# AECOM

Appendi x D Laboratory Dat a

r



## VES01809 3

### Metho d 5/26 A



## VES0180 9AECO M Repor t Environmen t 

## Cas e Narrativ e Re. : Gravimetri cAnalysi s o f Filte ran d Fron t Hal f Prob e Rins e Sample s - Veoli a E S Tech , Sauget , I L Projec t #: 

### 6013321 6 LA B I D #: 09-064 , 09-067 , 09-06 9 ANALYTICA L PROCEDURE : Eleve n (11 ) Teflon®

typ e filters an d 1 2 front hal f aceton e rins e sample s wer e analyze d vi a EP AMetho d 5 Gravimetri cAnalysi s a s governe d b yAECOM' s SO P 2629-300 . Consecutiv e gravimetri cweight s o f filters an d beake rresidue s wer e take n wit h a n annuall ycalibrate d Mettle rbalance , an d weighe d withi n specifie d limit s a s outline d i n EP AMetho d 5 an d AECOM' s SO P 2629-300 .
1 . Fo rtw

o o f thre e shipment s received , 09-06 7 an d 09-069 , on e fiel d blan k o f bot h filte ran d aceton e wer e analyze d a s specifie d byEP AMetho d 5 Gravimetri cAnalysi s an d AECOM' s SO P 2629-300 . Th e firs t se t of samples , 09-064 , containe d on e aceton e blank , bu t n o filte rblan k wa s received . 2 . Laborator

yblanks of bot h filte ran d aceton e wer e analyze d fo reac h of th e thre e set s of sample s pe rth e sam e Metho d an d SO P a s liste d above . 1 . Fo rth e first se t o f sample s received , La b ID : 09-064 , two of th e aceton e sampl e bottles , M5-Acetone-R B an d M5-U3-AR-R3 , di d not hav e th e leve l o f aceton e marke d o n th e bottle . Additionally , followin g evaporatio n of th e firs t o f thes e tw

o samples , i.e . th e fiel d blank , a moist , oily-appearin g residu e wa s observe d i n th e sampl e beaker . Th e gravimetri cresul t fo rtha t sampl e indicate d a net gai n o f 1. 9 mg . 2 . Fo rth e thir

d se t o f samples , La b ID : 09-069 , on e o f th e aceton e rins e sampl e bottles , M5-U4-FHR-R2 , wa s foun d t o contai n a piec e o f aluminu m foil , whic h wa s remove d durin g th e aceton e rins e procedur e an d prio rt o weighing . QUALIT YCONTROL :

DISCUSSION :

Dat e Sample s Receive d b yth e Laboratory : 12/04 , 12/1 1 & 12/21/0 9 Dat e Analysi s Started : 12/07/0 9 R:\AirDBase\M5DBWIetho d 5 DatabaseWETHO D 5 CLIEN TFILESWeolia\09-064_067_069_CaseNarrative.do c



### Pag e 2 o f 1 4

## j AECO M i Metho d 5 Expose d Filte rDataShee t Balanc e Used : Mettle r3 Projec tManager: Projec tName: Projec tNumber: Analysi s Method : Jef

f Gorma n Da y Dal

e Tim

e R.H.(%)";

, R.T.CF ) Analys tj Projec tManager: Projec tName: Projec tNumber: Analysi s Method : Veoli

a Star t Tuesda

y 12/15/200

9 9:0 0 4

1 5

8 W

V Projec tManager: Projec tName: Projec tNumber: Analysi s Method : 6013321

6 Wt , 1 Wednesda

y 12/16/200

9 9.0 0 3

8 6

8 M

W Projec tManager: Projec tName: Projec tNumber: Analysi s Method : Ove n Drie d Wt . Z Frida

y 12/18/200

9 16:3 0 3

3 6

8 AC Projec tManager: Projec tName: Projec tNumber: Analysi s Method : Wt . 3 Wt . 4 vQAsSheet:

- Paaof f , X, Initia

l Weigh t' . Fille

r#_ , Sampl e RunDat e Sampl

e I D ' Hltef

- . Typa/Siz e 1s tWt . Gram s 2n d Wt . • Gram s A 1&

2 Wt . Gram s - ' 3rdWt

, Gram s A2&

3 Wti: Gram s 41hWt

. Gram s A 38.

4 Wt . Gram s Fina

l Wt . Gram s A FW-I

W Tota l Gram s vQAsSheet:

- Paaof f •at

e Grams

, - Fille r#_ , Sampl e RunDat e Sampl

e I D ' Hltef

- . Typa/Siz e 1s tWt . Gram s 2n d Wt . • Gram s A 1&

2 Wt . Gram s - ' 3rdWt

, Gram s A2&

3 Wti: Gram s 41hWt

. Gram s A 38.

4 Wt . Gram s Fina

l Wt . Gram s A FW-I

W Tota l Gram s 8 8 11/25/0

9 0.392

6 T182

8 

# — La b Blan k 82.

6 0.392

7 0.392

7 0.000

0 o kb y Wt . 0.392 7 0.000

3 8 7 11/25/0

9 0.406

0 T181

2 12/10/0

9 M5-Filte

rBlan k 82.

6 0.405

9 0.405

8 0.000

1 okbyWt

. 0.405 9 0.000

3 8 8 11/25/0

9 0.413

7 T182

0 12/08/0

9 M5-U2-F-R

1 82.

6 0.414

2 0.414

3 0.000

1 o k b y Wt . 0.414 3 0.000

6 8 7 11/25/0

9 0.397

1 T1811 12/09/0

9 M5-U2-F-R

2 82.

6 0.398

2 0.398

1 0.000

1 o kb y Wt . 0.398 2 0,0011 8 7 11/25/0

9 0.397

9 T181

0 12/10/0

9 M5-U2-F-R

3 82.

6 0.398

4 0.39B

4 0.000

0 o k byWt . 0.398 4 0.000

3
o

Filte

rType ; G=Glas

s ^^T^wjiff i Q=Quart z 1 . Delt a Weigh t toleranc e +i - O.OOOS g of tota l weigh t les s tar e weigh t betwee n tw o consecutiv e weighting s o raverag e weight . 2 . Filter s mus t b e weighe d wit h Ui e prope rcondition s (R H = 25-5 0 % an d R T= 59-7 8 de g f ) 3 . Filler s mus t b e properl yconditione d (2& hou rdesiccation ; Furthe rConditionin g > 6 hours) . 4. Conditionin g fo rove n method ; Ove n drie d a t 10 5 de g c f o 2- 3 hours ; Furthe rconditionin g > 6 hours , 5 . Tota l gram s belo wo requa l t o .000 5 (LDL ) i s presente d a s .0003 .

Veoli aJ)9-067__6013321

6 email.xl

s 

## VES01809 6

## AECO M Metho d 5 Fron tHal f Aceton e Prob e Rins e Dat aShee t Jef f Gorma n Balanc e Used : Projec tManager: Projec tName: Projec tNumber: Analysi s Method : Veoli

a 6013321 6 'Hea tAopllcatlg

n Ca y Dat

e Tim

e ;R.H.(%

) . R.T.<°F) . Analys

t Star t Thursda

y 12/17/200

9 10:3 0 3 4 6

7 R B Wt . 1 Frida

y 12/18/200

9 16:2 3 3 3 6

8 A C Wt . 2 Monda

y 12/21/200

9 8:4 5 3

3 6

8 W V Wt . 3 Tuesda

y 12/22/200

9 10:3 2 3 2 6

8 P T Wt . 4 G A Shee t Page T Beake r# . •Sampl e Ru n Date ' Sampl

e 1 0 Fiel

d mL ' La

b m L 1s tWt . Grams ; 2n d Wt , : Gram s •41&2Wt

. Gram s 3r d Wt . Gram s A2BWL . Gram s 4t h Wt . Grams . A3&4Wt

. Gram s Fina l Wt . Gram s 48 5 12/11/0

9 110.441

2 45 7 La b blan k 110.441 4 110.442

1 0.000

7 110.441

6 o

kb y Wt . 48 5 12/11/0

9 90.558

0 M5-Acetone-R8-U 2 o kb y Wt . 90.557 9 48 5 12/11/0

9 97.522

8 M5-U2-AR-R 1 97.524 2 97.524

9 0.000

7 97.524

4 o

kb y Wt . 12/11/0 9 94.935

8 36 1 12/09/0

9 M5-U2-AR-R

2 94.938 2 94.938

6 0.000

4 o kb y Wt . 94.938 4 48 5 12/11/0

9 106.178

4 40 9 12/10/0

9 M5-U2-AR-R

3 7

0 5

0 106.179

8 106.180

1 0.000

3 o kb y Wt . 106.180 0

Aceton e Manufacturer/Lo

tNo. : Rsher/092950_ _ Aceton e Rins e = 2 5 mi s twic e - (5 0 mi s total ) 1 . Delt a Weigh ! toleranc e +l~ 0.0005 g of tota l weigh t les s tar e weigh t betwee n tw o consecutiv e weighting s D raverag e weight . 2 . Beaker s mus t b e weighe d wit h th e prope rcondition s (R H = 2 5 - 5 0 % an d R T= 50-7 8 de g f ) 3 . Beaker s mus t b e properl yconditione d (2 4 hou rdesiccation : Furthe rConditionin g > 6 hours) . 4 . Natura l Evaporatio n Metho d = Evaporat e t o drynes s a t roo m temperatur e unde ra hoo d / watc h glas s cove r 5 . Hea t Applicatio n = Unde ra hco d an d watc h glas s ove rsample , appl yhea t belo wth e boilin g poin t c f sampl e unti l evaporate d t o 2 5 mis : the n follo wste p 4 {above ) fo rremainin g portio n 6 . Tota l gram s belo wo requa f t o .000 5 (LDL ) I s presente d a s .0003 .



## VES01809 7SAMPL E LOG-I N & RECEIP T CHECKLIS T 

### Client/Proj#
_ Projec t Mqr : O^'fi ^ £?<£> ri^nA^ La b Poo l # : 

## 09 -1 ^ 7 Inspecte d & Logge d i n by:_ 

### Dat e & Tme -Mifa
lis 

## KMaiy

s iSMi g 

## H Du'ei/^/^ f
Due : lil^tU 

### HT : Due : Circl e th e appropnat e response : 

### 1 ) $Jtippe$J

Han d delivere d 2 ) CO C p^seEr i /

no t presen t o n receip t 3 ) Sample s broke n /

leakin g /<Jrjtac£

) o n receip t 4 ) Sample s ^^^gji t / chille d o n receip t 5 ) Sample s preserve d correctl y/ incorrectl y^^e^recommende d 6 ) ReceivedCw|[^ /

outsid e holdin g tim e 7 ) CO C tape s presen t / gfitjjjj^sen t o n sample s / N A 9 ) DiscrepanciesiN^JpS-iscrepancie s note d betwee n COC s an d sample s Additiona l Comments : -

6 1 Pag e 1 3 o f 1 4 

### 8/26/2O0 8Sampl e Traceabilst y Lis t Sit e of Program : Veoli a E S Tec h Sampl e Date : rZ-lo-o < j - ii- A - 0 < i Projec t Location : Ssuge i I t P .O . # : Typ e o f Program : CP T Dat e Shipped : | 

### V~lo-ot Laboratory : AECO M Eiw h oilmen- . Projec t # : 6013321 6 Progra m Office : Syracus e N Y Shippe r/ Steve n Mil o Recovery : si> **• f \««u ^ ("Jef f Gorma n Laboratory : AECO M Eiw h oilmen- . Progra m Contact : Jef f Gorma n FedE x Ai rBil l # : Ite m Sampl e I D Cod e Sampl e Matri x Sampl e Descriptio n Analitica l Parameter s Specia l Instruction s 1 M5-U2-F-R 1 Filte r WIS , Filter , Ru n 1 Particular - M^lo r 

### O T- ac 7 - ^T . 2 MS-U2-AR-R 1 Aceton e iM5 , F M Aceton e Rinsa , Ru n ! Paniculat e tviaiiot ' ry?~ O'-">-. - 3 4 M5-U2-F-R 2 Filte r WIS , Filter , Ru n 2 Particulat e twsiln i 

### O c 

### ?~Q6"?~ -T 5 M5-U2-AR-R 2 Aceton e M S , F H .Aceton e Rinse , Ru n Z Pintliculatt ; iviaUe i 

### O c 

### '"Oz',-~ 6 7 W15-U2-F-R 3 Filte r WIS , Filter , Ru n 3 Particulat e Mailo i 8 iW!5-U2-AR-R 3 Acston e M 5 , F H Aceton e Rinss , Ru n . : Pariiculsit. - ivisfi^ v 9 1 0 1 1 1 2 1 3 1 4 1 5 1 6 1 7 1 8 • 1 9 o 1 " ' -o<r~"-- / 2 0 (yi5-Acetone-RB-U 2 Aceton e M5-Aceton e Blan k particulat e Waite r Fiel d Notes /

Comment s Pag e o f Relinquishe d B y(print) : Date : Signature : Time :

^Ad a 

### \1oO Relinquishe d B y(print) : Date : Signature : Time : Relinquishe d B y(print) : Date : Signature : Time : Receive d b yLa b (print) : Date : Signature : Time : Receive d B y(print) : Date : Signature : Time : Receive d B y(print) : Date : Signature : Time : Receive d B y(print) : Date : Signature : Time : Analytica l Laborator yDestination : AECO M Environmen t 32 5 Aye rRoa d Harvard , M A0145 1 Attn : Mr . Pau l Tavern a (978 ) 772-234 5 Ex t 3 2 

## VES01809 9

### TestAmeric a Laboratories , Inc .


## ANALYTICA L REPOR T

PROJEC T NO . 6013321 6 Veoli a - E S Tech . L o t # : H9L14040 2

Jef f Gorma n AECOM , In c 510 5 Caiqpuswoo d Driv e Suit e 10 4 Eas t Syracuse , N Y 1305 7

TESTAMERIC A

LABORATORIES , XHC .

Kevi nS . Woodcoc k Projec t Manage r

Decembe r 17, 200 9

S81 5 Middlebroo k Pik e Knoxville, TN3792 t te l 865.291.300 0 fax 865.584.431 5 www.testamericainc.co m 

## VES0181 0

## ANALYTICA L METHOD S SUMMAR Y H9L14040 2

ANALYTICA L PARAMETER — METH0 P Chlorin e Emission s KNO X00S0/2S A

Mo d Hydroge nChlorid e Emission s KNO X0050/26 A

Mo d References : KNO XTestAmeric a Laboratorie s Inc. , Knoxvill e Laborator y Standar d Operatin g Procedur e

### 3 

## SAMPL E SUMMAR Y

H9L14040 2

W O # SAMPLE # CLIEN T SAMPL E I D SAMPLED SAM P DAT E TIM E LQ2R G LQ2R K LQ2R M LQ2R N LQ2R V LQ2R W LQ2R 1 LQ2R 2 LQ2R 3 00 1

00 2 00 3 00 4 00 5 00 6 00 7 00 8 00 9 CPT-HCL-FB-U 2

CPT-CL2-FB-U 2 CPT-U2-HCL-IMP1 - 4-RI A CPT-U2-CL2-IMP5-6-R l CPT-U2-CL2-IMP1-4-R2 A CPT-TJ2-CL2-IMP5-6-R 2 CPT-U2-HCL-IMP1-4-R3 A CPT-U2-CL2-IMP5-6-R 3 CPT-H20-U2-F B 12/08/0 9 12/08/0 9 12/09/0 9 12/09/0 9 12/10/0 9 12/10/0 9 12/06/0 9 12/08/0 9 12/08/0 9 HOTE(S) :

- Th e analytica l results o f lit e sample s liste d abov e at e presente d o n th e followin g pages . • Al l calculation

s ar e performe d befor e roundin g t o avoi d round-of

f error s i n calculate d results .

- Result s note d a s "ND " wer e no tdetecte d a to rabov e th e state d limit .

- Thi s repor tmus tno tb e reproduced

, ctccp ti n full , withou tth e writte n approva l o f di e laboratory

.

- Kcsult s lo rlit e followin g parameter

s ar e neve rreporte d o n adr y weigh tbasis : color , corrosiviiy

. density , (lashpoini

. iEniiabtlliy

, layers , odor , pal m fillertest

. pH . porosit y pressure , rcaciivity , redo x potential

, specifi c gravity , spo ttests , solids , solubility , temperature

, viscosity , an d weight .



## VES01810 :

## PROJEC T NARRATIV E H9L14040 2 The result

s reporte d herei n ar e applicable t

o th e sample

s submitte

d fo ranalysi

s only . This repor

tshall no

tb e reproduce

d excepti n foil, withou tth e writte n approva

l o f th e laboratory

. 

### Th e origina l chai n o f custod y documentatio

n i s include d wit h thi s report . Sampl e Receip t Custod y seal s wer e no tpresent . 

### Qualit y Control an

d Dat aInterpretatio

n Unless otherwis

e noted , all holding time s an d Q C criteriawer

e me tand th e tes tresult s show n in thi s repor tmee tall applicable NELA C requirements. Sample s wer e analyzed forchloride by io n chromatograph y using SO Pnumbe

rICNOX WC-00 5 (base

d on EP A method

s 9056 , 905

7 an d 26A) . Al l sampl

e result s wer e reporte d a s tota l u g hydroge

n chloride (HCI) an

d tota l u g chlorine (Cb) . Result s wer e calculate

d usin g tlie foUowin g equations :

C l 2 , u g = (Chloride , u g /

mL) * (Sampl

e Volume , mL) * Bench Dilutio n 

### NaO H impinge

rsample

s wer e treate d wit h sodiu m thiosulfat

e (Na^SzOj) priorto th e fina l analysi s in ordert

o conver tresidua l hypochlorit

e (OCT) t

o chloride ion . Note : A sampl

e volume o f

10 0 m L wa

s use d t o conver tth e result s t o tota l u g fo rth

e metho d blanks , laborator

y contro l samples , an

d clien treagen tblank s i n orde rt o standardiz

e th e analyt e sampl e total .

TestAmerici

i Knoxvill e maintain

s th e following certifications , approval s an d accreditations : Arkansa s DE Q La

b #88 - 0688 , CaliforniaDH S ELA PCert . #2423 , Colorado DPHE , Connecticu tDP H La

b //PH-0223 , FloridaDO H La b #E87177

, GeorgiaDN RLa

b #906 , Hawai i DOH , Illinois EPA La b #200012

, Indian aDO H La

b #C-TN-02 , Iow

aDN R La b #375 , Kansa s DH E Cer

u #E-)0349 , Kentuck

y DE PLa

b #90101 , Louisian

aDE Q Cert. #03079

, Louisian

aDOHH , Marylan d DO E Cert. #277

, Michiga

n DE Q Lab #9933, Nevad aDEP , New Jerse

y DE PLa

b #TN001 , Ne

w Yor kDO H La b #10781, Nort

h CarolinaDP H La

b #21705, Nort

h Carolin

aDEHM RCert

. #64 , Ohi o EP A VA PLa

b «CL0059 , Oklahom aDE Q La

b #9415, Pennsylvani

aDE PLa

b #68-00576

, Sout h CarolinaDHE C Ce n #84001001 , Tennesse e DO H La b #02014

, Texa s CEQ , Uta

h DO H Lab S QUAN3 , Virgini aDG S La b #00165

. Washingio

n DO E La

b #C1314, Wes tVirgini aDE PCert . #345, Wes tVirgini aDHH RCer

tS9955C , Wisconsin DN RLa b #998044300

, Nava l Facilities Engineerin

g Servic e Cente ran d USD A Soi l Permi

t#S-46424

. This lis to f approval

s is subjec

tt o chang e an d doe s no t impl y tha tlaborator

y certification i

s availabl

e fo ral l parameter

s reporte d in thi s environmenta

l sampl e dat areport . HCi , u g = (Chloride , ug /

mL) * (Sample Volume , mL ) Molecula rWeigh tHC p Molecula rWeigh tC l * Benc h Dilutio n

## PROJEC T NARRATIV E H9L14040 2 Fo rdemonstratio

n o f analytica

l metho d perfonnanc

e on thes e samples , TestAmeric a Knoxvill e analyze

d matri x spike s (MS ) an

d matri x spik e duplicate

s (MSD) . Acceptabl

e recoverie

s o f thes e spikes demonstrat

e tha tquantitatio

n fro m thi

s particularstac

k ga s matri x i s accurat

e an d acceptable. Impinge rsample s containin

g O.I N H2SO

4 an d 0.1 N NaO H displa

y matri x interferenc

e effect s causing poormetlio

d performanc

e an d possibl

y givin g unreliabl

e dat aunless th

e interferenc

e i s removed . Therefore , th e sample s wer e diluted in th

e la b t o remov e th e interferenc

e fo ramor

e accurat e chloride response

. The sample s ma y b e analyzed a

tincreasin

g dilutions along wit

h matri x spike s until matri

x spike s recove rfrom th

e sampl e within laborator

y contro l limits . The io n chromatograp h calibration rang

e use d t o quantitat

e th e sample result

s permit s astandar

d ten-fol d sampl

e dilution while supportin g th e reportin

g limi twit

h th e low calibratio

n standard. Th e dilution factorreporte d o n tlie sampl

e resul tfor m doe s no trepresen

tth e benc h dilution factor. I

tis actually th

e combination o f

factor s require d b y th e metho d t o conver t th e anio n reportin

g limi tan

d metho d detectio

n limi tfrom ug/m L t

o tota l ug . I tma y appea rt o b e elevate d becaus

e i tincludes th

e tota l sampl e volume in mL .

### 6 

## Q C DAT A ASSOCIATIO N SUMMAR Y

H9L14040 2
Sampl e Preparatio nan d Analysi s Contro l Number s

SAMPLE S MATRI X ANALYTICA L METHO D LEAC H

BATC H # PRE P

BATC H # M

S RUN # 00 1 AI R KNO X 0050/2S A

Mod 934912 2 934910 7 00 2 AI R KNO X 00SO/26 A

Mo d 935015 3 935012 7 00 3 AI R KNO X 0050/26 A

Mo d 934912 2 934910 7 00 4 AI R KNO X O0SO/26 A

Mo d 93S015 3 935012 7 00 5 . AI R KNO X 0050/26 A

Mo d 934912 2 934910 7 OO S AI R KNO X 0050/26 A

Mod 935015 3 935012 7 00 7 AI R KNO X 005O/26 A

Mo d 934912 2 934910 7 00 8 AI R KNO X 00SO/2S A

Mod 934912 2 934910 7 00 9 AI R KNO X 0050/26 A

Mo d 935015 3 935012 7



## VES0181 0

### 7


# Sample Dat aSummar

y

VES0181 08

AECOM , la c Clien t Sainpl e ID : CPT-TT2-HCL-IMP1-4-R1 A

Genera l Chemistr y Lot-Sairtpl e # . .. : H9L14Q402-00 1 Wor k Orde r #... : LQ2R G Matri xAI R Dat e Sampled. ; 12/06/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRK P PARAMETE

R RESUL T R L ONIT S METHO D ANALYSI S DAT E BATC H # Hydroge nchlorid e 1670 0 200 0 u g KNO X0050/26 A

Mo d 12/14/0 9 934912 2 Dilutio n Factor : 19951.5 3 MD L . . t84

0



## VES0181 0

### 9

AECOM , In c Clien t Sampl e ID : CPT-U2-CL2-IMP5-6-R 1

Genera l Chemistr y Lot-Sampl e #... : H9L140402-00 2 Wor k Orde r LQ2R KMatri x: AI R Dat e Sampled... : 12/08/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRE P PARAMETER RESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H # Chlorin e 27 8 B 48 0 u g KNO X0050/26 A

Mo d 12/15/0 9 935015 3 Dilutio n Factor : 480 0 MD

L : 200 NOTK(S ) : .. . R L Reportin

g Limi t B Estimate

d result. Resul

ti s les s tha n HL .



## VES01810 8

### 10

AECOM , In c Clien t Sampl e ID : CPT-TJt2-CL2-_l_?l-4-R2 A

Genera l Chemistr y Lot-Sampl e it... : H9L140402-00 3 Wor k Orde r #. : LQ2R M Matri x: AI R Dat e Sample d : 12/09/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PREP PARAMETE

R RESUL T RL UNIT S METHO D ANALYSI S DAT E BATCH # Hydroge nchlorid e 2200 0 203 0 u g KNO X0050/26 A

Mo d 12/14/0 9 934912 2 Dilutio n Factor : 20250.0 6 MD L , : 85

0



## VES01810 !

### 1 1

Lot-Sampl e # . Dat e Sampled .
PARAMETER AECOM , In c Clien t Sampl e XDi CPT-U2-CL2-IMP5-6-R 2

Genera l Chemistr y
: H9L140402-00 4 Wor k Orde r #... : LQ2R N , : 12/09/0 9 Dat e Received.. : 12/11/0 9 Matrix . . : AI R

Chlorin e RESUL T R L N D UNIT S

48 0 u g Dilutio n Factor : 480 0 METHO

D PREPARATION - PRE P

ANALYSI S DAT E BATC H # KNO X0050/26 A

Mo d 12/15/0 9 HD L : 200 93501S 3



## VES01811 01 2

AECOM , In c Clien t Sampl e ID : CPT-TJ2-HCL-IMP1-4-R3 A
Lot-Sampl e #... : H9L140402-00 5 Dat e Sampled... : 12/10/0 9
PARAMETE

R RESOL T Genera l Chemistr y Wor k Orde r #... : LQ2R V Dat e Received.. : 12/11/0 9
R L UNIT S METHO D Matri x: AI R

PREPARATION - PRE P ANALYSI S DAT E BATCH # Hydroge nchlorid e 3240 0 399 0 u g KNO X0050/26 A

Mod 12/14/0 9 934912 2 Dilutio n Factor : 39903.0 5 MD L : no o



## VES01811 1

### 1 3

Lot-Sampl e # . Dat e Sampled .
PARAMETER AECOM , In c Clien t Sampl e ID : CPT-TJ2-CL2-TMP5-6-R 3

Genera l Chemistr y

. : H9L140402-00 6 Wor k Orde r #... : LQ2R W

. : 12/10/0 9 Dat e Received.. : 12/11/0 9 Matrox . AI R

Chlorin e RESUL T R L DHIT S N D 49 0 u g

Dilutio n Factor : 490 0 METHO

D PREPARATION - PRE P

ANALYSI S DAT E BATC H # KNO X0050/26 A

Mo d 12/15/0 9 MD L : 21 0 935015 3



## VES01811 2

### 1 4

AECOM , In c Clien t Sampl e ID : CPT-H20-U2-F B

Genera l Chemistr y Lot-Sampl e #... : H9L140402-00 7 Wor k Orde r : LQ2R 1 Matri x: AI R Dat e Sampled. : 12/08/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRE P PARAMETE

R RESUL T R L UNIT S METHO D ANALYSI S DAT E BATCH # Hydroge nchlorid e N D 10 3 u g KNO X0050/26 A

Mo d 12/14/0 9 934912 2



## VES01811 31 5

AECOM , In c Clien t Sampl e ID : CPT-HCL-FB-U Genera l Chemistr y Lot-Sampl e : H9L140402-00 8 Wor k Orde r #... ; LQ2E 2 Matri x: AI R Dat e Sampled... : 12/08/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRE P PARAMETE

R RESUL T R L UNIT S METHO D ANALYSI S DAT E BATCH # Hydroge nchlorid e N D 41 1 u g KNO X0050/26 A

Mod 12/14/0 9 934912 2 Dilutio n Factor : 4113.7 2 MD L = 17

0



## VES01811 4

### 1 6

Lot-Sampl e # , Dat e Sampled .
PARAMETE

R AKCOM , In c Clien t Sampl e ID. - CPT-CL2-FB-U 2

Genera l Chemistr y

. : H9L140402-00 9 Wor k Orde r #-.. : LQ2R 3

. : 12/08/0 9 Dat e Received.. : 12/11/0 9
RESUL T R L UNIT S METHO D Matri x: AI R

PREPARATION - PRE P ANALYSI S DAT E BATCH # Chlorin e N D 10 0 u g

Dilutio n Factor : 100 0 KNO

X0050/26 A

Mo d 12/15/0 9 MD - : 4 2 935015 3



## VES01811 !

### 1 7

METHO D BLAN KREPOR T Genera l Chemistr y Clien t Lo t H9L1 4 040 2
PARAMETER RESUL T Chlorin e
Hydroge nchlorid e REPORTIN G LIMI T UNIT S METHO D Matri x, : AI R

PREPARATION - PRE P ANALYSI S DAT E BATCH # Work Orde r # : LQ6MH1A A M B Lot-Sampl e # : H9L160000-15 3 N D 10. 0 u g KNO X0050/26 A

Mo d 12/15/0 9 935015 3 Dilutio nFactor : 10

0 Wor k Orde r # : LQ4NF1A A M B Lot-Sampl e # : H9L150000-12 2 N D 10. 3 u g KNO X0050/26 A

Mo d 12/14/0 9 934912 2 Dilutio nFactor : 102. 8 NOTECS ) : Calculation

s ar e performe d befor e roundin g c o avoi d round-of

f error s i n calculate d results.



## VES01811 6

### 18

LABORATOR

YCONTRO

L SAMPL E EVALUATIO N REPORT Genera l Chemistr y Lot-Sampl e H9L14040 2 Matrix . . : AI R
PARAMETER Chlorin e PERCENT

RECOVER

Y 9 8 9 9 RECOVER Y LIMIT S RPD RP D LIMIT S METHO

D PREPARATION ANALYSI S DAT E PRE P

BATC H # W0#:LQ6MH1AC-LCS/LQ6MH1AD-LCS D LC S Lot-Sampled : H9L160000-15 3 (9 0 - 110 ) KNO X0050/26 A

Mo d 12/15/0 9 935015 3 (9 0 - 110 ) 0.8 1 (0-20 ) KNO X0050/26 A

Mo d 12/15/0 9 935015 3 Dilutio n Factor ; 10 0 Hydroge nchlorid e

10 1 9 8 W0#:LQ4NF1AC-L_S/LQ4NF1AD-LCS D LC S Lot-Samplefr : H9L150000-12 2

(9 0 - 110 ) KNO X0050/26 A

Mo d 12/14/0 9 934912 2 (9 0 - 110 ) 2. 4 (0-20 ) KNO X0050/26 A

Mo d 12/14/0 9 934912 2 Dilutio n Factor : 102. 8 NOTE(S ) : Calculation

s ar c performe d befor e roundin g 1 0 ovoi d round-of

f error s i ncalculate d rcsulis .



## VES0181 1

### 1 9

LABORATOR

YCONTRO

L SAMPL E DAT A

REPORT Genera l Chemistr y Lot-Sampl e H9L14040 2 Matrix . AI R
PARAMETER Chlorin e PERCN T PREPARATION - PRE P RECVR YRPD METHO

D ANALYSI S DAT E BATCH # W0#:LQ6MH1AC-LCS/LQ5MH1AD-LCS D LC S Lot-Sample# : H9L160000-15 3 73. B u g 9 8 KNO X0050/26 A

Mo d 12/15/0 9 935015 3 74. 4 u g 9 9 0-8 1 KNO X0050/26 A

Mo d 12/15/0 9 935015 3 Dilutio n Factor : 10 0 SPIK E MEASURED AMOUN T AMOUN

T UNIT S 75. 0 75. 0 Hydroge nchlorid e

77. 1 77. 1 W0

# : LQ4NF1A

C - LC S / LQ4NF1A

D -LCS D LC S Lot-Satnple# : H9L150000-12 2 77. S u g 10 1 KNO X0050/2S A

Mo d 12/14/0 9 934912 2 75. 8 u g 9 8 2. 4 KNO X0050/26 A

Mo d 12/14/0 9 934912 2 Dilutio n Factor : 102. 8
NOTECS ) ; Calculation s ar cperforme d befor e roundin g t o avoi d round-of

f error s i n calculate d results .



## VES01811 8

### 20

MATRI XSPIK E SAMPL E EVALUATIO N REPORT Genera l Chemistr y Clien t Lo t #.. . Dat e Sampled... . : H9L14040 2

: 12/09/0 9 Dat e Received . 12/11/0 9
PARAMETE

R Chlorin e PERCENT RECOVER Y RECOVER

YLIMIT S RPD RP D LIMIT S METHO

D Matrix . : AI R

PREPARATION ANALYSI S DAT E PRE P

BATC H # 10 1 10 3 WO# : LQ2RN1AD-MS/LQ 2 RN1AE - MSD M S Lot-Sampl e # : H9L14O402-0O 4 (7 5 - 125 ) KNO X0050/26 A

Mo d 12/15/0 9 935015 3 (7 5 - 125 ) 1. 7 (0-20 ) KNO X0050/26 A

Mo d 12/15/0 9 935015 3 Dilutio n Factor : 4800 Hydroge nchlorid e

9 8 (7 5 9 4 (7 5 WO# : LQ2RM1AD-MS/LQ2RM1AE-MS D M S Lot-Sampl e # : H9L140402-00 3 125 ) KNO X0050/26 A

Mo d 12/14/0 9 934912 2 125 ) 0.5 6 (0-20 ) KNO X0050/2S A

Mo d 12/14/0 9 934912 2 Dilutio n Factor : 2026 0 NO — (S ) : CalculM-ion

s ar cperforme d befor e roundin g l o avoi d round-of

f error s i o calcufcue d results .



## VES01811 9

### 21

MATRI XSPIK E SAMPL E DATA , REPOR T

Genera l Chemistr y Clien t Lo t #... : H9L14040 2 Dat e Sampled... : 12/09/0 9

SAMPL E SPIK E PARAMETER AMOUN T AM T Matrix . . : AI R

Dat e Received.. : 12/11/0 9

Chlorin e N

D N D 96 0

96 0 Hydroge nchlorid e

2200 0 405 0 22O0 0 405 0 MEASR D AMOUN T UNIT S PERCNT

RBCVR YRP D METHO

D PREPARATIO N - PRE P ANALYSI S DAT E BATC H # WO# : LQ2RN1AD-MS/LQ2RN1AE-MS D M S Lot-Sampl e # : H9L140402-00 4 97 1 u g 10 1 KNO X0050/26 A

12/15/0 9 935015 3 98 8 u g 10 3 1. 7 KNO X0050/26 A

12/15/0 9 935015 3 Dilutio n Factor : 480 0 WO# : LQ2RM17AD-MS/LQ2RM1AE-MSD M S Lot-Sampl e # : H9L140402-00 3 2590 0 u g 9 8 KNO X0050/26 A

12/14/0 9 934912 2 2580 0 u g 9 4 0.5 6 KNO X0050/26 A

12/14/0 9 934912 2 Dilutio n Factor : 2026 0 NOTB(S ) ; _________ _ Calcataiiti B ar e performe d befor e rounding i

o avoi d round-of

f error s i n calculaie d rcsulis .



## VES01812 C

### 22

Clien t Lo t #... : H9L14040 2 Dat e Sampled... : 12/08/0 9 SAMPL E DUPLICAT E EVALUATIO N JREPOR T Genera l C_emistr y Wor k Orde r #...- . LQ2RG-SM P LQ2RG-DU

P Dat e Received.. : 12/11/0 9
PARA M RESUL T Hydroge nchlorid e 1670 0 1690 0 Matrix . AI R

DUPLICAT E RESUL T UNIT S RPD RPD LIMI T METHO D PREPARATION - PRE P

ANALYSI S DAT E BATC H # S D Lot-Sampl e # : H9L140402-00 1

U g 0.9 5 (0-20 ) KNO X0050/26 A

Mo d 12/14/0 9 934912 2 Dilutio n Factor : 19951.5 3



## VES01812 '

### 2 3

Clien t Lo t Dat e Sampled .
PARM M RESUL T Chlorin e 27 8 B SAMPL E DUPLICAT E EVALUATIO N REPOR T Genera l Chemistr y

. : H9L14040 2 Wor k Orde r #... : LQ2RK-SM P LQ2RK-DUP , : 12/08/0 9 Dat e Received.. : 12/11/0 9 Matrix . AI R

DUPLICAT E RESUL T UNIT S RP D RP D LIMI T METHO D 28 9 B PREPARATION - PRE P ANALYSI S DAT E BATCH # S D LOt-Sampl e # : H9L140402-00 2 u g 4. 1 (0-20 ) KNO XD050/26 A

Mo d 12/15/0 9 935015 3 Dilutio n Factor : 4800
NOT E (S ) Calculation s ar e performe

d befor e roundin g i o avoi d round-of f error s i n calculate d results . B Estimate

d result . Resul ti s les s tha n RL .



