# VES013871

. pdf

# APPENDIXF 

# Sampling Documentation

VES013871

## Un it 2 

# - Run 1
Pr o j ect Name 

### Veol i • Sou,et P r o j ect Number 

### 4094
. 2525

U

n i t 2 Unit 2 U nit 2 Unit2 Averages 

### 1 1 1 1 1A 

### 18 

### lB 18 10/8/2013 10/8/2013 10/8/2013 10/8/2013

11 :50 15:40 15:AO 15 : 40 

### 13:00 16 : 40 18:43 18:55 11 :50-13:00 15:40

- 1 6 : 4 0 1
. 5:40- 1 8 : 4 3 15 : 40-1 8 :55 D i ame t e r 

### ( ft t itqu#l> olent ifsqU«t MtJ 

### 3.21 3 .21 3.21 3.21 Tube Correct i :m Factor 0.84 0.84 0. 84 0
. 84



### Diameter (indies) 0.437 0.425 0
. 436 0
. 436 1.002 1.011 1.002 0
. 999 Temperature ('f) 68 68 

### 68 68



### Pressu r e Measured ( " 

### t-18) 29
. 89 2 9.89 29
. 89 29.89 {fl) {ftlat l ve to Baromote ,. 

### 34 34 34 34
DGM Te lll>{ ' F ) 77.2 75.0 8 2.0 83 .5 Delta H (in we) 

### 1 .6 2 1.39 1.72 1.41 Water :Sl 

### 604.9 649
. 5 1500.4 2072.3

( monutes) 60 60 120 180



### ("H,O) 0.02 0.02 0.02 0.02 M

o n ox i d e 

## ;co) C ont ent (%) 0 0 0 0 Diox i d e ( C0 1 ) 

### Content ( %) 6.35 7
. 95 7
. 95 7.95 (0 1 ) 

### Conten t (%) 11 .5 6 10
. 0 8 10 .08 10
. 08

(H 1 ) 

### Content(%) 0
. 0 0.0 0.0 0.0 (CH.) Content (") 0.0 0.0 0
. 0 0.0 (N,) Content(%) 82.09 8 1 .97 81.97 81.97 Vo l ume (acl) 41.365 37 A 20 86.843 124.679
850.1 849 .3 44.10 44.10
37 .384 Gas 

### Volo<ity 30.50 29.97 31.41 30.05 3 0. 4 8 Flow Rate (aofh) 887,777 872,197 914,101 874,661 887,184 

### Row Rate (adm) 

### 1 4 ,796 14 , 537 15,23 5 14 ,57 8 14 ,786 Row Rate {set>) 

### 550,260 539,756 567,438 544,139 550,398 Row Rate (sclm) 

### 9,171 8,996 9, 4 57 9,069 9 ,173 F

l o w R a t e ( d scftl) 323,699 296 ,49 1 309,383 301,009 307,645 F

l o w R ate (ds c lm) 5 ,395 4 , 94 2 5 , 1 56 

### 5 , 017 5 , 1 2 7



# VESO J 3872

## Un it 2

- Run 2A Project Name VeOIII Sa uc et Project Numb er 4()9.42525



# . F adli Comprehentill<! 

### Performonce 

### ty Test U nit 2 fSamp le Type MS Averaaes jsource Unit2

### ~onditlon 1

### ~un 2A

### ~ate 10/9/2013

### tnm~ Start 09 : 45



### i me Stop 10:53 09 : 4 5· 10 : 53 Duct Diameter (fl) 

### · <- rlf-dua} 3. 21 itot Tube Correction Factor 0.84 Noute Diame t er ( I nches) 0.437 OGMCF 1.002 tandard T emper r.u re ('F) 68 Ba rom etr i c PressUie Mea sured ( " Hg) 29.85 

### tack E . l evatlon (ft)**(;(~a:~** 

### to**B~rOmeterl** 34 Baromet nc Presswe "H 29

. 816 Averace Stack Temperature ('F) 389. 8 389.8 Average D G M Terrp ("f ) 70.7 Averaee Delta H (In we) 1.63 

### Condensed Water 

### Cil 638

. 5 est Duration**(mir utes)**  60 Static Press u re ( " H,O) 0

. 02 prbon Monoxide (CO) Content (") 0 prb on DioJ<ide (CO ,) Content !") 6 .5 6 PJCYgen (0 2 ) Content(%) 11.23

### ~ydrogen (H,) C:O.tent 

### I") 0

. 0 r,etha ne ( OiJ Content 

### I" I 0.0

### ~lttogen (N 2 ) Con tent( %) 82.20 Meter Vo l wne (ad) 42.4 63 f\verage square root of liP**(l~t.P)** ) 0.40 3 Absolute Stack P rusure ( " H8 ) 29

. 82 Abso lute stack Temperatu r e ( 'R ) 84 9
. 8 849.8

### ~ue Gas Mo i sture 

## 1"1 41 .59 41

. 59 

### Mo i sture at 

### saturnlon N /A 

### Moist ure used in Cala.dation 41

. 59 41.59 Gas Molecu lar W eig ht (W et)

### (g/g·~:: 24.72 l:o<rected Volume of Gas samoled ( 42.548

o lu me 

### at Meter (dsc:f) 42.3 5 6 Average Gas VefQtlty (fl/s ec) 31.0 7 31

. 07 Avg F low Rate (acfh) 904, 2 04 904,204 Avg Flow Rate (adm) 15,0 70 15,070 Avg Row Rate ( set h ) 559, 910 55 9,910 Avg f l o w Rate ( sctm ) 9,332 9,332 Avg Flow Rate (dltfh) 327,067 327 ,067 Avg F lo w Rate (dmm) 5, 451 5 , 451 I · 

### <• • lin • A;t• I'll;\ 100 .5 2

F · 2 

## VES013873Project Nam e Project Num ber 

### Facilih F>•mple Type

### ~ource Co n d iti on Run

# ~·· tnme Start lr1me S t op Duct Oiameter (ft)**""""''*••****><~•.,.doctl** Pitot Tube Correct>>n Fac1or**~onle** Diameter (mche$) pGMCF**~tan ard**  Tempera t ure ('F) Barometric Pressure Measured(" Kg)**~tack** 

### Elevatlon (It) 

### c .- ... _ B arometric Preuure ("H•l**~ve rage**  Stack Terrperature ( ' F) fve r age OGM Temp (' F )**~verage** Delta H ( i n we) f-ondensed Water ( g) lrest Durat i on (minutes) f>latic P ressure ("H.O) Car bo n Mono•lde 

### ! CO l Conte nt (%)**~arb n**  Oio•lde {C0 2 ) Coo tent (%) bxygen (O,) Content(%) Hydrogen (H,) Content 

### I"J Methane (CH.) Coot ent (%) Nitroge n {N,) Con t en t {%)**~eter** V ol ume (acf) Average square root of Ill'**((114Pl~l** AbsoiUle Stack Pr5$Ure ("Hs) Absolu t e Sta ck Temperature ('R) fl u e Gas Moi s t ure(%) Mo i sture at SDturctio n 

### Moisture**u~d** 

### i n Calcu l ation Gas Molecular Weight (Wet) (i/g-mote) <"orrected Volume of Gas samoled racri Vo l ume at Mete r i dscf) Average Gas Ve l odty (ft/sec) Avs Row Rate (odh) Avs Flow Rate (ac'm) Avg Flow Rate (scll1) Avg Flow Rato ( scfm) Avs Flow Rate {ds:f h) Avg R ow Rate (dsr.fm) l so kl netic Samollro Rate'"' 

## Uni t 2

- Run 3
V.oliaSaucet 40942525 Comprehensive**Perform<~** nco lost· Unit 2 MS ModM26A M29 M0023A Unit 

### 2 Unit 2 Unit 2 Un i t 2



### I I 1 1 3A 38 38 38 10/10/2013 10/10/2013 1 0/10/2013 10/10/2013

09 : 15 12:30 12 : 30 

### 12:30 10 : 23 1 3 : 30 15:10 15:40 09 : 1S.10 : 23 12 :30

- 13:30 12:30·15:10 12:3()-15 : 40 3.2 1 3
. 21 3
. 21 3
. 21 0.84 0.84 0.84 0.84 0
. 437 0 .425 0.436 0.436 1.002 1.0 11 1.002 0.999

