IU:Sl 'LTS OF TilE Jl: 28-29. 2005

o Xlm:s OF M TK(M;[:O;CO'lPU ,\ NO : r xs'r

ox rur "A", " II",-c-, " II" SClllIllll Ek ST,\CKS

AT TIU: ISI'AT ISIA'\" 11 SH U . MI:'IiING CO lI \N

L()CAT[ .~ \"II((;I."'IA, II L'i .\

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Kq>OrI :O;umb(r 5-21710

Aug ' 9. 200S

EJI j

Illle'l',,1I 1.aI'<,r.l1<>r;",. In,

4500 lJall R<>3d N.E.

Cire,", ('i1M;'>. Min...,...." 550LJ· I119

ITL: 1763) ~~O

FAX: rl'63lill6-711SJ

Subm;u,..J 10.>:

(SPAT 1~L\'\i SlU:L MI" "'C:nl~I ."N\

' Iin......:,1 \Iin"

r ,0 . ll", I - 5'lSll Old Iii".!". ..},SJ

Virgini.. Miml,-, ,,I,, 55792

"11," 1;00' Gulota> It,J"...q>hwn

SlaIT s.. rn}' k En. in","","l..l .....:r

':1/ f '-, • I 'J.d. £.. . ....... dJ t::a " alh....... F.icL.i,..lt

C''I<"J ituk'l'

Source T 'l Ik p.trtrnCnl

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InlC1'f'OIi LnbQf:l1()rio!. I"., 4500 nail K03d 1'1 .10, 

Cordi: I'ines. Min .... wu ;SO 1~·1 1]9 

TEL: (763) 786·6020 

" AX: (1 3)736-7115~ 

It[SUL 1'S OF Til E JUN.: 28-19.1005 

OXJI)[S OF NITKOGE:O; em! rU,\NO: n :S1' 

0:-; TilE ·'A". " II ", " e", .. .," SCllUllH El{ STACKS 

AT TIU: ISl'K r INLAi\'I) STHL MI;\'lNG O~lI'ANV 

LOCATEI) IN VIRGINIA, II NNI: OTA 

Subm;lh.-.J to: 

ISI'I\'I' ,NIANIJ STEEL J\ lI'-': ING COM I'M'Y 

inorc a Mille 

1'.0 . ~ I - 5950 Old Ilig' '''''')" 53 

Virgini n. Minrl.'sola 55792 

,\lIel1t;OI1 : GII S1:,,· It. JOseph SOTI 

StntYSarCIY & n" ro",ncl lt 1 EnBin.:". 

, _/ l.~ 

\{~pon Nnm"'" 5·21110 

Au!;u,! 9, 2005 

CN,<AL, ~ikk. t:a 

Kathk.:n Eicbbdl 

Coordi"ator 

E,Jldti Sou,ce TI!'llinll ["'!''''tmonl 
- TAIlU: OF CONH NTS

A liBREV IA JO __'__ '_M'_' ' __'_' ' ' __'_'_"'_'_'_ __ _._._._._._._. jij

C[ RTIFICA1 10:'\ i.·

I SD I AR \ ",\;"; [) IlISCt SSIO:O; .__ __•__._._._ _...........•..._._._._ _._._._.2

J AII{ E.\ l ISSION IU :SIILTS " " " 4

J,I ", uf lliilks..f :-; "~ ,, s.. mr>l ,, _._ 5

l .2 FIo ,.oo :\kI"" ulc S:lmplilt!l lb tJ._ __._._._ _._.__._ _._._._._...•. ._._ 10

A L,,,,. ti,,,," f 1(>l I'''I1'

1\ f idJ Data ShC'cts

C In,..."", ml S}>lcrn I"n ptt it:aI on~

o lc l.abo.lfa lt";... C(lII1puI,.. Prinlouls

E Cntihrali" " (; "-, C~rt li," on SItc l'

F I' ,..~ 'i 0:11,\

G ",,>t;WUMo

II Cakulatiorlr"l ""'l ioo

t M\ Plan

J S,ll11l'!ing T." in Cali!lrati'lI\Data

- TAIlLE OF CONH NTS 

,\ lJlJREVIA TJONS .................... , .......... , ....... , ....................................................................................... iii 

C ER TI FleA TIOl\ ......•........ _._ •.••.•..• _ ... _._ •..... _._._ .....•..... _ ......•.•..•........•.• " ................ " .............. ,". , ... i,' 

I N l' It 0 II UCT ION . , •.••.•.......•. , ....................................... * ........................................... ' •..• _..... I 

l SUMMAlt\' ANll IllSCUSSION ......................................................................................... 2 

J Alit EMISSION IU:SUI.. TS ..................... "" ..... , ......... " ......... " ........ " ................... """ .......... 4 

l. l Results crOxi","s of NilrogclI Samplillg .... _ ........• _ ...... _._ ...•..•... _ .........•... _ .... _._ •.•. 5 

1.2 Flow and Moislufe Sampling 1);]13.. ......................................................................... 10 

Al'1'1;1" I)ICI;S; 

A Loxo rill1l ofTc>ll'oru 

IJ Field Dala SlI«ts 

C Meas uremenl Syslcm l'crfonrrarrcc Spcc; li cn ion~ 

I) In erpoll l. lxlfDlori ~s Computer l'r;nloul5 

E Cnlibmri,," Gos Ccnir "" I;on Sht.""rl 

F 'nx; ~s D:lw 

G 1'roc:c.lul\."S 

11 CnkuTnliotl E'T iol\ ~ 

TtSl l'l:tn 

J S.mpling Tm;n C3!ibrnt;0l1 I)~!a 
L"'TR IWcr O~

On J..-.c. ~"2 :0<15 Inlerpoll Labor- l< rmooo nel ronductnl an O~ do.'1. " f il ...

Con'plw..;c Tflo( JI the 1'l"J1 lnbnd Sled Mining ompon~ b;al<:!J in Vi'l!-inq" M,nnc...u Mil"

I\<lnlwn and roc lkrj;lol' <lI'T1 ~<IfTT1Cd on~'" ""'i~ GUloll<-' Joscp/lson ofInW Slcd Pro\ iJc,J

roordin:otion b"t",..,., lbling ;>l;thil;"" and rUn! "f""'a1im, A ropr""",tati,e of 1hc Milll>C1Ol.:l

Pollution Control did 1lOI .. ilnC'U Ill<: IC'>! .

The loOUltti lNed " c,c lhe - A-. -Ir. -C- and lr In duf"<llin~ \' ~ c h ino: 'imrbf'<f :\I"<:Ls ,

h . IUllions ....." performed in "'cord.>ncc .. i,h [PA 1hod 1-1 ..,d 71:.CFR Tille l'3n 60.

ppcndi~ A (",,'i..,.j Jul I. OOll

\!<,;mll't:" del,·.",;n3t;"", ""''' "",r"nt",d in xc,,,d.,,,,,, .. ith EPA el "'~ V" lumeuic

now .~t" &"lmninalj"ns ""re dcl.....nined u,ing EPA Melhod 2 .. ;lh an - S" 1'" pit", . Flo..

l1\"a, u,,,mel1\' "ere I'<',f" " ''''d from lWO le,t I'<,ns "ri""t"d al "i n"')' def""" " 'I the , tacl. u,i,,1,[ a

16'I'<,i", na,'eN,:,

A , lip"re3l1l " ( """'ple !,l.' ".' withdrawn r"'Ill Ihe ""h.",t "''' ,I",.", " ,irl g le'>l p" n,

tl',,,,'idcd by th" plant) l'II Ihe lloek ,,,in 0 heaH ,xed

",,>be and tille. a,,,.,,, hl)'. Arte. po"i""

th 'O\l uie filter , Ib" l'a, ,,,,l lhll>u,,I, I"' '' eooden>cr-tnlC moi,tu,,, ,..,........ 1 i},.tem. """.arin;

in ",.i".. The p.:>rli, ub t,,·f.... df)' l'o'-' "'i IhI:.. Inln' l">r1ed 10 lhe '"'H,...... anal}'11'T " ilb IIw ""

o/lau"cd to .he "lJ"OO'\~ .h [th • eali br ~l ed "'ifi"". " hich " as uwd to C,",,", Ihat lho: nu'"

from 1hc""" I< "'«:ccd, lhc .,"l"i" rs of .he a.... 'l

"The IN run, " .,..c pnI"........-.l 11)' """ing lhe ""mplc prot.: • lhm:-poinl Ir:>\ ...",

(1/6, Jl6 md 5'6 ofthc weI;, <kpIh~ t he ;n-uumcnb "ere uhhr.ued bef,," and . f'cr the rons a>

pn I:I'A MrthOO. 3A and 7E "''''It :"/31ion:ol Spc.:i>.1ty ulibratiun 1:;ll.C1.. The ref........." llIt1llod 0 ,.

..... 1'0. ' '''''''''''n1lioJ.. ""'" .e. a llied ....i..S • WIIlpulotl" d:m k>f:~....t h.:J,kd " P 00 w ip

ctwli; copi~ of lhe ''''''If'Ul''' l"inlOU1u,.., i..dll<kd in !hi,J'l:'f"-'>rI.

Th" Ie>l ports were ~ed 3.7 dillmel"n p>t,..,~m from .he ilal: 1< n il and 11.7 diamn =

d"" l1>t rr from Ih" .....a. e>! n"" di>!urhan",. lb< 1,-.. ron>i>tN of usee 6O-minu.c n,n•.

Th" ;mpona"t rr,uh. " f the lc, t arc . umm", i,N in S""tioo 2 ;n table, 1-4. ,\ i, emi..;""

' Mults are pr.:>c,lted in 5'.... ,ill" J. Fidd data and all ,~hcr n" inf""""ti,,,, 0'" I',c,cnled in

tlte appcndk "i.

I

INTRODUCTION 

On ne 28·29. 2005 Inlerpol! t abornlOfies personne l ronducl"d nn Oxi"',s of ilmg~n 

Compli~ ll cc Te5l ~I lhc ~pal Inland Sloet M ining Com p~ny I"nte~ in Virginia. i"n~S<IIa . Mikc 

I~h~m and Joe IJ.crgslIOm pcffonncd Il<Hilc C~lin8, GU~lav Josephson of InlMld Slcei prul·id;:d 

coofdin ~lion bet"'"",n ing aelil'ilics ami pl'lII opcrmion. 1\ cpr.~" IHli"c of Ihe MinneSOl3 

1'0l1uli on Comrul Agcllcydid nOI wilness lhe Ic>st 

The r.ources t<'Stal were Ihe '.1\". ·'11", •. C' alld '.1)"" Indur:lIi ng Machine Scfll bbi:f 5101C1;s. 

E'·ailI3Iions " 'ere pcrfonnal in acconbncc " -i,h 1'.1',\ Mc'lIod~ 1-4 and 7E. CFR Tille 40. I'an 60. 

Apl"'nd ~ 1\ (",.,i....! July I. 2(0 1). 

M,,;ilu'" """.n" illations "no pe,fomK'd in :lCCOfl':lIIce ...-ilh EPA Melhod 4. Volumetric 

flow ",te <k~cnn;n lion s Wert (Jc1mnincd using EI'" Melhod 2 "ilh an "5" 1)'1'" pilOl. ~low 

mc.lSUlC"'''''' ' we," pcrfon""d from IWO ~51 pons oriellled m nincly degrc~$ on the ~c~ u~i g a 

16.poinl 113\'"'-":. 

