VES013871 .pdf 
APPENDIXF 

Sampling Documentation 

VES013871 
Unit 2 - Run 1 

Project Name Veoli• Sou,et 

Project Number 4094.2525 

Unit 2 Unit 2 Unit 2 Unit2 Averages 

1 1 1 1 

1A 18 lB 18 

10/8/2013 10/8/2013 10/8/2013 10/8/2013 

11:50 15:40 15:AO 15:40 

13:00 16:40 18:43 18:55 

11:50-13:00 15:40-16:40 1.5:40-18:4 3 15:40-18:55 

Diameter (ftt itqu#l>olent ifsqU«t MtJ 3.21 3.21 3.21 3.21 

Tube Correcti:m Factor 0.84 0.84 0.84 0.84 

Diameter (indies) 0.437 0.425 0.436 0.436 

1.002 1.011 1.002 0.999 

Temperature ('f) 68 68 68 68 

Pressure Measured (" t-18) 29.89 29.89 29.89 29.89 

{fl) {ftlatlve to Baromote,. 34 34 34 34 

DGM Telll>{' F) 77.2 75.0 82.0 83.5 

Delta H (in we) 1.62 1.39 1.72 1.41 

Water :Sl 604.9 649.5 1500.4 2072.3 

(monutes) 60 60 120 180 

("H,O) 0.02 0.02 0.02 0.02 

Monoxide ;co) Content(%) 0 0 0 0 

Dioxide (C01) Content (%) 6.35 7.95 7.95 7.95 

(01) Content (%) 11.56 10.08 10.08 10.08 

(H1) Content(%) 0.0 0.0 0.0 0.0 

(CH.) Content (") 0.0 0.0 0.0 0.0 

(N,) Content(%) 82.09 81.97 81.97 81.97 

Volume (acl) 41.365 37A20 86.843 124.679 

850.1 849.3 

44.10 

44.10 

37.384 

Gas Volo<ity 30.50 29.97 31.41 30.05 30.48 

Flow Rate (aofh) 887,777 872,197 914,101 874,661 887,184 

Row Rate (adm) 14,796 14,537 15,235 14,578 14,786 

Row Rate {set>) 550,260 539,756 567,438 544,139 550,398 

Row Rate (sclm) 9,171 8,996 9,457 9,069 9,173 

Flow Rate (dscftl) 323,699 296,491 309,383 301,009 307,645 

Flow Rate (dsclm) 5,395 4,942 5,156 5,017 5,127 

VESOJ3872 
Unit 2 - Run 2A 

Project Name VeOIII Saucet 

Project Number 4()9.42525 

. Fadli Comprehentill<! Performonce 

ty Test Unit 2 

fSample Type MS Averaaes 

jsource Unit2 

~onditlon 1 

~un 2A 

~ate 10/9/2013 

tnm~ Start 09:45 

ime Stop 10:53 

09:45·10:53 

Duct Diameter (fl) ·<-rlf-dua} 3.21 

itot Tube Correction Factor 0.84 

Noute Diameter (Inches) 0.437 

OGMCF 1.002 

tandard Temperr.ure ('F) 68 

Barometric PressUie Measured (" Hg) 29.85 

tack E.levatlon (ft) (;(~a:~ to B~rOmeterl 34 

Barometnc Presswe "H 29.816 

Averace Stack Temperature ('F) 389.8 389.8 

Average DGM Terrp ("f) 70.7 

Averaee Delta H (In we) 1.63 

Condensed Water Cil 638.5 

est Duration (mir utes) 60 

Static Pressure ("H,O) 0.02 

prbon Monoxide (CO) Content (") 0 

prbon DioJ<ide (CO,) Content !") 6.56 

PJCYgen (02) Content(%) 11.23 

~ydrogen (H,) C:O.tent I") 0.0 

r,ethane (OiJ Content I" I 0.0 

~lttogen (N2) Content(%) 82.20 

Meter Volwne (ad) 42.463 

f\verage square root of liP (l~t.P) ) 0.403 

Absolute Stack Prusure ("H8) 29.82 

Absolute stack Temperature ('R) 849.8 849.8 

~ue Gas Moisture 1"1 41.59 41 .59 

Moisture at saturnlon N/A 

Moisture used in Cala.dation 41.59 41.59 

Gas Molecular Weight (Wet) (g/g·~:: 24.72 

l:o<rected Volume of Gas samoled ( 42.548 

olume at Meter (dsc:f) 42.356 

Average Gas VefQtlty (fl/sec) 31.07 31.07 

Avg Flow Rate (acfh) 904,204 904,204 

Avg Flow Rate (adm) 15,070 15,070 

Avg Row Rate (seth) 559,910 559,910 

Avg flow Rate (sctm) 9,332 9,332 

Avg Flow Rate (dltfh) 327,067 327,067 

Avg Flow Rate (dmm) 5,451 5,451 

I · <•• lin• A;t• I'll;\ 100.52 

F·2 

VES013873 
Project Name 

Project Number 

Facilih 

F>•mple Type 

~ource 

Condition 

Run 

tnme ~·· Start 

lr1me Stop 

Duct Oiameter (ft) """"''*•• ><~•.,.doctl 

Pitot Tube Correct>>n Fac1or 

~onle Diameter (mche$) 

pGMCF 

~tan ard Temperature ('F) 

Barometric Pressure Measured(" Kg) 

~tack Elevatlon (It) c.-... _ 

Barometric Preuure ("H•l 

~verage Stack Terrperature (' F) 

fverage OGM Temp ('F) 

~verage Delta H (in we) 

f-ondensed Water (g) 

lrest Duration (minutes) 

f>latic Pressure ("H.O) 

Carbon Mono•lde !COl Content(%) 

~arb n Oio•lde {C02 ) Cootent (%) 

bxygen (O,) Content(%) 

Hydrogen (H,) Content I"J 

Methane (CH.) Cootent (%) 

Nitrogen {N,) Content {%) 

~eter Volume (acf) 

Average square root of Ill' ((114Pl~l 

AbsoiUle Stack Pr5$Ure ("Hs) 

Absolute Stack Temperature ('R) 

flue Gas Moisture(%) 

Moisture at SDturction 

Moisture u~d in Calculation 

Gas Molecular Weight (Wet) (i/g-mote) 

<"orrected Volume of Gas samoled racri 

Volume at Meter idscf) 

Average Gas Velodty (ft/sec) 

Avs Row Rate (odh) 

Avs Flow Rate (ac'm) 

Avg Flow Rate (scll1) 

Avg Flow Rato (scfm) 

Avs Flow Rate {ds:fh) 

Avg Row Rate (dsr.fm) 

lsoklnetic Samollro Rate'"' 

Unit 2 - Run 3 

V.oliaSaucet 

40942525 

Comprehensive Perform<~ nco lost· Unit 2 

MS ModM26A M29 M0023A 

Unit 2 Unit 2 Unit 2 Unit 2 

I I 1 1 

3A 38 38 38 

10/10/2013 10/10/2013 10/10/2013 10/10/2013 

09:15 12:30 12:30 12:30 

10:23 13:30 15:10 15:40 

09:1S.10:23 12:30-13:30 12:30·15:10 12:3()-15:40 

3.21 3.21 3.21 3.21 

0.84 0.84 0.84 0.84 

0.437 0 .425 0.436 0.436 

1.002 1.011 1.002 0.999 

68 68 68 68 

29.82 29.82 29.82 29.82 

34 34 34 34 

29.186 29.786 29.786 29.786 

391.2 396.4 393.3 39S.S 

70.2 81.3 84.0 88.1 

l.S5 1.38 1.48 1.41 

632.1 669.0 14ll.8 2096.1 

60 60 120 180 

0.02 O.Q2 0.02 0.02 

0 0 0 0 

6.28 7.50 7.50 7.50 

11.48 10.38 10.38 10.38 

0.0 0.0 0.0 0.0 

0.0 0.0 0.0 0.0 

82.24 82.12 82.12 82.12 

41.392 37.857 81.243 124.366 

0.393 0.409 0.402 0.411 

29.19 29.79 29.19 29.79 

851.2 856.4 853.3 8SS.5 

41.97 45.87 45.78 45.29 

N/A N/A N/A N/A 

4L97 45.87 45.78 45.29 

24.65 24.29 24.30 24.35 

41.475 38.273 81.405 124.242 

41.278 37.290 78.951 119.568 

30.42 31.95 31.36 32.05 

885,200 929,898 912,708 932,661 

14,753 15,498 15,2U 15,544 

546,619 570,763 S62,264 573,054 

9,111 9, 513 9,311 9,551 

317,249 308,979 304,833 313.504 

5,287 5,150 5,081 

j 

5,225 

100.99 99.04 100.97 99.)3 

Averages 

394.1 

854.1 

44.73 

44.73 

31.44 

915,117 

15,252 

563, 190 

9.387 

311,141 

5,186 

VES013874 
Unit 2 - Run 48 

Project Name 

Proj ect Number 

Facill" 

~mpleType 

fSource 

COndition 

fun 

oate 

Time Start 

Tlme Stop 

Duct Olan n:h:r (ft) (itfiV~olt:l'lll/ squo'11 tNttl 

Pitot Tube Corre«ion factor 

Nozzle Diameter (ioches) 

DGMCf 

Standord Temperawre t•F) 

Barometric Pressure Measured (" Hg) 

~tack Elevation (It; C~tlw to """""''"' 

Barometric Presst.ro I'H• I 

Average Stack Temperature ("f) 

Average DGM Temp ("f) 

Average Delta H (In we) 

tondensed Wale< (sl est Duration (millvtes) 

Stalk Pre ssure ("H,O) 

carbon Mono><ide (CO) Content(") 

arbon Dioxide (C0 1) Content(%) 

Oxygen (0,1 Content{") 

Hydrogen (H1) Co1tent 1"1 

Methane (CH,) CDnttnt (%) 

Nitrogen {N1) Cor tent(%) 

Meter Volume (ad) 

l\lferoge SQuare root of AP ((~llPlul 

llbsolute Stack Pressure ("Hg) 

Atw>lvte Stack Tomperature (•R) 

Flue Gas Moisture {%1 

Moisture at saturation 

Moisture Ys.od in Calculation 

Gas Molecular Weight {Wet) (g/g-mole) 

Com-cted Volume of Gas samoled lacfl 

Volume at Meter (dscf) 

Average Gas Velodty (ft/sec) 

Avg Flow Rate (acfh) 

Avg Flow R~te (acfml 

llvg Flow Rote (scfh) 

llvg Flow Rate (scfm) 

Avg Flow Rate (dscfh) 

Avg Flow Rate (dscfm) 

soklnetic Samolno at ~ 

Veoli<o S.uget 

40942525 

Comprehenslw Performance Test • Unit 2 

ModM26A M29 M0023A Averages Unh2 un~2 Unit 2 

1 1 1 

48 48 49 

10/11/2013 10/11/2013 10/11/2013 

09:4S 09:45 09:45 

10:45 12:25 U:55 

09:45-10:45 09:45-U :25 09:45-12:55 

3.21 3.21 3.21 

0.94 0.94 0.84 

0.425 0.436 0.436 

1.011 1.002 0.999 

68 68 68 

29.74 29.74 29.74 

34 34 34 

29.706 29.706 29.706 

391.3 387.6 390.6 389.8 

74.7 74.8 n A 

1.28 1.39 1.33 

631.2 1382.8 2087.3 

60 120 180 

0 .04 0.04 0.04 

0 0 0 

7.69 7.69 7.69 

10.18 10.18 10.18 

0.0 0.0 0.0 

0.0 0.0 0.0 

82.13 82.13 82.13 

36.206 79.138 121.269 

0.394 0.395 0.402 

29.71 29.71 29.71 

851.3 947.6 85o.6 849.8 

45.29 45.:>7 4.:i,40 S.~2 

N/A N/A N/A 

45.29 45.57 45.40 45.42 

24.37 24.33 24.35 

36.604 79.296 121.148 

36.003 78.003 118.568 

30.71 30.74 31.32 30.92 

893,784 894,553 9 11,665 900,001 

14,896 141909 15,194 15,000 

550,472 553,329 561,924 555,242 

9, 175 9,222 9,365 9,254 

301,138 301,181 306,832 303,050 

5,019 5,020 5,114 5,051 

98.11 100.97 100.44 

VES0 13875 
Unit 2 - Run SB 

Project Name 

Project Number 

FadUty 

jSample Type 

!Source 

Fondllion 

Run 

~ .. h'lme Start 

tnmestop 

~t Oiometer (ft) '«q.~l'w'k"'t if,.,_,., ctwt) 

~hot Tube C<>rrectlon Factor 

otzle Diameter (ioches) 

OGMCf 

tand ard Temperature ('F) 

je.rometric Pressure Measured (" Hg) 

Stack Elevation (ft) {rel.1t1Ye to 6arometer) 

Barometric Pressu'e I' H•l 

f<~verage Stack Temperature ("F) 

~ver.~ge DGM Temp ('F) 

Average Delta H (in we) 

P,ndensed Water(g) 

h'est Dur.~tlon (mir.utes) 

Static Pressure {"~ ) 

~arbon Monoxide (CO) Content(%) 

prbon Dioxide (02) Cont ent l"l 

pxv8en (0 2) Content(%) 

liydrogen (H,) C<>ntent (%) 

thane (CHJ Content l"l trogen (N,) Content(%) 

ter Volume (acO 

"verage square root of 6P ((~APl. ) 

~bsolute Stack Pressure ("Hg) 

f'<bsolute Stack Temperature ('R) 

~ue Gas Moisture (%) 

~oisture at Silturation 

olsture used in calculation 

as Moletulor Welct>t (Wet) (gig-mole) 

Corrected Volume of Gas .. ,;p;.;d {ac0 

f.lotume at Meter(dsd) 

f~veroge Gas Velodty (It/sec) "'va Flow Rate (adh) 

Avg flow Rate (acfm) 

Avg flow Rate (scfh) 

A"8 Row Rate (sdm) 

Avg Flow Rate (d;dlt) 

Avg flow Rate (d;d m) 

lsokinetic Samolin• Rate 11>1 

Voolla Sauget 

40942525 

Com 11ehensJve Performance Test- U11t 2 

Mod M26A M29 M0023A Averages Unit2 Unit 2 Unit 2 

1 1 1 

SB sa 58 

10/30/2013 10/30/2013 10/30/2013 

12:45 12:45 12:45 

13:45 15:32 16:02 

12:45-13:45 12:45-15:32 12:45-16:()2 

3.21 3.21 3.21 

0.84 0.84 0.84 

0.426 0.438 0.437 

1.011 1.002 0.999 

68 68 68 

29.70 29.70 29.70 

34 34 34 

29.666 29.666 29.666 

392.0 386.3 389.1 389.1 

75.1 78.9 74.6 

1.33 1.47 1.56 

609.1 1314.1 1988.9 

60 120 liD 

.0.03 .0.03 .().03 

0 0 0 

7.25 7.25 7.25 

10.50 10.50 10.50 

0.0 0.0 0.0 

0.0 0.0 0.0 

82.26 82.26 82.26 

37.161 81.488 127.192 

0.401 0.401 0.427 

29.66 29.66 29.66 

852.0 846.3 849.1 849.1 

43.82 4l.U 42.92 43.52 

N/A N/A N/A 

43.82 43.81 42.92 43.52 

24.51 24.51 24.61 

37.570 8 1.651 127.065 

36.879 79.607 124.921 

31.21 31.06 33.10 31.79 

908,296 903,845 963,377 925,172 

15,138 15.064 16,056 15,420 

558,068 559,106 593,943 570,372 

9,301 9,318 9,899 9,506 

313,523 314, 180 339,028 322,244 

5,225 5,236 5,650 5,371 

96.08 97.89 95.33 

VES013876 
5ample Type - Partlwlate Motter (Mel1wd 5) Dlste7 {)- 1$ - { <, Fillet No. Page I ol I 

Pro)ocl Name: VeoUa • S.uget. IL Qrdtlan; 1 ~K 7.5'0"1 Train Leak Rate (dm 0 'H!I) 

Project !'lumber: 4094252s.30-o2 RtJn: I A ~O<Ji e 10 - lr;tlal I> llt'1 4 e I ') 

FadMty: Fbced Hearth • Unjt 2 COflS<ie IDA I!./ '1, 41 Noule Ola (il) l'l.lf 3 7 Anal o. Oo I 4ll 5I ~: tack DGMCF I 002.. s--norer 10 /3 P-2. Pltot Tlb! 10 f>-30 <' 

Operator: 71\? AH@ ( 7Cro Baf. Pross. ("119) ;<"1 f1 PTCF 0 , ~-

Duct~(s) · 3~~" t~L~ Kf l {J 7C/ -· Preos. {"li,,) /J, 0 :z_ Pitot Tube L4ak 0\ack 

NouleC.Iibfodon 

-e-tJ. '13P ·" o.CJn ._ tJ.'fF 

BevaUcn (1\) lritial (+)~/3 (·)~;> ) 

Coli-n> 7jtJ'!i.o"3 ~ ....... _, 31 

Anal <•>oc:e ::-·3 (·)"~'] 

- OodcTme Oty Gas \d (It') t.P AH TemperotL<e (•f) varuun (!11. H,O) (ln. H,O) Stxlt ,_ -Itnp Belt OG.'lln OGMOut (il. Hg) 

1,./f I 1--z; 0 '-jq7 ~5'1 {). I 7 I. I "'Jtf I -;{_ 'H· =!ft2 t3 . 7'f 3. 0 

c-,-z lt<Z: ~t'k' 5 1-r) /7 (<{, ')~2 1. 'I<'( .2.0 s' 7'\ 'l.O 

/,.,j'f Jl. OD io)."i 0 . /C. IX' 3'11 2-5~ <~<; 53 7") :'1.0 

0 3 i) {)7, ~5 I {I 17 7.'l ~q,z 2s< :ur.. u.. 7'} l\. !,~ 12 / D Y'l f.( OF! :l.D ·y12. 2~ s 2!. 'f I. 7;:. 5.c.l 

wj lllj ~15/l 71./1. /,'f ~I ulr 2.r. "2. (,.,?/ - 77 <:. ( 

<f'Df 172o 1'1r. n:z. Wf•l •• ~ (.. .k.h 11 c.oJ b 7"!).. ;Q rh.t J := 6 tlO [),.-;o I 7' 

5~ 17 3{) ¥'1 ( C..IJ "t., IO.!Z ' f. 3 ~0 ~ 1. ?1 '< ~ - It; 4-co 

5( /7 7:7: {2/.4. o. T<i- Tt., )("~ 7 <z. l..C'f lt-'1 7ff 4-:C:. ~Jt 17 ~0 714.7 (} r? I < 1-z."l i "? (l 7t:: ~ llfL /l;' 4< ~ 17 If:?; tz:6''F r/,, 17 , -<(: 3'12 :2.-'t 3 ::u~ Lff. 7~ <'> 

'52 ')2 < D y·<,..2. 2 I fl IL I. 7 "-/12 7. 5f{ 12~ < if<{' - 4'1) ~ l 

51 !T« ~~ q o Fi { S '(jij ;2<) ") :ZN ¥1 -ro 5' ~ 

51oP {\f')Q nq 21.s 

Co<T'fnents: 5l>S·26' PM by ePA Method 5 

Pv EM SOf'.QJ5 i&Yi:IAifl I).:JM : F~ 2t)J2 

~t..nc.~~2011 

VES013877 
< [Tl 

en 

0 

...., 

00 

-.1 

00 

ProjtctNa:tM Veoia-Saucet.IL 

Project Number 4094251S.»>2 

Cote to/3 /13 

Source lJnh: 2 Stade 

Moisture Determination 

Imp No. COnte.nts Vol (ml) Confil:untlon final wt (I) 

1 Wate.r 100 Mod Cf~o.z_ 

2 Wit er 100 G/S t oo7. 1 

3 Empty - Mod 762-. I 

4 SiDcaGel "300& Mod Cf'fl .3 

5 

6 !,.,_,_ - -- -- - ----- ----------

Sample Log 

SSmplt 10 Number Sample 

Container 

COndition No. 1 

Particulate Matter 

EPA MethodS 

Run No. i A 

Bat•nc• ID / £ ~/{)1 ,4 

Initial wt 1111 

71/'1. z. 

751. 3 

(,'ft.. r 

Cft 't. 4{- i 

Otscrf!>tlon I 

Roa>vtro<lby .J;lpl"\ 

/ Sample Recovery Checklist __ RJnse and brush protJe and noule wttn a:et one lnto PNR sample bottle. 

~ Transfer bottle(s) to laboratOIY with impinge< train. 

~ Separate filter holder and place filt er in dean pre-rinsed aJ•ss petri dish. 

Complete filter sample label. 

/ Rinse front ha~ of filter holder with acetone Into PNR botde. Complete 

probe and nonle rin$2 (PNR) sample Iobei. 

/ Disassemble sample train, wipe off excess water and weigh each lmpinger. 

Re<:Ord the final weights In the Moisture Determination section of this data 

/ Note cond lon of the silica ael lmplnger."'Z--0% spent 

/ tog samples into logbook and store appropriately. 

Comments 

1/52-STK·l fA -MS-PNR 250ml Probe and Nottle l 

IJS2·STK· l.JA...· MS· Ait Petri Dish 

... 

" 

Rinst! ' 

Fitter 

---- - -----

ROS·JJ: PM byfi'A V.cllwKI 5 

Pu Ei11 SOP-lJJ!J 

R'~ Ootc: Jcfl.ll:rY 2013 
Simple Type: HCl, Cl, (M<>dlfled EP~ Mtthod 26A) Date /6· P-I 3 r.M~e.r No. Pa&e of J 

Veolla . Saueet, ll Condlt~n: 1 Projec.t Name: / N'A Semp4inl Train Le1k Rate Cdr.. o ..._, 

Project Number: 40942.5"2S.3D-02 Run: · _Le NonleiO - ln'tial o. o•<t 4f t~-0 

FacUlty: F'uc:ed Hearth · Unit 2 console oo MI./~ 'IS Nozzle Ola (kl) 6.-.v.; fl">l (J,d01.. @> /(}.,() 

SOurce: Stack DGMCf I ,OJ( Barometer 10 oN. Pltot Tubt iD ~ "f>52~ I 

Operator lcAMM. GH4f I. ~zH O.r. PIOSL ('1'£) 2't ._&'f_ PT(f (l .!.,"\ 

Duct Ol""'nslon(s) 3 B5" Kf '1'.~ Stat. PTe" . ('H,OJ d ,() 2 Pitot Tube leak Check 

Noul• C:.libratSon 

--- Ml£_ ~ ~ ~ .MfU, 

M<tttr Elevation 11'1 lnltlol (+) cot. 7t, H.-I!> 

caliper 10 7«?'?03 Cldltwe oa.~• 3 f 

Final (+)4:.1; H d<-7"!> 

Point Clock T'm• DGM Re.1dlnc AP j•~,o) .6H (' .. ItO) 

Temperoture ('FI Vawum("Hc) 

·~ Stack Probe Flltei Imp EKH OGM 

~oJ't ~ll I. Sf>P} o.r'/ ,'~0 ~I z.~ :Z.Iol (,( ~ _3. 0 

t-6'<S c{_£~ 0 . 16 ~c) 3'\ t UR H"l- 'l& ;s- ~-0 

1~0 I ~-"'1.. 0 ·'" 

1.~ 3'\l 2 "' 2~'1 'tf iS ~.0 

16l')~ tl.oo b·"' 1. '30 ~"' t Z.("\ '2-S9. '18 I~S' .,S.o 

u.«) ~ 0 . }(. r.i\1 . ~·h Z.C..t z.<;i!, 't?\ I =IS 3.cf 

1(,0~ t?-.•? ,~ 1.'{0 1"1,'\1. Z.<;'\ 2G.o ~ :}S' !. ~ 

lf.t>rD ?o.% o JS o 1.1/o '!li'!> Wb z-m ~ :rs 3 . .:; 

'"'s '23. <\l o.,~ J.t{o I> ft.- ZS& ~ S'\ _1:5' 4 .t> 

lhW lu..-;t, 0. IS' ,.-Ia 3crt- 1<,.'!> z.~ S1 I =!5 .i/.0 

t«.· 11..ti.=i'Z .. o. tS' l.t-\0 'l Zb~ ~ <2 "J..c;- 'f·O 

J(,'fA ~t l,'o 0 . \6 l·'tO 

~· t.c.'; lz.9<> S'!> ~ oi-o ,, th''' :;).COO <L\(o •. so ~'i'l ?..<o't U..l <;.'Z, ;'l.;' 'f.~ 

/fo~O ~<\~_ ·• 

~ 

I 

Notes: 5()5·21: HC1, ct,byfPA ~fethod26A 

p.,,. FM .~OP.()2J 

-0,~: s.~-20/J 

VES013879 
< 

tn 

(I) 

0 

,.... 

w 

00 

00 

0 

Project Name voolla - saucet, 11. Co.1dltion No. 1 

Project NUmber 60942525.30-02 

Dote /0/8'(/.3 

HCI/CI2 

BPA Method Z6A 

Run No. 15 

Balance 10 T f£ tfrotA 

Sourc~ Unit 2 Slid 

Molsture Oetermination 

Imp No .. COfltenu Vol(""q Confl,uration FlnoiWt(d Initial W't (t) 

l ' 0.1 N K,SO, 50 XO 'tglf. I (,i{f), g> 

2 0.1 N H,SO, 100 G/S 't (p ?. 'f 71-Cf."' 

3 0.1 H H-.S()• 100 G(S 'io3. 3 74l.3 

4 O.lN NaOH 100 Mod 757.7 17~.'1'.> 

s O.l NNaON 100 Mod "3.~ 7"/.0 

6 SQica Gel -300e Mod Cf'f.(. ~ 'f$'f. I - -- ··---- -- ----- -

t:hts lrtlp1ngtor opt1onal,, pet Method 26A 

Sample Log 

Sample ID Number S.mple Oe sa'iption Container 

VS2·STK·l .tli_ -M26A·Acdlmp HN•Isene Add lmpi'ISO' 

C.t<h & RO>se 

VS2 -STX-ll!_-M26A·Aiklmp SOO ml. AJb fine rm, lnaer 

Nalsene _ __ C.tch_& Rinse __ 

., 

~ 

L 

.,/ 

.,/ 

Recoven!d Ill' "]:>/>1Yl 

Sample Recovery Checklist 

~ If transfer llne is used). OtsconMct transfer liM, and rtnse three times with Of 

water Into acld lmplnger catch bottle . Transfer bottse to laborttory with lmptn.gef 

n ln. 

Dlsas.st mble sampfetraln, wfpe aff excess wne1 and Wtigh each imptnger. Record 

the. flnal wcta:hts In the Moisture. Oeterminatlon settlon of t.h1s data sheet. 

~condition of the sllico aol im.,...., . .: ,. spent 

_ / our contents of tile lJt, 2nd and 3rd (contamir,a acid) lmplngen Into tile Acid 

implngtr catd'l bottle{s}. Rinse lmplnaets and thnnectinc glassware with deionized 

WitN k'lto tht Ami!' bottlit(s-). CDmplttt add inlplnger SJmplc La-beJ. 

_L 

./ 

Not8s: 

Pour the contents of the 4th and Sd\ tmp;ngets (containtna NaOti) into the alkali'ne 

implnger catch bottie{s). Rinse aer$ and coMecting Ji~ware with dek>nlztd 

wJttr Into the same bottle(s). Comple:tt alkaUne Jmphl&er sample libel. 

t.oa samp$es into logbook 1nd storelppl'opriattfy. 

RDS-19; Ht:l/r:b by /fPA AWIJ.od t6A 

Pv EM SOP-ell 

F&Wion ()ate' July 20/J 
Sample Type~ Mult1 Metals (Mtthod 29) Date /0 • ft-1 3 ----- ----- Pagt / of / b-------------------~~~~~ 

Project Name: VeoGa • Saur et, L COndiUon: 1 ~ ------. Sam:pling Triitn Leak Rite (dl'llrHQ 

Project Number: 40941525.30.02 R\ln: J.. 8 Not.de 10 -

Facility: fi<ed tl.,..th- un;t2 CoNoletD A J&! 311 !louie Oli ~ 0 ~ 

SOur«: Stodc I>GMCf / . QO ,Z Barometer 10 'JR· z._ 

Operator f 0 f '-'Hill /, 7 &)() &or. Pre» .I"Hol 2"?. { "/_ 

Doct Dfm• nsk>n(s) ~ !>e ~ kf 10, '3 iJ Stor. Pross. rw,o1 tJ, D .z 

Nou:1eCallbratJon '"til"t ~~ .{ A Etevation tl't} d. 

eauper•o -zooq() 3 ---.....- ~ J- ~ o~ 1"''""'.'"•m'"'1 ) 1 

'""'"' o.oo?. @ •S.o 

Pltot ~ 10 S ~I '1 

PTCF o.zq 

Pkot TU~ l eak Check 

lnklll (•) ct. 7} (-1 do?:> 

Final l,o;~ 7"> HOk':> .) 

Point CJoc:k Time DGM Attding 4P ("M:M AH f"Jot:O) Tempt•nturo t'"fJ Vawum 

(h~ Slid< Probe fKttr Imp Ed DGM In ~I 

5t. 1'\ l.fi) 3"1.1- 6.1": (' <; 21-17 -:< 5c> t. \ 1 1 :3. 5 %5' ~.; 

~ .. =e; ,.,1tz'i( ~ ; t. La 'J.lf(( .252 tr S 151 3.,5 

L-.1 2 I r; 6/ c: 11 s "';; I 7 /. X'_ 3 10 2 5 2 2.(.(: If~ "t3 . 0 

f>ft>.P I f / t "':Z 3>. 1h · ''"' &', { -..1 / 'vlo~.l~ I" _,r.,. c._ t/ =- .,b:2..Q. t.r 

I q3 l) .<'l /) 7:!> '1. '-\ '?>'?:4 ').If-<{ ;(~( 51' 1_.<_ ~ t ) 

'>ftJ f 1 ~P, 1 qzc *71 

Notes 

-------------------------------------- Sl>S-07 Mc!Dis by EPA M<tMd l9 

N EM S~ 0/7 

v/;'20/J 

VES013881 
~ Cl.l 

0 

<H 

00 

00 

N 

Condfdon No. 1 Project Name Veoll - s·aucet, IL Multi-Metals 11\Jn Ho- / B 

Prl)jett Numbef" 40941S25o.l0.0~ 

Date 1~/? /1 3 

No Determination of PM 

EPA Method 29 Baionce 10 TE if I o 1 14 

Recovered by L::fl.tVt 

Source Untt 2. Stadl: 

Moisture Determination 

tmpinatr ConttnU 

votume 

No. (ml) 

Confli:utation l'lnaiWt. lcl lnltiol Wl. (II) 

1 ·' 0 r./0 '!71. 0 {e:l5. I 

2 Nlt~cll'e<exldo 100 Mod 'f'l<f. { 7 5'1 .fl 

3 Hlt~d· 100 S/G qq'-,3 7Z3 ." 

• Mod /tJ/:l .Cf ~37.8' 

5 kMnO, SOin 100 Mod '133.8 75~ '1 

6 KMnO,S01n 100 Mod 76(.5' ~/ ff 

7 SiliCa Gel "300s Mod Cflf/p, ~ 't:J. '?. 1 

if A - - ~tl 701 ~ ~33. z._ 1 Per the method, thb flr.st l,mplnttr I! optional and may be excluded for source..s with 

mol!ture catch ;nrldpa:ttd to bt '"'INA 100 c (Sed ion 8.l.3.2) 

Sample Log 

Sample tO Number Sample Desalptlon Containers 

VS2-m<-1 I e. ·M29-PNR v l.50 ml Probe and Nozzk Rlrue 

VS2-STK-1 t8 ·M29-Filt ,/ Pe!Ji Dish Allor 

. VS2-S'TK·l~·M29-NPI ,/ ~ !OOOml Nltrlc lmplnctr~ /-' 

S2-STK·l~·M29;J.Ifft./l'l '+ ./ 

t O DO l ~ IM9ln&er""-'f 

VS2·STK·11Jl·M29·Perm 2. lOOO ml Permanaanltelrrplnae~.r 

vS.i STK·l~·M2 HCIRns l.S()ml HO Rlnso ol 

V' Pt~ onpnlte lmplfller 

VS2.·STJ<. · 118 -l'\2., P~r ... :1. ./ sw....t p-J·~·~ :c..., 0 

-··-

* 

z.. 

1 

,/ 

-

........ 

/ 

/ 

........ 

v 

..£ 

...£ 

,/ 

/ 

Sample Recovery Checklist 

Rinse and bc\10<1 (lrntw- wntt nnu ~ with O.lM nltr\c tdd into PNR bottle. Note - use 

Teflon brush. usc a tot"el of 100 ml for the PNR and front-half filter ti n~. 

Rinse the (op<iOIIaQTeflon 1ransfer tine w1th 0.1M nltrlt acid Into Nl bottle. Use o total 

of 100 ml for tile transfer line and lmplnger rinses. 

Sepantt filter holder and piau niter In cletn Petri dlsh.. COm~te $ample label 

Rinse front half of fUter ho'dt.r wtth O.lM nltrk: add into PN:R bottle. Use a total of 100 

mL fo< the PNRand front-hoW ~r rinse. Complett PNR sample label 

Ois.-assemble Simp1e tnln, wtpe off ew:ess yqter atd weigtt tidl impinger. R.KOf'd t'bl 

final weiC)lts In tho MobNro oetannlnotlon section. 

NotecondltionolsillciaoL "':lO "'pont 

Pour contents of Hnt l tmplnsers Into the NhrtcJperoxide impineeratcll bottJe(s). 

Rinse the tmpingers, filter support end badc·half of the fitter ho&W and c:oonec:ting 

gJassware w1th 0.1 M nit(oc acid nm• bcmle{s). uv. • total o~mL fo< tht tmuler 

fine and impineel' lii\St.J. Comp~te Nl sample labe!(s). 100 

Rinse the 4,. (initially empty) lmplncer with O.IM nitric acid into the tl'n9tv lmplncer 

rlnso (EIR) bottle. use • totol of 100 ml fo< this rln••· Complete EIR sample Iobei. 

Pour the contents of the 51,. and 6tt.1mpingcrs {penn<lfl&anate impin..gers) tnto the 

pormancanate lmplnger eatch bottlt (Perm). Rln" wltlla tot>l of 100 ml of 

pe:rm01npnate soluuon and tOO ml of 01 water. Cc~tte Perm samp.., Ia bti 

Put 100 ml 01 water Into HORns s1mp~ bottle. R.ii\Se t'he permanpnate impin&trs with 

a total of 25 mt of 8N HO into the .sarne bottle. RJue im:pingers wtth 100 rnl 01 Wl t ef 

into the same botda. ~ttt HCIRII.s sample tab!.l. (Note, thls i.s not ttq\l•red if there 

is no YLstbSe solid reSldut) 

l.Og sample$ !nU> lotbook and sto"' appr.,.,_ly. 

1; I COmments J:H. 'fA k., ~r.J ):..,;> • 'f €)_ /?/ 6 _ I Nd:if<- 1'~-r.idl!. ~~~ ~ r--t-s .. te... lo&l"rL C4rrtJ 

O~r ;,.!., it.-.- J$+ 1(('1 0"' ,;..p; ... ~. "ftL .2J 

/(tY1 ,.()/f i-.p o~!IH' w·~ .... t a/feef-4:1'. 

RO$-ZS; Metlls byE!' A MZ9. no PM,,_,,""""""' 

PvfM SOP·OIT 

llcvisioft Cotct: JIJIWllr'Y 2013 
S.mplt T~ PCDD/PCDf' (Methcd 0023AI Date / 0 I?~ 13 

~ Pate I ot 2-

Project Name: Vtolio - Saucet,IL COn<fotlon: 1 T<ain l .. lo Ita~ (dm @I "'Hcl 

Pro)eC"t Number: 4094:ZS15.,30.02 Run: .J:_a Nou:le iO - lnltial o.ooo • 1 0 

FadUty: f lxtd H.-· Unit 2 Ccnsole iD It/ If() 1 Noulo ola (lnl 0 . 't l ( ... Oc:>C) f! It 

Source: Stodc DGMCF (). fff S.romt~riO af- z.. to:TubeiO s--O) 

Ope<ator . J' C. t.H@ I, (If'/ ear. Press. ("Hal 'Z?. ~ 9' PTCF e!), 8' ?t 

OuaOimenslotl(tl 1't\..."J.-...., • '•~ Kl - Sbt. PltiS. ("'H,OI 0. () <.. Pilot Tube l eali:: Check 

NO'ldt CGiibraUon 

-.-&:!..!.!_ J!lo.'H> ~ rJ87_! 

Elevotlon (ftJ nitlal (+) ._,.- (-) I/ 

IJtliMWt to !!oromtt.ttt 

Cl.periD ? 0(1 ~ 0 ) "'14 Final (•) I..--' H / 

P~nt Clock Time Dry Gas Vol. t.P 4H Temperature rFl v......,. 

(ft1

) ("H,O) ("H,O) Stack Probe Flltt.r XAD Inlet lmpb1t DGM HtTrt.blt (in. He) 

0 W -t l!i 'fO ¥'1 t . 'l'l 'l 0./) /.c.. '37} l.'ft '1.1/~ s> !i' ro <~• if'. sI f ~~ ;,. v~ 1./t~ ? > {)..tO o.n 1 s-f <.4? "t.l() j""' S"") 80 <-o-~ (_ t> 

)C l"'r' I\ J"tl v. t'6.f/) 0.1() (). , l.. 

') '"'" 'I..S'O 'ZSS' S'6 !ift fo ~s- •-o 

'l:l ,___. /5~~ 'f1Jt. 5~ Q.Jq lr.() 1'i~ '7.V' 'l.S"f 61 5'f '7? U.r 'i'- 0 

~ 1-«"" 1600 . 'f?'l.f('l. cut /.(~ "3.t> <. q r~ 67 >S" 79' "2~ r 9.o 

7~ "l.6 llo f: Yn.o9 0 If I. 'J!' '3 :1i'' 'L H .. 2.{<1 66 >z.... /9- l't'r I'~ l:) 

' 1{10 Ot. . ~{"' 0,/ > I, $') '1 L.\'7 l-~6 '(, >I f'O "l.(r /q. 0 

~ I(/~ J«.c l. cJ./7 • s-s- 1f'L "H't" '1~ (/ l't lC> '26s- 10..(:) 

9b ~--13 16 ,_ () S'01. ~9' (7./f /. "):;,- 'l' t. "l.V~ "'Z "G 6~ '1-7 (C) "?_~,- /(1. S" 

I~ q4:. 1 a 1.. s- S ll ,y-0 ()./6 J.SO JH. ~so ''"'' 0~ V')> v '(.6.} '· () II.< . II ·-" 11:,., 0 -s-t(. r? 0./? /.60 ..,,/ ?H. 'l.c-g-- ("7 ~go ~I -z.o-r 9-.S 

) 4-'f tl'l r ~ 1-P.o "'!. 0./7 t.t:o ) ,,... • 1 'Z.; ;> 6~ > sz.. Z(!>- ? . .> 

19, ~~ ;; v() }1.1 ~~ t> II. qo ...,.d )...\'~ 11-S" 7 0 '17 f3 ru-~ D II '5-6- I( (j~ 5l.. '7.1 'l.. 11.1(' I. '10 110 7.. 'f, 'l...rt ·~ 'f'7 n u.s- p.o 

IC! ! I(C'cJ ~~" 6~ '" I . {() 770 'l.3CC t r 8 6</ "17 ~ ur 9.r-

(; I{> 5" n'f.::>o b . l(/ ' ·• 0 'J '() '1...)/ ._,, 6 "\ '{f ~~ ~ "2.Gf"' t . .s-

_£. /)0() In>. s-9 0-1{, I. s-O "110 l.D It n·· n Cff rt.t ~r 9. /") 

6 /")(1~ Pll.o<.. 0./'\ lt. ~O 1,~ ·u s- l<{o r;-, <;~ IH z_{(' f( ' (J 

1 'J/0 "Y'f l:<g~ ~-~-t 11 .... ~ e' • ( _i_ "" P, o ~v~ /I/ II Jl. A./. !. -~- ,( .:: o_ ~~ 

s- 1 t '7lr- t; t/CI ~ 1 'L 0.1'> 1.1.(0 '1~ z~, '7..6() '+I 5''1 ~s- 'J: t: $ 1/.) 

I 1'7 10 <;Cff,)7 0./'J /. 'tV -,y-o "Z.H. '~ I <~r ~6 us- /I. 0 

I / 7l ~ HI. S'C. O.r) /. 7..[) l t"l zn .... l. C'~ 't1- 'I"J y$" -z~r II. tJ 

1 /") 'f 0 SS"f',OI l.t~ l/. 110 1't6 H'~ ~n lll Yt" ("" ?..((" ~. r 

't. /71/S"' q ·<[. 6'1 d •t6 1.)0 JH , n. 'lrt '·1'1 ~9 I&S" 't('r' )'l.·T 

"L tls-0 H/.lo 0.16 t. ro 7 1tJ 1';1/ Z..lO !/) S'O %"> 't61" lt.r 

~ /")f) ~(f',l( 0 0. (7 t. co '3''0 -z..o z6o v.q ., i'-6 ?...rr- l t. r 

'} I1JO () '> 6,.0, 0.1c; /. 1/() 17L "2.~l... ~J"9' 1./r"' S"/ f'6 ~r 1~. (I 

't / to<) S"'t.' u ().I} I.VO 1"19/ z.n '-fi' y.~ St. ~d ?..(r . 0 

"i I Y'/0 ~''· )~ <?, ,.,. I. 'I o ~~, '1-S'/ as-r w s-s u ·ur I~. 0 

!Hotor. Ad.!..! <lh.ul CQ!M~tw o..I'W ~ .~~ ~ kj!~c!wr-. SDs-11' I'Ct>OIPa>F by SW..fi46 ..... 11N>dOOZJA 

lfe,o£M SCJl)-t»J 

II•>~~~<M&.fcl~zoJl 

VESOJ 3883 
Project ~ Veolll. -Sauret. IL. 

Projlct N\lml>e< 4094252.5.3U2 

oat~ te / '?" (!.3 

SOurce Unit 2 Stack 

Moisture Oetermlnation 

Imp Conh!nts Vol (ml) Conflcuration Anal Wt (g) No. 

