# Quarterly Groundwater Monitoring Report – Outside (Non-Tunnel) Wells Red Hill Fuel Storage Facility Pearl Harbor, Oahu, Hawaii Latitude: 21 o 

# 22’15” N Longitude: 157 o 

# 53’33” W
HDOH Facility ID No. 9-102271 HDOH Release ID No. 99051, 010011, 020028
May 2010

Prepared by:

TEC Inc. 1003 Bishop St. Suite 1550 Pauahi Tower Honolulu, Hawaii 96813

Prepared for:

Commander Navy Region Hawaii Environmental Department, Code N45 850 Ticonderoga Street, Suite 110 Pearl Harbor, Hawaii 96860-5101

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility May 2010

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# Table of Contents

Table of Contents

............................................................................................................................. i Executive Summary ......................................................................................................................... 1 1.0 Introduction .......................................................................................................................... 2 1.1 Project Objective ............................................................................................................. . 2 1.2 Previous Reports .............................................................................................................. 2 1.3 Background .................................................................................................................... .. 3 1.3.1 Site Description ......................................................................................................... 3 1.3.2 Facility Information .................................................................................................. 3 1.3.3 UST Information ....................................................................................................... 5 1.4 Regulatory Updates .......................................................................................................... 5 2.0 Sample Collection and Analyses .......................................................................................... 5 2.1 Monitoring Well Purging ................................................................................................. 6 2.2 Groundwater Sample Collection ...................................................................................... 6 2.3 Groundwater Sample Analyses ........................................................................................ 6 3.0 Groundwater Sample Analytical Results ............................................................................ 6 3.1 April 2010 Sample Analytical Results ............................................................................. 6 4.0 Summary and Conclusions ............................................................................................... 8 5.0 References .......................................................................................................................... 10

List of Tables Table 1 Monitoring Well Information ........................................................................................5 Table 2 Analytical Results for Quarte rly Groundwater Sampling (April 26, 2010) ...................7 List of Figures Figure 1 Groundwater Monitoring Well Locations ......................................................................9 List of Appendices Appendix A – Laboratory Analytical Reports Appendix B – Monitoring Well Construction Logs

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility May 2010

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## 1 

# Executive Summary There are 18 active and 2 inactive, 12.5 million gallon, field-constructed underground storage tanks (USTs) located at the Red Hill Fuel Storage F acility (the Facility). Previous environmental site investigations i ndicated a release had o ccurred and contaminated the groundwater underlying the Facility. The United States (US) Navy implemented a gr oundwater monitoring program, which includes collecting groundwater samples quarterly from US Navy Well 2254-01 (RHMW2254-01) and four wells installed in the Facility lower access tunnel (RHMW01, RHMW02, RHMW03, and RHMW05). The US Navy Well 2254-01 is located approximately 3,000 feet downgradient from the Facility and provides approx imately 24 percent of the potable water to the Pearl Harbor Water System (PHWS). The groundwater samples are analyzed for petroleum constituents and compared against State of Hawaii Depart ment of Health (HDOH) Drinking Water Environmental Action Levels (EALs) (HDOH, 2008). In response to increasing concentr ations of contaminants of poten tial concern in the groundwater monitoring wells within the faci lity (specifically RHMW02) dur ing 2008, plans were made to conduct quarterly sampling at the followi ng outside monitoring well locations:

 RHMW04;

 Oily Waste Disposal Facility monitoring well 01 (OWDFMW01); and

 Halawa Deep Well 2253-03 (referred to as HDMW2253-03 in this report). This groundwater monitoring report presents the an alytical results for samples collected on April 26, 2010, at the three groundwater monitoring wells outside of the Facility. Laboratory analytical results indicate that Total Petroleu m Hydrocarbons (TPH) as Diesel Range Organics (TPH-DRO) is present in groundwater from OWDFMW01. TPH-DRO in OWDFMW01 was detected at 288F micrograms per liter (μg/L) [F indicates that the compound was identified, but the concentration was above the laboratory method detection limit (MDL) and below the reporting limit (RL), therefore is considered an estimate]. The HDOH Drinking Water EAL for TPH-DRO is 100 μg/L. Although the TPH-DRO concentration at OWDFMW01 remains above the HDOH Drinking Water EAL, April 2010 results show a significant de crease in concentration for TPH-DRO at this location. The previous sampling event in January 2010 at OWDFMW01 had a TPH-DRO concentration of 1,490 μg/L. No other compounds were detected above the MDL at any other sampling location during April 2010.

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## 2 

# 1.0 Introduction This report presents the results of the fourth groundwater sampling event, conducted in April 2010 at two groundwater monitoring wells (i .e., RHMW04 and OWDFMW01). The first, second, and third sampling events for OWDF MW01 and RHMW04 were conducted in August 2009, October 2009, and January 2010, respectively. In addition, this report presents data from the third sampling event conducted in Apr il 2010 at HDMW2253-03. The first and second sampling events at HDMW2253-03 were conducted in October 2009, and January 2010, respectively. An August 2009 sampling even t for HDMW2253-03 was not conducted due to access issues.

These three wells surround the Red Hill Fuel Stor age Facility, Oahu, Hawaii (hereafter referred to as “the Facility”). This outside groundwater sampling and analysis is considered supplemental to the quarterly groundwater monitoring progr am conducted within the Facility. This supplemental sampling was conducted in response to increasing concentrati ons of contaminants of potential concern in a groundwater monitoring well within the Facil ity, specifically RHMW02 during 2008. 

# 1.1 Project Objective This groundwater sampling project was performed to evaluate the presence of chemicals of potential concern in gr oundwater surrounding the Facility. The projec t was conducted to ensure the Navy remains in compliance with Hawaii De partment of Health (HDOH) UST release response requirements. The groundwater sampli ng program followed the procedures described in Red Hill Bulk Fuel Storage Fa cility Groundwater Protection Plan [TEC Inc. (TEC), 2008 updated in 2009], also refe rred to as “the Plan”. This groundwater sampling event was condu cted by TEC under United States (US) Navy Contract Number N47408-04-D-8514, Task Orde r No. 54, Amendment/Modification No. 01. 

# 1.2 Previous Reports As indicated earlier, this outside well sa mpling supplements the quarterly groundwater monitoring of wells within the Facility, which began in 2005. The following groundwater monitoring reports were previously submitted to the HDOH, for groundwater monitoring wells within the Facility:

1. Groundwater Sampling Report, First Quarter 2005 (submitted April 2005); 2. Groundwater Sampling Report, Second Quarter 2005 (submitted August 2005); 3. Groundwater Sampling Report, Third Quarter 2005 (submitted November 2005); 4. Groundwater Sampling Report, Fourth Quarter 2005 (submitted February 2006); 5. Groundwater Monitoring Results, July 2006 (submitted September 2006); 6. Groundwater Monitoring Results, December 2006 (submitted January 2007); 7. Groundwater Monitoring Results, March 2007 (submitted May 2007);

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility May 2010

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## 3 8. Groundwater Monitoring Results, June 2007 (submitted August 2007); 9. Groundwater Monitoring Results, September 2007 (submitted October 2007); 10. Groundwater Monitoring Results, January 2008 (submitted March 2008); 11. Groundwater Monitoring Results, April 2008 (submitted May 2008); 12. Groundwater Monitoring Results, July 2008 (submitted October 2008); 13. Groundwater Monitoring Results, October and December 2008 (submitted February 2009); 14. Groundwater Monitoring Results, February 2009 (submitted May 2009); 15. Groundwater Monitoring Results, May 2009 (submitted July 2009); 16. Groundwater Monitoring Results, July 2009 (submitted September 2009); 17. Groundwater Monitoring Results, Oct ober 2009 (submitted December 2009); and 18. Groundwater Monitoring Results, January, February, and March 2010 (submitted April 2010).
The following groundwater monitoring reports we re previously submitted to the HDOH for groundwater monitoring wells outside the Facility:

1. Groundwater Monitoring Results, August 2009 (submitted September 2009); 2. Groundwater Monitoring Results, Oct ober 2009 (submitted December 2009); and 3. Groundwater Monitoring Results, January 2010 (submitted April 2010). 

# 1.3 Background The following sections provide a description of th e site and information on the Facility and USTs.
1.3.1 Site Description The Facility is located in Red Hill, Oahu, Hawaii. Land adjacent to the north of the Facility is occupied by the Halawa Correctional Facility and private businesses. Land to the south and west of the Facility includes the Coas t Guard Reservation. Moanalua Valley is located east of the Facility (Dawson, 2006). The Navy Public Works Department operates a pot able water infiltratio n tunnel approximately 1,550 feet from the Facility (Dawson, 2006) . The US Navy Well 2254-01 is located approximately 3,000 feet west of the Facility and provides approximatel y 24% of the potable water to the Pearl Harbor Water System, whic h serves approximately 52,200 military consumers (TEC, 2008).
1.3.2 Facility Information The Facility consists of 18 ac tive and two inactive USTs operat ed by Navy Fleet and Industrial Supply Center (FISC) Pearl Harbor. Each UST has a capacity of 12.5 million gallons. The Facility is located approximately 100 feet above the basal aquifer (Dawson, 2006).

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## 4 In 2002, the US Navy installed a groundwater monitoring well (cur rently named RHMW01) into the basal aquifer, directly down-gradient from the Facility, within th e lower access tunnel. Groundwater samples from this well indicated that petroleum from the Facility has migrated to the basal aquifer (AMEC, 2002). In 2005, the US Navy began quarterly monitoring of the aquifer to protect their down-grad ient drinking water resource a ssociated with the US Navy Well 2254-01. By September 2005, the US Navy had installe d two more groundwater monitoring wells (RHMW02 and RHMW03) within the Facility UST system, a groundwater monitoring well (RHMW04) north of the Facility adjacent to the US Navy Firing Range, and a groundwater monitoring well within the US Navy Well 2254-01 infiltration ga llery (RHMW2254-01). Since 2005, RHMW01, RHMW02, RHMW03, and RHMW2254-01 ha ve been sampled quarterly for TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved lead. Due to increasing concentrations of contamin ants of potential con cern at the groundwater monitoring wells within the Fa cility (specifically RHMW02) during 2008, response measures were warranted. In April 2009, another groundwa ter monitoring well (RHMW05) was installed within the lower access tunne l between RHMW01 and RHMW2254- 01. It was installed to identify the extent of contaminant migration be fore it reaches the infiltration gallery at RHMW2254-01. Additionally, plans were made to sample three monitoring wells surrounding and outside of the Facility, RHMW04, OWDFMW01, and HDMW2253- 03. RHMW04 was installed to provide contaminant chemistry data for water moving through the basal aquifer beneath the Facility. OWDFMW01 (originally known as MW08) was inst alled into the basal aquifer in 1998 for a Phase II Remedial Investigation/ Feasibility St udy for the Red Hill Oily Waste Disposal Facility (Earth Tech Inc., 2000). It is located geographi cally down-gradient of the USTs and US Navy Well 2254-01. HDMW2253-03 is controlled by the State of Hawaii Commission on Water Resource Management. It is located between the Facility and the mu nicipal drinking water supply well run by the City and County of H onolulu Board of Water Supply (Halawa Shaft pumping station 2354-01). Table 1 summarizes basic gr oundwater monitoring well information, Figure 1 shows groundwater monitoring well locat ions, Appendix A provides the laboratory data, and Appendix B includes the well construction logs for RHMW04 and OWDFMW01.

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## 5 Table 1. Monitoring Well Information

Groundwater Well TOC Elevation (ft msl) DTW (ft) TD (ft)

RHMW04 313.03 293 320 OWDFMW01 138.94 120 142.8 HDMW2253-03 225 210 1,575 Notes: DTW - Distance to water TD - Total depth of well TOC - Top of casing ft – Feet ft msl - Feet from mean sea level



## 1.3.3 UST Information The USTs were constructed in th e early 1940s. The tanks were c onstructed of steel and currently contain Jet Propulsion (JP)–5 fuel, JP-8, and F-76 (diesel marine fuel). Previously, several tanks stored Navy Special Fuel Oil, Navy Distillate, av iation gasoline, and motor gasoline. Each tank measures approximately 245 feet in height and 100 feet in diameter. The upper domes of the tanks lie at depths varying between approxima tely 100 feet and 200 feet below the existing ground surface (TEC, 2006). 

# 1.4 Regulatory Updates During the summer and fall of 2008, HDOH updated their EALs, which resulted in significant changes to the action levels associated with me thylnaphthalenes. The drinking water toxicity EAL for these compounds was 240  g/L. This concentration pres umed that methylnaphthalenes were non-carcinogenic. Evidence th at they are human carcinogens has now been accepted by the US Environmental Protection Agency (USEPA). As a result, HDOH adopted more rigorous EALs of 4.7  g/L for 1-methylnaphthalene and 24  g/L for 2-methylnaphthalene, corresponding to a residential tap water scenario, and a 1 in a million cancer risk (HDOH, 2008).
Also, the drinking water EAL for na phthalene was increased from 6.2  g/L to 17  g/L (HDOH, 2008). Finally, the HDOH Drinking Water EA L for TPH-DRO was increased from 100  g/L to 210  g/L, although the HDOH Groundw ater Gross Contamination EAL for TPH-DRO remains 100  g/L. 

# 2.0 Sample Collection and Analyses Field activities relating to groundw ater sample collection were conducted on Ap ril 26, 2010. Groundwater samples were collected from three monitoring wells, RHMW04, OWDFMW01, and HDMW2253-03. Sampling and analysis were conducted according to Red Hill Bulk Fuel Storage Facility Groundwater Protection Plan (TEC, 2008). A total of six samples were collected as follows:

 one environmental sample from RHMW04, OWDFMW01, and HDMW2253-03;

 one duplicate sample from RHMW04 (sampled as RHMWA01 and reported as RHMW04D); and

 one matrix spike and matrix sp ike duplicate from OWDFMW01.

