# Client U.S. Steel Location Line 4 Waste Gas Stack (SV118) Date 7/12/2005 Operator T. Kuchinski City, State Mt. Iron, Minnesota

Calibration Input

Analyzer

# U.S. Steel 

# Project Sample Loc. Date Operators Line 4 Waste Gas Stack (SV118) 

# 711212005 T. Kuchinski

Analyzer Make 

# I Mod. 

# I SN 100AH Analyzer Range (span), PPM: 100 Stripchart Speed (units): 20 cm/hr



# ANALYZER CALIBRATION DATA Note: Difference must be less than 

# +1- 2 percent of span

Cylinder Test Runs : Test 4 R1 Value, PPM Zero Gas 0 Mid-range 51.2 High-range: 93.1



# SYSTEM CALIBRATION BIAS AND DRIFT DATA: EPA METHOD 

# 6C

- 502 ANALYZER CALIBRATION

Cylinder Serial No. Zero Gas Nitrogen Mid-range CC63443 High-range CC121446

Analyzer Absolute Difference, Calibration Difference Percent of Response, PPM PPM Span
0.0 0.0 0.00%
51.2 0.0 0.00% 93.0 0.1 0.10%

Note: System Cal bias cannot exceed 

# +1- 5 percent of span. Drift cannot exceed +/- 

# 3 percent of span

Initial Values Final Values Analyzer Cal System Cal System Cal System Cal System Cal Response Response, Response, Cal. Bias Response, Cal. Bias TEST RUN 1 Time (sec) PPM PPM %of Span PPM %of Span
Zero Gas



# - 0 1.3 1.30% 2.2 2.20% Upscale Gas



# - 51 49 -2.20% 49.0 -2.20%

TEST RUN 2
Zero Gas



# - 0 2 2.20% 2.6 2.60% Upscale Gas



# - 51 49.0 -2.20% 50.0 -1.20%

TEST RUN 3
Zero Gas



# - 0 2.6 2.60% 3.30 3.30% Upscale Gas



# - 51.2 50.0 -1.20% 51.10 -0.10%

System Calibration Bias =[(System Cal. Response- Analyzer Cal. Response) 

# I Span] x 100

Drift= [(Final System Cal. Response -Initial System Cal Response)/ Span] x 100 Cert. PPM 0 51.2 93.1

Drift, Percent of span 0.90%
0.00%

0.40%
1.00%

0.70%
1.10%

# U.S. Steel Project Sample Loc. Date Operators Line 4 Waste Gas Stack (SV118) 711212005 T. Kuchinski

Analyzer Make 

# I Mod. 

# I SN Teco48 Analyzer Range (span), PPM: =-1-"0:-'0'--- Stripchart Speed (units): 20 cmlhr



# ANALYZER CALIBRATION DATA
Note: Difference must be less than 

# +1- 2 percent of span

Cylinder Test Runs: Test 4 R1 Value, PPM Zero Gas 0 Mid-range 34.1 High-range: 60.4



# SYSTEM CALIBRATION BIAS AND DRIFT DATA: EPA METHOD 

# 10· CO
ANALYZER CALIBRATION

Cylinder Serial No. Zero Gas Nitrogen Mid-ran_lle CC78171 High-range CC12600

Analyzer Absolute Difference, Calibration Difference Percent of Response, PPM PPM Span
0.4 0.4 0.40% 33.7 0.4 0.40% 60.1 0.3 0.30%

Note: System Cal bias cannot exceed 

# +I- 5 percent of span. Drift cannot exceed 

# +I- 3 percent of span

Initial Values Final Values Analyzer Cal System Cal System Cal System Cal System Cal Response Response, Response, Cal. Bias Response, Cal. Bias TEST RUN 1 Time (sec)_ PPM PPM %of Span PPM %of Span
Zero Gas 0 0.6 0.20% 0.4 0.00%
L!!Jscale Gas 33.7 33.7 ·o.OO% 33.2 -0.50%

TEST RUN 2
Zero Gas 0 0.4 0.00% 0.3 -0.10% Upscale Gas 33.7 33.2 -0.50% 32.3 -1.40%

TEST RUN 3
Zero Gas 0.4 0.3 -0.10% 0.3 -0.10% Upscale Gas 33.7 32.3 -1.40% 32.7 -1.00% System Calibration B1as

- [(System Cal. Response

- Analyzer Cal. Response) 

# I Span] x 100

Drift= [(Final System Cal. Response- Initial System Cal Response) 

# I Span] x 100 Cert. PPM 0 34.1 60.4

Drift, Percent of span -0.20%
-0.50%

-0.10%
-0.90%

0.00% 0.40%

# EPA METHOD 25A-THC 

# as methane ANALYZER CALIBRATION

Project Sample Loc. Date Operators U.S. Steel 

# Line 4 Waste Gas Stack (SV118)



# 711212005 T. Kuchinski

Analyzer Make 

# I Mod. 

# I SN Ratfisch Rs 55 CA Analyzer Range (span), PPM: 110 methane Stripchart Speed (units): 20 cmlhr



# Linearity Demonstration Zero Gas Low-range ·Mid-range High-range

Note: Response must be less than 

# +/- 5 percent of actual calibibration gas values.

Cert. PPM System Response Percent Diff Zero Gas 0 0.3 0.3 Low-range 30.2 30.4 0.66 Mid-range 46.5 47.3 1.72 High-range 90.4 90 0.44 

# SYSTEM CALIBRATION AND DRIFT DATA: (;ylinder Serial No. Air cylinder SG9165492BAL CC2937 CC47777 Cert. PPM 0 30.2 46.5 90.4

Note: System Calibration cannot exceed +/- 5 percent of span gas value. Drift cannot exceed +/- 3 percent of span

Initial Values Final Values

System Cal System Cal Drift, Response Response, Response, Percent of TEST RUN 1 Time (sec) PPM PPM span Zero Gas 0.3 2.0 1.55% Upscale Gas 30.4 29.2 -1.09%

TEST RUN 2
Zero Gas 2.0 2.1 0.09% Upscale Gas 29.2 28.3 -0.82%

TEST RUN 3
Zero Gas 2.1 1.7 -0.36% Upscale Gas 28.3 29.5 1.09%

## Project U.S. Steel 

## Sample Location 

## Date Line 4 Wasre Gas Stack (SV118) 

## 7112/2005 Operators T. Kuchinski

Analyzer Make 

## I Model/ SN Analyzer 0 2 

### Range (span),%: 

## CaL Anal. Model 

## 200 25 Analyzer C0 2 

### Range (span),%: 

## 10 Stripchart Speed (units): 

## 20 cm/hr



## ANALYZER CALIBRATION DATA
Note: Difference must be less than 

### +f. 2 percent of span



# o, Cylinder

Test Runs: Test 1 R1 Value,


### %
Zero Gas 

### 0.0 Midwrange: 

### 9.1 HiQhwranQe: 

### 20.0



# co, Cylinder

Test Runs: Test 1 R1 Value,


### %
Zero Gas 

### 0.0 Midwra_t:lge: 5.0 High-range: 

### 9.1



## SYSTEM CALIBRATION BIAS AND DRIFT DATA: EPA METHOD 3A ANALYZER CALIBRATION

Analyzer Absolute
Calibration Difference Response,% 

### %
0.0 0.0
9.0 0.1
20.0 0.0

Analyzer Absolute
Calibration Difference Response,% 

### %


# o.o 0.0
5.0 0.0
9.0 0.1 Difference,

Percent of

Span
0.00%


### 0.28%
0.00%

Difference,

Percent of



## Span
0.00%
0.00%
0.50%

Note: System Cal bias cannot exceed+/- 5 percent of span. Drift cannot exceed 

### +1- 3 percent of span

Initial Values Final Values Analyzer Cal System Cal System Cal System Cal System Cal Response Response, Response, Cal. Bias Response, Cal. Bias


### TEST RUN 1 Time (sec) 

### % 

## % %of Span 

### % %of Span
Zero Gas 0 2 

### 0.0 0.1 0.40% 

### 0.00 0.00% Upscale Gas 0 2 

### 20.0 20.0 0.00% 19.90 -0.40%

Zero Gas C02 

### 0.0 0.0 0.00% 

### 0.1 0.50% Upscale Gas**C~** 

### 5.0 5.0 0.00% 

### 5.0 0.00%

TEST RUN 2
Zero Gas 0 2 

### 0.0 

# o.oo 0.00% 

### 0.1 0.40% Upscale Gas 0 2 

### 20.0 

### 19.90 -0.40% 

### 20.0 0.00%

Zero Gas C02 

### 0.0 0.05 0.50% 

### 0.1 1.00% Upscale Gas C0 2 

### 5.0 5.00 0.00% 

### 5.0 0.00%

TEST RUN3 Zero**Gas~** 

### 0.0 0.1 0.40% 

### 0.1 0.40% Upscale Gas 0 2 

### 9.07 9.00 -0.28% 

### 9.13 0.24%

Zero Gas C02 

### 0.0 0.1 1.00% 

### 0.0 0.00% Upscale Gas C0 2 

### 9.05 

### 9.0 -0.50% 

### 9.05 0.00%

Fluorides Test Run 4 Zero Gas 0 2 

### 0.0 0.1 0.40% 

### 0.0 0.00% Upscale Gas 

## 0:l 9.1 9.1 0.24"/

.. 