## VES01812 2

### 24

Clien t Lo t #... : H9L14040 2 Dat e Sampled... : 1 2 /09/0 9 DUPLICAT E PARA M RESUL T RESUL T Hydroge nchlorid e 2200 0 2160 0 SAMPL E DUPLICAT E EVALUATIO N REPOR T Genera l Chemistr y Wor k Orde r #... : LQ2RM-SM P LQ2RM-DU

P Dat e Received.. : 12/11/0 9 Matrix . AI R

UNIT S RP D

RPD LIMI T METHO D PREPARATION - PRE P

ANALYSI S DAT E BATC H # S D Lot-Sampl e # : H9L140402-00 3

U g 1. 7 (0-20 ) KNO X0050/26 A

Mo d 12/14/0 9 934912 2 Dilutio n Factor : 20260.0 6



## VES01812 32 5

H9L14040 2 12/09/0 9 DUPLICAT E RESUL T SAMPL E DUPLICAT E EVALUATIO N REPORT Genera l Chemistr y Wor k Orde r #... : LQ2RN-SM P LQ2RN-D- P Dat e Received.. : 12/11/0 9

N D Matrix . A I R

UNIT S RPD

RPD LIMI T METHO D PREPARATION - PRE P

ANALYSI S DAT E BATCH #

~ ~ S D Lot-Sampl e # : H9L140402-00 4 u g o (0-20 ) KNO X0050/26 A

Mod 12/15/0 9 935015 3 Dilutio n Factor ; 480 0



## VES01812 4

### 2 6

Clien t Lo t #... : H9L14040 2 Dat e Sampled... : 12/10/0 9 SAMPL E DOPLICAT E EVALUATIO N EEPOR T Genera l Chemistr y Wor k Orde r #... : LQ2RV-SM P LQ2RV-DUP Dat e Received.. ; 12/11/0 9
PARA M RESUL T DUPLICAT E

RESUL T Hydroge nchlorid e

3240 0 3160 0 Matrix . AI R

UNIT S RPD

RP D LIMI T METHO D PREPARATION - PRE P

ANALYSI S DATE . BATC H # S D Lot-Sampl e # : H9L140402-00 5 u g 2. 4 (0-20 ) KNO X0050/26 A

Mo d 12/14/0 9 934912 2 Dilutio n Factor ; 39903.0 5



## VES01812 5

### 2 7

H9L14040 2 12/10/0 9 DUPLICAT E RESUL T SAMPL E DUPLICAT E EVALUATIO N REPORT Genera l Chemistr y Wor k Orde r ft...: LQ2RW-SM P LQ2RW-DU

P Dat e Received.. : 12/11/0 9

N D Matrix . AI R

UNIT S RPD

RP D LIMI T METHO D PREPARATION - PRE P

ANALYSI S DAT E BATC H # S D Lot-Sampl e # : H9L140402-00 6 u g 0 (0-20 ) KNO X0050/26 A

Mo d 12/15/0 9 935015 3 Dilutio n Factor : 490 0



## VES01812 J

### 2 8

Clien t Lo t # . . . : H9L14040 2 Dat e Sampled... : 12/08/0 9 DUPLICAT E PARfl M RESUL T RESUL T Hydroge nchlorid e N D N

D SAMPL E DUPLICAT E EVALUATIO N REPOR T Genera l Chemistr y Wor k Orde r LQ2R1-SMP LQ2R1-DUP Dat e Received.. : 12/11/0 9 Matrix . AI R

UNIT S RPD

RP D LIMI T METHO D PREPARATION - PRE P

ANALYSI S DAT E BATC H # S D Lot-Sampl e # : H9L140402-00 7

u g0 (0-20 ) KNO X0050/26 A

Mod 12/14/0 9 934912 2 Dilutio n Factor : 1028.4 3



## VES01812 7

### 2 9

Clien t Lo t #..- : H9L14040 2 Dat e Sampled... : 12/08/0 9 DUPLICAT E PARA N RESUL T RESUL T Hydroge nchlorid e N D N

D SAMPL E DUPLICAT E EVALUATIO N REPORT Genera l Chemistr y Wor k Orde r #... : LQ2R2-SM P LQ2R2-DUP Dat e Received.. : 12/11/0 9
UNIT S RPD

RPD LIMI T METHO D Matrix . AI R

PREPARATION - PRE P ANALYSI S DAT E BATC H ft S D Lot-Sample " # : .H9L140402-0O 8 u g 0 (0-20 ) KNO X0050/26 A

Mod 12/14/0 9 934912 2 Dilutio n Factor ; 4113.7 2



## VES01812 8

### 30

H9L14040 2 12/08/0 9 DUPLICAT E RESUL T SAMPL E DUPLICAT E EVALUATIO N REPORT Genera l Chemistry Wor k Orde r #... : LQ2R3-SM P LQ2R3-DUP Dat e Received.. : 12/11/0 9

N D Matrix . . : AI R

UNIT S RP D RP D LIMI T METHO D PREPARATION - PRE P

ANALYSI S DAT E BATC H #

— ' S D Lot-Sampl e # : H9L140402-00 9

u go (0-20 ) KNO X0050/26 A

Mod 12/15/0 9 935015 3 Dilutio n Factor : 100 0



## VES01812 J

### 31



# Sample Receip t

Documentatio n

VES01813 0

## Sampl e Traceabilit y Lis t 

## j AECO M Site o f Program : Veoli aE S Tec h Sampl e DatB : i„-?\-o< ? - tS-'lo-o ^ Projec tLocation : Sauget , I L Lab P0#' : Tvo e o f Pronram : CP T Dat e Shipped : iZ r| o -o l Laboratory : TestAmerica, Inc . Knoxville . T N Project* : 6013321 6 Shipper/ Steve n Mil o Recovery : \

_rW_>- , peff Gorma n Laboratory : TestAmerica, Inc . Knoxville . T N Proqra m Office : Syracuse N Y Shipper/

Steve n Mil o Recovery : \

_rW_>- , peff Gorma n Laboratory : TestAmerica, Inc . Knoxville . T N Program Contact : Jef f Gorma n FedE x Ai rBil l # : Ite m Sampl e I D Code Sampl e Matri x Sampl e Descriptio

n Analytica l Parameter

s Specia l Instruction

s 1 CPT-U2-HCL-IMP1-4- R1 A 0.1N H2S0 4 Uni t2, Impinger

s 1-4 , Ru n 1 A H C Lj o

M f i irrr^-r v AV

Oil (\ \ ^



### _ 3 CPT-U2-CI2-JWIP5-6- R1 0.1 N NaOH Uni t2 , Impinger

s 5-6 , Ru n 1 '—fcB
J
- TxiJlrAVi^y ?n<~Kn o 4 1X7. °\AJC^> 5 CPT-U2-HCL-IMP1-4- R2 A 0.1N H2S0 4 Uni t2 , ImpingBr

s 1-4 , Ru n 2 A flXL. 5 7 CPT-U2-CI2-IW1P5-6- R2 0.1 N NaOH Uni t2 , Impinger

s 5-8 , Ru n 2 c i 2 a#l „ A 

### a 9 4 n CPT-U2-HCL-1MP1-4- R3 A 0.1N H2S0 4 Uni t2 , Impinger

s 1-4 . Ru n 3 A HC L Sto^Lj * j ti n °i f ^tt r I U 1 1 U r1 -Ux» l 1—t-"Jftft l N-"!"! * o U CPT-U2-CI2-IIWP5-6- R3 0.1N NaOH Uni t2 , Impinger

s 5-6 , Ru n 3 

### . M 

### .V L

### s&HU ' f ; CI 2 8U^I/ > < 1 2 N b JA.aTt»n \ j j 1 3 1 4 1 5 1 6 1 7 

### f?P T - \A 7 

### 0 -OvF © V\x O Fie. U PiU k )AC\ rvvi A C>l^ - 1 8 CPT-HCL-FB-U 2 0.1N H2S0 4 0.1 N H2S04 Fiel d Blan k HC L 19 CPT-CI2-FB-U 2 0.1N NaO H 0.1 N NaOH Fiel d Blan k CI 2 2 0 Fiel d Notes / Comment

s Pag e of Relinquishe

d B y (print) : Date : Steven Mil o &~lO-Ol Signature ; /

> Time : 

### -W/ l !7oo Relinquishe d By (print) : Date ; Signature : Time : Relinquishe d B y (print) : Date : Signature : Time : Receive d b y La b (print) : Date : Signature : Time : Receive d By (print) : Date : —Signature^ . Time : Receive d B y (print) : Date : Signature : Time : j Receive d By (print) ; Date : Signature : Time : Analytica l Laborator

y Destination : Receive d By (print) : Date : —Signature^ . Time : Receive d B y (print) : Date : Signature : Time : j Receive d By (print) ; Date : Signature : Time : TestAmericaInc . 5815 Middlebroo

kPik e Knoxville , T N 3792

1 Attn : Mr . Kevi n Woodcoc

k865-291-300

0 O

J t o 

## VES01813 1

### TESTAMERIC A KNOXVILL E SAMPL E RECEIPT/CONDITIO N UPON RECEIP T ANOMAL Y CHECKLIS T LotNumber: r^uMTHOT) , Revie w Items N A I f No , whatwas th e problem ? Comments/Action s Take n 1 . D o sample containe rlabels matc

h COC ? (IDs , Dates , Times ) 

# /

—L a l aD o no tmatc h CO C D l b Incomplet

e information • l c Markin g smeare

d • I d Labe l tor

n Q l e N o labe

l U I f CO C no treceived a l g Other : 1 . D o sample containe rlabels matc

h COC ? (IDs , Dates , Times ) 

# /

—L a l aD o no tmatc h CO C D l b Incomplet

e information • l c Markin g smeare

d • I d Labe l tor

n Q l e N o labe

l U I f CO C no treceived a l g Other : 1 . D o sample containe rlabels matc

h COC ? (IDs , Dates , Times ) 

# /

—L a l aD o no tmatc h CO C D l b Incomplet

e information • l c Markin g smeare

d • I d Labe l tor

n Q l e N o labe

l U I f CO C no treceived a l g Other : 1 . D o sample containe rlabels matc

h COC ? (IDs , Dates , Times ) 

# /

—L a l aD o no tmatc h CO C D l b Incomplet

e information • l c Markin g smeare

d • I d Labe l tor

n Q l e N o labe

l U I f CO C no treceived a l g Other : 1 . D o sample containe rlabels matc

h COC ? (IDs , Dates , Times ) 

# /

—L a l aD o no tmatc h CO C D l b Incomplet

e information • l c Markin g smeare

d • I d Labe l tor

n Q l e N o labe

l U I f CO C no treceived a l g Other : 1 . D o sample containe rlabels matc

h COC ? (IDs , Dates , Times ) 

# /

—L a l aD o no tmatc h CO C D l b Incomplet

e information • l c Markin g smeare

d • I d Labe l tor

n Q l e N o labe

l U I f CO C no treceived a l g Other : 1 . D o sample containe rlabels matc

h COC ? (IDs , Dates , Times ) 

# /

—L a l aD o no tmatc h CO C D l b Incomplet

e information • l c Markin g smeare

d • I d Labe l tor

n Q l e N o labe

l U I f CO C no treceived a l g Other : 1 . D o sample containe rlabels matc

h COC ? (IDs , Dates , Times ) 

# /

—L a l aD o no tmatc h CO C D l b Incomplet

e information • l c Markin g smeare

d • I d Labe l tor

n Q l e N o labe

l U I f CO C no treceived a l g Other : I. I s th e coole rtemperatur

e withi n limits ? (

> freezin g temp . ofwaterto6 p C;NC , 1668, 1613B : 0-4"C ; VOST : 10°C;MA:2-6°C ) 

# J 1 • 2 aTem p Blank= I. I s th e coole rtemperatur

e withi n limits ? (

> freezin g temp . ofwaterto6 p C;NC , 1668, 1613B : 0-4"C ; VOST : 10°C;MA:2-6°C ) 

# J 1 • 2 b Coole rTem p = I. I s th e coole rtemperatur

e withi n limits ? (

> freezin g temp . ofwaterto6 p C;NC , 1668, 1613B : 0-4"C ; VOST : 10°C;MA:2-6°C ) 

# J 1 3 . Wer e sample s received wit

h correc tchemica

l preservativ

e (excluding Encore) ? 0 3 aSample preservativ e = i 3 . Wer e sample s received wit

h correc tchemica

l preservativ

e (excluding Encore) ? 0 3 aSample preservativ e = i 4 . Were custod

y seals present/intac

ton coole rand/or containers ? 

# \ 4aNo tpresen t • 4b No tintac

t • 4 c Other : 4 . Were custod

y seals present/intac

ton coole rand/or containers ? 

# \ 4aNo tpresen t • 4b No tintac

t • 4 c Other : 4 . Were custod

y seals present/intac

ton coole rand/or containers ? 

# \ 4aNo tpresen t • 4b No tintac

t • 4 c Other : 5 . Were al l o f

th e sample s listed o n th e CO C received ? 0 S aSample s received-noto n CO C • 5 b Sample

s no treceived-on CO C 5 . Were al l o f

th e sample s listed o n th e CO C received ? 0 S aSample s received-noto n CO C • 5 b Sample

s no treceived-on CO C 6. Were al l o f

th e sampl e container

s received intact? 

### I • 6 aLeakin g • 6b Broken 6. Were al l o f

th e sampl e container

s received intact? 

### I • 6 aLeakin g • 6b Broken 7 . Wer e VO A sample

s received withou

theadspace ? 

## -1 • 7 aHeadspac e (VO A only ) S . Were sample

s received i n appropriat e containers ? 

### J —f- D 8 aImprope rcontainer 9. Di d yo u check forresidua l chlorine , i f

necessary ? i . 

# J • 9aCoul d no tb e determine

d du e t o matri x interferenc

e 9. Di d yo u check forresidua l chlorine , i f

necessary ? i . 

# J • 9aCoul d no tb e determine

d du e t o matri x interferenc

e 10 . Were sample

s received witlii n holdin g time ? J i • 10 aHoldin g tim

e expired 11 . Fo rra

d samples , wa

s sampl e activit y info , provided ? 

## 1, • Incomplet e information 12 . Fo rI613 B wate

rsample s i s pH<9 ? 

# J I f no , wa s p H adjuste

d t o p H 7 - 9 wit h sulfuri c acid ? 12 . Fo rI613 B wate

rsample s i s pH<9 ? 

# J I f no , wa s p H adjuste

d t o p H 7 - 9 wit h sulfuri c acid ? 13. Ar e tli

e shippin g container

s intact? 

# i
-f — • 13aLeakin g

D 13b Other : 13. Ar e tli

e shippin g container

s intact? 

# i
-f — • 13aLeakin g

D 13b Other : 13. Ar e tli

e shippin g container

s intact? 

# i
-f — • 13aLeakin g

D 13b Other : 14. Was CO C relinquished ? (Signed/Dated/Timed ) • 14 aNo trelinquished 15. Ar e tests/parameter s listed fo reac

h sample ? D 15 aIncomplet

e information 16 . I s th e matri x ofth e sample

s noted ? • 15 n Incomplet

e information 17, I s th e date/tim

e o f sample collectio n noted ? 

### h • 15aIncomplet e information 18 , I s th e clien tan

d projec tname/t f identified ? 

## 1 1 0 15aIncomplet e information 19 . Wa s tlie sampleridentifie d o n th e COC ? 

## / Ouote# : ^"Yi ^

P M Instructions : ""~"N/ \ -.r,, . - Sample Receivin g Associat e Date:Jj4l]]0^ _ QA026R21.doc , 090409

w co 

## VES01813 2

### 34



# We t Chemistr y

VES01813 3

### 35



# Sampl e Summar

y

VES01813 4

### 3 6

AECOM , In c Clien t Sampl e ID : CPT-D2-HCD-IMP1-4-RX A Genera l Chemistr y Lot-Sampl e #... : H9L140402-00 1 Wor k Orde r #... : LQ2R G Matri x: AI R Dat e Sampled... : 12/08/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRE P PARAMETER RESUL T R L OKIT S METHO D ANALYSI S DAT E BATC H # Hydroge nchlorid e 1670 0 200 0 u g KHO X005Q/26 A

Mo d 12/14/0 9 934912 2 Dilutio n Factor : 19951.5 3 MD L : 84

0



## VES01813 5

### 3 7

AECOM . In c Clien t Sampl e ID : CPT-D2-CL2-IMP5-6-S 1

Genera l Chemistr y Lot-Sampl e #... : H9L140402-00 2 Wor k Orde r #... : LQ2R KMatri x: AI R Dat e Sampled... : 12/08/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRE P PARAMETER RESUL T R L UNIT S METHO D ANALYSI S DAT S BATCH # Chlorin e 27 8 B 48 0 u g KNO X0050/2S A

Mo d 12/15/0 9 935015 3 Dilutio n Factor : 480 0 MD

L : 20

0 NOT E (S ) : R l Rq>ortin

g Limi t B Esiirmic

d result . Resul ti s les s tha n RL .



## VES01813 6

### 3 8

AECOM , In c Clien t Sampl e ID : CET-D2-CL2-IMP1-4-R2 A

Genera l Chemistr y Lot-Sannpl e H9L140402-00 3 Wor k Orde r #... : LQ2R M Matri x: AI R Dat e Sampled... : 12/09/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRE P PARAMETER RESUL T R L UNIT S METHO D ANALYSI S DAT E BATCH # Hydroge ncnlorid e 2200 0 203 0 u g KHO X0050/26 A

Mo d 12/14/0 9 934912 2 Dilutio n Factor : 20260.0 6 MD L : SS

O



## VES01813 7

### 3 9

AECOM , In c - Clien t Sampl e ID : CPT-D2-CL2-IMP5-6-E 2

Genera l Chemistr y Lot-Sampl e #... : H9L140402-00 4 Wor k Orde r : LQ2R N Matri x: AI R Dat e Sampled... : 12/09/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRE P PARAMETER RESUL T R L UNIT S METHO D ANALYSI S DAT E BATCH # Chlorin e N D 48 0 u g KNO XO05O/26 A

Mo d 12/15/0 9 935015 3 Dilutio n Factor ! 480 0 MD

L : 20

0



## VES01813 8

### 4 0

AECOM , In c Clien t Sampl e ID : CPT-02-HCL-IME>l-4-R3 A

Genera l Chemistr y Lot-Sampl e it... : H9L140402-00 5 Wor k Orde r #... : LQ2R V Matri x: AI R Dat e Sampled... : 12/10/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRE P PARAMETER RESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H # Hydroge nchlorid e 3240 0 399 0 u g KNO X0050/26 A

Mo d 12/14/0 9 934912 2 Dilutio n Factor : 399Q3.0 5 MD L : 170

0



## VES01813 9

### 4 1

AECOM , In c Clien t Sampl e ID t CPT-U2-CL2-IMP5-6-E 3

Genera l Chemistr y Lot-Sampl e #... : H9L140402-00 6 Wor k Orde r #... : LQ2R W Matri x: AI R Dat e Sampled... : 12/10/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRE P PARAMETE

R RESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H J Chlorin e N D 49 0 u g KNO XO05O/26 A

Mo d 12/15/0 9 935015 3 Dilutio n Factor : 490 0 MD

L : 21 0



## VES01814 0

### 42

AECOM , In c Clien t Sampl e ID : CPT-H20-02-5 B

Genera l Chemistr y Lot-Sampl e #... : H9L140402-00 7 Wor k Orde r LQ2R 1 Dat e Sampled... : 12/08/0 9 Dat e Received.. : 12/11/0 9
PARAMETE

R RESUL T R L UNIT S METHO D Hydroge nchlorid e Matrix . . : AI R
PREPARATION - PRE P ANALYSI S DAT S BATCH # N D 10 3 u g KNO X0050/2S A

Mod 12/14/0 9 Dilutio n Factor- . 1028.4 3 MD L i 4

3 934912 2



## VES01814 1

### 4 3

AECOM , In c Clien t Sampl e ID : CPT-HCL-PB-0 2

Genera l Chemistr y Lot-Sampl e # . H9L140402-00 8 Work Orde r #... : LQ2R 2 Matri x= AI R Dat e Sampled... : 12/08/0 9 Dat e Received.. s 12/11/0 9 PREPARATION - PRE P PARAMETER RESUL T R L UNIT S METHO D ANALYSI S DAT E BATCH ft Hydroge nchlorid e N D 41 1 u g KNO X0050/26 A

Mo d 12/14/0 9 934912 2 Dilutio n Factor : 4113.7 2 MDL . : 17

0



## VES01814 2

### 44

AECOM , In c Clien t Sampl e ID : CPT-CL2-FB-02

Genera l Chemistr y H9L140402-00 9 Wor k Orde r #... : LQ2R 3 12/08/0 9 Dat e Received.. : 12/11/0 9
RESUL T R L UNIT S METHO D Matrix . AI R

PREPARATION - PRE P ANALYSI S DAT E BATCH # N D 10 0 u g

Dilutio n Factor : 100 0 KNO

X005O/2S A

Mo d 12/15/0 9 MD L : 4

2 935015 3



## VES01814 3

### 4 5



# Q C Summar

y

VES01814 4

### 4 6

Clien t Lo t H9L1404D 2
PARAMETE R RESUL T 

### Chlorin e
Hydroge nchlorid e N D

N D METHO D BLAN KREPOR T Genera l Chemistr y Matrix . A I R REPORTIN

G LIMI T UNIT S METHO D PREPARATION - PRE P

ANALYSI S DAT E BATCH # Wor k Orde r # : LQ6MH1A A M B Lot-Sampl e # : H9LI6000Q-15 3 10. 0 u g KNO X0050/26 A

Mo d 12/15/0 9 935015 3 Dilutio n Factor : 10 0 Wor k Orde r # : LQ4NF1A A M B Lot-Sampl e # : H9L150000-12 2 10. 3 u g KNO X0050/26 A

Mo d 12/14/0 9 934912 2 Dilutio n Factor : 102. 8 

### NOT E (S) : Calculiiion s ar e performe

d befor e roundin g l o avoi d round-of

f error s i n calculaie d results .



## VES01814 5

### 4 7

LABORATOR

YCOHTROL SAMPL E EVALuATTO H REPOR T

PARAMETE R Chlorin e Genera l Chemistr y Lot-Sampl e #. . H9L14040 2

PERCEN T RECOVER

Y 9 8 9 9 RECOVER Y LIMIT S RP D RP D LIMIT S METHO

D Matri x: AI R

PREPARATION ANALYSI S DAT E PRE P

BATC H # W0#:LQ6MH1AC-LCS/LQSMH1AD-LCS D LC S Lot-Satnple# : H9L160OD0-15 3 (9 0 - 110 ) KNO X0O50/26 A

Mod 12/15/0 9 935015 3 (9 0 - 110 ) 0.8 1 (0-20 ) KNO XD050/26 A

Mod 12/15/0 9 935015 3 Dilutio n Factor : 10 0 Hydroge nchlorid e

10 1 9 8 W0#:LQ4NF1AC-LCS/LQ4NF1AD-LCS D LC S Lot-Sample# : H9L150000-12 2

(9 0 - 110 ) KNO X0050/26 A

Mod 12/14/0 9 934912 2 (9 0 - 110 ) 2. 4 (0-20 ) KNO X0050/26 A

Mo d 12/14/0 9 934912 2 Dilutio n Factor : 102. 8
NOT E (S ) ; Calculation

s ar e performe d befor e roundin g t o avoi d round-of

f error s i n calculate d results .



## VES01814 6

### 4 8

LABORATOR

YCOHTROI . SAMPL E DATA REPORT Genera l Cnemistx y Lot-Sampl e #... : H9L14040 2 Matrix . AI R
PARAMETE R Chlorin e SPIK E MEASORE D AMOUN T AMOUN

T UNIT S PERCN T

RECVRYRPD METHO D PREPARATION ANALYSI S DAT E 75. 0 75. 0 PRE P BATC H # W0#:LQSMH1AC-LCS/LQ6MH1AD-LCS D LC S Lot-Sample# : H9L160000-15 3 73. 8 ug- 9 8 KNO X0050/26 A

Mo d 12/15/0 9 935015 3 74: 4 u g 9 9 0.8 1 KNO X0050/2S A

Mo d 12/15/0 9 935015 3 Dilutio n Factor : 10 0 Hydroge nchlorid e

77. 1 77. 1 W0#:LQ4NF1AC-LCS/LQ4NF1AD-LCS D LC S Lot-Sample* : H9L150OO0-12 2

77. 6 u g 10 1 KNO X0050/26 A

Mo d 12/14/0 9 934912 2 75. 8 u g 9 8 2. 4 KNO X0050/26 A

Mod 12/14/0 9 934912 2 Dilutio n Factor : 102. 8 HOTE(S ) Calculation

s ar cperforme d befor e roundin g t o avoi d round-of

f error s i n calculate d results .



## VES01814 7

### 4 9

MATRI XSPIK E SAMPL E EVALUATION REPOR T Genera l Chemistr y Clien t Lo t H9L14040 2 Dat e Sampled... : 12/09/0 9 Dat e Received.. : 12/11/0 9
PARAMETER Chlorin e PERCEN T RECOVER

Y RECOVER

YLIMIT S RP D RP D LIMIT S METHO

D Matrxx . AI R

PREPARATION ANALYSI S DAT E PRE P

BATC H # 10 1 10 3 WO# : LQ2RN1AD-MS/LQ2RN1AE-MS D M S Lot-Sampl e # : H9L140402-00 4 (7 5 - 125 ) KNO X0050/2S A

Mod 12/15/0 9 935015 3 (7 5 - 125 ) 1. 7 (0-20 ) KNO X0050/26 A

Mod 12/15/0 9 935015 3 Dilutio n Factor ; 480 0 Hydroge nchlorid e

9 8 (7 5 9 4 (7 5 W0# : LQ2RM1AD-MS/LQ2RM1AE-MS D M S Lot-Sampl e # : H9L14O402-OO 3 125 ) KNO X0050/26 A

Mo d 12/14/0 9 934912 2 125 ) 0.5 6 (0-20 ) KNO X0050/26 A

Mo d 12/14/0 9 934912 2 Dilutio n Factor : 20260 NOTE{S) : Calculation

s ar cperforme d befor e roundin g t o avoi d round-of

f error s i n calculate d results .



## VES01814 8

### 5 0

MATRI XSPIK E SAMPL E DAT A REPOR T Genera l Chemistr y Clien t Lo t H9L14040 2 Dat e Sampled... : 12/09/0 9

SAMPL E SPIK E MEASR D Matrxx . AI R Dat e Received.. : 12/11/0 9
PARAMETER AMOUN T AM T Chlorin e N

D N D 96 0

96 0 AMOUN

T UNIT S PERCN T RECVR YRPD METHO

D PREPARATION - PRE P

ANALYSI S DAT E BATCH # WO# : LQ2RN1AD-MS/LQ2RN1AE-MS D M S Lot-Sampl e # : H9L14O402-00 4 97 1 u g 10 1 KNO X0050/26 A

12/15/0 9 935015 3 98 6 u g 10 3 1. 7 KNO X0050/26 A

12/15/0 9 935015 3 Dilutio n Factor s 480 0 Hydroge nchlorid e

2200 0 405 0 2200 0 405 0 WO# : LQ2RM1AD-MS/LQ2RM1AE-MS D M S Lot-Sampl e # : H9L14O402-00 3 2590 0 u g 9 8 KNO X0050/26 A

12/14/0 9 934912 2 2580 0 u g 9 4 0.5 6 KNO X0050/26 A

12/14/0 9 934912 2 Dilutio n Facto n 2026 0 NOTE(S) ; Calculation

s ar cpcrfacme d befor e roundin g t o avoi d round-of

f error s i n calculate d results .



## VES01814 9

### 5 1

Clien t Lo t #... : H9L14040 2 Dat e Sampled... : 12/08/0 9 DUPLICAT E PARA M RESUL T RESUL T Hydroge nchlorid e 1S70 0 1690 0 SAMPL E DUPLICAT E EVALUATIO N REPOR T Genera l Chemistr y Wor k Orde r # . „. : LQ2RG-SM P LQ2RG-DU

P Dat e Received.. : 12/11/0 9 Matrix: . AI R

UNIT S RPD

RPD LIMI T METHO D PREPARATION - PRE P

ANALYSI S DAT E BATC H # S D Lot^Sampl e # : H9L140402-00 1 •u g 0.9 6 (0-20 ) KNO X0050/2S A

Mo d 12/14/0 9 934912 2 Dilutio n Factor ! 19351.5 3



## VES01815 0

### 5 2

Clien t Lo t # . Dat e Sampled .
PARA M RESUL T Chlorin e 27 8 B H9L14040 2

12/08/0 9 DUPLICAT E RESUL T SAMPL E DUPLICAT E EVALUATION REPOR T Genera l Chemistr y Wor k Orde r #... : LQ2RK-SM P LQ2RK-DUP Dat e Received.. : 12/11/0 9 Matrix . AI R

UNIT S RPD RP D LIMI T METHO

D 28 9 B PREPARATION - PRE P ANALYSI S DAT E BATCH # S D Lot-Sampl e # : H9L140402-00 2 u g 4. 1 (O-20 ) KNO X0050/2S A

Mo d 12/15/0 9 935015 3 Dilutio nFactor : 480 0 NOTB(S ) : Calculation

s at e performe

d befor e roundio

g t o avoi d round-of

f error s i n calculate

d results . B Estimate

d result . Resul ti s les s tha n RL .



## VES01815 1

### 53

Clien t Lo t #... : H9L14040 2 Dat e Sampled... : 12/09/0 9 SAMPL E DUPLICAT E EVALUATION REPOR T Genera l Chemistr y Wor k Orde r #.-. : LQ2RM-SM P LQ2RM-DU

P Dat e Received.. : 12/11/0 9 DUPLICAT E RESUL T PARA M RESUL T Hydroge nchlorid e 2200 0 2160 0 UNIT S RPD RPD LIMI T METHO D Matrix . : AI R

PREPARATION - PRE P ANALYSI S DAT E BATC H # S D Lot-Sampl e # : H9L140402-0O 3 u g 1. 7 (0-20 ) KNO X0050/26 A

Mo d 12/14/0 9 934912 2 Dilutio nFactor ; 20260.0 6



## VES01815 2

### 54

H9L14040 2 12/09/0 9 DUPLICAT E RESUL T SAMPL E DUPLICAT E EVALUATION REPOR T Genera l Chemistr y Wor k Orde r #... : LQ2RN-SM P LQ2RN-DU

P Dat e Received.. : 12/11/0 9

ND UNIT S RPD RPD LIMI T METHO

D Matrix . AI R

PREPARATION - PRE P I ANALYSI S DAT E BATCH # f S D Lot-Sampl e # : H9L140402-00 4 u g 0 (0-20 ) KNO X0050/26 A

Mo d 12/15/0 9 935015 3 Dilutio nFactor : 480 0



## VES01815 3

### 5 5

Clien t Lo t #... : H9L14040 2 Dat e Sampled... : 12/10/0 9 DUPLICAT E PARA M RESUL T RESUL T Hydroge nchlorid e 3240 0 3160 0 SAMPL E DUPLICAT E EVALUATIO N REPOR T Genera l Chemistr y Wor k Orde r #... : LQ2RV-SM P LQ2RV-DUP Dat e Received.. : 12/11/0 9 Matrix . AI R

UNIT S RPD

RP D LIMI T METHO D PREPARATION - PRE P

ANALYSI S DAT E BATC H # S D Lot-Sampl e # : H9L140402-00 5 u g 2. 4 (0-20 ) KNO X0050/26 A

Mod 12/14/0 9 934912 2 Dilutio nFactor : 39903.0 5



## VES01815 4

### 5 9

H9L14040 2 12/08/0 9 DUPLICAT E RESUL T SAMPL E DUPLICAT E EVALUATION REPOR T Genera l C_emistr y • Wor k Orde r #... i LQ2R3-SMP LQ2R3-DUP Dat e Received.. : 12/11/0 9

N D Matrix . AI R

UNIT S RP D RP D LIMI T METHO D PREPARATION - PRE P

ANALYSI S DAT E BATC H # S D Lot-Sampl e # : H9L140402-00 9 u g 0 (0-20 ) KNO X0050/26 A

Mo d 12/15/0 9 935015 3 Dilution . Factor : 100 0



## VES01815 5

# Metho d 0023 A

VES01815 6

# •Vist a Analytica l Laborator y


### Decembe r27,200 9 

### VistaProjec

tLD. : 3227

5 Mr . Jeffre y Gorma n AECO M Environmen t 501 5 Campuswoo d Driv e Suit e 10 4 Eas tSyracuse , N Y 13057-4232 Dea rMr . Gorman , Enclose d ar

e th e result s fo rth e fou rMM 5 samples receive d a tVist aAnalytica l Laborator y o n Decembe r12

, 200 9 underyou rProjectNam e "60133216" . Thes e samples wer e extracte d an

d analyze d usin g Metho d 0023 A fo rtetra-through-oct achlorinate d dioxin s an d furans . Th e fron tan d back halve s wer

e extracted an d analyze d separatel y fo rsamples Rl , R 2 and R3 . A standard turnaround time wa

s provide d fo rthis work . Th e followin g repor tconsist

s o f aSampl e Inventor

y (Sectio n I) , Analytica l Result s (Sectio n II

) an d the Appendix , whic h contains th e chain-of-custody , alis to f dat aqualifier s an

d abbreviations , Vista' s curren

tcertifications , and copie s o f th e ra w dat a(i f requested) . Vist aAnalytica l Laboratory i s committe d t o servin g yo u effectively . I f yo u requir

e additiona l information , pleas e contac tme a t916-673-1520 o rb y emai l a tmmaier@vista-analytical.com . Than kyo u fo rchoosin g Vist aa s par to f you ranalytical suppor tteam . Sincerely ,
MarthaM . Maie r Laboratory Directo r Vista Anaiyiicai Laboratory certifies thai Ihe report herein meets all

Ihe requirements set

forth by NELAC

forthose applicable y , test methods. Results relate only lo ihe samples as received by the laboratory. This report should not be reproduced

except in full i-i. without

the written approval

cf Vista Analytical

Laboratory.

