1

Test item GK10051-0370 fllüssig

CAS No. 

Inventory name

Batch identification

Date of production (test item)

Origin of test item

Sponsor

Date of receipt of order 17.02.2014 14:51:07

Date of receipt of test item 03.03.2014

Testing facility 

Study director

Storage conditions of test item Room temperature

Test period 1 day

Storage of records Archives, GKC

Storage of sample of test item Room temperature

TS-MF06Y4_
2

Number average Mn n.a. g/mol

Weight average Mw n.a. g/mol

Mw/Mn n.a. -

Molar mass < 500 g/mol n.a. Area %

Molar mass < 1000 g/mol n.a. Area %

SEC RI Overlay curve see page 4

Slice printout see page 5 and following

Type of analysis: Molar mass distribution by Size Exclusion,

Chromatography (SEC), formerly called GPC

Aim of the measurement Determination of the molar mass distribution. 

Result should include distribution curve of the 

molar mass distribution, Mw, Mn and Slice Printout.

Remarks:

Polymer is totally insoluble. At a tenfold (40 mg/mL) of the usual concentration still no signal could be 

detected. Note however that the injection volume of the sample needed to be strongly reduced. 

At standard injection volume, the column upper pressure limits was exceeded due to sample's viscosity. 

It is therefore that no molar mass distribution of the polymer could be determined. 

This polymer is stronlgy crosslinked and therefore no longer soluble enough to preform SEC

measurements at ordinary concentrations. A raw curve is depicted. 

In the used calibration range from 300 up to 1.6 Mio. equivalents no polymer peak could be detected.

Date of test 03.03.2014

Head of laboratory

Study director ( Date 03.03.2014
3

SEC-equipment : App_F

Solvent : 

Column temperatur : 85 °C

Flow. : 1 mL/min

Injection volume : 5 μL

Concentration : 40 mg/mL

Sample preparation

Column combination :

Column material

Nr. i.D. Length

mm cm

1494 8 5 Polyester copoGRAM Vorsäule

1501 8 30 Polyester copoGRAM 30A

1496 8 30 Polyester copoGRAM 1000A

1497 8 30 Polyester copoGRAM 1000A

Plate height at given flow: 20000

calibration curve: F_628_normal_PMMA_Gram_S1494_S1501_S1496_S1497.CAL

Detector:

Calibration: 

Integration limits:

 DRI Agilent 1100

DMAC + 0.5% LiBr

Colums Column type

The callibration was obtained with narrow molar mass standards 

(PMMA, molar mass range 800-1820000 g/mol, PSS). Extrapolation 

was used to estimate the molecular weight distribution outside the 

range of these calibration standards with respect to the exclusion 

and permeation limits.

The lowest possible integration limit was set at 32,37mL (M(300) ca. 

) 

No lower molar masses could be obtained due to possible polymer 

additives or impurities.
4

SEC curve

0

0.0002

0.0004

0.0006

0.0008

0.001

0.0012

0.0014

0.0016

0.0018

0.002

100 1,000 10,000 100,000 1,000,000

dM/dLogM

Relative Molar mass (g/mol)

GMC-Nr 14Y08133

System Int. limit 300 g/mol

Non applicable

14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44

0

0.05

0.1

0.15

0.2

0.25

0.3

0.35

Vol. (mL)

Int. (mV)

GMC-Nr 14Y08133

System Int. limit 300 g/mol

GK10051-0370 fllüssig DRI
5

Calibration curve:
6

Slice table:

M (g/mol) mL WlogM by Area Intergral distribution

300 32.37 1.687E-03 0.001

303 32.36 1.665E-03 0.003

306 32.34 1.643E-03 0.004

309 32.32 1.639E-03 0.006

312 32.31 1.631E-03 0.007

316 32.29 1.628E-03 0.009

319 32.28 1.617E-03 0.011

322 32.26 1.619E-03 0.012

326 32.25 1.621E-03 0.014

329 32.23 1.622E-03 0.016

332 32.22 1.629E-03 0.017

336 32.20 1.626E-03 0.019

339 32.19 1.637E-03 0.020

343 32.17 1.624E-03 0.022

346 32.16 1.621E-03 0.024

350 32.14 1.626E-03 0.025

353 32.13 1.635E-03 0.027

357 32.11 1.617E-03 0.029

360 32.09 1.619E-03 0.030

364 32.08 1.630E-03 0.032

368 32.06 1.629E-03 0.033

372 32.05 1.624E-03 0.035

375 32.03 1.624E-03 0.037

379 32.02 1.632E-03 0.038

383 32.00 1.636E-03 0.040

387 31.99 1.623E-03 0.042

391 31.97 1.634E-03 0.043

395 31.96 1.635E-03 0.045

399 31.94 1.649E-03 0.046

403 31.93 1.645E-03 0.048

407 31.91 1.642E-03 0.050

412 31.90 1.651E-03 0.051

416 31.88 1.645E-03 0.053

420 31.86 1.633E-03 0.055
7

465 31.71 1.570E-03 0.071

470 31.70 1.570E-03 0.072

475 31.68 1.553E-03 0.074

480 31.67 1.550E-03 0.075

485 31.65 1.557E-03 0.077

490 31.64 1.560E-03 0.078

495 31.62 1.565E-03 0.080

500 31.60 1.565E-03 0.082

505 31.59 1.565E-03 0.083

510 31.57 1.571E-03 0.085

515 31.56 1.571E-03 0.086

520 31.54 1.553E-03 0.088

526 31.53 1.544E-03 0.089

531 31.51 1.543E-03 0.091

537 31.50 1.542E-03 0.093

542 31.48 1.528E-03 0.094

548 31.47 1.516E-03 0.096

553 31.45 1.519E-03 0.097

559 31.44 1.513E-03 0.099

565 31.42 1.504E-03 0.100

570 31.41 1.496E-03 0.102

576 31.39 1.494E-03 0.103

582 31.37 1.473E-03 0.105

588 31.36 1.473E-03 0.106

594 31.34 1.473E-03 0.108

600 31.33 1.473E-03 0.109

606 31.31 1.463E-03 0.110

613 31.30 1.459E-03 0.112

619 31.28 1.466E-03 0.113

625 31.27 1.476E-03 0.115

632 31.25 1.479E-03 0.116

638 31.24 1.484E-03 0.118

645 31.22 1.484E-03 0.119

651 31.21 1.463E-03 0.121

658 31.19 1.470E-03 0.122

665 31.18 1.467E-03 0.124

672 31.16 1.459E-03 0.125

678 31.15 1.455E-03 0.127

685 31.13 1.451E-03 0.128

692 31.11 1.424E-03 0.129

700 31.10 1.411E-03 0.131

707 31.08 1.416E-03 0.132

714 31.07 1.425E-03 0.134
8

791 30.92 1.397E-03 0.148

799 30.90 1.391E-03 0.149

807 30.88 1.387E-03 0.151

815 30.87 1.383E-03 0.152

824 30.85 1.384E-03 0.153

832 30.84 1.398E-03 0.155

841 30.82 1.403E-03 0.156

849 30.81 1.416E-03 0.158

858 30.79 1.409E-03 0.159

867 30.78 1.411E-03 0.160

876 30.76 1.409E-03 0.162

885 30.74 1.413E-03 0.163

894 30.73 1.411E-03 0.165

903 30.71 1.409E-03 0.166

912 30.70 1.412E-03 0.167

921 30.68 1.422E-03 0.169

931 30.67 1.419E-03 0.170

940 30.65 1.410E-03 0.172

950 30.64 1.411E-03 0.173

960 30.62 1.415E-03 0.175

970 30.60 1.423E-03 0.176

980 30.59 1.431E-03 0.177

990 30.57 1.433E-03 0.179

1000 30.56 1.428E-03 0.180

1010 30.54 1.427E-03 0.182

1020 30.52 1.422E-03 0.183

1031 30.51 1.401E-03 0.185

1041 30.49 1.412E-03 0.186

1052 30.48 1.415E-03 0.187

1063 30.46 1.435E-03 0.189

1074 30.45 1.449E-03 0.190

1085 30.43 1.447E-03 0.192

1096 30.41 1.438E-03 0.193

1107 30.40 1.454E-03 0.195

1118 30.38 1.452E-03 0.196

1130 30.37 1.444E-03 0.197

1141 30.35 1.442E-03 0.199

1153 30.33 1.436E-03 0.200

1165 30.32 1.434E-03 0.202

1177 30.30 1.445E-03 0.203

1189 30.28 1.449E-03 0.205

1201 30.27 1.436E-03 0.206

1214 30.25 1.437E-03 0.208
9

1344 30.09 1.490E-03 0.222

1358 30.07 1.498E-03 0.224

1372 30.06 1.498E-03 0.225

1386 30.04 1.479E-03 0.227

1400 30.02 1.466E-03 0.228

1414 30.01 1.470E-03 0.230