### 9.0 -0.12% Zero Gas C02 

### 0.0 0.0 0.00% 

### 0.0 0.00% Upscale Gas CO:z 

### 9.05 9.05 0.00% 

### 9.08 0.30%

Particulate Test Run 4 Zero Gas 0 2 

### 0.0 0.0 0.00% 

### 0.1 0.40% Upscale Gas 0 2 

### 9.1 9.0 -0.12% 

### 9.1 -0.08% Zero Gas C02 

### 0.0 0.0 0.00% 

### 0.1 0.50% Upscale Gas C0 2 

### 9.05 9.08 0.30% 

### 9.0 -0.10%



# - nnft- 

### UFtnal Svstem Cal. Response lmtlal System Cal Response) 

### I Span] x 100 Drift,
Percent of

span 0.40%
0.40%

-0.50%
0.00%

-0.40%
-0.40%

-0.50%
0.00%

0.00%
-0.52%

1.00% -0.50%



### 0.40%
0.36% 0.00% -0.30%

-0.40%
-0.04% -0.50% 0.40%

## Control Module C-2 Barometric Pressure 

## 29.2 Project: Routine 

## Leak checks Previous Y

--- 

## 0.9969 Date: 6/25/2005 Negative-· ok >5W.C. Previous Delta H

-- 1.8844 Technician: 

## NRS 

# Positive- ok > in.Hg

Orifice 

## Dry Gas Wet Test Dry Gas Meter WetTest Elapsed Meter Orifice



## Diff Volume Volume, Temp, F Meter Time of 

# Coefficient Coefficient Presure H 

## Cubic Feet Cubic Feet Inlet Outlet Temp, F Cal. Point 

# y dH@ 1Nomma1 t-mal ,final Final t-1nal Final 

## Minutes 

## SEC 0.500 673.635 3940.50 76.0 73.0 71.5 17 44.03 !Actual Initial Initial Initial Initial Initial Minutes 

## 666.680 3933.50 73.0 72.0 71.0 0.50 Total Total Average Average 

## Average 6.955 7.00 74.5 72.5 71.3 17.73 1.0095 1.8464 73.5 Nominal 

## Final Final Final Final Final Minutes 

## SEC 1.000 707.320 3974.00 78.0 75.0 73.0 8.0 57.81 !Actual Initial Initial**ln~ial** 

## Initial Initial Minutes 

## 702.290 3969.00 75.0 74.0 73.0 1.00 Total Total Average Average Average 

## 5.030 5.00 76.5 74.5 73.0 8.96 0.9962 1.8544 75.5 Tm Nominal 

## Fmal Final Final Final Final Minutes 

## SEC 2.000 687.110 3954.00 83.0 75.0 71.5 8.0 58.94 Actual Initial**ln~ial** 

## Initial Initial Initial Minutes 

## 680.085 3947.00 80.0 74.0 71.5 2".00 Total Total Average 

# Average Average 7.025 7.00 81.5 74.5 71.5 8.98 1.0036 1.8895 78.0 Tm Nominal Final 

## Final Final Final Final Minutes 

## SEC 3.000 693.190 3960.00 84.0 76.0 71.5 5.0 15.64 !Actual Initial 

## Initial Initial Initial Initial Minutes 

## 688.125 3955.00 83.0 75.0 71.5 3.00 Total Total Average 

## Average Average 

## 5.065 5.00 83.5 75.5 71.5 5.26 0.9945 1.9019 79.5 Tm Nominal 

## Final Final Final Final Final Minutes 

## SEC 4.000 699.275 3966.00 86.0 76.0 71.5 4.0 33.88 Actual Initial Initial Initial Initial Initial Minutes 

## 694.210 3961.00 84.0 76.0 71.5 4.00 Total Total Average 

## Average Average 

## 5.065 5.00 85.0 76.0 71.5 4.56 0.9939 1.9075 80.5 Tm Average 0.9995 1.8799

# Routine 

# Dry Gas Meter Calibration

Control Module Number: 

# C- "2--

Date: 

# (o- 

# 25' 

# -osTechnician: -lfiVL/t"'S.,__

_____ _
Dry gas 

### WetTest 

## Leak Checks Barometric Press.: 

# "2. c1. 

# '2-

Positive

_ _.:::o..ck:__at 5 in.H20 Previous Y: Negative 0 

## 1<-- at 

# 15 in.Hg Previous t,.H: --'"-'--

WetTest Elapsed Time of Meter Orifice

# Project Name: USS Minntac Module Number: ..::C:...-;:.2**~:--::-:­** 

# Date: 6-Aug-05 Tecb:..:..N:o;R;::_S

__ _ 

# EPA MS POST TEST METER CALIBRATION

Nominal sample conditions

Delta 

# H: 2 W.C. Vacuum: ----'9'--_in. Hg 

# Project No.: 23/69-927- Barometric Pressure: --::-::-::2':9':;."'12::. Previous 

# Y: 0.9995 Previous Delta H:

# -~1:::.8::7~9_:e9_

Pre cal +5% 

# Pre**cal~** 

## 5% 

# Within 5% YIN 

# 1.0495 0.9495 

# YES 1.9739 1.7859 

# YES

# EPA M5 POST TEST METER CALIBRATION

Prqj ect Name: 

# uss M:."hc Project No.: 

# 23/&'1- '12..lModule Number: 

# C/2.. Nominal sample conditions Barometric Pressure: 

# 2'1.1?

Date: 

# Y-(p-os- DeltaH: 

# z..o w.c. Previous Y:



# . 7"'195""

Tech: 

# NR.."> Vacuum: 

# q in. Hg Previous Delta H : 

# /.8792

Equip Cal Data Sheets1

### Control Module C-5 Barometric Pressure 29.14 Project Routine Leak checks Previous Y

-- 0.9961 Date: 

## 71912005 Negaf1ve -· 

## ok >SW.C. Previous Delta H

-- 1.9659 Technician: NRS Positive-- 

## ok > in.Hg

M5APR.WQ1

# Routine Dry Gas Meter Calibration

Control Module Number: 

# C./'i

Date: 

# 7 1'7 

# I o<:;

# Technici~n! ---"N"-'12.."'-"S'--------- Leak Checks
Positive 

# ok
Negative o 

# kOrifice 

## Dry gas 

### WetTest WetTest 

# Barometric Press.: 

# Z. 

# '1. 

# I'-!

at 5 in. H20 Previous Y:
at 15 in.Hg Previous**~H:**

Elapsed 

# • 9 "t(.,( 

# /. "Hos-4'

Meter 

### Orifice

# Project Name: USS Minntac Module Number: _,C'--"-5-::-:--::--:- Date: 6-Aug-05
Tech: -"NRS='--- 

# EPA MS POST TEST METER CALIBRATION

Nominal sample conditions

Delta H: 0.92 W.C. Vacuum: 18 in. Hg Project No.: 23/69-927- Barometric Pressure:**--,:-;c;:2C;9'c'.~l2::..** 

# Previous Y : 0.9946 Previous Delta H : --:l-:.9,.:6:;:9::;-2-

Pre cal +5% 

# Pre cal- 5% Within 5% YIN 

# !.0443 0.9449 YES 

# 2.0677 !.8707 

# YES

# EPA MS POST TEST METER CALffiRATION 

# BARR

Project Name: 

# u :;,s M**~.** 

# nh c


# Module Number: 

# _...:C...=-----=:5:._

__ _ Date: 

# __,8:.,_-....::(p:._-....::Cf5=---

Tech: 

# ---'-N=R:o::S:.__

__ _

Equip Cal Data Sheets1 

# Nominal sample conditions

DeltaH: 

# o.9'L W.C.

Vacuum: \ 

# 'i' in. Hg ProjectNo.: 

# 2:C,/!ocr-92lBarometric Pressure: 2 'l.l )>



# Previous Y : .....:..· 

# 'l,__'l:.._'-l:...:!a:___

Previous Delta H : 

# (.9<.'1'2...

# ANEROID BAROMETER CALl BRA TION

Barometer LD. Number: 

# i3 A- OS""
Barometer Reference: 

# f 12..J:.AJC.u

Pretest Calibration:

Before Adjustment After Adjustment

Posttest Check:

Notes:

Barr Engineering Co. 

## 4700 W. 77th St Minneapolis, MN 55437 

## (952) 832-2600 

# Reference ("Hg) 

# 2'1 

# 0'-/

Reference ("Hg) Project Name:---------- Project Number:

---------

Barometer ("Hg) Date Technician



# 2c;.oo 

# 7/2'-1/D.,. NR5

Barometer ("Hg) Date Technician

# ANEROID BAROMETER CALIBRATION

Barometer 

# I. D. Number: 

# 'J? A 

# ...osBarometer Reference: 

# f r ; A.. 

# c <->



# Pretest Calibration:

Before Adjustment
After Adjustment

Pastiest Check:

Notes:

Barr Engineering Co. 

## 4700 W. 77th St Minneapolis, MN 55437 

## (952) 832·2600 

# Reference ("Hg) 

# 2'7. 2....( 

# 2..4. (.C:. 

# -

Reference ("Hg) Project Name: \ [ S" 

# s

# ""'--1·~ .., 

# -/<-,._ \
Project Number: 2.. 

# > G, 

# 9 "7 Z 7 / (-'> 

# 0**~** 

# C 

# v s \L >D



# - vse

.. e[c.**of<!~** 

# I 1

Barometer ("Hg) Date Technician 

# 2-{. 

# z... D 

# 7 /{1 I <>::> /V1-Lr 

# 2 

# c;' {**:;,~** 

# 7/111.;;-- 7'+ / c

Barometer ("Hg) Date Technician

# BARR

Engineering Company

PitotTubeNumber:

# ~ 

# 7-1
\ 

# length:

Function: M-5 

# Probe I Free

1. 

## Are face openings perpendicuiar" 

## to 

# tube axis?

# ~ES (gotoZ) 

# 0 NO (go 

## to 1a) / 

# '**""""'~** I

# ·-~~~~---- ' 

# - '**l---~----{** 

# . .

2.. Are 

## face openings paraDel 

## to longitudinal axis?

# ~ES(goto3) 

# 0 NO(gotoZa)**~** 

# J



# ._.....,. t 

# --_,

3. Are 

## legs of equal length?

# ~ES(goto4) 

# 0 NO (go to 

## 3a)

# k----~~~~-~-----

4. Are**center-1i~es** 

## of 

## legs coincident?
9J--:(ES ( go to 5) 

# 0 NO (go to 

## 4a)

5. Does this pilot tube pass afi 

## of the above criteria?

Technician Signab.Jre: 

# S-Type Pitot Tube Geometry Check

Inspection Date:



# Technician:

. ' N' ""-



## 1a. If NO, is an9Ie less 

## fhan-10"1 

# 0 YES (gotoZ) 

# 0 NO (discontinue use)



# ,.., ' !L __t;

. 