,\ slip,rream of sa l It pic g;,~ was wilhdrn"n fmmlhc cxh~uSII,;olS Itream 1I_'ing le>l pons 

(p",,·idoo by Ihe planl) 011 Ihe ll~cllllsi"g a ht~Hrncoo probe and fill tr as""", bly. A(k, p:l sing 

IhlOUgh !he filler. Ihc gas pUK ll hfO~g.t 1 1",0 ,ooldcn>l:f-I)'JlC moislure """",·al 5y§I'",!> opcl1l1;n£ 

;n K';es. Th .. p:l11;CUble·r,,,,, dry ga..~ ",liS Ihtrllr:msporloo 10 II", ""n .. ''''' anal}'ttf ",ilh lhe c.\(0:55 

v.113u,ted 10 11K' aln>OS~ Ihrough • ca\ibr31oo orificc. which was uK'll 10 ~u", IhJI 111;: flo" · 

f.om III( WIck nnxd~ Ihe rC'(ju;""lC1lIS of IIIC an.~ rL<,>r. 

Th~ 1 .. 51 run l WCIC I"',formlod by moving the sample probe Ihrough • Ih ree·poin t trn,'cr", 

( 116,316 and 516 oftbe srock deplb). The II rull\en ~ were c~librn cd bl:forc ~I\d Bfler Ihe rulll a~ 

PCf EP" Melhods JA nnd 7£ usillS 1'-'31;01,;,1 Specialty caHbrnl;On GaKs. The rdel cncc IIIcll100 0,. 

COl and 1'\0, OOllcentrnrioll, welc I'COroW u>'''S a compuler d~la Ioj:ger and bnckcd up 01\ su ;p 

chans: copies oflhe comJlUlcr pI imoulJ n", included in thi, "'pori. 

The Inl pons were 1oc~ al 3.1 diamrlers up>t"'3m from lhe st:ICk exil Bnd 11.7 diamtlCfS 

dO .... " .1"'3m flOm th . ... 3n'S! flo", diSlIllb3nu. The Il'S! consisted Oflhl« 6Q.minUlC mns. 

The ;mponanl'csuits or 11K' le,t are summao-i zN in Scdioo 2 in lables 1-4. Ai. omission 

II'SUltS an: presenloo ;n SC-Clion J. field dala nd all Il<her sUJlJIOI1;ng infom"" ion are Il'0knl.d in 

Ihe "MlCndic .. :i. 

I 
2 SC:'II.\l,\lH ' AlIo' ll11JSClTSS10:-;

An ........ """ of the """,It, of lhe >t ",'rformN June 28·29. 2005 on the Indun lipg

Scrubt-.:, ' l.1"ks a," p"" ""lc'<l in Ilk,: u bI" I><:low:

NA .~_ ~. __..

NA _ __ 13U S

S ,\ ." ~. 02

N,\ 294.S7

1081 ..._ 75536

I""uroll i_\: ,\ b r hi. r ScT1l hhrr Slar....

1. lm;1 S" " rn '> n.I ", r nil.

- A- ND>. (L111IR)

-U- NO. (1.1ll lRj

..C~ O~ (Ul11R)

-o- () (LIl ll ll{)

All Sout-o... Com!>illC'd (UI1IR)

f'I<;1 ilJlJ ft "ompk t" ", 'i ~" or h~ il~ J "ta ,, ~l ""ult. , il i<nil' op;ni" " lh,l III " ""ull' ",ported

",,",in aJ ~ "'~"""IC and c\osc1)' ,e n",,! ""'(un1 u 1..."" which C"i'IN al llIe lime the Ic.1 ..as

z

J 

! SWlIMAIH' A,'{., IJISCUSSION 

An <I, nvj" ... of the f'Csults o f the lostitlg I"'rf nn~d lIme 28·29. 2005 On the lnd"rolling 

Scrubl,." n.ols a'" prclCnlc-d in tbe u blc be lo,,'; 

I ndUr~l ;nl! Ma r hin" Snubbrr Sl ~rlu 

SnUIW 1' ~"''''~ f[ Iin;l< /.J",;/ 

"A" NO, (1.llfl IR) NA ............................ I07.92 

"If' NO, (U IIHIt) NA ................... " ....... 138.HS 

.. C~ NO" (lBll IR) NA ............................ 21 4.02 

"D" ~ (LlJIJ lit) NA ............................ 29·1.S7 

An SOH,ces Comb,,,...! (LllIllR) t08l ....... " ............ " ... 75S.36 

No difflCullics ""rt: Cll"'U I,",~ in d", field M in the ~ ~'d "" joo. On the ba"i of this 

f,,,,[ Hl'd ft complete "" -;ew o f th. e<lli!t dilia nnd R:sull'l. il is our opinion lil at the ",sull, ",ported 

..-c " al. occurnlc and closely ",na:l the xIllnl vahlt.'S, which exi;[<"" 31 the time the test "OIS 

(>(rfonucd. 

, 
Tohlc L Swnm"l)' of ~~ of lh June 28.29, 2005 O . id", or :-iilrogcn Compliance

leS! lhe Scrubbn- Slac'" 01 ."" " pal Inlond S1",,1 Mining CClmJWIy in

V"gini nn "'ll

C"o<onl..l i"n Em,,,;un }(.Ic

Tim. ll'pm,d ) 1I.B,1 IR I

(Scnbl...r A)

0810·(191 0 11 8.29 IllJ6

0935. 1035 IOJ.S6 10·U 9

~5- IIJS IIJOi 1!i621

'" 11 2.30 107.92

(SeruM...r OJ

12 1Q.1310 n 9.7S 137.66

132S·IJ2S lUIS IJO.19

IH O.ISJO ! )9,92 mIll

'" IJO.9J nus

(Serubl,• • q

0750.(\850 221.47 W d8

t:HOS-lOOS 215.17 216.88

IO::q-II 2G JOZ.2) 201 10

,hI,( 2 14.82 21J.02

(Scrubhrr DI

I IJO·1 2J O 29J.SS 290.~

12S5· 1JSS 30J.H 298.S3

.. 141Q.!SI0 '01.07 29H9

A'. ~. S 7

3

T.ble I. 

" 

SLlmm3.y of Ih ~ II. c~uhs orlhe June 18·29, 2005 O .• idos o r i'iilrnl:cn Compliance 

IeSI 00 Lhe s.,rubbtr Slaciu al die 15p;ol Inland SI.,.,I .... in ing Comp;on)' in 

Virgini. , Mi" "cl1olJ. 

m~ 

Si: nohl rA) 

0811).1)9Hl 

(9)$.1035 

S. 5 

A,·S 

(s.,ru bbtr U) 

1210· 1310 

1325· 1425 

1440·1540 

",·S 

s., rubl~r C) 

0750-0850 

0905· 1005 

1029: 1120 

"'.!I 

(Si:rul,her I» 

1140·1 240 

11SS·I3SS 

14 10- 1510 

"'·K 

Co ~nl"'lion 

(['p"",I) 

118.29 

IOJ.56 

II4.CH 

112.30 

139.75 

14}.IS 

132.92 

40 9~ 

221.47 

215.77 

207.23 

21.1.82 

293.55 

30J.3·1 

10 1.07 

299.32 

J 

£lIIi ~l iu" H. le 

<I.!!ItIH) 

t 13.36 

104.19 

196·2 1 

107.92 

137.66 

140.1 9 

JJ8.70 

IJU S 

116.38 

216.88 

20S.80 

2 14.02 

290.99 

298.53 

29U 9 

294.S7 

75s.l6 
TI", r..~ of all air ( ",i"ion I"% ;u,, I'..-scnl,-.I ill .bi. 14-..:li,,". The tc....lIs hne 1:>0.......

"alculated on a I',:,,,,""l ''''''I''''e, using I''''t:mm, Wrille" in Micro'of! E' cd . p"" d, heel'

' I"'"ifica lly for ",,,1\;,, le.l; nt: ", k\, lati"n.. 101'A' pllhli,hcd eq"'li",,, haw been used M the basi, of

the t i, l<..:hniq".... in rho"" I"'l>gr:l n" . l he Ox <'m;..;"n rat", h,,'c t......... UkU ~ 1:'d using

II,,, pfOd"". oFthc cooccn1 r.1lio.. l;n.... no'" "...1000

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The r.-s"lls of ull air cm ~,ion (e.us IIfc Ilfescnl,"", ip Ihis !.ttlion. The rc.wlls ha,.., ixo..-n 

<.lcubtcd on a P<',,,,,,,,,i computet usi ng 1""gmOl' "Tin"" in Microsoft Es~tI spreadshe"ts 

Sl"'c ific~ lI y for source le'li ng c,itl,lmions. 101' A_pl.bli, hed cq,,"lio!1, hJ\'c been uscd nS Ih" b.lS;S of 

lh" caicuillion l<'Chniques in these 1'",,&r:"" 5. Th: NOs "mission 0 \<"5 h"-,, b..-.;n cakui,.M using 

lho prodUCt ofth., cooccntmlion l;nlL"l' no\\' ,o><lIlOd. 

• -
[[r

3.1 H...a lt.or !'i0.Ikl...... inlTion.

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:'oI••hod 71:::

Run I Run 2 Run )

06·28·0$ 06- 21-05 06-21.05

USIll·0910 flCJ 35· )O)S 10·15-11·1 5

'"

1[/.60 10.7S u.sI

' 9,61 19.1 1 IIts.!

1337'XJ 13911 1 D OO!·l

118.29 ll O~

11l.36 104 19 106.21

6

Tal a i s:m,plillj: lilll( IMI!'.:)

V" \""'OI';OF1,,,, 11. 01 0(OSe FM )

();,Ie of run

To,! Nc>. 1

Scn,bOcr Sta<l A

Rl'$ults of (hidn ..r:"" "'1:." ()o-'o. m' '''''i..'''' _

;m ru n ",t! ", (HRS)

lnlnl'''U Labs 11......101 No. 5-21710

l>f'oll lnb ml Stcct in in <'ffi IU"

\' l~ ll n c ,,

:"00.roac.n.n"""(1'l'mAl

:\\";'il ure (omcnt 1'Y.V,v)

o..Yf on ronlcnl (%VN j

;\,0. .....;....... n it (LlJ,l lltJ

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Test NG. 1 

Scmbocr Stack A 

O" le of run 

Time ruTl i!n rllclKl (I IRS) 

TOIal s:unp1ins lime: (MIN) 

Mo;,wn: CO" lml <".VN) 

Vo\umcuic Flow ROI" (OSeI'M) 

/'iO. C<HIcrnl nlliun (ppm .... ) 

I"O~ ~'" iu iun .. ~t~ (LllIIIllJ 

-

RUII I 

06·23·05 

0810·0910 

.. 

to.60 

19.6 1 

133790 

118.29 

113.36 

6 

Interpoll l.~b s It.'port No, 5·2 1 i I 0 

I~)a l Inland St",,1 M inin!; CO"'i"ny 

Vils ni~. Mi n~SOIa 

________ ~lrtl\O .. 7.; 

R"" 2 Run 3 

06-2ll.05 06-2X-05 

0935·103$ 10·IS-II·15 

60 .. 

10.78 I \.S I 

19 ~1 19.53 

119111 13002·\ 

10~.S6 114.0·1 

]().1. 19 1()6 ~1 
[

:\k ll",d 7E

Run 2 I{"".1

6·2K.OS (,·28-05

uis.ms IS ~

so en

12.11 1l.1>!

19.11 19.21

l.lf> lJ ~J'n

1·1.1 ,I 5 D 'I.'I2

140. 19 138.70

"'

11 .32

19.30

137.66

139.75

lJ151J

7

Run \

6·18.(lS

Ilt ,ult. lO r(hi, I~ . of :'i 0l: ~ n lJ"Io" n inal i"no__ _

101"'1"'11 Lob, R,'JK"1 No. 5-21710

l.p.al lnbnd St«l Minint Comp.ll1Y

in ia, Mi.........""