1429 29.99 1.468E-03 0.231

1443 29.97 1.478E-03 0.233

1458 29.96 1.485E-03 0.234

1473 29.94 1.479E-03 0.235

1488 29.92 1.484E-03 0.237

1503 29.91 1.506E-03 0.238

1519 29.89 1.504E-03 0.240

1534 29.87 1.511E-03 0.241

1550 29.86 1.524E-03 0.243

1566 29.84 1.521E-03 0.245

1582 29.82 1.507E-03 0.246

1598 29.81 1.502E-03 0.248

1615 29.79 1.502E-03 0.249

1631 29.77 1.503E-03 0.251

1648 29.76 1.516E-03 0.252

1665 29.74 1.518E-03 0.254

1682 29.72 1.545E-03 0.255

1699 29.71 1.539E-03 0.257

1717 29.69 1.545E-03 0.258

1734 29.67 1.549E-03 0.260

1752 29.66 1.540E-03 0.261

1770 29.64 1.538E-03 0.263

1788 29.62 1.544E-03 0.264

1806 29.61 1.534E-03 0.266

1825 29.59 1.527E-03 0.267

1844 29.57 1.549E-03 0.269

1863 29.55 1.555E-03 0.271

1882 29.54 1.549E-03 0.272

1901 29.52 1.527E-03 0.274

1920 29.50 1.512E-03 0.275

1940 29.49 1.513E-03 0.277

1960 29.47 1.519E-03 0.278

1980 29.45 1.528E-03 0.280

2000 29.44 1.535E-03 0.281

2021 29.42 1.541E-03 0.283

2042 29.40 1.543E-03 0.284

2063 29.38 1.544E-03 0.286
10

2284 29.21 1.558E-03 0.301

2307 29.19 1.567E-03 0.303

2331 29.18 1.567E-03 0.305

2355 29.16 1.568E-03 0.306

2379 29.14 1.569E-03 0.308

2404 29.12 1.569E-03 0.309

2428 29.11 1.570E-03 0.311

2453 29.09 1.566E-03 0.312

2478 29.07 1.554E-03 0.314

2504 29.05 1.545E-03 0.315

2529 29.04 1.538E-03 0.317

2555 29.02 1.561E-03 0.319

2581 29.00 1.565E-03 0.320

2608 28.98 1.567E-03 0.322

2635 28.97 1.578E-03 0.323

2662 28.95 1.584E-03 0.325

2689 28.93 1.601E-03 0.326

2717 28.91 1.611E-03 0.328

2744 28.89 1.596E-03 0.330

2773 28.88 1.581E-03 0.331

2801 28.86 1.567E-03 0.333

2830 28.84 1.577E-03 0.334

2859 28.82 1.585E-03 0.336

2888 28.81 1.582E-03 0.338

2918 28.79 1.565E-03 0.339

2948 28.77 1.557E-03 0.341

2978 28.75 1.556E-03 0.342

3008 28.73 1.560E-03 0.344

3039 28.72 1.562E-03 0.345

3070 28.70 1.572E-03 0.347

3102 28.68 1.568E-03 0.348

3134 28.66 1.585E-03 0.350

3166 28.64 1.594E-03 0.352

3198 28.63 1.586E-03 0.353

3231 28.61 1.610E-03 0.355

3264 28.59 1.614E-03 0.356

3298 28.57 1.609E-03 0.358

3331 28.55 1.624E-03 0.360

3366 28.54 1.623E-03 0.361

3400 28.52 1.615E-03 0.363

3435 28.50 1.605E-03 0.365

3470 28.48 1.600E-03 0.366

3506 28.46 1.604E-03 0.368
11

3882 28.28 1.630E-03 0.384

3922 28.26 1.613E-03 0.386

3962 28.24 1.615E-03 0.387

4003 28.22 1.633E-03 0.389

4044 28.21 1.650E-03 0.390

4085 28.19 1.653E-03 0.392

4127 28.17 1.642E-03 0.394

4169 28.15 1.647E-03 0.395

4212 28.13 1.671E-03 0.397

4255 28.11 1.673E-03 0.399

4299 28.10 1.684E-03 0.400

4343 28.08 1.684E-03 0.402

4388 28.06 1.670E-03 0.404

4433 28.04 1.672E-03 0.405

4478 28.02 1.667E-03 0.407

4524 28.00 1.670E-03 0.409

4570 27.98 1.650E-03 0.410

4617 27.96 1.644E-03 0.412

4665 27.95 1.635E-03 0.414

4712 27.93 1.623E-03 0.415

4761 27.91 1.647E-03 0.417

4810 27.89 1.657E-03 0.419

4859 27.87 1.665E-03 0.420

4909 27.85 1.675E-03 0.422

4959 27.83 1.677E-03 0.424

5010 27.82 1.685E-03 0.425

5061 27.80 1.694E-03 0.427

5113 27.78 1.677E-03 0.429

5166 27.76 1.662E-03 0.430

5218 27.74 1.664E-03 0.432

5272 27.72 1.667E-03 0.434

5326 27.70 1.653E-03 0.435

5381 27.68 1.649E-03 0.437

5436 27.66 1.631E-03 0.439

5492 27.65 1.645E-03 0.440

5548 27.63 1.652E-03 0.442

5605 27.61 1.641E-03 0.444

5662 27.59 1.641E-03 0.445

5720 27.57 1.652E-03 0.447

5779 27.55 1.669E-03 0.449

5838 27.53 1.658E-03 0.450

5898 27.51 1.653E-03 0.452

5958 27.49 1.631E-03 0.453
12

6598 27.30 1.607E-03 0.470

6666 27.28 1.623E-03 0.471

6734 27.26 1.644E-03 0.473

6803 27.24 1.650E-03 0.475

6873 27.23 1.639E-03 0.476

6944 27.21 1.639E-03 0.478

7015 27.19 1.648E-03 0.480

7087 27.17 1.631E-03 0.481

7159 27.15 1.632E-03 0.483

7233 27.13 1.634E-03 0.484

7307 27.11 1.639E-03 0.486

7382 27.09 1.658E-03 0.488

7458 27.07 1.649E-03 0.489

7534 27.05 1.628E-03 0.491

7611 27.03 1.609E-03 0.493

7689 27.01 1.611E-03 0.494

7768 26.99 1.588E-03 0.496

7848 26.97 1.582E-03 0.497

7928 26.95 1.597E-03 0.499

8010 26.94 1.611E-03 0.501

8092 26.92 1.613E-03 0.502

8175 26.90 1.622E-03 0.504

8258 26.88 1.638E-03 0.505

8343 26.86 1.620E-03 0.507

8429 26.84 1.617E-03 0.509

8515 26.82 1.622E-03 0.510

8602 26.80 1.615E-03 0.512

8691 26.78 1.600E-03 0.514

8780 26.76 1.600E-03 0.515

8870 26.74 1.619E-03 0.517

8961 26.72 1.625E-03 0.518

9052 26.70 1.633E-03 0.520

9145 26.68 1.633E-03 0.522

9239 26.66 1.631E-03 0.523

9334 26.64 1.631E-03 0.525

9429 26.62 1.617E-03 0.527

9526 26.60 1.610E-03 0.528

9624 26.58 1.608E-03 0.530

9723 26.56 1.615E-03 0.531

9822 26.54 1.607E-03 0.533

9923 26.53 1.615E-03 0.535

10025 26.51 1.638E-03 0.536

10127 26.49 1.644E-03 0.538
13

11215 26.29 1.646E-03 0.554

11330 26.27 1.643E-03 0.556

11446 26.25 1.653E-03 0.558

11564 26.23 1.641E-03 0.559

11682 26.21 1.647E-03 0.561

11802 26.19 1.636E-03 0.563

11923 26.17 1.621E-03 0.564

12045 26.15 1.629E-03 0.566

12169 26.13 1.625E-03 0.567

12293 26.11 1.635E-03 0.569

12419 26.09 1.620E-03 0.571

12547 26.07 1.599E-03 0.572

12675 26.05 1.626E-03 0.574

12805 26.03 1.621E-03 0.576

12937 26.01 1.617E-03 0.577

13069 25.99 1.625E-03 0.579

13203 25.97 1.610E-03 0.580

13339 25.95 1.626E-03 0.582

13475 25.93 1.639E-03 0.584

13614 25.91 1.626E-03 0.585

13753 25.89 1.640E-03 0.587

13894 25.87 1.650E-03 0.589

14037 25.85 1.647E-03 0.590

14181 25.83 1.642E-03 0.592

14326 25.81 1.625E-03 0.594

14473 25.79 1.636E-03 0.595

14621 25.77 1.639E-03 0.597

14771 25.75 1.634E-03 0.598

14923 25.73 1.626E-03 0.600

15076 25.71 1.644E-03 0.602

15230 25.69 1.620E-03 0.603

15386 25.67 1.644E-03 0.605

15544 25.65 1.649E-03 0.607

15703 25.63 1.612E-03 0.608

15864 25.61 1.618E-03 0.610

16027 25.59 1.620E-03 0.611

16191 25.57 1.615E-03 0.613

16357 25.55 1.611E-03 0.615

16525 25.53 1.618E-03 0.616

16694 25.51 1.625E-03 0.618

16866 25.49 1.611E-03 0.620

17039 25.47 1.620E-03 0.621

17213 25.45 1.615E-03 0.623
14

19062 25.26 1.599E-03 0.639

19257 25.24 1.612E-03 0.640

19455 25.22 1.667E-03 0.642

19654 25.20 1.688E-03 0.644

19856 25.18 1.674E-03 0.645

20059 25.16 1.679E-03 0.647

20265 25.14 1.667E-03 0.649

20473 25.12 1.655E-03 0.651

20683 25.10 1.638E-03 0.652

20895 25.08 1.666E-03 0.654

21109 25.06 1.661E-03 0.655

21325 25.04 1.659E-03 0.657

21544 25.02 1.679E-03 0.659

21765 25.00 1.712E-03 0.661

21988 24.98 1.691E-03 0.662

22213 24.96 1.689E-03 0.664

22441 24.94 1.694E-03 0.666

22671 24.92 1.701E-03 0.667

22904 24.90 1.683E-03 0.669

23139 24.88 1.672E-03 0.671

23376 24.86 1.674E-03 0.672

23615 24.84 1.646E-03 0.674

23858 24.82 1.657E-03 0.676

24102 24.80 1.677E-03 0.677

24349 24.78 1.669E-03 0.679

24599 24.76 1.689E-03 0.681

24851 24.74 1.653E-03 0.682

25106 24.72 1.651E-03 0.684

25363 24.70 1.640E-03 0.686

25623 24.68 1.635E-03 0.687

25886 24.66 1.641E-03 0.689

26151 24.64 1.651E-03 0.691

26420 24.62 1.627E-03 0.692

26690 24.60 1.649E-03 0.694

26964 24.58 1.664E-03 0.695

27241 24.56 1.661E-03 0.697

27520 24.54 1.651E-03 0.699

27802 24.52 1.649E-03 0.700

28087 24.50 1.656E-03 0.702

28375 24.48 1.655E-03 0.704

28666 24.46 1.670E-03 0.705

28960 24.44 1.677E-03 0.707

29257 24.42 1.682E-03 0.709
15

32399 24.22 1.746E-03 0.726

32731 24.20 1.730E-03 0.727

33067 24.18 1.734E-03 0.729

33406 24.16 1.701E-03 0.731

33748 24.14 1.703E-03 0.733

34094 24.12 1.698E-03 0.734

34444 24.10 1.686E-03 0.736

34797 24.08 1.692E-03 0.738

35154 24.06 1.688E-03 0.739

35514 24.05 1.712E-03 0.741

35878 24.03 1.703E-03 0.743

36246 24.01 1.686E-03 0.744

36618 23.99 1.660E-03 0.746

36993 23.97 1.639E-03 0.748

37372 23.95 1.650E-03 0.749

37755 23.93 1.654E-03 0.751

38143 23.91 1.646E-03 0.753

38534 23.89 1.659E-03 0.754

38929 23.87 1.669E-03 0.756

39328 23.85 1.657E-03 0.758

39731 23.83 1.659E-03 0.759

40138 23.81 1.658E-03 0.761

40550 23.79 1.633E-03 0.763

40966 23.77 1.636E-03 0.764

41386 23.75 1.634E-03 0.766

41810 23.73 1.619E-03 0.768

42239 23.71 1.613E-03 0.769

42672 23.69 1.612E-03 0.771

43109 23.67 1.595E-03 0.772

43551 23.65 1.601E-03 0.774

43998 23.63 1.591E-03 0.776

44449 23.61 1.612E-03 0.777

44905 23.60 1.608E-03 0.779

45365 23.58 1.594E-03 0.780

45830 23.56 1.608E-03 0.782

46300 23.54 1.639E-03 0.784

46775 23.52 1.599E-03 0.785

47254 23.50 1.609E-03 0.787

47739 23.48 1.620E-03 0.788

48228 23.46 1.617E-03 0.790

48723 23.44 1.601E-03 0.792

49222 23.42 1.586E-03 0.793

49727 23.40 1.585E-03 0.795
16

55067 23.21 1.610E-03 0.811

55632 23.19 1.583E-03 0.812

56202 23.17 1.587E-03 0.814

56778 23.15 1.594E-03 0.816

57360 23.13 1.565E-03 0.817

57949 23.11 1.585E-03 0.819

58543 23.09 1.571E-03 0.820

59143 23.07 1.587E-03 0.822

59749 23.06 1.586E-03 0.824

60362 23.04 1.612E-03 0.825

60981 23.02 1.571E-03 0.827

61606 23.00 1.596E-03 0.828

62238 22.98 1.580E-03 0.830

62876 22.96 1.557E-03 0.831

63520 22.94 1.572E-03 0.833

64172 22.92 1.547E-03 0.835

64830 22.90 1.552E-03 0.836

65494 22.88 1.520E-03 0.838

66166 22.87 1.530E-03 0.839

66844 22.85 1.552E-03 0.841

67530 22.83 1.558E-03 0.842

68222 22.81 1.541E-03 0.844

68921 22.79 1.539E-03 0.845

69628 22.77 1.567E-03 0.847

70342 22.75 1.554E-03 0.849

71063 22.73 1.543E-03 0.850

71792 22.71 1.544E-03 0.852

72528 22.70 1.497E-03 0.853

73271 22.68 1.481E-03 0.855

74023 22.66 1.461E-03 0.856

74782 22.64 1.455E-03 0.857

75548 22.62 1.452E-03 0.859

76323 22.60 1.430E-03 0.860

77105 22.58 1.465E-03 0.862

77896 22.56 1.443E-03 0.863

78695 22.55 1.449E-03 0.865

79501 22.53 1.449E-03 0.866

80317 22.51 1.433E-03 0.868

81140 22.49 1.434E-03 0.869

81972 22.47 1.412E-03 0.870

82812 22.45 1.409E-03 0.872

83661 22.43 1.386E-03 0.873

84519 22.42 1.374E-03 0.875
17

93596 22.23 1.269E-03 0.888

94555 22.21 1.248E-03 0.889

95525 22.19 1.231E-03 0.890

96504 22.18 1.254E-03 0.892

97494 22.16 1.247E-03 0.893

98493 22.14 1.243E-03 0.894

99503 22.12 1.231E-03 0.895

100523 22.10 1.229E-03 0.897

101554 22.08 1.245E-03 0.898

102595 22.07 1.227E-03 0.899

103647 22.05 1.218E-03 0.900

104710 22.03 1.228E-03 0.901

105783 22.01 1.215E-03 0.903

106868 21.99 1.204E-03 0.904

107964 21.97 1.201E-03 0.905

109071 21.96 1.199E-03 0.906

110189 21.94 1.159E-03 0.907

111319 21.92 1.173E-03 0.909

112460 21.90 1.153E-03 0.910

113613 21.88 1.168E-03 0.911

114778 21.87 1.157E-03 0.912

115955 21.85 1.158E-03 0.913

117144 21.83 1.157E-03 0.914

118345 21.81 1.117E-03 0.916

119558 21.79 1.104E-03 0.917

120784 21.78 1.083E-03 0.918

122022 21.76 1.097E-03 0.919

123273 21.74 1.065E-03 0.920

124537 21.72 1.075E-03 0.921

125814 21.70 1.094E-03 0.922

127104 21.69 1.074E-03 0.923

128407 21.67 1.061E-03 0.924

129724 21.65 1.059E-03 0.925

131054 21.63 1.057E-03 0.926

132397 21.62 1.052E-03 0.927

133755 21.60 1.042E-03 0.928

135126 21.58 1.044E-03 0.929

136512 21.56 1.047E-03 0.930

137911 21.54 1.042E-03 0.932

139325 21.53 1.015E-03 0.933

140754 21.51 9.931E-04 0.934

142197 21.49 9.969E-04 0.935

143655 21.47 9.631E-04 0.935
18

159082 21.30 8.911E-04 0.945

160713 21.28 8.761E-04 0.946

162361 21.26 8.694E-04 0.946

164025 21.25 8.574E-04 0.947

165707 21.23 8.437E-04 0.948

167406 21.21 8.437E-04 0.949

169122 21.19 8.358E-04 0.950

170856 21.18 8.109E-04 0.951

172608 21.16 8.029E-04 0.951

174378 21.14 8.010E-04 0.952

176166 21.13 7.796E-04 0.953

177972 21.11 7.438E-04 0.954

179797 21.09 7.677E-04 0.955

181640 21.07 7.732E-04 0.955

183502 21.06 7.642E-04 0.956

185384 21.04 7.273E-04 0.957

187285 21.02 7.195E-04 0.958

189205 21.01 7.097E-04 0.958

191145 20.99 7.389E-04 0.959

193104 20.97 7.183E-04 0.960

195084 20.95 7.290E-04 0.960

197084 20.94 7.290E-04 0.961

199105 20.92 7.042E-04 0.962

201147 20.90 7.139E-04 0.963

203209 20.89 7.132E-04 0.963

205292 20.87 6.854E-04 0.964

207397 20.85 6.737E-04 0.965

209524 20.84 6.696E-04 0.965

211672 20.82 6.604E-04 0.966

213842 20.80 6.576E-04 0.967

216034 20.79 6.560E-04 0.967

218249 20.77 6.531E-04 0.968

220487 20.75 6.420E-04 0.969

222748 20.73 6.328E-04 0.969

225032 20.72 6.322E-04 0.970

227339 20.70 6.335E-04 0.970

229670 20.68 6.219E-04 0.971

232024 20.67 6.225E-04 0.972

234403 20.65 6.150E-04 0.972

236807 20.63 6.107E-04 0.973

239235 20.62 5.980E-04 0.974

241687 20.60 5.795E-04 0.974

244165 20.58 5.731E-04 0.975
19

270386 20.42 5.098E-04 0.980

273159 20.40 5.010E-04 0.981

275959 20.39 5.153E-04 0.981

278789 20.37 4.893E-04 0.982

281647 20.35 4.843E-04 0.982

284535 20.34 5.013E-04 0.983

287452 20.32 4.525E-04 0.983

290399 20.31 4.336E-04 0.983

293377 20.29 4.306E-04 0.984

296385 20.27 4.292E-04 0.984

299423 20.26 4.279E-04 0.985

302493 20.24 4.409E-04 0.985

305595 20.22 4.151E-04 0.986

308728 20.21 4.057E-04 0.986

311893 20.19 4.042E-04 0.986

315091 20.18 3.962E-04 0.987

318322 20.16 3.926E-04 0.987

321585 20.14 3.846E-04 0.988

324882 20.13 3.809E-04 0.988

328213 20.11 3.669E-04 0.988

331579 20.10 3.771E-04 0.989

334978 20.08 3.636E-04 0.989

338413 20.06 3.556E-04 0.989

341882 20.05 3.193E-04 0.990

345388 20.03 3.131E-04 0.990

348929 20.02 3.224E-04 0.990

352506 20.00 3.124E-04 0.991

356121 19.98 2.984E-04 0.991

359772 19.97 2.952E-04 0.991

363460 19.95 2.955E-04 0.992

367187 19.94 3.024E-04 0.992

370952 19.92 3.052E-04 0.992

374755 19.90 2.879E-04 0.993

378597 19.89 2.873E-04 0.993

382479 19.87 2.882E-04 0.993

386400 19.86 2.868E-04 0.993

390362 19.84 2.672E-04 0.994

394364 19.83 2.258E-04 0.994

398408 19.81 2.499E-04 0.994

402493 19.79 2.402E-04 0.994

406619 19.78 2.351E-04 0.995

410788 19.76 2.310E-04 0.995

415000 19.75 2.174E-04 0.995
20

459567 19.59 1.642E-04 0.997

464279 19.58 1.699E-04 0.997

469039 19.56 1.613E-04 0.997

473848 19.55 1.389E-04 0.997

478707 19.53 1.259E-04 0.998

483615 19.52 1.233E-04 0.998

488573 19.50 1.202E-04 0.998

493582 19.49 1.138E-04 0.998

498643 19.47 1.128E-04 0.998

503755 19.46 1.169E-04 0.998

508920 19.44 1.120E-04 0.998

514138 19.42 1.088E-04 0.998

519410 19.41 1.138E-04 0.998

524735 19.39 1.106E-04 0.999

530115 19.38 9.821E-05 0.999

