Quarterly Groundwater Monitoring Report – Outside 

(Non-Tunnel) Wells 

Red Hill Fuel Storage Facility 

Pearl Harbor, Oahu, Hawaii 

Latitude: 21o

22’15” N 

Longitude: 157o

53’33” W 

HDOH Facility ID No. 9-102271 

HDOH Release ID No. 99051, 010011, 020028 

May 2010 

Prepared by: 

TEC Inc. 

1003 Bishop St. Suite 1550 

Pauahi Tower 

Honolulu, Hawaii 96813 

Prepared for: 

Commander 

Navy Region Hawaii 

Environmental Department, Code N45 

850 Ticonderoga Street, Suite 110 

Pearl Harbor, Hawaii 96860-5101 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility May 2010 

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Table of Contents 

Table of Contents ............................................................................................................................. i

Executive Summary ......................................................................................................................... 1

1.0 Introduction.......................................................................................................................... 2

1.1 Project Objective .............................................................................................................. 2

1.2 Previous Reports .............................................................................................................. 2

1.3 Background ...................................................................................................................... 3

1.3.1 Site Description ......................................................................................................... 3

1.3.2 Facility Information .................................................................................................. 3

1.3.3 UST Information ....................................................................................................... 5

1.4 Regulatory Updates .......................................................................................................... 5

2.0 Sample Collection and Analyses .......................................................................................... 5

2.1 Monitoring Well Purging ................................................................................................. 6

2.2 Groundwater Sample Collection ...................................................................................... 6

2.3 Groundwater Sample Analyses ........................................................................................ 6

3.0 Groundwater Sample Analytical Results ............................................................................ 6

3.1 April 2010 Sample Analytical Results ............................................................................. 6

4.0 Summary and Conclusions ............................................................................................... 8

5.0 References .......................................................................................................................... 10

List of Tables 

Table 1 Monitoring Well Information ........................................................................................5 

Table 2 Analytical Results for Quarterly Groundwater Sampling (April 26, 2010) ...................7 

List of Figures 

Figure 1 Groundwater Monitoring Well Locations ......................................................................9 

List of Appendices 

Appendix A – Laboratory Analytical Reports 

Appendix B – Monitoring Well Construction Logs
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility May 2010 

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Executive Summary 

There are 18 active and 2 inactive, 12.5 million gallon, field-constructed underground storage 

tanks (USTs) located at the Red Hill Fuel Storage Facility (the Facility). Previous environmental 

site investigations indicated a release had occurred and contaminated the groundwater underlying 

the Facility. 

The United States (US) Navy implemented a groundwater monitoring program, which includes 

collecting groundwater samples quarterly from US Navy Well 2254-01 (RHMW2254-01) and 

four wells installed in the Facility lower access tunnel (RHMW01, RHMW02, RHMW03, and 

RHMW05). The US Navy Well 2254-01 is located approximately 3,000 feet downgradient from 

the Facility and provides approximately 24 percent of the potable water to the Pearl Harbor 

Water System (PHWS). The groundwater samples are analyzed for petroleum constituents and 

compared against State of Hawaii Department of Health (HDOH) Drinking Water 

Environmental Action Levels (EALs) (HDOH, 2008). 

In response to increasing concentrations of contaminants of potential concern in the groundwater 

monitoring wells within the facility (specifically RHMW02) during 2008, plans were made to 

conduct quarterly sampling at the following outside monitoring well locations: 

 RHMW04; 

 Oily Waste Disposal Facility monitoring well 01 (OWDFMW01); and 

 Halawa Deep Well 2253-03 (referred to as HDMW2253-03 in this report). 

This groundwater monitoring report presents the analytical results for samples collected on April 

26, 2010, at the three groundwater monitoring wells outside of the Facility. Laboratory 

analytical results indicate that Total Petroleum Hydrocarbons (TPH) as Diesel Range Organics 

(TPH-DRO) is present in groundwater from OWDFMW01. TPH-DRO in OWDFMW01 was 

detected at 288F micrograms per liter (μg/L) [F indicates that the compound was identified, but 

the concentration was above the laboratory method detection limit (MDL) and below the 

reporting limit (RL), therefore is considered an estimate]. The HDOH Drinking Water EAL for 

TPH-DRO is 100 μg/L. 

Although the TPH-DRO concentration at OWDFMW01 remains above the HDOH Drinking 

Water EAL, April 2010 results show a significant decrease in concentration for TPH-DRO at this 

location. The previous sampling event in January 2010 at OWDFMW01 had a TPH-DRO 

concentration of 1,490 μg/L. No other compounds were detected above the MDL at any other 

sampling location during April 2010. 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility May 2010 

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1.0 Introduction

This report presents the results of the fourth groundwater sampling event, conducted in April 

2010 at two groundwater monitoring wells (i.e., RHMW04 and OWDFMW01). The first, 

second, and third sampling events for OWDFMW01 and RHMW04 were conducted in August 

2009, October 2009, and January 2010, respectively. In addition, this report presents data from 

the third sampling event conducted in April 2010 at HDMW2253-03. The first and second 

sampling events at HDMW2253-03 were conducted in October 2009, and January 2010, 

respectively. An August 2009 sampling event for HDMW2253-03 was not conducted due to 

access issues. 

These three wells surround the Red Hill Fuel Storage Facility, Oahu, Hawaii (hereafter referred 

to as “the Facility”). This outside groundwater sampling and analysis is considered supplemental 

to the quarterly groundwater monitoring program conducted within the Facility. This 

supplemental sampling was conducted in response to increasing concentrations of contaminants 

of potential concern in a groundwater monitoring well within the Facility, specifically RHMW02 

during 2008. 

1.1 Project Objective 

This groundwater sampling project was performed to evaluate the presence of chemicals of 

potential concern in groundwater surrounding the Facility. The project was conducted to ensure 

the Navy remains in compliance with Hawaii Department of Health (HDOH) UST release 

response requirements. The groundwater sampling program followed the procedures described 

in Red Hill Bulk Fuel Storage Facility Groundwater Protection Plan [TEC Inc. (TEC), 2008 

updated in 2009], also referred to as “the Plan”. 

This groundwater sampling event was conducted by TEC under United States (US) Navy 

Contract Number N47408-04-D-8514, Task Order No. 54, Amendment/Modification No. 01. 

1.2 Previous Reports 

As indicated earlier, this outside well sampling supplements the quarterly groundwater 

monitoring of wells within the Facility, which began in 2005. The following groundwater 

monitoring reports were previously submitted to the HDOH, for groundwater monitoring wells 

within the Facility: 

1. Groundwater Sampling Report, First Quarter 2005 (submitted April 2005); 

2. Groundwater Sampling Report, Second Quarter 2005 (submitted August 2005); 

3. Groundwater Sampling Report, Third Quarter 2005 (submitted November 2005); 

4. Groundwater Sampling Report, Fourth Quarter 2005 (submitted February 2006); 

5. Groundwater Monitoring Results, July 2006 (submitted September 2006); 

6. Groundwater Monitoring Results, December 2006 (submitted January 2007); 

7. Groundwater Monitoring Results, March 2007 (submitted May 2007); 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility May 2010 

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8. Groundwater Monitoring Results, June 2007 (submitted August 2007); 

9. Groundwater Monitoring Results, September 2007 (submitted October 2007); 

10. Groundwater Monitoring Results, January 2008 (submitted March 2008); 

11. Groundwater Monitoring Results, April 2008 (submitted May 2008); 

12. Groundwater Monitoring Results, July 2008 (submitted October 2008); 

13. Groundwater Monitoring Results, October and December 2008 (submitted February 

2009); 

14. Groundwater Monitoring Results, February 2009 (submitted May 2009); 

15. Groundwater Monitoring Results, May 2009 (submitted July 2009); 

16. Groundwater Monitoring Results, July 2009 (submitted September 2009); 

17. Groundwater Monitoring Results, October 2009 (submitted December 2009); and 

18. Groundwater Monitoring Results, January, February, and March 2010 (submitted April 

2010). 

The following groundwater monitoring reports were previously submitted to the HDOH for 

groundwater monitoring wells outside the Facility: 

1. Groundwater Monitoring Results, August 2009 (submitted September 2009); 

2. Groundwater Monitoring Results, October 2009 (submitted December 2009); and 

3. Groundwater Monitoring Results, January 2010 (submitted April 2010). 

1.3 Background 

The following sections provide a description of the site and information on the Facility and USTs. 

1.3.1 Site Description 

The Facility is located in Red Hill, Oahu, Hawaii. Land adjacent to the north of the Facility is 

occupied by the Halawa Correctional Facility and private businesses. Land to the south and west 

of the Facility includes the Coast Guard Reservation. Moanalua Valley is located east of the 

Facility (Dawson, 2006). 

The Navy Public Works Department operates a potable water infiltration tunnel approximately 

1,550 feet from the Facility (Dawson, 2006). The US Navy Well 2254-01 is located 

approximately 3,000 feet west of the Facility and provides approximately 24% of the potable 

water to the Pearl Harbor Water System, which serves approximately 52,200 military consumers 

(TEC, 2008). 

1.3.2 Facility Information 

The Facility consists of 18 active and two inactive USTs operated by Navy Fleet and Industrial 

Supply Center (FISC) Pearl Harbor. Each UST has a capacity of 12.5 million gallons. The 

Facility is located approximately 100 feet above the basal aquifer (Dawson, 2006). 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility May 2010 

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In 2002, the US Navy installed a groundwater monitoring well (currently named RHMW01) into 

the basal aquifer, directly down-gradient from the Facility, within the lower access tunnel. 

Groundwater samples from this well indicated that petroleum from the Facility has migrated to 

the basal aquifer (AMEC, 2002). In 2005, the US Navy began quarterly monitoring of the 

aquifer to protect their down-gradient drinking water resource associated with the US Navy Well 

2254-01. 

By September 2005, the US Navy had installed two more groundwater monitoring wells 

(RHMW02 and RHMW03) within the Facility UST system, a groundwater monitoring well 

(RHMW04) north of the Facility adjacent to the US Navy Firing Range, and a groundwater 

monitoring well within the US Navy Well 2254-01 infiltration gallery (RHMW2254-01). Since 

2005, RHMW01, RHMW02, RHMW03, and RHMW2254-01 have been sampled quarterly for 

TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved lead. 

Due to increasing concentrations of contaminants of potential concern at the groundwater 

monitoring wells within the Facility (specifically RHMW02) during 2008, response measures 

were warranted. In April 2009, another groundwater monitoring well (RHMW05) was installed 

within the lower access tunnel between RHMW01 and RHMW2254-01. It was installed to 

identify the extent of contaminant migration before it reaches the infiltration gallery at 

RHMW2254-01. 

Additionally, plans were made to sample three monitoring wells surrounding and outside of the 

Facility, RHMW04, OWDFMW01, and HDMW2253-03. RHMW04 was installed to provide 

contaminant chemistry data for water moving through the basal aquifer beneath the Facility. 

OWDFMW01 (originally known as MW08) was installed into the basal aquifer in 1998 for a 

Phase II Remedial Investigation/ Feasibility Study for the Red Hill Oily Waste Disposal Facility 

(Earth Tech Inc., 2000). It is located geographically down-gradient of the USTs and US Navy 

Well 2254-01. HDMW2253-03 is controlled by the State of Hawaii Commission on Water 

Resource Management. It is located between the Facility and the municipal drinking water 

supply well run by the City and County of Honolulu Board of Water Supply (Halawa Shaft 

pumping station 2354-01). 

Table 1 summarizes basic groundwater monitoring well information, Figure 1 shows 

groundwater monitoring well locations, Appendix A provides the laboratory data, and Appendix 

B includes the well construction logs for RHMW04 and OWDFMW01. 
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Red Hill Fuel Storage Facility May 2010 

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Table 1. Monitoring Well Information 

Groundwater Well TOC Elevation 

(ft msl) 

DTW (ft) TD (ft) 

RHMW04 313.03 293 320 

OWDFMW01 138.94 120 142.8 

HDMW2253-03 225 210 1,575 

Notes: 

 DTW - Distance to water 

 TD - Total depth of well 

 TOC - Top of casing 

ft – Feet 

ft msl - Feet from mean sea level 

1.3.3 UST Information 

The USTs were constructed in the early 1940s. The tanks were constructed of steel and currently 

contain Jet Propulsion (JP)–5 fuel, JP-8, and F-76 (diesel marine fuel). Previously, several tanks 

stored Navy Special Fuel Oil, Navy Distillate, aviation gasoline, and motor gasoline. Each tank 

measures approximately 245 feet in height and 100 feet in diameter. The upper domes of the 

tanks lie at depths varying between approximately 100 feet and 200 feet below the existing 

ground surface (TEC, 2006). 