Vist a Analytica l Laborator y| H04WindfieldWa y| E l Dorad o Hills , C A9576 2 I ph : 916-673-152 0 | fx : 916-673-010 6 I wwww.vista-analytical.co m 

### Project 3227

5 Pag e 1 o f 1 8 

### VES01815 7

# Wist a

Sectio n I : Sampl

e Inventor

y Repor t Dat e Received : 12/12/200 9 Projec tNo. : 3227 5 Projec tName : 6013321 6
Lab . Sampl

e I D Clien

tSampl e I D Componen tI D 

### 001 CPT-U2-M23A-XAD-R 1 BH

R XA D 00 2 CPT-U2-M23A-PF-R 1 FH

R FILTER 00 3 CPT-U2-M23A-XAD-R 2 BH

R XA D 00 4 CPT-U2-M23A-PF-R 2 FH

R FILTE R 005 CPT-U2-M23A-XAD-R 3 BH

R XA D 00 6 CPT-U2-M23A-PF-R 3 FH

R FILTER 00 7 CPT-U2-M23A-U2-F B ACE/MeC12/TO L FILTER XA D

SmpinvgnmmS.rpI



### Projec t 3227 5 Pag e 2 of 1 8 

## VES01815 8

# Wist a

SECTIO N n

Projec t 32275 Pag e 3 o f 1 8 VES01815 9

## Avist a
Metho d Blan k 

### Metho d 0023 A Matrix : MM 5 Q C Batc h No. : 264 6 L a b Sample : 0-MB00 1 Sampl e Size : Sampl e Date Extracte d 21-Dec-0 9 Dat e Analyze d DB-5 : 23-Dec-0 9 Dat e Analyze d DB-225 : N A Analyt e Cone . (pg/Sample ) D L a EMP C bQualifier s Labele d Standar d 

### % R LCL-UCL dQualifier s 2,3,7,8-TCD D N D 2.6 9 I S 13C-2,3,7,8-TCD D 94. 7 40-13 5 1,2,3,7,8-PeCD D N D 4.0 0 13C-1,2,3,7,8-PeCD D 98. 9 40 - 13 5 1,2,3,4,7,8-HxCD D N D 6.5 8 13C-l,2,3,6,7,8-HxCD D 79. 8 40-13 5 1,2,3,6,7,8-HxCD D N D 5.1 7 13C - 1,2,3,4,6,7,8-HpCD D 10 5 40 - 13

5 1,2,3,7,8,9-HxCD D N D 5.43 13C-OCD D 11 1 40-13 5 1,2,3,4,6,7.8-HpCD D N D 3.0 9 13C-2,3,7,8-TCD F 96. 6 40 - 13 5 OCD D N D : 5.1 0 13C-l,2,3,7,8-PeCD F 108 40-13 5 2,3,7,8-TCD F N D 2.3 6 13C-l,2,3,6,7,8-HxCD F 75. 7 40 - 13 5 1,2,3,7,8-PeCD F N D 2.7 5 13C-l,2,3,4,6,7,8-HpCD F 95. 1 40 - 13 5 2,3,4,7,8-PeCD F N D 2.9 1 13C-OCD F 99. 4 40 - 13 5 1.2,3,4,7,8-HxCD F N D 2.0 5 P S 37Cl-2,3,7,8-TCD D 107 70-13 0 1,2,3,6,7,8-HxCD F N D 1.6 3 13C-2,3,4,7,8-PeCD F 10 2 70 - 130 2,3,4,6,7,8-HxCD F N D 2.0 6 13C-l,2,3,4,7,8-HxCD D 12 4 70 - 130 1,2,3,7,8,9-HxCD F N D 2.3 1 13C-l,2,3,4,7,8-HxCD F 12 6 70 - 13

0 1,2,3,4,6,7,8-HpCD F N D 2.7 4 13C-l,2,3,4,7,8,9-HpCD F 11 0 70-13 0 1,2,3,4,7.8,9-HpCD F - N D 3.5 2 A S 13C-l,2.3,7,8,9-HxCD F 10 7 40 - 13

5 OCD F N D 6.3 3 Total s Toxi c Equivalen tQuotien t(TEQ ) Dat a e Tota l TCD D N D 2.6 9 T E Q (Min-Max) : 0 - 9.1 5 Tota l PeCD D N D 4.0 0 Tota l HxCD D N D 5.6 7 a . Sampl e specifi c estimate

ddetection limit . Tota l HpCD D N D 3.0 9 b . Estimatedmaximu mpossible concentration . Tota l TCD F N D 2.3 6 c . Metho ddetection limit . Tota l PeCD F N D 2.83 d . Lower control limi t

- uppe r contro l limit . Tota l HxCD F N D 1.9 8 e . TE Q base do n (1989 ) Internationa

l Toxi c Equivalen

t Factors (ITEF) . Tota l HpCD F N D 3.0 8 Analyst : MA S Approve dBy : Willia m J . Luksembur g 27-Dec-200 9 07:0 8

3227 5 Pag e 4 o f 1 8 

## VES01816 0OP RResult s 

### Metho d 0023 A Matrix : MM 5 Q C Balc hNo. : 264 6 Lab Sample : 0-OPR00 1 Sampl e Size : Sampl e Dat e Extracted : 21-Dec-0 9 Dat e Analyze d DB-5 : 23-Dec-0 9 Date Analyze d DB-225 : N A Analyt e Spik e Cone . Cone . (ng/mL ) O P RLimit s Labele d Standar d % R LCL-UC L Qualifie r 2,3,7,8-TCD D 2.5 0 2.3 8 : 1.75-3.2 5 I S 13C-2,3,7,8-TCD D 10 3 4 0 - 13

5 1,2,3,7,8-PeCD D 12. 5 11.5 8.75 - 16.25 13C-l,2,3,7,8-PeCD D 11 9 40 - 13 5 1,2,3,4,7,8-HxCD D 12. 5 14. 9 8.75 - 16.25 13C-l,2,3,6,7,8-HxCD D 88: 7 4 0 - 13 5 1,2,3,6,7,8-HxCD D 12.5 11.2 8.75 - 16.25 13C-l,2,3,4,6,7,8-HpCD D 11 9 4 0 - 13 5 1,2,3,7,8,9-HxCD D 12. 5 12. 8 8.75 - 16.2 5 13C-OCD D 12 6 4 0 - 13

5 1,2,3,4,6,7,8-HpCD D 12.5 11.5 8.75 - 16.2 5 13C-2,3,7,8-TCD F 10 3 4 0 - 13

5 OCD D 25. 0 22. 3 17.5-32. 5 13C-l,2,3,7,8-PeCD F 12 2 40-13 5 2,3,7,8-TCD F 2.5 0 2.3 9 1.75-3.2 5 13C-l,2,3,6,7,8-HxCD F 90. 1 40-13 5 1,2,3,7,8-PeCD F 12. 5 11. 9 8.75 - 16.25 13C-l,2,3,4,6,7,8-HpCD F 107 40-13 5 2,3,4,7,8-PeCD F 12.5 11.4 8.75 - 16.25 13C-OCD F 11 2 40 - 13 5 1,2,3,4,7,8-HxCD F 12.5 14.7 8.75 - 16.25 A S 13C-l,2,3,7,8,9-HxCD F 10 4 4 0 - 13

5 1,2,3,6,7,8-HxCD F 12.5 12. 0 8.75 - 16.25 2,3,4,6,7,8-HxCD F 12.5 13. 1 8.75 - 16.2 5 1,2,3,7,8,9-HxCD F 12.5 13.0 8.75 - 16.25 1,2,3.4,6,7,8-HpCD F 12. 5 11.5 8.75 - 16.25 1,2,3,4,7,8,9-HpCD F 12. 5 12. 4 8.75 - 16.2 5 OCD F 25. 0 22. 9 17.5-32. 5 Analyst : MA S Approve dBy : Willia m J . Luksembur g 27-Dec-200 9 07:0 8

Project3227 5 Pag e 5 o f 1 8 

## VES01816 1

# V vist a Sampl e ID : CPT-U2-M23A-XAD-R 1 

### Metho d 0023 A Clien tDat a Sampl e Dat a Laborator y Dat a Name : AECO M Environmen t Project : 6013321 6 Dat e Collected : 8-Dec-0 9 Time Collected : N A Matrix : Sampl e Size : M M 5

Sampl e La

b Sample : 32275-00 1 Q C Batc hNo. : 264 6 Dat e Analyze dDB-5 " 23-Dec-0 9 Dat e Received : 12-Dec-0 9 Dat e Extracte d21-Dec-0 9 Date s Analyze dDB-22S : 24-Dec-0 9 Analyt e Cone . (pg/Sample ) D L a EMPC b Qualifier s Labele d Standar d % R LCL-UCL dQualifier s 2,3,7,8-TCD D 4.1 4 J I S 13C-2,3,7,8-TCD D 99. 1 40-13 5 1,2,3,7,8-PeCD D 21. 1 J 13C-l,2,3,7,8-PeCD D 10 5 4 0 - 13

5 1,2,3,4,7,8-HxCD D 27: 0 J 13C-l,2,3,6,7,8-HxCD D 89. 4 40-13 5 1,2,3,6,7,8-HxCD D 49. 0 J 13C-1,2,3,4,6,7,8-HpCD D 11 6 40-13 5 1,2,3,7,8,9-HxCD D 31. 0 J 13C-OCD D 12 6 40-13 5 1,2,3,4,6,7,8-HpCD D 203 13C-2,3,7,8-TCD F 10 5 40-13 5 OCD D 167 13C-l,2,3,7,8-PeCD F 11 7 40-13 5 2,3,7,8-TCD F 22. 5 13C-l,2 7 3,6,7,8-HxCD F 82. 6 40 - 13 5 •1,2,3,7,8-PeCD F 32. 5 J 13C-1,2,3,4,6,7,8-HpCD F 10 5 40-13 5 2,3,4,7,8-PeCD F 10 4 13C-OCD F 11 4 40-13 5 1,2,3,4,7,8-HxCD F 55. 1 E S 37Cl-2,3,7,8-TCD D 89. 0 70-13 0 1,2,3,6,7,8-HxCD F 47. 0 L P 13C-2,3,4,7,8-PeCD F 89. 7 70 - 13 0 2,3,4,6,7,8-HxCD F 96. 0 13C-1,2,3,4,7,8-HxCD D 101 70-13 0 1,2,3,7,8,9-HxCD F 24. 8 J 13C-l,2,3,4,7,8-HxCD F 10 6 70-13 0 1,2,3,4,6,7,8-HpCD F 11 4 13C - 1,2,3,4,7,8,9-HpCD F 93. 2 70 - 13 0 1,2,3,4,7,8,9-HpCD F 22. 5 J A S !3C-l,2,3,7,8,9-HxCD F 10 8 40-13 5 OCD F 42. 5 J Total s Toxi c Equivalen tQuotieii t(TEQ ) Dat a e Tota l TCD D 253 0 254 0 T E Q (Min-Max) : 107-10 7 Tota l PeCD D 193 0 Tota l HxCD D 454 0 a. Sampl e specifi c estimate

ddetection limit . Tota l HpCD D 45 7 b . Estimatedmaximu mpossible concentration . Tota l TCD F 147 0 151 0 P c . Metho ddetection limit . Tota l PeCD F 1120 P d . Lower contro l limi t

- uppe r contro l limit . Tota l HxCD F 66 9 P e . TE Q base do n(1989 ) Internationa

l Toxi c Equivalen

t Factors (ITEF) . Tota l HpCD F 20 2 Analyst : MA S Approve dBy : Willia m J . Luksembur g 27-Dec-200 9 07:08

ec t3227 5 Pag e 6 o f 1 8 

## VES01816 2Sampl e 11) : 

### CPT -U2-M23A -PF -R 1 Metho d 0023 A Clien tDat a Sampl e Dat a Laborator y Dat a Name : AECO M Environmen t Project : 6013321 6 Dat e Collected : 8-Dec-0 9 Tim e Collected : N A Matrix : Sample Size : M M 5

Sampl e La

b Sample : 32275-00 2 Q C BatchNo. : 264 6 Dat e Analyze dDB-5 : 23-DCC-0 9 Dat e Received : 12-Dec-0 9 Dat e Extracted : 21-Dec-0 9 Dat e Analyze dDB-22 5 Ny \ Analyt e Cone . (pg/Sample ) D L a E!YIPC b Qualifier s Labele d Standar d % R LCL-UCL dQualifier s 2,3,7,8-TCD D N D 2.8 7 I S 13C-2,3,7,8-TCD D 10 2 40 - 13

5 1,2,3,7,8-PeCD D N D 4.1 3 13C-l,2,3,7,8-PeCD D 106 40 - 13 5 1,2,3,4,7,8-HxCD D N D 5.22 13C-l,2,3,6,7,8-HxCD D 85. 7 40 - 13 5 1,2,3,6,7,8-HxCD D N D 4.1 1 13C-1,2,3,4,6,7,8-HpCD D 115 40 - 13 5 1,2,3,7,8,9-HxCD D N D 4.3 1 13C-OCD D 12 1 40-13 5 1,2,3,4,6,7,8-HpCD D N D 8.0 3 13C-2,3,7,8-TCD F 10 6 40 - 13

5 OCD D N D 8.8 9 13C-l,2,3,7,8-PeCD F 11 6 4 0 - 13 5 2,3,7,8-TCD F N D 2.5 8 13C-1,2,3,6,7,8-HxCD F 80. 6 40 - 13 5 1 2.3,7,8-PeCD F N D 3.9 2 13C-l,2,3,4,6,7,8-HpCD F 10 3 40-13 5 2,3,4,7,8-PeCD F N D 4.1 5 13C-OCD F 109 4 0 - 13 5 1,2,3,4,7,8-HxCD F N D 3.9 3 ES 37Cl-2,3,7,8-TCD D N A 70-13 0 1,2,3,6,7,8-HxCD F N D 4.6 0 13C-2,3,4,7,8-PeCD F N A 70-13 0 2,3,4,6,7,8-HxCD F N D 1 ,6 8 13C-l,2,3,4,7,8-HxCD D N A 70 - 130 1 ,2,3,7,8,9-HxCD F N D 1 .8 9 13C-l,2,3,4,7,8-HxCD F N A 70-13 0 1,2,3,4,6,7,8-HpCD F N D 3.1 1 13C-1,2,3,4,7,8,9-HpCD F N A 70-13 0 1.2,3,4,7,8.9-HpCD F N D 4.1 0 M 13C-l,2,3,7,8,9-HxCD F 11 0 40-13 5 OCD F N D 6.3 3 Total s Toxi c Equivalen tQuotien t(TEQ ) Dat a e Tota l TCD D N D 2.8 7 T E Q (Min-Max) : 0-10. 2 Tota l PeCD D N D 4.1 3 Tota l HxCD D N D 8.34 a . Sampl e specifi c estimate

ddetection limit . Tota l HpCD D N D 8.0 3 b . Estimatedmaximu mpossible concentration . Tota l TCD F N D 2.9 7 c . Metho ddetection limit . Tota l PcCD F N D 4.03 d . Lowe r contro l limi t

- uppe r contro l limit . Tota l HxCD F N D 5.72 e. TE Q base don(1989 ) Internationa

l Toxi c Equivalen

t Factors (ITEF ) Tota l HpCD F N D 3.1 1 Analyst : MA S Approve dBy : Willia mJ Luksembur g 27-Dec-200 9 11:3 4
Project3227 5 Pag e 7 o f 1 8 

## VES01816 3Sampl e ID : 

### CPT-U2-M2 3 A-XAD-R 2 Metho d 0023 A Clien tDat a Sampl e Dat a Laborator y Dat a Name : AECO M Environmen t Project . 6013321 6 Dat e Collected : 9-DeC-0 9 Tim e Collected : N A Matrix : Sampl e Size : M M 5

Sampl e Lab Sample : 32275-00 3

Q C BatchNo. : 264 6 Dat e Analyze dDB-5 : 23-Dec-0 9 Dat e Received : ] 2-Dec-0 9 Dat e Extracted : 2 1 -Dec-0 9 Dale s Analyze dDB-225 : 24-Dec-0 9 Analyt e Cone . (pg/Sample ) D L a EMPC b Qualifier s Labele d Standar d % R LCL-UCL dQualifier s 2,3,7,8-TCD D N D 3.3 4 I S 13C-2,3,7,8-TCD D 95. 0 4 0 - 13 5 1,2,3,7,8-PeCD D 18. 6 J 13C-1,2,3,7,8-PeCD D 10 5 4 0 - 13

5 1,2,3,4,7,8-HxCD D 21. 9 J 13C-1,2,3,6,7,8-HxCD D 90. 1 40-13 5 1,2,3,6,7,8-HxCD D 43. 2 J 13C-1,2,3,4,6,7,8-HpCD D 11 7 40 - 13 5 1,2,3,7,8,9-HxCD D 24. 7 J 13C-OCD D 12 5 40-13 5 1,2,3,4,6,7,8-HpCD D 194 13C-2,3,7,8-TCD F 10 7 40 - 13

5 OCD D 182 13C-l,2,3,7,8-PeCD F 11 4 40 - 13 5 2,3,7,8-TCD F 15. 0 13C-l,2,3,6,7,8-HxCD F 84. 8 40-13 5 1,2,3,7,8-PeCD F 21. 8 J 13C-1,2,3,4,6,7,8-HpCD F 106 4 0 - 135 2,3,4,7,8-PeCD F 56. 3 13C-OCD F 11 3 40-13 5 1,2,3,4,7,8-HxCD F 46. 1 i 37Cl-2,3,7,8-TCD D 102 70-13 0 1,2,3,6,7,8-HxCD F 32. 8 L P 13C-2,3,4,7,8-PeCD F 101 70-13 0 2,3,4,6,7,8-HxCD F 55. 0 13C - 1,2,3,4,7,8-HxCD D 12 0 70-13 0 1,2,3,7,8,9-HxCD F 15. 3 J 13C-l,2,3,4,7,8-HxCD F 12 3 70-13 0 1,2,3,4,6,7,8-HpCD F 13 3 13C-1,2,3,4,7,8,9-HpCD F 11 6 70-13 0 1,2,3,4,7,8,9-HpCD F 19. 2 J A S 13C-l,2,3,7,8,9-HxCD F 106 40-13 5 OCD F 73. 0 J Total s Toxi c Equivalen tQuotien t(TEQ ) Dat a e Tota l TCD D 1960 198 0 T E Q (Min-Max) : 67. 7 - 71. 0 Tota l PeCD D 1420 Tota l HxCD D 344 0 a . Sampl e specifi c estimate

ddetectio n limi t Tota l HpCD D 41 1 b . Estimatedmaximu mpossible concentration . Tota l TCD F 74 0 745 P c . Metho ddetection limit . Tota l PeCD F 59 0 59 6 P d . Lower contro l limi t

- uppe r contro l limit . Tota l HxCD F 42 2 P e. TE Q base do n (1989 ) Internationa

l Toxi c Equivalen

t Factors (ITEF) . Tota l HpCD F 21 4 Analyst : MA S Approve dB y Willia mJ . Luksembur g 27-Dec-200 9 07:0 8

ec t 3227 5 Pag e 8 o f 18 

## VES01816 4Sampl e ID : CPT-U2-M23A-PF-R 2 

### Metho d 0023 A Clien t Dat a Sampl e Dat a Laborator y Dat a Name : .AECO M Environmen t Project : 601332 ] 6 Dat e Collected : 9-Dec-0 9 Time Collected : N A Matrix : Sample Size : M M 5

Sampl e Lab Sample : 32275-00 4

Q C Batc hNo. : 264 6 Dat e Analyze d DB-5 . 23-Dec-0 9 Dat e Received : 12-Dec-0 9 Dat e Extracted : 21-Dec-0 9 Dat e Analyze dDB-225 : Analyt e Cone . (pg/Sainple ) D L a EMPC b Qualifier s Labele d Standar d % R LCL-UCL dQualifier s 2,3,7,8-TCD D N D 2.2 7 I S 13C-2,3,7,8-TCD D 10 7 40-13 5 1,2,3,7,8-PeCD D N D 3.3 4 13C-l,2,3,7,8-PeCD D 113 40 - 13 5 1,2,3,4,7,8-HxCD D N D 7.6 8 13C-l,2,3,6,7,8-HxCD D 88. 4 40-13 5 1,2,3,6,7,8-HxCD D N D 6.04 13C-l,2,3,4,6,7,8-HpCD D 12 4 40 - 13

5 1,2,3,7,8,9-HxCD D N D 6.3 4 13C-OCD D 13 2 40 - 13

5 1,2,3,4,6,7,8-HpCD D 5.4 1 J 13C-2,3,7,8-TCD F 10 8 40 - 13

5 OCD D 17. 6 J 13C-l,2,3,7,8-PeCD F 12 3 40 - 13

5 2,3,7,8-TCD F N D 3.8 4 13C-1,2,3,6,7,8-HxCD F 82. 7 40-13 5 1,2,3,7,8-PeCD F N D 4.3 3 13C-1,2,3,4,6,7,8-HpCD F 107 40 - 13 5 2,3,4,7,8-PeCD F N D 4.5 8 13C-OCD F 11 8 40 - 13 5 1,2,3,4,7,8-HxCD F N D 3.1 1 P J 37Cl-2,3,7,8-TCD D N A 70-13 0 1,2,3,6,7,8-HxCD F N D 2.4 8 13C-2,3,4,7,8-PeCD F N A 70-13 0 2,3,4,6,7,8-HxCD F N D 3:1 3 13C-1,2,3,4,7,8-HxCD D N A 70 - 130 1.2,3,7,8,9-HxCD F N D 1.8 5 13C-l,2,3,4,7,8-HxCD F N A 70 - 130 1,2,3,4,6,7,8-HpCD F 9.3 5 . 1 13C-1,2,3,4,7,8,9-HpCD F N A 70 - 13 0 1,2,3,4,7,8,9-HpCD F N D 3.5 6 A S 13C-l,2,3,7,8,9-HxCD F 11 0 40 - 13 5 OCD F 5.7 5 1 Total s Toxi c Equivalen tQuotien t(TEQ ) Dat a e Tota l TCD D N D 3.8 6 T E Q (Min-Max) ; 0.17 1 - 10. 1 Tota l PeCD D N D 6.3 5 Tota l HxCD D 11. 2 a . Sampl e specifi c estimate

ddetection limit . Tota l HpCD D 5.4 1 b . Estimate dmaximu mpossible concentration . Tota l TCD F 3.0 9 5.70 c . Metho ddetection limit . Tota l PeCD F N D 4.4 5 d . Lower contro l Hmi

t - uppe r control limit . Tota l HxCD F N D 6.4 5 e. TE Q base do n(1989 ) Internationa

l Toxi c Equivalen

t Factors (ITEF) . Tota l HpCD F 9.3 5 Analyst : MA S Approve dBy : Willia m J . Luksembur g 27-Dec-200 9 1 1 :34
Project3227 5 Page 9 o f 1 8 

## VES01816 5

### V vist a Sampl e ro. 

### CPT-U2-M23A-XAD-R 3 Metho d 

### 0023 A Clien tDat a Sampl e Dat a Laborator y Dat a Name : AECO M Environmen t Project : 6013321 6 Dal e Collected : 10-Dec-0 9 Tim e Collected : N A Matrix : Sampl e Size : MM 5

Sampl e La

b Sample : 32275-00 5 Q C Batc hNo. : 264 6 Dat e Analyze dDB-5 : 23-Dec-0 9 Dat e Received : 12-Dec-0 9 Dat e Extracted : 21-Dec-0 9 Date s Analyze dDB-225 : 24-Dec-0 9 Analyt e Cone . (pg/SampIe ) D L a EMPC b Qualifier s Labele d Standar d % R LCL-UCL dQualifier s 2,3,7,8-TCD D N D 4.8 0 I S 13C-2,3,7,8-TCD D 99. 3 40 - 13 5 1 ,2,3,7,8-PeCD D 17. 1 J 13C -l ,2,3,7,8-PeCD D 10 3 4 0 - 13

5 1,2,3,4,7,8-HxCD D , : NT ) 17. 7 13C-l,2,3,6,7,8-HxCD D 86. 6 40 - 13 5 1 ,2,3,6,7,8-HxCD D 32. 2 J 13C-1,2,3,4,6,7,8-HpCD D 113 40-13 5 1,2,3,7,8,9-HxCD D 23. 7 J 13C-OCD D 11 8 40-13 5 1 ,2,3,4,6,7,8-HpCD D 14 9 13C-2,3,7,8-TCD F 10 5 40 - 13

5 OCD D 11 7 13C -l ,2,3,7,8-PeCD F 109 40 - 13 5 2,3,7,8-TCD F 14. 1 13C - 1,2,3,6,7,8-HxCD F 82. 6 40 - 13 5 1,2,3,7,8-PeCD F 16. 6 J 13C-1,2,3,4,6,7,8-HpCD F 10 1 40-13 5 2,3,4,7,8-PeCD F 50. 1 13C-OCD F U l 40-13 5 1,2,3,4,7,8-HxCD F 25. 9 J £ S 37Cl-2,3,7,8-TCD D 97. 4 70-13 0 1,2,3,6,7,8-HxCD F 23. 7 L P 13C-2,3,4,7,8-PeCD F 10 3 70 - 130 2,3,4,6,7,8-HxCD F 44. 0 J 13C-1,2,3,4,7,8-HxCD D 12 2 7 0 - 130 1 .2,3,7,8,9-HxCD F 11. 2 J 13C -l ,2,3,4,7,8-HxCD F 12 0 70 - 130 1,2,3,4,6,7,8-HpCD F 63. 5 13C -l ,2,3,4,7,8,9-HpCD F 11 5 70-13 0 1,2,3,4,7,8,9-HpCD F 11. 6 J A S 13C -l ,2,3,7,8,9-HxCD F 10 8 40-13 5 OCD F 21. 0 J Total s Toxi c Equivalen tQuotien t(TEQ ) Dat a c Tota l TCD D 1880 T E Q (Min-Max) : 54. 2 - 60. 8 Tota l PeCD D 151 0 Tota l HxCD D 273 0 275 0 a . Sampl e specifi c estimate

ddetection limit . Tota l HpCD D 31 9 b . Estimatedmaximu mpossible concentration . Tota l TCD F 68 8 P c . Metho ddetection limit . Tota l PeCD F 50 1 51 6 P d . Lower contro l limi t

- uppe r contro l limit . Tota l HxCD F 31 3 P e . TE Q base don (1989 ) Internationa

l Toxi c Equivalen

t Factors (ITEF) . Tota l HpCD F 11 1 Analyst : MA S Approve dBy : Willia mJ . Luksembur g 27-Dec-200 9 07:0 8
Projec t3227 5 Pag e 1 0 o f 1 8 

## VES01816 6

### i i ' 

# V vist a Sampl e BD : CPT-U2-M23A-PF-R 3 

### Metho d 0023 A Clien tDat a Sampl e Dat a L abor ator y Dat a Name : AECO M Environmen t Project : 6013321 6 Dat e Collected : 10-Dec-0 9 Tim e Collected : N A Matrix : Sample Size : M M 5

Sampl e La

b Sample : 32275-00 6 Q C Batc hNo. : 264 6 Dat e Analyze dDB -5 : 23-Dec-0 9 Dat e Received : 12-Dec-0 9 Dat e Extracted : 21-Dec-0 9 Dat e Analyze dDB-22 5 N A Analyt e Cone . (pg/Sample ) D L a EMPC b Qualifier s Labele d Standar d % R LCL-UCL dQualifier s 2,3,7,8-TCD D N D 2.3 7 I I 13C-2,3,7,8-TCD D 10 7 40-13 5 1,2,3,7,8-PeCD D N D 3.7 0 13C-1,2,3,7,8-PeCD D 12 0 40 - 13

5 1,2,3,4,7,8-HxCD D N D 4.9 8 13C-1,2,3,6,7,8-HxCD D 88. 1 40 - 13 5 1,2,3,6,7,8-HxCD D N D 3.9 2 13C-l,2,3,4,6,7,8-HpCD D 12 2 40 - 13

5 1,2,3,7,8,9-HxCD D N D 4.1 1 13C-OCD D 13 1 4 0 - 135 1,2,3,4,6,7,8-HpCD D N D 8.70 13C-2,3,7,8-TCD F 10 5 40-13 5 OCD D 14. 2 J 13C-l,2,3,7,8-PeCD F 141 40-13 5 H 2,3,7,8-TCD F N D 3.0 2 13C-l,2,3,6,7,8-HxCD F 83. 1 40 - 13 5 1,2,3,7,8-PeCD F K D 3.5 2 : 13C-1,2,3,4,6,7,8-HpCD F 107 40-13 5 2,3,4,7,8-PeCD F N D 3.7 3 13C-OCD F 12 0 40-13 5 1,2,3,4,7,8-HxCD F N D 2.6 1 P S 37Cl-2,3,7,8-TCD D N A 70-13 0 1,2,3,6,7,8-HxCD F N D 1.5 7 13C-2,3,4,7,8-PeCD F N A 70 - 130 2,3,4,6,7,8-HxCD F N D 1.9 8 13C-l,2,3,4,7,8-HxCD D N A 7 0 - 13 0 1.2,3,7,8,9-HxCD F N D 2.22 13C-l,2,3,4,7,8-HxCD F N A 70 - 13 0 1,2,3,4,6,7,8-HpCD F 6.4 9 J 13C-l,2,3,4,7,8,9-HpCD F N A 7 0 - 130 1,2,3,4,7,8,9-HpCD F N D 2.2 8 A S 13C-l,2,3,7,8,9-HxCD F 10 9 40-13 5 OCD F N D 7.4 4 Total s Toxi c Equivalen tQuotien t(TEQ ) Dat a e Tota l TCD D N D 3.9 0 T E Q (Min-Max) : 0.079 1 - 8.8 9 Tota l PeCD D N D 6.85 Tota l HxCD D 7.84 a . Sampl e specifi c estimate

ddetection limi t Tota l HpCD D N D 8.70 b . Estimatedmaximu mpossible concentration . Tota l TCD F N D 3.65 c . Metho ddetectio n limit . Tota l PeCD F N D 3.6 2 d . Lower contro l limi t

- uppe r contro l limit . Tota l HxCD F 3.0 4 e , TE Q base

do n(1989 ) Internationa

l Toxi c Equivalen

t Factors (ITEF) . Tota l HpCD F 6.4 9 Analyst : MA S Approve dBy : Willia mJ . Luksembur g 27-Dec-200 9 U :3 4
Project3227 5 Pag e I I o f I S 

## VES01816 7

# w V vist a Sampl e ID : 

### CPT-TJ2-M23A-U2-F B Metho d 0023 A Clien tDat a Sampl e Dat a Laborator y Dat a Name : AECO M Environmen t Project : 6013321 6 Dat e Collected : 10-Dec-0 9 Time Collected : N A Matrix : Sampl e Size : M M 5

Sampl e Lab Sample : 32275-00 7

Q C Batc hNo. : 264 6 Dat e Analyze dDB-5 . 23-Dec-0 9 Dat e Received : 12-Dec-0 9 Dat e Extracted : 2 1 -Dec-0 9 Dat e Analyze dDB-225 : N A Analyt e Cone . (pg/Sainple ) D L 2 EMPC b Qualifier s Labele d Standar d % R LCL-UCL dQualifier s 2,3,7,8-TCD D N D 2.6 0 I S l3C-2,3,7,8-TCD D 10 6 40-13 5 1,2,3,7,8-PeCD D N D 4.1 0 13C - 1,2,3,7,8-PeCD D 11 1 4 0 - 13 5 1,2,3,4,7,8-HxCD D N D 5.6 2 13C-l,2,3,6,7,8-HxCD D 87. 6 4 0 - 13 5 1,2,3,6,7,8-HxCD D N D 4.4 2 13C-1,2,3,4,6,7,8-HpCD D 11 9 40 - 13 5 1,2,3,7,8,9-HxCD D N D 4.6 4 13C-OCD D 12 5 40 - 13

5 1,2,3,4,6,7,8-HpCD D N D 2.8 0 13C-2,3,7,8-TCD F 10 3 40 - 13

5 OCD D N D 6.1 0 13C-l,2,3,7,8-PeCD F 12 0 40-13 5 2,3,7,8-TCD F N D 1.96 13C-1,2,3,6,7,8-HxCD F 86. 1 40-13 5 1,2,3,7,8-PeCD F N D 2.9 7 13C-l,2,3,4,6,7,8-HpCD F 108 40-13 5 2,3,4,7,8-PeCD F N D 3.1 5 13C-OCD F 11 5 40 - 13 5 1,2,3,4,7,8-HxCD F N D 2.5 4 ES 37Cl-2,3,7,8-TCD D 99. 5 70 - 130 1,2,3,6,7,8-HxCD F N D 2.0 2 13C-2,3 : 4,7,8-PeCD F 10 4 70 - 13

0 2,3,4,6,7,8-HxCD F N D 2.5 5 13C-l,2,3,4,7,8-HxCD D 129 70 - 130 1,2,3,7,8,9-HxCD F N D 2.8 7 13C-l,2,3,4,7,8-HxCD F 12 5 70-13 0 1,2,3,4,6,7,8-HpCD F N D 1.7 4 13C-1,2,3,4,7,8,9-HpCD F 113 70-13 0 1,2,3,4,7,8,9-HpCD F N D 2.23 A § 13C-l,2,3,7,8,9-HxCD F 11 0 40-13 5 OCD F N D 6.7 0 Total s Toxi c Equivalen tQuotien t(TEQ ) Dat a e Tota l TCD D N D 2.6 0 T E Q (Min-Max) : 0-9.1 2 Tota l PeCD D N D 4.1 0 Tota l HxCD D N D 4.8 4 a. Sampl e specifi c estimate

ddetection limit . Tota l HpCD D N D 2.8 0 b Estimate dmaximu mpossible concentration . Tota l TCD F N D 1.9 6 c . Methoddetectio n limit . Tota l PeCD F N D 3.0 6 d . Lower contro l limi t

- uppe r contro l limit . Tota l HxCD F N D 2.4 6 e. TE Q base do n (1989 ) Internationa

l Toxi c Equivalen

t Factors (ITEF) . Tota l HpCD F N D 1.96 Analyst : MA S Approve dBy : Willia m J . Luksembur g 27-Dec-200 9 07:08

ect3227 5 Page 1 2 o f 1 8 

## VES01816 8

### Vist a

APPENDI X

Projec t3227 5 Pag e 1 3 o f 1 8 

## VES01816 9

# ^VlSt Q DAT A QUALIFIER S & ABBREVIATION S

B Thi s compoun d wa s als o detected i n th

e metho d blank . D Dilutio n E Th e amoun tdetected is above th e Hig h Calibratio n Limit . PTh e amoun treporte d is the maximu m possibl e concentratio n due t o possibl e chlorinate d diphenylethe rinterference . H Recover y wa s outsid e laborator y acceptance limits . I Chemica l Interferenc e J Th e amoun tdetected i s belo w the Lo w Calibratio n Limit . * Se

e Cove rLette r Cone . Concentratio n D L Sample-specifi c estimated detectio n limi t IVED L Th e minimu m concentratio n o f asubstanc e tha tca n b e measure d an d reporte d wit h 99 % confidenc e tha tth e analyte concentratio n i s greate r tha n zer o i n th e matri x tested . EMP C Estimate d Maximu m Possibl e Concentratio n N A No tapplicabl e R L Reportin g Limi t- concentration s tha tcorrespon d t o lo w calibratio n poin t N D No tDetecte d T E Q Toxi c Equivalenc y
Unles s otherwis e noted , soli d sampl e result s are reporte d i n dr y weight. Tissu e samples ar e reporte d i n we tweight .