# --£3Ei----·**-~~---** ' I I I 

# . . 

# . .

2a. If NO, 

## is angle le_ss than 

## So?

_ 

# 0 YES (goto3)



# I· 

# -17 

# '"**~- ~**  

# 0 NO (discontinue Use)

## ~· 

# -'D 

# ,, es:

..._

3a. If NO, 

## is difference less than 1/8 inch? 

# 0 YES (goto4) 

# · 0 NO (discontinue use)



## 4a. If NO, are center-lines of face openings less than 1/32 inch? 

# 0 YES (goto5) 

# 0 NO (discontinue use)



## tzlYES 

## ONO**-~** 

# ·.

# BARR
Engineering 

# Company

Pilot Tube Number: 

# i Length: ] 

# =

Function:

# ~ Free

1. Are face openings perpendicular to 

## tube axis? 

# 0 NO (go 

# to 1a)



## 2. Are face openings parallel 

# to longitudinal 

## axis?

# )~?~s {go 

# to 3)

_ 

# 0 NO (go to 

## 2a)



## 3. Are legs 

## of equal length? 

# ---,**~YES{goto4)** 

# 0 NO (go 

# to 3a)



# f--**-~~~---={--)-----**

4. Are center-lines 

## of legs 

## coincident? 

# R._ YES (go 

# to 5) 

# 0 NO (go to 

## 4a)

# ~-**--~~--=<--?-----**

5. Does this pitot tube pass 

## all**o~** 

## tlle af:love criteria?



## Tectinidan Signature: 

# S-Type Pitot Tube Geometry Check

Inspection Date:

Technician: 

# M""'**~~~----------**



## 1a. If 

## NO, is ang"le less than· 10°? 

# 0 YES (goto2) 

# 0 NO (discontinue use) 

# ""'

. rL

. .

_ __t; 

# --£3E3----·**-~~~--** 1 I I I 

# . . 

# . .

2a. If NO, is 

## angle**I~** 

## than 5"?

_ 

# 0 YES (go to 3)

. 

# 0 NO (discontinue use)

3a. If NO, is difference Jess than 1/8 inch? 

# 0 YES (goto4) 

# · 0 NO (discontinue use)



## 4a.. 

# If_ NO, are center-lines of face openings less than 1/32 inch? 

# 0 YES (go to 5) 

# 0 NO (discontinue use)



## 0NO

# REFERENCE STANDARDS

Hart Scientific 91 03-A s/n A 1 8289
Hart Scientific 9140 sin A18086 

# Temperature Calibraion Points

Reference Deg 

# F (To) Probe Temp (deg F) Reference Temp (deg R) deg F 

# + 460 Probe Temp (deg R), deg F 

# + 460 Difference (degrees) % DiffAbs. T Is difference less than 1 .5% at all measured points?



# 1700
1600
1500

# ~ 1400 

# .::**~** 

# 1300 

# "**~** 

# 1200

w 

# g; 1100
w 

# :;; 1000 

# K 

# 8 900 

# lil 800

# ~ 700 

# 600
500


# 400 

# THERMOCOUPLE CALIBRATION

THERMOCOUPLE ID 

# C-2-1

Cal Date: 4/15/2005 

# Meter In or Out CALIBRATION TECHNICIAN: JMM

TRACEABILITY

Report No. A180718 Report No. A1 82024


# 32

32 

# 32 

# 492 492

0 0.0%

YES 

# 212

212 210 

# 672 

# 670

2 0.3% DATE

12/11/2003
12/11/2003


# 400

400 

# 392 860 852



# 8 0.9% LABORATORY

Hart Scientific
Hart Scientific 

# 650

650 645 1110 1105



# 5 0.5% 

# 70

70 

# 68 530 528



# 2 0.4%



# 400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 REFERENCE TEMPERATURE, 

## deg.R



# Are extrapolated lim its less than 1.5%? YES



# If not acceptable, describe corrective action: FAHRENHEIT CALIBRATION RANGE -20 1200

# BARR

Engineering Company**~** 

# ...... -r Thermocouple Number: 

# -l.L-· -_,<?<:::__dd:==-

Media

Std Used

Reference Deg F (To)

Reference Corr Temp (deg R) deg F 

## + 460

Probe Temp ( deq 

## F)

Probe Temp (del!_ R), deg_F 

## + 460

Difference (degrees)


# % Diff Abs. T (Renkin)

Olff_ less than 1.5% at all points 

# Graph Attached
Extrapolated Range with Diff. 

## <= 1.5%

Description of the thermocouple's function: 

## 32

# ~~



# 3;i....

If 

## not acceptable, describe corrective procedures undertaken: 

## 212

# .;2t~


# J.tO 

# THERMOCOUPLE CALIBRATION

400



# "ictJ
-y,qd--

(Yes/No) (Yes/No) Date: 

# L(**~** i 

# S

- 0 

# S:

Technician:
,_,, 

# )_.f'A-'-'":...r

____ _

650 

## Ambient



# &70 

# 70
{pL.( 'j 

# &_'{

to

# BARR

REFERENCE STANDARDS

Hart Scientific 9103-A 

# sin A1B289
Hart Scientific 9140 s/n A1B086 Temperature Calibraion Points
Reference Deg F (To) Probe Temp (deg 

# F) Reference Temp (deg R) deg 

# F + 

# 460 Probe Temp (deg R), deg 

# F 

# + 460 Difference (degrees) % DiffAbs. T Is difference less than 1.5% at all measured points?

1700
1600
1500

# ~ 1400 

# ; 

# ::! 1300 

# "**~** 

# 1200

w 

# !l; 1100**~** 

# i 1000 

# 8 900

# ~ 800 rr w 

# i: 700
600
500
400 

# THERMOCOUPLE CALIBRATION

THERMOCOUPLE ID 

# C-2-0
Cal Date: 4/15/2005 Meter In or Out
CALIBRATION TECHNICIAN: JMM

TRACEABILITY
Report No. A1B0718 Report No. A1B2024


# 32 212

32 212 32 211 492 672 492 671

0 1 0.0% 0.1%

YES 

# DATE

12/11/2003 12/11/2003


# 400

400 394 860 854

6 0.7% 

# LABORATORY

Hart Scientific
Hart Scientific


# 650 70

650 70 645 

# 69 1110 530 1105 529

5 1 0.5% 0.2%

400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 REFERENCE TEMPERATURE, 

## deg.R



# Are extrapolated limits less than 1 

# .5%? YES



# If not acceptable, describe corrective action: FAHRENHEIT CALIBRATION RANGE 

# -20 1200

# BARR
Engineering Company

Thermocouple Number: 

# C

-**~** 

# CJ

Media

Std Used

Reference Deg F (To)

Reference CorrTem_IJ_(deg R) deg F + 460

Probe Temp (deg 

## F)

Probe Temp (deg R), deg F +460

Difference (degrees)



## % 

## Oiff Abs. T (Renkin}

Dift less than 1.5% at all points 

# Graph Attached ExtrapOlated Range with Oiff. <= 

## 1.5%

Description of the thermocouple's function; 

## 32


# <,:1**3~**

If 

# not acceptable, describe corrective procedures undertaken: 

## 212



# J 

# £)._



# J Ll THERMOCOUPLE

. CAL! BRA TION

400



# '-(tJO



# s <7 

# "1

(Yes/No)
(Yes/No) 

# Date: 

# '-j**~** 

# I 5"-**~** 

# 0 

# 5'

Technician: 

# 0 f"V"'.

650 Ambient



# &s-o {0

& 

# '-i.s c,c;

to

# THERMOCOUPLE CAll BRA TION 

# BARR

THERMOCOUPLE ID 

# C-5-0 Cai;Date: 12/27/2004 

# Meter In or Out CALIBRATION TECHNICIAN: NRS

REFERENCE STANDARDS TRACEABILITY DATE LABORATORY

Hart Scientific 91 03-A s/n A 1 B289 Report No. A1B0718 12/11/2003 Hart Scientific
Hart Scientific 9140 s/n A18086 Report No. A182024 12/11/2003 Hart Scientific
Temperature Calibraion Points 

# 20 70 150

Reference Deg F (To) "20 70 150 Probe Temp (deg F) 19 

# 69 149 

# Reference Temp (deg R) deg F + 460 480 530 610 Probe Temp (deg R). deg F + 460 479 529 609 Difference (degrees) 1 1 1 % DiffAbs. T 0.2% 0.2% 0.2% Is difference less than 1.5% at all measured points? YES

THERMOCOUPLE CALIBRATION 1700
1600**~500**

# ~400 <( 

# ffi' 300

# ~200

# ~14itlO w"' 

# n:t®o

6900 0 

# 0 800 

# 2 0:: 

# 700 llJ 

# F: 600
500
400 400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 REFERENCE TEMPERATURE, deg.R

Are extrapolated limits less than 1.5%? YES

If not acceptable, describe corrective action: FAHRENHEIT CALIBRATION RANGE -20 1200

# BARR
Engineering Company

Thermocouple Number:**T~** 

## GS'"- 

# o

Media



## Std Used 

# D-&

Reference Deg F (To)

Reference GorrTemp (deq R) deq F 

## + 460

Probe Temp {deq F)



## Probe Temfl (deg R), deg F +460

Difference (degrees)


# % Diff Abs. T (Renkin)

Oiff. less than 1.5% at all points 

## Graph Attached
Extrapolated Range 

## with Oiff. <= 

## 1.5%

Description of _the thermocouple"'s.function: 

## 20



# z_o '-/ S'O 

# 19 

# W-'7

-1

0 

# ·2- 70



# +o $30 

# (9"\ S<.."'i

-I

0 

## .<._ 

# THERMOCOUPLE CALl BRA TION**Date~** 

# \.**~-!..-7-Ct-{** 

# T echnician: 

# __,N=' ,2-,;S:._

__ _

150



# !s-D (,>\0 

# l';i"f (,09



# -r
0-"Z..

to



# C.M1-.-ol**MoJ~\._** 

# s**ts~K** 

# oo:f-le.f tl...u...,c_o.,.'i'k

If 

# not acceptable, descnbe corrective procedures undertaken:

# THERMOCOUPLE CALIBRATION 

# BARR

THERMOCOUPLE ID C-5-1
Cal; Date: 12/27/2004 Meter 

# In or Out CALIBRATION TECHNICIAN: NRS

REFERENCE STANDARDS TRACEABILITY DATE LABORATORY

Hart Scientific 9103-A s/n A1B289 Report No. A180718 12/11/2003 Hart Scientific
Hart Scientific 9140 s/n A18086 Report No. A1B2024 12/11/2003 Hart Scientific
Temperature Calibraion Points 

# 20 

# 70 150

Reference Deg F (To) 20 70 150 Probe Temp (deg F) 

# 20 69 148 Reference Temp (deg R) deg F.,. 460 480 530 610 Probe Temp (deg R), deg F.,. 460 480 529 608 Difference (degrees) 0 1 2 % DiffAbs. T 0.0% 0.2% 0.3% Is difference less than 1.5% at all measured points? YES

THERMOCOUPLE CALIBRATION 1700
1600

# ~500 p400
fE1300

# ~200

# ~1llt>O wO> ([1®0 

# 6 900 (.) 

# 0 

# 800 

# :::;; 0:: 

# 700 w

# ~ 600
500
400 400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 REFERENCE TEMPERATURE, deg.R

Are extrapolated limits less than 1 .5%? YES

If not acceptable, describe corrective action: FAHRENHEIT CALIBRATION RANGE -20 1200

# BARR
Engineering Company

Thermocouple Number: TC- 

# c.:-s-- 1:..-

Media



## Std Used 

# D-'it

Reference Deg F (To)

Reference Carr Temp ( deg R) deq F 

## + 460

Probe Temp {deg F)

Probe Temp (deq R), deq F 

## + 460

Difference

## (deqree~) 

# % Diff Abs. T (Renkin)



## Diff. less than 1.5% at all points 

# Graph Attached
Extrapolated Range 

## with Diff. <= 

## 1.5%

Description of the thennocouple

.. s. function: 20



## 2.0

## 4~0 

# 20 '-j 

# >'O

0
0-0 70



# +o S$0 

# (.; c\
SZ.9



# - \



# o:z. THERMOCOUPLE CALIBRATION

150

l 

## <;:"0**~{0** 

# 1'-1:<6

C.Cl?
-"Z.


# 0-3



# @I No) @No) 

# Date' I'Qi (L-2't--C'{ 

## Technician: "-'i'Li

to

# C..~-1--r-.l**1-\cel~\.__** 

# S"' b bM**:c-~** 1

..



# 1- +t-,.._..""-"<•-f' 1<-

If 

# not acceptable, describe corrective procedures undertaken:

# BARR PYROMETER CALIBRATION

Pyrometer Number: (" '"''

- 

# :t Pyrometer Reference: 

# C L 5rJiJ 

# 1L- (Pte• 

# tF Technician:

Reference (°F) Reference 

# rc) Pyrometer 

# L__)



# 1000 538 

# (003

950 510 

# cr,;--1

900 482 

# CfD'i

850 454

# ~s?> 800 427 

# g-o_>

750 399 

# 75>

700 371 

# 7D'I

650 343

# (c.>~ 600 316 

# t,;c vj

550 288 

# 553

500 260 

# so :f.-



# 450 232

# '--i~> 

# I

400 204 

# t.{oJ....

350 177 

# ss-J300 149 

# _5c'-l

250 121 ;;! 

# :,-'I

200 93 

# :/63

150 67

# iS~ 100 38 

# iO)

50 10 

# !?)-,

0 -18 

# 3

-50 -46


# - '1 )-

Notes:

# BARR PYROMETER CALIBRATION

Pyrometer Number: {_- 

# 5'

Pyrometer Reference: 

# {1_ 

# -J uC/ 

# -locc+

Reference CFJ Reference ( 0 

# C}



# 1000 538
950 510
900 482
850 454
800 427
750 399
700 371
650 343
600 316
550 288
500 260
450 232

400 204
350 177 -:- 

# 300 149

250 121
200 93

150 67

100 38



# - 50 10

0 -18
-50 -46



# · Notes: Date: 

# 1 }_-). 

# 9 

# -o<f

Technician:

# ~S;._

Pyrometer C_l 

# f001 

# '15o 

# cz 60 

# "?)So 

# gvo /)1 

# po

(;;50 

# s '7 

# i ')in 

# LJ 

# 1/ 

# 41/c 

# sn ]er_;

2_ 

# 'l 

# 'i 

# z<t"'

11Y**i'i~** 

# ']6 

# 41 -1 -5')_

# BARR

REFERENCE STANDARDS

Hart Scientific 9103-A s/n A1B289
Hart Scientific 9140 

# sin A 18086 

# Temperature Calibraion Points

Reference Deg F (To) Probe Temp ( deg F) Reference Temp (deg R) deg F 

# + 460 Probe Temp (deg R), deg F 

# + 460 Difference (degrees) % Diff Abs. T Is difference less than 1.5% at all measured points?

1700
1600
1500 '; 1400 

# • 

# .,**~** 

# 1300 

# "**~** 

# 1200

# ~ 1100

w 

# :;; 1000



# .... 

# .. " 900 

# §**~** 

# 800

w 

## j: 

# 700
600
500
400 

# THERMOCOUPLE CALIBRATION

THERMOCOUPLE ID TC 7-1 Cal;Date: 1/3/2005 

# CALIBRATION TECHNICIAN: 

# M-5 Probe
JMM

TRACEABILITY
Report No. A1B0718 Report No. A1B2024 

# 32 212

32 212 

# 32 209 492 672 492 669

0 3 0.0% 0.4%

YES DATE LABORATORY

12/11/2003 Hart Scientific
12/11/2003 Hart Scientific

400 650 Ambient

400 650 70 395 642 70 860 1110 530 855 1102 530

5 8 0 0.6% 0.7% 0.0%

400 500 600 700 800 900 1 000 11 00 1200 1300 1400 1500 1600 1700 REFERENCE TEMPERATURE, deg.R



# Are extrapolated limits less than 1.5%? YES

If not acceptable, describe corrective action: FAHRENHEIT CALIBRATION RANGE 950 -20 490

# BARR
Engineering Company



# ,-c_ Thermocouple Number:_,·'--' _·--'------

Media

Std Used

Reference Deg F (To)

Reference Carr Temp (deq Rl deo F 

## + 460

Probe Temp (deg 

# l'l

Probe Temp (deg R), deg F 

## + 460

Difference (degrees)

%Dill Abs. T (Renkin)



## Dlff. less than 1.5% at all points 

# Graph Attached
Extrapolated Range with Dill. <= 

## 1.5%

Description of the thermocouple's function:



# . j'A,l{,,j 

# .5:**1/v~~** 32



# 3J4'1 "2. 

# s}- 

# 49<-

0 

# o.o

If not acceptable, describe corrective procedures undertaken: 70



# 76 <;;"30


# /0
5"30

C) 

# o.o THERMOCOUPLE CALIBRATION

212



# ;:n:l.
, (o 

# 7Z. 

# ;;>a"'

"' lo"t 

# -;, O·Lj

# (~No)**(~/No)** Date: 

# I-$ 

# -asTechnician: 1 

# 1**~**



## 400 650



# L-/b() 

# (o.>()

'i;C.O 1110 

# 5 "l'f 

# G"i :L 2s-s- I I 07_ 

# -r -'51 

# "'·"' o.j

to

# REFERENCE STANDARDS

Hart Scientific 9103-A s/n A1B289
Hart Scientific 9140 s/n A1 8086 

# Temperature Calibraion Points

Reference Deg F (To) Probe Temp (deg F) Reference Temp (deg R) deg F 

# + 460 Probe Temp (deg R), deg F + 

# 460 Difference (degrees) % DiffAbs. T Is difference less than 1.5% at all measured points?

1700
1600
1500**~** 

# 1400 

# •**~** 

# ili 1300 

# " 

# s 1200

# ~ 1100

w 

# :;; 1000 

# o! " 900

# ~ : 800

w 

# i= 700
600
500

400 

# THERMOCOUPLE CALIBRATION

THERMOCOUPLE ID TC7-4 Cai;Date: 1/3/2005 

# CALIBRATION TECHNICIAN: M-5 Probe 

# JMM

TRACEABILITY

Report No. A1 B0718 Report No. A1B2024 

# 32

32 

# 32 492 492



# 0 0.0%

YES 

# 212

212 

# 211 672 671



# 1 0.1% DATE

12/11/2003
12/11/2003 

# 400

400 

# 399 860 859

1 0.1% LABORATORY

Hart Scientific
Hart Scientific 

# 650

650 650 1110 1110



# 0 0.0% 

# Ambient

70 70 530 530



# 0 0.0%

400 500 600 700 800 900 1000 11 00 1200 1300 1400 1500 1600 1700 REFERENCE TEMPERATURE, deg.R



# Are extrapolated limits less than 1.5%? YES

If not acceptable, describe corrective action: FAHRENHEIT CALIBRATION RANGE -20 1200

# BARR
Engineering Company

# ~--- '-'( Thermocouple Number:---,</'--·---'----

Media

Std Used 

# D-'6

Reference Deo F 

## (To)_

Reference Carr Temp (deg R) deg F 

## + 460

Probe Temp (deg F)

Probe Temp (deQ R), deo F 

## + 460

Difference {decrees)


# % Diff Abs. T (Renkin)



## Diff. less than 1.5% at all points 

# Graph Attached
Extrapolated Range with Diff. <::;;: 

## 1.5% 

## 32


# $.).__ 

# 492. 

# .? 1

# '-1'1-z0



## 0-0



## If not 

## acceptable, describe corrective procedures undertaken: 70



# 7d 5"30 

# 70 5"30

'0



# o.o 

# THERMOCOUPLE CALIBRATION

Date: /- 

# 3

- C! '{"
Technician:

## j~



## 212 400 650



# :JD- _Lj_!}/)

# ~so 

# c, I '2._ 

# Sc.o lifO 

# ,y 

# I ) 

# ] 1"'7 

# G)O
&>/.( 

# l?s; { 1{0 

# -I 

# -r 0 

# 6-f 0.( 

# O.D

toN 

### § 

# f 

# "'

0 

### 2 

# • a:**~** 

# • •**~** 

### _;;**~ ~**  

### r
1- 

## -" -" !<'
E 

# "

m 

# "' §!I 

## a: • 

# t

• 

# . £ 

### ;,; 

# :t**~** 0 

# f5 "- c**~**

### ~

# ~ .1:**~** 

### c 

# "' 0 

### :I 

## 0::



# = • 0 

### c 0 

## z a: 0 

# B: 

# il 1-**~**



## z

# ~ rJ

0 

# "**~** =>



# z 

# " 1" 

# "' {; 

# . " _..;**~~** 0**~**



# . "" 

# .. • 

# •

0 

# " > 

# "

w 

# • 1- 

### J 

# .**~** N 

### § § 

# •

<r 

## a: g

w 

## -" m ;u 

# *

rr 

## E i'- .£ 

# = = u.. .E 0**~** 0 

# I! I

0

- 0 

# .8**0~** 

# . -**~** 

### o9- .'!! 

# • ' c 

# •**~** 

## "- w 0 

### 0 

### >lectpiLac•srators.k,dLtvG7·1L·o5lAck.L>ampleISamplellMeterPointTestNo,CM)._Runs1.2sdTESTRUN1TrainEPAMETHOD13B·FLUORIDESFIELDDATASHEETMetery•"]'i1(Bar.PresZS.3InHgAH@I.•1<1J.Stat.Pres-6.J:JJInH20cpC>.?5'lProbeLngth2ftpLinerType;OS.S.OOther!LSampleTrainLeakRate(cfmRun1Pretest()at151nHg!PretestPosttestPilot(3ln.)Pos.NozzleCalibrationDate1-fl><..,rNozzleNo.()10:/752""·17f6Nu-zzJeC21I;b,<-t.f;o"'.........._3"'·•7"'I7Avg.ln:"'ol7J.:;...