1.4 Regulatory Updates 

During the summer and fall of 2008, HDOH updated their EALs, which resulted in significant 

changes to the action levels associated with methylnaphthalenes. The drinking water toxicity 

EAL for these compounds was 240 g/L. This concentration presumed that methylnaphthalenes 

were non-carcinogenic. Evidence that they are human carcinogens has now been accepted by the 

US Environmental Protection Agency (USEPA). As a result, HDOH adopted more rigorous 

EALs of 4.7 g/L for 1-methylnaphthalene and 24 g/L for 2-methylnaphthalene, corresponding 

to a residential tap water scenario, and a 1 in a million cancer risk (HDOH, 2008). 

Also, the drinking water EAL for naphthalene was increased from 6.2 g/L to 17 g/L (HDOH, 

2008). Finally, the HDOH Drinking Water EAL for TPH-DRO was increased from 100 g/L to 

210 g/L, although the HDOH Groundwater Gross Contamination EAL for TPH-DRO remains 

100 g/L. 

2.0 Sample Collection and Analyses 

Field activities relating to groundwater sample collection were conducted on April 26, 2010. 

Groundwater samples were collected from three monitoring wells, RHMW04, OWDFMW01, 

and HDMW2253-03. Sampling and analysis were conducted according to Red Hill Bulk Fuel 

Storage Facility Groundwater Protection Plan (TEC, 2008). A total of six samples were 

collected as follows: 

 one environmental sample from RHMW04, OWDFMW01, and HDMW2253-03; 

 one duplicate sample from RHMW04 (sampled as RHMWA01 and reported as 

RHMW04D); and 

 one matrix spike and matrix spike duplicate from OWDFMW01. 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility May 2010 

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2.1 Monitoring Well Purging

RHMW04 and OWDFMW01 were purged prior to sampling. Well purging was considered 

complete when no less than three successive water quality parameter measurements had 

stabilized within approximately 10 percent. Field parameters were measured at regular intervals 

during well purging and included pH, temperature, specific conductivity, dissolved oxygen, and 

turbidity. Due to the well construction characteristics of HDMW2253-03, the well was not 

purged prior to sampling, but field parameters were recorded. Rather than purging, a grab 

sample was collected at a depth below the solid casing (which extends about 50 feet below the 

water table) and within the open-holed portion of the well. 

2.2 Groundwater Sample Collection 

Immediately following purging, RHMW04 was sampled directly from a dedicated bladder pump 

system, and OWDFMW01 was sampled using a disposable bailer. HDMW2253-03 was sampled 

using a disposable bailer designed to collect samples at desired depths. Samples were placed 

into sampling containers with appropriate preservatives [i.e., hydrochloric acid (HCl) for volatile 

organic analysis, nitric acid (HNO3) for dissolved lead]. Dissolved lead samples were filtered in 

the field and placed in preserved bottles. Sample containers were labeled with the date, sample 

identification number, type of analysis, and sampler’s name. The containers were placed on ice 

in sample coolers and transported under chain-of-custody procedures to the certified laboratory 

for analysis. 

2.3 Groundwater Sample Analyses 

Groundwater samples were analyzed by SGS Environmental Service, Inc. in Anchorage, Alaska 

for TPH-DRO and TPH-GRO by EPA Method 8015B, VOCs by EPA Method 8260B, PAHs by 

EPA Method 8270C SIM, and dissolved lead by EPA Method 6020. 

3.0 Groundwater Sample Analytical Results 

This section provides a summary of analytical results for groundwater samples collected from 

three monitoring wells, RHMW04, OWDFMW01, and HDMW2253-03. Duplicate sample 

results from monitoring well RHMW04 are reported in this document as RHMW04D. A 

summary of groundwater analytical results for TPH-DRO and TPH-GRO, VOCs, PAHs, and 

dissolved lead is included in Table 2. Complete analytical laboratory reports are provided in 

Appendix A. 

3.1 April 2010 Sample Analytical Results 

All groundwater samples were analyzed for TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved 

lead. The results for each groundwater monitoring well are discussed below. 

RHMW04

No potential chemical of concern was detected above the laboratory method detection limit 

(MDL) in RHMW04 (Table 2).
Table 2. Analytical Results for Quarterly Groundwater Monitoring Release Response Report (April 26, 2010)

Red Hill Fuel Storage Facility, Pearl Harbor, Hawaii

Result Q MDL RL Result Q MDL RL Result Q MDL RL Result Q 

TPH as DIESEL RANGE ORGANICS 210 100 ND U 176 471 288 F 176 471 ND U 174 465 ND U 

TPH as GASOLINE RANGE ORGANICS 100 100 ND U 30 100 ND U 30 100 ND U 30 100 ND U 

1-METHYLNAPHTHALENE 4.7 10 ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 

2-METHYLNAPHTHALENE 24 10 ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 

ACENAPHTHENE 370 20 ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U ACENAPHTHYLENE 240 2000 ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 

ANTHRACENE 1800 22 ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 

BENZO(a)ANTHRACENE 0.092 4.7 ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U BENZO(a)PYRENE 0.2 0.81 ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 

BENZO(b)FLUORANTHENE 0.092 0.75 ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 

BENZO(g,h,i)PERYLENE 1500 0.13 ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U BENZO(k)FLUORANTHENE 0.92 0.4 ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 

CHRYSENE 9.2 1 ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 

DIBENZ(a,h)ANTHRACENE 0.0092 0.52 ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 

FLUORANTHENE 1500 130 ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U FLUORENE 240 950 ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 

INDENO(1,2,3-c,d)PYRENE 0.092 0.095 ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 

NAPHTHALENE 17 21 ND U 0.036 0.116 ND U 0.0365 0.118 ND U 0.0365 0.118 ND U 

PHENANTHRENE 240 410 ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 

PYRENE 180 68 ND U 0.0174 0.0581 ND U 0.0176 0.0588 ND U 0.0176 0.0588 ND U 

1,1,1,2-TETRACHLOROETHANE 0.52 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 

1,1,1-TRICHLOROETHANE 200 970 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 1,1,2,2-TETRACHLOROETHANE 0.067 500 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 

1,1,2-TRICHLOROETHANE 5 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 

1,1-DICHLOROETHANE 2.4 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 

1,2,3-TRICHLOROPROPANE (TCP) 0.6 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 

1,2,4-TRICHLOROBENZENE 70 3000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 

1,2-DIBROMO-3-CHLOROPROPANE (DBCP) 0.04 10 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 

1,2-DIBROMOETHANE (EDB) 0.0065 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 

1,2-DICHLOROBENZENE 600 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 

1,2-DICHLOROETHANE 0.15 7000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 1,2-DICHLOROPROPANE 5 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 

1,3-DICHLOROBENZENE 180 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 1,4-DICHLOROBENZENE 75 5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 

ACETONE 22000 20000 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 

BENZENE 5 170 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND U 

April 26, 2010 April 26, 2010 A

UG/L

RHMW04

UG/L 

Method

HDOH Drinking Water 

EALs1

for Human Toxicity 

UG/L

HDOH Groundwater 

Gross Contamination 

EALs2

UG/L

Chemical

HDMW2253-03

UG/L

8015B (Petroleum)

8270C SIM 

(PAHs)

April 26, 2010

OWDFMW01

BROMODICHLOROMETHANE 0.22 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U BROMOFORM 100 510 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U BROMOMETHANE 8.7 50000 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3 ND U CARBON TETRACHLORIDE 5 520 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U CHLOROBENZENE 100 50 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U CHLOROETHANE 8600 16 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U CHLOROFORM 70 2400 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1 ND U CHLOROMETHANE 1.8 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U cis-1,2-DICHLOROETHYLENE 70 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U cis-1,3-DICHLOROPROPENE 0.43 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U DIBROMOCHLOROMETHANE 0.16 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U ETHYLBENZENE 700 30 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U HEXACHLOROBUTADIENE 0.86 6 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U M,P-XYLENE (SUM OF ISOMERS) 10000 20 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U METHYL ETHYL KETONE (2-BUTANONE) 7100 8400 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U METHYL ISOBUTYL KETONE (4-METHYL-2-PENTANONE) 2000 1300 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U METHYLENE CHLORIDE 4.8 9100 ND U 1 5 ND U 1 5 ND U 1 5 ND U NAPHTHALENE 17 21 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U STYRENE 100 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U TETRACHLOROETHYLENE(PCE) 5 170 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U TOLUENE 1000 40 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U trans-1,2-DICHLOROETHENE 100 260 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U TRICHLOROETHYLENE (TCE) 5 310 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U VINYL CHLORIDE 2 3400 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 

XYLENES, TOTAL 10000 20 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3 ND U 

6020 LEAD 15 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 

PAHs - Polynuclear aromatic hydrocarbons MDL - Method detection limit

VOCs - Volatile organic compounds RL - Reporting limit

UG/L - Micrograms per Liter TPH - Total petroleum hydrocarbons 

Q - Data qualifier ND - Indicates that the compound was not detected above the stated method detectio

U - Indicates that the compound was analyzed for but not detected at or above the stated limit

F - Indicates that the compound was identified but the concentration was above the MDL and below the RL

- Result exceeds one or both HDOH EALs

12

8260B 

(VOCs)

Final Drinking Water Action Levels for Human Toxicity, Table D-3a, Screening for Environmental Concerns at Sites with Contaminated Soil and Groundwater , HDOH, 2009Groundwater Gross Contamination Action Levels, Table G-1, Screening for Environmental Concerns at Sites with 

Contaminated Soil and Groundwater , HDOH, 2009

200

Page 7
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Red Hill Fuel Storage Facility May 2010 

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8 

OWDFMW01

TPH-DRO was detected at 288F μg/L [F indicates that the compound was identified at a 

concentration above the MDL, but below the reporting limit (RL), therefore is considered an 

estimate], exceeding the HDOH Groundwater Gross Contamination EAL and Drinking Water 

EAL (i.e., 100 μg/L and 210 μg/L, respectively). No other potential chemical of concern was 

detected above the laboratory MDLs in OWDFMW01 (Table 2). 

HDMW2253-03

No potential chemical of concern was detected above the laboratory MDLs in HDMW2253-03 

(Table 2). 

4.0 Summary and Conclusions 

Summary

At OWDFMW01, TPH-DRO was detected at 288F μg/L. This TPH-DRO concentration is 

above the HDOH Drinking Water EAL, and the HDOH Gross Contamination EAL. However, 

the April 2010 results show a significant decrease in concentration for TPH-DRO at this location. 

The previous sampling event conducted in January 2010 at OWDFMW01 had a TPH-DRO 

concentration of 1,490 μg/L. 

 

No other potential chemicals of concern were detected above the laboratory MDLs in 

OWDFMW01, HDMW2253-03, or RHMW04 during the April 2010 sampling event. 

Conclusions/Recommendations

No compounds were detected above the MDLs during the August 2009 sampling event at 

OWDFMW01 and RHMW04 (HDMW2253-03 was not sampled in August 2009 due to access 

issues); or during the October 2009 sampling event at OWDFMW01, RHMW04, or 

HDMW2253-03. 

Despite the detection of TPH-DRO at HDMW2253-03 during January 2010, TPH-DRO was not 

detected above the laboratory MDL during the April 2010 sampling event. Since two or more 

consecutive sampling events of increasing (or decreasing) concentrations of TPH-DRO at 

HDMW2253-03 have not occurred, no trend for TPH-DRO has been established at this location. 

TPH-DRO detected at OWDFMW01 during January 2010 significantly decreased in April 2010 

(i.e., from 1,490 μg/L in January 2010 to 288F μg/L in April 2010). 

 

TPH-DRO (detected at both HDMW2253-03 and OWDFMW01 in January 2010 and only at 

OWDFMW01 in April 2010) has been the only parameter detected above HDOH Drinking 

Water EALs during all four outside well sampling rounds. For the three wells surrounding the 

Facility (i.e., RHMW04, OWDFMW01, and HDMW2253-03), only one more sampling event 

remains tasked under this contract (i.e., to conduct the fourth and final round of sampling at 

HDMW2253-03 since it was not sampled in August 2009). Consequently, consideration should 

be given to conducting follow-on, periodic (perhaps semi-annually), targeted monitoring of these 

outside wells for TPH-DRO. 

Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility May 2010 

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5.0 References 

AMEC. Red Hill Bulk Fuel Storage Facility Investigation Report, Prepared for NAVFAC 

Pacific, August 2002. 

Dawson Group, Inc. Fourth Quarter 2005 Groundwater Sampling Report, Red Hill Fuel 

Storage Facility, Hawaii. February 2006. 

Earth Tech, Inc. Remedial Investigation Phase II, Volume I, Technical Report, Red Hill Oily 

Waste Disposal Facility, Halawa, Oahu, Hawaii. September 2000. 

Hawaii Administrative Rules, Title 11, Chapter 281, Subchapter 7. 

