Index to EPA Test Methods

April 2003 revised edition 

Peg Nelson 

US EPA New England Region 1 Library 

Boston, MA USA 

Operated under contract with ASRC Aerospace Corporation 
Preface 

To respond to frequent requests for agency test methods, Region 1 Library staff developed this methods 

index as a tool to help locate copies of them. Confirming that there was no one volume containing all 

agency methods and no comprehensive list of them, the project commenced and in 1988 the first printed 

Index to EPA Test Methods was published as EPA 901/3-88-001. It has been updated periodically to 

reflect new procedures and revoked methods and the current edition includes about 1600 method 

references. The index includes only EPA methods and its primary goal remains as a reference tool to 

identify a source from which the actual method can be obtained, either free or for a fee. 

Originally sources were primarily print documents, but in the mid 1990's electronic versions of EPA air 

methods began to appear on bulletin board systems (BBS) and then some water methods on floppy 

disks. In the late 1990's, EPA issued two compendium of methods on CD ROM for waste and for water. 

Internet access was more recent and commenced with the air methods and in 1998 the entire SW-846 

compendium was placed on the web. In 1999 the EPA New England Region 1 Library website first 

offered the Index in Adobe Acrobat format for easy distribution. In 2002, the revamped web version of 

EMMI appeared as National Environmental Methods Index (NEMI) offering summary information about 

water methods from EPA and other organizations, with links to full text of those from EPA. 

The Index to EPA Test Methods is an ever changing product and your feedback helps keep it current and 

useful. Please contact me with your comments, questions and contributions. 

Peg Nelson (contractor) email: nelson.peg@epa.gov 

EPA New England Region 1 Library phone: (617) 918-1991 

1 Congress Street, Suite 1100 LIB fax: (617) 918-1992 

Boston, MA 02114-2023 April 2003 

Table of Contents 

Preface

Table of Contents

Introduction to the Index to EPA Test Methods

Method Number Index

Chemical/Name Index

Sources for EPA Test Methods including live links to methods when connected to the Internet

Key to Obtaining Source Documents
Introduction 

Q What are test methods?

A Test methods are approved procedures for measuring the presence and concentration of physical and

chemical pollutants; evaluating properties, such as toxic properties, of chemical substances; or

measuring the effects of substances under various conditions. 

Q Why an index?

A This Index was developed to improve access to US EPA test methods. It is not an official EPA

publication nor does inclusion or exclusion of methods indicate EPA approval or disapproval of any

method. The most recent version can be downloaded from the EPA New England Region 1 Library

website www.epa.gov/ne/oarm/index.html

Q What information is included?

A This Adobe Acrobat version contains the following pieces of information: 

C Method Number -- the official method number or a compiler assigned number if un-numbered 

Examples: 0330.1 or 3810 or TO-15 or 8080A or SAMPLIN 

C Chemical or Method Description -- chemical, analyte, chemical group or name of protocol. If 

you don’ t find one you want, try a broader term e.g., metals for mercury or pesticides for diquat 

Examples: asbestos or absorption or Maneb or larval survival or mercury 

C Reference source of where to get the method by one of four categories: 

EPA Report # EPA report number 

Examples: 600/4-82-029 or SW-846 Ch 3.3 

40 CFR Part Title 40 of the Code of Federal Regulations part numbers 

Examples: 136 App A = 40 CFR 136 Appendix A 

Region 1 # EPA Region 1 Library local call number 

Examples: 01A0006125a or 01A0006706 

Electronic Version -- abbreviated reference to an electronic version if available 

Examples: www or ttn/emc or NEMI; full web address provided in Source List 

CD indicates included in the Water Methods CD ROM (EPA 821/C-99-004) 

• Date Issued date method was issued or published 

Examples: 09/25/1996 or / / / (date unknown) 

Q Where are the methods?

A This compilation is only an index, not a collection of actual methods. The Sources for EPA Test

Methods, following the two indexes, indicates how to obtain print or electronic copies of the methods

listed. If you are using the Adobe version while connected to the internet, you’ll find over 75 % of the

sources listed have live weblinks to the actual method. 

Q Why are there multiple entries for some method numbers?

A This was done intentionally to accommodate multiple substances determined by a single method. 

Some numbers appear to have been used for more than one media and method, and no attempt was

made to reconcile these apparent discrepancies. A look at the source list should let you know for what

general purpose the method was intended (wastewater, soil, air, or multi-media).

Q What if I can't find a method I need?

A In some cases individual substances are listed; in others a family of substances is listed under one

name. For example, look for related or broader terms such as metals rather than mercury or pesticides

as well as a specific one such as dursban. EPA does not have a test method for all chemicals, only 

those which it in some way regulates. You are welcome to contact the Region 1 Library to inquire about

methods not found in the index and for suggestions on where else to look. In many cases, we will be

able to email the method to you or direct you to a website or someone who can assist you.
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

0001 Asbestos Abatement 600/2-85-028 

0001 Traverse Points - Stationary Sources 60 App A /ttn/emc 09/25/1996

00-01 Gross alpha & gross beta particle - radiochem 520/5-84-006 CD 08/01/1994 

0001.0 Field & Laboratory for Overburdens & Minesoils 600/2-78-054 03/01/1978 

0001A Small Ducts - Sample & Velocity Traverses 60 App A /ttn/emc 09/25/1996 

0002 Absorption in decontamination at Superfund sites 600/2-85-028 

0002 Velocity and S-type Pitot 60 App A /ttn/emc 09/25/1996 

00-02 Gross alpha in DW by coprecipitation 520/5-84-006 CD 08/01/1994 

0002.1 Field Clues - Overburdens and Minesoils 600/2-78-054 03/01/1978 

0002.2 Overburden Sampling and Labeling 600/2-78-054 03/01/1978 

0002.3 Minesoils - Field Clues and Sampling Methods 600/2-78-054 03/01/1978 

0002A Volume Meters through Pipes & Small Ducts 60 App A /ttn/emc 09/25/1996 

0002B Exhaust Volume Flow Rate - Gasoline Vapor 60 App A /ttn/emc 04/01/1996 

0002C Velocity & Flow Rate - Standard Pitot 60 App A /ttn/emc 09/25/1996 

0002D Volumetric Flow Rate Meters in Small Pipes 60 App A /ttn/emc 09/25/1996 

0002E Landfill Gas Production Flow Rate 60 App A /ttn/emc 06/20/1996 

0002F Stack gas-velocity/volumetric flow rate-3D probe 60 App A /ttn/emc 

0002G Stack gas-velocity/volumetric flow rate-2D probe 60 App A /ttn/emc 

0002H Stack gas velocity / (decay near stack wall) 60 App A /ttn/emc 

0003 Demolition - Hazardous Waste 600/2-85-028 

0003 Molecular Weight - Carbon Dioxide, Oxygen 60 App A /ttn/emc 09/25/1996 

0003.1 Characterizing, Subsampling and Crushing Samples 600/2-78-054 03/01/1978 

0003.1 Closed Conduit Flow Measurement 600/4-82-029 www 

0003.2 Chemical Methods - Overburdens and Minesoils 600/2-78-054 03/01/1978 

0003.2 Flow from Pipes Discharging to Atmosphere 600/4-82-029 www 

0003.3 Flow Measurements - Open Channel 600/4-82-029 www 

0003.3 Mineralogical Methods - Overburdens & Minesoils 600/2-78-054 03/01/1978 

0003.4 Flow Measurement, Misc. 600/4-82-029 www 

0003.4 Physical Methods - Overburdens & Minesoils 600/2-78-054 03/01/1978 

0003.5 Microbiological Methods - Overburdens & Minesoil 600/2-78-054 03/01/1978 

0003.5 Secondary Devices 600/4-82-029 www 

0003A Carbon Dioxide & Oxygen concentrations - IAP 60 App A /ttn/emc 05/06/1989 

0003B O2, CO2, CO - emission rate correction factor 60 App A /ttn/emc 02/01/2000 

0003C Carbon dioxide, methane, nitrogen, oxygen 60 App A /ttn/emc 06/20/1996 

0004 Dismantling 600/2-85-028 

0004 Moisture Content in Stack Gases 60 App A /ttn/emc 09/25/1995 

0004.1 Laboratory & Field Methods - Weathering 600/2-78-054 03/01/1978 

0004.2 Samples, Number of 600/4-82-029 www 

0004.3 Sample Frequency 600/4-82-029 www 

0004.4 Parameters to Monitor 600/4-82-029 www 

0004.5 Monitoring Network and In-Plant Sampling 600/4-82-029 www 

0005 Dusting/Vacuuming/Wiping 600/2-85-028 

0005 Particulate Matter (PM) - Stationary Sources 60 App A /ttn/emc 08/16/1996 

0005A PM Asphalt Roofing (Particulate Matter) 60 App A /ttn/emc 06/13/1990 

0005B PM Nonsulfuric Acid (Particulate Matter) 60 App A /ttn/emc 06/13/1990 

0005D PM Baghouses (Particulate Matter) 60 App A /ttn/emc 08/20/1996 

0005E PM Fiberglass Plants (Particulate Matter) 60 App A /ttn/emc 08/20/1996 

0005F PM Fluid Catalytic Cracking Unit 60 App A /ttn/emc 09/25/1996 

04/16/2003 see Sources list for full reference and website address Method Number Index Page 1 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

0005G PM Wood Heaters from a Dilution Tunnel 60 App A /ttn/emc 08/20/1996 

0005H PM Wood Heaters from a Stack 60 App A /ttn/emc 08/20/1996 

0005I Low Level Particulate Matter - Stationary Source 60 App A /ttn/emc 12/30/1997 

0006 Encapsulation/Enclosure 600/2-85-028 

0006 Sulfur Dioxide Emissions (SO2) 60 App A /ttn/emc 09/25/1996 

0006.8 Sampling Industrial Wastewaters 600/4-82-029 www 

0006A Sulfur Dioxide & Carbon Dioxide - Fossil Fuel 60 App A /ttn/emc 09/25/1997 

0006B Sulfur Dioxide & Carbon Dioxide - Daily Fossil 60 App A /ttn/emc 08/20/1996 

0006C Sulfur Dioxide Emissions - Stationary by IAP 60 App A /ttn/emc 09/25/1996 

0007 Gritblasting 600/2-85-028 

0007 Nitrogen Oxide Emissions - Stationary Sources 60 App A /ttn/emc 03/12/1996 

0007.8 Sampling Agricultural Discharges 600/4-82-029 www 

0007A Nitrogen Oxide - Ion Chromatographic 60 App A /ttn/emc 01/28/1991 

0007B Nitrogen Oxide - Ultraviolet Spectrophotometry 60 App A /ttn/emc 08/20/1996 

0007C Nitrogen Oxide - Colorimetric 60 App A /ttn/emc 09/25/1996 

0007D Nitrogen Oxide - Ion Chromatographic 60 App A /ttn/emc 09/25/1996 

0007E Nitrogen Oxide - Instrumental 60 App A /ttn/emc 08/14/1990 

0008 Hydroblasting/Waterwashing 600/2-85-028 

0008 Sulfuric Acid Mist 60 App A /ttn/emc 10/29/1996 

0008.7 Sampling Waters, Organisms & Sediments 600/4-82-029 www 

0009 Painting/coating 600/2-85-028 

0009 Visual Opacity 60 App A /ttn/emc 08/20/1996 

0009 Alt 1 Opacity of Emissions - Remotely by Lidar 60 App A 

0010 Carbon Monoxide - NDIR 60 App A /ttn/emc 09/25/1996 

0010 Sampling Train - Modified Method 5 semi-volatile SW-846 Ch 10 www 09/01/1986 

0010 Scarification 600/2-85-028 

0010.8 Sampling Sludges 600/4-82-029 www 

0010A Carbon Monoxide - for certifying CEMS 60 App A /ttn/emc 09/25/1996 

0010B Carbon Monoxide from Stationary Sources 60 App A /ttn/emc 11/08/1994 

0011 Formaldehyde Emissions - Stationary Sources SW-846 Ch 10 www 12/01/1996 

0011 Hydrogen Sulfide of Fuel 60 App A /ttn/emc 09/25/1996 

0011 RadKleen 600/2-85-028 

0012 Inorganic Lead - Stationary Sources 60 App A /ttn/emc 09/25/1996 

0012 Solvent Washing 600/2-85-028 

0012.1 Sample Collection 600/4-82-029 www 

0013 Steam Cleaning 600/2-85-028 

0013A Fluoride, Total (SPADNS Zirconium Lake) 60 App A /ttn/emc 09/25/1996 

0013B Fluoride, Total - Specific Ion Electrode 60 App A /ttn/emc 08/20/1996 

0014 Fluoride - Potroom Roof Monitors/Prim Aluminum 60 App A /ttn/emc 09/25/1996 

0014 Vapor-Phase Solvent Extraction 600/2-85-028 

0014.4 Sample Methods & Equipment - Microbiological 600/4-82-029 www 

0014A Total Fluoride emissions - primary aluminum 60 App A 10/07/1998 

0015 Acid Etching 600/2-85-028 

0015 Hydrogen Sulfide/Carbon Disulfide/Carbon Sulfide 60 App A /ttn/emc 10/10/1996 

0015A Sulfur, Total Reduced (TRS Alt.) 60 App A /ttn/emc 04/01/1996 

0016 Bleaching 600/2-85-028 

0016 Sulfur (Semicontinuous Determination) 60 App A /ttn/emc 10/10/1996 

0016A Sulfur, Total Reduced - Stationary/Impinger 60 App A /ttn/emc 09/25/1996 

04/16/2003 see Sources list for full reference and website address Method Number Index Page 2 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

0016B Total Reduced Sulfur - (GC Analysis) 60 App A /ttn/emc 04/01/1996 

0017 Flaming 600/2-85-028 

0017 Particulate Matter (PM) - Instack Filtration 60 App A /ttn/emc 04/23/1996 

0017.1 Sample Preservation 600/4-82-029 www 

0018 Drilling and Spalling 600/2-85-028 

0018 VOC - GC 60 App A /ttn/emc 09/25/1996 

0019 K-20 Sealant 600/2-85-028 

0019 Sulfur Dioxide Removal & PM, SO2, NOx Rates 60 App A /ttn/emc 04/15/1996 

0020 Microbial Degradation 600/2-85-028 

0020 Nitrogen Oxides (NOx) - Stationary Gas Turbines 60 App A /ttn/emc 09/25/1996 

0020 Source Assessment Sampling System (SASS) SW-846 Ch 10 www 09/01/1986 

0021 Photochemical Degradation 600/2-85-028 

0021 Volatile Organic Compounds (VOC) Leaks 60 App A /ttn/emc 04/27/1995 

0022 Fugative Opacity 60 App A /ttn/emc 05/21/1995 

0023 Dioxin & Furan (PCDD & PCDF) 60 App A /ttn/emc 05/25/1995 

0023A PCDDs and PCDFs - Stationary Sources Sampling SW-846 Ch 10 www 12/01/1996 

0024 Surface Coatings - Volatile Matter Content 60 App A /ttn/emc 09/11/1995 

0024A Volatile Matter Content & Density/Printing Inks 60 App A /ttn/emc 08/06/1993 

0025 Gaseous Nonmethane Organic Emissions 60 App A /ttn/emc 09/25/1996 

0025A Gaseous Organic Concentration - Flame Ionization 60 App A /ttn/emc 09/25/1996 

0025B Gaseous Organic Concentration - Infrared Analyze 60 App A /ttn/emc 11/08/1994 

0025C NMOC in Landfill Gases 60 App A /ttn/emc 06/20/1996 

0025D VOC of Waste Samples 60 App A /ttn/emc 08/20/1996 

0025E Vapor Phase Organic Concentration /Waste SampleS 60 App A /ttn/emc 09/25/1996 

0026 Hydrogen Chloride, Halides, Halogens Emissions 60 App A /ttn/emc 08/28/1996 

0026A Hydrogen Halide & Halogen - Isokinetic /ttn/emc 03/03/1994 

0027 Vapor Tightness of Gasoline Tank - Pressure Vac. 60 App A /ttn/emc 01/21/1994 

0028 Wood Heaters - Certificate & Auditing 60 App A /ttn/emc 09/25/1996 

0028A Wood Fired Appliances - Burn Rate & Air:Fuel 60 App A /ttn/emc 09/25/1996 

0029 Metals Emissions from Stationary Sources 60 App A /ttn/emc 06/25/1996 

0030 Volatile Organic Sampling Train SW-846 Ch 10 www 09/01/1986 

0031 VOCs - Sampling (SMVOC) SW-846 Ch 10 www 12/01/1996 

0040 Organic Hazardous Consitutents - Tedlar Bags SW-846 Ch 10 www 12/01/1996 

0050 Isokinetic HCL/LC2 Emission Sampling Train SW-846 Ch 10 www 12/01/1996 

0051 Midget Impinger HCL/CL2 Emission Sampling Train SW-846 Ch 10 www 12/01/1996 

0060 Metals in Stack Emissions SW-846 Ch 10 www 12/01/1996 

0061 Hexavalent Chromium Emissions - Stationary Sourc SW-846 Ch 10 www 12/01/1996 

0100 Formaldehyde & Carbonyl Compounds in Indoor Air SW-846 Ch 10 www 12/01/1996 

0100.1 Asbestos Fibers in Water (Chatfield Method) 600/4-83-043 NEMI 09/01/1983 

0100.1 Sediments - Survival Test / Hyalella azteca 10-d 600/R-99-064 www 03/01/2000 

0100.2 Asbestos Fibers in DW Using MCE Filters 600/R-94-134 NEMI 06/01/1994 

0100.2 Sediments - Survival & Growth/Chironomus tentans 600/R-99-064 www 03/01/2000 

0100.3 Sediments - Bioaccumulation / Lumbriculus varieg 600/R-99-064 www 03/01/2000 

0100.4 Sediment - freshwater amphipods 42-d survival 600/R-99-064 www 03/01/2000 

0100.4 Sediment - marine amphipods 10-d survival test 600/R-94-025 www 03/01/2000 

0100.5 Sediment - Chironomus tentans life-cycle test 600/R-99-064 www 03/01/2000 

0101 Mercury Emissions - Chlor-Alkali Plants (Air) 61 App B /ttn/emc 09/25/1996 

0101A Mercury Emissions - Sewage/Sludge Incinerator 61 App B /ttn/emc 05/20/1991 

04/16/2003 see Sources list for full reference and website address Method Number Index Page 3 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

0102 Mercury Emissions - Chlor-Alkali Hydrogen Stream 61 App B /ttn/emc 05/20/1991 

0103 Beryllium Screening Method 61 App B /ttn/emc 09/25/1996

0104 Beryllium Emissions Determination 61 App B /ttn/emc 01/18/1995

0105 Mercury in Wastewater Plant Sewage Sludge 61 App B /ttn/emc 09/25/1996

0106 Vinyl Chloride from Stationary Sources 61 App B /ttn/emc 05/23/1995

0107 Vinyl Chloride Content of Inprocess Wastewater 61 App B /ttn/emc 08/20/1996

0107A Vinyl Chloride Content of Solvents 61 App B /ttn/emc 09/25/1996

0108 Particulate & Gaseous Arsenic Emissions 61 App B /ttn/emc 09/25/1996

0108A Arsenic in Ore Samples - Nonferrous Smelters 61 App B /ttn/emc 08/20/1996

0108B Arsenic in Ore Samples from Nonferrous Smelters 61 App B /ttn/emc 01/01/1996

0108C Arsenic in Ore Samples from Nonferrous Smelters 61 App B /ttn/emc 01/01/1996

0110.1 Color - Colorimetric, ADMI 600/4-79-020 NEMI

0110.2 Color - Colorimetric-Platinum-Cobalt 600/4-79-020 NEMI

0110.3 Color - Spectrophotometric 600/4-79-020 NEMI

0111 Polonium-210 Emissions from Stationary Sources 61 App B /ttn/emc 04/01/1996

0114 Radionuclide Emissions from stationary sources 61 App B /ttn/emc 04/01/1996

0115 Radon-222 Emissions 61 App B /ttn/emc 04/01/1996

0120.1 Conductance - Specific Conductance, at 25 C 600/4-79-020 NEMI

0120.6 Conductance-Specific/Wet Deposition Electrolytic 600/4-86-024 03/01/1986

0130.1 Hardness, Total - Colorimetric, Automated EDTA 600/4-79-020 NEMI

0130.2 Hardness, Total - Titrimetric, EDTA 600/4-79-020 NEMI

0140.1 Odor, Threshold - Consistent Series 600/4-79-020 www

0150.1 pH - Electrometric 600/4-79-020 NEMI

0150.2 pH - Continuous Monitoring (Electrometric) 600/4-79-020 NEMI

0150.6 pH of Wet Deposition -Electrolytic Determination 600/4-86-024 03/01/1986

0160.1 Residue, Filterable 600/4-79-020 NEMI

0160.2 Residue, Non-Filterable & Total Suspended Solids 600/4-79-020 NEMI

0160.3 Residue, Total 600/4-79-020 NEMI

0160.4 Residue, Volatile 600/4-79-020 NEMI

0160.5 Residue, Settleable Matter 600/4-79-020 www

0170.1 Temperature - Thermometric 600/4-79-020 NEMI

0180.1 Turbidity - Nephelometric 600/R-93-100 NEMI 08/01/1993

0200 Metals - Atomic Absorption 600/4-79-020 www

0200.1 Metals:Arsenic/Cadmium/Chromium/Copper/Lead/Mer600/4-91-010 www 04/01/1991

0200.10 Trace Elements in Marine Water by ICP/MA 600/4-91-010 NEMI 04/01/1991

0200.10 Trace Elements/Marine by Online chelation-ICP/MS 600/R-97-072 /nerlcwww /ordmeth 09/01/1997

0200.11 Metals in Fish Tissue by ICP/EES 600/4-91-010 www 04/01/1991

0200.12 Trace Elements by Stabilized Temp GF/AA 600/R-97-072 /orthmeth NEMI 09/01/1997

0200.13 Trace Elements by Off-line Chelation 600/R-97-072 /orthmeth NEMI 09/01/1997

0200.15 Trace Elements - Stabilized Temperature GFAA 600/R-94-111 www 05/01/1994

0200.2 Aluminum - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Antimony - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Arsenic - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Barium - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Beryllium - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Cadmium - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Calcium - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Chromium - Sample Preparation 600/R-94-111 www 05/01/1994

04/16/2003 see Sources list for full reference and website address Method Number Index Page 4 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

0200.2 Cobalt - Sample Preparation 600/R-94-111 www 05/01/1994 

0200.2 Copper - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Iron - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Lead - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Lithium - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Magnesium - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Manganese - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Mercury, Total - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Metals, Total Recoverable Elements - Sample Prep 600/R-94-111 www 05/01/1994

0200.2 Molybdenum - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Nickel - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Phosphorus - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Potassium - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Selenium - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Silica - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Silver - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Sodium - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Strontium - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Thallium - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Thorium - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Tin - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Uranium - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Vanadium - Sample Preparation 600/R-94-111 www 05/01/1994

0200.2 Zinc - Sample Preparation 600/R-94-111 www 05/01/1994

0200.3 Metals, Total Recoverable in Biological Tissues 600/4-91-010 www 04/01/1991

0200.6 Metals - Calcium, Magnesium, Potassium & Sodium 600/4-86-024 03/01/1986

0200.7 Metals and Trace Elements - ICP/AES 600/R-94-111 www 05/01/1994

0200.7 Trace Element (Metals) - ICP 600/4-79-020 www

0200.7 Trace Element in water/wastes by ICP 136 App C www CD

0200.7 Trace elements in Water, Solids & biosolids/ICP NEMI 08/01/1998

0200.7 CL Trace element by ICP/AE in water & wastes ILM04.0 exhibit D www clp

0200.8 Trace Elements in Water & Wastes - ICP/MS 600/R-94-111 NEMI 05/01/1994

0200.8 Trace elements in waters & wastes/ ICP MS CD

0200.9 Trace Elements - GFAA 600/R-94-111 NEMI 05/01/1994

0200.9 Trace Elements - Stabilized Temp Graphite FAAS 821/R-93-010-B CD 04/01/1991

0200.9 Trace elements in water, solid & biosolids CD 09/01/1998

0201 PM10 - In-Stack, CRS (Constant Sampling Rate) 51 App M /ttn/emc 04/17/1990

0201A PM10 - In-stack, CRS (Constant Sampling Rate) 51 App M /ttn/emc 09/25/1996

0202 PM Condensible Particulate Matter 51 App M /ttn/emc 09/25/1996

0202.1 Aluminum - AA, Direct Aspiration 600/4-79-020 NEMI

0202.2 Aluminum - AA, Furnace Technique 600/4-79-020 NEMI

0203 Continuous Opacity Monitoring for Compliance /ttn/emc 01/30/1995

0203A Visual Opacity - Time-Averaged /ttn/emc 01/06/1994

0203B Visual Opacity - Time-Exception /ttn/emc 01/06/1994

0203C Opacity of Emissions, Instantaneous Limitation /ttn/emc 01/06/1994

0204 Capture Efficiency - Permanent/Temporary TTE 51 App M /ttn/emc 06/16/1997

0204.1 Antimony - AA, Direct Aspiration 600/4-79-020 NEMI

0204.2 Antimony - AA, Furnace Technique 600/4-79-020 NEMI

04/16/2003 see Sources list for full reference and website address Method Number Index Page 5 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

0204.2 CL Antimony - AA, furnace technique ILM04.0 exhibit D www clp

0204A VOCs in Liquid Imput Stream 51 App M /ttn/emc 06/16/1997

0204B VOCs in Captured Stream 51 App M /ttn/emc 08/01/1995

0204C VOCs in Captured Stream (Dilution) 51 App M /ttn/emc 06/16/1997

0204D VOCs, Fugitive from Temporary Total Enclosure 51 App M /ttn/emc 06/16/1997

0204E VOCs, Fugitive from Building Enclosure 51 App M /ttn/emc 06/16/1997

0204F VOCs in Liquid Imput Stream - Distillation 51 App M /ttn/emc 06/16/1997

0205 Gas Dilution - Field Instrument Calibration 51 App M /ttn/emc 09/25/1996

0206.2 Arsenic - AA, Furnace Technique 600/4-79-020 NEMI

0206.2 CL Arsenic - AA, furnace technique ILM04.0 exhibit D www clp

0206.3 Arsenic - AA, Gaseous Hydride 600/4-79-020 NEMI

0206.4 Arsenic - Spectrophotometric - SDDC 600/4-79-020 NEMI

0206.5 Arsenic - Digestion Prior to Total Analysis 600/4-79-020 NEMI

0207-1 Isocyanates Draft Sampling Method /ttn/emc 02/29/1996

0207-2 Isocyanates Draft Sampling Method by HPLC /ttn/emc 02/29/1996

0208.1 Barium - AA, Direct Aspiration

0208.2 Barium - AA, Furnace Technique

0210.1 Beryllium - AA, Direct Aspiration

0210.2 Beryllium - AA, Furnace Technique

0210.2 CL Beryllium - AA, furnace technique

0212.3 Boron - Colorimetric, Curcumin

0213.1 Cadmium - AA, Direct Aspiration

0213.2 Cadmium - AA, Furnace Technique

0213.2 CL Cadmium - AA, furnace technique

0215.1 Calcium - AA, Direct Aspiration

0215.1 CL Calcium - AA, flame technique

0215.2 Calcium - Titrimetric, EDTA

0218.1 Chromium, total - AA, Direct Aspiration

0218.2 Chromium, total - AA, Furnace

0218.2 CL Chromium - AA, furnace technique

600/4-79-020 NEMI

600/4-79-020 NEMI

600/4-79-020 NEMI

600/4-79-020 NEMI 09/01/1997

ILM04.0 exhibit D www clp

600/4-79-020 NEMI

600/4-79-020 NEMI

600/4-79-020 NEMI

ILM04.0 exhibit D www clp

600/4-79-020 NEMI

ILM04.0 exhibit D www clp

600/4-79-020 NEMI

600/4-79-020 NEMI

600/4-79-020 NEMI

ILM04.0 exhibit D www clp

0218.3 Chromium, total - AA, Chelation-Extraction 600/4-79-020 NEMI

0218.4 Chromium VI (Hexavalent) - Chelation Extraction 600/4-79-020 NEMI

0218.5 Chromium, Hexavalent Dissolved - AA, Furnace 600/4-79-020 www

0218.6 Chromium, Dissolved Hexavalent by IC CD 09/01/1998

0218.6 Chromium, Dissolved Hexavalent by Ion Chromatogr 600/R-94-111 www 05/01/1994

0219.1 Cobalt - AA, Direct Aspiration 600/4-79-020 NEMI 

0219.2 Cobalt - AA, Furnace 600/4-79-020 NEMI 

0220.1 Copper - AA, Direct Aspiration 600/4-79-020 NEMI 

0220.2 Copper - AA, Furnace 600/4-79-020 NEMI 

0231.1 Gold - AA, Direct Aspiration 600/4-79-020 NEMI 

0231.2 Gold - AA, Furnace 600/4-79-020 NEMI 

0235.1 Iridium - AA, Direct Aspiration 600/4-79-020 NEMI 

0235.2 Ididium - AA, Furnace 600/4-79-020 NEMI 

0236.1 Iron - AA, Direct Aspiration 600/4-79-020 NEMI 

0236.2 Iron - AA, Furnace 600/4-79-020 NEMI 

0239.1 Lead - AA, Direct Aspiration 600/4-79-020 NEMI 

0239.2 Lead - AA, Furnace 600/4-79-020 NEMI 

0239.2 CL Lead - AA, furnace technique ILM04.0 exhibit D www clp 

04/16/2003 see Sources list for full reference and website address Method Number Index Page 6 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

0242.1 Magnesium - AA, Direct Aspiration 600/4-79-020 NEMI

0242.2 CL Magnesium - AA, flame technique ILM04.0 exhibit D www clp

0243.1 Manganese - AA, Direct Aspiration 600/4-79-020 NEMI

0243.2 Manganese - AA, Furnace 600/4-79-020 NEMI

0245.1 Mercury - Cold Vapor, Manual 600/4-79-020 NEMI 03/01/1983

0245.1 Mercury in Water by Cold Vapor AAS 600/R-94-111 www 05/01/1994

0245.1 CL Mercury in water - manual cold vapor technique ILM04.0 exhibit D www clp

0245.2 Mercury - Cold Vapor, Automated 600/4-79-020 NEMI

0245.2 CL Mercury in water - automated cold vapor ILM04.0 exhibit D www clp

0245.3 Mercury, Inorganic II by HPLC/ECD 600/4-91-010 www 04/01/1991

0245.3 Organomercurials, Selected by HPLC/ECD 600/4-91-010 www 04/01/1991

0245.5 Mercury - Cold Vapor, Sediment Manual 600/4-79-020 www

0245.5 Mercury in Sediment by Cold Vapor (CV/AAS) 600/4-91-010 www 04/01/1991

0245.5 CL Mercury in soil/sediment - manual cold vapor ILM04.0 exhibit D www clp

0245.6 Mercury in Tissues by Cold Vapor (CV/AAS) 600/4-91-010 www 04/01/1991

0245.7 Mercury - CVA Fluorescence spectrometry 821/R-01-008 CD 02/01/1999

0246.1 Molybdenum - AA, Direct Aspiration

0246.2 Molybdenum - AA, Furnace

0249.1 Nickel - AA, Direct Aspiration

0249.2 Nickel - AA, Furnace

0252.1 Osmium - AA, Direct Aspiration

0252.2 Osmium - AA, Furnace

0253.1 Palladium - AA, Direct Aspiration

0253.2 Palladium - AA, Furnace

0255.1 Platinum - AA, Direct Aspiration

0255.2 Platinum - AA, Furnace

0258.1 Potassium - AA, Direct Aspiration

0258.1 CL Potassium - AA, flame technique

0264.1 Rhenium - AA, Direct Aspiration

0264.2 Rhenium - AA, Furnace

0265.1 Rhodium - AA, Direct Aspiration

0265.2 Rhodium - AA, Furnace

0267.1 Ruthenium - AA, Direct Aspiration

0267.2 Ruthenium - AA, Furnace

0270.2 Selenium - AA, Furnace

0270.2 CL Selenium - AA, furnace technique

0270.3 Selenium - AA, Gaseous Hydride

0272.1 Silver - AA, Direct Aspiration

0272.2 Silver - AA, Furnace

0272.2 CL Silver - AA, furnace technique

0273.1 Sodium - AA, Direct Aspiration

0273.1 CL Sodium - AA, flame technique

0273.2 Sodium - AA, Furnace

0279.1 Thallium - AA, Direct Aspiration

0279.2 Thallium - AA, Furnace

0279.2 CL Thallium - AA, furnace technique

0282.1 Tin - AA, Direct Aspiration

0282.2 Tin - AA, Furnace

600/4-79-020 NEMI 

600/4-79-020 NEMI 

600/4-79-020 NEMI 

600/4-79-020 NEMI 

600/4-79-020 NEMI 

600/4-79-020 NEMI 

600/4-79-020 NEMI 

600/4-79-020 NEMI 

600/4-79-020 NEMI 

600/4-79-020 NEMI 

600/4-79-020 NEMI 

ILM04.0 exhibit D www clp 

600/4-79-020 www 

600/4-79-020 www 

600/4-79-020 NEMI 

600/4-79-020 NEMI 

600/4-79-020 NEMI 

600/4-79-020 NEMI 

600/4-79-020 NEMI 

ILM04.0 exhibit D www clp 

600/4-79-020 www 

600/4-79-020 NEMI 

600/4-79-020 NEMI 

ILM04.0 exhibit D www clp 

600/4-79-020 NEMI 

ILM04.0 exhibit D www clp 

600/4-79-020 www 

600/4-79-020 NEMI 

600/4-79-020 NEMI 

ILM04.0 exhibit D www clp 

600/4-79-020 NEMI 

600/4-79-020 NEMI 

04/16/2003 see Sources list for full reference and website address Method Number Index Page 7 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

0282.3 Tributyltin Chloride in Marine & Fresh Waters 01A0006709 www 10/01/1989 

0283.1 Titanium - AA, Direct Aspiration 600/4-79-020 NEMI 

0283.2 Titanium - AA, Furnace 600/4-79-020 NEMI 

0286.1 Vanadium - AA, Direct Aspiration 600/4-79-020 NEMI 

0286.2 Vanadium - AA, Furnace 600/4-79-020 NEMI 

0289.1 Zinc - AA, Direct 600/4-79-020 NEMI 

0289.2 Zinc - AA, Furnace 600/4-79-020 NEMI 

0300.0 Chloride - IC 600/4-79-020 NEMI 03/01/1984 

0300.0 Fluoride - IC 600/4-79-020 www 

0300.0 Inorganic Anions by Ion Chromatography 600/R-93-100 www 08/01/1993 

0300.0 Inorganic Anions in DW by Ion Chromatography CD 08/01/1993 

0300.0 Nitrate-N by IC 600/4-79-020 www 

0300.0 Nitrite by IC 600/4-79-020 www 

0300.0 Ortho-Phosphate-P 600/4-79-020 www 

0300.0 Sulfate 600/4-79-020 www 

0300.1 Inorganic Anions in DW by Ion Chromatography 815/R-00-014 NEMI 09/01/1997 

0300.6 Inorganics:Chloride/Sulfate/Nitrate/Orthophospha 600/4-86-024 03/01/1986 

0300.7 Metals:Sodium/Ammonium/Potassium/Magnesium/Cal 600/4-86-024 03/01/1986 

0301 Field Validation - Pollutant Measurement 63 App A /ttn/emc 12/30/1992 

0303 Visible Emissions/By-Product Coke Oven Batteries 63 App A /ttn/emc 09/25/1996 

0303A Visible Emissions from Non-Recovery Coke Oven 63 App A /ttn/emc 10/27/1993 

0304A Organic Compounds Biodegredation Rates - Vent 63 App A /ttn/emc 03/03/1994 

0304B Organic Compounds Biodegredation Rates -Scrubber 63 App A /ttn/emc 03/03/1994 

0305 VOC Emission Potential in Waste 63 App A /ttn/emc 09/25/1996 

0305.1 Acidity - Titrimetric 600/4-79-020 NEMI 

0305.2 Acidity - Titrimetric (Acid Rain) 600/4-79-020 www 

0305.6 Acidity in Wet Deposition 600/4-86-024 03/01/1986 

0306 Chromium Emissions - Electroplating & Anodizing 63 App A /ttn/emc 02/08/1996 

0306A Chromium Emissions Electroplating - Mason Jar 63 App A /ttn/emc 09/25/1996 

0306B Surface Tension - Tanks Electroplating/Anodizing /ttn/emc 02/08/1996 

0307 Solvent Vapor Cleaner Emissions 63 App A /ttn/emc 09/25/1997 

0308 Methanol Emissions 63 App A /ttn/emc 11/14/1997 

0310.1 Alkalinity - Titrimetric, pH 4.5 600/4-79-020 NEMI 

0310.2 Alkalinity - Colorimetric, Automated 600/4-79-020 NEMI 

0310A Residual Hexane 63 App A /ttn/emc 03/17/1997 

0310B Residual Solvent 63 App A /ttn/emc 03/17/1997 

0310C Residual N-Hexane in EDPM Rubber 63 App A /ttn/emc 03/17/1997 

0311 HAPS in Paints & Coatings - Direct Injection GC 63 App A /ttn/emc 01/17/1996 

0312A Residual Styrene in SBR Latex by GC 63 App A /ttn/emc 03/17/1997 

0312B Styrene in SBR Latex by Capillary GC 63 App A /ttn/emc 03/17/1997 

0312C Styrene in SBR Latex produced by Emulsion Polym 63 App A /ttn/emc 03/17/1997 

0313A Residual Hydrocarbon in Rubber Crumb 63 App A /ttn/emc 03/17/1997 

0313B Residual HC in Rubber Crumb by Capillary GC 63 App A /ttn/emc 03/17/1997 

0314 Perchlorate in DW using Ion Chromatography 815/R-00-014 www 11/01/1999 

0315 PM and MCEM from Aluminum Production Facilities 63 App A /ttn/emc 10/07/1997 

0316 Formaldehyde - Mineral Wool & Wool Fiberglass 63 App A /ttn/emc 03/31/1997 

0317 Inorganic Oxhyalide disinfection by-products- DW 815/R-00-014 NEMI 08/01/2000 

0317 Inorganic Oxhyalide disinfection by-products- DW 815/B-01-001 www 07/19/2001 

04/16/2003 see Sources list for full reference and website address Method Number Index Page 8 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

0318 Extractive FTIR - Mineral Wool & Wool Fiberglass 63 App A /ttn/emc 03/31/1997 

0319 Filtration Efficiency - Paint Overspray Arrestor 63 App A /ttn/emc 10/19/1996

0320 Vapor Phase Organic & Inroganic Emission - FTIR 63 App A /ttn/emc 05/02/1997

0320.1 Bromide - Titrimetric 600/4-79-020 NEMI

0321 Gaseous HCl Emissions at Portland Cement Kilns 63 App A /ttn/emc 03/11/1998

0321.8 Bromate in DW by IC/ICP/MS 815/R-00-014 NEMI 12/01/1997

0322 HCl Emissions from Portland Cement Kilns by FTIR /ttn/emc 03/11/1998

0325.1 Chloride - Colorimetric, Auto. Ferricyanide A I 600/4-79-020 NEMI

0325.2 Chloride - Colorimetric, Auto Ferricyanide A II 600/4-79-020 NEMI

0325.3 Chloride - Titrimetric, Mercuric Nitrate 600/4-79-020 NEMI

0325.6 Chloride in Wet Deposition/Automated Colorimetri 600/4-86-024 03/01/1986

0330.1 Chlorine, Total Residual - Titrimetric 600/4-79-020 NEMI

0330.2 Chlorine, Total Residual - Titrimetric, Back 600/4-79-020 NEMI

0330.3 Chlorine, Total Residual - Titrimetric, Iodomet. 600/4-79-020 NEMI

0330.4 Chlorine, Total Residual - Titrimetric, DPD-FAS 600/4-79-020 NEMI

0330.5 Chlorine, Total Residual - Spectrophotometric, 600/4-79-020 NEMI

0335.1 Cyanides, Available to Chlorination/Titrimetric 600/4-79-020 NEMI

0335.2 Cyanide, Total - Titrimetric, Spectrophotometric 600/4-79-020 NEMI

0335.2 CL Total Cyanide in water, soil/sediment ILM04.0 exhibit D www clp

0335.3 Cyanide, Total - Colorimetric, Automated UV 600/4-79-020 NEMI

0335.4 Total Cyanide by Semi-Automated Colorimetry 600/R-93-100 NEMI 08/01/1993

0340.1 Fluoride, Total - Colorimetric 600/4-79-020 NEMI

0340.2 Fluoride - Potentiometric 600/4-79-020 NEMI

0340.3 Fluoride - Colorimetric 600/4-79-020 NEMI

0340.6 Fluoride in Wet Deposition by Potentiometric 600/4-86-024 03/01/1986

0345.1 Iodide - Titrimetric 600/4-79-020 www

0349.0 Ammonia in Estuarine by Gas Segmented CF/CA 600/R-97-072 NEMI 09/01/1997

0350.1 Ammonia (as nitrogen) - Colorimetric 600/4-79-020 NEMI

0350.1 Ammonia (as N) Semi-Automated Colorimetry 600/R-93-100 www 08/01/1993

0350.2 Ammonia (as N) - Colorimetric, Titrimetric 600/4-79-020 NEMI

0350.3 Ammonia (as N) - Potentiometric 600/4-79-020 NEMI

0350.6 Ammonium in Wet Deposition by Electrometric 600/4-86-024 03/01/1986

0350.7 Ammonium in Wet Deposition/Automated Colormetric 600/4-86-024 03/01/1986

0351.1 Nitrogen, Kjeldahl, Total - Colorimetric/Auto. 600/4-79-020 NEMI

0351.2 Nitrogen, Kjeldahl, Total - Colorimetric 600/4-79-020 NEMI

0351.2 Total Kjeldahl Nitrogen - Semi-Automated Colori 600/R-93-100 www 08/01/1993

0351.3 Nitrogen, Kjeldahl, Total - Colorimetric/Titri. 600/4-79-020 NEMI

0351.4 Nitrogen, Kjeldahl, Total - Potentiometric 600/4-79-020 NEMI

0352.1 Nitrate (as Nitrogen) - Colorimetric, Brucine 600/4-79-020 NEMI

0353.1 Nitrogen, Nitrate-Nitrite - Colorimetric/Hydra. 600/4-79-020 NEMI

0353.2 Nitrate-Nitrate by Automated Colorimetry 600/R-93-100 www 08/01/1993

0353.2 Nitrate-Nitrite (as N) - Colorimetric/Cadmium 600/4-79-020 NEMI

0353.3 Nitrate-Nitrite (as N) - Manual Cadmium 600/4-79-020 NEMI

0353.4 Nitrate & Nitrite by Gas Segmented CF/CA 600/R-97-072 /nerlcwww /ordmeth 09/01/1997

0353.6 Nitrate-Nitrite by Automated Colormetric 600/4-86-024 03/01/1986

0354.1 Nitrate (as Nitrogen) - Spectrophotometric 600/4-79-020 NEMI

0360.1 Oxygen, Dissolved - Membrane Electrode (Probe) 600/4-79-020 NEMI

0360.2 Oxygen, Dissolved - Modified Winkler 600/4-79-020 NEMI

04/16/2003 see Sources list for full reference and website address Method Number Index Page 9 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

0365.1 Orthophosphate (as P) - Automated Colorimetry 600/R-93-100 www 08/01/1993 

0365.1 Phosphorus, All Forms - Colorimetric/Automated 600/4-79-020 NEMI

0365.2 Phosphorus - manual colorimetric/1 reagent 600/4-79-020 NEMI

0365.3 Phosphorus - colorimetric/ 2 reagents 600/4-79-020 NEMI

0365.4 Phosphorus, Total - Colorimetric/Automated 600/4-79-020 NEMI

0365.5 Orthophosphate by automated colorimetric 600/R-97-072 /nerlcwww /ordmeth 09/01/1997

0365.6 Orthophosphate in Wet Depositon 600/4-86-024 03/01/1986

0366.0 Dissolved Silicate by gas segmented CF/CA 600/R-97-072 /orthmeth NEMI 09/01/1997

0370.1 Silica, Dissolved - Colorimetric 600/4-79-020 NEMI

0375.1 Sulfate - Colorimetric, Automated, Chloranilate 600/4-79-020 NEMI

0375.2 Sulfate - Colorimetric, Automated, Methylthymol 600/4-79-020 NEMI

0375.2 Sulfate - Colorimetry, Automated 600/R-93-100 www 08/01/1993

0375.3 Sulfate - Gravimetric 600/4-79-020 NEMI

0375.4 Sulfate - Turbidimetric 600/4-79-020 NEMI

0376.1 Sulfide - Titrimetric, Iodine 600/4-79-020 NEMI

0376.2 Sulfide - Colorimetric, Methylene Blue 600/4-79-020 NEMI

0377.1 Sulfite - Titrimetric 600/4-79-020 NEMI

0388-0393 Helminth ova or cysts in sludge 625/R-92-013 www 11/25/1991

0405.1 Biochemical Oxygen Demand (BOD) - 5 Days, 20 C 600/4-79-020 NEMI

0410.1 Chemical Oxygen Demand - Titrimetric, Mid-Level 600/4-79-020 NEMI

0410.2 Chemical Oxygen Demand - Titrimetric, Low Level 600/4-79-020 NEMI

0410.3 Chemical Oxygen Demand - Titrimetric, High Level 600/4-79-020 NEMI

0410.4 Chemical Oxygen Demand - Colorimetric 600/4-79-020 NEMI

0410.4 Chemical Oxygen Demand - Semi-Automated Colorim 600/R-93-100 www 08/01/1993

0413.1 Oil & Grease, Total, Recoverable - Gravimetric 600/4-79-020 see 1664 www

0413.2 Oil & Grease, Total Recoverable - Spectrophot. 600/4-79-020 www

0415.1 Organic Carbon, Total - Combustion or Oxidation 600/4-79-020 NEMI

0415.2 Organic Carbon, Total - UV Promoted 600/4-79-020 www

0418.1 Petroleum Hydrocarbons, Total Recoverable 600/4-79-020 www

0420.1 Phenols - Spectrophot/4-AAP 600/4-79-020 NEMI

0420.2 Phenols - Colorimetric4-AAP 600/4-79-020 NEMI

0420.3 Phenols - Spectrophot/MBTH 600/4-79-020 www

0420.4 Total Recoverable Phenolics - Semi-Automated Col 600/R-93-100 www 08/01/1993

0425.1 Surfacants Methylene Blue Active Substant (MBAS) 600/4-79-020 NEMI

0430.1 NTA - Colorimetric, Manual, Zinc-Zincon 600/4-79-020 www

0430.2 NTA - Colorimetric, Automated, Zinc-Zincon 600/4-79-020 www

0435 Asbestos in Serpentine Aggregate CARB Method 435 /ttn/emc 10/10/1991

0440.0 Carbon & Nitrogen in sediments & particulates 600/R-97-072 /ordmeth NEMI 09/01/1997

0445.0 In Vitro Chlorophyll & Pheophytin by fluoresence 600/R-97-072 /nerlcwww /ordmeth 09/01/1997

0446.0 In Vitro Chlorophylls & Pheopigments in algae 600/R-97-072 /nerlcwww /ordmeth 09/01/1997

0447.0 Chlorophylls & other pigments by HPCL 600/R-97-072 /nerlcwww /ordmeth 09/01/1997

0450.1 Total Organic Halide 600/4-81-056

0501.1 Trihalomethanes in Drinking Water -purge & trap 01A0008190 11/01/1979

0501.2 Trihalomethanes in DW liquid/liquid extraction 999Zb1118 01A0008190 www NEPI 11/01/1979

0501.3 Trihalomethanes in Drinking Water - GC/MS 01A0005114

0502.1 Volatile Halogenated Organic Compounds in Water 600/4-88-039 www 07/01/1991

0502.2 Volatile Organic Compounds - Water/Purge & Trap 600/R-95-131 NEMI 08/01/1995

0503.1 Volatile Aromatic & Unsaturated Organic Compound 600/4-88-039 www 07/01/1991

04/16/2003 see Sources list for full reference and website address Method Number Index Page 10 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