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# 2.1 Monitoring Well Purging RHMW04 and OWDFMW01 were purged prior to sampling. Well purging was considered complete when no less than three successive water quality parameter measurements had stabilized within approximately 10 percent. Fiel d parameters were measured at regular intervals during well purging and included pH, temperature, specific conductivity, dissolved oxygen, and turbidity. Due to the well c onstruction characteristics of HDMW2253-03, the well was not purged prior to sampling, but field parameters were recorded. Rather than purging, a grab sample was collected at a depth below the solid casing (which extends about 50 feet below the water table) and within the open-holed portion of the well. 

# 2.2 Groundwater Sample Collection Immediately following purging, RHMW04 was sample d directly from a dedicated bladder pump system, and OWDFMW01 was sampled using a disposable bailer. HDMW2253-03 was sampled using a disposable bailer designed to collect samples at desired depths. Samples were placed into sampling containers with a ppropriate preservatives [i.e., hydroc hloric acid (HCl) for volatile organic analysis, nitric acid (HNO 3 

## ) for dissolved lead]. Dissolved lead samples were filtered in the field and placed in preserved bottles. Sample containers were labeled with the date, sample identification number, type of analysis, and sampler’s name. The containers were placed on ice in sample coolers and transporte d under chain-of-custody procedur es to the certified laboratory for analysis. 

# 2.3 Groundwater Sample Analyses Groundwater samples were analyzed by SGS Environm ental Service, Inc. in Anchorage, Alaska for TPH-DRO and TPH-GRO by EPA Method 8015B, VOCs by EPA Method 8260B, PAHs by EPA Method 8270C SIM, and dissolved lead by EPA Method 6020. 

# 3.0 Groundwater Sample Analytical Results This section provides a summary of analytical results for groundwater samples collected from three monitoring wells, RHMW04, OWDFMW 01, and HDMW2253-03. Duplicate sample results from monitoring well RHMW04 are re ported in this document as RHMW04D. A summary of groundwater analytical results for TPH-DRO and TPH-GR O, VOCs, PAHs, and dissolved lead is included in Table 2. Complete analytical laboratory reports are provided in Appendix A. 

# 3.1 April 2010 Sample Analytical Results All groundwater samples were analyzed for TP H-DRO, TPH-GRO, VOCs, PAHs, and dissolved lead. The results for each groundwater monitoring well are discussed below.

RHMW04 No potential chemical of concern was detected above the laboratory method detection limit (MDL) in RHMW04 (Table 2).Table 2. Analytical Results for Quarterly Groundwater MonitoringRelease Response Report (April 26, 2010)Red Hill Fuel Storage Facility, Pearl Harbor, HawaiiResult Q MDL RL Result Q MDL RL Result Q MDL RL Result Q MDL RLTPH as DIESELRANGE ORGANICS210100ND U 176 471288F 176 471 ND U 174 465 ND U 176 471TPH as GASOLINE RANGE ORGANICS100100ND U 30 100 ND U 30 100 ND U 30 100 ND U 30 1001-METHYLNAPHTHALENE4.710ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 0.0176 0.05882-METHYLNAPHTHALENE2410ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 0.0176 0.0588ACENAPHTHENE37020ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 0.0176 0.0588ACENAPHTHYLENE2402000ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 0.0176 0.0588ANTHRACENE180022ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 0.0176 0.0588BENZO(a)ANTHRACENE0.0924.7ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 0.0176 0.0588BENZO(a)PYRENE0.20.81ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 0.0176 0.0588BENZO(b)FLUORANTHENE0.0920.75ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 0.0176 0.0588BENZO(g,h,i)PERYLENE15000.13ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 0.0176 0.0588BENZO(k)FLUORANTHENE0.920.4ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 0.0176 0.0588CHRYSENE9.21ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 0.0176 0.0588DIBENZ(a,h)ANTHRACENE0.00920.52ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 0.0176 0.0588FLUORANTHENE1500130ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 0.0176 0.0588FLUORENE240950ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 0.0176 0.0588INDENO(1,2,3-c,d)PYRENE0.0920.095ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 0.0176 0.0588NAPHTHALENE1721ND U 0.036 0.116 ND U 0.0365 0.118 ND U 0.0365 0.118 ND U 0.0365 0.118PHENANTHRENE240410ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 0.0176 0.0588PYRENE18068ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 0.0176 0.05881,1,1,2-TETRACHLOROETHANE0.5250000ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.51,1,1-TRICHLOROETHANE200970ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,1,2,2-TETRACHLOROETHANE0.067500ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.51,1,2-TRICHLOROETHANE550000ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,1-DICHLOROETHANE2.450000ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,2,3-TRICHLOROPROPANE (TCP)0.650000ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,2,4-TRICHLOROBENZENE703000ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,2-DIBROMO-3-CHLOROPROPANE (DBCP)0.0410ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 21,2-DIBROMOETHANE (EDB)0.006550000ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,2-DICHLOROBENZENE60010ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,2-DICHLOROETHANE0.157000ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.51,2-DICHLOROPROPANE510ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,3-DICHLOROBENZENE18050000ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,4-DICHLOROBENZENE755ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5ACETONE2200020000ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10BENZENE5170ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4April 26, 2010April 26, 2010April 26, 2010UG/LRHMW04UG/LUG/LMethodHDOH Drinking WaterEALs1for Human ToxicityUG/LHDOH GroundwaterGross ContaminationEALs2UG/LChemicalHDMW2253-03UG/LRHMW04D8015B (Petroleum)8270C SIM(PAHs)April 26, 2010OWDFMW01BROMODICHLOROMETHANE0.22 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5BROMOFORM100 510 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1BROMOMETHANE8.7 50000 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3CARBON TETRACHLORIDE5 520 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1CHLOROBENZENE100 50 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5CHLOROETHANE8600 16 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1CHLOROFORM70 2400 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1CHLOROMETHANE1.8 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1cis-1,2-DICHLOROETHYLENE70 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1cis-1,3-DICHLOROPROPENE0.43 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5DIBROMOCHLOROMETHANE0.16 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5ETHYLBENZENE700 30 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1HEXACHLOROBUTADIENE0.86 6 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1M,P-XYLENE (SUM OF ISOMERS)10000 20 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2METHYL ETHYL KETONE (2-BUTANONE)7100 8400 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10METHYL ISOBUTYL KETONE (4-METHYL-2-PENTANONE)2000 1300 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10METHYLENE CHLORIDE4.8 9100 ND U 1 5 ND U 1 5 ND U 1 5 ND U 1 5NAPHTHALENE17 21 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2STYRENE100 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1TETRACHLOROETHYLENE(PCE)5 170 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1TOLUENE1000 40 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1trans-1,2-DICHLOROETHENE100 260 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1TRICHLOROETHYLENE (TCE)5 310 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1VINYL CHLORIDE23400NDU0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1XYLENES, TOTAL1000020ND U 0.94 3 ND U 0.94 3 ND U 0.94 3 ND U 0.94 36020LEAD1550000ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1PAHs - Polynuclear aromatic hydrocarbonsMDL - Method detection limitVOCs - Volatile organic compoundsRL - Reporting limitUG/L - Micrograms per LiterTPH - Total petroleum hydrocarbonsQ - Data qualifierND - Indicates that the compound was not detected above the stated method detection limitU - Indicates that the compound was analyzed for but not detected at or above the stated limitF - Indicates that the compound was identified but the concentration was above the MDL and below the RL-Result exceeds one or both HDOH EALs128260B(VOCs)Final Drinking Water Action Levels for Human Toxicity, Table D-3a,Screening for Environmental Concerns at Sites withContaminated Soil and Groundwater, HDOH, 2009Groundwater Gross Contamination Action Levels, Table G-1,Screening for Environmental Concerns at Sites withContaminated Soil and Groundwater, HDOH, 2009200Page 7

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## 8 OWDFMW01 TPH-DRO was detected at 288F μg/L [F indicates that the compound was identified at a concentration above the MDL, but below the reporting limit (RL), therefore is considered an estimate], exceeding the HDOH Groundwater Gro ss Contamination EAL and Drinking Water EAL (i.e., 100 μg/L and 210 μg/L, respectively). No other potential chemical of concern was detected above the laboratory MDLs in OWDFMW01 (Table 2).

HDMW2253-03 No potential chemical of concern was detect ed above the laborator y MDLs in HDMW2253-03 (Table 2). 

# 4.0 Summary and Conclusions Summary At OWDFMW01, TPH-DRO was detected at 288F μg/L. This TPH-DRO concentration is above the HDOH Drinking Water EAL, and the HDOH Gross Contamination EAL. However, the April 2010 results show a significant decrease in concentration for TPH-DRO at this location. The previous sampling event conducted in January 2010 at OWDFMW01 had a TPH-DRO concentration of 1,490 μg/L. No other potential chemicals of concern we re detected above the laboratory MDLs in OWDFMW01, HDMW2253-03, or RHMW04 during the April 2010 sampling event.

Conclusions/Recommendations No compounds were detected above the MDLs during the August 2009 sampling event at OWDFMW01 and RHMW04 (HDMW2253-03 was not sampled in August 2009 due to access issues); or during the October 2009 sa mpling event at OWDFMW01, RHMW04, or HDMW2253-03. Despite the detection of TPH-DRO at HDMW2 253-03 during January 2010, TPH-DRO was not detected above the laboratory MDL during the April 2010 sampling event. Since two or more consecutive sampling events of increasing (or decreasing) concentrat ions of TPH-DRO at HDMW2253-03 have not occurred, no trend for TPH-DRO has been es tablished at this location.

TPH-DRO detected at OWDFMW 01 during January 2010 significantly decreased in April 2010 (i.e., from 1,490 μg/L in January 2010 to 288F μg/L in April 2010).
TPH-DRO (detected at both HDMW2253-03 and OWDFMW01 in January 2010 and only at OWDFMW01 in April 2010) has been the only parameter detected above HDOH Drinking Water EALs during all four outside well samp ling rounds. For the th ree wells surrounding the Facility (i.e., RHMW04, OWDFMW01, and HDM W2253-03), only one more sampling event remains tasked under this contract (i.e., to conduct the fourth and final round of sampling at HDMW2253-03 since it was not sampled in August 2009). Consequently, consideration should be given to conducting follow-on, pe riodic (perhaps semi-annually), targeted monitoring of these outside wells for TPH-DRO.

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## 10 

# 5.0 References AMEC. Red Hill Bulk Fuel Storage Facility Investigation Report , Prepared for NAVFAC Pacific, August 2002. Dawson Group, Inc. Fourth Quarter 2005 Groundwater Sam pling Report, Red Hill Fuel Storage Facility, Hawaii. February 2006.
Earth Tech, Inc. Remedial Investigation Phase II, Volume I, Technical Report, Red Hill Oily Waste Disposal Facility, Halawa, Oahu, Hawaii . September 2000.
Hawaii Administrative Rules, Titl e 11, Chapter 281, Subchapter 7.

HDOH. Screening for Environmental Concerns at Sites with Contaminated Soil and Groundwater, Summary Lookup Tables. March 2009.

HDOH. Use of May 2005 Environmental Action Levels (“EALs”) at Leaking Underground Storage Tank Sites . Memo. July 2005.

HDOH. Evaluation of Environmental Hazards at Sites with Contaminated Soil and Groundwater . Summer 2008 (updated October 2008).
TEC, Inc. Red Hill Bulk Fuel Storage Facility, Fi nal – Addendum Planning Documents, Pearl Harbor, Hawaii. May 2006.
TEC, Inc. Red Hill Bulk Fuel Storage Facility, Final Groundwater Protection Plan, Pearl Harbor, Hawaii. January 2008 revised in December 2009.

# Appendix A Laboratory Analytical Reports

## SGS Work Order:

Contents:
Cover Page Case Narrative Final Report Pages Quality Control Summary Forms Chain of Custody/Sample Receipt Forms 

## Project: Client: 

# SGS North America Inc. Alaska Division Level II Laboratory Data Report

Released by:

Note: Unless otherwise noted, all quality assurance/quality control criteria is in compliance with the standards set forth by the proper regulatory authority, the SGS Quality Assurance Program Plan, and the National Environmental Accreditation Conference. 

## 3354-010 Red Hill BFSF The Environmental Company, Inc. (TEC) 1101763

# Case Narrative THEENVC The Environmental Company, Inc. (TEC) 1101763 3354-010 Red Hill BFSF Customer: Project: 

# SGS North America Inc.

Refer to the sample receipt form for information on sample condition. 

### 1101763002 BMS OWDFMW01-WG-04 MS 8260B - MS recovery for chloroethane does not meet QC criteria (biased high). This analyte was not detected above LOQ in the associated samples. 

### 1101763003 BMSD OWDFMW01-WG-04 MSD 8260B - MSD recovery for chloroethane does not meet QC criteria (biased high). This analyte was not detected above LOQ in the associated samples. 

### 958813 CCV V MS/11191 ] 8260B - CCV recovery for bromomethane, acetone, and carbon tetrachloride does not meet QC criteria (biased high). These analytes were not detected above LOQ in the associated samples.

### 3354-010 Red Hill BFSF

Project Manager jennifer.serna@sgs.com Jennifer Serna T: (808)528-1445 F:(808)528-0768 Attn: Rick Adkisson 1003 Bishop Street, Pauahi Tower Suite 1550 Honolulu, HI 96813

Certification:
This data package is in compliance with the terms and conditions of the contract, both technically and for completeness, unless otherwise noted on the sample data sheet(s) and/or case narrative. This certification applies only to the tested parameters and the specific sample(s) received at the laboratory. If you have any questions regarding this report, or if we can be of further assistance, please contact your SGS Project Manager. 