# Sill I

BARROl 

# SCOTT-MARRIN, INC.

6531 BOX SPRINGS BLVD. • RIVERSIDE, CA 92507 TELEPHONE (909) 653-6780 • FAX (909) 653-2430



# REPORT OF ANALYSIS EPA PROTOCOL GAS MIXTURES

TO: Sam Foss DATE: 

# July 13 2004 Barr Engineering Co 

# 7390 OHMS Lane Edina MN 55439-2330

CUSTOMER ORDER NUMBER: 

# Vbl/S FOSS

COMPONENT CONCENTRATION(v/v) REFERENCE ±EPA UNCERTAINTY STANDARD CYLINDER NO: 

# CC121446

Sulfur Dioxide 93.1 ± 

## 0.9 

## ppm GMIS 

## CYLINDER#: 

## Nitrogen 

# Balance CC12025 

## CYLINDER PRESSURE: 1150 

## psig @ 111.8 ppm



## ppm = 

## pmole/mole % 

### = 

## mole-% 

## ANALVZER EXPIRATION REPLICATE MAKE, MODEL. SIN, DETECTION 

## DATE ANALYSIS DATA

BOVAR MODEL 922M 07/12/04 

## S/N VD922B4844 07/12/06 

## 93.1 

## ppm CONTINUOUS 93.1 ppm
UV PHOTOMETRY 

### 93.3 

## ppm 

## LAST CAL DATE: 06/14/04 

## MEAN: 93.2 

## ppm



## The above analyses were performed in accordance with Procedure G1 of the EPA Trac ility Protocol, Report Number EPA-600/R97/121, dated September 1997. This cyiinder should not be used if the pressure is less than 150 psig.

# ANALYST:}~ M.J.MONSON

The only liability of this company for gas which falls to comply with this analysis shall be replacement r reanalysis thereof 

### by the company without extra cost. 

## STANDARD CALIBRATION GASES IN ALUMINUM CYLINDERS

# I SCOTT -MARRIN, INC.

CHRONOLOGICAL RECORD OF CERTIFIED CONCENTRATIONS

CUSTOMER: Barr Engineering co



# PURCHASE ORDER: Vbl/S Foss



# CYLINDER NUMBER: CC121446

COMPONENT 502

DATE

07/10/02

07/17/02

07/12/04



# AVERAGE

NOTES: 93.0 ppm



# 93.0 ppm



# 93.2 ppm



# 93.1 ppm

S,._UTECH\CHRONOl.OOC 6!9fi 

# CUSTOMER CODE: BARROl



# DATE: 07 

# I 13/04

# 51111

BJ\RROl 

# SCOTT-MARRIN, INC.

653 1 BOX SPRINGS BLVD. • RIVERSIDE, CA 92507 TELEPHONE(9St) 653-6780 • FAX (951) 653-2430



# REPORT OF ANALYSIS EPA PROTOCOL GAS MIXTURES



# ·o: Jason McCann DATE: June 28 2005 

# Barr Engineering Co 4700 W 77th St Minneapolis, MN 55435-4803

USTOMER ORDER NUMBER: 20050516A

# --------~---~---------------------------------------------------

# ----------------------~-----------------------------------------

COMPONENT CONCENTRATION(v/V) REFERENCE ANALVZER EXPIRATION REPLICATE ±EPA UNCERTAINTY STANDARD MAKE, MODEL, 

### &JN, DETECTION 

# DATE ANALYSIS DATA CYLINDER NO: 

# CC63443 BOVAR MODEL 922M 06/15/05 

## 06/23/05 

## .lfur Dioxide 

# 51.0 ± 0.6 ppm GMIS S/N VD922U844 06/23/07 51.0 ppm 50.9 ppm 

# CYLINDER#: CONTINUOUS 50.9 ppm 50.9 ppm 

## fitrogen 

# Balance CC12172 UV PHOTOMETRY 

## 51.0 ppm 51.0 ppm 

# ;YLINDER PRESSURE: 2000 psig @53.9ppm 

# LAST CAL DATE: 06/07/05 MEAN: 

## 51.0 ppm 50.9 ppm

m • !lftlOle/mole 

## \ = mole-\



## The above analyses were performed in accordance with Procedure G1 of the EPA Tra eability Protocol, Report Number

0 

## "A·600/R97/121, dated September 1997.

lis cylinder should not be used if the pressure 

## is less than 150 psig.



# I>.NALYST:

# ~ ?P- APPROVED:

# -.flA~r.lL:::~----------**~**

The only liability of this company lor gas which fails to comply with this analysis shall be 

### replacement or reanalysis thereof 

## by the company without extra cost.



## STANDARD CAURRATION

## AAR.F~ IN

## AlliUINII~lr:VIINn5=R.C:..

# Sill I

BARROl 

# SCOTT-MARRIN, INC.

6531 BOX SPRINGS BLVD. • RIVERSIDE, CA 

# 92507 TELEPHONE 

# (909) 653-6780 o FAX 

# (909) 653-2430



# REPORT OF ANALYSIS EPA PROTOCOL GAS MIXTURES

TO: John Stock DATE: June 26 2003 

# Barr Engineering Co 7390 OHMS Lane Edina MN 55439-2330

CUSTOMER ORDER NUMBER: 20030619A**~~~-----------------~--------------------------------------------~~**

### ----------------------------------------------------------------~·· 

## COMPONENT CONCENTRATION(v/v) REFERENCE ANALVZER EXPIRATION REPLICATE ±EPA UNCERTAINTY STANDARD MAKE, MODEL, S/N, DETECTION 

## DATE ANALYSIS DATA CYLINDER NO: 

# CC12600 CARLE INST MODEL 8000 01/18/01 06/25/03 

# Carbon Monoxide 60.4 ± 

## 0.6 

## ppm GMIS 

## SIN 8249 06/25/06 

## 60.5 ppm 60.2 ppm 

## CYLINDER#: METHANATION/FID 

### 60.5 ppm 60.2 

## ppm 

# Nitrogen 

# Balance CC85729 GAS CHROJ.iATOGRAPHY 

## 60.7 ppm 

## 60.1 ppm 

## CYLINDER PRESSURE: 2000 

# psig @ 55.4 ppm 

## LAST CAL DATE: 06/24/03 

## MEAN: 60.6 

### ppm 

## 60.2 ppm

ppm = 

### 1-UJlOle/mole 

## \ "" mole-%



## The above analyses were performed in accordance with Procedure G1 of the EPA Traceabil(ly Protocol, Report Number EPA-600/RS?/121, dated September 1997. / This cylinder should not be used if the pressure is less than 150 psig. 

# I

ANALYST:

__

# ~~----~~~~~==~~, 

# _________ APPROVED:

____

# ~~~----------------------- M.J.MONSON

The only llabHity of this company for gas which fails to comply With this analysis shall be replacement or reana ysis thereof by the company without extra cost. 

## STANDARD CALIBRATION GASES IN ALUMINUM CYLINDERS

# Ellll

BARROl 

# SCOTT-MARRIN, INC.

6531 BOX SPRINGS BLVD. • RIVERSIDE, CA 92507 TELEPHONE (951) 653-6780 • FAX (951) 653-2430



# REPORT OF ANALYSIS EPA PROTOCOL GAS MIXTURES

TO: Nicholas Shreve Barr Engineering Co 

# 7390 OHMS Lane DATE: December 

# 22 2004

Edina 

# MN 55439-2330

CUSTOMER ORDER NUMBER: 

# 20041123ANRS

COMPONENT CONCENTRATION(v/v) REFERENCE ANALYZER EXPIRATION REPLICATE "'EPA UNCERTAINTY STANDARD MAKE, MODEL, S/N, DETECTION 

## DATE ANALYSIS DATA CYLINDER NO: 

# CC78171 CARLE IHST MODEL 8000 12/14/04 12/21/04 

## Carbon Monoxide 34. 1 :t 

## 0.3 ppm GMIS 

## S/N 8249 12/21/07 34.0 

### ppm 34.2 

### ppm 

## CYLIIIDER 

## #: METHANATION/FID 34.0 

### ppm 

## 34.1 

## ppm 

## Nitrogen Balance CA03684 

## GAS CHROMATOGRAPHY 34.1 

## ppm 

## 34.1 ppm 

## CYLIIIDER PRESSURE: 2000 ps ig @54.5 ppm 

## LAST CAL DATE: 12/13/04 

## MEAII: 34.0 

## ppm 34.1 ppm

ppm 

## = IJiti.Ole/mole % 

## = mole-\



## The above analyses were performed in accordance with Procedure G1 of the EPA Trace bility Protocol, Report Number EPA-600/R97/121, dated September 1997. This cylinder should not be used 

# if the pressure is less than 150 psig.

# ANALYST:--~~-'-~"'-":...:...;""--'....:..:'--.=::.....;·:;_··--- APPROVED: 

## M.J.MONSON

The only liability of this company tor gas which fails 10 comply with this analysis shall be replacement or eana\ysls thereof 

## by the company without extra cost.



## STANDARD CALIBRATION GASES IN ALUMIIIUM CYLINDERS

# NATIONAL SPECIALTY GASES 630 UNITED DRIVE DURHAM, NC 27713



# CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS MIXTURE

Customer: Twin City Oxygen Reference# 88-89053
NSGPO# 4271165 Certification Date: 02/19/04
Customer PO# 42921 Expiration Date: 02/19/07 Cylinder# cC47n7

. Pressure, psig* 2000


# ANALYTICAL INFORMATION
METHOD: This standard was analyzed 

## according 

# to EPA Traceability Protocol 

## for A={ 

## and Certification of Ga:se<l\lS 

## Callbration standards: Procedure G1 (September 1997)


# ANAL Y2ED CYLINDER Components

Methane

Balance

- Air

REFERENCE STANDARD Type/SRM Sample#
GMIS (Traceable to SRM # 2751 )

