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NBS MONOGRAPH 34

Tables of Chemical Kinetics

U.S. DEPARTMENT OF COMMERCE

NATIONAL BUREAU OF STANDARDS
Tables of Chemical Kinetics

Homogeneous Reactions

(Supplementary Tables)

These tables are issued in the form of punched loose sheets, temporarily assembled

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Each table is designated by a six-digit number, the first two of which refer to the

type of reaction, the third to the phase of the homogeneous reaction, gaseous (1), liquid

(2), or solid (3). The indication of the phase is repeated at the upper right-hand

corner of the first sheet of each table. The second three-digit group of the table number

refers to the types of substances involved. Within each table, reactions are numbered.

In tables including more than one page, the table number is repeated at the head of

each page, and the pages are numbered. Each table starts on a new sheet. Earlier tables in this series were published as Circulars of the National Bureau of

Standards. The present tables on this subject will appear in the NBS Monograph

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UNITED STATES DEPARTMENT OF COMMERCE • Luther H. Hodges, Secretary

NATIONAL BUREAU OF STANDARDS • A. V. Astin, Director

Tables of Chemical Kinetics

Homogeneous Reactions

(Supplementary Tables)

National Bureau of Standards

A. V. Astin, Director

National Research Council, Division of Chemistry

Committee on Kinetics of Chemical Reactions

M. L. Kilpatrick, Chairman

J. Bigeleisen H. Taube

R. Noyes K. Wiberg

C. Satterfield

Project Office: Hepburn Hall, St. Lawrence University, Canton, Nave York

C. H. Stauffer, Project Director

A. R. Amell D. M. Kern

E. Buncel H. G. Kuivila T. W. Davis P. E. Merritt

J. O. Edwards M. Szwarc H. B. Feldman H. Taube

C. L. Gage M. H. J. Wijnen

H. S. Johnston

National Bureau of Standards Monograph 34

To Accompany National Bureau of Standards C510, Supplements 1 and 2

Issued September 15, 1961
Katronal Bureau of Standards

JUN I 1955

QClOO

r \ } : ^ \

Contents

^ / (Supplementary Tables)

Page

Preface iii

Subject index iv

Tables 1

II
SUPPLEMENT 3 TO TABLES OF

CHEMICAL KINETICS

HOMOGENEOUS REACTIONS

PREFACE

A description of these Tables and definition of the terms and abbreviations used may be

found In the Introduction to the 1951 publication. A brief description of the method used In compiling these tables and the limitation of coverage Is given in the preface to Supplement 1. A description of the numbering system used In classifying reactions for the tables is given In Supplement 2. The present supplement contains information pertaining to Substitution, Exchange

and Elimination reaction types. It is not complete as still more material falling in these groups

Is being prepared. The amount of kinetic data to be studied made it seem advisable to present

all the material completed to date without further delay. The date on each section gives the year

and month to which the literature had been surveyed. Significant omissions or errors should be reported to Dr. Charles H. Stauffer, Head, Department of Chemistry, St. Lawrence university.

Canton, New York.

The Director and his associates gratefully aclmowledge the financial assistance provided by

the Office of Ordnance Research, Department of the Army which made this work possible. The Di- rector of the Project gratefully acknowledges the able assistance of his associates and collaborators, the help of the National Bureau of Standards, the National Academy of Sciences and the members of the Committee on Chemical Kinetics of N. R. C. Division of Chemistry.

C.H. Stauffer

National Bureau of Standards - National Research Council December, 1959

III
Homogeneous Reaction Klnetlbs 1

SUBJECT INDEX

3oo EXCHANGE-SUBSTITUTION

300 ISOTOPIC EXCHANGE

301

302

Title of Tab I

e

(number of pages)

Isotopic exchange (gas)

hydrogen exchange on

Tab I e number

Isotopic exchange;

aliphatic C (2) Isotopic exchange;

Isotopic exchange;

Isotopic exchange;

hallde (1) Isotopic exchange;

Isotopic exchange;

Isotopic exchange;

oxide of carbon (2) halogen on aliphatic C halogen In IVth group

(4)

oxides of nitrogen (l) hydrogen-hydrogen hallde (l) halogen-halogen hallde (3)

Isotopic exchange (liquid)

Isotopic exchange; ammonia (amine) complex

on group I element (l) Isotopic exchange; halogen complex on

group I element (l) Isotopic exchange; valence state group I ions (1) Isotopic exchange;

element (2) Isotopic exchange; Ions (11)

Isotopic exchange;

aliphatic C (12)

Isotopic exchange;

aromatic C (10)

Isotopic exchange;

heterocyclic ring

Isotopic exchange; on carbon (6) Isotopic exchange;

disulfide and thiol

Isotopic exchange;

hallde (l) Isotopic exchange;

organic compounds

Isotopic exchange;

cyanide complex group II

valence state group III

H-D, (T) exchange on

H-D, exchange on

H-D exchange on C In

(1)oxygen Isotope exchange

sulfur exchange between

(2) halogen on ivth group

halogen for halogen In

(25)

hydrogen Isotope exchange

between Vth group element and H-0 bond (3) Isotopic exchange; hydrogen Isotope exchange

on N In VI nth group complex (l) Isotopic exchange; hydrogen Isotope exchange

on N with molecular hydrogen (l)

301.401

301.464

301.471

301.474

301.565

301.701

301.770

302.150

302. 170

302. 190

302. 240

302. 390

302.401

302.402

302.403

302.461

302.466

302.474

302.477

302.506

302.508

302.511

National Bureau of Standards - National Research Council December, 1959
Homogeneous Reaction Kinetics 2

SUBJECT INDEX ( continiied)

310 HYDROGEN SUBSTITUTION Title of Table Table

(number of pages) number

311 Hydrogen substitution (gas)

Hydrogen substitution; halogen replaced by H on aliphatic C (4) 311.417

Hydrogen substitution; H replaced by halogen

on aliphatic C (4) 311.471

Hydrogen substitution; hydrogen-cyanogen (2) 311.540

312 Hydrogen substitution (liquid)

Hydrogen substitution; H on aliphatic C with group II metal (2) 312.421

Hydrogen substitution; H of aromatic compound

with group II metal (s) 312.422

Hydrogen substitution; nitration of aliphatic

compounds (l) 312.451

Hydrogen substitution; nitration of aromatic

compounds (22) 312.452

Hydrogen substitution; aryl hydrogen substitution by azo (Dlazonlum coupling) (15) 312.455

Hydrogen substitution; sulfonatlon of

aromatic compounds (7) 312.462

Hydrogen substitution; aryl sulfone

formation (2) 312.467

Hydrogen substitution; H by halogen on aliphatic C (21) 312.471

Hydrogen substitution; H by halogen on aromatic C (50) 312.472

Hydrogen substitution; H by halogen on heterocyclic ring (3) 312.473

Hydrogen substitution; replacement of H by halogen on SI (4) 312.474

Hydrogen substitution; H by halogen on NHg or amine (3) 312.570

Hydrogen substitution; H by halogen on N m amide (3) 312.571

330 EXCHANGE OF SUBSTITUENTS

331 Exchange of substituents (gas)

Exchange of substituents; replacement of halogen by NH^ and :NH (l) 331.754

332 Exchange of substituents (Liquid)

Exchange of substituents; alkali metal

replaced by C (3) 332.141

National Bureau of Standards - National Research Counci December, 1959V
Homogeneous Reaction Kinetics 3

SUBJECT INDEX (continued)

330 EXCHANGE OF SUBSTITUENTS Title of Table Table

(number of pages) number

(continued)

332 Exchange of substituents (liquid)

Exchange of substituents; replacement of Boron by 0 on aromatic C (3) 332.363

Exchange of substituents; replacement of Boron by halogen on aromatic C (6) 332.373

Exchange of substituents; replacement of

C by N on aromatic C (3) 332.452

Exchange of substituents; replacement of

C by sulfate on SI (l) 332.464

Exchange of substituents; replacement of

C by halogen on aromatic C (2) 332.472

Exchange of substituents; replacement of

SI by halogen on aromatic C (l) 332.473

Exchange of substituents; replacement of N by

0 on aliphatic C (2) 332.501

Exchange of substituents; replacement of N= by

0= on aromatic C (6) 332.503

Exchange of substituents; replacement of

Ar(SOg), (ArSOg), (ArSO) by NR' R"R'" (2) 332.653

Exchange of substituents; replacement of

halogen by C (of enolate) (2) 332.741

Exchange of substituents; replacement of

halogen on SI by C (2) 332.744

Exchange of substituents; replacement of

halogen by NO^ and (or) ONO on aliphatic C (4) 332.750

Exchange of substituents; replacement of

halogen by NOg~ (3) 332.751

Exchange of substituents; replacement of

halogen by azlde (2) 332.753

Exchange of substituents; replacement of

halogen by NH^ and :NH (l) 332.754

Exchange of substituents; replacement of

halogen by S^Og^ (15) 332.761

Exchange of substituents: replacement of

halogen by Thlo alkyl (aryl) (8) 332.763

Exchange of substituents; replacement of

halogen by thlocyanate (2) 332.765

Exchange of substituents; replacement of

halogen by S of thiourea (2) 332.766

Exchange of substituents; halogen for halogen

on aliphatic carbon (34) 332.771

National Bureau of Standards - National Research Council December, 1959
Homogeneous Reaction Kinetics 4

SUBJECT INDEX (continued)

350 EXCHANGE ON Vth GROUP ELEMENT Title of Table Table

(number of pages) number

(continued)

352 Exchange on Vth group element (liquid)

Exchange on Vth group element; halogen replaced

by nitrogen on P (2) 352.750

Exchange on Vth group elemenu. halogen for halogen on P (1) 352.770

4oo ELIMINATION

400 PROTON ELIMINATION

1^02 Proton elimination (liquid) Proton elimination; from CH bond activated

by adjacent CO. (COO R), (CN), (NO^) (s) 402.450

420 BOND-UNSATURATIOfI ELIMINATION

U22 Bond-unsaturation elimination (liquid)

Bond-unsaturatlon elimination; of C H N and h"^ 5

"5 to form C: C (l) 422.450

Bond-unsaturatlon elimination; of HNOg and (or) HNOg from nitrate ester (9) 422.451

Bond-unsa1;urat Ion elimination; of NO^" and

hallde Ion to form C: C (1) 422.457

Bond-unsaturatlon elimination; thlo ether and

H"*" from alkyl sulfonlum Ion (5) 422.461

Bond-unsaturatlon elimination; aryl sulfonic

acid from alkyl arylsulfonate (10) 422.463

Bond-unsaturatlon elimination; ArSOg" and

hallde Ion to form C:C (1) 422.467

Bond-unsaturatlon elimination; hydrogen

hallde to form C:C (4l) 422.471

Bond-unsaturatlon elimination; halogen

molecule by hallde Ion (15) 422.477

430 RING-CLOSURE ELIMINATION

432 Ring-closure elimination (liquid)

Ring-closure elimination; CO^" from

dlcarboxylate (2) 432.404

Ring-closure elimination; of H^o or ROH (6) 432.441

Ring- closure elimination; of H^o with

formation of aromatic ring (2) 432.442

Ring-closure elimination; of NOg" (l) 432.455

Ring-closure elimination; of halogen from

halo thlo ether (l) 432.476

National Bureau of Standards - National Research Council December, 1959

VU
Homogeneous Reaction Kinetics 5

SUBJECT INDEX (continued)

450 ELIMINATION FROM Vth GROUP ELEMENT Title of Table Table

(number of pages) number

(continued)

^52 Elimination from Vth group elenent (liquid)

Elimination from Vth group element; carbonlum

Ion from quaternary ammonium salt (l) 452.474

460 ELIMINATION FROM FUNCTIONAL GROUP

tie 2 Elimination from functional group (liquid)

Elimination from functional group; N^G from

acl form of nltro alkane (l) 462.451

National Bureau of Standards - National Research Council

December, 1959

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