I . - K/0 t't?(J 

2 H20 -I(X) G/S ?3o.o 

3 H,O -too Mod -:m:t 

4 Silica Gel -300g Mod f8(.'1 

s 

6 

Sample Log 

Sample lD Number Sample 

COntaine_.r 

VS2 -STK·1L -M0023A-PNR 500ml 

VS2-STt<-1 ·M0023A-Filt Petti Db~ 

VS2•STK·l_ ~ •MOD23A-e'R 500ml 

VS2 STK·~ M0023A-XAD Sorbent Trap 

1' 

< u 

g] 

0 

w -

00 

00 

""' 

Condition No. 1 

Dioxins and Furans 

SW-846 - Method 0023A 

Run No. I {3 

8alantel0 775- ~f 0 I A 

Initial Wt. (C) 

'/3f;,.O 

7.Zg. 8' 

72(, . (p 

rso .Lf 

"-"f'lon 

Probe •nd Noulo 

Rlruc 

Fllt!r 

Cond•,.,.,. Rinse 

XADSorbent 

Reco.,.red bv Of?M 

Sample Recovery Checklist 

_L_ Rinse and brush probe and nozzle: three times with acetone, twice with 

methylene chloride and twice with toluene. Recovor Into one bottle 

(PNR). 

_..:::'_ Separate filter holder and place f~ter In dean pre-rtrued, glass petri dish. 

complete F'~t sample label. 

_:L_ Seal XAD trap ends. Complete XAO samplel•bel. 

v Rinse front half of filter holder Into PNR bot1le: three times with acetone, 

- -- twice with methylene dllortde and twice with toluene. Complete PNR 

sample label. I _ _ _ Disassemble sample train, wipe off c.xuss water and wei8h eac:h lmplnger. 

Record the final weights In the Moisture OO(ermlnatlon section. DISCARD 

the lml>in&er solution. 

_ _ "'_ Note condition of the silica gel implnger. --"spent 

__ /_ Rinse the back half of the filter holder, Teflcn transfer line( If used), all 

connectins glassware1 and the coU condenser: three times with ltCetone. 

I twice with methylene chloride and twlce with toluene. Complete CR 

sample label. 

_ _ _ Log samples into log book and place In refrqerator or Ice chest. 

Comments 

RDS·30.· Otoxfnsrrw:!Flnllti,SW..U&~A MMd:J 

Prr EM SOP-<123 

ll.Wsitrn Oct~: JtJN<rY 20/J 
U-em

roje<.t 

_;_p_le_T

Hime

ype ~--

: 

PCDD_;_/

VeoUa 

Pc

.. 

F 

Sauaet. 

(:.... M_oth_o_d_

IL 

002_3A_;_J _ _ -1-o.

Concutton

t_•.:._f0.:._-.:::

: 

8'

1 

.:_.:::.3:__~ 

___.,--

~ 

----..., 

Peae :2- of z_. 

Tfllln luk Rate (dm § "H1J 

Proje(t Humbor: 40942525.30412 Run: _Ls NO D ~ nidal /" • Jl , 1 

IF~clllty: flxf<l H<tlrth - Unit 2 

~rce: St&ck 

Duct DlmE<IJion(sJ "5 C. ;' 'I 

Nou:~ C.lbt-aUon 

ClliperiO 70091'\ 

5 

I ?:::I 

Noted: 

OrfGIIV

-· ol. 

(ft~ 

G t'\. ?l) 

C<><uoleiO f6/illl Noni•Dia(inJO.~'fc( 

DGMCf fJ. 9 ff Barom<t<r 10 ,t /J-'2.. PhotTUboiD S"· G/' 

Kf - Sl>l . Press. ("H,OJ 0. () 1.. Pitot TUbe Leak Check 

Initial (+l c "" !;J. I 

(·J . f 

Sl>S-m /IC1){)/Kf)l'by SW4146 t.',.th«/002JA 

PuEMSOP.OZ~ 

Rcw'sion d4t<i'4A/N'If i!OU 

VESOL3885 
PK J-5ro 

~ 'l'rPe - Particulate Hatter (Mdllod 5) Da<e f ()- 'j· 1 3 

Projfcl Nome: VftOJia ·Sauget. IL Co<l!Jtlon: 1 

Fitter No. Page 1 ot ; 

Train L•ak Rote (cfm 0 ' Hg) 

Pro!«t _, 40941525.30-<12 ~~m: k...A 4ou~e to .__ wt~a~ (}. (JO '(- ~ !5 

Fodlily: FlxcdttearUt- Unlt2 ConsoloiDAff. i"<,CJCf Norne Oia (ln) /?.4<.3_2 Final (J 00 < 4:> 10 

SotrCe: Stllck DGHCF ( (J 0 z. ~ 10 ·fl.. P- Pitot Tube 10 p _ 3 0 ;:t 

w 1- M .; 'l "133. 1 o- rh •. ~ 1 '16 2 ~'i 1 t.c. l.f¥· t c. '1: , W'3 Jo ooq-::.75 0 .17 1.7 3'102S1 :u.."i .Lj·C · t 5 

~5 loH ~/ c; O.fl 7 '3'10 7~'i <C1 lfq I f 15.0 

SO.S-rlk PM byB'AMctlfDdS 

Por EM SOP-015 ll~l>ltt# F~20/2 

Ro"'-cdi' 2013 

VES01 3886 
r;i 

en 

0 

-

w 

00 

00 

_, 

4' 

~i 

Pro)e<t Name \l on~- Sau.cet, fl 

Prfijtct Number 4094252.S.10.ol. 

Date !o/9 /!3 

SOorce Unit2Stedc 

Moisture Determination 

lm~No. Contonts Vol (ml) Configuration Final WI(&) 

n- Water 100 Moo Cf.2/. ~ 

/3 Water 100 G/S <J51.!> 

Tlf Empty - Moo (pS'/. 7 

~~ Silica Gtl - 3001 MOO 951. <t 

11 C...t>ty - Ko 'f~.'f 

6 

Sample Log 

Samp~ 10 Numbc!:r SamP'e 

Contatner 

Condl& n No. 1 

Particulate Matter 

EPA MethodS 

Run No. :Z A 

Bolan« IC I£ 'flo/It 

Initial VII (G) ' 

7#..8' j 

7 53.!!{" i 

~£!-F..:i... i 

't'f! . .3 ! 

S11. 'i" 1 ~ 

' 

DesuiptfOfl I 

ROCOYe<fd by -.pf/111. 

Sample Recovery Checklist 

...L_ Rinse ond brush probe and noule with acetone Into PNR sample bottle. 

~ Transfer bottfe{s) to laboratory with lmplnger train. 

_::::__ Separate filter holder and place flltorln dl!ln pr«lnsed glass petri dish. 

Complete filter sample label. 

__:::___ Rinse front half of Olter holder with acetone Into PNR bottle. Cornplete 

probe and nou!e rinse (PNR) sample label. 

~ Oisassemble sample train, wipe off excess water and weigh each lmpinger. 

Record the final welshts In the Mols1ure Determlnatioft section of this daUl 

__:::::._ Note condition of the silica gellmplnger-:-'5'"'0% spent 

.....J:::::_ Log .amples Into logbook and store appropriately. 

commtt~ts~ /Mad SS KO ·;,Lu- e-,.t-y \ a._. "-

VS2-STK-1 2A -M5-PNR 250ml Probe and =tie ~ ... fL k .... ~-o.-r al.-eJ ~f' -.--...L 

VS2-STK-1 2A -MS·Filt 

" o; 

Rinse 

Petr1 Olsll Filter 

-

i 

ttll t- tl S" o .... f,t',.,,.f,.;..... 

Rt>S-J3:PM byEPAM•tlo>d$ 

Pu <M SONJ/5 

R•viSIM O.te: J"""""Y 2013 
san.- Type- Parllculate Matter (Method S) Dote /0 -16 -{ '3 FAter No. P~gt J of / 

Pro)CGt Name: Veolla - Sa1190~ IL COndition: .& f'(< .< 5'" / / Train l eak Roto (ctm 0 "Hg) 

ProjeciHtmll>or: 4094252S.JCI.{)2 Rul: ~ Noule ID - Initial {). ()b 1/ 0 /:; 

Facility: fllced Hearth · Unit 2 Console ID--;t;j{j '\ <;~ Nozzle Clio (lo) t;,ij-3 ~ Rnol () .,C02 @l / t) 

SOIJrca: Stacl< OGMCF f ,00 :z. er ID f4., fJ- ~ l'@l Tube ID /). 3 0 2 

Operator: { (J r: 6H@ I ntM Bar. Press. ("Hg) ::z q <; 2 PTCF 6. f 't 

Comments: SDS· l6: PM by EPA M.IW 5 

Por EM SOP·OI5 

l«:viNJJ l>af• : F~wy 2012 

~ZOIJ 

VESOI3888 
< tTl 

t/) 

0 

w -

00 

00 

\0 

r 

I' 

Pro jed Na~ Veolia-SauJet.IL 

""'Joct HUIOOer 409-42525.30.02 

Date /O/;oU3 

Source Unit 2 SUd< 

Moisture DetermlnatioD 

IIT1> No. COntents Vol{ml) Confiauratlon Final Wt {g) 

/ 7. Water 100 Mod 'lt8. g 

I > W~ter 100 G/S g5S:Z.. 

!Lf Empty -- Mod 6~1. z. I~ Silico Gel -300c Mod '/3fJ. 7 

/1 G-.,ty ~ ,..,._S5k ' 8K.Z. I 

6 *"'.ef'l 

Sample Log 

Sample 10 Number Sample 

Container 

Condition No. 1 

Particulate Matter 

EPA MethodS 

RunNo. 3A 

Bal.lnce iO T£ ¥1c1A 

Initial lilt {B) 

7r;3.t.f 

1~·b 

~l.{-g.3 

913.'+ 

~oo . 2-- ~ 

Doscri ptlon 

R""""'red b! ];f7V/ 

Sample Recovery Chec.klist 

V Rinse and brush probe and nonle with acetone Into PNR sample bottle. 

,/" Transfer bottle{s) to laboratory with lmpincer train. 

.L_ Separate filter holder and place filter in dean pre-rinsed glass petri dish. 

Complete filter sample label. 

~ Rinse front half of fllter holder with acetone Into PNR bottle. Complete 

probe and nonle rinse (PNR) sample label. 

~ Disassemble sample train, wipe off excess water and weigh eadl impinger. 

Record the final wetahts In the M oisture Determination section of this data 

~ Note cond"ion of the 511ica get lmplnger:<=ZD % spent 

_v_ I.Dg samples into logbook and store appropriately. 

IIS2·STK-1 3A ·MS·PNR 250mL Probe and Nonie a~ ~ cc--Jl..-s 

VS2·STK-1 3A ·MS-FIIt S~-

7' 

c; 

Petn Oish 

RlllSe 

Fitte-r 

RDS • J 3: PM by fi'A M<tii«J 5 

hr EM SOP-Of~ 

ll#vfsion /Mfe: Jorwry Z0/3 
Sample Type: HCl, a, (Modified EPA Method l6A) 0a1e I()-{ (J - i) ~ N(A Pa&e I or I 

Pro)Kt Name: VeoUa ~ Saucet. ll CO:ncllt\on: 1 1107•'..-.. Sctmpllns Train leak Rate (rl""O •ttc) 

Project Number: •0942515.30-02 Run: 3 8 Nozzle 10 - lnitiaC (), CJOC CU) 

Facility: Fixed Knt1h - Unk z Const>lt 10 A I c i3"' 5 MouloOio~J o.'{1.S Flnal o .cCIIS 0 '\ ,<;; 

Souru: Stade OGMCF ftl/ earometer 10 (3 f- 2. ~ot Tube 10 iJ,. S' .2.1 

OpeNtor [ /J { /i<. Jl/ 4Hf!l /. '{)./i Bor. Pross.l"l<oJ 2li.q,1,. PTCF (}, ft 

Duct Oim<nsion(sl ~ lf '!) '' kf S.u. SUL Press. r>tA 0 0 2_ Pitot Tube !.elk Cbedl 

No~ CAUbration 

---0~~ ~~ Meter E1evatlon (ftl Initial (+)~? 3 HOe')) C.Nper 10 'h> dfol (rti;MMtolltont!ttf) 3 't 

Fi."\1.1 1+1 ot..T"} c-ld::.?j 

PoJnt Clod< Time DGM Rtodinc 4PrH.OJ '="'' 

Tempenoture rfl Vocuwn , • ..,, ~~~ Stade Probo fMtei Imp Exh OGM 

itJv'l ~/".. 11-~ 7ttq:n t), 1':\- • lA't~ lfJi<. 'tS'-\ 1G.o fc.S' 9.\ y.o 

, ,< ?'a .o1 0 . 11- /.l{o 'i;q'~ l:«=~ U.l i.f~ 9.\ ~.c 

\ 1,.~0 S1.1; 

0 ' " 

..... "0 ~'i' !> 7~• U.!.. I{ c., &o ~~ 

nc.\<" -~4-~e, o.ls 1-"l< ..;;,-9: 11J..t... 71.-,'1~ L(-:f !>I r.~ 

/~C,O 8'·\.'{o o,u ;.r..< I ;z,'ft> 'Z.<..t.. Z.<..-; -IR ~c::. (, -0 

~<; <to. 'l.t .. o.lt. f.~ '3'12. ?~1 ""' ~ &I l..o 

1?>00 '1 1~ o. 14. J/i,o 31-l· 'Z.c..l z.t-S so & \ b-0 

13<1!> ~t '!A o. l~ l.t~ ..,'\<.> '25'\ 2.Co'3. 9:> S'L (. . 0 

l?>\t> lo<>-1\ o. ll. 1·'3o -'ctr ~~ UA St> ~"L <.. • ..:> 

1!>1!> ~- a.\3 o, 11. ~0 ~ '2."' 'l.J..1. 5':> S't <...o 

fl.1-D (0'-·"'' ~ '1';. tAo ~'iQ l(.t> .,,_~ Sl 82.. t..o 

32.~ I 6"f V.~ 0 -11. ,.:,o .¥.4 1(.\ u.~ ~I 8J (.. (.) 

~3o fti3fl( 

. 

Notes: SDS-ZI: HCI, C11 by EPA MctMd 26.4 

Pu £MSCNJ21 

-Dcic> ~110/J 

VESOl3890 
< rn 

0 

-

w 

00 

\() 

-

Project Name Vtolh~ - Seuset IL Condition r.o. 1 

Ptq<a Humb<r 40t41525.30-0Z 

Doto /8 0 o /13 

HCI/ CI2 

EPA Method 26A 

RunNo. 38 

llolonce 10 T£ tfl {)/A 

Source Unit 2 Stade 

Moisture Det e rmination 

Imp No •. Contents Vol ("") Conf"curation RniiWt(&l Initial Ylt 131 

l . 0 .1 NH,SO, 50 KO 'f3S::{ 1.7 

2 0.1 N H2S04 100 GIS lf(p{)-1 7'+1.0 

3 0.1 N H,SO, 100 G/S !7b.9' 7'(5". z_j 

4 0.1 N Na011 100 Mod ?u~/Z 71'-·1 1 

5 0.1NHoOH 100 Mod 7~-Lf 7C?(). zJ 

6 Silica Gel ~300& Mod M;;.. Cfs/.2) 

! 

I 

this lmpintQf opttonal. per Mothod 26A 

Sample Log 

Sarnplt 10 Numb~ S.mple Dts<riptlon Contolnt< 

VS2·STK·13 B ·M26A·Acdlmp ll a~ ne Acid lmplnaer 

Cotdi&Rinse 

SOOml Albl:ne lmplngtr VS2·STK·1M_·M26A·Aiklmp Nolcene C.tch & lllnso_ ·- - ·-·· --- ---- --

... 

i!J 

s,/ 

.......... 

v 

R""""""d by "Pf/YI 

Sample Recovery Checklist 

{Otlly If transff!r line iS used). Ol.scof'nect ttansftr line, and t1nse three tlm.s with 01 

water klto acid lmplnger catch bottle. r ransfer bottle to laboratory with ..-npinger 

train. 

Oba.ssemb&e: nmph!: tTJin, Wipe off exce-1S waw 1nd weigh. each 1mpinger. Record 

the fklel weights In the Moisture DetcrmlnatlonHctlon of this data sheet. 

Note condition oftlle sib eel lmplnaor.""'Z-S; spent 

.,.- Pour contents o.f the 1st, 2nd and 3rd (contaloirtJ add) impfngtrs into the Aci~ 

lmpln.ger catch bottle(s). RJnst implngers artd connecting glassware w1th deionized 

wot<r Into tho some botlle{s). Compk!to add lmplnaer Simplt label 

,/' Povr the: Q)ntents of the Cth and Sth lmping«n (containJna NaOH} into the afkafine 

lflll)(naer catch bottle(s). Rlnso lmplnaers and conna<ttng glassware with deionized 

wattr into the n me bonJe{s}. Complete alkallre lmplr'lger nmple 18Jbe1. 

,_/' lOS nmpk!s lnlo logbook and store appropr-oately. 

Notes: 

tDS- 19: HCVQ, 6y EPA rh«i 26A 

IV-EMSONJ21 

Rttt~~'skm f>Dfl-; July 2013 
t-Sa-m'--plo'--1\1><!-'-- u_l<l_M<121s_:(_e••><~ :z9_l __ -+-o-•••...u/ b"-·...., 1 <b=<...-_,_1)-'-----l ------------- llo-Pa..;.'' .:../ ~-•'-='--=! 

Ptojecl Name: Veoll:a- Sauaet. l. ConditiOn: l __..-_.....--~ Samplina Tfafn l.e:Jk Rate (d.,."Htd 

Proje<lllumjler. 40942S2.S.30-02 Run: ~B Noul< 10 - lnllial 6 ,M 'f ~ /J 

FacUlty: FhcedHoOtlh·Unll2 C4nso et0A 1'!~ ou Oia ~) tJ.:'tB ' Final &..06·3 @ 't 

Source: Slade OGMCF {.,() ~ j B>rometeriO (!, P-7_ PltOI Tube 10 C)-( 9 

Operator £: f\ f ~H@ 1, 7 '1 11 B•r. ''""· ,.,.,, ;:z_ 4. ~ :::2.. PTCF {) fj '-! 

OuctOfmenslon(s) 3~.5' Kl q,O<;f $,.t.Press.c•oo,ot ().0'2. PitotTube lukO.ec* 

Nonl< C.libr.otlon - . ~ ~ Ele111tlon Cftl Initial l•l ,1@ > 3 (·) o:e ;>) •-•~lo '7oo"'~ --",If 7:/ A 1./.7. / I• i?:V ,, .. ., ,.,.., ,,.,.,~ 3d- ~..... VJ....,!L ~ (.,41..=2! \ """' HCI@73 -l ~>J 

Polnt OockTlme OGMRt ldlne b.Pf'HtOI A!lJ~.OJ Tempe,.turem Vacuum 

(It') ( '? Stadt Prob<l Filter Imp £Jot OGM In l"ll 

6 / t ( "6 J.:Z.7 .• ~ /).l'f /,') 3.'1 ::(~2.. :?6< sc -n 'f.ll 

Notes SD$-07 M•lt>is by EPA M<tiood i!9 

h r EM $11P..017 

!!<~:oil• Nt: July 2013 

VESOJ3892 
;ii 

Vl 

0 

,_ 

.... 

00 

'Q 

.... 

Pro)ect Namt! V•otia - Sau1!!t: IL Condillon No. 1 

Multi-Metals P~HU-r C0941525.SO.OZ Aun No. :3 B 

/Obo/;.3 No Determination of PM 

Date EPA M -rE- ~101 A ethod 29 Balance 10 

Sout<e Unft2Stod< 

Moisture Determination 

Imp!"'" Contents Volume Conr!juration Fino I wt. (C) lniti• l wt. (C) No. (ml) ,;, ... - 1 1 

;.~d. ;1.2.7/J. 7 o/f(). 2-

2 Nitric:/Pf!roxide 100 Mod '8't7.fl 75'1. &' 

3 Hittk:/- 100 S/G 74C.7 us-.o ' 

I 

• . . Mod {p tj(). 0 IP'!J8.lf I 

5 t.Mno.SOin 100 

- 7~5: b 7f,Lf, z_.. l 

6 JCMri04 SOin tOO Mod 75/S. {:, . 7£5'. 7 ! 

7 SliCll Gel -300$ 

- '111-7 '317. 7 ' 

'.., .... _....,,..._., .. _.,and _ ... _lot __ 

mokt~mt catd'llnticipaeiCI to bt ..,_, thJn 100 11 (Secdol'l$.1.3..2) 

Sample Log 

$Jmple .10 Number ' Somple Dosutptfoo Contalnen 

VS2-STK-& ·M29-PNR 250ml Probe and Nozzle Rlnse 

VS2-STK-136 -M29-FIIt Petri Oi5h FUter 

VS2·ST M29-NI lOOOml Nitric ITil!>lnctr 

VS2 STK·l~· 29-EIR 2SOml Empty lmpince• Rinse 

VS2·STK-1 .3 6 -M29-Penn 1000ml Penn.anpnate lnpinger 

., HO Rinse of V~ STK·l3a_·M29 HORns ~50ml 

Permang nat llf!~~~! 

J 

_L 

(/ 

-.1-

-1-

.L_ 

,/' 

./ 

_L 

_J_ _ 

Recovered by Pf>/11 

Sample Recovery Cbecklist 

Rinu smd btus.h probe :~~nd noo.nH!: with O.JM nitric add into PHR botde. Note- use 

Teflon bn.tsh. Use a tot-al of 100 mL for t'he PNR atld front-hatr fltttr rinse. 

Rinse tl>c (optional) Teflon tronslor Une wtth O.lM nitric acid Into Nl bottle. Use a total 

of 100 ml for tl>o tn<nsfer lin<~ 1 nd lmpi"itr rinse>. 

se.paf'ltt fitter holder and pia ~ flltt.r in duo Petr141Jh. ~te sample label. 

Rlnso front 1\aij offilter holder wltll 0.1M nitric acid Into PNR bottlo. Use o!Dtal of 100 

ml. for the PNR and front ~atf Olter mse. Cotnp~Mt PHR n mpN- Label. 

Oisass~e sampJe train. wipe off excess water and weigh eat'h lmpinger. Re<.:ord thefinal welJhts in the Moisture Determination s.ettiol'l. 

Non! condition of slllco Jel "spoOl 

Pour contents of nrst 3 imptnsers itlto tht NiUic/ptroxlde fmplngeratd'l bottle{s) . 

Rinse th•lmplnaers, niter support and blckAilalf of the tliltet' holder and conne~int 

classware wi1l> 0.1 M nitric add same bottle(.s). Usa a total of 200 m1 for tile transfer 

&no ond lmpincer -.. Complete Nlsample label(s). 

Ri~ tht 4

10 (lnltlaUy empty) lmpi11ger with 0.1M nitric add Into tho empty lmplnger nn .. (EIR) bottle. Use • lotil of 100 ml for this riroe. Complete EIR Slmplel•bel . 

Pour the contents of the s"' and 6 .. imp\I>JII> (perNnpna"' ilnpingen) Into tile 

permanaanate fmptncer utch bottle (Perm). EUnn with~ totil of 100 ml o f 

perman~n te solution and 100 ml of 01 water. Complete POf'm Silmple label 

Put 100 mJ 01 wat:e.r tnto HCIRns .samp4e bettie.. ftlMe the perm~n.cJnate tm,otncers with 

a total o12S mL of &N HO Into the same. bonf ~t- Rlttse impinc•rs Witt!' 100 ml Dl wattt 

into the same bottle. Comple-te HCfRns sample label. {Note, this is not required if !I'Kuels no visible solid residue) 

toe Amplts Into locbool< and store opprop.-lotely. 

Comments 

RDS·23: 1.1etollbyEPA M29, ,.PM, .-1 vohmu 

l'u EM SCf'.()/7 

Pilvl"siM Ottte: JtlfXIOI"J' zon 
D-5.-rm_pte_TvPe _·_PCD_ ot_OCDF_IM_ •_tt,cd _ oo_UA_I __ -1-o-n_e"'-' /(/'-!O.J..;/_<Q =<---/~'l'-; ----:><: 

Project Na:m4: VeoUa • Saueet.. I. Condition: 1 ...----- ~ 

P>ge f oi -.... 

Train Leak Rote(cfm IP •11e1 

Project Number: 40942SZ5.30.02 Run; ~~ Holdero -

Foctlity: Fl•ed H .. m. • Unit 2 Flnol () • 00 > @I ''~, :>" 

Source: SUdc DGMCF ~.f~f Barome<er tO /]P- 2.. Pltot Tu'bo 10 f'- 0 J 

Operator -;iC. 111!1!> /. {lf9 S.r.Press. ('Hcl 2.~. T'2.. 

Duct Dlr'Mnslon(s) ,8', ; 11 _,6 Pltot Tube lu k OW!ck 

lnlllal 1•1 / Hv' 

Final 1+1 " "' H "" 

Polnt Clo<* 11m Dry Gas Vol. AP 4H TempefltiM'e { .. f"l Vacuum 0 (ft') ("H,D) ("H,OI Stadt Probe Falor XAD tnlet Imp Exk OGM HtTrc Eklt (ln. HI) 

t ~ 'l.3f" (62..o~ IO.tt t • .ro l'~ ~ 'f'7 "'Z.sU s' 'f6 i'S" '2.6~ 11. o 

1 nvo ((~; ~tJ rJ.tfi /(0 "1'19 2.4t ?.n <;cJ </ t ~6 ur 11..> 

'?. II..V> 6(.~. ~? o./7 f, '10 J',f' ?>I 7.51 V.t? <f6 t?s- Uj- t;..r 

~ ''l.. r;u tn .. ?'l IJ. n t. ff' 11f '-s·o ~r~ ~~ </7 r~ ur IT. r 

"t. nJT 67,. -:>~ /9 t.C() ""!~' <.sl u .. ~ I'lL <,1~ 1'lb «or n.r 

J I)Ol'J . q ft <J ./? /.110 7f? "'.J'() 'l. ~l l!t (I ~0 ?;; 14 ( S"' ll..r 

3 not; 6't'-/. ot " ·16 1f' 'J?'t i<-~1 ~n <Ill >t &-6 c.(~ 1~ • .r 

J 1:}10 C't?.S"? fN7 I· YO '3,7 '2..</C" '2.s':S <lo S'Z.. 8"7 "'4ff' l tJ..> 

~ lJt(' 69t.n ~.n t.vo ~96 "1.\'., ls'"3 V"? SL r7 ur h?..r 

'I nw I69C/.::Ji? ~-16 /. Jr' "!'/& 1.10 1-n ¥f H ~.? us- /".or ~ ~'Z..S"' ~t;r;7.93 o.;.rlt .<.s- 196 <so zn c,t3 £ ' 8'7 'ZG> 111.o 

5" r-r-ro 7dt ~) o.,r; I1. 1.S"' -r96 '£>t ~ :</t. 5''- 'ff IUS' /~.o 

s- n 1r l7o<t.t:i' r!.r7 t .t/0 ~9r ""?.s-o 2.{'~ 1Yl.. s-~ R-~ ~~ ~/)'.t:) 

') 1/'fttO '707.~ 17.t'l' lt.~;o "']9(" '"2.,)0 'H) 'it~ 5}' ~,_ 7.6(" 11.0 

b /HT 71!.'2..'/ tl.r~ /. )0"1'') "tc;'-'S'..7 <// ~~ 90 ·u /1~! 

71 "·,t 1. it. ... 4. Gt :D. P:l (Q) ~ "II. r>,. .. L ~ ... ~ ,.. J. of ·o. mi>c> tO /t '' h'.t 

'lo l,c..{ to ·o 

~9 "'L(~ /2.. () 

~ f 7.t'r 11. sS/)5·1 7, PQ){)II'C()F by SW-846 Method (I()ZJA 

Pw-£U sa> .. OJJ 

b>l•iD• ~pril Z0/2 

VESOJ3894 
(/) 

~ 

0 

...... 

w 

00 

'C 

v. 

Project NJmc Veolta Sa~o~,cet,lt. 

Projtct Number 409U.S25.3().02 

Date \o{t611'2 

Source Unit 2 Stack 

Moisture Detennlna tlon 

Imp Contents Vot (ml) Conflcuratlon Final Wt (g) No. 

I . . K/0 _3o ~,<; 

2 li,O -100 G/S 1-u..o 

) H,O ·too Mod 11-2.. 1 

I SiliQ G•l -3aoc Mod 't=f1:z.. 

s 

i 

Sample Log 

5ampJe 10 Number S.mplo 

CQntllner 

VS2-STK-ll& -M0023A-PNR SOOmL 

VS2-STK·l ·M0023A·Ait Petri Dish 

VS2-STK-1 -M0023A-Q\ SOO ml 

_VS2-ST_K-1_ ( -M0023A-XAD_ So !'bent 

- _Trop ----------- -

~ 

Condltlotl No. 1 

Dioxins and Furans 

SW-846 - Method 0023A 

RunNo. 38 

Bola~ ID Tf£ tj( {) / ,4 

Initial Wt. (g) 

93S:9 

1-Z'/. ~ 

72Z.!f_ 

9t(5: ~ 

Oescrlptlo n I 

Probe and Houle 

Rw. l 

f ilter I 

Condensor Rlnse 

XAOSolbent ! 

- --------------

Rtcovtred by t::M ~ 

Sample Recovery Checklist 

..1t::::.._ Rinse and brush probe and nozzle: three times with acetone, twk:e with 

methylene chloride and twice with totuene. Recover Into one boule 

(PNR). 

~ Separate fo lter holder and place filter in dean pre-rinsed, glass petri dish . 

Complete Filt sample label. 

~ Seat XAO trap .,..ds. COmplete XAO sample bbel. 

~ Rinse front half of fitter holder into PNR bot~ e: three times with acetone, 

twice witl1 methylene chloride and twice wllh toluene. Complete PNR 

sample label. 

,/ 

./ 

./ 

../ 

Disassemble sample tralnf wipe off exccs:s water and wetch each lmpinger. 

Record the flnal weights In the Moisture Determination section. DISCARD 

the lmplnger solution. 

Note condition of the silica get implnger. !!{_%spent 

Rins<o the back half of t11e fllter holder, Teflon transfer line( if used), all 

connecting glassware. and the coli condenser: three times with acetone, 

twia. witll methylene chloride and twice wi1h toluene. Complete CR 

sample label. 

_ _ LO(Isamples Into log book and place In refrlcerator or ice chest. 