0504 EDB, DBCP - DW by Microextraction 600/4-88-039 www 07/01/1991 

0504.1 EDB, DBCP, 123TCP by Microextractin & GC 600/R-95-131 NEMI 08/01/1995 

0505 Organohalide Pesticides & PCB Products by GC 600/R-95-131 NEMI 08/01/1995 

0505 Organohalide Pesticides & PCB Products in Water 821/R-93-010-B CD 01/01/1989 

0506 Phthalate & Adipate Esters in DW by LLE or LSE 821/R-93-010-B NEMI 07/01/1990 

0506 Phthalate & Adipate Esters/Liquid-Liquid or LSE 600/R-95-131 www 08/01/1995 

0507 Nitrogen- & Phosphorus-Containing Pesticides 821/R-93-010-B CD 01/01/1989 

0507 Pesticides, Nitrogen & Phosphorus in GW by GC 600/R-95-131 NEMI 08/01/1995 

0508 Chlorinated Pesticides in Water by GC/ECD 821/R-93-010-B CD 01/01/1989 

0508 Pesticides, Chlorinated in Water by GC with ECD 600/R-95-131 NEMI 08/01/1995 

0508.1 Chlorinated Pesticides, Herbicides & Organohal. 600/R-95-131 NEMI 08/01/1995 

0508.1 Chlorinated pesticides/herbicides/organohalides CD 01/01/1994 

0508A PCBs screening by perchlorination & GC NEMI 01/01/1989 

0509 Ethylene Thiourea (ETU) - GC CD 12/01/1992 

0509 Ethylene Thiourea (ETU) in Water by GC 600/R-95-131 www 08/01/1995 

0510.1 Trihalomethane, Maximum Total - Potential 600/4-81-044 

0513 Dioxin (TCDD) & GC/MS [replaced by 1613A] 600/4-90-020 www 07/01/1990 

0515.1 Chlorinated Acids by GC/ECD 600/R-95-131 NEMI 08/01/1995 

0515.1 Chlorinated Acids in Water by GC/ECD 821/R-93-010-B CD 01/01/1989 

0515.2 Chlorinated acids - liquid-solid extraction/GC/ CD 08/01/1992 

0515.2 Chlorinated Acids (Herbicides) by LSE & GC/ECD 600/R-95-131 NEMI 08/01/1995 

0515.2 Chlorinated Acids in Water by LSE/GC/ECD 821/R-93-010-B CD 08/01/1992 

0515.3 Chlorinated Acids (herbicides)in DW / LLE GC/ECD 815/R-00-014 NEMI 07/01/1996 

0515.4 Chlirinated Acids in DW by LL fast GC/ECD 01A0008028 NEMI 04/01/2000 

0524.1 VOC - by Purge & Trap/Packed Column GS/MS 600/4-88-039 www 07/01/1991 

0524.2 Purgeable organic compounds - capillary column CD 08/01/1992 

0524.2 VOCs (MTBE) - Purge & Trap / Cap Column GC/MS 600/R-95-131 NEMI 08/01/1995 

0525 Organic Compounds in Drinking Water by LSE/GC/M 01A0008190 01/01/1988 

0525.1 Organic Compounds by Liquid/Solid Extract GCMS 600/4-88-039 www 07/01/1991 

0525.1 Organic Compounds in Drinking Water by LSE/GC/M 821/R-93-010-B CD 05/01/1991 

0525.2 Organic compounds - LSE/capillary/GCMS CD 03/01/1994 

0525.2 Organic Compounds in DW by LSE/Cap Col GC/MS 600/R-95-131 NEMI 08/01/1995 

0526 Semivolatile organic by SPE & cap col GC/MS 815/R-00-014 NEMI 06/01/2000 

0528 Phenols in DW by SPE & cap col GC/MS 815/R-00-014 NEMI 04/01/2000 

0531.1 N-Methylcarbamoyloximes & N-Methylcarbamates 821/R-93-010-B CD 01/01/1989 

0531.1 N-Methylcarbamoylozimes/ates - Aqueous In/HPLC 600/R-95-131 NEMI 08/01/1995 

0531.2 N-Methylcarbamoylozimes/ates - Aqueous In/HPLC 815/B-01-002 www 09/01/2001 

0532 Phenylurea compounds in DW by SPE & HPLC/UV 815/R-00-014 NEMI 06/01/2000 

0547 Glyphosate by HPLC 600/4-90-020 NEMI 07/01/1990 

0547 Glyphosate in DW - Direct-Aqueous-Injection HPLC 821/R-93-010-B CD 07/01/1990 

0548 Endothall in DW - LSE 600/4-90-020 www 07/01/1990 

0548 Endothall in DW - LSE/GC/ECD 821/R-93-010-B CD 07/01/1990 

0548.1 Endothall by LSE & GC/MS 600/R-92-129 NEMI 08/01/1992 

0548.1 Endothall in DW - Ion-Exchange Extraction/GCMS 821/R-93-010-B CD 08/01/1992 

0549 Herbicides (Diquat & Paraquat) by LSE 600/4-90-020 www 07/01/1990 

0549.1 Diquat & Paraquat by LSE & HPLC with Ultraviolet 600/R-92-129 www 08/01/1992 

0549.2 Diquat & Paraquat - LSE / HPLC/UD 815/R-00-014 NEMI 06/01/1997 

0550 PAHs by Liquid-Liquid Extraction (LLE) & HPLC 600/4-90-020 NEMI 07/01/1990 

04/16/2003 see Sources list for full reference and website address Method Number Index Page 11 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

0550.1 PAHs by Liquid-Solid Extraction (LSE) & HPLC 600/4-90-020 NEMI 07/01/1990 

0551 Chlorination Disinfection Byproducts/Solvents 600/4-90-020 www 07/01/1990 

0551 Trihalomethanes, Total by LLE/GC/ECD 600/4-90-020 www 07/01/1990 

0551.1 Chlorination Disinfection Byproducts, Pesticides 600/R-95-131 NEMI 08/01/1995 

0552 Haloacetic Acids by LLE & GC/ECD 600/4-90-020 www 07/01/1990 

0552.1 Dalapon & Haloacetic Acids by LSE & GC/ECD 600/R-92-129 NEMI 08/01/1992 

0552.2 Haloacetic Acids & Dalapon in DW by LLE/GC/ECD 600/R-95-131 NEMI 08/01/1995 

0553 Benzidine & Nitrogen-containing Pesticides 600/R-92-129 www 08/01/1992 

0553 Benzidines & Nitrogen-Containing Pesticides 821/R-93-010-B CD 08/01/1992 

0554 Carbonyl Compounds & Formaldehyde by HPLC 600/R-92-129 www 08/01/1992 

0555 Chlorinated Acids by HPLC 600/R-92-129 NEMI 08/01/1992 

0555 Chlorinated Acids in Water - HPLC 821/R-93-010-B CD 08/01/1992 

0556 Carbonyl Compounds in DW by PD/GC/ECD 01A0007878 NEMI 06/01/1998 

0556.1 Carbonyl compounds in DW by fast GC 815/R-00-014 NEMI 09/01/1999 

0601 Purgeable Halocarbons /waterscience 136 App A NEMI 

0602 Benzene, Chlorobenzene, Ethylbenzene. /waterscience 136 App A NEMI 

0602 Purgeable Aromatics /waterscience 136 App A NEMI 

0602 Toluene, Dichlorobenzene, 1,3 & 1,2 & 1,4 /waterscience 136 App A NEMI 

0603 Acrolein & Acrylonitrile /waterscience 136 App A NEMI 

0604 Phenols /waterscience 136 App A NEMI 

0604.1 Dichlorophen & Hexachlorphene 821/R-93-010-A CD 06/01/1993 

0605 Benzidines /waterscience 136 App A NEMI 

0606 Phthalate Ester /waterscience 136 App A NEMI 

0607 Nitrosamines /waterscience 136 App A NEMI 

0608 PCBs & Organochlorine Pesticides /waterscience 136 App A NEMI 

0608.1 Organochlorine Pesticides in Wastewater 821/R-93-010-A CD 06/01/1993 

0608.2 Chlorothalonil, DCPA, Dichloran, Methoxychlor 821/R-93-010-A CD 06/01/1993 

0608.2 Organochlorine Pesticides in Wastewater - GC 821/R-93-010-A CD 06/01/1993 

0608.2 Permethrin 821/R-93-010-A CD 06/01/1993 

0609 Nitroaromatics and Isophorone /waterscience 136 App A NEMI 

0610 Polynuclear Aromatic Hydrocarbons /waterscience 136 App A NEMI 

0611 Haloethers /waterscience 136 App A NEMI 

0612 Chlorinated Hydrocarbons /waterscience 136 App A NEMI 

0613 Dioxin, TCDD [use 1613A] /waterscience 136 App A NEMI 

0614 Pesticides, Organophosphorus In WW 821/R-93-010-A CD 06/01/1993 

0614.1 Pesticides, Organophosphorous in WW 821/R-93-010-A CD 06/01/1993 

0614.1 Pesticides: Ethion/EPN/Dioxathion/Terbufos 821/R-93-010-A CD 06/01/1993 

0615 Herbicides, Chlorinated (Dinoseb) - Wastewater 821/R-93-010-A CD 06/01/1993 

0616 Cycloprate/Kinoprene/Methoprene/Resmethrin 821/R-93-010-A CD 06/01/1993 

0616 Pesticides, Carbon/Hydrogen/Oxygen Containing 821/R-93-010-A CD 06/01/1993 

0617 Pesticides, Organohalide & PCBs in WW 821/R-93-010-A CD 06/01/1993 

0618 Pesticides, Volatile:Chloropicrim/Ethyl Dibromid 821/R-93-010-A CD 06/01/1993 

0619 Pesticides, Triazine: Simetryn/Terbutryn in WW 821/R-93-010-A CD 06/01/1993 

0620 Diphenylamine - Wastewater by GC 821/R-93-010-A CD 06/01/1993 

0622 Pesticides, Organophosphorus: Trichloronate - WW 821/R-93-010-A CD 06/01/1993 

0622.1 Pesticides, Thiophosphate:Aspon/Phosmet/Thionazi 821/R-93-010-A CD 06/01/1993 

0624 Purgeables /waterscience 136 App A NEMI 

0624-S Organic Priority Pollutants in Sludges 600/4-84-001 

04/16/2003 see Sources list for full reference and website address Method Number Index Page 12 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

0625 Acids and Base/Neutrals including PCBs /waterscience 136 App A NEMI 

0625-S Priority Pollutants, Organic, in Sludges 600/4-84-001 

0627 Pesticides, Dinitroaniline in Wastewater 821/R-93-010-A CD 06/01/1993 

0629 Cyanazine - Pesticides in Wastewater 821/R-93-010-A CD 06/01/1993 

0630 AOP/Busan/Carban/Ferban/Mancozeb/Maneb/Metham 821/R-93-010-A CD 06/01/1993 

0630 KN Methyl/Polyram/Thiram/Zineb/Ziram/ZAC 821/R-93-010-A CD 06/01/1993 

0630 Nabam/Niacide/Sodium Dimethyldithiocarbamate 821/R-93-010-A CD 06/01/1993 

0630 Pesticides, Dithiocarbamates in Wastewater 821/R-93-010-A CD 06/01/1993 

0630.1 Amobam/Busan/Ferbam/KN Methyl/Nabam/Nabonate 821/R-93-010-A CD 06/01/1993 

0630.1 EDX/Metham/Thiram/Zineb/Ziram 821/R-93-010-A CD 06/01/1993 

0630.1 Pesticides, Dithiocarbamates by GC 821/R-93-010-A CD 06/01/1993 

0631 Pesticides: Benomyl & Carbendazim in Wastewater 821/R-93-010-A CD 06/01/1993 

0632 Carbofuran/Fluometuron/Methomyl/Oxamyl - in WW 821/R-93-010-A CD 06/01/1993 

0632 Pesticides, Carbamate and Urea 821/R-93-010-A CD 06/01/1993 

0632.1 Pesticides, Carbamate & Amide 821/R-93-010-A CD 06/01/1993 

0632.1 Pesticides: Napropamide/Propanil/Vacor 821/R-93-010-A CD 06/01/1993 

0633 Metribuxin/Terbacil/Triadimefon/Tricyclozole 821/R-93-010-A CD 06/01/1993 

0633 Pesticides, Organonitrogen:Bromacil/Deet/Hexazin 821/R-93-010-A CD 06/01/1993 

0633.1 Pesticides, Netural Nitrogen-Containing 821/R-93-010-A CD 06/01/1993 

0633.1 Pesticides: Fenarimol/MGK/Pronamide 821/R-93-010-A CD 06/01/1993 

0634 Butylate/cycloate/EPTC/Molinate/Pebulate/Vernola 821/R-93-010-A CD 06/01/1993 

0634 Pesticides, Thiocarbamate in WW - GC 821/R-93-010-A CD 06/01/1993 

0635 Rotenone - LC 821/R-93-010-A CD 06/01/1993 

0636 Bensulide - LC 821/R-93-010-A CD 06/01/1993 

0637 MBTS & TCMTB in Wastewater by LC 821/R-93-010-A CD 06/01/1993 

0638 Oryzalin in Wastewater 821/R-93-010-A CD 06/01/1993 

0639 Bendiocarb - Wastewater by LC 821/R-93-010-A CD 06/01/1993 

0640 Mercaptobenzothiazole in Wastewater by LC 821/R-93-010-A CD 06/01/1993 

0641 Thiabendazole 821/R-93-010-A CD 08/01/1993 

0642 Biphenyl and o-Phenylphenol by LC 821/R-93-010-A CD 06/01/1993 

0643 Bentazon (Basagran) - Wastewater by LC 821/R-93-010-A CD 06/01/1993 

0644 Picloram in Wastewater - LC 821/R-93-010-A CD 06/01/1993 

0645 Alachlor/Butachlor/Diphenamid/Norflurazon/Flurid 821/R-93-010-A CD 06/01/1993 

0645 Pesticides, Certain Amine & Lethane in WW - GC 821/R-93-010-A CD 06/01/1993 

0646 Pesticides, Dinitro Aromatic by GC 821/R-93-010-A CD 06/01/1993 

0646 Pesticides: Basalin (Fluchloralin)/CDN/Dinocap 821/R-93-010-A CD 06/01/1993 

0680 PCBs & pesticides in water & soil/sediment -GCMS 01A0005295 CD 11/01/1985 

0681 Dioxins & Furans, Chlorinated (CDD & CDF) - Soil 01A0006706 12/15/1986 

0810 Product performance test guidelines - TSCA/FIFRA www OPPT 

0830 Product properties test guidelines - TSCA/FIFRA www OPPT 09/22/1996 

0835 Fate, transport & transformation guidelines TSCA/FIFRA www OPPT 04/21/1996 

0840 Spray drift test guidelines - TSCA/FIFRA www OPPT 

0850 Ecological effects test guidelines - TSCA/FIFRA www OPPT 05/01/1996 

0860 Residue chemistry test guidelines - TSCA/FIFRA www OPPT 

0870 Health effects test guidelines - TSCA/FIFRA www OPPT 06/25/1996 

0875 Occupational & residential exposure guidelines TSCA/FIFRA www OPPT 09/29/1996 

0880 Biochemicals test guidelines - TSCA/FIFRA www OPPT 09/25/1996 

0885 Microbial pesticide test guidelines - TSCA/FIFRA www OPPT 

04/16/2003 see Sources list for full reference and website address Method Number Index Page 13 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

0900 Radioactivity, Gross Alpha and Gross Beta 600/4-80-032 NEMI 08/01/1980 

0900.1 Radium, Gross Alpha Screening Procedure 600/4-80-032 www 

0901 Radioactive Cesium 600/4-80-032 www 08/01/1980 

0901.1 Radionuclides, Gamma Emitting 600/4-80-032 www 

0902 Radioactive Iodine 600/4-80-032 www 

0903 Radium, Alpha-Emitting Isotopes 600/4-80-032 www 08/01/1980 

0903.1 Radium-226 Radon Emanation Technique 600/4-80-032 NEMI 08/01/1980 

0904 Radium-228 600/4-80-032 www 

0905 Radioactive Strontium 600/4-80-032 www 

0906 Tritium 600/4-80-032 www 

0907 Actinide Elements 600/4-80-032 www 

0908 Uranium - Radiochemical Method 600/4-80-032 www 

0908.1 Uranium - Fluorometric Method 600/4-80-032 www 

0908.2 Uranium - Laser Indirect Fluorometry in DW 600/4-80-032 www 

0909 Lead-210 in Drinking Water 01A0004860 

0910 Thorium - Drinking Water 01A0004860 

0911 Plutonium in Drinking Water 01A0004860 

0912 Polonium-210 in Drinking Water 01A0004860 

0913 Radon in DW by Liquid Scintillation Counting 01A0006252 05/01/1991 

1000 Survival & Growth - Fathead Minnow Larval 821/R-02-013 WET www 10/01/2002 

1001 Lead in DW by DPASV (differential pulse anodic) 01A0007909 08/01/1999 

1001 Survival & Teratogenicity -Fathead Minnow Larval 821/R-02-013 WET www 10/01/2002 

1002 Survival & Reproduction - Ceridaphnia 821/R-02-013 WET www 10/01/2002 

1003 Growth of Green Alga - Chronic Toxicity 821/R-02-013 WET www 10/01/2002 

1004 Survival & Growth - Sheepshead Minnow Larval 821/R-02-014 WET www 10/01/2002 

1005 Shell Development - Pacific Oyster & Mussel 600/R-95-136 www 08/01/1995 

1005 Survival & Teratogenicity - Minnow Embryo Larval 821/R-02-014 WET www 10/01/2002 

1006 Larval Survival & Growth - Inland Silverside 821/R-02-014 WET www 10/01/2002 

1006 Larval Survival & Growth - Toppsmelt 600/R-95-136 www 08/01/1995 

1007 Survival & Growth - Mysid 600/R-95-136 www 08/01/1995 

1007 Survival, Growth & Fecundity - Mysid 821/R-02-014 WET www 10/01/2002 

1008 Fertilization - Sea Urchin & Sand Dollar 600/R-95-136 www 08/01/1995 

1008 Fertilization, Sea Urchin - Chronic Toxicity 821/R-02-014 WET www 10/01/2002 

1009 Germination & Germ-Tube Length - Giant Kelp 600/R-95-136 www 08/01/1995 

1009 Reproduction - Red Macroalga 821/R-02-014 WET www 10/01/2002 

1010 Ignitability - Pensky-Martins Closed-Cup Method SW-846 Ch 8.1 www 09/01/1986 

1010A Ignitability - Pensky-Martins Closed-Cup Method SW-846 Ch 8 Update IIIB www 10/30/2002 

1020A Ignitability - Setaflash Closed-Cup Method SW-846 Ch 8.1 www 07/01/1992 

1020B Ignitability - Small scale closed-cup Method SW-846 Ch 8 Update IIIB www 10/30/2003 

1030 Ignitability of Solids SW-846 Ch 6 www 12/01/1996 

1040 Oxidizing Solids (conical pile type burning UN) SW-846 www Update IVB www 09/01/1199 

1050 Substances Liable to Spontaneous Combustion SW-846 www Update IVB www 07/01/1999 

1103.1 E. coli & Enterococci in Water - Membrane Filter 600/4-85-076 www 07/01/1985 

1103.1 E. coli modified (mTEC) 821/R-97-004 www 03/01/2000 

1104 E. coli in Drinking Water/EC Medium with Mug Tub 600/4-91-016 www 07/01/1991 

1105 E. coli in Drinking Water /Nutrient Agar/Mug Tub 600/4-91-016 www 07/01/1991 

1106.1 Enterococci Bacteria in Water by Membrane Filter 600/4-85-076 www 07/01/1985 

1106.1 Original Enterocci method 821/R-97-004 www 03/01/2000 

04/16/2003 see Sources list for full reference and website address Method Number Index Page 14 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

1110 Corrosivity Toward Steel SW-846 Ch 8.2 www 09/01/1986 

1110A Corrosivity Toward Steel SW-846 Ch 8 Update IIIB www 10/30/2002 

1120 Dermal Corrosion SW-846 Ch 6 www 12/01/1996 

1310A Extraction Procedure (EP) Toxicity Test SW-846 Ch 8.4 www 07/01/1992 

1310B Extraction Procedure (EP) Toxicity & struct inte SW-846 Ch 8 Update IIIB www 10/30/2002 

1311 TCLP (Toxicity Characteristic Leaching Procedure SW-846 Ch 8.4 www 07/01/1992 

1312 Synthetic Precipitation Leaching Procedure SW-846 Ch 6 www 09/01/1994 

1320 Extraction Procedure, Multiple for Delisting SW-846 Ch 6 www 09/01/1986 

1330A Extraction Procedure for Oily Wastes SW-846 Ch 6 www 07/01/1992 

1556A Organohalide pesticides -ww, soil, tissue-GC/HSD 821/R-93-017 www 

1600 Membrane Filter for Enterococci (mEI Agar) 821/R-97-004 /microbes www 05/01/1997 

1601 Somatic Coliphage in DW enrichment presence 821/R-01-030 /nerlcwww www 04/01/2001 

1602 Male-specific & somatic coliphage by SAL 821/R-01-029 /nerlcwww www 04/01/2001 

1605 Aeromonas -finished water / membrane filtration 821/R-01-034 /nerlcwww www 09/01/2000 

1613 Dioxins & Furans - HRGC/HRMS 821/B-94-005 NEMI 10/01/1994 

1613A Furans (CDFs) & Dioxins, Tetra- through Octa 821/R-93-017 www 10/01/1993 

1613B Dioxins, tetra- thru octa- (CDDs) & Furans (CDFs 821/B-94-005 136 App A www 10/01/1994 

1618 Aldrin/Chlordane/Diazinon/Dinoseb/Endrin/Phosmet 01A0006086 07/01/1989 

1618 Herbicides, Phenoxy-acid by Wide Bore Capillary 01A0006086 07/01/1989 

1618 Pesticides, Organo-halide/phosphorus:Malathion 01A0006086 07/01/1989 

1620 Metals by ICP, FGAA and CVAA 01A0006085 CD 09/01/1989 

1622 Cryptosporidium in Water by Filtration/IMS/FA 821/R-01-026 NEMI 04/01/2001 

1623 Cryptosporidium & Giardia by Filtration/IMS/FA 821/R-01-025 NEMI 04/01/2001 

1624B Volatile Organic Compounds - Isotope Dilution 136 App A NEMI 

1624C Volatile Organics/VOCs by Isotope Dilution GCMS 01A0006089 CD 01/22/1991 

1625B Semivolatile Organic Compounds -Isotope Dilution 136 App A NEMI 

1625C Semivolatile Organic Compounds/Isotope Dillution 01A0006089 CD 01/22/1991 

1630 Methyl Mercury in Water by Distillation...CVAFS 01A0007846 NEMI 08/01/1998 

1631 Mercury in Water/ Oxidation, Purge & Trap, CVAFS 821/R-96-012 CD 01/01/1996 

1631B Mercury in Water by Oxidation Purge & Trap CVAFS 821/R-99-005 136 App A www 06/08/1999 

1631C Mercury in Water by Oxidation Purge & Trap CVAFS 821/R-01-024 NEMI 03/01/2001 

1631D Mercury in Water by Oxidation Purge & Trap CVAFS 821/R-02-019 www 08/01/2002 

1632 Inorganic Arsenic - hydride generation FAA 821/R-96-013 NEMI 07/01/1996 

1632A Arsenic in Water & tissue by HGQ/FAA 821/R-01-006 SEL2-TRA 01/01/2000 

1636 Choromium, Hexavalent by Ion Chromatography 821/R-96-003 NEMI 01/01/1996 

1637 Trace Elements in Ambient Waters by Chelation 821/R-96-004 NEMI 01/01/1996 

1638 Trace Elements in Ambient Waters by ICP/MS 821/R-96-005 NEMI 01/01/1996 

1639 Trace Elements in Ambient Waters by Stabilized 821/R-96-006 NEMI 01/01/1996 

1640 Trace Elements in Ambient Waters by On-Line Chel 821/R-96-007 NEMI 01/01/1996 

1648 Organic Halides - Solid Matrices/Neutron Activat CD 06/01/1991 

1650 Organic Halides, Absorbable (AOX) ver 1 CD CD 11/01/1996 

1650B Organic Halides, Absorbable (AOX) 821/R-93-017 www 10/01/1993 

1650C Adsorbably organic halides - Adsorption/titratio CD 08/01/1997 

1651 Oil & Diesel Oil / Drilling Muds & Drill Cutting 821/R-92-008 www 12/01/1992 

1653 Chlorinated Phenolics - In Situ Acetylation/GCMS 821/R-93-017 NEMI 12/01/1991 

1653A Chlorinated Phenolics - In Situ Acetylation/GCMS CD 11/01/1996 

1654 PAH Content of Oil by HPLC/UV 821/R-92-008 www 12/01/1992 

1656 Organohalide Pesticides 821/R-93-010-A CD 06/01/1993 

04/16/2003 see Sources list for full reference and website address Method Number Index Page 15 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

1656A Organohalides-ww, soil, sludge, sediment, tissue 821/R-00-017 SEL-01 09/01/2000 

1657 Organophosphorus Pesticides 821/R-93-010-A CD 06/01/1993 

1657A Organo-Phosphorus in ww, soil, sed, tissue 821/R-00-018 SEL2-BIO 09/01/2000 

1658 Phenoxy-Acid Pesticides 821/R-93-010-A CD 06/01/1993 

1659 Dazomet 821/R-93-010-A CD 06/01/1993 

1660 Pyrethrins & Pyrethoids 821/R-93-010-A CD 06/01/1993 

1661 Bromoxynil 821/R-93-010-A CD 06/01/1993 

1662 Total Extractable Material in Drilling Mud /SDS 821/R-92-008 www 12/01/1992 

1662A Total extractable material in drilling mud - SDS CD 

1663 Differentiation of Diesel & Crude Oil by GC/FID 821/R-92-008 www 12/01/1992 

1663A Differentiation of diesel & crude oil - GC/FI CD 

1664 Oil & Grease and Total Petroleum Hydrocarbons 821/B-94-004b NEMI 04/01/1995 

1664A Oil & Grease (HEM/SGT-HEM) by extraction 821/R-98-002 waterscien NEMI 02/01/1999 

1665 Semivolatile Organic Compounds - Pharmaceutical 821/B-94-001 CD 01/01/1995 

1666 Volatile Organic Compounds - Pharmaceutical 821/B-94-001 CD 01/01/1995 

1666A Volatile Organic Compounds by Isotope Dilution 821/B-98-016 CD 07/01/1998 

1667 Formaldehyde, Isobutyraldehyde, Furfural 821/B-94-001 CD 01/01/1995 

1667A Formaldehyde, Isobutyraidehyde, Furfural 821/B-98-016 CD 07/01/1998 

1668 PCBs in Water, Soil - Isotope Dilution HRGC/HRMS 821/R-97-001 www 03/01/1997 

1668A Chlorinated biopheny cogeners by HRGC/HRMS 821/R-00-02 www /Region8 12/01/1999 

1669 Metals, Trace at Water Quality Criteria Levels 821/R-96-008 www 01/01/1996 

1671 Volatile Organic Compounds - GC/FID 821/B-94-001 CD 01/01/1995 

1671A Volatile Organic Compounds by GC/FID 821/B-98-016 CD 07/01/1998 

1673 Poly(ethylene glycol)-600 - Pharmaceutical 821/B-94-001 NEMI 01/01/1995 

1677 OIA-Method 1677 available cyanide 821/R-99-013 ost/methods 08/01/1999 

1680 Fecal coliform in biosolids - 821/R-98-003 CD 07/01/1998 

1682 Salmonella sp. in biosolids 821/R-98-004 CD 08/01/1998 

1683 Specific oxygen uptake rate (SOUR) in biosolids 821/R-01-014 CD 02/01/2000 

1684 Total, fixed & volatile solids in biosolids 821/R-01-015 CD 02/01/1999 

1685 Nitrate/nitrite-N in biosolids - auto photometry 821/R-01-016 CD 02/01/1999 

1686 Nitrate/nitrite-N in biosolids/ manual colimetry 821/R-01-005 CD 02/01/1999 

1687 Total Kjeldahl nitrogen / prelim distill digest 821/R-01-004 CD 02/01/1999 

1688 Total Kjeldahl nitrogen /prelim semi-auto digest 821/R-01-007 CD 02/01/1999 

1689 Ammonia-N /ion-selective electrode potentiometry 821/R-01-012 CD 02/01/1999 

1690 Ammonia-Nitrogen / automated colimetry / 821/R-01-009 CD 02/01/1999 

3005A Acid Digestion of Waters for Metals - FAA/ICP SW-846 Ch 3.2 www 07/01/1992 

3010A Acid Digestion of Aqueous Samples for Metals SW-846 Ch 3.2 www 07/01/1992 

3015 Microwave Assisted Acid Digestion/Aqueous Metals SW-846 Ch 3.2 www 09/01/1994 

3015A Microwave Assisted Acid Digestion Aqueous Sample SW-846 Ch 3.2 Update IVA www 01/01/1998 

3020A Acid Digestion of Aqueous Samples - Metals/GFAA SW-846 Ch 3.2 www 07/01/1992 

3031 Acid Digestion of Oils for Metals by FLAA or ICP SW-846 Ch 3.2 www 12/01/1996 

3040A Dissolution Procedure for Oils, Greases or Waxes SW-846 Ch 3.2 www 12/01/1996 

3050B Acid Digestion of Sediments, Sludges and Soils SW-846 Ch 3.2 www 12/01/1996 

3051 Microwave Assisted Acid Digestion/Sludges, Soils SW-846 Ch 3.2 www 09/01/1994 

3051A Microwave Asst Acid Digestion Sediments/Soil/Oil SW-846 Ch 3.2 Update IVA www 01/01/1998 

3052 Microwave Assisted Acid Digestion of Siliceous.. SW-846 Ch 3.2 www 12/01/1996 

3060A Alkaline Digestion for Hexavalent Chromium SW-846 Ch 3.2 www 12/01/1996 

3200 Organic, inorganic & total mercury in soils not available SW-846 dev 

04/16/2003 see Sources list for full reference and website address Method Number Index Page 16 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

3500B Organic Extractin & Sample Preparation SW-846 Ch 4.2.1 www 12/01/1996 

3500C Organic Extraction and Sample Preparation SW-846 www Update IVB www 01/01/1999 

3510C Separatory Funnel Liquid-Liquid Extraction SW-846 Ch 4.2.1 www 12/01/1996 

3511 Organic compounds in water by microextraction SW-846 new www 11/01/2002 

3520C Continuous Liquid-Liquid Extraction - Organics SW-846 Ch 4.2.1 www 12/01/1996 

3535 Solid Phase Extraction (SPE) - Organics SW-846 Ch 4.2.1 www 12/01/1996 

3535A Solid Phase Extraction (SPE) SW-846 Ch 4.2.1 Update IVA www 01/01/1998 

3535A Solid Phase Extraction (SPE) including explosive SW-846 Ch 4.2.1 Update IVB www 11/01/1998 

3540C Soxhlet Extraction - Organics SW-846 Ch 4.2.1 www 12/01/1996 

3541 Automated Soxhlet Extraction SW-846 Ch 4.2.1 www 09/01/1994 

3542 Extraction of Semivolatile Analytes using 0010 SW-846 Ch 4.2.1 www 12/01/1996 

3545 Accelerated Solvent Extraction - Organics SW-846 Ch 4.2.1 www 12/01/1996 

3545A Pressurized Fluid Extraction (PFE) SW-846 Ch 4.2.1 Update IVA www 01/01/1998 

3546 Microwave Extraction SW-846 www Update IVB www 09/01/1999 

3550B Ultrasonic Extraction - Organics SW-846 Ch 4.2.1 www 12/01/1996 

3550C Ultrasonic Extraction (non or semi-volatile) SW-846 www Update IVB www 03/01/1999 

3560 Supercritical Fluid Extraction - TRPH (Petroleum SW-846 Ch 4.2.1 www 12/01/1996 

3561 Supercritical Fluid Extraction - PAH SW-846 Ch 4.2.1 www 12/01/1996 

3562 SFE of PCBs & Orgaochlorine Pesticides (OCPs) SW-846 Ch 4.2.1 Update IVA www 01/01/1998 

3570 Microscale solvent extraction (MSE) SW-846 new www 11/01/2002 

3580A Waste Dilution SW-846 Ch 4.2.1 www 07/01/1992 

3585 Waste Dilution for Volatile Organics SW-846 Ch 4.2.1 www 12/01/1996 

3600C Cleanup SW-846 Ch 4.2.2 www 12/01/1996 

3610B Alumina Cleanup SW-846 Ch 4.2.2 www 12/01/1996 

3611B Alumina Column Cleanup & Separation Petroleum SW-846 Ch 4.2.2 www 12/01/1996 

3620B Florisil Column Cleanup SW-846 Ch 4.2.2 www 12/01/1996 

3620C Florisil cleanup SW-846 www Update IVB www 01/01/1999 

3630C Silica Gel Cleanup (florisil) SW-846 Ch 4.2.2 www 12/01/1996 

3640A Gel-Preparation Cleanup SW-846 Ch 4.2.2 www 09/01/1994 

3650B Acid Base Partition Cleanup SW-846 Ch 4.2.2 www 12/01/1996 

3660B Sulfur Cleanup SW-846 Ch 4.2.2 www 12/01/1996 

3665A Sulfuric Acid/Permanganate Cleanup SW-846 Ch 4.2.2 www 12/01/1996 

3810 Headspace - Screening Method (5021 replacement) SW-846 Ch 4.5 www 09/01/1986 

3815 Screen for Use of High of Low-Level VOA Prep/PID SW-846 www Update IVB www 09/01/1999 

3820 Hexadecane Extraction & Screening of Organics SW-846 Ch 4.5 www 09/01/1986 

4000 Immunoassay SW-846 Ch 4.4 www 12/01/1996 

4010A Pentachlorophenol Screening by Immunoassay SW-846 Ch 4.4 www 12/01/1996 

4015 2,4-Dichlorophenoxyacetic Acid by Immunoassay SW-846 Ch 4.4 www 12/01/1996 

4020 PCBs Screening by Immunoassay SW-846 Ch 4.4 www 12/01/1996 

4025 Dioxin PCDD/Fs screening by Immunoassay SW-846 new www 10/01/2002 

4026 Coplanar polychlorinated biphernyls (PCBs) not available SW-846 dev 

4030 Petroleum Hydrocarbons Soil Screen by Immunoassy SW-846 Ch 4.4 www 12/01/1996 

4035 PAHs Soil Screening by Immunoassy SW-846 Ch 4.4 www 12/01/1996 

4040 Toxaphene Soil Screening by Immunoassy SW-846 Ch 4.4 www 12/01/1996 

4041 Chlordane Soil Screening by Immunoassy SW-846 Ch 4.4 www 12/01/1996 

4042 DDT Soil Screening by Immunoassy SW-846 Ch 4.4 www 12/01/1996 

4050 TNT Explosives in Water and Soils by Immunoassy SW-846 Ch 4.4 www 12/01/1996 

4051 RDX in Soil and Water by Immunoassay SW-846 Ch 4.4 www 12/01/1996 

04/16/2003 see Sources list for full reference and website address Method Number Index Page 17 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

4425 PCBs, Dioxins/Furans PAH - HRGS SW-846 www Update IVB www 09/01/1999 

4430 Dioxin TEQ by DELFIA Immunoassay not available SW-846 dev

4500 Mercury in Soil by Immunoassay SW-846 Ch 3.3 Update IVA www 01/01/1998

4510 Lead in water & soil by immunoassay not available SW-846 dev

4655 TNT and RDX - Flow cell detection Immunoassay not available SW-846 dev

4656 TNT and RDX - fiberoptic florescent Immunoassay not available SW-846 dev

4670 Triazine Herbicides as Atrazine by Immunoassay SW-846 Ch 4.4 Update IVA www 01/01/1998

5000 Sample Preparation for Volatile Organics SW-846 Ch 4.2.1 www 12/01/1996

5021 VOCs in Soils/Solid Matrices by Equilibrium Head SW-846 Ch 4.2.1 www 12/01/1996

5030B Purge & Trap for Aqueous Samples - Organic SW-846 Ch 4.2.1 www 12/01/1996

5031 Volatile, Nonpurgeable, Water-Soluble by Azeotro SW-846 Ch 4.2.1 www 12/01/1996

5032 Volatile Organic Compounds - Vacuum Distillation SW-846 Ch 4.2.1 www 12/01/1996

5035 Closed-System Purge/Trap/Extraction - Organics SW-846 Ch 4.2.1 www 12/01/1996

5035 CLP- Volatiles in low level soils OLM04.2 www clp

5035A Closed-System Purge/Trap/Extraction - Organics SW-846 new www 07/01/2002

5041A Desorption Sorbent Cartridges VOST - Cap GC/MS SW-846 Ch 4.2.1 www 12/01/1996

5050 Bomb Preparation Method for Solid Waste/Metallic SW-846 Ch 5 www 09/01/1994

6010B Inorganics by ICP - Atomic Emission Spectroscopy SW-846 Ch 3.3 www 12/01/1996

6010C Inorganics by ICP - AES SW-846 Ch 3.3 Update IVB www

6020 Metals by ICP/MS SW-846 Ch 3.3 www 09/01/1994

6020 CLP- Inductively Coupled Plasma - Mass Spectrometry 01A0007861 05/01/1990

6020A Inductively Coupled Plasma/MS SW-846 Ch 3.3 Update IVA www 01/01/1998

6200 Field Portable X-Ray Fluorescence Spectrometry SW-846 Ch 3.3 Update IVA www 01/01/1998

6250 X-ray fluorescence spect elemental concentration not available SW-846 dev

6300 X-ray diffraction - crystalline phases not available SW-846 dev

6500 Inorganic Anions in Aqueous Matrices - CIE SW-846 Ch 3.3 Update IVA www 01/01/1998

6800 Elemental & Speciated Isotope Dilution MS SW-846 Ch 3.3 Update IVA www 01/01/1998

7000A Metals by AA (Atomic Absorption Methods) SW-846 Ch 3.3 www 07/01/1992

7000B Flame Atomic Absorption Specto (Consolidate FLAA SW-846 Ch 3.3 Update IVA www 01/01/1998

7010 Graphite Furnace Atomic Absorption (GFAA) SW-846 Ch 3.3 Update IVA www 01/01/1998

7020 Aluminum - AA, Direct Aspiration SW-846 Ch 3.3 www 09/01/1986

7040 Antimony - AA, Direct Aspiration SW-846 Ch 3.3 www 09/01/1986

7041 Antimony - AA, Furnace Technique SW-846 Ch 3.3 www 09/01/1986

7060A Arsenic - AA, Furnace Technique SW-846 Ch 3.3 www 09/01/1994

7061A Arsenic - AA, Gaseous Hydride SW-846 Ch 3.3 www 07/01/1992

7062 Antimony & Arsenic - AA, Gaseous Borohydride SW-846 Ch 3.3 www 09/01/1994

7063 Arsenic in Aqueous Samples & Extracts by ASV SW-846 Ch 3.3 www 12/01/1996

7080A Barium - AA, Direct Aspiration SW-846 Ch 3.3 www 09/01/1994

7081 Barium - AA, Furnace Technique SW-846 Ch 3.3 www 07/01/1992

7090 Beryllium - AA, Direct Aspiration SW-846 Ch 3.3 www 09/01/1986

7091 Beryllium - AA, Furnace Technique SW-846 Ch 3.3 www 09/01/1986

7130 Cadmium - AA, Direct Aspiration SW-846 Ch 3.3 www 09/01/1986

7131A Cadmium - AA, Furnace Technique SW-846 Ch 3.3 www 09/01/1994

7140 Calcium - AA, Direct Aspiration SW-846 Ch 3.3 www 09/06/1986

7190 Chromium - AA, Direct Aspiration SW-846 Ch 3.3 www 09/01/1986

7191 Chromium - AA, Furnace Technique SW-846 Ch 3.3 www 09/01/1986

7195 Chromium, Hexavalent - Coprecipitation Method SW-846 Ch 3.3 www 09/01/1986

7196A Chromium, Hexavalent - Colorimetric Method SW-846 Ch 3.3 www 07/01/1992

04/16/2003 see Sources list for full reference and website address Method Number Index Page 18 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

7197 Chromium, Hexavalent - Chelation Extraction SW-846 Ch 3.3 www 09/01/1986 

7198 Chromium, Hexavalent - Diff. Pulse Polarography SW-846 Ch 3.3 www 09/01/1986 

7199 Hexavalent Chromium in DW, GW, WW by Ion Chro SW-846 Ch 3.3 www 12/01/1996 

7200 Cobalt - AA, Direct Aspiration SW-846 Ch 3.3 www 09/01/1986 

7201 Cobalt - AA, Furnace Technique SW-846 Ch 3.3 www 09/01/1986 

7210 Copper - AA, Direct Aspiration SW-846 Ch 3.3 www 09/01/1986 

7211 Copper - AA, Furnace Technique SW-846 Ch 3.3 www 07/01/1992 

7380 Iron - AA, Direct Aspiration SW-846 Ch 3.3 www 09/01/1986 

7381 Iron - AA, Furnace Technique SW-846 Ch 3.3 www 07/01/1992 

7420 Lead - AA, Direct Aspiration SW-846 Ch 3.3 www 09/01/1986 

7421 Lead - AA, Furnace Technique SW-846 Ch 3.3 www 09/01/1986 

7430 Lithium - AA, Direct Aspiration SW-846 Ch 3.3 www 07/01/1992 

7450 Magnesium - AA, Direct Aspiration SW-846 Ch 3.3 www 09/01/1986 

7460 Manganese - AA, Direct Aspiration SW-846 Ch 3.3 www 09/01/1986 

7461 Manganese - AA, Furnace Technique SW-846 Ch 3.3 www 07/01/1992 

7470A Mercury in Liquid Waste - Manual Cold Vapor Tech SW-846 Ch 3.3 www 09/01/1994 

7471A Mercury in Solid or Semisolid Waste SW-846 Ch 3.3 www 09/01/1994 

7471B Mercury in Solid/Semisolid Waste (Manual Cold-Va SW-846 Ch 3.3 Update IVA www 01/01/1998 

7472 Mercury in Aqueous Samples & Extracts by ASV SW-846 Ch 3.3 www 12/01/1996 

7473 Mercury in Solids/Solutions - TDA/AAS SW-846 Ch 3.3 Update IVA www 01/01/1998 

7474 Mercury in Sediment & Tissue Samples by AFS SW-846 Ch 3.3 Update IVA www 01/01/1998 

7480 Molybdenum - AA, Direct Aspiration SW-846 Ch 3.3 www 09/01/1986 

7481 Molybdenum - AA, Furnace Technique SW-846 Ch 3.3 www 09/01/1986 

7520 Nickel - AA, Direct Aspiration SW-846 Ch 3.3 www 09/01/1986 

7521 Nickel by AA, Furnace Method SW-846 Ch 3.3 www 12/01/1996 

7550 Osmium - AA, Direct Aspiration SW-846 Ch 3.3 www 09/01/1986 

7580 White Phosphorus by Solvent Extraction and GC SW-846 Ch 3.3 www 12/01/1996 

7610 Potassium - AA, Direct Aspiration SW-846 Ch 3.3 www 09/01/1986 

7740 Selenium - AA, Furnace Technique SW-846 Ch 3.3 www 09/01/1986 

7741A Selenium - AA, Gaseous Hydride SW-846 Ch 3.3 www 09/01/1994 

7742 Selenium - AA, Gaseous Borohydride SW-846 Ch 3.3 www 09/01/1994 

7760A Silver - AA, Direct Aspiration SW-846 Ch 3.3 www 07/01/1992 

7761 Silver - AA, Furnace Technique SW-846 Ch 3.3 www 07/01/1992 

7770 Sodium - AA, Direct Aspiration SW-846 Ch 3.3 www 09/01/1986 

7780 Strontium - AA, Direct Aspiration SW-846 Ch 3.3 www 07/01/1992 

7840 Thallium - AA, Direct Aspiration SW-846 Ch 3.3 www 09/01/1986 

7841 Thallium - AA, Furnace Technique SW-846 Ch 3.3 www 09/01/1986 

7870 Tin - AA, Direct Aspiration SW-846 Ch 3.3 www 09/01/1986 

7910 Vanadium - AA, Direct Aspiration SW-846 Ch 3.3 www 09/01/1986 

7911 Vanadium - AA, Furnace Technique SW-846 Ch 3.3 www 09/01/1986 

7950 Zinc - AA, Direct Aspiration SW-846 Ch 3.3 www 09/01/1986 

7951 Zinc - AA, Furnace Technique SW-846 Ch 3.3 www 07/01/1992 

8000B Determinative Chromatographic Separations SW-846 Ch 4.3.1 www 12/01/1996 

8011 DBCP & EDB by Microextraction & GC SW-846 Ch 4.3.1 www 07/01/1992 

8015B Nonhalogenated Organics Using GC/FID SW-846 Ch 4.3.1 www 12/01/1996 

8015C Nohalogenated volatiles (GRO, DRO) / GC/FID SW-846 Ch 4.3 Update IVB www 

8021B Halogenated Volatiles by GC+ Cap Column SW-846 Ch 4.3.1 www 12/01/1996 

8031 Acrylonitrile by GC SW-846 Ch 4.3.1 www 09/01/1994 

04/16/2003 see Sources list for full reference and website address Method Number Index Page 19 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