### 1101763 The Environmental Company, Inc. (TEC)

Workorder No.:

Client:

Project: 

# Laboratory Analytical Report

Contents (Bookmarked in PDF):
Cover Page Glossary Sample Summary Forms Case Narrative Sample Results Forms Batch Summary Forms (by method) Quality Control Summary Forms (by method) Chain of Custody/Sample Receipt Forms Attachments (if applicable)

SGS No rth Americ a Inc . En vir onmenta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com Member of SG S Group

### Enclosed are the analytical results associated with the above work order. All results are intended to be used in their entirety and SGS is not responsible for use of less than the complete report. If you have any questions regarding this report, or if we can be of any other assistance, please contact your SGS Project Manager at 907-562-2343. All work is provided under SGS general terms and conditions (<http://www.sgs.com/terms_and_conditions.htm>), unless other written agreements have been accepted by both parties.
SGS maintains a formal Quality Assurance/Quality Control (QA/QC) program. A copy of our Quality Assurance Plan (QAP), which outlines this program, is available at your request. The laboratory certification numbers are AK00971 (DW Chemistry & Microbiology) & UST-005 (CS) for ADEC and AK100001 for NELAP (RCRA methods: 1020A, 1311, 3010A, 3050B, 3520C, 3550C, 5030B, 5035B, 6010B, 6020, 7470A, 7471B, 8021B, 8081B, 8082A, 8260B, 8270D, 8270D-SIM, 9040B, 9045C, 9056A, 9060A, AK101 and AK102/103). Except as specifically noted, all statements and data in this report are in conformance to the provisions set forth by the SGS QAP and, when applicable, the National Environmental Laboratory Accreditation Program and other regulatory authorities. The following descriptors or qualifiers may be found in your report:

* The analyte has exceeded allowable regulatory or control limits. ! Surrogate out of control limits. B Indicates the analyte is found in a blank associated with the sample. CCV Continuing Calibration Verification CL Control Limit D The analyte concentration is the result of a dilution. DF Dilution Factor DL Detection Limit (i.e., maximum method detection limit) E The analyte result is above the calibrated range. F Indicates value that is greater than or equal to the DL GT Greater Than ICV Initial Calibration Verification J The quantitation is an estimation. JL The analyte was positively identified, but the quantitation is a low estimation. LCS(D) Laboratory Control Spike (Duplicate) LOD Limit of Detection (i.e., 2xDL) LOQ Limit of Quantitation (i.e., reporting or practical quantitation limit) LT Less Than M A matrix effect was present. MB Method Blank MS(D) Matrix Spike (Duplicate) ND Indicates the analyte is not detected. Q QC parameter out of acceptance range. R Rejected RL Reporting Limit RPD Relative Percent Difference U Indicates the analyte was analyzed for but not detected.
Note: Sample summaries which include a result for "Total Solids" have already been adjusted for moisture content.

All DRO/RRO analyses are integrated per SOP. Print Date: 5/11/2010

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

## SAMPLE SUMMARY Client Name: The Environmental Company, Inc. (TEC) Project Name: 3354-010 Red Hill BFSF Workorder No.: 1101763 

## Analytical Methods

Method Description Analytical Method 8270 PAH SIM Semi-Vol GC/MS Liq/Liq ext. 8270D SIMS AFCEE 3.1 8260 (W) SW8260B Dissolved Metals by ICP-MS SW6020 DRO by 8015C (W) SW8015C GRO (W) SW8015C Print Date: 5/11/2010 12:34 pm



## Sample ID Cross Reference
Client Sample ID Lab Sample ID 1101763001 OWDFMW01-WG-04 1101763002 OWDFMW01-WG-04 MS 1101763003 OWDFMW01-WG-04 MSD 1101763004 RHMW04-WG-04 1101763005 RHMWA01-WG-04 1101763006 HDMW2253-03-WG-04 1101763007 TB01-WG-04

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### OWDFMW01-WG-04 SGS Ref. #: 1101763001 Collection Date/Time: 04/26/10 08:35 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 ug/L MMS6414 MXX22933 0.310 5

Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS6414 Analytical Method: SW6020 Analysis Date/Time: 05/04/10 11:31 Prep Batch: MXX22933 Prep Method: SW3010A Prep Date/Time: 04/29/10 16:05 Container ID:1101763001-K Dilution Factor: 5 Analyst: SCL

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### OWDFMW01-WG-04 SGS Ref. #: 1101763001 Collection Date/Time: 04/26/10 08:35 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 ug/L VFC9914 VXX20617 30.0 1 4-Bromofluorobenzene <surr> 108 50-150 % VFC9914 VXX20617 1

Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9914 Analytical Method: SW8015C Analysis Date/Time: 05/07/10 10:16 Prep Batch: VXX20617 Prep Method: SW5030B Prep Date/Time: 05/07/10 08:48 Container ID:1101763001-A Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### OWDFMW01-WG-04 SGS Ref. #: 1101763001 Collection Date/Time: 04/26/10 08:35 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 0.288J 0.471 mg/L XFC9168 XXX22543 0.176 1 5a Androstane <surr> 88.5 50-150 % XFC9168 XXX22543 1

Batch Information Initial Prep Wt./Vol.: 850 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC9168 Analytical Method: SW8015C Analysis Date/Time: 05/03/10 16:38 Prep Batch: XXX22543 Prep Method: SW3520C Prep Date/Time: 04/29/10 08:15 Container ID:1101763001-I Dilution Factor: 1 Analyst: LCE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### OWDFMW01-WG-04 SGS Ref. #: 1101763001 Collection Date/Time: 04/26/10 08:35 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 1,1,1-Trichloroethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 1,1,2-Trichloroethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,1-Dichloroethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,1-Dichloroethene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,1-Dichloropropene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2,3-Trichloropropane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L VMS11191 VXX20600 0.620 1 1,2-Dibromoethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2-Dichlorobenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2-Dichloroethane 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 1,2-Dichloropropane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,3-Dichlorobenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,3-Dichloropropane 0.240 U 0.400 ug/L VMS11191 VXX20600 0.120 1 1,4-Dichlorobenzene 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 1-Chlorohexane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 2,2-Dichloropropane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 2-Butanone (MEK) 6.20 U 10.0 ug/L VMS11191 VXX20600 3.10 1 2-Chlorotoluene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 4-Chlorotoluene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 4-Isopropyltoluene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L VMS11191 VXX20600 3.10 1 Acetone 6.20 U 10.0 ug/L VMS11191 VXX20600 3.10 1 Benzene 0.240 U 0.400 ug/L VMS11191 VXX20600 0.120 1 Bromobenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Bromochloromethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Bromodichloromethane 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 Bromoform 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Bromomethane 1.88 U 3.00 ug/L VMS11191 VXX20600 0.940 1 Carbon tetrachloride 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Chlorobenzene 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### OWDFMW01-WG-04 SGS Ref. #: 1101763001 Collection Date/Time: 04/26/10 08:35 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Chloroethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Chloroform 0.600 U 1.00 ug/L VMS11191 VXX20600 0.300 1 Chloromethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 cis-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 cis-1,3-Dichloropropene 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 Dibromochloromethane 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 Dibromomethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Dichlorodifluoromethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Ethylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Hexachlorobutadiene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Methylene chloride 2.00 U 5.00 ug/L VMS11191 VXX20600 1.00 1 Methyl-t-butyl ether 3.00 U 5.00 ug/L VMS11191 VXX20600 1.50 1 Naphthalene 1.24 U 2.00 ug/L VMS11191 VXX20600 0.620 1 n-Butylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 n-Propylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 o-Xylene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 P & M -Xylene 1.24 U 2.00 ug/L VMS11191 VXX20600 0.620 1 sec-Butylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Styrene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 tert-Butylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Tetrachloroethene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Toluene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 trans-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 trans-1,3-Dichloropropene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Trichloroethene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Trichlorofluoromethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Vinyl chloride 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Xylenes (total) 1.88 U 3.00 ug/L VMS11191 VXX20600 0.940 1 1,2-Dichloroethane-D4 <surr> 103 73-120 % VMS11191 VXX20600 1 4-Bromofluorobenzene <surr> 107 76-120 % VMS11191 VXX20600 1 Toluene-d8 <surr> 102 80-120 % VMS11191 VXX20600 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### OWDFMW01-WG-04 SGS Ref. #: 1101763001 Collection Date/Time: 04/26/10 08:35 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS11191 Analytical Method: SW8260B Analysis Date/Time: 04/30/10 13:38 Prep Batch: VXX20600 Prep Method: SW5030B Prep Date/Time: 04/30/10 08:55 Container ID:1101763001-D Dilution Factor: 1 Analyst: JPI

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### OWDFMW01-WG-04 SGS Ref. #: 1101763001 Collection Date/Time: 04/26/10 08:35 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

DL DF

1-Methylnaphthalene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 2-Methylnaphthalene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Acenaphthene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Acenaphthylene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Anthracene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Benzo(a)Anthracene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Benzo[a]pyrene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Benzo[b]Fluoranthene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Benzo[g,h,i]perylene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Benzo[k]fluoranthene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Chrysene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Dibenzo[a,h]anthracene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Fluoranthene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Fluorene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Indeno[1,2,3-c,d] pyrene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Naphthalene 0.0730 U 0.118 ug/L XMS5395 XXX22544 0.0365 1 Phenanthrene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Pyrene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Terphenyl-d14 <surr> 81.8 50-126 % XMS5395 XXX22544 1

Batch Information Initial Prep Wt./Vol.: 850 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS5395 Analytical Method: 8270D SIMS Analysis Date/Time: 05/08/10 09:39 Prep Batch: XXX22544 Prep Method: SW3520C Prep Date/Time: 04/29/10 08:00 Container ID:1101763001-G Dilution Factor: 1 Analyst: JDH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### RHMW04-WG-04 SGS Ref. #: 1101763004 Collection Date/Time: 04/26/10 13:10 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 ug/L MMS6414 MXX22933 0.310 5

Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS6414 Analytical Method: SW6020 Analysis Date/Time: 05/04/10 11:53 Prep Batch: MXX22933 Prep Method: SW3010A Prep Date/Time: 04/29/10 16:05 Container ID:1101763004-K Dilution Factor: 5 Analyst: SCL

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### RHMW04-WG-04 SGS Ref. #: 1101763004 Collection Date/Time: 04/26/10 13:10 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 ug/L VFC9914 VXX20617 30.0 1 4-Bromofluorobenzene <surr> 107 50-150 % VFC9914 VXX20617 1

Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9914 Analytical Method: SW8015C Analysis Date/Time: 05/07/10 11:15 Prep Batch: VXX20617 Prep Method: SW5030B Prep Date/Time: 05/07/10 08:48 Container ID:1101763004-A Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### RHMW04-WG-04 SGS Ref. #: 1101763004 Collection Date/Time: 04/26/10 13:10 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 0.348 U 0.465 mg/L XFC9168 XXX22543 0.174 1 5a Androstane <surr> 98 50-150 % XFC9168 XXX22543 1

Batch Information Initial Prep Wt./Vol.: 860 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC9168 Analytical Method: SW8015C Analysis Date/Time: 05/03/10 17:41 Prep Batch: XXX22543 Prep Method: SW3520C Prep Date/Time: 04/29/10 08:15 Container ID:1101763004-I Dilution Factor: 1 Analyst: LCE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### RHMW04-WG-04 SGS Ref. #: 1101763004 Collection Date/Time: 04/26/10 13:10 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 1,1,1-Trichloroethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 1,1,2-Trichloroethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,1-Dichloroethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,1-Dichloroethene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,1-Dichloropropene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2,3-Trichloropropane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L VMS11191 VXX20600 0.620 1 1,2-Dibromoethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2-Dichlorobenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2-Dichloroethane 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 1,2-Dichloropropane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,3-Dichlorobenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,3-Dichloropropane 0.240 U 0.400 ug/L VMS11191 VXX20600 0.120 1 1,4-Dichlorobenzene 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 1-Chlorohexane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 2,2-Dichloropropane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 2-Butanone (MEK) 6.20 U 10.0 ug/L VMS11191 VXX20600 3.10 1 2-Chlorotoluene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 4-Chlorotoluene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 4-Isopropyltoluene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L VMS11191 VXX20600 3.10 1 Acetone 6.20 U 10.0 ug/L VMS11191 VXX20600 3.10 1 Benzene 0.240 U 0.400 ug/L VMS11191 VXX20600 0.120 1 Bromobenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Bromochloromethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Bromodichloromethane 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 Bromoform 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Bromomethane 1.88 U 3.00 ug/L VMS11191 VXX20600 0.940 1 Carbon tetrachloride 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Chlorobenzene 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### RHMW04-WG-04 SGS Ref. #: 1101763004 Collection Date/Time: 04/26/10 13:10 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Chloroethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Chloroform 0.600 U 1.00 ug/L VMS11191 VXX20600 0.300 1 Chloromethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 cis-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 cis-1,3-Dichloropropene 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 Dibromochloromethane 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 Dibromomethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Dichlorodifluoromethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Ethylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Hexachlorobutadiene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Methylene chloride 2.00 U 5.00 ug/L VMS11191 VXX20600 1.00 1 Methyl-t-butyl ether 3.00 U 5.00 ug/L VMS11191 VXX20600 1.50 1 Naphthalene 1.24 U 2.00 ug/L VMS11191 VXX20600 0.620 1 n-Butylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 n-Propylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 o-Xylene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 P & M -Xylene 1.24 U 2.00 ug/L VMS11191 VXX20600 0.620 1 sec-Butylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Styrene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 tert-Butylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Tetrachloroethene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Toluene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 trans-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 trans-1,3-Dichloropropene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Trichloroethene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Trichlorofluoromethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Vinyl chloride 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Xylenes (total) 1.88 U 3.00 ug/L VMS11191 VXX20600 0.940 1 1,2-Dichloroethane-D4 <surr> 98.8 73-120 % VMS11191 VXX20600 1 4-Bromofluorobenzene <surr> 106 76-120 % VMS11191 VXX20600 1 Toluene-d8 <surr> 99.7 80-120 % VMS11191 VXX20600 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### RHMW04-WG-04 SGS Ref. #: 1101763004 Collection Date/Time: 04/26/10 13:10 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS11191 Analytical Method: SW8260B Analysis Date/Time: 04/30/10 16:15 Prep Batch: VXX20600 Prep Method: SW5030B Prep Date/Time: 04/30/10 08:55 Container ID:1101763004-D Dilution Factor: 1 Analyst: JPI

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### RHMW04-WG-04 SGS Ref. #: 1101763004 Collection Date/Time: 04/26/10 13:10 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

DL DF

1-Methylnaphthalene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 2-Methylnaphthalene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Acenaphthene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Acenaphthylene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Anthracene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Benzo(a)Anthracene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Benzo[a]pyrene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Benzo[b]Fluoranthene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Benzo[g,h,i]perylene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Benzo[k]fluoranthene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Chrysene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Dibenzo[a,h]anthracene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Fluoranthene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Fluorene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Indeno[1,2,3-c,d] pyrene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Naphthalene 0.0730 U 0.118 ug/L XMS5395 XXX22544 0.0365 1 Phenanthrene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Pyrene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Terphenyl-d14 <surr> 83.3 50-126 % XMS5395 XXX22544 1