535550 19.36 8.435E-05 0.999

541041 19.35 8.335E-05 0.999

546588 19.33 8.083E-05 0.999

552192 19.32 7.101E-05 0.999

557854 19.30 6.868E-05 0.999

563574 19.29 7.217E-05 0.999

569352 19.27 6.255E-05 0.999

575189 19.26 6.832E-05 0.999

581087 19.24 3.569E-05 0.999

587044 19.23 1.403E-05 0.999

593063 19.21 2.676E-05 0.999

599144 19.20 4.166E-05 0.999

605287 19.18 3.289E-05 0.999

611493 19.17 1.019E-05 0.999

617762 19.15 6.356E-06 0.999

624096 19.14 8.606E-06 0.999

630495 19.12 1.890E-05 0.999

636959 19.11 2.851E-05 1.000

643490 19.10 3.058E-05 1.000

650087 19.08 1.692E-05 1.000

656753 19.07 1.407E-05 1.000

663486 19.05 1.288E-05 1.000

670289 19.04 5.690E-06 1.000

677161 19.02 1.664E-06 1.000

684104 19.01 9.913E-07 1.000

691118 18.99 2.621E-07 1.000

698204 18.98 1.538E-05 1.000

705363 18.96 9.342E-06 1.000
21

781112 18.82 5.908E-06 1.000

789120 18.80 8.830E-06 1.000

797211 18.79 1.254E-05 1.000

805385 18.77 1.393E-05 1.000

813642 18.76 8.194E-06 1.000

821984 18.75 4.543E-06 1.000

830412 18.73 3.554E-06 1.000

838926 18.72 2.158E-06 1.000

847528 18.70 5.204E-07 1.000

856217 18.69 0.000E+00 1.000

864996 18.67 0.000E+00 1.000

873864 18.66 0.000E+00 1.000

882824 18.65 0.000E+00 1.000

891876 18.63 0.000E+00 1.000

901020 18.62 0.000E+00 1.000

910258 18.60 0.000E+00 1.000

919590 18.59 0.000E+00 1.000

929019 18.58 0.000E+00 1.000

938544 18.56 0.000E+00 1.000

948167 18.55 9.640E-07 1.000

957888 18.53 1.360E-06 1.000

967709 18.52 1.136E-06 1.000

977631 18.50 4.032E-07 1.000

987654 18.49 1.854E-07 1.000

997781 18.48 3.670E-06 1.000

1008011 18.46 1.009E-05 1.000

1018346 18.45 8.656E-06 1.000

1028787 18.43 8.355E-06 1.000

1039335 18.42 8.534E-06 1.000

1049991 18.41 5.602E-06 1.000

1060756 18.39 2.380E-06 1.000

1071632 18.38 6.137E-06 1.000

1082619 18.37 4.787E-06 1.000

1093719 18.35 1.393E-06 1.000

1104933 18.34 0.000E+00 1.000

1116262 18.32 0.000E+00 1.000

1127706 18.31 0.000E+00 1.000

1139269 18.30 2.831E-06 1.000

1150949 18.28 2.536E-06 1.000

1162750 18.27 9.028E-07 1.000

1174671 18.26 0.000E+00 1.000

1186715 18.24 0.000E+00 1.000

1198882 18.23 0.000E+00 1.000
22

1327631 18.09 0.000E+00 1.000

1341243 18.08 0.000E+00 1.000

1354994 18.06 0.000E+00 1.000

1368887 18.05 0.000E+00 1.000

1382922 18.04 0.000E+00 1.000

1397101 18.02 0.000E+00 1.000

1411425 18.01 0.000E+00 1.000

1425896 18.00 0.000E+00 1.000

1440516 17.98 0.000E+00 1.000

1455285 17.97 2.478E-06 1.000

1470206 17.96 7.230E-06 1.000

1485280 17.94 7.390E-06 1.000

1500508 17.93 2.487E-06 1.000

1515893 17.92 3.113E-07 1.000

1531435 17.90 0.000E+00 1.000

1547136 17.89 0.000E+00 1.000

1562999 17.88 0.000E+00 1.000

1579024 17.86 0.000E+00 1.000

1595213 17.85 0.000E+00 1.000

1611569 17.84 0.000E+00 1.000

1628092 17.82 0.000E+00 1.000

1644785 17.81 0.000E+00 1.000

1661648 17.80 0.000E+00 1.000

1678685 17.78 0.000E+00 1.000

1695896 17.77 0.000E+00 1.000

1713284 17.76 0.000E+00 1.000

1730850 17.74 0.000E+00 1.000

1748596 17.73 0.000E+00 1.000

1766524 17.72 0.000E+00 1.000

1784636 17.70 0.000E+00 1.000

1802934 17.69 0.000E+00 1.000

1821419 17.68 2.098E-08 1.000

1840094 17.66 6.687E-06 1.000

1858960 17.65 6.586E-06 1.000

1878020 17.64 3.167E-06 1.000

1897275 17.62 0.000E+00 1.000

1916727 17.61 0.000E+00 1.000

1936379 17.60 0.000E+00 1.000

1956232 17.58 0.000E+00 1.000

1976289 17.57 0.000E+00 1.000

1996552 17.56 0.000E+00 1.000

2017022 17.54 0.000E+00 1.000

2037702 17.53 0.000E+00 1.000
23

2256532 17.40 0.000E+00 1.000