HDOH. Screening for Environmental Concerns at Sites with Contaminated Soil and 

Groundwater, Summary Lookup Tables. March 2009. 

HDOH. Use of May 2005 Environmental Action Levels (“EALs”) at Leaking Underground 

Storage Tank Sites. Memo. July 2005. 

HDOH. Evaluation of Environmental Hazards at Sites with Contaminated Soil and 

Groundwater. Summer 2008 (updated October 2008). 

TEC, Inc. Red Hill Bulk Fuel Storage Facility, Final – Addendum Planning Documents, Pearl 

Harbor, Hawaii. May 2006. 

TEC, Inc. Red Hill Bulk Fuel Storage Facility, Final Groundwater Protection Plan, Pearl 

Harbor, Hawaii. January 2008 revised in December 2009. 
Appendix A 

Laboratory Analytical Reports 
SGS Work Order:

Contents:

Cover Page

Case Narrative

Final Report Pages

Quality Control Summary Forms

Chain of Custody/Sample Receipt Forms

Project:

Client:

SGS North America Inc.

 Alaska Division

Level II Laboratory Data Report

Released by: 

Note:

Unless otherwise noted, all quality assurance/quality control criteria is in compliance with the standards set forth by the proper regulatory authority, the 

SGS Quality Assurance Program Plan, and the National Environmental Accreditation Conference.

3354-010 Red Hill BFSF

The Environmental Company, Inc. (TEC)

1101763

1 of 73
Case Narrative

THEENVC The Environmental Company, Inc. (TEC)

1101763 3354-010 Red Hill BFSF

Customer:

Project:

SGS North America Inc.

Refer to the sample receipt form for information on sample condition.

1101763002 BMS OWDFMW01-WG-04 MS

8260B - MS recovery for chloroethane does not meet QC criteria (biased high). This analyte was not detected 

above LOQ in the associated samples.

1101763003 BMSD OWDFMW01-WG-04 MSD

8260B - MSD recovery for chloroethane does not meet QC criteria (biased high). This analyte was not detected 

above LOQ in the associated samples.

958813 CCV VMS/11191]

8260B - CCV recovery for bromomethane, acetone, and carbon tetrachloride does not meet QC criteria (biased 

high). These analytes were not detected above LOQ in the associated samples.

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3354-010 Red Hill BFSF

Project Manager

jennifer.serna@sgs.com

Jennifer Serna

T: (808)528-1445 F:(808)528-0768

Attn: Rick Adkisson

1003 Bishop Street,

Pauahi Tower Suite 1550

Honolulu, HI 96813

Certification:

This data package is in compliance with the terms and conditions of the contract, both 

technically and for completeness, unless otherwise noted on the sample data sheet(s) and/or 

case narrative. This certification applies only to the tested parameters and the specific 

sample(s) received at the laboratory. If you have any questions regarding this report, or if we 

can be of further assistance, please contact your SGS Project Manager.

1101763

The Environmental Company, Inc. (TEC)

Workorder No.:

Client:

Project:

Laboratory Analytical Report

Contents (Bookmarked in PDF):

Cover Page

Glossary

Sample Summary Forms

Case Narrative

Sample Results Forms

Batch Summary Forms (by method)

Quality Control Summary Forms (by method)

Chain of Custody/Sample Receipt Forms

Attachments (if applicable)

SGS No rth Americ a Inc . En vir onmenta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com Member of SG S Group

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Enclosed are the analytical results associated with the above work order. All results are intended to be used in their entirety and SGS is not 

responsible for use of less than the complete report. If you have any questions regarding this report, or if we can be of any other assistance, please 

contact your SGS Project Manager at 907-562-2343. All work is provided under SGS general terms and conditions 

(<http://www.sgs.com/terms_and_conditions.htm>), unless other written agreements have been accepted by both parties.

SGS maintains a formal Quality Assurance/Quality Control (QA/QC) program. A copy of our Quality Assurance Plan (QAP), which outlines this 

program, is available at your request. The laboratory certification numbers are AK00971 (DW Chemistry & Microbiology) & UST-005 (CS) for 

ADEC and AK100001 for NELAP (RCRA methods: 1020A, 1311, 3010A, 3050B, 3520C, 3550C, 5030B, 5035B, 6010B, 6020, 7470A, 7471B, 

8021B, 8081B, 8082A, 8260B, 8270D, 8270D-SIM, 9040B, 9045C, 9056A, 9060A, AK101 and AK102/103). Except as specifically noted, all 

statements and data in this report are in conformance to the provisions set forth by the SGS QAP and, when applicable, the National Environmental 

Laboratory Accreditation Program and other regulatory authorities. The following descriptors or qualifiers may be found in your report:

* The analyte has exceeded allowable regulatory or control limits.

! Surrogate out of control limits.

B Indicates the analyte is found in a blank associated with the sample.

CCV Continuing Calibration Verification

CL Control Limit

D The analyte concentration is the result of a dilution.

DF Dilution Factor

DL Detection Limit (i.e., maximum method detection limit)

E The analyte result is above the calibrated range.

F Indicates value that is greater than or equal to the DL

GT Greater Than

ICV Initial Calibration Verification

J The quantitation is an estimation.

JL The analyte was positively identified, but the quantitation is a low estimation.

LCS(D) Laboratory Control Spike (Duplicate)

LOD Limit of Detection (i.e., 2xDL)

LOQ Limit of Quantitation (i.e., reporting or practical quantitation limit)

LT Less Than

M A matrix effect was present.

MB Method Blank

MS(D) Matrix Spike (Duplicate)

ND Indicates the analyte is not detected.

Q QC parameter out of acceptance range.

R Rejected

RL Reporting Limit

RPD Relative Percent Difference

U Indicates the analyte was analyzed for but not detected.

Note: Sample summaries which include a result for "Total Solids" have already been adjusted for moisture content.

All DRO/RRO analyses are integrated per SOP.

Print Date: 5/11/2010

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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SAMPLE SUMMARY

Client Name: The Environmental Company, Inc. (TEC)

Project Name: 3354-010 Red Hill BFSF

Workorder No.: 1101763

Analytical Methods

Method Description Analytical Method

8270 PAH SIM Semi-Vol GC/MS Liq/Liq ext. 8270D SIMS

AFCEE 3.1 8260 (W) SW8260B

Dissolved Metals by ICP-MS SW6020

DRO by 8015C (W) SW8015C

GRO (W) SW8015C

Print Date: 5/11/2010 12:34 pm

Sample ID Cross Reference

Lab Sample ID Client Sample ID

1101763001 OWDFMW01-WG-04

1101763002 OWDFMW01-WG-04 MS

1101763003 OWDFMW01-WG-04 MSD

1101763004 RHMW04-WG-04

1101763005 RHMWA01-WG-04

1101763006 HDMW2253-03-WG-04

1101763007 TB01-WG-04

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: OWDFMW01-WG-04

SGS Ref. #: 1101763001 Collection Date/Time: 04/26/10 08:35

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 0.310 ug/L 5 MMS6414 MXX22933

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6414

Analytical Method: SW6020

Analysis Date/Time: 05/04/10 11:31

Prep Batch: MXX22933

Prep Method: SW3010A

Prep Date/Time: 04/29/10 16:05 Container ID:1101763001-K

Dilution Factor: 5 Analyst: SCL

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: OWDFMW01-WG-04

SGS Ref. #: 1101763001 Collection Date/Time: 04/26/10 08:35

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 30.0 ug/L 1 VFC9914 VXX20617

4-Bromofluorobenzene <surr> 108 50-150 % 1 VFC9914 VXX20617

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9914

Analytical Method: SW8015C

Analysis Date/Time: 05/07/10 10:16

Prep Batch: VXX20617

Prep Method: SW5030B

Prep Date/Time: 05/07/10 08:48 Container ID:1101763001-A

Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: OWDFMW01-WG-04

SGS Ref. #: 1101763001 Collection Date/Time: 04/26/10 08:35

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 0.288J 0.471 0.176 mg/L 1 XFC9168 XXX22543

5a Androstane <surr> 88.5 50-150 % 1 XFC9168 XXX22543

Batch Information

Initial Prep Wt./Vol.: 850 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC9168

Analytical Method: SW8015C

Analysis Date/Time: 05/03/10 16:38

Prep Batch: XXX22543

Prep Method: SW3520C

Prep Date/Time: 04/29/10 08:15 Container ID:1101763001-I

Dilution Factor: 1 Analyst: LCE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: OWDFMW01-WG-04

SGS Ref. #: 1101763001 Collection Date/Time: 04/26/10 08:35

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11191 VXX20600

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11191 VXX20600

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

1-Chlorohexane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11191 VXX20600

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11191 VXX20600

Acetone 6.20 U 10.0 3.10 ug/L 1 VMS11191 VXX20600

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11191 VXX20600

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11191 VXX20600

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: OWDFMW01-WG-04

SGS Ref. #: 1101763001 Collection Date/Time: 04/26/10 08:35

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11191 VXX20600

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11191 VXX20600

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11191 VXX20600

Naphthalene 1.24 U 2.00 0.620 ug/L 1 VMS11191 VXX20600

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

o-Xylene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11191 VXX20600

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Xylenes (total) 1.88 U 3.00 0.940 ug/L 1 VMS11191 VXX20600

1,2-Dichloroethane-D4 <surr> 103 73-120 % 1 VMS11191 VXX20600

4-Bromofluorobenzene <surr> 107 76-120 % 1 VMS11191 VXX20600

Toluene-d8 <surr> 102 80-120 % 1 VMS11191 VXX20600

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: OWDFMW01-WG-04

SGS Ref. #: 1101763001 Collection Date/Time: 04/26/10 08:35

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11191

Analytical Method: SW8260B

Analysis Date/Time: 04/30/10 13:38

Prep Batch: VXX20600

Prep Method: SW5030B

Prep Date/Time: 04/30/10 08:55 Container ID:1101763001-D

Dilution Factor: 1 Analyst: JPI

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: OWDFMW01-WG-04

SGS Ref. #: 1101763001 Collection Date/Time: 04/26/10 08:35

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

DL DF

1-Methylnaphthalene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

2-Methylnaphthalene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Acenaphthene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Acenaphthylene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Anthracene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Benzo(a)Anthracene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Benzo[a]pyrene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Benzo[b]Fluoranthene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Benzo[g,h,i]perylene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Benzo[k]fluoranthene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Chrysene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Dibenzo[a,h]anthracene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Fluoranthene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Fluorene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Indeno[1,2,3-c,d] pyrene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Naphthalene 0.0730 U 0.118 0.0365 ug/L 1 XMS5395 XXX22544

Phenanthrene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Pyrene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Terphenyl-d14 <surr> 81.8 50-126 % 1 XMS5395 XXX22544

Batch Information

Initial Prep Wt./Vol.: 850 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5395

Analytical Method: 8270D SIMS

Analysis Date/Time: 05/08/10 09:39

Prep Batch: XXX22544

Prep Method: SW3520C

Prep Date/Time: 04/29/10 08:00 Container ID:1101763001-G

Dilution Factor: 1 Analyst: JDH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: RHMW04-WG-04

SGS Ref. #: 1101763004 Collection Date/Time: 04/26/10 13:10

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 0.310 ug/L 5 MMS6414 MXX22933

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6414

Analytical Method: SW6020

Analysis Date/Time: 05/04/10 11:53

Prep Batch: MXX22933

Prep Method: SW3010A

Prep Date/Time: 04/29/10 16:05 Container ID:1101763004-K

Dilution Factor: 5 Analyst: SCL

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: RHMW04-WG-04

SGS Ref. #: 1101763004 Collection Date/Time: 04/26/10 13:10

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 30.0 ug/L 1 VFC9914 VXX20617

4-Bromofluorobenzene <surr> 107 50-150 % 1 VFC9914 VXX20617

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9914

Analytical Method: SW8015C

Analysis Date/Time: 05/07/10 11:15

Prep Batch: VXX20617

Prep Method: SW5030B

Prep Date/Time: 05/07/10 08:48 Container ID:1101763004-A

Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: RHMW04-WG-04

SGS Ref. #: 1101763004 Collection Date/Time: 04/26/10 13:10

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 0.348 U 0.465 0.174 mg/L 1 XFC9168 XXX22543

5a Androstane <surr> 98 50-150 % 1 XFC9168 XXX22543

Batch Information

Initial Prep Wt./Vol.: 860 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC9168

Analytical Method: SW8015C

Analysis Date/Time: 05/03/10 17:41

Prep Batch: XXX22543

Prep Method: SW3520C

Prep Date/Time: 04/29/10 08:15 Container ID:1101763004-I

Dilution Factor: 1 Analyst: LCE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