Batch Information Initial Prep Wt./Vol.: 850 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS5395 Analytical Method: 8270D SIMS Analysis Date/Time: 05/08/10 11:18 Prep Batch: XXX22544 Prep Method: SW3520C Prep Date/Time: 04/29/10 08:00 Container ID:1101763004-G Dilution Factor: 1 Analyst: JDH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### RHMWA01-WG-04 SGS Ref. #: 1101763005 Collection Date/Time: 04/26/10 12:05 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 ug/L MMS6414 MXX22933 0.310 5

Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS6414 Analytical Method: SW6020 Analysis Date/Time: 05/04/10 11:55 Prep Batch: MXX22933 Prep Method: SW3010A Prep Date/Time: 04/29/10 16:05 Container ID:1101763005-K Dilution Factor: 5 Analyst: SCL

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### RHMWA01-WG-04 SGS Ref. #: 1101763005 Collection Date/Time: 04/26/10 12:05 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 ug/L VFC9914 VXX20617 30.0 1 4-Bromofluorobenzene <surr> 108 50-150 % VFC9914 VXX20617 1

Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9914 Analytical Method: SW8015C Analysis Date/Time: 05/07/10 11:34 Prep Batch: VXX20617 Prep Method: SW5030B Prep Date/Time: 05/07/10 08:48 Container ID:1101763005-A Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### RHMWA01-WG-04 SGS Ref. #: 1101763005 Collection Date/Time: 04/26/10 12:05 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 0.352 U 0.471 mg/L XFC9168 XXX22543 0.176 1 5a Androstane <surr> 98.8 50-150 % XFC9168 XXX22543 1

Batch Information Initial Prep Wt./Vol.: 850 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC9168 Analytical Method: SW8015C Analysis Date/Time: 05/03/10 18:02 Prep Batch: XXX22543 Prep Method: SW3520C Prep Date/Time: 04/29/10 08:15 Container ID:1101763005-I Dilution Factor: 1 Analyst: LCE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### RHMWA01-WG-04 SGS Ref. #: 1101763005 Collection Date/Time: 04/26/10 12:05 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 1,1,1-Trichloroethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 1,1,2-Trichloroethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,1-Dichloroethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,1-Dichloroethene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,1-Dichloropropene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2,3-Trichloropropane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L VMS11191 VXX20600 0.620 1 1,2-Dibromoethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2-Dichlorobenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2-Dichloroethane 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 1,2-Dichloropropane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,3-Dichlorobenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,3-Dichloropropane 0.240 U 0.400 ug/L VMS11191 VXX20600 0.120 1 1,4-Dichlorobenzene 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 1-Chlorohexane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 2,2-Dichloropropane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 2-Butanone (MEK) 6.20 U 10.0 ug/L VMS11191 VXX20600 3.10 1 2-Chlorotoluene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 4-Chlorotoluene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 4-Isopropyltoluene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L VMS11191 VXX20600 3.10 1 Acetone 6.20 U 10.0 ug/L VMS11191 VXX20600 3.10 1 Benzene 0.240 U 0.400 ug/L VMS11191 VXX20600 0.120 1 Bromobenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Bromochloromethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Bromodichloromethane 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 Bromoform 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Bromomethane 1.88 U 3.00 ug/L VMS11191 VXX20600 0.940 1 Carbon tetrachloride 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Chlorobenzene 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### RHMWA01-WG-04 SGS Ref. #: 1101763005 Collection Date/Time: 04/26/10 12:05 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Chloroethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Chloroform 0.600 U 1.00 ug/L VMS11191 VXX20600 0.300 1 Chloromethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 cis-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 cis-1,3-Dichloropropene 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 Dibromochloromethane 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 Dibromomethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Dichlorodifluoromethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Ethylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Hexachlorobutadiene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Methylene chloride 2.00 U 5.00 ug/L VMS11191 VXX20600 1.00 1 Methyl-t-butyl ether 3.00 U 5.00 ug/L VMS11191 VXX20600 1.50 1 Naphthalene 1.24 U 2.00 ug/L VMS11191 VXX20600 0.620 1 n-Butylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 n-Propylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 o-Xylene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 P & M -Xylene 1.24 U 2.00 ug/L VMS11191 VXX20600 0.620 1 sec-Butylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Styrene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 tert-Butylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Tetrachloroethene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Toluene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 trans-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 trans-1,3-Dichloropropene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Trichloroethene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Trichlorofluoromethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Vinyl chloride 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Xylenes (total) 1.88 U 3.00 ug/L VMS11191 VXX20600 0.940 1 1,2-Dichloroethane-D4 <surr> 99.4 73-120 % VMS11191 VXX20600 1 4-Bromofluorobenzene <surr> 108 76-120 % VMS11191 VXX20600 1 Toluene-d8 <surr> 104 80-120 % VMS11191 VXX20600 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### RHMWA01-WG-04 SGS Ref. #: 1101763005 Collection Date/Time: 04/26/10 12:05 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS11191 Analytical Method: SW8260B Analysis Date/Time: 04/30/10 16:46 Prep Batch: VXX20600 Prep Method: SW5030B Prep Date/Time: 04/30/10 08:55 Container ID:1101763005-D Dilution Factor: 1 Analyst: JPI

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### RHMWA01-WG-04 SGS Ref. #: 1101763005 Collection Date/Time: 04/26/10 12:05 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

DL DF

1-Methylnaphthalene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 2-Methylnaphthalene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Acenaphthene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Acenaphthylene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Anthracene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Benzo(a)Anthracene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Benzo[a]pyrene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Benzo[b]Fluoranthene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Benzo[g,h,i]perylene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Benzo[k]fluoranthene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Chrysene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Dibenzo[a,h]anthracene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Fluoranthene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Fluorene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Indeno[1,2,3-c,d] pyrene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Naphthalene 0.0730 U 0.118 ug/L XMS5395 XXX22544 0.0365 1 Phenanthrene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Pyrene 0.0352 U 0.0588 ug/L XMS5395 XXX22544 0.0176 1 Terphenyl-d14 <surr> 84.3 50-126 % XMS5395 XXX22544 1

Batch Information Initial Prep Wt./Vol.: 850 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS5395 Analytical Method: 8270D SIMS Analysis Date/Time: 05/08/10 11:51 Prep Batch: XXX22544 Prep Method: SW3520C Prep Date/Time: 04/29/10 08:00 Container ID:1101763005-G Dilution Factor: 1 Analyst: JDH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### HDMW2253-03-WG-04 SGS Ref. #: 1101763006 Collection Date/Time: 04/26/10 09:40 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 ug/L MMS6414 MXX22933 0.310 5

Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS6414 Analytical Method: SW6020 Analysis Date/Time: 05/04/10 11:57 Prep Batch: MXX22933 Prep Method: SW3010A Prep Date/Time: 04/29/10 16:05 Container ID:1101763006-K Dilution Factor: 5 Analyst: SCL

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### HDMW2253-03-WG-04 SGS Ref. #: 1101763006 Collection Date/Time: 04/26/10 09:40 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 ug/L VFC9914 VXX20617 30.0 1 4-Bromofluorobenzene <surr> 108 50-150 % VFC9914 VXX20617 1

Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9914 Analytical Method: SW8015C Analysis Date/Time: 05/07/10 11:53 Prep Batch: VXX20617 Prep Method: SW5030B Prep Date/Time: 05/07/10 08:48 Container ID:1101763006-A Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### HDMW2253-03-WG-04 SGS Ref. #: 1101763006 Collection Date/Time: 04/26/10 09:40 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 0.352 U 0.471 mg/L XFC9168 XXX22543 0.176 1 5a Androstane <surr> 100 50-150 % XFC9168 XXX22543 1

Batch Information Initial Prep Wt./Vol.: 850 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC9168 Analytical Method: SW8015C Analysis Date/Time: 05/03/10 18:23 Prep Batch: XXX22543 Prep Method: SW3520C Prep Date/Time: 04/29/10 08:15 Container ID:1101763006-I Dilution Factor: 1 Analyst: LCE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### HDMW2253-03-WG-04 SGS Ref. #: 1101763006 Collection Date/Time: 04/26/10 09:40 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 1,1,1-Trichloroethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 1,1,2-Trichloroethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,1-Dichloroethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,1-Dichloroethene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,1-Dichloropropene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2,3-Trichloropropane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L VMS11191 VXX20600 0.620 1 1,2-Dibromoethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2-Dichlorobenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2-Dichloroethane 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 1,2-Dichloropropane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,3-Dichlorobenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,3-Dichloropropane 0.240 U 0.400 ug/L VMS11191 VXX20600 0.120 1 1,4-Dichlorobenzene 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 1-Chlorohexane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 2,2-Dichloropropane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 2-Butanone (MEK) 6.20 U 10.0 ug/L VMS11191 VXX20600 3.10 1 2-Chlorotoluene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 4-Chlorotoluene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 4-Isopropyltoluene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L VMS11191 VXX20600 3.10 1 Acetone 6.20 U 10.0 ug/L VMS11191 VXX20600 3.10 1 Benzene 0.240 U 0.400 ug/L VMS11191 VXX20600 0.120 1 Bromobenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Bromochloromethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Bromodichloromethane 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 Bromoform 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Bromomethane 1.88 U 3.00 ug/L VMS11191 VXX20600 0.940 1 Carbon tetrachloride 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Chlorobenzene 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### HDMW2253-03-WG-04 SGS Ref. #: 1101763006 Collection Date/Time: 04/26/10 09:40 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Chloroethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Chloroform 0.600 U 1.00 ug/L VMS11191 VXX20600 0.300 1 Chloromethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 cis-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 cis-1,3-Dichloropropene 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 Dibromochloromethane 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 Dibromomethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Dichlorodifluoromethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Ethylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Hexachlorobutadiene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Methylene chloride 2.00 U 5.00 ug/L VMS11191 VXX20600 1.00 1 Methyl-t-butyl ether 3.00 U 5.00 ug/L VMS11191 VXX20600 1.50 1 Naphthalene 1.24 U 2.00 ug/L VMS11191 VXX20600 0.620 1 n-Butylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 n-Propylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 o-Xylene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 P & M -Xylene 1.24 U 2.00 ug/L VMS11191 VXX20600 0.620 1 sec-Butylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Styrene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 tert-Butylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Tetrachloroethene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Toluene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 trans-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 trans-1,3-Dichloropropene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Trichloroethene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Trichlorofluoromethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Vinyl chloride 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Xylenes (total) 1.88 U 3.00 ug/L VMS11191 VXX20600 0.940 1 1,2-Dichloroethane-D4 <surr> 98.5 73-120 % VMS11191 VXX20600 1 4-Bromofluorobenzene <surr> 108 76-120 % VMS11191 VXX20600 1 Toluene-d8 <surr> 102 80-120 % VMS11191 VXX20600 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### HDMW2253-03-WG-04 SGS Ref. #: 1101763006 Collection Date/Time: 04/26/10 09:40 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS11191 Analytical Method: SW8260B Analysis Date/Time: 04/30/10 17:18 Prep Batch: VXX20600 Prep Method: SW5030B Prep Date/Time: 04/30/10 08:55 Container ID:1101763006-D Dilution Factor: 1 Analyst: JPI

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### HDMW2253-03-WG-04 SGS Ref. #: 1101763006 Collection Date/Time: 04/26/10 09:40 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

DL DF

1-Methylnaphthalene 0.0348 U 0.0581 ug/L XMS5395 XXX22544 0.0174 1 2-Methylnaphthalene 0.0348 U 0.0581 ug/L XMS5395 XXX22544 0.0174 1 Acenaphthene 0.0348 U 0.0581 ug/L XMS5395 XXX22544 0.0174 1 Acenaphthylene 0.0348 U 0.0581 ug/L XMS5395 XXX22544 0.0174 1 Anthracene 0.0348 U 0.0581 ug/L XMS5395 XXX22544 0.0174 1 Benzo(a)Anthracene 0.0348 U 0.0581 ug/L XMS5395 XXX22544 0.0174 1 Benzo[a]pyrene 0.0348 U 0.0581 ug/L XMS5395 XXX22544 0.0174 1 Benzo[b]Fluoranthene 0.0348 U 0.0581 ug/L XMS5395 XXX22544 0.0174 1 Benzo[g,h,i]perylene 0.0348 U 0.0581 ug/L XMS5395 XXX22544 0.0174 1 Benzo[k]fluoranthene 0.0348 U 0.0581 ug/L XMS5395 XXX22544 0.0174 1 Chrysene 0.0348 U 0.0581 ug/L XMS5395 XXX22544 0.0174 1 Dibenzo[a,h]anthracene 0.0348 U 0.0581 ug/L XMS5395 XXX22544 0.0174 1 Fluoranthene 0.0348 U 0.0581 ug/L XMS5395 XXX22544 0.0174 1 Fluorene 0.0348 U 0.0581 ug/L XMS5395 XXX22544 0.0174 1 Indeno[1,2,3-c,d] pyrene 0.0348 U 0.0581 ug/L XMS5395 XXX22544 0.0174 1 Naphthalene 0.0720 U 0.116 ug/L XMS5395 XXX22544 0.0360 1 Phenanthrene 0.0348 U 0.0581 ug/L XMS5395 XXX22544 0.0174 1 Pyrene 0.0348 U 0.0581 ug/L XMS5395 XXX22544 0.0174 1 Terphenyl-d14 <surr> 75.9 50-126 % XMS5395 XXX22544 1

Batch Information Initial Prep Wt./Vol.: 860 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS5395 Analytical Method: 8270D SIMS Analysis Date/Time: 05/08/10 12:24 Prep Batch: XXX22544 Prep Method: SW3520C Prep Date/Time: 04/29/10 08:00 Container ID:1101763006-G Dilution Factor: 1 Analyst: JDH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### TB01-WG-04 SGS Ref. #: 1101763007 Collection Date/Time: 04/26/10 08:05 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 ug/L VFC9914 VXX20617 30.0 1 4-Bromofluorobenzene <surr> 108 50-150 % VFC9914 VXX20617 1

Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9914 Analytical Method: SW8015C Analysis Date/Time: 05/07/10 12:12 Prep Batch: VXX20617 Prep Method: SW5030B Prep Date/Time: 05/07/10 08:48 Container ID:1101763007-B Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### TB01-WG-04 SGS Ref. #: 1101763007 Collection Date/Time: 04/26/10 08:05 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 1,1,1-Trichloroethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 1,1,2-Trichloroethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,1-Dichloroethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,1-Dichloroethene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,1-Dichloropropene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2,3-Trichloropropane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L VMS11191 VXX20600 0.620 1 1,2-Dibromoethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2-Dichlorobenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,2-Dichloroethane 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 1,2-Dichloropropane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,3-Dichlorobenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 1,3-Dichloropropane 0.240 U 0.400 ug/L VMS11191 VXX20600 0.120 1 1,4-Dichlorobenzene 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 1-Chlorohexane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 2,2-Dichloropropane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 2-Butanone (MEK) 6.20 U 10.0 ug/L VMS11191 VXX20600 3.10 1 2-Chlorotoluene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 4-Chlorotoluene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 4-Isopropyltoluene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L VMS11191 VXX20600 3.10 1 Acetone 6.20 U 10.0 ug/L VMS11191 VXX20600 3.10 1 Benzene 0.240 U 0.400 ug/L VMS11191 VXX20600 0.120 1 Bromobenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Bromochloromethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Bromodichloromethane 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 Bromoform 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Bromomethane 1.88 U 3.00 ug/L VMS11191 VXX20600 0.940 1 Carbon tetrachloride 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Chlorobenzene 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### TB01-WG-04 SGS Ref. #: 1101763007 Collection Date/Time: 04/26/10 08:05 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Chloroethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Chloroform 0.600 U 1.00 ug/L VMS11191 VXX20600 0.300 1 Chloromethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 cis-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 cis-1,3-Dichloropropene 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 Dibromochloromethane 0.300 U 0.500 ug/L VMS11191 VXX20600 0.150 1 Dibromomethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Dichlorodifluoromethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Ethylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Hexachlorobutadiene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Methylene chloride 2.00 U 5.00 ug/L VMS11191 VXX20600 1.00 1 Methyl-t-butyl ether 3.00 U 5.00 ug/L VMS11191 VXX20600 1.50 1 Naphthalene 1.24 U 2.00 ug/L VMS11191 VXX20600 0.620 1 n-Butylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 n-Propylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 o-Xylene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 P & M -Xylene 1.24 U 2.00 ug/L VMS11191 VXX20600 0.620 1 sec-Butylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Styrene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 tert-Butylbenzene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Tetrachloroethene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Toluene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 trans-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 trans-1,3-Dichloropropene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Trichloroethene 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Trichlorofluoromethane 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Vinyl chloride 0.620 U 1.00 ug/L VMS11191 VXX20600 0.310 1 Xylenes (total) 1.88 U 3.00 ug/L VMS11191 VXX20600 0.940 1 1,2-Dichloroethane-D4 <surr> 101 73-120 % VMS11191 VXX20600 1 4-Bromofluorobenzene <surr> 106 76-120 % VMS11191 VXX20600 1 Toluene-d8 <surr> 102 80-120 % VMS11191 VXX20600 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: 

### TB01-WG-04 SGS Ref. #: 1101763007 Collection Date/Time: 04/26/10 08:05 Receipt Date/Time: 04/28/10 11:50 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS11191 Analytical Method: SW8260B Analysis Date/Time: 04/30/10 12:35 Prep Batch: VXX20600 Prep Method: SW5030B Prep Date/Time: 04/30/10 08:55 Container ID:1101763007-A Dilution Factor: 1 Analyst: JPI

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S GroupMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 05/11/2010 12:34 Batch Method Date Prep 

### 958413 Method Blank The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) XXX22543 SW3520C 04/29/2010 QC results affect the following production samples: 

### 1101763001, 1101763004, 1101763005, 1101763006

Parameter Results LOQ/CL Units Analysis Date DL



### Semivolatile Organic Fuels Department


### Diesel Range Organics 0.300 U 0.400 mg/L 05/03/10 

### 0.150
Surrogates


### 5a Androstane <surr> 105 60-120 % 05/03/10

Instrument Method Batch XFC9168

SW8015C HP 7890A FID SV E RMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 05/11/2010 12:34 Batch Method Date Prep 

### 958415 Method Blank The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) XXX22544 SW3520C 04/29/2010 QC results affect the following production samples: 

### 1101763001, 1101763004, 1101763005, 1101763006

Parameter Results LOQ/CL Units Analysis Date DL


### Polynuclear Aromatics GC/MS


### 1-Methylnaphthalene 0.0300 U 0.0500 ug/L 05/08/10 

### 0.0150 2-Methylnaphthalene 0.0300 U 0.0500 ug/L 05/08/10 

### 0.0150 Acenaphthene 0.0300 U 0.0500 ug/L 05/08/10 

### 0.0150 Acenaphthylene 0.0300 U 0.0500 ug/L 05/08/10 

### 0.0150 Anthracene 0.0300 U 0.0500 ug/L 05/08/10 

### 0.0150 Benzo(a)Anthracene 0.0300 U 0.0500 ug/L 05/08/10 

### 0.0150 Benzo[a]pyrene 0.0300 U 0.0500 ug/L 05/08/10 

### 0.0150 Benzo[b]Fluoranthene 0.0300 U 0.0500 ug/L 05/08/10 

### 0.0150 Benzo[g,h,i]perylene 0.0300 U 0.0500 ug/L 05/08/10 

### 0.0150 Benzo[k]fluoranthene 0.0300 U 0.0500 ug/L 05/08/10 

### 0.0150 Chrysene 0.0300 U 0.0500 ug/L 05/08/10 

### 0.0150 Dibenzo[a,h]anthracene 0.0300 U 0.0500 ug/L 05/08/10 

### 0.0150 Fluoranthene 0.0300 U 0.0500 ug/L 05/08/10 

### 0.0150 Fluorene 0.0300 U 0.0500 ug/L 05/08/10 

### 0.0150 Indeno[1,2,3-c,d] pyrene 0.0300 U 0.0500 ug/L 05/08/10 

### 0.0150 Naphthalene 0.0620 U 0.100 ug/L 05/08/10 

### 0.0310 Phenanthrene 0.0300 U 0.0500 ug/L 05/08/10 

### 0.0150 Pyrene 0.0300 U 0.0500 ug/L 05/08/10 

### 0.0150
Surrogates 

### Terphenyl-d14 <surr> 86.8 50-126 % 05/08/10

Instrument Method Batch XMS5395

8270D SIMS HP 6890 Series II MS2 SVOAMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 05/11/2010 12:34 Batch Method Date Prep 

### 958689 Method Blank The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) MXX22933 SW3010A 04/29/2010 QC results affect the following production samples: 

### 1101763001, 1101763004, 1101763005, 1101763006

Parameter Results LOQ/CL Units Analysis Date DL


### Metals by ICP/MS



### Lead 0.620 U 1.00 ug/L 05/04/10 

### 0.310

Instrument Method Batch MMS6414

SW6020 Perkin Elmer Sciex ICP-MS P3Matrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 05/11/2010 12:34 Batch Method Date Prep 

### 958806 Method Blank The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20600 SW5030B 04/30/2010 QC results affect the following production samples: 

### 1101763001, 1101763004, 1101763005, 1101763006, 1101763007

Parameter Results LOQ/CL Units Analysis Date DL


### Volatile Gas Chromatography/Mass SpectroscopyMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 05/11/2010 12:34 Batch Method Date Prep 

### 958806 Method Blank The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20600 SW5030B 04/30/2010

Parameter Results LOQ/CL Units Analysis Date DL


### Volatile Gas Chromatography/Mass Spectroscopy


### 1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L 04/30/10 

### 0.150 1,1,1-Trichloroethane 0.620 U 1.00 ug/L 04/30/10 

### 0.310 1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L 04/30/10 

### 0.150 1,1,2-Trichloroethane 0.620 U 1.00 ug/L 04/30/10 

### 0.310 1,1-Dichloroethane 0.620 U 1.00 ug/L 04/30/10 

### 0.310 1,1-Dichloroethene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 1,1-Dichloropropene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 1,2,3-Trichloropropane 0.620 U 1.00 ug/L 04/30/10 

### 0.310 1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L 04/30/10 

### 0.620 1,2-Dibromoethane 0.620 U 1.00 ug/L 04/30/10 

### 0.310 1,2-Dichlorobenzene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 1,2-Dichloroethane 0.300 U 0.500 ug/L 04/30/10 

### 0.150 1,2-Dichloropropane 0.620 U 1.00 ug/L 04/30/10 

### 0.310 1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 1,3-Dichlorobenzene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 1,3-Dichloropropane 0.240 U 0.400 ug/L 04/30/10 

### 0.120 1,4-Dichlorobenzene 0.300 U 0.500 ug/L 04/30/10 

### 0.150 1-Chlorohexane 0.620 U 1.00 ug/L 04/30/10 

### 0.310 2,2-Dichloropropane 0.620 U 1.00 ug/L 04/30/10 

### 0.310 2-Butanone (MEK) 6.20 U 10.0 ug/L 04/30/10 

### 3.10 2-Chlorotoluene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 4-Chlorotoluene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 4-Isopropyltoluene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L 04/30/10 

### 3.10 Acetone 6.20 U 10.0 ug/L 04/30/10 

### 3.10 Benzene 0.240 U 0.400 ug/L 04/30/10 

### 0.120 Bromobenzene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 Bromochloromethane 0.620 U 1.00 ug/L 04/30/10 

### 0.310 Bromodichloromethane 0.300 U 0.500 ug/L 04/30/10 

### 0.150 Bromoform 0.620 U 1.00 ug/L 04/30/10 

### 0.310 Bromomethane 1.88 U 3.00 ug/L 04/30/10 

### 0.940 Carbon tetrachloride 0.620 U 1.00 ug/L 04/30/10 

### 0.310 Chlorobenzene 0.300 U 0.500 ug/L 04/30/10 

### 0.150 Chloroethane 0.620 U 1.00 ug/L 04/30/10 

### 0.310 Chloroform 0.600 U 1.00 ug/L 04/30/10 

### 0.300 Chloromethane 0.620 U 1.00 ug/L 04/30/10 

### 0.310Matrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 05/11/2010 12:34 Batch Method Date Prep 

### 958806 Method Blank The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20600 SW5030B 04/30/2010

Parameter Results LOQ/CL Units Analysis Date DL


### Volatile Gas Chromatography/Mass Spectroscopy


### cis-1,2-Dichloroethene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 cis-1,3-Dichloropropene 0.300 U 0.500 ug/L 04/30/10 

### 0.150 Dibromochloromethane 0.300 U 0.500 ug/L 04/30/10 

### 0.150 Dibromomethane 0.620 U 1.00 ug/L 04/30/10 

### 0.310 Dichlorodifluoromethane 0.620 U 1.00 ug/L 04/30/10 

### 0.310 Ethylbenzene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 Hexachlorobutadiene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L 04/30/10 

### 0.310 Methylene chloride 2.00 U 5.00 ug/L 04/30/10 

### 1.00 Methyl-t-butyl ether 3.00 U 5.00 ug/L 04/30/10 

### 1.50 Naphthalene 1.24 U 2.00 ug/L 04/30/10 

### 0.620 n-Butylbenzene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 n-Propylbenzene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 o-Xylene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 P & M -Xylene 1.24 U 2.00 ug/L 04/30/10 

### 0.620 sec-Butylbenzene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 Styrene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 tert-Butylbenzene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 Tetrachloroethene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 Toluene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 trans-1,2-Dichloroethene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 trans-1,3-Dichloropropene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 Trichloroethene 0.620 U 1.00 ug/L 04/30/10 

### 0.310 Trichlorofluoromethane 0.620 U 1.00 ug/L 04/30/10 

### 0.310 Vinyl chloride 0.620 U 1.00 ug/L 04/30/10 

### 0.310 Xylenes (total) 1.88 U 3.00 ug/L 04/30/10 

### 0.940
Surrogates 

### 1,2-Dichloroethane-D4 <surr> 99.5 73-120 % 04/30/10 

### 4-Bromofluorobenzene <surr> 109 76-120 % 04/30/10 

### Toluene-d8 <surr> 99 80-120 % 04/30/10

Instrument Method Batch VMS11191

SW8260B HP 5890 Series II MS3 VNAMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 05/11/2010 12:34 Batch Method Date Prep 

### 959759 Method Blank The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20617 SW5030B 05/07/2010 QC results affect the following production samples: 

### 1101763001, 1101763004, 1101763005, 1101763006, 1101763007

Parameter Results LOQ/CL Units Analysis Date DL



### Volatile Fuels Department


### Gasoline Range Organics 60.0 U 100 ug/L 05/07/10 

### 30.0
Surrogates


### 4-Bromofluorobenzene <surr> 107 50-150 % 05/07/10

Instrument Method Batch VFC9914

SW8015C HP 5890 Series II PID+FID VCAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 05/11/2010 12:34
Batch Method Date Prep 

### 958416 Lab Control Sample
The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) XXX22544 SW3520C 04/29/2010

QC results affect the following production samples: 

### 1101763001, 1101763004, 1101763005, 1101763006

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Polynuclear Aromatics GC/MS 

### 1-Methylnaphthalene LCS 0.392 78 ( 42-92 ) 0.5 ug/L 05/08/2010
2-Methylnaphthalene LCS 0.353 71 ( 45-89 ) 0.5 ug/L 05/08/2010
Acenaphthene LCS 0.396 79 ( 45-93 ) 0.5 ug/L 05/08/2010
Acenaphthylene LCS 0.406 81 ( 50-101 ) 0.5 ug/L 05/08/2010