Volumw 1<; Flnw R.'IC(l>SCFM )

:'\o, e" ,,"cn Iru I j" n (1'1'III ,.II

Tim" run S1an.'cnd (I lKS)

., No. 2

Sc,uI>l>cr SI.1o; II

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~ .. No. 2 

Scn )btr SlaCk Il 

iJJtc of rom 

Ti ..... run $Lartk'tld (IlKS) 

Total s.1!lIrlin~ tim., (M IN) 

,\\oist "rc Co! ~nt W. VN) 

o.~)'!;cn COOle'll (% VN) 

Volumwif; F~,w R31c (I>sON ) 

NO, (,,"ccnl r~II n (pp""d) 

NO, nli ~ilo n ratc (!.IIIJI R) 

7 

~Ull \ 

6·28.(15 

1210.1310 

60 

11 .32 

19.30 

1}7S2J 

\39,75 

L17.66 

Inte' po ll La'" R,'pen Nil, 5·21 7 1 0 

I.<pJl InlJml Steci Min;,,!; C""'I"'II), 

Vi,&iu ia, lI1 innc>01n 

M~LII<HI H ; 

Run 2 R UII ) 

6·28·05 6-28-05 

1325·1425 1440· 15·10 

'" 

12.38 11.6 1 

19. 11 19.!2 

1l"72~ 13819) 

\·13.15 139.92 

\40.19 138.70 
_ ) 1, 1".... 71:

Run:! Run )

6·29·05 6-29-05

1)905-1005 1020· l \20

eo

1l ~4 IHl

185 2 ISAlI

140))) \ 411 MlI

21Ul 20L!J

216.18 201.10

nlA7

13.7'1

21&.31

eo

l.l 6)<)7

075(1·0851l

Inlcfl'Oll13t>i Rcpon No. 5-21710

hp.1l lnl:J1I<I Sl,..,l M'nins Con l"'n~

i;l . Miool:'SOl"

O. em..... " " nil' (1.8I1I R)

Volumetric 1'1"", Rate (DSCFM)

Itn ul... or (bilk< ,,' :\';U....:,.. lI' I'nn;II"I'''... _

Tc,t No.J

Scruhbc r St;)( C

M"ilolUrc oont,-nl (%V1\' ,

o;"c ofrun

Toul """,,,hnl; Ii"", (MIN)

r

L

[

[

[

[

[

[

[

[

[

[

[

[

[

r

-

r

L

r

L

rL

[ 8

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

r 

L 

[ 

TeSI Na.) 

Scrubber Sud C 

[Inul!.! or O~idt~ or Nitru!:tn Urterrllin:ltion, 

Time non start/clld (I IRS) 

T0UI1 saml'Iing ti",., (MIN) 

Moist"", COnic,,! W. VN) 

Volumetric Flow Rale (DSCrM) 

8 

Run I 

6·29.05 

0 75 0·0850 

60 

13.79 

18.48 

136]9; 

22IA7 

216.38 

IlIlerpoll bbi RCIIOi'1 No. 5-2 \ 71 0 

ISP.lt Ini:",.d St,..,\ Mining COIllI" "'Y 

Virgini:J. MinncSOI3 

··_ :\Irll1oo 71: 

Run 2 Ru" J 

6·29·05 6·29.(15 

0905-1005 1020· 11 20 

60 ., 

llA'\ 13.47 

18.52 18.48 

1·10))3 \4066H 

215.71 207.23 

2 16.88 20UO 
[

[

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L

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[

[

[

[

[

[

[

[

[

[

[

nI l.ab< R.1'M :-la. 5_21 710

1'f"U lnbnd Sl...,' Mininjl C""'I'"Il)

Vi' g;n;a. Minnc' '''13

f e'INo.4

s.:ro\lh:. Sla<l lJ

R....uh. of (hidn 0' Nil'''!:u ."" c...ina lioa. _ M t ' hod 7. :

'00 I lI.uo 11.0',)

Dale ,,' ,ull 6-29-05 6-:!9.05 6-29.{lS

Tim" nm ,Iart!e<ld (IIRS) t 1·!n·1240 1255·1355 1410·1 510

r ...31",mpling l im. (MIS) '" so

Moi >lUlf C.....lrnl ('tOV,'\'. 15.07 Is.n IHo7

(h -gcn "",""nl (".V,vl IU S l U ll 17.17

Voluruetric fl<m ROlle (DSCH' ) U S) 'J·l 1373'1'1 136-120

!"O. w .", Dlr3.1" n (pl'm A, 2'lJ.S5 JOJ.H ) 01.Q7

:'1'0, em i..iooo n it l l.ll,l lIt) :?90.99 ::on.SJ 29U o,l

s

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[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

r 

C~I N(l. ~ 

Scrubb:. Slack 0 

I) I" of fUll 

illl~ nm M"rtle<ld (1 IRS) 

TOIal .unlplinS lime (MIN) 

VO\UnlW;" Flow Rale (DSCFM) 

1"0, ~", l!~lo ll .... ~ (1.1111111) 

Run I 

6·29·05 

\ 1.10·1 240 

60 

15.07 

17.85 

118J9·\ 

29J.SS 

290.99 

, 

Interpoll Lab~ Report No. 5-21 710 

Isral In land S,...,I Minin!: C""'pa ll}' 

V; ~ini . MinncSO/3 

• _ ______ M~thod 7f: 

RUII 2 Run J 

6-29.05 6-29.oS 

1255· 1355 1410·1510 

60 60 

15. 11 14.67 

IUO 17.&1 

137399 13&120 

303.)4 )Olm 

298.53 294.19 
[L[[[r

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[

r InletpOl laboralories Report Numbe r 5-2 1710

L lrnand Steel

[ Virginia , MN

Test Number 1

A Indurating Stack

[ Resu lts of Instrumental Sam pling

[ Run 1 Run 2 Run 3

Date of Test 06-28-CS 06-28-05 06-26·05

rc Tlmeel Runs (HIs) 0810 I 09 10 0935 I 1035 1045 I 114 5

[ Stene Pressure (In. 01 We) -04 1 ·0 42 -0.42

Cross SecliOrlal Area (Sq II) 56.19 56.19 56 19

[ Pitot TUbe c cerrceot 0 84 0." 0,84

waer in Sample Gas

[ T....' (gJ 980 105 ,0 115,0

[ Waler", Sample Gas (%J 10 ' 10.8 11.5

Gas MeIer Coeft,cie nl U lO76 1 0078 1,0078

I[ Barometnc Pressure (In. or Hg) 28.31 26,31 28,3 1

Avg Orifice Pressure Drop (In. of We ) 1.89 1,89 1.89

Avg Gas MeIer Temper ature (oF) 74 ,5 79.5 810

[ Volume Through Gas Meter

[ MeIer Cond,loons ICFj 41 .15 4361 " 66

Slat'ldard Cooclilions (DSCFj ,,9< "'0 94 4 1 66

r Tolal SamplIng Time (M,n I 00 00 00 00 60.00

Avg Stack Gas Temperature (oF)

'" 11. "'

[ Volumet ric Flow Ra te

Actual (ACFM) 112.123 179,960 110,472

[ Dry Standard (OSCf M) 133.790 139.111 130,024

[

[

r

c 11

[ 

[ Interpoll Labora tories Report Number 5-21710 

Inland Steel 

[ Virginia, MN 

Test Number 1 

A Indurating Stack 

[ Results of Instrumental Sampling 

[ Run 1 Run 2 Run 3 

Dale ofTesl 06·28-05 06-28-05 06-28-05 

[ Time of Runs (HIs) 0810 I 0910 0935 I 1035 1045 I 1145 

r Sialic Pressure (In. 01 We) -0.41 -0.42 -0.42 

Cross Sectional Area (Sq. II) 56.19 56.19 56.19 

[ Pilot Tube Coefficient 0.84 0." 0.84 

Waler in Sample Gas 

[ Tolal (" " .0 105.0 \ 15.0 

[ Waler in Sample Gas (0/0) 10.6 10.8 11 .5 

Gas MeIer Coefficienl 1.(1078 1.0078 1.0078 

[ Baromeuic Pressure (In. of Hg) 28.31 28.31 28.31 

Avg. Orifice Pressure Drop (In. of We) 1.89 1.69 1.89 

Avg. Gas Meier Temperalurc (oF) 74.5 79.5 81.0 

[ Volume Through Gas Meier 

[ Meier Condilions (CF) 41 .15 4).61 44.56 

Slandard Conditions (DSCF) 38.94 40.94 41 .66 

r Total Sampling Time (Min.) 60.00 60.00 60.00 

Avg. Stack Gas Temperature (oF) '" 11. '" [ Volumetric Flow Rale 

Actual (ACFM) 172.123 179.960 170.472 

[ Ory Standard (OSCFM) 133.790 139.111 130.024 

[ 

[ 

r 

11 
[

[

r

'-

[

[

[

r

L

[

[

[

[

[

[

[

[

[

[

[

[

Inlerpo!l l aboralOfies Repor1 Number 5-2 1110

Inland Steel

V.rgir'lia , MN

Test Number 2

B Indurating Stac k

Resu lts of Instrumental Sampling

Run 1 Run 2 Run 3

Dale of Tesl 06·28·05 06·28·05 06-28·05

Tm e of Runs {HfI.l 1210 f 1310 1325 I 1425 1440 I ,,.,,

state Pressure (In 01WC) .0.62 .. 52 -0 62

Cros s Sectional Area (Sq. It) 56.19 56 ,19 56.19

Ptto! Tube CoeffIcient oe. ... ,..

Water in Sample Gas

Tolal 191 111.0 121,0 115,0

Water in Sample Gas (%1 11,3

",

11,6

Gas MeIer c eeireeot 1 0078 1 0078 1 0078

8.lromelrie Pressure (In. 01 Hg) 28 ,35 28 35 2835

AV[I On flCe Presscre Drop (In. oI WC) 189 1 89 1.89

Avg Gas MeIer Temperature (oF, 78.0 eo, eo,

Volume Through Gas Meier

MeIer Cond,tions (CF) 43.50 43 02 43,98

Standard Conditions IOSeF) 40,95 40 35 41 25

Total Sampling Time (Mil' ,) 6000 60 ,00 60.00

Avg Slack Gas Temperature (oF) u s 113 113

Volumetric Flow Rale

Actual (ACFM) 119.767 182,124 182}43

Dry Slal1dard (DSCFM) 131,523 136,724 139,393

12

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

[ 

r 

Test Numbor 2 

B Indurating Stack 

Results of Instrumental Sampling 

Dale of Tesl 

Time of Runs [HIs) 

Sialic Pressure (In. of We) 

Cross Sectional Area (Sq. II) 

Pilot Tube Coefficient 

Waler in Sample Gas 

Total (g) 

Water in Sample Gas (%) 

Gas Meier Coelficicn\ 

Barometric Pressure (In. 01 Hg) 

Avg. Orifice Pressure Drop (irl. of WC) 

Avg. Gas Meier Temperature (oF) 

Volume Through Gas Meier 

Meier Conditions (CF) 

Standard Cond,lions (OSeF) 

Tolal Sampling Time (Min.) 

