## Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

-down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

-down boxes to fill in the units of

measure.

## Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

-
5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units of

### EIA

Facility Code Facility Name Boiler ID Fuel Type 1

58048 Wh elan Energy

Center 1 

## Subbituminous

### Fuel Type 2 Fuel Type 3 Other Fuel Description

### EIA Facility Code Facility Name Boiler ID Basis Analyte Analysis Method for each Analyte (example: ASTM D5865-04)


### 58048 Whelan Energy Center 1 As Received Higher Heating Value 

### ASTM D 5373-02 58048 Whelan Energy Center 1 As Received % Moisture 

### ASTM D 5373-02 58048 Whelan Energy Center 1 As Received % Ash 

### ASTM D 5373-02 58048 Whelan Energy Center 1 As Received % Sulfur 

### ASTM D 5373-02 58048 Whelan Energy Center 1 Dry basis Higher Heating Value 

### ASTM D 5373-02 58048 Whelan Energy Center 1 Dry basis % Ash 

### ASTM D 5373-02 58048 Whelan Energy Center 1 Dry basis % Sulfur 

### ASTM D 5373-02 58048 Whelan Energy Center 1 Dry basis Antimony 

### EPA SW-846 Method 3030B 58048 Whelan Energy Center 1 Dry basis Arsenic 

### EPA SW-846 Method 3030B 58048 Whelan Energy Center 1 Dry basis Beryllium 

### EPA SW-846 Method 3030B 58048 Whelan Energy Center 1 Dry basis Cadmium 

### EPA SW-846 Method 3030B 58048 Whelan Energy Center 1 Dry basis Chlorine 

### USGS Bulletin 1823 58048 Whelan Energy Center 1 Dry basis Chromium 

### EPA SW-846 Method 3030B 58048 Whelan Energy Center 1 Dry basis Cobalt 

### EPA SW-846 Method 3030B 58048 Whelan Energy Center 1 Dry basis Fluorine 

### ASTM 3761-96 58048 Whelan Energy Center 1 Dry basis Lead 

### EPA SW-846 Method 3030B 58048 Whelan Energy Center 1 Dry basis Manganese 

### EPA SW-846 Method 3030B 58048 Whelan Energy Center 1 Dry basis Mercury 

### ASTM 6722 58048 Whelan Energy Center 1 Dry basis Nickel 

### EPA SW-846 Method 3030B 58048 Whelan Energy Center 1 Dry basis Selenium 

### EPA SW-846 Method 3030BEIA Facility Code Facility Name Boiler ID 

### HAPs Test Group



### 58048 Whelan Energy Center 1 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher

Heating Value (HHV) (as received) HHV Units % Moisture (as received) % Ash

(as received) % Sulfur

(as received) 

### 1 

### 3/23/2010 3/23/2010 9679.00 Btu/lb 18.86 5.62 0.42 2 3/24/2010 3/24/2010 9632.00 Btu/lb 19.15 5.61 0.43 3 3/25/2010 3/25/2010 9654.00 Btu/lb 19.01 5.69 0.44 4 3/26/2010 3/26/2010 9618.00 Btu/lb 18.84 5.96 0.41 Fuel Testing ResultsHigher

Heating Value (HHV) (Dry Basis) HHV Units % Ash (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) 

### 11929 Btu/lb 6.93 0.52 11913 Btu/lb 6.94 0.53 120 mg/kg 0.075 mg/kg 0.03 mg/kg 4.96 11920 Btu/lb 7.03 0.54 97 mg/kg 0.076 m 0.01 mg/kg 5.24 11851 Btu/lb 7.34 0.51 124 mg/kg 0.072 mg/kg 0 mg/kg 7.01Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units



### mg/kg 0.2 mg/kg 0.09 mg/kg 1.44 mg/kg 2.92 mg/kg 6.15 mg/kg mg/kg 0.23 mg/kg 0.09 mg/kg 1.49 mg/kg 3.03 mg/kg 6.48 mg/kg mg/kg 0 mg/kg 0.1 mg/kg 1.64 mg/kg 3.06 mg/kg 6.68 mg/kgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units



### 1.58 mg/kg 10.42 mg/kg 0.48 mg/kg 1.62 mg/kg 11.49 mg/kg 0.5 mg/kg 0.03 mg/kg 0.48 mg/kg 0.52 mg/kgEIA

Facility Code Facility

Name Boiler ID 

### HAPs Test Group


## 58048 Whelan Energy Center 1

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 

### Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

UnitsMercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis)Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel UnitsSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsEIA

Facility Code Facility

Name Boiler ID 

### HAPs Test Group


## 58048 Whelan Energy Center 1

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

UnitsMercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis)Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel UnitsSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsEIA

Facility Code Facility

Name Boiler ID 

### HAPs Test Group


## 58048 Whelan Energy Center 1

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

UnitsMercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis)Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel UnitsSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units