INSTRUMENTATION Instrument/Model/Serial#

Rosemount 400A THC 00335 Certified Concentratjon

90.4 ppm

Cylinder#

CC36118

Last Date Calibrated

01/23/04 AnaMical Accuracy**

+/-1%

Concentration

100.3 ppm CH4/AIR

Analytical Method

Flame Ionization Detector

Analyst: -------,-----J::.;e:::.r.::;em=y.:..K:;:e:::.nw:.:.o:::rt:::.h,..y_

This report states accurately the results of the investigation made upon the material submitted to the analytical laboratory. Every effort has been made to determine objectively the information requested. However, in connection with this report, National Specialty Gases shall have no liability in excess of established charge for this service. Assayed at National Specialty Gases, 630 United Drive, Durham, NC 2n13 (919) 544-3772

•oo not use this 

## standard When cylinder pressure is below 150 pslg. 

## -Analytical accuracy includes typical known error sources 

## which. at least, include precision of the analytical 

# instUmenl NSG020149L

# NATIONAL SPECIALTY GASES 630 UNITED DRIVE DURHAM, NC 27713



# CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS MIXTURE

Customer:
NSG PO#
Customer PO# Twin City Oxygen
3558412
39278 Cylinder# CC2937
ANALYTICAL INFORMATION 

# Reference# 88-78516
Certification Date: 08/01/02 Expiration Date: 08/01/05 -Pressure, psig* 2000

METHOD: This standard was analyzed according to EPA Traceability Prctocol for Assay and certification of Gaseous Calibration Standards: Procedure G-1: September 1997.


# ANALVZED CYLINDER Components

Methane

Balance

- Air

REFERENCE STANDARD Type/SRM Sample#
GMIS (Traceable to SRM # 2751 )

INSTRUMENTATION Instrument/Model/Serial #

Rosemount 400A THC 00335 Certified Concentration

46.5 PPM

Cylinder#

CC36118

Last Date Calibrated

07/16/02 Analytical Accuracy**



# +/-1%

Concentration

100.3 ppm CH4/AIR

Analytical Method

Flame Ionization Detector

Analyst: ------------'-Am=y'-J"-''-'P-'r"'ok'-"oOJ:p'-"o"'w"'ic:::z:_
This report states accurately the results of the investigation made upon the material submitted to the analytical laboratory. Every effort has been made to determine objectively the information requested. However, in connection with this report, National Specialty Gases shall have no liability in excess of established charge for this service. Assayed at National Specialty Gases, 630 United Drive, Durham, NC 27713 (919) 544-3772

*oo not use this standard when cylinder pressure is below 150 psig. **Analytical accuracy includes typical known error sources which, at least, include precision of the analytical instrument 

# NSG 020149L

# CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS MIXTURE

Customer: Twin City Oxygen Reference# 88-91148 NSGPO# 4424096 Certification Date: 06/15/04
Customer PO# 43778 Expiration Date: 06/15/07 Cylinder# SG9165492BAL Pressure, psig* 2000 

# ANALYTICAL INFORMATION

METHOD: This standard was analyzed according to EPA Traceabirrty Protocol for Assay and Certification of Gaseous calibration Standards: Procedure G1 (September 1997) 

# ANALYZED CYLINDER Components

Methane

Balance

- Air

REFERENCE STANDARD Type/SRM Sample# GMIS ( Traceable to SRM # 2750 )

INSTRUMENTATION I nstrument/Modei/Serial #

Rosemount 400A THC 00335 Certified Concentration

30.2 ppm

Cylinder#

CC16937

Last Date Calibrated

06/08/04 Analytical Accuracy••

+/-1%



# Concentration
51.57 ppm CH4/AIR

Analytical Method

Flame Ionization Detector

Analyst: -----------'-'R"'ic:..::ha::.rd:::...::S£yk.::e::::s_
This report states accurately the results of the investigation made upon the material submitted to the analytical laboratory. Every effort has been made to determine objectively the information requested. However, in connection with this report, National Specialty Gases shall have no liability in excess of established charge for this service. Assayed at National Specialty Gases, 630 United Drive, Durham, NC 27713 (919) 544-3772

"'Do not use this standard when cylinder pressure is below 150 psig. **Analytical accuracy Includes typical known error sources 

## which, at least, include precision of the analytical instrument. 

# NSG 020149L

# .. 1111

BARROl 

# SCOTT-MARRIN, INC

. 6531 BOX SPRINGS BLVD. • RIVERSIDE. CA 92507 TELEPHONE (909) 653·6780 • FAX (909) 653-2430



# REPORT OF ANALYSIS EPA PROTOCOL GAS MIXTURES

TO: Sam Foss DATE: August 13 2004 

# Barr Engineering Co 7390 OHMS Lane Edina MN 55439-2330

CUSTOMER ORDER NUMBER: VBL/S Foss**-..-.~.~-** .... 

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## COMPONENT CONCENTRATION(v/V) REFERENCE ANALVZER EXPIRATION REPLICATE "EPA UNCERTAINTY STANDARD MAKE, MODEL, S/N, DETECTION 

## DATE ANALYSIS DATA CYLINDER NO: 

# CC12009 VARIAN MODEL 1860 TCD 08/10/04 

## Carbon Dioxide 5.01 :t. 

## 0.05% GMIS S/N NONE 

## OB/10/07 

## 5.00% 

## CYLINDER#: THERMAL CONDUCTIVITY 5.01%-


### CC42814 GAS CHROMATOGRAPHY 5.03%


## @B.OB 

## LAST CAL DATE: 07/2B/04 

## MEAN: 5.01%



### VARIAN MODEL 1860 TCD 

### 08/12/04 

## Oxygen 19.97 " 0.20% GMIS 5/N NONE 

### 08/12/01 

## 19.98% 

## CYLINDER#: THERMAL CONDUCTIVITY 19.97% 

## Nitrogen Balance CA03201 

## GAS**CHROMATOGRAPH~** 

### 19.96% 

## CYLINDER PRESSURE: 2000 

## psig @ 24.B2% 

## LAST CAL DATE: 07/23/04 

## MEAN: 19.97%



## ppm =**~ole/mole** 

## % 

## =mole-%



## The above analyses were performed in accordance wtth Procedure G1 of the EPA Trac ability Protocol, Report Number EPA·600/R97/121, dated Sep ember 1997. This cylinder sh uld o e d if the pressure is less than 150 psig.

The only liability of this company for gas which fails to comply with lhis analysis shall be replacement or reanalysis thereof by the company without extra cost.


## STANDARD CALIBRATION GASES IN ALUMINUM CYLINDERS

# 51111

BARROl 

# SCOTT-MARRIN, INC.

6531 BOX SPRINGS BLVD. • RIVERSIDE, CA 92507 TELEPHONE (909l 653-67BO o 

# FAX (909) 653-2430



# REPORT OF ANALYSIS EPA PROTOCOL GAS MIXTURES

TO: Sam Foss 

## DATE: April 

# 16 2004 

# Barr Engineering Co 7390 OHMS Lane Edina MN 55439-2330

CUSTOMER ORDER NUMBER: 200402l0ASMF2

COMPONENT CONCENTRATION(v/V) REFERENCE +EPA UNCERTAINTY STANDARD CYLINDER NO: 

# CC12898

Carbon Dioxide 9.05 

## ± 0. 03% GMIS 

## CYLINDER#: CC51172
@ 

## 17.98%



## Oxygen 9.07 

## ± 0.05% GMIS 

## CYLINDER#: 

# Nitrogen Balance CC81204 

## CYLINDER PRESSURE: 2000 

# psig @ 

## 9. 88%

ppm 

### = JUYIOle/mole 

### % 

# = mole-% 

## ANALVZER EXPIRATION REPLICATE
MAKE, MODEL., SlN, DETECTION 

## DATE ANALYSIS DATA

VARIAN MODEL 1860 TCD 04/12/04 

## SIN NONE 04/12/07 9.06% 

## THERMAL CONDUCTIVITY 9.05% 

## GAS CHROMATOGRAPHY 9.05% 

## LAST CAL DATE: 03/29/04 

## MEAN: 9.05%



## VARIAN MODEL 1860 TCD 04/15/04 

## S/N NONE 04/15/07 9.08% THERMAL CONDUCTIVITY 9.08% 

## GAS CHROMATOGRAPHY 9.05% 

## LAST CAL DATE: 03/25/04 

## MEAN: 9.07%



## The above analyses were performed in accordance with Procedure G1 of the EPA Traceability Protocol, Report Number EPA-600/R97/121, dated Se mber 1997. This cylinder shou d if the pressure is less than 150 psig.

The only liability of1his company for gas wh·rch fails to comply with this analysis shall be replacement or reanalysis thereof by the company without extra cost.


## STANDARD CALIBRATION GASES IN ALUMINUM CYLINDERS, 

### .. -:: 

# VISIBLE EMISSIONS EVALUATOR

This is to certify' that

met)he specifications of Federal Reference Method 9 ond.qualified OS 0 

# visible emissions evoluqtor. Maxienum deviation on white and block smoke did not exceed7;5% opacity and no single error exceeding 15%ppocity was incurred during the certification test conducted by Eastern Technical Associates of Raleigh, North Carolina. This certificate is valid for six months rrdm'date of issue.