15 of 73
The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: RHMW04-WG-04

SGS Ref. #: 1101763004 Collection Date/Time: 04/26/10 13:10

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11191 VXX20600

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11191 VXX20600

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

1-Chlorohexane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11191 VXX20600

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11191 VXX20600

Acetone 6.20 U 10.0 3.10 ug/L 1 VMS11191 VXX20600

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11191 VXX20600

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11191 VXX20600

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

16 of 73
The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: RHMW04-WG-04

SGS Ref. #: 1101763004 Collection Date/Time: 04/26/10 13:10

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11191 VXX20600

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11191 VXX20600

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11191 VXX20600

Naphthalene 1.24 U 2.00 0.620 ug/L 1 VMS11191 VXX20600

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

o-Xylene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11191 VXX20600

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Xylenes (total) 1.88 U 3.00 0.940 ug/L 1 VMS11191 VXX20600

1,2-Dichloroethane-D4 <surr> 98.8 73-120 % 1 VMS11191 VXX20600

4-Bromofluorobenzene <surr> 106 76-120 % 1 VMS11191 VXX20600

Toluene-d8 <surr> 99.7 80-120 % 1 VMS11191 VXX20600

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

17 of 73
The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: RHMW04-WG-04

SGS Ref. #: 1101763004 Collection Date/Time: 04/26/10 13:10

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11191

Analytical Method: SW8260B

Analysis Date/Time: 04/30/10 16:15

Prep Batch: VXX20600

Prep Method: SW5030B

Prep Date/Time: 04/30/10 08:55 Container ID:1101763004-D

Dilution Factor: 1 Analyst: JPI

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

18 of 73
The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: RHMW04-WG-04

SGS Ref. #: 1101763004 Collection Date/Time: 04/26/10 13:10

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

DL DF

1-Methylnaphthalene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

2-Methylnaphthalene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Acenaphthene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Acenaphthylene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Anthracene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Benzo(a)Anthracene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Benzo[a]pyrene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Benzo[b]Fluoranthene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Benzo[g,h,i]perylene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Benzo[k]fluoranthene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Chrysene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Dibenzo[a,h]anthracene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Fluoranthene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Fluorene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Indeno[1,2,3-c,d] pyrene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Naphthalene 0.0730 U 0.118 0.0365 ug/L 1 XMS5395 XXX22544

Phenanthrene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Pyrene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Terphenyl-d14 <surr> 83.3 50-126 % 1 XMS5395 XXX22544

Batch Information

Initial Prep Wt./Vol.: 850 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5395

Analytical Method: 8270D SIMS

Analysis Date/Time: 05/08/10 11:18

Prep Batch: XXX22544

Prep Method: SW3520C

Prep Date/Time: 04/29/10 08:00 Container ID:1101763004-G

Dilution Factor: 1 Analyst: JDH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

19 of 73
The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: RHMWA01-WG-04

SGS Ref. #: 1101763005 Collection Date/Time: 04/26/10 12:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 0.310 ug/L 5 MMS6414 MXX22933

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6414

Analytical Method: SW6020

Analysis Date/Time: 05/04/10 11:55

Prep Batch: MXX22933

Prep Method: SW3010A

Prep Date/Time: 04/29/10 16:05 Container ID:1101763005-K

Dilution Factor: 5 Analyst: SCL

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

20 of 73
The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: RHMWA01-WG-04

SGS Ref. #: 1101763005 Collection Date/Time: 04/26/10 12:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 30.0 ug/L 1 VFC9914 VXX20617

4-Bromofluorobenzene <surr> 108 50-150 % 1 VFC9914 VXX20617

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9914

Analytical Method: SW8015C

Analysis Date/Time: 05/07/10 11:34

Prep Batch: VXX20617

Prep Method: SW5030B

Prep Date/Time: 05/07/10 08:48 Container ID:1101763005-A

Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

21 of 73
The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: RHMWA01-WG-04

SGS Ref. #: 1101763005 Collection Date/Time: 04/26/10 12:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 0.352 U 0.471 0.176 mg/L 1 XFC9168 XXX22543

5a Androstane <surr> 98.8 50-150 % 1 XFC9168 XXX22543

Batch Information

Initial Prep Wt./Vol.: 850 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC9168

Analytical Method: SW8015C

Analysis Date/Time: 05/03/10 18:02

Prep Batch: XXX22543

Prep Method: SW3520C

Prep Date/Time: 04/29/10 08:15 Container ID:1101763005-I

Dilution Factor: 1 Analyst: LCE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

22 of 73
The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: RHMWA01-WG-04

SGS Ref. #: 1101763005 Collection Date/Time: 04/26/10 12:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11191 VXX20600

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11191 VXX20600

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

1-Chlorohexane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11191 VXX20600

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11191 VXX20600

Acetone 6.20 U 10.0 3.10 ug/L 1 VMS11191 VXX20600

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11191 VXX20600

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11191 VXX20600

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

23 of 73
The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: RHMWA01-WG-04

SGS Ref. #: 1101763005 Collection Date/Time: 04/26/10 12:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11191 VXX20600

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11191 VXX20600

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11191 VXX20600

Naphthalene 1.24 U 2.00 0.620 ug/L 1 VMS11191 VXX20600

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

o-Xylene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11191 VXX20600

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Xylenes (total) 1.88 U 3.00 0.940 ug/L 1 VMS11191 VXX20600

1,2-Dichloroethane-D4 <surr> 99.4 73-120 % 1 VMS11191 VXX20600

4-Bromofluorobenzene <surr> 108 76-120 % 1 VMS11191 VXX20600

Toluene-d8 <surr> 104 80-120 % 1 VMS11191 VXX20600

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

24 of 73
The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: RHMWA01-WG-04

SGS Ref. #: 1101763005 Collection Date/Time: 04/26/10 12:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11191

Analytical Method: SW8260B

Analysis Date/Time: 04/30/10 16:46

Prep Batch: VXX20600

Prep Method: SW5030B

Prep Date/Time: 04/30/10 08:55 Container ID:1101763005-D

Dilution Factor: 1 Analyst: JPI

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

25 of 73
The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: RHMWA01-WG-04

SGS Ref. #: 1101763005 Collection Date/Time: 04/26/10 12:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

DL DF

1-Methylnaphthalene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

2-Methylnaphthalene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Acenaphthene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Acenaphthylene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Anthracene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Benzo(a)Anthracene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Benzo[a]pyrene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Benzo[b]Fluoranthene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Benzo[g,h,i]perylene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Benzo[k]fluoranthene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Chrysene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Dibenzo[a,h]anthracene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Fluoranthene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Fluorene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Indeno[1,2,3-c,d] pyrene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Naphthalene 0.0730 U 0.118 0.0365 ug/L 1 XMS5395 XXX22544

Phenanthrene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Pyrene 0.0352 U 0.0588 0.0176 ug/L 1 XMS5395 XXX22544

Terphenyl-d14 <surr> 84.3 50-126 % 1 XMS5395 XXX22544

Batch Information

Initial Prep Wt./Vol.: 850 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5395

Analytical Method: 8270D SIMS

Analysis Date/Time: 05/08/10 11:51

Prep Batch: XXX22544

Prep Method: SW3520C

Prep Date/Time: 04/29/10 08:00 Container ID:1101763005-G

Dilution Factor: 1 Analyst: JDH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

26 of 73
The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: HDMW2253-03-WG-04

SGS Ref. #: 1101763006 Collection Date/Time: 04/26/10 09:40

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 0.310 ug/L 5 MMS6414 MXX22933

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6414

Analytical Method: SW6020

Analysis Date/Time: 05/04/10 11:57

Prep Batch: MXX22933

Prep Method: SW3010A

Prep Date/Time: 04/29/10 16:05 Container ID:1101763006-K

Dilution Factor: 5 Analyst: SCL

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

27 of 73
The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: HDMW2253-03-WG-04

SGS Ref. #: 1101763006 Collection Date/Time: 04/26/10 09:40

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 30.0 ug/L 1 VFC9914 VXX20617

4-Bromofluorobenzene <surr> 108 50-150 % 1 VFC9914 VXX20617

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9914

Analytical Method: SW8015C

Analysis Date/Time: 05/07/10 11:53

Prep Batch: VXX20617

Prep Method: SW5030B

Prep Date/Time: 05/07/10 08:48 Container ID:1101763006-A

Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

28 of 73
The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: HDMW2253-03-WG-04

SGS Ref. #: 1101763006 Collection Date/Time: 04/26/10 09:40

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 0.352 U 0.471 0.176 mg/L 1 XFC9168 XXX22543

5a Androstane <surr> 100 50-150 % 1 XFC9168 XXX22543

Batch Information

Initial Prep Wt./Vol.: 850 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC9168

Analytical Method: SW8015C

Analysis Date/Time: 05/03/10 18:23

Prep Batch: XXX22543

Prep Method: SW3520C

Prep Date/Time: 04/29/10 08:15 Container ID:1101763006-I

Dilution Factor: 1 Analyst: LCE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

29 of 73
The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: HDMW2253-03-WG-04

SGS Ref. #: 1101763006 Collection Date/Time: 04/26/10 09:40

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11191 VXX20600

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11191 VXX20600

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

1-Chlorohexane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11191 VXX20600

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11191 VXX20600

Acetone 6.20 U 10.0 3.10 ug/L 1 VMS11191 VXX20600

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11191 VXX20600

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11191 VXX20600

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

30 of 73
The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: HDMW2253-03-WG-04

SGS Ref. #: 1101763006 Collection Date/Time: 04/26/10 09:40

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11191 VXX20600

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11191 VXX20600

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11191 VXX20600

Naphthalene 1.24 U 2.00 0.620 ug/L 1 VMS11191 VXX20600

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

o-Xylene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11191 VXX20600

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Xylenes (total) 1.88 U 3.00 0.940 ug/L 1 VMS11191 VXX20600

1,2-Dichloroethane-D4 <surr> 98.5 73-120 % 1 VMS11191 VXX20600

4-Bromofluorobenzene <surr> 108 76-120 % 1 VMS11191 VXX20600

Toluene-d8 <surr> 102 80-120 % 1 VMS11191 VXX20600

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

31 of 73
The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: HDMW2253-03-WG-04

SGS Ref. #: 1101763006 Collection Date/Time: 04/26/10 09:40

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11191

Analytical Method: SW8260B

Analysis Date/Time: 04/30/10 17:18

Prep Batch: VXX20600

Prep Method: SW5030B

Prep Date/Time: 04/30/10 08:55 Container ID:1101763006-D

Dilution Factor: 1 Analyst: JPI

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

32 of 73
The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: HDMW2253-03-WG-04

SGS Ref. #: 1101763006 Collection Date/Time: 04/26/10 09:40

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

DL DF

1-Methylnaphthalene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5395 XXX22544

2-Methylnaphthalene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5395 XXX22544

Acenaphthene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5395 XXX22544

Acenaphthylene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5395 XXX22544

Anthracene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5395 XXX22544

Benzo(a)Anthracene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5395 XXX22544

Benzo[a]pyrene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5395 XXX22544

Benzo[b]Fluoranthene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5395 XXX22544

Benzo[g,h,i]perylene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5395 XXX22544

Benzo[k]fluoranthene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5395 XXX22544

Chrysene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5395 XXX22544

Dibenzo[a,h]anthracene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5395 XXX22544

Fluoranthene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5395 XXX22544

Fluorene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5395 XXX22544

Indeno[1,2,3-c,d] pyrene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5395 XXX22544

Naphthalene 0.0720 U 0.116 0.0360 ug/L 1 XMS5395 XXX22544

Phenanthrene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5395 XXX22544

Pyrene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5395 XXX22544

Terphenyl-d14 <surr> 75.9 50-126 % 1 XMS5395 XXX22544

Batch Information

Initial Prep Wt./Vol.: 860 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5395

Analytical Method: 8270D SIMS

Analysis Date/Time: 05/08/10 12:24

Prep Batch: XXX22544

Prep Method: SW3520C

Prep Date/Time: 04/29/10 08:00 Container ID:1101763006-G

Dilution Factor: 1 Analyst: JDH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

33 of 73
The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: TB01-WG-04

SGS Ref. #: 1101763007 Collection Date/Time: 04/26/10 08:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 30.0 ug/L 1 VFC9914 VXX20617

4-Bromofluorobenzene <surr> 108 50-150 % 1 VFC9914 VXX20617

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9914

Analytical Method: SW8015C

Analysis Date/Time: 05/07/10 12:12

Prep Batch: VXX20617

Prep Method: SW5030B

Prep Date/Time: 05/07/10 08:48 Container ID:1101763007-B

Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

34 of 73
The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: TB01-WG-04

SGS Ref. #: 1101763007 Collection Date/Time: 04/26/10 08:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11191 VXX20600

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11191 VXX20600

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

1-Chlorohexane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11191 VXX20600