68 

### 68 68 68 29.82 29.82 29 .82 29 .82

34 34 34 34 29.186 29
. 786 29
. 786 29.786 391
. 2 396.4 393
. 3 39S.S 7 0.2 8 1.3 84 .0 88 .1 l.S5 1.38 1 .48 1.4 1 632.1 669.0 14ll
. 8 2096.1



### 60 60 120 180 0.02 O.Q2 0.02 0.02

0 0 0 0 6
. 28 7.50 7.50 7
. 50 

### 11.48 10
. 38 10.38 10.38 0.0 0
. 0 0
. 0 0
. 0 0.0 0
. 0 0.0 0.0 82 .2 4 82.12 82.12 82.12 41.3 9 2 3 7 .857 81.2 43 124
. 366 0. 393 0.409 0
. 402 0
. 411 29.19 29.79 29.19 29.79 851.2 856.4 853.3 8SS
. 5 4 1 .9 7 45
. 87 4 5.78 4 5.29 N

/A N/A N /A N /A 4L97 45.87 45
. 78 4 5
. 29 24
. 65 24.29 24
. 30 24.35 41.475 38.273 8 1. 405 124.242 41.278 37.290 78.951 119
. 568 30.42 31.95 31
. 36 32
. 05 885,200 929,8 98 912 ,708 932,661 14 , 753 15,498 15,2U 15,544 546,619 570,763 S62,264 573,054

9 ,111 9 , 513 9,311 9,551 317 , 24 9 3 08 ,979 304,833 313.504 5,287 5,15 0 5,081 j 5,225 100
. 99 99.04 100
. 97 99.)3 Averages

394.1

854
. 1 44.73 44
. 73

31.44 915,117 15 , 252 563 , 190

9.38 7 311,141 5 , 186



# VES013874

## Unit 2

- Run 48
Pr o ject Na me Pr

o j e ct Num ber 

### Fa cill "**~mp leType**  fSource 

### COndit i o n fun oate Ti m e S ta r

t Tlme Stop Duct Olan n :h: r (ft)**(itfiV~ol t:** **l'lll/** sq uo' 11 tNttl Pitot Tube Corre«ion f act or N

ozz le D i am ete r (i och es) DGMCf Standord Temperawre t•F) Baromet r ic Pressure Me a sure d ( " Hg)**~tack** Elevation 

### (It;**C~tlw** t o """""''"' Ba rometr ic P ress t.ro I'H • I Ave ra ge S t ack T emperatu r e ( " f ) A

verage DGM T em p ("f) Av e rage Delta H (I n w e) tondensed Wale< 

### (s l

es t Duration (millvtes) Stalk Pr e ssur e 

### ("H,O) car bon Mono><ide (C O ) C ontent(") arbon Diox ide 

### ( C 0 1 ) Content(%) Oxygen 

### (0,1 Content{" ) Hydrogen (H 1 ) Co1tent 

## 1"1 Meth a n e (C H ,) CDn ttn t (% ) N

it

roge n {N 1 ) Co r t en t(%) Met er Volume ( a d) l\lf

ero ge SQuar e root o f AP**((~llPlul** llb solu te Stack Pre ssur e ("Hg) A

tw> lvte Stac k T o mperature ( • R ) F

l ue Gas M oisture 

### {%1 

### Mo i sture at saturat i on Mo i stur e 

### Y s.od i n Calculation Ga s Mo l ecula r Weight {W e t) (g/g

- mole) Com-cted Volume of Gas samoled lacfl Vol ume at Me t e r ( dscf) A

v erag e Gas Ve l odty (ft/se c) Avg Flow Rate 

### (acfh) A

v g Flow**R~te** (acfm l llvg 

### Flow Rote (scfh) llv g Flo w Rate (scfm) Avg Flo w Rate (d s cf h ) Avg Flo w Rate (dscfm) sok l netic Samolno**at ~**  Veo l i<o S. uget 40942525 Comprehenslw Performan ce T est • Uni t 2 ModM 2 6A M29 M0 0 23A 

### Ave r ag e s Unh2**un~2** Un i t 2



### 1 1 1 48 48 49 10/11/2013 10/11/2013 10 /11/ 2013 09 : 4 S 09:45 0 9 :4 5 1 0:4 5 1 2: 25 U:55 09 : 4 5-10: 45 09 : 45

- U : 25 09 :45-1 2 :55 3
. 21 3.21 3.2 1 0
. 94 0. 94 0. 84 0 .425 0 .436 0
. 4 36 1
. 011 

### 1 .002 0 .99 9

68 68 68 29.74 29 .74 29.74



### 34 34 3 4 29
. 70 6 29. 706 29
. 706 391.3 387.6 390
. 6 389.8 74
. 7 7 4.8 

## n A 1.28 1.3 9 1.33 631. 2 1382.8 2087.3

60 120 

### 180 0
. 04 0.04 0. 04

0 0 0 7
. 69 7
. 69 7
. 69 1 0 .1 8 10. 1 8 10. 1 8 0
. 0 0
. 0 0.0 0.0 0
. 0 0
. 0 82
. 13 82
. 13 82.13 36
. 206 79.1 38 121.269 0
. 394 0
. 3 95 0.402 29.71 29.71 2 9 .71 851.3 947
. 6 85o.6 849
. 8 4 5 .29 4 5 .:>7 4 . :i ,40**S.~2** N/A N /A N /A 45.29 4 5
. 57 4 5
. 40 45
. 4 2 24
. 37 24.33 24.35 36

. 604 79. 296 121
. 1 48 36.003 78.003 118.568 30.71 30.7 4 31.32 3 0.92 893,784 894 , 553 9 11 ,6 6 5 900,001 14,89 6 141909 15, 194 15,000 5 50,4 72 553, 3 2 9 561,924 555,242

9 , 175 9,2 22 9,36 5 9, 2 5 4 30 1,1 3 8 301,181 306,832 303,050 5,0 19 5,0 20 5 ,11 4 5,051 98.11 100.97 100.44



## VES0 1 3875

## Unit 2

- Run SB
Pro je ct N ame Pro ject Num ber FadUty jSamp l e Typ e 

### !So urce Fondl li on Run

### ~ 

# .. h' l me Start tn mes to p**~t** O io meter ( ft )**'«q.~l'w'k "'t**  

# if,.,_ ,., ctwt)

### ~hot T ub e C<>rrectlon Factor

### otzle Diameter (ioches) OGMCf

### tand**ard** Tempe r a tu r e ('F) je.rometric Pres su re Measured (" Hg) Stack E leva tion ( ft) {rel.1t1Ye to 6arometer) 

### B arom etri c Press u 'e I ' H•l**f<~verage** 

### Stac k Temperature ("F)**~ver.~ ge**  

### DGM Te mp ('F) Av era ge De l ta H ( i n we) P,ndensed Wate r ( g) h' es t**Dur.~tlon** 

### (mir.u t es) S tatic P r ess ur e**{"~ )** **~arbon** 

### Monox i de (CO) Content(%) prbon Diox id e 

### (0 2 ) 

### Con t ent 

### l"l pxv8en ( 0 2 ) 

### C

onte nt(% ) liydrogen (H ,) C<> nt en t (%)

### thane (CHJ Content 

### l"l**trogen** 

### ( N,) Co nt ent(%)

### ter Vo lu m e 

### ( acO "ve ra ge square root of 6P**((~APl.** 

### )**~bsolute** 

### Sta c k P ressu r e (" H g) f'<bso lut e S t ac k Tem pera ture ('R)

### ~ue Gas Moisture (%)**~oisture** 

### at Silturation**ols ture**  

### u sed i n calcu l ation

### as Molet ulor W elct>t (Wet) (gig-mo l e) Corrected Volume of 

### Gas
.. ,;p;.;d {ac0 f.lotume at Meter(d sd )**f~v ero** **ge** 

### Gas Velod t y (It/ sec) 

# "'va Flow Rate ( adh ) Avg f low Rate (a cfm) Avg fl ow Rate (s cfh) A"8 Row 

### Rate (sdm ) Avg F l ow Rate ( d;dlt) Av

g flow Rate ( d; d m) lsokinetic Sam ol i n• Rate 11>1 Voolla Sauget 40942525 Com 11ehensJve Performance Test- U11t 2 

### M od M2 6A M29 M00 23A 

### Averages

Unit2 Unit 2 Unit 2

1 1 1 

## SB 

# sa 5 8 10/30/ 2 013 10/30/2013 10/30/2013 12: 4 5 12:45 12:45 13:4 5 15:32 16 : 0 2 12 : 45-13 : 4 5 12 : 45-15:32 12: 45- 16:()2 3.21 3.21 3. 21 0. 84 0.84 0.84 0.426 0
. 438 0.437 1.011 1
. 00 2 

### 0.999

68 

### 68 68 29.70 29.70 29.70

34 34 34 29 .666 29.666 2 9 .666 392.0 386
. 3 389 .1 38 9.1 75.1 78.9 74 .6 1.3 3 1.47 1.56 609. 1 13 14
. 1 198 8 .9

60 

### 120 

### liD .0.03 .0
. 03 .() .03



### 0 0 0 7.25 7
. 25 7. 25 1 0.5 0 10 .5 0 10.50 0. 0 0 .0 0 .0 0.0 0.0 0.0 82.26 82
. 26 82.26 37. 16 1 81 .488 127 .1 92 0
. 40 1 0
. 401 0.427 29.66 29
. 66 29.66 85 2
. 0 8 4 6.3 849.1 849
. 1 43.82 4l
. U 42.92 

### 43
. 52 N

/A N /A N/A 4 3.8 2 4 3
. 8 1 42
. 9 2 43.52 24.51 24 .51 2 4. 61 37
. 57 0 8 1.65 1 127
. 065 36.8 79 79.60 7 12 4 .921 31. 2 1 31
. 06 33.10 31.79 908,296 

### 903,845 963 , 377 925 , 172 15,138 15.064 16 ,056 15, 420 55 8,0 6 8 5 59,1 06 593,94 3 570 ,372

9,301 9,318 9 , 899 9,5 06 313,5 23 314 , 180 3 39 , 028 322, 244 5,2 25 5 ,236 5 , 6 50 5,3 71 

### 96.08 97.89 

### 95.33



# VES01387 65ample Type

- Partlwla te Motte r ( M el1 wd 5) 

# Dlst e7 {)- 1$

- { 

## <, Fi ll et No

. Page 

# I ol 

# I Pro)ocl Name : Veo Ua • S.uget. IL Qrdtlan; 1

# ~K 

# 7.5'0"1 Train Lea k Rate (dm 0 'H!I) Project !'lumb er: 4094252s.30-o2 RtJn: 

### I A**~O<Ji e**  10 

# - lr;tlal 

# I> llt'1 4 

# e I ') FadMty: Fbced Hearth • Unjt 2 COflS<ie ID A 

# I!./ '1, 

# 41 N oule O la (

il) 

## l'l.lf 

# 3 7 Anal 

# o. Oo I 4ll 

# 5I**~: tack**  DGMCF 

# I 002.. 

## s--norer 10 

# /3 P- 

## 2. Pltot Tlb! 1 0 

# f>
- 3 0 

# <' Op erat or: 

# 71\? AH@ 

# ( 7Cro Baf. Pross. ("119) 

# ;<"1 

# f1 PTCF 

## 0 ,**~-**

## Duct~(s)**· 3~~** **" t~L~**  Kf 

# l {J 7C/ -· Preos. {"li,, ) 

# /J, 0 

# :z_ Pi to t Tube L 4a k 0\ac k NouleC.Iibfodon 

# -e- tJ
. '13P · " 

## o . CJn ._ tJ
. 'f

F BevaUcn (1\) lritial**(+)~/3 (·)~;>** **)** 

### Coli-n> 

## 7jtJ'!i.o "3**~** 

# ....... _, 31 Anal 

# < •>oc:e ::- · 3**(·)"~']** 

# - OodcTme Oty Gas \d (It') 

### t.P AH TemperotL<e (•f) 

### varuun (!11. H,O) (ln. H,O) Stxlt 

# ,_ 

# - Itnp Belt OG.'lln OGMOut (il. Hg) 

## 1,./f 

## I 

# 1 --z; 0 

# '-jq7**~5'1** 

## {)

. I 

# 7 I. I 

# "'Jtf I 

# -;{_ 'H · =!ft2 

# t3 . 

# 7'f 

# 3. 0 

# c-,-z lt <Z:**~t'k'** 

# 5 

# 1- r) / 7 

# (<{,**') ~2**  

## 1. 

# 'I<'( .2.0 

# s' 7'\ 

# 'l.O /,.,j'f 

### Jl. OD 

## io)."i 

# 0
. /C. 

# IX' 3'1 1**2-5~ <~<;**  

# 53 7") 

# :'1. 0 0 3 

# i) {)7,**~5** 

# I {I 

# 17 

# 7.'l**~q,z** 

# 2s< :u r.. 

# u.. 7'} 

# l\.**!,~** 

## 1 2 / D 

## Y' l 

# f.( 

# OF ! :l

. D ·y1 2.**2~ s**  

## 2!. 'f 

# I. 7;:. 

# 5.c.l wj 

## lllj

# ~15/l 

# 71

. / 1. /,'f**~I** 

# ul r 2.r. "2. 

# (,.,?/ 

# - 77 

# <:. ( <f'Df 

# 172 o 1'1r. 

# n:z. ••**~** 

# (.. 

# .k.h 11 c.oJ b 7"! ).. 

# ;Q 

# r h.t J := 

# 6 tlO 

## [),.-;o I 

### 7' Wf•l

## 5~ 

## 1 7 

# 3 {) ¥' 1 ( 

# C.. IJ "t., 

# I O.! Z ' f

. 

# 3**~0 ~**  

# 1. 

# ?1

# '<**~** 

# - It; 

# 4-co 5( /7 

# 7:7: {2/
. 4. 

# o. T<i- 

# Tt.,**)("~** 

## 7 

# <z. l..C'f 

# lt-'1 7ff 

# 4-:C:.**~Jt 17** **~0** 

# 714.7 

# (} r ? I 

# < 

# 1 -z."l i "? (l**7t:: ~**  

# l lfL /l;' 

# 4<**~** 

# 17 If: ?; 

# tz:6''F 

# r/,, 17 , - <(: 

# 3 '1 2 

# :2.-'t 3**::u~** 

# Lff.**7~** 

# <'> '52 ' ) 2 

# < D 

# y · <,..2. 

# 2 I 

# fl 

# IL I

. 

# 7 "- / 12 

# 7. 5f{

## 12~**<** if<{ ' 

## - 4'1)**~** l 

# 51 

# ! T«**~~ q**  

# o Fi { S '(j ij 

# ; 2<) ") 

# :ZN ¥1 

# -ro**5' ~**  

# 51oP {\f')Q 

# nq 2 1.s

Co<T'fnents: 5l>S·26 ' PM by ePA Me thod 5 Pv EM SOf'.QJ5 i&Yi:IAifl I).:J M :**F~** 2t)J2**~t..nc.~~2011** 

# VES013877

# < [Tl 

## en 0 

# ...., 00 -.1 00 ProjtctNa:tM Veo ia-Sau c et.IL Project Number 4094251S.»>2 Cote 

# to/3 /13 Source lJnh: 2 Stade 

# Moi s tur e D ete rmin a tion Im p No
. 

### COnte
. nts Vol (ml) 

### Confil:untlon final 

### wt (I) 1 Wate.r 

### 100 Mod

### Cf~o.z_ 2 Wi t er 

### 100 

### G/S 

# t oo7. 1 3 Empty 

# - Mod 

# 762-. I 4 

### SiDcaGel "300& M od 

# Cf'fl 

# .3 5 6 !,.,_,_

- -- -- - ----- ---------- 

# S a mp l e L og SSmplt 10 N umber Samp l e Container COndition No. 1 

# Particu l ate Matter EPA M e thodS Run No. 

# i A Bat•nc • ID 

# / £**~/{)1** 

## ,4

Initial 

### wt 1111 

# 71/'1. 

# z. 751
. 3 (,'ft.. 

# r Cft 

# 't. 4{- i

Otscrf!>tlon 

# I Roa>vtro<lby 

## .J;lpl"\ 

# / Samp l e R eco v e ry C h ec kli s t

__ RJnse and brush protJe and noule w t tn a:e t one l nto PNR sample bottle
.**~** Transfer bottle(s) to laboratOIY 

### with impinge< train
.**~** Separate filter holder and place fil t er in dean pre-rinsed aJ•ss pet ri dish
. Complete filter sample la be l
. / Rinse front

## ha~ of fi lter holder with acetone Into PNR botde
. Comp l ete probe and nonle rin$2 (PNR) sample I obe i. / Disassemb l e sample 

### train, wipe off excess wate r and weigh each lmp i nger . Re<:Ord the final weights In the M oisture Determ i nation section of this data / Note

### cond**lon** of the s ilica ae l lmp ln ger. "'Z--0 % spent / tog samp l es into logbook an d store appropriately.

C

o mm e nts 1/52-STK·l 

# f A -MS

- PNR 250m l Probe a nd Not tle 

# l

IJS2 · STK · l .JA... · M S · Ait Pet ri Dish



# ... 

# " Rinst! ' Fitter

---- - -----

ROS·JJ: PM byfi' A V.cllwKI 5 Pu 

### Ei11 SOP-lJJ!J**R'~** Ootc : Jc fl.ll:rY 2013Simple Type : HCl, Cl, ( M<>dlfled**EP~** Mtthod 26A) Date 

# /6· 

# P -I 3**r.M~e.r** N o . P a&e o f 

# J V

eo ll a . S aueet, ll**Condlt~n :**  1 / 

# N'A Projec.t Name : Semp4 inl Train Le1k Rate Cdr.. o ..._, Project Numbe r: 4094 2.5"2 S.3 D-02 Run · : 

## _Le NonleiO 

# - ln'tia l 

## o . o•<t 4f**t~ -0**  FacUlty : F'uc:ed Hearth · Unit 2 

### console oo**MI./~** 

# 'IS Nozz le Ola (kl) 

# 6
. -.v.; fl"> l 

## (J , d01.

. @> /(}.,() SOu rce : Stack DGM Cf I ,OJ( Barometer 10 

# oN. Pl to t T ubt i D

### ~**"f>52~** I O

pera tor 

## lcAMM. GH4f 

## I.

## ~zH O.r
. PIOSL ('1'£) 

# 2 't
. _ &'f
_ PT(f (l 

# . !.,"\ Duc t Ol""'n s lon(s ) 

# 3 B5" Kf

## '1'.~ Stat
. PTe "
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# -- -- -- -- -- -- ---- ---- -- ---------- -- ---- Sl>S-0 7 Mc!Dis by EP A M<tMd l9 N E M**S~ 0/** **7 v/;'20/** **J** 

# VES0 138 81

# ~ Cl.l 0 <H 00 00 N Condfdon No

. 1 Project Name Veoll - s · aucet, IL 

# Multi-Metals 11\Jn Ho- / 

# B Prl)jett Numbef"**40941S25o.l0.0~** Date

# 1~/? /1 3 

# No Determination of PM EPA M e thod 29 Baionce 10 

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### i on 8.l.3.2) 

# Samp l e Log Sample tO Number Sample Desa lptlon Contain ers 

### VS2

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## VS2.·STJ<. · 118

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# -

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## Sa mpl e Recovery Checklist Rinse and bc\ 10<1 (lrntw- wntt**nnu ~**  wi th O.lM n l tr\c tdd i nto P NR bott l e. Note

- u se Teflon brush

. usc a tot"e l of 100 ml f o r the PNR and f r o nt-h a lf filt e r**ti n~.**  Ri nse the (op<iOIIaQTeflon 1ransfer tine w1th 0.1 M nltrlt acid I nto Nl bottle. Use o tota l of 1 00 m l for tile transfer l ine and lmplnger rinses. Sepantt filte r holder and piau niter In cletn Petri dlsh..**COm~te** $ample labe l Rinse front half 

### of fUter ho'dt.r wtth O
. lM nltrk: ad d i nto PN:R bott l e. Use a tota l of 100 mL fo< the PNRand front-hoW**~r** rinse. Complett PNR sample l abel Ois.-ass emble Simp1e tnln, wtpe 

### off ew:ess yqter atd weigtt tidl i mpinge r. R.KOf'd t'bl fina l weiC)lts In tho MobNro oetannlnotlon section. Notecondltionolsillciao L 

## "':l O "'pont Pour contents of Hnt l tmplnsers Into the NhrtcJperoxide impineeratcll bo ttJ e(s ). Rinse the tmp i ngers, f il ter support end 

### badc·half of the fi tter ho&W and c:oonec:t i ng 

### gJassware w1t h 0.1 M nit(oc 

### acid nm• b cmle{s). uv. • total**o~mL** fo< 

### tht tmuler fine and impi n eel' lii\St.J
.**Comp~te** Nl sample l abe ! (s)

. 100 Rinse the 4 ,. (in it ia lly empty) lmplncer 

### with O.IM nitric 

### ac id i n to the tl'n9tv lmp l ncer r lns o (EIR) bott l e. use • to t o l o f 100 ml fo< this rln•• · Complete E I R sample Iobei
. 

### Pour the 

### contents of the 

### 5 1

,. 

### and 6tt.1mp i ngcrs {penn<lfl& anate im pin..g ers) t nto the porm a n ca nat e l m p ln g er eatch bott l t ( P erm). Rln" wltlla tot>l o f 1 00 ml of 

### pe:rm01npnate so lu uon and tOO m l of 01 water .**Cc~tte** 

### Pe r m s a mp.., I a bti Put 100 m l 01 water Int o HORns**s1mp~** bottle. R.ii\Se t'he pe rmanpnate i mpin&t r s with a tota l of 25 mt of 8N HO into the .sarne bottle. RJue im:pinger s wtth 100 rnl 0 1 W l t ef i nto the same botda
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# o..I'W**~ .~~** **~ kj!~c!wr-** **.** SDs-11' I'Ct>OIPa>F by SW..fi46

..... 11N>dOOZ JA lfe,o£M SCJl)-t»J**II• >~~~<M&.fcl~zoJl**  

# VESOJ 388 3Project**~** Veol ll. -Sauret. I L. Projlct N\lml>e< 4094252.5.3U2

# oat~ 

# te 

# / '?" (!.3
SOurce Unit 2 Stack 

## Mois tur e Oetermlnation Imp Conh!nts Vol (ml) 

### Conflcuration Anal Wt (g) 

### No
.

I 

# . 

# - K/0 

# t't?(J 2 H 2 0 -I(X) G/S 

# ?3o.o 3 

### H ,O 

## -too Mod 

# -:m : t 4 Silica 

### Gel -30 0g Mod 

# f8(.'1 s 6 

# Sa mple Lo g Sample lD Number Sample COntaine_.r 

### VS2 -STK·1 L

- M0023A-PNR 500ml 

### VS2-STt<-1 ·M0023A-Filt Petti**Db~** VS2•STK·l_

### ~ •MOD23A-e'R 500ml

## VS2**STK·~ M0023A-XAD**  Sorbent 

### Trap



### 1' 

# < u 

# g] 0 

# - w 00 00 

# ""' Condition No. 1 

# Dioxins and Furans SW-846
- Method 002 3A Run No. 

# I 

# {3 8alantel0 

# 775-**~f** 0 I 

# A

Initia l Wt. (C) 

# '/3f;,.O 

# 7.Z g . 

# 8' 72 (,
. (p 

# rso . Lf

"-"f'lon Probe •nd Nou l o 

### Rlruc Fllt!r Cond•,.,.,. Rinse

XADSorbent Reco.,.red 

### bv 

## Of? M 

# Samp l e Recovery Che c kli st _L_ Rinse and brush pr obe and nozzle: three times with acetone , twice with m ethylene chloride and twice with 

### toluene. R ecovor I nto one bottle (PNR)
. _..:::'_ Separate filter holder and place

### f~ter In dean pr e-rtrued, glass 

### petri dish. complet e**F'~t** 

### sample label. 

## _:L_ Seal XAD 

### trap ends. Complete XAO 

### samplel•bel. 

## v Rinse front half of 

### filter holder Into PNR 

### bot1le: three times with acetone,

- -- twice with methylene dllortde 

### and twice with 

### toluene. Complete PNR samp l e label. 

## I

_ _ _ Disa ssem b le sample tr ai n , wip e off 

### c.xuss wate r an d 

### wei8h eac:h lm p ln ger . 

### Record the final weights In the M oistu re OO(ermlnatlon section. DISCARD the lml>in&er solution
.

_ _ "'
_ Note condition of the silica gel implnger. --"spent

__ /_ R inse th e ba c k h alf of the fi l ter ho l der, Teflcn transfe r li n e( If used), all 

### connectins glassware 1 and the coU conden ser : three times with ltCeto ne. 

# I twice with methylene chloride and twlce with 

### toluene
. Complete CR sample label
.

_ _ _ L og samples i nto l og book and place In refrqerator or Ice chest
.
Comments

RDS·30. ·**Otoxfnsrrw:!Flnllti,SW..U&~A MMd:J**  Prr EM SOP-<123 ll.Wsitrn**Oct~ :**  JtJN<rY 20/J

### U-**em _;_p_le** **_T ype** **~-- PC** **DD_;_/ Pc** **F** ( :.... M

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# :2- o f 

# z_.

Tfll ln luk Rat e (dm § "H1J Proje(t Humbor: 40942525.30412 R u n : _L s**NO D** **~** n i da l /" • 

## Jl , 1**IF~clllty:** flxf<l H<tl rth

- Uni t 2

### ~rce: St&ck


### D

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## "5 

## C
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### 700 91'\



## 5

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# ?:::I

N oted : 

# - · OrfGIIV o l
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### t'\
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## f6/illl**Noni•D ia(i** **nJO .~'fc(**  D GMCf 

## fJ

. 

## 9 

# ff Barom<t<r 10 

# ,t /J- '2.. PhotTUboiD 

## S" · 

# G/'

K f

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. Press. ("H,OJ 

# 0
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### (+l c 

### "" !;J
. I ( · J
. f



### Sl>S-m /IC1){)/Kf)l'by SW41 46 t.' ,. th«/002JA**PuEMSOP.OZ~** Rcw'sion 

### d4t<i ' 4A/N'If i!O

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## VESOL3885

# PK J-5ro**~** 

### 'l'rPe

- Particulate Hatter (Mdllod 5) Da< e 

## f ()- 'j· 1 

# 3 Projfcl Nome : V ftOJi a ·Sau get. IL Co<l! Jt lon: 1 Fitt er No . Pa ge 

# 1 

# ot ; Train L•ak Rote (cfm 

### 0 ' H g ) 

### Pro!«t _, 40941525.30-<12**~~m :**  

## k...A**4ou~e** t o .__**wt~a~** 

## (}. (JO '(-**~** 

# !5 Fodlily : FlxcdttearUt - U nlt2 

# ConsoloiDA ff. i"<, CJ Cf N o rne Oia (ln) 

## /?
. 4<.3_2 F i na l 

## (J 

# 0 0 

# < 4:> 

# 1 0 SotrCe : Stll ck DGH CF ( 

### (J 

## 0 

# z.**~** 1 0 

# ·fl.. P- Pitot T ube 10 

# p _ 

# 3 0 ;:t



# w 1- 

# M .; 

# 'l "133
. 1 o- r h •.**~** 

# 1 '16 2**~'i** 

# 1 

# t.c. l.f¥ · 

# t c. 

# '1: , W'3 

# Jo o oq -::. 75 0
. 17 1.7 3 '102S 1 :u.." i 

# .Lj · C**·** 

# t 5**~5** 

# l oH**~/ c;**  

# O .fl 7 '3'1 0**7~'i** 

# <C1 lfq I f 

# 1 5
. 0

SO.S- rlk PM byB' AMc t lfDd S Por EM SOP- 015**ll ~l>ltt#** **F~ 20/2** **Ro"'-cdi' 2013**  

# VES01 3 886

# r;i en 0 

# - w 00 00 

# _, 

# 4'**~i** P ro)e< t Name**\l on~-**  Sau

. cet, fl P rfij tct Number 4094252.S
. 10.ol. Date 

# !o/9 

# /!3
SOorce Unit2S tedc 

## M o i sture Determin a tion**lm~No.** Contonts Vo l ( m l) Configu ra tion F i n a l W I(&) 

# n- Wate r 100 

### Moo 

## Cf.2/.**~** 

# /3 Water 

### 100 G /S 

# <J 51.!> 

# Tlf Empty 

# - Moo 

# (pS'/. 

# 7**~~** Silica Gt l 

### - 3001 MOO 

# 951. 

# <t 

# 11 C... t>ty 

# - Ko**'f~.'f** 6 

# Sa mple Lo g**Samp~** 10 Numbc!:r SamP'e Contatner Cond l & n No. 1 

# Particulate Matter EPA MethodS Ru n No
. 

# :Z 

# A
Bo l

an« I C 

# I£ 'flo/It

I nit i a l 

### V II (G ) ' 

# 7#..8' j 

## 7 53.!!{" i

## ~£!-F..:i... i 

# 't'f!

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# S11
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## -.pf/111. 

# S

ampl e Re cove ry Ch ec kli s t 

# ...L_ Rinse ond brush probe and noule with aceton e Into PN R samp l e bottle.**~** Transfer bottfe{s) to labo ratory w ith lmpln ger train. _::::__ Separate filter holder and place flltorln dl!ln pr« l nsed glass petri dish
. Complete filter samp l e l abel. __:::___ Rinse front half of Olter holder with ace to n e I nto PNR bottle. Co rnp le te prob e a n d nou!e rinse (PNR) sample labe l.

## ~ Oisassemb le sample train, wipe off excess water and weigh each l m pinger
. Reco r d the final welshts In the Mo ls1 ure Determ l natioft section of this daUl __:::::._ Note condition of th e s ilica gellmplnger-:-'5'"'0% s p ent 

## .....J:::::_ Log .amples In to l ogboo k and store ap prop riately
.

### commtt~ts~ 

# /Mad SS KO**·;,Lu- e-,.t-y**  

## \ 

# a._. "- VS2

- S T K

- 1 2A

- M5-PNR 2 50ml Probe and =t ie

### ~ 

## ... 

## fL k
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# al.-e J**~f'** 

# -.--...L VS2-STK-1 2A

- MS·Filt



# " o; Rinse Petr1 Olsll F ilter 

# - i

### ttll**t- tl**  

# S" 

# o .... f, t ' ,.,,.f, .;.....

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### J"""""Y 2013

# san.- T ype- P a rllcu l ate M atter ( M e thod S) 

### Dote 

# / 0

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# '3 FA t er N o .

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)CGt Name : V eo ll a -

## Sa**1190~** IL COn di tion : .& 

# f'(< 

# .< 5'" / / T rain l ea k Roto ( ctm 

### 0 " Hg ) ProjeciHtmll>or : 409425 2S.JCI.{)2 Rul :

### ~ N oule I D

- I nit ial {)
. 

### () b 

# 1/ 0 /:; F

acility : fllc ed Hearth · Unit 2 C onsole ID --;t;j{ j '\

### <;**~** No zz le Clio (lo) 

## t;,ij- 

# 3**~** Rno l () 

## . ,C 02 @l / 

### t) SOIJr ca : Sta cl< OGMCF 

## f ,0 0 

# :z .**er** ID 

## f4., 

# fJ
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. 

# 3 0 

# 2 Operator : { 

### (J 

# r: 6H@ 

# I ntM Ba r . Pre ss. ("Hg ) 

# ::z q <; 

# 2 PT CF 

# 6

. f 't

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· OI5 l«: v iNJJ l>a f • :**F~ wy**  2012**~ZOIJ** 

# VES O I 3 888

# < tTl t/) 0 

# - w 00 00 \0 

# r I' Pro jed**Na~** Veolia- SauJet.IL 

### ""'Joct HUIOOer 409-42525.30.02 

### D

ate 

# /O/;oU3 Source Unit 2 SUd< 

## Moisture D eter mlnatioD IIT1> No. 

### COntents Vol{ml) Confiauratlon Final Wt {g)



# / 7. Water 

### 1 00 Mod 

# 'lt8. 

# g 

# I >**W~ter** 

### 100 G/S 

# g5S:Z.. 

# !Lf Empty 

# -- Mod

## 6~1. 

# z.**I~** Silico Gel 

### -300c Mod 

# '/3fJ. 

# 7 /1 G-.,ty**~** 

# ,..,._S5k 

# ' 8K.Z. I

6 

# *"'.ef'l Sam pl e Log Sample 10 Number Sampl e Container Conditio n No

. 1 

# Particulate Matter EPA M e thodS RunNo. 

# 3A
Bal.lnce i O 

# T£ 

# ¥1c1A

I nitial lilt 

### {B ) 

## 7r;3.t.f

## 1~·b**~l.{-g.3** 

# 913.'+**~oo .**  

# 2--**~**

Doscri ptlon R""""'red 

### b! 

# ];f7V/ Sample Recovery Chec
. klist 

# V R i ns e and brush p r obe and 

### nonle with 

### ace tone I nto PNR 

### samp l e bott le
. ,/" Transf e r bottle{s) to laboratory with lmp incer tra i n. 

## .L_ Sepa ra te filter holder and place filter in dean pre-rinsed glas s petri dish
. 

### Complete filter sample l abel.

## ~ Ri nse f ront half 

### of fllter holder w ith 

### acetone Int o PNR 

### bo ttle
. Co mpl e te probe 

### and nonle rinse (PNR) 

### samp le labe l.

### ~ Disa sse mble sample 

### t rain, wipe 

### off 

### excess water and weigh 

### eadl impinger. Record the 

### fina l w et ahts In 

### the M oistur e 

### De t erm i n at io n section of 

### th is data

# ~ Note cond"ion of the 511ica 

### get lmplnge r:<=ZD % 

### s pent



# _ v _ I.Dg samples into logbook and store appropriately
.



### IIS2 · STK-1 3A ·M S· PNR 250mL Probe and No nie**a~ ~**  

# c c--Jl..-s**S~-** VS2 · STK-1 3A · MS-F II t

7' c; 

### Petn Oish RlllSe Fitte- r

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## a, (Modifi e d EP A Method l6A) 0a1e 

# I()-{ (J
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# i)

# ~ 

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# I Pro)Kt Name: V eoUa**~** Sau cet. ll CO:ncllt\on: 1 

# 1107 •'..-.. Sctmpllns Tra i n leak Rat e (rl""O • ttc) Project Numbe r: •0942515
. 30-02 Run: 

## 3 8 Nozzle 10 

# - l nitiaC 

# (), CJOC CU ) Fac i l ity: Fixed Knt1h

- Unk z Const>lt 10 

# A I 

# c

i3"' 5**MouloOio~J** 

## o . '{1.S Flnal 

# o . cCIIS 0 '\ 

## ,<;; Souru: Stade O GM CF 

# ftl/ ea rome ter 10 

# (3 

# f- 

# 2.**~ot** T ub e 1 0 

# iJ ,. 

# S' 

# .2.1 O

pe N to r [ 

# /J { 

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# ft Du ct O i m< nsion(s l

## ~ 

# lf '!) '' kf 

# S
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# 0 0 2_ P i tot Tube !.elk Cbedl**No~** CAUbration

# ---0~~**~~** Mete r E1ev atlon (ftl I n

itia l**(+)~?** 

# 3 HOe')) C.Nper 1 0 

## 'h> 

# dfol (rti;MMtolltont! ttf ) 

# 3 

# 't Fi."\1.1 1+ 1 

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# c -ld::.?j PoJnt Clod< Time DGM Rtodinc 4PrH.OJ 

# ' ="' ' Tempenotu r e 

### rfl Vocuwn , • ..,,**~~~** Stade Probo fM t ei Imp Exh OGM 

## itJv'l**~/".. 11-~**  

# 7ttq:n t) , 

## 1 ':\- •

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## '25'\ 2.Co'3. 9:> 

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## VESOl3890

# < 

# rn 0 

# - w 00 \() 

# - Pro ject Na me**Vtolh~** - Seuset IL Cond i t ion 

## r.o . 1 Ptq<a Humb<r 40t41525.30-0Z 

### D

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# /13 

# HC I / C I 2 EP A M e th o d 26 A RunNo
. 

# 38
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# T£ 

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## M ois tur e D e t e rmin atio n I mp No • . Contents Vol ( "") Conf"cur at ion RniiWt(&l I nitial Ylt 131 l

. 0 .1 NH,SO , 50 KO 

# 'f3 S::{**1.7** 2 0 . 1 N H 2 S 0 4 100 GIS 

# lf(p{)-1 

# 7'+1.0 3 0
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### G/S 

# !7b.9' 

# 7'(5"

. 

# z_j
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## ?u~/Z 

# 71'- · 1 1 5 0
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## 7~-Lf 

# 7 C?()
. 

# zJ 6 Si lica Gel**~300&** M od 

# M;;.. Cfs/

. 2) ! 

## I th i s lm pintQf opt tonal. per M otho d 26A 

# Sa mpl e Log Sarnpl t 10**Numb~** S.mple Dts<rip tlon Contolnt< 

### VS2·STK·1 3 B ·M2 6A ·Acdlmp ll**a~ ne**  Acid l m pln aer 

### Cotdi&Rinse SOOml Albl:ne lmplngtr 

### VS2· STK · 1M_·M26A·Aiklmp No lcene C.tch 

### & lllnso

_

· - - ·-·· -- - -- -- --



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# s, /

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# "Pf/YI 

# Sa mp l e R e cov ery C h ec klis t {Otlly If t r ansff!r li ne iS us ed ) . Ol.scof'nect ttansftr l ine , an d t1nse three tlm.s wit h 0 1 

### wa ter klto acid l mplnger 

### catch bottle . r r an sf er 

### bo ttl e to labo rato ry with ..-npinge r train
. 

### O ba.ssemb &e: nmph!: tTJ i n, Wipe off 

### exce-1S waw 1nd weigh. 

### each 1mpinger. 

### Record the fkle l weight s In the M ois ture 

### DetcrmlnatlonH ct lon o f thi s data sheet . 

### Note condition 

### oftlle sib eel lmplnaor

. ""'Z-S; 

### spent .,.- Pour contents o . f the 1st, 2nd an d 3 rd 

### (contalo irtJ add) im pfngt rs 

### in to the**Aci~** 

### lmp ln.g er catch bott l e(s). 

### RJ ns t implngers artd co nn ect i ng g l ass ware 

### w1 t h deionized wot<r Into tho some botll e{s). Com pk!to add lmplnaer Simplt labe l ,/' Pov r t he: Q) nt ents of the Cth a nd S th lm ping «n (co ntainJna NaO H} into 

### the afkafine l flll)(nae r catch bott l e(s)

. Rlnso l mplnaers and co n na<ttng g l ass wa r e wi t h d e ion ized wattr i nto the n me bonJ e{s} . Complete al ka llre l mplr'l ge r nmple 1 8Jbe1. ,_/' lOS nmpk!s l nl o logbook and store 

### appropr-oately
.

Notes:

tDS
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## u_l<l_M<12**1s_:( _e** **••><~ :z9_l**  __ -+-o-•••...u/ 

### b"-

· ...., 1 

## <b=<... -_,_

1)-'-----l

-------------

## llo-Pa..;.''**.:../ ~-•'-='** **--=!** Ptoj ecl Name: Veoll:a- Sauae t . l. Co ndi t iOn : l

### __..-_.....--~ Sam plin a Tfafn l.e:Jk Rate (d.,."Htd Proje<lllumjler. 

### 40942S2.S
. 30-02 Run :

### ~B Noul< 10

- 

### ln llial 

# 6 , M 'f**~** 

# /J FacUlty : FhcedHoOtlh·Unll2

### C4nso**et0A 1'!~** **ou Oia** **~)** 

# tJ.:'tB ' Final 

## &..06 · 3 @ 

# 't Source : Slade OGMCF

### {.,()**~** 

### j B>rometeriO 

# (!, P- 7_ PltOI Tube 1 0 

## C)- ( 

# 9 Operato r 

# £: f\ 

# f**~H@** 

## 1, 

# 7 '1 11 B•r

. ''" "· ,.,. ,, 

## ;:z_ 

# 4.**~** 

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# q,O<;f $,.t.Press.c• o o,ot 

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### M<tiood i!9 h r EM $11P..017**!!<~ :oil•**  Nt : July 2013 

# VESOJ3892

# ;ii Vl 0 

## ,_ 

# .... 00 'Q 

# .... Cond i llo n No
. 1 P r o)ect Namt! V•otia

- Sau1 !!t: IL 

# Multi

- Metals 

# :3 B C0941525.SO.OZ**P~HU-r** Aun No
. 

# /Ob o/;.3 No Determinati on of PM 

# -rE-**~101** 

# A Date 

## EPA M e th o d 29 Balance 10 Sout< e 

### Unft2Stod< 

# Mo is tur e Determ i nation Imp!"'" Conte nt s Volume Conr!juration Fino I 

### wt. ( C) lniti • l 

### wt. (C) N o . 

### (ml ) 

# ,;, 

# ... 

# -

1 1

### ;.~d. 

# ;1.2.7/J. 

# 7 o/f()
. 

# 2- 2 Nitric:/Pf!roxide 

### 1 00 Mod 

# '8't7 .fl 75'1. 

# &' 3 

### Hitt k:/- 100 S/G 

# 74C

. 7 

# us- .o ' 

### I 

# • . . M od 

# {p tj(). 0 

# IP'!J8.lf I 5 t.Mno.SOin 

### 100 

# -**7~5:** 

# b 7 f,Lf , 

# z_.. l 6 JCM ri0 4 SO i n tOO M od 

# 75/S

. {:,


# . 7£5'. 

# 7 ! 7 SliCll Gel 

### -300$ 

# - '111-7 

# '317. 7 ' 

# '..,
.... _....,,..._., .. _.,and
_ ... _lot

__**mokt~mt** catd'llnticipaeiCI to bt ..,_, thJn 100 11 (Secdol'l$.1.3..2) 

# Sample Log $Jmple

. 10 Number 

## ' Somple Dosutptfoo Cont a lnen 

### VS2-STK- & ·M29-PNR 250ml Pr obe and N ozzle Rl nse 

### VS2-STK- 136

- M29-F II t Petri Oi5h F Uter

### VS2·ST**M29-NI** lOOOml 

### N itric ITil!>lnctr

### VS2**STK·l~· 29-E** **IR** 2SOml Empty 

### lmpince• Rinse VS2 · STK-1 .3 

# 6

- M29-Penn 1000m l Penn.anpnate lnp inger 

# ., HO Rinse 

### of

### V~**STK·l 3a_·** **M29 HORns** **~50m l** **Perma ng** **nat llf!~** **~~!** J 

## _L

(/ 

## -.1- 

# -1- .L_

,/' 

## ./ 

# _L 

# _J_
_ Recover e d by 

# Pf>/11 Sa mpl e R ecove r y Cbecklist Rinu smd btus.h probe**:~~nd** noo.nH!: with O.JM nitric add into PHR botde. N o te- use Teflon bn.tsh. U se a tot-al of 100 mL for t'h e PNR a tld f ront -hatr fltttr ri ns e. 

### Rinse tl>c (o ptiona l) Te flon tro nslor 

### Une wtth O. lM nit ric acid 

### I nto Nl bott le
. Use a t ota l of 

### 100 ml for tl>o 

### tn<nsfe r**lin<~** 1 

### nd lmpi"itr rinse>. se .

pa f'ltt fi tter holder and**pia ~**  flltt.r in duo Petr141Jh
.**~te** samp le label
. R

l ns o front 1\aij 

### o ffilter h old er wltll 0.1M nitric 

### aci d Into PNR 

### bott l o. Use 

### o!D t a l o f 100 ml. for the PNR and**front ~atf**  Ol ter mse .**Cotnp~Mt** PHR n mpN- Label
.**Oisass~e** sampJe train. wipe off e xcess water and wei gh eat'h lmpinger
. Re<.:o r d 

### thefin a l w elJh ts in the Moistur e Det erm i n at ion s.ettiol'l
. Non! 

### condi tion of slllco Jel

### "spoOl Pou r contents of nrst 3 imp tnsers itlto tht NiUic/ptroxlde fmpl ngeratd'l bottle{s)

. 

### R

i nse t h•lm p l naer s, 

### n it

er su p po rt 

### and blc k A ilalf o f th e t liltet' 

### holder and**conne~int** 

### classwa r e wi1l> 0.1 M nitric add 

### same bottle(.s)
. Usa a 

### total of 200 m1 for tile 

### trans fer &no 

### ond lmpincer**-..** 

### Complete Nlsample label(s)
.**Ri~** 

### t ht 4 10 

### ( l nltlaUy empty) lmp i 11ger wit h 

### 0.1M nitric a dd 

### Int o tho empty lmplnger nn .. 

### (EIR) bottle. 

### Use • lotil o f 100 m l for th is riroe. Co m plet e EIR Slmp l el•be l
. Pour the 

### contents of the 

## s"' and 6
.. imp\I>JII> 

### ( perNnpna"' ilnpingen) Into tile perma naanate fmptncer utch bottle (Perm). EUnn**with~** totil o f 100 m l o f**pe rman~n** **te** so l ut i on a nd 100 m l of 0 1 w at er. Complete POf'm Silm pl e l abel Put 1 00 mJ 0 1 wat:e.r tnto HCIRns .samp4e bettie.. ftlMe the**perm~n.cJnate** tm,otncers w i th a total o12 S mL of &N HO I nto the same.**bonf ~t-**  R lt t

se impinc•rs Witt!' 100 ml Dl wattt into the same bott l e . Comp l e-te HCfRns s a mple labe l. {Note, thi s is not r equ i r e d i f !I'Kuels no vi s i ble solid residue) 

### toe Amplts Into 

### locbool< and store opprop.-lotely
. Comments

RDS· 23 : 1.1e tollbyEPA M 29, ,.PM , .-1 vohmu l'u EM SCf'.()/ 7 Pilvl"siM Ottte : JtlfXIOI"J' 

## zonD-5.

- rm

_pte_ TvPe _·_ PCD

_ ot

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_ •_tt,cd

_ oo_UA _I

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# ----:><: Project Na:m4 : Veo Ua • Saueet.. I. Cond it ion: 1 ...-----**~** 

### P>ge 

## f oi -.... Train Lea k Rot e( cfm IP 

### •11e1 P roje ct Numbe r: 40942SZ5.30.02 Run;

### ~~ Holdero - Foctlity: Fl•ed H
.. 

## m. • Unit 2 Flnol () • 00 

# > @I

### ''~, :>" So ur ce : SUdc DGMCF

### ~.f~f Ba r ome<er t O 

# /] P- 2.. Pltot Tu'bo 10 

## f'- 0 

## J Operator 

## -;iC. 111!1!> /. 

## {lf9 S.r.Press
. ('Hcl

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# T'2.. Duct Dlr'Mnslon( s ) 

## ,8' , ; 11 

## _,6 Plt ot Tube l u k OW!ck 

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### 1+1 " "' H "" P olnt Clo<* 11m Dry Gas Vol . AP 4H TempefltiM'e { .. 

### f"l Vacuum 0 (ft') (" H,D) ("H,OI Stadt Probe Falor XAD tnlet Imp Exk OGM HtTrc Eklt (ln. HI) 

### t

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# sS/)5·1 7, PQ){)II'C()F by SW -846 Method (I()ZJA

Pw-£U sa> .. OJJ b>l•iD•**~pril** Z0/2 

# VESOJ3894

# ~ (/) 0



## ...... w 00 'C 

### v. Project NJm c**Veolta Sa~o~,cet,lt.**  Projtct Nu mber 409U.S25.3().02 

### Date \o{t611'2 So urce Unit 2 Stack 

## M ois tur e D et e nnln a tl o n Imp Contents Vot (ml) 

### Conflcura t lon Fina l Wt (g) 

### No

.

I 

# . 

# . K/0**_3o ~,<;**  2 li ,O 

### -100 G/S 

# 1-u..o ) H ,O 

# ·too Mod 

## 11-2.. 1 I 

### Sil iQ G •l 

# - 3aoc Mod 

# 't=f1:z.. s i 

# Sa mpl e Log 5ampJe 10 N um ber S.mplo CQntllne r 

### V

S 2-S T K-ll & -M00 23A -PNR SOOmL 

### VS2-STK · l · M002 3A· Ait Pe tr i Dish 

### VS2

- STK

- 1 -M0023A-Q\ SOO ml



### _ VS2

- ST

_ K-1
_ ( -M0023A

- XAD
_ So !'bent



### - _Trop

----------- -

# ~ Condl t lotl 

### No
. 1 

# Dioxins and Furans SW-846
- Method 0023A RunNo. 

# 38**Bola~** ID 

# Tf£ tj( {) / 

# ,4

I nitia l W t . (g) 

# 93 S:9 1-Z'/.**~** 

# 72Z.!f_ 9t(5:**~**

Oescrlptlo n 

# I P

robe a nd Houle 

# l Rw. f ilter I Condensor Rlnse



### XAOSolbent !

- --- ----------- 

### Rtcovtre d by 

# t::M**~** 

# S

ampl e R ec o ve ry C h ec kli s t ..1t::::.._ 

### Rinse and brush probe and noz zle: three t im es with acetone, tw k:e with me t h y l e ne chloride and tw i ce wit h totuene. R eco ver Into one b ou l e 

### (PNR)
.**~** 

### Separ a te fo lte r ho l der and place filter in de an pre- rinsed, gl ass petri dish
. Complete Fi l t sample l abel
.**~** 

### Seat XAO 

### trap .,..ds. COmplete XAO 

### sample bbel.**~** 

### Rinse f ron t h a l f of fit ter hol der i n to PNR**bot~ e:**  

### three times w i th acetone, twi ce witl1 

### me thy l ene chl o ride and twice wllh toluen e. C omplete PNR samp le l abel. ,/ 

## ./
./ 

# ../ D isassem b le sam ple traln f wipe off e xccs:s water and 

### we t ch each lmpi nge r. 

### R

ec o rd the fln al we i ghts I n the Mo ist u r

e Determination s ection. D IS CARD the lmp lnger solution. N

ote condition of the silica get imp l nger. !!{_ %s pent Ri ns<o 

### the back half o f t11 e 

### fll ter hold er , Teflon tran sfer line( if used) , all 

### connecting 

### glasswa r e. an d the 

### coli condenser : 

### th ree times 

### with acetone, twia. witll 

### met hylen e chloride and t wice wi1h 

### toluene
. Com p le t e C R sample label
.

_ _ LO(Isamp les Into log b oo k and pla ce In 

### re frlcerato r 

### or ice 

### chest.
Comments

Rl>$-.10/ D/oJdM 11rd Ftlr'riM, SW-846 M00 23

A , fltJ MeCf Per EM SOP-OlJ

__ _, JdfO#Yi!OlJSa mple T ype - PCOO/PCDF (Metho<l 0023A) Date 

### IO·t0-1) 

# >s;::**~ac•** 

## '2 ol , 

# z. Project Namt : Veolfa - Sau get. l l Con ditiOn : 1 Train l ea k Rate (dm@) " Hs) Projea Numbo r: 40942S2S.J0o02 Run:**~8** NouloiO 

# - nlti•l 

## C

.**~** I Facili t y: Fixed H e.rth • Unit 2. Cons ole 10,1/ 

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I n) 

## 0. 1/ 

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## 0. 

# fff Baromet« I D

### /~ 

## P-**~** tot Tube 10**.** 

### fJ) pporno r 

## :J{.**~HO** /. 

## {(( f Bar. Pre$$. ("Ha) 

## "l. f. f**~** TCF 

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# ,.'<
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## 1 t . 

## f Kf**so~** Pross
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# -e- o.l(v 

# J!l**11~r~ ~**  Elevat ion (It ) 

### nid a l (+l(' , ..**~-~** I ( rtll \lve to S.nnuer) CailperiO ?

### 00~} 

## 74 Final ( +) 

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Point Clod< T i me DryG01Vol M 6H TemperJture t•F) Vacuum 

## Itt'! ("H,o) ("H,O) Stack Probe Fltt •r XADinl t t**·~Exit** DGM HtTr<Ellt (in. 

### Hal 

# 'f lt;"OO "7 t(.f 

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## 19¥ l.r;/ "l. 

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## - "-'EM -Sn'412J**-daf·J.~7ZOIZ** 

# VES013896S.mplo Type : 110, 0, (Modffild EPA Method 26A) 0 •"' 

### 10 · 

### /, ' ·I } Fllter No

. 

### P aae 

# I of 

# I**Proj ~et**  N &me : Ve otla - Sauatt.. 1\ Condltlon : 1 

# JJ/It S1mpli.nc Train Luk R• te f<hr.•**~IJ** Projoct Humber: 41l942S25.30-02 

### Run; -![_a NouleiO
- lnMiaJ 

# C.OOC 0l 

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# l l f (, f 

## )'j ') N on ie 013 (In) 

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# o.o a 'f @t O Sourc:e: Stade DGM Cf 

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### ~ 

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# 14-o.v- 611 " 

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. 

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## 9
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# 3 6 ,**~** 11 

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## 0 

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## 7**~** 

### <>'1!2**~ (rt~w**  to l t nn:ndf'l'. 

# 3 

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### Vacuum ('"'Hst**[A~** SUck Probe flttef lm

_ pblt OG M

### IN-.~-c.**'\~S** 

# I 11 

# tit;'/ · o.r < 

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# VES0 138 97

# <**~** 0 

## ,..... 

# .__, 00 \0 00 Project Nlme: VeoO.. -S!uCe.t..ll Condition No. 1 P r o)ect Numbe r •0942.52$.3()42 Oato 

# /0/11/ 1.3 

# HCI/CI2 EPA M e th o d 26A RunNo. 

# i(-lJ BaJa nee

# 1~ 

# -r;::.. /.fl {) 1 

# A

Source Unit 2 Stack 

# Moisture Determination
I mp No • . Contents Vot lmlJ ConfcurWon F1 n1I W t{&J 1 nilla 1 Wt Ill 1' 0

. 1 N H,S0 4 

## so KO 

# 't35.'f**5'** 2 0.1 N H,SO , 100 

### GIS 

# ?'f7.1 75/.1 3 0

. 1 N H,SO• 100 

### G/S

### 1o2.~ 

# 1tfl. 

# 7 

# • O.INNoOH 

### 100 

# - 7&5.7 

# 74-7.!±
. 5 0.1 NNaOH 100 Mod

### 7~>. 

# I**?~.b** 6 SiBt11 Gel •JOOg Mod 

# 't u . 9 9.59.2.

t h

is tmplnaer opdnntt J*f' Me t hod 26A 

# Samp l e Log SampleiO**Num~er Sam~**  D.scriplion 

# Conti-**VS2-STK l~-M26A-Acdlmp** **llNa~&one** Adcllmplocor Catch & flru4 

# I**VS2-STK-l M2** **6A-Aiklmp** SOOml 

### Albnne lmJ>lncor 

### Notcene eatch&F J nse



# .,**~** ' 

## ,/ Rea>Ye red 

### bv

# .1:>~ Sampl e Re c overy OJecklist (OnJy 

### If tran s fer Un t I s u '

sed). 

### D i sconnect transter line. 

### a n d rinse thte t t ime s wi th 01 

### wa t er i nto add**~oatr** 

### catch botde. 

### Traosfef'bottle to l abof'atory 

### wfth.lmplnecrr troln. / Otsa.ssemb le sa mp S. 

### tratn, wipe off ucess watu 

### 1n d welch each 

### impin& er . Re<C)(d the final wt:'&hts In 

### tht Motsture Oetermtna:tloa section of this 

### data sheet
.
:::: Jllote a.>dition of tire $1UCa c<l l mplrcer. 

## <: 521 " spent 

# v Pour contents of 

### d-oe 1St. 2nd and 3rd (conainh g add) lmp!na..-s IAto 1ht Aad imp<rl&er atch bo<tlo(s)

. l\lmc l mp l ns.rs a nd coonectioo glassware wrtll dolon ll od WJ"ttr into the Mme bO't:t»(s,
. CofTiplete a dd ilnpinge: t sample label. ./ P oor tl>!! cont•nts of the 4th and Stl> lmpi ngers (corotalning Na OH) I n to the allcaAne 

### impinge:r catch bott1e(s). Rinse lmpMc,m il\d 

### coonecting**glauwa r~**  

### wtth cS el onlled wate r into the 

### nme bottle(.s). Comp lete a l ka lf he 

### lmpin&e r samp le lJbel. / L og s atn ples Into logbook a nd s tore

# approp**lat~fv .** 

N otes:

IU>S-19 : HCVCI,byE1'AM•t/oodZ6A Pu- EM SOI'·OZI """'._ D<Jto: J<lfy ZOI3t-s a_mp

_;

le

_; Ty.;_

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