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# I I I IOPI:<.._'-'Ci.._ING...,..ceo..-..-..FQ.._,..._.._,._.JCE&"'.;;,vJRCL"'Juoe-99TestDate(s):711212005ProcessEquipmentNumba/Identification:Line4WasteGasstack(SV118)CompanyName:U.S.MinnesotaOreOperations-(Minntac)Equipment&OperatingData1.ProcessEquipmentDescription:Ste11Alomerator-Line4WasteGasStackPM/Fiuorides/S02,CO,VOC2.Weretheprocessandcontrolequipmentoperatedconsistentwithnormaloperatingprocedure?YESNO3.Includecopyofproductionrecordsorinstrumentswhichindicatesrateofproductionoroperationoftheequipment,i.e.unitsperhour,poundsperhour,pressure,airflow,etc.4.Date(s)andprocedure(s)oflastmaintenance/cleaningwithin6monthsRemainsunchangedfromTestPlanLine4downforannalmajorrepairfromMay31throughJune21-seeattachedR.Pottse-mail5.Processrate(amountofrawmaterialorfinishedproductperhour,wetordrybasis)whilecombusting(listfueltype(s)andratiosasapp<::r:.o.t:p:.:ria:ot:.:e'-)---------------------------------ProcessParameter:listtypeandunitsRun1Run2Run3Greenballfeedrate,longtonsperhour(LTPH)588584595FiredQroductionrate,(LTPH)465463472HeatInput(106Britishthermalunits/hour)Wood90.6185.8394.91HeatInput(106British thermalunits/hour)Gas123.8898.29111.38HeatInput(106British thermalunits/hour)Total151.29126.38142.196.Summarizecontrolequipmentoperatingdatadocumentedduringtesting.Valuesreportedshouldreflectmaximum,minimum,averages,orasapprovedinthetestplan.(SeetestplanandaPProvalletter)ExamplesofAPCequipmentandparametersgenerallymonitoredMonitorasspecifiedinthetestplanapprovalletter.•Scrubb&(listtypeofscrubb&}:AP(in.w.c.)andfeedrate•Baghouse,Cyclone,andMulti-clone:AP(in.w.c.)(!WTilandvsig_)•andThermal•Nmnberandidentityofoperatingelectrostaticprecipitatorfield(s)Incinaator:eFt=po,ru.JAPCequipmentandparametermonitoreRun1Run2Run3WetScrubber,dP(in.w.c.)-average11.0911.2011.21WetScrubber,feedrate(gpm)-average298529912985Listpollutant&averagingbasi!i-SbouldreflectpermitRun1Run2Run3ContinuousOpacityMonitor(listhourlyaverage)NANAMonitor(listaveragingbasis):NANAMonitor(listaveragingbasis):NAAbbreviatioDs:APC-airpollutioncontrollbs.-poundsgpm.-gallonspaminutepsig-pressurepersquareinchgaugein.w.c.-inchesofwatercolumnM-pressuredropNOTE:Thisformprovidesonlya:;ummaryoftheoperatingCJJnditionsduringtheperformancetesLAdditionalandmoredetailedrecordsarerequiredtomeettherequirementsofMinn.R.7017.2035.ThisformistobesubmittedtiSpartoftfJeperformancetestreportto:North,Metro,orSouthDistrict,PerformanceTestCoordinator,MNPollutionControlAgency,520LafayetteRd.,St.Paul,MNPMRun459458847146393.9695.22102.0995.76128.92146.69F-Run4PMRun411.2311.0029852987Run3Run3!JIRunDateDATACOLLECTEDDURINGSTACKTESTINGLine4July12,2005AcidPelletProductionFeedRatesLTPHProd.FuelDataPollutantStartEndGreen1·RateWoodIGasMBTUHITotalTestedforTimeTimeballToGrateLTPHMBTUHIGrateIKilnIMBTUHWasteGasStackLine417/12/2005PM-Qases10:0011:09588.39 522.22464.7890.610.00123.88214.4927/12/2005PM-gases11:5513:06584.25520.22463.0085.830.0098.29184.1237/12/2005PM-gases16:0017:16595.29530.52472.1694.910.00111.38206.2947/12/2005PM19:2520:21587.65520.40463.1693.360.00102.09195.4547/12/2005Fluoride17:5519:05594.35528.66470.5195.220.0095.76190.98---WetScrubberDPIGPM11.09298511.20299111.21298511.00298711.232985AVG589.99524.40466.6490.450.00106.28201.6411.152987Basedon10-minuteaveragesthatapproximatelyalignwiththetesttimes.Note:Gasmeterwasinerror-read17.67%low.Correctedvaluesareshown

# Run Date 

# Data Collected During Stack Testing Line 4 July 12, 2005 Acid Pellet Production

Wood Moisture, sulfur and BTU Analyses As Received Dry basis Start End 

# % % BTU 

# % BTU Time Time 

# H 2 

# 0 

# s per lb 

# s per lb

Waste 

# Gas Stack Line 4


# 1 7/12/2005 10:00 11:09 11.8 0.021 7576.48 0.024 8470.50
2 7/12/2005 11:55 13:06 9.2 0.050 7140.29 0.055 7797.20
3 7/12/2005 16:00 17:16 4.6 0.022 7767.11 0.023 8124.40
4 7/12/2005 19:25 20:21 6 0.031 7615.38 0.033 8072.30 4 7/12/2005 17:55 19:05 4.6 0.022 7767.11 0.023 8124.40 AVG 

# 7.24 0.029 7573.27 0.034 8130.70

# Tom Kuchinski

From: 

# Sent: To: 

# Cc: Subject: Raymond Potts [RPotts@uss.com] Thursday, August 04, 2005 1 :07 PM Tom Kuchinski Chrissy L Bartovich; Richard Berg Re: Line 4 maintenance and repairs

Line 4 was down for its "scheduled" annual major repair from May 31 through June 21. The entire line including the wet scrubber and cooler areas received attention (repairs) during this shutdown.


# Ray

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# Tom Kuchinski

From: 

# Sent: To: 

# Subject: Chrissy L Bartovich [clbartovich@uss.com] Wednesday, June 29, 2005 10:53 AM Richard Berg RE: Line 4 Initial Performance Test



# Forwarded by Chrissy L Bartovich/Minntac/USS on 06/29/2005 10:54 AM



# <Clbartovich®uss.corn> "Place, Andrew" <Andrew.Place®sta

te.mn.us> <Robert.Beresford®state.mn.us> To: Chrissy L 

# Bartovich

cc: 11 

# Beresford, Robert"
Subject: RE: Line 4 Initial Performance Test 05/20/2005 02:49 PM

Chrissy, that sounds fine. Keep me posted. I would agree that unless there is some major modification to the test plan, or, the testing gets postponed for an indefinite amount of time, we can communicate via email and avoid redoing the complete testing process.

Talk to you later and have a good weekend.
-----Original Message----- From: Chrissy L Bartovich [mailto:clbartovich®uss.com] Sent: Thursday, May 19, 2005 1:34 PM To: Place, Andrew Cc: Robert.Beresford®state.mn.us; Raymond Potts Subject: Line 4 Initial Performance Test



# Hi Andy,

It looks like we won't be doing the initial performance testing on Line 4 this week. We are having difficulty operating the line. This line will be going down at the end of the month for a 16 day major repair, It looks like it would be late June or early July when we would be able to conduct the initial performance test. We need to do this test by July 31 as a part of our pending PSD permit.

I'm assuming we can work this the same as the SV054

- an email notification when we are able to test rather than going through the entire process again. If you have any questions please let me know.
Thanks, Chrissy

1

# Message Page 1 of 1



# Tom Kuchinski

From: Tom Kuchinski
Sent: Thursday, May 12, 2005 9:08AM
To: Richard Berg Subject: FW: Test Plan Approval for 5/16/05 test and 5/31/05 GEMS cert.
Attachments: CERTIFICATION PAGE.doc; MICROFICHE CD SUBMITTALS.doc; OPERATING DATA SUMMARY FOR COMBUSTION SOURCES.doc; OPERATING DATA SUMMARY FOR PROCESS SOURCES.doc; USS-Minn, SV1 03, SV118, SV127, 5-05.doc; USS-Minn, SV144&151, GEMS RATA, 5-05.doc

From: Place, Andrew [mailto:Andrew.Piace@state.mn.us] Sent: Thursday, May 12, 2005 9:02AM To: Chrissy L Bartovich 

# Cc: Tom Kuchinski; Beresford, Robert Subject: Test Plan Approval for 5/16/05 test and 5/31/05 CEMS cert.
Chrissy,

The test plan approval forms associated with the upcoming performance test on Agglomerator Lines 3, 4, and 5 (SV103, SV118, & SV127) on May 16th, and initial GEMS RATA on Agglomerator Lines 6 and 7 (SV144 and SV151) on May 31st, are attached to this message. They include the Test Plan Approvals, Operating Data Summarys, Certifications, and Microfiche/CO Submittals. Please use the forms attached as they have recently been updated. Also, please print a copy of this email message and include it in the report for each test with the approval letter

. The email provides authentication for the test plan approvals.

If you have problems with any of the attachments feel free to contact me. Additional forms are provided at .wWWJJr;;a.state.mn.us/air/performan<;<ete.§.l.html

Sincerely,

Andy Place 

# Performance Test Coordinator Minnesota Pollution Control Agency 520 Lafayette Road St. Paul, MN 55155-4194 (651) 296-7169



# 8/5/2005

# Facility Name: US Steel-Minnesota Ore Operations Facility Contact: Chrissy Bartovich Address: Minntac Plant, P.O. Box 417, 8819 Old Highway 169, Mountaio Iron, MN 55768 Fax: (218)749-7360 Emission Unit(s): Agglomerator Lines 3, 4, and 5 (SV103, SV118 and SV127) Scheduled For: May 16, 2005, at your Facility located in 

# Mountain Iron, Minnesota. AQ#26A

Your test plan submitted on Aprill8, 2005, and discussed on May 11, 2005, has been approved by the Minnesota Pollution Control Agency (MPCA) as follows: 

# 0 Shortened test notification approved 

# 0 Test plan approved without modification


# [8J Test plan approved with the following provisions:

Equipment should be operated at maximum capacity during testiog. Include process equipment and control equipment operatiog rates on the Operating Data Summary form.

Include io the final testreport(s) the full reference method data record (strip chart and/or datalogger output) used to calculate emissions. The data record should ioclude calibration values for any instrumental analyzer used for emissions compliance testing.

For SV103, the public notice process has been conducted for Air Emission Permit No. 13700005-004, which contains an Opacity Standard Adjustment ofless than or equal to 40 % opacity as authorized by Minn. R. 7011.0120, subp. 3, for SVJ 03 Lioe 3 Waste Gas Stack (Agglomerator Line 3). This Opacity Standard Adjustment will become effective upon permit issuance and extend until Startup of the upgraded particulate pollution control equipment at SV103. This upgrade is required by the permit no later than October 30, 2006. The particulate control equipment upgrade must enable the Permittee to comply with the 0.01 gr/dscf emission limit for Front-HalfParticulate Matter in Table 1 of 40 CFR 63, Subpart RRRRR, and is expected to reduce opacity emissions to below 20%. The MPCA understands that to demonstrate compliance with the 

# AO% opacity limit for SV103, the unit,
at the time of testing, may be out of compliance with the current 20% limit. This exemption from current permit conditions applies only for the duration of the upcoming test.