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11191 VXX20600

Acetone 6.20 U 10.0 3.10 ug/L 1 VMS11191 VXX20600

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11191 VXX20600

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11191 VXX20600

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

35 of 73
The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: TB01-WG-04

SGS Ref. #: 1101763007 Collection Date/Time: 04/26/10 08:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11191 VXX20600

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11191 VXX20600

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11191 VXX20600

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11191 VXX20600

Naphthalene 1.24 U 2.00 0.620 ug/L 1 VMS11191 VXX20600

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

o-Xylene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11191 VXX20600

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11191 VXX20600

Xylenes (total) 1.88 U 3.00 0.940 ug/L 1 VMS11191 VXX20600

1,2-Dichloroethane-D4 <surr> 101 73-120 % 1 VMS11191 VXX20600

4-Bromofluorobenzene <surr> 106 76-120 % 1 VMS11191 VXX20600

Toluene-d8 <surr> 102 80-120 % 1 VMS11191 VXX20600

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

36 of 73
The Environmental Company, Inc. (TEC) Print Date: 5/11/2010 12:34 pm

Client Sample ID: TB01-WG-04

SGS Ref. #: 1101763007 Collection Date/Time: 04/26/10 08:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 04/28/10 11:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11191

Analytical Method: SW8260B

Analysis Date/Time: 04/30/10 12:35

Prep Batch: VXX20600

Prep Method: SW5030B

Prep Date/Time: 04/30/10 08:55 Container ID:1101763007-A

Dilution Factor: 1 Analyst: JPI

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

37 of 73
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Prep

958413 Method Blank

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX22543

SW3520C

04/29/2010

QC results affect the following production samples:

1101763001, 1101763004, 1101763005, 1101763006

Parameter Results LOQ/CL Units

Analysis

DL Date

Semivolatile Organic Fuels Department

Diesel Range Organics 0.300 U 0.400 0.150 mg/L 05/03/10

Surrogates 

5a Androstane <surr> 105 60-120 % 05/03/10

Instrument

Method

Batch XFC9168

SW8015C

HP 7890A FID SV E R

38 of 73
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Prep

958415 Method Blank

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX22544

SW3520C

04/29/2010

QC results affect the following production samples:

1101763001, 1101763004, 1101763005, 1101763006

Parameter Results LOQ/CL Units

Analysis

DL Date

Polynuclear Aromatics GC/MS

1-Methylnaphthalene 0.0300 U 0.0500 0.0150 ug/L 05/08/10

2-Methylnaphthalene 0.0300 U 0.0500 0.0150 ug/L 05/08/10

Acenaphthene 0.0300 U 0.0500 0.0150 ug/L 05/08/10

Acenaphthylene 0.0300 U 0.0500 0.0150 ug/L 05/08/10

Anthracene 0.0300 U 0.0500 0.0150 ug/L 05/08/10

Benzo(a)Anthracene 0.0300 U 0.0500 0.0150 ug/L 05/08/10

Benzo[a]pyrene 0.0300 U 0.0500 0.0150 ug/L 05/08/10

Benzo[b]Fluoranthene 0.0300 U 0.0500 0.0150 ug/L 05/08/10

Benzo[g,h,i]perylene 0.0300 U 0.0500 0.0150 ug/L 05/08/10

Benzo[k]fluoranthene 0.0300 U 0.0500 0.0150 ug/L 05/08/10

Chrysene 0.0300 U 0.0500 0.0150 ug/L 05/08/10

Dibenzo[a,h]anthracene 0.0300 U 0.0500 0.0150 ug/L 05/08/10

Fluoranthene 0.0300 U 0.0500 0.0150 ug/L 05/08/10

Fluorene 0.0300 U 0.0500 0.0150 ug/L 05/08/10

Indeno[1,2,3-c,d] pyrene 0.0300 U 0.0500 0.0150 ug/L 05/08/10

Naphthalene 0.0620 U 0.100 0.0310 ug/L 05/08/10

Phenanthrene 0.0300 U 0.0500 0.0150 ug/L 05/08/10

Pyrene 0.0300 U 0.0500 0.0150 ug/L 05/08/10

Surrogates 

Terphenyl-d14 <surr> 86.8 50-126 % 05/08/10

Instrument

Method

Batch XMS5395

8270D SIMS

HP 6890 Series II MS2 SVOA

39 of 73
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Prep

958689 Method Blank

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

MXX22933

SW3010A

04/29/2010

QC results affect the following production samples:

1101763001, 1101763004, 1101763005, 1101763006

Parameter Results LOQ/CL Units

Analysis

DL Date

Metals by ICP/MS

Lead 0.620 U 1.00 0.310 ug/L 05/04/10

Instrument

Method

Batch MMS6414

SW6020

Perkin Elmer Sciex ICP-MS P3

40 of 73
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Prep

958806 Method Blank

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20600

SW5030B

04/30/2010

QC results affect the following production samples:

1101763001, 1101763004, 1101763005, 1101763006, 1101763007

Parameter Results LOQ/CL Units

Analysis

DL Date

Volatile Gas Chromatography/Mass Spectroscopy

41 of 73
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Prep

958806 Method Blank

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20600

SW5030B

04/30/2010

Parameter Results LOQ/CL Units

Analysis

DL Date

Volatile Gas Chromatography/Mass Spectroscopy

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 04/30/10

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 04/30/10

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 04/30/10

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 04/30/10

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 04/30/10

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 04/30/10

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 04/30/10

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 04/30/10

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 04/30/10

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 04/30/10

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 04/30/10

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 04/30/10

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 04/30/10

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 04/30/10

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 04/30/10

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 04/30/10

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 04/30/10

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 04/30/10

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 04/30/10

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 04/30/10

1-Chlorohexane 0.620 U 1.00 0.310 ug/L 04/30/10

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 04/30/10

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 04/30/10

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 04/30/10

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 04/30/10

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 04/30/10

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 04/30/10

Acetone 6.20 U 10.0 3.10 ug/L 04/30/10

Benzene 0.240 U 0.400 0.120 ug/L 04/30/10

Bromobenzene 0.620 U 1.00 0.310 ug/L 04/30/10

Bromochloromethane 0.620 U 1.00 0.310 ug/L 04/30/10

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 04/30/10

Bromoform 0.620 U 1.00 0.310 ug/L 04/30/10

Bromomethane 1.88 U 3.00 0.940 ug/L 04/30/10

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 04/30/10

Chlorobenzene 0.300 U 0.500 0.150 ug/L 04/30/10

Chloroethane 0.620 U 1.00 0.310 ug/L 04/30/10

Chloroform 0.600 U 1.00 0.300 ug/L 04/30/10

Chloromethane 0.620 U 1.00 0.310 ug/L 04/30/10

42 of 73
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Prep

958806 Method Blank

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20600

SW5030B

04/30/2010

Parameter Results LOQ/CL Units

Analysis

DL Date

Volatile Gas Chromatography/Mass Spectroscopy

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 04/30/10

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 04/30/10

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 04/30/10

Dibromomethane 0.620 U 1.00 0.310 ug/L 04/30/10

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 04/30/10

Ethylbenzene 0.620 U 1.00 0.310 ug/L 04/30/10

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 04/30/10

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 04/30/10

Methylene chloride 2.00 U 5.00 1.00 ug/L 04/30/10

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 04/30/10

Naphthalene 1.24 U 2.00 0.620 ug/L 04/30/10

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 04/30/10

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 04/30/10

o-Xylene 0.620 U 1.00 0.310 ug/L 04/30/10

P & M -Xylene 1.24 U 2.00 0.620 ug/L 04/30/10

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 04/30/10

Styrene 0.620 U 1.00 0.310 ug/L 04/30/10

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 04/30/10

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 04/30/10

Toluene 0.620 U 1.00 0.310 ug/L 04/30/10

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 04/30/10

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 04/30/10

Trichloroethene 0.620 U 1.00 0.310 ug/L 04/30/10

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 04/30/10

Vinyl chloride 0.620 U 1.00 0.310 ug/L 04/30/10

Xylenes (total) 1.88 U 3.00 0.940 ug/L 04/30/10

Surrogates 

1,2-Dichloroethane-D4 <surr> 99.5 73-120 % 04/30/10

4-Bromofluorobenzene <surr> 109 76-120 % 04/30/10

Toluene-d8 <surr> 99 80-120 % 04/30/10

Instrument

Method

Batch VMS11191

SW8260B

HP 5890 Series II MS3 VNA

43 of 73
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Prep

959759 Method Blank

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20617

SW5030B

05/07/2010

QC results affect the following production samples:

1101763001, 1101763004, 1101763005, 1101763006, 1101763007

Parameter Results LOQ/CL Units

Analysis

DL Date

Volatile Fuels Department

Gasoline Range Organics 60.0 U 100 30.0 ug/L 05/07/10

Surrogates 

4-Bromofluorobenzene <surr> 107 50-150 % 05/07/10

Instrument

Method

Batch VFC9914

SW8015C

HP 5890 Series II PID+FID VCA

44 of 73
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Prep

958416 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX22544

SW3520C

04/29/2010

QC results affect the following production samples:

1101763001, 1101763004, 1101763005, 1101763006

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

1-Methylnaphthalene LCS 0.392 78 ( 42-92 ) 0.5 ug/L 05/08/2010

2-Methylnaphthalene LCS 0.353 71 ( 45-89 ) 0.5 ug/L 05/08/2010

Acenaphthene LCS 0.396 79 ( 45-93 ) 0.5 ug/L 05/08/2010

Acenaphthylene LCS 0.406 81 ( 50-101 ) 0.5 ug/L 05/08/2010

Anthracene LCS 0.435 87 ( 55-105 ) 0.5 ug/L 05/08/2010

Benzo(a)Anthracene LCS 0.448 90 ( 55-120 ) 0.5 ug/L 05/08/2010

Benzo[a]pyrene LCS 0.448 90 ( 57-110 ) 0.5 ug/L 05/08/2010

Benzo[b]Fluoranthene LCS 0.485 97 ( 45-120 ) 0.5 ug/L 05/08/2010

Benzo[g,h,i]perylene LCS 0.447 89 ( 49-116 ) 0.5 ug/L 05/08/2010

Benzo[k]fluoranthene LCS 0.456 91 ( 56-112 ) 0.5 ug/L 05/08/2010

Chrysene LCS 0.428 86 ( 56-109 ) 0.5 ug/L 05/08/2010

Dibenzo[a,h]anthracene LCS 0.470 94 ( 54-113 ) 0.5 ug/L 05/08/2010

Fluoranthene LCS 0.418 84 ( 58-109 ) 0.5 ug/L 05/08/2010

Fluorene LCS 0.423 85 ( 50-98 ) 0.5 ug/L 05/08/2010

Indeno[1,2,3-c,d] pyrene LCS 0.476 95 ( 55-111 ) 0.5 ug/L 05/08/2010

Naphthalene LCS 0.350 70 ( 44-89 ) 0.5 ug/L 05/08/2010

Phenanthrene LCS 0.415 83 ( 50-104 ) 0.5 ug/L 05/08/2010

Pyrene LCS 0.395 79 ( 56-105 ) 0.5 ug/L 05/08/2010

Surrogates 

Terphenyl-d14 <surr> LCS 87 ( 50-126 ) 05/08/2010

45 of 73
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Prep

958416 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX22544

SW3520C

04/29/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Batch

Method

Instrument

XMS5395

8270D SIMS

HP 6890 Series II MS2 SVOA

46 of 73
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Prep

958690 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

MXX22933

SW3010A

04/29/2010

QC results affect the following production samples:

1101763001, 1101763004, 1101763005, 1101763006

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Metals by ICP/MS

Lead LCS 975 98 ( 80-120 ) 1000 ug/L 05/04/2010

Batch

Method

Instrument

MMS6414

SW6020

Perkin Elmer Sciex ICP-MS P3

47 of 73
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Prep

958807 Lab Control Sample

958808 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20600

SW5030B

04/30/2010

QC results affect the following production samples:

1101763001, 1101763004, 1101763005, 1101763006, 1101763007

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

48 of 73
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Prep

958807 Lab Control Sample

958808 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20600

SW5030B

04/30/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

1,1,1,2-Tetrachloroethane LCS 29.9 100 ( 80-120 ) 30 ug/L 04/30/2010

LCSD 30.8 103 3 (< 20 ) 30 ug/L 04/30/2010

1,1,1-Trichloroethane LCS 31.4 105 ( 80-122 ) 30 ug/L 04/30/2010

LCSD 32.0 107 2 (< 20 ) 30 ug/L 04/30/2010

1,1,2,2-Tetrachloroethane LCS 31.0 103 ( 76-123 ) 30 ug/L 04/30/2010

LCSD 30.7 102 1 (< 20 ) 30 ug/L 04/30/2010

1,1,2-Trichloroethane LCS 29.5 98 ( 77-120 ) 30 ug/L 04/30/2010

LCSD 29.8 99 1 (< 20 ) 30 ug/L 04/30/2010

1,1-Dichloroethane LCS 35.1 117 ( 80-120 ) 30 ug/L 04/30/2010

LCSD 34.8 116 1 (< 20 ) 30 ug/L 04/30/2010

1,1-Dichloroethene LCS 32.6 109 ( 76-130 ) 30 ug/L 04/30/2010

LCSD 32.4 108 1 (< 20 ) 30 ug/L 04/30/2010

1,1-Dichloropropene LCS 30.9 103 ( 80-122 ) 30 ug/L 04/30/2010

LCSD 31.0 103 0 (< 20 ) 30 ug/L 04/30/2010

1,2,3-Trichlorobenzene LCS 29.6 99 ( 77-120 ) 30 ug/L 04/30/2010

LCSD 30.0 100 1 (< 20 ) 30 ug/L 04/30/2010

1,2,3-Trichloropropane LCS 30.8 103 ( 80-120 ) 30 ug/L 04/30/2010

LCSD 31.6 105 2 (< 20 ) 30 ug/L 04/30/2010

1,2,4-Trichlorobenzene LCS 28.6 95 ( 80-120 ) 30 ug/L 04/30/2010

LCSD 28.9 96 1 (< 20 ) 30 ug/L 04/30/2010

1,2,4-Trimethylbenzene LCS 31.2 104 ( 80-125 ) 30 ug/L 04/30/2010

LCSD 31.8 106 2 (< 20 ) 30 ug/L 04/30/2010

1,2-Dibromo-3-chloropropane LCS 32.6 109 ( 73-130 ) 30 ug/L 04/30/2010

LCSD 32.2 107 1 (< 20 ) 30 ug/L 04/30/2010

1,2-Dibromoethane LCS 27.8 93 ( 80-120 ) 30 ug/L 04/30/2010

LCSD 27.7 93 0 (< 20 ) 30 ug/L 04/30/2010

1,2-Dichlorobenzene LCS 29.0 97 ( 80-120 ) 30 ug/L 04/30/2010

LCSD 29.2 97 1 (< 20 ) 30 ug/L 04/30/2010

49 of 73
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Prep

958807 Lab Control Sample

958808 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20600

SW5030B

04/30/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

1,2-Dichloroethane LCS 30.0 100 ( 80-129 ) 30 ug/L 04/30/2010

LCSD 29.7 99 1 (< 20 ) 30 ug/L 04/30/2010

1,2-Dichloropropane LCS 30.3 101 ( 80-121 ) 30 ug/L 04/30/2010

LCSD 29.7 99 2 (< 20 ) 30 ug/L 04/30/2010

1,3,5-Trimethylbenzene LCS 32.1 107 ( 80-128 ) 30 ug/L 04/30/2010

LCSD 32.3 108 1 (< 20 ) 30 ug/L 04/30/2010

1,3-Dichlorobenzene LCS 28.6 95 ( 80-120 ) 30 ug/L 04/30/2010

LCSD 29.4 98 3 (< 20 ) 30 ug/L 04/30/2010

1,3-Dichloropropane LCS 29.5 98 ( 80-121 ) 30 ug/L 04/30/2010

LCSD 29.1 97 1 (< 20 ) 30 ug/L 04/30/2010

1,4-Dichlorobenzene LCS 28.8 96 ( 80-120 ) 30 ug/L 04/30/2010

LCSD 28.4 95 1 (< 20 ) 30 ug/L 04/30/2010

1-Chlorohexane LCS 45.2 100 ( 70-125 ) 45 ug/L 04/30/2010

LCSD 45.6 101 1 (< 20 ) 45 ug/L 04/30/2010

2,2-Dichloropropane LCS 31.5 105 ( 80-132 ) 30 ug/L 04/30/2010

LCSD 31.7 106 1 (< 20 ) 30 ug/L 04/30/2010

2-Butanone (MEK) LCS 93.4 104 ( 66-136 ) 90 ug/L 04/30/2010

LCSD 95.2 106 2 (< 20 ) 90 ug/L 04/30/2010

2-Chlorotoluene LCS 31.3 104 ( 80-125 ) 30 ug/L 04/30/2010

LCSD 31.7 106 1 (< 20 ) 30 ug/L 04/30/2010

4-Chlorotoluene LCS 31.9 106 ( 79-128 ) 30 ug/L 04/30/2010

LCSD 32.5 108 2 (< 20 ) 30 ug/L 04/30/2010

4-Isopropyltoluene LCS 30.9 103 ( 80-125 ) 30 ug/L 04/30/2010

LCSD 31.0 103 0 (< 20 ) 30 ug/L 04/30/2010

4-Methyl-2-pentanone (MIBK) LCS 94.6 105 ( 69-134 ) 90 ug/L 04/30/2010

LCSD 91.1 101 4 (< 20 ) 90 ug/L 04/30/2010

Acetone LCS 109 121 ( 50-135 ) 90 ug/L 04/30/2010

50 of 73
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Prep

958807 Lab Control Sample

958808 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20600

SW5030B

04/30/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

LCSD 103 115 5 (< 20 ) 90 ug/L 04/30/2010

Benzene LCS 28.6 95 ( 80-120 ) 30 ug/L 04/30/2010

LCSD 28.6 96 0 (< 20 ) 30 ug/L 04/30/2010

Bromobenzene LCS 28.9 96 ( 80-120 ) 30 ug/L 04/30/2010

LCSD 29.0 97 0 (< 20 ) 30 ug/L 04/30/2010

Bromochloromethane LCS 31.0 103 ( 77-129 ) 30 ug/L 04/30/2010

LCSD 30.6 102 1 (< 20 ) 30 ug/L 04/30/2010

Bromodichloromethane LCS 35.3 118 ( 80-120 ) 30 ug/L 04/30/2010

LCSD 35.4 118 0 (< 20 ) 30 ug/L 04/30/2010

Bromoform LCS 34.4 115 ( 80-120 ) 30 ug/L 04/30/2010

LCSD 34.8 116 1 (< 20 ) 30 ug/L 04/30/2010

Bromomethane LCS 36.8 123 ( 30-140 ) 30 ug/L 04/30/2010

LCSD 35.8 119 3 (< 20 ) 30 ug/L 04/30/2010

Carbon tetrachloride LCS 37.1 124 ( 80-126 ) 30 ug/L 04/30/2010

LCSD 37.2 124 0 (< 20 ) 30 ug/L 04/30/2010

Chlorobenzene LCS 28.5 95 ( 80-120 ) 30 ug/L 04/30/2010

LCSD 29.0 97 2 (< 20 ) 30 ug/L 04/30/2010

Chloroethane LCS 35.7 119 ( 67-133 ) 30 ug/L 04/30/2010

LCSD 36.1 120 1 (< 20 ) 30 ug/L 04/30/2010

Chloroform LCS 29.8 99 ( 80-124 ) 30 ug/L 04/30/2010

LCSD 30.1 100 1 (< 20 ) 30 ug/L 04/30/2010

Chloromethane LCS 29.1 97 ( 67-125 ) 30 ug/L 04/30/2010

LCSD 30.1 100 3 (< 20 ) 30 ug/L 04/30/2010

cis-1,2-Dichloroethene LCS 30.3 101 ( 80-125 ) 30 ug/L 04/30/2010

LCSD 30.0 100 1 (< 20 ) 30 ug/L 04/30/2010

cis-1,3-Dichloropropene LCS 34.1 114 ( 80-120 ) 30 ug/L 04/30/2010

LCSD 34.0 113 0 (< 20 ) 30 ug/L 04/30/2010

51 of 73
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Prep

958807 Lab Control Sample

958808 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20600

SW5030B

04/30/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Dibromochloromethane LCS 31.4 105 ( 80-120 ) 30 ug/L 04/30/2010

LCSD 31.2 104 1 (< 20 ) 30 ug/L 04/30/2010

Dibromomethane LCS 30.8 103 ( 80-120 ) 30 ug/L 04/30/2010

LCSD 29.8 99 3 (< 20 ) 30 ug/L 04/30/2010

Dichlorodifluoromethane LCS 31.4 105 ( 62-153 ) 30 ug/L 04/30/2010

LCSD 31.7 106 1 (< 20 ) 30 ug/L 04/30/2010

Ethylbenzene LCS 29.2 97 ( 80-120 ) 30 ug/L 04/30/2010

LCSD 29.7 99 2 (< 20 ) 30 ug/L 04/30/2010

Hexachlorobutadiene LCS 28.4 95 ( 77-125 ) 30 ug/L 04/30/2010

LCSD 28.2 94 1 (< 20 ) 30 ug/L 04/30/2010

Isopropylbenzene (Cumene) LCS 27.9 93 ( 80-121 ) 30 ug/L 04/30/2010

LCSD 27.7 92 1 (< 20 ) 30 ug/L 04/30/2010

Methylene chloride LCS 32.0 107 ( 63-131 ) 30 ug/L 04/30/2010

LCSD 31.5 105 2 (< 20 ) 30 ug/L 04/30/2010

Methyl-t-butyl ether LCS 49.3 110 ( 80-120 ) 45 ug/L 04/30/2010

LCSD 47.6 106 4 (< 20 ) 45 ug/L 04/30/2010

Naphthalene LCS 29.8 99 ( 75-120 ) 30 ug/L 04/30/2010

LCSD 29.8 99 0 (< 20 ) 30 ug/L 04/30/2010

n-Butylbenzene LCS 31.3 104 ( 80-124 ) 30 ug/L 04/30/2010

LCSD 31.6 105 1 (< 20 ) 30 ug/L 04/30/2010

n-Propylbenzene LCS 33.1 110 ( 80-129 ) 30 ug/L 04/30/2010

LCSD 33.2 111 0 (< 20 ) 30 ug/L 04/30/2010

o-Xylene LCS 29.5 98 ( 80-120 ) 30 ug/L 04/30/2010

LCSD 29.5 98 0 (< 20 ) 30 ug/L 04/30/2010

P & M -Xylene LCS 58.0 97 ( 80-120 ) 60 ug/L 04/30/2010

LCSD 58.7 98 1 (< 20 ) 60 ug/L 04/30/2010

sec-Butylbenzene LCS 32.1 107 ( 80-120 ) 30 ug/L 04/30/2010

LCSD 32.3 108 1 (< 20 ) 30 ug/L 04/30/2010

52 of 73
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Prep

958807 Lab Control Sample

958808 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20600

SW5030B

04/30/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Styrene LCS 29.7 99 ( 80-120 ) 30 ug/L 04/30/2010

LCSD 29.9 100 1 (< 20 ) 30 ug/L 04/30/2010

tert-Butylbenzene LCS 30.9 103 ( 80-122 ) 30 ug/L 04/30/2010

LCSD 30.9 103 0 (< 20 ) 30 ug/L 04/30/2010

Tetrachloroethene LCS 27.5 92 ( 79-122 ) 30 ug/L 04/30/2010

LCSD 28.4 95 3 (< 20 ) 30 ug/L 04/30/2010

Toluene LCS 27.6 92 ( 77-120 ) 30 ug/L 04/30/2010

LCSD 28.2 94 2 (< 20 ) 30 ug/L 04/30/2010

trans-1,2-Dichloroethene LCS 32.5 108 ( 79-132 ) 30 ug/L 04/30/2010

LCSD 32.5 108 0 (< 20 ) 30 ug/L 04/30/2010

trans-1,3-Dichloropropene LCS 33.5 112 ( 80-124 ) 30 ug/L 04/30/2010

LCSD 33.4 111 0 (< 20 ) 30 ug/L 04/30/2010

Trichloroethene LCS 30.1 100 ( 80-125 ) 30 ug/L 04/30/2010

LCSD 30.5 102 1 (< 20 ) 30 ug/L 04/30/2010

Trichlorofluoromethane LCS 33.4 111 ( 68-145 ) 30 ug/L 04/30/2010

LCSD 34.8 116 4 (< 20 ) 30 ug/L 04/30/2010

Vinyl chloride LCS 32.6 109 ( 72-145 ) 30 ug/L 04/30/2010

LCSD 32.6 109 0 (< 20 ) 30 ug/L 04/30/2010

Xylenes (total) LCS 87.4 97 ( 80-120 ) 90 ug/L 04/30/2010

LCSD 88.2 98 1 (< 20 ) 90 ug/L 04/30/2010

Surrogates 

1,2-Dichloroethane-D4 <surr> LCS 103 ( 73-120 ) 04/30/2010

LCSD 97 6 04/30/2010

4-Bromofluorobenzene <surr> LCS 100 ( 76-120 ) 04/30/2010

LCSD 99 1 04/30/2010

Toluene-d8 <surr> LCS 99 ( 80-120 ) 04/30/2010

LCSD 98 1 04/30/2010

53 of 73
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Prep

958807 Lab Control Sample

958808 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20600

SW5030B

04/30/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Batch

Method

Instrument

VMS11191

SW8260B

HP 5890 Series II MS3 VNA

54 of 73
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Prep

959066 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX22543

SW3520C

04/29/2010

QC results affect the following production samples:

1101763001, 1101763004, 1101763005, 1101763006

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Semivolatile Organic Fuels Department

Diesel Range Organics LCS 4.86 97 ( 75-125 ) 5 mg/L 05/03/2010

Surrogates 

5a Androstane <surr> LCS 98 ( 60-120 ) 05/03/2010

Batch

Method

Instrument

XFC9168

SW8015C

HP 7890A FID SV E R

55 of 73
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Prep

959760 Lab Control Sample

959761 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20617

SW5030B

05/07/2010

QC results affect the following production samples:

1101763001, 1101763004, 1101763005, 1101763006, 1101763007

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Fuels Department

Gasoline Range Organics LCS 220 110 ( 80-116 ) 200 ug/L 05/07/2010

LCSD 215 107 3 (< 20 ) 200 ug/L 05/07/2010

Surrogates 

4-Bromofluorobenzene <surr> LCS 110 ( 50-150 ) 05/07/2010

LCSD 112 2 05/07/2010

Batch

Method

Instrument

VFC9914

SW8015C

HP 5890 Series II PID+FID VCA

56 of 73
Matrix

SGS Ref.# Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Original

Prep

1101763002 Billable Matrix Spike

1101763003 Billable Matrix Spike Dup.

1101763001

Water (Surface, Eff., Ground)

MXX22933

3010 H20 Digest for Metals ICP-MS

04/29/2010

QC results affect the following production samples:

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Dissolved Metals by ICP/MS

Lead BMS (0.620) U 912 91 ( 80-120 ) 1000 ug/L 05/04/2010

BMSD 976 98 7 (< 15 ) 1000 ug/L 05/04/2010

Batch

Method

Instrument

MMS6414

SW6020

Perkin Elmer Sciex ICP-MS P3

Volatile Fuels Department

Gasoline Range Organics BMS (60.0) U 484 108 ( 80-116 ) 450 ug/L 05/07/2010

BMSD 467 104 4 (< 20 ) 450 ug/L 05/07/2010

Surrogates 

4-Bromofluorobenzene <surr> BMS 55.4 111 ( 50-150 ) 05/07/2010

BMSD 54.8 110 1 05/07/2010

Batch

Method

Instrument

VFC9914

SW8015C

HP 5890 Series II PID+FID VCA

Semivolatile Organic Fuels Department

Diesel Range Organics BMS 0.288J 5.59 90 ( 75-125 ) 5.88 mg/L 05/03/2010

BMSD 6.17 100 10 (< 30 ) 5.88 mg/L 05/03/2010

Surrogates 

5a Androstane <surr> BMS .109 92 ( 50-150 ) 05/03/2010

BMSD 0.120 102 10 05/03/2010

Batch

Method

Instrument

XFC9168

SW8015C

HP 7890A FID SV E R

Volatile Gas Chromatography/Mass Spectroscopy

57 of 73
Matrix

SGS Ref.# Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Original

Prep

1101763002 Billable Matrix Spike

1101763003 Billable Matrix Spike Dup.

1101763001

Water (Surface, Eff., Ground)

VXX20600

Volatiles Extraction AFCEE 3.1 8260 (

04/30/2010

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

1,1,1,2-Tetrachloroethane BMS (0.300) U 32 107 ( 80-120 ) 30.0 ug/L 04/30/2010

BMSD 31.0 103 3 (< 20 ) 30.0 ug/L 04/30/2010

1,1,1-Trichloroethane BMS (0.620) U 31.7 106 ( 80-122 ) 30.0 ug/L 04/30/2010

BMSD 31.4 105 1 (< 20 ) 30.0 ug/L 04/30/2010

1,1,2,2-Tetrachloroethane BMS (0.300) U 31.5 105 ( 76-123 ) 30.0 ug/L 04/30/2010

BMSD 30.4 101 4 (< 20 ) 30.0 ug/L 04/30/2010

1,1,2-Trichloroethane BMS (0.620) U 30.9 103 ( 77-120 ) 30.0 ug/L 04/30/2010

BMSD 31.4 105 1 (< 20 ) 30.0 ug/L 04/30/2010

1,1-Dichloroethane BMS (0.620) U 35.4 118 ( 80-120 ) 30.0 ug/L 04/30/2010

BMSD 34.9 116 1 (< 20 ) 30.0 ug/L 04/30/2010

1,1-Dichloroethene BMS (0.620) U 32.7 109 ( 76-130 ) 30.0 ug/L 04/30/2010

BMSD 32.6 109 1 (< 20 ) 30.0 ug/L 04/30/2010

1,1-Dichloropropene BMS (0.620) U 30.9 103 ( 80-122 ) 30.0 ug/L 04/30/2010

BMSD 31.4 105 2 (< 20 ) 30.0 ug/L 04/30/2010

1,2,3-Trichlorobenzene BMS (0.620) U 30.4 101 ( 77-120 ) 30.0 ug/L 04/30/2010

BMSD 29.6 99 3 (< 20 ) 30.0 ug/L 04/30/2010

1,2,3-Trichloropropane BMS (0.620) U 31.7 106 ( 80-120 ) 30.0 ug/L 04/30/2010

BMSD 30.7 102 3 (< 20 ) 30.0 ug/L 04/30/2010

1,2,4-Trichlorobenzene BMS (0.620) U 30.1 100 ( 80-120 ) 30.0 ug/L 04/30/2010

BMSD 28.8 96 5 (< 20 ) 30.0 ug/L 04/30/2010

1,2,4-Trimethylbenzene BMS (0.620) U 32.5 108 ( 80-125 ) 30.0 ug/L 04/30/2010

BMSD 30.8 103 6 (< 20 ) 30.0 ug/L 04/30/2010

1,2-Dibromo-3-chloropropane BMS (1.24) U 32 107 ( 73-130 ) 30.0 ug/L 04/30/2010

BMSD 31.8 106 1 (< 20 ) 30.0 ug/L 04/30/2010

1,2-Dibromoethane BMS (0.620) U 28.7 96 ( 80-120 ) 30.0 ug/L 04/30/2010

BMSD 27.6 92 4 (< 20 ) 30.0 ug/L 04/30/2010

1,2-Dichlorobenzene BMS (0.620) U 30 100 ( 80-120 ) 30.0 ug/L 04/30/2010

BMSD 28.9 96 4 (< 20 ) 30.0 ug/L 04/30/2010

1,2-Dichloroethane BMS (0.300) U 29.3 98 ( 80-129 ) 30.0 ug/L 04/30/2010

BMSD 29.6 99 1 (< 20 ) 30.0 ug/L 04/30/2010

1,2-Dichloropropane BMS (0.620) U 30.8 103 ( 80-121 ) 30.0 ug/L 04/30/2010

BMSD 29.7 99 4 (< 20 ) 30.0 ug/L 04/30/2010

1,3,5-Trimethylbenzene BMS (0.620) U 33.2 111 ( 80-128 ) 30.0 ug/L 04/30/2010

BMSD 31.7 106 5 (< 20 ) 30.0 ug/L 04/30/2010

1,3-Dichlorobenzene BMS (0.620) U 30.3 101 ( 80-120 ) 30.0 ug/L 04/30/2010

BMSD 29.5 98 3 (< 20 ) 30.0 ug/L 04/30/2010

1,3-Dichloropropane BMS (0.240) U 30.5 102 ( 80-121 ) 30.0 ug/L 04/30/2010

BMSD 30.3 101 0 (< 20 ) 30.0 ug/L 04/30/2010

1,4-Dichlorobenzene BMS (0.300) U 29.6 99 ( 80-120 ) 30.0 ug/L 04/30/2010

BMSD 28.1 94 5 (< 20 ) 30.0 ug/L 04/30/2010

58 of 73
Matrix

SGS Ref.# Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Original

Prep

1101763002 Billable Matrix Spike

1101763003 Billable Matrix Spike Dup.

1101763001

Water (Surface, Eff., Ground)

VXX20600

Volatiles Extraction AFCEE 3.1 8260 (

04/30/2010

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

1-Chlorohexane BMS (0.620) U 47 105 ( 70-125 ) 45.0 ug/L 04/30/2010

BMSD 46.8 104 0 (< 20 ) 45.0 ug/L 04/30/2010

2,2-Dichloropropane BMS (0.620) U 28.9 96 ( 80-132 ) 30.0 ug/L 04/30/2010

BMSD 29.2 97 1 (< 20 ) 30.0 ug/L 04/30/2010

2-Butanone (MEK) BMS (6.20) U 94.7 105 ( 66-136 ) 90.0 ug/L 04/30/2010

BMSD 92.7 103 2 (< 20 ) 90.0 ug/L 04/30/2010

2-Chlorotoluene BMS (0.620) U 32.5 108 ( 80-125 ) 30.0 ug/L 04/30/2010

BMSD 31.2 104 4 (< 20 ) 30.0 ug/L 04/30/2010

4-Chlorotoluene BMS (0.620) U 33.4 111 ( 79-128 ) 30.0 ug/L 04/30/2010

BMSD 31.8 106 5 (< 20 ) 30.0 ug/L 04/30/2010

4-Isopropyltoluene BMS (0.620) U 32.4 108 ( 80-125 ) 30.0 ug/L 04/30/2010

BMSD 30.6 102 6 (< 20 ) 30.0 ug/L 04/30/2010

4-Methyl-2-pentanone (MIBK) BMS (6.20) U 93.7 104 ( 69-134 ) 90.0 ug/L 04/30/2010

BMSD 92.0 102 2 (< 20 ) 90.0 ug/L 04/30/2010

Acetone BMS (6.20) U 109 121 ( 50-135 ) 90.0 ug/L 04/30/2010

BMSD 107 119 2 (< 20 ) 90.0 ug/L 04/30/2010

Benzene BMS (0.240) U 29.1 97 ( 80-120 ) 30.0 ug/L 04/30/2010

BMSD 28.2 94 3 (< 20 ) 30.0 ug/L 04/30/2010

Bromobenzene BMS (0.620) U 29.4 98 ( 80-120 ) 30.0 ug/L 04/30/2010

BMSD 28.5 95 3 (< 20 ) 30.0 ug/L 04/30/2010

Bromochloromethane BMS (0.620) U 30.6 102 ( 77-129 ) 30.0 ug/L 04/30/2010

BMSD 30.6 102 0 (< 20 ) 30.0 ug/L 04/30/2010

Bromodichloromethane BMS (0.300) U 35 117 ( 80-120 ) 30.0 ug/L 04/30/2010

BMSD 34.9 116 0 (< 20 ) 30.0 ug/L 04/30/2010

Bromoform BMS (0.620) U 34.6 115 ( 80-120 ) 30.0 ug/L 04/30/2010

BMSD 34.9 116 1 (< 20 ) 30.0 ug/L 04/30/2010

Bromomethane BMS (1.88) U 38.5 128 ( 30-140 ) 30.0 ug/L 04/30/2010

BMSD 37.8 126 2 (< 20 ) 30.0 ug/L 04/30/2010

Carbon tetrachloride BMS (0.620) U 36.3 121 ( 80-126 ) 30.0 ug/L 04/30/2010

BMSD 37.2 124 2 (< 20 ) 30.0 ug/L 04/30/2010

Chlorobenzene BMS (0.300) U 30.3 101 ( 80-120 ) 30.0 ug/L 04/30/2010

BMSD 30.0 100 1 (< 20 ) 30.0 ug/L 04/30/2010

Chloroethane BMS (0.620) U 50.4 168* ( 67-133 ) 30.0 ug/L 04/30/2010

BMSD 45.0 150* 12 (< 20 ) 30.0 ug/L 04/30/2010

Chloroform BMS (0.600) U 30.2 101 ( 80-124 ) 30.0 ug/L 04/30/2010

BMSD 29.9 100 1 (< 20 ) 30.0 ug/L 04/30/2010

Chloromethane BMS (0.620) U 31.2 104 ( 67-125 ) 30.0 ug/L 04/30/2010

BMSD 31.5 105 1 (< 20 ) 30.0 ug/L 04/30/2010

cis-1,2-Dichloroethene BMS (0.620) U 30.5 102 ( 80-125 ) 30.0 ug/L 04/30/2010

BMSD 30.2 101 1 (< 20 ) 30.0 ug/L 04/30/2010

59 of 73
Matrix

SGS Ref.# Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Original

Prep

1101763002 Billable Matrix Spike

1101763003 Billable Matrix Spike Dup.

1101763001

Water (Surface, Eff., Ground)