Projec t 3227 5 Pag e 1 4 o f 1 8 

## VES01817 0

## CERTIFICATION S Accreditin g Authorit y Certificat e Numbe r Stat e o f Alaska , DE C CA413-200 8 Stat e o f Arizon a AZ063 9 Stat e o f Arkansas , DE Q 08-043- 0 Stat e o f Arkansas , DO H Reciprocit ythroug h C A Stat e o f Californi a - NELA P Primar yA A 02102C A Stat e o f Colorad o N/ A Stat e o f Connecticu t PH-018 2 Stat e o f Florida , DE P E8777 7 Stat e o f Indian a Departmen t o f Healt h C-CA-0 2 Commonwealt h o f Kentuck y 9006 3 Stat e o f Louisiana , Healt h an d Hospital s LA0800 0 Stat e o f Louisiana , DE Q 0197 7 Stat e o f Main e 200802 4 Stat e o f Michiga n 993 2 Stat e o f Mississipp i Reciprocit ythroug h C A Nava l Facilitie s Engineerin g Servic e Cente r NFESC41 3 Stat e o f Nevad a CA004132007 A Stat e o f Ne wJerse y CA00 3 Stat e o f Ne wMexic o Reciprocit ythroug h C A Stat e o f Ne wYork , DO H 1141 1 Stat e o f Nort h Carolin a 0670 0 Stat e o f Nort h Dakota , DO H R-07 8 Stat e o f Oklahom a D991 9 Stat e o f Orego n CA200001-00 6 Stat e o f Pennsylvani a 68-0049 0 Stat e o f Sout h Carolin a 8700200 1 Stat e o f Tennesse e TN0299 6 Stat e o f Texa s T104704189-08-T X U.S
. Arm yCorp s o f Engineer s N/ A Stat e o f Uta h CA1640 0 Commonwealt h o f Virgini a 0001 3 Stat e o f Washingto n C128 5 Stat e o f Wisconsi n 99803616 0 Stat e o f Wyomin g 8TMS- Q

Projec t3227 5 Pag e 1 5 o f 1 8 

## VES01817 1

## Sampl e Traceabilit y Lis t \ AECO M
Site of Program ; VeoliaE S Tech Sampl e Date : |-2./«/e> 1 - \i\\a\o*\ ProjectLocation : Sauqet , I L Lab P O #' : Typ e o f Program : CP T •at e Shipped : ' tl/io/ol ' Laboratory : Vist aAnalytica

l E l Dorad o Hills , C A Project* : 6013321 6 Shippe r1 Steve n Mil o Recovery : .N- , »>

• rAoeni i /

Jef f Gorma n Laboratory : Vist aAnalytica

l E l Dorad o Hills , C A Proora m Office : Syracus e N Y Shippe r1 Steve n Mil o Recovery : .N- , »>

• rAoeni i /

Jef f Gorma n Laboratory : Vist aAnalytica

l E l Dorad o Hills , C A Program Contact : Jef f Gorma n 1 , 1 FedE x Ai rBil l # : Ite m Sample I D Code Sample Matri x Sampl e Descriptio

n Analytica l Parameter

s Specia l Instruction

s 1 CPT-U2-M23A-XAD-R 1 XAD 2 RESI N M2 3 XA D Resi

n Trap , Ru

n 1 PCDDs/PCDF s EPA 0023 A 2 CPT-U2-M23A-PF-R 1 FILTE R M2 3 P M Filter , Ru n 1 PCDDs/PCDF s EP A 0023 A 3 4 CPT-U2-M23A-XAD-R 2 XAD 2 RESI N M2 3 XAD Resi

n Trap , Ru

n 2 PCDDs/PCDF s EPA 0023 A 5 CPT-U2-M23A-PF-R 2 FILTE R M2 3 P M Filter , Ru n 2 PCDDs/PCDF s EPA 0023 A 6 7 CPT-U2-M23A-XAD-R 3 XAD 2 RESIN M2 3 XA D Resi

n Trap , Ru

n 3 PCDDs/PCDF s 8 CPT-U2-M23A-PF-R 3 FILTE R M2 3 P M Filter , Ru n 3 PCDDs/PCDF s 9 10 CPT-M23A-PF-U2-F B FILTE R Particulat e Filte rFiel d Blan k PCDDs/PCDF s EPA 0023 A 1 1 CPT-M23A-XAD-U2-F B XAD 2 RESI N Xad Resin Tra p Field Blan

k PCDDs/PCDF s EPA 0023 A 1 2 CPT-M23A-U 2 Fiel d Blan k Acetone/MeClaToluefl e M2 3 Blan k PCDDs/PCDF s EPA 0023 A 1 3 1 4 CPT-U2-M23A-FHR-R 1 Aceione/MaClj/Toiuen e M23 A Fron tHal f Rinse , Ru

n 1 PCDDs/PCDF s EP A 0023 A 1 5 C PT-U2-M23A-F H R-R 2 Acelone/MeCI^Toluen e M23 A Fron tHal f Rinse , Ru

n 2 PCDDs/PCDF s EPA 0023 A 1 6 CPT-U2-M23A-FHR-R 3 AcetoneyMeCI 2 Toluen e M23 A Fron tHal f Rinse , Ru

n 3 PCDDs/PCDF s EPA 0023 A 1 7 1 8 CPT-U2-M23A-BHR-R 1 Acelone/MeCl2/Toluen e M23 A Bac kHal f Rinse , Ru

n 1 PCDDs/PCDF s EP A 0023 A 1 9 CPT-U2-M23A-BHR-R 2 Acetone/MeCl2/To!uen e M23 A Bac kHal f Rinse , Ru

n 2 PCDDs/PCDF s EP A 0023 A 2 0 CPT-U2-M23A-BHR-R 3 Acetone/MeCI B Toluen e M23 A Bac kHal f Rinse , Ru

n 3 PCDDs/PCDF s EP A 0023 A Fiel d Notes / Comment

s Pag e 1 o f 1 Relinquishe

d By (print) : Date : Steve n Mil o ffifZp, 

## 2 f c ,; r Relinquishe d B y (print) : Date : Signature : Time : Relinquishe d B y (print) : Date : Signature : Time : t Received b y La b (print): , Date : j . 1

Received B

y (print) : Date : Signature : Time : Received B y (print) : Date : Signature : Time : Received B y (print) : Date : Signature : Time : Analytica l Laborator

y Destination : Received B

y (print) : Date : Signature : Time : Received B y (print) : Date : Signature : Time : Received B y (print) : Date : Signature : Time : Vist aAnalytica

l Laboratories, Inc

. 110 4 Wlndfiel

d Wa y E l Dorad o Hills , C A 9576

2 Attn : Ms . Marth

aMaie r916-673-152

0 Projec t3227 5 Page 1 6 o f I S 

## VES01817 2

## Vist a Projec t # : SAMPL E LOG-I N CHECKLIS T TA T Wvist a

w Analytica l Laborator y 

## Date/Tim e Sample s Arrival : i r

## . „ ^ Initials : Location : [^Jj^''^- ' Shelf/Rack : 1^/ ^ Logge d In : Date/Tim e initials : Location : J Shelf/Rack : U.// ^ Delivere d By : fTFedEx) ! UP S 

# I^JGg l DH L " a n d 

## , Othe r Delivere d Preservation : Ic e f Blu e Ice ^ Dr yIc e Non e Temp° C ti . Time : Q6f [ Thermomete rID : IR- 1 

# mmmmmmmmmmmmmmmmmmm YE S N O N A Adequat e Sampl e Volum e Received ? 1 / Holdin g Tim e Acceptable ? Shippin g Container(s ) Intact ? Shippin g Custod ySeal s Intact ? 1 ^ Shippin g Documentatio n Present ? Airbil l Trk # 

# $(flb WfrQttl Sampl e Containe rIntact ? Sampl e Custod ySeal s Intact ? Chai n of Custod y/

Sampl e Documentatio n Present ? CO C Anomaly/Sampl e Acceptanc e For m completed ? I f Chlorinate d o rDrinkin g Wate rSamples , Acceptabl e Preservation ? Na 2 

## S 2 

## 0 3

## Preservatio n Documented ? Shippin g Containe r(^Vista ^ Clien t {^eTalrf^ ^ Return ^ Dispos e

U 2 - 

# F/ 3 h\ur

fob
4 Projec t 3227 5 Sample Login 3/2007 rmh Pag e 1 7 o f

1 8 

## VES01817 3

## SAMPL E LOG-I N CHECKLIS T Vist a Projec

t #: . TA T Vist a

V Analytica l Laboraior y 

## Sample s Arrival : Daterrim e Initials : Location : (j(J \Z-£ — Shelf/Rack : ^ ^

A Logge d In : Date/Tim e initials : Location : j Shelf/Rack : Wffif Delivere d By : ^ UP S Ca l DH L * and 

## . Othe r Delivere d Preservation : Ic e Blu e Ice Dr yIce Non e Tem p ° C 

# /^m W vy V Time : Q<\Z\ Thermomete rID : IR- 1 Adequat e Sampl e Volum e Received ? Holdin g Tim e Acceptable ? Shippin g Container(s ) Intact ? Shippin g Custod ySeal s Intact ? Shippin g Documentatio n Present ? Airbil l Trk # <=>?Jt ^11 0 

## Sampl e Containe rIntact ? Sampl e Custod ySeal s Intact ? Chai n o f Custod y/

Sampl e Documentatio n Present ? CO C Anomaly/Sampl e Acceptanc e For m completed ? I f Chlorinate d o rDrinkin g Wate rSamples , Acceptabl e Preservation ? Na 2 

## S 2 

## 0 3

## Preservatio n Documented ? Shippin g Containe r Vist a Comments: 

# CPT-MZ3A-UZ F

B
i 

## Retai n



# 3tfR 

# /Fff£ .

Sampl e Containe r


# R 3

Projec t3227

5 Sample Login 3/7007 rmh Pag e 1

8 o f 18 

## VES01817 4

# Wast e Fee d

VES01817 5

# festAmencQ

TH E LEADE R I N ENVIRONMENTA L TESTIN G TestAmeric a Laboratories , Inc ,


## ANALYTICA L REPOR T

PROJEC T NO . 6013321 6 Veoli a - E S Tec h Lo t # : H9L14040 3

Jef f Gorma n AECOM , In c 510 5 Carrrpuswop

dDriv e Suit e 10 4 Eas t Syracuse , N T 1305 7

TESTAMERICA

LABORATORIES , INC .

Kevi nS . Woodcoc k Projec t Manage r

Decembe r 31 , 200 9

581 5 Middlebroo k

Pik e Knoxville , T N 3792 1 te l 865.291.300 0 fa x865.584.431 5 www.testamericainc.co m 

## VES01817 6

## ANALYTICA L METHOD S SUMMAR Y H9L1404O 3

PARAMETER ANALYTICA L METHO D As hConten t Hea t o f Combustio n Hea t o f Combustio nD5B6 5 Tota l Chlorin e References : AST M Annua l Boo k O f ASTM Standards . AST M D482-00 a •AST M D240-0 2 AST M D5865-0 0 KNO XWC-001 6

KNO X TestAmeric a Laboratorie s Inc. , Knoxvill e Laborator y Standar d Operatin g Procedur e

### 3 

## SAMPL E SUMMAR Y

H9H.4040 3

W O # SAMPLE S CLIEN T SAMPL E I D SAMPLED SAM P DAT E TIM E LQ2T C 00 1 HBTU-U2-M23A-R 1 12/08/0 9 LQ2T D 00 2 HBTU-U2-M23A-R 2 12/09/0 9 LQ2T E 00 3 HBTU-02-M23A-R 3 12/10/0 9 LQ2T F 00 4 LBTU-U2-M23A-R 1 12/08/0 9 LQ2T G 00 5 LBTU-TJ2-M23A-R 2 12/09/0 9 LQ2T H 00 6 LBTU-U2-M23A-R 3 12/10/0 9 LQ2T J 00 7 SF-U2-M23A-R 1 12/08/0 9 LQ2T K 00 8 SF-U2-M23A-R2 . 12/09/0 9 LQ2T L 00 9 SF-U2-M23A-R 3 12/10/0 9 LQ2T M 01 0 CS-U2-M23A-R 1 12/08/0 9 LQ2T P O i l CS-U2-M23A-R 2 12/09/0 9 LQ2T Q 01 2 CS-U2-M23A-R 3 12/10/0 9 LQ2T R 01 3 HBTU-U2-M26A-R 1 12/08/0 9 LQ2T T 01 4 HBTU-U2-M26A-R 2 12/09/0 9 LQ2T V 01 5 'HBTO-U2-M26A-R 3 12/10/0 9 LQ2T W 01 6 LBTU-U2-M26A-R 1 12/08/0 9 LQ2T 0 01 7 LBTU-U2-M26A-R 2 12/09/0 9 LQ2T L 01 8 LBTU-U2-M26A-R 3 12/10/0 9 LQ2T 3 01 9 SF-U2-M26A-R 1 12/08/0 9 LQ2T 4 02 0 SF-U2-M26A-R 2 . 12/09/0 9 LQ2T 5 02 1 SF-U2-M26A-R 3 12/10/0 9 LQ2T 5 02 2 CS-U2-M26A-R 1 12/08/0 9 LQ2T 7 02 3 CS-U2-M26A-R 2 12/09/0 9 LQ2T 3 02 4 CS-U2-M26A-R 3 12/10/0 9 HQTE(S ) ;

- Till ! anaiyiica

i result s o f di e sample s liste d abov e ar e presente d o n tli e followin

g pages .

- Al l calculation

s ar e performe

d befor e roundin g t o avoi d round-of

f error s i n calculate

d results .

- Result s note d a s "ND " wer

e no tdetecte d o to rabov e di e slate d limit .

- Tlit s repor tmus tno tb e reproduced

, excep ti n full , withou

tdi e writte n approva

l of di e laboralory

.

- Result s fo r(li e followin

g parameter

s ar e neve rreporte d o n adr y weigh tbasis : color, corrosiviiy. density , flashpoint

, ignitability

, layers , odor , pain tfilte rtest . pH , porosit

y pressure

, reactivity

, redo x poiemial

. specifi c gravity , spo tlests . solids , solubility

, temperature

, viscosity

, an d weight .



## VES01817 8

### 7 

## Q C DAT A ASSOCIATIO N SUMMAR

Y H9L14040 3
Sampl e Preparatio nan d Analysi s Contro l Number s
ANALYTICA

L METHO D SAMPLE * MATRI X 00 1 WASTE AST M D482-O0 a WASTE KNO

XWG-001 6 HAST E AST

M D240-0 2 00 2 WASTE AST M D482-O0 a WASTE KNO

XWC-001 6 WASTE AST

M D240-0 2 00 3 WASTE AST M D482-O0 a WASTE KNO

XWC-001 6 WASTE AST

M D240-0 2 00 4 WASTE AST M D482-0pa WASTE KNO

XWC-001 6 WASTE AST

M D240-0 2 00 5 WASTE AST M D482-00 a WASTE KNO

XWC-001 6 WASTE AST

M D240-0 2 00 6 WASTE AST M D482-00 a WASTE KNO

XWC-001 6 WAST E AST

M D240-0 2 ' 00 7 WASTE AST M D482-00 a WAST E KNO

XWC-001 6 WASTE AST

M D240-0 2 00 8 WAST

E AST

M D482~00 a WASTE KNO

XWC-001 6 WAST E AST

M D2 4 0-0 2 00 9 WAST

E AST

M D4B2-O0 a WASTE KNO

XWC-001 6 WASTE AST

M D240-0 2 01 0 SOLI D AST M D482-00 a SOLI D KNO

XWC-001 6 SOLI D AST

M D5865-0 0 01 1 SOLI D AST M D482-00 a SOLI D KNO

XWC-001 6 SOLI D AST

M D5865-0 0 LEAC H BATC H PRE

P BATC H '4 936343 4 935108 2 935634 8 936343 4 935108 2 93S634 8 9363434 - 935108 2 935634 8 936343 4 935108 2 935634 8 936343 4 935108 2 93563 4 8 936343 4 935108 2 935634 8 936343 4 935203 1 935718 8 936343 4 935203 1 935718 8 936343 4 935203 1 935718 8 936343 3 935606 5 935003 2 936343 3 935606 5 935003 2 M

S RON S 936322 4

936322 4 935111 6 935619 0

936322 3 935603 6 935002 1 (Continue do n nex t page )



## VES01817 9

### 8 

## Q C DAT A ASSOCIATION SUMMAR Y H9L14040 3
Sampl e Preparatio nand Analysi s Contro l Number s

SAMPLE S 01 2 ANALYTICA L METHO D

01 3

01 4

01 5

01G



## o n
01 8

01 9

02 0

02 1

02 2 SOLI D AST M D482-00 a SOLI D KNO

XWC-001 6 SOLI D AST

M D5865-0 0 WAST E , AST

M D482-00 a WAST E KNO

XWC-001 6 WAST E ' AST

M D240-0 2 WAST E . AST

M D482-O0 a WAST E KNO

XWC-001 6 WAST E AST

M D240-0 2 WAST E AST

M D4B2-00 a WAST E KNO

XWC-O01 6 WAST E AST

M D240-0 2 WAST E ' AST

M D482-00 a WAST E KNO

XWC-O0I 6 WAST E AST

M D240-0 2 WAST E AST

M D482-00 a WAST E KNO

XWC-001 6 WAST E AST

M D240-0 2 WAST E AST

M D4B2-O0 a WAST E KNO

XWC-001 6 WAST E AST

M D240-0 2 WAST E AST

M D482-00 a WAST E KNO

XWC-001 6 WAST E AST

M D24O-0 2 WAST E AST

M D482-00 a WAST E KNO

XWC-001 6 WAST E AST

M D24O-0 2 WAST E AST

M D482-00 a WAST E KNO

XWC-001 6 WAST E AST

M D240-0 2 SOLI D AST

M D482-00 a SOLI D KNOX.WC-001 6 SOLI D AST

M D5865-0 0 LEACH '

BATC H # PRE

P BATC H $ 936343 3 935606 5 935003 2 936343 4 935203 1 935718 8 936343 4 935203 1 935718 8 936343 4 935203 1 935718 8 936343 4 •935203 1 935718 8 936343 4 935203 1 935718 8 936343 4 935203 1 935718 8 936343 4 935203 1 935718 8 936343 4 935203 1 935718 B 936343 4 935203 1 935718 8 936343 3 935606 5 935003 2 M

S RON S

935201 1 935712 5

.935201 1

935712 5

(Continue do n nex t page )



## VES01818 0

### 9 

## Q C DAT A ASSOCIATIO N SUMMAR Y

H9L14040 3
Sampl e Preparatio nand Analysi s Contro l Number s

ANALYTICA

L SAMPLE * MATRI X. METHO D 02 3 SOLI D AST M D482-00 a SOLI D KNO

XWC-001 6 SOLI D AST

M D5865-0 0 02 4 SOLI D AST M D482-00 a SOLI D KNO

XWC-001 6 SOLI D AST

M D5865-0 0 LEAC H BATC H PRE

P BATC H » 936343 3 935606 5 935003 2 936343 3 935606 5 935003 2 M

S RU N i f



## VES01818 1

### 1 0

### 1 1

Lot-Sampl e # . Bat e Sampled . PARAMETE R AECOM , In c Clien t Sampl e ZD : HBTU-02-M23A-R 1

Genera l Chemistr y H9L140403-00 1 Wor k Orde r #... : LQ2T C 12/08/0 9 Dat e Received.. : 12/11/0 9 Matri x: WAST E

RESDL T RL ONIT S As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 137 0 20 0 mg/k g Dilutio nFactor : 1 919 0 180 0 BT0/l b

Dilutio nFactor : 1 • 1620 0 169 0 mg/k g

Dilutio nFactor : 8.4 6 METHO D AST M D482-00 a MD L : 5 1 AST M D240-0 2 MD L : 13 0 KHO XWC-001 6 MDL . i : 51 0 PREPARATION - PRE P ANALYSI S DAT E BATC H # 12/29-12/31/0 9 936343 4
12/22/0 9 935634 8
12/17-12/18/0 9 935108 2



## VES01818 3

### 1 2

AECOM , In c Clien t Sampl e IDs HBTU-U 2 -M23A-R 2

Genera l Chemistr y Lot-Sampl e #... 1 H9L140403-00 2 Wor k Orde r #. . Dat e Sampled— : 12/09/0 9 Dat e Received .
PARAMETE

R RESUL T R L DNIT S As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 191 0 20 0 mg/k g Dilutio nFactor : 1 943 0 180 0 BTO"/l b

Dilutio nFactor : 1 1420 0 154 0 mg/k g

Dilutio nFactor : 8.1 8 LQ2T D 12/11/0 9 Matrix . WAST E

_METHO

D - AST M D482-00 a MD L : 5 1 AST M D240-0 2 MD L ' : 13 0 KNO XWC-001 6 MD L J: 49 0 PREPARATION - PRE P ANALYSI S DAT E BATC H # 12/29-12/31/0 9 936343 4 12/22/0 9 935634 8
12/17-12/18/0 9 935108 2



## VES01818 4

### 1 3

AECOM , In c Clien t Sampl e ID : HBTO-02-M23A-R 3

Genera l Chemistr y Lot-Sampl e #.., : H9L140403-00 3 Wor k Orde r #... : LQ2T E Dat e Sampled. : 12/10/0 9 Dat e Received.. : 12/11/0 9 Matrix . WAST E

PARAMETE

R RESUL T R L UNIT S As hContent . Gros s Calorifi c Valu e
Tota l Chlorin e 249 0 20 0 mg/kg Dilutio nFactor : l 987 0 180 0 BTU/l b

Dilutio nFactor : 1 1390 0 170 0 mg/kg

Dilutio nFactor : 8.E l _ • METHO D AST M D482-00 a MDI . : S I AST M D240-0 2 MDL. . . : 13 0 KNO XWC-001 6 MD L : 51 0 PREPARATION - PRE P ANALYSI S DAT E BATC H # 12/29-12/31/0 9 936343 4 12/22/0 9 935634 8
12/17-12/18/0 9 935108 2



## VES01818 5

### 1 4

AECOM , In c Clien t Sampl e ID : LBTET-U2-M23A-R 1

Genera l Chemistr y Lot-Sampl e #... : H9L140403-00 4 Wor k Orde r #.. . t LQ2T F Matri x: WAST E Dat e Sampled.12/08/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRE P PARAMETER RESPL T R L DNIT S METHO D • ANALYSI S DAT E BATC H # As hConten t 234 0 20 0 mg/kg AST M D482-00 a 12/29-12/31/0 9 936343 4 Dilutio nFactor : 1 MD L : 5 1 Gros s Calorifi c N D 180 0 BTD/l bASTM D240-0 2 12/22/0 9 935634 8 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 112 0 30 6 mg/kg KNO XWC-001 6 12/17-12/18/0 9 935108 2 Dilutio nFactor : 1.5 3 MD L : 3 2



## VES01818 6

### 1 5

AECOM , In c Clien t Sampl e ID : LBTU-TJ2-M23A-R 2

Genera l Chemistr y Lot-Sampl e #... : H9L140403-00 5 Wor k Orde r ft...: LQ2T G Matrix . : WAST E Dat e Sample d : 

## 12/09/0 9 Dat e Received.. : 

### 12/11/0 9
PARAMETE R RESUL T R L OMIT S 20 0 mg/kg Dilutio nFactor s 1 180 0 BTU/l b Dilutio nFactor : 1 29 0 mg/k g Dilutio nFactor : 1.4 5 METHO D AST M D482-00 a MDL . . : 5 1 AST M D240-0 2 MD L : 13 0 KNO XWC-001 6 MD L : 8 7 PREPARATION - PRE P ANALYSI S DAT E BATC H # 12/29-12/31/0 9 936343 4 12/22/0 9 935634 8
12/17-12/18/0 9 935108 2 As hConten t 190 0
Gros s Calorifi c N D Valu e
Tota l Chlorin e 98 8



## VES01818 7

### 1 6

AECOM , In c Clien t Sampl e ID : LBTTJ-D 2 -M23A-R 3

Genera l Chemistr y tot-Sample #... : H9L140403-00 6 Wor k Orde r ft-..: LQ2T H Matrix.... . : . WASTE Dat e Sampled... : 12/10/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRE P PARAMETER ' RESUL T R L UNIT S METHO D ANALYSI S DAT E BATCH # A s hConten t 229 0 20 0 mg/kg AST M D482-00 a 12/29-12/31/0 9 936343 4 Dilutio nFactor : 1 MD L S I Gros s Calorifi c 13 4 B 180 0 BTU/l bAST M D240-0 2 12/22/0 9 935634 8 Valu e Dilutio nFactor : 1 MD L -

. : 13 0 Tota l Chlorin e 114 0 28 8 mg/kg KNO XWC-001 6 12/17-12/18/0 9 935108 2 Dilutio nFactor : 1.4 4 MD L s . 8 6 HOT E (S ) : \ . ' • • * . . R L Reportin

g Limi t B Estimate

d result. Resul

tis les s tha n Rl .



## VES01818 8

### 1 7

AECOM , In c Clien t Sample.ID : SF-D2-M23A-R 1

Genera l Chemistr y Lot-Sampl e #... : H9L140403-00 7 Wor k Orde r #-.. : LQ2T J Matri x. .. : WAST E Dat e Sampled... : 12/08/0 9 Dat e Received..: . 12/11/0 9 PREPARATION - PRE P PARAMETER RESUL T R L OMIT S . METHO D ANALYSI S DAT E BATC H # As hConten t 742 0 20 0 mg/k g AST M D482-00 a 12/29-12/31/0 9 936343 4 Dilutio nFactor : 1 MDL. - : 5 1 Gros s Calorifi c N D 180 0 BTU/l bAST M D240-0 2 12/23/0 9 935718 8 Value . Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 473 0 84 0 mg/k g KNO XWC-001 6 12/21-12/28/0 9 935203 1 Dilutio nFactor : 4. 2 MD L : 25 0



## VES01818 9

### 1 8

AECOM , In c Clien t Sampl e ID : SF-U2-M23A-R 2

Genera l Caemistr y Lot-Sampl e ii...: H9L140403-OOB Wor k Orde r : LQ2T KMatri x: WAST E Dat e Sampled... : 12/09/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRE P PARAMETER RESUL T R L UNIT S METHO D ANALYSI S DAT E BATCH # As hConten t 772 0 20 0 mg/k g AST M D482^00 a 12/29-12/31/0 9 936343 4 Dilutio nFactor : 1 MD L : 5 1 Gros s Calorifi c N D 180 0 BTU/l bASTM D240-0 2 12/23/0 9 935718 8 Valu e Dilutio nFactor : 1 MDL . : 13 0 Tota l Chlorin e 483 0 82 4 mg/k g KNO X WC-001 6 12/21-12/28/0 9 935203 1 Dilutio nFactor : 4.1 2 MD L 25 0



## VES01819 0

### 1 9

AECOM , In c Clien t Sampl e ID : SF-TJ2-M23A-R 3

Genera l Chemistry Lot-Sampl e #... : H9L140403-00 9 .Wor k Orde r #... : LQ2T L Dat e Sampled. .
PARAMETER 12/10/0 9
RESUL T Dat e Received.. : 12/11/0 9

R L UNIT S METHO D Matri x: WAST E

PREPARATION - PRE P ANALYSI S DAT E BATC H # As hConten t
Gros s Calorifi c VaLu e
Tota l Chlorin e 754 0 20 0 mg/kg Dilutio nFactor : i N D 180 0 BTU/l b

Dilutio nFactor ; 1 481 0 83 8 mg/kg

Dilutio nFactor : 4.1 9 ASTM D482-00 a MD L : 5 1 AST M D240-0 2

KNO XWC-001 6 MD L : 2S0 12/29-12/31/0 9 936343 4 12/23/0 9 93571B 8
12/21-12/28/0 9 935203 1



## VES01819 1

### 2 0

AECOM , In c Clien t Sampl e ID : CS-U2-M23A-R 1

Genera l Chemistr y Lot-Sampl e #... : H9L140403-010 . Wor k Orde r #... : LQ2T M Matrix..,...... : SOLI D Dat e Sampled... : 12/08/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRE P PARAMETER RESUL T R L . UNIT S METHO D . ANALYSI S DAT E BATC H # A s hConten t 71600 0 20 0 mg/k g AST M D482-00 a 12/29-12/31/0 9 936343 3 Dilutio nFactor : 1 MDL , : 5 1 Gros s Calorifi c N D . 180 0 BTU/l b. ASTM D5865-0 0 12/16/0 9 935003 2 valu e Dilutio nFactor : 1 MD L 13 0 Tota l Chlorin e 12 9 B 20 2 mg/kg KNO XWC-001 6 12/22-12/29/0 9 935606 5 Dilutio nFactor : 1.0 1 MD L : 6 1 NOTB<S) : ' [ . ; R l Reportin

g Umi l B Estiniatn

l result . Resul ti s les s tha n RL .



## VES01819 2

### 2 1

AECOM , In c Clien t Sampl e ID : CS-02-M23A-R 2

Genera l Chemistr y Lot-Sampl e #... : H9L140403-01 1 Wor k Orde r #... : LQ2T P Matri x: SOLI D Dat e Sampled... : 12/09/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRE P PARAMETER RESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H # A s hConten t 71300 0 20 0 mg/kg AST M D482-00 a 12/29-12/31/0 9 936343 3 Dilutio nFactor : 1 MD L : 5 1 Gros s Calorifi c N D 180 0 BTU/l bASTM D586S-0 0 12/16/0 9 935003 2 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 13 4 B 20 0 mg/kg KNO XWC-001 6 12/22-12/29/0 9 935606 5 Dilutio nFactor : 1 MD L : 6 0 HOTE(S ) : ; ; ' \ R L Reportin

s Limi l B Estimate

d result . Resul ti s les s tha n RL .



## VES01819 3

### 2 2

AECOM , In c Clien t Sampl e ID : CS-02-M23A-R 3

Genera l Chemistr y Lot-Sampl e : H9L140403r01 2 Wor k Orde r #... : LQ2T Q Matri x.. : SOLI D Dat e Sample d : 12/10/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRE P PARAMETERRESOL T R L DNIT S METHO D ANALYSI S DAT E BATCH # Ash . Conten t 70800 0 20 0 mg/kg AST M D482-00 a 12/29-12/31/0 9 936343 3 Dilutio n Factor : 1 ' MD L = 5 1 Gros s Calorifi c N D 180 0 BTO/l bASTM D5S65-0 0 12/16/0 9 935003 2 Valu e Dilutio n Factor : 1 MD L ...' : 13

0 Tota l Chlorin e 14 1 B 20 0 mg/kg KNO XWC-001 6 12/22-12/29/0 9 935606 5 Dilutio n Factor : 1 MD L : 6

0 

## mot e ts) : ' ; ; ; R L Reportin

g Limi t B Estimate

d result . Resul ti s les s tha n M- .



## VES01819 4

### 2 3

AECOM , In c Clien t Sampl e JD : HBTU-T/2-M26A-R1

Genera l Chemistr y Lot-Sampl e ii... : H9L14Q403-01 3 Wor k Orde r : LQ2T R Matri x: WAST E Dat e Sampled... : 12/08/0 9 Dat e Received . 12/11/0 9
PARAMETER RESUL T RL UNIT S As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 136 0 20 0 mg/kg Dilutio nFactor : 1 1020 0 180 0 BTU/l b

Dilutio nFactor : 1 1530 0 168 0 mg/kg

Dilutio nFactor : 8.3 9 _METHO D _ _ AST M D482-00 a MD L : 5 1 AST M D240-0 2 MD L : 13 0 KNO X WC-001 6 MD L : 50 0 PREPARATION - PRE P ANALYSI S DAT E BATCH # 12/29-12/31/0 9 936343 4 12/23/0 9 935718 8
12/21-12/28/0 9 935203 1



## VES01819 5

### 24

AECOM , In c Clien t Sampl e Hi : HBTU-U2-M26A-R 2

Genera l Chemistr y Lot-Sampl e if... : H9L140403-.01 4 Wor k Orde r #... : LQ2T T Matrix . : WAST E Dat e Sampled... ; 12/09/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRE P PARAMETE

R RESUL T R L UNIT S • METHO D ANALYSI S DAT E BATCH # As hConten t I86 0 20 0 rag/kg AST M D482-00 a 12/29-12/31/0 9 936343 4 Dilutio nFactor : 1 MD L .. : 5 1 Gros s Calorifi c 981 0 180 0 BT0/l bAST M D240-0 2 12/23/0 9 935718 8 Valu e Dilutio nFactor : 1 MD L 13 0 Tota l Chlorin e 1350 0 169 0 mg/k g KNO

XWC-001 6 12/21-12/28/0 9 935203 1

. Dilutio nFactor : 8.4 7 MD L , i 51 0



## VES01819 6

### 25

AECOM , In c ' _ Clien t Sampl e ID : HBTU-02-M26A-R 3 _

Genera l Chemistr y Lot-Sampl e #...: • H9L140403-01 S Wor k Orde r ft...: LQ2T V Matri x: WAST E Dat e Sampled... : 12/10/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRE P PARAMETER RESUL T R L UNIT S METHO D ANALYSI S DAT E BATCH # As hConten t 295 0 20 0 mg/kg AST M D482-00 a 12/29-12/31/0 9 936343 4 Dilutio nFactor : 1 MDL . >.... ! 5 1 Gros s Calorifi c 981 0 180 0 BTU/l bAST M D240-0 2 12/23/0 9 935718 8 Valu e Dilutio nFactor : 1 MD L ;.. : 13 0 Tota l Chlorin e 1450 0 168 0 mg/kg KNO XWC-001 6 12/21-12/28/0 9 935203 1 Dilutio nFactor : a. 4 MD L : 50 0



## VES01819 7

### 26

AECOM , In c Clien t Sampl e ID : LBTU-U2-M26A-R 1

Genera l Chemistry Lot-Sampl e # . .. : H9L140403-01 6 Wor k Orde r #... : LQ2T W Dat e Sampled--. : 12/08/0 9 Dat e Received.. : 12/11/0 9
PARAMETE

R RESUL T R L UNIT S METHO D Matri x: WAST E

PREPARATION - PRE P ANALYSI S DAT E BATCH # As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 226 0 20 0 mg/kg Dilutio nFactor : 1 N D 180 0 BTU/l b

Dilutio n Factor : 1 118 0 27 8 mg/k g

Dilutio n Factor : 1.-3 9 AST M

D482-00 a MDL . : 51 -

' ASTM D240-0 2 MD L , : 13

0 KNO XWC-001 6 12/29-12/31/0 9 936343 4

12/23/0 9 935718 B
12/21-12/29/0 9 935203 1 MDL . S 3



## VES01819 8

### 27

AECOM , In c Clien t Sampl e ID : LBTU-U2-M26A-R 2

Genera l Chemistr y lot-Sample*... : H9L140403-01 7 Wor k Orde r LQ2T 0 Matri x. : WAST E Dat e Sampled... : 12/09/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRE P PARAMETER RESUL T R L UNIT S METHO D ' ANALYSI S DAT E BATC H # As hConten t 199 0 20 0 mg/k g ASTM D482-O0 a 12/29-12/31/0 9 936343 4 Dilutio nFactor : 1 MD L : 5 1 Gros s Calorifi c N D 180 0 BTU/l bASTM D240-0 2 . 12/23/0 9 935718 8 Valu e Dilutio nFactor : 1 MDI.. . : 13 0 Tota l Chlorin e 106 0 28 0 mg/k g KNO XWC-001 6 12/21-12/29/0 9 935203 1 Dilutio nFactor : 1. 4 MD L : 8 4



## VES01819 9

### 2 8

AECOM , In c Clien t Sampl e ID : JLBTO-U2-M26A-R 3

, . Genera l Chemistr y Lot-Sampl e it. .. : H9L140403-01 8 Wor k Orde r #... : LQ2T 1 Matri x.. : WAST E Dat e Sampled... : 12/10/0 9 Dat e Received.. = 12/11/0 9 PREPARATION - PRE P PARAMETE

R , RESUL T R L UNIT S METHO D • ANALYSI S DAT E BATCH # As hConten t 235 0 20 0 mg/k g ASTM

D482-00 a 12/29-12/31/0 9 936343 4 Dilutio nFactor : 1 MD L : 5 1 Gros s Calorifi c N D 180 0 BTU/l bASTM D240-0 2 .12/23/0 9 935718 8 Valu e Dilutio nFactor : 1 MD L 1 3 0 Tota l Chlorin e 123 0 28 2 mg/kg KNO XWC-001 6 12/21-12/29/0 9 935203 1 Dilutio nFactor : 1.4 1 MD L : 8 5



## VES01820 0

### 2 9

AECOM , In c Clien t Sampl e ID : SF-U2-M26A-R 1

Genera l Chemistr y Lot-Sampl e ft...: H9L140403-01 9 Wor k Orde r : LQ2T 3 Matrix... . : WAST E Dat e Sample d : 12/08/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRE P PARAMETE

R RESUL T RL UNIT S METHO D ANALYSI S DAT E BATCH # As hConten t 776 0 20 0 mg/k g AST M D482-00 a 12/29-12/31/0 9 936343 4 Dilutio nFactor ; 1 MD L : 5 1 Gros s Calorifi c N D 180 0 BTU/l bASTM D240-0 2 12/23/0 9 935718 8 Valu e Dilutio nFactor : 1 MDL........:... ; 13 0 Tota l Chlorin e 497 0 84 0 mg/k g KHO

XWC-001 6 12/21-12/28/0 9 935203 1 Dilutio nFactor : 4. 2 MDL . : 25 0



## VES01820 1

### 30

Lot-Sampl e ft.., Dat e Sampled.. .
PARAMETE

R As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e AECOM , In c Clien t Sampl e XTJ : SF-U2-M26A-R 2

Genera l Chemistr y H9L140403-02 0 12/09/0 9
RESUL T Wor k Orde r #.. .

Dat e Received. .
R L UNIT S 806 0 20 0 mg/kg

Dilutio nFactor : 1 N D 180 0 BTU/l b

Dilutio nFactor : 1 451 0 83 6 mg/k g

Dilutio nFactor : 4.1 8 LQ2T 4 12/11/0 9
METHO D Matrix . WAST E

AST M D482-00 a MDL, , : 5 1 AST M D240-0 2 MDL . : 13 0 KNO XWC-001 6 MDL . 25 0 PREPARATION - PRE P ANALYSI S DAT E BATCH ft 12/29-12/31/0 9 936343 4 12/23/0 9 935718 8
12/21-12/28/0 9 935203 1



## VES01820 2

### 3 1

AECOM , In c Clien t Sampl e ID : SF-U2-M26A-R 3

Genera l Chemistr y Lot-Sampl e : H9L140403-02 1 Wor k Orde r : LQ2T 5 Matri x: WASTE Dat e Sampled. : 12/10/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRE P PARAMETER . RESUL T Rl ; UNIT S METHO D ANALYSI S DAT E BATCH # As hConten t 793 0 20 0 mg/k g AST M

D4B2-00 a 12/29-12/31/0 9 936343 4 Dilutio nFactor : 1 MD L .