8032A Acrylamide by GC SW-846 Ch 4.3.1 www 12/01/1996 

8033 Acetonitrile by GC with Nitrogen-Phosphorus SW-846 Ch 4.3.1 www 12/01/1996 

8041 Phenols by GC: Capillary Column Technique SW-846 Ch 4.3.1 www 12/01/1996 

8041A Phenols by GC: SW-846 Ch 4.3 Update IVB www 

8061A Phthalate Esters by Cap GC/ECD SW-846 Ch 4.3.1 www 12/01/1996 

8070A Nitrosamines by GC SW-846 Ch 4.3.1 www 12/01/1996 

8081A Organochlorine Pesticides by Cap Column GC SW-846 Ch 4.3.1 www 12/01/1996 

8081B Organochlorine Pesticides by GC SW-846 Ch 4.3.1 Update IVA www 01/01/1998 

8081B Organochlorine pesticides by GC with ECD or ELCD SW-846 www Update IVB www 05/01/1999 

8082 PCBs by Cap Column GC SW-846 Ch 4.3.1 www 12/01/1996 

8082A PCBs by GC SW-846 www Update IVB www 05/01/1999 

8085 Pesticides by GC/AED (Atomic Emission Detection) SW-846 Update IVB www 03/15/1999 

8091 Nitroaromatics and Cyclic Ketones - Cap Column SW-846 Ch 4.3.1 www 12/01/1996 

8095 Explosives by Gas Chromatography SW-846 www Update IVB www 11/01/1998 

8100 Polynuclear Aromatic Hydrocarbons SW-846 Ch 4.3.1 www 09/01/1986 

8111 Haloethers - Cap Column SW-846 Ch 4.3.1 www 12/01/1996 

8121 Chlorinated Hydrocarbons by GC Cap SW-846 Ch 4.3.1 www 09/01/1994 

8131 Aniline & Selected Derivatives by Cap Column GC SW-846 Ch 4.3.1 www 12/01/1996 

8141A Organophosphorus Pesticides - GC Capillary Colum SW-846 Ch 4.3.1 www 09/01/1994 

8141B Organophosphorus Compounds by GC SW-846 Ch 4.3.1 Update IVA www 01/01/1998 

8141B organophosphorus compounds by GC SW-846 Update IVB www 09/01/1999 

8151A Chlorinated Herbicides by GC+ Cap Column SW-846 Ch 4.3.1 www 12/01/1996 

8260B VOCs by GC/MS Capillary Column Technique SW-846 Ch 4.3.2 www 12/01/1996 

8261 Volatile Organic Compounds by VD/GC/MS SW-846 Update IVB www 03/15/1999 

8265 VOCs in water, soil, soil gas, air by DSITMS SW-846 new www 03/01/2002 

8270C Semivolatile Organic Compounds by GC/MS Cap Col SW-846 Ch 4.3.2 www 12/01/1996 

8270D Semivolatile Organic Compounds by GC/MS SW-846 Ch 4.3.2 Update IVA www 01/01/1998 

8275A PAHs and PCBs in Soils/Sludges by TE/GC/MS SW-846 Ch 4.3.2 www 12/01/1996 

8280A PCDD and PCDF by HRGC/LRMS SW-846 Ch 4.3.2 www 12/01/1996 

8280B PCDD and PCDF by HRGC/LRMS SW-846 Ch 4.3.2 Update IVA www 01/01/1998 

8290 PCDD & PCDF - HRGC/HRMS SW-846 Ch 4.3.3 www 09/01/1994 

8290A PCDD and PCDF by HRGC/HRMS SW-846 Ch 4.3.2 Update IVA www 01/01/1998 

8310 Polynuclear Aromatic Hydrocarbons (PAH) - HPLC SW-846 Ch 4.3.3 www 09/01/1986 

8315A Carbonyl Compounds by HPLC SW-846 Ch 4.3.3 www 12/01/1996 

8316 Acrylamide, Acrylonityrile & Acrolein - HPCL SW-846 Ch 4.3.3 www 09/01/1994 

8318 N-Methylcarbamates - HPLC SW-846 Ch 4.3.3 www 09/01/1994 

8318A N-Methylcarbamates by HPLC SW-846 www Update IVB www 09/01/1999 

8321A Solvent Extractable Non-Volatile by HPLC/TS/MS SW-846 Ch 4.3.3 www 12/01/1996 

8321B Solvent-Extractable Nonvolatile Compounds - UV SW-846 Ch 4.3.3 Update IVB www 01/01/1998 

8322 Solvent-extractable non-volatile HPLC/E/MS UV not available SW-846 dev 

8323 Organotins by micro LC-ES-ITMS SW-846 new www 02/01/2003 

8325 Solvent Extractable Non-Volatile by HPLC/PB/MS SW-846 Ch 4.3.3 www 12/01/1996 

8330 Nitroaromatics & Nitramines - HPLC SW-846 Ch 4.3.3 www 09/01/1994 

8330A Nitroaromatics & Nitramines by HPLC SW-846 Ch 4.3.3 Update IVA www 01/01/1998 

8331 Tetrazene - Reverse Phase HPLC SW-846 Ch 4.3.3 www 09/01/1994 

8332 Nitroglycerine by HPLC SW-846 Ch 4.3.3 www 12/01/1996 

8355 Polar organic compound/capillary electrophoresis not available SW-846 dev 

8410 Semivolatile Organics - GC/FT-IR Cap Column SW-846 Ch 4.3.4 www 09/01/1994 

04/16/2003 see Sources list for full reference and website address Method Number Index Page 20 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

8430 Bis(2-chloroethyl)ether Hydrolysis Prod GC/FT-IR SW-846 Ch 4.3.4 www 12/01/1996 

8440 Total Recoverable Petroleum Hydrocarbons - IS SW-846 Ch 4.3.4 www 12/01/1996 

8510 Field Method for RDX in Soil SW-846 Update IVB www 

8515 TNT in Soil by Coloimetric Screening SW-846 Ch 4.5 www 12/01/1996 

8520 Formaldehyde in Ambient Air, Continuous Measure SW-846 Ch 4.3.4 www 12/01/1996 

8535 TCE & other halogenated Aliphatic hydrocarbons SW-846 Update IVB www 09/11/2001 

8540 Pentachlorophenol (PCP) - colimetric field test SW-846 Update IVB www 

9000 Water in Wastes by Karl-Fisher Titration SW-846 Ch 3.3 Update IVA www 01/01/1998 

9001 Water in Waste Materials by Quantitative Calcium SW-846 Ch 3.3 Update IVA www 01/01/1998 

9010B Cyanide, Total and Amenable - Colorimetric, Manu SW-846 Ch 5 www 12/01/1996 

9010C Cyanide, Total and Amenable - distillation SW-846 Ch 5 Update IIIB www 10/30/2002 

9012A Total and Amenable Cyanide - Colorimentric UV SW-846 Ch 5 www 12/01/1996 

9012B Cyanide, total and amenable - colorimentric SW-846 Ch 5 Update IIIB www 02/13/2002 

9013 Cyanide Extraction for Solids & Oils SW-846 Ch 5 www 07/01/1992 

9014 Cyanide - Titrimetric & Manual Spectrophotometri SW-846 Ch 5 www 12/01/1996 

9015 Total dissolved iron cyanide by ion chromatograp not available SW-846 dev 

9020B Total Organic Halides (TOX) SW-846 Ch 5 www 09/01/1994 

9021 Purgeable Organic Halides (POX) SW-846 Ch 5 www 07/01/1992 

9022 Total Organic Halides (TOX) SW-846 Ch 5 www 09/01/1986 

9023 Extractible Organic Halides (EOX) in Solids SW-846 Ch 5 www 12/01/1996 

9030B Sulfides, Acid-Soluble & Insoluble -Distillation SW-846 Ch 5 www 12/01/1996 

9031 Extractable Sulfides SW-846 Ch 5 www 07/01/1992 

9034 Sulfides, Acid-Soluble & Insoluble - Titrimetric SW-846 Ch 5 www 12/01/1996 

9035 Sulfate - Colorimetric, Automated, Chloranilate SW-846 Ch 5 www 09/01/1986 

9036 Sulfate - Colorimetric, Automated, Methylthymol SW-846 Ch 5 www 09/01/1986 

9038 Sulfate - Turbidimetric SW-846 Ch 5 www 09/01/1986 

9040B pH - Electrometric Measurement SW-846 Ch 8.2 www 01/01/1995 

9040C pH - Electrometric Measurement SW-846 Ch 8 Update IIIB www 10/30/2002 

9041A pH - Paper Method SW-846 Ch 6 www 07/01/1992 

9045D Soil and Waste pH SW-846 Ch 6 Update IIIB www 10/30/2002 

9050A Specific Conductance SW-846 Ch 6 www 12/01/1996 

9056 Inorganic Anions by Ion Chromatography SW-846 Ch 5 www 09/01/1994 

9056A Inorganic Anions by Ion Chromatography SW-846 Ch 5 Update IVB www 

9057 Chloride - Methods 50/51 by Anion Chromatography SW-846 Ch 5 www 12/01/1996 

9058 Perchlorate by Ion Chromatography SW-846 Update IVB www 

9060 Total Organic Carbon SW-846 Ch 5 www 09/01/1986 

9060A Total Organic Carbon SW-846 Ch 5 Update IIIB www 10/30/2002 

9065 Phenolics - Spectrophotometric, Manual 4-AAP SW-846 Ch 5 www 09/01/1986 

9066 Phenolics - Colorimetric Automated 4-AAp SW-846 Ch 5 www 09/01/1986 

9067 Phenolics - Spectrophotometric, MBTH SW-846 Ch 5 www 09/01/1986 

9070 Oil & Grease, Total Recoverable - Gravimetric SW-846 Ch 5 replaced by 9070A&1664 09/01/1986 

9070A n-Hexane extractable meterial (HEM) - aqueous SW-846 Ch 5 Update IIIB www 10/30/2002 

9070A* Oil & grease method - referral to Method 1664 www 05/14/1999 

9071A Oil & Grease - Extraction for Sludge & Sediment SW-846 Ch 5 www 09/01/1994 

9071B n-Hexane extractable material (HEM)/oil & grease www 04/01/1998 

9074 Petroleum Hydrocarbons in Soil by Turbidmetric SW-846 Ch 4.5 Update IVA www 01/01/1998 

9075 Total Chlorine - New & Used Petroleum Prod/XRF SW-846 Ch 5 www 09/01/1994 

9076 Total Chlorine - New & Used Petroleum/Oxidative SW-846 Ch 5 www 09/01/1994 

04/16/2003 see Sources list for full reference and website address Method Number Index Page 21 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

9077 Total Chlorine - New & Used Petroleum-Field Kit SW-846 Ch 5 www 09/01/1994 

9078 PCBs in Soil Screening Test SW-846 Ch 4.5 www 12/01/1996

9079 PCBs in Transformer Oil Screening Test SW-846 Ch 4.5 www 12/01/1996

9080 Cation-Exchange Capacity of Soils (Ammonium) SW-846 Ch 6 www 09/01/1986

9081 Cation-Exchange Capacity of Soils (Sodium) SW-846 Ch 6 www 09/01/1986

9090A Compatibility Test / Wastes & Membrane Liners SW-846 Ch 6 www 07/01/1992

9095A Paint Filter Liquids Test SW-846 Ch 6 www 12/01/1996

9095B Paint Filter Liquids Test SW-846 Ch 6 Update IIIB www 10/30/2002

9096 Liquid Release Test (LRT) Procedure SW-846 Ch 6 www 09/01/1994

9100 Conductivity, Hydraulic/Leachate/Permeability SW-846 Ch 6 www 09/01/1986

9131 Total Coliform - Multiple Tube Fermentation SW-846 Ch 5 www 09/01/1986

9132 Total Coliform - Membrane Filter SW-846 Ch 5 www 09/01/1986

9210 Nitrate - Potentiometric in Aqueous/Ion-Sel Elec SW-846 Ch 5 www 12/01/1996

9210A Nitrate - Potentiometric in Aqueous/Ion-Sel Elec SW-846 Ch 5 Update IVB www

9211 Bromide - Potentiometric in Aqueous/Ion-Sel Elec SW-846 Ch 5 www 12/01/1996

9212 Chloride - Potentiometric in Aqueous/Ion-Sel Ele SW-846 Ch 5 www 12/01/1996

9213 Cyanide - Potentiometric in Aqueous/Ion-Sel Ele SW-846 Ch 5 www 12/01/1996

9214 Fluoride - Potentiometric in Aqueous/Ion-Sel Ele SW-846 Ch 5 www 12/01/1996

9215 Sulfide - Potentiometric in Aqueous/Ion-Sel Ele SW-846 Ch 5 www 12/01/1996

9216 Potentiometric Determination of Nitrite Aqueous SW-846 Ch 5 Update IVA www 01/01/1998

9250 Chloride - Colorimetric, Auto Ferricyanide AAI SW-846 Ch 5 www 09/01/1986

9251 Chloride - Colorimetric, Auto Ferricyanide AAII SW-846 Ch 5 www 09/01/1986

9253 Chloride - Titrimetric, Silver Nitrate SW-846 Ch 5 www 09/01/1994

9310 Alpha & Beta Particles, Gross SW-846 Ch 6 www 09/01/1986

9315 Alpha-Emitting Radium Isotopes SW-846 Ch 6 www 09/01/1986

9320 Radium-228 SW-846 Ch 5 www 09/01/1986

AIR Carbon Monoxide - Non-Dispersive Infrared Photo 50 App C www

AIR Lead in Particulate Matter from Ambient Air 50 App G www

AIR Nitrogen Dioxide - Gas Phase Chemiluminescence 50 App F www

AIR Ozone in Atmosphere - measurment & calibration 50 App D www

AIR Particulate Matter in Atmosphere - High-Volume 50 App B www

AIR Sulfur Dioxide in Atmosphere - Pararosaniline 50 App A www

ALT 001-7 Approved Alternatives air emission methods /ttn/emc

AMES Salmonella/Microsomal Mutagenicity Assay (Ames) 600/4-82-068 03/01/1983

AN208 Coliform & E. coli / Colisure medium (IDEXX Lab) 01A0007292 01/01/1996

AQUATIC Algal Acute Toxicity Test 797.1050 www

AQUATIC Daphnid acute toxicity test 797.1300 www

AQUATIC Daphnid chronic toxicity test 797.1330 www

AQUATIC Fish acute toxicity test 797.1400 www

AQUATIC Fish early life stage toxicity test 797.1600 www

AQUATIC Mysid shrip acute toxicity test 797.1930 www

AQUATIC Mysid shrip chronic toxicity test 797.1950 www

AQUIFER Groundwater Level/Pressure Measurement (4.1-4.5 625/R-93-003a www 05/01/1993

ASBESTO Asbestos - bulk insulation samples interim 763 Sub E App E www

ASBESTO Asbestos in Bulk Building Materials 600/R-93-116 07/01/1993

ASBESTO Asbestos Screening for Soil & Sediment 01A0007115 www 12/05/1997

ASBESTO Asbestos, Airborne by Electron Microscopy 01A0006408 07/01/1984

ASBESTO Clearance Test - Asbestos Abatement Completion 560/5-89-001 05/01/1989

04/16/2003 see Sources list for full reference and website address Method Number Index Page 22 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

ASH Microbial Survivability - Med Waste Incinerator /ttn/emc 02/06/1997

ATMP Antimicrobial Testing Methods & Procedures /oppbead1 /methods

AVS Acid Volatiole Sulfide (AVS) in Sediment 821/R-91-100 www 12/03/1991

BIF BIF (Burning Hazardous Waste/Boilers & Furnaces 266 App IX www 12/01/1990

BIOASSE Estuarine & coastal marine bioassessmen 822/B-00-024 www 12/01/2000

BIOMONI Biomonitoring, in Situ - Marine Sewage 600/4-83-000

BIOMONI Macroinvertebrate - Biological Integrity 600/4-90-030 www 11/01/1990

BIOMONI Molluscs, Caged for In Situ Biomonitoring 600/4-83-000

BIOMONI RPBs - Rapid Bioassessment of Periphyton, fish 841/B-99-002 www 07/01/1999

BLOOD Volatile Organic Compounds in Whole Blood 560/5-87-008

CEMS PS CEMS Performance Specifications (PS-1 to PS-9) /ttn/emc

CHARAC Vadose Zone Hydrologic Properties (6.6.1-6.3.3) 625/R-93-003b www 05/01/1993

CHARAC Vadose Zone Infiltration, Flux (7.1.1-7.5.6) 625/R-93-003b www 05/01/1993

CHARAC Vadose Zone Water Budget Models (8.1.1-8.4.6) 625/R-93-003b www 05/01/1993

CLP Contract Laboratory Program - CLP SOW, Guideline www clp

CLP-SOW Dioxins & Furans

CLP-SOW Inorganics - multi media, multi-concentration

CLP-SOW Organics - multi-media, multi-concentration

CLP-SOW Organics analysis - low concentration water

CTM 1-30 EMC Conditional Test Methods

DISPERS Swirling flask dispersant effectiveness test

DREDGE Dredged Material - Inland Testing Manual

DREDGE Dredged Material Disposal in NE waters

DREDGE Dredged Material in Open Waters - Region 1

DREDGE Dredged Material Testing for Ocean Disposal

ECM Pesticides in soil & water

EMAP Ecological condition/non-wadeable rivers/streams

EMAP Estuaries laboratory methods manual

EMAP Lakes - surface waters field operations manual

EMAP Streams - field & lab for macroinvertebrate

EMAP Surface water - Ecological condition of wadeable

EMISSIO Microbial Survivability - Medical Waste Incinera

EQ-01+ Calibration (EQ-01 thru EQ-08)Microbio Lab

EQUIVAL Designated reference & equivalent air methods

ESTUARI Bacteria, Enterococcus

ESTUARI Bacteria, Fecal Coliform

ESTUARI Bacteria, Total Coliform (TC)

ESTUARI Biochemical Oxygen Demand (BOD)

ESTUARI Carbon, Total Organic (TOC)

ESTUARI Chemical Oxygen Demand (COD)

ESTUARI Grain Size

ESTUARI Infauna

ESTUARI Oil & Grease

ESTUARI Particulates, Floating

ESTUARI Phytoplankton

ESTUARI Priority Pollutant - Organic Compounds, Metals

ESTUARI Salinity

ESTUARI Solids, Total Volatile

DLM01.4 /superfund 

ILM04.0 /superfund 

OLM04.2 /superfund 

OLC02.1. /superfund 

/ttn/emc 

300 App C www 

823/B-98-004 www 02/01/1998 

01A0008260 www 09/17/2001 

01A0006218 05/15/1989 

503/8-91-001 www 02/01/1991 

/oppbead1 /methods 

620/R-00-007 09/01/2000 

620/R-95-008 www EMA 08/01/1995 

620/R-97-001 www EMA 06/01/1997 

01A0007986 www /maia 07/01/1997

620/R-94-004F www 09/01/1998

/ttn/emc 02/06/1997

/oppbead1 /methods 

ttn/amtic/ 

430/9-86-004 03/01/1986 

430/9-86-004 03/01/1986 

430/9-86-004 03/01/1986 

430/9-86-004 03/01/1986 

430/9-86-004 03/01/1986 

430/9-86-004 03/01/1986 

430/9-86-004 03/01/1986 

430/9-86-004 03/01/1986 

430/9-86-004 03/01/1986 

430/9-86-004 03/01/1986 

430/9-86-004 03/01/1986 

430/9-86-004 03/01/1986 

430/9-86-004 03/01/1986 

430/9-86-004 03/01/1986 

04/16/2003 see Sources list for full reference and website address Method Number Index Page 23 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

ESTUARI Solids, Total Water Content 430/9-86-004 03/01/1986 

ESTUARI Sulfides, Total & Water Soluble 430/9-86-004 03/01/1986 

ESTUARI Tissue/Demersal Fishes & Epibenthic Macroinvert 430/9-86-004 03/01/1986 

ESTUARI Tissue/Priority Pollutant Metals - Bioaccumulat 430/9-86-004 03/01/1986 

ESTUARI Tissue/Priority Pollutant Organic Compounds 430/9-86-004 03/01/1986 

ESTUARI Transmissivity 430/9-86-004 03/01/1986 

EV-024/25 Total Tin & Triorganotin (AUTOCHEM North Americ 821/R-93-010-A CD 08/01/1996 

FATE Chemical fate testing guidelines 796 

FIELD PCBs - Field Screening by SPE Membranes 540/R-94-519 www 10/01/1994 

FIELD IN Calibration of field instruments - Region 1 SOP 01A0008143 wpd 06/03/1998 

FISH Bioassessment, Surface Waters - Fish Field & Lab 600/R-92-111 www 03/01/1993 

FISH Fish & Shellfish Tissue - sampling & analysis 823/B-00-007 www 11/01/2000 

FISH IBI (Index of Biotic Integrity) - Surface Waters 600/R-92-111 www 03/01/1993 

FISH IWB (Index of Well-Being) - Surface Waters 600/R-92-111 www 03/01/1993 

FISH PCDF & PCDD in Fish 600/3-90-022 03/01/1990 

FISH Pesticides in Fish 600/3-90-023 03/01/1990 

FISH QHEI (Qualitative Habitat Evaluation Index) 600/R-92-111 www 03/01/1993 

FISH Sampling Surface Waters - Fish Field & Lab 600/R-92-111 www 03/01/1993 

FISH Xenobiotic Chemical Contaminants in Fish 600/3-90-023 03/01/1990 

FM-01 Field Atomic Absorption Analysis 540/2-88-005 09/01/1988 

FM-02 Heavy Metals - X-Ray Fluorescence in Laboratory 540/2-88-005 09/01/1988 

FM-03 Heavy Metals - X-Ray Fluorescence / On-Site 540/2-88-005 09/01/1988 

FM-04 Volatile Organic Compounds - Air Monitoring Prog 540/2-88-005 09/01/1988 

FM-05 Volatile Organic Compounds - GC/ Auto Head Samp 540/2-88-005 09/01/1988 

FM-06 Volatile Organic Compounds - Headspace / Ion Det 540/2-88-005 09/01/1988 

FM-07 Volatile Organic Compounds - Headspace / OVA 540/2-88-005 09/01/1988 

FM-08 Volatile Organic Compounds - Headspace / HNU 540/2-88-005 09/01/1988 

FM-09 Volatile Organic Compounds - Headspace/Mobile GC 540/2-88-005 09/01/1988 

FM-10 Soil Gas Sampling, Passive - Industrial Hygiene 540/2-88-005 09/01/1988 

FM-11 Soil Gas Sampling - Mini-Barrel Sampler 540/2-88-005 09/01/1988 

FM-12 Soil Gas Sampling - One-Liter Syringe 540/2-88-005 09/01/1988 

FM-13 Soil Gas Sampling - Direct Injection Stopper 540/2-88-005 09/01/1988 

FM-14 Soil Gas Sampling - Perforated Tube 540/2-88-005 09/01/1988 

FM-15 Soil Gas Sampling - Tenax Tubes 540/2-88-005 09/01/1988 

FM-16 Soil Gas Sampling - Downhole Profiling 540/2-88-005 09/01/1988 

FM-17 Soil Gas Sampling - Direct Injection Auger 540/2-88-005 09/01/1988 

FM-18 PCB - GC On-Site Lab Hexane/Methanol/H20 Extr 540/2-88-005 09/01/1988 

FM-19 PCB - GC On-Site Lab Hexane Extraction 540/2-88-005 09/01/1988 

FM-20 PCB - GC On-Site Lab Hexane/Methanol Extraction 540/2-88-005 09/01/1988 

FM-21 PCB - GC On-Site Lab Hexane/Acetone Extraction 540/2-88-005 09/01/1988 

FM-22 Pesticide - GC/ECD Hexane/Methanol Extraction 540/2-88-005 09/01/1988 

FM-23 Pesticide - Isothermal GC/ECD Hexane Extraction 540/2-88-005 09/01/1988 

FM-24 Phenol - Liquid-Liquid Extraction & GC 540/2-88-005 09/01/1988 

FM-25 PAH - GC with Heated Column 540/2-88-005 09/01/1988 

FM-26 PNA, Total - Ultraviolet Fluorescence Spectropho 540/2-88-005 09/01/1988 

FM-D1 Trace Atmospheric Gas Analyzer (TAGA) 540/2-88-005 09/01/1988 

FM-D2 Pesticide by Bonded Sorbents 540/2-88-005 09/01/1988 

FM-D3 Semivolatile by Bonded Sorbents 540/2-88-005 09/01/1988 

04/16/2003 see Sources list for full reference and website address Method Number Index Page 24 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

FM-D4 Trace Organic - Immunoassays 540/2-88-005 09/01/1988 

FM-D5 Environmental Monitoring - Fiber Optic Sensors 540/2-88-005 09/01/1988

FUEL Diesel, Sampling 80 App G www

FUEL Fuel, Sampling for Volatility 80 App D www

FUEL Gasoline - Reid Vapor Pressure (RVP) 80 App E www 03/22/1989

FUEL Gasoline, Determination of Phosphorus 80 App A www

FUEL Gasoline, Quantity of Alcohol - Water Extraction 80 App F 1 www 03/22/1989

FUEL Gasoline, Quantity of MBTE by GC 80 App F 2 www 03/22/1989

FUEL Lead in Gasoline - Automated Method by AAS 80 App B 2 www

FUEL Lead in Gasoline - Standard Method by AAS 80 App B 1 www

FUEL Lead in Gasoline - X-Ray Spectometry 80 App B 3 www 04/04/1991

GEOPHYSRemote Sensing & Surface Geophysical (1.1-1.6) 625/R-93-003a www 05/01/1993

GLP Good Laboratory Practice Standards 792 www

GUIDANCData Validation Manual - EPA New England region01 /oeme 12/01/1996

GUIDANCTrace Metal Clean Rooms - Establish in Existing 821/B-95-001 www 04/01/1995

GUIDANCTrace Metals, Documentation & Evaluation of Data 821/B-95-002 www 04/01/1995

GUIDELI aquatic environmental effects guidelines 797 www

GUIDELI chemical/environmental/health effects guidelines 795 www

GUIDELI Health effects test guidelines - TSCA 799 www

GUIDELI Health Effects Testing Guidelines 798 www

GUIDELI Reg 1 Lab Data Validation-volatile/semivolatile 01A0006125 02/01/1988

H-02 Tritium - radiochemical / dioxane method 520/5-84-006 CD 08/01/1994

H2S Hydrogen Sulfide released from wastes - guidance SW-846 Ch 7.3 www 12/01/1996

HCN Hydrogen Cyanide released from wastes - guidance SW-846 Ch 7.3 www 12/01/1996

HRS Hazardous Waste Ranking System 300 App A www

ICR DBP/ICR methods manual 814/B-96-002 www 04/01/1996

ICR Giardia & Cryptosporidium - ICR Microbial 600/R-95-178 www 04/01/1997

ICR ICR Sampling manual 814/B-96-001 www 04/01/1996

ICR Protozoa & Enteric Virus Sample Collection 814/B-95-001 www 06/01/1995

ICR Protozoan Method - Giardia & Cryptosporidium 814/B-95-003 www 06/01/1995

ICR Virus Monitoring Protocol - Info Collection Req 814/B-95-002 www 06/01/1995

IMMUNO Immunoassay - sampling & analysis techniques 540/R-94-509 www 03/01/1994

IMMUNO Immunoassay Guidlines (IA) Planning Env Projects 01A0007541 www 10/01/1996

INDOOR Asbestos 600/8-90-041 www 06/01/1990

INDOOR Formaldehyde 600/8-90-041 www

INDOOR Indoor Air 600/8-90-041 www

INDOOR Indoor Air Quality Protocols - Large Buildings 600/A-92-226 06/01/1992

INDOOR Non-Ionizing Radiation 600/8-90-041 www

INDOOR Organic Compounds 600/8-90-041 www 06/01/1990

INDOOR PAHs 600/8-90-041 www

INDOOR Paricles 600/8-90-041 www

INDOOR Pesticides 600/8-90-041 www

INDOOR Radon 600/8-90-041 www 06/01/1990

INDOOR Tobacco Smoke 600/8-90-041 www

INORGANInorganic Analytes SW-846 Ch 3 Update IVA www 01/01/1998

INORGANSample Preparation Methods - Inorganic Analytes SW-846 Ch 3.2 www 12/01/1996

IO-1 PM10 - continuous determination of SPM in ambien 625/R-96-010a ttn/amtic/ 07/01/1999

IO-1.1 PM10 - Andersen Continuous Beta Attenuation 625/R-96-010a ttn/amtic/ 07/01/1999

04/16/2003 see Sources list for full reference and website address Method Number Index Page 25 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

IO-1.2 PM10 - Thermo Environmental Instruments (Wedding 625/R-96-010a ttn/amtic/ 07/01/1999 

IO-1.3 PM10 - Ruppecht & Patashnick (R&P) TEOM Particle 625/R-96-010a ttn/amtic/ 07/01/1999 

IO-2 PM10 - Integrated sampling of SPM in ambient 625/R-96-010a ttn/amtic/ 07/01/1999 

IO-2.1 PM10 and SPM - High Volume (HV) Sampler 625/R-96-010a ttn/amtic/ 07/01/1999 

IO-2.2 PM10 - Andersen Dichotomous Sampler 625/R-96-010a ttn/amtic/ 07/01/1999 

IO-2.3 PM10 - Rupprecht & Patashnick LV Partisol Sample 625/R-96-010a ttn/amtic/ 07/01/1999 

IO-2.4 PM10 - Calculations for Standard Volume 625/R-96-010a ttn/amtic/ 07/01/1999 

IO-3 Suspended PM - chemical species /filter-collect 625/R-96-010a ttn/amtic/ 07/01/1999 

IO-3.1 SPM - selection, preparation & extraction 625/R-96-010a ttn/amtic/ 07/01/1999 

IO-3.2 SPM - Metals in ambient by AAS 625/R-96-010a ttn/amtic/ 07/01/1999 

IO-3.3 SPM - Metals in ambient PM by XRF 625/R-96-010a ttn/amtic/ 07/01/1999 

IO-3.4 SPM - Metals in ambient by ICP 625/R-96-010a ttn/amtic/ 07/01/1999 

IO-3.5 PM - Metals in ambient by ICP/MS 625/R-96-010a ttn/amtic/ 07/01/1999 

IO-3.6 SPM - Metals in ambient by Proton X-Ray (PIXE) 625/R-96-010a ttn/amtic/ 07/01/1999 

IO-3.7 SPM - Metals / Neutron Activation (NAA) 625/R-96-010a ttn/amtic/ 07/01/1999 

IO-4 PM 2.5 - acidic & basic gases by Annular Deuder 625/R-96-010a ttn/amtic/ 07/01/1999 

IO-4.1 PM 2.5 - strong acidity of atmospheric 625/R-96-010a ttn/amtic/ 07/01/1999 

IO-4.2 PM 2.5 - reactive acidic & basic gases 625/R-96-010a ttn/amtic/ 07/01/1999 

IO-5 Mercury - Sampling & analysis by CVAFS 625/R-96-010a ttn/amtic/ 07/01/1999 

IP-1 VOCs in Indoor Air 600/4-90-10 04/01/1990 

IP-10 Respirable Particulate Matter (PM) in Indoor Air 600/4-90-10 04/01/1990 

IP-10A Size Specific Impaction 600/4-90-10 04/01/1990 

IP-10B Continuous Particulate Monitor 600/4-90-10 04/01/1990 

IP-1A Stainless Steel Canister 600/4-90-10 04/01/1990 

IP-1B Solid Adsorbent Tubes 600/4-90-10 04/01/1990 

IP-2 Nicotine in Indoor Air 600/4-90-10 04/01/1990 

IP-2A XAD-4 Sorbent Tubes 600/4-90-10 04/01/1990 

IP-2B Treated Filter Cassette 600/4-90-10 04/01/1990 

IP-3 Carbon Monoxide or Carbon Dioxide in Indoor Air 600/4-90-10 04/01/1990 

IP-3A Nondispersive Infrared (NDIR) 600/4-90-10 04/01/1990 

IP-3b Gas Filter Correlation (GFC) 600/4-90-10 04/01/1990 

IP-3C Electrochemical Oxidation 600/4-90-10 04/01/1990 

IP-4 Air Exchange Rate in Indoor Air 600/4-90-10 04/01/1990 

IP-4A Perfluorocarbon Tracer (PFT) 600/4-90-10 04/01/1990 

IP-4B Tracer Gas 600/4-90-10 04/01/1990 

IP-5 Nitrogen Dioxide in Indoor Air 600/4-90-10 04/01/1990 

IP-5A Continuous Luminox Monitor 600/4-90-10 04/01/1990 

IP-5B Palmes Diffusion Tube 600/4-90-10 04/01/1990 

IP-5C Passive Sampling Device 600/4-90-10 04/01/1990 

IP-6 Formaldehyde & other Aldehydes in Indoor Air 600/4-90-10 04/01/1990 

IP-6A Solid Adsorbent Cartridge 600/4-90-10 04/01/1990 

IP-6B Continuous Colorimetric Analyzer 600/4-90-10 04/01/1990 

IP-6C Passive Sampling Device 600/4-90-10 04/01/1990 

IP-7 Benzo(a)Pyrene [B(a)P] & PAHs in Indoor Air 600/4-90-10 04/01/1990 

IP-8 Organochlorine Pesticides in Indoor Air 600/4-90-10 04/01/1990 

IP-9 Reactive Acidic, Basic Gases, PM in Indoor Air 600/4-90-10 04/01/1990 

LEACHA Leaching Methods, Compilation & Evaluation of 600/2-78-095 

LEACHA Water Balance Method For Predicting Leachate 530/SW-168 

04/16/2003 see Sources list for full reference and website address Method Number Index Page 26 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

LEAD Lead Levels by XRF Instruments/Chemical Test Kit 747/R-95-002a www 05/01/1995 

LMMB(10 Lake Michigan Mass Balance - Water sampling waterscien www

LMMB(12 Lake Michigan Mass Balance - Plankton sampling waterscien www

LMMB(1- Lake Michigan Mass Balance - Air sampling waterscien www

LMMB(19 Lake Michigan Mass Balance - Sediment sampling waterscien www

LMMB(25 Lake Michigan Mass Balance - Fish sampling waterscien www

LMMB(28 Lake Michigan Mass Balance - Organic (PCB, PAH) waterscien www

LMMB(45 Lake Michigan Mass Balance - Mercury analysis waterscien www

LMMB(54 Lake Michigan Mass Balance - Metals analysis waterscien www

LMMB(58 Lake Michigan Mass Balance - Conventionals waterscien www

LMMB(82 Lake Michigan Mass Balance - Radiochemistry waterscien www

LMMB(85 Lake Michigan Mass Balance - Biomonitoring waterscien www

LMMB(90 Lake Michigan Mass Balance - Shipboard Measures waterscien www

M-14A Total Fluoride - Primary Aluminum Plants /ttn/emc 12/02/1996

MB-01+ Microbiology Lab antimicrobial SOPs /oppbead1

MDL Method Detection Limit (MDL), Rev. 1.11 136 App B www CD 02/04/1994

METALS Precision & Accuracy/Recovery for Metals - ICP 136 App D www CD

MICROBI Actinomycetes - Microbiological Monitoring 600/8-78-017 www

MICROBI Coliform Sampling / Nutrient Agar plus MUG 141.21 www 06/01/1990

MICROBI Coliform Sampling, E. coli 141.21 www 06/01/1990

MICROBI Coliform Sampling, E. coli / ONPG-MUG (Coliert) 141.21 www 06/01/1990

MICROBI Coliform Sampling, E. coli/EC Medium plus MUG 141.21 www 06/01/1990

MICROBI Coliforms, Fecal - Monitoring of Water & Wastes 600/8-78-017 www

MICROBI Coliforms, Total - Monitoring of Water & Wastes 600/8-78-017 www

MICROBI E. coli & total coliform/Membrane Filter/MI agar 600/R-00-013 /microbes www 02/01/2000

MICROBI Fecal Coliforms - Microbiological Monitoring 600/8-78-017 www

MICROBI Fecal Streptococci - Microbiological Monitoring 600/8-78-017 www

MICROBI Giardia Cysts & Cyrptosporidium Oocysts in Water 814/B-95-003 /nerlcwww

MICROBI Salmonella - Microbiological Monitoring/Water 600/8-78-017 www

MICROBI Standard Plate Count (SPC) 600/8-78-017 www

MISC Miscellaneous Test Methods SW-846 Ch 5 Update IVA www 01/01/1998

MNA Natural Attenuation of Chlorinated Sovents 600/R-98-128 www 09/01/1998

MONITO Groundwater SW-846 Ch 11 www 09/01/1986

MONITO Incineration SW-846 Ch 13 www 09/01/1986

MONITO Land Treatment SW-846 Ch 12 www 09/01/1986

MONITO Leachate/GW at Solid Waste Disposal Facilities 530/SW-611

MONITO Low-Level Radioactive Waste/Deep Ocean Sediment 520/1-88-002 08/01/1988

MONITO Monitoring Wells, Design & Construction (A.1-A.7 625/R-93-003a www 05/01/1993

MONITO Soil & Foliar in Long-Term Environ Monitoring 600/R-95-077 www 06/01/1995

MONITO Vadose Zone Soil-Solute/Gas (9.1.1-9.5.2) 625/R-93-003b www 05/01/1993

MONITO Volunteer Estuary Monitoring Methods 842/B-93-004 /owow www 12/01/1993

MONITO Volunteer Lake Monitoring 440/4-91-002 /owow /monitoring 12/01/1991

MONITO Volunteer Stream Monitoring 841/B-97-003 /owow www 11/01/1997

MPA Microscopic particulate analysis consensus 910/9-92-029 10/01/1992

NAT_ATT Natural Attenuation - methane, ethane, ethene 01A0008217 www 02/21/2002

NATATTEMethand, ethane, ethene - nattural attenuation www 07/01/2001

NCASI 25 Color - Pulping Wastes & Receiving Waters 821/R-93-017 www 06/01/1978

NITODNO Nitric Oxide, Nitrogen Dioxide & NOx - Electro /ttn/emc 06/15/1995

04/16/2003 see Sources list for full reference and website address Method Number Index Page 27 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

OIA-1677 Available Cyanide by Flow Injection (FIA)/Ligand 821/R-99-013 www 07/07/1998 

OPPTS OPPTS Harmonized Test Guidelines /OPPTS 03/01/1996 

ORGANIC Cleanup - Organic Analytes SW-846 Ch 4.2.2 www 12/01/1996 

ORGANIC Cleanup - Organic Analytes SW-846 Ch 4.2.2 Update IVA www 01/01/1998 

ORGANIC Determination of Organic Analytes SW-846 Ch 4.3 Update IVA www 01/01/1998 

ORGANIC Extractions & Preparations - Organic Analytes SW-846 Ch 4.2.1 www 12/01/1996 

ORGANIC Gas Chromatographic (GC) Methods SW-846 Ch 4.3.1 www 12/01/1996 

ORGANIC Gas Chromatographic/Mass Spectroscopic Methods SW-846 Ch 4.3.2 Update IVA www 01/01/1998 

ORGANIC Immunoassay Methods

ORGANIC Immunoassay Methods

ORGANIC Infrared Methods

ORGANIC Infrared Methods

ORGANIC Miscellaneous Screening Methods

ORGANIC Miscellaneous Screening Methods

ORGANIC Organic Analytes

SW-846 Ch 4.4 www 12/01/1996 

SW-846 Ch 4.4 Update IVA www 01/01/1998 

SW-846 Ch 4.3.4 www 12/01/1996 

SW-846 Ch 4.3.4 Update IVA www 01/01/1998 

SW-846 Ch 4.5 www 12/01/1996 

SW-846 Ch 4.5 Update IVA www 01/01/1998 

SW-846 Ch 4 Update IVA www 01/01/1998 

PCB PCBs in Transformer Fluid and Waste Oils 600/4-81-045 www 

PCBs Polychlorinated Biphenyls (PCBs) in Fish 600/3-90-023 03/01/1990 

PEST Pesticides in Humans and Environmental Samples 600/8-80-038 06/01/1980 

PEST-04 Pesticides in GW - HPLC/Ultraviolet Detector EMSL 01A0005658 

PF Performance Specifications 1-7 60 App B www 

PM10 PM10 - Particulate Matter as PM10 in Atmosphere 50 App J www 08/07/1987 

PM10 PM10 - Particulate Matter as PM10 in Atmosphere 50 App M www 08/07/1987 

PM2.5 PM2.5 - fine particulate matter in atmosphere 50 App L www 12/13/1996 

PP-001 Pesticides, Chlorinated - Neutrals/Sediments 

PP-002 Pesticides, Chlorinated in Fish 

PP-003 Arsenic and Selenium in Sediment 

PP-003 Selenium in Sediment 

PP-005 Metals in Fish 

PP-005 Metals in Sediment 

PP-006 Mercury in Fish 

PP-007 Mercury in Sediment 

PP-008 Phenols in Sediment 

PP-009 Cyanide in Fish 

PP-010 Cyanide in Sediment 

PP-011 Volatile Organics - Fish by Purge & Trap 

PP-012 Organics, Purgeable in Sediment 

PP-012 Purgeable Organics in Sediment 

PP-013 Organics, General in Sediment 

PRE 1-4 Preliminary Methods 

600/4-81-055 

600/4-81-055 

600/4-81-055 

600/4-81-055 

600/4-81-055 

600/4-81-055 

600/4-81-055 

600/4-81-055 

600/4-81-055 

600/4-81-055 

600/4-81-055 

600/4-81-055 

600/4-81-055 

600/4-81-055 

600/4-81-055 

/ttn/emc 

PROPEL Velocity & Volumetric Flowrate - Cyclonic Flow /ttn/emc 08/22/1996 

PROPERT Solid & Hazardous Wastes SW-846 Ch 6 www 12/01/1996 

QA/G-10 Developing a training program for quality system 240/B-00-004 quality1/ 12/01/2000 

QA/G-4 Data quality objectives process 600/R-96-055 quality1/ 08/01/2000 

QA/G-4D Decision Error Feasibility Trials DEFT software 600/R-96-056 quality1/ 09/01/1994 

QA/G-4H DQO process for hazardous waste sites 600/R-00-007 quality1/ 01/01/2000 

QA/G-5 Quality assurance project plans 600/R-98-018 quality1/ 02/01/1998 

QA/G-5i Data quality indicators quality1/ 09/01/2001 

QA/G-5S Sampling design for environmental data collect quality1/ 08/01/2000 

04/16/2003 see Sources list for full reference and website address Method Number Index Page 28 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

QA/G-6 Preparation - Standard Operating Procedures SOPs 240/B-01-004 quality1/ 03/01/2001 

QA/G-7 Technical audits & assessments 600/R-99-080 quality1/ 01/01/2000

QA/G-8 Environmental data verification & validation quality1/ 06/01/2001

QA/G-9 DQA practical methods for data analysis 600/R-96-084 quality1/ 07/01/2000

QA/G-9D DQA assessment statistical toolbox (DataQUEST) 600/R-96-085 quality1/ 12/01/1997

QA/R-1 Requirements for Environmental Programs EPA Manual 536 quality1/ 05/01/2000

QA/R-2 Quality Management Plans (replace 004/80) 240/B-01-002 quality1/ 03/01/2001

QA/R-5 Requirements for QA project plans 240/B-01-003 quality1/ 03/01/2001

QA-01+ Microbio Lab SOP's (QC-01-QA-03) /oppbead1 /methods

QA-GUID Region 1 Compendium of QA Project Plan Guidance 01A0007832 www 10/01/1999

QC-01+ Microbio Lab SOP's (QC-01-QC-20) /oppbead1 /methods

QUALITY Choosing the Correct Procedure SW-846 Ch 2 Update IVA www 01/01/1998

QUALITY Quality Control Procedures SW-846 Ch 1 www 07/01/1992

Ra-03 Radium-226 radiochemical in water 520/5-84-006 CD 08/01/1994

Ra-04 Radium-226 radiochemical de-emanation 520/5-84-006 CD 08/01/1994

Ra-05 Radium-228 radiochemical in water 520/5-84-006 CD 08/01/1994

RA-CI-A& Gross alpha & beta in drinking water 600/4-75-008 CD 03/01/1976

RA-CI-Ces Radioactive Cesium in drinking water 600/4-75-008 CD 03/01/1976

RA-CI-Io- Radioactive Iodine in DW - distillation 600/4-75-008 CD 03/01/1976

RA-CI-Io- Radioactive Iodine in DW - precipitation 600/4-75-008 CD 03/01/1976

RA-CI-R2 Radium-226 in DW - radon emanation 600/4-75-008 CD 03/01/1976

RA-CI-R2 Radium-228 in DW - sequential method 600/4-75-008 CD 03/01/1976

RA-CI-Ra Alpha-emitting radium isotopes in DW - precip 600/4-75-008 CD 03/01/1976

RA-CI-Str Radioactive strontium in drinking water 600/4-75-008 CD 03/01/1976

RA-CI-Trit Tritum in drinking water 600/4-75-008 CD 03/01/1976

RADON Radon & Radon Decay Product Measurement Devices 402/R-92-004 www 07/01/1992

RADON Radon & Radon Decay Product Measurements / Homes402/R-92-003 www 06/01/1993

RADON Radon, Protocols for Screening and Measurement 520/1-86-014 02/01/1987

RA-LV-A Gross alpha & beta in water EMSL-LV-0539- CD 03/01/1979

RA-LV-IsoIsotopic analysis by gamma ray spectra / lithium EMSL-LV-0539- CD 03/01/1979

RA-LV-Pl Plutonium, uranium & thorium / soil, air, tissue EMSL-LV-0539- CD 03/01/1979

RA-LV-Ra Radium-226 & Radium-228 / soil, air, tissue EMSL-LV-0539- CD 03/01/1979

RA-LV-Str Strontium-89 & -90 / vegetation, soil, tissue EMSL-LV-0539- CD 03/01/1979