AV9, Slack Gas Temperature (oF) 

Volumetric Flow Rate 

Actual (ACFM) 

Dry Standard (DSCFM) 

Inierpol ~boralo ies Roper! Number 5·21710 

Inland Steel 

Virginia, MN 

Run 1 Run 2 Run 3 

06-26·05 06·26·05 06-26·05 

1210 I 1310 1325 I 1425 1440 I " .. 0 

-0.62 -0.62 -0.62 

56.19 56.19 56.19 

0 .... 0 .... 0.8< 

11 1.0 121 .0 115.0 

11.3 12.4 11.6 

1.0078 1.0078 1.0078 

28.35 2835 28.35 

1.89 1.69 1.89 

78.0 80.0 60.0 

43.50 43.02 43.98 

40.95 40.35 4 1.25 

60.00 60,00 60.00 

'" '" '" 

179.767 182.124 182.143 

137,523 136,724 139.393 

12 
Run 1 Run 2 Run 3

Dale or Test 06·29·05 01-00-00 06-29-05

T,meof Runs (Hrs) 0750 I 0850 0905 I 1005 1020 I 1120

Slat it Press.ure (In. 01We) -0,71 · 0,72 -069

Cross SecliOnai Area (Sq II) "99 "99 "99

Pdol Tube CoeffICient 084 0.84 0 84

Water in Sample Gas

Total (g) 135.0 1J' ,0 130 0

Waler in Sample Gas 1%) 138 134 13,5

Gas Meter ceeseeot 1.0078 1,00 78 1,0078

Baromellic Pressure (In 01Hg) 28 35 2835 2835

Avg. oorce Preswre Drop lin 01we) 189 ' .89 1.69

Avg Gas MeIer Temperature (oF) 78,0 77. 5 78 0

(CF) 42 22 42.18 4 1.80

JOSC F) 39,75 39 74 39 35

(Min.) 60,00 60.00 60.00

(oF) 133 126 123

Results of Instrumental Sam pling

Inlerpoll l aboratones Report Number 5-21710

Inlanel Steel

Vilglnia. MN

189.769

140.668

190.247

140.333

187,883

135.397

13

(ACFM)

(OSCFM)

Test Num oor 3

Indurating SliIck C

VOlume Tlvough G<ls Meier

Meter Cond,hons

Standard Conditions

Total Sampling Time

Avg Stack Gas Temperature

Volumetnc Flow Rale

Ad~

Dry Standard

r

L

[

[

[

[

[

[

[

[

r

L

r

L

[

[

[

[

[

[

[

[

[ 

[ Interpol! LaboriUorics Repolt Number 5-21710 

Inland Steel 

[ Virginia, MN 

Tosl Numoof 3 

indurating Stack C 

[ Res ults of Instrumental Sampling 

[ Run 1 Run 2 Run 3 

Date 01 Test 06-29-05 01-00-00 06-29-05 

[ Time of Runs (HIs) 0750 I 0850 0905 f 1005 1020 I 1120 

[ Slatic Pressure {In. of We) -0.7 1 -0.72 -0,69 

Cross Sectional Area (Sq. It) 55.99 56,99 58.99 

[ Pilol Tube Coefficient 0.84 0.84 0,84 

[ 

Water in Sample Gas 

Total {oJ 135.0 131 .0 130.0 

[ Water in Sample Gas (%) 13.8 13.4 13.5 

Gas Meier CoeffICient 1.0078 l.()()78 U)()78 

[ Barometric Pressure (In. 01 Hg) 28.35 28.35 28.35 

Avg. Orifice Pressure Drop (In. of We ) 1.89 1.89 1.89 

[ Avg. Gas Meier TemperalUic 

Volume Through Gas Meier 

{oF} 76.0 77.5 780 

[ Mete, Condilions (CF) 42,22 42.18 41.80 

Standard Conditions (DSCF) 39.75 39.74 39.35 

[ Total Sampling Time (Min.) 60.00 60.00 60.00 

Avg. Stack Gas Temperatllre (oF) 133 126 123 

[ Volumetric Flow Rate 

Actual (ACFM) 181.883 190.2<17 189.169 

[ Dry Standard (OSCFM) 136.391 140.333 1<10.668 

[ 

[ 

r 

13 
[

[

[

[

[

[

[

[

[

[

[

[

[

[

[

-

L

[

[

[

Interpoll Laboratories Report Number 5-21710

Inland steer

Virginia, MN

Test Number 4

Indurating Slack D

Resu lts of Instrumental Sampling

Ru n 1 Run 2 Run 3

Dale or Test 06-29-05 06·29·05 06-29·05

T,me of Runs (Hrs) 1140 I 1240 1255 I 1355 1410 I 1510

Stalic Pressure (In.or WC) -0 77 -0 75 -0.72

Cross Sectional Area (Sq . It) 56 ,99 58,99 58.99

Pilot Tube Coefficient 08' 0,64 Oil<

Water in Sa mple Gas

Tolal (g) 142.0 161.0 122,0

Water in Sample Gas (%) 15.1 15,1 14,7

Gas Meter Coefficient 1.0076 1.0076 1,0076

Barometric Pressure (In. or Hg) 28.35 28 ,35 2635

~g Onf,ce Pressure Drop (In. of We ) 1.89 1,89 1 89

Avg Gas Meter Te mperature (oF) 76,0 77.0 78.0

Vo lume Through Ga s Mei er

Meier Conditions (CF) 40 03 45 .17 35.50

Standard Conditions (DSCF) 3766 42.60 33.42

TOla l Sa mpling Time (Min) 60 ,00 60.00 60.00

Avg Slack Gas Tem peratu re (oF) ias 129 130

Volum etric Flow Rate

Actual (ACFM) 192,234 190 .925 188,897

Dry Standard (DSCFM) 138,394 137,399 136.420

[ 

[ Interpoll Laboratories Report Number 5-21710 

lolalld Sleel 

[ 

Virginia, MN 

Test Number 4 

Indurating Stack D 

[ Results of Instrumental Sampling 

[ Run 1 Run 2 Run 3 

Date of Test 06-29-05 06·29·05 06·29·05 

[ Time of Runs (Hrs) 11 40 I 1240 1255 I 1355 1410 I 1510 

[ Static Pressure (In. ofWCj -0.77 -0.75 ·0.72 

Cross Sectional Area (Sq. II) 56.99 58.99 58.99 

[ Pilot Tube Coefficient 0." 0." 0.64 

Water in Sample Gas 

[ Total (g) 142.0 161 .0 122.0 

[ Water in Sample Gas (%) 15. 1 15.1 14,7 

Gas Meter Coefficient 1.0078 1.0078 1.0078 

[ Barometric Pressure (In. of Hg) 28.35 28.)5 26.35 

A~g . Orifice Pressure Drop (In. of We) 1.89 1.89 1.69 

Avg. Gas MeIer Temperature (oF) 78,0 77.0 78.0 

[ Volume Through Gas MeIer 

[ Meter Conditions (CF) 40.03 45.17 35.50 

Standard Conditions (DSCF) 37.66 42.60 33.42 

[ Total Sampling Time (Min.) 60.00 60.00 60.00 

~vg . Stack Gas Temperature (oF) '" '" 130 

[ Volumetric Flow Rate 

Actual (ACFM) t92.234 190.925 166,697 

[ Dry Standard (DSCFM) 136,394 137,399 136.420 

[ 

[ 

[ 14 
,'

Summa')' of the Rc,"It, of lhc June 28-29, 2005 (hide. or Nil rt>J:cn Com pliance

Te' l on the Snuh l",. Stud.., at the Ispal Inland Steel Milling Company in

~SJ6

13 7.66

140.19

nS.70

1.1 8.85

3

]-10.94

221 .41 216.38

215.77 216.88

297.2J ~_

214.82 214.02

293.55 290.99

303.34 298,53

' 0 1.07 2\M 19

299.32 294.57

13'.1.75

m.rs

139.92

(Scru hl",. II)

11 40·1240

1255.1355

14 10. 15\0

Virginia. )'linnc sola.

C"n centOlli" n [ mi.linn Rate

T inle lI1 ~n /U lIIml

(Snuhl",r A )

0810 ·0910 118.29 113.36

0935_1035 IM.56 10.\.19

IM S-I !4) 114 ,04 106.21

A,-S 112,)0 107.92

(S<:rulo hc r II)

tno-u to

1325-1 425

1440·1 540

Su m of Fnu. t: oil>

(S<ru hho. C)

0750.0850

1)90 , .)005

---lQ2.0.t 1;;.0'-__"'''' -'

A"g

Table I.

"

[

[

[

[

[

[

,

[

[

[

[

[

[

I' [

[

[

[

[

[

I [

[ 

[ Table I. 

[ 

[ 

[ 

[ 

, 

[ 

[ 

[ 

[ 

I ' 

[ 

[ 

[ 

t' 

[ " 

[ 

[ 

[ 

[ 

[ 

SlUllmary or Ihe Rc:mlr. of !he JUlie 28·29. 2005 O~ i" fS <lr Nil n>j:cn Corn pli3nce 

Tell on Ihc s':ruhlotr ~rks Ul the Ispat Inland Sleel Mining Comp.my in 

Vir~i"j" . Mi"nc rol~. 

in' ~ 

(Scr uhl"r,\ ) 

081 0·0910 

0935·1035 

]().lS·114S 

A"S 

(Sc ru l.o hcr II) 

1210·13 10 

1325·1 425 

1440·1540 

,\" g 

(Sc ru hl". C) 

0750·0850 

()9(JS·]OOS 

1020. \120 

(s.: ru~ lx-r 1.1) 

1140·1 2·10 

1255·1355 

1410.J5 10 

Avg 

CUMc n!r !i on 

r. ,,,"~I ) 

118,29 

1(j.1.56 

114.Q4 

112.30 

139.75 

143. 15 

139.92 

140.9·1 

22 1.41 

2\5.77 

207.23 

214.82 

293.55 

303.34 

301.07 

299..12 

Sum ofFou. Uni ts 

3 

Emis!;o" ltalc 

(U lIl m ) 

11 3.36 

]04.19 

106.2 1 

107.92 

137.66 

140.19 

138.70 

138.85 

216.38 

216.88 

20g,80 

214.02 

29ll,99 

298,53 

29 19 

294,57 

755..16 
lOCATIO;'li OF TEST PORTS

APPENDIX A 

LOCATION OF TEST PORTS 
I

I

I

I

I

I

I

I

I

II

I

I

I

I

II

I

I

I

ISPAT INLAND MINING

INDURATING "'ACHINE SCRUBBER STACKS 010. & 8" ISVO' '',SV01Sl

1,0 -101 .75

0

az _ N

@ IJ

101 91 '

Cl

,

I 

I 

I 

I 

I 

I 

I 

I 

I 

I 

I 

I 

I 

I 

I 

I 

I 

I 

ISPAT INLAND MINING 

INOURATING MACHINE $CRUBSER STACKS "A & VO SV01~) 

1.0" '0' .75 

0 

'" _ N 

© P 

V 

101.91' 

CJ 

1 
ISPAT INLAND MINING

INOtJRAliNG MACHINE SCRUBBER STACKS -c & 0 " tS\I016.SVOI 7)

10.•10. "

0

3> _ N

• @ ::D

101 91'

a

I

I

I

I

I

I

I

I

I

I

I

I

I

I

I

I

I

I

I ----

ISPAT INLAND MINING 

INDURATING MACHINE SCRUBBER STACKS 'C & O' tSV016.SVOl 7) 

10,,1 0.· 

0 

". _ N 

• @ ~ 

~ 

10191' 

C 

, 

- -

I 

I 

r 

I 

I 

I 

I 

I 

I 

I 

I 

I 

I 

I 

I 

I 

I 

I 

I 
FIELD DATA SIIEETS

APPENDIX B 

FIELD DATA SHEETS 
I

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I

I

I

I

I

I

lnl erpo ll Laboratorie s

(763) 786-6020

EPA Method 2 Field Data Sheet

"'u " lndur lIn9 Sl4>d<

h . , '"" , ,= .,., c....·_ - St. "" Do;o_tet C'" ) 10 1.50 "- Dry tlUlOr FI

'" Wete",b I Fl e """"lure Contont 10 60%

Monon,.,!o,

BD''''''''1I1C Pren " '" 2631

_

S~...oc: 'e ~s..." _I· ·0 4 1

.- ,~ ~m ~lJ<l 'Ofll

Po\Ol 0 1-12·Pl ....,... ,.. ,, """""

.-

- • ._..... f """ End of ".- 1...., ~31"'"

- ..

-

Wa. Coo) Poot t.. ) o ' ...... \ r /

I'cwl l oonglh j"I S"'rl T""" II ili A'"

,., 0.032 '" 7.TS ceec '" .-, 0.105 ,,~ IS 18 Cl 610

.,

'"

0 194 19 69 24 19 0,120

.. o32J 32.78 3128 0,140

'"

.-, OS71 68 .72 7322 e eso

'"

..

'"

'"00 61 61 00 " 0 1120

.-,

'" '" "'

.. ."

. '"" '"

•• "''' 101 75

..

