n- 1

Form Approved . O.M.B. No . 2070-0012 . Approval Expires 10-31-96 .

U. S. ENVIRONMENTAL PROTECTION AGENCY AGENCY USE ONLY

Date of receip t

&EPA PREMANUFACTURE

N~GNTi~I N S 0

FOR NEW CHEMICAL SUBST~1f~Sk

~When

form to is

5 0 0 0 0 0 9 7 S DMPANY SANITIZED

Enter the total

P, 52

Document control number EPA case number

in the Premanufacture Notice :JG

GENERAL INSTRUCTIONS Ts-L9_11 3 114 U T 11 2

You must provide all information requested in this form to the extent that it is known to or reasonably asce rtainable by you . Make reasonable estimates if you do not have actual data.

Before you complete this form, you should read the "Instructions Manual for Premanufacture Notification" (the Instructions Manual is available from the Toxic Substances Control Act (TSCA) Information Service by calling 202-554-1404, or faxing 202-554-5603) .

. If a user fee has been remi tt ed for this notice (40 CFR 700 .45), indicate in the boxes above the TS-user fee identification number you hav,~generated .

Remember, your user fee ID number must also appear on your corresponding fee remi tt ance, which is sent to: EPA, HQ Accounting O^d~tions Branch (PNI-266), P .O . 360399M, Pi ttsburgh, PA 15251-6399, Attn. TSCA User Fee .

Part I -- GENERAL INFORMATION TEST DATA AND OTHER DATA

You must provide the currently correct Chemical Abstracts (CA) Name of the You are required to submit all test data in your possession or control

new chemical substance, even if you claim the identity as confidential . You may and to provide a description of all other data known to or reasonably

authorize another person to submit chemical identi ty information for you, but asce rtainable by you, if these data are related to the health an d

your submission will not be complete and the review will not begin until EPA environmental effects of the manufacture, processing, distribution

receives this information. A le tt er in suppo rt of your submission should reference in commerce, use, or disposal of the new chemical substance . Standard your TS user fee identification number. You must submit an original and two literature citations may be submi tted for data in the open scientific copies of this notice including all test data . If you claimed any information as literature . Complete test data ( wri tt en in En alish) not summ a ries of data, confidential, a single sanitized copy must also be submitt ed. must he submi tted if they do not appear in the open literature. You shoul d

clearly identify whether test data is on the substance or on an analog . Also,

Part II -- HUMAN EXPOSURE AND ENVIRONMENTAL RELEASE the chemical composition of the tested material should be characterized .

Following are examples of test data and other data. Data should b e

If there are several manufacture, processing, or use operations to be desc ribed in submitted according to the requirements of §720.50 of the Premanufacture

Part II, sections A and B of this notice, reproduce the sections as needed . Notification Rule (40 CFR Part 720).

Part III -- LIST OF ATTACHMENTS

Test Data (Check Below any included in this notice)

A ttach additional sheets if there is not enough space to answer a question fully .

Label each continuation sheet with the corresponding sec ti on heading . In Part • Environmental fate data Yes • Other data Yes III, list these a ttachments, any test data or other data and any optiona l

information included in the notice

. Health effectsdata F-1 Yes Risk assessments

OPTIONAL INFORMATION • Environmental effects data Yes Structure/activity relationships

You may include any information that you want EP4 to consider in evaluating Physical/Chemical Prope

the new substance rties Yes Test data not in the possession . On page 11 of this form, space has been provided for you to or control of the submitter

describe pollution prevention and recycling information you may have regardin g

the new substance. A physical and chemical p ro pe rt ies worksheet is located on the last page

of this form.

So-called "binding" boxes are included throughout this form for you to indicat e

your willingness to be bound to certain statements you make in this notice, such TYPE OF NOTICE (Check Only One)

as use, production volume, protective equipment . . . This option is intended to

reduce delays that routinely accompany the development of consent orders or ® PMN (Premanufacture Notice) Significant New Use Rules. Except in the case of exemption applications (such as

TMEA, LVE, LOREX) where certain information provided in such notification is

binding on the submi tter when the Agency approves the exemption application, El INTERMEDIATE PMN (submi tted in sequence with final product

checking a binding box in this notice does not by itself prohibit the submi tter PMN)

from later deviating from the information ( except chemical identi ty ) repo rt ed in SNUN (Significant New Use Notice)

the form .

TMEA (Test Marketing Exemption Application)

CONFIDENTIALITY CLAIMS LVE

(Low Volume Exemption) Ca 40 CFR 723.50 (c)(1) You may claim any information in this notice as confidential. To assert a clai m

on the form, mark (X) the confidential box next to the information that you claim LOREX (Low Release/Low Exposure Exemption) @ 723 .50(c)(2) as confidential . To assert a claim in an attachment, circle or bracket th e

information you claim as confidential

confidential , you must also provide a sanitized version of the

. If you claim information in the notice as ❑ LVE Modification LOREX Modification notice, (includin g

attachments). For additional instructions on claiming information as

confidential, read the Instructions Manual

. IS THIS A CONSOLIDATED PMN? F-] Yes

® x of chemicals

Mark (X) if any information in this notice is claimed as confidential . ( Prenotice Communication tt required, enter C on page 3 )

EPA FORM 7710-25 (Rev

. 5-95) Replaces previous editions of EPA Form 7710-25 .

~77~~~
p. 2

Form Approved. O.M.B . No . 2070-0012 . Approval Expires 10-31-96.

U. S. ENVIRONMENTAL PROTECTION AGENCY AGENCY USE ONLY

Date of receip t

~

E PA

PREMANUFACTURE

NOTICE t

C '; ~.iafr ~ ( (.i

FOR NEW CHEMICAL SUBSTANC^FC

~•y , . , ~

~ ".,,0 }ry

~! Ip,'3.rcv 67 ; p

4

L___ . _ . .,, .~,•u~ ..uii~vci t~i Ya~e~ ~/ e t A s r

in the Premanufacture Notice

GENERAL INSTRUCTIONS TS 9 3 4 U T 2

You must provide all information requested in this form to the extent that it is known to or reasonably ascertainable by you . Make reasonable estimates if you do

not have actual data.

• Before you complete this form, you should read the "Inst ru ctions Manual for Premanufacture Notifica tion" (the Instructions Manual is available from the Toxic

Substances Control Act (TSCA) Information Se rvice by calling 202-554-1404, or faxing 202-554-5603).

• If a user fee has been remi

tt

ed for this notice (40 CFR 700 .45), indicate in the boxes above the TS-user fee identification number you have generated .

Remember, your user fee ID number must also appear on your corresponding fee remi ttance, which is sent to : EPA, HQ Accounting Operations Branch (PM-266),

P .O. 360399M, Pittsburgh, PA 15251-6399, Attn . TSCA User Fee . :

r

`

>

Part I -- GENERAL INFORMATION TEST DATA AND OTHER DATA

You must provide the currently correct Chemical Abstracts ( CA) Name of the You are required to submit all test data in your possession or control

new chemical substance, even if you claim the identity as confidential . You may and to p rovide a description of all other data known to or reasonably

authorize another person to submit chemical identi ty information for you, but ascertainable by you, if these data are related to the health an d

your submission will not be complete and the review will not begin until EPA environmental effects of the manufacture, processing, distri bution

receives this information. A le tt er in suppo rt of your submission should reference in commerce, use, or disposal of the new chemical substance . Standard

your TS user fee identification number. You must submit an o ri ginal and two literature cita tions may be submitted for data in the open scientific

copies of this notice including all test data . If you claimed any information as literature . Complete test data (written in English), not summa ri es of data

confidential, a single sanitized copy must also be submi tted. must be submi tted ifthey do not appear in the open literature. You should

clearly identify whether test data is on the substance or on an analog. Also,

Pa rt II -- HUMAN EXPOSURE AND ENVIRONMENTAL RELEASE the chemical composi ti on of the tested material should be characterized.