RA-LV-TriTritium / water & biological tissue EMSL-LV-0539- CD 03/01/1979

RAM Pesticide residue in food & feed commodities /oppbead1 /methods

RCRA Groundwater monitoring draft technical guidance 530/R-93-001 www 11/01/1992

REACTIV Solid & Hazardous Wastes - Characteristics SW-846 Ch 8.3 www 12/01/1996

RSK SOP Dissolved gases: methane, ethane, ethylene in gw 01A0008284 12/12/2001

SAMPLES Sediment & Water Samples - Handling & Analysis 01A0005044 05/01/1981

SAMPLIN Groundwater guidlines for Superfund & RCRA 542/S-02-001 /tio 05/01/2002

SAMPLIN Asbestos - Small Water Systems/Sample & Monitor 814/B-94-001 www 07/01/1994

SAMPLIN Coal Overburdens & Minesoils, Field & Lab Anal 600/2-78-054 03/01/1978

SAMPLIN Coliform, total coliform rule - drinking water 816/R-01-017A 06/01/2001

SAMPLIN Coliwasa - Composite Liquid Waste Sampler 600/2-80-018 www

SAMPLIN Drilling & Solids Sampling (2.1.1-2.5.3) 625/R-93-003a www 05/01/1993

SAMPLIN Drilling Methods for Groundwater Sampling 600/2-81-160

SAMPLIN Explosives in Soil - Field Sampling- RDX/TNT/HMX 540/R-97-501 sss 11/01/1996

SAMPLIN Field Sampling & Analysis Technologies Matrix 542/B-98-002 www.frtr. gov 03/01/1998

04/16/2003 see Sources list for full reference and website address Method Number Index Page 29 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

SAMPLIN Geophysical Logging of Boreholes (3.1.1-3.6.3) 625/R-93-003a www 05/01/1993 

SAMPLIN Grain Sampler - Powdered or Granual Waste 600/2-80-018 www

SAMPLIN Groundwater Quality Sampling Procedures 600/2-81-160

SAMPLIN Groundwater Sampling 600/2-81-160

SAMPLIN Groundwater Sampling & Monitoring 600/2-85-104 www 09/01/1985

SAMPLIN Groundwater Sampling (5.1-5.7) 625/R-93-003a www 05/01/1993

SAMPLIN Groundwater Sampling (B.1-B.4) 625/R-93-003a www 05/01/1993

SAMPLIN Inorganic Compounds - Small Water Systems 814/B-94-001 www 07/01/1994

SAMPLIN Lead in Drinking Water - Nursery School/Day Care 812/B-94-003 04/01/1994

SAMPLIN Lead Sampling - Collect Soil & Dust Wipe/Vacuum 747/R-95-001 03/01/1995

SAMPLIN Low-flow (minimal drawdown) groundwater 540/S-95-504 tio/pub.htm 04/01/1996

SAMPLIN Minesoils & Coal Overburdens, Field & Lab 600/2-78-054 03/01/1978

SAMPLIN Monitoring Well Design 600/2-85-104 www 09/01/1985

SAMPLIN Monitoring Wells for Groundwater Sampling 600/2-81-160

SAMPLIN Municipal Waste Combustion Ash for TC 530/R-95-036 www 06/01/1995

SAMPLIN Nitrite & Nitrate - Small Water Systems 814/B-94-001 www 07/01/1994

SAMPLIN NPDES Storm Water Sampling Guidance 833/B-92-001 07/01/1992

SAMPLIN Organic Compounds - ambient gaseous/particles 600/4-83-027

SAMPLIN Pesticide Sampling - NEIC 01A0005249 08/01/1985

SAMPLIN Pond Sampler - Liquid Wastes 600/2-80-018 www

SAMPLIN QA/QC Plan & Data Validation Procedures -Removal 540/G-90-004 www 04/01/1990

SAMPLIN Radon, Indoor & Decay Product Measurements 402/R-92-004 www 07/01/1992

SAMPLIN RCRA waste - updates SW-846 Chapter 9 530/D-02-002 www

SAMPLIN Sample Collection Protocol 600/2-85-104 www 09/01/1985

SAMPLIN Sampling House Dust for Lead by Wipe & Vacuum 747/R-95-007 09/01/1995

SAMPLIN Sludge, Ntl Sewage Survey Procedures & Protocols 01A0006083 08/01/1989

SAMPLIN Soil Samplers - Auger, Sampling Trier 600/2-80-018 www

SAMPLIN Soil sampling guidance -Superfund 540/R-95-141 www.ert.org 12/01/1995

SAMPLIN Soil Sampling Protocols 600/R-92-128 www 07/01/1992

SAMPLIN Soils - Description & Sampling Field Guide 625/12-91-002 11/01/1991

SAMPLIN Subsurface Solids for Groundwater Quality 600/2-81-160

SAMPLIN Synthetic Organic Compounds (SOC) - Small Water 814/B-94-001 www 07/01/1994

SAMPLIN Trowel or Scoop - Sampling Solid Waste 600/2-80-018 www

SAMPLIN Veihmeyer Soil Sampler 600/2-80-018 www

SAMPLIN VOCs - Comparison of VOA Compositing Procedures 821/R-95-035 www 09/01/1995

SAMPLIN VOCs - Small Water Systems / Sample & Monitor 814/B-94-001 www 07/01/1994

SAMPLIN Weighted Bottle Sampler - Storage Tanks, Wells 600/2-80-018 www

SAMPLIN Well Development, Hydraulic Performance/Purging 600/2-85-104 www 09/01/1985

SAMPLIN Well, Drilling & Completion Methods 600/2-85-104 www 09/01/1985

SCREEN Field Screening & Analytical (10.1.1-10.6.6) 625/R-93-003b www 05/01/1993

SCREEN Purgeable Organic Compounds, Rapid Screening 01A0005957 06/29/1983

SCREEN Screening Method for Air Toxics Emission Factors /ttn/emc 10/11/1991

SEDIMEN Apparent Effects Threshold Approach (AET) 823/R-92-006 www 09/01/1992

SEDIMEN Bulk Sediment Toxicity Test Approach (BSTT) 823/R-92-006 www 09/01/1992

SEDIMEN Equilibrium Partioning Approach (EqP) 823/R-92-006 www 09/01/1992

SEDIMEN Estuarine & Marine sediments - pesticides 503/6-90-004 05/01/1986

SEDIMEN field sample sediments & interstitial water 823/B-01-002 www 10/01/2001

SEDIMEN Freshwater Benthic Macroinvertebrate Community 823/R-92-006 www 09/01/1992

04/16/2003 see Sources list for full reference and website address Method Number Index Page 30 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

SEDIMEN Greenbook Approach for Ocean Disposal 823/R-92-006 www 09/01/1992

SEDIMEN Interstitial Water Tox Ident Eval (TIE) Approach 823/R-92-006 www 09/01/1992

SEDIMEN Marine Benthic Community Structure Assessment 823/R-92-006 www 09/01/1992

SEDIMEN National Status and Trends Program Approach 823/R-92-006 www 09/01/1992

SEDIMEN Sediment Assessment Strategy Recommended by IJC 823/R-92-006 www 09/01/1992

SEDIMEN Sediment Bioaccumulation, Bedded Marine/Estuarin 600/R-93-183 09/01/1993

SEDIMEN Sediment Quality Triad Approach 823/R-92-006 www 09/01/1992

SEDIMEN Spiked-Sediment Toxicity Test Approach (SSTT) 823/R-92-006 www 09/01/1992

SEDIMEN Tissue Residue Approach 823/R-92-006 www 09/01/1992

SOD SOD (Sediment Oxygen Demand) by Bench Model 01A0006379 www 05/01/1979

SOIL Soil Sampling Quality Assurance User's Guide 600/8-89-046 www 03/01/1989

SOIL VOC Soil Sampling & Analysis 540/4-91-001 02/01/1991

SOIL Tox Sediment 28-d chronic toxicity - marine amphipod 600/R-01-020 www 03/01/2001

SOIL-ATT Adsorption, Batch-Type - Soil Attenuation 530/SW-87-006 www

SOIL-GAS Off-Site / Portable Gas Chromatograph 600/8-87-036

SOIL-GAS Portable THC Analyzer 600/8-87-036

SOIL-GAS Soil Gas Sampling, Grab of VOCs - LGAS 600/2-87-027

SOIL-GAS VOC Analyzer - Adsorbent 600/8-87-036

SOIL-GAS VOC Analyzer - Flame Inization Detector (FID) 600/8-87-036

SOIL-GAS VOC Analyzer - Photoionization Detector (PID) 600/8-87-036

SOIL-GAS VOC Analyzer - Whole Air 600/8-87-036

SOIL-GAS VOC Portable Analyzer - Non-dispersive Infrared 600/8-87-036

SOIL-GAS VOCs, Subsurface - Soil-Gas Passive Sampling 600/2-87-027

SOP Field screening for VOC in aqueous, soil & drum 01A0008123 03/01/1998

SOP #2006Sampling Equipment Decontamination

SOP #2007Groundwater Well Sampling

SOP #2009Drum Sampling

SOP #2010Tank Sampling

SOP #2011Chip, Wipe & Sweep Sampling

SOP #2012Soil Sampling

SOP #2013Surface Water Sampling

SOP #2015Asbestos Sampling

SOP #2016Sediment Sampling

SOP #2017Waste Pile Sampling

SOP #20207-Day Standard Test - Larval Pimephales Promelas

SOP #202124-Hour Rangefinding - Daphnia Magna or Pulex

SOP #202296-Hour Acute - Larval Pimephales Promelas

SOP #202324-Hour Rangefinding -Larval Pimephales Promelas

SOP #202448-Hour Acute - Daphnia Magna or Daphnie Pulex

SOP #20257-Day Static Renewal - Ceridaphnia Dubia

SOP #20267-Day Static Toxic- Larval Pimephales Promelas

SOP #202796-Hour Static - SelenastrumCapricornutum

SOP #202810-Day Chronic - Daphnia Magna or Daphnia Pulex

SOP #2149Soil Gas Sampling

SOP #2150Monitor Well Installation

SOP #2151Water Level Measurement

SOP #2156Monitor Well Development

SOP #2157Controlled Pumping Test

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04/16/2003 see Sources list for full reference and website address Method Number Index Page 31 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

SOP #2158Slug Tests www.ert.org 

SOP GW0 Low Stress (low flow) pumping & sampling - Reg 1 01A0007431 www 07/30/1996 

SPE-500 Endrin/Lindane/Methoxychlor/Toxaphene EMSL 01A0005392 

Sr-04 Radiostrontium - radiochemical in aqueous, sea 520/5-84-006 CD 08/01/1994 

STATS Arc Sine Square Root - Chronic Toxicity 821/R-02-013 WET www 10/01/2002 

STATS Dunnett's Procedure for Acute Toxicity 821/R-02-013 WET www 10/01/2002 

STATS Fisher's Exact Test - Chronic Toxicity 821/R-02-013 WET www 10/01/2002 

STATS Probit Analysis for Chronic Toxicity 821/R-02-013 WET www 10/01/2002 

STATS Spearman-Karber Method for Acute Toxicity 821/R-02-013 WET www 10/01/2002 

STATS Steel's Many-One Rank Test - Chronic Toxicity 821/R-02-013 WET www 10/01/2002 

STATS Wilcoxon Rank Sum Test for Acute Toxicity CD 

STREAM Guide to Method Flexibility & Approval of Water 821/D-96-006 CD 12/01/1996 

STREAM Methods for Organic Chemical - Wastewater 821/B-96-005 www 12/01/1996 

TCDD Dioxin - 2,3,7,8-TCDD 600/3-85-019 05/01/1986 

TCDD Dioxin - 2,3,7,8-TCDD in Soil & Sediment 01A0003682 05/01/1983 

TEM Asbestos in Ambient Air by Direct/Indirect TEM 540/2-90-005a www 05/01/1990 

TEM-ASB Asbestos - Transmission Electron Microscopy 763 Sub E App A www 

TIE Ammonia (3.0) 600/R-92-080 www 09/01/1993 

TIE Chlorine (5.0) 600/R-92-080 www 09/01/1993 

TIE Metals (4.0) 600/R-92-080 www 09/01/1993 

TIE Non-polar Organic Compounds (2.0) 600/R-92-080 www 09/01/1993 

TIE Sample Confirmation Procedures for Toxicity 600/R-92-081 www 09/01/1993 

TIE-ACUTEDTA Chelation (8.8) 600/6-91-003 www 02/01/1991 

TIE-ACUTEffluent Toxicity, Acute Baseline (8.2) 600/6-91-003 www 02/01/1991 

TIE-ACUTEffluent Toxicity, Acute Initial (8.1) 600/6-91-003 www 02/01/1991 

TIE-ACUTGraduated pH (8.9) 600/6-91-003 www 02/01/1991 

TIE-ACUTOxidant Reduction (8.7) 600/6-91-003 www 02/01/1991 

TIE-ACUTpH Adjustment Test, Acute Effluent (8.3) 600/6-91-003 www 02/01/1991 

TIE-ACUTpH Adjustment/C18 Solid Phase Extraction (8.6) 600/6-91-003 www 02/01/1991 

TIE-ACUTpH Adjustment/Filtration Test (8.4) 600/6-91-003 www 02/01/1991 

TIE-ACUTpH Adjustment/Filtration Test, (8.5) 600/6-91-003 www 02/01/1991 

TIE-CHR Aeration & pH Adjustment (6.11) 600/6-91-005F www 05/01/1992 

TIE-CHR Aeration, Chronic Toxicity (6.4) 600/6-91-005F www 05/01/1992 

TIE-CHR EDTA Addition, Chronic Toxicity (6.2) 600/6-91-005F www 05/01/1992 

TIE-CHR Effluent Toxicity, Baseline (6.1) 600/6-91-005F www 05/01/1992 

TIE-CHR Filtration & pH Adjustment (6.12) 600/6-91-005F www 05/01/1992 

TIE-CHR Filtration, Chronic Toxicity (6.5) 600/6-91-005F www 05/01/1992 

TIE-CHR Filtration, Chronic Toxicity (6.5) 600/6-91-005F www 05/01/1992 

TIE-CHR Graduated pH (6.8) 600/6-91-005F www 05/01/1992 

TIE-CHR Methanol Eulate (6.7) 600/6-91-005F www 05/01/1992 

TIE-CHR Methanol Eulate (for pH Adjusted Samples) (6.14) 600/6-91-005F www 05/01/1992 

TIE-CHR pH Adjustment (6.10) 600/6-91-005F www 05/01/1992 

TIE-CHR Post C18 Solid Phase Extraction Column (6.6) 600/6-91-005F www 05/01/1992 

TIE-CHR Post C18 SPEC & pH Adjustment (6.13) 600/6-91-005F www 05/01/1992 

TIE-CHR Sodium Thiosulfate Addition (6.3) 600/6-91-005F www 05/01/1992 

TIE-CHR Tier 2 Characterization (6.9) 600/6-91-005F www 05/01/1992 

TIE-MARI Marine Toxicity Identification Evaluation (TIE) 600/R-96-054 www 09/01/1996 

TISSUE PCDD & PCDF in Human Adipose Tissue 560/5-86-020 

04/16/2003 see Sources list for full reference and website address Method Number Index Page 32 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

TO-01 Tenax GC Adsorption 600/4-89-017 ttn/amtic 

TO-02 Carbon Molecular Sieve Adsorption 600/4-89-017 ttn/amtic

TO-03 Cryogenic Trapping 600/4-89-017 ttn/amtic

TO-04 Organochlorine Pesticides and PCBs - High VolPUF 600/4-89-017

TO-04A Pesticides and PCBs by high volume PUF & GC/MD 625/R-96-010b ttn/amtic 01/01/1999

TO-05 Aldehydes and Ketones by Liquid Impinger Sample 600/4-89-017 ttn/amtic

TO-06 Phosgene by HPLC 600/4-89-017 ttn/amtic

TO-07 N-Nitrosodimethylamine by Thermosorb/N GC/MS 600/4-89-017 ttn/amtic

TO-08 Cresol/Phenol by Sodium Hyudoxide LI/HPLC 600/4-89-017 ttn/amtic

TO-09 Dioxin by High Vol PUF/HRGC/HRMS 600/4-89-017

TO-09A PCBs and TCDD and Dibenzofurans 625/R-96-010b ttn/amtic 01/01/1999

TO-10 Pesticides by Low Volume Polyurethane (PUF) 600/4-89-017 06/01/1988

TO-10A Pesticides & PCBs by low volume PUF & GC/MD 625/R-96-010b ttn/amtic 01/01/1999

TO-11 Formaldehyde by Adsorbent Cartridge/HPLC 600/4-89-017 06/01/1988

TO-11A Formaldehyde by adsorbent cartridge & HPLC 625/R-96-010b ttn/amtic 01/01/1999

TO-12 Organic Compounds, Non-Methane (NMOC)/PDFID 600/4-89-017 ttn/amtic 06/01/1988

TO-13 Polynuclear Aromatic Hydrocarbons (PAHs) 600/4-89-017 06/01/1988

TO-13A PAHs by GC/MS 625/R-96-010b ttn/amtic 01/01/1999

TO-14 Organic Compounds, Semi-Volatile and Volatile 600/4-89-017 06/01/1988

TO-14A VOCs by canisters and GC 625/R-96-010b ttn/amtic 01/01/1999

TO-15 VOCs Collected in Canisters - GC/MS 625/R-96-010b ttn/amtic 01/01/1997

TO-16 VOCs by Long-Path/Open-Path FT/IR Monitoring 625/R-96-010b ttn/amtic 01/01/1999

TO-17 VOCs using active sampling onto sorbent tubes 625/R-96-010b ttn/amtic 01/01/1999

TOXICIT Ames Test for Mutagenicity (Rapid Screening) 330/9-80-002

TOXICIT Biomonitoring - Effluent to Marine Environment 625/8-89-015 09/01/1989

TOXICIT Dispersant & bioremediation effectiveness test 300 App C www

TOXICIT Gammarid Acute Toxicity Test 795.120 www

TOXICIT In Situ Biomonitoring 625/8-89-015 09/01/1989

TOXICIT Larval Development - Sea Urchin 600/R-95-136 www 08/01/1995

TOXICIT Life-cycle chronic toxicity - fathead minnows 600/8-81-011 07/01/1981

TOXICIT Marine Algae - Enumeration of Living & Dead Cell 600/8-87-043

TOXICIT Marine Algae - Growth Test/Complex Liquid Waste 600/8-87-043

TOXICIT Marine Algae Growth Test/Single Substances 600/8-87-043

TOXICIT Reproductive of endocrine-disrupting / minnow 600/R-01-067 www 06/01/2002

TOXICIT Toxicity, Acute - Algal Growth/Haz Waste 600/3-88-029

TOXICIT Toxicity, Acute - Bioassays/Haz Waste Sites 600/8-87-043

TOXICIT Toxicity, Acute - Earthworm Survival/Haz Waste 600/3-88-029

TOXICIT Toxicity, Acute - Fathead Minnow/Haz Waste 600/3-88-029

TOXICIT Toxicity, Acute - Freshwater & Marine Organisms 600/4-90-027F OST/WET www 08/01/1993

TOXICIT Toxicity, Acute - Freshwater & Marine Organisms 821/R-01-012 OST/WET www 10/01/2002

TOXICIT Toxicity, Acute - Freshwater & Marine Organisms 821/R-02-012 www 10/01/2002

TOXICIT Toxicity, Acute - Freshwater Region 1 NPDES www 12/01/1995

TOXICIT Toxicity, Acute - Lettuce Root Elongation 600/3-88-029

TOXICIT Toxicity, Acute - Lettuce Seed Germination 600/3-88-029

TOXICIT Toxicity, Acute - Marine Region 1 NPDES www 09/01/1996

TOXICIT Toxicity, Aquatic - Baseline Effluent 600/6-91-003 www

TOXICIT Toxicity, Aquatic - EDTA Chelation Test 600/6-91-003 www

TOXICIT Toxicity, Aquatic - Graduated pH Test 600/6-91-003 www

04/16/2003 see Sources list for full reference and website address Method Number Index Page 33 
Method Number Index to EPA Test Methods 

Method Chemical or Method Description EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

TOXICIT Toxicity, Aquatic - Initial Effluent 600/6-91-003 www 

TOXICIT Toxicity, Aquatic - Oxidant Reduction Test 600/6-91-003 www 

TOXICIT Toxicity, Aquatic - pH Adjustment/Aeration 600/6-91-003 www 

TOXICIT Toxicity, Aquatic - pH Adjustment/Filtration 600/6-91-003 www 

TOXICIT Toxicity, Chronic - Freshwater Region 1 NPDES www 12/01/1995 

TOXICIT Toxicity, Chronic - Marine Region 1 NPDES www 09/01/1996 

TOXICIT Toxicity, Early Life Stage with Japanese Medaka 600/3-91-063 www 

TP-SERIE Mobile Sources (TP101B - TP754C) www OMS 10/25/1996 

TRE Toxicity Reduction Evaluation - POTW 833/B-99-002 www 08/01/1999 

TRE Toxicity Reduction Evaluation Protocol - POTW 600/2-88-062 www 04/01/1989 

VIRUS-05 Virus Adsorption-Elution (Viradel) Disc Filter 600/4-84-013 www 

VIRUS-06 Virus Adsorption-Elution (Viradel) Cartridge 600/4-84-013 www 

VIRUS-07 Viruses, Recovering from Sludges/Solids 600/4-84-013 www 

VIRUS-08 Viruses, Reduction of Cytotoxicity in Sample 600/4-84-013 www 04/01/1986 

VIRUS-09 Viruses, Cell Preparation & Maintenance 600/4-84-013 www 01/01/1987 

VIRUS-10 Viruses, Cell Culture for Plaque-Forming Assay 600/4-84-013 www 12/01/1987 

VIRUS-11 Viruses, Plaque Confirmation of Enteroviruses 600/4-84-013 www 03/01/1988 

VIRUS-12 Enteroviruses, Identification of 600/4-84-013 www 05/01/1988 

VIRUSES Water-borne viruses by immuoenzymatic methods 600/4-80-034 www 06/01/1980 

WASTES Characterize Heterogeneous -debris,trash,rubbish 600/R-92-033 02/01/1992 

WASTES Compatibility of Hazardous Wastes, Determining 600/2-80-076 04/01/1980 

WATER Lead and Copper Rule - Sampling 814/B-92-001 04/01/1992 

WATER Surface Water Treatment Rule (SWTR) - Sampling 814/B-92-001 04/01/1992 

WATER Total Coliform Rule - Sampling 814/B-92-001 04/01/1992 

WATER Total Organic Carbon, Low Level 01A0005510 

WATER VOC Rule - Sampling 814/B-92-001 04/01/1992 

X-MET 92 Field X-Ray Fluroescence - X-MET 920 Analyzer 01A0007540 www 10/30/1996 

04/16/2003 see Sources list for full reference and website address Method Number Index Page 34 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

10-Day Chronic - Daphnia Magna or Daphnia Pulex SOP #2028 www.ert.org 

2,4-Dichlorophenoxyacetic Acid by Immunoassay 4015 SW-846 Ch 4.4 www 12/01/1996

24-Hour Rangefinding - Daphnia Magna or Pulex SOP #2021 www.ert.org

24-Hour Rangefinding -Larval Pimephales Promelas SOP #2023 www.ert.org

48-Hour Acute - Daphnia Magna or Daphnie Pulex SOP #2024 www.ert.org

7-Day Standard Test - Larval Pimephales Promelas SOP #2020 www.ert.org

7-Day Static Renewal - Ceridaphnia Dubia SOP #2025 www.ert.org

7-Day Static Toxic- Larval Pimephales Promelas SOP #2026 www.ert.org

96-Hour Acute - Larval Pimephales Promelas SOP #2022 www.ert.org

96-Hour Static - SelenastrumCapricornutum SOP #2027 www.ert.org

Absorption in decontamination at Superfund sites 0002 600/2-85-028

Accelerated Solvent Extraction - Organics 3545 SW-846 Ch 4.2. www 12/01/1996

Acetonitrile by GC with Nitrogen-Phosphorus 8033 SW-846 Ch 4.3. www 12/01/1996

Acid Base Partition Cleanup 3650B SW-846 Ch 4.2. www 12/01/1996

Acid Digestion of Aqueous Samples - Metals/GFAA 3020A SW-846 Ch 3.2 www 07/01/1992

Acid Digestion of Aqueous Samples for Metals 3010A SW-846 Ch 3.2 www 07/01/1992

Acid Digestion of Oils for Metals by FLAA or ICP 3031 SW-846 Ch 3.2 www 12/01/1996

Acid Digestion of Sediments, Sludges and Soils 3050B SW-846 Ch 3.2 www 12/01/1996

Acid Digestion of Waters for Metals - FAA/ICP 3005A SW-846 Ch 3.2 www 07/01/1992

Acid Etching 0015 600/2-85-028

Acid Volatiole Sulfide (AVS) in Sediment AVS 821/R-91-100 www 12/03/1991

Acidity - Titrimetric 0305.1 600/4-79-020 NEMI

Acidity - Titrimetric (Acid Rain) 0305.2 600/4-79-020 www

Acidity in Wet Deposition 0305.6 600/4-86-024 03/01/1986

Acids and Base/Neutrals including PCBs 0625 /waterscience 136 App A NEMI

Acrolein & Acrylonitrile 0603 /waterscience 136 App A NEMI

Acrylamide by GC 8032A SW-846 Ch 4.3. www 12/01/1996

Acrylamide, Acrylonityrile & Acrolein - HPCL 8316 SW-846 Ch 4.3. www 09/01/1994

Acrylonitrile by GC 8031 SW-846 Ch 4.3. www 09/01/1994

Actinide Elements 0907 600/4-80-032 www

Actinomycetes - Microbiological Monitoring MICROBI 600/8-78-017 www

Adsorbably organic halides - Adsorption/titratio 1650C CD 08/01/1997

Adsorption, Batch-Type - Soil Attenuation SOIL-ATT 530/SW-87-006 www

Aeration & pH Adjustment (6.11) TIE-CHR 600/6-91-005F www 05/01/1992

Aeration, Chronic Toxicity (6.4) TIE-CHR 600/6-91-005F www 05/01/1992

Aeromonas -finished water / membrane filtration 1605 821/R-01-034 /nerlcwww www 09/01/2000

Air Exchange Rate in Indoor Air IP-4 600/4-90-10 04/01/1990

Alachlor/Butachlor/Diphenamid/Norflurazon/Flurid 0645 821/R-93-010-A CD 06/01/1993

Aldehydes and Ketones by Liquid Impinger Sample TO-05 600/4-89-017 ttn/amtic

Aldrin/Chlordane/Diazinon/Dinoseb/Endrin/Phosmet 1618 01A0006086 07/01/1989

Algal Acute Toxicity Test AQUATIC 797.1050 www

Alkaline Digestion for Hexavalent Chromium 3060A SW-846 Ch 3.2 www 12/01/1996

Alkalinity - Colorimetric, Automated 0310.2 600/4-79-020 NEMI

Alkalinity - Titrimetric, pH 4.5 0310.1 600/4-79-020 NEMI

Alpha & Beta Particles, Gross 9310 SW-846 Ch 6 www 09/01/1986

Alpha-Emitting Radium Isotopes 9315 SW-846 Ch 6 www 09/01/1986

Alpha-emitting radium isotopes in DW - precip RA-CI-Ra 600/4-75-008 CD 03/01/1976

Alumina Cleanup 3610B SW-846 Ch 4.2. www 12/01/1996

Alumina Column Cleanup & Separation Petroleum 3611B SW-846 Ch 4.2. www 12/01/1996

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 1 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Aluminum - AA, Direct Aspiration 0202.1 600/4-79-020 NEMI 

Aluminum - AA, Direct Aspiration 7020 SW-846 Ch 3.3 www 09/01/1986

Aluminum - AA, Furnace Technique 0202.2 600/4-79-020 NEMI

Aluminum - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Ames Test for Mutagenicity (Rapid Screening) TOXICIT 330/9-80-002

Ammonia (as nitrogen) - Colorimetric 0350.1 600/4-79-020 NEMI

Ammonia (3.0) TIE 600/R-92-080 www 09/01/1993

Ammonia (as N) - Colorimetric, Titrimetric 0350.2 600/4-79-020 NEMI

Ammonia (as N) - Potentiometric 0350.3 600/4-79-020 NEMI

Ammonia (as N) Semi-Automated Colorimetry 0350.1 600/R-93-100 www 08/01/1993

Ammonia in Estuarine by Gas Segmented CF/CA 0349.0 600/R-97-072 NEMI 09/01/1997

Ammonia-N /ion-selective electrode potentiometry 1689 821/R-01-012 CD 02/01/1999

Ammonia-Nitrogen / automated colimetry / 1690 821/R-01-009 CD 02/01/1999

Ammonium in Wet Deposition by Electrometric 0350.6 600/4-86-024 03/01/1986

Ammonium in Wet Deposition/Automated Colormetric 0350.7 600/4-86-024 03/01/1986

Amobam/Busan/Ferbam/KN Methyl/Nabam/Nabonate 0630.1 821/R-93-010-A CD 06/01/1993

Aniline & Selected Derivatives by Cap Column GC 8131 SW-846 Ch 4.3. www 12/01/1996

Antimicrobial Testing Methods & Procedures ATMP /oppbead1 /methods

Antimony - AA, Direct Aspiration 0204.1 600/4-79-020 NEMI

Antimony - AA, Direct Aspiration 7040 SW-846 Ch 3.3 www 09/01/1986

Antimony - AA, Furnace Technique 0204.2 600/4-79-020 NEMI

Antimony - AA, furnace technique 0204.2 CL ILM04.0 exhibit D www clp

Antimony - AA, Furnace Technique 7041 SW-846 Ch 3.3 www 09/01/1986

Antimony - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Antimony & Arsenic - AA, Gaseous Borohydride 7062 SW-846 Ch 3.3 www 09/01/1994

AOP/Busan/Carban/Ferban/Mancozeb/Maneb/Metham 0630 821/R-93-010-A CD 06/01/1993

Apparent Effects Threshold Approach (AET) SEDIMEN 823/R-92-006 www 09/01/1992

Approved Alternatives air emission methods ALT 001-7 /ttn/emc

aquatic environmental effects guidelines GUIDELI 797 www

Arc Sine Square Root - Chronic Toxicity STATS 821/R-02-013 WET www 10/01/2002

Arsenic - AA, Furnace Technique 0206.2 600/4-79-020 NEMI

Arsenic - AA, furnace technique 0206.2 CL ILM04.0 exhibit D www clp

Arsenic - AA, Furnace Technique 7060A SW-846 Ch 3.3 www 09/01/1994

Arsenic - AA, Gaseous Hydride 0206.3 600/4-79-020 NEMI

Arsenic - AA, Gaseous Hydride 7061A SW-846 Ch 3.3 www 07/01/1992

Arsenic - Digestion Prior to Total Analysis 0206.5 600/4-79-020 NEMI

Arsenic - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Arsenic - Spectrophotometric - SDDC 0206.4 600/4-79-020 NEMI

Arsenic and Selenium in Sediment PP-003 600/4-81-055

Arsenic in Aqueous Samples & Extracts by ASV 7063 SW-846 Ch 3.3 www 12/01/1996

Arsenic in Ore Samples - Nonferrous Smelters 0108A 61 App B /ttn/emc 08/20/1996

Arsenic in Ore Samples from Nonferrous Smelters 0108B 61 App B /ttn/emc 01/01/1996

Arsenic in Ore Samples from Nonferrous Smelters 0108C 61 App B /ttn/emc 01/01/1996

Arsenic in Water & tissue by HGQ/FAA 1632A 821/R-01-006 SEL2-TRA 01/01/2000

Asbestos INDOOR 600/8-90-041 www 06/01/1990

Asbestos - bulk insulation samples interim ASBESTO 763 Sub E App E www

Asbestos - Small Water Systems/Sample & Monitor SAMPLIN 814/B-94-001 www 07/01/1994

Asbestos - Transmission Electron Microscopy TEM-ASB 763 Sub E App A www

Asbestos Abatement 0001 600/2-85-028

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 2 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Asbestos Fibers in DW Using MCE Filters 0100.2 600/R-94-134 NEMI 06/01/1994 

Asbestos Fibers in Water (Chatfield Method) 0100.1 600/4-83-043 NEMI 09/01/1983

Asbestos in Ambient Air by Direct/Indirect TEM TEM 540/2-90-005a www 05/01/1990

Asbestos in Bulk Building Materials ASBESTO 600/R-93-116 07/01/1993

Asbestos in Serpentine Aggregate CARB Method 435 0435 /ttn/emc 10/10/1991

Asbestos Sampling SOP #2015 www.ert.org

Asbestos Screening for Soil & Sediment ASBESTO 01A0007115 www 12/05/1997

Asbestos, Airborne by Electron Microscopy ASBESTO 01A0006408 07/01/1984

Automated Soxhlet Extraction 3541 SW-846 Ch 4.2. www 09/01/1994

Available Cyanide by Flow Injection (FIA)/Ligand OIA-1677 821/R-99-013 www 07/07/1998

Bacteria, Enterococcus ESTUARI 430/9-86-004 03/01/1986

Bacteria, Fecal Coliform ESTUARI 430/9-86-004 03/01/1986

Bacteria, Total Coliform (TC) ESTUARI 430/9-86-004 03/01/1986

Barium - AA, Direct Aspiration 0208.1 600/4-79-020 NEMI

Barium - AA, Direct Aspiration 7080A SW-846 Ch 3.3 www 09/01/1994

Barium - AA, Furnace Technique 0208.2 600/4-79-020 NEMI

Barium - AA, Furnace Technique 7081 SW-846 Ch 3.3 www 07/01/1992

Barium - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Bendiocarb - Wastewater by LC 0639 821/R-93-010-A CD 06/01/1993

Bensulide - LC 0636 821/R-93-010-A CD 06/01/1993

Bentazon (Basagran) - Wastewater by LC 0643 821/R-93-010-A CD 06/01/1993

Benzene, Chlorobenzene, Ethylbenzene. 0602 /waterscience 136 App A NEMI

Benzidine & Nitrogen-containing Pesticides 0553 600/R-92-129 www 08/01/1992

Benzidines 0605 /waterscience 136 App A NEMI

Benzidines & Nitrogen-Containing Pesticides 0553 821/R-93-010-B CD 08/01/1992

Benzo(a)Pyrene [B(a)P] & PAHs in Indoor Air IP-7 600/4-90-10 04/01/1990

Beryllium - AA, Direct Aspiration 0210.1 600/4-79-020 NEMI

Beryllium - AA, Direct Aspiration 7090 SW-846 Ch 3.3 www 09/01/1986

Beryllium - AA, Furnace Technique 0210.2 600/4-79-020 NEMI 09/01/1997

Beryllium - AA, furnace technique 0210.2 CL ILM04.0 exhibit D www clp

Beryllium - AA, Furnace Technique 7091 SW-846 Ch 3.3 www 09/01/1986

Beryllium - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Beryllium Emissions Determination 0104 61 App B /ttn/emc 01/18/1995

Beryllium Screening Method 0103 61 App B /ttn/emc 09/25/1996

BIF (Burning Hazardous Waste/Boilers & Furnaces BIF 266 App IX www 12/01/1990

Bioassessment, Surface Waters - Fish Field & Lab FISH 600/R-92-111 www 03/01/1993

Biochemical Oxygen Demand (BOD) ESTUARI 430/9-86-004 03/01/1986

Biochemical Oxygen Demand (BOD) - 5 Days, 20 C 0405.1 600/4-79-020 NEMI

Biochemicals test guidelines - TSCA/FIFRA 0880 www OPPT 09/25/1996

Biomonitoring - Effluent to Marine Environment TOXICIT 625/8-89-015 09/01/1989

Biomonitoring, in Situ - Marine Sewage BIOMONI 600/4-83-000

Biphenyl and o-Phenylphenol by LC 0642 821/R-93-010-A CD 06/01/1993

Bis(2-chloroethyl)ether Hydrolysis Prod GC/FT-IR 8430 SW-846 Ch 4.3. www 12/01/1996

Bleaching 0016 600/2-85-028

Bomb Preparation Method for Solid Waste/Metallic 5050 SW-846 Ch 5 www 09/01/1994

Boron - Colorimetric, Curcumin 0212.3 600/4-79-020 NEMI

Bromate in DW by IC/ICP/MS 0321.8 815/R-00-014 NEMI 12/01/1997

Bromide - Potentiometric in Aqueous/Ion-Sel Elec 9211 SW-846 Ch 5 www 12/01/1996

Bromide - Titrimetric 0320.1 600/4-79-020 NEMI

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 3 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Bromoxynil 1661 821/R-93-010-A CD 06/01/1993 

Bulk Sediment Toxicity Test Approach (BSTT) SEDIMEN 823/R-92-006 www 09/01/1992

Butylate/cycloate/EPTC/Molinate/Pebulate/Vernola 0634 821/R-93-010-A CD 06/01/1993

Cadmium - AA, Direct Aspiration 0213.1 600/4-79-020 NEMI

Cadmium - AA, Direct Aspiration 7130 SW-846 Ch 3.3 www 09/01/1986

Cadmium - AA, Furnace Technique 0213.2 600/4-79-020 NEMI

Cadmium - AA, furnace technique 0213.2 CL ILM04.0 exhibit D www clp

Cadmium - AA, Furnace Technique 7131A SW-846 Ch 3.3 www 09/01/1994

Cadmium - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Calcium - AA, Direct Aspiration 0215.1 600/4-79-020 NEMI

Calcium - AA, Direct Aspiration 7140 SW-846 Ch 3.3 www 09/06/1986

Calcium - AA, flame technique 0215.1 CL ILM04.0 exhibit D www clp

Calcium - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Calcium - Titrimetric, EDTA 0215.2 600/4-79-020 NEMI

Calibration (EQ-01 thru EQ-08)Microbio Lab EQ-01+ /oppbead1 /methods

Calibration of field instruments - Region 1 SOP FIELD IN 01A0008143 wpd 06/03/1998

Capture Efficiency - Permanent/Temporary TTE 0204 51 App M /ttn/emc 06/16/1997

Carbofuran/Fluometuron/Methomyl/Oxamyl - in WW 0632 821/R-93-010-A CD 06/01/1993

Carbon & Nitrogen in sediments & particulates 0440.0 600/R-97-072 /ordmeth NEMI 09/01/1997

Carbon Dioxide & Oxygen concentrations - IAP 0003A 60 App A /ttn/emc 05/06/1989

Carbon dioxide, methane, nitrogen, oxygen 0003C 60 App A /ttn/emc 06/20/1996

Carbon Molecular Sieve Adsorption TO-02 600/4-89-017 ttn/amtic

Carbon Monoxide - for certifying CEMS 0010A 60 App A /ttn/emc 09/25/1996

Carbon Monoxide - NDIR 0010 60 App A /ttn/emc 09/25/1996

Carbon Monoxide - Non-Dispersive Infrared Photo AIR 50 App C www

Carbon Monoxide from Stationary Sources 0010B 60 App A /ttn/emc 11/08/1994

Carbon Monoxide or Carbon Dioxide in Indoor Air IP-3 600/4-90-10 04/01/1990

Carbon, Total Organic (TOC) ESTUARI 430/9-86-004 03/01/1986

Carbonyl Compounds & Formaldehyde by HPLC 0554 600/R-92-129 www 08/01/1992

Carbonyl Compounds by HPLC 8315A SW-846 Ch 4.3. www 12/01/1996

Carbonyl compounds in DW by fast GC 0556.1 815/R-00-014 NEMI 09/01/1999

Carbonyl Compounds in DW by PD/GC/ECD 0556 01A0007878 NEMI 06/01/1998

Cation-Exchange Capacity of Soils (Ammonium) 9080 SW-846 Ch 6 www 09/01/1986

Cation-Exchange Capacity of Soils (Sodium) 9081 SW-846 Ch 6 www 09/01/1986

CEMS Performance Specifications (PS-1 to PS-9) CEMS PS /ttn/emc

Characterize Heterogeneous -debris,trash,rubbish WASTES 600/R-92-033 02/01/1992

Characterizing, Subsampling and Crushing Samples 0003.1 600/2-78-054 03/01/1978

Chemical fate testing guidelines FATE 796

Chemical Methods - Overburdens and Minesoils 0003.2 600/2-78-054 03/01/1978

Chemical Oxygen Demand - Colorimetric 0410.4 600/4-79-020 NEMI

Chemical Oxygen Demand - Semi-Automated Colorim 0410.4 600/R-93-100 www 08/01/1993

Chemical Oxygen Demand - Titrimetric, High Level 0410.3 600/4-79-020 NEMI

Chemical Oxygen Demand - Titrimetric, Low Level 0410.2 600/4-79-020 NEMI

Chemical Oxygen Demand - Titrimetric, Mid-Level 0410.1 600/4-79-020 NEMI

Chemical Oxygen Demand (COD) ESTUARI 430/9-86-004 03/01/1986

chemical/environmental/health effects guidelines GUIDELI 795 www

Chip, Wipe & Sweep Sampling SOP #2011 www.ert.org

Chlirinated Acids in DW by LL fast GC/ECD 0515.4 01A0008028 NEMI 04/01/2000

Chlordane Soil Screening by Immunoassy 4041 SW-846 Ch 4.4 www 12/01/1996

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 4 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Chloride - Colorimetric, Auto Ferricyanide A II 0325.2 600/4-79-020 NEMI 

Chloride - Colorimetric, Auto Ferricyanide AAI 9250 SW-846 Ch 5 www 09/01/1986

Chloride - Colorimetric, Auto Ferricyanide AAII 9251 SW-846 Ch 5 www 09/01/1986

Chloride - Colorimetric, Auto. Ferricyanide A I 0325.1 600/4-79-020 NEMI

Chloride - IC 0300.0 600/4-79-020 NEMI 03/01/1984

Chloride - Methods 50/51 by Anion Chromatography 9057 SW-846 Ch 5 www 12/01/1996

Chloride - Potentiometric in Aqueous/Ion-Sel Ele 9212 SW-846 Ch 5 www 12/01/1996

Chloride - Titrimetric, Mercuric Nitrate 0325.3 600/4-79-020 NEMI

Chloride - Titrimetric, Silver Nitrate 9253 SW-846 Ch 5 www 09/01/1994

Chloride in Wet Deposition/Automated Colorimetri 0325.6 600/4-86-024 03/01/1986

Chlorinated acids - liquid-solid extraction/GC/ 0515.2 CD 08/01/1992

Chlorinated Acids (Herbicides) by LSE & GC/ECD 0515.2 600/R-95-131 NEMI 08/01/1995

Chlorinated Acids (herbicides)in DW / LLE GC/ECD 0515.3 815/R-00-014 NEMI 07/01/1996

Chlorinated Acids by GC/ECD 0515.1 600/R-95-131 NEMI 08/01/1995

Chlorinated Acids by HPLC 0555 600/R-92-129 NEMI 08/01/1992

Chlorinated Acids in Water - HPLC 0555 821/R-93-010-B CD 08/01/1992

Chlorinated Acids in Water by GC/ECD 0515.1 821/R-93-010-B CD 01/01/1989

Chlorinated Acids in Water by LSE/GC/ECD 0515.2 821/R-93-010-B CD 08/01/1992

Chlorinated biopheny cogeners by HRGC/HRMS 1668A 821/R-00-02 www /Region8 12/01/1999

Chlorinated Herbicides by GC+ Cap Column 8151A SW-846 Ch 4.3. www 12/01/1996

Chlorinated Hydrocarbons 0612 /waterscience 136 App A NEMI

Chlorinated Hydrocarbons by GC Cap 8121 SW-846 Ch 4.3. www 09/01/1994

Chlorinated Pesticides in Water by GC/ECD 0508 821/R-93-010-B CD 01/01/1989

Chlorinated Pesticides, Herbicides & Organohal. 0508.1 600/R-95-131 NEMI 08/01/1995

Chlorinated pesticides/herbicides/organohalides 0508.1 CD 01/01/1994

Chlorinated Phenolics - In Situ Acetylation/GCMS 1653 821/R-93-017 NEMI 12/01/1991

Chlorinated Phenolics - In Situ Acetylation/GCMS 1653A CD 11/01/1996

Chlorination Disinfection Byproducts, Pesticides 0551.1 600/R-95-131 NEMI 08/01/1995

Chlorination Disinfection Byproducts/Solvents 0551 600/4-90-020 www 07/01/1990

Chlorine (5.0) TIE 600/R-92-080 www 09/01/1993

Chlorine, Total Residual - Spectrophotometric, 0330.5 600/4-79-020 NEMI

Chlorine, Total Residual - Titrimetric 0330.1 600/4-79-020 NEMI

Chlorine, Total Residual - Titrimetric, Back 0330.2 600/4-79-020 NEMI

Chlorine, Total Residual - Titrimetric, DPD-FAS 0330.4 600/4-79-020 NEMI

Chlorine, Total Residual - Titrimetric, Iodomet. 0330.3 600/4-79-020 NEMI

Chlorophylls & other pigments by HPCL 0447.0 600/R-97-072 /nerlcwww /ordmeth 09/01/1997

Chlorothalonil, DCPA, Dichloran, Methoxychlor 0608.2 821/R-93-010-A CD 06/01/1993

Choosing the Correct Procedure QUALITY SW-846 Ch 2 Update IVA www 01/01/1998

Choromium, Hexavalent by Ion Chromatography 1636 821/R-96-003 NEMI 01/01/1996

Chromium - AA, Direct Aspiration 7190 SW-846 Ch 3.3 www 09/01/1986

Chromium - AA, furnace technique 0218.2 CL ILM04.0 exhibit D www clp

Chromium - AA, Furnace Technique 7191 SW-846 Ch 3.3 www 09/01/1986

Chromium - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Chromium Emissions - Electroplating & Anodizing 0306 63 App A /ttn/emc 02/08/1996

Chromium Emissions Electroplating - Mason Jar 0306A 63 App A /ttn/emc 09/25/1996

Chromium VI (Hexavalent) - Chelation Extraction 0218.4 600/4-79-020 NEMI

Chromium, Dissolved Hexavalent by IC 0218.6 CD 09/01/1998

Chromium, Dissolved Hexavalent by Ion Chromatogr 0218.6 600/R-94-111 www 05/01/1994

Chromium, Hexavalent - Chelation Extraction 7197 SW-846 Ch 3.3 www 09/01/1986

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 5 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Chromium, Hexavalent - Colorimetric Method 7196A SW-846 Ch 3.3 www 07/01/1992 

Chromium, Hexavalent - Coprecipitation Method 7195 SW-846 Ch 3.3 www 09/01/1986

Chromium, Hexavalent - Diff. Pulse Polarography 7198 SW-846 Ch 3.3 www 09/01/1986