Attached Forms:



# [8J Operating Data Summary- Combustion Sources 

# [8J Operating Data Summary- Process Sources 

# I:8J Certifications Form 

# 0 Operating Data Summary- Waste Combustors 

# 0 Operating Data Summary- Asphalt Plants 

# [8J Microfiche/CD-ROM Submittal Form

Note: Forms are also available at: www.pca.state.mn.us/air/performancetest.html


# Approved by: Date: May 12, 2005

# Andrew Place Performance Test Coordinator Compliance and Enforcement Section Industrial Division

Please contact me at (651) 296-7169 if 

# you have any questions regarding this approval.

Please be aware that enforcement action will be taken for performance test failures indicating emissions above applicable limits (excess actual emissions to the environment). Failures commonly result in assessment of a monetary penalty. Upon the first test failure, the Company should take immediate measures to minimize emissions. The measures taken should be documented, as 

# they will become part of the record of corrective actions.

Hard Copy Peiformance Test Reports and Microfiche or CD Copy submittals will be addressed to: Compliance Tracking Coordinator, Compliance and Enforcement Unit, Industrial Division, Minnesota Pollution Control Agency, 520 Lafayette Road North, St. Paul, Minnesota 55155-4194

cc: Tom Kuchinski, Barr Engineering, Minneapolis (email) Bob Beresford, MPCA, Duluth (email) AQ Correspondence File No. 26A

## U. S. Steel Corporation Minnesota Ore Operations P.O. Box 417 Mt. Iron, MN 55768



# Aprill5,2005



# Mr. Andrew Place North District, Major Facilities Minnesota Pollution Control Agency 520 Lafayette Road St. Paul, Minnesota 55155-3898

RE: USS -Minnesota Ore Operations (Minntac) Notification of Testing and Test Plan

Dear Andrew,

This document is the Notification of Testing and Test Plan for performance tests to be conducted during the week of May 16, 2005. Tests will be performed on the Agglomerator Lines 3, 4 and 5
waste gas stacks (SV103, SV118 and SV127 respectively).



# TEST PLAN

Part 1. General Information

(1) Name and address of the emission facility.

U.S. Steel- Minnesota Ore Operations Minntac Plant P.O. Box417 8819 Old Hwy 169 Mountain Iron, Minnesota 55768

(2) Name, title and telephone number of contact person at the emission facility.

Chrissy Bartovich Environmental Control Engineer Voice phone 218-749-7364 Fax phone 218-749-7360 Electronic mail: clbartovich@uss.com

(3) Permit number or name of other applicable document.

Pending Air Emissions Permit 13 700005-004 (PSD Permit)

( 4) Reason for testing.

Initial performance test per the pending permit.

- 1-

# ( 5) Schematic drawing of the stacks and sample ports.

Enclosed herein.

a) Location of Plant

Within the corporate limits of the city of Mountain Iron, MN.

b) Name, contact person, and telephone number for testing company

Barr Engineering, Minneapolis, MN. Richard Berg (952) 832-2787



# Part 2. Testing Requirements

(1) List ofpollutsnts to be tested, the emission limit for each po!lutsnt and the applicable rule or regulation for the emission limit.

Group 9 Agglomerator Line 

# 3 & 

# Group 10 Agglomerator Line 4 and Line 

# 5- PM, 

# PMw, Opacity, CO, S0 2 , 

# VOC, and Fluoride

There are no permitted emissions limits for PM 10 

# CO, VOC and Fluoride until the PSD permit is in effect. The following emissions limits are in effect.

Particulate Matter (PM) Minn. R 7011.0610 subp. l(A)(l) 0.30 grains per dry stsndard cubic foot, or the less stringent of either Minn. R 7011.0730 or Minn. 

# R. 7011.0735

Opacity

- Line 3 only Minn. R 7011.0120 subp. 2(B) Less than or equal to 40%

Opacity

- Line 4 and Line 5 Minn. R 7011.0610 subp. l(A)(2) Less than or equal to 20% except for one six-minute period per hour of not more than 60% opacity.

(2) Description of procedure for fuel sampling and analysis, where applicable.



# If biomass is used as a fuel during the test, wood will be sampled and analyzed for heat and sulfur content.



# Part 3. Operating Conditions

(1) List the process or operating rate and conditions of the process equipment and the air pollution control equipment for the test.

All tests will be performed while the associated process equipment is operating at maximum capacity and all control equipment will be operated normally.

-2-

# Green ball feed rate range is 280 to 350 LTPH on Line 3. Green ball feed rate range is 525 to 625 LTPH for Lines 4 and 5. Fuel will be either a blend of 

# natural gas and wood or 100% gas during the 

# tests.

(2) Explanation of why the proposed conditions are considered 

# to be in accordance with Part 7017.2025, Subpart 2, for required testing conditions.

The statement about the assumption of worst case conditions in the cited subpart applies.

(3) List the range of process or operating rates for this emission nnit.

The minimum process rate is zero. The maximum green ball feed process rate is approximately 350 LTPH for Line 3 and 625 LTPH for Lines 4 and 5.

( 4) Descriptions of how air pollution control and process equipment will 

# be monitored.

The emission control nnits will 

# be monitored for pressure drop and water flow during all tests.



# Part 4. Test Methods

(1) List of the methods to be 

# used to determine the emission rate of each pollutant.

Test Port Location Determination of velocity and volumetric flow Determination of gas molecular weight Determination of moisture content Determination of PM Determination of Condensable PM Determination ofPM 10 

# Determination of CO concentration Determination ofVOC concentration Determination of SO, concentration Determination of Fluoride concentration Visual Determination of 

# the Opacity of Emissions EPA Method 1 EPAMethod2 EPAMethod3A EPAMethod4 EPAMethod5 EPA Method 202 EPA Method201A EPA Method 10 EPA Method 25A EPA Method 6C EPA Method 13B EPAMethod9

Note- both filterable and condensable particulate matter will 

# be measured. PM 10 

# measurements (Method 201A) cannot be made at the waste gas staclJ; because of high moisture content in the gas stream. PM 10 

# will be determined by adding the inorganic condensible particulates to the 

# dry plus organic particulates on Lines 4 

# & 5. PM 10 

# will be conducted on Line 3 only.

(2) Number oftest runs, length of the test runs, and sampling rate for each method.

3 one-hour test runs except for Methods 1, 2 and 9 Method 9 will be 1 one-hour observation performed in conjunction with one Method 5
test run.

-3-

# (3) Reference to any compliance document, federal regulation, or Minnesota rule or statute requiring use of specific methods or procedures.

Not applicable

( 4) Summary of reasons for proposing to use alternative or equivalent method.

None proposed

( 5) For test methods other than reference methods, statement of the detection limit and the degree of accuracy of that method at the expected emission rate and under the conditions of the performance test.

None applicable



# Test Schedule and Pretest Meeting

The testing is scheduled to occur dUring the week of May 17-20, 2005. At the preference of the MPCA, we would suggest the pretest meeting could occur no less than 7 days before the testing begins and be conducted via telephone.


# Closing Remarks



# If

there are any questions or comments on the information given in this document, please
contact me at the telephone numbers listed above.

Chrissy Barto tch Environmental Control Engineer

Enclosures: STEP! AGG WG.doc STEP2 AGG WG.doc

CERTIFIED MAIL# 7003 2260 0000 2381 8071

cc: Robert Beresford, MPCA- Duluth Regional Office Hongming Jiang, MPCA North District Major Facilities Richard Berg- Barr Engineering Ray Potts- Minntac Cory Bird- Minntac Ron Braski- Minntac

-4-

# 10'-0"

. 

# j. .j TOP OF STACK EL. 1212'-0"



# 13 '-0"



# -.---+-X --+--rl'----<c----Four Sample Points @ 90° 

# 5 '-0" ROOF

__________**-L~**



# Elevation View

1. 

# Emission Source Number- SV 103 (Old Source Number 8.3) 2. Emission Unit Nurnber-223, 224, 225, 226 

# 68'-0"



# 35' -0"

STRUCTURAL SUPPORT EL. 1096'-0"



# STEP I AGGLOMERATOR WASTE GAS

3. Plant Equipment Number- 242-03:2; 261-03-1; 252-03-1; 262-03-1 4. Stack Diameter- 10 '-0" 5. Stack Design Gas 

# Velocity- 56.8 FPS. 6. Stack Design Volume- 267,775 CFM. 7. Stack Design Temperature- 200°F. 8. Pollutants- Particulates and Combustion Emissions

Step I Agglomerator Minnesota Ore Operations Minntac, Mt. Iron, MN

# 5'-0" ROOF



# FAN 

# -·- 15' -0"**~** 

# Steel 14'-0" Liner

; ; 

# ; 

# '



# _ ........ -········f,;

...... -

; ; 

# ; 

# ' ; 

# ; 

# ' ; ; ; ; 

# i 

# ' ; ; ; ; 

# i



# Elevation View 1. Emission Source Numbers- Line 4 SV 118, Line 5 SV 127

# ~I Top of Stack El. 1236'-0"



# 34. -0"

52' -0"

53 '-5"

Bottom /Steel EL 

# 1097"-5"



# STEP II AGGLOMERATOR WASTE GAS

2. Emission Unit Number- Line 4 EU 259, 260, 261, 262 Line 5 EU 280, 282,282, 283 3. Plant Equipment Number- 242; 261; 252; 262 

# 4. Stack Diameter- 15.0' with 14'-0" diameter fiberglass liner 5. Stack Design Gas Velocity- 56.3 FPS 6. Stack Design Gas Volume- 591,000 CFM 7. Stack Design Gas Temperature- 125 to 150'F

s:\air\stacks\STEP 2 AGG WG.doc Step IT Agglomerator Minnesota Ore Operations Minntac, Mt. Iron, MN

# Minnesota Pollution Control Agency
Andrew Place- Performance Test Coordinator Hongming Jiang- Permit Engineer

U.S. Steel Corporation- Minnesota Ore Operations 

# Project Participants

Larry Salmela

- Department Manager Environmental Control Chrissy Bartovich

- Environmental Control Engineer Ray Potts- Environmental Control Engineer
Ron Braski

- Agglomerator Coordination

Barr Engineering Company
Tim Russell -Vice President/Chemical Engineer
Richard Berg- Project Manager
Tom Kuchinski- Senior Air Quality Technician/Team Leader

Dan Koschak

- Environmental Engineering Technician

Jon Stock- Technician
Bill Scott- Technician

#2369927001



# J-1