### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

10641 Cambria Cogen B2 

### coal refuse (culm or gob)Fuel Type 2 Fuel Type 3 Other Fuel Description



### other natural gasEIA

Facility Code Facility Name Boiler ID Basis An alyte



### 10641 Cambria Cogen B2 As Received Higher Heating Value 

### 10641 Cambria Cogen B2 As Received % Moisture 

### 10641 Cambria Cogen B2 As Received % Ash 

### 10641 Cambria Cogen B2 As Received % Sulfur 

### 10641 Cambria Cogen B2 Dry basis Higher Heating Value 

### 10641 Cambria Cogen B2 Dry basis % Ash 

### 10641 Cambria Cogen B2 Dry basis % Sulfur 

### 10641 Cambria Cogen B2 Dry basis Antim ony 

### 10641 Cambria Cogen B2 Dry basis Arsenic 

### 10641 Cambria Cogen B2 Dry basis Beryllium 

### 10641 Cambria Cogen B2 Dry basis Cadmium 

### 10641 Cambria Cogen B2 Dry basis Chlorine 

### 10641 Cambria Cogen B2 Dry basis Chromium 

### 10641 Cambria Cogen B2 Dry basis Cobalt 

### 10641 Cambria Cogen B2 Dry basis Fluorine 

### 10641 Cambria Cogen B2 Dry basis Lead 

### 10641 Cambria Cogen B2 Dry basis Manganese 

### 10641 Cambria Cogen B2 Dry basis Mercury 

### 10641 Cambria Cogen B2 Dry basis Nickel 

### 10641 Cambria Cogen B2 Dry basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) 

### D5865 D2961 D3302 D3173 D3174 D4239 D5865 D3174 D4239 D3683 D3684 D3684 Mod D3683 D3684 D3684 Mod D3683 D3684 D3684 Mod D3683 D3684 D3684 Mod D3683 D3684 D3684 Mod D3683 D3684 D3684 Mod D3683 D3684 D3684 Mod D3761 D3683 D3684 D3684 Mod D3683 D3684 D3684 Mod D3683 D3684 D3684 Mod D3683 D3684 D3684 Mod D3683 D3684 D3684 ModEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 10641 Cambria Cogen B2 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units M5/29 R1 

### 5/10/2010 5/10/2010 7689.00 Btu/lb M5/29 R2, M27/28 R1

5/11/2010 5/11/2010 8194.00 Btu/lb M5/29 R3, M27/28R25/11/2010 5/11/2010 8038.00 Btu/lb M30B R1 

### 5/18/2010 5/18/2010 8175.00 Btu/lb M30B R2 

### 5/18/2010 5/18/2010 7922.00 Btu/lb Fuel Testing Results

### Mercury and non-mercury metalic HAPs

% Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 2.35 43.18 1.72 7874 Btu/lb 44.21 1.76 3.09 39.46 1.81 8455 Btu/lb 40.72 1.87 3.09 40.29 1.77 8294 Btu/lb 41.57 1.83 3.30 39.50 1.80 8484.00 Btu/lb 40.85 1.86 3.35 39.65 1.92 8196.00 Btu/lb 41.34 1.99Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 899 ppm 510.78 ppb <4.85 ppm 17.48 ppm <0.04 965 ppm 513.02 ppb <4.87 ppm 25.21 ppm <0.04 0.11 % 575.9 ppb <4.75 ppm 25.4 ppm <0.04 982.00 ppm 405.020 ppb <4.97 ppm 27.10 ppm <0.04 0.10 % 540.740 ppb <4.67 ppm 25.92 ppm <0.04Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### ppm <0.05 ppm 58 ppm 26.5 ppm 53 ppm ppm <0.05 ppm 47.4 ppm 24.8 ppm 35.5 ppm ppm <0.05 ppm 45.1 ppm 25.3 ppm 31.9 ppm ppm <0.05 ppm 48.60 ppm 27.00 ppm 31.30 ppm ppm <0.05 ppm 52.40 ppm 27.60 ppm 30.60 ppmNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 16.1 ppm 1.7 ppm 167 ppm <0.25 ppm 2.35 17.2 ppm 1.2 ppm 249 ppm <0.25 ppm 3.09 14.3 ppm 1.14 ppm 148 ppm <0.25 ppm 3.09 14.00 ppm 1.25 ppm 161.00 ppm <0.25 ppm 3.30 16.40 ppm 1.57 ppm 143.00 ppm <0.25 ppm 3.35 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 

### 19.54 44.21 36.25 45.27 2.63 0.79 1.76 19.92 40.72 39.36 47.95 2.83 0.82 1.87 20.27 41.57 38.16 47.35 2.82 0.8 1.83 21.06 40.85 38.09 47.89 3.05 0.90 1.86 20.75 41.34 37.91 47.01 3.10 0.83 1.99 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen



### 5.34 5.81 5.63 5.43 5.73EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 10641 Cambria Cogen B2 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units M 6C, 7E, 320 R1 

### 5/18/2010 5/18/2010 8175.00 Btu/lb M 6C, 7E, 320 R2 5/18/2010 5/18/2010 7922.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 3.30 39.50 1.80 8484.00 Btu/lb 40.85 1.86 3.35 39.65 1.92 8196.00 Btu/lb 41.34 1.99Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 982.00 ppm 405.020 ppb <4.97 ppm 27.10 ppm <0.04 0.10 % 540.740 ppb <4.67 ppm 25.92 ppm <0.04Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### ppm <0.05 ppm 48.60 ppm 27.00 ppm 31.30 ppm ppm <0.05 ppm 52.40 ppm 27.60 ppm 30.60 ppmNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 

### 14.00 ppm 1.25 ppm 161.00 ppm <0.25 ppm 16.40 ppm 1.57 ppm 143.00 ppm <0.25 ppmNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur



### 3.30 21.06 40.85 38.09 47.89 3.05 0.90 1.86 3.35 20.75 41.34 37.91 47.01 3.10 0.83 1.99 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 

### 5.43 5.73EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 10641 Cambria Cogen B2 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units M0010, M0031 R1 

### 5/18/2010 5/18/2010 8175.00 Btu/lb M0010, M0031 R2 5/18/2010 5/18/2010 7922.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 3.30 39.50 1.80 8484.00 Btu/lb 40.85 1.86 3.35 39.65 1.92 8196.00 Btu/lb 41.34 1.99Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 982.00 ppm 405.020 ppb <4.97 ppm 27.10 ppm <0.04 0.10 % 540.740 ppb <4.67 ppm 25.92 ppm <0.04Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### ppm <0.05 ppm 48.60 ppm 27.00 ppm 31.30 ppm ppm <0.05 ppm 52.40 ppm 27.60 ppm 30.60 ppmNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 14.00 ppm 1.25 ppm 161.00 ppm <0.25 ppm 3.30 16.40 ppm 1.57 ppm 143.00 ppm <0.25 ppm 3.35 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

### 21.06 40.85 38.09 47.89 3.05 0.90 1.86 5.43 20.75 41.34 37.91 47.01 3.10 0.83 1.99 5.73 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 10641 Cambria Cogen B2

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals sy nfuel mg /g petroleum coke μg/g other mg /KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm