 and 9 

Method 9 will be 1 one-hour observation performed in conjunction with one Method 5 

test run. 

-3-
(3) Reference to any compliance document, federal regulation, or Minnesota rule or statute 

requiring use of specific methods or procedures. 

Not applicable 

( 4) Summary of reasons for proposing to use alternative or equivalent method. 

None proposed 

( 5) For test methods other than reference methods, statement of the detection limit and the 

degree of accuracy of that method at the expected emission rate and under the conditions of 

the performance test. 

None applicable 

Test Schedule and Pretest Meeting 

The testing is scheduled to occur dUring the week of May 17-20, 2005. At the preference 

of the MPCA, we would suggest the pretest meeting could occur no less than 7 days 

before the testing begins and be conducted via telephone. 

Closing Remarks 

If there are any questions or comments on the information given in this document, please 

contact me at the telephone numbers listed above. 

Chrissy Barto tch 

Environmental Control Engineer 

Enclosures: 

STEP! AGG WG.doc 

STEP2 AGG WG.doc 

CERTIFIED MAIL# 7003 2260 0000 2381 8071 

cc: Robert Beresford, MPCA- Duluth Regional Office 

Hongming Jiang, MPCA North District Major Facilities 

Richard Berg-Barr Engineering 

Ray Potts- Minntac 

Cory Bird- Minntac 

Ron Braski-Minntac 

-4-
10'-0" . j. .j TOP OF STACK 

EL. 1212'-0" 

13 '-0" 

-.---+-X --+--rl'----<c----Four Sample Points @ 90° 

5 '-0" ROOF __________ -L~ 

Elevation View 

1. Emission Source Number- SV 103 (Old Source Number 8.3) 

2. Emission Unit Nurnber-223, 224, 225, 226 

68'-0" 

35' -0" 

STRUCTURAL 

SUPPORT 

EL. 1096'-0" 

STEP I 

AGGLOMERATOR 

WASTE GAS 

3. Plant Equipment Number- 242-03:2; 261-03-1; 252-03-1; 262-03-1 

4. Stack Diameter- 10 '-0" 

5. Stack Design Gas Velocity- 56.8 FPS. 

6. Stack Design Volume- 267,775 CFM. 

7. Stack Design Temperature- 200°F. 

8. Pollutants- Particulates and Combustion Emissions 

Step I Agglomerator 

Minnesota Ore Operations 

Minntac, Mt. Iron, MN 
5'-0" 

ROOF 

FAN 

-·-

15' -0" ~ Steel 

14'-0" Liner 

; 

; 

; 

' _ ........ -········f,; ...... -

; 

; 

; 

; '

; 

; '

; 

; 

; 

i 

; '

; 

; 

; 

i 

Elevation View 

1. Emission Source Numbers- Line 4 SV 118, Line 5 SV 127 

~I Top of Stack 

El. 1236'-0" 

34. -0" 

52' -0" 

53 '-5" 

Bottom /Steel 

EL 1097"-5" 

STEP II 

AGGLOMERATOR 

WASTE GAS 

2. Emission Unit Number- Line 4 EU 259, 260, 261, 262 Line 5 EU 280, 282,282, 283 

3. Plant Equipment Number- 242; 261; 252; 262 

4. Stack Diameter- 15.0' with 14'-0" diameter fiberglass liner 

5. Stack Design Gas Velocity- 56.3 FPS 

6. Stack Design Gas Volume- 591,000 CFM 

7. Stack Design Gas Temperature- 125 to 150'F 

s:\air\stacks\STEP 2 AGG WG.doc 

Step IT Agglomerator 

Minnesota Ore Operations 

Minntac, Mt. Iron, MN 


Minnesota Pollution Control Agency 

Andrew Place- Performance Test Coordinator 

Hongming Jiang- Permit Engineer 

U.S. Steel Corporation- Minnesota Ore Operations 

Project Participants 

Larry Salmela - Department Manager Environmental Control 

Chrissy Bartovich - Environmental Control Engineer 

Ray Potts- Environmental Control Engineer 

Ron Braski - Agglomerator Coordination 

Barr Engineering Company 

Tim Russell -Vice President/Chemical Engineer 

Richard Berg- Project Manager 

Tom Kuchinski- Senior Air Quality Technician/Team Leader 

Dan Koschak - Environmental Engineering Technician 

Jon Stock- Technician 

Bill Scott- Technician 

#2369927001 

J-1