VXX20600

Volatiles Extraction AFCEE 3.1 8260 (

04/30/2010

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

cis-1,3-Dichloropropene BMS (0.300) U 34.3 114 ( 80-120 ) 30.0 ug/L 04/30/2010

BMSD 33.6 112 2 (< 20 ) 30.0 ug/L 04/30/2010

Dibromochloromethane BMS (0.300) U 32.3 108 ( 80-120 ) 30.0 ug/L 04/30/2010

BMSD 32.4 108 0 (< 20 ) 30.0 ug/L 04/30/2010

Dibromomethane BMS (0.620) U 31.1 104 ( 80-120 ) 30.0 ug/L 04/30/2010

BMSD 30.0 100 4 (< 20 ) 30.0 ug/L 04/30/2010

Dichlorodifluoromethane BMS (0.620) U 32.8 109 ( 62-153 ) 30.0 ug/L 04/30/2010

BMSD 32.9 110 0 (< 20 ) 30.0 ug/L 04/30/2010

Ethylbenzene BMS (0.620) U 31.2 104 ( 80-120 ) 30.0 ug/L 04/30/2010

BMSD 30.3 101 3 (< 20 ) 30.0 ug/L 04/30/2010

Hexachlorobutadiene BMS (0.620) U 28.5 95 ( 77-125 ) 30.0 ug/L 04/30/2010

BMSD 27.7 92 3 (< 20 ) 30.0 ug/L 04/30/2010

Isopropylbenzene (Cumene) BMS (0.620) U 29.8 99 ( 80-121 ) 30.0 ug/L 04/30/2010

BMSD 28.6 95 4 (< 20 ) 30.0 ug/L 04/30/2010

Methylene chloride BMS (2.00) U 32.2 107 ( 63-131 ) 30.0 ug/L 04/30/2010

BMSD 32.0 107 1 (< 20 ) 30.0 ug/L 04/30/2010

Methyl-t-butyl ether BMS (3.00) U 47.6 106 ( 80-120 ) 45.0 ug/L 04/30/2010

BMSD 46.9 104 2 (< 20 ) 45.0 ug/L 04/30/2010

Naphthalene BMS (1.24) U 31.3 104 ( 75-120 ) 30.0 ug/L 04/30/2010

BMSD 30.0 100 4 (< 20 ) 30.0 ug/L 04/30/2010

n-Butylbenzene BMS (0.620) U 32.2 107 ( 80-124 ) 30.0 ug/L 04/30/2010

BMSD 30.9 103 4 (< 20 ) 30.0 ug/L 04/30/2010

n-Propylbenzene BMS (0.620) U 35 117 ( 80-129 ) 30.0 ug/L 04/30/2010

BMSD 32.3 108 8 (< 20 ) 30.0 ug/L 04/30/2010

o-Xylene BMS (0.620) U 31 103 ( 80-120 ) 30.0 ug/L 04/30/2010

BMSD 30.6 102 2 (< 20 ) 30.0 ug/L 04/30/2010

P & M -Xylene BMS (1.24) U 61.6 103 ( 80-120 ) 60.0 ug/L 04/30/2010

BMSD 60.6 101 2 (< 20 ) 60.0 ug/L 04/30/2010

sec-Butylbenzene BMS (0.620) U 33.9 113 ( 80-120 ) 30.0 ug/L 04/30/2010

BMSD 31.8 106 6 (< 20 ) 30.0 ug/L 04/30/2010

Styrene BMS (0.620) U 30.4 101 ( 80-120 ) 30.0 ug/L 04/30/2010

BMSD 29.4 98 4 (< 20 ) 30.0 ug/L 04/30/2010

tert-Butylbenzene BMS (0.620) U 32.1 107 ( 80-122 ) 30.0 ug/L 04/30/2010

BMSD 30.7 102 5 (< 20 ) 30.0 ug/L 04/30/2010

Tetrachloroethene BMS (0.620) U 29.9 100 ( 79-122 ) 30.0 ug/L 04/30/2010

BMSD 29.3 98 2 (< 20 ) 30.0 ug/L 04/30/2010

Toluene BMS (0.620) U 29.7 99 ( 77-120 ) 30.0 ug/L 04/30/2010

BMSD 28.9 96 3 (< 20 ) 30.0 ug/L 04/30/2010

trans-1,2-Dichloroethene BMS (0.620) U 32.2 107 ( 79-132 ) 30.0 ug/L 04/30/2010

BMSD 32.1 107 1 (< 20 ) 30.0 ug/L 04/30/2010

60 of 73
Matrix

SGS Ref.# Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Original

Prep

1101763002 Billable Matrix Spike

1101763003 Billable Matrix Spike Dup.

1101763001

Water (Surface, Eff., Ground)

VXX20600

Volatiles Extraction AFCEE 3.1 8260 (

04/30/2010

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

trans-1,3-Dichloropropene BMS (0.620) U 34.8 116 ( 80-124 ) 30.0 ug/L 04/30/2010

BMSD 34.2 114 2 (< 20 ) 30.0 ug/L 04/30/2010

Trichloroethene BMS (0.620) U 30.7 102 ( 80-125 ) 30.0 ug/L 04/30/2010

BMSD 30.6 102 0 (< 20 ) 30.0 ug/L 04/30/2010

Trichlorofluoromethane BMS (0.620) U 35.8 119 ( 68-145 ) 30.0 ug/L 04/30/2010

BMSD 35.9 120 0 (< 20 ) 30.0 ug/L 04/30/2010

Vinyl chloride BMS (0.620) U 35.4 118 ( 72-145 ) 30.0 ug/L 04/30/2010

BMSD 34.8 116 2 (< 20 ) 30.0 ug/L 04/30/2010

Xylenes (total) BMS (1.88) U 92.6 103 ( 80-120 ) 90.0 ug/L 04/30/2010

BMSD 91.1 101 2 (< 20 ) 90.0 ug/L 04/30/2010

Surrogates 

1,2-Dichloroethane-D4 <surr> BMS 29.3 98 ( 73-120 ) 04/30/2010

BMSD 29.6 99 1 04/30/2010

4-Bromofluorobenzene <surr> BMS 30 100 ( 76-120 ) 04/30/2010

BMSD 29.4 98 2 04/30/2010

Toluene-d8 <surr> BMS 30.7 102 ( 80-120 ) 04/30/2010

BMSD 30.2 101 2 04/30/2010

Batch

Method

Instrument

VMS11191

SW8260B

HP 5890 Series II MS3 VNA

Polynuclear Aromatics GC/MS

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Matrix

SGS Ref.# Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Original

Prep

1101763002 Billable Matrix Spike

1101763003 Billable Matrix Spike Dup.

1101763001

Water (Surface, Eff., Ground)

XXX22544

3520 Liquid/Liquid Ext for 8270 SIM

04/29/2010

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Polynuclear Aromatics GC/MS

1-Methylnaphthalene BMS (0.0352) U .468 80 ( 42-92 ) 0.588 ug/L 05/08/2010

BMSD 0.455 77 3 (< 30 ) 0.588 ug/L 05/08/2010

2-Methylnaphthalene BMS (0.0352) U .426 73 ( 45-89 ) 0.588 ug/L 05/08/2010

BMSD 0.409 70 4 (< 30 ) 0.588 ug/L 05/08/2010

Acenaphthene BMS (0.0352) U .486 83 ( 45-93 ) 0.588 ug/L 05/08/2010

BMSD 0.464 79 5 (< 30 ) 0.588 ug/L 05/08/2010

Acenaphthylene BMS (0.0352) U .487 83 ( 50-101 ) 0.588 ug/L 05/08/2010

BMSD 0.478 81 2 (< 30 ) 0.588 ug/L 05/08/2010

Anthracene BMS (0.0352) U .56 95 ( 55-105 ) 0.588 ug/L 05/08/2010

BMSD 0.552 94 2 (< 30 ) 0.588 ug/L 05/08/2010

Benzo(a)Anthracene BMS (0.0352) U .56 95 ( 55-120 ) 0.588 ug/L 05/08/2010

BMSD 0.557 95 1 (< 30 ) 0.588 ug/L 05/08/2010

Benzo[a]pyrene BMS (0.0352) U .555 94 ( 57-110 ) 0.588 ug/L 05/08/2010

BMSD 0.556 95 0 (< 30 ) 0.588 ug/L 05/08/2010

Benzo[b]Fluoranthene BMS (0.0352) U .6 102 ( 45-120 ) 0.588 ug/L 05/08/2010

BMSD 0.606 103 1 (< 30 ) 0.588 ug/L 05/08/2010

Benzo[g,h,i]perylene BMS (0.0352) U .562 96 ( 49-116 ) 0.588 ug/L 05/08/2010

BMSD 0.566 96 1 (< 30 ) 0.588 ug/L 05/08/2010

Benzo[k]fluoranthene BMS (0.0352) U .556 95 ( 56-112 ) 0.588 ug/L 05/08/2010

BMSD 0.553 94 0 (< 30 ) 0.588 ug/L 05/08/2010

Chrysene BMS (0.0352) U .521 89 ( 56-109 ) 0.588 ug/L 05/08/2010

BMSD 0.519 88 0 (< 30 ) 0.588 ug/L 05/08/2010

Dibenzo[a,h]anthracene BMS (0.0352) U .609 103 ( 54-113 ) 0.588 ug/L 05/08/2010

BMSD 0.623 106 2 (< 30 ) 0.588 ug/L 05/08/2010

Fluoranthene BMS (0.0352) U .523 89 ( 58-109 ) 0.588 ug/L 05/08/2010

BMSD 0.515 88 2 (< 30 ) 0.588 ug/L 05/08/2010

Fluorene BMS (0.0352) U .519 88 ( 50-98 ) 0.588 ug/L 05/08/2010

BMSD 0.507 86 3 (< 30 ) 0.588 ug/L 05/08/2010

Indeno[1,2,3-c,d] pyrene BMS (0.0352) U .6 102 ( 55-111 ) 0.588 ug/L 05/08/2010

BMSD 0.609 103 1 (< 30 ) 0.588 ug/L 05/08/2010

Naphthalene BMS (0.0730) U .418 71 ( 44-89 ) 0.588 ug/L 05/08/2010

BMSD 0.403 69 4 (< 30 ) 0.588 ug/L 05/08/2010

Phenanthrene BMS (0.0352) U .527 90 ( 50-104 ) 0.588 ug/L 05/08/2010

BMSD 0.515 88 2 (< 30 ) 0.588 ug/L 05/08/2010

Pyrene BMS (0.0352) U .486 83 ( 56-105 ) 0.588 ug/L 05/08/2010

BMSD 0.482 82 1 (< 30 ) 0.588 ug/L 05/08/2010

Surrogates 

Terphenyl-d14 <surr> BMS .508 86 ( 50-126 ) 05/08/2010

BMSD 0.494 84 3 05/08/2010

62 of 73
Matrix

SGS Ref.# Printed Date/Time 05/11/2010 12:34

Batch

Method

Date

Original

Prep

1101763002 Billable Matrix Spike

1101763003 Billable Matrix Spike Dup.

1101763001

Water (Surface, Eff., Ground)

XXX22544

3520 Liquid/Liquid Ext for 8270 SIM

04/29/2010

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Polynuclear Aromatics GC/MS

Batch

Method

Instrument

XMS5395

8270D SIMS

HP 6890 Series II MS2 SVOA

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Appendix B 

Monitoring Well Construction Logs 
GEOLOGIC BOREHOLE LOG

Location: RHFSF Station Name: Location Type:

Location Description:

RHMW04

Establishing Company: TEC Inc.

Drilling Foreman: Tomas Fernandez Drilling Company: Valley Well Drilling

Geologist: N. Griffin/S. MacMillan Ground Surface Elevation (ft): Datum: MSL

Drilling Sampling Method: Borehole Diameter (in): 8

Total Depth (ft): Date Drilling Started: 22 July 2005 Date Drilling Ended: 26 July 2005

Monitoring Well

Remarks: 

Rock Coring

west. access rd., S of Navy Firing Range

313.03

320.5

Page 1 of 2
GEOLOGIC BOREHOLE LOG

Location: RHFSF Station Name: Location Type:

Location Description:

RHMW04

Establishing Company: TEC Inc.

Drilling Foreman: Tomas Fernandez Drilling Company: Valley Well Drilling

Geologist: N. Griffin/S. MacMillan Ground Surface Elevation (ft): Datum: MSL

Drilling Sampling Method: Borehole Diameter (in): 8

Total Depth (ft): Date Drilling Started: 22 July 2005 Date Drilling Ended: 26 July 2005

Monitoring Well

Remarks: 

Rock Coring

west. access rd., S of Navy Firing Range

313.03

320.5

Page 2 of 2