Following are examples of test data and other data . Data should be

If there are several manufacture, processing, or use operations to be desc ribed in submi tted according to the requirements of §720 .50 of the Premanufacture

Part II, sections A and B of this notice, rep roduce the sections as needed . Notification Rule (40 CFR Part 720) .

Part III -- LIST OF ATTACHMENTS

Test Data (Check Below any included in this notice)

Attach additional sheets if there is not enough space to answer a question fully.

Label each continuation sheet with the corresponding section heading . In Pa rt •Environmental fate data Yes • Other data ~ Yes

III, list these attachments, any test data or other data and any optiona l

information included in the notice . Health effects data Yes Risk assessment s

OPTIONAL INFORMATION Environmental effects data Yes Structure/activity relationships

You may include any information that you want EPA to consider in evaluating Physical/Chemical P

roperties "® Yes Test data not in the possession the new substance . On page 11 of this form, space has been p rovided for you to or control of the submitter describe pollution prevention and recycling informa tion you may have regarding

the new substance . *A physical and chemical properties worksheet is located on the last page

of this form.

So-called "binding" boxes are included throughout this form for you to indicat e

your willingness to be bound to ce rtain statements you make in this notice, such TYPE OF NOTICE (Check Only One)

as use, production volume, protective equipment . . . This option is intended to

reduce delays that routinely accompany the development of consent orders or PMN ( Premanufacture Notice) Significant New Use Rules. Except in the case of exemption applications (such a s

TMEA, LVE, LOREX) where certain information provided in such notification is

with final

p

binding on the submi tt er when the Agency approves the exemption application, INTERMEDIATE PMN (submitted in sequenc roduct

checking a binding box in this notice does not by itself p ) e PMN rohibit the submitter

from later deviating from the information ( except chemical identity ) repo rted in

F-]

SNUN (Significant New Use Notice)

Z:- the form.

TMEA (Test Marketing Exemption Application

) CONFIDENTIALITY CLAIMS LVE (Low Volume Exemption) @ 40 CFR 723.50 (c)(1) r\3 -' !-''

You may claim any information in this notice as confidential. To assert a claim ❑ C .~ {~' l

on the form, mark (X) the confidential box next to the information that you claim LOREX (Low Release/Low Exposure Exemption) 0 723.50(c)(2)

as confidential. To asse rt a claim in an attachment, circle or bracket the f• .

information you claim as confidential. If you claim information in the notice as LVE Modification LOREX Modificatio n confidential, you must also provide a sanitized version of the notice, (including

attachments). For additional inst ru ctions on claiming information as ••

confidential, read the Instru ctions Manual . IS THISA CONSOLIDATED PMN? F-] Yes C7)CCl.9

® At of chemicals

Mark ( X) if any information in this notice is claimed as confidential . ( Prenotice Communication !t required, enter # on page 3 )

EPA FORM 7710-25 (Rev. 5-95) 1 d Replaces previous editions of EPA Form 7710-25.

I/v~
3

Public reporting burden for this collection of information is estimated to average 110 hours per response, including time for reviewing instructions,

searching existing data sources, gathering and maintaining the data needed, and completing and reviewing the collection of information . Send

comments regarding the burden estimate or any other aspect of this collection of information, including suggestions for reducing this burden ,

to Chief, Information Policy Branch, PM-223, U .S . Environmental Protection Agency, 401 M. St., S.W.,, Washington, D.C. 20460; and to the Office of

Management and Budget, Paperwork Reduction Act (2070-0012), Washington, D .C. 20503.

CERTIFICATION

I certify that to the best of my knowledge and belief:

1 . The company named in Part I, section A, subsection la of this notice form intends to manufacture or import for a

commercial purpose, other than in small quantities solely for research and development, the substance identified in

Part I, Section B.

2 . All information provided in this notice is complete and truthful as of the date of submission .

3 . I am submitting with this notice all test data in my possession or control and a description of all other data known to

or reasonably ascertainable by me as required by §720 .50 of the Premanufacture Notification Rule .

Additional Certification Statements:

If you are submitting a PMN, Intermediate PMN, Consolidated PMN, or SNUN, check the following user fee certification

statement that applies:

The Company named in Part I, Section A has remitted the fee of $2500 specified in 40 CFR 700 .45 (b), or

The Company named in Part I, Section A has remitted the fee of $1000 for an Intermediate PMN (defined @ 40 CFR 700 .43) in

accordance with 40 CFR 700 .45(b), or

The Company named in Part I, Section A is a small business concern under 40 CFR 700 .43 and has remitted

a fee of $100 in accordance with 40 CFR 700.45(b).

If you are submitting a low volume exemp tion (LVE) application in accordance with 40 CFR 723 .50 (c) (1) or a Low

release and low exposure exemption (LoREX) application in accordance with 40 CFR 723 .50 (c) (2), check the following

certification statements:

F-] The manufacturer submitting this notice intends to manufacture or import the new chemical substance for

commercial purposes, other than in small quantities solely for research and development, under the terms

of 40 CFR 723 .50 .

The manufacturer is familiar with the terms of this section and will comply with those terms ; and

The new chemical substance for which the notice is submitted meets all applicable exemption conditions.

If this application is for an LVE in accordance with 40 CFR 723 .50 (c)(1), the manufacturer intends to commence

manufacture of the exempted substance for commercial purposes within 1 year of the date of the expiration of the

30 day review period .

The accuracy of the statements you make in this notice should reflect your best prediction of the anticipated facts regarding the chemical

substance described herein . Any knowing and willful misinterpretation is subject to criminal penalty pursuant to 18 USC 1001 . Confidential

Signature and title of Authorized Official (Original Signature Required) Date

Manager, Regulatoi~ Affairs

Signature of agent - (ifapplicable) Date

FORM EPA 7710-25 (Rev. 5-95) Page 2
p. 4

Part I -- GENERAL INFORMATIO N

Section A -- SUBMITTER IDENTIFICATION Confidential

Mark (X) the "Confidential" box next to any subsection you claim as confidential.

Name of authorized official Position

Ia . Person

sutimitting Teresa Borzcik Manager, Regulatory Affairs

Notice Company

(in U.S .) 3M

Mailing address (number and street)

3M Center Building 236-1 B-10

City, State, ZIP Code

St.Paul, MN 55144-1000

.: :

. . . . . . . . . .. .:: •::

.; . . .. . . . . . . . . . .:: •::

. . :

.:::::. ;; ::.;•::::. ~.: ::•;:

.: •.;::

.::.;;.;• .; ;:. ~:::.:::

.;•:: : :,•>:>:o>:>~•~>•::•:;;:;:;:;

. . . . ;. . . . .. . . . . . . .

b. Agent (if Position Name of authorized officia l

applicable)

Company

Mailing address (number and street )

City, State, ZIP Code Area Code Number

Telephone

c . If you are submitting this notice as part of a joint submission, mark (X) this box. ❑

Joint Name of authorized official Position

Submitter

(if applicable)

Company

Mailing address (number and street )

City, State, ZIP Code Area Code Number

Telephone

2 . Technical Name Position

Contact Jay Schulz Regulatory Affairs Specialist (in U.S.) Company

3M

Mailing address (number and street)

3M Center Building 236-1 B-1 0

City, State, ZIP Code Area Code Number

Telephone

St. Paul, MN 55144-1000 651 733-546

3

3. If you have had a prenotice communication (PC) concerning this notice PC-433

and EPA assigned a PC Number to the notice, enter the number. Mark (X) -~y 8 ❑

4. If you previously submitted an exemption application for the chemica

--~ if none X

l

substance covered by this notice, enter the exemption number assigned

by EPA

PMN number assigned by EPA (i

. If you previously submitted a PMN for this substance enter the Mark (X) ~~~

.e . withdrawn or incomplete)

❑

. if none

5 . If you have submitted a notice of Bona fide intent to manufacture or

import for the chemical substance covered by this notice, enter the Mark (X) ❑

notice number assigned by EPA . if none

~--►

1 6 . Type of Notice -- Mark (X) Manufacture 2. Import

Only Only

3 . ❑ Both

❑ Binding Option ❑ Binding Option

Mark (x) Mark (x)

FORM EPA 7710-25 (Rev. 5-95) Page 3
p- 5

Part I -- GENERAL INFORMATION -- Continue d

, Section B -- CHEMICAL IDENTITY INFORMATION : You must provide a currently correct Chemical Abstracts (CA) name of the substance

based on the ninth Collective Index (9CI) of CA nomenclature rules and conventions.

Mark (X) the "Confidential" box next to any item you claim as confidential .

Complete either item 1 (Class 1 or 2 substances) or 2 (Polymers) as appropriate . Complete all other items.

If another person will submit chemical identity information for you (for either item 1 or 2), mark (X) the box at the right

. ❑ ConfiIdentify the name, company, and address of that person in a continuation sheet . dential

1 . Class 1 or 2 chemical substances (for definitions of class I and class 2 substances, see the Instructions Manual )

a . Class of substance -- Mark (X) 1

1 Class 1 or 2 l Class 2 X

b . Chemical name (Currently correct Chemical Abstracts (CA) Name that is consistent with TSCA Inventory listings for similar substances.

For Class 1 substances a CA Index Name must be provided . For Class 2 substances either a CA Index Name or CA Preferred Name must

be provided, whichever is appropriate based on CA 9CI nomenclature rules and conventions .).

Cobalt lithium manganese nickel oxide

c . Please identify which method you used to develop or obtain the specified chemical identity information reported in this notice :

(check one).

F ]Method 2 (Other Source) Method 1 (CAS Inventory Expert Service - a copy of the Identification

report obtained from the CAS Inventory Expert Service must be

submitted as an attachment to this notice)

. . .. . . . . . . . . . .

d . Molecular formula and CAS Registry Number (if a number already exists for the substance)

X

CASA

X

e. For a class 1 substance, provide a complete and correct chemical structure diagram. For a class 2 substance -- (1) List the immediate

precursor substances with their respective CAS Registry Numbers . (2) Describe the nature of the reaction or process. (3) Indicate the X

range of composition and the typical composition (where appropriate) . (4) Provide a correct representative or partial chemica l

structure diagram, as complete as can be known, if one can be reasonably ascertained .

Mark (X) this box if you attach a continuation sheet.

FORM EPA 7710-25 (Rev. 5-95) Page 4
p. 6

Part I -- GENERAL INFORMATION -- Continue d

10- Section B -- CHEMICAL IDENTITY INFORMATION -- Continue d

2. Polymers (For a definition of polymer, see the Instructions Manual.) Confiential

a . Indicate the number-average weight of the lowest molecular weight composition of the polymer you intend to manufacture .

d

Indicate maximum weight percent of low molecular weight species (not including residual monomers, reactants, or solvents) below

500 and below 1,000 absolute molecular weight of that composition .

Describe the methods of measurement or the basis for your GPC [:] Other :(Specify)

i) lowest number average molecula r

ii) maximum weight % below 500 molecular weight :

iii) maximum weight % below 1000 molecular weight :

Mark (X) this box if you attach a continuation sheet.

b . You must make separate confidentiality claims for monomer or other reactant identity, composition information, and residual information.

Mark (X) the "Confidential" box next to any item you claim as confidential.

(1) -- Provide the specific chemical name and CAS Registry Number (if a number exists) of each monomer or other reactant used in the

manufacture of the polymer.

(2) -- Mark (X) this column if entry in column (1) is confidential .

(3) -- Indicate the typical weight percent of each monomer or other reactant in the polymer.

(4) -- Mark (X) the identity column if you want a monomer or other reactant used at two weight percent or less to be listed as part of the

polymer description on the TSCA Chemical Substance Inventory .

(5) -- Mark (X) this column if entries in columns (3) and (4) are confidential .

(6) -- Indicate the maximum weight percent of each monomer or other reactant that may be present as a residual in the polymer as

manufactured for commercial purposes.

(7) -- Mark (X) this column if entry in column (6) is confidential .

Monomer or other reactant and CAS Registry Number Confi- Typical Identity Confi- Maximum Confidential composition Mark (X) dential residual dential

(2) (3) (4) (5) (6) (7)

% %

% %

% %

Mark (X) this box if you attach a continuation sheet.

C . Please identify which method you used to develop or obtain the specified chemical identity information reported in this notice (Check one) .

F-1 Method 1(CAS Inventory Expert Service - a copy of the identification report Method 2 (other source )

obtained from CAS Inventory Expert Service must be submitted as

an attachment to this notice )

d . The currently correct Chemical Abstracts (CA) name for the polymer that is consistent with TSCA Inventory listings for similar polymers .

e . Provide a correct representative or partial chemical structure diagram, as complete as can be known, if one can be reasonably ascertained.

F] Mark (X) this box if you attach a continuation sheet.

FORM EPA 7710-25 (Rev . 5-95) Page 5
7

Part I -- GENERAL INFORMATION -- Continued

, Section B -- CHEMICAL IDENTITY INFORMATION -- Continued

3. Impurities

(a) -- Identify each impuri ty that may be reasonably anticipated to be present in the chemical substance as manufactured for commercial purposes .

Provide the CAS Registry Number if available. If there are unidentified impurities, enter " unidentified ."

(b) -- Estimate the maximum weight % of each impuri ty . If there a re unidentified impurities, estimate their total weight % .

Impurity and CAS Regist ryNumber Maximum Confi-

(a) percent dential

(b)

o/ X°

o/ X°

% X

o/ X0

o/ X0

%

%

Mark (X) this box if you attach a continuation sheet .

4. Synonyms -- Enter any chemical synonyms for the new chemical substance identified in subsection 1 or 2. Confidenti al

X

F1 Mark (X) this box if you attach a continuation sheet.

5. Trade identification -- List trade names for the new chemical substance identified in subsection 1 or 2 .

X

Mark (X) this box if you attach a continuation sheet.

6. Generi c chemical name --If you claim chemical identity as confidential, you must provide a generic chemical name for your substance

that reveals the specific chemical identi ty of the new chemical substance to the maximum extent possible .

Refer to the TSCA Chemical Substance Inventory, 1985 Edition, Appendix B for guidance on developing

generic names.

Mixed metal oxide

1:1 Mark (X) this box if you attach a continuation sheet.

7. By-products - - Describe any by-products resulting from the manufacture, processing, use, or disposal of the new chemical substance . Provide the CAS

Registry Number if available.

By-product CAS Registry Number Confi-

(1) (2) dential

Not applicable -impo rt only

~ Mark (X) this box if you attach a continuation sheet .

FORM EPA 7710-25 ( Rev. 5-95) Page 6
Part I -- GENERAL INFORMATION -- Continued

, Section C -- PRODUCTION, IMPORT, AND USE INFORMATION :

Mark (X) the "Confidential" box next to any item you claim as confidential .

1 . Production volume -- Estimate the maximum production volume during the first 12 months of produc tion. Also estimate the

maximum production volume for any consecutive 12-month period during the first three years of production . Estimates should be on

100% new chemical substance basis. For a Low Volume Exemption application, if you choose to have your notice reviewed at a lower

production volume than 10,000 kg/yr, specify the volume and mark (x) in the binding box . If granted, you are bound to this volume. .

Maximum first 12-month production (kg/yr) Maximum 12-month production (kg/yr) Confi- Binding

(100% new chemical substance basis) (100% new chemical substance basis) dential option

Mark (x)

x

2. Use Information -- You must make separate confidentiality claims for the description of the category of use, the percent of production volume

devoted to each category, the formulation of the new substance, and other use information . Mark (X) the "Confidential" Box next to any item you

claim as confidential.

a. (1) -- Describe each intended category of use of the new chemical substance by function and application .

(2) -- Mark (X) this column if entry in column ( 1) is confidential business information (CBI) .

(3) -- Indicate your willingness to have the information provided in column ( 1) binding.

(4) --Estimate the percent of total production for the first three years devoted to each catego ry of use .

(5) --Mark (X) this column if entry in column ( 4) is confidential business information (CBI) .

(6) -- Estimate the percent of the new substance as formulated in mixtures, suspensions, emulsions, solutions, or gels

as manufactured for commercial purposes at sites under your control associated with each catego ry of use .

( 7) --Mark (X) this column if entry in column ( 6) is confidential business information (CBI) .

(8) -- Indicate % of product volume expected for the listed "use" sectors . Mark more than one box if appropriate . Mark

( X) to indicate your willingness to have the use type provided in (8) binding .

( 9) --Mark (X) this column if entry(ies) in column (8) is (are) confidential business information (CBI).

Category of use (

1) CBI Binding

Produc- CBI

% in CBI % of substance expected per use CB

Option I

(by function and application i .e . a dispersive dye for Mark (x) tion % Form- (8

)

ulation Site- Con-* Indus- Com- indin finishing polyester fibers) (2) (3) (4) (5) (

6) (7) limite sumer trial mercial Option (9)

battery cathode material 100 0/ 100 % 100

o/ Q/

% o/

% %

% o/

o~ o/

*If you have identified a "consumer" use, please provide on a continuation sheet a detailed description of the use(s) of this chemical

substance in consumer products. In addition include estimates of the concentration of the new chemical substance as expected in

consumer products and describe the chemical reactions by which this substance loses its identity in the consumer product .

D Mark (X) this box if you attach a continuation sheet .

b

. Generic If you claim any category of use description in subsection 2a as confidential, enter a generic description of

use that

description

1:1 Mark (X) this box if you attach a continuation sheet.

I Hazard Information -- Include in the notice a copy of reasonable facsimile of any haz ard warning statement, label, material safety data sheet, B inding

or other information which will be provided to an y person who is reasonably likely to be exposed to this subst an ce regarding protective Option

equipment or practices for the safe h an dling, tran sport, use, or disposal of the new substan ce . List in part III hazard information you include

. Mark (x)

Mark (X) this box if you attach hazard information.

FORM EPA 7710-25 (Rev . 5-95) Page 7
P. 9

Part II -- HUMAN EXPOSURE AND ENVIRONMENTAL RELEASE

, Section A -- INDUSTRIAL SITES CONTROLLED BY THE SUBMITTER Mark (X) the "Confidential" box next to any item you claim as confidential.

Complete section A for each typ e of manufacture, processing, or use operation involving the new chemical substance at industrial sites you control .

Importers do not have to complete this section for operations outside the U.S. ; however, you may still have reporting requirements if there are

further industrial processing or use operations after import. You must describe these operations. See instructions manual .

1 . Operation description Confia . Identity -- Enter the identity of the site at which the operation will dential

Nam e

Site address (number and street)

City, County, State, ZIP Code

If the same operation will occur at more than one site, enter the number of sites. Identify the it of sites

additional sites on a continuation sheet, and if any of the sites have significantly differen t

production rates or operations, include all the information requested in this section for those

sites as attachments.

. . . .. . . . . . . . . . . .. . . . .. . . . . . . . . . . . ..

❑ Mark (X) this box if you attach a continuation sheet.

b . Type -- ❑ Manufacturing ❑ Processing ❑ Use

Mark (X)

c . Amount and Duration -- Complete 1 or 2 as appropriat e

Maximum kg/batch (too% new chemical substance) Hours/batch Batches/year

1 . Batch

Maximum kg/day (100% new chemical substance) Hours/day Days/year

2 . Continuou s

d . Process description ❑ Mark (X) to indicate your willingness to have your process desc rip ti on binding.

(1) Diagram the major unit operation steps and chemical conversions . Include interim storage and transport containers (specify-e .g . 5 gallon pails, 55

gallon drum, rail car, tank truck, etc .).

(2) Provide the identity, the approximate weight (by kg/day or kg/batch on an 100% new chemical substance basis), and entry point of all starting

materials and feedstocks (including reactants, solvents, and catalysts, etc .), and of all products, recycle streams, and wastes . Include cleaning

chemicals (note frequency if not used daily or per batch .).

(3) Identify by number the points of release, including small or intermittent releases, to the environment of the new chemical substance .

The PMN substance is imported and shipped directly to a contract manufacturer for relabelling and distribution (see

page 10). No manufacturing or processing occurs at a site controlled by 3M, therefore both pages 8 and 9 are not

applicable.

❑ Mark (X) this box if you attach a continuation sheet.

FORM EPA 7710-25 (Rev. 5-95) Page 8
10

Part II -- HUMAN EXPOSURE AND ENVIRONMENTAL RELEASE -- Continued

Section A -- INDUSTRIAL SITES CONTROLLED BY THE SUBMITTER -- Continued

2. Occupational Exposure -- You must make separate confidentiality claims for the description of worker activity, physical form of the new chemical

substance, number of workers exposed, and duration of activity . Mark (X) the "Confidential" box next to any item you claim as confidential.

(1) --Describe the activities (e .g. bag dumping, tote filling, unloading drums, sampling, cleaning, etc.) in which workers may be exposed to the

substahce .

(2) - Mark (X) this column if entry in column (1) is confidential business information (CBI).

(3) -- Describe any protective equipment and engineering controls used to protect workers .

(4) and (6) -- Indicate you willingness to have the information provided in column (3) or (5) binding .

(5) -- Indicate the physical form(s) of the new chemical substance (e .g . solid : crystal, granule, powder, or dust) and 'G new chemical substance (if part of

a mixture) at the time of exposure .

(7) -- Mark (X) this column if entry in column (5) is confidential business information (CBI) .

(8) -- Estimate the maximum number of workers involved in each activity for all sites combined .

(9) -- Mark (X) this column if entry in column (8) is confidential business information (CBI) .

(10) and (11) -- Estimate the maximum duration of the activity for any worker in hours per day and days per year.

(12) --Mark (X) this column if entries in columns (10) and (11) are confidential business information (CBI) .

Worker activity CBI Protective Equipment/ Binding Physlcal fo Binding CBI # of CBI Maximum duration CBI

p (e .g . bag dumping, filling drums) Engineering Controls Option (e. solid: owder) Optio

an% ne Worker n s

Mark (x substance Mark (x) Hrs/day Days/yr Ex osed

(I) 2 (3) (4) (5) 6 7 8 9 (10) (11) 12

No manufacturing or

processing at a 3M site

E__T_

❑ Mark (X) this box if you attach a continuation sheet.

3 . Environmental Release and Disposal -- You must make separate confidentiality claims for the release number and the amount of the new chemical

substance released and other release and disposal information . Mark (X) the "Confidential" box next to each item you claim as confidential

.

(1) -- Enter the number of each release point identified in the process description, part II, section A, subsection ld(3)

.

(2) -- Estimate the amount of the new substance released (a) directly to the environment or (b) into control technology (in kg/day or kg/batch)

.

(3) -- Mark (X) this column if entries in columns (1) and (2) are confidential business information (CBI)

.

(4) --Identify the media of release i.e . stack air, fugitive air (optional-see Instruction Manual), surface water, on-site or off-site land or incineration,

POTW, or other (please specify) to which the new substance will be released from that release point

.

(5) -- a . Describe control technology, if any, and control efficiency that will be used to limit the release of the new substance to the environment

.

For releases disposed of on land, characterize the disposal method and state whether it is approved for disposal of RCRA hazardous waste .

On a continuation sheet, for each site describe any additional disposal methods that will be used and whether the waste is subject to

secondary or tertiary on-site treatment. b. Estimate the amount released to the environment after control technology (in kg/day ; .

(6) -- Mark (X) this column if entries in columns (4) and (5) are confidential business information (CBI) .

(7) -- Identify the destination(s) of releases to water. Please supply NPDES (National Pollutant Discharge Elimination System) numbers for direct

dischargers or NPDES numbers of the POTW (Publicly Owned Treatment Works) . Mark (X) if the POTW name or NPDES # is confidential

business information (CBI).

Release Amount of new substance CBI Media of Control technology and efficiency (you may wish to optionally attach efficiency data) CBI

Number released releas e

(1) (2a) (2b) e

.g . stack air Binding

(3) (4) (5a) Mark (x) (5b) (6)

FTI

(7) Mark (X) the ❑ CBI Navigable Other - Specify rovide NPDES # CBI destination(s) of POTW provide name(s) below : waterway El p

releases to water.

❑ Mark (X) this box if you attach a continuation sheet .

FORM EPA 7710-25 (Rev . 5-95) Page 9
12 .11

Part II -- HUMAN EXPOSURE AND ENVIRONMENTAL RELEASE -- Continued

Section B -- INDUSTRIAL SITES CONTROLLED BY OTHER S

Complete section B for typical processing or use operations involving the new chemical substance at sites you do not control. Importers do not have to

complete this section for operations outside the U.S.; however, you must report any processing or use activities after import . See the Instructions

Manual . Complete a separate section B for each type of processing, or use operation involving the new chemical substance. If the same operation is performe d

at more than one site describe the typical operation common to these sites . Identify additional sites on a continuation sheet .

1 . Operation Descripti on - To claim information in this section as confidential, circle or bracket the specific information that you claim as confidential

.

(1) -- Diagram the major unit operation steps and chemical conversions, including interim storage and tran sport containers (specify- e .g . 5 gallon pails ,

5 5 gallon drums, rail cars, tank trucks, etc) . On the diagram, identify by letter and briefly describe each worker activi ty . (2) -- Provide the identi ty,

the approximate weight (by kg/day or kg/batch, on an 100% new chemical substance b asis), and entry point of all feedstocks ( including reactants,

solvents and catalysts, etc) and of all products, recycle streams, and wastes. Include clean ing chemicals (note frequency if not used daily or per

batch). ( 3) -- Identify by number the points of release, including small or intermittent rele ases, to the environment of the new chemical substance.

(4) Please enter the # of sites ( remember to identify the locations of these sites on a continuation sheet) :

1

- p

if of sites J

C

~

❑ Mark (X) this box if you attach a continuation sheet .

2 . Worker Exposure/Environmental Releas e

(1) From the diagram above, provide the letter for each worker activity . Complete 2-8 for each worker activity described .

( 2) Estimate the number of workers exposed for all sites combined .

( 4) Estimate the typical duration of exposure per worker in (a) hours per day and (b) days per year .

(6) Describe physical form of exposure and % new chemical substance (if in mixture), and any protective equipment and engineering controls used

to protect workers .

( 7) Estimate the percent of the new substance as formulated when packaged or used as a final product .

( 9) From the process diagram above, enter the number of each release point . Complete 9-13 for each release point identified .

(10) Estimate the amount of the new substance released (a) directly to the environment or (b) into control technology to the environment

( in kg/day or kg/batch) .

(12) Describe media of release i .e. stack air, fugitive air ( optional-see Instructions Manual), surface water, on-site or off-site land or incineration,

POTW, or other ( specify) and control technology, if any, that will be used to limit the release of the new substance to the environment

.

( 14) Identify byproducts which may result from the operation .

(3), (5), ( 8), (11), ( 13) and ( 15) - Mark ( X) this column if any of the proceeding entries are confidential business information (CBI) .

Letter # of CBI Duration CBI Protective Equip . / % in CBI Release Amount of CBI Control CBI

of Workers of Engineering Controls/ Form- Number New Technology

Act- Exposed Exposure Physical Form and % ulation Substance

ivity new substance Released

(1) (2) 3 (4a) (4b) 5 (6) (7) g (9) (l0a) (lOb) 13

A X X }{

(14) -- By-products: (15)

❑ Mark (X) this box if you attach a continuation sheet .

FORM EPA 7710-25 (Rev. 5-95) Pagex !~ q

~d
~ r) ANI`~_~.~

PMN Page 10 ;

Part II-- HUMAN EXPOSURE AND ENVIRONM ENTA L RELEASE -- Continued

Section B -- INDUSTRIAL SITES CONTROLLED BY OTHERS

Complete section B for typical processing or use operations involving the new chemical substance at sites you do not control . Importers do not have to complete this section for

operations outside the U .S . however, you must report any processing or use activities after import . See the Instructions Manual. Complete a separate section B for each type of

processing or use operation involving the new chemical substance . If the same operation is performed at more than one site describe the typical operation common to these

sites. Identify additional sites on a continuation sheet.

1(a). Operation Description -- To claim information in this section as confidential, circle or bracket the specific information that you claim as confidential

.

(1) -- Diagram the major unit operation steps and chemical conversions, including interim storage and transport containers (specify - e .g . 5 gallon pails, 55 gallon drums, rail

cars, tank trucks, etc). On the diagram, identify by letter and briefly describe each worker activity . (2) -- Either in the diagram or in the text field 1(b) below, provide the

identity, the approximate weight (by kg/day or kg/batch, on an 100% new chemical substance basis), and entry point of all feedstocks (including reactants, solvents and

catalysts, etc) and all products, recycle streams, and wastes. Include cleaning chemicals (note frequency if not used daily or per batch) . (3) -- Either in the diagram or in the

text field l(b) below, identify by number the points of release, including small or intermittent releases. to the environment of the new chemical substance . (4) Please enter

the # of sites (remember to identify the locations of these sites on a continuation sheet) :

ff of sites C81

I(b). (Optional) This space is for a text description to clarify the diagram above .

Mark (X) this box if you att ach a continuation sheet .

EPA FORiVt 7710-25 (Rev . 5-95) PageX

/O(3
A( ; ~°^,. e " „a ~R AN ~.

PMN Page 10 AI ~ 13

2 . Worker Exposure/Environmental Releas e

( 1) -- From the diagram above, provide the le tter for each worker activity . Complete 2-3 for each worker activity described.

(2) -- Estimate the number of workers exposed for all sites combined .

(4) -- Estimate the typical duration of exposure per worker in (a) hours per day and ( b) days per year.

(6) -- Describe physical form of exposure and % new chemical substance ( if in mixture), and any protective equipment and engineering controls, if any, used to protect

workers.

(7) -- Estimate the percent of the new substance as formulated when packaged or used as a final product .

( 9) -- From the process diagram above, enter the number of each release point . Complete 9-13 for each release point identified .

(10) -- Estimate the amount of the new substance released ( a) directly to the environment or (b) into control technology to the environment (in kg/day or kg/batch)

.

(I2) -- Describe media of release i .e stack air, fugitive air (optional-see Instructions Manual), surface water, on-site or off-site land or incineration, POTW, or other (specify)

and control technology, if any, that will be used to limit the release of the new substance to the environment.

(14) -- Identify byproducts which may result from the operation .

(3), (5), (S), (1 l), (13) and (I 5 ) -- Mark ( X) this column if any of the proceeding entries are confidential business information (CBI)

Letter 4 of CBI Duration of CBI Protective Equip. /Engineering Controls/Physical Form and/ % new substance ~'~ in CBI

Acn- Exposed ulanon

of Workers Exposure Fonnvity

(1) (2) (3 ) (4a) 14b) ( 5

) (6) (7) ($)

See mS_,S X

❑ ❑

❑ ❑ ❑

❑ ❑ ❑

❑

Release ,ainotutt of CBI Media of Release & Control Technology CBI Number New

Substance

Released

(9) (10a) (IOb (IL) ( 12) (

13

)

~ _ ❑

~

❑ ❑

❑

(14) -- Byproducts

❑ ❑

❑ ❑

(15)

® Mark ( X) this box if you att ach a continuation sheet,

OPTIONAL POLLUTION PREVENTION INFORMATION

To claim information in the following section as confidential circle or bracket the specific information that you claim as con fidential.

In this section you may provide information not reported elsewhere in this form regardin g your efforts to reduce or minimize potential risks

associated with activities surrounding manufacturing, processing, use and disposal of the PMN substance . Please include new information

pertinent to pollution prevention, including source reduction, recycling activities and safer processes or products available due to the new

chemical substance . Source reduction includes the reduction in the amount or toxici ty of chemical wastes by technological modi fication,

process and procedure modification, product reformulation, raw materials substitution, and/or invento ry control. Recycling refers to the

reclamation of useful chemical components from wastes that would otherwise be treated or released as air emissions or water discharges, or

land disposal . Descriptions of pollution prevention, source reduction and recycling should emphasize potential risk reduction subsequent to

compliance with existing regulato ry requirements and can be either quantitative or qualitative . The EPA is interested in the information to

assess overall net reductions in toxici ty or environmental releases and exposures, not the shifting of risks to other environmental media or nonenvironmental areas (e .g ., occupational or consumer exposure) . In addition, information on the relative cost or performance characteristics of

the PMN substance to potential alternatives may be provided .

All information provided in this section will be taken into consideration during the review of this substance . See PIVIN Instructions

Nlanual and Pollution Prevention Guidance manu a l for guidance and examples.

EPA FORM 7710-2 5 ( Rev . 5-95) Page X

l~ ~.
14

OPTIONAL POLLUTION PREVENTION INFORMATION

To claim information in this section as confidential circle or bracket the specific information that you claim as confidential .

In this section you may provide information not reported elsewhere in this form regarding your

effo'rts to reduce or minimize potential risks associated with activities surrounding

manufacturing, processing, use and disposal of the PMN substance . Please include new

information pertinent to pollution prevention, including source reduction, recycling activities

and safer processes or products available due to the new chemical substance . Source reduction

includes the reduction in the amount or toxicity of chemical wastes by technological

modification, process and procedure modification, product reformulation, raw materials

substitution, and/or inventory control . Recycling refers to the reclamation of useful chemical

components from wastes that would otherwise be treated or released as air emissions or water

discharges, or land disposal. Descriptions of pollution prevention, source reduction and

recycling should emphasize potential risk reduction subsequent to compliance with existing

regulatory requirements and can be either quantitative or qualitative . The EPA is interested in

this information to assess overall net reductions in toxicity or environmental releases and

exposures, not the shifting of risks to other environmental media or non-environmental areas

(e.g., occupational or consumer exposure) . In addition, information on the relative cost or

performance characteristics of the PMN substance to potential alternatives may be provided .

All information provided in this section will be taken into consideration during the review

of this substance. See the revised Instructions Manual that includes a Pollution Prevention

manual for guidance and examples.

Describe the expected net benefits, such as (1) an overall reduction in risk to human health or the environment; (2) a reduction

in the volume manufactured; (3) a reduction in the generation of waste materials through recycling, source reduction or other

means; (4) a reduction in potential toxicity or human exposure and/or environmental release ; (5) an increase in product

performance, a decrease in the cost of production and/or improved operation efficiency of the new chemical substance in

comparison to existing chemical substances used in similar applications; or (6) the extent to which the new chemical substance

may be a substitute for an existing substance that poses a greater overall risk to human health or the environment

.

C L

® Mark (X) this box if you attach a continuation sheet .

FORM EPA 7710-25 (Rev. 5-95) Page 11

► a
p. 15

C-3 Q

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16

Part III -- LIST OF ATTACHMENTS

Attach continuation sheets for sections of the form and test data and other data (including physical/chemical properties and

structure/activity information), and optional information after this page . Clearly identify the attachment and the section of the form to

which it relates, if appropriate. Number consecutively the pages of the attachments . In the column below, enter the inclusive page

numbers of each attachment .

Mark (X) the "Confidential" box next to any attachment name you claim as confidential. Read the Instructions Manual for

guidance on how to claim any information in an attachment as confidential . You must include with the sanitized copy of the notice

form a sanitized version of any attachment in which you claim information as confidential .

Attachment name Attachment Confipage number(s) dential

Material Safety Data Sheet (MSDS)

13A-13H

Pre-communication notification # PC-4338 14A-14F

Nomenclature Report, Method # I 15A-151

Technical Data Package - 16A-16M

ICP 16C

Morphology -SEM 16D

PSD, Particle size distribution 16E-16G

Density 16H

X-Ray diffraction 161-16M

Physical and Chemical Properties Worksheet 17

1 :1 Mark (X) this box if you attach a continuation sheet. Enter the attachment name and number .

FORM EPA 7710-25 (Rev. 5-95) Page 12

14
p. 17

3M MATERIAL SAFETY DATA SHEET Developmental Material 09/09/2003

Material Safety Data Sheet

Copyright, 2003, 3M Company. All rights reserved. Copying and/or downloading of this information for the purpose of properly

utilizing 3M products is allowed provided that : (1) the information is copied in full with no changes unless prior written agreement is

obtained from 3M, and (2) neither the copy nor the original is resold or otherwise distributed with the intention of earning a profit

thereon .

SECTION 1 : PRODUCT AND COMPANY IDENTIFICATION

PRODUCT NAME:

I j Developmental Material (Expe rimental)

MANUFACTURER: 3M

DIVISION: Performance Materials Division

ADDRESS : 3M Center

St. Paul, MN 55144-100 0

EMERGENCY PHONE : 1-800-364-3577 or (651) 737-6501 (24 hours)

Issue Date: 09/09/2003

Supercedes Date: 09/09/2003

Document Group: C ~

Product Use : Specific Use : Research Sample

SECTION 2 : INGREDIENTS

Ingredient C.A.S. No. % by Wt --

LITIIIUM COBALT MANGANESE NICKEL OXIDE 100

SECTION 3 : HAZARDS IDENTIFICATION

3.1 EMERGENCY OVERVIEW

Specific Physical Form : Powder

Odor, Color, Grade: Black powder

General Physical Form: Solid

Immediate health, physical, and environmental hazards: May cause allergic skin reaction . May cause allergic respiratory reaction . Contains a chemical or chemicals which can cause cancer . May cause target organ effects.

3.2 POTENTIAL HEALTH EFFECTS

Page 1 of 8

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13M MATERIAL SAFETY DATA SHEET , Developmental Material 09/09/200 3

Eye Contact:

Mechanical eye irritation : Signs/symptoms may include pain, redness, tea ring and corneal abrasion.

Skin Contact:

Allergic Skin Reaction (non-photo induced) : Signs/symptoms may include redness, swelling, bliste ring, and itching.

Mechanical Skin irritation: Signs/symptoms may include abrasion, redness, pain, and itching .

Inhalation :

Allergic Respiratory Reaction : Signs/symptoms may include difficulty breathing, wheezing, cough, and tightness of chest.

May be harmful if inhaled.

Upper Respiratory Tract Irritation: Signs/symptoms may include cough, sneezing, nasal discharge, headache, hoarseness, and nose

and throat pain .

Lung Effects : Signs/symptoms may include difficul ty breathing, cough, wheezing, weakness, increased heart rate, bluish colored skin ( cyanosis), sputum production and changes in lung function tests .

Ingestion :

May be harmful if swallowed.

Carcinogenicity :

Contains a chemical or chemicals which can cause cancer .

Ingredient C.A.S. No. ClassDescriptio Regulation

COBALT COMPOUNDS NONE Group 2B International Agency for Research on

Cancer

NICKEL COMPOUNDS (EXCEPT NONE Group

ALLOYS) Cancer

1 International Agency for Research on

NICKEL COMPOUNDS (EXCEPT NONE

ALLOYS) Carcinogens

Known human carcinogen National Toxicology Program

SECTION 4 : FIRST AID MEASURES

4.1 FIRST AID PROCEDURES

Page 2 of 8

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P. 19

3M MATERIAL SAFETY DATA SHEET Developmental Material 09/09/2003

The following first aid recommendations are based on an assumption that appropriate personal and industrial hygiene practices are

followed .

Eye Contact: Flush eyes with large amounts of water. If signs/symptoms persist, get medical attention .

Skin Contact: Remove contaminated clothing and shoes. Immediately flush skin with large amounts of water. Get medical attention . Wash contaminated clothing and clean shoes before reuse.

Inhalation : Remove person to fresh air. If signs/symptoms develop, get medical attention.

If Swallowed : Do not induce vomiting unless instructed to do so by medical personnel . Give victim two glasses of water. Never give anything by mouth to an unconscious person . Get medical attention.

SECTION 5 : FIRE FIGHTING MEASURES

5 .1 FLAMMABLE PROPERTIE S

Autoignition temperature NotApplicable

Flash Point Not Applicable

Flammable Limits - LEL Not Applicable

Flammable Limits - UEL Not Applicable

5.2 EXTINGUISHING MEDIA

Use fire extinguishers with class B extinguishing agents (e .g ., dry chemical, carbon dioxide).

5.3 PROTECTION OF FIRE FIGHTERS

Special Fire Fighting Procedures: Wear full protective clothing, including helmet, self-contained, positive pressure or pressure

demand breathing apparatus, bunker coat and pants, bands around arms, waist and legs, face mask, and protective covering for

exposed areas of the head .

Unusual Fire and Explosion Hazards: Not applicable .

Note: See STABILITY AND REACTIVITY (SECTION 10) for hazardous combustion and thermal decomposition

information.

SECTION 6 : ACCIDENTAL RELEASE MEASURES

Accidental Release Measures: Refer to other sections of this MSDS for information regarding physical and health hazards,

respiratory protection, ventilation, and personal protective equipment . Call 3M-HELPS line (1-800-364-3577) for more information on handling and managing the spill . Evacuate unprotected and untrained personnel from hazard area. The spill should be cleaned up by qualified personnel. Ventilate the area with fresh air. Collect as much of the spilled mate ri al as possible. Use wet sweeping compound or water to avoid dusting . Sweep up. Clean up residue with an appropriate solvent selected by a qualified and authorized

person. Ventilate the area with fresh air. Read and follow safety precautions on the solvent label and MSDS . Collect the resulting residue containing solution . Place in a closed container approved for transportation by appropriate authorities

material as soon as possible . Dispose of collected

.

In the event of a release of this material, the user should determine if the release qualifies as repo rtable according to local, state, and federal regulations.

Page 3 of 8

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p. 20

13M MATERIAL SAFETY DATA SHEET L

Developmental Material 09/09/200 3

SECTION 7: HANDLING AND STORAGE

7.1 HANDLING

For industrial or professional use only. Avoid eye contact with dust or airborne particles. Avoid skin contact. Avoid breathing of

dust. Do not eat, drink or smoke when using this product . Wash exposed areas thoroughly with soap and water . Do not breathe

thermal decomposition products . Use general dilution ventilation and/or local exhaust ventilation to control airbo rne exposures to

below Occupational Exposure Limits. If ventilation is not adequate, use respirato ry protection equipment. Keep away from moisture .

7.2 STORAGE

Store away from areas where product may come into contact with food or pharmaceuticals . Keep container tightly closed . Store away

from heat. Store out of direct sunlight .

SECTION 8: EXPOSURE CONTROLS/PERSONAL PROTECTION

8 .1 ENGINEERING CONTROLS

Use with appropriate local exhaust ventilation. Do not use in a confined area or areas with little or no air movement. Provide

appropriate local exhaust when product is heated .

8.2 PERSONAL PROTECTIVE EQUIPMENT (PPE)

8 .2 .1 Eye/Face Protection

Avoid eye contact.

The following eye protection(s) are recommended: Safety Glasses with side shields.

8.2.2 Skin Protectio n

Avoid skin contact.

Select and use gloves and/or protective clothing to prevent skin contact based on the results of an exposure assessment . Consult with

your glove and/or protective clothing manufacturer for selection of appropriate compatible mate rials.

Gloves made from the following material(s) are recommended : Neoprene, Nitrile Rubber .

8 .2 .3 Respiratory Protectio n

Avoid breathing of dust.

During heating :

Avoid breathing of fumes.

Select one of the following NIOSH approved respirators based on airborne concentration of contaminants and in accordance with

OSHA regulations : Half facepiece or fullface air-pu rifying respirator with N95 particulate filters . Consult the current 3M Respirato ry

Selection Guide for additional information or call 1-800-243-4630 for 3M technical assistance .