- S I Grps s Calorifi c N D . 180 0 BTU/l bAST M D240-0 2 12/23/0 9 935718 8 Valu e Dilutio nFactor : 1 MD L : 1 3 0 Tota l Chlorin e 479 0 84 4 mg/k g KNO

XWC-001 6 12/21-12/28/0 9 935203 1 Dilutio nFactor : 4.2 2 . HD L .. : 25 0



## VES01820 3

### 32

Lot-Sampl e #... : H9L140403-02 2 Dat e Sample d : 12/08/0 9 AECOM , In c Clien t Sampl e ID : CS-U2-M26A-R 1

Genera l Chemistry Wor k Orde r #... : LQ2T 6 Dat e Received.. : 12/11/0 9 Matrix. » i SOLI D

RESUL T R L UNIT S METHO D PREPARATION - PRE P

ANALYSI S DAT E BATC H # PARAMETE

R As hConten t , 80900 0 20 0 mg/kg Dilutio nFactor : 1 Gros s Calorifi c N D 180 0 BTU/l b Valu e Dilutio nFactor : 1 Tota l Chlorin e N D 20 0 mg/k g Dilutio nFactor : 1 AST M D482-00 a 12/29-12/31/0 9 936343 3 MD L : 5 1 AST M D5865-0 0 12/16/0 9 935003 2 MD L .. : 13 0 KNO XWC-001 6 12/22-12/29/0 9 935606 5 MD L : 6 0



## VES01820 4

### 3 3

AECOM , In c Clien t Sampl e ID : CS-D2-M26A-R 2

Genera l Chemistr y Lot-Sampl e H9L140403-02 3 Wor k Orde r : LQ2T 7 Dat e Sampled... : 12/09/0 9 Dat e Received.. : 12/11/0 9 Matri x: SOLI D

PARAMETE

R RESUL T R L UNIT S As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 78700 0 20 0 mg/k g Dilutio nFactor : 1 N D 180 0 BTU/l b

Dilutio nFactor : 1 N D 20 0 mg/kg

Dilutio nFactor : 1 _METHO D AST M D482-00 a .MD L : 5 1 ASTM D5865-00 . MD L : 13 0 KNO XWC-0-01 6 MD L : 6

0 PREPARATION - PRE P ANALYSI S DAT E BATCH # 12/29-12/31/0 9 936343 3 12/16/0 9 935003 2
12/22-12/29/0 9 935606 5



## VES01820 5

### 34

AECOM, . In c Clien t Sampl e ID : CS-U2-M26A-R 3

Genera l Chemistr y Lot-Sampl e # . . . : H9L140403-02 4 Wor k Orde r #... : LQ2T 8 Dat e Sample d : 12/10/0 9 Dat e Received.. : 12/11/0 9
PARAMETE

R . RESUL T R L UNIT S METHO D Matri x: SOLI D

PREPARATION - PRE P ANALYSI S DAT E BATCH # As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 76900 0 20 0 mg/kg AST M D482-00 a 12/29-12/31/0 9 936343 3 Dilutio nFactor : 1 MD L : S I N D

N D 180 0 BTU/l bAST M DS865-0 0 12/16/0 9 Dilutio nFactor : 1 MD L ,... : 13 0 935003 2

20 0 mg/k g KNO XWC-001 6 12/22-12/29/0 9 935605 5 Dilutio nFactor : 1 MD L : 6 0



## VES01820 6

### 35

Clien t lo t H9L14040 3
PARAMETE

R As hConten t RESUL T METHO D BLAN KREPOR T Genera l Chemistr y

REPORTIN

G LIMI T UNIT S METHO D Matri x: WAST E

PREPARATION - PRE P ANALYSI S DAT E BATCH # Wor k Orde r # : LRPQFIA A M B Lot-Sampl e # : H9L290000-43 4 N D 20 0 mg/kg AST M D482-O0 a 12/29-12/31/0 9 93S343 4 Dilutio nFactor : 1 Tota l Chlorin e Wor k Orde r # : LQ76D1A A M B Lot-Sampl e # : H9L170000-08 2 N D 20 0 tng/kg KNO XWC-001 6 12/17-12/18/0 9 935108 2 Dilutio nFactor : 1 . Tota l Chlorin e Wor k Orde r # ; LRAEQ1A A M B Lot-Sampl e # : H9L180000-03 1 N D 20 0 mg/k g KNO

XWC-001 6 12/21-12/28/0 9 935203 1 Dilutio nFactor : 1 NOTJtS ) Calculator

s ar c pcrrormc

d bcfori : roundin

g t o avoi d rauntl-of

f error s i n calculate

d results .



## VES01820 7

### 3 6

Clien t Lo t H9L14040 3
PARAMETER RESUL T As hConten t N D METHO D BLAN KREPOR T Genera l Chemistr y Matrxx . SOLI D REPORTIN

G LIMI T UNIT S METHO D PREPARATION - PRE P

• ANALYSI S DAT E BATCH # Work Orde r # : LRPQE1A A M B Lot-Sampl e # : H9L290000-43 3 20 0 mg/k g ASTM D482-00 a 12/29-12/31/0 9 936343 3 Dilutio nFactor : 1 Tota l Chlorin e Work Orde r #: ' LRGLV1A A M B Lot-Sampl e #.

- H9L220000-06 5 N D 20 0 mg/k g KNO XWC-001 6 

## 12/22-12/29/0 9 935606 5 Dilutio nFactor : 1 NOTE(S ) : . Calculation

s ar c performe

d befor e roundin g l o avoi d roundof

f error s i n calculate

d results .



## VES01820 8

### 37

LABORATOR

YCONTRO

L SAMPL E EVALUATION REPORT Genera l Chemistr y Lot-Sampl e # . H9L14040 3 Matri x: SOLI D

PERCENT RECOVER YRPD PARAMETE

RRECOVER

YLIMIT S RPD LIMIT S METHO D As hConten t 10 0



## i o o PREPARATION - PRE P ; ANALYSI S DAT E BATC H # W0#:LRPQE1AC-LCS/LRPQE1AD-LCS D LC S Lot-Sample* : H9L290000-43 3 (9 0 - 110 ) ASTM D482-O0 a 12/29-12/31/0 9 936343 3 (9 0 - 110 ) 0.3 2 (0-10 ) AST M D4B2-O0 a 12/29-12/31/0 9 936343 3 Dilutio nFactor ; 1 Gros s Calorifi c Valu e 10 0

10 0 W0#:LQS8P1AA-LCS/LQ58P1AC-LCS D LC S Lot-Sample* : H9L160000-03 2

(9 8 - 102 ) ASTM D5865-0 0 (9 8 - 102 ) 0.1 0 (0-2.0 ) ASTM D5865-0 0 Dilutio nFactor : 1 12/16/0 9 12/16/0 9 935003 2

935003 2
NOTB(S ) : Calculation

s ar cpcrrormc

d befor e roundin

g t o avoi d round-of

f error s i n calculate

d results .



## VES01820 9

### 38

LABORATOR

YCOHTROL SAMPL E DATA REPOR T Genera l Chemistr y Lot-Sampl e #... : H9L14040 3 Matri x: SOLI D
PARAMETE

R As hConten t SPIK E MEASURE D AMOUN T AMOUN

T UNIT S PERCNT

RECVR YRPD . METHO

D 400 0 400 0 PREPARATION - PRE P ANALYSI S DAT E BATCH # W0#:LRPQE1AC-LCS/LRPQE1AD-LCS D LC S Lot-Sample# : H9L290000-43 3 400 0 mg/k

g 10 0 ASTM D482-0O a 12/29-12/31/0 9 936343 3 399 0 mg/k

g 10 0 0.3 2 ASTM D4B2-00 a 12/29-12/31/0 9 93S343 3 Dilutio nFactor. - 1 Gros s Calorifi c Valu e 1140 0

1140 0 WO#-.LQ58PlAA-LCS/LQ58PlAC-LCS D LC S Lot-Sample* : H9L160000-03 2

1130 0 BTU/l b10 0 1130 0 BTU/l b10 0

Dilutio nFactor : 1 ASTM D58S5-0 0 0.1 0 AST M

D5865-0 0 12/16/0 9 12/16/0 9 93S003 2

935003 2
NOTE(S ) : Calculation

s ar c performe

d befor e roundin g t o avoi d round-of

f error s i n calculate

d results .



## VES01821 0

### .3 9

LABORATOR

YCONTRO

L SAMPL E EVALUATION REPOR T Genera l Chemistr y Lot-Sampl e H9L14040 3

PERCENT RECOVER YRPD PARAMETER RECOVER YLIMIT S RPD

_LIMIT S METHO

D As hConten t 

### Matrix : rWAST E PREPARATION - PRE P ANALYSI S DAT E BATC H # W0#:LRPQP1AC-LCS/LRPQP1AD-LCS D LC S Lot-Sample# : H9L290000-43 4 10 0 (9 0 - 110 ) ASTM D482-00 a 12/29-12/31/0 9 936343 4 9 9 (9 0 - 110 ) 0.9 3 (0-10 ) ASTM D482-00 a 12/29-12/31/0 9 936343 4 Dilutio nFactor : 1 Gros s Calorifi c Valu e 10 0

9 9 W0#:LRG6J1AA-LCS/LRG6J1AC-LCS D LC S Lot -r Sample* : H9L220000-34 8

(9 8 - 102 ) ASTM D240-0 2 (9 8 - 102 ) 0.4 2 (0-2.0 ) ASTM D240-0 2 Dilutio nFactor : 1 12/22/0 9 935634 8 12/22/0 9 935634 8
Gros s Calorifi c Valu e 10 0

10 0 W0#:LRJKE1AA-LCS/LRJKE1AC-LCS D LC S Lot-Sample* : H9L2300O0-18 8

(9 8 - 102 ) ASTM D240-0 2 (9 8 - 102 ) 0.0 4 (0-2.0 ) AST M D240-0 2 Dilutio nFactor : 1 12/23/0 9 935718 8 12/23/0 9 935718 8

NOTE(S) : Calculation

s ar cpcrrormc

d befor e roundin g t o avoi d round-or

f error s i n calculate

d results .



## VES01821 1

### 4 0

LABORATOR

YCONTRO

L SAMPL E DAT A

REPOR T Genera l Chemistr y Lot-Sampl e #. . H9L14040 3 Matrix . WAST E
PARAMETER As hConten t SPIK E

AMOUN T 400 0 400 0 MEASURE

D AMOUN T UNIT S PERCN T RECVR YRP D METHO

D PREPARATION ANALYSI S DAT E PRE P

BATCH # W0#:LRPQF1AC-LCS/LRPQF1AD-LCS D LC S Lot-Sample# : H9L290O00-43 4 398 0 mg/k

g 10 0 AST M D482-O0 a 12/29-12/31/0 9 936343 4 394 0 mg/k

g 9 9 0.9 3 AST M D482-00 a 12/29-12/31/0 9 936343 4 Dilutio nFactor : 1 Gros s Calorifi c Valu e 2060 0

2060 0 W0#:LRG6J1AA-LCS/LRG6J1AC-LCS D LC S Lot-Sample* : H9L220O00-34 8

2050 0 BTU/l b10 0 2050 0 BTU/l b9 9

Dilutio nFactor : 1 AST M D240-0 2 0.4 2 AST M

D240-0 2 12/22/0 9 12/22/0 9 93S634 B

935634 8
Gros s Calorific ' Valu e 2060 0

2060 0 W0#:LRJKE1AA-LCS/LRJKE1AC-LCS D LC S Lot-Sample* : H9L230O00-18 8

2050 0 BTU/l b10 0 2050 0 BTU/l b10 0

Dilutio nFactor : 1 AST M D240-0 2 0.0 4 AST M

D240-0 2 12/23/0 9 12/23/0 9 935718 8

935718 8

NOTB(S ) : Calculation

s ar c performe

d befor e roundin g t o avoi d round-of

f error s in calculate

d results .



## VES01821 2

### 4 1

LABORATOR

YCOHTROL SAMPL E EVALXJATIO H REPOR T Genera l Chemistr y Clien t Lo t : H9L14040 3 Matri x: WAST E PERCENT RECOVER YPREPARATION - PRE P PARAMETE

R RECOVER

YLIMIT S - METHO D ' ANALYSI S DAT E BATC H # Tota l Chlorin e Wor k Orde r # : LQ76D1A C LC S Lot-Sample# : H9L170000-08 2 10 0 (8 0 - 120 ) KNO XWC-001 6 12/17-12/18/0 9 935108 2 Dilutio nFactor : S Tota l Chlorin e Wor k Orde r # : LRAEQ1A C LC S Lot-Sample* : H9L180000-03 1 9 6 - (8 0 - 120 ) KNO XWC-001 6 12/21-12/28/0 9 935203 1 Dilutio nFactor : 5 NOTE(S ) : . . ' • CalculMion

s ar c pcrrormc

d befor e roundin g l o avoi d round-of

f error s i n calculate

d results .



## VES01821 3

### 4 2

LABORATOR

YCOHTROL SAMPL E DAT A REPORT Genera l Chemistr y Clien t Lo t : H9L14040 3 Matrix.... . : WAST E

SPIK E MEASURE

D .PERCN T PREPARATION - PRE P PARAMETE

R AMOUN

T AMOUN

T UNIT S RECVR YMETHO

D ANALYSI S DAT E BATC H # Tota l Chlorin e Wor k Orde r # : LQ76D1A C LC S Lot-Sample* : H9L170000-08 2 1000 0 995 0 mg/kg 10 0 KNO XWC-001 6 12/17-12/18/0 9 935108 2 Dilutio nFactor : S Tota l Chlorin e Wor k Orde r # : LRAEQ1A C LC S Lot-Sample* : H9L180000-03 1 10OO 0 957 0 mg/kg 9 6 KNO XWC-001 6 . 12/21-12/28/0 9 935203 1 Dilutio nFactor : S NOTE(S ) : ; Calculation

s ar c pcrrormc

d befor e roundin

g i o avoi d round-of

rerror s in calculous ! results

.



## VES01821 4

### 4 3

LABORATOR

YCONTRO

L SAMPL E EVALUATION REPOR T Genera l Chemistr y Clien t Lo t #.-. : H9L1404Q 3 Matri x; SOLI D PERCENT RECOVER YPREPARATION - PRE P PARAMETER ' RECOVER YLIMIT S METHO D ' ANALYSI S DAT E BATC H # Tota l Chlorin e Wor k Orde r # : LRGLV1A C LC S Lot-Sample* : H9L22000G-OS 5 9 5 [8 0 - 120 ) KNO XWC-001 S 12/22-12/29/0 9 935606 5 Dilutio nFactor ; 5

_HOTE(S ) : ' \ Calculation

s ar c pcrrormc

d befor e roundin

g i d avoi d round-of

f error s i n calculaie

d results .



## VES01821 5

### 44

LABORATOR

YCONTROL SAMPL E DATA REPORT Genera l Chemistr y Clien t Lo t H9L14040 3 Matri x: SOLI D

SPIK E MEASURE

D • PERCN T PREPARATION - PRE P PARAMETER AMOUN T AMOUN

T UNIT S RECVR YMETHO

D ANALYSI S DAT E BATC H # Tota l Chlorin e Work Orde r # : LRGLV1A C LC S Lot-Sample# : H9L220000-06 5 1000 0 948 0 mg/k g 9 5 KNO XWC-001 6 12/22-12/29/0 9 935606 5 Dilutio nFactor : 5 NOTE(S ) ; • ; Calculation

s ar e performe

d befor e roundin g i o avoi d round-of

f error s i n calculate

d rcsulis .



## VES01821 6

### 4 5

MATRI XSPIK E SAMPL E EVALUATION REPOR T
Clien t Lo t #... : H9L14040 3 Dat e Sample d : 12/08/0 9 Genera l Chemistr y
Dat e Received.. : 12/11/0 9 Matri x: WAST E

PARAMETER PERCENT RECOVER Y RECOVER

YLIMIT S RPD RPD LIMIT S METHO

D PREPARATION ANALYSI S DAT E PRE P

BATC H # Tota l Chlorin e

100 - 9 9 WOft : LQ2TG1AG-MS/LQ2TG1AH-MS D M S Lot-Sampl e # : H9L14O403-00 5 (8 0 - 120 ) KNO XWC-001 6 12/17-12/18/0 9 935108 2 (8 0 - 120 ) 1. 5 (0-10 ) KNO XWC-001 6 12/17-12/18/0 9 935108 2 Dilutio nFactor : 6. S B Tota l Chlorin e

8 7 9 7 W0# : LQ2TR1AE-MS/LQ2TR1AF-MS D M S Lot-Sampl e # : H9L140403-01 3 (8 0 - 120 ) KNO XWC-001 6 12/21-12/28/0 9 935203 1 (8 0 - 120 ) 1. 0 (0-10 ) KNO XWC-001 6 12/21-12/28/0 9 935203 1 Dilutio n Factor : 9.5 7 NOTE( S ) : Calculation

s ar c performe

d befor e roundin g t o avoi d round-of

f error s i n calculate

d results .



## VES01821 7

### 4 6

MATRI XSPIK E SAMPL E DAT A REPOR T Genera l Chemistr y Clien t Lo t #.. . Dat e Sampled — : H9L140403 ' : 12/08/0 9 Dat e Received.. : 12/11/0 9 Matrxx . WAST E
SAMPL E SPIK E MEASR D PARAMETER AMOUN T AMT Tota l Chlorin e

98 8 1400 0 98 8 1440 0 AMOUN T UNIT S PERCN T RECVR YRPD • METHO

D PREPARATION - PRE P

ANALYSI S DAT E BATC H # W 0#J LQ2TG1AG-MS/LQ2TG1AH-MS D M S Lot-Sampl e # : H9L140403-00 5 1490 0 mg/kg 10 0 KNO X WC-001 6 12/17-12/18/0 9 935108 2 1520 0 mg/kg 9 9 1. 5 KNO X WC-001 6 12/17-12/18/0 9 935108 2 Dilutio nFactor : 6.3 8 Tota l Chlorin e

1530 0 1910 0 1530 0 1730 0 WO# : LQ2TR1AB-MS/LQ2TR1AF-MS D M S Lot-Sampl e # : H9L140403-01 3 3180 0 mg/kg 8 7 KNO X WC-001 6 12/21-12/28/0 9 935203 1 3220 0 mg/kg 9 7 1. 0 KNO X WC-001 6 12/21-12/2B/0 9 935203 1 Dilutio nFactor : 9.5 7 NOTS(S ) Calculation

s ar c pcrrormc

d befor e roundin

g t o avoi d round-of

f error s i n calculate

d results .



## VES01821 8

### 4 7

MATRI XSPIK E SAMPL E EVALUATIO N REPOR T
Cliea t Lo t #.. . Dat e Sampled... . : H9L14040 3 : 12/09/0 9 Genera l Chemistr y
Dat e Received . 12/11/0 9 Matri x: SOLI D

PARAMETER Tota l Chlorin e

8 8 9 1 PERCENT RECOVER

Y RECOVER

YLIMIT S RPD RPD LIMIT S METHO

D PREPARATION ANALYSI S DAT E PRE P

BATC H # WO# : LQ2TP1AG-MS/LQ2TP1AH-MS D M S Lot-Sampl e # : H9L140403-01 1 (8 0 - 120 ) KNO XWC-001 6 12/22-12/29/0 9 935606 5 (8 0 - 120 ) 2. 2 (0-10 ) KNO XWC-001 6 12/22-12/29/0 9 935606 5 Dilufci-oi l Factor ; 5.0 1 NOTE(S ) Calculation

s ar c performe

d befor e roundin

g t o avoi d round-of

f error s i n calculate

d results .



## VES01821 9

### 4 8

MATRIX.SPIK

E SAMPL E DAT A REPOR T Genera l CSaemi s try Clien t Lo t #... : H9L14040 3 

### Dat e Sampled— : 12/09/0 9 Matri x: SOLI D Dat e Received.. : 12/11/0 9
PARAMETER SAMPL E SPIK E

AMOUN T AM T Tota l Chlorin e

13 4 13 4 1000 0

994 0 MEASR

D AMOUN T UNIT S •PERCN T RECVR YRPD METHO

D PREPARATION ANALYSI S DAT E PRE P BATC H # WO# : LQ2TP1AG-MS/LQ2TP1AH-MS D M S Lot-Sampl e # : H9L14O403-01 1 896 0 mg/kg 8 8 KNO XWC-001 6 12/22-12/29/0 9 935606 5 916 0 mg/k

g 9 1 2. 2 KNO XWC-001 6 12/22-12/29/0 9 935606 5 Dilutio nFactor : 5. O X HOTE(S ) : Calcutiiion

s or e pcrrormc

d befor e roundin

g r o avoi d round-of

f error s h i calculate

d results .



## VES01822 0

### 4 9

Clien t Lo t # . Dat e Sampled .
PARA M RESUL T As hConten t

137 0 SAMPL E DUPLICAT E EVALUATIO N REPOR T Genera l Chemistr y

. : H9L14040 3 Wor k Orde r #-.. : LQ2TC-SMP LQ2TC-DUP .
. : 12/08/0 9 Dat e Received.. : 12/11/0 9 DUPLICAT E RESUL T UNIT S RPD RP D LIMI T METHO D Matri x: WAST E

PREPARATION - PRE P ANALYSI S DAT E BATC H # 134 0 mg/k

g 1. 8 Dilutio nFactor : 1 S D Lot-Sampl e # : H9L140403-00 1 (0-10 ) ASTM

D482-00 a 12/29-12/31/0 9 936343 4



## VES01822 1

### 50

SAMPL E DUPLICAT E EVALUATION REPOR T Genera l Chemistr y Clien t Lo t H9L14040 3 Wor k Orde r LQ2TG-SM P Matri x: WAST E LQ2TG-DUP Dat e Sampled... : 12/09/0 9 Dat e Received.. : 12/11/0 9 DUPLICAT E RPD PREPARATION - PRE P PARA M RESUL T RESUL T UNIT S RPD LIMI T METHO D ANALYSI S DAT E BATC H # Gros s Calorifi c S D Lot-Sampl e # : H9L140403-00 5 Valu e N

D N

D BTU/l b0 (0-10 ) AST M D240-0 2 12/22/0 9 935634 8 Dilutio nFactor : l As hConten t S D Lot-Sampl e # : H9L140403-0O 5 190 0 188 0 mg/k g 1. 1 (0-10 ) AST M D482-00 a 12/29-12/31/0 9 936343 4 Dilutio nFactor : 1 Tota l Chlorin e S D Lot-Sampl e # : H9L140403-00 5 98 8 99 9 • mg/k g 1. 2 (0-10 ) KNO XWC-001 6 12/17-12/18/0 9 935108 2 Dilutio nFactor : 1.-4 5



## VES01822 2

### 51

SAMPL E DUPLICAT E EVALUATIO N REPOR T Genera l Chemistr y Clien t Lo t # . .. : H9L14040 3 Wor k Orde r #.-. : LQ2TP-SMP Matri x: SOLI D LQ2TP-DUP Dat e Sampled... : 12/09/0 9 Dat e Received.. : 12/11/0 9 DUPLICAT E . RP D PREPARATION - PRE P PARA M RESUL T RESUL T UNIT S RPD LIMI T METHOD , ANALYSI S DAT E BATC H # Gros s Calorifi c S D Lot-Sampl e # : H9L140403-01 1 Valu e N

D N

D BTU/l b0 (0-10 ) AST M D586S-0 0 12/16/0 9 935003 2 Dilutio nFactor : 1 As hConten t ' S D Lot-Sampl e # : H9L140403-01 1

71300 0 70300 0 mg/k g 1. 3 (0-10 ) ASTM D482-00 a 12/29-12/31/0 9 936343 3 Dilutio nFactor : 1 Tota l Chlorin e S D Lot-Sampl e # : H9L140403-01 1 13 4 B 13 2 B mg/k g 1. 6 (0-10 ) KNO XWC-001 6 12/22-12/29/0 9 935606 5 Dilutio nFactor : 1 NOTE(S ) : Calculalioui

s ar c performe

d befor e roundin g l o avoi d round-of

f error s i n calculaie

d results . B Estimate

d result . Resul ti s les s tha n Rl .



## VES01822 3

### 5 2

Clien t Lo t #. , Dat e Sampled. .
PARA M RESUL T Gros s Calorifi c Valu e 1020 0
Tota l Chlorin e 1530 0 H9L14040 3

12/08/0 9 DUPLICAT E RESUL T SAMPL E DUPLICAT E EVALUATIO N REPOR T Genera l Chemistr y Wor k Orde r #... : LQ2TR-SM P LQ2TR-DUP Dat e Received.. : 12/11/0 9

990 0

1520 0 UNIT S RPD RPD LIMI T METHO D Matri x: WAST E

PREPARATION - PRE P ANALYSI S DAT E BATC H # BTU/l b2. 9 Dilutio nFactor : l S D Lot-Sampl e # : H9L140403-01 3 (0-10 ) ASTM

D240-0 2 12/23/0. 9 935718 8
S D Lot-Sampl e # : H9L140403-01 3 mg/k g 0.1 9 (0-10 ) KNO XWC-001 6 12/21-12/28/0 9 935203 1 Dilutio nFactor : 8.3 9



## VES01822 4

### 53

Clien t Lo t #... : H9L14040 3 Dat e Sampled... : 12/08/0 9 SAMPL E DUPLICAT E EVALUATIO N REPOR T Genera l Chemistr y Wor k Orde r #... : LQ2T3-SMP LQ2T3-DO T Dat e Received.. : 12/11/0 9
PARA M RESUL T Tota l Chlorin e 497 0 DUPLICAT E

RESUL T 479 0 Matrox . WAST E

UNIT S RPD

RPD LIMI T METHO D PREPARATION - PRE P

ANALYSI S DAT E BATC H # S D Lot-Sampl e # : H9L140403-01 9 mg/k g 3. 6 (0-10 ) KNO XWC-001 6 12/21-12/28/0 9 935203 1 Dilutio nFactor s 4. 2



## VES01822 5

### 54

Cliecn t Lo t #... : H9L14040 3 Dat a Sampled... : 12/10/0 9 SAMPL E DUPLICAT E EVALUATIO N REPOR T Genera l Chemistr y Work . Orde r #. . . : LQ2T5-SM P LQ2T5-DUP Dat e Received.. : 12/11/0 9
PARA M RESUL T DUPLICAT E

RESUL T Gros s Calorifi c Valu e N

D N

D UNIT S RP D RPD LIMI T METHO D Matri x: WAST E

PREPARATION - PRE P ANALYSI S DAT E BATC H # BTU/l b0 Dilutio nFactor : 1 S D Lot-Sampl e # : H9L140403-02 1 (0-10 ) AST

M D240-0 2 12/23/0 9 935718 8



## VES01822 6

### 55



# Sample Receip t

Documentation

VES01822 7

## Sampl e Traceabilit y Lis t AECO M
Site o f Program : VeoliaE S Tec h Sampl e Date : itfsc- \2,f/o/o^> Projec tLocation : Sauget , I L P.O. * Typ e o f Proqram ; CP T Dat e Shipped : Laboratory : TestAmerica, Inc . Knoxville , T N Project * 60133216 . Progra m Office : Syracuse N Y Shipper/

Steve n Mil o Recovery : Jef f Gorma n Laboratory : TestAmerica, Inc . Knoxville , T N Progra m Contact : Jef f Gorma n FedE x Ai rBil l ft Ite m Sampl e I D Code Sample Matri x Sampl e Descriptio

n Analitloa l Parameter

s Specia l Instruction

s 1 HBTU-U2-M23A-R 1 Liqui d Hig

h Btu, Uni

t2 , Ru n 1 Physica l Parameter

s 5 C l -fofaA

r.U l ( 2 HBTU-U2-M23A-R 2 Liqui d Hig

h Btu, Uni

t2 , Ru n Z Physica l Parameter

s & C l Tok J ^ 3 HBTU-U2-W123A-R3 Liqui d Hig

h Btu , Uni t2 , Ru n 3 Physica l Parameter

s & C l ' f^ , 7 4 S LBTU-U2-M23A-R 1 Liqui d Lo

w Btu, Uni

t2 , Ru n 1 Physica l Parameter

s & Cl T o I 6 LBTU-U2-M23A-R 2 Liqui d Lo

w Btu, Uni

t2 , Ru n 2 Physica l Parameter

s 5 C l ' •fo.fa

j c X 7 LBTU-U2-M23A-R 3 Liqui d Lo

w Btu , Uni t2 , Ru n 3 Physica l Parameter

s & C t-^uf f.

f/<7ie.ije.£ > 8 9 SF -U2-M23A-R 1 Liqui d Specialit

y Feeder , Uni t2 , Ru n 1 Physica

l Parameter

s & C l -fSfc, /

f10 SF-U2-WI23A-R 2 Liqui d Specilait

y Feeder , Uni t2 , Ru n 2 Physica

l Parameter

s & C ) ' /

, 11 SF-U2-M23A-R 3 Liqui d Specialit

y Feeder , Uni t2. Ru n 3 Physica

l Parameter

s & C l ' ffifa f 1 2 1 1 3 CS-U2-M23A-R 1 Solid Containerize d Solids , Uni

t2 , Ru n 1 Physica

l Parameter

s SC I -y

S fe. / 1 4 CS -U2-M23A-R 2 Soli d Containerize d Solids , Uni

t2 , Ru n 2 Physica

l Parameter

s S Cl -rCf e I t 1 5 CS-U2-M23A-R 3 Soli d Containerize d Solids , Uni

t2 , Ru n 3 Physica

l Parameter

s & C l 1 -7^ , ,

f C.hloit.i« 16 1 7 18 1 9 2 0 Fiel d Notes / Comment

s 1. Physica l Parameter

s = Tota l chlorides, hea

tconten t& as h content

. 2 . C l Page 1 o f _ 2 Relinquishe

d B y (print) : Dale : SH ««r * H .l o |2«t » Signature : . Time : 

## -fYuj L I7CO Relinquishe d By (print) : Date : Signature : Time : Relinquishe d B y (print) : Date : Signature : Time : [Receive d b y La b (print) : Date : Signature : Time : Receive d B y (print) : Date : ^loftature^

_

. Time : 

# %TMth DVC D Receive d B y (print) : Date : Signature : Time : Receive d B y (print) : Date : Signature : Time : [Analytica l Laborator

y Destination : TestAmericaInc

. 5B1 5 Middlebroo

kPik e Knoxville , T N 37921 I Attn : Mr

. Kevi n Woodcoc

k885-291-300

0 

## VES01822 8

# Sampl e Traceabilit y List AECO M
Sit e o f Program : Veoli aE S Tech Sampl e Date : - ll-lO^Sl Projec

tLocation ; Sauqet , I L P.O . #

: Typ e o f Program : CP T Dat e Shipped : / JZ - /< 3 7 Laboratory : Tes tAmerica, Inc

. Knoxville

, T N Projec t# : 6013321 B Progra m Office : Syracuse N Y Shippe r/

Steve n Mil o Recovery : Jef f Gorma n Laboratory : Tes tAmerica, Inc

. Knoxville

, T N Progra m Contact : Jef f Gorma n FedE x Ai rBill # : Ite m Sampl e I D Code Sampl e Matri x Sampl e Descriptio

n Analitlca l Parameter

s Specia l instruction

s 2 1 HBTU-U2-M26A-R 1 Liqui d Hig

h Btu , Uni t2 , Ru n 1 Physica l Parameter

s & C i -fS-fa l 2 2 HBTU-U2.M26A-R 2 Liqui d Hig

h Btu , Uni t2 , Ru n 2 Physica l Parameter

s & C l ' -rS4r J f 2 3 HBTU-U2-M26A-R 3 Liqui d Hig

h Btu , Uni t2, Ru n 3 Physica l Parameter

s & C l ' | ~ 2 4 1 2 5 LBTU-U2-M26A-R 1 Liqui d Lo

w Btu , Uni t2 , Ru n 1 Physica l Parameter

s & C l

## ~Jofe,l

/ ' if l cl n tie . » 2 6 LBTU-U2-M26A-R 2 Liqui d Lo

w Btu , Uni l 2 , Ru n 2 Physica l Parameter

s & C l -r^-fc. / 27 LBTU-U2-M26A-R 3 Liqui d Lo

w Btu , Uni t2 , Ru n 3 Physica l Parameter

s & C l ' fok^1 2 8 2 9 SF-U2-M26A-R 1 Liqui d Specialit

y Feeder , Uni t2, Ru n 1 Physica

l Parameter

s & C l ( ~X~ o h i1 30 SF-U2-M26A-R 2 Liqui d Specilail

y Feeder , Uni t2 , Ru n 2 Physica

l Parameter

s & C l -T^-fa J 3 1 SF-U2-M26A-R 3 Liqui d Specialit

y Feeder , Uni t2 , Ru n 3 Physica

l Parameter

s & C l ^-f

, feJ | \r\

\r\f.\n*> 3 2 3 3 CS-U2-M26A-R 1 Soli d Containerize d Solids , Uni

t2 , Ru n 1 Physica

l Parameter

s S Cl | -t^,t a j r 3 4 CS-U2-WI26A-R 2 Solid Containerize d Solids , Uni

t2 , Ru n 2 Physica

l Parameter

s & C l ' ^rtJkiA 3 5 CS-U2-W126A-R3 Soli d Containerize d Solids, Uni

t2 , Ru n 3 Physica

l Parameter

s & C l -^-j^ J 3 6 

## { 0 PflXt ^ 

## (35'JO fcXYi ^PN T Pin 3 7 

## : Wpdf 9\M 38 

## ^$1 * <o1f

^ Pin 3 9 

## 51A%q<*6

L 40 

# m Fiel d Notes / Comment

s 1 . Physica l Parameter

s = Tota l chlorides, hea

tconten t& as h content

. 2. C l Page _2_

_o f 2 Relinquishe

d By (print) : Date ; 

## 5ioaa n ti.'l o U/JO/O T Signature : J Time : 

## Stettin ~4WtJb iloo Relinquishe d B y (print) : Date : Signature : Time : Relinquishe d B y (print) : Date : Signature : Time : Receive d b y La b (print) : Date : Signature : Time : Receive d B y (print) : Dale : sSignature : Time : 

# JP^m h lO'.D O Receive

d B y (print) : Date : Signature : Time : Receive d By (print) : Date : Signature : Time : Analytica l Laborator

y Destination : TestAmeric

aInc . 581 5 Middlebroo

k Pik e Knoxville

, T N 3792

1 Attn : Mr

. Kevi n Woodcoc

k 865-291-300

0 O l 

## VES01822 9

### TESTAMERIC A KNOXVILL E SAMPL E RECEIPT/CONDITIO N UPON RECEIP T ANOMAL Y CHECKLIS T Lo tNumber : MU^Hl k Revie w Items M o | I f

No , whatwa

s th e problem ? Comments/Action s Take n 1. D o sampl

e containerlabels matc h COC ? (IDs , Dates , Times ) 

## {

/ B l aD o no tmatc h CO C • l b Incomplet

e information O l c Markin g smeare d 0 I d Labe l tor

n • l e N o labe

l • l f CO C no

treceive d • l g Other : l f \ P&t , UM X 51ftmiR B IJBTU, - 1. D o sampl

e containerlabels matc h COC ? (IDs , Dates , Times ) 

## {

/ B l aD o no tmatc h CO C • l b Incomplet

e information O l c Markin g smeare d 0 I d Labe l tor

n • l e N o labe

l • l f CO C no

treceive d • l g Other : iAZ. " WTJ / J A . - kl. 1. D o sampl

e containerlabels matc h COC ? (IDs , Dates , Times ) 

## {

/ B l aD o no tmatc h CO C • l b Incomplet

e information O l c Markin g smeare d 0 I d Labe l tor

n • l e N o labe

l • l f CO C no

treceive d • l g Other : ?jaKSVM \\SV7 . 1 (A W L ST S 1. D o sampl

e containerlabels matc h COC ? (IDs , Dates , Times ) 

## {

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e information O l c Markin g smeare d 0 I d Labe l tor

n • l e N o labe

l • l f CO C no

treceive d • l g Other : 

### LJROk-UZL.- frATXeA- fiZ> .LA D <3 |\ J 1. D o sampl

e containerlabels matc h COC ? (IDs , Dates , Times ) 

## {

/ B l aD o no tmatc h CO C • l b Incomplet

e information O l c Markin g smeare d 0 I d Labe l tor

n • l e N o labe

l • l f CO C no

treceive d • l g Other : 1. D o sampl

e containerlabels matc h COC ? (IDs , Dates , Times ) 

## {

/ B l aD o no tmatc h CO C • l b Incomplet

e information O l c Markin g smeare d 0 I d Labe l tor

n • l e N o labe

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treceive d • l g Other : 1. D o sampl

e containerlabels matc h COC ? (IDs , Dates , Times ) 

## {

/ B l aD o no tmatc h CO C • l b Incomplet

e information O l c Markin g smeare d 0 I d Labe l tor

n • l e N o labe

l • l f CO C no

treceive d • l g Other : 1. D o sampl

e containerlabels matc h COC ? (IDs , Dates , Times ) 

## {

/ B l aD o no tmatc h CO C • l b Incomplet

e information O l c Markin g smeare d 0 I d Labe l tor

n • l e N o labe

l • l f CO C no

treceive d • l g Other : 2. I s th e coole rtemperatur

e within limits ? (

> freezin g temp , o f wate rt o 6"C ; NC , 1668,16T3B : 0-4°C ; VOST : 10"C;MA:2-6 , 'C ) 

# J • 2 aTenr o Blan k = 2. I s th e coole rtemperatur

e within limits ? (

> freezin g temp , o f wate rt o 6"C ; NC , 1668,16T3B : 0-4°C ; VOST : 10"C;MA:2-6 , 'C ) 

# J • 2 b Coole rTem p = 2. I s th e coole rtemperatur

e within limits ? (

> freezin g temp , o f wate rt o 6"C ; NC , 1668,16T3B : 0-4°C ; VOST : 10"C;MA:2-6 , 'C ) 

# J 3 . Were sample

s received wit

h correc tchemica

l preservativ

e (excludin g Encore) ? 