""c

'"

,-,

'"

aezo '"

e.a .... '"

,

•

-,

•

..'"

'"

..'" "

.

,. ..

"

'"

,-, 0.610

'"

,"

ceao '"

.., ' ( .. " ,

l

I 

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I 

I 

I 

I 

I 

I 

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I 

I 

I 

I 

I 

I 

I 

I 

I 

... ~ 

". 

Slacl ~rnetet flft ) 

Dry B ... O r F) 

,,"ltu,e Content 

Monon,cte, 

B~,omellic P,e.~r" 

S~"' ic Press",,, .,. 

()per31on 

P,IO! No. . 

"~vorle 

, .. 

-~ 

,. , 

,., 

" '" 

,. '" 

... '" 

,. , 

,., 

,., 

.. 

,., 

,., 

,., 

,., 

.. , umt)el{s) • 

Intcrpoil l aboratories 

(163) 786·6020 

EPA Method 2 Field Data Sheet 

Inland SIDer 

, , 

'"" -'- , .. c .... ·_ 

"- " '''". I , 

, 

, 

F'~Clion Dillance Di,lan<:(l 

" From Sl<J<:' From E~d 01 Vclocoly 

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(763) 786-6020

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(763) 766·6020 

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(763) 786-6020

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(763) 7B6·6020

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(763) 786-6020 

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(763) 786-6020

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(763) 766·6020

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(763) 786-.6020

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(763) 786·6020 

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(763) 786-6020

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(763) 786-6020 

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(763) 786·6020

EPA Method 2 Field Data Sheet

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(763) 786·6020 

EPA Method 2 Field Data Sheet 

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(763) 786·6020

EPA Method 4 Data Sheet

FInal "rc

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Interpoll Laboratories 

(763) 786-6020 

EPA Meth od 4 Data Sheet 

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(7631 786-6020

EPA Method 2 Field Data Sheet

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(763) 786-6020 

EPA Method 2 Field Data Sheet 

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(763) 786-6020

EPA Method 4 Data Sheet

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(763) 786-6020 

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(763) 786·6020

EPA Method 2 Field Data Sheet

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(763) 786-6020 

EPA Method 2 Field Data Sheet 

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(763) 786-6020 

EPA Method 4 Data Sheet 

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(763) 786-6020

EPA Method 2 Field Data Sheet

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(7631786.6020 

EPA Method 2 Field Data Sheet 

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(76 3) 786·6020

EPA Method 4 Data Sheet

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(763) 786·6020 

EPA Method 4 Data Sheet 

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(763) 786-6020

EPA Method 2 Field Data Sheet

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(763) 786-6020 

EPA Method 2 Field Data Sheet 

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(76 3) 786-6020

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APPENIJIX C

MEASUREMENT SYSTEM PERFORMAl'"CE SPECIFICAT IONS

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APPENDIX C 

M EASUREMENT SYSTEM )'ERFQRMANCE SPECIFICATIONS 
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6/28/2005

Test 1

NOX ITEe O Mod el 43Bl

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INT ERI'OLL LABORATORIES COMPUTER PRINTOUTS

APPENDIX D 

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APPENDIX E

CALIBRAT ION GAS CERTIFICAT ION SIIETS

APPENDIX E 

CALIURATION GAS CERTIFICATION SHETS 
NSG 020 149L

all- 93103

10111 04

1011810 7

'"''

AnaM ,ca l ACClJ, "!:X· ·

Conce nl,ation

19.62 '4 COZiN2

2{l04 % 0 2JN2

Param agnetic

' .0 . 11<>. 1l0n

.........ch p, •• . N,C. 17709

........... 9 19{S,ol-) ; ;:

Rele,ence •

cen,IIcaMn Call':

EJpir allOfl Oar..-

PreSSUle, ps;g"

10111fO.l

10.'13J(l4

110G'4

10 99%

Cyl!lldl:r !

SG91191056 Al

CC46336

Ce.lIlie Cl Cgncl'"rmhon

M;nneapollS OtY91M

61 99

Cust om..' POI' 33361

I"IOOb& V1A·$10 C0 2 " 2399380022

CarDon OlOxide

REfERENCE STANDARD

,.

,

C\'IInd.., . SG9 4~ ~Al.

ANALYTICAllNFO RMAliON

,, mer:

NSG Po-

...£THOlI ' ''' _ 4_ _ a«,"*", .( .T_'' I>Ml ..... .... c.....r..-''G_c_s....-n

P...._ . II ' 9'J7)

....w..l YIEO·CYliNDE R

ComflSM nts

INSTRUMENT4TION

Sl 'Y"",nttMlld .-llS ~al ..

,

T~ pe S R Sample "

GMIS ( Traceable 10 SRM " 1675b )

GMI$ ( T,aceable 'o SRI.! . 26593 )

, n.1 (I :Z;:~ Jer('fTlYKe'h'fOftlly

/ TIl,s l eperl slales accurately Ihe reslllts oj Ihe invn hgill,on made upon Ill" mal eriill 5llbmrlted 10 11M! ar'l.1lylical

laooral0ry. EvelY elfelrl" " s been made 10 del e" ",ne el bjeetively tne infelrmatlll n ,equested However, in

eonneclion wll n lhis report. Nat'onal Speciaky Gases slta. have no ab< .y In n cess of esl ablislt ed cha'ge for

tn,s serv'ce Assayed al Nahonal Specialty Gases. 630 United Drive. Ournam. NC 27113 (9 ' 91 5••·3772

0

00 "'" _" "".-..a"""." ""'''''''',.....lIt."too""" ' 50 ~''Il

/t .. 0«\,0""" ,,,,,,,,,,," 'I? , "' ' ''''''''' .n" ....... """Cn, ol IO..!,"" ludt "'~o! 111. "" tj1.o::.ol "" !'"",,,,"'

CERTIFICATE OF LYSI PA PROTOCOL GAS MIXTURE

Bntance • Nitrogen

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CU5!Omc r: 

NSG POll 

Minneapclls o.ygen 

461899' 

CuSIOrrlcrPQ, 33361 ) " 

~l inder " SG9 14ge16BAL 

ANAL YTlCAllNFORMATION 

YSIS: 

p.o, eo. lIOI) 

~ .. <h ' , .. ""~ p.,1.. N.C. 1770'1 

Phot>e'l91SU ) tlJ 

Reference /I a8.&J70~ 

Cenific;llion Onle: 10118104 

Eopiralion Onl/!: l e /le/07 

PressUlc, pSIO· 2000 

METHOD T"" _~ .... ..... IfH"IO« .. ~ .. fP. 1r . ... t4.<, p,_r .. A .. .,. .... C....r..-.. 0 . ....... c~_ 510 ...... .,.. 

P",,_. 0 1 ~HI91) 

ANAL yzeo' CYL INDER 

ComMMnts 

Call1on Dioxide 

Oxygen 

Bo!nner· Nitrogen 

GMIS (Traceable 10 SRM tI. 1675b ) 

GMIS ( Traceable ' o SRM If. 26S9.} ) 

I' 

Horil>D VIA·SIO C02 423993S0022 

Horiba MPA -51002 991500~2 

, 

Ce ,frMld Cgncl'nlmlion 

1 Ul1)'4 

10.99'10 

CX!ind llf tI 

SG9119705eAl 

CC46336 

Las! ODie Cpl"waled 

10111104 

10113/04 

AnalvIocli1 ACQI, I\CY" 

COnCM\'i'!IQn 

19.62 '4 C02IN2 

2(1.04 '4 02/N2 

Ncn·dlspcl'5lvc Infrared 

Param agnelle 

, An.1Iy ~t: (/ "Z:_ Jeremy l(e"WOfthy 

Tnl$ ,epol1 ~Ia n accuralely Inc ~s"ns 01 Ille ve~I";Ji ion madfupon the malerial subm;lIed 10 lite analylical 

labOratory. EvelY 1'1101111;'15 been made 10 de le,,",ne ebjea,vely Ille infermalicJn requesled. However. In 

eonnecllon wil h lhis repcn. Nalie na l SpeclaMy Gases shall have no ~abl ~~ In e~cess of eSlabIi!lled Charge for 

Ihi$ servIce. Assayed I NUllon.1 Specially Gases. 630 I.IMed Drive, ournam. NC 2771 3 (9 19) 5 •• ·3772 

'00 "" _" WI o!M"4Md ""'.n ~, ..... "'. it _ ' 50 ~"II 

A""'II " """'IC'/ IocludeO I)?io" me.." ."'" .... , ......... ~. O! It .. , . .... "'<It pr«"""'~! \11 • ..,.~tlc>l "'.,"""" .... r~ SG020 14gL 

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" SG 02014;1..

58·59350

OJI0 5/D7

2000

Conce r!,al,oll

Allalyl'cal Accuracy"

20 22 '.of. C02/N2

20 04 'lIo OliN2

,Ii<> .'20I

"",...<h1""".'"P,..,N C. 21;0,

"J"' "' J ~ ~ ~

on In'ra red

gerere oce e

Ce<t,f,cal'OO Dale:

",,~ on Oale

Pressure, ps,g'

03103104

0 3102104

20.9690

11 16'>lo

LaSl DaTe lN

Cx!,nde' " CCU 64eg

CC.63J6

Cert,fied Concenl. aloOn

M,nnenpghs Oxygen

4300305

Cuslomer:

CuSlome' PO- 031100

Cylinder " CCtt7035

ANALYTICAL INf ORMAnON

TypelSRM am pl _

GMfS(Traceable 10 SRM " 1675b )

ewe Tr~ bl to SRId " 2659a 1

mounl 5SOA C0 2 U· l 002157

'N TR U~ ON

\l Il O<l o1 "

" ,;FloRENCE S I ..NQ" RD

\lEl 1'100 T..........d_.......... .. EP"'T'oc•.....,_... "' _""' ...... G.-C_ ...... S1..-C>

P"",_... a, ($.oJJIo_ l ll(l7)

AN.ol,l YZED CYLINDER

CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS MIXTURE

2

Analyst I X .."0'\g;", Je remy Kenworthy

Thos.epocl st~ les telJ l~T tne leslJh 01 the ""ve stog at_ upoo me et ~1 su t mrll ed to lhe arulyl,ca l

labocalory Every encn " as made to ddermine obJect,vety Ille ;nl",rnabon requested, However, ,n

cc nnecuc n w,lh t~ ,s report, National Specially Gases sh~1I have no ab~'t in excess 01 I~ blishe ch3rl)1l for

In,s serv«e. sa 1"d al Nalional peeia ~ c ases.630 Un,led OAve. Outflam, NC 27713 ~ ~ 77

·Oo ""'.... _ _ <__.. ...-\

•• "' ~' ''' .. ooc"'.., ""'" 1;".... _ .."" -'to. """"" al ,...., ""'..... ._ "'.... _ ..........,""""""

P. O . Bc . 120 Tl 

"", .. ch 1 """gie p,. ... N C. 21,09 

Phone 9T9/P .- J; ~ 

CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS MIXTURE 

CUSTomer: 

NSG PO. 

CuSl0nlCI PO. 