Anthracene LCS 0.435 87 ( 55-105 ) 0.5 ug/L 05/08/2010
Benzo(a)Anthracene LCS 0.448 90 ( 55-120 ) 0.5 ug/L 05/08/2010
Benzo[a]pyrene LCS 0.448 90 ( 57-110 ) 0.5 ug/L 05/08/2010
Benzo[b]Fluoranthene LCS 0.485 97 ( 45-120 ) 0.5 ug/L 05/08/2010
Benzo[g,h,i]perylene LCS 0.447 89 ( 49-116 ) 0.5 ug/L 05/08/2010
Benzo[k]fluoranthene LCS 0.456 91 ( 56-112 ) 0.5 ug/L 05/08/2010
Chrysene LCS 0.428 86 ( 56-109 ) 0.5 ug/L 05/08/2010
Dibenzo[a,h]anthracene LCS 0.470 94 ( 54-113 ) 0.5 ug/L 05/08/2010

Fluoranthene LCS 0.418 84 ( 58-109 ) 0.5 ug/L 05/08/2010

Fluorene LCS 0.423 85 ( 50-98 ) 0.5 ug/L 05/08/2010
Indeno[1,2,3-c,d] pyrene LCS 0.476 95 ( 55-111 ) 0.5 ug/L 05/08/2010
Naphthalene LCS 0.350 70 ( 44-89 ) 0.5 ug/L 05/08/2010

Phenanthrene LCS 0.415 83 ( 50-104 ) 0.5 ug/L 05/08/2010
Pyrene LCS 0.395 79 ( 56-105 ) 0.5 ug/L 05/08/2010

Surrogates 

### Terphenyl-d14 <surr> LCS 87 ( 50-126 ) 05/08/2010Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 05/11/2010 12:34
Batch Method Date Prep 

### 958416 Lab Control Sample
The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) XXX22544 SW3520C 04/29/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Polynuclear Aromatics GC/MS

Batch Method Instrument 

### XMS5395

8270D SIMS HP 6890 Series II MS2 SVOAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 05/11/2010 12:34
Batch Method Date Prep 

### 958690 Lab Control Sample
The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) MXX22933 SW3010A 04/29/2010

QC results affect the following production samples: 

### 1101763001, 1101763004, 1101763005, 1101763006

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Metals by ICP/MS



### Lead LCS 975 98 ( 80-120 ) 1000 ug/L 05/04/2010

Batch Method Instrument 

### MMS6414

SW6020 Perkin Elmer Sciex ICP-MS P3Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 05/11/2010 12:34
Batch Method Date Prep 

### 958807 Lab Control Sample 958808 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20600 SW5030B 04/30/2010

QC results affect the following production samples: 

### 1101763001, 1101763004, 1101763005, 1101763006, 1101763007

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass SpectroscopyMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 05/11/2010 12:34
Batch Method Date Prep 

### 958807 Lab Control Sample 958808 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20600 SW5030B 04/30/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy 

### 1,1,1,2-Tetrachloroethane LCS 29.9 100 ( 80-120 ) 30 ug/L 04/30/2010 LCSD 30.8 103 3 (< 20 ) 30 ug/L 04/30/2010

1,1,1-Trichloroethane LCS 31.4 105 ( 80-122 ) 30 ug/L 04/30/2010 LCSD 32.0 107 2 (< 20 ) 30 ug/L 04/30/2010

1,1,2,2-Tetrachloroethane LCS 31.0 103 ( 76-123 ) 30 ug/L 04/30/2010 LCSD 30.7 102 1 (< 20 ) 30 ug/L 04/30/2010

1,1,2-Trichloroethane LCS 29.5 98 ( 77-120 ) 30 ug/L 04/30/2010 LCSD 29.8 99 1 (< 20 ) 30 ug/L 04/30/2010

1,1-Dichloroethane LCS 35.1 117 ( 80-120 ) 30 ug/L 04/30/2010 LCSD 34.8 116 1 (< 20 ) 30 ug/L 04/30/2010

1,1-Dichloroethene LCS 32.6 109 ( 76-130 ) 30 ug/L 04/30/2010 LCSD 32.4 108 1 (< 20 ) 30 ug/L 04/30/2010
1,1-Dichloropropene LCS 30.9 103 ( 80-122 ) 30 ug/L 04/30/2010 LCSD 31.0 103 0 (< 20 ) 30 ug/L 04/30/2010

1,2,3-Trichlorobenzene LCS 29.6 99 ( 77-120 ) 30 ug/L 04/30/2010 LCSD 30.0 100 1 (< 20 ) 30 ug/L 04/30/2010
1,2,3-Trichloropropane LCS 30.8 103 ( 80-120 ) 30 ug/L 04/30/2010 LCSD 31.6 105 2 (< 20 ) 30 ug/L 04/30/2010

1,2,4-Trichlorobenzene LCS 28.6 95 ( 80-120 ) 30 ug/L 04/30/2010 LCSD 28.9 96 1 (< 20 ) 30 ug/L 04/30/2010
1,2,4-Trimethylbenzene LCS 31.2 104 ( 80-125 ) 30 ug/L 04/30/2010 LCSD 31.8 106 2 (< 20 ) 30 ug/L 04/30/2010
1,2-Dibromo-3-chloropropane LCS 32.6 109 ( 73-130 ) 30 ug/L 04/30/2010 LCSD 32.2 107 1 (< 20 ) 30 ug/L 04/30/2010

1,2-Dibromoethane LCS 27.8 93 ( 80-120 ) 30 ug/L 04/30/2010 LCSD 27.7 93 0 (< 20 ) 30 ug/L 04/30/2010

1,2-Dichlorobenzene LCS 29.0 97 ( 80-120 ) 30 ug/L 04/30/2010 LCSD 29.2 97 1 (< 20 ) 30 ug/L 04/30/2010Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 05/11/2010 12:34
Batch Method Date Prep 

### 958807 Lab Control Sample 958808 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20600 SW5030B 04/30/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### 1,2-Dichloroethane LCS 30.0 100 ( 80-129 ) 30 ug/L 04/30/2010 LCSD 29.7 99 1 (< 20 ) 30 ug/L 04/30/2010
1,2-Dichloropropane LCS 30.3 101 ( 80-121 ) 30 ug/L 04/30/2010 LCSD 29.7 99 2 (< 20 ) 30 ug/L 04/30/2010
1,3,5-Trimethylbenzene LCS 32.1 107 ( 80-128 ) 30 ug/L 04/30/2010 LCSD 32.3 108 1 (< 20 ) 30 ug/L 04/30/2010

1,3-Dichlorobenzene LCS 28.6 95 ( 80-120 ) 30 ug/L 04/30/2010 LCSD 29.4 98 3 (< 20 ) 30 ug/L 04/30/2010
1,3-Dichloropropane LCS 29.5 98 ( 80-121 ) 30 ug/L 04/30/2010 LCSD 29.1 97 1 (< 20 ) 30 ug/L 04/30/2010

1,4-Dichlorobenzene LCS 28.8 96 ( 80-120 ) 30 ug/L 04/30/2010 LCSD 28.4 95 1 (< 20 ) 30 ug/L 04/30/2010

1-Chlorohexane LCS 45.2 100 ( 70-125 ) 45 ug/L 04/30/2010 LCSD 45.6 101 1 (< 20 ) 45 ug/L 04/30/2010
2,2-Dichloropropane LCS 31.5 105 ( 80-132 ) 30 ug/L 04/30/2010 LCSD 31.7 106 1 (< 20 ) 30 ug/L 04/30/2010
2-Butanone (MEK) LCS 93.4 104 ( 66-136 ) 90 ug/L 04/30/2010 LCSD 95.2 106 2 (< 20 ) 90 ug/L 04/30/2010

2-Chlorotoluene LCS 31.3 104 ( 80-125 ) 30 ug/L 04/30/2010 LCSD 31.7 106 1 (< 20 ) 30 ug/L 04/30/2010

4-Chlorotoluene LCS 31.9 106 ( 79-128 ) 30 ug/L 04/30/2010 LCSD 32.5 108 2 (< 20 ) 30 ug/L 04/30/2010
4-Isopropyltoluene LCS 30.9 103 ( 80-125 ) 30 ug/L 04/30/2010 LCSD 31.0 103 0 (< 20 ) 30 ug/L 04/30/2010
4-Methyl-2-pentanone (MIBK) LCS 94.6 105 ( 69-134 ) 90 ug/L 04/30/2010 LCSD 91.1 101 4 (< 20 ) 90 ug/L 04/30/2010

Acetone LCS 109 121 ( 50-135 ) 90 ug/L 04/30/2010Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 05/11/2010 12:34
Batch Method Date Prep 

### 958807 Lab Control Sample 958808 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20600 SW5030B 04/30/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### LCSD 103 115 5 (< 20 ) 90 ug/L 04/30/2010

Benzene LCS 28.6 95 ( 80-120 ) 30 ug/L 04/30/2010 LCSD 28.6 96 0 (< 20 ) 30 ug/L 04/30/2010

Bromobenzene LCS 28.9 96 ( 80-120 ) 30 ug/L 04/30/2010 LCSD 29.0 97 0 (< 20 ) 30 ug/L 04/30/2010

Bromochloromethane LCS 31.0 103 ( 77-129 ) 30 ug/L 04/30/2010 LCSD 30.6 102 1 (< 20 ) 30 ug/L 04/30/2010

Bromodichloromethane LCS 35.3 118 ( 80-120 ) 30 ug/L 04/30/2010 LCSD 35.4 118 0 (< 20 ) 30 ug/L 04/30/2010

Bromoform LCS 34.4 115 ( 80-120 ) 30 ug/L 04/30/2010 LCSD 34.8 116 1 (< 20 ) 30 ug/L 04/30/2010

Bromomethane LCS 36.8 123 ( 30-140 ) 30 ug/L 04/30/2010 LCSD 35.8 119 3 (< 20 ) 30 ug/L 04/30/2010

Carbon tetrachloride LCS 37.1 124 ( 80-126 ) 30 ug/L 04/30/2010 LCSD 37.2 124 0 (< 20 ) 30 ug/L 04/30/2010

Chlorobenzene LCS 28.5 95 ( 80-120 ) 30 ug/L 04/30/2010 LCSD 29.0 97 2 (< 20 ) 30 ug/L 04/30/2010

Chloroethane LCS 35.7 119 ( 67-133 ) 30 ug/L 04/30/2010 LCSD 36.1 120 1 (< 20 ) 30 ug/L 04/30/2010

Chloroform LCS 29.8 99 ( 80-124 ) 30 ug/L 04/30/2010 LCSD 30.1 100 1 (< 20 ) 30 ug/L 04/30/2010

Chloromethane LCS 29.1 97 ( 67-125 ) 30 ug/L 04/30/2010 LCSD 30.1 100 3 (< 20 ) 30 ug/L 04/30/2010

cis-1,2-Dichloroethene LCS 30.3 101 ( 80-125 ) 30 ug/L 04/30/2010 LCSD 30.0 100 1 (< 20 ) 30 ug/L 04/30/2010
cis-1,3-Dichloropropene LCS 34.1 114 ( 80-120 ) 30 ug/L 04/30/2010 LCSD 34.0 113 0 (< 20 ) 30 ug/L 04/30/2010Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 05/11/2010 12:34
Batch Method Date Prep 

### 958807 Lab Control Sample 958808 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20600 SW5030B 04/30/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### Dibromochloromethane LCS 31.4 105 ( 80-120 ) 30 ug/L 04/30/2010 LCSD 31.2 104 1 (< 20 ) 30 ug/L 04/30/2010

Dibromomethane LCS 30.8 103 ( 80-120 ) 30 ug/L 04/30/2010 LCSD 29.8 99 3 (< 20 ) 30 ug/L 04/30/2010

Dichlorodifluoromethane LCS 31.4 105 ( 62-153 ) 30 ug/L 04/30/2010 LCSD 31.7 106 1 (< 20 ) 30 ug/L 04/30/2010
Ethylbenzene LCS 29.2 97 ( 80-120 ) 30 ug/L 04/30/2010 LCSD 29.7 99 2 (< 20 ) 30 ug/L 04/30/2010

Hexachlorobutadiene LCS 28.4 95 ( 77-125 ) 30 ug/L 04/30/2010 LCSD 28.2 94 1 (< 20 ) 30 ug/L 04/30/2010
Isopropylbenzene (Cumene) LCS 27.9 93 ( 80-121 ) 30 ug/L 04/30/2010 LCSD 27.7 92 1 (< 20 ) 30 ug/L 04/30/2010
Methylene chloride LCS 32.0 107 ( 63-131 ) 30 ug/L 04/30/2010 LCSD 31.5 105 2 (< 20 ) 30 ug/L 04/30/2010
Methyl-t-butyl ether LCS 49.3 110 ( 80-120 ) 45 ug/L 04/30/2010 LCSD 47.6 106 4 (< 20 ) 45 ug/L 04/30/2010
Naphthalene LCS 29.8 99 ( 75-120 ) 30 ug/L 04/30/2010 LCSD 29.8 99 0 (< 20 ) 30 ug/L 04/30/2010
n-Butylbenzene LCS 31.3 104 ( 80-124 ) 30 ug/L 04/30/2010 LCSD 31.6 105 1 (< 20 ) 30 ug/L 04/30/2010
n-Propylbenzene LCS 33.1 110 ( 80-129 ) 30 ug/L 04/30/2010 LCSD 33.2 111 0 (< 20 ) 30 ug/L 04/30/2010
o-Xylene LCS 29.5 98 ( 80-120 ) 30 ug/L 04/30/2010 LCSD 29.5 98 0 (< 20 ) 30 ug/L 04/30/2010
P & M -Xylene LCS 58.0 97 ( 80-120 ) 60 ug/L 04/30/2010 LCSD 58.7 98 1 (< 20 ) 60 ug/L 04/30/2010
sec-Butylbenzene LCS 32.1 107 ( 80-120 ) 30 ug/L 04/30/2010 LCSD 32.3 108 1 (< 20 ) 30 ug/L 04/30/2010Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 05/11/2010 12:34
Batch Method Date Prep 