# V • 3aSample preservativ e =

_ x , 3 . Were sample

s received wit

h correc tchemica

l preservativ

e (excludin g Encore) ? 

# V • 3aSample preservativ e =

_ x , 4. Wer

e custod y seal s present/intac

ton coole rand/or containers ? 

# 7 S I 4 a No tpresen

t 0 4 b No tintac

t D 4 c Other : 4. Wer

e custod y seal s present/intac

ton coole rand/or containers ? 

# 7 S I 4 a No tpresen

t 0 4 b No tintac

t D 4 c Other : 4. Wer

e custod y seal s present/intac

ton coole rand/or containers ? 

# 7 S I 4 a No tpresen

t 0 4 b No tintac

t D 4 c Other : 5. Wer

e al l o f th e sample

s listed o

n th e CO C received ? 0 5aSample s received-noto n CO C Q 5b Sample

s no treceived-on CO C 5. Wer

e al l o f th e sample

s listed o

n th e CO C received ? 0 5aSample s received-noto n CO C Q 5b Sample

s no treceived-on CO C 6 . Wer

e ail o f th e sampl e container

s received intact ? 

## •j / • 6aLeakin g 0 6b Broken 6 . Wer

e ail o f th e sampl e container

s received intact ? 

## •j / • 6aLeakin g 0 6b Broken 7 . Wer e VO A sample

s received withou

theadspace ? y _ 

### V D 7aHeadspac e (VO A only ) 8. Wer

e sample

s received in appropriat e containers ? 

### V D 8 aImprope rcontainer 9 , Di d yb u chec

k fo rresidua

l chlorine , i f

necessary ? / 

## J • 9 aCoul d no tbe determine

d du e t o matri x interferenc

e 9 , Di d yb u chec

k fo rresidua

l chlorine , i f

necessary ? / 

## J • 9 aCoul d no tbe determine

d du e t o matri x interferenc

e 10 . Were sample

s received withi n holdin g time ? I M • 10 aHoldin g tim e expired 11 . Fo rra

d samples , wa

s sampl e activit y info , provided ? • Incomplet e information 12 . Fo r1613

B wate rsample

s is pH<9 ? 

### y If no , wa s p H adjuste

d t o p H 7 - 9 wit h sulfuri c acid ? 12 . Fo r1613

B wate rsample

s is pH<9 ? 

### y If no , wa s p H adjuste

d t o p H 7 - 9 wit h sulfuri c acid ? 13 . Ar e th

e shippin g container

s intact? f D 13 a Leakin g • 13 b Other : 13 . Ar e th

e shippin g container

s intact? f D 13 a Leakin g • 13 b Other : 14. Wa s CO C relinquished ? (Signed/Dated/Timed ) 

# I • 14 aNo trelinquished IS . Ar e tests/parameter s listed fo reac

h sample ? D 15a Incomplet e information 16 . I s th e matri x ofth e sample

s noted ? D 15aIncomplet e information 17. I s th e date/tim

e o f sample collectio n noted ? 

# 7 0 15 aIncomplet

e information 18. I s th e clientan

d projec tname/ #identified ? 

### J 

# / • 15 aIncomplet

e information 19. Wa s th e sample

ridentifie d o n th

e COC ? 

# / Ouote# : ftM-7?, c 'i . P M Instructions : 

### Sampl e Receivin

g Assoc! ) QA026R21.doc , 090409

CO 

## VES01823 0

### 5 9

### 60



# Sample Summar

y

VES01823 2

### 61

Lot-Sampl e # . Dat e Sampled .
PARAMETE

R Ash . Conten t
Gros s Calorifi c Valu e
Tota l Chlorin e AECOM , In c Clien t Sampl e TD : HBTU-U2-M23A-R 1

Genera l Chemistr y H9L140403-00 1 Wor k Orde r : LQ2T C 12/08/0 3 Dat e Received.. : 12/11/0 9 Matri x: WAST E

RESUL T R L UNIT S 137 0 20 0 rag/kg

Dilutio nFactor : 1 919 0 180 0 BTU/l b

Dilutio nFactor : 1 1620 0 169 0 mg/kg

Dilutio nFactor : 8.4 6 _METHO D AST M D482-00 a MD L 5 1 AST M D240-0 2 HD L 1 3 0 KNO XHC-001 6 HD L : 51 0 PREPARATION - PRE P ANALYSI S DAT S BATC H ft 12/29-12/31/0 9 936343 4 12/22/0 9 935634 8
12/17-12/18/0 9 935108 2



## VES01823 3

### 62

AECOM , In c Clien t Sampl e ID : HBTO-TJ2-M23A-R 2

Genera l Chemistr y Lot-Sampl e - . H9L140403-00 2 Wor k Orde r #... : LQ2T D Matrix. . : WAST E Dat e Sampled... : 12/09/0 9 Dat e Received . 12/11/0 9
PARAMETER RESUL T R L UNIT S As hConten t
Gros s Calorifi c VaLu e
Tota l Chlorin e 191 0 20 0 mg/k g Dilutio nFactor : 1 943 0 180 0 BTD/I b

Dilutio nFactor : 1 1420 0 164 0 mg/k g

Dilutio nFactor : 8.1 8 _METHO D AST M D482-00 a MDIJ . : 5 1 ASTM D240-0 2
MD L 13 0 KNO XWC-001 6 MD L 49 0 PREPARATION - PRE P ANALYSI S DAT E BATCH # 12/29-12/31/0 9 936343 4 12/22/0 9 935634 8
12/17-12/18/0 9 935108 2



## VES01823 4

### 6 3

AECOM , In c Clien t Sampl e ID : HBTO-02-M23A-R 3

Genera l Chemistr y Lot-Sampl e : H9L140403-00 3 Wor k Orde r : LQ2T E Matri x: WAST E Dat e Sampled... : 12/10/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRE P PARAMETE

R RESUL T S L UNIT S METHO D ANALYSI S DAT E BATCH # As hConten t 249 0 20 0 mg/kg ASTM D482-00 a 12/29-12/31/0 9 936343 4 Dilutio nFactor : 1 MDI . : 5 1 Gros s Calorifi c 987 0 180 0 BTTJ/l bASTM D240-0 2 12/22/0 9 935634 8 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 1390 0 170 0 mg/k g KNO XWC-001 6 12/17-12/18/0 9 935108 2 Dilutio nFactor : 8.5 1 MD L : 51 0



## VES01823 5

### 64

AECOM , In c Clien t Sampl e ID : LBTU-U2-M23A-R 1

Genera l Chemistr y Lot-Sampl e #... : H9L140403-00 4 Wor k Orde r «... : LQ2T F Dat e Sampled... : 12/08/0 9 Dat e Received.. : 12/11/0 9 Matri x: WAST E

PARAMETE

R As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e RESUL T R L UNIT S 234 0 20 0 mg/kg

Dilutio nFactor s 1 N D 180 0 BTU/l b

Dilutio nFactor ; 1 112 0 30 6 mg/kg

Dilutio nFactor s 1.S 3 _METHO D AST M D4B2-00 a MD L : B l AST M D24O-0 2 HD L , 13 0 KNO XWC-001 6 HD L : 9 2 PREPARATION - PRE P ANALYSI S DAT E BATCH # 12/29-12/31/0 9 936343 4 12/22/0 9 935634 B
12/17-12/18/0 9 935108 2



## VES01823 6

### 6 5

Lot-Sampl e # . Dat e Sampled 

### PARAMETE

R As hConten t
Gros s Calorifi c Valu e 

### Tota l Chlorin e AECOM , In c Clien t Sampl e ID : LBTO-U2-M23A-R 2

Genera l Chemistr y H9L140403-00 5 Wor k Orde r #... : LQ2T G 12/09/0 9 Dat e Received.. : 12/11/0 9 Matri x: WAST E

RESUL T R L UNIT S 190 0 20 0 mg/kg

Dilutio nFactor : 1 N D 180 0 BTU/l b

Dilutio nFactor : 1 98 8 29 0 mg/k g Dilutio nFactor : 1.4 5 _METHO D ASTM D482-00 a MD L : 5 1 AST M D240-0 2 MD L : 13 0 KNO XWC-001 6 MD L .... : 8 7 PREPARATION - PRE P ANALYSI S DAT E BATC H # 12/29-12/31/0 9 936343 4 12/22/0 9 935634 8
12/17-12/18/0 9 935108 2



## VES01823 7

### 6 6

AECOM , In c Clien t Sampl e ID : LBTU-U2-M23A-R 3

Genera l Chemistr y Lot-Sampl e #... : H9L140403-00 6 Wor k Orde r #... : LQ2T H Matrix. . : WASTE Dat e Sampled... : 12/10/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRE P PARAMETER RESDL T R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 229 0 20 0 mg/k g ASTM D482-O0 a 12/29-12/31/0 9 936343 4 Dilutio nFactor s 1 MD L : 5 1 Gros s Calorifi c 13 4 B 180 0 BTU/l bASTM D240-0 2 12/22/0 9 935634 8 • Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 114 0 28 8 mg/k g KNO XWC-001 6 12/17-12/18/0 9 935108 2 Dilutio nFactor : 1.4 4 MD L 8 6 MOTB(S ) : t . R L Rsporiin

s Limi t B Estimate

d result . Resul ti s les s Ula n RL .



## VES01823 8

### 6 7

AECOM , In c Clien t Sampl e ID : SF-TJ2-M23A-R 1

Genera l Chemistr y Lot-Sampl e H9L140403-00 7 Wor k Orde r : LQ2T J Matri x: WAST E Dat e Sampled... : 12/08/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRE P PARAMETER RESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 742 0 20 0 mg/k g ASTM D482-00 a 12/29-12/31/0 9 936343 4 Dilutio nFactor : 1 MD L : 5 1 Gros s Calorifi c N D 180 0 BTU/l bASTM D240-0 2 12/23/0 9 935718 8 Valu e Dilutio nFactor : 1 MDL . : 13 0 Tota l Chlorin e 473 0 84 0 mg/kg KNO XWC-001 6 12/21-12/28/0 9 935203 1 Dilutio nFactor : 4. 2 MDL... . : 25 0



## VES01823 9

### 68

AECOM , In c Clien t Sampl e XD : SF-TJ2-M23A-H 2

Genera l Chemistr y Lot-Sampl e #... : H9L140403-00 8 Wor k Orde r LQ2T KMatri x: WAST E Dat e Sample d : 12 /09 /0 9 Dat e Received.. : 12/11 /0 9 PREPARATION - PRE P PARAMETE

R RESUL T RL UNIT S METHO D ANALYSI S DAT E BATCH # As hConten t 772 0 20 0 mg/k g ASTM D482-00 a 12/29-12/31/0 9 93S343 4 Dilutio nFactor : 1 MD L . : S I Gros s Calorifi c N D 180 0 BTU/l bASTM D240-0 2 12/23/0 9 935718 8 Valu e Dilutio nFactor : 1 MD L s 13 0 Tota l Chlorin e 483 0 82 4 mg/kg KNO X WC-001 6 12/21-12/28/0 9 935203 1 Dilutio nFactor : 4 .1 2 MDL.... . : 2S 0



## VES01824 0

### 69

AECOM , In c Clien t Sampl e ID : SF-U2-M23A-E 3

Genera l Chemistr y Lot-Sampl e #... : H9L140403-00 9 Wor k Orde r LQ2T L Dat e Sampled. : 12/10/0 9 Dat e Received.. : 12/11/0 9
PARAMETER RESUL T RL UNIT S METHO D Matrix . : WAST E

PREPARATION - PRE P ANALYSI S DAT E BATCH # As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 754 0 20 0 mg/k g Dilutio nFactor : 1 N D 180 0 BTU/l b

Dilutio nFactor : 1 481 0 83 8 mg/k g

Dilutio nFactor : 4.1 9 AST M D482-00 a MD L : 5 1 ASTM D240-0 2 MD L : 130 -KNO XWC-001 6 MD L : 25 0 12/29-12/31/0 9 936343 4 12/23/0 9 935718 8
12/21-12/28/0 9 935203 1



## VES01824 1

### 7 0

AECOM , In c Clien t Sampl e ID : CS-U2-M23A-R 1

Genera l Chemistr y Lot-Sampl e #... : H9L140403-01 0 Wor k Orde r #.. . = LQ2T M Matri x: SOLI D Dat e Sampled... : 12/OB/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRE P PARAMETER RESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 71600 0 20 0 mg/k g AST M D4B2-O0 a 12/29-12/31/0 9 936343 3 Dilutio nFactor : 1 MD L : S I Gros s Calorifi c N D 180 0 BTU/l bAST M D5865-0 0 12/15/0 9 935003 2 Valu e Dilutio nFactor : 1 HD L : 13 0 Tota l Chlorin e 12 9 B 20 2 mg/k g KNO XWC-001 6 12/22-12/29/0 9 935606 5 Dilutio nFactor : 1.0 1 MD L : 6 1 MOT S <S ) : r _, R L Rtportin

g Limi t B Estimate

d result . Resul ti s les s tha n RL .



## VES01824 2

### 7 1

AECOM , In c Clien t Sampl e ID : CS-TJ2-M23A-R 2

Genera l Chemistr y Lot-Sampl e #... : H9L140403-01 1 Wor k Orde r #... : LQ2T P Dat e Sampled... : 12/09/0 9 Dat e Received.. : 12/11/0 9 Matrix . SOLI D

PARAMETE

R RESUL T R L UNIT S As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 71300 0 20 0 mg/k g Dilutio nFactor s 1 N D 180 0 BTU/l b

Dilutio nFactor : 1 13 4 B 20 0 mg/k g

Dilutio nFactor : 1 _METHO D AST M D482-00 a MDL . : 5 1 AST M D58S5-0 0 MD L : 13 0 KNO XWC-001 6 MD L . s S

O PREPARATION - PRE P ANALYSI S DAT E BATC H # 12/29-12/31/0 9 936343 3 12/16/0 3 935003 2
12/22-12/29/0 9 935606 5 NOTE(S ) : R L Reportin g Limi i B Estimate

dresult . Resul

t i s les s tha nRL .



## VES01824 3

### 72

AECOM , In c Clien t Sampl e ID : CS-U2-M23A.-R3

Genera l Chemistr y Lot-Sampl e ft-..: H9L140403-01 2 Wor k Orde x#.-. : LQ2T Q Matri x: SOLI D Dat e Sample d : 12/10 /0 9 Dat e Received.. : 12/11 /0 9 PREPARATION - PRE P PARAMETER RESUL T R L UNIT S METHO D ANALYSI S DAT E BATCH # As hConten t 70800 0 20 0 mg/k g AST M D482-00 a 12/29-12/31/0 9 936343 3 Dilutio nFactor : 1 HD L . : 5 1 Gros s Calorifi c N D .180 0 BTU/l bASTM D5865-0 0 12/16/0 9 935003 2 VaLu e Dilutio nFactor : 1 HD L : 13 0 Tota l Chlorin e 14 1 B 20 0 mg/k g KNO X WC-001 6 12/22-12/29/0 9 935606 5 Dilutio nFactor : 1 MD L : S

O NOTE(S ) : : R L Repottin

g Limi t B Estimate

d result. Resul

ti s les s tha n RL .



## VES01824 4

### 7 3

AECOM , In c Clien t Sampl e ID : HBTO-02-M26A-R 1

• Genera l Chemistr y Lot-Sampl e #... : H9L140403-01 3 Wor k Orde r #-.. : LQ2T R Matri x: WAST E Dat e Sample d : 12 /08/0 9 Dat e Received.. : 12/11 /0 ? PREPARATION - PRE P PARAMETER RESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 136 0 20 0 mg/k g AST M D482-00 a 12/29-12/31/0 9 936343 4 Dilutio nFactor. - 1 MD L : 5 1 Gros s Calorifi c . 1020 0 180 0 BTtr/l bAST M D240-0 2 12/23/0 9 935718 8 Valu e Dilutio nFactor. - 1 MD L 13 0 Tota l Chlorin e 1530 0 168 0 mg/k g KNO X WC-001 6 12/21-12/28/0 9 935203 1 Dilutio nFactor : 8.3 9 MD L : 50 0



## VES01824 5

### 7 4

AECOM , In c Clien t Sampl e XX) : HBTO-02-M26A-R 2

Genera l Chemistr y Lot-Sampl e #... : H9L140403-01 4 Wor k Orde r #... : LQ2T T Matri x: WAST E Dat e Sampled... : 12/09/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - PRE P PARAMETER RESOL T R L TJNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 1BS 0 20 0 mg/k g ASTM D482-00 a 12/29-12/31/0 9 936343 4 Dilutio nFactor s 1 MDI . : 5 1 Gros s Calorifi c 981 0 180 0 BT0/l bASTM D240-0 2 12/23/0 9 935718 8 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 1350 0 169 0 mg/k g KNO XWC-001 6 12/21-12/28/0 9 935203 1 Dilutio nFactor : 8.4 7 MD L : 51 0



## VES01824 6

### 75

AECOM , In c Clien t Sampl e ID : HBTU-TJ2-M26A-R 3

Genera l Chemistr y Lot-Sampl e #... : H9L140403-01 5 Wor k Orde r #... : LQ2T V Dat e Sampled— : 12/10/0 9 Dat e Received.. : 12/11/0 9
PARAMETER RESUL T R L UNIT S METHO D Matri x: WAST E

PREPARATION - PRE P

- ANALYSI S DAT E BATCH # As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 295 0 20 0 rag/kg Dilutio nFactor s 1 981 0 180 0 BTU/l b

Dilutio nFactor : 1 1450 0 168 0 mg/kg

Dilutio nFactor : 8. 4 AST M D482-00 a MD L s 5 1 AST M D240-0 2 MD L : 13 0 KNO XWC-001 6 MD L : 50 0 12/29-12/31/0 9 936343 4 12/23/0 9 935718 B
12/21-12/28/0 9 935203 1



## VES01824 7

### 7 6

AECOM , In c Clien t Sampl e ID : LBTU-U2-M2SA-R 1

Genera l Chemistr y Lot-Sampl e #... : H9L140403-01 6 Wor k Orde r #... : LQ2T W Dat e Sampled. : 12/08/0 9 Dat e Received.. : 12/11/0 9 Matri x: WAST E

PARAMETE

R RESDL T RL UNIT S As hConten t
Gros s Calorifi c valu e
Tota l Chlorin e 226 0 20 0 mg/k g Dilutio nFactor : 1 N D 1 8 0 0 BTU/l b

Dilutio nFactor : 1 118 0 27 8 mg/kg

Dilutio nFactor : 1. 3 9 _METHO D AST M D482-00 a MD L : 5 1 AST M D240-0 2 MD L 13 0 KNO XWC-001 6 MD L : 8 3 PREPARATION - PRE P ANALYSI S DAT E BATCH # 12/29-12/31/0 9 936343 4 12/23/0 9 935718 8
12/21-12/29/0 9 935203 1



## VES01824 8

### 7 7

Lot-Sampl e #.. . Dat e Sampled.. . AECOM , la c Clien t Sampl e TD : LBTU-U2-M26A-R 2

Genera l Chemistr y H9L140403-01 7 Wor k Orde r : LQ2T 0 12/09/0 9 Dat e Received.. : 12/11/0 9 Matrix . WAST E

PARAMETE

R RESUL T R L UNIT S As hConten t 199 0
Gros s Calorifi c N D Valu e
Tota l Chlorin e 10S 0 20 0 mg/kg Dilutio nFactor : 1 180 0 BTU/l b Dilutio nFactor : 1 28 0 mg/kg Dilutio nFactor ; 1. 4 _METHO D AST M D482-00 a MD L : 5 1 ASTM D240-0 2 MD L : 13 0 KNO XWC-001 6 MD L : 8 4 PREPARATION - PRE P ANALYSI S DAT E BATCH # 12/29-12/31/0 9 936343 4 12/23/0 9 935718 8
12/21-12/29/0 9 935203 1



## VES01824 9

### 7 8

Lot-Sampl e # . Dat e Sampled .
PARAMETE

R AECOM , In c Clien t Sampl e ZD : LBTU-U2-M26A-R 3

Genera l Chemistr y H9L140403-01 8 Wor k Orde r #... : LQ2T 1 12/10/0 9 Dat e Received.. r 12/11/0 9 Matri x: WASTE

RESUL T RL UNIT S As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 236 0 20 0 mg/kg Dilutio nFactor : 1 N D 180 0 BTU/l b

Dilutio nFactor : 1 123 0 28 2 mg/k g Dilutio nFactor : 1.4 1 _METHO D AST M D482-O0 a MD D . : 5 1 ASTM D240-0 2 MD L : 13 0 KNO XWC-001 6 MD L : 8 5 PREPARATION - PRE P ANALYSI S DAT E BATCH # 12/29-12/31/0 9 936343 4 12/23/0 9 935718 8
12/21-12/29/0 9 935203 1



## VES01825 0

### 79

AECOM , In c Clien t Sampl e ID : SF-U2-M26A-R 1

Genera l Chemistr y Lot-Sampl e #... : H9L140403-01 9 Wor k Orde r Dat e Sampled... : 12/ 0 8/0 9 Dat e Received. .
PARAMETE

R RESUL T R L UNIT S As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 776 0 20 0 mg/kg Dilutio nFactor s 1 N D 180 0 BTU/l b

Dilutio nFactor s 1 497 0 84 0 mg/kg

Dilutio nFacto r s 4. 2 LQ2T 3 12/11/0 9 Matrix . WAST E

_METHO

D ASTM D482-00 a MD L : 5 1 AST M D240-0 2 MD L 13 0 KNO XWC-001 6 MD L s 25 0 PREPARATION - PRE P ANALYSI S DAT E BATCH # 12/29-12/31/0 9 936343 4 12/23/0 9 93S718 8
12/21-12/28/0 9 935203 1



## VES01825 1

### 8 0

AECOM , In c Clien t Sampl e ID : SF-U2-M26A-R 2

Genera l Chemistr y Lot-Sampl e .

- H9L140403-02 0 Work Orde r #... : LQ2T 4 Dat e Sampled... : 12/09/0 9 Dat e Received. . - . 12/11/0 9 Matrxx . WAST E

PARAMETE

R RESUL T R L 

### TJNIT S As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 806 0 20 0 mg/kg Dilutio nFactor : 1 N D 180 0 BTD/l b

Dilutio nFactor : 1 451 0 83 6 mg/kg

Dilutio nFactor : 4.1 8 _METHO D AST M D482~00 a MD L : 5 1 AST M D2 4 0-0 2 MD L : 13 0 KNO XWC-001 6 MD L ; 25 0 PREPARATION - PRE P ANALYSI S DAT E BATCH # 12/29-12/31/0 9 936343 4 12/23/0 9 93571B 8
12/21-12/28/0 9 935203 1



## VES01825 2

### 8 1

AECOM , In c Clien t Sampl e ID : SF-D2-M26A-E 3

Genera l Chemistr y Lot-Sampl e #._. : H9L140403-02 1 Wor k Orde r #... : LQ2T 5 Matri x: WAST E Dat e Sample d : 12/10/0 9 Dat e Received.. s 12/11/0 9 PREPARATION - PRE P PARAMETE

R RESDL T R L UNIT S METHO D ANALYSI S DAT E BATCH # As hConten t 793 0 20 0 mg/k g AST M D4B2-00 a 12/29-12/31/0 9 93S343 4 Dilutio nFactor : 1 MD L 5 1 Gros s Calorifi c N D 180 0 BTU/l bASTM D24O-0 2 12/23/0 9 935718 8 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 479 0 84 4 mg/kg KNO XWC-001 S 12/21-12/28/0 9 935203 1 Dilutio nFactor : 4 .2 2 

### MDL ... W : 25 0



## VES01825 3

### 8 2

AECOM , In c Clien t sampl e XB : CS-xr2-M26A.-R l

Genera l Chemistr y Lot-Sampl e #... : H9L14O403-02 2 Wor k Orde r #.-. : LQ2T 6 Matri x: SOLI D Dat e Sampled... : 12/08/0 9 Dat e Received.. : 12/11/0 9 PREPARATION - •PRE P PARAMETE

R, RESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 80900 0 20 0 mg/kg ASTM D482-00 a 12/29-12/31/0 9 936343 3 Dilutio nFactor ; 1 MD L . : 5 1 

### Gros s Calorifi c N D 1B0 O BTU/l bAST M D58S5-0 0 12/16/0 9 935003 2 Valu e Dilutio nFactor : 1 MD L : 13 0 

### Tota l Chlorin e N D 20 0 mg/k g KNO

XWC-001 6 12/22-12/29/0 9 935606 5 Dilutio nFactor : 1 MD L : 6 0



## VES01825 4

### 83

Lot-Sampl e # . Dat e Sampled .
PARAMETE

R AECOM , In c Clien t Sampl e 3D : CS-TX2-M26A-R 2

Genera l Chemistr y H9L140403-02 3 Wor k Orde r #... : LQ2T 7 12/09/0 9 Dat e Received.. : 12/11/0 9 Matrix . SOLI D

RESUL T R L UNIT S As hConten t
Gros s Calorifi c Valu e
Tota l chlorin e 78700 0 20 0 mg/kg Dilutio nFactor ; 1 N D 180 0 BTU/l b

Dilutio nFactor : 1 N D 20 0 mg/k g Dilutio nFactor : 1 _METHO D AST M D482-00 a MDL . 5 1 ASTM D586S-0 0 MD L : 13 0 KNO XWC-001 6 MD L : 6 0 PREPARATION - PRE P ANALYSI S DAT E BATCH # 12/29-12/31/0 9 936343 3 12/16/0 9 935003 2
12/22-12/29/0 9 935606 5



## VES01825 5

### 8 4

Lot-Sampl e #.. . Dat e Sampled —

As hConten t AECOM , In c Clien t Sampl e ID : CS-D2-M26A-R 3

Genera l Chemistr y H9L140 4 03-02 4 Wor k Orde r #... : LQ2T 8 12/10/0 9 Dat e Received.. : 12/11/0 9 Matrix . SOLI D

PARAMETER RESUL T R L UNIT S 7S9000 20 0 mg/k g

Dilution . Factor ; 1 Gros s Calorifi c N D Valu e
Tota l Chlorin e N D 180 0 BTU/l b

Dilutio nFactor : 1 20 0 mg/k

g Dilutio nFactor : 1 METHO D AST M D482-00 a MD L : S I ASTM D58S5-0 0 MD L : 13 0 KNO XWC-001 S MD L : S

O PREPARATION - PRE P ANALYSI S DAT E BATCH # 12/29-12/31/0 9 936343 3 12/16/0 9 935003 2
12/22-12/29/0 9 935606 5



## VES01825 6

### 8 5


# Q C Summar

y

VES01825 7

### 8 6

Clien t Lo t #.. . H9L14040 3 METHO D BLAN KEEPOR T Genera l Chemistr y Matri x; WAST E
PARAMETER As hConten t RESUL T N D REPORTIN G LIMI T UNIT S METHO D PREPARATION - PRE P

ANALYSI S DAT E BATCH # Work Orde r # : LRPQF1A A M B Lot-Sampl e # : H9L290000-43 4 20 0 mg/k

g AST M

D482-00 a 12/29-12/31/0 9 936343 4 Dilutio nFactor ; 1 Tota l Chlorin e Work Orde r # : LQ76D1A A M B Lot-Sampl e # : H9L170000-08 2 N D 20 0 mg/kg KNO XWC-001 6 12/17-12/18/0 9 93S108 2 Dilutio nFactor : 1 Tota l Chlorin e Wor k Orde r # : LRAEQ1A A M B Lot-Sampl e # : H9L180000-03 1 N D 20 0 mg/k g KNO

XWC-001 6 12/21-12/28/0 9 935203 1 Dilutio nFactor : 1 KOTEfS) : Calculation

s ar c performe

d befor e roundin g 1 0 avoi d round-of

f error s i n calculate

d results .



## VES01825 8

### 8 7

Clien t lo t H9L1 4 040 3
PARAMETE

R RESUL T As hConten t

Tota l Chlorin e N D

N D METHO D BLAN KREPOR T Genera l Chemistr y Matrix . SOLI D REPORTIN

G LIMI T UNIT S METHO D PREPARATION - PRE P

ANALYSI S DAT E BATCH # Wor k Orde r # : LRPQE1A A M B Lot-Sampl e # : H9L290000-43 3 20 0 mg/kc j ASTM D482-00 a 12/29-12/31/0 9 936343 3 Dilutio nFactor : 1 Wor k Orde r # : LRGLV1A A M B Lot-Sampl e # : H9L220000-O6 5 20 0 mg/kg KNO XWC-001 6 12/22-12/29/0 9 935606 5 Dilutio nFactor : 1 NOT E (S ) : Calculation

s ar c performe

d befor e roundin g i o avoi d round-off

error s i u calculate

d results .



## VES01825 9

### 8 8

LABORATOR

YCONTROL SAMPL E EVALUATIO N REPORT Genera l Chemistr y Lot-Sampl e H9L14040 3 Matrix .
PARAMETER As hConten t PERCENT

RECOVER

Y 10 0 10 0 RECOVER Y LIMIT S RPD RPD LIMIT S METHO

D PREPARATION ANALYSI S DAT E : SOLI D

PRE P BATC H # W0#:LRPQE1AC-LCS/LRPQE1AD-LCS D LC S Lot-Sample# : H9L290O00-43 3 (9 0 - 110 ) AST M D482-00 a 12/29-12/31/0 9 936343 3 (9 0 - 110 ) 0.3 2 (0-10 ) ASTM D482-0O a 12/29-12/31/0 9 936343 3 Dilutio nFactor : 1 Gros s Calorifi c Valu e 10 0

10 0 W0#:LQ58P1AA-LCS/LQ58P1AC-LCS D LC S Lot-Sample# : H9L1S0O00-03 2

(9 8 - 102 ) AST M D5B65-0 0 (9 8 - 102 ) 0.1 0 (0-2.0 ) AST M D5865-0 0 Dilutio nFactor : 1 12/16/0 9 12/16/0 9 935003 2

935003 2
NOTE(S) : Calcutiiion

s ar e performe

d befor e roundin g l o avoi d round-of

f error s in calculate

d results .



## VES01826 0

### 8 9

LABORATOR

YCONTROL SAMPL E DAT A REPOR T Genera l Chemistr y Lot-Sampl e : H9L14040 3 Matri x: SOLI D
PARAMETER As hConten t SPIK E MEASURE D AMOUN T AMOUN

T UNIT S PERCNT

RECVR YRPD METHO

D PREPARATION ANALYSI S DAT E 400 0 400 0
Gros s Calorifi c Valu e 1140 0

1140 0 PRE P BATC H # W0#:LRPQE1AC-LCS/LRPQE1AD-LCS D LC S Lot-Sample# : H9L290QO0-43 3 400 0 mg/k

g 10 0 ASTM D4B2-00 a 12/29-12/31/0 9 936343 3 399 0 mg/k

g 10 0 0.3 2 ASTM D4B2-00 a 12/29-12/31/0 9 936343 3 Dilutio nFactor : x W0#:LQ58P1AA-LCS/LQ58P1AC-LCS D LC S Lot-Sample# : H9L1600O0-03 2 11 3 0 0 BTU/l b10 0 1130 0 BTU/l b10 0

Dilutio nFactor : 1 ASTM D5865-0 0 0.1 0 AST

M DS86S-0 0 12/16/0 9 12/16/0 9 . 935003 2

935003 2
NOTE(S ) ; Calculation

s ar e performe

d befor e roundin g t o avoi d round-of

f error s i n calculate

d results .



## VES01826 1

### 90

LABORATOR

YCONTROI . SAMPL E EVALUATIO N REPOR T Genera l Chemistr y Lot-Sampl e #... : H9L14040 3 Matri x: WAST E

PERCENT RECOVER YRP D PARAMETE

RRECOVER

YLIMIT S RP D LIMIT S METHO D Ash . Conten t PREPARATION - PRE P ANALYSI S DAT E BATC H ft 10 0 9 9 W0#;LRPQF1AC-LCS/LRPQF1AD-LCS D LC S Lot-Sample# : H9L290000-43 4

(9 0 - 110 ) AST M D482-00 a 12/29-12/31/0 9 936343 4 (9 0 - 110 ) 0.9 3 (0-10 ) ASTM D482-00 a 12/29-12/31/0 9 936343 4 Dilutio nFactor : 1 Gros s Calorifi c Valu e 10 0

9 9 W0#:LRG6J1AA-LCS/LRG6J1AC-LCS D LC S Lot-Sample# : H9L220000-34 8

(9 8 - 102 ) AST M D240-0 2 (9 8 - 102 ) 0.4 2 (0-2.0 ) ASTM D240-0 2 Dilutio nFactor : 1 12/22/0 9 12/22/0 9 935634 8

935634 8
Gros s calorifi c Valu e 10 0

1 0 0 W0#:LRJKE1AA-LCS/LRJKE1AC-LCS D LC S Lot-Sample# : H9L230000-18 8

(9 8 - 102 ) AST M D240-0 2 (9 8 - 102 ) 0.0 4 (0-2.0 ) AST M D240-0 2 Dilutio nFactor : 1 12/23/0 9 12/23/0 9 935718 8

935718 8


### SOTB(S ) ; Calculltiort

s ar c performe

d befor e roundin

g t o avoi d round-of

f error s i n calculate

d results .



## VES01826 2

### 9 1

LABORATOR

YCOHTROL SAMPL E DAT A REPORT Genera l Chemistr y Lot-Sampl e #. . H9L14040 3 Matri x: WAST E
PARAMETE

R As hConten t SPIK E

AMOUN T 400 0 400 0 MEASURE

D AMOUN T UNIT S PERCN T RECVR YRP D METHO

D PREPARATION ANALYSI S DAT E PRE P

BATCH # W0#:LRPQF1AC-LCS/LRPQF1AD-LCS D LC S Lot-Sample* : H9L290000-43 4 398 0 mg/k g 10 0 ASTM D482-00 a 12/29-12/31/0 9 93S343 4 394 0 mg/k g 9 9 0.9 3 ASTM D482-00 a 12/29-12/31/0 9 936343 4 Dilutio nFactor : 1 Gros s Calorifi c W0#:LRG6J1AA-LCS/LRGSJ1AC-LCS D LC S Lot-Sample# : H9L220000-34 8 Valu e 2060 0 2050 0 BTU/l b10 0 ASTM D24O-0 2 12/22/0 9 935634 8 2060 0 2050 0 BTU/l b9 9 0.4 2 ASTM D240-0 2 12/22/0 9 935634 8 Dilutio nFactor : 1 Gros s Calorifi c Valu e 2060 0

2060 0 W0#:LRJKE1AA-LCS/LRJKE1AC-LCS D LC S Lot-Sample# : H9L230000-18 8

2050 0 BTU/l b10 0 2050 0 BTU/l b10 0

Dilutio nFactor : l ASTM D240-0 2 0.0 4 ASTM

D240-0 2 12/23/0 9 12/23/0 9 935718 8

935718 8
NOTE(S ) ; Calculation

s ar c performe

d befor e roundin g l o avoi d round-of

f error s i n calculate

d results .



## VES01826 3

### 9 2

LABORATOR

YCONTROL SAMPL E EVALUATION REPORT Genera l Chend s try Clien t Lo t #... : H9L14040 3 Matri x: WAST E PERCEN T RECOVER

YPREPARATION - PRE P PARAMETERRECOVER YLIMIT S METHO D ANALYSI S DAT E BATC H # Tota l Chlorin e Work Orde r # : LQ76D1A C LC S Lot-Sample# : H9L170000-08 2 10 0 (8 0 - 120 ) KNO XWC-001 6 12/17-12/18/0 9 935108 2 Dilutio nfactor : S Tota l Chlorin e Wor k Orde r # : LRAEQ1A C LC S Lot-Sample# : H9L180000-03 1 9 6 (8 0 - 120 ) KNO XWC-001 6 12/21-12/28/0 9 935203 1 Dilutio nFactor : 5 NOTE(S ) : , Calculation

s ar cperforme

d befor e roundin g i o avoi d round-of

f error s i n calculate

d results .