Comments 

Rl>$-.10/ D/oJdM 11rd Ftlr'riM, SW-846 M0023A, fltJ MeCf 

__ Per EM SOP-OlJ _, JdfO#Yi!OlJ 
Sample Type - PCOO/PCDF (Metho<l 0023A) Date IO·t0-1) >s;:: ~ac• '2 ol , z. 

Project Namt: Veolfa - Sauget. ll ConditiOn: 1 Train l eak Rate (dm@) "Hs) 

Projea Numbor: 40942S2S.J0o02 Run: ~8 NouloiO - nlti•l C. ~ I 

Facility: Fixed He.rth • Unit 2. Console 10,1/ l(lft()l Noule Oia (In) 0. 1/ l 6 Fln•l I 

SOurce: Stack DGMCf 0. fff Baromet« ID /~ P- ~ tot Tube 10 . fJ) 

ppornor :J{. ~HO /. {((f Bar. Pre$$. ("Ha) "l. f. f ~ TCF o. ,.'< 

0\>a Olmension(s) 1 t . f Kf so~ Pross. ("H,Ol ,.'-~ Pitot Tu!M l•alc 0.«1< 

Noultt CaJibt'atlon 

-e- o.l(v J!l 11~r~ ~ Elevation (It) nidal (rtll\lve to S.nnuer) (+l(', .. ~-~ I CailperiO ? 00~} 74 Final (+) . ~- r 

Point Clod< Time DryG01Vol M 6H TemperJture t•F) Vacuum 

Itt'! ("H,o) ("H,O) Stack Probe Fltt•r XADinlt t ·~Exit DGM HtTr<Ellt (in. Hal 

'f lt;"OO "7 t(.f tf &./? r. ~ ?'Is- "l. Vt -z.s-z.. lt,.t ({ >~ 'i9 '-6~ f l.. 0 

~£ / 'iOs- ?f'?.s-o 8-1~ / . ..,r "J')(! ?.ro '2.(""t. <I 'I n i'"~ <.or- 11 . .r 

5" 1r1o 6~ . 9z. 0-16 / • ., s- "J~<' "7. s-J 1_)"2- Y<' 5"6 g., ur //. st; I 'i/ ~ "?(( • .., t_ o.n /. 'I() 19¥ l.r;/ "l. S") (,!~ f~ &"%' 'Z.tfS" 1/. ss:;g / 5 1-0 7 (-,. > 3 1?.1_6 / . ., ( 19~ "l..~O "l.{") '~''- 5if '!?-? 76r II. s6 t>zs -; '1-1 r ~-16 /.}.r ..,. ") 1. ~I "Z ~") '1-z... >-z.. ~g- 2.(".5"" 1/.sh 15" 10 ? 7(. r6 "() ./t;" I· t r; "H'} 1. II~ l.S"} (/L n r~ 't(~ II. o 

b /5)5" ., ',.s-f ~-1'> /, "l. ,.._ "JH (._Cj ~ t r ") $10 >s- n- "2~> I/. o 

[' .. .l /'i llo ?~"3 ./,8 

T,~ 

Not .. : Sl>S· I ?: I'CDIJIPCDF by SW-846/oWthod OOZJA - "-'EM -Sn'412J 

-daf·J.~7ZOIZ 

VES013896 
S.mplo Type: 110, 0, (Modffild EPA Method 26A) 0•"' 10· /,'·I } Fllter No. Paae I of I Proj~et N&me: Veotla - Sauatt.. 1\ Condltlon: 1 JJ/It S1mpli.nc Train Luk R•te f<hr.• ~IJ 

Projoct Humber: 41l942S25.30-02 Run; -![_a NouleiO - lnMiaJ C.OOC 0l I 5 

Facllltv: F'iXed H«arth. Unit 2 ComoltiO l l f (, f )'j ') Nonie 013 (In) o .'l, t ~ Final o.oa'f @tO 

Sourc:e: Stade DGMCf /.0 fl Borom•tt<IO ~ /J-z PirotTubc 10 f-'l, Z "f 

Ol)efator 14-o.v- 611" I. n1 Bor. Pri!JS.I"fcl ;( tj . 1 'f PTCF (). 9. 'f· 

Duct Olmenslon{s) 3 6, ~ 11 Kf Q , lO Stot. Press. (.,., (). 0 'f Pitot TUbe leillk Chtdc: 

Nonlec.r.-n / 

~~ Meter Etev1tlon tft) lllltlal t•lbe >.> t-1()&>) -e- o .'{l.<;' J' o.'{z..,- Cllper ID 7 ~ <>'1!2 ~ (rt~w to l tnn:ndf'l'.

3 1 fi n~ I (•)0@:>1 (- )~-:>} 

Point OodcTimo OGM Re:adlna 6J> ('ll,O) 61li"H.OI Temper.ltuTe (•f) · Vacuum ('"'Hst [A~ SUck Probe flttef lm_pblt OGM 

IN-.~-c. '\~S I 11 tit;'/· o.r< /.t<: -z9.q '2."> \ ~t.1. '>"\ C:.."\ ! .o 

'\<;l> llf \~ " . 1"\ • 1,1 { ~<\0 Zlo~ U.'-1 '{( .. <..'\ 3 . o 

(\<;<;" ll8 .-:t3 o. rc.( '·'~ 3'16 ~" ~ <T- To $ . o 

IOoO ru.')L\ 1~ l.oS ~B'\ 1.<.~ -u.~ J 1:1- +I D 

~~ {Z.'f.V) 0 -1 < I.,( 3'lo U.<. l.Co'-{ S"t> 1L 6" 

IDI ~ r1:l . 1>S o . If /. <t ~ J"h ""'" u.~ c,3 ::j'{ '-{. o 

IOI~ l}d ~oS o. \~ ~ ~92 f'-~~ t<o3 <;\ i-<... 0 

1070 ~.1<> 0. \C. qo ~<n lu.9. 2'-'1, '{'i .J:::J- D 

01.~ l:SC..lt. 0 . l'- (.~ ,.n. ZA"t lu.-=t 4% :t-e 'l. o 

~~ ~~~~0 o.t'T <\.o ~~?> '2.4:>'-\ 1.-<o< !{i" 1:¥:1 I • () 

to'!;( r\17. 15 0 . 1 t. I 1 :~o ~-n 2,.(.<. z.r-c. 1./S ~0 j . 0 

1o~o 1'-IS. \ o 1~ '1~ ;qr.{ V<>'-1 ]&.( '{'\ i,l 411.0 

lo'\~ 1'-R. 1 <..o 

otes : SDS-lJ' HC1. C/: byEPA Morl><>dl6A 

l'orEM SOP~/ 

1/cvisionl>#IO: ~lOIJ 

VES013897 
< 

~ 0 

,..... 

.__, 

00 

\0 

00 

Project Nlme: VeoO.. -S!uCe.t..ll Condition No. 1 

Pro)ect Number •0942.52$.3()42 

Oato /0/11/1.3 

HCI/CI2 

EPA Method 26A 

RunNo. i(-lJ 

BaJa nee 1~ -r;::.. /.fl {) 1 A 

Source Unit 2 Stack 

Moisture Determination 

Imp No •. Contents Vot lmlJ ConfcurWon F1n1I Wt{&J 1 nilla 1 Wt Ill 

1' 0.1 N H,S04 so KO 't35.'f 5' 

2 0.1 N H,SO, 100 GIS ?'f7.1 75/.1 

3 0.1 N H,SO• 100 G/S 1o2.~ 1tfl. 7 

• O.INNoOH 100 

- 7&5.7 74-7.!± . 5 0.1 NNaOH 100 Mod 7~>. I ?~.b 

6 SiBt11 Gel •JOOg Mod 'tu . 9 9.59.2. 

this tmplnaer opdnntt J*f' Method 26A 

Sample Log 

SampleiO Num~er Sam~ D.scriplion Conti- VS2-STK l~-M26A-Acdlmp llNa~&one Adcllmplocor 

Catch & flru4 

I VS2-STK-l M26A-Aiklmp SOOml Albnne lmJ>lncor 

Notcene eatch&FJnse 

., 

~ 

' 

,/ 

Rea>Yered bv .1:>~ 

Sample Recovery OJecklist 

(OnJy If transfer Unt Is u'sed). Disconnect transter line. and rinse thtet times with 01 

water into add ~oatr catch botde. Traosfef'bottle to labof'atory wfth.lmplnecrr 

troln. 

/ Otsa.ssemble sampS. tratn, wipe off ucess watu 1nd welch each impin&er. Re<C)(d 

the final wt:'&hts In tht Motsture Oetermtna:tloa section of this data sheet. 

:::: Jllote a.>dition of tire $1UCa c<l lmplrcer. <:521" spent 

v Pour contents of d-oe 1St. 2nd and 3rd (conainhg add) lmp!na..-s IAto 1ht Aad 

imp<rl&er atch bo<tlo(s). l\lmc lmplns.rs and coonectioo glassware wrtll dolonllod 

WJ"ttr into the Mme bO't:t»(s,. CofTiplete add ilnpinge:t sample label. 

./ Poor tl>!! cont•nts of the 4th and Stl> lmpingers (corotalning NaOH) Into the allcaAne 

impinge:r catch bott1e(s). Rinse lmpMc,m il\d coonecting glauwar~ wtth cSelonlled 

water into the nme bottle(.s). Complete alkalfhe lmpin&er sample lJbel. 

/ Log satnples Into logbook and store approp lat~fv. 

Notes: 

IU>S-19: HCVCI,byE1'AM•t/oodZ6A 

Pu-EM SOI'·OZI 

"""'._ D<Jto: J<lfy ZOI3 
t-sa_mp_;le_;Ty.;_pe_- M_ u_tu_Me_tat_;' t_M•-•hod__.: 29J __ -+o-ate...!:!' [/).t.-1 -/_.._'1-- 1 /·- l-11 )"----1 -._____ ------ Poge l of J 

Profect Harne.: v•o~ S-auget, II. COndition: 1 ----- ----......... Samplir\c Trlin leak Aate (d,.."'fll 

Project Number: 4094252530.02 Run: i,_e Noute iD -

SOUrce: Stacl< DGMCf { • .()() 2_ Boromet<r ID /3. P-2 PltOl Tube ID S -/1 

Operator f {) ~ AH@ /. 7 'I{) Bar. P~n. l"'ll :Z &(, 7<{ 

Pilot Tube Ltak Check 

tnld•t r•loe.>3 Hoce?>J 

.. ..., c-1 o~:>"3 -l~ > 3 

P om . t a kn DGM"·ad~- •• &U I--:--:---1~-:--.,. T•_;mpora.:..•" "' ;-:f"'l..,--::-:--cr---=-:=--i V""Um <>< me ~ . ,. ~ r>to<>l ~ t"H,OI - (ft~ Stod< Probe Alltr Imp £1<\ DGM In 1"'11 

1005 ltf-3.0 ~ ttf 1.2 317 ?tC 7U '1-5 69 J.O 

V l.f lo o 4 I !ft. I 0 17 I. 5 ~ 'XCf liu. Jr:.q- tr-~ 13 't.IJ 

!o :zt, t<;U CJ11 ~ 1.&12 'Z5c; ;nr> lf-9: 7Z 'f.C 

VI //'J 35 1//. "2.1 ~ 17 I > "l.-.2.. :ZS-7 2?1 /:f.., 7'+ if.( 

I J')tJ ' -,', • t ? I '1 I. 2. "'1 7 3 '"Z ~ lf < ( 7 'H 7 3 "\ 

.ss 11"!> ~ /"to.3 n .t, '·" n ;z<;J ~ '+1 79. tf.~ 

"' ..... 

tJ. IO ~"3.' O.l't 1. 2 '3~, -:z._'fi ~tt 5o <To .5 

50$·07 Mct•ls by EI'A MerMd 29 

l'u-EM SQ-017' 

ll~ Julyl()/:1 

VES013899