### 958807 Lab Control Sample 958808 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20600 SW5030B 04/30/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### Styrene LCS 29.7 99 ( 80-120 ) 30 ug/L 04/30/2010 LCSD 29.9 100 1 (< 20 ) 30 ug/L 04/30/2010
tert-Butylbenzene LCS 30.9 103 ( 80-122 ) 30 ug/L 04/30/2010 LCSD 30.9 103 0 (< 20 ) 30 ug/L 04/30/2010

Tetrachloroethene LCS 27.5 92 ( 79-122 ) 30 ug/L 04/30/2010 LCSD 28.4 95 3 (< 20 ) 30 ug/L 04/30/2010

Toluene LCS 27.6 92 ( 77-120 ) 30 ug/L 04/30/2010 LCSD 28.2 94 2 (< 20 ) 30 ug/L 04/30/2010

trans-1,2-Dichloroethene LCS 32.5 108 ( 79-132 ) 30 ug/L 04/30/2010 LCSD 32.5 108 0 (< 20 ) 30 ug/L 04/30/2010
trans-1,3-Dichloropropene LCS 33.5 112 ( 80-124 ) 30 ug/L 04/30/2010 LCSD 33.4 111 0 (< 20 ) 30 ug/L 04/30/2010

Trichloroethene LCS 30.1 100 ( 80-125 ) 30 ug/L 04/30/2010 LCSD 30.5 102 1 (< 20 ) 30 ug/L 04/30/2010

Trichlorofluoromethane LCS 33.4 111 ( 68-145 ) 30 ug/L 04/30/2010 LCSD 34.8 116 4 (< 20 ) 30 ug/L 04/30/2010
Vinyl chloride LCS 32.6 109 ( 72-145 ) 30 ug/L 04/30/2010 LCSD 32.6 109 0 (< 20 ) 30 ug/L 04/30/2010
Xylenes (total) LCS 87.4 97 ( 80-120 ) 90 ug/L 04/30/2010 LCSD 88.2 98 1 (< 20 ) 90 ug/L 04/30/2010

Surrogates 

### 1,2-Dichloroethane-D4 <surr> LCS 103 ( 73-120 ) 04/30/2010 LCSD 97 6 04/30/2010

4-Bromofluorobenzene <surr> LCS 100 ( 76-120 ) 04/30/2010 LCSD 99 1 04/30/2010

Toluene-d8 <surr> LCS 99 ( 80-120 ) 04/30/2010 LCSD 98 1 04/30/2010Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 05/11/2010 12:34
Batch Method Date Prep 

### 958807 Lab Control Sample 958808 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20600 SW5030B 04/30/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy

Batch Method Instrument 

### VMS11191

SW8260B HP 5890 Series II MS3 VNAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 05/11/2010 12:34
Batch Method Date Prep 

### 959066 Lab Control Sample
The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) XXX22543 SW3520C 04/29/2010

QC results affect the following production samples: 

### 1101763001, 1101763004, 1101763005, 1101763006

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits



### Semivolatile Organic Fuels Department 

### Diesel Range Organics LCS 4.86 97 ( 75-125 ) 5 mg/L 05/03/2010

Surrogates 

### 5a Androstane <surr> LCS 98 ( 60-120 ) 05/03/2010

Batch Method Instrument 

### XFC9168

SW8015C HP 7890A FID SV E RMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 05/11/2010 12:34
Batch Method Date Prep 

### 959760 Lab Control Sample 959761 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20617 SW5030B 05/07/2010

QC results affect the following production samples: 

### 1101763001, 1101763004, 1101763005, 1101763006, 1101763007

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits



### Volatile Fuels Department 

### Gasoline Range Organics LCS 220 110 ( 80-116 ) 200 ug/L 05/07/2010 LCSD 215 107 3 (< 20 ) 200 ug/L 05/07/2010

Surrogates 

### 4-Bromofluorobenzene <surr> LCS 110 ( 50-150 ) 05/07/2010 LCSD 112 2 05/07/2010

Batch Method Instrument 

### VFC9914

SW8015C HP 5890 Series II PID+FID VCAMatrix SGS Ref.# Printed Date/Time 

### 05/11/2010 12:34 Batch Method Date Original Prep 

### 1101763002 Billable Matrix Spike 1101763003 Billable Matrix Spike Dup.

1101763001 Water (Surface, Eff., Ground) MXX22933 3010 H20 Digest for Metals ICP-MS 04/29/2010

QC results affect the following production samples:

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Dissolved Metals by ICP/MS


### Lead BMS (0.620) U 912 91 ( 80-120 ) 1000 ug/L 05/04/2010 BMSD 976 98 7 (< 15 ) 1000 ug/L 05/04/2010
Batch Method Instrument 

### MMS6414

SW6020 Perkin Elmer Sciex ICP-MS P3

Volatile Fuels Department 

### Gasoline Range Organics BMS (60.0) U 484 108 ( 80-116 ) 450 ug/L 05/07/2010 BMSD 467 104 4 (< 20 ) 450 ug/L 05/07/2010 Surrogates 

### 4-Bromofluorobenzene <surr> BMS 55.4 111 ( 50-150 ) 05/07/2010 BMSD 54.8 110 1 05/07/2010
Batch Method Instrument 

### VFC9914

SW8015C HP 5890 Series II PID+FID VCA

Semivolatile Organic Fuels Department 

### Diesel Range Organics BMS 0.288J 5.59 90 ( 75-125 ) 5.88 mg/L 05/03/2010 BMSD 6.17 100 10 (< 30 ) 5.88 mg/L 05/03/2010 Surrogates 

### 5a Androstane <surr> BMS .109 92 ( 50-150 ) 05/03/2010 BMSD 0.120 102 10 05/03/2010
Batch Method Instrument 

### XFC9168

SW8015C HP 7890A FID SV E R

Volatile Gas Chromatography/Mass SpectroscopyMatrix SGS Ref.# Printed Date/Time 

### 05/11/2010 12:34 Batch Method Date Original Prep 

### 1101763002 Billable Matrix Spike 1101763003 Billable Matrix Spike Dup.

1101763001 Water (Surface, Eff., Ground) VXX20600 Volatiles Extraction AFCEE 3.1 8260 (W) 04/30/2010

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy 

### 1,1,1,2-Tetrachloroethane BMS (0.300) U 32 107 ( 80-120 ) 30.0 ug/L 04/30/2010 BMSD 31.0 103 3 (< 20 ) 30.0 ug/L 04/30/2010 1,1,1-Trichloroethane BMS (0.620) U 31.7 106 ( 80-122 ) 30.0 ug/L 04/30/2010 BMSD 31.4 105 1 (< 20 ) 30.0 ug/L 04/30/2010 1,1,2,2-Tetrachloroethane BMS (0.300) U 31.5 105 ( 76-123 ) 30.0 ug/L 04/30/2010 BMSD 30.4 101 4 (< 20 ) 30.0 ug/L 04/30/2010 1,1,2-Trichloroethane BMS (0.620) U 30.9 103 ( 77-120 ) 30.0 ug/L 04/30/2010 BMSD 31.4 105 1 (< 20 ) 30.0 ug/L 04/30/2010 1,1-Dichloroethane BMS (0.620) U 35.4 118 ( 80-120 ) 30.0 ug/L 04/30/2010 BMSD 34.9 116 1 (< 20 ) 30.0 ug/L 04/30/2010 1,1-Dichloroethene BMS (0.620) U 32.7 109 ( 76-130 ) 30.0 ug/L 04/30/2010 BMSD 32.6 109 1 (< 20 ) 30.0 ug/L 04/30/2010 1,1-Dichloropropene BMS (0.620) U 30.9 103 ( 80-122 ) 30.0 ug/L 04/30/2010 BMSD 31.4 105 2 (< 20 ) 30.0 ug/L 04/30/2010 1,2,3-Trichlorobenzene BMS (0.620) U 30.4 101 ( 77-120 ) 30.0 ug/L 04/30/2010 BMSD 29.6 99 3 (< 20 ) 30.0 ug/L 04/30/2010 1,2,3-Trichloropropane BMS (0.620) U 31.7 106 ( 80-120 ) 30.0 ug/L 04/30/2010 BMSD 30.7 102 3 (< 20 ) 30.0 ug/L 04/30/2010 1,2,4-Trichlorobenzene BMS (0.620) U 30.1 100 ( 80-120 ) 30.0 ug/L 04/30/2010 BMSD 28.8 96 5 (< 20 ) 30.0 ug/L 04/30/2010 1,2,4-Trimethylbenzene BMS (0.620) U 32.5 108 ( 80-125 ) 30.0 ug/L 04/30/2010 BMSD 30.8 103 6 (< 20 ) 30.0 ug/L 04/30/2010 1,2-Dibromo-3-chloropropane BMS (1.24) U 32 107 ( 73-130 ) 30.0 ug/L 04/30/2010 BMSD 31.8 106 1 (< 20 ) 30.0 ug/L 04/30/2010 1,2-Dibromoethane BMS (0.620) U 28.7 96 ( 80-120 ) 30.0 ug/L 04/30/2010 BMSD 27.6 92 4 (< 20 ) 30.0 ug/L 04/30/2010 1,2-Dichlorobenzene BMS (0.620) U 30 100 ( 80-120 ) 30.0 ug/L 04/30/2010 BMSD 28.9 96 4 (< 20 ) 30.0 ug/L 04/30/2010 1,2-Dichloroethane BMS (0.300) U 29.3 98 ( 80-129 ) 30.0 ug/L 04/30/2010 BMSD 29.6 99 1 (< 20 ) 30.0 ug/L 04/30/2010 1,2-Dichloropropane BMS (0.620) U 30.8 103 ( 80-121 ) 30.0 ug/L 04/30/2010 BMSD 29.7 99 4 (< 20 ) 30.0 ug/L 04/30/2010 1,3,5-Trimethylbenzene BMS (0.620) U 33.2 111 ( 80-128 ) 30.0 ug/L 04/30/2010 BMSD 31.7 106 5 (< 20 ) 30.0 ug/L 04/30/2010 1,3-Dichlorobenzene BMS (0.620) U 30.3 101 ( 80-120 ) 30.0 ug/L 04/30/2010 BMSD 29.5 98 3 (< 20 ) 30.0 ug/L 04/30/2010 1,3-Dichloropropane BMS (0.240) U 30.5 102 ( 80-121 ) 30.0 ug/L 04/30/2010 BMSD 30.3 101 0 (< 20 ) 30.0 ug/L 04/30/2010 1,4-Dichlorobenzene BMS (0.300) U 29.6 99 ( 80-120 ) 30.0 ug/L 04/30/2010 BMSD 28.1 94 5 (< 20 ) 30.0 ug/L 04/30/2010Matrix SGS Ref.# Printed Date/Time 

### 05/11/2010 12:34 Batch Method Date Original Prep 

### 1101763002 Billable Matrix Spike 1101763003 Billable Matrix Spike Dup.

1101763001 Water (Surface, Eff., Ground) VXX20600 Volatiles Extraction AFCEE 3.1 8260 (W) 04/30/2010

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy


### 1-Chlorohexane BMS (0.620) U 47 105 ( 70-125 ) 45.0 ug/L 04/30/2010 BMSD 46.8 104 0 (< 20 ) 45.0 ug/L 04/30/2010 2,2-Dichloropropane BMS (0.620) U 28.9 96 ( 80-132 ) 30.0 ug/L 04/30/2010 BMSD 29.2 97 1 (< 20 ) 30.0 ug/L 04/30/2010 2-Butanone (MEK) BMS (6.20) U 94.7 105 ( 66-136 ) 90.0 ug/L 04/30/2010 BMSD 92.7 103 2 (< 20 ) 90.0 ug/L 04/30/2010 2-Chlorotoluene BMS (0.620) U 32.5 108 ( 80-125 ) 30.0 ug/L 04/30/2010 BMSD 31.2 104 4 (< 20 ) 30.0 ug/L 04/30/2010 4-Chlorotoluene BMS (0.620) U 33.4 111 ( 79-128 ) 30.0 ug/L 04/30/2010 BMSD 31.8 106 5 (< 20 ) 30.0 ug/L 04/30/2010 4-Isopropyltoluene BMS (0.620) U 32.4 108 ( 80-125 ) 30.0 ug/L 04/30/2010 BMSD 30.6 102 6 (< 20 ) 30.0 ug/L 04/30/2010 4-Methyl-2-pentanone (MIBK) BMS (6.20) U 93.7 104 ( 69-134 ) 90.0 ug/L 04/30/2010 BMSD 92.0 102 2 (< 20 ) 90.0 ug/L 04/30/2010 Acetone BMS (6.20) U 109 121 ( 50-135 ) 90.0 ug/L 04/30/2010 BMSD 107 119 2 (< 20 ) 90.0 ug/L 04/30/2010 Benzene BMS (0.240) U 29.1 97 ( 80-120 ) 30.0 ug/L 04/30/2010 BMSD 28.2 94 3 (< 20 ) 30.0 ug/L 04/30/2010 Bromobenzene BMS (0.620) U 29.4 98 ( 80-120 ) 30.0 ug/L 04/30/2010 BMSD 28.5 95 3 (< 20 ) 30.0 ug/L 04/30/2010 Bromochloromethane BMS (0.620) U 30.6 102 ( 77-129 ) 30.0 ug/L 04/30/2010 BMSD 30.6 102 0 (< 20 ) 30.0 ug/L 04/30/2010 Bromodichloromethane BMS (0.300) U 35 117 ( 80-120 ) 30.0 ug/L 04/30/2010 BMSD 34.9 116 0 (< 20 ) 30.0 ug/L 04/30/2010 Bromoform BMS (0.620) U 34.6 115 ( 80-120 ) 30.0 ug/L 04/30/2010 BMSD 34.9 116 1 (< 20 ) 30.0 ug/L 04/30/2010 Bromomethane BMS (1.88) U 38.5 128 ( 30-140 ) 30.0 ug/L 04/30/2010 BMSD 37.8 126 2 (< 20 ) 30.0 ug/L 04/30/2010 Carbon tetrachloride BMS (0.620) U 36.3 121 ( 80-126 ) 30.0 ug/L 04/30/2010 BMSD 37.2 124 2 (< 20 ) 30.0 ug/L 04/30/2010 Chlorobenzene BMS (0.300) U 30.3 101 ( 80-120 ) 30.0 ug/L 04/30/2010 BMSD 30.0 100 1 (< 20 ) 30.0 ug/L 04/30/2010 Chloroethane BMS (0.620) U 50.4 168* ( 67-133 ) 30.0 ug/L 04/30/2010 BMSD 45.0 150 * 12 (< 20 ) 30.0 ug/L 04/30/2010 Chloroform BMS (0.600) U 30.2 101 ( 80-124 ) 30.0 ug/L 04/30/2010 BMSD 29.9 100 1 (< 20 ) 30.0 ug/L 04/30/2010 Chloromethane BMS (0.620) U 31.2 104 ( 67-125 ) 30.0 ug/L 04/30/2010 BMSD 31.5 105 1 (< 20 ) 30.0 ug/L 04/30/2010 cis-1,2-Dichloroethene BMS (0.620) U 30.5 102 ( 80-125 ) 30.0 ug/L 04/30/2010 BMSD 30.2 101 1 (< 20 ) 30.0 ug/L 04/30/2010Matrix SGS Ref.# Printed Date/Time 