## VES01826 4

### 9 3

LABORATOR

YCOHTRO

L SAMPL E DAT A

REPORT Genera l Chemistry Clien t Lo t #... : H9L14040 3 Matri x: WAST E

SPIK E MEASURED PERCN T PREPARATION - PRE P PARAMETERAMOUN T AMOUN

T UNIT S RECVR YMETHO

D ANALYSI S DAT E BATCH f f Tota l Chlorin e Wor k Orde r ff : LQ76D1A C LC S Lot-Sampleff : H9L170000-08 2 1000 0 995 0 mg/k g 10 0 KNO XWC-001 6 12/17-12/18/0 9 935108 2 Dilutio n Factor : 5 Tota l Chlorin e Wor k Orde r ff : LRAEQ1A C LC S Lot-Sample# : H9L180000-03 1 1000 0 957 0 mg/k g 9 6 KNO XWC-001 S 12/21-12/28/0 9 935203 1 Dilutio n Factor : 5 NOT E (S ) ; Calculation

s ar e perrarme

d befor e roundin s ' aavoi d round-of

f error s i n calculaie

d results .



## VES01826 5

### 94

LABORATOR

YCONTRO

L SAMPL E EVALUATIO N REPOR T Genera l Chemistr y Clien t Lo t if.-. : H9L14040 3 Matrix . = SOLI D PERCENT RECOVER YPREPARATION - PRE P PARAMETE R RECOVER YLIMIT S METHO D ANALYSI S DAT E BATC H ft Tota l Chlorin e Wor k Orde r ft: LRGLV1A C LC S Lot-Sample# : H9L220000-OS 5 9 5 (8 0 - 120 ) KNO XWC-001 6 12/22-12/29/0 9 935606 5 Dilutio nFactor : 5 NOTE(S ) : ; , Calculation

s ar e performe

d befor e roundin s t o avoi d round-of

f error s in calculate

d results .



## VES01826 6

### 9 5

IABORBXOE

YCONTRO

L SAMPL E DAT A

REPOR T Genera l Chendstr y Clien t Lo t #... : H9L14040 3 Matri x: SOLI D

SPIK E MEASURED PERCNT PREPARATION - PRE P PARAMETERAMOUN T AMOUN

T UNIT S RECVR YMETHO

D ANALYSI S DAT E BATC H # Tota l Chlorin e Wor k Orde r # : LRGLV1A C LC S Lot-Sample# : H9L220000-OS 5 1000 0 948 0 mg/k g 9 S KNO XWC-001 6 12/22-12/29/0 9 9356d6 5 Dilutio nFactor : S NOTB(S ) : Calculation

s ar c performe

d befor e roundin g t o avoi d round-of

f error s i n calculate

d results ,



## VES01826 7

### 96

MATRI XSPIK E SAMPL E EVALUATIO N REPORT Genera l Chemistr y Clien t Lo t #... : H9L14040 3 Matri x: WAST E Dat e Sampled... : 12/08/0 9 Dat e Received.. : 12/11/0 9

PERCENT RECOVER

YRP

D PREPARATION - PRE P PARAMETE

RRECOVER

YLIMIT S RPD LIMIT S METHO D ANALYSI S DAT E BATC H # Tota l Chlorin e W0# : LQ2TG1AG-MS/LQ2TG1AH-MS D M S Lot-Sampl e # : H9L14O403-0O 5 10 0 (8 0 - 120 ) KNO XWC-001 6 12/17-12/18/0 9 93S108 2 9 9 (8 0 - 120 ) 1. 5 (0-10 ) KNO XWC-001 6 12/17-12/18/0 9 935108 2 Dilutio nFactor : 6.9 8 Tota l Chlorin e WO# : LQ2TR1AE-MS/LQ2TR1AF-MS D M S Lot-Sampl e # : H9L140403-01 3 8 7 (8 0 - 120 ) KNO XWC-001 6 12/21-12/28/0 9 935203 1 9 7 (8 0 - 120 ) 1. 0 (0-10 ) KNO XWC-001 6 12/21-12/28/0 9 935203 1 Dilutio nFactor : 9.5 7 NOTE(S ) : Calculou s ar

e performe

d befor e roundin

g i o avoi d round-of

f error s in calculate

d results .



## VES01826 8

### 97

MATRI XSPIK E SAMPL E DAT A REPOR T Genera l Chemistry Clien t Lo t #. . Dat e Sampled. . . : H9L14040 3

, : 12/08/0 9 Dat e Received.. ; 12/11/0 9 Matrix . WAST E
SAMPL E SPIK E MEASR D PARAMETER AMOUN T AM T Tota l Chlorin e

98 8 1400 0 98 8 1440 0 PERCN T RECVR YRP D METHO

D PREPARATION - PRE P

ANALYSI S DAT E BATCH # AMOUN T UNIT S WO# : LQ2TG1AG-MS/LQ2TG1AH-MS D M S Lot-Sampl e # : H9L140403-00 5 1490 0 mg/k

g 10 0 KNO XWC-001 6 12/17-12/18/0 9 935108 2 1520 0 mg/k

g 9 9 1. 5 KNO XWC-001 6 12/17-12/18/0 9 935108 2 Dilutio nFactor : 6.9 8 Tota l Chlorin e

1530 0 1910 0 1530 0 1730 0 W0# : LQ2TR1AE-MS/LQ2TR1AF-MS D M S Lot-Sampl e # : H9L140403-01 3 3180 0 mg/kg 8 7 KNO XWC-001 6 12/21-12/28/0 9 935203 1 3220 0 mg/k

g 9 7 1- 0 KNO XWC-001 6 12/21-12/28/0 9 935203 1 Dilutio nFactor : 9.S 7 NOTE(S) : emulation

s ar e performe

d befor e roundin

g t o avoi d round-of

f error s i n calculate

d results .



## VES01826 9

### 9 8

MATRI XSPIK E SAMPL E EVALUATIO N REPORT Genera l Cnetnistr y Clien t Lo t # : H9L14040 3 Matri x: SOLI D Dat e Sampled... : 12/09/0 9 Dat e Received.. : 12/11/0 9

PERCENT RECOVER YRP

D PREPARATION - PRE P PARAMETER RECOVER YLIMIT S RPD LIMIT S METHO D ANALYSI S DAT E BATC H # Tota l Chlorin e WO# : LQ2TP1AG-MS/LQ2TP1AH-MS D M S Lot-Sampl e # : H9L14O403-01 1 8 8 (B

O - 120 ) KNO XWC-001 6 12/22-12/29/0 9 935606 5 9 1 (8 0 - 120 ) 2. 2 (0-10 ) KNO XWC-001 6 12/22-12/29/0 9 935606 5 Dilutio nFactor : 5.0 1 NOTE(S) : Calculnion s ar c performe d befor e roundin g l o avoi d round-of

f error s i n calculaie d results .



## VES01827 0

### 9 9

MATRI XSPIK E SAMPL E DAT A REPOR T Genera l Chemistr y Clien t Lo t #.. . Dat e Sampled... . H9L14040 3 12/09/0 9 Dat e Received . 12/11/0 9 Matri x: SOLI D

PARAMETER SAMPL E SPIK E

AMOUN T AM T Tota l Chlorin e

13 4 ' 13 4 MEASR D AMOUN T UNIT S PERCNT

RECVR YRP D METHO

D PREPARATION ANALYSI S DAT E 1000 0 994 0 PRE P BATC H # WO# : LQ2TP1AG-MS/LQ2TP1AH-MS D M S Lot-Sampl e # : H9L140403-01 1 896 0 mg/kg 8 8 KNO XWC-001 6 12/22-12/29/0 9 935606 S 916 0 mg/kg 9 1 2. 2 KNO XWC-001 6 12/22-12/29/0 9 935606 5 Dilutio nPacto n5.0 1 HOT S (5 ) : Calculation

s ar e performe

d befor e roundin g l o avoi d round-of

f error s i n calculate

d rcsulis .



## VES01827 1

### 10 0

SAMPL E DUPLICAT E EVALUATIO N EEPOR T Genera l Chemistr y H9L14040 3 Wor k Orde r : LQ2TC-SMP Matri x: WAST E LQ2TC-DUP 12/08/0 9 Dat e Received.. : 12/11/0 9 DUPLICAT E RP D PREPARATION - PRE P RESUL T UNIT S RPD LIMI T METHO D ANALYSI S DAT E BATCH # S D Lot-Sampl e # : H9L140403-00 1 134 0 mg/k g 1. 8 (0-10 ) AST M D482-00 a 12/29-12/31/0 9 936343 4 Dilutio nFactor : 1



## VES01827 2

### 10 1

Clien t Lo t # . .. : Dat e Sampled —

:
PARA M RESUL T Gros s Calorifi c Valu e M

D
As hConten t 190 0
Tota l Chlorin e 98 8 SAMPL E DUPLICAT E EVALUATIO N REPOR T Genera l Chemistr y H9L14040 3 Work Orde r # . 12/09/0 9 LQ2TG-SM P LQ2TG-DUP Dat e Received.. : 12/11/0 9 Matrix . WAST E

DUPLICAT E RESUL T
N D

188 0

99 9 RPD

UNIT S RPD LIMI T METHO D PREPARATION - PRE P

ANALYSI S DAT E BATCH # . . BTU/l b0 (0-10 ) AST M D240-0 2 Dilutio n Factor : 1 S D Lot-Sampl e # : H9L140403-00 5 12/22/0 9 935634 8
S D Lot-Sampl e # : H9L140403-0O S • mg/k g 1. 1 (0-10 ) AST M D482-00 a Dilutio n Factor : 1 12/29-12/31/0 9 936343 4
S D Lot-Sampl e # ; H9L140403-0O 5 mg/k g 1. 2 (0-10 ) KNO XWC-001 6 Dilutio n Factor : 1.4 5 12/17-12/18/0 9 935108 2 .



## VES01827 3

### 10 2

SAMPL E DUPLICAT E EVALUATIO N REPORT Genera l Chemistr y Clien t Lo t #... : H9L14040 3 Wor k Orde r #-.. : LQ2TP-SMP Matrix . : SOLI D LQ2TP-DUP Dat e Sample d : 12/09/0 9 Dat e Received.. : 12/11/0 9 DUPLICAT E RP D PREPARATION - PRE P PARA M RESUL T RESUL T UNIT S RPD LIMI T METHO D ANALYSI S DAT E BATC H # Gros s Calorifi c S D Lot-Sampl e # : H9L14G403-01 1 Valu e N

D N

D BTU/l b0 (0-10 ) ASTM D5865-0 0 12/16/0 9 935003 2 Dilutio nFactor : 1 As hConten t S D Lot-Sampl e # ; H9L140403-01 1 71300 0 70300 0 mg/kg ' 1. 3 (0-10 ) ASTM D482-00 a 12/29-12/31/0 9 936343 3 Dilutio nFactor : 1 Tota l Chlorin e S D Lot-Sampl e # : H9L140403-01 1 13 4 B 13 2 B mg/k g 1. 6 (0-10 ) KNO XWC-001 6 12/22-12/29/0 9 935606 5 Dilutio nFactor : 1
NOT E (S ) : Calculation

s ar c pcrrormc

d befor e roundin

g t o avoi d round-of

f error s i n calculate

d results . B Estimate

d result . Resul ti s les s ton RL .



## VES01827 4

### 10 3

Clien t Lo t it... : H9L14040 3 Dat e Sampled... : 12/08/0 9 SAMPL E DUPLICAT E EVALUATIO N EEPOR T Genera l Chemistr y Wor k Orde r #... : LQ2TR-SM P LQ2TR-DUP Dat e Received.. : 12/11/0 9
PARA M RESUL T DUPLICAT E

RESUL T Gros s Calorifi c Valu e 1020 0
Tota l Chlorin e 1530 0 990 0

1520 0 Matrxx . WAST E

UNIT S RPD

RP D LIMI T METHO D PREPARATION - PRE P

ANALYSI S DAT E BATC H # S D Lot-Sampl e # : H9L140403-01 3 BTU/l b2. 9 (0-10 ) AST M D240-0 2 12/23/0 9 Dilutio nFactor : 1 935718 8
S D Lot-Sampl e # : H9L140403-01 3 mg/k g 0.1 9 (0-10 ) KNO XWC-001 6 12/21-12/28/0 9 935203 1 Dilutio n Factor : 8.3 9



## VES01827 5

### 10 4

Clien t Lo t #... : H9L14040 3 Dat e Sampled... : 12/08/0 9
PARA M RESUL T Tota l Chlorin e 497 0 SAMPL E DUPLICAT E EVALUATIO N REPORT Genera l Chemistr y Wor k Orde r #..- : LQ2T3 -SM P LQ2T3-DUP Dat e Received.. : 12/11/0 9

479 0 Matrxx . WAST E

DUPLICAT E RESUL T UNIT S RPD RPD LIMI T METHO D PREPARATION - PRE P

ANALYSI S DAT E BATC H # S D Lot-Sampl e #: - H9L140403-01 9 mg/k g 3. 5 (0-10 ) KNO XWC-001 6 12/21-12/28/0 9 935203 1 Dilutio nFacto r s 4. 2



## VES01827 6

### 10 5

Clien t Lo t #... : H9L14040 3 Dat e Sampled... : 12/10/0 9 SAMPL E DUPLICAT E EVALUATIO N REPORT Genera l Chemistr y Wor k Orde r #.. . Dat e Received. .
PARA M RESUL T DUPLICAT E

RESUL T Gros s Calorifi c Valu e N

D N

D LQ2T5-SM P LQ2T5-DUP 12/11/0 9
UNIT S RP D

RP D LIMI T METHO D Matri x: WAST E

PREPARATION - PRE P ANALYSI S DAT E BATC H # BTU/l b0 Dilutio nFactor : 1 S D Lot-Sampl e # : H9L140403-02 1 (0-10 ) AST M

D240-0 2 12/23/0 9 935718 8



## VES01827 7r



## VES01827 8

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Content s 1. 0 Introductio n • •1- 1 

### 1. 1 Progra m Summar

y1- 1 1. 2 Purpos e an d Objective o f th e Performanc

e Tes t 1- 1 1.3 Progra m Descriptio n 1-1 1.3. 1 Test Operatin g Condition s 1- 1 1.3. 2 Baghous e Cleanin g Cycl e 1- 2 1.3. 3 Chlorin e Fee d 1- 2 1. 4 Condition s i n USEP ACP TApprova l Lette rDate d Novembe r25 , 200 9 1- 2 1.4. 1 Incinerato r2 DR E Dat a i n Lie u Request 1- 2 1.4. 2 Incinerator

s 2 , 3 , an d 4 Metal s Dat

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### 2. 1 Proces s Overvie w2- 6 2. 2 Waste Fee d System s [4 0 CF R § 63.1207(f)(1)(ii)(c ) an d (f)(1)(iii)(D) an d (E) ] 2- 6 2.2, 1 Uni t 3 Liqui d Wast e Fee d Syste m an d Blendin g Operation s 2- 6 2.2.1. 1 Organi can d Aqueou s Liqui d Wast e Feed s 2- 6 2.2.1. 2 Package d Waste Fee d 2- 7 2.2.1. 3 Specialt

yLiqui d Waste Feed s 2- 7 2. 3 Manufacturer , Make an d Mode l o f th e Incinerato r[4

0 CF R § 63.1207(f)(1)(iii)(A) ] 2- 7 2.3. 1 Combustio n Chambe ran d Burner s [4 0 CF R §63.1207(f)(1)(iii)(B ) an d (C ) 2- 7 2.3. 2 Secondar

yCombustio n Chambe r2- 8 2.3. 3 Locatio n o

f Combustio n Zon e Temperatur e Device [4

0 CF R §63.1207(f)(1)(xix) ] 2- 8 2.3. 4 Hazardou s Wast e Residence Tim e [4 0 CF R §63.1207(f)(1)(ix) ] 2- 8 2.3. 5 Combustio n Syste m Leak.. . 2- 9 2.3. 6 Emergenc

ySafet yVen t 2-9 2. 4 Procedure s fo rRapidl yStoppin g Hazardou s Wast e Fee d Durin g Equipmen t Malfunctio n [4 0 CF R §63.1207(f)(1)(viii) ] 2- 9 2. 5 Ai rPollutio n Contro l Equipmen t [4 0 CF R §63.1207(f)(1)(iii)(G) ] 2- 9 2.5. 1 Ai rPollutio n Contro l System s Description s 2- 9 2.5.1. 1 Lim e Syste m 2-1 0 2.5.1. 2 Spra

yDr yAbsorbe r2-1 0 2.5.1. 3 Fabri cFilte r2-1 1 2.5.1. 4 Induced Draf

t Fa n an d Stac k

2-1 1 2. 6 Stac k

Emission s Monitorin g [4

0 CF R §63.1207(f)(1)(iii)(H) ] 2-1 1

i Februar y 2O1 0 

## VES01828 1

# A-COM 2.6. 1 CEM S Syste m Descriptio n 2-1 2 2. 7 Proces s Monitorin g an d Contro l 2-1 2 2. 8 Automati cWast e Fee d Cut-of f Syste m [4

0 CF R §63.1207(f)(1)(iii)(F) ] : 2-1 3 2.8. 1 • AWFC O Syste m Testin g 2-1 4 2. 9 Ai rPollutio n Contro l Equipment Maintenanc e Practice s [4

0 CF R §63.1207(f)(1)(iii)(G) ] 2-1 4 2.9. 1 Progra m Overvie

w2-1 4 2.9. 2 Tes t Progra m Preparatio n Activities. , 2-1 5 3.0 Summar

y of Result s 3- 1 

### 3. 1 Proces s Operatin g Condition s 3- 1 3. 2 Stac k

Emissio n Results fo rTota l Chloride s (HCI/CI 2

### ) : 3- 1 3. 3 Stac k

Emissio n Results fo rParticulate Matter... . 3- 1 3. 4 Stac k

Emissio n Results fo rDioxin s an d Furan s 3- 1 3. 5 Stac k

Emissio n Results fo rTota l Hydrocarbon s 3- 1 4. 0 Samplin g an d Analytica l Progra m 4- 1 

### 4. 1 Waste Fee d Strea m Samplin g Procedure s 4- 1 4. 2 Stac k

Samplin g Procedure s 4- 1 4.2. 1 Stac k

Samplin g Locatio n 4- 1 4.2. 2 Velocity , Moistur

e an d Fixe d Ga s Determination s 4-2 4.2. 3 Particulat e Matte r(PM) , HC I an d Cl 2

### 4-2 4.2. 4 PCDDs/PCDF s 4- 2 4.2. 5 Continuou s Emissio n Monitorin g 4-2 4. 3 Analytica l Procedures... . 4- 3 4.3. 1 Analysi s o

f Wast e fee d Stream s 4- 3 4.3.1. 1 Chemica l an d Physica l Propertie s o f Wast e fee d Stream s 4- 3 4.3. 2 Analysi s o

f Stac k Ga s Sample s : 4-3 4.3.2. 1 Tota l Chloride s (HCI/CI 2 

### ) i n Stac k Ga s Sample s 4-3 4.3.2. 2 Particulate Matte r(Gravimetri cAnalysis ) 4- 3 4.3.2. 3 Stac k

Gas-Analysi s fo rPCDDs/PCDF s 4- 3 5.0 Qualit

y Assuranc e 5- 1 

### 5. 1 Sampl e Collectio n QA/QC : 5- 1 5.1. 1 Wast e Fee d Stream s 5- 1 5.1. 2 Stac k

Samplin g QA/Q C 5- 1 5.1. 3 Pre-Samplin g Activitie s 5- 1 5.1. 4 Equipmen t Calibration.
. 5- 1 5.1. 5 Glassware Preparatio n 5- 2 5.1.5. 1 Sampl e Medi a Preparatio n 5- 2 5. 2 Chain-of-Custod y5- 3 5.3 Analytica l QA/Q C 5- 3

i i February 201 0 

## VES01828 2

# AZCOM 5.3. 1 Analysi s o

f Waste Fee d Stream s 5- 3 5.3.1. 1 Chemica l an d Physica l Propertie s o f Waste Fee d Stream s 5- 3 5.3. 2 Analysi s o

f Stac k Ga s Sample s : 5-3 5.3.2. 1 Tota l Chloride s (HCI/CI 2 

### ) i n Stac k Ga s Samples...
. 5-3 5.3.2. 2 Particulate Matte r(Gravimetri cAnalysis ) 5- 3 5.3.2. 3 PCDDs/PCDF s i n Stac k Ga s Sample s 5- 4 

# Lis t o fAppendice s Appendi xAFacilit

yOperatin g Dat

a Appendi xB Reference Metho d Fiel d Dat a an d Calculation s Appendi xC Reference Metho d Calibrations , Verifications , an d Certification s Appendi xD Laborator

yData 

# Lis t o fTables Tabl e 1 - 1 Summar

yo f Applicabl e MAC TEmissio n Standard s 1- 4 Tabl e 1- 2 MAC TOPL s Establishe d Durin g th e Performance Tes t 1 - 5 Tabl e 2- 1 Continuou s Emissio n Monitor s 2-1 2 Tabl e 2-2 Technica l Informatio n Summar yo n Incinerato rNo . 3 2-1 6 Tabl e 2- 3 Curren t AWFC O Parameter s an d Limit

s fo rIncinerato rNo . 3 2-1 7 Tabl e 3- 1 Waste Fee d Rate s an d Operatin g Condition s 3- 2 Tabl e 3- 2 R M 5/26ASamplin g Parameter s an d Emissio n Results - Tota l Chloride/P M 3-3 Tabl e 3-3 R M 0023ASamplin g Parameter s an d Emissio n Result

s - Dioxi n an d Fura n 3- 4 Tabl e 3- 4 R M 25ASamplin g Parameter s an d Emissio n Results 3-5 Tabl e 4- 1 Travers e Poin t Location s 4- 4 Tabl e 5- 1 QA/Q C Requirements fo rChemical/Physica l Propertie s o f Wast e Fee d 5- 5 Tabl e 5- 2 QA/Q C Requirements fo rChloride s i n Stac k Ga s 5- 6 Tabl e 5-3 QA/Q C Requirements fo rPCDD/PCD F Analyse s o f Stac k Ga s Sample s 5- 7 

# Lis t o fFigures Figure 2- 1 Hydrated Lim e Specification s 2-1 8 Figure 4- 1 Unit 3 Exhaust Stac k Schemati c4- 5

ii i Februar y 201 0 

## VES01828 3

# 1.

0 Introductio n 1. 1 Progra m Summar y AECO M Environmen t (AECOM ) was retaine d b yVeoli a E S Technica l Solution s (Veolia) , t o conduc t a comprehensive performanc e test (CPT) fo rits Incinerato rNo . 3 as required unde r40 CF R § 63.1207 o f th e Hazardou s Wast e Combusto r(HWC ) MAC Tregulations . Th e CP Twa s conducte d durin g th e wee k o f Novembe r30 , 200 9 fo rth e Sauget , I L facility . Th e results fro m thi s testin g indicate tha t emission s fo rdioxin s an d furan s (PCDDs/PCDFs) , tota l hydrocarbons , hydroge n chlorid e an d chlorine , an d particulate matte r(PM ) me t th e applicabl e emissio n standard s unde r4 0 CF R 6 3 Subpar t EE E (otherwise known a s th e HW C MAC Tregulations) . Asummar yo f th e test results ca n be foun d i n Sectio n 3 o f thi s report . 

## 1. 2 Purpos e an d Objectiv e o f th e Performanc e Tes t Th e purpos e o

f th e CP Twas t

o validate th e performanc

e leve l o f th e incinerato ragains

t th e requirement

s i n 40 CF R Par t 63 , Subpar

t EEE . T o thi s end , th e specifi cobjective s o f thi s CP Twer

e to :

• Demonstrat

e tha t th e emission s fro m th e incinerato rmee t th e HW C MAC Temissio n limit s whil e treatin g hazardou s waste forth e parameter s bein g tested .
• Collec

t monitorin g data i n orde rt o re-establis h operatin g paramete rlimit s (OPLs ) o rset ne

wOPL s o n ke yoperatin g variable s tha

t wil l ensur

e tha t th e incinerato roperate s withi n th e HW C MAC Temissio n limit s whil e treatin g hazardou s waste . Th e test progra m include d feedin g a variet yo f liqui d an d soli d waste material s t o th e incinerator , samplin g an d analyzin g th e fee d streams , monitorin g certai n proces s parameter s an d conductin g emission s testing . Th e emission s standard s tha

t wer e evaluate d unde rth e HW C MAC Tregulation s ar e summarized i n Tabl e 1 -1 . 

## 1. 3 Progra m Descriptio n 1.3. 1 Tes t Operatin g Condition s Th e test conditio n fo rthi s CP Twas designe d t o demonstrate compliance wit h th e applicabl e MAC Tdioxin s an d furan s (PCDDs/PCDFs) ; tota l hydrocarbons , hydroge n chlorid e an d chlorine , an d particulate matte r(PM ) emission s standards . Durin g th e dioxin/fura n emissio n testing , Uni t 3 was operate d a t minimu m combustio n zon e temperature s whil e maximizin g pumpabl e an d tota l waste feeds . Norma l (o rhigher ) level s o f chlorin e were fed . Th e flu e ga s flo wrat e an d baghous e inle

t temperatur

e wer e maximized . Durin g th e HCI/CI 2 emissio n testing , Uni t 3 wa s operate d a t maximu m flu e ga s flo

wrat e an d maximu m chlorin e fee d rate . Sorben t fee d rat e an d carrie rflui d flo

wrat e wer e minimized .

1- 1 Februar y 201 0

# AZCONl Durin g th e P M emissio n testing , Unit 3 was operate d a t maximu m flu e gas flo

wrat e an d maximu m as h fee d rate . T o ensur e tha t th e particulate matte rcontro l devic e underwent it

s norma l (o rmor

e frequent ) cleanin g cycle , a cleanin g cycl e wa s manuallyinitiate d durin g eac h ru n if a timed cleanin g cycl e wa s no t anticipated . Th e waste fee d rate s tha

t wer e use d fo rth e performanc e test progra m ar

e summarized i n Tabl e 1-2 . Acop y o f th e actua l proces s monitorin g data i s include d i n Appendi xA . 

## 1.3. 2 Baghous e Cleanin g Cycl e Durin g al l thre e test run s i n th e P M an d HCI/CI 2 

### testin g program s o n Unit 3 , cleanin g cycle s forth e baghouses wer e manuall yinitiate d durin g th e testing . Th e cleanin g cycle s wer e manuallyinitiated t

o ensur e th e baghouse s went throug h a cleanin g cycl e durin g th e stac k samplin g since th e typica l operatio n ofth e cleanin g cycl e i s initiate d b

ya time rever

yfou rhours . Th e baghous e cleanin g cycle s occurre d a t approximately11:3 1 durin g Ru n 1 , a

t 10:20 durin g Ru n 2 , an d a t 10:58 durin g Ru n 3 ofth e P M an d HCI/CI 2 

### testin g programs . Relativel yhighe rpressur

e drops ca n be noted i n th e operatin g data fo rapproximatelyseve n minutes durin g whic h th e baghouse s wer e undergoin g th e cleanin g cycle . Thi s satisfie s th e requirement s i n 4 0 CF R §63.1207(g)(1)(C)
. 

## 1.3. 3 Chlorine Fee d Pursuan t t o 4 0 CF R §63.1207(g)(1)(A) , norma l o rhighe rlevel s o f chlorin e wer

e fed t o Unit 3 durin g th e dioxin/fura n performanc

e tests . Th e historica l averag e feedrate fo rchlorin e i s 60 Ib/hr
. Th e tes t feedrates fo r chlorin e durin g al l dioxin/fura n tes t run s wer e >13 1 Ib/hr
. 

## 1. 4 Condition s i n USEP ACP TApprova l Lette rDate d Novembe r25 , 2009 1.4. 1 Incinerato r2 DR E Data i n Lie u Reques t USEP Astate d i n th e CP Tapprova l lette rtha t Veoli a ma

yre-submi t th e reques

t t o us e previou s DR E tes

t data a s documentatio n o

f compliance wit h th e HW C MAC Temissio n standar d fo rDRE . O n Decembe r3 , 2009 , Veoli a submitte d results o f a n Incinerato r2 DR E tes t (repor t date d Marc h 8 , 1993

) t o th e USEPA
. EP A reviewe d th e Incinerato r2 data an d conclude d tha t it meet s th e criteri a set fort h i n 40 C.F.R
. § 63.1207(c)(2)(i)(A-D) . USEP Asen t Veoli a a lette rdated Decembe r11 , 200 9 approvin g Veolia' s reques t t o us e prio rRCR ATria l Burn DR E data fo rIncinerato r2 t o demonstrated compliance wit h th e DR E standar d i n 4 0 C.F.R
. § 63.1219(c

) an d t o establis h th e DR E OPL' s require d b y40 C.F.R
. § 63.12190) . 

## 1.4. 2 Incinerator s 2 , 3 , an d 4 Metal s Data i n Lie u Reques t Th e USEP Aapprove s Veolia' s reques t t o us e metal s performanc

e tes t dat a fro m Augus

t an d Septembe r200 8 to demonstrate compliance wit h th e mercury , SVM , an d LV M emissio n standard s an d t o establis h th e applicabl e mercury , SVM , an d LV M OPL' s if metal s fee d rate s ar e base d solel yo n th e spik e concentrations . Th e results o

f th e performance tests o n eac h hazardou s wast e incinerato rdemonstrate complianc e with th e mercury , SVM , an d LV M emissio n standard s unde rth e condition s tha t existe d durin g testing . Du e t o th e questionabl e moistur

e conten t ofth e soli d waste samples , agreemen t o n th e metal s concentratio n ofth e soli d wast e i s th e subjec

t o f curren t discussion s Veoli a an d USEP Aar e havin g regardin g th e inclusio n o f metal s feed s tha t wer e nativ e t o th e waste s t

o determin e th e metal s fee d rates fo rth e 2008 performanc e tests .

1- 2 Februar y 201 0 

## VES01828 5

## 1.4. 3 Reques t t o Us e Metho d 23 fo rDioxins/Furan s o n Incinerators 2 an d 3 . USEP Adisapprove d Veolia' s reques t t o us e Method 2 3 instead o f Metho d 0023 At o conduc t th e dioxin/fura n performanc

e tests o n Incinerator

s 2 an d 3 . Veoli a use d Method 0023 Afo rth e dioxin/fura n performanc e tests o n al l thre e incinerators . 

## 1.4. 4 "A s Fired " Wast e Analyse s an d Wast e Description s Veoli a agree d t

o includ e i n th e fina l tes

t bur n repor t th e "a s fired " heatin g valu e an d concentration s o f ash , mercury , SVM , LVM , tota l chlorin e an d organi cHAP' s i n eac h wastestrea m burned durin g th e CPT
. Include d i n Appendi xAar

e th e waste fee d profil e sheets , whic h contai n th e chemica l composition s o f th e wastes , an d th e analyse s ofth e wastes , whic h contai n th e "a s fired" heatin g valu e an d concentration s o f ash , mercury , SVM , LVM , an d tota l chlorine . 

## 1.4. 5 Table s 1- 1 an d 5- 1 o f th e CP TPlan s fo rIncinerators 2 , 3 , an d 4 Fo rth e hydroge n chlorid e an d chlorin e emission s paramete ri n Table s 1- 1 an d 5-1 , th e correc

t limit shoul d be 32 ppm vCl " o n a dr

ybasis , correcte d t

o 7 % oxygen . Th e correc

t citatio n i s 4 0 C.F.R
. § 63.1219(a)(6) . Thes e hav e bee n correcte d i n thi s report . Fo rth e PCDDs/PCDF s (TE Q basis ) emission s paramete ri n Table s 1-1 an d 5-1 , th e limi t o f 0.20 ng/dscm fo r operatio n abov

e 40 0 de g F an d th e limit o f 0.4 0 ng/dsc m fo roperatio n belo w40 0 de g F ca n applyt

o Veolia' s hazardou s waste incinerator s sinc e th e inle

t temperatur

e to th e particulat

e matte rcontro l devic

e ca n b e controlle d abov

e o rbelo w40 0 de g F . Incinerator

s 2 an d 3 demonstrated compliance a t a n emissio n leve l <0.20 ng/dsc m s o bot h unit s continu e t

o hav e th e abilit

yt o operate thei rrespectiv

e pollutio n contro l equipment wit h a n inle

t temperatur

e above 40 0 de g F . Incinerato r4 ha s historicall ydemonstrate d complianc e a t a n emissio n leve l o

f <0.20 ng/dsc m howeve rwa s onlycapabl e o

f demonstratin g compliance a t a n emissio n leve l o f <0.4 0 ng/dscm
. Th e inlet temperatur e mus t b e controlle d belo

w400 deg F . Veoli a i s currentlyconsiderin g whethe rt o continu e operatin g belo w40 0 de g F o rrepea

t th e test .

1- 3 Februar y 201 0 

## VES01828 6

# AZCOM Tabl e 1- 1 Summar

y o fApplicabl e MAC TEmissio n Standard s 

### I Emission s Paramete r Limi t Citatio n PCDDs/PCDF s (TE Q basis) £0.2 0 ng/dsc m £ 0.4 0 ng/dsc m 40 CF R 63.1219(a)(1)(i)(A ) 40 CFR§63.1219(a)(1)(i)(B ) Carbo n Monoxid e < 10 0 ppm v 4

0 CFR§63.1219(a)(5)(i ) Tota l Hydrocarbon s s1 0 ppm v 40 CF R § 63.1219(a)(5)(ii ) Hydroge n Chlorid e & Chlorin e £ 3 2 ppm vdr ya s Cl " 40 CF R § 63.1219(a)(6) Particulate Matte r(PM ) £ 0.01 3 gr/dsc f 4

0 CF R § 63.1219(a)(7) Note : Al l emissio n concentration s ar e correcte d t

o 7 % oxygen .

1- 4 Februar y 201 0 

## VES01828 7

# AZCOM Tabl e 1- 2 MAC TOPL s Establishe d Durin g th e Performance Tes t Proces s Paramete r Unit s Avg . Perio d Ho

wLimit Establishe d 

### Maximu m Pumpabl e Waste Fee d Rat e Ib/h r 1-h r Avg . o f max. HRAs fo r eac h ru n Maximu m Tota l Hazardou s Wast e Fee d Rate Ib/h r 1-h r Avg . o f max . HRA s fo r eac h ru n Minimu m PC C Temperatur e ° F 1-h r Avg . o f th e tes t ru n averages Minimu m SC C Temperatur e ° F 1-h r Averag e ofth e tes t ru n averages Maximu m Flu e Ga s Flowrat e acf m 1-h r Averag e o f maximu m HRAs fo reac h ru n Maximu m As h Fee d Rate Ib/h r 12-h r Averag e o f th e tes t ru n averages Maximu m Chlorine/Chlorid e Fee d Rat e Ib/h r 12-h r Average , o f th e tes t ru n averages Minimu m Sorben t Feedrate lb/l b Cl 2 

### 1-h r Avg . o f th e tes t ru n averages Minimu m Carrie rFlui d Flowrate gal/l b Cl 2 

### 1-h r Avg . of th e tes t ru n average s Maximu m Fabri cFilte rInle t Temperatur

e op 

### 1-h r Averag e o f th e test ru n averages

1- 5 Februar y 201 0 

## VES01828 8

# 2. 0 Incinerato r Proces s Descriptio n 

# A-COM

2. 1 Proces s Overvie w Veoli a operate s tw

o Fixe d Heart h Dua l Chambere d Incinerator s (Unit s 2 an d 3 ) an d on e rotar

ykil n incinerato r (Unit 4) a t th e Sauget , I L facility . Th e tw o fixe d heart h unit

s ar e rated a t 1 6 millio n Btu/h reach . Incineratio n Unit No . 3 i s a mirro rimag e o f Uni t No . 2 . Both o

f thes e unit

s hav e thei row n wast e handlin g system s a

s describe d i n th e section s tha t follow . Th e onlydifference bein g Uni t No . 2 i s equippe d wit h fou r(4 ) baghouse modules , whil e Uni t No . 3 i s equippe d wit h thre e (3 ) baghous e modules . However , eac h incinerato ri s operate d identicall ywit h onlythre e baghous e module s i n service durin g operation . Unit 4 i s rated a t 50 millio n Btu/h ran d i s equippe d wit h it s own tan k

far m system , dru m storage , bul k solid s storag e an d fee d systems . 