8 .2 .4 Prevention of Swallowing

Do not eat, drink or smoke when using this product . Wash exposed areas thoroughly with soap and water .

8.3 EXPOSURE GUIDELINES

Ingredient Authority Type Limit Additional Information

COBALT COMPOUNDS ACGIH TWA - 0.02 mg/m3 as Co; Table A3

specific form

MANGANESE COMPOUNDS OSHA CEIL - 5 mg/m3 as Mn; Table Z- I A

specific form

MANGANESE, INORGANIC COMPOUNDS ACGIH TWA - 0 .2 mg/m3 as Mn

specific form

Page 4 of 8

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13M MATERIAL SAFETY DATA SHEET ~ Developmental Material 09/09/2003

SOURCE OF EXPOSURE LIMIT DATA:

ACGIH: American Conference of Governmental Industrial Hygienists

CMRG: Chemical Manufacturer Recommended Guideline

OSHA : Occupational Safety and Health Administratio n

AIHA: American Industri al Hygiene Association Workplace Environmental Exposure Level (WEEL)

SECTION 9 : PHYSICAL AND CHEMICAL PROPERTIE S

Specific Physical Form : Powder

Odor, Color, Grade: Black powder

General Physical Form: Solid

Autoignition temperature Not Applicable

Flash Point Not Applicable

Flammable Limits - LEL Not Applicable

Flammable Limits - UEL Not Applicable

Boiling point Not Applicable

Density No Data Available

Vapor Density NotApplicable

Vapor Pressure Not Applicable

Specific Gravity No Data Available

pH Not Applicable

Melting point >=1,100 °C

Solubility in Water Negligibl e

SECTION 10: STABILITY AND REACTIVITY

Stability: Stable .

Materials and Conditions to Avoid: None known

Additional Information : Easily oxidisable materials. Protect from moisture .

Hazardous Polymerization : Hazardous polymerization will not occur.

Hazardous Decomposition or By-Products

Substance Condition

Oxides of Cobalt During Combustion

Toxic Vapor, Gas, Particulate During Combustion

Hazardous Decomposition : Thermal dcomposition product may include Lithium Oxides, Manganese/Manganese Oxides and

Nickel/Nickel Oxides.

SECTION 11 : TOXICOLOGICAL INFORMATION

Page 5 of 8

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13M MATERIAL SAFETY DATA SHEET Developmental Material 09/09/200 3

J

Please contact the address listed on the first page of the MSDS for Toxicological Information on this materi al and/or its

components .

SECTION 12 : ECOLOGICAL INFORMATION

ECOTOXICOLOGICAL INFORMATIO N

Not determined.

CHEMICAL FATE INFORMATION

Not determined .

SECTION 13 : DISPOSAL CONSIDERATION S

Waste Disposal Method: Reclaim if feasible. As a disposal alternative, dispose of waste product in a facility permitted to accept

chemical waste .

EPA Hazardous Waste Number (RCRA): Not regulate d

I Since regulations vary, consult app licable regulations or authorities before disposal .

SECTION 14 :TRANSPORT INFORMATION

Please contact the emergency numbers listed on the fi rst page of the MSDS for Transportation Information for this

material.

SECTION 15 : REGULATORY INFORMATION

US FEDERAL REGULATION S

Contact 3M for more information .

Section 313 Toxic Chemicals subject to the reporting requirements of that section and 40 CFR part 372 (EPCRA):

Insredient C.A.S. No % by Wt

LITHIUM COBALT MANGANESE NICKEL 100

OXIDE (COBALT COMPOUNDS )

LITHIUM COBALT MANGANESE NICKEL 100

OXIDE (MANGANESE COMPOUNDS)

Page 6 of 8

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1 3M MATERIAL SAFETY DATA SHEET (~ ~ Developmental Material 09/09/2003

LITHIUM COBALT MANGANESE NICKEL 100

OXIDE (NICKEL COMPOUNDS)

STATE REGULATIONS

Contact 3M for more information .

CALIFORNIA PROPOSITION 6 5

InEredient C.A.S. No. Classification

NICKEL COMPOUNDS NONE **Carcinogen

** WARNING: contains a chemical which can cause cancer .

CHEMICAL INVENTORIES

This material is not listed on the TSCA inventory and should be used for research and development purposes only under the direct

supervision of a technically qualified individual .

Contact 3M for more information.

INTERNATIONAL REGULATIONS

Contact 3M for more information .

This MSDS has been prepared to meet the U .S. OSHA Hazard Communication Standard, 29 CFR 1910 1200

SECTION 16 : OTHER INFORMATION

Revision Changes:

Section 2: Ingredient information was modified.

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3M MATERIAL SAFETY DATA SHEET 7Developmental Material 09/09/200 3

Section 15 : EPCRA 313 information was modifi ed.

DISCLAIMER: The information in this Mate ri al Safety Data Sheet (MSDS) is believed to be correct as of the date issued . 3M

MAKES NO WARRANTIES, EXPRESSED OR IMPLIED, INCLUDING, BUT NOT LIMITED TO, ANY IMPLIED WARRANTY

OF MERCHANTABILITY OR FITNESS FOR A PARTICULAR PURPOSE OR COURSE OF PERFORMANCE OR USAGE OF

TRADE. User is responsible for determining whether the 3M product is fit for a particular purpose and suitable for user's method of

use or application. Given the vari e ty of factors that can affect the use and application of a 3M product, some of which are uniquely

within the user's knowledge and control, it is essential that the user evaluate the 3M product to determine whether it is fit for a

particular purpose and suitable for user's method of use or application .

3M provides information in electronic form as a se rvice to its customers. Due to the remote possibility that electronic tr an sfer may

have resulted in errors, omissions or alterations in this information, 3M makes no representations as to its completeness or accuracy .

In addition, information obtained from a database may not be as current as the information in the MSDS available directly from 3M.

Page 8 of 8

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PHYSICAL AND CHEMICAL PROPERTIES WORKSHEET

To assist EPA's review of physical and chemical properties data, please complete the following worksheet for data you provide and

include it in the notice. Identify the property measured, the page of the notice on which the property appears, the valu e

of the property, the units in which the property is measured as necessary), and whether or not the property is claimed as

confidential . The physical state of the neat substance should be provided . These measured properties should be for the neat (100%

pure) chemical substance. Properties that are measured for mixtures or formulations should be so noted (% PMN substance in _) .You

are not required to submit this worksheet; however, EPA strongly recommends that you do so, as it will simplify review and ensure

that confidential information is properly protected . You should submit this worksheet as a supplement to your submission of test

data.This worksheet is not a substitute for submission of test data .

Measured ConfiProperty Mark (X) if Page Value Estimate dential

provided number Mark (X)

(a) (b) (c) (M or E) (d)

Physical state of neat substance 13E X(s) _(1) _(g) M

Vapor pressur

@ Temperature " C Torr

e

2 .0-2.4(tap)

Density/relative density Tap and Pellet 16H 3 .0-3.5(pellet)

g/cm3 M

Solubilit y

@ Temperature " C

Solvent g/L

Solubility in water @ Temperature C 13E Negligible C E

Melting temperature 13E >1,100 C E

Boiling/sublimation temperature torr pressur e

Spectra ICP, SEM, XRD 16C-M M

Dissociation constant

Particle size distribution 16F-G 0.2 to 60 um M

Octanol/water partition coefficien t

Henry's Law constant

Volitalization from water

Volitalization from soil

pH @ concentration

Flammability

Explodability

Adsorption/coefficient

Other - Specify

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