Chromium, Hexavalent Dissolved - AA, Furnace 0218.5 600/4-79-020 www

Chromium, total - AA, Chelation-Extraction 0218.3 600/4-79-020 NEMI

Chromium, total - AA, Direct Aspiration 0218.1 600/4-79-020 NEMI

Chromium, total - AA, Furnace 0218.2 600/4-79-020 NEMI

Cleanup 3600C SW-846 Ch 4.2. www 12/01/1996

Cleanup - Organic Analytes ORGANIC SW-846 Ch 4.2. www 12/01/1996

Cleanup - Organic Analytes ORGANIC SW-846 Ch 4.2. Update IVA www 01/01/1998

Clearance Test - Asbestos Abatement Completion ASBESTO 560/5-89-001 05/01/1989

Closed Conduit Flow Measurement 0003.1 600/4-82-029 www

Closed-System Purge/Trap/Extraction - Organics 5035 SW-846 Ch 4.2. www 12/01/1996

Closed-System Purge/Trap/Extraction - Organics 5035A SW-846 new www 07/01/2002

Coal Overburdens & Minesoils, Field & Lab Anal SAMPLIN 600/2-78-054 03/01/1978

Cobalt - AA, Direct Aspiration 0219.1 600/4-79-020 NEMI

Cobalt - AA, Direct Aspiration 7200 SW-846 Ch 3.3 www 09/01/1986

Cobalt - AA, Furnace 0219.2 600/4-79-020 NEMI

Cobalt - AA, Furnace Technique 7201 SW-846 Ch 3.3 www 09/01/1986

Cobalt - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Coliform & E. coli / Colisure medium (IDEXX Lab) AN208 01A0007292 01/01/1996

Coliform Sampling / Nutrient Agar plus MUG MICROBI 141.21 www 06/01/1990

Coliform Sampling, E. coli MICROBI 141.21 www 06/01/1990

Coliform Sampling, E. coli / ONPG-MUG (Coliert) MICROBI 141.21 www 06/01/1990

Coliform Sampling, E. coli/EC Medium plus MUG MICROBI 141.21 www 06/01/1990

Coliform, total coliform rule - drinking water SAMPLIN 816/R-01-017A 06/01/2001

Coliforms, Fecal - Monitoring of Water & Wastes MICROBI 600/8-78-017 www

Coliforms, Total - Monitoring of Water & Wastes MICROBI 600/8-78-017 www

Coliwasa - Composite Liquid Waste Sampler SAMPLIN 600/2-80-018 www

Color - Colorimetric, ADMI 0110.1 600/4-79-020 NEMI

Color - Colorimetric-Platinum-Cobalt 0110.2 600/4-79-020 NEMI

Color - Pulping Wastes & Receiving Waters NCASI 25 821/R-93-017 www 06/01/1978

Color - Spectrophotometric 0110.3 600/4-79-020 NEMI

Compatibility of Hazardous Wastes, Determining WASTES 600/2-80-076 04/01/1980

Compatibility Test / Wastes & Membrane Liners 9090A SW-846 Ch 6 www 07/01/1992

Conductance - Specific Conductance, at 25 C 0120.1 600/4-79-020 NEMI

Conductance-Specific/Wet Deposition Electrolytic 0120.6 600/4-86-024 03/01/1986

Conductivity, Hydraulic/Leachate/Permeability 9100 SW-846 Ch 6 www 09/01/1986

Continuous Colorimetric Analyzer IP-6B 600/4-90-10 04/01/1990

Continuous Liquid-Liquid Extraction - Organics 3520C SW-846 Ch 4.2. www 12/01/1996

Continuous Luminox Monitor IP-5A 600/4-90-10 04/01/1990

Continuous Opacity Monitoring for Compliance 0203 /ttn/emc 01/30/1995

Continuous Particulate Monitor IP-10B 600/4-90-10 04/01/1990

Contract Laboratory Program - CLP SOW, Guideline CLP www clp

Controlled Pumping Test SOP #2157 www.ert.org

Coplanar polychlorinated biphernyls (PCBs) 4026 not available SW-846 dev

Copper - AA, Direct Aspiration 0220.1 600/4-79-020 NEMI

Copper - AA, Direct Aspiration 7210 SW-846 Ch 3.3 www 09/01/1986

Copper - AA, Furnace 0220.2 600/4-79-020 NEMI

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 6 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Copper - AA, Furnace Technique 7211 SW-846 Ch 3.3 www 07/01/1992 

Copper - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Corrosivity Toward Steel 1110 SW-846 Ch 8.2 www 09/01/1986

Corrosivity Toward Steel 1110A SW-846 Ch 8 Update IIIB www 10/30/2002

Cresol/Phenol by Sodium Hyudoxide LI/HPLC TO-08 600/4-89-017 ttn/amtic

Cryogenic Trapping TO-03 600/4-89-017 ttn/amtic

Cryptosporidium & Giardia by Filtration/IMS/FA 1623 821/R-01-025 NEMI 04/01/2001

Cryptosporidium in Water by Filtration/IMS/FA 1622 821/R-01-026 NEMI 04/01/2001

Cyanazine - Pesticides in Wastewater 0629 821/R-93-010-A CD 06/01/1993

Cyanide - Potentiometric in Aqueous/Ion-Sel Ele 9213 SW-846 Ch 5 www 12/01/1996

Cyanide - Titrimetric & Manual Spectrophotometri 9014 SW-846 Ch 5 www 12/01/1996

Cyanide Extraction for Solids & Oils 9013 SW-846 Ch 5 www 07/01/1992

Cyanide in Fish PP-009 600/4-81-055

Cyanide in Sediment PP-010 600/4-81-055

Cyanide, Total - Colorimetric, Automated UV 0335.3 600/4-79-020 NEMI

Cyanide, Total - Titrimetric, Spectrophotometric 0335.2 600/4-79-020 NEMI

Cyanide, total and amenable - colorimentric 9012B SW-846 Ch 5 Update IIIB www 02/13/2002

Cyanide, Total and Amenable - Colorimetric, Manu 9010B SW-846 Ch 5 www 12/01/1996

Cyanide, Total and Amenable - distillation 9010C SW-846 Ch 5 Update IIIB www 10/30/2002

Cyanides, Available to Chlorination/Titrimetric 0335.1 600/4-79-020 NEMI

Cycloprate/Kinoprene/Methoprene/Resmethrin 0616 821/R-93-010-A CD 06/01/1993

Dalapon & Haloacetic Acids by LSE & GC/ECD 0552.1 600/R-92-129 NEMI 08/01/1992

Daphnid acute toxicity test AQUATIC 797.1300 www

Daphnid chronic toxicity test AQUATIC 797.1330 www

Data quality indicators QA/G-5i quality1/ 09/01/2001

Data quality objectives process QA/G-4 600/R-96-055 quality1/ 08/01/2000

Data Validation Manual - EPA New England GUIDANC region01 /oeme 12/01/1996

Dazomet 1659 821/R-93-010-A CD 06/01/1993

DBCP & EDB by Microextraction & GC 8011 SW-846 Ch 4.3. www 07/01/1992

DBP/ICR methods manual ICR 814/B-96-002 www 04/01/1996

DDT Soil Screening by Immunoassy 4042 SW-846 Ch 4.4 www 12/01/1996

Decision Error Feasibility Trials DEFT software QA/G-4D 600/R-96-056 quality1/ 09/01/1994

Demolition - Hazardous Waste 0003 600/2-85-028

Dermal Corrosion 1120 SW-846 Ch 6 www 12/01/1996

Designated reference & equivalent air methods EQUIVAL ttn/amtic/

Desorption Sorbent Cartridges VOST - Cap GC/MS 5041A SW-846 Ch 4.2. www 12/01/1996

Determination of Organic Analytes ORGANIC SW-846 Ch 4.3 Update IVA www 01/01/1998

Determinative Chromatographic Separations 8000B SW-846 Ch 4.3. www 12/01/1996

Developing a training program for quality system QA/G-10 240/B-00-004 quality1/ 12/01/2000

Dichlorophen & Hexachlorphene 0604.1 821/R-93-010-A CD 06/01/1993

Diesel, Sampling FUEL 80 App G www

Differentiation of diesel & crude oil - GC/FI 1663A CD

Differentiation of Diesel & Crude Oil by GC/FID 1663 821/R-92-008 www 12/01/1992

Dioxin - 2,3,7,8-TCDD TCDD 600/3-85-019 05/01/1986

Dioxin - 2,3,7,8-TCDD in Soil & Sediment TCDD 01A0003682 05/01/1983

Dioxin & Furan (PCDD & PCDF) 0023 60 App A /ttn/emc 05/25/1995

Dioxin (TCDD) & GC/MS [replaced by 1613A] 0513 600/4-90-020 www 07/01/1990

Dioxin by High Vol PUF/HRGC/HRMS TO-09 600/4-89-017

Dioxin PCDD/Fs screening by Immunoassay 4025 SW-846 new www 10/01/2002

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 7 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Dioxin TEQ by DELFIA Immunoassay 4430 not available SW-846 dev 

Dioxin, TCDD [use 1613A] 0613 /waterscience 136 App A NEMI 

Dioxins & Furans CLP-SOW DLM01.4 /superfund

Dioxins & Furans - HRGC/HRMS 1613 821/B-94-005 NEMI 10/01/1994

Dioxins & Furans, Chlorinated (CDD & CDF) - Soil 0681 01A0006706 12/15/1986

Dioxins, tetra- thru octa- (CDDs) & Furans (CDFs 1613B 821/B-94-005 136 App A www 10/01/1994

Diphenylamine - Wastewater by GC 0620 821/R-93-010-A CD 06/01/1993

Diquat & Paraquat - LSE / HPLC/UD 0549.2 815/R-00-014 NEMI 06/01/1997

Diquat & Paraquat by LSE & HPLC with Ultraviolet 0549.1 600/R-92-129 www 08/01/1992

Dismantling 0004 600/2-85-028

Dispersant & bioremediation effectiveness test TOXICIT 300 App C www

Dissolution Procedure for Oils, Greases or Waxes 3040A SW-846 Ch 3.2 www 12/01/1996

Dissolved gases: methane, ethane, ethylene in gw RSK SOP 01A0008284 12/12/2001

Dissolved Silicate by gas segmented CF/CA 0366.0 600/R-97-072 /orthmeth NEMI 09/01/1997

DQA assessment statistical toolbox (DataQUEST) QA/G-9D 600/R-96-085 quality1/ 12/01/1997

DQA practical methods for data analysis QA/G-9 600/R-96-084 quality1/ 07/01/2000

DQO process for hazardous waste sites QA/G-4H 600/R-00-007 quality1/ 01/01/2000

Dredged Material - Inland Testing Manual DREDGE 823/B-98-004 www 02/01/1998

Dredged Material Disposal in NE waters DREDGE 01A0008260 www 09/17/2001

Dredged Material in Open Waters - Region 1 DREDGE 01A0006218 05/15/1989

Dredged Material Testing for Ocean Disposal DREDGE 503/8-91-001 www 02/01/1991

Drilling & Solids Sampling (2.1.1-2.5.3) SAMPLIN 625/R-93-003a www 05/01/1993

Drilling and Spalling 0018 600/2-85-028

Drilling Methods for Groundwater Sampling SAMPLIN 600/2-81-160

Drum Sampling SOP #2009 www.ert.org

Dunnett's Procedure for Acute Toxicity STATS 821/R-02-013 WET www 10/01/2002

Dusting/Vacuuming/Wiping 0005 600/2-85-028

E. coli & Enterococci in Water - Membrane Filter 1103.1 600/4-85-076 www 07/01/1985

E. coli & total coliform/Membrane Filter/MI agar MICROBI 600/R-00-013 /microbes www 02/01/2000

E. coli in Drinking Water /Nutrient Agar/Mug Tub 1105 600/4-91-016 www 07/01/1991

E. coli in Drinking Water/EC Medium with Mug Tub 1104 600/4-91-016 www 07/01/1991

E. coli modified (mTEC) 1103.1 821/R-97-004 www 03/01/2000

Ecological condition/non-wadeable rivers/streams EMAP 620/R-00-007 09/01/2000

Ecological effects test guidelines - TSCA/FIFRA 0850 www OPPT 05/01/1996

EDB, DBCP - DW by Microextraction 0504 600/4-88-039 www 07/01/1991

EDB, DBCP, 123TCP by Microextractin & GC 0504.1 600/R-95-131 NEMI 08/01/1995

EDTA Addition, Chronic Toxicity (6.2) TIE-CHR 600/6-91-005F www 05/01/1992

EDTA Chelation (8.8) TIE-ACUT 600/6-91-003 www 02/01/1991

EDX/Metham/Thiram/Zineb/Ziram 0630.1 821/R-93-010-A CD 06/01/1993

Effluent Toxicity, Acute Baseline (8.2) TIE-ACUT 600/6-91-003 www 02/01/1991

Effluent Toxicity, Acute Initial (8.1) TIE-ACUT 600/6-91-003 www 02/01/1991

Effluent Toxicity, Baseline (6.1) TIE-CHR 600/6-91-005F www 05/01/1992

Electrochemical Oxidation IP-3C 600/4-90-10 04/01/1990

Elemental & Speciated Isotope Dilution MS 6800 SW-846 Ch 3.3 Update IVA www 01/01/1998

EMC Conditional Test Methods CTM 1-30 /ttn/emc

Encapsulation/Enclosure 0006 600/2-85-028

Endothall by LSE & GC/MS 0548.1 600/R-92-129 NEMI 08/01/1992

Endothall in DW - Ion-Exchange Extraction/GCMS 0548.1 821/R-93-010-B CD 08/01/1992

Endothall in DW - LSE 0548 600/4-90-020 www 07/01/1990

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 8 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Endothall in DW - LSE/GC/ECD 0548 821/R-93-010-B CD 07/01/1990 

Endrin/Lindane/Methoxychlor/Toxaphene SPE-500 EMSL 01A0005392

Enterococci Bacteria in Water by Membrane Filter 1106.1 600/4-85-076 www 07/01/1985

Enteroviruses, Identification of VIRUS-12 600/4-84-013 www 05/01/1988

Environmental data verification & validation QA/G-8 quality1/ 06/01/2001

Environmental Monitoring - Fiber Optic Sensors FM-D5 540/2-88-005 09/01/1988

Equilibrium Partioning Approach (EqP) SEDIMEN 823/R-92-006 www 09/01/1992

Estuaries laboratory methods manual EMAP 620/R-95-008 www EMA 08/01/1995

Estuarine & coastal marine bioassessmen BIOASSE 822/B-00-024 www 12/01/2000

Estuarine & Marine sediments - pesticides SEDIMEN 503/6-90-004 05/01/1986

Ethylene Thiourea (ETU) - GC 0509 CD 12/01/1992

Ethylene Thiourea (ETU) in Water by GC 0509 600/R-95-131 www 08/01/1995

Exhaust Volume Flow Rate - Gasoline Vapor 0002B 60 App A /ttn/emc 04/01/1996

Explosives by Gas Chromatography 8095 SW-846 www Update IVB www 11/01/1998

Explosives in Soil - Field Sampling- RDX/TNT/HMX SAMPLIN 540/R-97-501 sss 11/01/1996

Extractable Sulfides 9031 SW-846 Ch 5 www 07/01/1992

Extractible Organic Halides (EOX) in Solids 9023 SW-846 Ch 5 www 12/01/1996

Extraction of Semivolatile Analytes using 0010 3542 SW-846 Ch 4.2. www 12/01/1996

Extraction Procedure (EP) Toxicity & struct inte 1310B SW-846 Ch 8 Update IIIB www 10/30/2002

Extraction Procedure (EP) Toxicity Test 1310A SW-846 Ch 8.4 www 07/01/1992

Extraction Procedure for Oily Wastes 1330A SW-846 Ch 6 www 07/01/1992

Extraction Procedure, Multiple for Delisting 1320 SW-846 Ch 6 www 09/01/1986

Extractions & Preparations - Organic Analytes ORGANIC SW-846 Ch 4.2. www 12/01/1996

Extractive FTIR - Mineral Wool & Wool Fiberglass 0318 63 App A /ttn/emc 03/31/1997

Fate, transport & transformation guidelines 0835 TSCA/FIFRA www OPPT 04/21/1996

Fecal coliform in biosolids - 1680 821/R-98-003 CD 07/01/1998

Fecal Coliforms - Microbiological Monitoring MICROBI 600/8-78-017 www

Fecal Streptococci - Microbiological Monitoring MICROBI 600/8-78-017 www

Fertilization - Sea Urchin & Sand Dollar 1008 600/R-95-136 www 08/01/1995

Fertilization, Sea Urchin - Chronic Toxicity 1008 821/R-02-014 WET www 10/01/2002

Field & Laboratory for Overburdens & Minesoils 0001.0 600/2-78-054 03/01/1978

Field Atomic Absorption Analysis FM-01 540/2-88-005 09/01/1988

Field Clues - Overburdens and Minesoils 0002.1 600/2-78-054 03/01/1978

Field Method for RDX in Soil 8510 SW-846 Update IVB www

Field Portable X-Ray Fluorescence Spectrometry 6200 SW-846 Ch 3.3 Update IVA www 01/01/1998

field sample sediments & interstitial water SEDIMEN 823/B-01-002 www 10/01/2001

Field Sampling & Analysis Technologies Matrix SAMPLIN 542/B-98-002 www.frtr. gov 03/01/1998

Field Screening & Analytical (10.1.1-10.6.6) SCREEN 625/R-93-003b www 05/01/1993

Field screening for VOC in aqueous, soil & drum SOP 01A0008123 03/01/1998

Field Validation - Pollutant Measurement 0301 63 App A /ttn/emc 12/30/1992

Field X-Ray Fluroescence - X-MET 920 Analyzer X-MET 92 01A0007540 www 10/30/1996

Filtration & pH Adjustment (6.12) TIE-CHR 600/6-91-005F www 05/01/1992

Filtration Efficiency - Paint Overspray Arrestor 0319 63 App A /ttn/emc 10/19/1996

Filtration, Chronic Toxicity (6.5) TIE-CHR 600/6-91-005F www 05/01/1992

Filtration, Chronic Toxicity (6.5) TIE-CHR 600/6-91-005F www 05/01/1992

Fish & Shellfish Tissue - sampling & analysis FISH 823/B-00-007 www 11/01/2000

Fish acute toxicity test AQUATIC 797.1400 www

Fish early life stage toxicity test AQUATIC 797.1600 www

Fisher's Exact Test - Chronic Toxicity STATS 821/R-02-013 WET www 10/01/2002

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 9 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Flame Atomic Absorption Specto (Consolidate FLAA 7000B SW-846 Ch 3.3 Update IVA www 01/01/1998 

Flaming 0017 600/2-85-028

Florisil cleanup 3620C SW-846 www Update IVB www 01/01/1999

Florisil Column Cleanup 3620B SW-846 Ch 4.2. www 12/01/1996

Flow from Pipes Discharging to Atmosphere 0003.2 600/4-82-029 www

Flow Measurement, Misc. 0003.4 600/4-82-029 www

Flow Measurements - Open Channel 0003.3 600/4-82-029 www

Fluoride - Colorimetric 0340.3 600/4-79-020 NEMI

Fluoride - IC 0300.0 600/4-79-020 www

Fluoride - Potentiometric 0340.2 600/4-79-020 NEMI

Fluoride - Potentiometric in Aqueous/Ion-Sel Ele 9214 SW-846 Ch 5 www 12/01/1996

Fluoride - Potroom Roof Monitors/Prim Aluminum 0014 60 App A /ttn/emc 09/25/1996

Fluoride in Wet Deposition by Potentiometric 0340.6 600/4-86-024 03/01/1986

Fluoride, Total - Colorimetric 0340.1 600/4-79-020 NEMI

Fluoride, Total - Specific Ion Electrode 0013B 60 App A /ttn/emc 08/20/1996

Fluoride, Total (SPADNS Zirconium Lake) 0013A 60 App A /ttn/emc 09/25/1996

Formaldehyde INDOOR 600/8-90-041 www

Formaldehyde - Mineral Wool & Wool Fiberglass 0316 63 App A /ttn/emc 03/31/1997

Formaldehyde & Carbonyl Compounds in Indoor Air 0100 SW-846 Ch 10 www 12/01/1996

Formaldehyde & other Aldehydes in Indoor Air IP-6 600/4-90-10 04/01/1990

Formaldehyde by adsorbent cartridge & HPLC TO-11A 625/R-96-010b ttn/amtic 01/01/1999

Formaldehyde by Adsorbent Cartridge/HPLC TO-11 600/4-89-017 06/01/1988

Formaldehyde Emissions - Stationary Sources 0011 SW-846 Ch 10 www 12/01/1996

Formaldehyde in Ambient Air, Continuous Measure 8520 SW-846 Ch 4.3. www 12/01/1996

Formaldehyde, Isobutyraidehyde, Furfural 1667A 821/B-98-016 CD 07/01/1998

Formaldehyde, Isobutyraldehyde, Furfural 1667 821/B-94-001 CD 01/01/1995

Freshwater Benthic Macroinvertebrate Community SEDIMEN 823/R-92-006 www 09/01/1992

Fuel, Sampling for Volatility FUEL 80 App D www

Fugative Opacity 0022 60 App A /ttn/emc 05/21/1995

Furans (CDFs) & Dioxins, Tetra- through Octa 1613A 821/R-93-017 www 10/01/1993

Gammarid Acute Toxicity Test TOXICIT 795.120 www

Gas Chromatographic (GC) Methods ORGANIC SW-846 Ch 4.3. www 12/01/1996

Gas Chromatographic/Mass Spectroscopic Methods ORGANIC SW-846 Ch 4.3. Update IVA www 01/01/1998

Gas Dilution - Field Instrument Calibration 0205 51 App M /ttn/emc 09/25/1996

Gas Filter Correlation (GFC) IP-3b 600/4-90-10 04/01/1990

Gaseous HCl Emissions at Portland Cement Kilns 0321 63 App A /ttn/emc 03/11/1998

Gaseous Nonmethane Organic Emissions 0025 60 App A /ttn/emc 09/25/1996

Gaseous Organic Concentration - Flame Ionization 0025A 60 App A /ttn/emc 09/25/1996

Gaseous Organic Concentration - Infrared Analyze 0025B 60 App A /ttn/emc 11/08/1994

Gasoline - Reid Vapor Pressure (RVP) FUEL 80 App E www 03/22/1989

Gasoline, Determination of Phosphorus FUEL 80 App A www

Gasoline, Quantity of Alcohol - Water Extraction FUEL 80 App F 1 www 03/22/1989

Gasoline, Quantity of MBTE by GC FUEL 80 App F 2 www 03/22/1989

Gel-Preparation Cleanup 3640A SW-846 Ch 4.2. www 09/01/1994

Geophysical Logging of Boreholes (3.1.1-3.6.3) SAMPLIN 625/R-93-003a www 05/01/1993

Germination & Germ-Tube Length - Giant Kelp 1009 600/R-95-136 www 08/01/1995

Giardia & Cryptosporidium - ICR Microbial ICR 600/R-95-178 www 04/01/1997

Giardia Cysts & Cyrptosporidium Oocysts in Water MICROBI 814/B-95-003 /nerlcwww

Glyphosate by HPLC 0547 600/4-90-020 NEMI 07/01/1990

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 10 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Glyphosate in DW - Direct-Aqueous-Injection HPLC 0547 821/R-93-010-B CD 07/01/1990 

Gold - AA, Direct Aspiration 0231.1 600/4-79-020 NEMI

Gold - AA, Furnace 0231.2 600/4-79-020 NEMI

Good Laboratory Practice Standards GLP 792 www

Graduated pH (6.8) TIE-CHR 600/6-91-005F www 05/01/1992

Graduated pH (8.9) TIE-ACUT 600/6-91-003 www 02/01/1991

Grain Sampler - Powdered or Granual Waste SAMPLIN 600/2-80-018 www

Grain Size ESTUARI 430/9-86-004 03/01/1986

Graphite Furnace Atomic Absorption (GFAA) 7010 SW-846 Ch 3.3 Update IVA www 01/01/1998

Greenbook Approach for Ocean Disposal SEDIMEN 823/R-92-006 www 09/01/1992

Gritblasting 0007 600/2-85-028

Gross alpha & beta in drinking water RA-CI-A& 600/4-75-008 CD 03/01/1976

Gross alpha & beta in water RA-LV-A EMSL-LV-0539 CD 03/01/1979

Gross alpha & gross beta particle - radiochem 00-01 520/5-84-006 CD 08/01/1994

Gross alpha in DW by coprecipitation 00-02 520/5-84-006 CD 08/01/1994

Groundwater MONITO SW-846 Ch 11 www 09/01/1986

Groundwater guidlines for Superfund & RCRA SAMPLIN 542/S-02-001 /tio 05/01/2002

Groundwater Level/Pressure Measurement (4.1-4.5 AQUIFER 625/R-93-003a www 05/01/1993

Groundwater monitoring draft technical guidance RCRA 530/R-93-001 www 11/01/1992

Groundwater Quality Sampling Procedures SAMPLIN 600/2-81-160

Groundwater Sampling SAMPLIN 600/2-81-160

Groundwater Sampling & Monitoring SAMPLIN 600/2-85-104 www 09/01/1985

Groundwater Sampling (5.1-5.7) SAMPLIN 625/R-93-003a www 05/01/1993

Groundwater Sampling (B.1-B.4) SAMPLIN 625/R-93-003a www 05/01/1993

Groundwater Well Sampling SOP #2007 www.ert.org 01/26/1995

Growth of Green Alga - Chronic Toxicity 1003 821/R-02-013 WET www 10/01/2002

Guide to Method Flexibility & Approval of Water STREAM 821/D-96-006 CD 12/01/1996

Haloacetic Acids & Dalapon in DW by LLE/GC/ECD 0552.2 600/R-95-131 NEMI 08/01/1995

Haloacetic Acids by LLE & GC/ECD 0552 600/4-90-020 www 07/01/1990

Haloethers 0611 /waterscience 136 App A NEMI

Haloethers - Cap Column 8111 SW-846 Ch 4.3. www 12/01/1996

Halogenated Volatiles by GC+ Cap Column 8021B SW-846 Ch 4.3. www 12/01/1996

HAPS in Paints & Coatings - Direct Injection GC 0311 63 App A /ttn/emc 01/17/1996

Hardness, Total - Colorimetric, Automated EDTA 0130.1 600/4-79-020 NEMI

Hardness, Total - Titrimetric, EDTA 0130.2 600/4-79-020 NEMI

Hazardous Waste Ranking System HRS 300 App A www

HCl Emissions from Portland Cement Kilns by FTIR 0322 /ttn/emc 03/11/1998

Headspace - Screening Method (5021 replacement) 3810 SW-846 Ch 4.5 www 09/01/1986

Health effects test guidelines - TSCA GUIDELI 799 www

Health effects test guidelines - TSCA/FIFRA 0870 www OPPT 06/25/1996

Health Effects Testing Guidelines GUIDELI 798 www

Heavy Metals - X-Ray Fluorescence / On-Site FM-03 540/2-88-005 09/01/1988

Heavy Metals - X-Ray Fluorescence in Laboratory FM-02 540/2-88-005 09/01/1988

Helminth ova or cysts in sludge 0388-0393 625/R-92-013 www 11/25/1991

Herbicides (Diquat & Paraquat) by LSE 0549 600/4-90-020 www 07/01/1990

Herbicides, Chlorinated (Dinoseb) - Wastewater 0615 821/R-93-010-A CD 06/01/1993

Herbicides, Phenoxy-acid by Wide Bore Capillary 1618 01A0006086 07/01/1989

Hexadecane Extraction & Screening of Organics 3820 SW-846 Ch 4.5 www 09/01/1986

Hexavalent Chromium Emissions - Stationary Sourc 0061 SW-846 Ch 10 www 12/01/1996

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 11 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Hexavalent Chromium in DW, GW, WW by Ion Chro 7199 SW-846 Ch 3.3 www 12/01/1996 

Hydroblasting/Waterwashing 0008 600/2-85-028

Hydrogen Chloride, Halides, Halogens Emissions 0026 60 App A /ttn/emc 08/28/1996

Hydrogen Cyanide released from wastes - guidance HCN SW-846 Ch 7.3 www 12/01/1996

Hydrogen Halide & Halogen - Isokinetic 0026A /ttn/emc 03/03/1994

Hydrogen Sulfide of Fuel 0011 60 App A /ttn/emc 09/25/1996

Hydrogen Sulfide released from wastes - guidance H2S SW-846 Ch 7.3 www 12/01/1996

Hydrogen Sulfide/Carbon Disulfide/Carbon Sulfide 0015 60 App A /ttn/emc 10/10/1996

IBI (Index of Biotic Integrity) - Surface Waters FISH 600/R-92-111 www 03/01/1993

ICR Sampling manual ICR 814/B-96-001 www 04/01/1996

Ididium - AA, Furnace 0235.2 600/4-79-020 NEMI

Ignitability - Pensky-Martins Closed-Cup Method 1010 SW-846 Ch 8.1 www 09/01/1986

Ignitability - Pensky-Martins Closed-Cup Method 1010A SW-846 Ch 8 Update IIIB www 10/30/2002

Ignitability - Setaflash Closed-Cup Method 1020A SW-846 Ch 8.1 www 07/01/1992

Ignitability - Small scale closed-cup Method 1020B SW-846 Ch 8 Update IIIB www 10/30/2003

Ignitability of Solids 1030 SW-846 Ch 6 www 12/01/1996

Immunoassay 4000 SW-846 Ch 4.4 www 12/01/1996

Immunoassay - sampling & analysis techniques IMMUNO 540/R-94-509 www 03/01/1994

Immunoassay Guidlines (IA) Planning Env Projects IMMUNO 01A0007541 www 10/01/1996

Immunoassay Methods ORGANIC SW-846 Ch 4.4 www 12/01/1996

Immunoassay Methods ORGANIC SW-846 Ch 4.4 Update IVA www 01/01/1998

In Situ Biomonitoring TOXICIT 625/8-89-015 09/01/1989

In Vitro Chlorophyll & Pheophytin by fluoresence 0445.0 600/R-97-072 /nerlcwww /ordmeth 09/01/1997

In Vitro Chlorophylls & Pheopigments in algae 0446.0 600/R-97-072 /nerlcwww /ordmeth 09/01/1997

Incineration MONITO SW-846 Ch 13 www 09/01/1986

Indoor Air INDOOR 600/8-90-041 www

Indoor Air Quality Protocols - Large Buildings INDOOR 600/A-92-226 06/01/1992

Inductively Coupled Plasma - Mass Spectrometry 6020 CLP- 01A0007861 05/01/1990

Inductively Coupled Plasma/MS 6020A SW-846 Ch 3.3 Update IVA www 01/01/1998

Infauna ESTUARI 430/9-86-004 03/01/1986

Infrared Methods ORGANIC SW-846 Ch 4.3. www 12/01/1996

Infrared Methods ORGANIC SW-846 Ch 4.3. Update IVA www 01/01/1998

Inorganic Analytes INORGAN SW-846 Ch 3 Update IVA www 01/01/1998

Inorganic Anions by Ion Chromatography 0300.0 600/R-93-100 www 08/01/1993

Inorganic Anions by Ion Chromatography 9056 SW-846 Ch 5 www 09/01/1994

Inorganic Anions by Ion Chromatography 9056A SW-846 Ch 5 Update IVB www

Inorganic Anions in Aqueous Matrices - CIE 6500 SW-846 Ch 3.3 Update IVA www 01/01/1998

Inorganic Anions in DW by Ion Chromatography 0300.0 CD 08/01/1993

Inorganic Anions in DW by Ion Chromatography 0300.1 815/R-00-014 NEMI 09/01/1997

Inorganic Arsenic - hydride generation FAA 1632 821/R-96-013 NEMI 07/01/1996

Inorganic Compounds - Small Water Systems SAMPLIN 814/B-94-001 www 07/01/1994

Inorganic Lead - Stationary Sources 0012 60 App A /ttn/emc 09/25/1996

Inorganic Oxhyalide disinfection by-products- DW 0317 815/R-00-014 NEMI 08/01/2000

Inorganic Oxhyalide disinfection by-products- DW 0317 815/B-01-001 www 07/19/2001

Inorganics - multi media, multi-concentration CLP-SOW ILM04.0 /superfund

Inorganics by ICP - AES 6010C SW-846 Ch 3.3 Update IVB www

Inorganics by ICP - Atomic Emission Spectroscopy 6010B SW-846 Ch 3.3 www 12/01/1996

Inorganics:Chloride/Sulfate/Nitrate/Orthophospha 0300.6 600/4-86-024 03/01/1986

Interstitial Water Tox Ident Eval (TIE) Approach SEDIMEN 823/R-92-006 www 09/01/1992

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 12 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Iodide - Titrimetric 0345.1 600/4-79-020 www 

Iridium - AA, Direct Aspiration 0235.1 600/4-79-020 NEMI

Iron - AA, Direct Aspiration 0236.1 600/4-79-020 NEMI

Iron - AA, Direct Aspiration 7380 SW-846 Ch 3.3 www 09/01/1986

Iron - AA, Furnace 0236.2 600/4-79-020 NEMI

Iron - AA, Furnace Technique 7381 SW-846 Ch 3.3 www 07/01/1992

Iron - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Isocyanates Draft Sampling Method 0207-1 /ttn/emc 02/29/1996

Isocyanates Draft Sampling Method by HPLC 0207-2 /ttn/emc 02/29/1996

Isokinetic HCL/LC2 Emission Sampling Train 0050 SW-846 Ch 10 www 12/01/1996

Isotopic analysis by gamma ray spectra / lithium RA-LV-Iso EMSL-LV-0539 CD 03/01/1979

IWB (Index of Well-Being) - Surface Waters FISH 600/R-92-111 www 03/01/1993

K-20 Sealant 0019 600/2-85-028

KN Methyl/Polyram/Thiram/Zineb/Ziram/ZAC 0630 821/R-93-010-A CD 06/01/1993

Laboratory & Field Methods - Weathering 0004.1 600/2-78-054 03/01/1978

Lake Michigan Mass Balance - Air sampling LMMB(1- waterscien www

Lake Michigan Mass Balance - Biomonitoring LMMB(85 waterscien www

Lake Michigan Mass Balance - Conventionals LMMB(58 waterscien www

Lake Michigan Mass Balance - Fish sampling LMMB(25 waterscien www

Lake Michigan Mass Balance - Mercury analysis LMMB(45 waterscien www

Lake Michigan Mass Balance - Metals analysis LMMB(54 waterscien www

Lake Michigan Mass Balance - Organic (PCB, PAH) LMMB(28 waterscien www

Lake Michigan Mass Balance - Plankton sampling LMMB(12 waterscien www

Lake Michigan Mass Balance - Radiochemistry LMMB(82 waterscien www

Lake Michigan Mass Balance - Sediment sampling LMMB(19 waterscien www

Lake Michigan Mass Balance - Shipboard Measures LMMB(90 waterscien www

Lake Michigan Mass Balance - Water sampling LMMB(10 waterscien www

Lakes - surface waters field operations manual EMAP 620/R-97-001 www EMA 06/01/1997

Land Treatment MONITO SW-846 Ch 12 www 09/01/1986

Landfill Gas Production Flow Rate 0002E 60 App A /ttn/emc 06/20/1996

Larval Development - Sea Urchin TOXICIT 600/R-95-136 www 08/01/1995

Larval Survival & Growth - Inland Silverside 1006 821/R-02-014 WET www 10/01/2002

Larval Survival & Growth - Toppsmelt 1006 600/R-95-136 www 08/01/1995

Leachate/GW at Solid Waste Disposal Facilities MONITO 530/SW-611

Leaching Methods, Compilation & Evaluation of LEACHA 600/2-78-095

Lead - AA, Direct Aspiration 0239.1 600/4-79-020 NEMI

Lead - AA, Direct Aspiration 7420 SW-846 Ch 3.3 www 09/01/1986

Lead - AA, Furnace 0239.2 600/4-79-020 NEMI

Lead - AA, furnace technique 0239.2 CL ILM04.0 exhibit D www clp

Lead - AA, Furnace Technique 7421 SW-846 Ch 3.3 www 09/01/1986

Lead - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Lead and Copper Rule - Sampling WATER 814/B-92-001 04/01/1992

Lead in Drinking Water - Nursery School/Day Care SAMPLIN 812/B-94-003 04/01/1994

Lead in DW by DPASV (differential pulse anodic) 1001 01A0007909 08/01/1999

Lead in Gasoline - Automated Method by AAS FUEL 80 App B 2 www

Lead in Gasoline - Standard Method by AAS FUEL 80 App B 1 www

Lead in Gasoline - X-Ray Spectometry FUEL 80 App B 3 www 04/04/1991

Lead in Particulate Matter from Ambient Air AIR 50 App G www

Lead in water & soil by immunoassay 4510 not available SW-846 dev

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 13 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Lead Levels by XRF Instruments/Chemical Test Kit LEAD 747/R-95-002a www 05/01/1995 

Lead Sampling - Collect Soil & Dust Wipe/Vacuum SAMPLIN 747/R-95-001 03/01/1995

Lead-210 in Drinking Water 0909 01A0004860

Life-cycle chronic toxicity - fathead minnows TOXICIT 600/8-81-011 07/01/1981

Liquid Release Test (LRT) Procedure 9096 SW-846 Ch 6 www 09/01/1994

Lithium - AA, Direct Aspiration 7430 SW-846 Ch 3.3 www 07/01/1992

Lithium - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Low Level Particulate Matter - Stationary Source 0005I 60 App A /ttn/emc 12/30/1997

Low Stress (low flow) pumping & sampling - Reg 1 SOP GW0 01A0007431 www 07/30/1996

Low-flow (minimal drawdown) groundwater SAMPLIN 540/S-95-504 tio/pub.htm 04/01/1996

Low-Level Radioactive Waste/Deep Ocean Sediment MONITO 520/1-88-002 08/01/1988

Macroinvertebrate - Biological Integrity BIOMONI 600/4-90-030 www 11/01/1990

Magnesium - AA, Direct Aspiration 0242.1 600/4-79-020 NEMI

Magnesium - AA, Direct Aspiration 7450 SW-846 Ch 3.3 www 09/01/1986

Magnesium - AA, flame technique 0242.2 CL ILM04.0 exhibit D www clp

Magnesium - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Male-specific & somatic coliphage by SAL 1602 821/R-01-029 /nerlcwww www 04/01/2001

Manganese - AA, Direct Aspiration 0243.1 600/4-79-020 NEMI

Manganese - AA, Direct Aspiration 7460 SW-846 Ch 3.3 www 09/01/1986

Manganese - AA, Furnace 0243.2 600/4-79-020 NEMI

Manganese - AA, Furnace Technique 7461 SW-846 Ch 3.3 www 07/01/1992

Manganese - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Marine Algae - Enumeration of Living & Dead Cell TOXICIT 600/8-87-043

Marine Algae - Growth Test/Complex Liquid Waste TOXICIT 600/8-87-043

Marine Algae Growth Test/Single Substances TOXICIT 600/8-87-043

Marine Benthic Community Structure Assessment SEDIMEN 823/R-92-006 www 09/01/1992

Marine Toxicity Identification Evaluation (TIE) TIE-MARI 600/R-96-054 www 09/01/1996

MBTS & TCMTB in Wastewater by LC 0637 821/R-93-010-A CD 06/01/1993

Membrane Filter for Enterococci (mEI Agar) 1600 821/R-97-004 /microbes www 05/01/1997

Mercaptobenzothiazole in Wastewater by LC 0640 821/R-93-010-A CD 06/01/1993

Mercury - Cold Vapor, Automated 0245.2 600/4-79-020 NEMI

Mercury - Cold Vapor, Manual 0245.1 600/4-79-020 NEMI 03/01/1983

Mercury - Cold Vapor, Sediment Manual 0245.5 600/4-79-020 www

Mercury - CVA Fluorescence spectrometry 0245.7 821/R-01-008 CD 02/01/1999

Mercury - Sampling & analysis by CVAFS IO-5 625/R-96-010a ttn/amtic/ 07/01/1999

Mercury Emissions - Chlor-Alkali Hydrogen Stream 0102 61 App B /ttn/emc 05/20/1991

Mercury Emissions - Chlor-Alkali Plants (Air) 0101 61 App B /ttn/emc 09/25/1996

Mercury Emissions - Sewage/Sludge Incinerator 0101A 61 App B /ttn/emc 05/20/1991

Mercury in Aqueous Samples & Extracts by ASV 7472 SW-846 Ch 3.3 www 12/01/1996

Mercury in Fish PP-006 600/4-81-055

Mercury in Liquid Waste - Manual Cold Vapor Tech 7470A SW-846 Ch 3.3 www 09/01/1994

Mercury in Sediment PP-007 600/4-81-055

Mercury in Sediment & Tissue Samples by AFS 7474 SW-846 Ch 3.3 Update IVA www 01/01/1998

Mercury in Sediment by Cold Vapor (CV/AAS) 0245.5 600/4-91-010 www 04/01/1991

Mercury in Soil by Immunoassay 4500 SW-846 Ch 3.3 Update IVA www 01/01/1998

Mercury in soil/sediment - manual cold vapor 0245.5 CL ILM04.0 exhibit D www clp

Mercury in Solid or Semisolid Waste 7471A SW-846 Ch 3.3 www 09/01/1994

Mercury in Solid/Semisolid Waste (Manual Cold-Va 7471B SW-846 Ch 3.3 Update IVA www 01/01/1998

Mercury in Solids/Solutions - TDA/AAS 7473 SW-846 Ch 3.3 Update IVA www 01/01/1998

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 14 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Mercury in Tissues by Cold Vapor (CV/AAS) 0245.6 600/4-91-010 www 04/01/1991 

Mercury in Wastewater Plant Sewage Sludge 0105 61 App B /ttn/emc 09/25/1996

Mercury in water - automated cold vapor 0245.2 CL ILM04.0 exhibit D www clp

Mercury in water - manual cold vapor technique 0245.1 CL ILM04.0 exhibit D www clp

Mercury in Water by Cold Vapor AAS 0245.1 600/R-94-111 www 05/01/1994

Mercury in Water by Oxidation Purge & Trap CVAFS 1631B 821/R-99-005 136 App A www 06/08/1999

Mercury in Water by Oxidation Purge & Trap CVAFS 1631C 821/R-01-024 NEMI 03/01/2001

Mercury in Water by Oxidation Purge & Trap CVAFS 1631D 821/R-02-019 www 08/01/2002

Mercury in Water/ Oxidation, Purge & Trap, CVAFS 1631 821/R-96-012 CD 01/01/1996

Mercury, Inorganic II by HPLC/ECD 0245.3 600/4-91-010 www 04/01/1991

Mercury, Total - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Metals - Atomic Absorption 0200 600/4-79-020 www

Metals - Calcium, Magnesium, Potassium & Sodium 0200.6 600/4-86-024 03/01/1986

Metals (4.0) TIE 600/R-92-080 www 09/01/1993

Metals and Trace Elements - ICP/AES 0200.7 600/R-94-111 www 05/01/1994

Metals by AA (Atomic Absorption Methods) 7000A SW-846 Ch 3.3 www 07/01/1992

Metals by ICP, FGAA and CVAA 1620 01A0006085 CD 09/01/1989

Metals by ICP/MS 6020 SW-846 Ch 3.3 www 09/01/1994

Metals Emissions from Stationary Sources 0029 60 App A /ttn/emc 06/25/1996

Metals in Fish PP-005 600/4-81-055

Metals in Fish Tissue by ICP/EES 0200.11 600/4-91-010 www 04/01/1991

Metals in Sediment PP-005 600/4-81-055

Metals in Stack Emissions 0060 SW-846 Ch 10 www 12/01/1996

Metals, Total Recoverable Elements - Sample Prep 0200.2 600/R-94-111 www 05/01/1994

Metals, Total Recoverable in Biological Tissues 0200.3 600/4-91-010 www 04/01/1991

Metals, Trace at Water Quality Criteria Levels 1669 821/R-96-008 www 01/01/1996

Metals:Arsenic/Cadmium/Chromium/Copper/Lead/Mer0200.1 600/4-91-010 www 04/01/1991

Metals:Sodium/Ammonium/Potassium/Magnesium/Cal 0300.7 600/4-86-024 03/01/1986

Methand, ethane, ethene - nattural attenuation NATATTE www 07/01/2001

Methanol Emissions 0308 63 App A /ttn/emc 11/14/1997

Methanol Eulate (6.7) TIE-CHR 600/6-91-005F www 05/01/1992

Methanol Eulate (for pH Adjusted Samples) (6.14) TIE-CHR 600/6-91-005F www 05/01/1992

Method Detection Limit (MDL), Rev. 1.11 MDL 136 App B www CD 02/04/1994

Methods for Organic Chemical - Wastewater STREAM 821/B-96-005 www 12/01/1996

Methyl Mercury in Water by Distillation...CVAFS 1630 01A0007846 NEMI 08/01/1998

Metribuxin/Terbacil/Triadimefon/Tricyclozole 0633 821/R-93-010-A CD 06/01/1993

Microbial Degradation 0020 600/2-85-028

Microbial pesticide test guidelines - TSCA/FIFRA 0885 www OPPT

Microbial Survivability - Med Waste Incinerator ASH /ttn/emc 02/06/1997

Microbial Survivability - Medical Waste Incinera EMISSIO /ttn/emc 02/06/1997

Microbio Lab SOP's (QC-01-QA-03) QA-01+ /oppbead1 /methods

Microbio Lab SOP's (QC-01-QC-20) QC-01+ /oppbead1 /methods

Microbiological Methods - Overburdens & Minesoil 0003.5 600/2-78-054 03/01/1978

Microbiology Lab antimicrobial SOPs MB-01+ /oppbead1

Microscale solvent extraction (MSE) 3570 SW-846 new www 11/01/2002

Microscopic particulate analysis consensus MPA 910/9-92-029 10/01/1992

Microwave Assisted Acid Digestion Aqueous Sample 3015A SW-846 Ch 3.2 Update IVA www 01/01/1998

Microwave Assisted Acid Digestion of Siliceous.. 3052 SW-846 Ch 3.2 www 12/01/1996

Microwave Assisted Acid Digestion/Aqueous Metals 3015 SW-846 Ch 3.2 www 09/01/1994

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 15 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Microwave Assisted Acid Digestion/Sludges, Soils 3051 SW-846 Ch 3.2 www 09/01/1994 

Microwave Asst Acid Digestion Sediments/Soil/Oil 3051A SW-846 Ch 3.2 Update IVA www 01/01/1998