2279668 17.38 0.000E+00 1.000

2303041 17.37 0.000E+00 1.000

2326654 17.36 0.000E+00 1.000

2350509 17.34 0.000E+00 1.000

2374608 17.33 0.000E+00 1.000

2398955 17.32 0.000E+00 1.000

2423551 17.30 0.000E+00 1.000

2448399 17.29 0.000E+00 1.000

2473502 17.28 0.000E+00 1.000

2498862 17.26 0.000E+00 1.000

2524483 17.25 0.000E+00 1.000

2550366 17.24 0.000E+00 1.000

2576514 17.22 0.000E+00 1.000

2602931 17.21 0.000E+00 1.000

2629619 17.20 0.000E+00 1.000

2656580 17.18 0.000E+00 1.000

2683817 17.17 0.000E+00 1.000

2711334 17.16 0.000E+00 1.000

2739133 17.14 0.000E+00 1.000

2767217 17.13 0.000E+00 1.000

2795588 17.12 0.000E+00 1.000

2824251 17.10 0.000E+00 1.000

2853208 17.09 0.000E+00 1.000

2882461 17.08 0.000E+00 1.000

2912015 17.06 0.000E+00 1.000

2941871 17.05 0.000E+00 1.000

2972034 17.04 0.000E+00 1.000

3002505 17.02 0.000E+00 1.000

3033290 17.01 0.000E+00 1.000

3064389 17.00 0.000E+00 1.000

3095808 16.98 0.000E+00 1.000

3127549 16.97 0.000E+00 1.000

3159615 16.96 0.000E+00 1.000

3192010 16.94 0.000E+00 1.000

3224737 16.93 0.000E+00 1.000

3257800 16.92 0.000E+00 1.000

3291202 16.90 0.000E+00 1.000

3324946 16.89 0.000E+00 1.000

3359036 16.88 0.000E+00 1.000

3393476 16.86 0.000E+00 1.000

3428269 16.85 0.000E+00 1.000

3463418 16.84 0.000E+00 1.000
24

3835356 16.70 0.000E+00 1.000

3874680 16.69 0.000E+00 1.000

3914406 16.68 0.000E+00 1.000

3954540 16.66 0.000E+00 1.000

3995085 16.65 0.000E+00 1.000

4036046 16.64 0.000E+00 1.000

4077427 16.62 0.000E+00 1.000

4119232 16.61 0.000E+00 1.000

4161466 16.60 0.000E+00 1.000

4204133 16.58 0.000E+00 1.000

4247237 16.57 0.000E+00 1.000

4290784 16.56 0.000E+00 1.000

4334776 16.54 0.000E+00 1.000

4379220 16.53 0.000E+00 1.000

4424119 16.52 0.000E+00 1.000

4469479 16.50 0.000E+00 1.000

4515304 16.49 0.000E+00 1.000

4561599 16.48 0.000E+00 1.000

4608368 16.46 0.000E+00 1.000

4655617 16.45 0.000E+00 1.000

4703350 16.44 0.000E+00 1.000

4751573 16.42 0.000E+00 1.000

4800290 16.41 0.000E+00 1.000

4849507 16.40 0.000E+00 1.000

4899228 16.38 0.000E+00 1.000

4949459 16.37 0.000E+00 1.000

5000205 16.36 0.000E+00 1.000

5051471 16.34 0.000E+00 1.000

5103263 16.33 0.000E+00 1.000

5155586 16.32 0.000E+00 1.000

5208446 16.30 0.000E+00 1.000

5261847 16.29 0.000E+00 1.000

5315796 16.28 0.000E+00 1.000

5370298 16.26 0.000E+00 1.000

5425359 16.25 0.000E+00 1.000

5480984 16.24 0.000E+00 1.000

5537180 16.22 0.000E+00 1.000

5593951 16.21 0.000E+00 1.000

5651305 16.20 0.000E+00 1.000

5709247 16.18 0.000E+00 1.000

5767783 16.17 0.000E+00 1.000

5826919 16.16 0.000E+00 1.000

5886662 16.14 0.000E+00 1.000
25

6518834 16.01 0.000E+00 1.000

6585670 16.00 0.000E+00 1.000

6653192 15.98 0.000E+00 1.000

6721406 15.97 0.000E+00 1.000

6790320 15.96 0.000E+00 1.000

6859940 15.94 0.000E+00 1.000

6930274 15.93 0.000E+00 1.000

7001329 15.92 0.000E+00 1.000

7073112 15.90 0.000E+00 1.000

7145632 15.89 0.000E+00 1.000

7218895 15.88 0.000E+00 1.000

7292909 15.86 0.000E+00 1.000

7367682 15.85 0.000E+00 1.000

7443222 15.84 0.000E+00 1.000

7519536 15.82 0.000E+00 1.000

7596632 15.81 0.000E+00 1.000

7674519 15.80 0.000E+00 1.000

7753205 15.78 0.000E+00 1.000

7832697 15.77 0.000E+00 1.000

7913005 15.76 0.000E+00 1.000

7994136 15.74 0.000E+00 1.000

8076098 15.73 0.000E+00 1.000

8158901 15.72 0.000E+00 1.000

8242553 15.70 2.167E-06 1.000

8327063 15.69 5.880E-06 1.000

8412439 15.68 8.994E-06 1.000

8498690 15.66 1.214E-05 1.000
29
26