### 05/11/2010 12:34 Batch Method Date Original Prep 

### 1101763002 Billable Matrix Spike 1101763003 Billable Matrix Spike Dup.

1101763001 Water (Surface, Eff., Ground) VXX20600 Volatiles Extraction AFCEE 3.1 8260 (W) 04/30/2010

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy 

### cis-1,3-Dichloropropene BMS (0.300) U 34.3 114 ( 80-120 ) 30.0 ug/L 04/30/2010 BMSD 33.6 112 2 (< 20 ) 30.0 ug/L 04/30/2010 Dibromochloromethane BMS (0.300) U 32.3 108 ( 80-120 ) 30.0 ug/L 04/30/2010 BMSD 32.4 108 0 (< 20 ) 30.0 ug/L 04/30/2010 Dibromomethane BMS (0.620) U 31.1 104 ( 80-120 ) 30.0 ug/L 04/30/2010 BMSD 30.0 100 4 (< 20 ) 30.0 ug/L 04/30/2010 Dichlorodifluoromethane BMS (0.620) U 32.8 109 ( 62-153 ) 30.0 ug/L 04/30/2010 BMSD 32.9 110 0 (< 20 ) 30.0 ug/L 04/30/2010 Ethylbenzene BMS (0.620) U 31.2 104 ( 80-120 ) 30.0 ug/L 04/30/2010 BMSD 30.3 101 3 (< 20 ) 30.0 ug/L 04/30/2010 Hexachlorobutadiene BMS (0.620) U 28.5 95 ( 77-125 ) 30.0 ug/L 04/30/2010 BMSD 27.7 92 3 (< 20 ) 30.0 ug/L 04/30/2010 Isopropylbenzene (Cumene) BMS (0.620) U 29.8 99 ( 80-121 ) 30.0 ug/L 04/30/2010 BMSD 28.6 95 4 (< 20 ) 30.0 ug/L 04/30/2010 Methylene chloride BMS (2.00) U 32.2 107 ( 63-131 ) 30.0 ug/L 04/30/2010 BMSD 32.0 107 1 (< 20 ) 30.0 ug/L 04/30/2010 Methyl-t-butyl ether BMS (3.00) U 47.6 106 ( 80-120 ) 45.0 ug/L 04/30/2010 BMSD 46.9 104 2 (< 20 ) 45.0 ug/L 04/30/2010 Naphthalene BMS (1.24) U 31.3 104 ( 75-120 ) 30.0 ug/L 04/30/2010 BMSD 30.0 100 4 (< 20 ) 30.0 ug/L 04/30/2010 n-Butylbenzene BMS (0.620) U 32.2 107 ( 80-124 ) 30.0 ug/L 04/30/2010 BMSD 30.9 103 4 (< 20 ) 30.0 ug/L 04/30/2010 n-Propylbenzene BMS (0.620) U 35 117 ( 80-129 ) 30.0 ug/L 04/30/2010 BMSD 32.3 108 8 (< 20 ) 30.0 ug/L 04/30/2010 o-Xylene BMS (0.620) U 31 103 ( 80-120 ) 30.0 ug/L 04/30/2010 BMSD 30.6 102 2 (< 20 ) 30.0 ug/L 04/30/2010 P & M -Xylene BMS (1.24) U 61.6 103 ( 80-120 ) 60.0 ug/L 04/30/2010 BMSD 60.6 101 2 (< 20 ) 60.0 ug/L 04/30/2010 sec-Butylbenzene BMS (0.620) U 33.9 113 ( 80-120 ) 30.0 ug/L 04/30/2010 BMSD 31.8 106 6 (< 20 ) 30.0 ug/L 04/30/2010 Styrene BMS (0.620) U 30.4 101 ( 80-120 ) 30.0 ug/L 04/30/2010 BMSD 29.4 98 4 (< 20 ) 30.0 ug/L 04/30/2010 tert-Butylbenzene BMS (0.620) U 32.1 107 ( 80-122 ) 30.0 ug/L 04/30/2010 BMSD 30.7 102 5 (< 20 ) 30.0 ug/L 04/30/2010 Tetrachloroethene BMS (0.620) U 29.9 100 ( 79-122 ) 30.0 ug/L 04/30/2010 BMSD 29.3 98 2 (< 20 ) 30.0 ug/L 04/30/2010 Toluene BMS (0.620) U 29.7 99 ( 77-120 ) 30.0 ug/L 04/30/2010 BMSD 28.9 96 3 (< 20 ) 30.0 ug/L 04/30/2010 trans-1,2-Dichloroethene BMS (0.620) U 32.2 107 ( 79-132 ) 30.0 ug/L 04/30/2010 BMSD 32.1 107 1 (< 20 ) 30.0 ug/L 04/30/2010Matrix SGS Ref.# Printed Date/Time 

### 05/11/2010 12:34 Batch Method Date Original Prep 

### 1101763002 Billable Matrix Spike 1101763003 Billable Matrix Spike Dup.

1101763001 Water (Surface, Eff., Ground) VXX20600 Volatiles Extraction AFCEE 3.1 8260 (W) 04/30/2010

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy 

### trans-1,3-Dichloropropene BMS (0.620) U 34.8 116 ( 80-124 ) 30.0 ug/L 04/30/2010 BMSD 34.2 114 2 (< 20 ) 30.0 ug/L 04/30/2010 Trichloroethene BMS (0.620) U 30.7 102 ( 80-125 ) 30.0 ug/L 04/30/2010 BMSD 30.6 102 0 (< 20 ) 30.0 ug/L 04/30/2010 Trichlorofluoromethane BMS (0.620) U 35.8 119 ( 68-145 ) 30.0 ug/L 04/30/2010 BMSD 35.9 120 0 (< 20 ) 30.0 ug/L 04/30/2010 Vinyl chloride BMS (0.620) U 35.4 118 ( 72-145 ) 30.0 ug/L 04/30/2010 BMSD 34.8 116 2 (< 20 ) 30.0 ug/L 04/30/2010 Xylenes (total) BMS (1.88) U 92.6 103 ( 80-120 ) 90.0 ug/L 04/30/2010 BMSD 91.1 101 2 (< 20 ) 90.0 ug/L 04/30/2010 Surrogates 

### 1,2-Dichloroethane-D4 <surr> BMS 29.3 98 ( 73-120 ) 04/30/2010 BMSD 29.6 99 1 04/30/2010 4-Bromofluorobenzene <surr> BMS 30 100 ( 76-120 ) 04/30/2010 BMSD 29.4 98 2 04/30/2010 Toluene-d8 <surr> BMS 30.7 102 ( 80-120 ) 04/30/2010 BMSD 30.2 101 2 04/30/2010
Batch Method Instrument 

### VMS11191

SW8260B HP 5890 Series II MS3 VNA

Polynuclear Aromatics GC/MSMatrix SGS Ref.# Printed Date/Time 

### 05/11/2010 12:34 Batch Method Date Original Prep 

### 1101763002 Billable Matrix Spike 1101763003 Billable Matrix Spike Dup.

1101763001 Water (Surface, Eff., Ground) XXX22544 3520 Liquid/Liquid Ext for 8270 SIM 04/29/2010

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Polynuclear Aromatics GC/MS 

### 1-Methylnaphthalene BMS (0.0352) U .468 80 ( 42-92 ) 0.588 ug/L 05/08/2010 BMSD 0.455 77 3 (< 30 ) 0.588 ug/L 05/08/2010 2-Methylnaphthalene BMS (0.0352) U .426 73 ( 45-89 ) 0.588 ug/L 05/08/2010 BMSD 0.409 70 4 (< 30 ) 0.588 ug/L 05/08/2010 Acenaphthene BMS (0.0352) U .486 83 ( 45-93 ) 0.588 ug/L 05/08/2010 BMSD 0.464 79 5 (< 30 ) 0.588 ug/L 05/08/2010 Acenaphthylene BMS (0.0352) U .487 83 ( 50-101 ) 0.588 ug/L 05/08/2010 BMSD 0.478 81 2 (< 30 ) 0.588 ug/L 05/08/2010 Anthracene BMS (0.0352) U .56 95 ( 55-105 ) 0.588 ug/L 05/08/2010 BMSD 0.552 94 2 (< 30 ) 0.588 ug/L 05/08/2010 Benzo(a)Anthracene BMS (0.0352) U .56 95 ( 55-120 ) 0.588 ug/L 05/08/2010 BMSD 0.557 95 1 (< 30 ) 0.588 ug/L 05/08/2010 Benzo[a]pyrene BMS (0.0352) U .555 94 ( 57-110 ) 0.588 ug/L 05/08/2010 BMSD 0.556 95 0 (< 30 ) 0.588 ug/L 05/08/2010 Benzo[b]Fluoranthene BMS (0.0352) U .6 102 ( 45-120 ) 0.588 ug/L 05/08/2010 BMSD 0.606 103 1 (< 30 ) 0.588 ug/L 05/08/2010 Benzo[g,h,i]perylene BMS (0.0352) U .562 96 ( 49-116 ) 0.588 ug/L 05/08/2010 BMSD 0.566 96 1 (< 30 ) 0.588 ug/L 05/08/2010 Benzo[k]fluoranthene BMS (0.0352) U .556 95 ( 56-112 ) 0.588 ug/L 05/08/2010 BMSD 0.553 94 0 (< 30 ) 0.588 ug/L 05/08/2010 Chrysene BMS (0.0352) U .521 89 ( 56-109 ) 0.588 ug/L 05/08/2010 BMSD 0.519 88 0 (< 30 ) 0.588 ug/L 05/08/2010 Dibenzo[a,h]anthracene BMS (0.0352) U .609 103 ( 54-113 ) 0.588 ug/L 05/08/2010 BMSD 0.623 106 2 (< 30 ) 0.588 ug/L 05/08/2010 Fluoranthene BMS (0.0352) U .523 89 ( 58-109 ) 0.588 ug/L 05/08/2010 BMSD 0.515 88 2 (< 30 ) 0.588 ug/L 05/08/2010 Fluorene BMS (0.0352) U .519 88 ( 50-98 ) 0.588 ug/L 05/08/2010 BMSD 0.507 86 3 (< 30 ) 0.588 ug/L 05/08/2010 Indeno[1,2,3-c,d] pyrene BMS (0.0352) U .6 102 ( 55-111 ) 0.588 ug/L 05/08/2010 BMSD 0.609 103 1 (< 30 ) 0.588 ug/L 05/08/2010 Naphthalene BMS (0.0730) U .418 71 ( 44-89 ) 0.588 ug/L 05/08/2010 BMSD 0.403 69 4 (< 30 ) 0.588 ug/L 05/08/2010 Phenanthrene BMS (0.0352) U .527 90 ( 50-104 ) 0.588 ug/L 05/08/2010 BMSD 0.515 88 2 (< 30 ) 0.588 ug/L 05/08/2010 Pyrene BMS (0.0352) U .486 83 ( 56-105 ) 0.588 ug/L 05/08/2010 BMSD 0.482 82 1 (< 30 ) 0.588 ug/L 05/08/2010 Surrogates 

### Terphenyl-d14 <surr> BMS .508 86 ( 50-126 ) 05/08/2010 BMSD 0.494 84 3 05/08/2010Matrix SGS Ref.# Printed Date/Time 

### 05/11/2010 12:34 Batch Method Date Original Prep 

### 1101763002 Billable Matrix Spike 1101763003 Billable Matrix Spike Dup.

1101763001 Water (Surface, Eff., Ground) XXX22544 3520 Liquid/Liquid Ext for 8270 SIM 04/29/2010

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Polynuclear Aromatics GC/MS

Batch Method Instrument 

### XMS5395

8270D SIMS HP 6890 Series II MS2 SVOA

# Appendix B Monitoring Well Construction Logs

# GEOLOGIC BOREHOLE LOG

Location: 

### RHFSF Station Name: Location Type: Location Description: 

### RHMW04 Establishing Company: 

### TEC Inc. Drilling Foreman: 

### Tomas Fernandez Drilling Company: 

### Valley Well Drilling Geologist: 

### N. Griffin/S. MacMillan Ground Surface Elevation (ft): Datum: 

### MSL Drilling Sampling Method: Borehole Diameter (in): 

### 8 Total Depth (ft): Date Drilling Started: 

### 22 July 2005 Date Drilling Ended: 

### 26 July 2005 Monitoring Well

Remarks: Rock Coring west. access rd., S of Navy Firing Range



### 313.03

320.5

Page 1 of 2

# GEOLOGIC BOREHOLE LOG

Location: 

### RHFSF Station Name: Location Type: Location Description: 

### RHMW04 Establishing Company: 

### TEC Inc. Drilling Foreman: 

### Tomas Fernandez Drilling Company: 

### Valley Well Drilling Geologist: 

### N. Griffin/S. MacMillan Ground Surface Elevation (ft): Datum: 

### MSL Drilling Sampling Method: Borehole Diameter (in): 

### 8 Total Depth (ft): Date Drilling Started: 

### 22 July 2005 Date Drilling Ended: 

### 26 July 2005 Monitoring Well

Remarks: Rock Coring west. access rd., S of Navy Firing Range



### 313.03

320.5

Page 2 of 2