Minneapolis ygen 

30030~ 

031100 

Cylinder /I. CC11 7038 

ANAL VTlCAL IIJfORMATlON 

Relcrel'lCf! /I. 811·89380 

Cert,'ic:llion Dale: 03108/0 ' 

e ' p,raMn O~ e 

Pressure. JlSI9" 

03108107 

'''' 

ME THO D T .... ... r>¢Ot~ w . ...... ~~tcI o.;oore"ll" EPA o<.~ P>.-oI lor ~ ... , _ c.""",.,,,,,, 01 (;0"-,, c .......... S'-..os 

P .... """. Cil 1StfJ!<.,.,.. li'91) 

ANALYZED CYLINDER 

Compontn!s 

X~\Ien 

Balance· NiHOI)cn 

GMIS (Tr ~e3 le 10 SRM 1/ 1675b) 

GMIS ( Traceable 10 SRM II 26593) 

NSTR ~' TION 

In strymcntlMOdcllS9 nai ll 

Rosemount 880A C02 U· 1OO2 157 

Horiba MPA·Sl002 41' 99150C42 

1 7 16% 

20.9S% 

C ylInder II 

CC"64$9 

CC' 6336 

03103/04 

03102104 

" '· 1'4 

Concec!.at;on 

20.22 % C021NZ 

20,04 % O2IN2 

Non-dispersive Infiared 

Param a<Jnetlc 

An31ySl: J&. --'\ ~ Jeremy Kenwort hy 

Th'$ report SlalC$ Ce a1 ly loe resulls ol lhe mv esli\l atton ma'il'e pon me maleroa ' $ullm'llcd 10 the analyt,cal 

labofalery Every cuon has been made tedetermine objectively the InfO/ma lion requested. Howeve r. in 

con Cl ~ w,l h 1M re port. Nalional Specially Gas(!S r.hall have no lia lY In excess 0' established cha'l)C 101' 

In,s serv,ee. Assayed at Nallonal SpeCially Gasu. 630 United Olive. Oumam. NC 27713 (9 19) 544-3772 

· Po lid uso ...... "oM'" """n c)1016tr pits." ..... low 150 .Ig 

........ >: .. ICC ..... ' Inc..,.. <;JOUI_ .......... , .. ......, .... ......... ""_ ~.,. .... _~ .....,...,..... 

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NSG 020149t

Jert'fl1y Ke llwotthy

ConCf nlri1.l!!i!!!

200 ,' ppm NOi N2

101 I ppm S021N2

+'· 1%

Rel erence It M ·870SS

Cc ~' e.' lo Date ' 10124103

E' p'taIlDfl Date 1012.105

'(' "" .. , PS'lJ' 2000

1.0 w '"

10.'01103

148 ,3 ppm

' 47,3 ppm

CCl 17335

~nde' •

CC51Z12

s t .: '1

---

M,ntte a pol1 5 Oxyge n

4120173

EN-au

NSG PO,

u~to m~,-

Cu!>!e"'''' PO. 29839

Cylon",,' " 50

ANAtYT ICAlINF R~ATlON

SUlfur DIOxide

ANALVIEp CYLINDER

Components

Nlt" e O. lde

Type/SRM $ample "

GMIS ( Traceable 10 $RM " '68

GMI$ ( Trilccnble lO SRM /I 1694a )

CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS MIXTURE

INSTRUMl::NTATIQN

lnSUltmCntJt.1osWlISenal "

ceTHOll 1....__-.-0<C<l0>g " (,,& I,"" 'I _O<CO""A_...C4"'IoIc_ of e-_ 5U._"" _ _ G-' 5.... ._ 1!19

EfERE~E STANDARp

i:»: .-"{ ..-<,- .. - - . %

/

Thrs ,epon Sl"'~ a«:ut al"'Y the 'csuns ol t"" inve5l'!l.l100n mace upon u'le malef''I1WtlfTII11«110 lIN' anall'\oUl

IaDofatOl"f' Every ,,110<1 h2$ beef! m<tete to ~rte otJJea'vely tIN' ""orrnallOfl '1"QLX'!>t\"d H......cver. in

o:onllC,'(:1000 ""'h ."'5 .e pOtt. NallOnal peaa. Gases $Il"" fl.iI v(' 00 atlo .l ," e xcess 01es.to:It>1!>ht'd dla rge 100'

tIllS. se....ice A»ayro al Nat,onal Spe la"~ G;JSI's. 6 30 UlIoIro Dowe, Durham NC 27713 (9 191 S4~· 3772

· Oo _ _ •..-.p'......*.. _ l:>O_ J

.. 0« ""."......... poul ._"*'n .""" "'''''''''. '' ....'.0lC..... p,,,,,..,,,,, or'''' ' ..,. .."''''_

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CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS MIXTURE 

Customer. 

NSG PO. 

Cu!>lorr>er po_ 

P.l intlcapol15 ~y(lc n 

~1 20 73 

29839 

CyllflOflr " CCSO~2 

ANALYTICAL INFORMATION 

Relc.cnce" 88.87055 

CC~' e.' lon Datc' 10124103 

~p"aIlOfl Date 

Pressure. 1lS00f 

ElItOO 1,.. .... """" ..... "",~7'" ~""'IIID [PA 1.;>< .. ""'1 Pr"''''''' , .. A ... ,.O<I •• ~", .o! .... 01 O" •• OIJO C_ot"", 

~.-". P'''' ...... "'" . 5."", nbtl 1997 

ANAL VZEP CYLINDER 

Cgmponcrns 

N,t"C Oxl(!e 

Sullur O<oxido 

148.3 ppm 

147.3 PP'" 

Balance· N'l!ogcn Trace Gas· "III'ogcn Oioxide I 0 ppm 

GMIS ( Traceable to SRM " 166 ~b ) 

GrAIS (T aton l~e 10 SRM" 169(3) 

KVS AnalCCI EN.844 

Cvl,n(lC' " 

CC5 12 12 

CC I17335 

1010 1103 

AMM ,ca l A!&lImcy" 

+'·1% 

' /· 1% 

Concrnlrilhon 

200. ' ppm 

101 1IIImi 

NOIN2 

S021N2 

ADaMlco! Method 

Foulier TrDnSlorm Inir aled 

Analyst J ·X .. . " ,-#; Jeremy Kenwol1lly 

Th,s report stmcs aecur el y Iho rCS<Jlls Ol lho;o i.lVcsllgation ".!rtc upon UIC matc"itl suomilledlo till! analyttCllI 

iallOralOry. Every el lort haS IlOcn mace 10 determme o~jcc vely tnc ,nfennatton requested. Howcver, in 

connCC1ion wilt' this report . Nntional SpeCIally Gases snail lIave nO liabi lity In e. ccss 01 eSlabl ishcd charge lor 

tIlis serviu. A5sayed at Nat, onal SpeCIalty Gases. 631l UM Cd Of,ve. Durham NC 27713 (919) 5<14 ·3772 

· O' .............. _....,.~<~ "' ....... * .. bo ..... ,50_ 3 

.• """'¥~ .. o«"'''''Y ""'''''''''' r,pco! ",-", .. '''' ....... " -" . ....... """"" "" .. "."", "' ... , OI)<c ................ NSG 02014\1t 
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NSG 020' 49L

ARaM ,cal Accu racy·'

+'- 1%

Cg ncrolralooo

103,9 ppm NOINZ

99 85 ppm S02!N2

Fo ...-.eo' Tt;lI" slorm Inf.ated

P.O . h . ' l<l I )

a.....,,<" ". " ~'" P. ,. , "'C, 1 7709 1'1",..., ,) 1'J/ $... n~

Re le ,ellO;e . 8&.966 89

Cetl~PCaI,"" Da le 03l3OJ05

EJ<p,. aM'lO"'''' 03130107

e ~....e.l:'SO\I· 2000

< 0.1 ppm

03101105

837 ppm

838 ppm

Las p air Cal'l1"Ij r g

Cy linder 1/

CC4 1504

Mtrwleapolis Oxygoer>

~3 e.o

Trace Gas · Nitrogen Dioxide

!

AfanoKRL l

'5PECIRLTYCeSES

NSG PoJe,emy Kenworlll y

/

TillS rcporl $tatcs accurately ltle ,e!>UII$ 01tile inY" S' "l3l10n mece upon tile material ,, ~tnIlt ed 10 1110' analytlc.11

laboratory Eyery el lort has been made 10" etermlne objcdiyel 'he 'nr,,,m atlCn 'eqllnlO'C Heweyer. In

eoeeecncn wllh nusrcport. NaliCnal SpecIally Gases shall nave no l,atltlily In excess or established charqe lor

uns servtce ss a l'd at NatIOnal Spee;a ll 03$C'. 630 UOiled O,,~e Durham. NC 2 7713 (919) 5• • ·3772

TypelSRM Sam ple II'

GMI$ ( Tr aCeable to SR M 1/ 16Mb)

GMIS ( Tra«Able 10 SRI.! II I

Balance · N,lrogen

AN,.l.l vIeR cnlNOER

ComAAnt ch

CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS MIXTURE

ClI' lom... PO# 3<'70S

Cpnd'" II CC41371

ANAl.YTICAL I/l;FORMAl ION

l.OETo<OO Thot. _ d _ onoIi'rt<I occ"'''''l_ EP" ',"'__""' . . .... .-.:l oI G>_C _

!''tIC....... GI '11'I71

REFEf<ENCE STANDARD

INSTRUME NTA TlQN

m.t•....,..'"'M Od"VS" nal •

' 00 "'" "" "..... . .."""d """" C~""'.. "'....... '..."'" ~"

..•". ~,<" o' Co""1 ,,',"""" ~fP'C" i<r<>wo ." ,,, _rc" "'"<". "....I, "" ..... ",,,,,..,,,,,01'o.....,,<... ' '''run..''

PO 9o. ,rol) 

~~.~ ... h r. ,.ft l~ P .. "- N C. 27709 

Pho...,"'' ... ·)1n 

CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS MIXTURE 

Customer; Mc pol is yO n Reference II 88·96689 

NSG POM 36033 Cc nilicatian Ollte: 03/30105 

Customer PO. 34705 Expiration DaHl: 03/3 0107 

der II CC47377 PrC S$U!c, pslg ' 2000 

ANAL ynCAL INFORMATION 

"'f l 1l0 0 T .... WU.....,.o<I 0<'"""119" [ PA "I<~ "'OCoool"" ...... ,.....:1 CoM"""",," G __ C,iI>< ... S,.,..,..,,,, 

Proc ....... GI !St\l':_ '1197) 

ANAL VZED CYliNDER 

CPmMnerh 

Nltne ~id e 

Sulfur O'OXide 

83 7 ppm 

83.8 ppm 

Trace Gas' NLtrogen Oioxide <O,l ppm 

G'AI$ ( Tra cUble 10 SRM" 1634b) 

GM' S ( Traceable 10 SRM I: 1694a ) 

INSTRUMENTATION 

n$lr um~!1V OO cI ISC,; ~1 1I 

KVB AnateC! EN·844 

Cylinder ' 

CC',S0' 

CC52269 

LIIS! p ale Ci!!ibraleg 

03/01105 

An3M IU I ACGllfac:c 

' /·1% 

CgoceOI!!l1ioo 

103.9 ppm NOIN2 

9985 porn S02lN2 

Ann!y! jca! MClh!ld 

Fourier Translorm Inlrared 

AnalY$I; ~ Jeremy Kenwonhy 

7 

This repon SlateS accurately the reSUIlS of tile inveSlioaiion made upon lhe material sunmlUed 10 Ihe nalylic.a l 

lallOratory, Every efllWl has been made 10 oelermine oDjoedively Ihe information requesre-a, However, In 

eOl1l1ection wdh Inls report, NallOn;}t Specially Gllses shall have no liabillly in excess of CS li ~ed charge lor 

thIS service, Assayed 011 NatIonal Speciall y Ga~s, 630 UMed Drove, Dutnilm, NC 277 13 (919) 5H -J772 

' 00 .... "" "'"' Il>r.cl>td _ cyt.ncltl "'"'c,. " .......... ~o ~I~ 

... "" ~" 00:<"'""1 "",,,,,," '/pc" """.," tI'" _re. , ,"' e ll, It I ..... ..., ..... "''''' .. ''''' <>, , .. 10000tc .. . ,,',""'"' NSG 020149L 