Microwave Extraction 3546 SW-846 www Update IVB www 09/01/1999

Midget Impinger HCL/CL2 Emission Sampling Train 0051 SW-846 Ch 10 www 12/01/1996

Mineralogical Methods - Overburdens & Minesoils 0003.3 600/2-78-054 03/01/1978

Minesoils - Field Clues and Sampling Methods 0002.3 600/2-78-054 03/01/1978

Minesoils & Coal Overburdens, Field & Lab SAMPLIN 600/2-78-054 03/01/1978

Miscellaneous Screening Methods ORGANIC SW-846 Ch 4.5 www 12/01/1996

Miscellaneous Screening Methods ORGANIC SW-846 Ch 4.5 Update IVA www 01/01/1998

Miscellaneous Test Methods MISC SW-846 Ch 5 Update IVA www 01/01/1998

Mobile Sources (TP101B - TP754C) TP-SERIE www OMS 10/25/1996

Moisture Content in Stack Gases 0004 60 App A /ttn/emc 09/25/1995

Molecular Weight - Carbon Dioxide, Oxygen 0003 60 App A /ttn/emc 09/25/1996

Molluscs, Caged for In Situ Biomonitoring BIOMONI 600/4-83-000

Molybdenum - AA, Direct Aspiration 0246.1 600/4-79-020 NEMI

Molybdenum - AA, Direct Aspiration 7480 SW-846 Ch 3.3 www 09/01/1986

Molybdenum - AA, Furnace 0246.2 600/4-79-020 NEMI

Molybdenum - AA, Furnace Technique 7481 SW-846 Ch 3.3 www 09/01/1986

Molybdenum - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Monitor Well Development SOP #2156 www.ert.org

Monitor Well Installation SOP #2150 www.ert.org

Monitoring Network and In-Plant Sampling 0004.5 600/4-82-029 www

Monitoring Well Design SAMPLIN 600/2-85-104 www 09/01/1985

Monitoring Wells for Groundwater Sampling SAMPLIN 600/2-81-160

Monitoring Wells, Design & Construction (A.1-A.7 MONITO 625/R-93-003a www 05/01/1993

Municipal Waste Combustion Ash for TC SAMPLIN 530/R-95-036 www 06/01/1995

Mysid shrip acute toxicity test AQUATIC 797.1930 www

Mysid shrip chronic toxicity test AQUATIC 797.1950 www

Nabam/Niacide/Sodium Dimethyldithiocarbamate 0630 821/R-93-010-A CD 06/01/1993

National Status and Trends Program Approach SEDIMEN 823/R-92-006 www 09/01/1992

Natural Attenuation - methane, ethane, ethene NAT_ATT 01A0008217 www 02/21/2002

Natural Attenuation of Chlorinated Sovents MNA 600/R-98-128 www 09/01/1998

n-Hexane extractable material (HEM)/oil & grease 9071B www 04/01/1998

n-Hexane extractable meterial (HEM) - aqueous 9070A SW-846 Ch 5 Update IIIB www 10/30/2002

Nickel - AA, Direct Aspiration 0249.1 600/4-79-020 NEMI

Nickel - AA, Direct Aspiration 7520 SW-846 Ch 3.3 www 09/01/1986

Nickel - AA, Furnace 0249.2 600/4-79-020 NEMI

Nickel - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Nickel by AA, Furnace Method 7521 SW-846 Ch 3.3 www 12/01/1996

Nicotine in Indoor Air IP-2 600/4-90-10 04/01/1990

Nitrate - Potentiometric in Aqueous/Ion-Sel Elec 9210 SW-846 Ch 5 www 12/01/1996

Nitrate - Potentiometric in Aqueous/Ion-Sel Elec 9210A SW-846 Ch 5 Update IVB www

Nitrate & Nitrite by Gas Segmented CF/CA 0353.4 600/R-97-072 /nerlcwww /ordmeth 09/01/1997

Nitrate (as Nitrogen) - Colorimetric, Brucine 0352.1 600/4-79-020 NEMI

Nitrate (as Nitrogen) - Spectrophotometric 0354.1 600/4-79-020 NEMI

Nitrate/nitrite-N in biosolids - auto photometry 1685 821/R-01-016 CD 02/01/1999

Nitrate/nitrite-N in biosolids/ manual colimetry 1686 821/R-01-005 CD 02/01/1999

Nitrate-N by IC 0300.0 600/4-79-020 www

Nitrate-Nitrate by Automated Colorimetry 0353.2 600/R-93-100 www 08/01/1993

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 16 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Nitrate-Nitrite (as N) - Colorimetric/Cadmium 0353.2 600/4-79-020 NEMI 

Nitrate-Nitrite (as N) - Manual Cadmium 0353.3 600/4-79-020 NEMI

Nitrate-Nitrite by Automated Colormetric 0353.6 600/4-86-024 03/01/1986

Nitric Oxide, Nitrogen Dioxide & NOx - Electro NITODNO /ttn/emc 06/15/1995

Nitrite & Nitrate - Small Water Systems SAMPLIN 814/B-94-001 www 07/01/1994

Nitrite by IC 0300.0 600/4-79-020 www

Nitroaromatics & Nitramines - HPLC 8330 SW-846 Ch 4.3. www 09/01/1994

Nitroaromatics & Nitramines by HPLC 8330A SW-846 Ch 4.3. Update IVA www 01/01/1998

Nitroaromatics and Cyclic Ketones - Cap Column 8091 SW-846 Ch 4.3. www 12/01/1996

Nitroaromatics and Isophorone 0609 /waterscience 136 App A NEMI

Nitrogen- & Phosphorus-Containing Pesticides 0507 821/R-93-010-B CD 01/01/1989

Nitrogen Dioxide - Gas Phase Chemiluminescence AIR 50 App F www

Nitrogen Dioxide in Indoor Air IP-5 600/4-90-10 04/01/1990

Nitrogen Oxide - Colorimetric 0007C 60 App A /ttn/emc 09/25/1996

Nitrogen Oxide - Instrumental 0007E 60 App A /ttn/emc 08/14/1990

Nitrogen Oxide - Ion Chromatographic 0007A 60 App A /ttn/emc 01/28/1991

Nitrogen Oxide - Ion Chromatographic 0007D 60 App A /ttn/emc 09/25/1996

Nitrogen Oxide - Ultraviolet Spectrophotometry 0007B 60 App A /ttn/emc 08/20/1996

Nitrogen Oxide Emissions - Stationary Sources 0007 60 App A /ttn/emc 03/12/1996

Nitrogen Oxides (NOx) - Stationary Gas Turbines 0020 60 App A /ttn/emc 09/25/1996

Nitrogen, Kjeldahl, Total - Colorimetric 0351.2 600/4-79-020 NEMI

Nitrogen, Kjeldahl, Total - Colorimetric/Auto. 0351.1 600/4-79-020 NEMI

Nitrogen, Kjeldahl, Total - Colorimetric/Titri. 0351.3 600/4-79-020 NEMI

Nitrogen, Kjeldahl, Total - Potentiometric 0351.4 600/4-79-020 NEMI

Nitrogen, Nitrate-Nitrite - Colorimetric/Hydra. 0353.1 600/4-79-020 NEMI

Nitroglycerine by HPLC 8332 SW-846 Ch 4.3. www 12/01/1996

Nitrosamines 0607 /waterscience 136 App A NEMI

Nitrosamines by GC 8070A SW-846 Ch 4.3. www 12/01/1996

N-Methylcarbamates - HPLC 8318 SW-846 Ch 4.3. www 09/01/1994

N-Methylcarbamates by HPLC 8318A SW-846 www Update IVB www 09/01/1999

N-Methylcarbamoyloximes & N-Methylcarbamates 0531.1 821/R-93-010-B CD 01/01/1989

N-Methylcarbamoylozimes/ates - Aqueous In/HPLC 0531.1 600/R-95-131 NEMI 08/01/1995

N-Methylcarbamoylozimes/ates - Aqueous In/HPLC 0531.2 815/B-01-002 www 09/01/2001

NMOC in Landfill Gases 0025C 60 App A /ttn/emc 06/20/1996

N-Nitrosodimethylamine by Thermosorb/N GC/MS TO-07 600/4-89-017 ttn/amtic

Nohalogenated volatiles (GRO, DRO) / GC/FID 8015C SW-846 Ch 4.3 Update IVB www

Nondispersive Infrared (NDIR) IP-3A 600/4-90-10 04/01/1990

Nonhalogenated Organics Using GC/FID 8015B SW-846 Ch 4.3. www 12/01/1996

Non-Ionizing Radiation INDOOR 600/8-90-041 www

Non-polar Organic Compounds (2.0) TIE 600/R-92-080 www 09/01/1993

NPDES Storm Water Sampling Guidance SAMPLIN 833/B-92-001 07/01/1992

NTA - Colorimetric, Automated, Zinc-Zincon 0430.2 600/4-79-020 www

NTA - Colorimetric, Manual, Zinc-Zincon 0430.1 600/4-79-020 www

O2, CO2, CO - emission rate correction factor 0003B 60 App A /ttn/emc 02/01/2000

Occupational & residential exposure guidelines 0875 TSCA/FIFRA www OPPT 09/29/1996

Odor, Threshold - Consistent Series 0140.1 600/4-79-020 www

Off-Site / Portable Gas Chromatograph SOIL-GAS 600/8-87-036

OIA-Method 1677 available cyanide 1677 821/R-99-013 ost/methods 08/01/1999

Oil & Diesel Oil / Drilling Muds & Drill Cutting 1651 821/R-92-008 www 12/01/1992

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 17 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Oil & Grease ESTUARI 430/9-86-004 03/01/1986 

Oil & Grease - Extraction for Sludge & Sediment 9071A SW-846 Ch 5 www 09/01/1994

Oil & Grease (HEM/SGT-HEM) by extraction 1664A 821/R-98-002 waterscien NEMI 02/01/1999

Oil & Grease and Total Petroleum Hydrocarbons 1664 821/B-94-004b NEMI 04/01/1995

Oil & grease method - referral to Method 1664 9070A* www 05/14/1999

Oil & Grease, Total Recoverable - Gravimetric 9070 SW-846 Ch 5 replaced by 9070A&1664 09/01/1986

Oil & Grease, Total Recoverable - Spectrophot. 0413.2 600/4-79-020 www

Oil & Grease, Total, Recoverable - Gravimetric 0413.1 600/4-79-020 see 1664 www

Opacity of Emissions - Remotely by Lidar 0009 Alt 1 60 App A

Opacity of Emissions, Instantaneous Limitation 0203C /ttn/emc 01/06/1994

OPPTS Harmonized Test Guidelines OPPTS /OPPTS 03/01/1996

Organic Analytes ORGANIC SW-846 Ch 4 Update IVA www 01/01/1998

Organic Carbon, Total - Combustion or Oxidation 0415.1 600/4-79-020 NEMI

Organic Carbon, Total - UV Promoted 0415.2 600/4-79-020 www

Organic Compounds INDOOR 600/8-90-041 www 06/01/1990

Organic Compounds - ambient gaseous/particles SAMPLIN 600/4-83-027

Organic compounds - LSE/capillary/GCMS 0525.2 CD 03/01/1994

Organic Compounds Biodegredation Rates - Vent 0304A 63 App A /ttn/emc 03/03/1994

Organic Compounds Biodegredation Rates -Scrubber 0304B 63 App A /ttn/emc 03/03/1994

Organic Compounds by Liquid/Solid Extract GCMS 0525.1 600/4-88-039 www 07/01/1991

Organic Compounds in Drinking Water by LSE/GC/M 0525 01A0008190 01/01/1988

Organic Compounds in Drinking Water by LSE/GC/M 0525.1 821/R-93-010-B CD 05/01/1991

Organic Compounds in DW by LSE/Cap Col GC/MS 0525.2 600/R-95-131 NEMI 08/01/1995

Organic compounds in water by microextraction 3511 SW-846 new www 11/01/2002

Organic Compounds, Non-Methane (NMOC)/PDFID TO-12 600/4-89-017 ttn/amtic 06/01/1988

Organic Compounds, Semi-Volatile and Volatile TO-14 600/4-89-017 06/01/1988

Organic Extractin & Sample Preparation 3500B SW-846 Ch 4.2. www 12/01/1996

Organic Extraction and Sample Preparation 3500C SW-846 www Update IVB www 01/01/1999

Organic Halides - Solid Matrices/Neutron Activat 1648 CD 06/01/1991

Organic Halides, Absorbable (AOX) 1650 ver 1 CD CD 11/01/1996

Organic Halides, Absorbable (AOX) 1650B 821/R-93-017 www 10/01/1993

Organic Hazardous Consitutents - Tedlar Bags 0040 SW-846 Ch 10 www 12/01/1996

Organic Priority Pollutants in Sludges 0624-S 600/4-84-001

Organic, inorganic & total mercury in soils 3200 not available SW-846 dev

Organics - multi-media, multi-concentration CLP-SOW OLM04.2 /superfund

Organics analysis - low concentration water CLP-SOW OLC02.1. /superfund

Organics, General in Sediment PP-013 600/4-81-055

Organics, Purgeable in Sediment PP-012 600/4-81-055

Organochlorine Pesticides and PCBs - High VolPUF TO-04 600/4-89-017

Organochlorine Pesticides by Cap Column GC 8081A SW-846 Ch 4.3. www 12/01/1996

Organochlorine Pesticides by GC 8081B SW-846 Ch 4.3. Update IVA www 01/01/1998

Organochlorine pesticides by GC with ECD or ELCD 8081B SW-846 www Update IVB www 05/01/1999

Organochlorine Pesticides in Indoor Air IP-8 600/4-90-10 04/01/1990

Organochlorine Pesticides in Wastewater 0608.1 821/R-93-010-A CD 06/01/1993

Organochlorine Pesticides in Wastewater - GC 0608.2 821/R-93-010-A CD 06/01/1993

Organohalide Pesticides 1656 821/R-93-010-A CD 06/01/1993

Organohalide Pesticides & PCB Products by GC 0505 600/R-95-131 NEMI 08/01/1995

Organohalide Pesticides & PCB Products in Water 0505 821/R-93-010-B CD 01/01/1989

Organohalide pesticides -ww, soil, tissue-GC/HSD 1556A 821/R-93-017 www

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 18 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Organohalides-ww, soil, sludge, sediment, tissue 1656A 821/R-00-017 SEL-01 09/01/2000 

Organomercurials, Selected by HPLC/ECD 0245.3 600/4-91-010 www 04/01/1991

Organophosphorus Compounds by GC 8141B SW-846 Ch 4.3. Update IVA www 01/01/1998

organophosphorus compounds by GC 8141B SW-846 Update IVB www 09/01/1999

Organo-Phosphorus in ww, soil, sed, tissue 1657A 821/R-00-018 SEL2-BIO 09/01/2000

Organophosphorus Pesticides 1657 821/R-93-010-A CD 06/01/1993

Organophosphorus Pesticides - GC Capillary Colum 8141A SW-846 Ch 4.3. www 09/01/1994

Organotins by micro LC-ES-ITMS 8323 SW-846 new www 02/01/2003

Original Enterocci method 1106.1 821/R-97-004 www 03/01/2000

Orthophosphate (as P) - Automated Colorimetry 0365.1 600/R-93-100 www 08/01/1993

Orthophosphate by automated colorimetric 0365.5 600/R-97-072 /nerlcwww /ordmeth 09/01/1997

Orthophosphate in Wet Depositon 0365.6 600/4-86-024 03/01/1986

Ortho-Phosphate-P 0300.0 600/4-79-020 www

Oryzalin in Wastewater 0638 821/R-93-010-A CD 06/01/1993

Osmium - AA, Direct Aspiration 0252.1 600/4-79-020 NEMI

Osmium - AA, Direct Aspiration 7550 SW-846 Ch 3.3 www 09/01/1986

Osmium - AA, Furnace 0252.2 600/4-79-020 NEMI

Overburden Sampling and Labeling 0002.2 600/2-78-054 03/01/1978

Oxidant Reduction (8.7) TIE-ACUT 600/6-91-003 www 02/01/1991

Oxidizing Solids (conical pile type burning UN) 1040 SW-846 www Update IVB www 09/01/1199

Oxygen, Dissolved - Membrane Electrode (Probe) 0360.1 600/4-79-020 NEMI

Oxygen, Dissolved - Modified Winkler 0360.2 600/4-79-020 NEMI

Ozone in Atmosphere - measurment & calibration AIR 50 App D www

PAH - GC with Heated Column FM-25 540/2-88-005 09/01/1988

PAH Content of Oil by HPLC/UV 1654 821/R-92-008 www 12/01/1992

PAHs INDOOR 600/8-90-041 www

PAHs and PCBs in Soils/Sludges by TE/GC/MS 8275A SW-846 Ch 4.3. www 12/01/1996

PAHs by GC/MS TO-13A 625/R-96-010b ttn/amtic 01/01/1999

PAHs by Liquid-Liquid Extraction (LLE) & HPLC 0550 600/4-90-020 NEMI 07/01/1990

PAHs by Liquid-Solid Extraction (LSE) & HPLC 0550.1 600/4-90-020 NEMI 07/01/1990

PAHs Soil Screening by Immunoassy 4035 SW-846 Ch 4.4 www 12/01/1996

Paint Filter Liquids Test 9095A SW-846 Ch 6 www 12/01/1996

Paint Filter Liquids Test 9095B SW-846 Ch 6 Update IIIB www 10/30/2002

Painting/coating 0009 600/2-85-028

Palladium - AA, Direct Aspiration 0253.1 600/4-79-020 NEMI

Palladium - AA, Furnace 0253.2 600/4-79-020 NEMI

Palmes Diffusion Tube IP-5B 600/4-90-10 04/01/1990

Parameters to Monitor 0004.4 600/4-82-029 www

Paricles INDOOR 600/8-90-041 www

Particulate & Gaseous Arsenic Emissions 0108 61 App B /ttn/emc 09/25/1996

Particulate Matter (PM) - Instack Filtration 0017 60 App A /ttn/emc 04/23/1996

Particulate Matter (PM) - Stationary Sources 0005 60 App A /ttn/emc 08/16/1996

Particulate Matter in Atmosphere - High-Volume AIR 50 App B www

Particulates, Floating ESTUARI 430/9-86-004 03/01/1986

Passive Sampling Device IP-5C 600/4-90-10 04/01/1990

Passive Sampling Device IP-6C 600/4-90-10 04/01/1990

PCB - GC On-Site Lab Hexane Extraction FM-19 540/2-88-005 09/01/1988

PCB - GC On-Site Lab Hexane/Acetone Extraction FM-21 540/2-88-005 09/01/1988

PCB - GC On-Site Lab Hexane/Methanol Extraction FM-20 540/2-88-005 09/01/1988

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 19 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

PCB - GC On-Site Lab Hexane/Methanol/H20 Extr FM-18 540/2-88-005 09/01/1988 

PCBs - Field Screening by SPE Membranes FIELD 540/R-94-519 www 10/01/1994

PCBs & Organochlorine Pesticides 0608 /waterscience 136 App A NEMI

PCBs & pesticides in water & soil/sediment -GCMS 0680 01A0005295 CD 11/01/1985

PCBs and TCDD and Dibenzofurans TO-09A 625/R-96-010b ttn/amtic 01/01/1999

PCBs by Cap Column GC 8082 SW-846 Ch 4.3. www 12/01/1996

PCBs by GC 8082A SW-846 www Update IVB www 05/01/1999

PCBs in Soil Screening Test 9078 SW-846 Ch 4.5 www 12/01/1996

PCBs in Transformer Fluid and Waste Oils PCB 600/4-81-045 www

PCBs in Transformer Oil Screening Test 9079 SW-846 Ch 4.5 www 12/01/1996

PCBs in Water, Soil - Isotope Dilution HRGC/HRMS 1668 821/R-97-001 www 03/01/1997

PCBs Screening by Immunoassay 4020 SW-846 Ch 4.4 www 12/01/1996

PCBs screening by perchlorination & GC 0508A NEMI 01/01/1989

PCBs, Dioxins/Furans PAH - HRGS 4425 SW-846 www Update IVB www 09/01/1999

PCDD & PCDF - HRGC/HRMS 8290 SW-846 Ch 4.3. www 09/01/1994

PCDD & PCDF in Human Adipose Tissue TISSUE 560/5-86-020

PCDD and PCDF by HRGC/HRMS 8290A SW-846 Ch 4.3. Update IVA www 01/01/1998

PCDD and PCDF by HRGC/LRMS 8280A SW-846 Ch 4.3. www 12/01/1996

PCDD and PCDF by HRGC/LRMS 8280B SW-846 Ch 4.3. Update IVA www 01/01/1998

PCDDs and PCDFs - Stationary Sources Sampling 0023A SW-846 Ch 10 www 12/01/1996

PCDF & PCDD in Fish FISH 600/3-90-022 03/01/1990

Pentachlorophenol (PCP) - colimetric field test 8540 SW-846 Update IVB www

Pentachlorophenol Screening by Immunoassay 4010A SW-846 Ch 4.4 www 12/01/1996

Perchlorate by Ion Chromatography 9058 SW-846 Update IVB www

Perchlorate in DW using Ion Chromatography 0314 815/R-00-014 www 11/01/1999

Perfluorocarbon Tracer (PFT) IP-4A 600/4-90-10 04/01/1990

Performance Specifications 1-7 PF 60 App B www

Permethrin 0608.2 821/R-93-010-A CD 06/01/1993

Pesticide - GC/ECD Hexane/Methanol Extraction FM-22 540/2-88-005 09/01/1988

Pesticide - Isothermal GC/ECD Hexane Extraction FM-23 540/2-88-005 09/01/1988

Pesticide by Bonded Sorbents FM-D2 540/2-88-005 09/01/1988

Pesticide residue in food & feed commodities RAM /oppbead1 /methods

Pesticide Sampling - NEIC SAMPLIN 01A0005249 08/01/1985

Pesticides INDOOR 600/8-90-041 www

Pesticides & PCBs by low volume PUF & GC/MD TO-10A 625/R-96-010b ttn/amtic 01/01/1999

Pesticides and PCBs by high volume PUF & GC/MD TO-04A 625/R-96-010b ttn/amtic 01/01/1999

Pesticides by GC/AED (Atomic Emission Detection) 8085 SW-846 Update IVB www 03/15/1999

Pesticides by Low Volume Polyurethane (PUF) TO-10 600/4-89-017 06/01/1988

Pesticides in Fish FISH 600/3-90-023 03/01/1990

Pesticides in GW - HPLC/Ultraviolet Detector PEST-04 EMSL 01A0005658

Pesticides in Humans and Environmental Samples PEST 600/8-80-038 06/01/1980

Pesticides in soil & water ECM /oppbead1 /methods

Pesticides, Carbamate & Amide 0632.1 821/R-93-010-A CD 06/01/1993

Pesticides, Carbamate and Urea 0632 821/R-93-010-A CD 06/01/1993

Pesticides, Carbon/Hydrogen/Oxygen Containing 0616 821/R-93-010-A CD 06/01/1993

Pesticides, Certain Amine & Lethane in WW - GC 0645 821/R-93-010-A CD 06/01/1993

Pesticides, Chlorinated - Neutrals/Sediments PP-001 600/4-81-055

Pesticides, Chlorinated in Fish PP-002 600/4-81-055

Pesticides, Chlorinated in Water by GC with ECD 0508 600/R-95-131 NEMI 08/01/1995

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 20 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Pesticides, Dinitro Aromatic by GC 0646 821/R-93-010-A CD 06/01/1993 

Pesticides, Dinitroaniline in Wastewater 0627 821/R-93-010-A CD 06/01/1993

Pesticides, Dithiocarbamates by GC 0630.1 821/R-93-010-A CD 06/01/1993

Pesticides, Dithiocarbamates in Wastewater 0630 821/R-93-010-A CD 06/01/1993

Pesticides, Netural Nitrogen-Containing 0633.1 821/R-93-010-A CD 06/01/1993

Pesticides, Nitrogen & Phosphorus in GW by GC 0507 600/R-95-131 NEMI 08/01/1995

Pesticides, Organohalide & PCBs in WW 0617 821/R-93-010-A CD 06/01/1993

Pesticides, Organo-halide/phosphorus:Malathion 1618 01A0006086 07/01/1989

Pesticides, Organonitrogen:Bromacil/Deet/Hexazin 0633 821/R-93-010-A CD 06/01/1993

Pesticides, Organophosphorous in WW 0614.1 821/R-93-010-A CD 06/01/1993

Pesticides, Organophosphorus In WW 0614 821/R-93-010-A CD 06/01/1993

Pesticides, Organophosphorus: Trichloronate - WW 0622 821/R-93-010-A CD 06/01/1993

Pesticides, Thiocarbamate in WW - GC 0634 821/R-93-010-A CD 06/01/1993

Pesticides, Thiophosphate:Aspon/Phosmet/Thionazi 0622.1 821/R-93-010-A CD 06/01/1993

Pesticides, Triazine: Simetryn/Terbutryn in WW 0619 821/R-93-010-A CD 06/01/1993

Pesticides, Volatile:Chloropicrim/Ethyl Dibromid 0618 821/R-93-010-A CD 06/01/1993

Pesticides: Basalin (Fluchloralin)/CDN/Dinocap 0646 821/R-93-010-A CD 06/01/1993

Pesticides: Benomyl & Carbendazim in Wastewater 0631 821/R-93-010-A CD 06/01/1993

Pesticides: Ethion/EPN/Dioxathion/Terbufos 0614.1 821/R-93-010-A CD 06/01/1993

Pesticides: Fenarimol/MGK/Pronamide 0633.1 821/R-93-010-A CD 06/01/1993

Pesticides: Napropamide/Propanil/Vacor 0632.1 821/R-93-010-A CD 06/01/1993

Petroleum Hydrocarbons in Soil by Turbidmetric 9074 SW-846 Ch 4.5 Update IVA www 01/01/1998

Petroleum Hydrocarbons Soil Screen by Immunoassy 4030 SW-846 Ch 4.4 www 12/01/1996

Petroleum Hydrocarbons, Total Recoverable 0418.1 600/4-79-020 www

pH - Continuous Monitoring (Electrometric) 0150.2 600/4-79-020 NEMI

pH - Electrometric 0150.1 600/4-79-020 NEMI

pH - Electrometric Measurement 9040B SW-846 Ch 8.2 www 01/01/1995

pH - Electrometric Measurement 9040C SW-846 Ch 8 Update IIIB www 10/30/2002

pH - Paper Method 9041A SW-846 Ch 6 www 07/01/1992

pH Adjustment (6.10) TIE-CHR 600/6-91-005F www 05/01/1992

pH Adjustment Test, Acute Effluent (8.3) TIE-ACUT 600/6-91-003 www 02/01/1991

pH Adjustment/C18 Solid Phase Extraction (8.6) TIE-ACUT 600/6-91-003 www 02/01/1991

pH Adjustment/Filtration Test (8.4) TIE-ACUT 600/6-91-003 www 02/01/1991

pH Adjustment/Filtration Test, (8.5) TIE-ACUT 600/6-91-003 www 02/01/1991

pH of Wet Deposition -Electrolytic Determination 0150.6 600/4-86-024 03/01/1986

Phenol - Liquid-Liquid Extraction & GC FM-24 540/2-88-005 09/01/1988

Phenolics - Colorimetric Automated 4-AAp 9066 SW-846 Ch 5 www 09/01/1986

Phenolics - Spectrophotometric, Manual 4-AAP 9065 SW-846 Ch 5 www 09/01/1986

Phenolics - Spectrophotometric, MBTH 9067 SW-846 Ch 5 www 09/01/1986

Phenols 0604 /waterscience 136 App A NEMI

Phenols - Colorimetric4-AAP 0420.2 600/4-79-020 NEMI

Phenols - Spectrophot/4-AAP 0420.1 600/4-79-020 NEMI

Phenols - Spectrophot/MBTH 0420.3 600/4-79-020 www

Phenols by GC: 8041A SW-846 Ch 4.3 Update IVB www

Phenols by GC: Capillary Column Technique 8041 SW-846 Ch 4.3. www 12/01/1996

Phenols in DW by SPE & cap col GC/MS 0528 815/R-00-014 NEMI 04/01/2000

Phenols in Sediment PP-008 600/4-81-055

Phenoxy-Acid Pesticides 1658 821/R-93-010-A CD 06/01/1993

Phenylurea compounds in DW by SPE & HPLC/UV 0532 815/R-00-014 NEMI 06/01/2000

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 21 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Phosgene by HPLC TO-06 600/4-89-017 ttn/amtic 

Phosphorus - colorimetric/ 2 reagents 0365.3 600/4-79-020 NEMI

Phosphorus - manual colorimetric/1 reagent 0365.2 600/4-79-020 NEMI

Phosphorus - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Phosphorus, All Forms - Colorimetric/Automated 0365.1 600/4-79-020 NEMI

Phosphorus, Total - Colorimetric/Automated 0365.4 600/4-79-020 NEMI

Photochemical Degradation 0021 600/2-85-028

Phthalate & Adipate Esters in DW by LLE or LSE 0506 821/R-93-010-B NEMI 07/01/1990

Phthalate & Adipate Esters/Liquid-Liquid or LSE 0506 600/R-95-131 www 08/01/1995

Phthalate Ester 0606 /waterscience 136 App A NEMI

Phthalate Esters by Cap GC/ECD 8061A SW-846 Ch 4.3. www 12/01/1996

Physical Methods - Overburdens & Minesoils 0003.4 600/2-78-054 03/01/1978

Phytoplankton ESTUARI 430/9-86-004 03/01/1986

Picloram in Wastewater - LC 0644 821/R-93-010-A CD 06/01/1993

Platinum - AA, Direct Aspiration 0255.1 600/4-79-020 NEMI

Platinum - AA, Furnace 0255.2 600/4-79-020 NEMI

Plutonium in Drinking Water 0911 01A0004860

Plutonium, uranium & thorium / soil, air, tissue RA-LV-Pl EMSL-LV-0539 CD 03/01/1979

PM - Metals in ambient by ICP/MS IO-3.5 625/R-96-010a ttn/amtic/ 07/01/1999

PM 2.5 - acidic & basic gases by Annular Deuder IO-4 625/R-96-010a ttn/amtic/ 07/01/1999

PM 2.5 - reactive acidic & basic gases IO-4.2 625/R-96-010a ttn/amtic/ 07/01/1999

PM 2.5 - strong acidity of atmospheric IO-4.1 625/R-96-010a ttn/amtic/ 07/01/1999

PM and MCEM from Aluminum Production Facilities 0315 63 App A /ttn/emc 10/07/1997

PM Asphalt Roofing (Particulate Matter) 0005A 60 App A /ttn/emc 06/13/1990

PM Baghouses (Particulate Matter) 0005D 60 App A /ttn/emc 08/20/1996

PM Condensible Particulate Matter 0202 51 App M /ttn/emc 09/25/1996

PM Fiberglass Plants (Particulate Matter) 0005E 60 App A /ttn/emc 08/20/1996

PM Fluid Catalytic Cracking Unit 0005F 60 App A /ttn/emc 09/25/1996

PM Nonsulfuric Acid (Particulate Matter) 0005B 60 App A /ttn/emc 06/13/1990

PM Wood Heaters from a Dilution Tunnel 0005G 60 App A /ttn/emc 08/20/1996

PM Wood Heaters from a Stack 0005H 60 App A /ttn/emc 08/20/1996

PM10 - Andersen Continuous Beta Attenuation IO-1.1 625/R-96-010a ttn/amtic/ 07/01/1999

PM10 - Andersen Dichotomous Sampler IO-2.2 625/R-96-010a ttn/amtic/ 07/01/1999

PM10 - Calculations for Standard Volume IO-2.4 625/R-96-010a ttn/amtic/ 07/01/1999

PM10 - continuous determination of SPM in ambien IO-1 625/R-96-010a ttn/amtic/ 07/01/1999

PM10 - In-Stack, CRS (Constant Sampling Rate) 0201 51 App M /ttn/emc 04/17/1990

PM10 - In-stack, CRS (Constant Sampling Rate) 0201A 51 App M /ttn/emc 09/25/1996

PM10 - Integrated sampling of SPM in ambient IO-2 625/R-96-010a ttn/amtic/ 07/01/1999

PM10 - Particulate Matter as PM10 in Atmosphere PM10 50 App J www 08/07/1987

PM10 - Particulate Matter as PM10 in Atmosphere PM10 50 App M www 08/07/1987

PM10 - Ruppecht & Patashnick (R&P) TEOM Particle IO-1.3 625/R-96-010a ttn/amtic/ 07/01/1999

PM10 - Rupprecht & Patashnick LV Partisol Sample IO-2.3 625/R-96-010a ttn/amtic/ 07/01/1999

PM10 - Thermo Environmental Instruments (Wedding IO-1.2 625/R-96-010a ttn/amtic/ 07/01/1999

PM10 and SPM - High Volume (HV) Sampler IO-2.1 625/R-96-010a ttn/amtic/ 07/01/1999

PM2.5 - fine particulate matter in atmosphere PM2.5 50 App L www 12/13/1996

PNA, Total - Ultraviolet Fluorescence Spectropho FM-26 540/2-88-005 09/01/1988

Polar organic compound/capillary electrophoresis 8355 not available SW-846 dev

Polonium-210 Emissions from Stationary Sources 0111 61 App B /ttn/emc 04/01/1996

Polonium-210 in Drinking Water 0912 01A0004860

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 22 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Poly(ethylene glycol)-600 - Pharmaceutical 1673 821/B-94-001 NEMI 01/01/1995 

Polychlorinated Biphenyls (PCBs) in Fish PCBs 600/3-90-023 03/01/1990

Polynuclear Aromatic Hydrocarbons 0610 /waterscience 136 App A NEMI

Polynuclear Aromatic Hydrocarbons 8100 SW-846 Ch 4.3. www 09/01/1986

Polynuclear Aromatic Hydrocarbons (PAH) - HPLC 8310 SW-846 Ch 4.3. www 09/01/1986

Polynuclear Aromatic Hydrocarbons (PAHs) TO-13 600/4-89-017 06/01/1988

Pond Sampler - Liquid Wastes SAMPLIN 600/2-80-018 www

Portable THC Analyzer SOIL-GAS 600/8-87-036

Post C18 Solid Phase Extraction Column (6.6) TIE-CHR 600/6-91-005F www 05/01/1992

Post C18 SPEC & pH Adjustment (6.13) TIE-CHR 600/6-91-005F www 05/01/1992

Potassium - AA, Direct Aspiration 0258.1 600/4-79-020 NEMI

Potassium - AA, Direct Aspiration 7610 SW-846 Ch 3.3 www 09/01/1986

Potassium - AA, flame technique 0258.1 CL ILM04.0 exhibit D www clp

Potassium - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Potentiometric Determination of Nitrite Aqueous 9216 SW-846 Ch 5 Update IVA www 01/01/1998

Precision & Accuracy/Recovery for Metals - ICP METALS 136 App D www CD

Preliminary Methods PRE 1-4 /ttn/emc

Preparation - Standard Operating Procedures SOPs QA/G-6 240/B-01-004 quality1/ 03/01/2001

Pressurized Fluid Extraction (PFE) 3545A SW-846 Ch 4.2. Update IVA www 01/01/1998

Priority Pollutant - Organic Compounds, Metals ESTUARI 430/9-86-004 03/01/1986

Priority Pollutants, Organic, in Sludges 0625-S 600/4-84-001

Probit Analysis for Chronic Toxicity STATS 821/R-02-013 WET www 10/01/2002

Product performance test guidelines - TSCA/FIFRA 0810 www OPPT

Product properties test guidelines - TSCA/FIFRA 0830 www OPPT 09/22/1996

Protozoa & Enteric Virus Sample Collection ICR 814/B-95-001 www 06/01/1995

Protozoan Method - Giardia & Cryptosporidium ICR 814/B-95-003 www 06/01/1995

Purge & Trap for Aqueous Samples - Organic 5030B SW-846 Ch 4.2. www 12/01/1996

Purgeable Aromatics 0602 /waterscience 136 App A NEMI

Purgeable Halocarbons 0601 /waterscience 136 App A NEMI

Purgeable organic compounds - capillary column 0524.2 CD 08/01/1992

Purgeable Organic Compounds, Rapid Screening SCREEN 01A0005957 06/29/1983

Purgeable Organic Halides (POX) 9021 SW-846 Ch 5 www 07/01/1992

Purgeable Organics in Sediment PP-012 600/4-81-055

Purgeables 0624 /waterscience 136 App A NEMI

Pyrethrins & Pyrethoids 1660 821/R-93-010-A CD 06/01/1993

QA/QC Plan & Data Validation Procedures -Removal SAMPLIN 540/G-90-004 www 04/01/1990

QHEI (Qualitative Habitat Evaluation Index) FISH 600/R-92-111 www 03/01/1993

Quality assurance project plans QA/G-5 600/R-98-018 quality1/ 02/01/1998

Quality Control Procedures QUALITY SW-846 Ch 1 www 07/01/1992

Quality Management Plans (replace 004/80) QA/R-2 240/B-01-002 quality1/ 03/01/2001

Radioactive Cesium 0901 600/4-80-032 www 08/01/1980

Radioactive Cesium in drinking water RA-CI-Ces 600/4-75-008 CD 03/01/1976

Radioactive Iodine 0902 600/4-80-032 www

Radioactive Iodine in DW - distillation RA-CI-Io- 600/4-75-008 CD 03/01/1976

Radioactive Iodine in DW - precipitation RA-CI-Io- 600/4-75-008 CD 03/01/1976

Radioactive Strontium 0905 600/4-80-032 www

Radioactive strontium in drinking water RA-CI-Str 600/4-75-008 CD 03/01/1976

Radioactivity, Gross Alpha and Gross Beta 0900 600/4-80-032 NEMI 08/01/1980

Radionuclide Emissions from stationary sources 0114 61 App B /ttn/emc 04/01/1996

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 23 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Radionuclides, Gamma Emitting 0901.1 600/4-80-032 www 

Radiostrontium - radiochemical in aqueous, sea Sr-04 520/5-84-006 CD 08/01/1994

Radium, Alpha-Emitting Isotopes 0903 600/4-80-032 www 08/01/1980

Radium, Gross Alpha Screening Procedure 0900.1 600/4-80-032 www

Radium-226 & Radium-228 / soil, air, tissue RA-LV-Ra EMSL-LV-0539 CD 03/01/1979

Radium-226 in DW - radon emanation RA-CI-R2 600/4-75-008 CD 03/01/1976

Radium-226 radiochemical de-emanation Ra-04 520/5-84-006 CD 08/01/1994

Radium-226 radiochemical in water Ra-03 520/5-84-006 CD 08/01/1994

Radium-226 Radon Emanation Technique 0903.1 600/4-80-032 NEMI 08/01/1980

Radium-228 0904 600/4-80-032 www

Radium-228 9320 SW-846 Ch 5 www 09/01/1986

Radium-228 in DW - sequential method RA-CI-R2 600/4-75-008 CD 03/01/1976

Radium-228 radiochemical in water Ra-05 520/5-84-006 CD 08/01/1994

RadKleen 0011 600/2-85-028

Radon INDOOR 600/8-90-041 www 06/01/1990

Radon & Radon Decay Product Measurement Devices RADON 402/R-92-004 www 07/01/1992

Radon & Radon Decay Product Measurements / HomesRADON 402/R-92-003 www 06/01/1993

Radon in DW by Liquid Scintillation Counting 0913 01A0006252 05/01/1991

Radon, Indoor & Decay Product Measurements SAMPLIN 402/R-92-004 www 07/01/1992

Radon, Protocols for Screening and Measurement RADON 520/1-86-014 02/01/1987

Radon-222 Emissions 0115 61 App B /ttn/emc 04/01/1996

RCRA waste - updates SW-846 Chapter 9 SAMPLIN 530/D-02-002 www

RDX in Soil and Water by Immunoassay 4051 SW-846 Ch 4.4 www 12/01/1996

Reactive Acidic, Basic Gases, PM in Indoor Air IP-9 600/4-90-10 04/01/1990

Reg 1 Lab Data Validation-volatile/semivolatile GUIDELI 01A0006125 02/01/1988

Region 1 Compendium of QA Project Plan Guidance QA-GUID 01A0007832 www 10/01/1999

Remote Sensing & Surface Geophysical (1.1-1.6) GEOPHYS 625/R-93-003a www 05/01/1993

Reproduction - Red Macroalga 1009 821/R-02-014 WET www 10/01/2002

Reproductive of endocrine-disrupting / minnow TOXICIT 600/R-01-067 www 06/01/2002

Requirements for Environmental Programs QA/R-1 EPA Manual 53 quality1/ 05/01/2000

Requirements for QA project plans QA/R-5 240/B-01-003 quality1/ 03/01/2001

Residual HC in Rubber Crumb by Capillary GC 0313B 63 App A /ttn/emc 03/17/1997

Residual Hexane 0310A 63 App A /ttn/emc 03/17/1997

Residual Hydrocarbon in Rubber Crumb 0313A 63 App A /ttn/emc 03/17/1997

Residual N-Hexane in EDPM Rubber 0310C 63 App A /ttn/emc 03/17/1997

Residual Solvent 0310B 63 App A /ttn/emc 03/17/1997

Residual Styrene in SBR Latex by GC 0312A 63 App A /ttn/emc 03/17/1997

Residue chemistry test guidelines - TSCA/FIFRA 0860 www OPPT

Residue, Filterable 0160.1 600/4-79-020 NEMI

Residue, Non-Filterable & Total Suspended Solids 0160.2 600/4-79-020 NEMI

Residue, Settleable Matter 0160.5 600/4-79-020 www

Residue, Total 0160.3 600/4-79-020 NEMI

Residue, Volatile 0160.4 600/4-79-020 NEMI

Respirable Particulate Matter (PM) in Indoor Air IP-10 600/4-90-10 04/01/1990

Rhenium - AA, Direct Aspiration 0264.1 600/4-79-020 www

Rhenium - AA, Furnace 0264.2 600/4-79-020 www

Rhodium - AA, Direct Aspiration 0265.1 600/4-79-020 NEMI

Rhodium - AA, Furnace 0265.2 600/4-79-020 NEMI

Rotenone - LC 0635 821/R-93-010-A CD 06/01/1993

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 24 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

RPBs - Rapid Bioassessment of Periphyton, fish BIOMONI 841/B-99-002 www 07/01/1999 

Ruthenium - AA, Direct Aspiration 0267.1 600/4-79-020 NEMI

Ruthenium - AA, Furnace 0267.2 600/4-79-020 NEMI

Salinity ESTUARI 430/9-86-004 03/01/1986

Salmonella - Microbiological Monitoring/Water MICROBI 600/8-78-017 www

Salmonella sp. in biosolids 1682 821/R-98-004 CD 08/01/1998

Salmonella/Microsomal Mutagenicity Assay (Ames) AMES 600/4-82-068 03/01/1983

Sample Collection 0012.1 600/4-82-029 www

Sample Collection Protocol SAMPLIN 600/2-85-104 www 09/01/1985

Sample Confirmation Procedures for Toxicity TIE 600/R-92-081 www 09/01/1993

Sample Frequency 0004.3 600/4-82-029 www

Sample Methods & Equipment - Microbiological 0014.4 600/4-82-029 www

Sample Preparation for Volatile Organics 5000 SW-846 Ch 4.2. www 12/01/1996

Sample Preparation Methods - Inorganic Analytes INORGAN SW-846 Ch 3.2 www 12/01/1996

Sample Preservation 0017.1 600/4-82-029 www

Samples, Number of 0004.2 600/4-82-029 www

Sampling Agricultural Discharges 0007.8 600/4-82-029 www

Sampling design for environmental data collect QA/G-5S quality1/ 08/01/2000

Sampling Equipment Decontamination SOP #2006 www.ert.org

Sampling House Dust for Lead by Wipe & Vacuum SAMPLIN 747/R-95-007 09/01/1995

Sampling Industrial Wastewaters 0006.8 600/4-82-029 www

Sampling Sludges 0010.8 600/4-82-029 www

Sampling Surface Waters - Fish Field & Lab FISH 600/R-92-111 www 03/01/1993

Sampling Train - Modified Method 5 semi-volatile 0010 SW-846 Ch 10 www 09/01/1986

Sampling Waters, Organisms & Sediments 0008.7 600/4-82-029 www

Scarification 0010 600/2-85-028

Screen for Use of High of Low-Level VOA Prep/PID 3815 SW-846 www Update IVB www 09/01/1999

Screening Method for Air Toxics Emission Factors SCREEN /ttn/emc 10/11/1991

Secondary Devices 0003.5 600/4-82-029 www

Sediment - Chironomus tentans life-cycle test 0100.5 600/R-99-064 www 03/01/2000

Sediment - freshwater amphipods 42-d survival 0100.4 600/R-99-064 www 03/01/2000

Sediment - marine amphipods 10-d survival test 0100.4 600/R-94-025 www 03/01/2000

Sediment & Water Samples - Handling & Analysis SAMPLES 01A0005044 05/01/1981

Sediment 28-d chronic toxicity - marine amphipod SOIL Tox 600/R-01-020 www 03/01/2001

Sediment Assessment Strategy Recommended by IJC SEDIMEN 823/R-92-006 www 09/01/1992

Sediment Bioaccumulation, Bedded Marine/Estuarin SEDIMEN 600/R-93-183 09/01/1993

Sediment Quality Triad Approach SEDIMEN 823/R-92-006 www 09/01/1992

Sediment Sampling SOP #2016 www.ert.org

Sediments - Bioaccumulation / Lumbriculus varieg 0100.3 600/R-99-064 www 03/01/2000

Sediments - Survival & Growth/Chironomus tentans 0100.2 600/R-99-064 www 03/01/2000

Sediments - Survival Test / Hyalella azteca 10-d 0100.1 600/R-99-064 www 03/01/2000

Selenium - AA, Furnace 0270.2 600/4-79-020 NEMI

Selenium - AA, furnace technique 0270.2 CL ILM04.0 exhibit D www clp

Selenium - AA, Furnace Technique 7740 SW-846 Ch 3.3 www 09/01/1986

Selenium - AA, Gaseous Borohydride 7742 SW-846 Ch 3.3 www 09/01/1994

Selenium - AA, Gaseous Hydride 0270.3 600/4-79-020 www

Selenium - AA, Gaseous Hydride 7741A SW-846 Ch 3.3 www 09/01/1994

Selenium - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Selenium in Sediment PP-003 600/4-81-055

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 25 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Semivolatile by Bonded Sorbents FM-D3 540/2-88-005 09/01/1988 