## 2. 2 Wast e Fee d System s [4 0 CF R § 63.1207(f)(1)(ii)(c ) an d (f)(1)(iii)(D ) an d (E) ] 2.2. 1 Uni t 3 Liqui d Wast e Fee d Syste m an d Blendin g Operation s Th e fixe d heart h incinerato ri s designe d t o receive containers , aqueou s liqui d wastes , organi cliqui d wastes , specialt yliqui d feed s an d direc

t injec t liquid s fe d throug h th e aqueou s o rorgani cliqui d fee d systems . Thes e unit s ca n receive anycombinatio n o f waste s - liquid , semi-soli d o rsoli d - with a hea t valu e o f u p t o 1 6 millio n Btu/hr
. Uni t 3 i s supporte d b

ystorage/blen d tank

s locate d i n Tan k

Farm #1 . Rate s o

f fee d ar e controlle d a

t eac h incinerator . Segregate d liqui d waste s ar e store d unti l utilize d i n th e wast e blendin g facilities . A

t tha t time , liquid s ar e delivere d t

o th e blendin g tank

s wher e th e dail yliqui d fee d t

o th e incinerato ri s formulated , tested , an d release d t

o th e incinerator . Biendin g o f store d liqui d waste s t

o achiev e optimu m heatin g valu e an d viscosit yfo rincineratio n take s place i n Tank s 2,4, 6 & 8 . Si xadditiona l tank s (10 , 20 , 30 , 40 , 50 & 60 ) ar e use d t o segregate differen t wast e strea m types fo rblendin g o f liqui d fee d t

o th e incinerator . Severa l criteri a are important i n designin g a blen d fro m availabl e Wastes tha t hav e bee n segregate d principall yb yphysica l an d chemica l properties . Thes e includ e compatibility , prope rrang e o f heatin g value , an d permit restriction s regardin g elementa l compositio n (base d o n emissio n limitations) . Th e materia l i s transferred throug h abovegroun d pipeline s fro m th e tan k farm t o th e incinerator . Pipeline s use d t o transfe rliqui d organi cwast e an d aqueou s wast e ar

e equippe d wit h strainers . I n compliance wit h th e Benzen e NESHAP , al l tank s ar e vented t o individua l carbo n adsorptio n canister s fo r remova l o f organics befor

e vapo ri s discharge d to th e atmosphere . Eac h carbo n adsorbe rcaniste ri s essentiall yequivalen t t

o a 5 5 gallo n containe ro rgreater , i f necessary . Al l tank s ar e equipped wit h conservatio n vents , i n additio n to th e carbo n caniste radsorber . Al l tank s ar e grounded , an d flam e arrestor s are installe d betwee n th e carbo n adsorber s an d th e tanks . 

## 2.2.1. 1 Organi can d Aqueou s Liqui d Wast e Feed s Th e liqui d wast e injector

s use d i n th e combustio n chamber s ar e air-atomizin g injectors . Thes e ar e used fo r injectio n o f hig h Btu , lo

wBt u liquid s an d specialt

yfee d liquids . Dua l flui d injectio n nozzle s wil l b e use d fo r atomizatio n o

f th e waste . Eac h o

f th e injector

s i s rated a

t 0-300 gph . Th e liqui d waste fee d nozzle s ar e serve d b yparalle l redundan t pumps an d recirculatio n system s wit h bac k pressur e control .

2- 6 Februar y 201 0 

## VES01828 9

# AsCO M 2.2.1. 2 Package d Wast e Fee d 

### Container s o f waste s ar

e sample d an d analyze d afte rreceipt i n accordance wit h th e facility' s Waste Analysi s Plan . Thes e waste s ca n the n be delivere d directl yt o Uni t 3 o rrepacke d int

o smal l combustibl e container s a t th e facility . Fiberboar

d o rplasti ccontainer

s (fullyo rpartiall yful l o

f waste) , u p t

o 40-gallo n size , ma

yb e charge d directl yt

o th e primar

ychamber . Thes e wil l b e receive d a t th e doc k adjoinin g eac h fixe d heart h incinerator , an d charge d t o th e incinerato rwithi n 2

4 hour s o rreturned t

o permitted storage . Solids , usuall ypackage d i n plasti co rfiberboar d containers , ar

e introduced int

o th e incinerato rthroug h a PL C controlle d airlock-ra m syste m locate d a t th e lowe rfron t o

f th e primar

ychambe ro

f th e incinerator . Th e airloc k i s compose d o

f a refractory-line d door , a doo rint o th e airloc k

enclosure , an d tw

o pneumati crams . The actio n o f th e feede ri s a s follows :

• Wit h th e incinerato rdoo rclosed , th e airloc k doo ri s opened . • Th e firs

t pneumati cra m (loa

d ram ) pushe s weighe d charge s o f waste int

o th e airloc k

chamber . • Th e airloc k

doo ri s closed . • Aswitc h i s activate d eithe rautomaticall yo rmanually , whic h open s th e doo rt o th e incinerato ran

d actuate s th e ram (charg e ram) tha t pushe s th e waste int

o th e incinerator . Th e ram the n retract s an d th e incinerato rdoo rcloses . 2.2 .1 . 3 Specialty Liqui d Wast e Feed s 

### Specialt yFee d System s associate d with incinerato rNo . 3 ar e a s follow

s
• Hoode d Specialt

yContaine rFeede r • Glov e Bo

xEmissio n Contro l System s • Direc t Injec t Liqui d Fee d Syste m 

## 2. 3 Manufacturer , Mak e an d Mode l o f th e Incinerato r[4 0 CF R § 63.1207(f)(1)(iii)(A) ] 2.3. 1 Combustio n Chambe ran d Burner s [40 CF R §63.1207(f)(1)(iii)(B ) an d (C ) Incinerato rNo . 3 feature s a two-stag e combustio n process . Ignitio n o f waste materia l take s place i n the primar y(lower ) combustio n chambe r(PCC)
. Asecondar y(upper ) combustio n chambe r(SCC ) serve s a s a n "after-burner " fo rproces s gases . Ignitio n o f th e waste take s place a t temperatures i n exces s o f 1700 degree s F . Th e secondar ycombustio n chambe rmaintain s a minimu m temperatur e o f approximately180

0 degree s F . Th e fixe d heart h incinerato ri s fabricate d o f carbo n steel . Th e primar ychambe rhas a n externa l diamete ro f 9 fee t an d i s 17. 5 feet long . Th e interio rwall s o f th e chambe rar

e line d wit h approximatel y1 0 inche s o f bric k refractor yan d insulatio n backing , makin g th e interna l operatin g diamete rapproximatel y7'2" . Th e cross sectiona l are a o

f th e chambe ri s thu s 40. 3 squar e feet . Tabl e 2-2 provides a summar yo f th e incinerato r desig n specifications . Liqui d an d soli d wast e feed s ente rth e lowe rchambe ro n th e front-fac e o f th e chamber . Th e primar yburne r an d th e specialt

yfee d injecto rare locate d nea rth e front-face o f th e chambe ran d ar

e mounte d tangentially .

2- 7 Februar y 201 0 

## VES01829 0

# AsCO M Th e primar

yburne ri s a North America n burne rrated a t 12. 0 millio n Btu/hr
. an d i s used i n th e lowe rchambe r to maintai n permitted temperatures . I t wil l bur n onl ynatura l gas o rNo . 2 fue l oil . Th e burne rsyste m i s supplie d wit h combustio n ai ra t a stati cpressur

e o f 30 " wate rcolum n (WC)
. Th e pilo t fo rth e primar

yburne rwil l bur n natura l gas . Th e fue l syste m fo rth e lowe rchambe r(an d secondar ycombustio n chamber

) i s controlle d b

ya Factor yMutua l approve d burne rmanagement syste m complete wit h interlock s an d safet

yvalves . 

## 2.3. 2 SecondaryCombustio n Chambe r Th e secondar

ycombustio n chambe r(SCC ) i s a horizontal , cylindrica l chambe rtha t has a n externa l diamete ro

f 9 feet an d i s 17. 5 feet long . Th e interio rwall s o f th e chambe rar

e line d with approximately1 0 inche s o f bric k refractor yan d insulatio n backing , makin g th e interna l operatin g diamete rapproximately 7'2" . Th e cross-sectiona l are a o f th e chambe ri s thu s 40. 3 square feet . Followin g ignitio n o

f th e wast e materia l unde rcontrolle d o rstarved-ai rcondition s i n th e lowe rchamber , offgase s trave l throug h a refractory-line d flu e ga s passag e into th e uppe rchamber , whic h act s a s a n afterburner . Turbulence i s achieve d b

yth e tangentia l introductio n o f ai ran d additiona l fue l i n th e uppe rchamber . Th e SC C i s equippe d wit h on e burne rmounte d tangentiall yo n th e sid e ofth e chamber . Th e burne ri s a Nort h America n burne rrate d a

t 6. 0 millio n Btu/h ran d i s fuele d wit h natura l gas o rfue l oil . A s wit h th e primar

ychambe rburner , th e SC C burne ri s supplie d wit h atomizin g ai ran d i s equipped wit h a burne rmanagemen t system . Thi s syste m control s th e ignitio n an d initiates a n automati cshutof f whe n ther

e i s a los s o f flame , combustio n ai rsupply , fue l pressure , atomizin g ai rpressure , o rpilo t burner . Leavin g th e uppe rchamber , th e ho t gas strea m travel s throug h 2 8 fee t o f refractory-line d stac k

section s befor

e reachin g th e star

t o f th e gas scrubbin g system . Th e combine d volum e o f th e uppe ran d lowe rchambers , th e flu e gas passag e an d th e ho t crossove rsectio n i s approximatel y1,56 7 cubi cfeet . Th e tota l retentio n tim e o f combustio n gase s withi n th e syste m i s approximatel y5 seconds . 

## 2.3. 3 Locatio n o f Combustio n Zon e Temperatur e Devic e [4 0 CF R §63.1207(f)(1)(xix) ] Th e thermocoupl e tha

t monitor s temperatur

e i n th e primar

ycombustio n chambe ri s located o n to p ofth e chambe rabou t five feet fro m th e transition . Th e thermocoupl e tha t monitor s temperatur

e i n th e SC C i s locate d o n to p o f th e chambe rabov

e th e transition . 

## 2.3. 4 Hazardou s Wast e Residenc e Tim e [4 0 CF R §63.1207(f)(1)(ix) ] Th e Hazardou s wast e ga s residence tim e fo rth e Fixe d Heart h Incinerato ri s calculate d as follows :
• Primar

yCombustio n Chambe rVolum e - 63 5 ft 3 • Secondar

yCombustio n Chambe rVolum e - 63 5 ft 3 • Tota l Volum e - 127

0 ft 3 • Maximu m Flu e Ga s Flowrate -17,38 2 acf m (29 0 ft 3 

### /sec ) • Tota l Combustio n Zon e Residence Tim e = (127 0 ft 3

### )/(29 0 ft

3 

### /sec) = 4. 4 se c

2- 8 Februar y 201 0 

## VES01829 1

# AECOM Since thes e incinerator

s ar e fixe d heart h unit

s residence tim e i s base d on th e elapse d tim e sinc e th e las t solid s charg e was pu

t int o th e combustio n zon e o rbase d o n th e trave l length o f th e as h ra m tha

t function s t

o clea rth e primar

ycombustio n chambe ro

f soli d waste residue . A n elapse d tim e o f on e hou ro ra trave l length , o f 11 0 inche s fo rth e as h ram hav e bee n establishe d as th e criteri a fo rdeterminin g whe n soli d wast e i s no longe ri n th e combustio n zones . 

## 2.3. 5 Combustio n Syste m Lea k Combustio n syste m leak

s ar e prevented throug h maintainin g a totall yseale d combustio n chamber , coupled with th e us e o

f a n induce d draf

t fa n tha t maintain s a vacuu m o

f normally- 4 t

o - 6 inches o

f wate rcolum n i n bot h combustio n chamber

s whil e waste s are bein g fe d t o th e unit . 

## 2.3. 6 EmergencySafetyVen t Th e incinerato ri s equippe d with a n emergenc ysafet yven t (ESV ) locate d a

t th e top o f th e secondar

y combustio n chamber . Thi s ES V i s a refractory-line d emergenc ytherma l relief vent (TRV ) whic h i s hel d i n th e close d positio n b

ya pneumati ccylinder . Th e contro l valve i n th e lin e supplyin g ai rt o th e cylinde ran d th

e cylinde rven t valve tha

t open s th e TR V are locate d i n th e contro l roo m fo reac h unit . Valve lock s (with key

s attached ) are utilize d t

o dete rindiscriminate operatio n o f thes e valves . Openin g ofth e TR V allow s ho t combustio n ga s t

o ven t fro m th e combustio n syste m durin g emergenc yshutdown events . Th e purpos e o f th e TR V i s t o protec t th e downstrea m APC S fro m excessive temperatur e situations . Alimi t switc h o n th e 1R V shut s of f al l wast e feed s t

o th e syste m a s it sense s tha t th e ca p i s opening . 

## 2. 4 Procedure s fo rRapidl yStoppin g Hazardou s Wast e Fee d Durin g Equipmen t Malfunctio n [4 0 CF R §63.1207(f)(1)(viii) ] Equipmen t malfunction s ar e identifie d b

yth e contro l system , observatio n o f proces s contro l variables , o rb y regula rfiel d inspections . I n th e even t o

f mino requipment malfunction s (e.g . waste fee d o rscrubbe rleaks) , th e contro l roo m operato r wil l be notified . Th e contro l roo m operato rwil l the n clos e th e waste fee d valve s an d disabl e th e waste feed pumps . I n th e even t o

f majo requipment malfunction s (e.g . fire), th e emergenc ysto p butto n locate d i n th e contro l roo m wii l be pushed . If thi s butto n i s pushed , al l equipmen t wil l switc h t o it s fail-safe position . 

## 2. 5 Ai rPollutio n Contro l Equipmen t [4 0 CF R §63.1207(f)( 1 )(iii)<G) ] 2.5. 1 Ai rPollutio n Contro l System s Description s Th e ai rpollutio n contro l syste m consists o f a spra ydrye rabsorbe ran d fabri cfilte rbaghouse . Th e ai rpollutio n contro l syste m neutralize s acidi ccompound s an d remove s particulate fro m th e exhaus t gas . Tw o subsystems , th e spraydrye rabsorbe ran d th e fabri cfilter , carr yout th e chemica l neutralizatio n an d particulat e remova l functions , respectively . Athir d subsystem , th e lim e system , i s use d t o prepar e an d provid e lim e slurr

y t o th e spra ydrye rabsorbe rfo rus e i n th e chemica l neutralizatio n process . Th e induced draf t fa n an d stack provid e th e mechanica l energyrequire d t o transpor

t th e flu e ga s throug h th e interconnectin g ductwork , t o it s eventua l discharg e poin t t o atmosphere .

2- 9 Februar y 201 0 

## VES01829 2

# AECOM 2.5.1. 1 Lim e Syste m 

### Th e lim e syste m prepare s lim e slurr yfo rus e i n th e chemica l neutralizatio n process i n sufficien t suppl yan d concentratio n t

o maintai n continuou s flu e gas treatmen t i n th e spra ydrye rabsorber . Th e syste m has bee n designe d fo rbatch mixin g t o provid e thi s service . Veoli a utilize s hydrated lim e a s it s neutralizin g agenti n th e ai rpollutio n contro l systems . Th e ke yneutralizatio n paramete ro f th e hydrated lim e i s th e "Ca O Equivalent" . Figure 2- 1 i s th e specificatio n shee t fo rth e hydrated lim e tha t Veoli a uses . Veoli a ha

s use d thi s specifi c produc t fo rove r2 0 year

s an d plan s t

o continu e wit h it

s use . Although , if Veoli a does chang e supplier s o rtyp e o f lim e i n th e future , it woul d hav e a "Ca O Equivalent " specificatio n equa l t o o rgreate rtha n th e 72.6 % show n o n Figur e 2-1 . 

### Hydrated lim e i s store d i n a storag e bi n abov e th e lim e preparatio n area . Th e storag e bi n i s size d t o hold enoug h hydrated lim e t

o maintai n severa l day

s o f syste m operatio n a

t th e maximu m combustio n rate ofth e incinerator . Lim e i s discharge d throug h th e conica l storag e bi n bottom . Th e flo wo f th e materia l fro m th e bi n i s aide d b ya vibratin g "live bottom, " o rbi n activator . Avariabl e spee d scre wfeede ri s used t

o mete rth e hydrated lim e i n th e proportion s require d fo rbatc h mixin g lim e slurry . Th e lim e i s mixed with wate ri n atan k beneat h th e iim e storag e bin . Th e screwfeede rspee d an d th e rat e tha t wate ri s added t

o th e lim e slurr

ytan k are variabl e so tha

t th e desire d lim e solid s concentratio n ca n be achieve d i n th e tank . Th e variabl e feed adjustment

s allo wwate ran d lim e t

o b e adde d to th e lim e slurr

ytan k a t a rat e tha t wil l allo wa batch mod e o

f mixing . A n agitato ri s provide d i n th e slurr ytan k t o mixth e wate ran d lim e an d t o maintai n th e suspensio n o f lim e solids . Th e mixe d lim e slurr yi s pumped a

t a continuou s rat

e o f flo wthroug h a recirculatio n loo p t o th e atomize ra

t a rat e o f u p t o 1 0 gpm . 2.5.1. 2 Spra

y Dr y Absorbe r 

### Uni t 3 i s equippe d wit h a Spra yDrye rAbsorbe r(SDA) locate d immediatelydownstrea m ofth e secondar y combustio n chamber . Th e SD Aunit i s fabricate d o f 3/ 8 inc h carbo n steel . Th e functio n o f th e SD Ai s to :

• Furthe rcoo l th e combustio n gase s fro m 1600-2000° F t o 300-500°F , • Neutraliz e an d remov e HC I an d othe racid s fro m th e combustio n gases , • Remov

e a portio n o

f th e particulate (flyash ) fro m thes e gases . Slurr yflo wt o th e spra ydrye rabsorbe r(SDA) i s metere d b ya flo wcontro l valve t

o obtai n th e prope rfeed concentratio n t

o th e spra ydrye rabsorbe ratomizer . Automati c(o rmanual ) adjustment t o th e flo wi s made a s a functio n o

f th e outpu t fro m a hydrochlori caci d (HCI ) analyze ri n th e ga s duc t downstrea m o

f th e fabri cfilter . Th e amount o

f slurr ymetere d i s proportiona l t o th e amoun t o

f HC I monitored . Th e slurr ypasse s throug h a stationar yswirl-typ e liqui d distributo rint o th e atomize rwhee l wher e induce d centrifuga l force fro m th e rapidl yspinnin g whee l discharge s th e slurr ythroug h th e whee l nozzle s a t hig h velocity . Th e desig n o

f th e atomize rwheel , it

s rate o f spin , an d th e discharg e velocit yo f th e slurry , create a clou d o f finel ydivide d droplets aroun d th e peripher yo f th e atomize rwheel . Afeedbac k signa l fro m th e atomize rpowe rtransmitte rprovide s verificatio n tha t wate rflo wt o th e atomize rincrease s o rdecrease s i n proportio n t

o th e spra ydrye rabsorbe routle

t temperature . Flu e ga s enter s fro m th e botto m o

f th e spra ydrye rabsorbe rthroug h a vertical , centrallylocate d disperser . Th e disperse rdirects th e flu e gas throug h th e zon e fille d b yth e atomize d slurr

yclou d wher

e th e flu e ga

s an d slurr ymi xan d mos

t ofth e absorptio n occurs . Th e gase s the n flo wdownwar

d throug h th e absorbe rchambe r

2-1 0 Februar y 201 0 

## VES01829 3

# AECOM an d exi t throug h a botto m sid e duct . A s th e gase s contac t an d pas s throug h th e clou d o f atomized lim e slurry , th e wate ri n th e slurr

yevaporates , coolin g th e gases . Simultaneously , th e lim e i n th e slurr yreact s wit h th e hydroge n chlorid e i n th e gase s t o produc e calciu m salts . Som e o

f th e resultin g dr

ymaterial , consistingof calciu m salts , flyas h an d exces s lime , fall s t o th e conica l botto m ofth e unit . Th e dr ymateria l fro m each unit i s discharge d t

o a conveyo rsyste m tha

t transport s it t o a dum p traile ro requivalen t type system . 2.5.1. 3 Fabri c Filte r 

### Ga s exhauste d fro m th e spra ydrye rabsorbe ri s distribute d b ymanifol d duct

s t o thre e fabri cfilte rmodules . Withi n eac h filte rmodule , th e ga s i s passe d throug h Teflon-coate d fiberglas s clot h bags . Th e gas passe s fro m th e outsid e t

o th e insid e ofth e filte rbags . Particulate , entraine d i n th e ga s stream , i s mechanicall ydeposite d o n th e outsid e ofth e filte rbag s a s th e gas passe s throug h th e cloth . Eac h modul e has a clea n ai rplenu m an d housin g sectio n to contai n approximately96 bags . Eac h ba g i s approximatel y6 " i n diamete rb y20 ' long . Th e baghouse s are fabricate d fro m 3/16 " mil d stee l plate , o f welde d construction , ga s tigh t an d stiffene d t o withstan d th e maximu m operatin g negativ e pressure . Eac h compartmen t has a tube sheet tha t support s th e bag s an d provide s fo rtop bag/cag e removal . Acces s ta th e clea n ai rplenu m i s vi a a sid e acces s doo ri n th e clea n ai rplenum . Th e fabri cfilte rcleanin g mechanis m utilize s jets o f ai rto clea n th e filte rbags . Periodically , th e cleanin g sequenc e wil l be initiated . Th e sequence i s eithe rstarte d a t th e en d o

f a timed cycle , o rwhe n th e differentia l pressure acros s th e filte rreache s a predetermined setpoin t o f approximately7.0 " w.c , o rwhe n th e operato r initiate s a cycle . Th e controlle rthe n sequence s t o eac h ro wo f filte rbag s i n eac h module , releasin g a burs t o f ai ropposite t

o th e directio n o

f ga s flow . Th e quickl yrelease d burs t o f ai rdislodge s dus

t cake o n th e exterio ro

f eac h bag a s it travel s fro m th e to p t o th e botto m ofth e bags . Release d fro m th e bag , th e dus t cak e fall s b y gravit yint o th e hoppe ra

t th e botto m o

f th e module . Fro m ther

e i t i s discharge d t

o a conveyo rsyste m tha

t transports it t

o a dum p trailer , o requivalen t type system . Treate d b yth e spra ydrye rabsorbe ran d filtere d b yth e fabri cfilter , th e cleane d flu e gas exits th e Fabri cfilte r module s to a n outle

t manifol d fo rexhaust . 2.5.1. 4 Induced Draf t Fa n an d Stac k 

### Th e induce d draf

t fa n an d stac k

are locate d downstrea m o f th e fabri cfilter . Combustio n gase s ar e drawn throug h th e syste m b

ya 7 5 h p induce d draf

t (ID ) fan , rate d a

t 15,000 acf m a

t 400 ° F saturated , an d 22 " wate r colum n pressure . Th e induce d draf t fa n provides th e mechanis m fo rtransportin g th e incinerato rflu e gas throug h th e spra

ydrye rabsorber , Fabri cfilter , an d al l interconnectin g ducts . Th e I D fa n include s an inle t volum e contro l dampe rt

o b e use d t

o contro l th e velocit

yo f th e ga s withi n th e ductin g an d treatment devices . Treate d gasse s exhauste d fro m th e induce d draf t fa n t o th e atmospher

e throug h a 90-ft . hig h stack . Th e stac k diamete ri s 39 inche s I.D . Th e stac k i s equippe d wit h instrument samplin g port s an d a samplin g platfor

m fo remission s testing . Figure 4-1 provides detail s o n th e desig n an d sampl e por t location s an d configuration s fo rth e stack . 

## 2. 6 Stac k

Emission s Monitorin g [4 0 CF R §63.1207(f)( 1 )(iii)(H) ] Th e continuou s emission s monitorin g syste m (CEMS ) consist s o f sampl e probes , sampl e deliver yan d conditionin g apparatus , an d ga s analyzers . Sample s ar e extracte d fro m th e samplin g port s o n th e stack . A

2-1 1 Februar y2010 

## VES01829 4

# AECOM CE M performanc

e tes t an d qualit

yassurance progra m has bee n implemented i n accordance with th e Appendi x to Subpar

t EE E o fPar t 63—Qualit

y Assuranc e Procedures fo r Continuou s Emission s , Monitor s Use d fo r Hazardou s Wast e Combustors . 

### Response s fro m eac h CEM S wer e fe d t o th e Contro l Syste m (CS ) wher e th e C O hourlyrollin g averag e wa s calculate d an d interlocke d t o th e waste fee d cutof

f valve s a s par

t ofth e Automati cWast

e Fee d Cutof

f Syste m (AWFCO ) discusse d i n Sectio n 2.8 , below . Th e followin g provide s a brie f descriptio n ofth e CEM S instruments includin g th e operatin g rang e an d measuremen t principal . 

## 2.6. 1 CEM S Syste m Descriptio n Th e Continuou s Emission s Monitorin g System s (CEMS ) currentl yutilize d a t Incinerato r3 analyze s fo ropacity , carbo n monoxide , hydroge n chloride , tota l hydrocarbon s an d oxygen . Thes e monitors , excep t opacity , ar

e extractive device s mounted i n samplin g port s o n th e stack . Th e tabl e belo wsummarize s th e analyze r specifications . Th e opacit

ymonito rcontinuousl ymeasure s th e stac k gas opacit

yan d report

s th e measurement

s t o a n indicato ran d a recorder . A n opacit ytha t exceed s a preset limi t trigger s a n alarm an d interlock . Carbo n monoxid e an d hydroge n chlorid e ar e monitored wit h extractiv

e non-dispers e infrared analyzers , Tota l hydrocarbo n i s monitored wit h a n extractiv e flam e io n detecto ranalyzer . Oxyge n i s monitored wit h a zirconiu m oxid e cell . Stac k ga s flow rat

e i s continuousl ymonitored usin g a n anuba rtha t send s a 4-2 0 m

Asigna l t o th e PL C tha

t converts th e signa l t

o acfm . Tabl e 2

- 1 Continuou s Emissio n Monitor s Paramete r Curren t Mfg . Rang e Principl e 

### Oxyge n COS A 0-25% Electrochemica l Carbo n Monoxid e Ecoche m MC 3 0-200 ppm v 0-3000 ppm

v Infrared Tota l hydrocarbon s Thermoelectro n 0-100 ppm v FID/

I nfrared Hydroge n chlorid e Ecoche m MC 3 0-1,000 ppm v infrare d Opacit y Teledyn e 0-100% Whit e light Stac k ga s flo w PSE/Rosemoun t 0-20,000 acf m Pressur e dro p 

## 2. 7 Proces s Monitorin g an d Contro l Th e facilit yi s equipped with a state-of-the-ar t monitorin g an d contro l system , whic h facilitate s complianc e wit h permi t conditions , an d otherwise , collects proces s contro l information , facilitate s efficien t operatio n an d detects an d prevents damag e t

o th e facility . Th e syste m consist s o f thre e majo rcomponents :

• Ahuman-machin e interface (HMI ) system , • Programmabl e logi ccontroller' s (PLC's) , an d

2-1 2 Februar y 201 0 

## VES01829 5

# AECOM

• Ahig h spee d etherne

t cabl e connects al l contro l syste m component s Th e desire d contro l function s are implemente d throug h th e HM I system . Al l digita l contro l an d emergenc y interlock s ar e accomplishe d b

yth e PLC
. Th e contro l syste m i s capabl e o f monitorin g th e "operationa l envelope " ofth e incinerato ran d i s capabl e o f performin g a numbe ro

f activitie s including :

• Contro l roo m indicatio n o f processo rsensor

s locate d withi n th e incinerato rsyste m (suc h as pressur e indicatio n o

f a fiel d installe d pressur

e transmitter) ; • Proces s controlle rfo rsingl e instrumen t loops o ra n individua l sub-system , suc h a s a temperatur e contro l loo p involvin g a senso rreadin g fro m on e temperatur e transmitte raffectin g th e functio n o f on e temperatur

e contro l valve ; an d
• Alar m fo ra n exceedance o f a designate d setpoint , suc h as a hig h pressur e o rlo wtemperature . Th e proces s contro l compute rwil l continuousl ycontro l an d monito rth e operatio n o f th e incinerator . Whe n out-of-rang e condition s exist , it wil l notif yth e operato ro

f thos e conditions . Th e proces s contro l compute ri s programme d t

o shut-down equipmen t (i.e. , brin g th e syste m int o a safe mode

) whe n designate d parameter s ar e exceeded , whic h i s a protectiv e mechanis m agains

t potentia l equipment damage , operatio n outsid e o f permi t limits , o rcondition s tha t might lea d to a releas e t o th e environment . Continuou s monitorin g ofth e incinerato ran d scrubbe rsyste m i s a n important aspec t o f th e syste m design . A digita l readou t o

f al l monitorin g instrumentatio n i s displaye d o n th e mai n contro l screen . A n audibl e an d visua l alarm alerts th e incinerato roperato rt o significan t deviation s fro m norma l operatin g conditions . Thi s syste m allows a n immediate respons e to advers e condition s b yth e operator . Automati cwaste fee d cut-of f an d incineratio n shutdown mechanism s ar e als o interlocke d wit h th e monitorin g syste m a t o rprio rt o reachin g permi t limi t levels . Monitorin g method s an d calibratio n frequencie s ar e liste d i n Tabl e 2-3 . Th e Incinerato rhas a n independen t proces s contro l compute rtha t interfaces t

o th e Quantu m Progammabl e controllers . Th e proces s compute ri s capabl e o f controllin g th e incinerato ri n cas e o f a failur e i n a HM I server . Thi s compute rrun s a RSVIE WHM I contro l softwar e tha t provide s operato rinterfac e t o al l instrumentatio n an d controls . 

## 2. 8 Automati cWast e Fee d Cut-of f Syste m [4 0 CF R §63.1207(f)(1)(iii)(F) ] Th e incinerato rhas a n Automati cWast e Fee d Cut-Of f (AWFCO ) Syste m tha

t wil l shu t waste feed s of

f in th e even t certai n operatin g parameter s deviate fro m allowabl e set points . Th e PL C continuousl ymonitor s operatin g parameters , makin g adjustments t o th e proces s a s neede d fo rprope rcontrol . Alar m logi ci s incorporate d int

o th e PL C syste m t

o automaticall yinitiate a n AWFCO
. Tabl e 2- 3 summarize s th e curren t AWFC O se t points . AWFC O limit s hav e bee n establishe d base d o n severa l factor s tha t ar e summarize d below .
• Regulatory/permi t limit s - establishe d t

o complywit h existin g permits . A n exampl e o f thi s typ e o

f limi t i s th e lo wtemperatur

e limit , belo

wwhic h waste ca n no

t b e fed unti l th e prope rlimi t i s re-established . I n addition , th e HWC MAC Tregulation s requir e tha t th e AWFC O syste m be interlocke d wit h the spa n o f eac h proces s instrumen t tha t i s par t ofth e Continuou s Monitorin g Syste m (CMS)
. Alistin g o f thes e
2-1 3 Februar y 201 0


## VES01829 6

### CM S instrument s an d thei rinterlocke d spa n setpoint s i s maintained a s par

t o f Veolia' s Operatin g Record . • Proces s safet

ylimit s - establishe d t

o assur e process equipmen t i s protected an d unsaf e operatin g condition s d o ho

t occur . A n exampl e o

f thi s i s inadequate exces s ai ri n th e combustio n chambe rtha t ca n lead t o fue l ric h conditions . • Utilit yo rPowe rfailur

e - establishe d t

o facilitate a controlle d shutdown o f th e proces s durin g loss o f proces s air , steam , wate ro relectricity . A n exampl e o f thi s i s th e los s o

f instrument ai rtha

t i s necessar yfo rcertai n types proces s instrument s t o functio n properly . Waste s wil l no t be re-introduced int o th e incinerator

s unti l prope roperatio n o

f ke yinstrument

s i s re-established . I n additio n t

o th e AWFC O system , operator s ca n manuallyshutdown waste feed s o rth e entir e proces s shoul d thi s b e needed . 

## 2.8.1 AWFC O System Testin g Veoli a tests th e AWFC O system s bi-weekly , a s weeklytestin g woul d undulyinterfer e with operation s b

y ceasin g an d restartin g waste feeds , potentiall yincreasin g emissions , incurrin g excessive downtime , burnin g additiona l natura l gas durin g th e downtime , an d increasin g operatin g costs . Testin g ofth e AWFC O syste m i s a time-consumin g an d manpowe rintensive process . Th e curren t testin g progra m ha s bee n i n place unde rth e RCRApermit fo rove r2 0 year s an d ha s prove n t

o be adequate i n detectin g problems . Thi s rational e i s include d i n th e facility' s AWFC O Plan . I n som e case s thi s testin g occur s mor e frequentlydependin g on ho w ofte n actua l AWFCO s occu ra t th e unit . Pe rth e required frequency, incinerato rpersonne l chec k th e functionalit

yo f AWFC O logi ctha

t i s par t o f th e incinerator' s PL C syste m t o mak e sur e tha t shoul d proces s condition s deviat e fro m allowabl e limits , th e compute rlogi cwil l initiate wast e fee d shutdown s a s required . Thi s i s accomplishe d b

ymanuallysimulatin g proces s condition s tha t ar e outsid e allowabl e limit

s an d observin g an d documentin g whe n th e contro l o rbloc k valve softwar

e logi co n th e waste fee d lin e begin s t o initiat e valve closure . Shoul d actua l AWFCO s occu rdurin g a give n testin g period , thes e ar e documented b

yoperatin g personne l to satisf

yregulator

yrequirement

s fo rsyste m testing . Results o t thi s testin g ar

e documente d o n a separate AWFC O Testin g Log an d maintaine d a s par t o f th e unit' s Operatin g Record . 

## 2. 9 Ai r Pollutio n Contro l Equipmen t Maintenanc e Practice s [4

0 CF R §63.1207{f)(1)(iii)(G) J 2.9. 1 Program Overvie w Onc e equipmen t i s installe d an d operational , Veoli a utilize s a n extensiv e preventativ

e maintenanc

e (PM ) progra m t o kee p equipmen t operationa l an d preven t breakdown s an d failures . Base d upo n th e typ e o f equipmen t an d historica l operation s an d maintenanc e experience , schedule s fo rvariou s inspectio n an d P M activitie s are followed . Thi s include s aspect s suc h as documentin g detaile d maintenanc e historie s o n equipment , routin e inspectio n an d lubricatio n program s fo rhig h wea requipmen t an d non-destructiv e testin g o

f pipin g an d vessel s usin g technique s like ultrasoun d t o asses s integrity . Th e frequenc yo f thes e activitie s varie s dependin g upo n th e equipment , P M activit yan d th e incinerator' s shutdown schedule . Fo rexample , frequen t (i.e. , weekly ) instrumen t an d certai n mechanica l equipment check s ar e mad e fo rcritica l proces s items . Lubrication , vibratio n analysi s an d othe rmechanica l integrit ycheck s ar e don e a t longe r frequencie s lik

e monthlyo rquarterly . Finally , suc h item s a s inspectin g refractor ybrick fo rwear , are typicall y performe d whe n th e entir

e incinerato ri s shu t down fo rmaintenance . 2-1 4 Februar y 201 0

# AECOM 2.9. 2 Tes t Progra m Preparatio n Activitie s Prio rt o testing , instrumentatio n associate d wit h ke yparameter s o f th e tes t wer e checked , calibrated , c r replaced , a s appropriate , to ensur e prope roperatio n o f th e instrumehtatio n durin g testin g (i.e. , wast e fee d flowmeter s an d scales , CEMS , pressur e transmitters , thermocouples , stac k flowmeters , etc.) .

2-1 5 Februar y 201 0 

## VES01829 8

# AECOM Tabl e 2- 2 Technica l Informatio n Summar y o n Incinerato r No . 3 Manufacture r Trad e Wast e Incineratio n Mode l No . TWI-2000 , Serie s 2 Typ e Fixe d Hearth , Dua l Chambe r Dat e o f Manufactur e 198 7 Dimension s Primar yChambe r Secondar yChambe r Externa l Lengt h 17.5 ' 17.5 ' Externa l Diamete r 9 ' 9 ' Interna l Diamete r 7'2 " 7'2 " Cross-sectiona l are a 40. 3 squar e fee t 40. 3 squar e fee t Burner s Primar yChambe rBurne r Secondar yChambe rBurne r Manufacture r Nort h America n Nort h America n Siz e 12. 0 Millio n Btu/h r 6. 0 Millio n Btu/h r Fue l Natura l Ga s Natura l Ga s Prime rMove r Induce d Draf t Fa n 15,00 0 acf m @ 400° F saturated , 2 2 in . wate rcolum n

2-1 6 Februar y 201 0


## VES01829 9