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• 
AI'PENDIX F

PROCESS DATA

APPENDIX F 

I'ROCESS DATA 
2005 Data

TYPE DATE SHIFT GREENFDHRS GP2LT AGASTOT BGASTOT CGASTOT CARSLOAD P1TONS AGASUSE F 6/27/2005 1 0.5 3513 328 197 275 0 765F 6/27/2005 2 7.8 3048 483 348 619 116 1971F 6/27/2005 3 8.0 4189 400 264 693 0 2918F 6/28/2005 1 8.0 4346 410 255 753 0 3200F 6/28/2005 2 8.0 4268 414 261 706 116 3091F 6/28/2005 3 8.0 4342 414 249 704 0 3105F 6/29/2005 1 8.0 4263 437 259 717 0 3136F 6/29/2005 2 8.0 3962 425 260 700 116 2745F 6/29/2005 3 8.0 3945 0 0 0 0 2890F 6/30/2005 1 8.0 3670 431 272 720 116 2729F 6/30/2005 2 8.0 3484 422 269 696 0 2875F 6/30/2005 3 8.0 0 413 246 697 0 3274

Page 1
AI'PENDIX G

PROCEDURES

Pia.., Noo:: In IIl'1 effOftlOoonsa"Ie p>p:r.

the proced= l«tion ofthe .ppendix hn bc=

...-..ed fot e:.pbnatlonsofEPA methodology

dn"wioM. Cori<-s ofllM: methodolot!i",

u..ro fot II:Sl:;ng In" ....ilableupm requeot,

or.l'lea<e refer to the 'P'CirlC

EPA Mdllodson lIM: fol"""ing EPA ...mites::

hnpl"" .c'pI.80"tnn.'emo' and

hltPl l"' .epa.goo."/SW.s.l6'main.hIm

APPENDIX G 

PROCEDURES 

1'1~a5" N(IIc: In an errort 10 conscr.·o p;!po:T. 

lile procedure $«1i(ll1 oflilo appcndi" hIlS been 

reser.·ed for c..xplanaliolu of EPA mClhodolog)' 

devlalioo1. Copies orlll<: ml:lhodI!logies 

used for Iesling are B'"lIi ~ble up<)Il request. 

or, pltMC refer 10 Ihe irlC 

HI'A Ml1i1odson the following EPA "'cbsiles: 

hltp:J,"wW.cp:I.govlnnfcmcl.nd 

hllp:J'"",,,w.c-pa.gc .... /SW.8-I6Im:.i nJttm 
APPENDIX H

CALCULAT ION EQUATIONS

APPENDIX H 

CALCULATION EQUATIONS 
,

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APPENDIX I

TEST PLAN

APPENDIX I 

TEST PLAN 
I

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U_ . P......lIoo.

-

'-

Perforrn.ance Test Plan Approval

Mbo.._ f'1)lh1Jo. Coalro! Aa

~1 r. rfU lt d. N. Sa'" 1'..1,MN 55155-41904 (4$111'H>-4)Oe

.......pa..ltIole.........

"Q/I'257

I

I

fadlil, ~. IM Ispat In'''nd ~ti omsun

radlil)' COllacl: Gus JoscphSO/'l

Add " ..: 59S0 Old ... 53. Virg ini•• MN H 791

fu: 121') 'l·S 1~

r.m ".i"n r.il(.): H ':016 (SVO14, SVOIS. 5\'016. VOll loC'1J1lt:ft II~ I

Sc . tdulnl t"or: June 18 and 19, 1(0). " ' }nu, r u llity Incaln! i. Virginia. Minln o' ''.

I 'l"ou, 'n' pl.. ,ubminrd 00 ~la 19, 2005. u d do..;l1 011 J UDe 2J. 2005, lin bttn .ppm.N

by 1M Miolnou 1'011111;011 C"lIlrol ~rllcy fPCAI'" rou.....:

I

I

o Shoo"", .. tn t nolifoc:a!;l.'Il applO'oN

I8J Tell ,,1.>10 If'PfO'N ...;,hocII mod ;rlC ion

o Te' l plo.. app""o:d "' ilh (0110" ;"8 I',,,,i, i,,,,s:

I

Ind ude in lhc fLn.J I le'l report the rutt rcrcrcn.:c method .II\;! rec ord (su ;p charl and/or

dala l(l l>( OUlpUl) used '0 (.Io ulal, cmi..ions. The dala . hould include calihrnli""

"alucs for ,,~' in,trumc"tal analp cr U'N f" r emissions compliance testing.

I Include in thc fi nal test ,cJI<l n a ", ,lied ,Jra'" ini/. of the test l<><:ati" nl ind u,lill g 1"'-' lIution

,onu,,1equipmenl. oricn1a li"n a",J t,,11"'" locations.

I

I

I'",iss;"" Unit ' hou td be <'""rate,l >l ",a,imum c. pacity ( H Olong lonsthoo" l ,Jur;ng the t,,1.

le ind ,lde lhe 1"<><:"'" nlln and cnn1l,,1"q ~m nt ,ale. on lhe O"........I;ng Oa13 Sum",a,,'

F,,,",,, inclu<Jed " ;th thi. apllfo,"1.

Ih,, JIl lJ. 2005

()pcnlin g D. ta Summal')- W.....e

Comb..""",

in.. O. ta Sum~ A"f'ha h PI.nt>

, ro w;h<: CD-RO~ Submittal Fonn

o

@

Opnalinj; Da.. Summ>-/)- Comb.."' ;.....

Op:n t;ng Dn l SllmmJr)-- p"",,,,,, Sour"...

Ccnifiuli<'OIs F<onn

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,\nJt' ''' Place

I'en onnan. e Te' l C.,..,.,JinJI'"

C" "'plian, e and Enf" rcemenl Scction

Ind..strial Divi, ion

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Perform.ance Test Plan Approval 

.- - Mlllllnotrol"olhlm Coalrol AI"1tCY 

~10 ul.ytfU ltd. N. SaID! .... I, MN' 55155-41,.. (651) 196-6lOt 

www.pea..ltalt.. ........ 

Facility NRm.: 'spat ln b od Mi ning Comp;ll'ly 

Fad lity Conlael: Gus Josephson 

,\oJ" r~.: 59S0 Old Highway 53, Virginia. MN S5 192 

Fu: (218) 7.19·5156 

,\ QIf257 

t:ml,.i,," lJn ill'): EUO:!6 (SVO 14, SVO IS. SVO 16. SVO 17 sequ entia ll y) 

Solltllultd For: J un.:: 28 and 29. 2005, M )'ou t .'wti liry locatC't.i in V i.gioia. M innr "1~ . 

Your If~1 I1 lwn , ubmillt d On ,\ Iay 19.2005, Rod di,cu~ on J unr lJ, 2005, hw. !>rrn 81'1" 0\"(-11 

by lb. Minnaolll l'oUu liop Cunlrol Agoncy (MPCA) .... r"lIo"'" 

o Sh.oncncd 'eSI 004 ific3lion appro>d 

o T cSt pl,n appro.'w wilh lhe following p,o " isjons: 

Include in the fi!lJ t 1.~1 repon the (utt rc(c,cllI:c method datll fl.'l:crd (su ip chan andlor 

dalatol!l!c, out put) uscd 10 (3IouI31< <miSlions. The data ~ord ~houl d include ~a ibrnlio" 

value s for any instJumc nlal,nalYl!e r used for cmiS5 ions compliance 1<."5ling. 

Incl~d~ ill Ihe final tcst rcpon a simpl if oed dra" in!! of the teSt locations i"dud i"H 1'011111 ion 

control eq uipmen t. SlaCK orientation nnd leSI pon lOCal ions. 

Emiui",u Un il ,hou ld be OfX"r:ltw at ma~ n"'m c.pacily (3JO IonS to" ./h",ur) d uring the tcSt. 

''' a~ i"clude the p<OCCSI ntU nnd c<NItrol equipment n ics on the O""",ti"l1 Oat. S"m",ary 

Form inc Ilkkd ,.;ith thi. app<oval. 

AII~c t" onns: 

o O!,<,ratinll Do t' Sum",ar)"- Combuslion 

Sources 

(@ ~ .. tinG Da ta Summa ry- Process Sour cc," 

[@ Ccnific,tions Fonn 

,\ ndrew PL1cc 

o 

~ 

" .rfoml,nc c T eSt Coordinator 

Conlpliancc and Enforcement ~c n 

Industrial Di vision 

O!'<'r1uing [latn Summary· Waste 

Combustor. 

Dl\<'mti n!l Data Summary- i\spl", 11 I'l nul. 

Micr fichc /C D·RO~ ' Subm;ttal Fonn 

[)~tt: Junt !J. 2005 

, 
n :ST I' l. ,\~ 01~ TACONln: 1'IUICESSI:"i(; F,\Cl U Tl'

ISI',H 1:"iI. ANll M IN ING CO. _ \'mC INIA• .\lI;'1; ;'I.'F.SOTA

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1'",1 I'lal1 Dale ,

T'.\1 [laic:

l"~ 2{ ~l

JUI'" 28 - 29. 2005 I

Nam" a"d add,e" "fern;>s;"" facility: h r.11 I" land illl ll\( Cnlll p"ny

5'150 Old 53

Virginia. lIol inncsota SS7'J2 I

!'cnn;ttcc """I"Cl person:

Penn;( :-<0,:

J,,,lq>cn<I" Tl ITc'l;ng C""'r;"'}':

C"nt"cl:

(ius Josephson

(218) ].1<)·5910 X 283

FAX (11K) 749·5256

137lJ(I062·IJO I

lmerpoll L"oo"w,ic<, Inc.

K~ hy Ei, h lmll (76 3) 786·6020

FAX (763) 781>-7 854

F,.,nail: K.",I,1'10E!,J,la'ltE..!me.'l \ll·l ,.1 ,,

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Rea,nn f"f (e,1ing: rille VII'Stl Permil C"mpli, "cc Tc,ting

Physical de<cril'l'O" "fFmis. i,'ll 1'<J jnh : Sec an,,<hcd ,Ir" , Ln g'

['ART II. n :STlN( ; IU:QlIIIU:J\IE:"iT S

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I

,.-.,..JI,>o,lI11t'!!lI mi ..1il_nil l!l' /{l lk" /{L !!J"'~ Il.I!1

lml" ratin c ,\ lu "hinc

S\'OI-t. 015. 016. 01 7 (>C~ llcn any)

l'AIH Ill. ()P ERATI:W: CO:"n lT IONS

NO, 1O Ul!lm

(, ,,m "ff"ur)

ao CF/{ 1'1 522 1

BACT

710 6[lmin

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L I',o.:c, ,; Ll l1l ri l [) ,i li (} I )n Ll ,.ll n~ I'll",aee: The n, lIral n~ furnace b a I)'avo lra' -c1ing Mmip ll

~r: lle f"m a"e. 'I he preheal w ne has lOmmrnUll l, I" ", NO, North

A",,,,icon nau" a l g" b"me,' . llic primary combustion challlh<:r has (2)

11)()lIItllBTUIII, nnW' a) ga,ifuc1 " il I" ", NO, North Ame,ieM b"mor;.

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TEST I'I. A~ 1'0 It T,\COI\Tn : I'ROCESSI:\'G F,\CIUTY 

lSI''\T I:-"LANI) !\lINING CO. - VIIIGIN"', MIN .... ESOTA 

I',\[IT 1. GENERAL Ira'ORMATION 

Test I' I~" Dale: 

Test 1).1I ~: 

M"y\ 7.2005 

JUlie 28 - 29. 2005 

No",e "lid odd,.," of crni .~ io" fnci lity: p~1 Inland M inillS Company 

5950 Old I Jighw"y 53 

vi,S;";'_ Minncsotn 55792 

I'cnn;ttce contaoll"',son: 

Perm;! No.: 

J,UICf'ClllIClll Tc~l;n ;; Company: 

Contact: 

Gus Josephson 

(218) 7.19-5910 X 283 

FAX (liS) 749·5256 

13700062·001 

Imerpoll L~bomtorics.lnc. 