Semivolatile organic by SPE & cap col GC/MS 0526 815/R-00-014 NEMI 06/01/2000

Semivolatile Organic Compounds - Pharmaceutical 1665 821/B-94-001 CD 01/01/1995

Semivolatile Organic Compounds by GC/MS 8270D SW-846 Ch 4.3. Update IVA www 01/01/1998

Semivolatile Organic Compounds by GC/MS Cap Col 8270C SW-846 Ch 4.3. www 12/01/1996

Semivolatile Organic Compounds -Isotope Dilution 1625B 136 App A NEMI

Semivolatile Organic Compounds/Isotope Dillution 1625C 01A0006089 CD 01/22/1991

Semivolatile Organics - GC/FT-IR Cap Column 8410 SW-846 Ch 4.3. www 09/01/1994

Separatory Funnel Liquid-Liquid Extraction 3510C SW-846 Ch 4.2. www 12/01/1996

SFE of PCBs & Orgaochlorine Pesticides (OCPs) 3562 SW-846 Ch 4.2. Update IVA www 01/01/1998

Shell Development - Pacific Oyster & Mussel 1005 600/R-95-136 www 08/01/1995

Silica - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Silica Gel Cleanup (florisil) 3630C SW-846 Ch 4.2. www 12/01/1996

Silica, Dissolved - Colorimetric 0370.1 600/4-79-020 NEMI

Silver - AA, Direct Aspiration 0272.1 600/4-79-020 NEMI

Silver - AA, Direct Aspiration 7760A SW-846 Ch 3.3 www 07/01/1992

Silver - AA, Furnace 0272.2 600/4-79-020 NEMI

Silver - AA, furnace technique 0272.2 CL ILM04.0 exhibit D www clp

Silver - AA, Furnace Technique 7761 SW-846 Ch 3.3 www 07/01/1992

Silver - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Size Specific Impaction IP-10A 600/4-90-10 04/01/1990

Sludge, Ntl Sewage Survey Procedures & Protocols SAMPLIN 01A0006083 08/01/1989

Slug Tests SOP #2158 www.ert.org

Small Ducts - Sample & Velocity Traverses 0001A 60 App A /ttn/emc 09/25/1996

SOD (Sediment Oxygen Demand) by Bench Model SOD 01A0006379 www 05/01/1979

Sodium - AA, Direct Aspiration 0273.1 600/4-79-020 NEMI

Sodium - AA, Direct Aspiration 7770 SW-846 Ch 3.3 www 09/01/1986

Sodium - AA, flame technique 0273.1 CL ILM04.0 exhibit D www clp

Sodium - AA, Furnace 0273.2 600/4-79-020 www

Sodium - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Sodium Thiosulfate Addition (6.3) TIE-CHR 600/6-91-005F www 05/01/1992

Soil & Foliar in Long-Term Environ Monitoring MONITO 600/R-95-077 www 06/01/1995

Soil and Waste pH 9045D SW-846 Ch 6 Update IIIB www 10/30/2002

Soil Gas Sampling SOP #2149 www.ert.org

Soil Gas Sampling - Direct Injection Auger FM-17 540/2-88-005 09/01/1988

Soil Gas Sampling - Direct Injection Stopper FM-13 540/2-88-005 09/01/1988

Soil Gas Sampling - Downhole Profiling FM-16 540/2-88-005 09/01/1988

Soil Gas Sampling - Mini-Barrel Sampler FM-11 540/2-88-005 09/01/1988

Soil Gas Sampling - One-Liter Syringe FM-12 540/2-88-005 09/01/1988

Soil Gas Sampling - Perforated Tube FM-14 540/2-88-005 09/01/1988

Soil Gas Sampling - Tenax Tubes FM-15 540/2-88-005 09/01/1988

Soil Gas Sampling, Grab of VOCs - LGAS SOIL-GAS 600/2-87-027

Soil Gas Sampling, Passive - Industrial Hygiene FM-10 540/2-88-005 09/01/1988

Soil Samplers - Auger, Sampling Trier SAMPLIN 600/2-80-018 www

Soil Sampling SOP #2012 www.ert.org

Soil sampling guidance -Superfund SAMPLIN 540/R-95-141 www.ert.org 12/01/1995

Soil Sampling Protocols SAMPLIN 600/R-92-128 www 07/01/1992

Soil Sampling Quality Assurance User's Guide SOIL 600/8-89-046 www 03/01/1989

Soils - Description & Sampling Field Guide SAMPLIN 625/12-91-002 11/01/1991

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 26 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Solid & Hazardous Wastes PROPERT SW-846 Ch 6 www 12/01/1996 

Solid & Hazardous Wastes - Characteristics REACTIV SW-846 Ch 8.3 www 12/01/1996

Solid Adsorbent Cartridge IP-6A 600/4-90-10 04/01/1990

Solid Adsorbent Tubes IP-1B 600/4-90-10 04/01/1990

Solid Phase Extraction (SPE) 3535A SW-846 Ch 4.2. Update IVA www 01/01/1998

Solid Phase Extraction (SPE) - Organics 3535 SW-846 Ch 4.2. www 12/01/1996

Solid Phase Extraction (SPE) including explosive 3535A SW-846 Ch 4.2. Update IVB www 11/01/1998

Solids, Total Volatile ESTUARI 430/9-86-004 03/01/1986

Solids, Total Water Content ESTUARI 430/9-86-004 03/01/1986

Solvent Extractable Non-Volatile by HPLC/PB/MS 8325 SW-846 Ch 4.3. www 12/01/1996

Solvent Extractable Non-Volatile by HPLC/TS/MS 8321A SW-846 Ch 4.3. www 12/01/1996

Solvent Vapor Cleaner Emissions 0307 63 App A /ttn/emc 09/25/1997

Solvent Washing 0012 600/2-85-028

Solvent-Extractable Nonvolatile Compounds - UV 8321B SW-846 Ch 4.3. Update IVB www 01/01/1998

Solvent-extractable non-volatile HPLC/E/MS UV 8322 not available SW-846 dev

Somatic Coliphage in DW enrichment presence 1601 821/R-01-030 /nerlcwww www 04/01/2001

Source Assessment Sampling System (SASS) 0020 SW-846 Ch 10 www 09/01/1986

Soxhlet Extraction - Organics 3540C SW-846 Ch 4.2. www 12/01/1996

Spearman-Karber Method for Acute Toxicity STATS 821/R-02-013 WET www 10/01/2002

Specific Conductance 9050A SW-846 Ch 6 www 12/01/1996

Specific oxygen uptake rate (SOUR) in biosolids 1683 821/R-01-014 CD 02/01/2000

Spiked-Sediment Toxicity Test Approach (SSTT) SEDIMEN 823/R-92-006 www 09/01/1992

SPM - Metals / Neutron Activation (NAA) IO-3.7 625/R-96-010a ttn/amtic/ 07/01/1999

SPM - Metals in ambient by AAS IO-3.2 625/R-96-010a ttn/amtic/ 07/01/1999

SPM - Metals in ambient by ICP IO-3.4 625/R-96-010a ttn/amtic/ 07/01/1999

SPM - Metals in ambient by Proton X-Ray (PIXE) IO-3.6 625/R-96-010a ttn/amtic/ 07/01/1999

SPM - Metals in ambient PM by XRF IO-3.3 625/R-96-010a ttn/amtic/ 07/01/1999

SPM - selection, preparation & extraction IO-3.1 625/R-96-010a ttn/amtic/ 07/01/1999

Spray drift test guidelines - TSCA/FIFRA 0840 www OPPT

Stack gas velocity / (decay near stack wall) 0002H 60 App A /ttn/emc

Stack gas-velocity/volumetric flow rate-2D probe 0002G 60 App A /ttn/emc

Stack gas-velocity/volumetric flow rate-3D probe 0002F 60 App A /ttn/emc

Stainless Steel Canister IP-1A 600/4-90-10 04/01/1990

Standard Plate Count (SPC) MICROBI 600/8-78-017 www

Steam Cleaning 0013 600/2-85-028

Steel's Many-One Rank Test - Chronic Toxicity STATS 821/R-02-013 WET www 10/01/2002

Streams - field & lab for macroinvertebrate EMAP 01A0007986 www /maia 07/01/1997

Strontium - AA, Direct Aspiration 7780 SW-846 Ch 3.3 www 07/01/1992

Strontium - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Strontium-89 & -90 / vegetation, soil, tissue RA-LV-Str EMSL-LV-0539 CD 03/01/1979

Styrene in SBR Latex by Capillary GC 0312B 63 App A /ttn/emc 03/17/1997

Styrene in SBR Latex produced by Emulsion Polym 0312C 63 App A /ttn/emc 03/17/1997

Substances Liable to Spontaneous Combustion 1050 SW-846 www Update IVB www 07/01/1999

Subsurface Solids for Groundwater Quality SAMPLIN 600/2-81-160

Sulfate 0300.0 600/4-79-020 www

Sulfate - Colorimetric, Automated, Chloranilate 0375.1 600/4-79-020 NEMI

Sulfate - Colorimetric, Automated, Chloranilate 9035 SW-846 Ch 5 www 09/01/1986

Sulfate - Colorimetric, Automated, Methylthymol 0375.2 600/4-79-020 NEMI

Sulfate - Colorimetric, Automated, Methylthymol 9036 SW-846 Ch 5 www 09/01/1986

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 27 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Sulfate - Colorimetry, Automated 0375.2 600/R-93-100 www 08/01/1993 

Sulfate - Gravimetric 0375.3 600/4-79-020 NEMI

Sulfate - Turbidimetric 0375.4 600/4-79-020 NEMI

Sulfate - Turbidimetric 9038 SW-846 Ch 5 www 09/01/1986

Sulfide - Colorimetric, Methylene Blue 0376.2 600/4-79-020 NEMI

Sulfide - Potentiometric in Aqueous/Ion-Sel Ele 9215 SW-846 Ch 5 www 12/01/1996

Sulfide - Titrimetric, Iodine 0376.1 600/4-79-020 NEMI

Sulfides, Acid-Soluble & Insoluble - Titrimetric 9034 SW-846 Ch 5 www 12/01/1996

Sulfides, Acid-Soluble & Insoluble -Distillation 9030B SW-846 Ch 5 www 12/01/1996

Sulfides, Total & Water Soluble ESTUARI 430/9-86-004 03/01/1986

Sulfite - Titrimetric 0377.1 600/4-79-020 NEMI

Sulfur (Semicontinuous Determination) 0016 60 App A /ttn/emc 10/10/1996

Sulfur Cleanup 3660B SW-846 Ch 4.2. www 12/01/1996

Sulfur Dioxide & Carbon Dioxide - Daily Fossil 0006B 60 App A /ttn/emc 08/20/1996

Sulfur Dioxide & Carbon Dioxide - Fossil Fuel 0006A 60 App A /ttn/emc 09/25/1997

Sulfur Dioxide Emissions - Stationary by IAP 0006C 60 App A /ttn/emc 09/25/1996

Sulfur Dioxide Emissions (SO2) 0006 60 App A /ttn/emc 09/25/1996

Sulfur Dioxide in Atmosphere - Pararosaniline AIR 50 App A www

Sulfur Dioxide Removal & PM, SO2, NOx Rates 0019 60 App A /ttn/emc 04/15/1996

Sulfur, Total Reduced - Stationary/Impinger 0016A 60 App A /ttn/emc 09/25/1996

Sulfur, Total Reduced (TRS Alt.) 0015A 60 App A /ttn/emc 04/01/1996

Sulfuric Acid Mist 0008 60 App A /ttn/emc 10/29/1996

Sulfuric Acid/Permanganate Cleanup 3665A SW-846 Ch 4.2. www 12/01/1996

Supercritical Fluid Extraction - PAH 3561 SW-846 Ch 4.2. www 12/01/1996

Supercritical Fluid Extraction - TRPH (Petroleum 3560 SW-846 Ch 4.2. www 12/01/1996

Surfacants Methylene Blue Active Substant (MBAS) 0425.1 600/4-79-020 NEMI

Surface Coatings - Volatile Matter Content 0024 60 App A /ttn/emc 09/11/1995

Surface Tension - Tanks Electroplating/Anodizing 0306B /ttn/emc 02/08/1996

Surface water - Ecological condition of wadeable EMAP 620/R-94-004F www 09/01/1998

Surface Water Sampling SOP #2013 www.ert.org

Surface Water Treatment Rule (SWTR) - Sampling WATER 814/B-92-001 04/01/1992

Survival & Growth - Fathead Minnow Larval 1000 821/R-02-013 WET www 10/01/2002

Survival & Growth - Mysid 1007 600/R-95-136 www 08/01/1995

Survival & Growth - Sheepshead Minnow Larval 1004 821/R-02-014 WET www 10/01/2002

Survival & Reproduction - Ceridaphnia 1002 821/R-02-013 WET www 10/01/2002

Survival & Teratogenicity - Minnow Embryo Larval 1005 821/R-02-014 WET www 10/01/2002

Survival & Teratogenicity -Fathead Minnow Larval 1001 821/R-02-013 WET www 10/01/2002

Survival, Growth & Fecundity - Mysid 1007 821/R-02-014 WET www 10/01/2002

Suspended PM - chemical species /filter-collect IO-3 625/R-96-010a ttn/amtic/ 07/01/1999

Swirling flask dispersant effectiveness test DISPERS 300 App C www

Synthetic Organic Compounds (SOC) - Small Water SAMPLIN 814/B-94-001 www 07/01/1994

Synthetic Precipitation Leaching Procedure 1312 SW-846 Ch 6 www 09/01/1994

Tank Sampling SOP #2010 www.ert.org

TCE & other halogenated Aliphatic hydrocarbons 8535 SW-846 Update IVB www 09/11/2001

TCLP (Toxicity Characteristic Leaching Procedure 1311 SW-846 Ch 8.4 www 07/01/1992

Technical audits & assessments QA/G-7 600/R-99-080 quality1/ 01/01/2000

Temperature - Thermometric 0170.1 600/4-79-020 NEMI

Tenax GC Adsorption TO-01 600/4-89-017 ttn/amtic

Tetrazene - Reverse Phase HPLC 8331 SW-846 Ch 4.3. www 09/01/1994

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 28 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Thallium - AA, Direct Aspiration 0279.1 600/4-79-020 NEMI 

Thallium - AA, Direct Aspiration 7840 SW-846 Ch 3.3 www 09/01/1986

Thallium - AA, Furnace 0279.2 600/4-79-020 NEMI

Thallium - AA, furnace technique 0279.2 CL ILM04.0 exhibit D www clp

Thallium - AA, Furnace Technique 7841 SW-846 Ch 3.3 www 09/01/1986

Thallium - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Thiabendazole 0641 821/R-93-010-A CD 08/01/1993

Thorium - Drinking Water 0910 01A0004860

Thorium - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Tier 2 Characterization (6.9) TIE-CHR 600/6-91-005F www 05/01/1992

Tin - AA, Direct Aspiration 0282.1 600/4-79-020 NEMI

Tin - AA, Direct Aspiration 7870 SW-846 Ch 3.3 www 09/01/1986

Tin - AA, Furnace 0282.2 600/4-79-020 NEMI

Tin - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Tissue Residue Approach SEDIMEN 823/R-92-006 www 09/01/1992

Tissue/Demersal Fishes & Epibenthic Macroinvert ESTUARI 430/9-86-004 03/01/1986

Tissue/Priority Pollutant Metals - Bioaccumulat ESTUARI 430/9-86-004 03/01/1986

Tissue/Priority Pollutant Organic Compounds ESTUARI 430/9-86-004 03/01/1986

Titanium - AA, Direct Aspiration 0283.1 600/4-79-020 NEMI

Titanium - AA, Furnace 0283.2 600/4-79-020 NEMI

TNT and RDX - fiberoptic florescent Immunoassay 4656 not available SW-846 dev

TNT and RDX - Flow cell detection Immunoassay 4655 not available SW-846 dev

TNT Explosives in Water and Soils by Immunoassy 4050 SW-846 Ch 4.4 www 12/01/1996

TNT in Soil by Coloimetric Screening 8515 SW-846 Ch 4.5 www 12/01/1996

Tobacco Smoke INDOOR 600/8-90-041 www

Toluene, Dichlorobenzene, 1,3 & 1,2 & 1,4 0602 /waterscience 136 App A NEMI

Total and Amenable Cyanide - Colorimentric UV 9012A SW-846 Ch 5 www 12/01/1996

Total Chlorine - New & Used Petroleum Prod/XRF 9075 SW-846 Ch 5 www 09/01/1994

Total Chlorine - New & Used Petroleum/Oxidative 9076 SW-846 Ch 5 www 09/01/1994

Total Chlorine - New & Used Petroleum-Field Kit 9077 SW-846 Ch 5 www 09/01/1994

Total Coliform - Membrane Filter 9132 SW-846 Ch 5 www 09/01/1986

Total Coliform - Multiple Tube Fermentation 9131 SW-846 Ch 5 www 09/01/1986

Total Coliform Rule - Sampling WATER 814/B-92-001 04/01/1992

Total Cyanide by Semi-Automated Colorimetry 0335.4 600/R-93-100 NEMI 08/01/1993

Total Cyanide in water, soil/sediment 0335.2 CL ILM04.0 exhibit D www clp

Total dissolved iron cyanide by ion chromatograp 9015 not available SW-846 dev

Total extractable material in drilling mud - SDS 1662A CD

Total Extractable Material in Drilling Mud /SDS 1662 821/R-92-008 www 12/01/1992

Total Fluoride - Primary Aluminum Plants M-14A /ttn/emc 12/02/1996

Total Fluoride emissions - primary aluminum 0014A 60 App A 10/07/1998

Total Kjeldahl Nitrogen - Semi-Automated Colori 0351.2 600/R-93-100 www 08/01/1993

Total Kjeldahl nitrogen / prelim distill digest 1687 821/R-01-004 CD 02/01/1999

Total Kjeldahl nitrogen /prelim semi-auto digest 1688 821/R-01-007 CD 02/01/1999

Total Organic Carbon 9060 SW-846 Ch 5 www 09/01/1986

Total Organic Carbon 9060A SW-846 Ch 5 Update IIIB www 10/30/2002

Total Organic Carbon, Low Level WATER 01A0005510

Total Organic Halide 0450.1 600/4-81-056

Total Organic Halides (TOX) 9020B SW-846 Ch 5 www 09/01/1994

Total Organic Halides (TOX) 9022 SW-846 Ch 5 www 09/01/1986

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 29 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Total Recoverable Petroleum Hydrocarbons - IS 8440 SW-846 Ch 4.3. www 12/01/1996 

Total Recoverable Phenolics - Semi-Automated Col 0420.4 600/R-93-100 www 08/01/1993

Total Reduced Sulfur - (GC Analysis) 0016B 60 App A /ttn/emc 04/01/1996

Total Tin & Triorganotin (AUTOCHEM North Americ EV-024/25 821/R-93-010-A CD 08/01/1996

Total, fixed & volatile solids in biosolids 1684 821/R-01-015 CD 02/01/1999

Toxaphene Soil Screening by Immunoassy 4040 SW-846 Ch 4.4 www 12/01/1996

Toxicity Reduction Evaluation - POTW TRE 833/B-99-002 www 08/01/1999

Toxicity Reduction Evaluation Protocol - POTW TRE 600/2-88-062 www 04/01/1989

Toxicity, Acute - Algal Growth/Haz Waste TOXICIT 600/3-88-029

Toxicity, Acute - Bioassays/Haz Waste Sites TOXICIT 600/8-87-043

Toxicity, Acute - Earthworm Survival/Haz Waste TOXICIT 600/3-88-029

Toxicity, Acute - Fathead Minnow/Haz Waste TOXICIT 600/3-88-029

Toxicity, Acute - Freshwater & Marine Organisms TOXICIT 600/4-90-027F OST/WET www 08/01/1993

Toxicity, Acute - Freshwater & Marine Organisms TOXICIT 821/R-01-012 OST/WET www 10/01/2002

Toxicity, Acute - Freshwater & Marine Organisms TOXICIT 821/R-02-012 www 10/01/2002

Toxicity, Acute - Freshwater Region 1 NPDES TOXICIT www 12/01/1995

Toxicity, Acute - Lettuce Root Elongation TOXICIT 600/3-88-029

Toxicity, Acute - Lettuce Seed Germination TOXICIT 600/3-88-029

Toxicity, Acute - Marine Region 1 NPDES TOXICIT www 09/01/1996

Toxicity, Aquatic - Baseline Effluent TOXICIT 600/6-91-003 www

Toxicity, Aquatic - EDTA Chelation Test TOXICIT 600/6-91-003 www

Toxicity, Aquatic - Graduated pH Test TOXICIT 600/6-91-003 www

Toxicity, Aquatic - Initial Effluent TOXICIT 600/6-91-003 www

Toxicity, Aquatic - Oxidant Reduction Test TOXICIT 600/6-91-003 www

Toxicity, Aquatic - pH Adjustment/Aeration TOXICIT 600/6-91-003 www

Toxicity, Aquatic - pH Adjustment/Filtration TOXICIT 600/6-91-003 www

Toxicity, Chronic - Freshwater Region 1 NPDES TOXICIT www 12/01/1995

Toxicity, Chronic - Marine Region 1 NPDES TOXICIT www 09/01/1996

Toxicity, Early Life Stage with Japanese Medaka TOXICIT 600/3-91-063 www

Trace Atmospheric Gas Analyzer (TAGA) FM-D1 540/2-88-005 09/01/1988

Trace Element (Metals) - ICP 0200.7 600/4-79-020 www

Trace element by ICP/AE in water & wastes 0200.7 CL ILM04.0 exhibit D www clp

Trace Element in water/wastes by ICP 0200.7 136 App C www CD

Trace Elements - GFAA 0200.9 600/R-94-111 NEMI 05/01/1994

Trace Elements - Stabilized Temp Graphite FAAS 0200.9 821/R-93-010-B CD 04/01/1991

Trace Elements - Stabilized Temperature GFAA 0200.15 600/R-94-111 www 05/01/1994

Trace Elements by Off-line Chelation 0200.13 600/R-97-072 /orthmeth NEMI 09/01/1997

Trace Elements by Stabilized Temp GF/AA 0200.12 600/R-97-072 /orthmeth NEMI 09/01/1997

Trace Elements in Ambient Waters by Chelation 1637 821/R-96-004 NEMI 01/01/1996

Trace Elements in Ambient Waters by ICP/MS 1638 821/R-96-005 NEMI 01/01/1996

Trace Elements in Ambient Waters by On-Line Chel 1640 821/R-96-007 NEMI 01/01/1996

Trace Elements in Ambient Waters by Stabilized 1639 821/R-96-006 NEMI 01/01/1996

Trace Elements in Marine Water by ICP/MA 0200.10 600/4-91-010 NEMI 04/01/1991

Trace Elements in Water & Wastes - ICP/MS 0200.8 600/R-94-111 NEMI 05/01/1994

Trace elements in water, solid & biosolids 0200.9 CD 09/01/1998

Trace elements in Water, Solids & biosolids/ICP 0200.7 NEMI 08/01/1998

Trace elements in waters & wastes/ ICP MS 0200.8 CD

Trace Elements/Marine by Online chelation-ICP/MS 0200.10 600/R-97-072 /nerlcwww /ordmeth 09/01/1997

Trace Metal Clean Rooms - Establish in Existing GUIDANC 821/B-95-001 www 04/01/1995

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 30 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Trace Metals, Documentation & Evaluation of Data GUIDANC 821/B-95-002 www 04/01/1995 

Trace Organic - Immunoassays FM-D4 540/2-88-005 09/01/1988

Tracer Gas IP-4B 600/4-90-10 04/01/1990

Transmissivity ESTUARI 430/9-86-004 03/01/1986

Traverse Points - Stationary Sources 0001 60 App A /ttn/emc 09/25/1996

Treated Filter Cassette IP-2B 600/4-90-10 04/01/1990

Triazine Herbicides as Atrazine by Immunoassay 4670 SW-846 Ch 4.4 Update IVA www 01/01/1998

Tributyltin Chloride in Marine & Fresh Waters 0282.3 01A0006709 www 10/01/1989

Trihalomethane, Maximum Total - Potential 0510.1 600/4-81-044

Trihalomethanes in Drinking Water - GC/MS 0501.3 01A0005114

Trihalomethanes in Drinking Water -purge & trap 0501.1 01A0008190 11/01/1979

Trihalomethanes in DW liquid/liquid extraction 0501.2 999Zb1118 01A0008190 www NEPI 11/01/1979

Trihalomethanes, Total by LLE/GC/ECD 0551 600/4-90-020 www 07/01/1990

Tritium 0906 600/4-80-032 www

Tritium - radiochemical / dioxane method H-02 520/5-84-006 CD 08/01/1994

Tritium / water & biological tissue RA-LV-Tri EMSL-LV-0539 CD 03/01/1979

Tritum in drinking water RA-CI-Trit 600/4-75-008 CD 03/01/1976

Trowel or Scoop - Sampling Solid Waste SAMPLIN 600/2-80-018 www

Turbidity - Nephelometric 0180.1 600/R-93-100 NEMI 08/01/1993

Ultrasonic Extraction - Organics 3550B SW-846 Ch 4.2. www 12/01/1996

Ultrasonic Extraction (non or semi-volatile) 3550C SW-846 www Update IVB www 03/01/1999

Uranium - Fluorometric Method 0908.1 600/4-80-032 www

Uranium - Laser Indirect Fluorometry in DW 0908.2 600/4-80-032 www

Uranium - Radiochemical Method 0908 600/4-80-032 www

Uranium - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Vadose Zone Hydrologic Properties (6.6.1-6.3.3) CHARAC 625/R-93-003b www 05/01/1993

Vadose Zone Infiltration, Flux (7.1.1-7.5.6) CHARAC 625/R-93-003b www 05/01/1993

Vadose Zone Soil-Solute/Gas (9.1.1-9.5.2) MONITO 625/R-93-003b www 05/01/1993

Vadose Zone Water Budget Models (8.1.1-8.4.6) CHARAC 625/R-93-003b www 05/01/1993

Vanadium - AA, Direct Aspiration 0286.1 600/4-79-020 NEMI

Vanadium - AA, Direct Aspiration 7910 SW-846 Ch 3.3 www 09/01/1986

Vanadium - AA, Furnace 0286.2 600/4-79-020 NEMI

Vanadium - AA, Furnace Technique 7911 SW-846 Ch 3.3 www 09/01/1986

Vanadium - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

Vapor Phase Organic & Inroganic Emission - FTIR 0320 63 App A /ttn/emc 05/02/1997

Vapor Phase Organic Concentration /Waste SampleS 0025E 60 App A /ttn/emc 09/25/1996

Vapor Tightness of Gasoline Tank - Pressure Vac. 0027 60 App A /ttn/emc 01/21/1994

Vapor-Phase Solvent Extraction 0014 600/2-85-028

Veihmeyer Soil Sampler SAMPLIN 600/2-80-018 www

Velocity & Flow Rate - Standard Pitot 0002C 60 App A /ttn/emc 09/25/1996

Velocity & Volumetric Flowrate - Cyclonic Flow PROPEL /ttn/emc 08/22/1996

Velocity and S-type Pitot 0002 60 App A /ttn/emc 09/25/1996

Vinyl Chloride Content of Inprocess Wastewater 0107 61 App B /ttn/emc 08/20/1996

Vinyl Chloride Content of Solvents 0107A 61 App B /ttn/emc 09/25/1996

Vinyl Chloride from Stationary Sources 0106 61 App B /ttn/emc 05/23/1995

Virus Adsorption-Elution (Viradel) Cartridge VIRUS-06 600/4-84-013 www

Virus Adsorption-Elution (Viradel) Disc Filter VIRUS-05 600/4-84-013 www

Virus Monitoring Protocol - Info Collection Req ICR 814/B-95-002 www 06/01/1995

Viruses, Cell Culture for Plaque-Forming Assay VIRUS-10 600/4-84-013 www 12/01/1987

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 31 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Viruses, Cell Preparation & Maintenance VIRUS-09 600/4-84-013 www 01/01/1987 

Viruses, Plaque Confirmation of Enteroviruses VIRUS-11 600/4-84-013 www 03/01/1988 

Viruses, Recovering from Sludges/Solids VIRUS-07 600/4-84-013 www 

Viruses, Reduction of Cytotoxicity in Sample VIRUS-08 600/4-84-013 www 04/01/1986 

Visible Emissions from Non-Recovery Coke Oven 0303A 63 App A /ttn/emc 10/27/1993 

Visible Emissions/By-Product Coke Oven Batteries 0303 63 App A /ttn/emc 09/25/1996 

Visual Opacity 0009 60 App A /ttn/emc 08/20/1996 

Visual Opacity - Time-Averaged 0203A /ttn/emc 01/06/1994 

Visual Opacity - Time-Exception 0203B /ttn/emc 01/06/1994 

VOC - by Purge & Trap/Packed Column GS/MS 0524.1 600/4-88-039 www 07/01/1991 

VOC - GC 0018 60 App A /ttn/emc 09/25/1996 

VOC Analyzer - Adsorbent SOIL-GAS 600/8-87-036 

VOC Analyzer - Flame Inization Detector (FID) SOIL-GAS 600/8-87-036 

VOC Analyzer - Photoionization Detector (PID) SOIL-GAS 600/8-87-036 

VOC Analyzer - Whole Air SOIL-GAS 600/8-87-036 

VOC Emission Potential in Waste 0305 63 App A /ttn/emc 09/25/1996 

VOC of Waste Samples 0025D 60 App A /ttn/emc 08/20/1996 

VOC Portable Analyzer - Non-dispersive Infrared SOIL-GAS 600/8-87-036 

VOC Rule - Sampling WATER 814/B-92-001 04/01/1992 

VOC Soil Sampling & Analysis SOIL 540/4-91-001 02/01/1991 

VOCs - Comparison of VOA Compositing Procedures SAMPLIN 821/R-95-035 www 09/01/1995 

VOCs - Sampling (SMVOC) 0031 SW-846 Ch 10 www 12/01/1996 

VOCs - Small Water Systems / Sample & Monitor SAMPLIN 814/B-94-001 www 07/01/1994 

VOCs (MTBE) - Purge & Trap / Cap Column GC/MS 0524.2 600/R-95-131 NEMI 08/01/1995 

VOCs by canisters and GC TO-14A 625/R-96-010b ttn/amtic 01/01/1999 

VOCs by GC/MS Capillary Column Technique 8260B SW-846 Ch 4.3. www 12/01/1996 

VOCs by Long-Path/Open-Path FT/IR Monitoring TO-16 625/R-96-010b ttn/amtic 01/01/1999 

VOCs Collected in Canisters - GC/MS TO-15 625/R-96-010b ttn/amtic 01/01/1997 

VOCs in Captured Stream 0204B 51 App M /ttn/emc 08/01/1995 

VOCs in Captured Stream (Dilution) 0204C 51 App M /ttn/emc 06/16/1997 

VOCs in Indoor Air IP-1 600/4-90-10 04/01/1990 

VOCs in Liquid Imput Stream 0204A 51 App M /ttn/emc 06/16/1997 

VOCs in Liquid Imput Stream - Distillation 0204F 51 App M /ttn/emc 06/16/1997 

VOCs in Soils/Solid Matrices by Equilibrium Head 5021 SW-846 Ch 4.2. www 12/01/1996 

VOCs in water, soil, soil gas, air by DSITMS 8265 SW-846 new www 03/01/2002 

VOCs using active sampling onto sorbent tubes TO-17 625/R-96-010b ttn/amtic 01/01/1999 

VOCs, Fugitive from Building Enclosure 0204E 51 App M /ttn/emc 06/16/1997 

VOCs, Fugitive from Temporary Total Enclosure 0204D 51 App M /ttn/emc 06/16/1997 

VOCs, Subsurface - Soil-Gas Passive Sampling SOIL-GAS 600/2-87-027 

Volatile Aromatic & Unsaturated Organic Compound 0503.1 600/4-88-039 www 07/01/1991 

Volatile Halogenated Organic Compounds in Water 0502.1 600/4-88-039 www 07/01/1991 

Volatile Matter Content & Density/Printing Inks 0024A 60 App A /ttn/emc 08/06/1993 

Volatile Organic Compounds - Air Monitoring Prog FM-04 540/2-88-005 09/01/1988 

Volatile Organic Compounds - GC/ Auto Head Samp FM-05 540/2-88-005 09/01/1988 

Volatile Organic Compounds - GC/FID 1671 821/B-94-001 CD 01/01/1995 

Volatile Organic Compounds - Headspace / HNU FM-08 540/2-88-005 09/01/1988 

Volatile Organic Compounds - Headspace / Ion Det FM-06 540/2-88-005 09/01/1988 

Volatile Organic Compounds - Headspace / OVA FM-07 540/2-88-005 09/01/1988 

Volatile Organic Compounds - Headspace/Mobile GC FM-09 540/2-88-005 09/01/1988 

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 32 
Chemical/Name Index to EPA Test Methods 

Chemical or Method Description Method EPA Report # 40 CFR Part Region 1 # Electronic Date Issued 

Number Version 

Volatile Organic Compounds - Isotope Dilution 1624B 136 App A NEMI 

Volatile Organic Compounds - Pharmaceutical 1666 821/B-94-001 CD 01/01/1995

Volatile Organic Compounds - Vacuum Distillation 5032 SW-846 Ch 4.2. www 12/01/1996

Volatile Organic Compounds - Water/Purge & Trap 0502.2 600/R-95-131 NEMI 08/01/1995

Volatile Organic Compounds (VOC) Leaks 0021 60 App A /ttn/emc 04/27/1995

Volatile Organic Compounds by GC/FID 1671A 821/B-98-016 CD 07/01/1998

Volatile Organic Compounds by Isotope Dilution 1666A 821/B-98-016 CD 07/01/1998

Volatile Organic Compounds by VD/GC/MS 8261 SW-846 Update IVB www 03/15/1999

Volatile Organic Compounds in Whole Blood BLOOD 560/5-87-008

Volatile Organic Sampling Train 0030 SW-846 Ch 10 www 09/01/1986

Volatile Organics - Fish by Purge & Trap PP-011 600/4-81-055

Volatile Organics/VOCs by Isotope Dilution GCMS 1624C 01A0006089 CD 01/22/1991

Volatile, Nonpurgeable, Water-Soluble by Azeotro 5031 SW-846 Ch 4.2. www 12/01/1996

Volatiles in low level soils 5035 CLP- OLM04.2 www clp

Volume Meters through Pipes & Small Ducts 0002A 60 App A /ttn/emc 09/25/1996

Volumetric Flow Rate Meters in Small Pipes 0002D 60 App A /ttn/emc 09/25/1996

Volunteer Estuary Monitoring Methods MONITO 842/B-93-004 /owow www 12/01/1993

Volunteer Lake Monitoring MONITO 440/4-91-002 /owow /monitoring 12/01/1991

Volunteer Stream Monitoring MONITO 841/B-97-003 /owow www 11/01/1997

Waste Dilution 3580A SW-846 Ch 4.2. www 07/01/1992

Waste Dilution for Volatile Organics 3585 SW-846 Ch 4.2. www 12/01/1996

Waste Pile Sampling SOP #2017 www.ert.org

Water Balance Method For Predicting Leachate LEACHA 530/SW-168

Water in Waste Materials by Quantitative Calcium 9001 SW-846 Ch 3.3 Update IVA www 01/01/1998

Water in Wastes by Karl-Fisher Titration 9000 SW-846 Ch 3.3 Update IVA www 01/01/1998

Water Level Measurement SOP #2151 www.ert.org

Water-borne viruses by immuoenzymatic methods VIRUSES 600/4-80-034 www 06/01/1980

Weighted Bottle Sampler - Storage Tanks, Wells SAMPLIN 600/2-80-018 www

Well Development, Hydraulic Performance/Purging SAMPLIN 600/2-85-104 www 09/01/1985

Well, Drilling & Completion Methods SAMPLIN 600/2-85-104 www 09/01/1985

White Phosphorus by Solvent Extraction and GC 7580 SW-846 Ch 3.3 www 12/01/1996

Wilcoxon Rank Sum Test for Acute Toxicity STATS CD

Wood Fired Appliances - Burn Rate & Air:Fuel 0028A 60 App A /ttn/emc 09/25/1996

Wood Heaters - Certificate & Auditing 0028 60 App A /ttn/emc 09/25/1996

XAD-4 Sorbent Tubes IP-2A 600/4-90-10 04/01/1990

Xenobiotic Chemical Contaminants in Fish FISH 600/3-90-023 03/01/1990

X-ray diffraction - crystalline phases 6300 not available SW-846 dev

X-ray fluorescence spect elemental concentration 6250 not available SW-846 dev

Zinc - AA, Direct 0289.1 600/4-79-020 NEMI

Zinc - AA, Direct Aspiration 7950 SW-846 Ch 3.3 www 09/01/1986

Zinc - AA, Furnace 0289.2 600/4-79-020 NEMI

Zinc - AA, Furnace Technique 7951 SW-846 Ch 3.3 www 07/01/1992

Zinc - Sample Preparation 0200.2 600/R-94-111 www 05/01/1994

04/16/2003 see Sources list for full reference and website address Chemical Number Index Page 33 
Sources for EPA Test Methods April 2003 

SOURCES FOR EPA TEST METHODS 

To retrieve method, click on underlined link (you must be connected to the Internet ) 

40 CFR Title 40 Code of Federal Regulations in 24+ volumes, current edition. (GPO or http://www.access.gpo.gov/ecfr/ ) 

EPA 240/B-00-004 Guidance for Developing a Training Program for Quality systems (G-10). December 2000. 

(http://www.epa.gov/quality1/qa_docs.html ) 

EPA 240/B-01-002 EPA Requirements for Quality Management Plans (QA/R-2). March 2001. 

(http://www.epa.gov/quality1/qa_docs.html ) 

EPA 240/B-01-003 EPA Requirements for QA Project Plans (QA/R-5). March 2001. 

(http://www.epa.gov/quality1/qa_docs.html ) 

EPA 240/B-01-004 Preparation of Standard Operating Procedures (G-6). March 2001. 

(http://www.epa.gov/quality1/qa_docs.html ) 

EPA 330/9-80-002 Microbial Bioassay for Toxic and Hazardous Materials (Ames Test for Mutagenicity). September 1980 

(Region 1 Library) 

EPA 402/R-92-003 Protocols for Radon and Radon Decay Product Measurements in Homes. June 1993. (NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleOAR.html ) 

EPA 402/R-92-004 Indoor Radon and Radon Decay Product Measurement Device Protocols. July 1992. (NTIS / PB92-

206176 and NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleOAR.html ) 

EPA 430/9-86-004 Quality Assurance/Quality Control (QA/QC) for 301(h) Monitoring Programs: Guidance on Field and 

Laboratory Methods. March 1987. (NTIS / PB87-221164) 

EPA 440/4-91-002 Volunteer Lake Monitoring. December 1991. 

(http://www.epa.gov/OWOW/monitoring/volunteer/lake/index.html or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleOAR.html ) 

EPA 503/6-90-004 Analytical Methods for U.S. EPA Priority Pollutants and 301(h) Pesticides in Estuarine and Marine 

Sediments. May 1986. (NTIS / PB95-169959) 

EPA 503/8-91-001 Evaluation of Dredged Material Proposed for Ocean Disposal (Testing Manual “Green Book”). EPA & 

ACOE, February 1991. (NTIS / AD-A269382 or http://www.epa.gov/OWOW/oceans/gbook/index.html ) 

EPA 520/1-86-014-1 Interim Protocols for Screening and Followup Radon and Radon Decay Product Measurements. 

February 1987. (NTIS / PB89-224265) 

EPA 520/1-88-002 Sediment Monitoring at Deep-Ocean Low-Level Radioactive Waste Disposal Sites: Methods Manual. 

August 1988. (NTIS / PB89-135875) 

EPA 520/5-84-006 Radiochemistry Procedures Manual. August 1984. (NTIS / PB84-215581; CD ROM) 

EPA 530/D-02-002 RCRA Waste Sampling Draft Technical Guidance: Planning, Implementation, and Assessment. August 

2002. updates technical information in SW-846 Chapter 9 ( http://www.epa.gov/epaoswer/hazwaste/test/samp_guid.htm ) 

EPA 530/R-93-001 RCRA Ground-Water Monitoring: Draft Technical Guidance. November 1992. (NTIS / PB93-139350 or 

http://www.epa.gov/correctiveaction/resource/guidance/sitechar/gwmonitr/rcra_gw.pdf ) 

EPA 530/R-95-036 Guidance for the Sampling and Analysis of Municipal Waste Combustion Ash for the Toxicity 

Characteristic. June 1995. (NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleOSWER.html ) 

EPA 530/SW-168 Use of the Water Balance Method for Predicting Leachate Generation from Solid Waste Disposal Sites. 

October 1975 (NTIS / PB87-194643) 

EPA 530/SW-611 Procedures Manual for Ground Water Monitoring at Solid Waste Disposal Facilities. 1977 (NTIS / 

PB84-174820) 

1 
Sources for EPA Test Methods April 2003 

EPA 530/SW-846 Test Methods for Evaluating Solid Waste: Physical/Chemical Methods 3rd ed - 4 vols. November 1986 

Information on print subscription from GPO or one-time print purchase from NTIS or CD ROM from NTIS plus full text of all 

methods including Updates IIIA, IIIB, IVA and IVB and others online at www.epa.gov/epaoswer/hazwaste/test/sw846.htm 

Plus article discussing SW-846 methods under development listed in Index as “not available” is found at: 

http://www.epa.gov/SW-846/pdfs/eta2000.pdf 

EPA 530/SW-87-006 Batch-Type Adsorption Procedures for Estimating Soil Attenuation of Chemicals. (NTIS / PB87-146155 

or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleOSWER.html ) 

EPA 540/G-90-004 Quality Assurance/Quality Control Guidance for Removal Activities: Sampling QA/QC Plan and Data 

Validation Procedures. Interim Final. April 1990. (NTIS / PB90-274481 or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleOSWER.html ) 

[EPA 540/P-91-005, 006, 007, 008, and 009 Compendium of ERT Procedures. January 1991. (NTIS / and NEPIS / 

http://www.epa.gov/cincl)] Superceded by revised ERT SOPs available under products at http://www.ert.org/ 

EPA 540/R-94-509 A User's Guide to Environmental Immunochemical Analysis. March 1994. (NTIS / PB95-138327 or 

NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleOSWER.html ) 

EPA 540/R-94-519 Field Screening Method for Polychlorinated Biphenyl Compounds in Water. October 1994. (NTIS / PB95-

129078 or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleOSWER.html ) 

EPA 540/R-95-141 Superfund Program Representative Sampling Guidance, Volume 1: Soil. Interim Final, December 1995. 

(NTIS / PB96-963207 or http://www.ert.org ) 

EPA 540/R-97-501 Federal Facilities Forum Issue: Field Sampling and Selecting On-site Analytical Methods for Explosives in 

Soil. November 1996. (NTIS / PB97-186613 or NEPIS http://www.epa.gov/clariton/clhtml/pubtitleOSWER.html ) 

EPA 540/S-95-504 Low-Flow (Minimal Drawdown) Ground-Water Sampling Procedures. April 1996. 

http://www.epa.gov/tio/tsp/download/lwflw2a.pdf ) 

EPA 540-2-88-005 Field Screening Methods Catalog: User's Guide. September 1988. (NTIS / PB89-134159) 

EPA 540/2-90-005a Environmental Asbestos Assessment Manual: Superfund Method for the Determination of Asbestos in 

Ambient Air, Part 1: Method. Interim Version, May 1990. (NTIS / PB90-274283 or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleOSWER.html ) 

EPA 540/4-91-001 Ground-Water Issue: Soil Sampling and Analysis for Volatile Organic Compounds. February 1991 (NTIS / 

DE91-016758) 

EPA 542/B-98-002 Field Sampling and Analysis Technologies Matrix and Reference Guide. March 1998. (NTIS / PB99-

101685) 

EPA 542/S-02-001 Ground-Water Sampling Guidelines for Superfund and RCRA Project Managers. May 2002. 

http://www.epa.gov/tio/tsp/download/gw_sampling_guide.pdf 

EPA 560/5-86-020 Analysis for Polychlorinated Dibenzo-p-Dioxins (PCDD) and Dibenzofurans (PCDF) in Human Adipose 

Tissue: Method Evaluation Study. October 1986 (NTIS / PB87-148706) 

EPA 560/5-87-008 Volatile Organic Compounds in Whole Blood-Determination by Heated Dynamic Headspace Purge and 

Trap Isotope Dilution GC/MS. July 1987 (NTIS / PB88-102918 or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleOSWER.html ) 

EPA 560/5-89-001 Guidelines for Conducting the AHERA TEM Clearance Test to Determine Completion of an Asbestos 

Abatement Project. May 1989. (NTIS / PB90-171778) 

EPA 600/A-92-226 Survey of Protocols for Conducting Indoor Air Quality Investigations in Large Buildings. June 1992. (NTIS 

/ PB93-119865) 

EPA 600/R-92-033 Characterizing Heterogeneous Wastes: Methods and Recommendations. EPA & DOE, February 1992. 

(NTIS / PB92-216894) 

2 
Sources for EPA Test Methods April 2003 

EPA 600/R-92-080 Methods for Aquatic Toxicity Identification Evaluations: Phase II Toxicity Identification Procedures for 

Samples Exhibiting Acute and Chronic Toxicity. September 1993. (NTIS / PB94-114907 or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/R-92-081 Methods for Aquatic Toxicity Identification Evaluations: Phase III Toxicity Confirmation Procedures for 

Samples Exhibiting Acute and Chronic Toxicity. September 1993. (NTIS / PB94-123833 or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/R-92-111 Fish Field and Laboratory Methods for Evaluating the Biological Integrity of Surface Waters. March 1993. 

(NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) [Revision and enlargement of EPA/670-4-73-001] 

EPA 600/R-92-128 Preparation of Soil Sampling Protocols: Sampling Techniques and Strategies. July 1992. (NTIS / PB92-

220532 or www.epa.gov/swerust1/cat/mason.pdf ) 

EPA 600/R-92-129 Methods for the Determination of Organic Compounds in Drinking Water, Supplement II. August 1992. 