Kalhy Eicksladl (763) ~6·6020 

FAX (763) 786-7854 

E'llla i1: K" II ". _ E ick <tadl£i!lli:ll'" 11_ J.n b'SOJ " 

Reason for le, l ing: Tille V I I'St) Permit Compliance Testing 

Physical <kscriplion of EmissiOIl l'u;"ls: Sec attached drawinG> 

,--,--fl',o""W"~"'~"'-c7-'F~J.i""";' ___ OAi!Illicahlc R"le 

[",[urntinc Mudlinr 

S VO 14. 0 I 5. 016. 01 7 (>eq"cntinllyl 

NO, lOS8 Ullim 

(sum offour) 

1',\lrr III. OI'EKATING CO;-" I)lT10NS 

I'rocc55 EqLliplllcnl D.:>eriplion: 

40 CFR pt 52.2 1 

BACT 

1'>kthod Run l,Cngth 

7E 60min 

Induraling Fumace: The indu rating f"mace is n Dra\'u tra,'cling rait;lll 

~r:II~ fl'm3c~ . The prcheal w ne hIlS (8) lOmmllTU/Hr low NO, Nurth 

A",",ican natural go. bum~r>. lllc primary combustiun cliu,"bcr lias (2) 

I OO'lltnllTUlllr nawrnl ga~lfud oil low NO. 1'10"1\ Amcrican bunter>. 

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lnd Machine ; n.c indoDling m:lchinc 1""1..,.:1l t>u mn' ...ill "f'C'ratc at

h:1 ccn limo and 1950 of fll' rhe liN heal ron.. and bcl" C1.-'n ~OOO and

Z2S0 or f<>r I"" ..,.,o.,d rr"h".11 11_ .t • If''-ro of . hour 7 fn1 JI<"f minule.

I.... nafc " jill-: p eatn than J aOof l1 u~ I'd lch p<"f IKJU',

ImJu li [t. "",d,,,,., ""ouhl>..-n. . II"" pl'C'l' u,c d"", ", ...ill "" hcl"' « 1l a_q"

at "n '......., ".; h.1f Icm\'Cr;lIU'Cof 1xI"",, l()().}Oll °F.

R,ni" ",11c 1'0' \\" ""1COl"': IT ", n: ,, tlo' 1"'"..1 1"''''''''' is a I" 'Ill"f)' e n,.,),.... funlal;c

"I"'rn tinn, The'" arc nIl " I"'male " l"' m11n1' ", ", lh" ' thi, i, ....."". "">C.

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.>. I>':sc'ir tiM of Ill," 1'" 11 ,,1,(\,, ('<mIlO! Equipmenl Will be M,,"il" rcd I)l1I in!, Te sting :

Prc"u", d",I" "ill he I1k'nil<l",d '"l anc'"lU,,1c<jui pnwm ,Iurinl' Ihe 10' t.

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InduflIlilll: MIlCh.",,: Tho: indur,lIi,,& lII.:1ehi"" plche:!t bun.e.$ " ill opcmlc 31 

bcl"OXn 1800 ami 1950 of for .he first prehe,,! :mile lind beI"",,-.., 2000 :md 

2250 °1' for Ih ~ 5«QlKl prehe"l lOll" at a i f'<.'I'd of Q\l1 7 fCOI (11."- mimlle, 

T"""'go "ill be: greater ,han )40 of flux pellels pcr 1100., 

Contml Equipm" ,'1 ncsc riptiurt: 

I"dnmt;"!: FIlnoac\" En\'iroll"",ing jl,lodcl ,\ 3) " l'nl"'; f:< od SCI1Ibl>c •• 

Indu!:II;"S ""x hine !.Crubbcrs . the pl'C'5su.o dmp "lOIs<' " il' be oclw«n ·9 · 

, 1 all opc'Dling disd~1f~'t' Icmpcr:lIllfC of b<: 1\'~ 100-300 °1'. 

2. Rmi"",,!e f or Wor.;! Case: Mi1lon:a"s fl ux 1"'11.:, PfOCC>i is ~ i inglc I" jm, ,)' "n's!le' . fUl1l;w,:c 

opemtion. There arc no nltem., I" """mling s.:c"arios.llms this ~ WOf'SI ,,:IS<:. 

,. No""al Opemt;n!; Cn p.,,,;.y " ill he Ih" 1\<1 "''' :IS opcmting tluril1S Ih o 1", 1. 

... lkscription of 11 0" I'ollu';on Control E'luipmCni Will be MOllilorcd Dming TC$I,ng: 

Pressure dlllf1 ~ ,, ;11 b." l1I{)n;lo",d on .11 control C'luiplTwnt durin\: Ih,' leSt. 

l 
I

PART IV. TEST METHODS I

A. EPA ~k ll"d I Ii" Ille h>enti"n " f "m,plin.,.; I'mh ~Tld ['<,i nts.

rxnr V. (' D IS !tElA T1VE xccunxcv

D. 1'.1',\ MCl h,><I 4 Ii" the d~ ll'nn ina ti"" " f ",,,i, t," e in lhe n"e l;'\'oC'. One te,t ,,'n e" neurrently

"i,1I eoch 1,·,t n", f,,, e\el)' pollutant.

II. EI'A Method 2 Ii" wlo<:i ly nnd .." I",netrie 11,\\\ nile. Three dct e"" n~ti", ,~ One

men, u,eUlell1 co ,,, ,, ll " irll each lest n u' fm e\ cry I"' lI l~nl.

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EI'A !\1eth,><I 7E f'" the de,,,,m;,,,,timl "f o,i,k, nf " iuntle" . l l"ee '>r,e-hour deterrni" ,,' ion, I ,, ;11 he eo"ducted

F.

C. EI'A Melhnd 3,\ for ~'s i" "(1" ..-.: dClen ninati" n" nne c~ ,uremc ll concurrently " 'ith

e~ tc,t no n f"rC\'cl), ['<,II "tm,1.

I

PAItT \"1. II :11

I. ,, \l tll ," " ill he reponed a< 1'1'''' :",d I.WIIK for NO,. I

2.

) n,,-e,iptioll , ,,d d,t" "fI "-" ", "' a"c e " urk d,,,,e I>cli',e h~ te, t'

0 ,," "''<llplete ['<1rt "illl>c , ,,I>,,,i11<·d "ithin ·15 days .Ikr Ihe t" of the lest.

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7. All SLlhm;nal, ,h, 1I 1>c Jdd"" ""d 10:

,\ ndy' I'b ee

I'e,f,'nn:mee Telt Cocm!i,,,,tor

~1I 'C Or1 11 Di, t,kt

520 blay"uc Koad

St. 1',1111. in ,, ,,' 55155-1194

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[,,\In' IV. TEST METHODS 

A. EI'A ~k lh od I for Ihe lrocnti on ofsmll plillS ports .. nd poi nts, 

n. EI',\ Method 2 for w locil)' .. lid \'olu",cuic flow mle. Three dclen" in ali ll~ : on" 

measurement co,wuncntly" itlt C~cI' t nLl' for c"c ry poll ulant. 

C. EI'A ~ k thod 3/\ for gas 'sis, 'O"'.:e dC en nin s: one measutemClI1 concurrently with 

"aeh teSI run for c\'cl)' pollutant. 

D. EI''' Mel hod ·1 for tlw dClcrmitlatim, of ",oistut<· in Ihe l1u<' g.1SCS. One tC.lt nln concurrentl y 

wi th each " 'S! nlll for e\'CI)' pollutant. 

F. EI' A 1',lethoo 7E for Ihe dc tennitt:ttioTi of o~idcs of IIitrogell, Tillec ouc·hour detcrmi""1 io1t~ 

will be conducted 

PAltT V. CEMS ItELA TIVE ,\ CCUItAC" 

NA 

I'AltT VI. OTIU:lI 

2. 

) 

5 

7. 

l'ollll1 nnts "ill he reponed as ppm "nd 1.11111 1( for NO,. 

List 3 11)" 51"--.;ial ",'er:rsins limes for emission limits if "rPlic" hk. 

Desc ription nnd date of I:l.st maime"anc" work done before the tcst: 

One complete lest rero" " ill h<: submim'd withi n -15 d"ys alier Ihe date oflhe lest. 

One microfid'c cop~' of the rcron ... ill be s""mined " ilhill 105 day . .. fter the dale of the test. 

All SLl"mittals ,hall be oJdrc,scd 10: 

/\ ndy I'b c.· 

1'.'rfon n.1nce T C5t Coonii"",or 

)T.II'CAfNonh Distric i 

520 L:lfoycl1e Road 

S1. I'mll. lI1 illtlesoto 55l55-1 19~ 

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APPENDlX J

SA'lPU:"G RA I~ CA LIBRATIO.'1 DATA

APPENDlXJ 

SAMPl.lroG TRAIN CAI.IBRATION DATA 
_ _ _ _ .. _ - - 11'< "'-1'0 ""'.,\1 """,\ I . '..... . ...... - - -

1(,11) 1111,.(,11141

- - -

M et er Clllihrn tion She et F.I'A/Metho d 5

IJilie " 0 ./,,, I..UnlfO l M OOUlc N O.

". ,

- Ilm.I'II:ss .19.t / IN.l IG Seri al No.on"n 1t ..., ~~ Wei Test Meier Nc . A!..2Q Technician

' ti'" JJ;; ACy

M G.. • • Go. Vol~", o G.. Tcmp<"I~ ..- Ti_ M.... 0<;('<0 e, l (IN WI:.) Volumo C., orr ().,. Tn t Mol•• c...rr. Con••.

W" InJ.. W" (ft')

'a'

M. ,•• M el.. W" ,~ 0.,. Tn.

I""",inal I\, u..l

" - V. V. '. (Mini V hll@

(ft'l ('f) '. '. $( ~) (rN.We ,) ('n ('F )

e.,

" ,

".• 0.01 k.<l.3f,.. 3;.." .'1D W of'- 77 !>' II 1.4101J I . J ("

• " t.t: ,

".. O,OH 3'-0.ti 3tSJ:i£.. U S J'9 77 S .o 'z. I .ilil" I ..r~

, J o , 100 00 ~~ .j"1 . 10 35"<1. 11.;' Cd . ? S; ,..- .o .;) I.til"" /. r«:

u J.\ , 100 ,00 e," U<,< L sn ""H- q < 71 7J <> If)09(' 1 5'i •

, • , • • • , • • .. ..

/l...J '" l co'ltf" I. i?

-

1>101., ..01 IlOl in lol.'ane . D ,.adju' l¢4li"k o••

M ol.. .... in ' 01" 0"'" ( Il'Y' M•••, ..", ,,01 ;" .01....... O :<"-'S¢d 4.,. •• " m.'••

AJ>I'«'_ ~y '-/\ 0.,. ;c------ --- ' n.. <d " " 1\I..l0 ......,••, '"''' ' . h~, '''' "' lI Nil )227 og. in. ' n.nr.o••' (lIllS T.....bl.) . Catl r O(Co.

r...il l. aIl (ho. k 1""''''

0121?7.0.ISTACK'wrflrollMSIS·OJalBII

____ • - - - I N ... I'il .... ,, I"",\ .~', . - - - - - -

(M l ) '"(,·(,U211 

Meter Cali bration Sheet EPA/Method 5 

Dnlc / &1 ~ r¥ 

D~r css .iTI/ IN.HG Serial 

Co"ml 

No. 

Moo,k 

DT"~ 

No. ~ 

. 

Wei Tesl Meier No. 

~ ...2! h , . 

G. • G<» Volum • ""I (IN.WI;.) I T;me M.I .. Or<lic< C. 

ol~_ D' 

"'" Dry Tnl M.I., Codr. Cnn ... 

W" ,~" W" (ft', 

T., ~ 

MOl., M ..... W" 

". ~ OryT"'1 

No".i .... 1 c"~'1 V. v. T. (Mini V hll@ 

(n'l ~'.) , 

('F) '. '. S. c) 

('F) ('f) 

-

' .S S· , ." .• 0.01 

~~",- iN "" 177 " ,I . . 

u E.. , ."., o.on ::f J"') 17 m 

I , 1" , 100.00 a.on 

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