(NTIS / PB92-207703 or CD ROM or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ). Supplement to EPA 

600/4-88-039 (NTIS / PB91-231480) 

EPA 600/R-93-100 Methods for the Determination of Inorganic Substances in Environmental Samples. August 1993. (NTIS / 

PB94-120821 or CD ROM or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/R-93-116 Method for the Determination of Asbestos in Bulk Building Materials. July 1993. (NTIS / PB93-218576) 

[Updates and replaces Interim version in 40 CFR 763 Subpart F App A] 

EPA 600/R-93-183 Guidance Manual: Bedded Sediment Bioaccumulation Tests. September 1993. (NTIS / PB94-131505) 

EPA 600/R-94-025 Methods for Assessing the Toxicity of Sediment-associated Contaminants with Estuarine and Marine 

Amphipods. June 1994. (NTIS / PB95-177374 or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html or 

http://www.epa.gov/ost/library/sediment/ ) 

EPA 600/R-94-111 Methods for the Determination of Metals in Environmental Samples, Supplement I. [to EPA/600-4-91-010] 

May 1994. (NTIS / PB95-125472 or CD ROM or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/R-94-134 Determination of Asbestos Structures over 10 [micrometers] in Length in Drinking Water. June 1994. 

(NTIS / PB94-201902 or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/R-95-077 Laboratory Methods for Soil and Foliar Analysis in Long-Term Environmental Monitoring Programs. June 

1995. (NTIS / PB95-231007 or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/R-95-131 Methods for the Determination of Organic Compounds in Drinking Water, Supplement III. 

August 1995. (NTIS / PB95-261616 or CD ROM or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

Supplement to EPA 600/4-88-039 (NTIS / PB91-231486) 

EPA 600/R-95-136 Short-Term Methods for Estimating the Chronic Toxicity of Effluents and Receiving Waters to West Coast 

Marine and Estuarine Organisms. August 1995. (NTIS / PB95-261665 or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/R-95-178 ICR Microbial Laboratory Manual. April 1996. (NTIS / PB95-157557 or EPA Microbiology web page at 

http://www.epa.gov/nerlcwww or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html or CD ROM) 

EPA 600/R-96-054 Marine Toxicity Identification Evaluation (TIE): Phase I Guidance Document. September 1996 (NTIS / 

PB97-149488 or NSCEP or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/R-96-055 Guidance for the Data Quality Objectives Process (G-4). August 2000. 

(http://www.epa.gov/quality1/qa_docs.html ) 

EPA 600/R-96-056 Decision Error Feasibility Trials (DEFT) Software (G-4D). September 1994. 

(http://www.epa.gov/quality1/qa_docs.html ) 

EPA 600/R-96-084 Guidance for the Data Quality Assessment: Practical Methods for Data Analysis (G-9). July 2000. 

(http://www.epa.gov/quality1/qa_docs.html ) 

EPA 600/R-96-085 Data Quality Assessment Statistical Toolbox--DataQUEST (G-9D). December 1997. 

(http://www.epa.gov/quality1/qa_docs.html ) 

3 
Sources for EPA Test Methods April 2003 

EPA 600/R-97-072 Methods for the Determination of Chemical Substances in Marine and Estuarine Environmental Matrices. 

2nd edition. September 1997. (NSCEP or NTIS /PB97-127326 or http://www.epa.gov/nerlcwww/ordmeth.htm or CD ROM) 

EPA 600/R-98-018 Guidance on Quality Assurance Project Plans (G-5). February 1998.. 

(http://www.epa.gov/quality1/qa_docs.html ) 

EPA 600/R-98-128 Technical Protocol for Evaluating Natural Attenuation of Chlorinated Solvents in Ground Water. 

September 1998. (NTIS / PB99-130023 or http://www.epa.gov/superfund/resources/gwdocs/protocol.htm or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/R-99-064 Methods for Measuring the Toxicity and Bioaccumulation of Sediment-associated Contaminants with 

Freshwater Invertebrates. 2d edition. March 2000. (NSCEP or http://www.epa.gov/ost/cs/freshfact.html or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/R-99-080 Guidance on Technical Audits and Related Assessments (G-7). January 2000. 

(http://www.epa.gov/quality1/qa_docs.html ) 

EPA 600/R-00-007 Guidance for the Data Quality Objectives Process for Hazardous Waste Sites (G-4HW). January 2000. 

(http://www.epa.gov/quality1/qa_docs.html ) 

EPA 600/R-00-013 Membrane Filter Method for the Simultaneous Detection of Total Coliforms and Escherichia coli in Drinking 

Water. February 2000. (http://www.epa.gov/nerlcwww/ ) 

EPA 600/R-01-020 Methods for Assessing the Chronic Toxicity of Marine and Estuarine Sediment-associated Contaminants 

with the Amphipod Leptocheirus plumulosus. First Edition, March 2001. (NSCEP or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleORD.html or http://www.epa.gov/waterscience/cs/leptofact.html ) Supplements 

EPA 600/R-94-025 

EPA 600/R-01-067 Short Term Test Method for Assessing the Reproductive Toxicity of Endrocrine-Disrupting Chemicals 

Using the Fathead Minnow (Pimephales Promelas). June 2002. ( NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/2-78-054 Field and Laboratory Methods Applicable to Overburdens and Minesoils. March 1978. (NTIS / 

PB280495) 

EPA 600/2-78-095 Compilation and Evaluation of Leaching Test Methods. May 1978 (NTIS / PB-285072) 

EPA 600/2-80-018 Samplers and Sampling Procedures for Hazardous Waste Streams. January 1980 (NTIS / PB80-135353 

or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/2-80-076 A Method for Determining the Compatibility of Hazardous Wastes. April 1980. (NTIS / PB80-221005) 

EPA 600/2-81-160 Manual of Ground-Water Quality Sampling Procedures. 1981 (NTIS / PB82-103045) 

EPA 600/2-85-028 Guide for Decontaminating Buildings, Structures, and Equipment at Superfund Sites. March 1985 (NTIS / 

PB85-201234). 

EPA 600/2-85-104 Practical Guide for Ground-Water Sampling. September 1985. (NTIS / PB86-137304 / NEPIS 

http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/2-87-027 Soil-Gas Measurement for Detection of Subsurface Organic Contamination. March 1987 (NTIS / 

PB87-174884) 

EPA 600/2-88-062 Toxicity Reduction Evaluation Protocol for Municipal Wastewater Treatment Plants. April 1989. (NTIS / 

PB89-195218 or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/3-85-019 Analytical Procedures and Quality Assurance Plan for the Analysis of 2,3,7,8-TCDD in Tier 3-7 Samples of 

the U.S. EPA National Dioxin Study. May 1986 (NTIS / PB-89-214431) 

EPA 600/3-88-029 Protocols for Short Term Toxicity Screening of Hazardous Waste Sites. (NTIS / PB88-235510/AS) 

EPA 600/3-90-022 Analytical Procedures and Quality Assurance Plan for the Determination of PCDD/PCDF in Fish. March 

1990. (NTIS / PB90-192774) 

4 
Sources for EPA Test Methods April 2003 

EPA 600/3-90-023 Analytical Procedures and Quality Assurance Plan for the Determination of Xenobiotic Chemical 

Contaminants in Fish. (National Dioxin Study-Phase II December 1989) March 1990. (NTIS / PB90-192782) 

EPA 600/3-91-063 Guidelines for Conducting Early Life Stage Toxicity Tests with Japanese Medaka (Oryzias latipes). 

December 1991. (NTIS / PB92-137488 or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/4-75-008 Interim Radiochemical Methodology for Drinking Water. Revised March 1976. (NTIS / PB253258 or CD 

ROM) 

EPA 600/4-79-020 Methods for Chemical Analysis of Water and Wastes. Revised March 1983 (NTIS / PB84-128677 or CD 

ROM or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/4-80-032 Prescribed Procedures for Measurement of Radioactivity in Drinking Water. August 1980 (NTIS / 

PB80-224744 or CD ROM or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/4-80-034 Identification and Detection of Water-Borne Viruses by Immunoenzymatic Methods. June 1980. (NTIS / 

PB80-224249 or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/4-81-044 The Determination of the Maximum Total Trihalomethane Potential: Method 510.1 April 1982 (NERL) 

EPA 600/4-81-045 The Determination of Polychlorinated Biphenyls in Transformer Fluid and Waste Oils September 1982 

(NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/4-81-055 Interim Methods for the Sampling and Analysis of Priority Pollutants in Sediments and Fish Tissue. 

August 1977, revised October 1980 (NERL) 

EPA 600/4-81-056 Total Organic Halide: Method 450.1. Interim (NERL) 

EPA 600/4-82-029 Handbook of Sampling and Sample Preservation of Water and Wastewater. September 1982 (NTIS / 

PB83-124503 or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/4-82-068 Interim Procedures for Conducting the Salmonella /Microsomal Mutagenicity Assay (Ames Test). March 

1983. (NTIS / PB88-205380) 

EPA 600/4-83-000 Methods for Use of Caged Molluscs for In Situ Biomonitoring of Marine Sewage Discharges (Draft). May 

1983 

EPA 600/4-83-027 Technical Assistance Document for Sampling and Analysis of Toxic Organic Compounds in Ambient Air. 

June 1983 (NTIS / PB83-2329020) 

EPA 600/4-83-043 Analytical Method for Determination of Asbestos Fibers in Water. September 1983 (NTIS / PB83-260471 

or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA-600/4-84-001 Development of Analytical Test Procedures for the Measurement of Organic Priority Pollutants in Sludge. 

January 1984. (NTIS / PB84-129048) 

EPA 600/4-84-013 US EPA Manual of Methods for Virology. February 1984 - June 1988 (NSCEP; NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleORD.html and http://www.epa.gov/nerlcwww/about.htm ) 

EPA 600/4-85-076 Test Methods for Escherichia coli and Enterococci in Water by the Membrane Filter Procedure. July 1985 

(NTIS / PB86-158052; NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/4-86-024 Development of Standard Methods for the Collection and Analysis of Precipitation. May 1986 (NTIS / 

PB86-201365) 

EPA 600/4-88-039 Methods for the Determination of Organic Compounds in Drinking Water. December 1988 (Revised July 

1991) (NTIS / PB91-231480 or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.htm or CD ROM) See EPA 600/R-92-

129 

EPA 600/4-89-017 Compendium of Methods for the Determination of Toxic Organic Compounds in Ambient Air. 

(Consolidation and republishing of Methods TO01-TO05 from EPA 600/4-84-041; TO06-TO09 from EPA 600/4-87-006; and 

TO10-TO14 from EPA 600/4-89-018, Second Supplement June 1988) June 1988 (NTIS / PB90-116989) see also EPA 

625/R-96-010b for Second Edition; all current TO methods are available from AMTIC http://www.epa.gov/ttn/amtic 

5 
Sources for EPA Test Methods April 2003 

EPA 600/4-90-10 Compendium of Methods for the Determination of Air Pollutants in Indoor Air. April 1990. (NTIS / PB90-

200288) 

EPA 600/4-90-020 Methods for the Determination of Organic Compounds in Drinking Water, Supplement I. July 1990. (NTIS 

/ PB91-146027 or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html or CD ROM) (supplement to EPA 

600/4-88-039) See also Supplement II, EPA 600/R-92-129 for later versions. 

[EPA 600/4-90-027F Methods for Measuring the Acute Toxicity of Effluents and Receiving Waters to Freshwater and Marine 

Organisms. Fourth Edition, August 1993. (NTIS / PB94-114733 or CD ROM or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) superceded by EPA 821/R-02-012] 

EPA 600/4-90-030 Macroinvertebrate Field and Laboratory Methods for Evaluating the Biological Integrity of Surface Waters. 

November 1990. (NTIS / PB91-171363 or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

[EPA 600/4-91-002 Short-Term Methods for Estimating the Chronic Toxicity of Effluents and Receiving Water to Organisms. 

Third Edition, July 1994. (NSCEP or CD ROM or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) superceded 

by EPA 821/R-02-013] 

[EPA 600/4-91-003 Short-Term Methods for Estimating the Chronic Toxicity of Effluents and Receiving Water to Marine and 

Estuarine Organisms. Second Edition, July 1994. (NSCEP or CD ROM or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleORD.html superceded by EPA 821/R-02-014 ] 

EPA 600/4-91-010 Methods for the Determination of Metals in Environmental Samples. June 1991. (NTIS / PB91-231498) 

supplemented by EPA 600/R-94-111 or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/4-91-016 Test Methods for Escherichia coli in Drinking Water. July 1991. (NTIS / PB91-234591 or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/6-91-003 Methods for Aquatic Toxicity Identification Evaluations: Phase I Toxicity Characterization Procedures. 

Second Edition, February 1991. (PB92-100072 or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/6-91-005F Toxicity Identification Evaluation: Characterization of Chronically Toxic Effluents, Phase I. May 1992. 

(NSCEP or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/8-78-017 Microbiological Methods for Monitoring the Environment: Water and Wastes. December 1978 (NTIS / 

PB290329 or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 600/8-80-038 Manual of Analytical Methods for the Analysis of Pesticides in Humans and Environmental Samples. June 

1980. (NTIS / PB82-208752) 

EPA 600/8-81-011 User’s Guide for Conducting Life-Cycle Chronic Toxicity Tests with Fathead Minnows (Pimephales 

Promelas). May 1982. (NTIS / PB82-238395) 

EPA 600/8-87-036 Soil Gas Sensing for Detection and Mapping of Volatile Organics. August 1987 (NTIS / 

PB87-228516/AS) 

EPA 600/8-87-043 Methods for the Toxicity Tests of Single Substances and Liquid Complex Wastes with Marine Unicellular 

Algae. March 1988 (NTIS / PB88-208681) 

EPA 600/8-89-046 Soil Sampling Quality Assurance User’s Guide. Second edition, March 1989. (NTIS / PB89-189864 or 

http://clu-in.org/download/char/soilsamp.pdf ) 

EPA 600/8-90-041 Indoor Air -- Assessment: Methods of Analysis for Environmental Carcinogens. June 1990. (NTIS / 

PB91-137273 or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 620/R-94-004F Field Operations and Methods for Measuring the Ecological Condition of Wadeable Streams. September 

1998. (EMAP / www.epa.gov/emap or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 620/R-95-008 Environmental Monitoring and Assessment Program (EMAP) Laboratory Methods Manual Estuaries, 

Volume 1: Biological and Physical Analyses. August 1995. (NTIS / PB96-151196 or EMAP / 

http://www.epa.gov/emap/html/pubs/docs/groupdocs/estuary/field/labman.html ) 

EPA 620/R-97-001 EMAP Surface Waters Field Operations Manual for Lakes. June 1997. (EMAP / www.epa.gov/emap or 

NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

6 
Sources for EPA Test Methods April 2003 

EPA 620/R-00-007 Environmental Monitoring and Assessment Program–Surface Waters: Field Operations and Methods for 

Measuring the Ecological Condition of Non-wadeable Rivers and Streams. September 2000. (NSCEP) 

EPA 625/R-92-013 Control of Pathogens and Vector Attraction in Sewage Sludge. December 1992. (NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 625/R-93-003a Subsurface Characterization and Monitoring Techniques: A Desk Reference Guide. Volume I: Solids 

and Ground Water, Appendices A and B. May 1993. (NTIS / PB94-136272 or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 625/R-93-003b Subsurface Characterization and Monitoring Techniques: A Desk Reference Guide. Volume II: The 

Vadose Zone, Field Screening and Analytical Methods, Appendices C and D. May 1993. (NTIS / PB94-131497 or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 625/R-96-010a Compendium of Methods for the Determination of Inorganic Compounds in Ambient Air. June 1999. 

(NSCEP or AMTIC at http://www.epa.gov/ttn/amtic/inorg.html or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html 

EPA 625/R-96-010b Compendium of Methods for the Determination of Toxic Organic Compounds in Ambient Air, Second 

Edition. January 1999. Compendium Methods TO-4A, 9A,10A, 11A, 13A, 14A, 15,16,17. (NSCEP or AMTIC or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 625/8-89-015 Biomonitoring for Control of Toxicity in Effluent Discharges to the Marine Environment. September 1989. 

(NTIS / PB94-210226) 

EPA 625/12-91-002 Description and Sampling of Contaminated Soils: A Field Pocket Guide. November 1991. (NSCEP) 

EPA 747/R-95-001 Residential Sampling for Lead: Protocols for Dust and Soil Sampling, Final Report. March 1995. (LEAD) 

EPA 747/R-95-002a A Field Test of Lead-Based Paint Testing Technologies: Summary Report. May 1995. (NTIS / PB97-

115760 or http://www.epa.gov/opptintr/lead/summary.txt ) 

EPA 747/R-95-007 Sampling House Dust for Lead: Basic Concepts and Literature Review. September 1995. (NTIS / PB96-

147947) 

EPA 812/B-94-003 Sampling for Lead in Drinking Water in Nursery Schools and Day Care Facilities. April 1994. (NTIS / 

PB94-218963) 

EPA 814/B-92-001 Pocket Sampling Guide for Operators of Small Water Systems. April 1992. 

(GPO / SN 055-000-00423-4) 

EPA 814/B-94-001 Pocket Sampling Guide for Operators of Small Water Systems: Phases II and V. July 1994. (NSCEP or 

NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleOW.html ) 

EPA 814/B-95-001 Information Collection Requirements Rule--Protozoa and Enteric Virus Sample Collection Procedures. 

June 1995. (NSCEP or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleOW.html ) 

EPA 814/B-95-002 Protocol for the Information Collection Requirements Rule. June 1995. (NSCEP or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleOW.html or CD ROM) 

EPA 814/B-95-003 ICR Protozoan Method for Detecting Giardia Cysts and Cryptosporidium Oocysts in Water by a 

Fluorescent Antibody Procedure. June 1995. (NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleOW.html ) 

EPA 814/B-96-001 ICR Sampling Manual. April 1996. (NTIS / PB96-157508 or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleOW.html ) 

EPA 814/B-96-002 DBP/ICR Analytical Methods Manual. April 1996. (NTIS / PB96-157516 or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleOW.html ) 

EPA 815/B-01-001 Method 317.0 Determination of Inorganic Oxyhalide Disinfection By-Products in Drinking Water Using Ion 

chromatography with the Addition of a Postcolumn Reagent for Trace Bromate Analysis. Revision 2.0, July 2002. 

(http://www.epa.gov/safewater/methods/met317rev2.pdf ) 

7 
Sources for EPA Test Methods April 2003 

EPA 815/B-01-002 Method 531.2 Measurement of N-Methylcarbamoyloximes and N-Methylcarbamates in Water by Direct 

Aqueous Injection HPLC with Postcolumn Derivatization. Rev 1.0, September 2001. 

http://www.epa.gov/safewater/methods/met531_2.pdf ) 

EPA 815/R-00-014 Methods for the Determination of Organic and Inorganic Compounds in Drinking Water, Volume 1. August 

2000. (NTIS / PB2000-106981 or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleOW.html ) 

EPA 816/R-01-017A A Small Systems Guide to the Total Coliform Rule: Monitoring Drinking Water to Protect Public Health. 

June 2001. ( http://www.epa.gov/safewater/smallsys/small-tcr.pdf ) 

EPA 821/B-94-001 Analytical Methods for the Determination of Pollutants in Pharmaceutical Manufacturing Industry 

Wastewater. February 1995. (NTIS / PB95-201679 or CD ROM) 

EPA 821/B-94-004b Method 1664: N-Hexane Extractable Material (HEM) and Silica Gel Treated N-Hexane Extractable 

Material (SGT-HEM) by Extraction and Gravimetry (Oil and Grease and Total Petroleum Hydrocarbons). revised April 1995. 

(NTIS / PB95-239232 or http://www.epa.gov/waterscience/methods/1664.html or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleOW.html or CD ROM) 

EPA 821/B-94-005 Method 1613: Tetra-Through Octa-Chlorinated Dioxins and Furans by Isotope Dilution HRGC/HRMS. 

Revision B, October 1994. (NTIS / PB95-104774 or http://www.epa.gov/ost/methods/ or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleOW.html or CD ROM) 

EPA 821/B-95-001 Guidance on Establishing Trace Metal Clean Rooms in Existing Facilities. Draft April 1995. (NTIS / 

PB95-262176 or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleOW.html or CD ROM) 

EPA 821/B-95-002 Guidance on the Documentation and Evaluation of Trace Metals Data Collected for Clean Water Act 

Compliance Monitoring. April 1995. (NTIS / PB95-262747 or Jan 1996 edition PB96-193279 or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleOW.html or CD ROM) 

EPA 821/B-96-005 Methods for Organic Chemical Analysis of Municipal and Industrial Wastewater. December 1996. (NTIS / 

PB97-125298 or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleOW.html ) 

EPA 821/B-98-016 Analytical Methods for the Determination of Pollutants in Pharmaceutical Manufacturing Industry 

Wastewater. July 1998. (NSCEP or CD ROM) 

EPA-821-B-01-002 Proposed Changes to Whole Effluent Toxicity Method Manuals. September 2001. 

http://www.epa.gov/OST/WET/ 

EPA 821/C-99-004 EPA Methods and Guidance for the Analysis of Water, Version 2.0. June 1999. CD ROM (NTIS/ PB99-

500209INQ details at http://www.ntis.gov/product/epa-water-methods.htm ) 

EPA 821/C-00-002 Selected OW Methods and Guidance. September 2000. (OST) 

EPA 821/D-96-006 Guide to Method Flexibility and Approval of EPA Water Methods. December 1996. (NTIS / PB97-117766 

or CD ROM) 

EPA 821/R-91-100 Draft Analytical Method for the Determination of Acid Volatile Sulfide in Sediment. December 1991. (NTIS 

/ PB93-155901 or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleOW.html ) 

EPA 821/R-92-008 Methods for the Determination of Diesel, Mineral, and Crude Oils in Offshore Oil and Gas Industry 

Discharges. December 1992. (NTIS / PB93-166932 or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleOW.html or CD 

ROM) 

EPA 821/R-93-010-A Methods for the Determination of Nonconventional Pesticides in Municipal and Industrial Wastewater, 

Volume I. Revision 1, August 1993. (NTIS / PB94-121654 or CD ROM) Supersedes EPA/821-R-92-002. 

EPA 821/R-93-010-B Methods for the Determination of Nonconventional Pesticides in Municipal and Industrial Wastewater, 

Volume II. Revision 1, August 1993. (NTIS / PB94-166311 or CD ROM) 

EPA 821/R-93-017 Analytical Methods for the Determination of Pollutants in Pulp and Paper Industry Wastewater. October 

1993. (NTIS / PB94-107059 or NEPIS http://www.epa.gov/clariton/clhtml/pubtitleOW.html ) 

EPA 821/R-95-035 Comparison of VOA Compositing Procedures. September 1995. (NTIS / PB96-112883 or CD ROM or 

NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleOW.html ) 

8 
Sources for EPA Test Methods April 2003 

EPA 821/R-96-003 Method 1636: Determination of Hexavalent Chromium by Ion Chromatography. January 1996 (NTIS / 

PB96-193461 or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleOW.html or CD ROM) 

EPA 821/R-96-004 Method 1637: Determination of Trace Elements in Ambient Waters by Chelation Preconcentration with 

Graphite Furnace Atomic Absorption. January 1996. (NTIS / PB96-193479 or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleOW.html or CD ROM) 

EPA 821/R-96-005 Method 1638: Determination of Trace Elements in Ambient Waters by Inductively Coupled Plasma-Mass 

Spectrometry. January 1996. (NTIS / PB96-193487 or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleOW.html or CD 

ROM) 

EPA 821/R-96-006 Method 1639: Determination of Trace Elements in Ambient Waters by Stabilized Temperature Graphite 

Furnace Atomic Absorption. January 1996. (NTIS / PB96-193255 or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleOW.html or CD ROM) 

EPA 821/R-96-007 Method 1640: Determination of Trace Elements in Ambient Waters by On-Line Chelation 

Preconcentration and Inductively Coupled Plasma-Mass Spectrometry. January 1996. (NTIS / PB96-193230 or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleOW.html or CD ROM) 

EPA 821/R-96-008 Method 1669: Sampling Ambient Water for Trace Metals at EPA Water Quality Criteria Levels. January 

1996. (NTIS / PB96-193313 or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleOW.html or CD ROM) 

EPA 821/R-96-012 Method 1631: Mercury in Water by Oxidation, Purge and Trap, and Cold Vapor Atomic Fluorescence 

Spectrometry. Draft July 1996 (NTIS / ? or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleOW.html or CD ROM) 

EPA 821/R-96-013 Method 1632: Inorganic Arsenic in Water by Hydride Generation Quartz Furnace Atomic Absorption. July 

1996. (NTIS / PB97-151674 or CD ROM) 

EPA 821/R-97-001 Method 1668: Toxic Polychlorinated Biphenyls by Isotope Dilution High Resolution Gas 

Chromatography/High Resolution. Mass Spectrometry. March 1997, draft. (NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleOW.html ) 

EPA 821/R-97-004 Improved Enumeration Methods for the Recreational Water Quality Indicators: Enterocci and Escherichia 

coli. March 2000. (NSCEP or http://www.epa.gov/nerlcwww/RecManv.pdf or http://www.epa.gov/nerlcwww/online.htm ) 

EPA 821/R-97-004a Method 1600: Membrane Filter Test Method for Enterococci in Water. May 1997. (NSCEP or 

http://www.epa.gov/nerlcwww/1600.pdf or http://www.epa.gov/nerlcwww/online.htm ) 

EPA 821/R-98-002 Method 1664, Revision A: N-Hexane Extractable Material (HEM; Oil and Grease) and Silica Gel Treated 

N-Hexane Extractable Material (SGT-HEM; Non-polar Material by Extraction and Gravimetry. February 1999. (NTIS / PB99-

121949 or http://www.epa.gov/waterscience/methods/16640514.pdf or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleOW.html ) 

EPA 821/R-98-003 Method 1680: Fecal Coliform in Biosolids by Multiple-Tube Fermentation and Membrane Filter Procedures. 

July 1998 draft (CD ROM) 

EPA 821/R-98-004 Method 1682: Salmonella sp. In Biosolids by Enrichment, Selection and Biochemical Characterization. 

August 1998. (CD ROM) 

EPA 821/R-99-005 Method 1631, Revision B: Mercury in Water by Oxidation, Purge and Trap, and Cold Vapor Atomic 

Fluorescence Spectrometry. May 1999. (NTIS / PB99-131989 or NSCEP or www.epa.gov/ost/Methods/1631.html ) 

EPA 821/R-99-013 Method OIA-1677: Available Cyanide by Flow Injection and Ligand Exchange and Amperometry. January 

2000. (NTIS /PB99-132011 or http://www.epa.gov/ost/methods/ ) 

EPA 821/R-00-017 on SEL CD 

EPA 821/R-00-018 on SEL CD 

EPA 821/R-00-02 Method 1668, Revision A: Chlorinated Biphenyl Cogeners in Water, Soil, Sediment, and Tissue by 

HRGC/HRMS. December 1999. http://www.epa.gov/Region8/water/wastewater/biohome/biosolidsdown/methods/1668a5.pdf 

EPA 821/R-01-004 on CD ROM 

EPA 821/R-01-005 on CD ROM 

9 
Sources for EPA Test Methods April 2003 

EPA 821/R-01-006 on SEL CD ROM 

EPA 821/R-01-007 on CD ROM 

EPA 821/R-01-008 on CD ROM 

EPA 821/R-01-009 on CD ROM 

EPA 821/R-01-012 on CD ROM 

EPA 821/R-01-014 on CD ROM 

EPA 821/R-01-015 on CD ROM 

EPA 821/R-01-016 on CD ROM 

EPA 821/R-01-025 Method 1623: Cryptosporidium and Giardia in Water by Filtration/IMS/FA. April 2001. (NSCEP or 

http://www.epa.gov/nerlcwww ) 

EPA 821/R-01-026 Method 1622: Cryptosporidium in Water by Filtration/IMS/FA. April 2001. (http://www.epa.gov/nerlcwww/) 

EPA 821/R-01-029 Method 1602: Male-specific (F+

) and Somatic Coliphage in Water by Single Agar Layer (SAL) Procedure. 

April 2001. (http://www.epa.gov/nerlcwww/ ) 

EPA 821/R-01-030 Method 1601: Male-specific (F+

) and Somatic Coliphage in Water by Two-step Enrichment Procedure. 

April 200l. (http://www.epa.gov/nerlcwww/ ) 

EPA 821-R-01-034 Method 1605: Aeromonas in Finished Water by Membrane Filtration Using Ampicillin-Dextrin Agar with 

Vancomycin (ADA-V). October 2001. ( http://www.epa.gov/nerlcwww/online.htm ) 

EPA 821/R-02-012 Methods for Measuring the Acute Toxicity of Effluents and Receiving Waters to Freshwater and Marine 

Organisms, 5th ed. October 2002. (http://www.epa.gov/waterscience/WET/disk2/ ) 

EPA 821/R-02-013 Short-term Methods for Estimating the Chronic Toxicity of Effluents and Receiving Waters to Freshwater 

Organisms, 4th ed. October 2002. ( http://www.epa.gov/waterscience/WET/disk3/ ) 

EPA 821/R-01-014 Short-term Methods for Estimating the Chronic Toxicity of Effluents and Receiving Waters to Marine and 

Estuarine Organisims, 3rd ed. October 2002. ( http://www.epa.gov/waterscience/WET/disk1/ or 

http://www.epa.gov/OST/WET/disk1/ctm.pdf 

EPA 821/R-02-019 Method 1631, Revision E: Mercury in Water by Oxidation, Purge and Trap, and Cold Vapor Atomic 

Fluorescence Sepctometry. August 2002. ( http://www.epa.gov/ost/methods/ ) 

EPA 822/B-00-024 Estuarine and Coastal Marine Waters: Bioassessment and Biocriteria Technical Guidance. December 

2000. (NSCEP or http://www.epa.gov/ost/biocriteria/States/estuaries/estuaries1.html ) 

EPA 823/B-98-004 Evaluation of Dredged Material Proposed for Discharge in Waters of the U.S. - Testing Manual: Inland 

Testing Manual. February 1998. (NTIS / AD A338 883/2 or http://www.epa.gov/ost/itm/ITM/ ) 

EPA 823/B-00-007 Guidance for Assessing Chemical Contaminant Data for Use in Fish Advisories: Volume 1, Fish Sampling 

and Analysis. Third edition, November 2000. (http://www.epa.gov/ost/fishadvice/volume1/index.html or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleOW.html ) 

EPA 823/B-01-002 Methods for Collection, Storage and Manipulation of Sediments for Chemical and Toxicological Analyses: 

Technical Manual. October 2001. (NSCEP or www.epa.gov/waterscience/cs ) 

EPA 823/R-92-006 Sediment Classification Methods Compendium. September 1992. (NTIS / PB93-115186 or 

http://www.epa.gov/ost/library/sediment/ or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleORD.html ) 

EPA 823 R-02-004 Field Sampling Plan for the National Study of Chemical Residues in Lake Fish Tissue 

( http://www.epa.gov/waterscience/fishstudy/fieldplan.pdf ) 

EPA 833/B-92-001 NPDES Storm Water Sampling Guidance Document. July 1992. (NTIS / PB92-227669) 

EPA 833/B-99-002 Toxicity Reduction Evaluation Guidance for Municipal Wastewater Treatment Plants. August 1999, 2nd 

edition. (NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleOW.html ) 

EPA 841/B-97-003 Volunteer Stream Monitoring: A Methods Manual. November 1997. (NSCEP or 

http://www.epa.gov/owow/monitoring/volunteer/stream/ or NEPIS / http://www.epa.gov/clariton/clhtml/pubtitleOW.html ) 

10 
Sources for EPA Test Methods April 2003 

EPA 841/B-99-002 Rapid Bioassessment Protocols for Use in Wadeable Streams and Rivers: Periphyton, Benthic 

Macroinvertebrates, and Fish. 2nd edition, July 1999. (http://www.epa.gov/owow/monitoring/rbp/ or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleOW.html ) 

EPA 842/B-93-004 Volunteer Estuary Monitoring: A Methods Manual. December 1993. (NSCEP or 

http://www.epa.gov/owow/estuaries/monitor/index.html#toc or NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleOW.html ) 

EPA 910/9-92-029 Consensus Method for Determining Groundwaters Under the Direct Influence of Surface Water using 

Microscopic Particulate Analysis (MPA). October 1992. (NTIS / PB93-180818) 

01A0003682 Determination of 2,3,7,8-TCDD in Soil and Sediment. May 1983, Rev 1. EPA Region VII Laboratory. (Region 1 

Library) 

01A0004860 Determination of Lead-210, Thorium, Plutonium and Polonium-210 in Drinking Water: Methods 909, 910, 911, 

912. March 1982. (Region 1 Library) 

01A0005044 Procedures for Handling and Chemical Analysis of Sediment and Water Samples. May 1981 (NTIS / 

AD-A103788) 

01A0005114 Measurement of Trihalomethanes (THMs) in Drinking Water with GC/MS and Selected Ion Monitoring: Method 

501.3. March 1982 (Region 1 Library) 

01A0005249 NEIC Pesticide Sampling Guide. August 1985. (Region 1 Library) 

01A0005295 Determination of Pesticides and PCBs in Water and Oil/Sediment by Gas Chromatography/Mass Spectrometry: 

Method 680. November 1985 (CD ROM) 

01A0005392 Rapid Extraction of Organochloride Pesticides from Drinking Water and Raw Source Water - J.T. Baker 

Chemical Test Method No. SPE-500. 1988 (Region 1 Library) 

01A0005658 Determination of Pesticides in Ground Water by High Performance Liquid Chromatography with an Ultraviolet 

Detector. [NPS Survey, Method 4] Draft June 1987 (Region 1 Library) 

01A0005957 The Use of a Portable PID Gas Chromatograph for Rapid Screening of Samples for Purgeable Organic 

Compounds in the Field and in the Lab. EPA Region 1, June 29, 1983. (Region 1 Library) 

01A0006083 Sampling Procedures and Protocols for the National Sewage Sludge Survey. August 1989. (Region 1 Library) 

01A0006085 Method 1620: Metals by Inductively Coupled Plasma Atomic Emission Spectroscopy and Atomic Absorption 

Spectroscopy. Draft September 1989. (NTIS / PB94-114840 or CD ROM) 

01A0006086 Method 1618: Organo-halide Pesticides, Organo-phosphorus Pesticides, and Phenoxy-acid Herbicides by Wide 

Bore Capillary Column Gas Chromatography with Selective Detectors. July 1989. (Region 1 Library) 

01A0006089 Method 1624: Volatile Organic Compounds by Isotope Dilution GCMA; and Method 1625: Semivolatile Organic 

Compounds by Isotope Dilution GCMS. Revision C, June 1989. (NTIS / PB92-231976 or CD ROM or 

http://www.epa.gov/OST/methods/ ) 

01A0006125 Region 1 Laboratory Data Validation Functional Guidelines for Evaluating Environmental Analyses. Part I, July 

1996, revised December 1996. Part II, Volatile/Semivolatile Data Validation Functional Guidelines. December 1996. (Region 

1 Library - http://www.epa.gov/ne/oeme/index.html ) 

01A0006218 Guidance for Performing Tests on Dredged Material to be Disposed of in Open Waters. Prepared by EPA 

Region 1 and ACOE, New England Division and NMFS of FWS. May 15, 1989. (Region 1 Library) 

01A0006252 Determination of Radon in Drinking Water by Liquid Scintillation Counting: Method 913.0. Draft, May 1991. 

(Region 1 Library) 

01A0006379 A Method for Measuring Sediment Oxygen Demand Using a Bench Model Benthic Respirometer. Peter M. 

Nolan and Arthur F. Johnson, EPA Region 1, May 1979. (Region 1 Library / http://www.epa.gov/ne/oarm/test.html ) 

01A0006408 Draft Methodology for the Measurement of Airborne Asbestos by Electron Microscopy. July 1984. (Region 1 

Library) 

11 
Sources for EPA Test Methods April 2003 

01A0006706 Determination of Chlorinated Dibenzo-p-dioxins and Dibenzofurans in Soils and Sediments by Gas 

Chromatography/Mass Spectrometry. December 15, 1986. (Region 1 Library) 

01A0006709 Method 282.3 The Determination of Tributyltin Chloride in Marine and Fresh Waters by Liquid-Solid Extraction 

(LSE) and Gas Chromatography with Electron-Capture Detection (GC/ECD). Version 1.0, October 1989. (Region 1 Library / 

http://www.epa.gov/ne/oarm/test.html ) 

01A0007115 The Protocol for Screening Soil and Sediment Samples for Asbestos Content used by the US Environmental 

Protection Agency, Region 1 Laboratory. December 1997. (Region 1 Library / http://www.epa.gov/ne/oarm/test.html ) 

01A0007292 ColiSure Medium: Presence/Absence Test Method for Detection and Identification of Coliform Bacteria and E. 

coli in Drinking Water. Millipore. (Region 1 Library) 

01A0007431 Region 1 Low Stress (low flow) Purging and Sampling Procedure for the Collection of Ground Water Samples 

from Monitoring Wells. SOW # GT 0001, Revision 2, July 30, 1996. (Region 1 Library or 

http://www.epa.gov/ne/measure/well/wellmon.html ) 

01A0007540 Region 1, EPA-New England Standard Operating Procedure for Elemental Analysis Using the X-Met 920 Field 

X-Ray Fluorescence Analyzer. SOP # X-MET 920, October 1996. (Region 1 Library or 

http://www.epa.gov/ne/measure/xray/xrayfluor.html ) 

01A0007541 Region 1, EPA-New England Immunoassay Guidelines for Planning Environmental Projects. October 1996. 

(Region 1 Library or http://www.epa.gov/ne/measure/ia/iaguide.html ) 

01A0007832 Region I, EPA-New England Compendium of Quality Assurance Project Plan Guidance, Final, October 1999 

(includes September 1998 QAPP Manual). (Region 1 Library or http://www.epa.gov/ne/measure/qappcompendium.pdf ) 

01A0007846 Method 1630: Methyl Mercury in Water by Distillation, Aqueous Ethylation, Purge and Trap, and CVAFS. Draft, 

August 1998. (Region 1 Library) 

01A0007861 Method 6020 CLP-M: Inductively Coupled Plasma-Mass Spectrometry. May 1990. (Region 1 Library) 

01A0007878 Method 556 Determination of Carbonyl Compounds in Drinking Water by Pentaflourobenzylhydroxylamine 

Derivation and Capillary Gas Chromatography with Electron Capture Detention. Revision 1.0, June 1998. 

http://www.epa.gov/safewater/methods/met556.pdf ) 

01A0007909 Method 1001: Lead in Drinking Water by Differential Pulse Anodic Stripping Voltametry. August 1999. 

PALINTEST LTD. (21 Kenton Lands Road, PO BOX 18395, Erlanger, KY 41018 (606) 341-7423) 

01A0007986 Field and Laboratory Methods for Macroinvertebrate and Habitat assessment of Low Gradient, Nontidal 

Streams. July 1997. ( http://www.epa.gov/maia/pdf/MACS-FieldandLabMethods.pdf ) 

01A0008028 Method 515.4 - Determination of Chlorinated Acids in Drinking Water by Liquid-Liquid Microextraction 

Derivatization, and Fast Gas Chromatography with Electron Capture Detection. 2000. (NERL-Cincinnatti) 

01A0008123 EPA Region 1 Standard Operating Procedure for Head Space Screening for Volatile Organic Compounds in 

Aqueous, Soil and Drum Samples. March 1998. (Region 1 Library) 

01A0008143 Draft Calibration of Field Instruments (temperature, pH, dissolved oxygen, conductivity/specific conductance, 

oxidation/reduction potential [ORP], and turbidity). EPA Region 1 SOP, June 3, 1998. (Region 1 Library - .wpd file) 

01A0008190 EPA Method 501.1 (1979), 501.2 (1979) and 525 Rev 2.1 (1988). (Region 1 Library; 501.2 also at NEPIS / 

http://www.epa.gov/clariton/clhtml/pubtitleOther.html ) 

01A0008217 Technical Guidance for the Natural Attenuation Indicators: Methane, Ethane, and Ethene. EPA Region 1, 

Revision 1, February 21, 2002. ( http://www.epa.gov/ne/measure/Natatten.pdf ) 

01A0008260 Regional Implementation Manual for the Evaluation of Dredged Material Proposed for Disposal in New England 

Waters. USACE, NE District & US EPA NE, 2002. ( www.nae.usace.army.mil ) 

01A0008284 RSK SOP 175: Analysis of Dissolved Methane, Ethane, and Ethylene in Ground Water by a Standard Gas 

Chromatographic Technique. Ada, 1997. (Region 1 Library) 

No report number 

12 
Sources for EPA Test Methods April 2003 

CLP Methods http://www.epa.gov/oerrpage/superfund/programs/clp/methods.htm 

Environmental Chemistry Methods (ECM) http://www.epa.gov/oppbead1/methods/ecmindex.htm 

Lake Michigan Mass Balance Study (LMMB) Methods Compendium. June 1997. ( www.epa.gov/glnpo/lmmb/methods/ or 

CD ROM) 

List of Designated Reference and Equivalent Methods. NERL updated periodically. (www.epa.gov/ttn/amtic/criteria.html ) 

Microbiology Laboratory Antimicrobial Testing Methods & Procedures. www.epa.gov/oppbead1/methods/atmpa2z.htm 

Quality System Documents including EPA QA/G series and EPA QA/R series can be found at 

http:/www.epa.gov/quality1/qa_docs.html 

Pesticides: Analytical Methods & Procedures: 

Antimicrobial Testing Methods & Procedures (ATMP) http://www.epa.gov/oppbead1/methods/atmpindex.htm 

Environmental Chemistry Methods (ECM) http://www.epa.gov/oppbead1/methods/ecmindex.htm 

Residue Analytical Methods (RAM) http://www.epa.gov/oppbead1/methods/ramindex.htm 

Region 1 fresh & marine toxicity 

http://www.epa.gov/ne/npdes/epa_attach.html 

http://www.epa.gov/ne/npdes/permits/generic/freshwateracutetoxtest.pdf 

http://www.epa.gov/ne/npdes/permits/generic/freshwatercronictoxtest.pdf 

http://www.epa.gov/ne/npdes/permits/generic/marinewateracutetoxtest.pdf 

http://www.epa.gov/ne/npdes/permits/generic/marinewaterchronictoxtest.pdf 

US EPA Contract Laboratory Program Statement of Work for Organics Analysis, Multi-Media, Multi-Concentration, OLM04.2. 

(http://www.epa.gov/superfund/programs/clp/methods.htm ) 

US EPA Contract Laboratory Program Statement of Work for Inorganics Analysis, Multi-Media, Multi-Concentration, ILM04.0. 

(http://www.epa.gov/superfund/programs/clp/methods.htm ) 

US EPA Contract Laboratory Program Statement of Work for Organics Analysis, Low Concentration Water, OLC02.1. 

(http://www.epa.gov/superfund/programs/clp/methods.htm ) 

US EPA Contract Laboratory Program Statement of Work for Multi-Media, Multi-Concentration Dioxins and Furans Analysis 

DLM01.4 (http://www.epa.gov/superfund/programs/clp/methods.htm ) 

13 
Sources for EPA Test Methods April 2003 

KEY TO OBTAINING SOURCE DOCUMENTS 

AMTIC Ambient Monitoring Technology Information Center 

http://www.epa.gov/ttn/amtic select file transfers; ambient monitoring; air toxics and pick from list 

CD or CD ROM EPA 821/C-99-004 EPA Methods and Guidance for the Analysis of Water, Version 2.0. June 1999. NTIS/ 

http://www.ntis.gov/product/epa-water-methods.htm 

CLP http://www.epa.gov/superfund/programs/clp/methods.htm 

Drinking Water Methods call Drinking Water Hotline (800)426-4791; some methods online 

http://www.epa.gov/nerlcwww/ordmeth.htm 

EMC Emission Measurement Center 

http://www.epa.gov/ttn/emc select Methods and choose promulgated, proposed or other 

EMAP Environmental Monitoring and Assessment Program http://www.epa.gov/emap 

ERT Environmental Response Team, Edison, NJ (732) 321-6740 http://www.ert.org/ 

GPO Government Printing Office, Superintendent of Documents (to purchase publications), US GPO, Washington, DC 20402. 

phone 202/ 512-1800; fax 202/512-2250; telex 710/822-9413; internet http://www.gpo.gov/ 

LEAD National Lead Information Center Clearinghouse. Send email request to: ehc@nsc.org or phone: 800-424-LEAD or 

complete document request online from http://www.epa.gov/opptintr/lead/nlic.htm 

MICE Methods Information Communications Exchange For technical questions or comments on SW-846. Basic information 

available 24 hours via recorded message (703) 676-4690; fax: (703)318-4682 or e-mail: mice@cpmx.saic.com 

http://www.epa.gov/epaoswer/hazwaste/test/mice.htm 

NEMI National Environmental Methods Index Brief method summary, analytes, relative cost, and download at 

http://www.nemi.gov 

NERL US EPA National Exposure Research Laboratory (NERL), Microbiological and Chemical Exposure Assessment 

Research Division (MCEARD), 26 West Martin Luther King Dr, Cincinnati, OH 45268-0001. Fax requests for 500 & 600 

methods series to: 513/569-7757 or email dwmethods.help@epa.gov 

NEPIS US EPA National Environmental Publications Internet Site, a database of over 9,000 EPA documents to browse/view, 

and print for free online at http://www.epa.gov/clariton/ 

NSCEP EPA National Center for Environmental Publications (free publications), PO Box 42419, Cincinnati, OH 45242-2419. 

(800)490-9198 or fax (513) 891-6685 or http://www.epa.gov/ncepihom 

NTIS National Technical Information Service (purchase publications), Dept. of Commerce, Springfield, VA 22161. phone 

(800)553-6847 ; fax (703) 321-8547; TDD (703)487-4639; telex 64617; Internet http://www.ntis.gov/ 

OPPTS Office of Prevention, Pesticides and Toxic Substances Harmonized test guidelines developed in 10 series 

http://www.epa.gov/OPPTS_Harmonized/ 

Pesticide Analytical Methods and Procedures Antimicrobial Testing Methods & Procedures (ATMP); Environmental Chemistry 

Methods (ECM); Residue Analytical Methods (RAM) http://www.epa.gov/oppbead1/methods/ 

OST Office of Science & Technology some selected methods (1600, 1613, 1623, 1631, 1664, O1A-1677) at 

www.epa.gov/ost/methods 

SEL CD Selected OW Methods and Guidance. September 2000. (EPA 821/C-00-002) 

SEL2 CD Selected Office of Water Methods and Guidance January 2001 (EPA 821/C-01-001 ) 

SOP # (2006-2058) all available online from ERT at http://www.ert.org/ 

ttn/amtic or ttn/emc http://www.epa.gov/ttn/ either AMTIC or EMC for specific methods 

14 
Sources for EPA Test Methods April 2003 

Water Office of Groundwater and Drinking Water selected methods at http://www.epa.gov/safewater/methods/sourcalt.html 

and http://www.epa.gov/waterscience/methods/ 

15